ML14080A196

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Letter from Erin Trent Radiochemistry Analysis Work Order: 334614
ML14080A196
Person / Time
Site: 05000134
Issue date: 10/28/2013
From: Trent E
GEL Labs
To: James Adler
NRC/FSME, TLG Services
References
334614
Download: ML14080A196 (72)
v • d • e


Text

October 28, 2013 Mr. Jay Adler TLG Services, Inc.

148 New Milford Rd. East Bridgewater, Connecticut 06752 Re: Radiochemistry Analysis Work Order: 334614

Dear Mr. Adler:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 03, 2013. This original data report has been prepared and reviewed in accordance with GELs standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.

Sincerely, PM_SIGN_HERE Erin Trent Project Manager Purchase Order: Signed Quote GELP13-1296 Enclosures Page 1 of 72

Certificate of Analysis Page 2 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Certificate of Analysis Report for TLGS001 TLG Services, Inc.

Client SDG: 334614 GEL Work Order: 334614 The Qualifiers in this report are defined as follows:

  • A quality control analyte recovery is outside of specified acceptance criteria
    • Analyte is a Tracer compound
    • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the U qualifier above.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Erin Trent.

Reviewed by USER_SIGN_HERE Page 3 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614001 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #1 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 1.62E01 5.69E01 1.04E+00 pCi/g Na22 10/15/13 U 3.43E02 3.85E02 7.93E02 pCi/g K40 10/15/13 3 2.43E+01 1.50E+00 5.73E01 pCi/g Cr51 10/15/13 U 9.19E02 1.14E+00 2.10E+00 pCi/g Mn54 10/15/13 U 1.08E02 4.16E02 7.75E02 pCi/g Fe59 10/15/13 U 7.17E02 1.73E01 3.02E01 pCi/g Co56 10/15/13 U 4.36E02 5.63E02 9.72E02 pCi/g Co57 10/15/13 UI 0.00E+00 5.42E02 7.24E02 pCi/g Co58 10/15/13 U 1.64E02 5.57E02 1.06E01 pCi/g Co60 10/15/13 3 1.71E01 7.30E02 6.11E02 pCi/g Zn65 10/15/13 U 3.71E03 1.81E01 1.86E01 pCi/g Y88 10/15/13 U 2.50E02 3.64E02 6.24E02 pCi/g Zr95 10/15/13 U 1.19E01 1.97E01 2.00E01 pCi/g Nb94 10/15/13 U 8.56E03 3.12E02 5.88E02 pCi/g Nb95 10/15/13 U 3.94E02 7.30E02 1.23E01 pCi/g Ru106 10/15/13 U 2.05E01 3.11E01 5.82E01 pCi/g Ag110m 10/15/13 U 2.25E02 5.52E02 1.04E01 pCi/g Sn113 10/15/13 U 2.08E03 5.77E02 1.05E01 pCi/g Sb124 10/15/13 U 1.05E02 8.41E02 1.77E01 pCi/g Sb125 10/15/13 U 4.06E03 8.66E02 1.56E01 pCi/g Cs134 10/15/13 UI 0.00E+00 6.41E02 9.50E02 pCi/g Cs136 10/15/13 U 1.13E+00 1.27E+00 2.47E+00 pCi/g Cs137 10/15/13 U 9.56E03 3.35E02 6.36E02 1.00E01 pCi/g Ba133 10/15/13 U 2.15E02 4.13E02 6.91E02 pCi/g Ba140 10/15/13 U 1.14E+00 3.33E+00 6.11E+00 pCi/g Ce139 10/15/13 U 1.05E02 3.72E02 6.42E02 pCi/g Ce141 10/15/13 U 6.51E02 1.81E01 3.23E01 pCi/g Ce144 10/15/13 U 2.31E03 2.62E01 4.12E01 pCi/g Nd147 10/15/13 3,U 1.12E+01 1.11E+01 2.11E+01 pCi/g Pm144 10/15/13 U 4.34E03 3.36E02 6.30E02 pCi/g Pm146 10/15/13 U 3.74E03 4.02E02 7.28E02 pCi/g Eu152 10/15/13 3 5.53E01 1.53E01 1.75E01 pCi/g Eu154 10/15/13 U 9.50E02 1.06E01 1.90E01 pCi/g Eu155 10/15/13 U 3.99E02 1.17E01 2.12E01 pCi/g Ir192 10/15/13 U 3.10E02 5.07E02 8.99E02 pCi/g Hg203 10/15/13 U 1.68E02 8.79E02 1.43E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 4 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614001 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #1 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 5.27E01 7.87E02 6.26E02 pCi/g Pb210 10/15/13 U 3.60E01 7.92E+00 1.46E+01 pCi/g Pb212 10/15/13 3 1.82E+00 1.25E01 1.00E01 pCi/g Pb214 10/15/13 3 1.73E+00 1.74E01 1.24E01 pCi/g Bi212 10/15/13 3 1.31E+00 7.58E01 8.31E01 pCi/g Bi214 10/15/13 3 1.27E+00 1.66E01 1.17E01 pCi/g Ra228 10/15/13 3 1.58E+00 2.98E01 2.39E01 pCi/g Ac228 10/15/13 3 1.58E+00 2.98E01 2.39E01 pCi/g Th234 10/15/13 3 3.27E+00 2.89E+00 3.20E+00 pCi/g U235 10/15/13 U 2.05E01 2.12E01 3.84E01 pCi/g U238 10/15/13 3 3.27E+00 2.89E+00 3.20E+00 pCi/g Np239 10/15/13 U 3.56E01 4.68E01 7.72E01 pCi/g Am241 10/15/13 U 1.49E01 2.48E01 4.22E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 5 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614001 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #1 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 1.58E+00 pCi/g 003.816 Bi212 1.31E+00 pCi/g 003.165 Bi214 1.27E+00 pCi/g 003.073 Co60 1.71E01 pCi/g 000.415 Eu152 5.53E01 pCi/g 001.339 Pb212 1.82E+00 pCi/g 004.401 Pb214 1.73E+00 pCi/g 004.183 K40 2.43E+01 pCi/g 058.699 Ra228 1.58E+00 pCi/g 003.816 Tl208 5.27E01 pCi/g 001.276 Th234 3.27E+00 pCi/g 007.910 U238 3.27E+00 pCi/g 007.910 Total Activity: 4.13E+01 Total % Abundance: 100.00 Page 6 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614002 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #2 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 1.32E01 4.60E01 8.30E01 pCi/g Na22 10/15/13 U 8.15E04 3.38E02 6.12E02 pCi/g K40 10/15/13 3 1.93E+01 1.32E+00 5.14E01 pCi/g Cr51 10/15/13 U 1.52E01 1.03E+00 1.74E+00 pCi/g Mn54 10/15/13 U 2.34E02 3.54E02 6.85E02 pCi/g Fe59 10/15/13 U 3.51E02 1.84E01 2.96E01 pCi/g Co56 10/15/13 U 1.71E02 4.82E02 8.72E02 pCi/g Co57 10/15/13 UI 0.00E+00 3.95E02 6.80E02 pCi/g Co58 10/15/13 U 3.10E02 5.05E02 8.96E02 pCi/g Co60 10/15/13 3 1.07E01 4.89E02 5.39E02 pCi/g Zn65 10/15/13 U 6.06E02 1.42E01 1.63E01 pCi/g Y88 10/15/13 U 1.23E03 2.88E02 5.87E02 pCi/g Zr95 10/15/13 U 5.96E02 1.02E01 1.97E01 pCi/g Nb94 10/15/13 U 1.28E02 2.65E02 5.15E02 pCi/g Nb95 10/15/13 U 2.71E02 7.24E02 1.14E01 pCi/g Ru106 10/15/13 U 4.04E01 5.40E01 5.04E01 pCi/g Ag110m 10/15/13 U 4.59E02 4.22E02 7.07E02 pCi/g Sn113 10/15/13 U 1.13E02 4.87E02 8.92E02 pCi/g Sb124 10/15/13 U 9.16E02 1.04E01 2.30E01 pCi/g Sb125 10/15/13 U 7.28E02 7.51E02 1.47E01 pCi/g Cs134 10/15/13 UI 0.00E+00 7.55E02 7.67E02 pCi/g Cs136 10/15/13 U 3.18E01 9.68E01 1.73E+00 pCi/g Cs137 10/15/13 U 5.67E03 2.83E02 5.00E02 1.00E01 pCi/g Ba133 10/15/13 U 1.27E02 3.77E02 6.04E02 pCi/g Ba140 10/15/13 U 2.93E+00 3.02E+00 5.86E+00 pCi/g Ce139 10/15/13 U 1.55E02 3.01E02 5.38E02 pCi/g Ce141 10/15/13 U 5.25E02 1.57E01 2.63E01 pCi/g Ce144 10/15/13 U 6.33E02 1.83E01 3.30E01 pCi/g Nd147 10/15/13 U 2.34E+00 8.44E+00 1.51E+01 pCi/g Pm144 10/15/13 U 6.58E03 2.84E02 5.45E02 pCi/g Pm146 10/15/13 U 2.42E02 3.16E02 6.16E02 pCi/g Eu152 10/15/13 3 6.15E01 1.23E01 1.47E01 pCi/g Eu154 10/15/13 U 2.25E03 9.35E02 1.69E01 pCi/g Eu155 10/15/13 U 2.82E02 8.83E02 1.68E01 pCi/g Ir192 10/15/13 U 2.15E02 4.14E02 7.60E02 pCi/g Hg203 10/15/13 3,U 7.52E02 6.79E02 1.22E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 7 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614002 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #2 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 3.80E01 7.91E02 4.87E02 pCi/g Pb210 10/15/13 U 9.24E01 4.21E+00 8.44E+00 pCi/g Pb212 10/15/13 3 1.44E+00 1.04E01 8.78E02 pCi/g Pb214 10/15/13 3 1.53E+00 1.69E01 2.67E01 pCi/g Bi212 10/15/13 3 1.15E+00 7.44E01 7.21E01 pCi/g Bi214 10/15/13 3 1.11E+00 1.40E01 1.04E01 pCi/g Ra228 10/15/13 3 1.47E+00 2.17E01 1.94E01 pCi/g Ac228 10/15/13 3 1.47E+00 2.17E01 1.94E01 pCi/g Th234 10/15/13 3 3.86E+00 2.39E+00 2.30E+00 pCi/g U235 10/15/13 U 2.05E01 2.35E01 2.83E01 pCi/g U238 10/15/13 3 3.86E+00 2.39E+00 2.30E+00 pCi/g Np239 10/15/13 U 3.01E01 3.84E01 6.13E01 pCi/g Am241 10/15/13 U 6.77E02 1.61E01 2.90E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 8 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614002 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #2 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 1.47E+00 pCi/g 004.036 Bi212 1.15E+00 pCi/g 003.176 Bi214 1.11E+00 pCi/g 003.055 Co60 1.07E01 pCi/g 000.294 Eu152 6.15E01 pCi/g 001.695 Pb212 1.44E+00 pCi/g 003.964 Pb214 1.53E+00 pCi/g 004.201 K40 1.93E+01 pCi/g 053.251 Ra228 1.47E+00 pCi/g 004.036 Tl208 3.80E01 pCi/g 001.046 Th234 3.86E+00 pCi/g 010.623 U238 3.86E+00 pCi/g 010.623 Total Activity: 3.63E+01 Total % Abundance: 100.00 Page 9 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614003 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #3 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 4.44E01 6.79E01 1.30E+00 pCi/g Na22 10/15/13 U 1.85E02 4.93E02 9.21E02 pCi/g K40 10/15/13 3 2.17E+01 1.58E+00 6.63E01 pCi/g Cr51 10/15/13 U 4.53E01 1.74E+00 2.63E+00 pCi/g Mn54 10/15/13 3,U 7.01E02 6.56E02 8.99E02 pCi/g Fe59 10/15/13 U 3.85E02 2.48E01 3.78E01 pCi/g Co56 10/15/13 U 5.23E02 7.56E02 1.46E01 pCi/g Co57 10/15/13 U 4.44E03 9.30E02 6.13E02 pCi/g Co58 10/15/13 3,U 8.58E02 7.42E02 1.48E01 pCi/g Co60 10/15/13 UI 0.00E+00 6.20E02 1.30E01 pCi/g Zn65 10/15/13 U 1.25E01 2.27E01 2.46E01 pCi/g Y88 10/15/13 U 2.87E04 4.98E02 9.66E02 pCi/g Zr95 10/15/13 U 2.24E02 1.45E01 2.61E01 pCi/g Nb94 10/15/13 U 1.07E02 4.82E02 7.56E02 pCi/g Nb95 10/15/13 U 5.80E02 9.29E02 1.70E01 pCi/g Ru106 10/15/13 U 3.77E01 4.30E01 7.36E01 pCi/g Ag110m 10/15/13 U 1.93E02 6.85E02 1.29E01 pCi/g Sn113 10/15/13 U 5.69E02 6.72E02 1.19E01 pCi/g Sb124 10/15/13 U 5.44E02 1.25E01 2.27E01 pCi/g Sb125 10/15/13 U 1.15E02 1.06E01 1.95E01 pCi/g Cs134 10/15/13 UI 0.00E+00 8.16E02 7.70E02 pCi/g Cs136 10/15/13 U 1.19E+00 1.33E+00 2.65E+00 pCi/g Cs137 10/15/13 U 4.10E02 4.56E02 7.64E02 1.00E01 pCi/g Ba133 10/15/13 U 4.08E02 6.40E02 8.89E02 pCi/g Ba140 10/15/13 U 3.57E+00 4.24E+00 7.28E+00 pCi/g Ce139 10/15/13 U 5.20E03 4.21E02 7.72E02 pCi/g Ce141 10/15/13 U 1.31E01 2.14E01 3.61E01 pCi/g Ce144 10/15/13 U 1.07E01 2.51E01 4.61E01 pCi/g Nd147 10/15/13 U 1.11E+00 1.52E+01 2.40E+01 pCi/g Pm144 10/15/13 U 7.13E03 7.56E02 7.57E02 pCi/g Pm146 10/15/13 U 3.47E02 4.62E02 8.92E02 pCi/g Eu152 10/15/13 3 9.11E01 1.99E01 2.19E01 pCi/g Eu154 10/15/13 U 4.68E02 1.36E01 2.53E01 pCi/g Eu155 10/15/13 3,U 2.10E01 1.35E01 2.51E01 pCi/g Ir192 10/15/13 U 2.31E02 6.48E02 1.17E01 pCi/g Hg203 10/15/13 U 3.39E02 9.29E02 1.69E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 10 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614003 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #3 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 5.17E01 9.97E02 7.33E02 pCi/g Pb210 10/15/13 U 3.02E+00 8.24E+00 1.53E+01 pCi/g Pb212 10/15/13 3 1.85E+00 1.39E01 1.16E01 pCi/g Pb214 10/15/13 3 1.75E+00 2.05E01 1.60E01 pCi/g Bi212 10/15/13 3 2.59E+00 9.23E01 9.89E01 pCi/g Bi214 10/15/13 3 1.53E+00 1.61E01 1.43E01 pCi/g Ra228 10/15/13 3 1.48E+00 3.20E01 2.98E01 pCi/g Ac228 10/15/13 3 1.48E+00 3.20E01 2.98E01 pCi/g Th234 10/15/13 U 2.24E+00 3.45E+00 3.48E+00 pCi/g U235 10/15/13 U 2.74E02 3.04E01 4.05E01 pCi/g U238 10/15/13 U 2.24E+00 3.45E+00 3.48E+00 pCi/g Np239 10/15/13 U 2.08E01 5.19E01 8.45E01 pCi/g Am241 10/15/13 3,U 4.62E01 2.61E01 4.62E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 11 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614003 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #3 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 1.48E+00 pCi/g 004.366 Bi212 2.59E+00 pCi/g 007.679 Bi214 1.53E+00 pCi/g 004.526 Eu152 9.11E01 pCi/g 002.696 Pb212 1.85E+00 pCi/g 005.474 Pb214 1.75E+00 pCi/g 005.183 K40 2.17E+01 pCi/g 064.179 Ra228 1.48E+00 pCi/g 004.366 Tl208 5.17E01 pCi/g 001.529 Total Activity: 3.38E+01 Total % Abundance: 100.00 Page 12 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614004 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #4 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 2.94E01 6.34E01 1.09E+00 pCi/g Na22 10/15/13 U 5.99E03 5.24E02 8.50E02 pCi/g K40 10/15/13 3 2.36E+01 1.57E+00 5.31E01 pCi/g Cr51 10/15/13 U 8.53E02 1.21E+00 2.19E+00 pCi/g Mn54 10/15/13 U 1.84E02 4.52E02 8.41E02 pCi/g Fe59 10/15/13 U 2.37E01 2.03E01 3.23E01 pCi/g Co56 10/15/13 U 9.52E03 6.07E02 1.12E01 pCi/g Co57 10/15/13 UI 0.00E+00 6.38E02 8.73E02 pCi/g Co58 10/15/13 U 4.52E02 6.10E02 1.18E01 pCi/g Co60 10/15/13 3 1.43E01 5.44E02 7.97E02 pCi/g Zn65 10/15/13 U 1.09E01 1.78E01 2.07E01 pCi/g Y88 10/15/13 U 5.43E03 4.07E02 7.76E02 pCi/g Zr95 10/15/13 U 5.68E03 1.25E01 2.30E01 pCi/g Nb94 10/15/13 U 5.00E03 4.13E02 6.13E02 pCi/g Nb95 10/15/13 U 8.54E03 8.69E02 1.38E01 pCi/g Ru106 10/15/13 U 4.15E02 3.42E01 6.29E01 pCi/g Ag110m 10/15/13 U 3.18E02 6.08E02 1.06E01 pCi/g Sn113 10/15/13 U 4.02E03 6.33E02 1.13E01 pCi/g Sb124 10/15/13 U 5.99E02 1.28E01 2.65E01 pCi/g Sb125 10/15/13 U 1.75E02 1.01E01 1.82E01 pCi/g Cs134 10/15/13 UI 0.00E+00 5.65E02 9.43E02 pCi/g Cs136 10/15/13 U 1.03E+00 1.32E+00 2.19E+00 pCi/g Cs137 10/15/13 U 2.62E03 4.40E02 7.13E02 1.00E01 pCi/g Ba133 10/15/13 U 5.05E04 4.68E02 7.43E02 pCi/g Ba140 10/15/13 U 1.20E+00 3.47E+00 6.00E+00 pCi/g Ce139 10/15/13 U 6.10E03 3.94E02 6.94E02 pCi/g Ce141 10/15/13 3,U 2.14E01 1.80E01 3.31E01 pCi/g Ce144 10/15/13 U 6.86E03 2.58E01 4.07E01 pCi/g Nd147 10/15/13 U 4.22E+00 1.19E+01 2.05E+01 pCi/g Pm144 10/15/13 U 3.70E02 4.37E02 7.56E02 pCi/g Pm146 10/15/13 U 6.30E04 4.35E02 7.79E02 pCi/g Eu152 10/15/13 3 9.51E01 1.71E01 1.98E01 pCi/g Eu154 10/15/13 U 7.61E03 1.44E01 2.32E01 pCi/g Eu155 10/15/13 3,U 2.08E01 1.80E01 2.11E01 pCi/g Ir192 10/15/13 U 2.62E02 5.85E02 9.71E02 pCi/g Hg203 10/15/13 3,U 1.05E01 9.09E02 1.56E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 13 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614004 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #4 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 5.44E01 8.14E02 6.54E02 pCi/g Pb210 10/15/13 U 1.03E+01 1.59E+01 1.45E+01 pCi/g Pb212 10/15/13 3 1.77E+00 1.29E01 1.12E01 pCi/g Pb214 10/15/13 3 1.84E+00 1.75E01 3.26E01 pCi/g Bi212 10/15/13 3 1.92E+00 1.05E+00 9.21E01 pCi/g Bi214 10/15/13 3 1.41E+00 1.84E01 1.37E01 pCi/g Ra228 10/15/13 3 1.94E+00 3.12E01 2.55E01 pCi/g Ac228 10/15/13 3 1.94E+00 3.12E01 2.55E01 pCi/g Th234 10/15/13 U 1.64E+00 3.24E+00 3.47E+00 pCi/g U235 10/15/13 U 1.05E01 2.18E01 3.76E01 pCi/g U238 10/15/13 U 1.64E+00 3.24E+00 3.47E+00 pCi/g Np239 10/15/13 U 9.05E02 5.02E01 7.89E01 pCi/g Am241 10/15/13 U 4.45E02 3.25E01 4.30E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 14 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614004 Client: TLG Services, Inc.

Client Sample ID: SU 1.6 #4 Collect Date: August 13, 2013 Matrix: Soil Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 1.94E+00 pCi/g 005.372 Bi212 1.92E+00 pCi/g 005.322 Bi214 1.41E+00 pCi/g 003.897 Co60 1.43E01 pCi/g 000.397 Eu152 9.51E01 pCi/g 002.635 Pb212 1.77E+00 pCi/g 004.915 Pb214 1.84E+00 pCi/g 005.106 K40 2.36E+01 pCi/g 065.475 Ra228 1.94E+00 pCi/g 005.372 Tl208 5.44E01 pCi/g 001.509 Total Activity: 3.61E+01 Total % Abundance: 100.00 Page 15 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614005 Client: TLG Services, Inc.

Client Sample ID: SU 1.3 #1 015cm Collect Date: August 22, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 3.46E01 4.87E01 9.55E01 pCi/g Na22 10/15/13 U 1.56E02 5.12E02 8.42E02 pCi/g K40 10/15/13 3 1.61E+01 1.32E+00 4.91E01 pCi/g Cr51 10/15/13 U 4.05E01 8.44E01 1.49E+00 pCi/g Mn54 10/15/13 U 2.13E02 3.54E02 6.15E02 pCi/g Fe59 10/15/13 U 7.76E02 1.59E01 2.80E01 pCi/g Co56 10/15/13 U 5.33E04 6.42E02 9.97E02 pCi/g Co57 10/15/13 UI 0.00E+00 4.14E02 7.71E02 pCi/g Co58 10/15/13 U 1.04E02 4.74E02 8.49E02 pCi/g Co60 10/15/13 3 1.21E01 5.22E02 5.89E02 pCi/g Zn65 10/15/13 U 1.33E01 1.62E01 1.99E01 pCi/g Y88 10/15/13 U 2.39E02 4.06E02 8.94E02 pCi/g Zr95 10/15/13 U 7.28E03 1.08E01 1.95E01 pCi/g Nb94 10/15/13 U 6.31E03 3.21E02 5.93E02 pCi/g Nb95 10/15/13 U 2.34E02 7.11E02 1.07E01 pCi/g Ru106 10/15/13 U 2.63E01 3.11E01 6.13E01 pCi/g Ag110m 10/15/13 U 3.91E02 5.49E02 9.15E02 pCi/g Sn113 10/15/13 U 8.30E03 4.91E02 8.95E02 pCi/g Sb124 10/15/13 U 9.34E02 9.99E02 1.61E01 pCi/g Sb125 10/15/13 U 5.48E02 8.39E02 1.58E01 pCi/g Cs134 10/15/13 3,U 6.27E02 4.19E02 8.51E02 pCi/g Cs136 10/15/13 U 1.83E01 7.47E01 1.43E+00 pCi/g Cs137 10/15/13 U 2.93E02 3.53E02 6.02E02 1.00E01 pCi/g Ba133 10/15/13 U 5.23E02 6.42E02 7.07E02 pCi/g Ba140 10/15/13 U 1.93E+00 1.96E+00 3.36E+00 pCi/g Ce139 10/15/13 U 1.60E02 3.05E02 5.60E02 pCi/g Ce141 10/15/13 U 5.80E02 1.28E01 2.30E01 pCi/g Ce144 10/15/13 U 1.19E02 2.10E01 3.31E01 pCi/g Nd147 10/15/13 U 1.91E+00 5.78E+00 1.05E+01 pCi/g Pm144 10/15/13 U 9.90E03 3.93E02 7.25E02 pCi/g Pm146 10/15/13 U 2.86E03 4.13E02 7.25E02 pCi/g Eu152 10/15/13 3 9.14E01 1.76E01 1.65E01 pCi/g Eu154 10/15/13 U 4.34E02 1.42E01 2.34E01 pCi/g Eu155 10/15/13 U 5.21E02 9.20E02 1.70E01 pCi/g Ir192 10/15/13 U 1.06E02 4.53E02 8.36E02 pCi/g Hg203 10/15/13 U 5.61E04 6.34E02 1.16E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 16 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614005 Client: TLG Services, Inc.

Client Sample ID: SU 1.3 #1 015cm Collect Date: August 22, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 2.68E01 6.79E02 5.61E02 pCi/g Pb210 10/15/13 U 1.23E+00 7.64E+00 6.55E+00 pCi/g Pb212 10/15/13 3 9.24E01 1.03E01 9.86E02 pCi/g Pb214 10/15/13 3 8.45E01 1.18E01 1.07E01 pCi/g Bi212 10/15/13 3 1.52E+00 9.54E01 8.54E01 pCi/g Bi214 10/15/13 3 5.27E01 1.21E01 1.09E01 pCi/g Ra228 10/15/13 3 8.00E01 2.42E01 2.20E01 pCi/g Ac228 10/15/13 3 8.00E01 2.42E01 2.20E01 pCi/g Th234 10/15/13 U 9.77E01 1.89E+00 2.07E+00 pCi/g U235 10/15/13 U 6.62E02 1.86E01 3.26E01 pCi/g U238 10/15/13 U 9.77E01 1.89E+00 2.07E+00 pCi/g Np239 10/15/13 U 2.28E01 4.18E01 6.43E01 pCi/g Am241 10/15/13 U 6.19E02 1.46E01 2.51E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 17 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614005 Client: TLG Services, Inc.

Client Sample ID: SU 1.3 #1 015cm Collect Date: August 22, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 8.00E01 pCi/g 003.506 Bi212 1.52E+00 pCi/g 006.665 Bi214 5.27E01 pCi/g 002.310 Co60 1.21E01 pCi/g 000.529 Eu152 9.14E01 pCi/g 004.007 Pb212 9.24E01 pCi/g 004.049 Pb214 8.45E01 pCi/g 003.704 K40 1.61E+01 pCi/g 070.551 Ra228 8.00E01 pCi/g 003.506 Tl208 2.68E01 pCi/g 001.173 Total Activity: 2.28E+01 Total % Abundance: 100.00 Page 18 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614006 Client: TLG Services, Inc.

Client Sample ID: SU 1.3 #3 015cm Collect Date: August 22, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 1.31E01 4.00E01 7.29E01 pCi/g Na22 10/15/13 U 7.24E03 3.58E02 6.81E02 pCi/g K40 10/15/13 3 1.37E+01 1.09E+00 4.48E01 pCi/g Cr51 10/15/13 U 3.31E01 7.29E01 1.36E+00 pCi/g Mn54 10/15/13 U 2.91E02 3.65E02 6.37E02 pCi/g Fe59 10/15/13 U 7.94E02 1.52E01 2.20E01 pCi/g Co56 10/15/13 U 1.21E02 4.27E02 8.18E02 pCi/g Co57 10/15/13 UI 0.00E+00 6.50E02 3.91E02 pCi/g Co58 10/15/13 U 6.72E02 9.01E02 8.04E02 pCi/g Co60 10/15/13 3 1.69E01 5.41E02 5.97E02 pCi/g Zn65 10/15/13 3,U 1.08E01 8.33E02 1.66E01 pCi/g Y88 10/15/13 U 8.52E04 3.07E02 6.07E02 pCi/g Zr95 10/15/13 U 5.17E02 9.43E02 1.76E01 pCi/g Nb94 10/15/13 U 2.50E02 2.97E02 5.07E02 pCi/g Nb95 10/15/13 U 3.07E02 5.20E02 1.01E01 pCi/g Ru106 10/15/13 U 1.56E01 2.68E01 5.10E01 pCi/g Ag110m 10/15/13 U 2.30E02 4.48E02 7.98E02 pCi/g Sn113 10/15/13 U 1.76E02 4.20E02 7.73E02 pCi/g Sb124 10/15/13 U 3.41E02 7.99E02 1.70E01 pCi/g Sb125 10/15/13 U 4.47E02 6.90E02 1.24E01 pCi/g Cs134 10/15/13 UI 0.00E+00 5.45E02 8.05E02 pCi/g Cs136 10/15/13 U 2.08E01 6.65E01 1.25E+00 pCi/g Cs137 10/15/13 U 1.97E02 3.21E02 5.42E02 1.00E01 pCi/g Ba133 10/15/13 U 9.83E03 3.69E02 5.71E02 pCi/g Ba140 10/15/13 U 6.31E01 1.82E+00 3.22E+00 pCi/g Ce139 10/15/13 U 4.82E03 2.55E02 4.86E02 pCi/g Ce141 10/15/13 U 1.09E02 1.03E01 1.92E01 pCi/g Ce144 10/15/13 U 6.56E02 1.81E01 2.81E01 pCi/g Nd147 10/15/13 U 1.22E+00 5.20E+00 9.46E+00 pCi/g Pm144 10/15/13 U 7.24E03 3.42E02 5.45E02 pCi/g Pm146 10/15/13 U 1.05E02 3.75E02 5.93E02 pCi/g Eu152 10/15/13 3 8.80E01 1.53E01 1.41E01 pCi/g Eu154 10/15/13 U 1.91E02 9.93E02 1.89E01 pCi/g Eu155 10/15/13 U 2.52E02 7.57E02 1.36E01 pCi/g Ir192 10/15/13 U 1.72E02 3.67E02 6.86E02 pCi/g Hg203 10/15/13 U 1.09E04 5.24E02 9.57E02 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 19 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614006 Client: TLG Services, Inc.

Client Sample ID: SU 1.3 #3 015cm Collect Date: August 22, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 2.50E01 6.01E02 5.37E02 pCi/g Pb210 10/15/13 3 2.75E+00 2.61E+00 2.21E+00 pCi/g Pb212 10/15/13 3 9.00E01 1.05E01 8.85E02 pCi/g Pb214 10/15/13 3 7.12E01 1.40E01 1.02E01 pCi/g Bi212 10/15/13 UI 0.00E+00 7.76E01 9.75E01 pCi/g Bi214 10/15/13 3 7.11E01 1.08E01 1.06E01 pCi/g Ra228 10/15/13 3 6.79E01 2.55E01 2.11E01 pCi/g Ac228 10/15/13 3 6.79E01 2.55E01 2.11E01 pCi/g Th234 10/15/13 UI 0.00E+00 1.86E+00 1.20E+00 pCi/g U235 10/15/13 U 1.52E02 1.42E01 2.66E01 pCi/g U238 10/15/13 UI 0.00E+00 1.86E+00 1.20E+00 pCi/g Np239 10/15/13 U 2.22E01 3.61E01 5.56E01 pCi/g Am241 10/15/13 U 2.35E02 8.03E02 1.38E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 20 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614006 Client: TLG Services, Inc.

Client Sample ID: SU 1.3 #3 015cm Collect Date: August 22, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 6.79E01 pCi/g 003.164 Bi214 7.11E01 pCi/g 003.312 Co60 1.69E01 pCi/g 000.787 Eu152 8.80E01 pCi/g 004.100 Pb210 2.75E+00 pCi/g 012.792 Pb212 9.00E01 pCi/g 004.194 Pb214 7.12E01 pCi/g 003.315 K40 1.37E+01 pCi/g 064.006 Ra228 6.79E01 pCi/g 003.164 Tl208 2.50E01 pCi/g 001.165 Total Activity: 2.15E+01 Total % Abundance: 100.00 Page 21 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614007 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #1 015cm Collect Date: August 13, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 3.61E01 4.34E01 8.36E01 pCi/g Na22 10/15/13 U 4.54E03 3.31E02 5.29E02 pCi/g K40 10/15/13 3 1.46E+01 1.20E+00 4.59E01 pCi/g Cr51 10/15/13 U 5.55E01 8.95E01 1.70E+00 pCi/g Mn54 10/15/13 U 5.68E03 3.27E02 6.07E02 pCi/g Fe59 10/15/13 U 1.11E01 1.72E01 2.37E01 pCi/g Co56 10/15/13 U 1.25E02 4.63E02 8.73E02 pCi/g Co57 10/15/13 U 6.43E03 2.16E02 3.90E02 pCi/g Co58 10/15/13 U 4.25E02 5.31E02 7.42E02 pCi/g Co60 10/15/13 3,U 3.28E02 3.01E02 6.41E02 pCi/g Zn65 10/15/13 U 2.68E02 8.47E02 1.31E01 pCi/g Y88 10/15/13 U 2.05E02 3.53E02 6.01E02 pCi/g Zr95 10/15/13 U 2.23E02 9.00E02 1.70E01 pCi/g Nb94 10/15/13 U 4.53E03 2.53E02 4.74E02 pCi/g Nb95 10/15/13 U 3.41E02 6.01E02 1.03E01 pCi/g Ru106 10/15/13 U 1.58E01 2.46E01 4.05E01 pCi/g Ag110m 10/15/13 U 3.48E03 4.30E02 7.97E02 pCi/g Sn113 10/15/13 U 1.15E02 4.67E02 8.27E02 pCi/g Sb124 10/15/13 U 3.31E02 6.35E02 1.14E01 pCi/g Sb125 10/15/13 U 1.54E03 7.40E02 1.31E01 pCi/g Cs134 10/15/13 3,U 3.89E02 3.30E02 6.69E02 pCi/g Cs136 10/15/13 U 2.55E01 9.72E01 1.72E+00 pCi/g Cs137 10/15/13 U 5.03E03 3.02E02 5.63E02 1.00E01 pCi/g Ba133 10/15/13 U 6.22E03 3.38E02 5.50E02 pCi/g Ba140 10/15/13 U 1.55E01 2.49E+00 4.45E+00 pCi/g Ce139 10/15/13 U 6.86E03 2.92E02 5.03E02 pCi/g Ce141 10/15/13 U 5.95E02 1.46E01 2.34E01 pCi/g Ce144 10/15/13 U 1.11E01 1.65E01 3.01E01 pCi/g Nd147 10/15/13 U 2.73E+00 7.41E+00 1.39E+01 pCi/g Pm144 10/15/13 U 3.95E02 3.09E02 5.07E02 pCi/g Pm146 10/15/13 U 2.47E05 3.28E02 5.89E02 pCi/g Eu152 10/15/13 U 6.88E03 7.57E02 1.23E01 pCi/g Eu154 10/15/13 U 1.31E02 9.14E02 1.46E01 pCi/g Eu155 10/15/13 3,U 9.50E02 7.67E02 1.46E01 pCi/g Ir192 10/15/13 U 8.99E03 4.06E02 7.50E02 pCi/g Hg203 10/15/13 3,U 6.08E02 5.90E02 1.14E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 22 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614007 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #1 015cm Collect Date: August 13, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 2.77E01 5.96E02 4.26E02 pCi/g Pb210 10/15/13 U 8.62E01 2.12E+00 4.00E+00 pCi/g Pb212 10/15/13 3 8.89E01 8.31E02 7.14E02 pCi/g Pb214 10/15/13 3 7.55E01 1.28E01 9.03E02 pCi/g Bi212 10/15/13 UI 0.00E+00 5.94E01 9.82E01 pCi/g Bi214 10/15/13 3 7.83E01 1.02E01 9.36E02 pCi/g Ra228 10/15/13 3 9.01E01 2.06E01 2.09E01 pCi/g Ac228 10/15/13 3 9.01E01 2.06E01 2.09E01 pCi/g Th234 10/15/13 3 2.13E+00 1.98E+00 1.53E+00 pCi/g U235 10/15/13 U 5.27E02 2.15E01 2.54E01 pCi/g U238 10/15/13 3 2.13E+00 1.98E+00 1.53E+00 pCi/g Np239 10/15/13 U 3.32E03 2.94E01 5.00E01 pCi/g Am241 10/15/13 U 5.96E02 1.04E01 1.78E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 23 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614007 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #1 015cm Collect Date: August 13, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 9.01E01 pCi/g 003.860 Bi214 7.83E01 pCi/g 003.356 Pb212 8.89E01 pCi/g 003.810 Pb214 7.55E01 pCi/g 003.235 K40 1.46E+01 pCi/g 062.451 Ra228 9.01E01 pCi/g 003.860 Tl208 2.77E01 pCi/g 001.186 Th234 2.13E+00 pCi/g 009.121 U238 2.13E+00 pCi/g 009.121 Total Activity: 2.33E+01 Total % Abundance: 100.00 Page 24 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614008 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #2 015cm Collect Date: August 13, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 4.52E02 3.30E01 5.93E01 pCi/g Na22 10/15/13 U 1.60E02 2.90E02 4.95E02 pCi/g K40 10/15/13 3 1.51E+01 8.55E01 3.01E01 pCi/g Cr51 10/15/13 U 9.07E02 8.03E01 1.38E+00 pCi/g Mn54 10/15/13 3,U 3.11E02 2.49E02 4.84E02 pCi/g Fe59 10/15/13 U 4.41E02 9.77E02 1.73E01 pCi/g Co56 10/15/13 U 1.74E02 3.55E02 5.66E02 pCi/g Co57 10/15/13 U 7.76E03 1.81E02 3.46E02 pCi/g Co58 10/15/13 U 3.09E02 3.48E02 5.88E02 pCi/g Co60 10/15/13 U 6.78E03 2.24E02 4.19E02 pCi/g Zn65 10/15/13 U 1.14E02 6.68E02 1.02E01 pCi/g Y88 10/15/13 U 1.26E02 2.53E02 3.91E02 pCi/g Zr95 10/15/13 U 4.85E02 6.92E02 1.20E01 pCi/g Nb94 10/15/13 U 2.56E03 1.85E02 3.41E02 pCi/g Nb95 10/15/13 U 3.49E02 4.67E02 7.77E02 pCi/g Ru106 10/15/13 U 1.02E01 2.07E01 3.94E01 pCi/g Ag110m 10/15/13 U 2.67E02 3.13E02 6.02E02 pCi/g Sn113 10/15/13 U 1.57E02 3.50E02 6.26E02 pCi/g Sb124 10/15/13 U 1.18E02 7.14E02 1.33E01 pCi/g Sb125 10/15/13 U 4.99E02 5.54E02 9.54E02 pCi/g Cs134 10/15/13 U 2.66E02 3.26E02 5.17E02 pCi/g Cs136 10/15/13 U 5.05E01 7.03E01 1.23E+00 pCi/g Cs137 10/15/13 U 1.96E03 2.19E02 4.05E02 1.00E01 pCi/g Ba133 10/15/13 U 1.72E02 2.94E02 4.89E02 pCi/g Ba140 10/15/13 U 1.30E01 1.94E+00 3.63E+00 pCi/g Ce139 10/15/13 U 9.68E03 2.48E02 4.62E02 pCi/g Ce141 10/15/13 3,U 1.30E01 1.12E01 2.17E01 pCi/g Ce144 10/15/13 U 7.85E02 1.64E01 2.75E01 pCi/g Nd147 10/15/13 U 3.93E01 6.53E+00 1.22E+01 pCi/g Pm144 10/15/13 U 1.81E02 2.11E02 3.65E02 pCi/g Pm146 10/15/13 U 4.40E03 2.43E02 4.37E02 pCi/g Eu152 10/15/13 U 2.19E02 8.36E02 1.09E01 pCi/g Eu154 10/15/13 U 4.42E02 8.03E02 1.27E01 pCi/g Eu155 10/15/13 U 4.37E02 7.07E02 1.31E01 pCi/g Ir192 10/15/13 U 2.08E02 3.28E02 6.28E02 pCi/g Hg203 10/15/13 U 8.02E02 9.82E02 8.77E02 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 25 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614008 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #2 015cm Collect Date: August 13, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 3.08E01 4.39E02 3.62E02 pCi/g Pb210 10/15/13 U 4.48E+00 5.37E+00 4.71E+00 pCi/g Pb212 10/15/13 3 1.07E+00 7.72E02 6.33E02 pCi/g Pb214 10/15/13 3 7.63E01 1.06E01 8.27E02 pCi/g Bi212 10/15/13 UI 0.00E+00 4.68E01 6.87E01 pCi/g Bi214 10/15/13 3 6.32E01 1.05E01 7.23E02 pCi/g Ra228 10/15/13 3 8.30E01 1.87E01 1.38E01 pCi/g Ac228 10/15/13 3 8.30E01 1.87E01 1.38E01 pCi/g Th234 10/15/13 U 1.35E+00 1.58E+00 1.66E+00 pCi/g U235 10/15/13 U 7.98E02 1.31E01 2.48E01 pCi/g U238 10/15/13 U 1.35E+00 1.58E+00 1.66E+00 pCi/g Np239 10/15/13 U 2.58E01 2.56E01 4.65E01 pCi/g Am241 10/15/13 U 2.83E02 1.21E01 1.99E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 26 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614008 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #2 015cm Collect Date: August 13, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 8.30E01 pCi/g 004.256 Bi214 6.32E01 pCi/g 003.240 Pb212 1.07E+00 pCi/g 005.499 Pb214 7.63E01 pCi/g 003.916 K40 1.51E+01 pCi/g 077.254 Ra228 8.30E01 pCi/g 004.256 Tl208 3.08E01 pCi/g 001.579 Total Activity: 1.95E+01 Total % Abundance: 100.00 Page 27 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614009 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #3 015cm Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 1.48E01 4.64E01 8.76E01 pCi/g Na22 10/15/13 U 3.06E02 3.66E02 7.22E02 pCi/g K40 10/15/13 3 1.41E+01 1.12E+00 4.99E01 pCi/g Cr51 10/15/13 U 5.42E04 9.72E01 1.73E+00 pCi/g Mn54 10/15/13 U 5.13E03 3.54E02 6.42E02 pCi/g Fe59 10/15/13 U 9.78E02 1.42E01 2.49E01 pCi/g Co56 10/15/13 U 1.06E02 5.16E02 8.92E02 pCi/g Co57 10/15/13 UI 0.00E+00 7.14E02 4.07E02 pCi/g Co58 10/15/13 U 4.90E03 5.27E02 9.41E02 pCi/g Co60 10/15/13 3 3.44E01 6.34E02 5.65E02 pCi/g Zn65 10/15/13 U 8.08E02 1.48E01 1.68E01 pCi/g Y88 10/15/13 U 1.58E02 3.04E02 6.62E02 pCi/g Zr95 10/15/13 U 5.63E02 1.24E01 2.02E01 pCi/g Nb94 10/15/13 U 1.27E02 2.88E02 4.77E02 pCi/g Nb95 10/15/13 U 1.37E02 7.08E02 1.12E01 pCi/g Ru106 10/15/13 UI 0.00E+00 2.87E01 4.84E01 pCi/g Ag110m 10/15/13 U 1.47E02 4.69E02 8.66E02 pCi/g Sn113 10/15/13 U 2.59E02 4.90E02 8.92E02 pCi/g Sb124 10/15/13 U 3.05E02 1.00E01 1.83E01 pCi/g Sb125 10/15/13 U 2.62E03 7.46E02 1.31E01 pCi/g Cs134 10/15/13 3,U 6.91E02 3.93E02 6.99E02 pCi/g Cs136 10/15/13 U 2.83E01 9.76E01 1.87E+00 pCi/g Cs137 10/15/13 U 4.61E03 3.02E02 5.38E02 1.00E01 pCi/g Ba133 10/15/13 U 4.02E03 3.99E02 6.22E02 pCi/g Ba140 10/15/13 U 1.42E01 2.46E+00 4.58E+00 pCi/g Ce139 10/15/13 U 9.19E03 2.82E02 5.23E02 pCi/g Ce141 10/15/13 U 8.85E02 1.28E01 2.41E01 pCi/g Ce144 10/15/13 U 6.33E02 2.50E01 2.87E01 pCi/g Nd147 10/15/13 U 7.65E+00 8.20E+00 1.41E+01 pCi/g Pm144 10/15/13 U 2.41E02 3.03E02 5.17E02 pCi/g Pm146 10/15/13 U 2.19E02 3.29E02 6.36E02 pCi/g Eu152 10/15/13 3 8.50E01 1.59E01 1.43E01 pCi/g Eu154 10/15/13 U 8.25E02 1.01E01 1.99E01 pCi/g Eu155 10/15/13 U 9.75E02 1.32E01 1.49E01 pCi/g Ir192 10/15/13 U 5.42E03 4.29E02 7.70E02 pCi/g Hg203 10/15/13 U 6.94E02 7.09E02 1.19E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 28 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614009 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #3 015cm Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 2.64E01 6.71E02 5.18E02 pCi/g Pb210 10/15/13 3 2.68E+00 1.49E+00 1.91E+00 pCi/g Pb212 10/15/13 3 1.09E+00 9.25E02 7.82E02 pCi/g Pb214 10/15/13 3 7.81E01 1.23E01 2.04E01 pCi/g Bi212 10/15/13 3,U 7.49E01 6.42E01 9.57E01 pCi/g Bi214 10/15/13 3 6.83E01 1.16E01 1.15E01 pCi/g Ra228 10/15/13 3 1.11E+00 2.34E01 2.07E01 pCi/g Ac228 10/15/13 3 1.11E+00 2.34E01 2.07E01 pCi/g Th234 10/15/13 3 1.64E+00 1.54E+00 1.22E+00 pCi/g U235 10/15/13 U 6.39E02 1.56E01 2.84E01 pCi/g U238 10/15/13 3 1.64E+00 1.54E+00 1.22E+00 pCi/g Np239 10/15/13 U 1.96E01 3.57E01 5.66E01 pCi/g Am241 10/15/13 U 5.35E02 8.16E02 1.34E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 29 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614009 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #3 015cm Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 1.11E+00 pCi/g 004.215 Bi214 6.83E01 pCi/g 002.598 Co60 3.44E01 pCi/g 001.310 Eu152 8.50E01 pCi/g 003.234 Pb210 2.68E+00 pCi/g 010.192 Pb212 1.09E+00 pCi/g 004.162 Pb214 7.81E01 pCi/g 002.972 K40 1.41E+01 pCi/g 053.603 Ra228 1.11E+00 pCi/g 004.215 Tl208 2.64E01 pCi/g 001.006 Th234 1.64E+00 pCi/g 006.247 U238 1.64E+00 pCi/g 006.247 Total Activity: 2.63E+01 Total % Abundance: 100.00 Page 30 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614010 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #4 015cm Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 2.32E01 4.06E01 7.98E01 pCi/g Na22 10/15/13 U 1.59E02 2.71E02 4.62E02 pCi/g K40 10/15/13 3 1.58E+01 1.17E+00 5.06E01 pCi/g Cr51 10/15/13 U 2.68E01 8.59E01 1.54E+00 pCi/g Mn54 10/15/13 U 2.03E02 2.76E02 5.36E02 pCi/g Fe59 10/15/13 U 8.03E02 1.35E01 1.99E01 pCi/g Co56 10/15/13 U 2.64E02 4.20E02 7.17E02 pCi/g Co57 10/15/13 U 1.24E02 1.97E02 3.68E02 pCi/g Co58 10/15/13 U 1.10E02 4.16E02 7.43E02 pCi/g Co60 10/15/13 U 1.58E02 3.30E02 5.65E02 pCi/g Zn65 10/15/13 U 2.33E02 8.13E02 1.34E01 pCi/g Y88 10/15/13 U 4.48E03 2.85E02 5.57E02 pCi/g Zr95 10/15/13 U 4.35E02 8.97E02 1.70E01 pCi/g Nb94 10/15/13 3,U 3.08E02 2.32E02 4.71E02 pCi/g Nb95 10/15/13 U 1.98E02 5.61E02 9.20E02 pCi/g Ru106 10/15/13 U 3.16E02 2.78E01 4.41E01 pCi/g Ag110m 10/15/13 U 3.78E02 3.77E02 6.13E02 pCi/g Sn113 10/15/13 U 8.03E03 4.13E02 7.60E02 pCi/g Sb124 10/15/13 U 3.15E02 1.13E01 2.01E01 pCi/g Sb125 10/15/13 U 2.61E03 5.96E02 1.14E01 pCi/g Cs134 10/15/13 UI 0.00E+00 3.01E02 5.22E02 pCi/g Cs136 10/15/13 U 6.14E02 8.10E01 1.54E+00 pCi/g Cs137 10/15/13 U 2.96E03 2.82E02 5.29E02 1.00E01 pCi/g Ba133 10/15/13 U 3.27E02 3.43E02 5.43E02 pCi/g Ba140 10/15/13 U 1.16E+00 2.14E+00 4.21E+00 pCi/g Ce139 10/15/13 3,U 2.59E02 2.49E02 4.96E02 pCi/g Ce141 10/15/13 U 1.21E01 1.86E01 2.10E01 pCi/g Ce144 10/15/13 U 5.19E03 1.66E01 2.84E01 pCi/g Nd147 10/15/13 U 3.00E+00 6.96E+00 1.27E+01 pCi/g Pm144 10/15/13 U 5.04E03 2.71E02 4.90E02 pCi/g Pm146 10/15/13 U 2.88E02 5.17E02 5.73E02 pCi/g Eu152 10/15/13 U 2.40E02 7.33E02 1.20E01 pCi/g Eu154 10/15/13 U 5.68E02 7.60E02 1.27E01 pCi/g Eu155 10/15/13 U 4.53E02 7.89E02 1.33E01 pCi/g Ir192 10/15/13 U 2.44E02 3.81E02 7.27E02 pCi/g Hg203 10/15/13 3,U 7.20E02 6.08E02 1.07E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 31 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614010 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #4 015cm Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 2.48E01 4.64E02 4.00E02 pCi/g Pb210 10/15/13 U 4.70E+00 5.10E+00 4.80E+00 pCi/g Pb212 10/15/13 3 9.86E01 8.69E02 6.97E02 pCi/g Pb214 10/15/13 3 7.77E01 9.89E02 1.89E01 pCi/g Bi212 10/15/13 3 1.09E+00 4.92E01 7.00E01 pCi/g Bi214 10/15/13 3 5.78E01 1.27E01 8.49E02 pCi/g Ra228 10/15/13 3 7.70E01 1.77E01 1.75E01 pCi/g Ac228 10/15/13 3 7.70E01 1.77E01 1.75E01 pCi/g Th234 10/15/13 U 3.03E01 9.23E01 1.71E+00 pCi/g U235 10/15/13 3,U 2.50E01 2.08E01 2.65E01 pCi/g U238 10/15/13 U 3.03E01 9.23E01 1.71E+00 pCi/g Np239 10/15/13 U 2.31E01 3.17E01 4.85E01 pCi/g Am241 10/15/13 U 1.40E02 1.07E01 2.01E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 32 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614010 Client: TLG Services, Inc.

Client Sample ID: SU 1.4 #4 015cm Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 7.70E01 pCi/g 003.667 Bi212 1.09E+00 pCi/g 005.200 Bi214 5.78E01 pCi/g 002.751 Pb212 9.86E01 pCi/g 004.693 Pb214 7.77E01 pCi/g 003.701 K40 1.58E+01 pCi/g 075.140 Ra228 7.70E01 pCi/g 003.667 Tl208 2.48E01 pCi/g 001.180 Total Activity: 2.10E+01 Total % Abundance: 100.00 Page 33 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614011 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #1 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 2.18E01 4.30E01 7.86E01 pCi/g Na22 10/15/13 U 1.34E02 3.12E02 5.48E02 pCi/g K40 10/15/13 U 1.17E01 4.51E01 7.41E01 pCi/g Cr51 10/15/13 U 5.27E02 8.32E01 1.48E+00 pCi/g Mn54 10/15/13 U 9.65E03 2.99E02 5.19E02 pCi/g Fe59 10/15/13 U 1.35E02 1.18E01 2.27E01 pCi/g Co56 10/15/13 U 2.36E02 5.00E02 8.47E02 pCi/g Co57 10/15/13 U 1.32E03 1.64E02 2.86E02 pCi/g Co58 10/15/13 U 2.49E02 4.77E02 8.09E02 pCi/g Co60 10/15/13 U 2.45E02 4.56E02 6.08E02 pCi/g Zn65 10/15/13 U 7.23E02 7.76E02 1.28E01 pCi/g Y88 10/15/13 U 1.87E02 4.99E02 9.02E02 pCi/g Zr95 10/15/13 U 1.35E02 8.63E02 1.59E01 pCi/g Nb94 10/15/13 U 2.19E02 2.77E02 5.29E02 pCi/g Nb95 10/15/13 U 4.26E02 5.05E02 9.85E02 pCi/g Ru106 10/15/13 U 1.41E01 2.64E01 4.56E01 pCi/g Ag110m 10/15/13 3,U 4.14E02 3.67E02 7.71E02 pCi/g Sn113 10/15/13 U 4.19E02 4.07E02 6.53E02 pCi/g Sb124 10/15/13 U 9.05E03 1.27E01 2.52E01 pCi/g Sb125 10/15/13 U 1.00E02 6.85E02 1.22E01 pCi/g Cs134 10/15/13 U 1.02E02 3.66E02 5.47E02 pCi/g Cs136 10/15/13 U 1.52E01 8.71E01 1.61E+00 pCi/g Cs137 10/15/13 U 4.25E03 3.24E02 5.01E02 1.00E01 pCi/g Ba133 10/15/13 U 1.29E02 3.24E02 5.52E02 pCi/g Ba140 10/15/13 U 1.37E+00 2.39E+00 4.40E+00 pCi/g Ce139 10/15/13 U 1.64E02 2.66E02 3.82E02 pCi/g Ce141 10/15/13 U 1.99E02 1.33E01 1.60E01 pCi/g Ce144 10/15/13 U 8.90E02 1.32E01 2.17E01 pCi/g Nd147 10/15/13 U 7.03E+00 7.60E+00 1.44E+01 pCi/g Pm144 10/15/13 U 7.22E03 3.09E02 5.66E02 pCi/g Pm146 10/15/13 U 3.17E04 3.32E02 5.79E02 pCi/g Eu152 10/15/13 U 2.55E02 7.28E02 1.31E01 pCi/g Eu154 10/15/13 U 4.91E02 8.91E02 1.53E01 pCi/g Eu155 10/15/13 U 8.88E03 6.12E02 1.08E01 pCi/g Ir192 10/15/13 U 3.57E03 4.25E02 6.70E02 pCi/g Hg203 10/15/13 U 7.09E03 5.52E02 9.05E02 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 34 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614011 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #1 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 U 8.53E03 3.27E02 5.36E02 pCi/g Pb210 10/15/13 U 1.19E+00 4.54E+00 6.63E+00 pCi/g Pb212 10/15/13 U 1.57E02 5.68E02 7.81E02 pCi/g Pb214 10/15/13 U 6.33E02 7.11E02 1.01E01 pCi/g Bi212 10/15/13 U 2.42E01 3.70E01 7.12E01 pCi/g Bi214 10/15/13 U 1.27E02 6.65E02 1.13E01 pCi/g Ra228 10/15/13 3,U 1.76E01 1.50E01 2.44E01 pCi/g Ac228 10/15/13 3,U 1.76E01 1.50E01 2.44E01 pCi/g Th234 10/15/13 U 3.42E01 1.23E+00 1.53E+00 pCi/g U235 10/15/13 U 2.64E02 1.54E01 2.25E01 pCi/g U238 10/15/13 U 3.42E01 1.23E+00 1.53E+00 pCi/g Np239 10/15/13 U 2.95E02 2.22E01 3.83E01 pCi/g Am241 10/15/13 U 5.97E02 1.25E01 1.95E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 35 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614011 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #1 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Total Activity: 0.00E+00 Total % Abundance: 000.00 Page 36 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614012 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #2 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 2.19E02 3.52E01 6.16E01 pCi/g Na22 10/15/13 U 1.06E02 2.94E02 5.02E02 pCi/g K40 10/15/13 U 8.24E04 3.73E01 4.58E01 pCi/g Cr51 10/15/13 U 4.11E01 6.38E01 1.38E+00 pCi/g Mn54 10/15/13 U 9.96E03 2.75E02 4.80E02 pCi/g Fe59 10/15/13 U 3.95E02 1.27E01 2.20E01 pCi/g Co56 10/15/13 U 2.86E02 4.01E02 6.71E02 pCi/g Co57 10/15/13 U 8.05E03 1.69E02 2.76E02 pCi/g Co58 10/15/13 U 2.49E04 3.66E02 6.73E02 pCi/g Co60 10/15/13 3,U 3.54E02 2.32E02 4.83E02 pCi/g Zn65 10/15/13 U 2.29E02 6.14E02 1.16E01 pCi/g Y88 10/15/13 U 2.61E03 3.99E02 6.84E02 pCi/g Zr95 10/15/13 U 2.96E02 7.16E02 1.25E01 pCi/g Nb94 10/15/13 U 5.87E03 2.34E02 4.14E02 pCi/g Nb95 10/15/13 U 1.88E02 5.47E02 9.44E02 pCi/g Ru106 10/15/13 U 4.57E02 2.60E01 4.54E01 pCi/g Ag110m 10/15/13 U 1.22E02 3.75E02 7.07E02 pCi/g Sn113 10/15/13 U 4.93E04 3.88E02 6.78E02 pCi/g Sb124 10/15/13 U 6.41E02 9.57E02 1.62E01 pCi/g Sb125 10/15/13 U 3.46E02 6.20E02 1.03E01 pCi/g Cs134 10/15/13 U 2.66E02 3.28E02 5.02E02 pCi/g Cs136 10/15/13 U 2.68E02 7.48E01 1.36E+00 pCi/g Cs137 10/15/13 U 3.91E04 2.56E02 4.42E02 1.00E01 pCi/g Ba133 10/15/13 U 6.69E03 3.07E02 4.86E02 pCi/g Ba140 10/15/13 U 1.72E01 1.92E+00 3.41E+00 pCi/g Ce139 10/15/13 U 1.21E02 2.37E02 3.80E02 pCi/g Ce141 10/15/13 U 4.22E03 1.31E01 1.66E01 pCi/g Ce144 10/15/13 U 8.78E02 1.29E01 2.25E01 pCi/g Nd147 10/15/13 3,U 5.83E+00 5.81E+00 1.27E+01 pCi/g Pm144 10/15/13 U 6.83E03 2.83E02 5.00E02 pCi/g Pm146 10/15/13 U 3.01E02 2.87E02 4.51E02 pCi/g Eu152 10/15/13 U 3.96E02 6.63E02 1.10E01 pCi/g Eu154 10/15/13 U 2.80E02 8.14E02 1.40E01 pCi/g Eu155 10/15/13 U 2.54E02 6.36E02 9.95E02 pCi/g Ir192 10/15/13 U 1.51E02 3.81E02 6.16E02 pCi/g Hg203 10/15/13 U 3.28E02 4.67E02 8.61E02 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 37 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614012 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #2 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 U 1.67E02 3.74E02 4.03E02 pCi/g Pb210 10/15/13 U 9.57E01 3.41E+00 5.94E+00 pCi/g Pb212 10/15/13 3 6.73E02 5.45E02 6.56E02 pCi/g Pb214 10/15/13 U 4.34E02 7.35E02 8.07E02 pCi/g Bi212 10/15/13 U 1.59E01 3.50E01 6.58E01 pCi/g Bi214 10/15/13 U 5.25E03 7.88E02 1.14E01 pCi/g Ra228 10/15/13 3 2.35E01 1.38E01 1.38E01 pCi/g Ac228 10/15/13 3 2.35E01 1.38E01 1.38E01 pCi/g Th234 10/15/13 U 9.18E01 1.25E+00 1.50E+00 pCi/g U235 10/15/13 U 5.06E03 1.57E01 1.92E01 pCi/g U238 10/15/13 U 9.18E01 1.25E+00 1.50E+00 pCi/g Np239 10/15/13 U 3.76E02 2.67E01 4.06E01 pCi/g Am241 10/15/13 U 6.35E02 1.20E01 1.92E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 38 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614012 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #2 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Ac228 2.35E01 pCi/g 043.734 Pb212 6.73E02 pCi/g 012.532 Ra228 2.35E01 pCi/g 043.734 Total Activity: 5.37E01 Total % Abundance: 100.00 Page 39 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614013 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #3 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 2.58E01 3.82E01 6.21E01 pCi/g Na22 10/15/13 U 4.02E03 2.25E02 4.23E02 pCi/g K40 10/15/13 U 2.80E01 4.10E01 3.65E01 pCi/g Cr51 10/15/13 U 1.39E02 6.89E01 1.21E+00 pCi/g Mn54 10/15/13 U 1.91E02 3.36E02 5.28E02 pCi/g Fe59 10/15/13 U 3.36E02 1.25E01 2.20E01 pCi/g Co56 10/15/13 U 1.94E02 4.04E02 6.76E02 pCi/g Co57 10/15/13 U 1.29E02 1.57E02 2.82E02 pCi/g Co58 10/15/13 U 9.18E03 4.26E02 7.34E02 pCi/g Co60 10/15/13 3 4.01E01 6.42E02 4.48E02 pCi/g Zn65 10/15/13 U 1.35E02 6.74E02 1.19E01 pCi/g Y88 10/15/13 U 7.80E03 3.04E02 6.12E02 pCi/g Zr95 10/15/13 U 9.60E03 8.33E02 1.32E01 pCi/g Nb94 10/15/13 U 1.28E02 2.10E02 3.53E02 pCi/g Nb95 10/15/13 U 6.70E03 4.52E02 7.85E02 pCi/g Ru106 10/15/13 U 3.62E02 2.40E01 4.23E01 pCi/g Ag110m 10/15/13 U 3.09E03 4.06E02 7.42E02 pCi/g Sn113 10/15/13 U 2.56E02 3.96E02 6.43E02 pCi/g Sb124 10/15/13 U 3.00E02 1.00E01 1.97E01 pCi/g Sb125 10/15/13 U 1.97E02 6.37E02 1.08E01 pCi/g Cs134 10/15/13 U 2.79E03 2.87E02 5.01E02 pCi/g Cs136 10/15/13 U 7.21E01 7.53E01 1.24E+00 pCi/g Cs137 10/15/13 U 3.98E03 2.66E02 4.32E02 1.00E01 pCi/g Ba133 10/15/13 3,U 3.03E02 2.79E02 4.71E02 pCi/g Ba140 10/15/13 U 9.75E01 2.18E+00 4.04E+00 pCi/g Ce139 10/15/13 U 5.92E03 2.17E02 3.36E02 pCi/g Ce141 10/15/13 U 2.78E02 9.34E02 1.62E01 pCi/g Ce144 10/15/13 U 7.40E02 1.28E01 2.08E01 pCi/g Nd147 10/15/13 U 4.73E+00 7.36E+00 1.15E+01 pCi/g Pm144 10/15/13 3,U 3.40E02 2.55E02 4.93E02 pCi/g Pm146 10/15/13 U 1.69E02 2.82E02 5.07E02 pCi/g Eu152 10/15/13 U 3.94E02 6.15E02 1.12E01 pCi/g Eu154 10/15/13 U 2.17E02 6.09E02 1.18E01 pCi/g Eu155 10/15/13 U 3.20E02 5.21E02 8.83E02 pCi/g Ir192 10/15/13 U 1.60E02 3.55E02 5.49E02 pCi/g Hg203 10/15/13 U 1.61E02 4.92E02 7.88E02 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 40 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614013 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #3 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3,U 3.57E02 3.38E02 4.04E02 pCi/g Pb210 10/15/13 U 1.84E01 3.14E+00 5.19E+00 pCi/g Pb212 10/15/13 3,U 5.12E02 4.83E02 6.87E02 pCi/g Pb214 10/15/13 U 1.29E02 7.30E02 8.94E02 pCi/g Bi212 10/15/13 U 4.60E03 3.87E01 6.07E01 pCi/g Bi214 10/15/13 U 1.15E02 7.75E02 8.23E02 pCi/g Ra228 10/15/13 U 7.46E02 1.64E01 2.00E01 pCi/g Ac228 10/15/13 U 7.46E02 1.64E01 2.00E01 pCi/g Th234 10/15/13 U 3.41E01 1.38E+00 1.80E+00 pCi/g U235 10/15/13 U 1.79E01 1.34E01 2.02E01 pCi/g U238 10/15/13 U 3.41E01 1.38E+00 1.80E+00 pCi/g Np239 10/15/13 U 3.13E03 2.28E01 3.55E01 pCi/g Am241 10/15/13 U 3.98E02 1.02E01 1.62E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 41 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614013 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #3 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Co60 4.01E01 pCi/g 100.000 Total Activity: 4.01E01 Total % Abundance: 100.00 Page 42 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614014 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #4 Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 3.49E01 8.50E01 1.38E+00 pCi/g Na22 10/15/13 U 3.06E03 5.23E02 9.16E02 pCi/g K40 10/15/13 U 2.70E01 7.15E01 1.01E+00 pCi/g Cr51 10/15/13 U 6.90E01 1.64E+00 2.81E+00 pCi/g Mn54 10/15/13 3,U 6.43E02 5.56E02 1.02E01 pCi/g Fe59 10/15/13 U 5.38E02 2.78E01 4.09E01 pCi/g Co56 10/15/13 U 3.82E02 8.57E02 1.51E01 pCi/g Co57 10/15/13 U 7.32E03 2.99E02 4.97E02 pCi/g Co58 10/15/13 U 2.26E02 8.78E02 1.53E01 pCi/g Co60 10/15/13 U 5.01E02 5.74E02 1.07E01 pCi/g Zn65 10/15/13 U 4.49E02 1.40E01 2.03E01 pCi/g Y88 10/15/13 U 2.63E02 6.19E02 1.22E01 pCi/g Zr95 10/15/13 U 8.00E02 1.64E01 2.90E01 pCi/g Nb94 10/15/13 U 4.09E03 5.04E02 8.65E02 pCi/g Nb95 10/15/13 U 1.10E02 9.88E02 1.67E01 pCi/g Ru106 10/15/13 U 1.16E01 4.83E01 8.44E01 pCi/g Ag110m 10/15/13 U 5.57E02 8.16E02 1.32E01 pCi/g Sn113 10/15/13 U 1.84E02 8.30E02 1.38E01 pCi/g Sb124 10/15/13 U 6.20E02 2.05E01 3.62E01 pCi/g Sb125 10/15/13 U 1.39E02 1.38E01 2.29E01 pCi/g Cs134 10/15/13 U 2.45E02 6.08E02 1.07E01 pCi/g Cs136 10/15/13 U 5.55E01 1.73E+00 3.11E+00 pCi/g Cs137 10/15/13 U 2.69E02 5.34E02 8.92E02 1.00E01 pCi/g Ba133 10/15/13 U 5.09E02 7.90E02 1.03E01 pCi/g Ba140 10/15/13 U 1.19E+00 4.87E+00 8.33E+00 pCi/g Ce139 10/15/13 U 1.44E02 4.73E02 7.62E02 pCi/g Ce141 10/15/13 UI 0.00E+00 2.89E01 3.33E01 pCi/g Ce144 10/15/13 U 1.73E01 2.39E01 3.82E01 pCi/g Nd147 10/15/13 U 5.17E01 1.81E+01 2.58E+01 pCi/g Pm144 10/15/13 U 1.86E03 5.58E02 9.57E02 pCi/g Pm146 10/15/13 U 2.79E02 6.02E02 9.79E02 pCi/g Eu152 10/15/13 U 3.26E02 1.77E01 2.29E01 pCi/g Eu154 10/15/13 U 1.75E03 1.44E01 2.53E01 pCi/g Eu155 10/15/13 U 5.76E02 8.33E02 1.78E01 pCi/g Ir192 10/15/13 U 7.07E02 7.46E02 1.21E01 pCi/g Hg203 10/15/13 U 2.19E02 9.85E02 1.68E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 43 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614014 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #4 Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3,U 7.64E02 7.11E02 8.52E02 pCi/g Pb210 10/15/13 U 5.94E01 6.66E01 8.62E01 pCi/g Pb212 10/15/13 U 1.67E02 9.53E02 1.32E01 pCi/g Pb214 10/15/13 U 8.60E02 1.44E01 1.89E01 pCi/g Bi212 10/15/13 U 8.91E01 1.06E+00 1.23E+00 pCi/g Bi214 10/15/13 U 7.61E03 1.43E01 2.02E01 pCi/g Ra228 10/15/13 U 1.68E01 3.27E01 4.03E01 pCi/g Ac228 10/15/13 U 1.68E01 3.27E01 4.03E01 pCi/g Th234 10/15/13 U 2.88E02 7.54E01 9.78E01 pCi/g U235 10/15/13 U 2.66E01 2.85E01 3.64E01 pCi/g U238 10/15/13 U 2.88E02 7.54E01 9.78E01 pCi/g Np239 10/15/13 U 9.18E02 4.23E01 7.04E01 pCi/g Am241 10/15/13 U 1.99E02 7.31E02 1.03E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 44 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614014 Client: TLG Services, Inc.

Client Sample ID: SU 1.1 #4 Collect Date: August 14, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Total Activity: 0.00E+00 Total % Abundance: 000.00 Page 45 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614015 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #1 Collect Date: August 09, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 3.60E01 4.75E01 8.34E01 pCi/g Na22 10/15/13 3,U 2.58E02 2.53E02 5.71E02 pCi/g K40 10/15/13 U 1.76E01 3.05E01 6.04E01 pCi/g Cr51 10/15/13 U 4.23E02 9.89E01 1.81E+00 pCi/g Mn54 10/15/13 U 3.56E02 3.42E02 5.80E02 pCi/g Fe59 10/15/13 U 7.49E02 1.66E01 3.25E01 pCi/g Co56 10/15/13 U 1.11E02 5.41E02 1.00E01 pCi/g Co57 10/15/13 UI 0.00E+00 3.82E02 3.59E02 pCi/g Co58 10/15/13 U 1.63E02 5.21E02 1.02E01 pCi/g Co60 10/15/13 3 9.51E01 1.03E01 4.49E02 pCi/g Zn65 10/15/13 3,U 9.61E02 6.18E02 1.49E01 pCi/g Y88 10/15/13 U 2.16E02 4.38E02 9.47E02 pCi/g Zr95 10/15/13 U 3.99E02 1.09E01 1.84E01 pCi/g Nb94 10/15/13 U 9.47E03 3.31E02 4.99E02 pCi/g Nb95 10/15/13 U 3.71E02 5.95E02 1.15E01 pCi/g Ru106 10/15/13 U 6.11E02 2.51E01 4.82E01 pCi/g Ag110m 10/15/13 U 6.56E03 5.39E02 1.02E01 pCi/g Sn113 10/15/13 U 1.48E02 4.32E02 8.01E02 pCi/g Sb124 10/15/13 U 1.41E02 7.31E02 1.69E01 pCi/g Sb125 10/15/13 U 3.19E02 7.52E02 1.33E01 pCi/g Cs134 10/15/13 UI 0.00E+00 7.23E02 7.16E02 pCi/g Cs136 10/15/13 U 1.76E01 1.35E+00 2.49E+00 pCi/g Cs137 10/15/13 U 2.32E02 2.74E02 4.59E02 1.00E01 pCi/g Ba133 10/15/13 U 1.76E03 3.28E02 5.90E02 pCi/g Ba140 10/15/13 U 1.36E02 3.21E+00 6.05E+00 pCi/g Ce139 10/15/13 U 8.12E03 2.82E02 4.80E02 pCi/g Ce141 10/15/13 U 4.75E02 1.34E01 2.31E01 pCi/g Ce144 10/15/13 U 8.10E02 1.36E01 2.69E01 pCi/g Nd147 10/15/13 U 3.87E+00 1.17E+01 2.20E+01 pCi/g Pm144 10/15/13 U 3.64E03 3.28E02 6.04E02 pCi/g Pm146 10/15/13 U 1.24E02 3.13E02 6.14E02 pCi/g Eu152 10/15/13 UI 0.00E+00 1.26E01 1.80E01 pCi/g Eu154 10/15/13 3,U 7.11E02 6.98E02 1.58E01 pCi/g Eu155 10/15/13 3,U 8.76E02 7.39E02 1.44E01 pCi/g Ir192 10/15/13 U 1.18E02 4.10E02 7.30E02 pCi/g Hg203 10/15/13 U 1.05E02 6.08E02 1.13E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 46 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614015 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #1 Collect Date: August 09, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 6.93E02 3.84E02 4.98E02 pCi/g Pb210 10/15/13 U 3.05E02 4.45E+00 8.25E+00 pCi/g Pb212 10/15/13 3,U 1.03E01 7.95E02 1.11E01 pCi/g Pb214 10/15/13 U 1.95E02 6.58E02 1.05E01 pCi/g Bi212 10/15/13 U 3.21E01 4.37E01 8.50E01 pCi/g Bi214 10/15/13 U 1.93E02 6.84E02 1.19E01 pCi/g Ra228 10/15/13 U 1.91E01 1.96E01 2.86E01 pCi/g Ac228 10/15/13 U 1.91E01 1.96E01 2.86E01 pCi/g Th234 10/15/13 U 9.73E01 1.13E+00 2.05E+00 pCi/g U235 10/15/13 U 7.21E03 1.32E01 2.49E01 pCi/g U238 10/15/13 U 9.73E01 1.13E+00 2.05E+00 pCi/g Np239 10/15/13 U 6.25E02 2.94E01 4.92E01 pCi/g Am241 10/15/13 U 1.11E02 1.28E01 2.38E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 47 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614015 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #1 Collect Date: August 09, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Co60 9.51E01 pCi/g 093.201 Tl208 6.93E02 pCi/g 006.799 Total Activity: 1.02E+00 Total % Abundance: 100.00 Page 48 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614016 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #2 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 2.27E01 2.75E01 4.94E01 pCi/g Na22 10/15/13 U 1.12E02 1.50E02 3.26E02 pCi/g K40 10/15/13 U 1.65E01 2.27E01 1.98E01 pCi/g Cr51 10/15/13 U 2.53E01 4.53E01 8.79E01 pCi/g Mn54 10/15/13 U 8.71E03 2.46E02 3.93E02 pCi/g Fe59 10/15/13 U 1.66E02 9.77E02 1.81E01 pCi/g Co56 10/15/13 U 8.19E04 3.25E02 6.28E02 pCi/g Co57 10/15/13 UI 0.00E+00 3.51E02 3.85E02 pCi/g Co58 10/15/13 U 9.84E03 3.05E02 5.77E02 pCi/g Co60 10/15/13 3 7.72E01 7.27E02 3.83E02 pCi/g Zn65 10/15/13 U 6.18E03 6.44E02 1.05E01 pCi/g Y88 10/15/13 U 1.36E02 2.20E02 5.02E02 pCi/g Zr95 10/15/13 U 4.56E02 5.53E02 1.17E01 pCi/g Nb94 10/15/13 U 7.29E04 1.80E02 3.54E02 pCi/g Nb95 10/15/13 U 2.90E02 3.24E02 6.77E02 pCi/g Ru106 10/15/13 U 8.65E02 1.76E01 3.16E01 pCi/g Ag110m 10/15/13 U 6.88E03 3.38E02 6.35E02 pCi/g Sn113 10/15/13 U 1.07E02 2.52E02 5.18E02 pCi/g Sb124 10/15/13 U 8.43E02 5.48E02 5.89E02 pCi/g Sb125 10/15/13 U 4.70E03 4.22E02 8.23E02 pCi/g Cs134 10/15/13 U 1.05E03 2.11E02 4.09E02 pCi/g Cs136 10/15/13 U 1.66E01 6.07E01 1.19E+00 pCi/g Cs137 10/15/13 U 1.56E02 1.77E02 3.02E02 1.00E01 pCi/g Ba133 10/15/13 U 1.78E03 1.78E02 3.60E02 pCi/g Ba140 10/15/13 U 1.49E01 1.48E+00 2.88E+00 pCi/g Ce139 10/15/13 U 9.71E03 1.38E02 2.88E02 pCi/g Ce141 10/15/13 U 2.45E02 7.19E02 1.33E01 pCi/g Ce144 10/15/13 U 6.75E02 9.23E02 1.74E01 pCi/g Nd147 10/15/13 U 4.98E+00 4.34E+00 7.38E+00 pCi/g Pm144 10/15/13 U 1.85E02 1.81E02 3.26E02 pCi/g Pm146 10/15/13 U 1.29E03 1.83E02 3.62E02 pCi/g Eu152 10/15/13 3 4.81E01 8.76E02 7.79E02 pCi/g Eu154 10/15/13 U 2.01E02 4.26E02 8.98E02 pCi/g Eu155 10/15/13 U 9.47E03 4.21E02 8.82E02 pCi/g Ir192 10/15/13 U 5.37E03 2.12E02 4.22E02 pCi/g Hg203 10/15/13 U 2.83E02 3.10E02 6.35E02 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 49 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614016 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #2 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 4.23E02 3.83E02 3.09E02 pCi/g Pb210 10/15/13 U 3.53E01 2.65E+00 5.25E+00 pCi/g Pb212 10/15/13 3 2.63E01 5.56E02 4.99E02 pCi/g Pb214 10/15/13 U 5.76E03 3.51E02 6.82E02 pCi/g Bi212 10/15/13 U 2.98E01 3.28E01 4.87E01 pCi/g Bi214 10/15/13 3,U 6.28E02 5.09E02 7.34E02 pCi/g Ra228 10/15/13 3,U 1.37E01 9.33E02 1.85E01 pCi/g Ac228 10/15/13 3,U 1.37E01 9.33E02 1.85E01 pCi/g Th234 10/15/13 U 3.22E02 1.65E+00 1.31E+00 pCi/g U235 10/15/13 U 3.81E03 8.26E02 1.53E01 pCi/g U238 10/15/13 U 3.22E02 1.65E+00 1.31E+00 pCi/g Np239 10/15/13 U 4.73E02 1.77E01 3.32E01 pCi/g Am241 10/15/13 U 2.05E02 8.09E02 1.62E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 50 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614016 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #2 Collect Date: August 15, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Co60 7.72E01 pCi/g 049.568 Eu152 4.81E01 pCi/g 030.855 Pb212 2.63E01 pCi/g 016.865 Tl208 4.23E02 pCi/g 002.712 Total Activity: 1.56E+00 Total % Abundance: 100.00 Page 51 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614017 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #3 Collect Date: August 16, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 2.41E02 2.08E01 4.03E01 pCi/g Na22 10/15/13 U 3.51E05 1.71E02 2.73E02 pCi/g K40 10/15/13 U 7.96E02 1.50E01 2.91E01 pCi/g Cr51 10/15/13 U 4.51E02 3.91E01 7.42E01 pCi/g Mn54 10/15/13 U 1.51E02 1.77E02 3.42E02 pCi/g Fe59 10/15/13 U 1.43E02 8.05E02 1.40E01 pCi/g Co56 10/15/13 U 1.49E02 2.67E02 5.15E02 pCi/g Co57 10/15/13 3,U 1.06E02 1.02E02 2.14E02 pCi/g Co58 10/15/13 U 9.20E03 2.75E02 5.03E02 pCi/g Co60 10/15/13 3 8.68E01 6.23E02 2.32E02 pCi/g Zn65 10/15/13 U 5.94E02 5.48E02 7.58E02 pCi/g Y88 10/15/13 U 4.27E03 2.11E02 3.96E02 pCi/g Zr95 10/15/13 U 5.11E04 4.55E02 8.62E02 pCi/g Nb94 10/15/13 U 6.84E03 1.63E02 2.55E02 pCi/g Nb95 10/15/13 U 1.18E02 2.80E02 5.10E02 pCi/g Ru106 10/15/13 U 6.95E02 1.35E01 2.71E01 pCi/g Ag110m 10/15/13 3,U 2.89E02 2.62E02 5.21E02 pCi/g Sn113 10/15/13 U 8.22E03 2.15E02 4.11E02 pCi/g Sb124 10/15/13 U 4.81E02 4.64E02 7.27E02 pCi/g Sb125 10/15/13 U 1.59E02 3.55E02 6.69E02 pCi/g Cs134 10/15/13 U 8.92E03 1.77E02 3.44E02 pCi/g Cs136 10/15/13 U 1.79E01 5.07E01 9.74E01 pCi/g Cs137 10/15/13 U 5.18E03 1.47E02 2.90E02 1.00E01 pCi/g Ba133 10/15/13 U 9.52E03 1.74E02 2.87E02 pCi/g Ba140 10/15/13 U 9.07E01 1.16E+00 2.06E+00 pCi/g Ce139 10/15/13 U 2.90E03 1.33E02 2.51E02 pCi/g Ce141 10/15/13 U 1.84E02 5.64E02 1.12E01 pCi/g Ce144 10/15/13 U 1.99E02 7.81E02 1.51E01 pCi/g Nd147 10/15/13 U 5.94E01 3.69E+00 6.90E+00 pCi/g Pm144 10/15/13 U 9.44E03 1.44E02 2.88E02 pCi/g Pm146 10/15/13 U 1.62E03 1.56E02 3.04E02 pCi/g Eu152 10/15/13 UI 0.00E+00 6.02E02 7.32E02 pCi/g Eu154 10/15/13 U 3.98E04 4.74E02 7.53E02 pCi/g Eu155 10/15/13 U 2.15E02 3.57E02 6.97E02 pCi/g Ir192 10/15/13 U 8.66E03 1.98E02 3.66E02 pCi/g Hg203 10/15/13 U 7.74E03 2.75E02 5.40E02 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 52 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614017 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #3 Collect Date: August 16, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 3 3.46E02 2.48E02 2.70E02 pCi/g Pb210 10/15/13 U 9.69E02 2.11E+00 4.02E+00 pCi/g Pb212 10/15/13 3 1.59E01 5.65E02 3.98E02 pCi/g Pb214 10/15/13 U 4.08E02 5.63E02 5.92E02 pCi/g Bi212 10/15/13 U 1.69E01 2.12E01 4.22E01 pCi/g Bi214 10/15/13 U 5.52E02 5.91E02 6.95E02 pCi/g Ra228 10/15/13 U 1.20E01 1.35E01 1.50E01 pCi/g Ac228 10/15/13 U 1.20E01 1.35E01 1.50E01 pCi/g Th234 10/15/13 U 3.88E01 1.16E+00 1.08E+00 pCi/g U235 10/15/13 U 7.61E03 7.97E02 1.38E01 pCi/g U238 10/15/13 U 3.88E01 1.16E+00 1.08E+00 pCi/g Np239 10/15/13 U 2.75E02 1.44E01 2.84E01 pCi/g Am241 10/15/13 U 4.90E02 6.90E02 1.40E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 53 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614017 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #3 Collect Date: August 16, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Co60 8.68E01 pCi/g 081.792 Pb212 1.59E01 pCi/g 014.949 Tl208 3.46E02 pCi/g 003.259 Total Activity: 1.06E+00 Total % Abundance: 100.00 Page 54 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614018 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #4 Collect Date: August 16, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Gamma Spec Be7 10/15/13 U 6.36E02 2.17E01 4.18E01 pCi/g Na22 10/15/13 U 4.30E03 1.35E02 2.46E02 pCi/g K40 10/15/13 U 4.10E03 1.78E01 2.27E01 pCi/g Cr51 10/15/13 U 6.11E02 5.97E01 8.47E01 pCi/g Mn54 10/15/13 U 3.89E03 2.04E02 3.16E02 pCi/g Fe59 10/15/13 U 6.00E02 7.76E02 1.36E01 pCi/g Co56 10/15/13 U 5.93E03 2.84E02 5.19E02 pCi/g Co57 10/15/13 UI 0.00E+00 2.79E02 2.22E02 pCi/g Co58 10/15/13 U 1.33E02 2.45E02 4.38E02 pCi/g Co60 10/15/13 3 7.64E01 5.60E02 2.58E02 pCi/g Zn65 10/15/13 U 2.11E02 4.38E02 8.40E02 pCi/g Y88 10/15/13 U 5.98E03 1.90E02 3.81E02 pCi/g Zr95 10/15/13 U 2.33E02 5.12E02 9.70E02 pCi/g Nb94 10/15/13 U 4.71E03 1.41E02 2.60E02 pCi/g Nb95 10/15/13 U 2.17E02 2.69E02 5.32E02 pCi/g Ru106 10/15/13 U 7.56E02 1.40E01 2.78E01 pCi/g Ag110m 10/15/13 U 3.51E03 2.88E02 4.48E02 pCi/g Sn113 10/15/13 U 1.07E02 2.41E02 4.48E02 pCi/g Sb124 10/15/13 U 5.20E04 4.99E02 9.69E02 pCi/g Sb125 10/15/13 U 2.29E02 3.60E02 6.55E02 pCi/g Cs134 10/15/13 U 1.17E02 1.81E02 3.52E02 pCi/g Cs136 10/15/13 U 1.47E01 4.58E01 8.42E01 pCi/g Cs137 10/15/13 U 5.95E03 1.42E02 2.74E02 1.00E01 pCi/g Ba133 10/15/13 U 1.75E02 1.86E02 2.85E02 pCi/g Ba140 10/15/13 U 9.56E02 1.15E+00 2.22E+00 pCi/g Ce139 10/15/13 U 8.92E05 1.39E02 2.72E02 pCi/g Ce141 10/15/13 UI 0.00E+00 2.71E01 1.13E01 pCi/g Ce144 10/15/13 U 1.52E02 8.26E02 1.63E01 pCi/g Nd147 10/15/13 U 5.98E01 3.50E+00 6.94E+00 pCi/g Pm144 10/15/13 3,U 1.71E02 1.50E02 3.05E02 pCi/g Pm146 10/15/13 U 5.12E03 1.76E02 3.39E02 pCi/g Eu152 10/15/13 UI 0.00E+00 8.83E02 9.50E02 pCi/g Eu154 10/15/13 U 1.10E02 3.75E02 6.87E02 pCi/g Eu155 10/15/13 U 2.99E02 3.91E02 8.23E02 pCi/g Ir192 10/15/13 U 5.55E03 2.39E02 3.97E02 pCi/g Hg203 10/15/13 U 2.28E02 5.15E02 5.47E02 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 55 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID: 334614018 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #4 Collect Date: August 16, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Geometry Received: Report Date: October 28, 2013 2

Analyte Run Date Qualifier Activity 2 Sigma 1 Uncertainty MDA RL Units Tl208 10/15/13 UI 0.00E+00 2.73E02 2.72E02 pCi/g Pb210 10/15/13 U 4.72E01 3.32E+00 2.92E+00 pCi/g Pb212 10/15/13 UI 0.00E+00 5.90E02 6.75E02 pCi/g Pb214 10/15/13 U 1.34E02 3.21E02 5.18E02 pCi/g Bi212 10/15/13 U 6.26E02 2.04E01 3.92E01 pCi/g Bi214 10/15/13 U 1.30E02 3.32E02 6.04E02 pCi/g Ra228 10/15/13 UI 0.00E+00 1.47E01 1.58E01 pCi/g Ac228 10/15/13 UI 0.00E+00 1.47E01 1.58E01 pCi/g Th234 10/15/13 U 1.74E01 5.54E01 1.12E+00 pCi/g U235 10/15/13 UI 0.00E+00 3.31E01 1.49E01 pCi/g U238 10/15/13 U 1.74E01 5.54E01 1.12E+00 pCi/g Np239 10/15/13 U 1.23E01 1.87E01 3.16E01 pCi/g Am241 10/15/13 U 2.29E02 5.93E02 1.15E01 pCi/g Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification Page 56 of 72

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID: 334614018 Client: TLG Services, Inc.

Client Sample ID: SU 1.2 #4 Collect Date: August 16, 2013 Matrix: Misc Solid Receive Date: October 03, 2013 Analyte Activity Units  % Abundance Gamma Spec Co60 7.64E01 pCi/g 100.000 Total Activity: 7.64E01 Total % Abundance: 100.00 Page 57 of 72

QC Summary Page 58 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: October 28, 2013 TLG Services, Inc. Page 1 of 8 148 New Milford Rd. East Bridgewater, Connecticut

Contact:

Mr. Jay Adler Workorder: 334614 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1336621 QC1202961675 334614002 DUP Actinium-228 1.47 1.16 pCi/g 23.6 * (0%-20%) MXR1 10/15/13 14:40 Uncertainty +/-0.217 +/-0.265 Americium-241 U 0.0677 U 0.0743 pCi/g N/A N/A Uncertainty +/-0.161 +/-0.0948 Antimony-124 U 0.0916 U -0.0372 pCi/g N/A N/A Uncertainty +/-0.104 +/-0.101 Antimony-125 U 0.0728 U 0.0329 pCi/g N/A N/A Uncertainty +/-0.0751 +/-0.0724 Barium-133 U -0.0127 U -0.00507 pCi/g N/A N/A Uncertainty +/-0.0377 +/-0.040 Barium-140 U 2.93 U -0.355 pCi/g N/A N/A Uncertainty +/-3.02 +/-3.14 Beryllium-7 U -0.132 U 0.274 pCi/g N/A N/A Uncertainty +/-0.460 +/-0.473 Bismuth-212 1.15 1.14 pCi/g 1.31 (0% - 100%)

Uncertainty +/-0.744 +/-0.743 Bismuth-214 1.11 1.24 pCi/g 10.9 (0%-20%)

Uncertainty +/-0.140 +/-0.136 Cerium-139 U -0.0155 U -0.0016 pCi/g N/A N/A Uncertainty +/-0.0301 +/-0.0297 Cerium-141 U 0.0525 U -0.11 pCi/g N/A N/A Uncertainty +/-0.157 +/-0.143 Cerium-144 U 0.0633 U 0.0983 pCi/g N/A N/A Uncertainty +/-0.183 +/-0.201 Cesium-134 UI 0.00 UI 0.00 pCi/g N/A N/A Uncertainty +/-0.0755 +/-0.0534 Cesium-136 U -0.318 U 0.153 pCi/g N/A N/A Uncertainty +/-0.968 +/-1.14 Cesium-137 U -0.00567 U -0.0226 pCi/g N/A N/A Uncertainty +/-0.0283 +/-0.0359 Chromium-51 U 0.152 U -0.615 pCi/g N/A N/A Uncertainty +/-1.03 +/-1.04 Cobalt-56 U -0.0171 U 0.00341 pCi/g N/A N/A Uncertainty +/-0.0482 +/-0.0555 Cobalt-57 UI 0.00 UI 0.00 pCi/g N/A N/A Uncertainty +/-0.0395 +/-0.0491 Cobalt-58 U -0.031 UI 0.00 pCi/g N/A N/A Uncertainty +/-0.0505 +/-0.152 Cobalt-60 0.107 0.0624 pCi/g 52.5 (0% - 100%)

Uncertainty +/-0.0489 +/-0.0536 Page 59 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 334614 Page 2 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1336621 Europium-152 0.615 0.660 pCi/g 7.00 (0% - 100%) MXR1 10/15/13 14:40 Uncertainty +/-0.123 +/-0.129 Europium-154 U -0.00225 U -0.0213 pCi/g N/A N/A Uncertainty +/-0.0935 +/-0.108 Europium-155 U 0.0282 U -0.00966 pCi/g N/A N/A Uncertainty +/-0.0883 +/-0.0843 Iridium-192 U -0.0215 U 0.0154 pCi/g N/A N/A Uncertainty +/-0.0414 +/-0.0456 Iron-59 U 0.0351 U -0.0141 pCi/g N/A N/A Uncertainty +/-0.184 +/-0.167 Lead-210 U 0.924 3.28 pCi/g 88.0 (0% - 100%)

Uncertainty +/-4.21 +/-2.90 Lead-212 1.44 1.43 pCi/g 0.418 (0%-20%)

Uncertainty +/-0.104 +/-0.104 Lead-214 1.53 1.48 pCi/g 3.20 (0%-20%)

Uncertainty +/-0.169 +/-0.131 Manganese-54 U 0.0234 U -0.00235 pCi/g N/A N/A Uncertainty +/-0.0354 +/-0.0343 Mercury-203 U 0.0752 U -0.0124 pCi/g N/A N/A Uncertainty +/-0.0679 +/-0.0731 Neodymium-147 U -2.34 U -6.01 pCi/g N/A N/A Uncertainty +/-8.44 +/-10.0 Neptunium-239 U -0.301 U -0.103 pCi/g N/A N/A Uncertainty +/-0.384 +/-0.367 Niobium-94 U 0.0128 U 0.000281 pCi/g N/A N/A Uncertainty +/-0.0265 +/-0.0298 Niobium-95 U -0.0271 U 0.0322 pCi/g N/A N/A Uncertainty +/-0.0724 +/-0.0669 Potassium-40 19.3 19.1 pCi/g 1.09 (0%-20%)

Uncertainty +/-1.32 +/-1.21 Promethium-144 U 0.00658 U 0.00715 pCi/g N/A N/A Uncertainty +/-0.0284 +/-0.0346 Promethium-146 U 0.0242 U -0.00326 pCi/g N/A N/A Uncertainty +/-0.0316 +/-0.0403 Radium-228 1.47 1.16 pCi/g 23.6 * (0%-20%)

Uncertainty +/-0.217 +/-0.265 Ruthenium-106 U 0.404 U -0.0578 pCi/g N/A N/A Uncertainty +/-0.540 +/-0.282 Silver-110m U -0.0459 U -0.0332 pCi/g N/A N/A Uncertainty +/-0.0422 +/-0.048 Sodium-22 U -0.000815 U -0.00734 pCi/g N/A N/A Uncertainty +/-0.0338 +/-0.039 Page 60 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 334614 Page 3 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1336621 Thallium-208 0.380 0.370 pCi/g 2.67 (0%-20%)

Uncertainty +/-0.0791 +/-0.0711 Thorium-234 3.86 2.78 pCi/g 32.4 (0% - 100%) MXR1 10/15/13 14:40 Uncertainty +/-2.39 +/-1.98 Tin-113 U -0.0113 U 0.00799 pCi/g N/A N/A Uncertainty +/-0.0487 +/-0.0477 Uranium-235 U 0.205 U 0.038 pCi/g N/A N/A Uncertainty +/-0.235 +/-0.163 Uranium-238 3.86 2.78 pCi/g 32.4 (0% - 100%)

Uncertainty +/-2.39 +/-1.98 Yttrium-88 U 0.00123 U -0.0103 pCi/g N/A N/A Uncertainty +/-0.0288 +/-0.0312 Zinc-65 U 0.0606 UI 0.00 pCi/g N/A N/A Uncertainty +/-0.142 +/-0.115 Zirconium-95 U 0.0596 U -0.0255 pCi/g N/A N/A Uncertainty +/-0.102 +/-0.110 QC1202961676 LCS Actinium-228 U 1.75 pCi/g 10/15/13 14:41 Uncertainty +/-2.44 Americium-241 491 565 pCi/g 115 (75%-125%)

Uncertainty +/-8.40 Antimony-124 U -0.19 pCi/g Uncertainty +/-0.438 Antimony-125 U -0.0307 pCi/g Uncertainty +/-1.25 Barium-133 U 0.0333 pCi/g Uncertainty +/-0.518 Barium-140 U -1.68 pCi/g Uncertainty +/-1.64 Beryllium-7 U -2.65 pCi/g Uncertainty +/-3.90 Bismuth-212 U 2.19 pCi/g Uncertainty +/-6.55 Bismuth-214 U -0.185 pCi/g Uncertainty +/-0.853 Cerium-139 2.40 pCi/g Uncertainty +/-0.415 Cerium-141 U 0.0139 pCi/g Uncertainty +/-0.400 Cerium-144 U 0.0487 pCi/g Uncertainty +/-1.93 Cesium-134 U 0.504 pCi/g Uncertainty +/-0.565 Cesium-136 U 0.0663 pCi/g Uncertainty Page 61 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 334614 Page 4 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1336621

+/-0.836 Cesium-137 192 184 pCi/g 95.8 (75%-125%) MXR1 10/15/13 14:41 Uncertainty +/-1.87 Chromium-51 U 1.21 pCi/g Uncertainty +/-3.13 Cobalt-56 U -0.59 pCi/g Uncertainty +/-0.547 Cobalt-57 15.7 pCi/g Uncertainty +/-0.540 Cobalt-58 U 0.266 pCi/g Uncertainty +/-0.507 Cobalt-60 237 220 pCi/g 92.8 (75%-125%)

Uncertainty +/-2.30 Europium-152 U 0.512 pCi/g Uncertainty +/-1.19 Europium-154 U 0.694 pCi/g Uncertainty +/-0.852 Europium-155 U -0.30 pCi/g Uncertainty +/-1.06 Iridium-192 U -0.399 pCi/g Uncertainty +/-0.369 Iron-59 U 0.625 pCi/g Uncertainty +/-1.19 Lead-210 5490 pCi/g Uncertainty +/-158 Lead-212 U 0.0886 pCi/g Uncertainty +/-0.596 Lead-214 U -0.419 pCi/g Uncertainty +/-0.894 Manganese-54 U -0.36 pCi/g Uncertainty +/-0.525 Mercury-203 U -0.181 pCi/g Uncertainty +/-0.345 Neodymium-147 U 2.18 pCi/g Uncertainty +/-3.14 Neptunium-239 U 0.640 pCi/g Uncertainty +/-4.42 Niobium-94 U 0.245 pCi/g Uncertainty +/-0.418 Niobium-95 U 0.0959 pCi/g Uncertainty +/-0.471 Potassium-40 U 0.221 pCi/g Uncertainty +/-2.04 Page 62 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 334614 Page 5 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1336621 Promethium-144 U -0.279 pCi/g Uncertainty +/-0.418 Promethium-146 U -0.37 pCi/g MXR1 10/15/13 14:41 Uncertainty +/-0.619 Radium-228 U 1.75 pCi/g Uncertainty +/-2.44 Ruthenium-106 U -4.38 pCi/g Uncertainty +/-4.61 Silver-110m U -0.124 pCi/g Uncertainty +/-0.821 Sodium-22 U 0.236 pCi/g Uncertainty +/-0.298 Thallium-208 U 0.0373 pCi/g Uncertainty +/-0.442 Thorium-234 U -43.9 pCi/g Uncertainty +/-20.6 Tin-113 1.33 pCi/g Uncertainty +/-0.694 Uranium-235 U 0.686 pCi/g Uncertainty +/-1.70 Uranium-238 U -43.9 pCi/g Uncertainty +/-20.6 Yttrium-88 1.38 pCi/g Uncertainty +/-0.451 Zinc-65 49.6 pCi/g Uncertainty +/-2.65 Zirconium-95 U 1.11 pCi/g Uncertainty +/-0.923 QC1202961674 MB Actinium-228 U -0.0156 pCi/g 10/15/13 14:39 Uncertainty +/-0.0512 Americium-241 U 0.0537 pCi/g Uncertainty +/-0.0799 Antimony-124 U 0.0076 pCi/g Uncertainty +/-0.0304 Antimony-125 U 0.0185 pCi/g Uncertainty +/-0.0288 Barium-133 U 0.0024 pCi/g Uncertainty +/-0.0156 Barium-140 U -0.0097 pCi/g Uncertainty +/-0.0396 Beryllium-7 U 0.00758 pCi/g Uncertainty +/-0.099 Bismuth-212 U 0.112 pCi/g Uncertainty Page 63 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 334614 Page 6 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1336621

+/-0.174 Bismuth-214 U -0.00775 pCi/g MXR1 10/15/13 14:39 Uncertainty +/-0.0271 Cerium-139 U 0.00151 pCi/g Uncertainty +/-0.00934 Cerium-141 U 0.00433 pCi/g Uncertainty +/-0.0367 Cerium-144 UI 0.00 pCi/g Uncertainty +/-0.129 Cesium-134 U -0.00466 pCi/g Uncertainty +/-0.0114 Cesium-136 U 0.00572 pCi/g Uncertainty +/-0.0177 Cesium-137 U 0.000936 pCi/g Uncertainty +/-0.0177 Chromium-51 U 0.00972 pCi/g Uncertainty +/-0.0838 Cobalt-56 U -0.00281 pCi/g Uncertainty +/-0.0109 Cobalt-57 U -0.0018 pCi/g Uncertainty +/-0.00747 Cobalt-58 U -0.00495 pCi/g Uncertainty +/-0.0111 Cobalt-60 U -0.0107 pCi/g Uncertainty +/-0.0147 Europium-152 U -0.0272 pCi/g Uncertainty +/-0.035 Europium-154 U -0.00512 pCi/g Uncertainty +/-0.0329 Europium-155 U -0.0181 pCi/g Uncertainty +/-0.0316 Iridium-192 U 0.00201 pCi/g Uncertainty +/-0.00978 Iron-59 U -0.00625 pCi/g Uncertainty +/-0.0252 Lead-210 U -1.72 pCi/g Uncertainty +/-3.08 Lead-212 U 0.0111 pCi/g Uncertainty +/-0.0409 Lead-214 U -0.0311 pCi/g Uncertainty +/-0.0306 Manganese-54 U 0.00843 pCi/g Uncertainty +/-0.0103 Page 64 of 72

GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 334614 Page 7 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Gamma Spec Batch 1336621 Mercury-203 U -0.00558 pCi/g Uncertainty +/-0.0115 Neodymium-147 U 0.0865 pCi/g MXR1 10/15/13 14:39 Uncertainty +/-0.130 Neptunium-239 U 0.00651 pCi/g Uncertainty +/-0.126 Niobium-94 U -0.0065 pCi/g Uncertainty +/-0.0126 Niobium-95 U 0.00527 pCi/g Uncertainty +/-0.0109 Potassium-40 U 0.140 pCi/g Uncertainty +/-0.159 Promethium-144 U -0.00589 pCi/g Uncertainty +/-0.014 Promethium-146 U 0.00216 pCi/g Uncertainty +/-0.0141 Radium-228 U -0.0156 pCi/g Uncertainty +/-0.0512 Ruthenium-106 U -0.0547 pCi/g Uncertainty +/-0.105 Silver-110m U -0.000892 pCi/g Uncertainty +/-0.0131 Sodium-22 U -0.000374 pCi/g Uncertainty +/-0.0112 Thallium-208 U 0.00121 pCi/g Uncertainty +/-0.0128 Thorium-234 U -0.141 pCi/g Uncertainty +/-0.704 Tin-113 U -0.00656 pCi/g Uncertainty +/-0.0137 Uranium-235 U 0.0184 pCi/g Uncertainty +/-0.156 Uranium-238 U -0.141 pCi/g Uncertainty +/-0.704 Yttrium-88 U 0.00392 pCi/g Uncertainty +/-0.0101 Zinc-65 U -0.00685 pCi/g Uncertainty +/-0.0257 Zirconium-95 U 0.000959 pCi/g Uncertainty +/-0.0188 Notes:

Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

The Qualifiers in this report are defined as follows:

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GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 334614 Page 8 of 8 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time

    • Analyte is a Tracer compound

< Result is less than value reported

> Result is greater than value reported BD Results are either below the MDC or tracer recovery is low FA Failed analysis.

H Analytical holding time was exceeded J Value is estimated K Analyte present. Reported value may be biased high. Actual value is expected to be lower.

L Analyte present. Reported value may be biased low. Actual value is expected to be higher.

M M if above MDC and less than LLD M REMP Result > MDC/CL and < RDL N/A RPD or %Recovery limits do not apply.

N1 See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.

R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification UJ Gamma Spectroscopy--Uncertain identification UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.

X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y Other specific qualifiers were required to properly define the results. Consult case narrative.

^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

  • Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 66 of 72

Chain of Custody Page 67 of 72

Page 68 of 72 Page 69 of 72 Page 70 of 72 Laboratory Certifications Page 71 of 72

List of current GEL Certifications as of 28 October 2013 State Certification Alaska UST110 Arkansas 880651 CLIA 42D0904046 California NELAP 01151CA Colorado SC00012 Connecticut PH0169 Delaware SC00012201310 DoD ELAP/ ISO17025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P3301200283, P3301200284 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012201310 Idaho Chemistry SC00012 Idaho Radiochemistry SC00012 Illinois NELAP 200029 Indiana CSC01 Kansas NELAP E10332 Kentucky 90129 Louisiana NELAP 03046 (AI33904)

Louisiana SDWA LA130005 Maryland 270 Massachusetts MSC012 Michigan 9976 Mississippi SC00012201310 Nebraska NEOS2613 Nevada SC0001220132 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 Oklahoma 9904 Pennsylvania NELAP 6800485 Plant Material Permit PDEP1200260 South Carolina Chemistry 10120001 South Carolina GVL 23611001 South Carolina Radiochemi 10120002 Tennessee TN 02934 Texas NELAP T104704235138 Utah NELAP SC00012201310 Vermont VT87156 Virginia NELAP 460202 Washington C78012 Wisconsin 999887790 Page 72 of 72

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