ML14080A196
| ML14080A196 | |
| Person / Time | |
|---|---|
| Site: | 05000134 |
| Issue date: | 10/28/2013 |
| From: | Trent E GEL Labs |
| To: | James Adler NRC/FSME, TLG Services |
| References | |
| 334614 | |
| Download: ML14080A196 (72) | |
Text
October 28, 2013 Mr. Jay Adler TLG Services, Inc.
148 New Milford Rd. East Bridgewater, Connecticut 06752 Re: Radiochemistry Analysis Work Order: 334614
Dear Mr. Adler:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on October 03, 2013. This original data report has been prepared and reviewed in accordance with GELs standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.
Sincerely, PM_SIGN_HERE Erin Trent Project Manager Purchase Order: Signed Quote GELP13-1296 Enclosures Page 1 of 72
Certificate of Analysis Page 2 of 72
Reviewed by USER_SIGN_HERE GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Certificate of Analysis Report TLGS001 TLG Services, Inc.
Client SDG: 334614 GEL Work Order: 334614 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the U qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Erin Trent.
The Qualifiers in this report are defined as follows:
- A quality control analyte recovery is outside of specified acceptance criteria
- Analyte is a Tracer compound
UI Gamma SpectroscopyUncertain identification for Page 3 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614001 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #1 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 1.62E01 3.43E02 2.43E+01 9.19E02 1.08E02 7.17E02 4.36E02 0.00E+00 1.64E02 1.71E01 3.71E03 2.50E02 1.19E01 8.56E03 3.94E02 2.05E01 2.25E02 2.08E03 1.05E02 4.06E03 0.00E+00 1.13E+00 9.56E03 2.15E02 1.14E+00 1.05E02 6.51E02 2.31E03 1.12E+01 4.34E03 3.74E03 5.53E01 9.50E02 3.99E02 3.10E02 1.68E02 5.69E01 3.85E02 1.50E+00 1.14E+00 4.16E02 1.73E01 5.63E02 5.42E02 5.57E02 7.30E02 1.81E01 3.64E02 1.97E01 3.12E02 7.30E02 3.11E01 5.52E02 5.77E02 8.41E02 8.66E02 6.41E02 1.27E+00 3.35E02 4.13E02 3.33E+00 3.72E02 1.81E01 2.62E01 1.11E+01 3.36E02 4.02E02 1.53E01 1.06E01 1.17E01 5.07E02 8.79E02 1.04E+00 7.93E02 5.73E01 2.10E+00 7.75E02 3.02E01 9.72E02 7.24E02 1.06E01 6.11E02 1.86E01 6.24E02 2.00E01 5.88E02 1.23E01 5.82E01 1.04E01 1.05E01 1.77E01 1.56E01 9.50E02 2.47E+00 6.36E02 6.91E02 6.11E+00 6.42E02 3.23E01 4.12E01 2.11E+01 6.30E02 7.28E02 1.75E01 1.90E01 2.12E01 8.99E02 1.43E01 1.00E01 U
U 3
U U
U U
UI U
3 U
U U
U U
U U
U U
U UI U
U U
U U
U U
3,U U
U 3
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 4 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614001 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #1 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 5.27E01 3.60E01 1.82E+00 1.73E+00 1.31E+00 1.27E+00 1.58E+00 1.58E+00 3.27E+00 2.05E01 3.27E+00 3.56E01 1.49E01 7.87E02 7.92E+00 1.25E01 1.74E01 7.58E01 1.66E01 2.98E01 2.98E01 2.89E+00 2.12E01 2.89E+00 4.68E01 2.48E01 6.26E02 1.46E+01 1.00E01 1.24E01 8.31E01 1.17E01 2.39E01 2.39E01 3.20E+00 3.84E01 3.20E+00 7.72E01 4.22E01 3
U 3
3 3
3 3
3 3
U 3
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 5 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614001 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #1 Analyte Activity Gamma Spec Ac228 Bi212 Bi214 Co60 Eu152 Pb212 Pb214 K40 Ra228 Tl208 Th234 U238 1.58E+00 1.31E+00 1.27E+00 1.71E01 5.53E01 1.82E+00 1.73E+00 2.43E+01 1.58E+00 5.27E01 3.27E+00 3.27E+00 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 003.816 003.165 003.073 000.415 001.339 004.401 004.183 058.699 003.816 001.276 007.910 007.910 Total Activity:
4.13E+01 Total % Abundance:
100.00 Page 6 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614002 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #2 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 1.32E01 8.15E04 1.93E+01 1.52E01 2.34E02 3.51E02 1.71E02 0.00E+00 3.10E02 1.07E01 6.06E02 1.23E03 5.96E02 1.28E02 2.71E02 4.04E01 4.59E02 1.13E02 9.16E02 7.28E02 0.00E+00 3.18E01 5.67E03 1.27E02 2.93E+00 1.55E02 5.25E02 6.33E02 2.34E+00 6.58E03 2.42E02 6.15E01 2.25E03 2.82E02 2.15E02 7.52E02 4.60E01 3.38E02 1.32E+00 1.03E+00 3.54E02 1.84E01 4.82E02 3.95E02 5.05E02 4.89E02 1.42E01 2.88E02 1.02E01 2.65E02 7.24E02 5.40E01 4.22E02 4.87E02 1.04E01 7.51E02 7.55E02 9.68E01 2.83E02 3.77E02 3.02E+00 3.01E02 1.57E01 1.83E01 8.44E+00 2.84E02 3.16E02 1.23E01 9.35E02 8.83E02 4.14E02 6.79E02 8.30E01 6.12E02 5.14E01 1.74E+00 6.85E02 2.96E01 8.72E02 6.80E02 8.96E02 5.39E02 1.63E01 5.87E02 1.97E01 5.15E02 1.14E01 5.04E01 7.07E02 8.92E02 2.30E01 1.47E01 7.67E02 1.73E+00 5.00E02 6.04E02 5.86E+00 5.38E02 2.63E01 3.30E01 1.51E+01 5.45E02 6.16E02 1.47E01 1.69E01 1.68E01 7.60E02 1.22E01 1.00E01 U
U 3
U U
U U
UI U
3 U
U U
U U
U U
U U
U UI U
U U
U U
U U
U U
U 3
U U
U 3,U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 7 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614002 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #2 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 3.80E01 9.24E01 1.44E+00 1.53E+00 1.15E+00 1.11E+00 1.47E+00 1.47E+00 3.86E+00 2.05E01 3.86E+00 3.01E01 6.77E02 7.91E02 4.21E+00 1.04E01 1.69E01 7.44E01 1.40E01 2.17E01 2.17E01 2.39E+00 2.35E01 2.39E+00 3.84E01 1.61E01 4.87E02 8.44E+00 8.78E02 2.67E01 7.21E01 1.04E01 1.94E01 1.94E01 2.30E+00 2.83E01 2.30E+00 6.13E01 2.90E01 3
U 3
3 3
3 3
3 3
U 3
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 8 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614002 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #2 Analyte Activity Gamma Spec Ac228 Bi212 Bi214 Co60 Eu152 Pb212 Pb214 K40 Ra228 Tl208 Th234 U238 1.47E+00 1.15E+00 1.11E+00 1.07E01 6.15E01 1.44E+00 1.53E+00 1.93E+01 1.47E+00 3.80E01 3.86E+00 3.86E+00 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 004.036 003.176 003.055 000.294 001.695 003.964 004.201 053.251 004.036 001.046 010.623 010.623 Total Activity:
3.63E+01 Total % Abundance:
100.00 Page 9 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614003 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #3 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 4.44E01 1.85E02 2.17E+01 4.53E01 7.01E02 3.85E02 5.23E02 4.44E03 8.58E02 0.00E+00 1.25E01 2.87E04 2.24E02 1.07E02 5.80E02 3.77E01 1.93E02 5.69E02 5.44E02 1.15E02 0.00E+00 1.19E+00 4.10E02 4.08E02 3.57E+00 5.20E03 1.31E01 1.07E01 1.11E+00 7.13E03 3.47E02 9.11E01 4.68E02 2.10E01 2.31E02 3.39E02 6.79E01 4.93E02 1.58E+00 1.74E+00 6.56E02 2.48E01 7.56E02 9.30E02 7.42E02 6.20E02 2.27E01 4.98E02 1.45E01 4.82E02 9.29E02 4.30E01 6.85E02 6.72E02 1.25E01 1.06E01 8.16E02 1.33E+00 4.56E02 6.40E02 4.24E+00 4.21E02 2.14E01 2.51E01 1.52E+01 7.56E02 4.62E02 1.99E01 1.36E01 1.35E01 6.48E02 9.29E02 1.30E+00 9.21E02 6.63E01 2.63E+00 8.99E02 3.78E01 1.46E01 6.13E02 1.48E01 1.30E01 2.46E01 9.66E02 2.61E01 7.56E02 1.70E01 7.36E01 1.29E01 1.19E01 2.27E01 1.95E01 7.70E02 2.65E+00 7.64E02 8.89E02 7.28E+00 7.72E02 3.61E01 4.61E01 2.40E+01 7.57E02 8.92E02 2.19E01 2.53E01 2.51E01 1.17E01 1.69E01 1.00E01 U
U 3
U 3,U U
U U
3,U UI U
U U
U U
U U
U U
U UI U
U U
U U
U U
U U
U 3
U 3,U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 10 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614003 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #3 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 5.17E01 3.02E+00 1.85E+00 1.75E+00 2.59E+00 1.53E+00 1.48E+00 1.48E+00 2.24E+00 2.74E02 2.24E+00 2.08E01 4.62E01 9.97E02 8.24E+00 1.39E01 2.05E01 9.23E01 1.61E01 3.20E01 3.20E01 3.45E+00 3.04E01 3.45E+00 5.19E01 2.61E01 7.33E02 1.53E+01 1.16E01 1.60E01 9.89E01 1.43E01 2.98E01 2.98E01 3.48E+00 4.05E01 3.48E+00 8.45E01 4.62E01 3
U 3
3 3
3 3
3 U
U U
U 3,U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 11 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614003 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #3 Analyte Activity Gamma Spec Ac228 Bi212 Bi214 Eu152 Pb212 Pb214 K40 Ra228 Tl208 1.48E+00 2.59E+00 1.53E+00 9.11E01 1.85E+00 1.75E+00 2.17E+01 1.48E+00 5.17E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 004.366 007.679 004.526 002.696 005.474 005.183 064.179 004.366 001.529 Total Activity:
3.38E+01 Total % Abundance:
100.00 Page 12 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614004 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #4 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.94E01 5.99E03 2.36E+01 8.53E02 1.84E02 2.37E01 9.52E03 0.00E+00 4.52E02 1.43E01 1.09E01 5.43E03 5.68E03 5.00E03 8.54E03 4.15E02 3.18E02 4.02E03 5.99E02 1.75E02 0.00E+00 1.03E+00 2.62E03 5.05E04 1.20E+00 6.10E03 2.14E01 6.86E03 4.22E+00 3.70E02 6.30E04 9.51E01 7.61E03 2.08E01 2.62E02 1.05E01 6.34E01 5.24E02 1.57E+00 1.21E+00 4.52E02 2.03E01 6.07E02 6.38E02 6.10E02 5.44E02 1.78E01 4.07E02 1.25E01 4.13E02 8.69E02 3.42E01 6.08E02 6.33E02 1.28E01 1.01E01 5.65E02 1.32E+00 4.40E02 4.68E02 3.47E+00 3.94E02 1.80E01 2.58E01 1.19E+01 4.37E02 4.35E02 1.71E01 1.44E01 1.80E01 5.85E02 9.09E02 1.09E+00 8.50E02 5.31E01 2.19E+00 8.41E02 3.23E01 1.12E01 8.73E02 1.18E01 7.97E02 2.07E01 7.76E02 2.30E01 6.13E02 1.38E01 6.29E01 1.06E01 1.13E01 2.65E01 1.82E01 9.43E02 2.19E+00 7.13E02 7.43E02 6.00E+00 6.94E02 3.31E01 4.07E01 2.05E+01 7.56E02 7.79E02 1.98E01 2.32E01 2.11E01 9.71E02 1.56E01 1.00E01 U
U 3
U U
U U
UI U
3 U
U U
U U
U U
U U
U UI U
U U
U U
3,U U
U U
U 3
U 3,U U
3,U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 13 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614004 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #4 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 5.44E01 1.03E+01 1.77E+00 1.84E+00 1.92E+00 1.41E+00 1.94E+00 1.94E+00 1.64E+00 1.05E01 1.64E+00 9.05E02 4.45E02 8.14E02 1.59E+01 1.29E01 1.75E01 1.05E+00 1.84E01 3.12E01 3.12E01 3.24E+00 2.18E01 3.24E+00 5.02E01 3.25E01 6.54E02 1.45E+01 1.12E01 3.26E01 9.21E01 1.37E01 2.55E01 2.55E01 3.47E+00 3.76E01 3.47E+00 7.89E01 4.30E01 3
U 3
3 3
3 3
3 U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 14 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614004 Soil TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.6 #4 Analyte Activity Gamma Spec Ac228 Bi212 Bi214 Co60 Eu152 Pb212 Pb214 K40 Ra228 Tl208 1.94E+00 1.92E+00 1.41E+00 1.43E01 9.51E01 1.77E+00 1.84E+00 2.36E+01 1.94E+00 5.44E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 005.372 005.322 003.897 000.397 002.635 004.915 005.106 065.475 005.372 001.509 Total Activity:
3.61E+01 Total % Abundance:
100.00 Page 15 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614005 Misc Solid TLG Services, Inc.
August 22, 2013 October 03, 2013 SU 1.3 #1 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 3.46E01 1.56E02 1.61E+01 4.05E01 2.13E02 7.76E02 5.33E04 0.00E+00 1.04E02 1.21E01 1.33E01 2.39E02 7.28E03 6.31E03 2.34E02 2.63E01 3.91E02 8.30E03 9.34E02 5.48E02 6.27E02 1.83E01 2.93E02 5.23E02 1.93E+00 1.60E02 5.80E02 1.19E02 1.91E+00 9.90E03 2.86E03 9.14E01 4.34E02 5.21E02 1.06E02 5.61E04 4.87E01 5.12E02 1.32E+00 8.44E01 3.54E02 1.59E01 6.42E02 4.14E02 4.74E02 5.22E02 1.62E01 4.06E02 1.08E01 3.21E02 7.11E02 3.11E01 5.49E02 4.91E02 9.99E02 8.39E02 4.19E02 7.47E01 3.53E02 6.42E02 1.96E+00 3.05E02 1.28E01 2.10E01 5.78E+00 3.93E02 4.13E02 1.76E01 1.42E01 9.20E02 4.53E02 6.34E02 9.55E01 8.42E02 4.91E01 1.49E+00 6.15E02 2.80E01 9.97E02 7.71E02 8.49E02 5.89E02 1.99E01 8.94E02 1.95E01 5.93E02 1.07E01 6.13E01 9.15E02 8.95E02 1.61E01 1.58E01 8.51E02 1.43E+00 6.02E02 7.07E02 3.36E+00 5.60E02 2.30E01 3.31E01 1.05E+01 7.25E02 7.25E02 1.65E01 2.34E01 1.70E01 8.36E02 1.16E01 1.00E01 U
U 3
U U
U U
UI U
3 U
U U
U U
U U
U U
U 3,U U
U U
U U
U U
U U
U 3
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 16 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614005 Misc Solid TLG Services, Inc.
August 22, 2013 October 03, 2013 SU 1.3 #1 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.68E01 1.23E+00 9.24E01 8.45E01 1.52E+00 5.27E01 8.00E01 8.00E01 9.77E01 6.62E02 9.77E01 2.28E01 6.19E02 6.79E02 7.64E+00 1.03E01 1.18E01 9.54E01 1.21E01 2.42E01 2.42E01 1.89E+00 1.86E01 1.89E+00 4.18E01 1.46E01 5.61E02 6.55E+00 9.86E02 1.07E01 8.54E01 1.09E01 2.20E01 2.20E01 2.07E+00 3.26E01 2.07E+00 6.43E01 2.51E01 3
U 3
3 3
3 3
3 U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 17 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614005 Misc Solid TLG Services, Inc.
August 22, 2013 October 03, 2013 SU 1.3 #1 015cm Analyte Activity Gamma Spec Ac228 Bi212 Bi214 Co60 Eu152 Pb212 Pb214 K40 Ra228 Tl208 8.00E01 1.52E+00 5.27E01 1.21E01 9.14E01 9.24E01 8.45E01 1.61E+01 8.00E01 2.68E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 003.506 006.665 002.310 000.529 004.007 004.049 003.704 070.551 003.506 001.173 Total Activity:
2.28E+01 Total % Abundance:
100.00 Page 18 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614006 Misc Solid TLG Services, Inc.
August 22, 2013 October 03, 2013 SU 1.3 #3 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 1.31E01 7.24E03 1.37E+01 3.31E01 2.91E02 7.94E02 1.21E02 0.00E+00 6.72E02 1.69E01 1.08E01 8.52E04 5.17E02 2.50E02 3.07E02 1.56E01 2.30E02 1.76E02 3.41E02 4.47E02 0.00E+00 2.08E01 1.97E02 9.83E03 6.31E01 4.82E03 1.09E02 6.56E02 1.22E+00 7.24E03 1.05E02 8.80E01 1.91E02 2.52E02 1.72E02 1.09E04 4.00E01 3.58E02 1.09E+00 7.29E01 3.65E02 1.52E01 4.27E02 6.50E02 9.01E02 5.41E02 8.33E02 3.07E02 9.43E02 2.97E02 5.20E02 2.68E01 4.48E02 4.20E02 7.99E02 6.90E02 5.45E02 6.65E01 3.21E02 3.69E02 1.82E+00 2.55E02 1.03E01 1.81E01 5.20E+00 3.42E02 3.75E02 1.53E01 9.93E02 7.57E02 3.67E02 5.24E02 7.29E01 6.81E02 4.48E01 1.36E+00 6.37E02 2.20E01 8.18E02 3.91E02 8.04E02 5.97E02 1.66E01 6.07E02 1.76E01 5.07E02 1.01E01 5.10E01 7.98E02 7.73E02 1.70E01 1.24E01 8.05E02 1.25E+00 5.42E02 5.71E02 3.22E+00 4.86E02 1.92E01 2.81E01 9.46E+00 5.45E02 5.93E02 1.41E01 1.89E01 1.36E01 6.86E02 9.57E02 1.00E01 U
U 3
U U
U U
UI U
3 3,U U
U U
U U
U U
U U
UI U
U U
U U
U U
U U
U 3
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 19 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614006 Misc Solid TLG Services, Inc.
August 22, 2013 October 03, 2013 SU 1.3 #3 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.50E01 2.75E+00 9.00E01 7.12E01 0.00E+00 7.11E01 6.79E01 6.79E01 0.00E+00 1.52E02 0.00E+00 2.22E01 2.35E02 6.01E02 2.61E+00 1.05E01 1.40E01 7.76E01 1.08E01 2.55E01 2.55E01 1.86E+00 1.42E01 1.86E+00 3.61E01 8.03E02 5.37E02 2.21E+00 8.85E02 1.02E01 9.75E01 1.06E01 2.11E01 2.11E01 1.20E+00 2.66E01 1.20E+00 5.56E01 1.38E01 3
3 3
3 UI 3
3 3
UI U
UI U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 20 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614006 Misc Solid TLG Services, Inc.
August 22, 2013 October 03, 2013 SU 1.3 #3 015cm Analyte Activity Gamma Spec Ac228 Bi214 Co60 Eu152 Pb210 Pb212 Pb214 K40 Ra228 Tl208 6.79E01 7.11E01 1.69E01 8.80E01 2.75E+00 9.00E01 7.12E01 1.37E+01 6.79E01 2.50E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 003.164 003.312 000.787 004.100 012.792 004.194 003.315 064.006 003.164 001.165 Total Activity:
2.15E+01 Total % Abundance:
100.00 Page 21 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614007 Misc Solid TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.4 #1 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 3.61E01 4.54E03 1.46E+01 5.55E01 5.68E03 1.11E01 1.25E02 6.43E03 4.25E02 3.28E02 2.68E02 2.05E02 2.23E02 4.53E03 3.41E02 1.58E01 3.48E03 1.15E02 3.31E02 1.54E03 3.89E02 2.55E01 5.03E03 6.22E03 1.55E01 6.86E03 5.95E02 1.11E01 2.73E+00 3.95E02 2.47E05 6.88E03 1.31E02 9.50E02 8.99E03 6.08E02 4.34E01 3.31E02 1.20E+00 8.95E01 3.27E02 1.72E01 4.63E02 2.16E02 5.31E02 3.01E02 8.47E02 3.53E02 9.00E02 2.53E02 6.01E02 2.46E01 4.30E02 4.67E02 6.35E02 7.40E02 3.30E02 9.72E01 3.02E02 3.38E02 2.49E+00 2.92E02 1.46E01 1.65E01 7.41E+00 3.09E02 3.28E02 7.57E02 9.14E02 7.67E02 4.06E02 5.90E02 8.36E01 5.29E02 4.59E01 1.70E+00 6.07E02 2.37E01 8.73E02 3.90E02 7.42E02 6.41E02 1.31E01 6.01E02 1.70E01 4.74E02 1.03E01 4.05E01 7.97E02 8.27E02 1.14E01 1.31E01 6.69E02 1.72E+00 5.63E02 5.50E02 4.45E+00 5.03E02 2.34E01 3.01E01 1.39E+01 5.07E02 5.89E02 1.23E01 1.46E01 1.46E01 7.50E02 1.14E01 1.00E01 U
U 3
U U
U U
U U
3,U U
U U
U U
U U
U U
U 3,U U
U U
U U
U U
U U
U U
U 3,U U
3,U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 22 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614007 Misc Solid TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.4 #1 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.77E01 8.62E01 8.89E01 7.55E01 0.00E+00 7.83E01 9.01E01 9.01E01 2.13E+00 5.27E02 2.13E+00 3.32E03 5.96E02 5.96E02 2.12E+00 8.31E02 1.28E01 5.94E01 1.02E01 2.06E01 2.06E01 1.98E+00 2.15E01 1.98E+00 2.94E01 1.04E01 4.26E02 4.00E+00 7.14E02 9.03E02 9.82E01 9.36E02 2.09E01 2.09E01 1.53E+00 2.54E01 1.53E+00 5.00E01 1.78E01 3
U 3
3 UI 3
3 3
3 U
3 U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 23 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614007 Misc Solid TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.4 #1 015cm Analyte Activity Gamma Spec Ac228 Bi214 Pb212 Pb214 K40 Ra228 Tl208 Th234 U238 9.01E01 7.83E01 8.89E01 7.55E01 1.46E+01 9.01E01 2.77E01 2.13E+00 2.13E+00 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 003.860 003.356 003.810 003.235 062.451 003.860 001.186 009.121 009.121 Total Activity:
2.33E+01 Total % Abundance:
100.00 Page 24 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614008 Misc Solid TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.4 #2 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 4.52E02 1.60E02 1.51E+01 9.07E02 3.11E02 4.41E02 1.74E02 7.76E03 3.09E02 6.78E03 1.14E02 1.26E02 4.85E02 2.56E03 3.49E02 1.02E01 2.67E02 1.57E02 1.18E02 4.99E02 2.66E02 5.05E01 1.96E03 1.72E02 1.30E01 9.68E03 1.30E01 7.85E02 3.93E01 1.81E02 4.40E03 2.19E02 4.42E02 4.37E02 2.08E02 8.02E02 3.30E01 2.90E02 8.55E01 8.03E01 2.49E02 9.77E02 3.55E02 1.81E02 3.48E02 2.24E02 6.68E02 2.53E02 6.92E02 1.85E02 4.67E02 2.07E01 3.13E02 3.50E02 7.14E02 5.54E02 3.26E02 7.03E01 2.19E02 2.94E02 1.94E+00 2.48E02 1.12E01 1.64E01 6.53E+00 2.11E02 2.43E02 8.36E02 8.03E02 7.07E02 3.28E02 9.82E02 5.93E01 4.95E02 3.01E01 1.38E+00 4.84E02 1.73E01 5.66E02 3.46E02 5.88E02 4.19E02 1.02E01 3.91E02 1.20E01 3.41E02 7.77E02 3.94E01 6.02E02 6.26E02 1.33E01 9.54E02 5.17E02 1.23E+00 4.05E02 4.89E02 3.63E+00 4.62E02 2.17E01 2.75E01 1.22E+01 3.65E02 4.37E02 1.09E01 1.27E01 1.31E01 6.28E02 8.77E02 1.00E01 U
U 3
U 3,U U
U U
U U
U U
U U
U U
U U
U U
U U
U U
U U
3,U U
U U
U U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 25 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614008 Misc Solid TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.4 #2 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 3.08E01 4.48E+00 1.07E+00 7.63E01 0.00E+00 6.32E01 8.30E01 8.30E01 1.35E+00 7.98E02 1.35E+00 2.58E01 2.83E02 4.39E02 5.37E+00 7.72E02 1.06E01 4.68E01 1.05E01 1.87E01 1.87E01 1.58E+00 1.31E01 1.58E+00 2.56E01 1.21E01 3.62E02 4.71E+00 6.33E02 8.27E02 6.87E01 7.23E02 1.38E01 1.38E01 1.66E+00 2.48E01 1.66E+00 4.65E01 1.99E01 3
U 3
3 UI 3
3 3
U U
U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 26 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614008 Misc Solid TLG Services, Inc.
August 13, 2013 October 03, 2013 SU 1.4 #2 015cm Analyte Activity Gamma Spec Ac228 Bi214 Pb212 Pb214 K40 Ra228 Tl208 8.30E01 6.32E01 1.07E+00 7.63E01 1.51E+01 8.30E01 3.08E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 004.256 003.240 005.499 003.916 077.254 004.256 001.579 Total Activity:
1.95E+01 Total % Abundance:
100.00 Page 27 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614009 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.4 #3 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 1.48E01 3.06E02 1.41E+01 5.42E04 5.13E03 9.78E02 1.06E02 0.00E+00 4.90E03 3.44E01 8.08E02 1.58E02 5.63E02 1.27E02 1.37E02 0.00E+00 1.47E02 2.59E02 3.05E02 2.62E03 6.91E02 2.83E01 4.61E03 4.02E03 1.42E01 9.19E03 8.85E02 6.33E02 7.65E+00 2.41E02 2.19E02 8.50E01 8.25E02 9.75E02 5.42E03 6.94E02 4.64E01 3.66E02 1.12E+00 9.72E01 3.54E02 1.42E01 5.16E02 7.14E02 5.27E02 6.34E02 1.48E01 3.04E02 1.24E01 2.88E02 7.08E02 2.87E01 4.69E02 4.90E02 1.00E01 7.46E02 3.93E02 9.76E01 3.02E02 3.99E02 2.46E+00 2.82E02 1.28E01 2.50E01 8.20E+00 3.03E02 3.29E02 1.59E01 1.01E01 1.32E01 4.29E02 7.09E02 8.76E01 7.22E02 4.99E01 1.73E+00 6.42E02 2.49E01 8.92E02 4.07E02 9.41E02 5.65E02 1.68E01 6.62E02 2.02E01 4.77E02 1.12E01 4.84E01 8.66E02 8.92E02 1.83E01 1.31E01 6.99E02 1.87E+00 5.38E02 6.22E02 4.58E+00 5.23E02 2.41E01 2.87E01 1.41E+01 5.17E02 6.36E02 1.43E01 1.99E01 1.49E01 7.70E02 1.19E01 1.00E01 U
U 3
U U
U U
UI U
3 U
U U
U U
UI U
U U
U 3,U U
U U
U U
U U
U U
U 3
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 28 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614009 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.4 #3 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.64E01 2.68E+00 1.09E+00 7.81E01 7.49E01 6.83E01 1.11E+00 1.11E+00 1.64E+00 6.39E02 1.64E+00 1.96E01 5.35E02 6.71E02 1.49E+00 9.25E02 1.23E01 6.42E01 1.16E01 2.34E01 2.34E01 1.54E+00 1.56E01 1.54E+00 3.57E01 8.16E02 5.18E02 1.91E+00 7.82E02 2.04E01 9.57E01 1.15E01 2.07E01 2.07E01 1.22E+00 2.84E01 1.22E+00 5.66E01 1.34E01 3
3 3
3 3,U 3
3 3
3 U
3 U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 29 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614009 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.4 #3 015cm Analyte Activity Gamma Spec Ac228 Bi214 Co60 Eu152 Pb210 Pb212 Pb214 K40 Ra228 Tl208 Th234 U238 1.11E+00 6.83E01 3.44E01 8.50E01 2.68E+00 1.09E+00 7.81E01 1.41E+01 1.11E+00 2.64E01 1.64E+00 1.64E+00 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 004.215 002.598 001.310 003.234 010.192 004.162 002.972 053.603 004.215 001.006 006.247 006.247 Total Activity:
2.63E+01 Total % Abundance:
100.00 Page 30 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614010 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.4 #4 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.32E01 1.59E02 1.58E+01 2.68E01 2.03E02 8.03E02 2.64E02 1.24E02 1.10E02 1.58E02 2.33E02 4.48E03 4.35E02 3.08E02 1.98E02 3.16E02 3.78E02 8.03E03 3.15E02 2.61E03 0.00E+00 6.14E02 2.96E03 3.27E02 1.16E+00 2.59E02 1.21E01 5.19E03 3.00E+00 5.04E03 2.88E02 2.40E02 5.68E02 4.53E02 2.44E02 7.20E02 4.06E01 2.71E02 1.17E+00 8.59E01 2.76E02 1.35E01 4.20E02 1.97E02 4.16E02 3.30E02 8.13E02 2.85E02 8.97E02 2.32E02 5.61E02 2.78E01 3.77E02 4.13E02 1.13E01 5.96E02 3.01E02 8.10E01 2.82E02 3.43E02 2.14E+00 2.49E02 1.86E01 1.66E01 6.96E+00 2.71E02 5.17E02 7.33E02 7.60E02 7.89E02 3.81E02 6.08E02 7.98E01 4.62E02 5.06E01 1.54E+00 5.36E02 1.99E01 7.17E02 3.68E02 7.43E02 5.65E02 1.34E01 5.57E02 1.70E01 4.71E02 9.20E02 4.41E01 6.13E02 7.60E02 2.01E01 1.14E01 5.22E02 1.54E+00 5.29E02 5.43E02 4.21E+00 4.96E02 2.10E01 2.84E01 1.27E+01 4.90E02 5.73E02 1.20E01 1.27E01 1.33E01 7.27E02 1.07E01 1.00E01 U
U 3
U U
U U
U U
U U
U U
3,U U
U U
U U
U UI U
U U
U 3,U U
U U
U U
U U
U U
3,U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 31 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614010 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.4 #4 015cm Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.48E01 4.70E+00 9.86E01 7.77E01 1.09E+00 5.78E01 7.70E01 7.70E01 3.03E01 2.50E01 3.03E01 2.31E01 1.40E02 4.64E02 5.10E+00 8.69E02 9.89E02 4.92E01 1.27E01 1.77E01 1.77E01 9.23E01 2.08E01 9.23E01 3.17E01 1.07E01 4.00E02 4.80E+00 6.97E02 1.89E01 7.00E01 8.49E02 1.75E01 1.75E01 1.71E+00 2.65E01 1.71E+00 4.85E01 2.01E01 3
U 3
3 3
3 3
3 U
3,U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 32 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614010 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.4 #4 015cm Analyte Activity Gamma Spec Ac228 Bi212 Bi214 Pb212 Pb214 K40 Ra228 Tl208 7.70E01 1.09E+00 5.78E01 9.86E01 7.77E01 1.58E+01 7.70E01 2.48E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units
% Abundance 003.667 005.200 002.751 004.693 003.701 075.140 003.667 001.180 Total Activity:
2.10E+01 Total % Abundance:
100.00 Page 33 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614011 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #1 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.18E01 1.34E02 1.17E01 5.27E02 9.65E03 1.35E02 2.36E02 1.32E03 2.49E02 2.45E02 7.23E02 1.87E02 1.35E02 2.19E02 4.26E02 1.41E01 4.14E02 4.19E02 9.05E03 1.00E02 1.02E02 1.52E01 4.25E03 1.29E02 1.37E+00 1.64E02 1.99E02 8.90E02 7.03E+00 7.22E03 3.17E04 2.55E02 4.91E02 8.88E03 3.57E03 7.09E03 4.30E01 3.12E02 4.51E01 8.32E01 2.99E02 1.18E01 5.00E02 1.64E02 4.77E02 4.56E02 7.76E02 4.99E02 8.63E02 2.77E02 5.05E02 2.64E01 3.67E02 4.07E02 1.27E01 6.85E02 3.66E02 8.71E01 3.24E02 3.24E02 2.39E+00 2.66E02 1.33E01 1.32E01 7.60E+00 3.09E02 3.32E02 7.28E02 8.91E02 6.12E02 4.25E02 5.52E02 7.86E01 5.48E02 7.41E01 1.48E+00 5.19E02 2.27E01 8.47E02 2.86E02 8.09E02 6.08E02 1.28E01 9.02E02 1.59E01 5.29E02 9.85E02 4.56E01 7.71E02 6.53E02 2.52E01 1.22E01 5.47E02 1.61E+00 5.01E02 5.52E02 4.40E+00 3.82E02 1.60E01 2.17E01 1.44E+01 5.66E02 5.79E02 1.31E01 1.53E01 1.08E01 6.70E02 9.05E02 1.00E01 U
U U
U U
U U
U U
U U
U U
U U
U 3,U U
U U
U U
U U
U U
U U
U U
U U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 34 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614011 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #1 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 8.53E03 1.19E+00 1.57E02 6.33E02 2.42E01 1.27E02 1.76E01 1.76E01 3.42E01 2.64E02 3.42E01 2.95E02 5.97E02 3.27E02 4.54E+00 5.68E02 7.11E02 3.70E01 6.65E02 1.50E01 1.50E01 1.23E+00 1.54E01 1.23E+00 2.22E01 1.25E01 5.36E02 6.63E+00 7.81E02 1.01E01 7.12E01 1.13E01 2.44E01 2.44E01 1.53E+00 2.25E01 1.53E+00 3.83E01 1.95E01 U
U U
U U
U 3,U 3,U U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 35 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614011 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #1 Analyte Activity Gamma Spec Units
% Abundance Total Activity:
0.00E+00 Total % Abundance:
000.00 Page 36 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614012 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #2 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.19E02 1.06E02 8.24E04 4.11E01 9.96E03 3.95E02 2.86E02 8.05E03 2.49E04 3.54E02 2.29E02 2.61E03 2.96E02 5.87E03 1.88E02 4.57E02 1.22E02 4.93E04 6.41E02 3.46E02 2.66E02 2.68E02 3.91E04 6.69E03 1.72E01 1.21E02 4.22E03 8.78E02 5.83E+00 6.83E03 3.01E02 3.96E02 2.80E02 2.54E02 1.51E02 3.28E02 3.52E01 2.94E02 3.73E01 6.38E01 2.75E02 1.27E01 4.01E02 1.69E02 3.66E02 2.32E02 6.14E02 3.99E02 7.16E02 2.34E02 5.47E02 2.60E01 3.75E02 3.88E02 9.57E02 6.20E02 3.28E02 7.48E01 2.56E02 3.07E02 1.92E+00 2.37E02 1.31E01 1.29E01 5.81E+00 2.83E02 2.87E02 6.63E02 8.14E02 6.36E02 3.81E02 4.67E02 6.16E01 5.02E02 4.58E01 1.38E+00 4.80E02 2.20E01 6.71E02 2.76E02 6.73E02 4.83E02 1.16E01 6.84E02 1.25E01 4.14E02 9.44E02 4.54E01 7.07E02 6.78E02 1.62E01 1.03E01 5.02E02 1.36E+00 4.42E02 4.86E02 3.41E+00 3.80E02 1.66E01 2.25E01 1.27E+01 5.00E02 4.51E02 1.10E01 1.40E01 9.95E02 6.16E02 8.61E02 1.00E01 U
U U
U U
U U
U U
3,U U
U U
U U
U U
U U
U U
U U
U U
U U
U 3,U U
U U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 37 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614012 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #2 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 1.67E02 9.57E01 6.73E02 4.34E02 1.59E01 5.25E03 2.35E01 2.35E01 9.18E01 5.06E03 9.18E01 3.76E02 6.35E02 3.74E02 3.41E+00 5.45E02 7.35E02 3.50E01 7.88E02 1.38E01 1.38E01 1.25E+00 1.57E01 1.25E+00 2.67E01 1.20E01 4.03E02 5.94E+00 6.56E02 8.07E02 6.58E01 1.14E01 1.38E01 1.38E01 1.50E+00 1.92E01 1.50E+00 4.06E01 1.92E01 U
U 3
U U
U 3
3 U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 38 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614012 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #2 Analyte Activity Gamma Spec Ac228 Pb212 Ra228 2.35E01 6.73E02 2.35E01 pCi/g pCi/g pCi/g Units
% Abundance 043.734 012.532 043.734 Total Activity:
5.37E01 Total % Abundance:
100.00 Page 39 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614013 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #3 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.58E01 4.02E03 2.80E01 1.39E02 1.91E02 3.36E02 1.94E02 1.29E02 9.18E03 4.01E01 1.35E02 7.80E03 9.60E03 1.28E02 6.70E03 3.62E02 3.09E03 2.56E02 3.00E02 1.97E02 2.79E03 7.21E01 3.98E03 3.03E02 9.75E01 5.92E03 2.78E02 7.40E02 4.73E+00 3.40E02 1.69E02 3.94E02 2.17E02 3.20E02 1.60E02 1.61E02 3.82E01 2.25E02 4.10E01 6.89E01 3.36E02 1.25E01 4.04E02 1.57E02 4.26E02 6.42E02 6.74E02 3.04E02 8.33E02 2.10E02 4.52E02 2.40E01 4.06E02 3.96E02 1.00E01 6.37E02 2.87E02 7.53E01 2.66E02 2.79E02 2.18E+00 2.17E02 9.34E02 1.28E01 7.36E+00 2.55E02 2.82E02 6.15E02 6.09E02 5.21E02 3.55E02 4.92E02 6.21E01 4.23E02 3.65E01 1.21E+00 5.28E02 2.20E01 6.76E02 2.82E02 7.34E02 4.48E02 1.19E01 6.12E02 1.32E01 3.53E02 7.85E02 4.23E01 7.42E02 6.43E02 1.97E01 1.08E01 5.01E02 1.24E+00 4.32E02 4.71E02 4.04E+00 3.36E02 1.62E01 2.08E01 1.15E+01 4.93E02 5.07E02 1.12E01 1.18E01 8.83E02 5.49E02 7.88E02 1.00E01 U
U U
U U
U U
U U
3 U
U U
U U
U U
U U
U U
U U
3,U U
U U
U U
3,U U
U U
U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 40 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614013 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #3 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 3.57E02 1.84E01 5.12E02 1.29E02 4.60E03 1.15E02 7.46E02 7.46E02 3.41E01 1.79E01 3.41E01 3.13E03 3.98E02 3.38E02 3.14E+00 4.83E02 7.30E02 3.87E01 7.75E02 1.64E01 1.64E01 1.38E+00 1.34E01 1.38E+00 2.28E01 1.02E01 4.04E02 5.19E+00 6.87E02 8.94E02 6.07E01 8.23E02 2.00E01 2.00E01 1.80E+00 2.02E01 1.80E+00 3.55E01 1.62E01 3,U U
3,U U
U U
U U
U U
U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 41 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614013 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.1 #3 Analyte Activity Gamma Spec Co60 4.01E01 pCi/g Units
% Abundance 100.000 Total Activity:
4.01E01 Total % Abundance:
100.00 Page 42 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614014 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.1 #4 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 3.49E01 3.06E03 2.70E01 6.90E01 6.43E02 5.38E02 3.82E02 7.32E03 2.26E02 5.01E02 4.49E02 2.63E02 8.00E02 4.09E03 1.10E02 1.16E01 5.57E02 1.84E02 6.20E02 1.39E02 2.45E02 5.55E01 2.69E02 5.09E02 1.19E+00 1.44E02 0.00E+00 1.73E01 5.17E01 1.86E03 2.79E02 3.26E02 1.75E03 5.76E02 7.07E02 2.19E02 8.50E01 5.23E02 7.15E01 1.64E+00 5.56E02 2.78E01 8.57E02 2.99E02 8.78E02 5.74E02 1.40E01 6.19E02 1.64E01 5.04E02 9.88E02 4.83E01 8.16E02 8.30E02 2.05E01 1.38E01 6.08E02 1.73E+00 5.34E02 7.90E02 4.87E+00 4.73E02 2.89E01 2.39E01 1.81E+01 5.58E02 6.02E02 1.77E01 1.44E01 8.33E02 7.46E02 9.85E02 1.38E+00 9.16E02 1.01E+00 2.81E+00 1.02E01 4.09E01 1.51E01 4.97E02 1.53E01 1.07E01 2.03E01 1.22E01 2.90E01 8.65E02 1.67E01 8.44E01 1.32E01 1.38E01 3.62E01 2.29E01 1.07E01 3.11E+00 8.92E02 1.03E01 8.33E+00 7.62E02 3.33E01 3.82E01 2.58E+01 9.57E02 9.79E02 2.29E01 2.53E01 1.78E01 1.21E01 1.68E01 1.00E01 U
U U
U 3,U U
U U
U U
U U
U U
U U
U U
U U
U U
U U
U U
UI U
U U
U U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 43 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614014 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.1 #4 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 7.64E02 5.94E01 1.67E02 8.60E02 8.91E01 7.61E03 1.68E01 1.68E01 2.88E02 2.66E01 2.88E02 9.18E02 1.99E02 7.11E02 6.66E01 9.53E02 1.44E01 1.06E+00 1.43E01 3.27E01 3.27E01 7.54E01 2.85E01 7.54E01 4.23E01 7.31E02 8.52E02 8.62E01 1.32E01 1.89E01 1.23E+00 2.02E01 4.03E01 4.03E01 9.78E01 3.64E01 9.78E01 7.04E01 1.03E01 3,U U
U U
U U
U U
U U
U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 44 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614014 Misc Solid TLG Services, Inc.
August 14, 2013 October 03, 2013 SU 1.1 #4 Analyte Activity Gamma Spec Units
% Abundance Total Activity:
0.00E+00 Total % Abundance:
000.00 Page 45 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614015 Misc Solid TLG Services, Inc.
August 09, 2013 October 03, 2013 SU 1.2 #1 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 3.60E01 2.58E02 1.76E01 4.23E02 3.56E02 7.49E02 1.11E02 0.00E+00 1.63E02 9.51E01 9.61E02 2.16E02 3.99E02 9.47E03 3.71E02 6.11E02 6.56E03 1.48E02 1.41E02 3.19E02 0.00E+00 1.76E01 2.32E02 1.76E03 1.36E02 8.12E03 4.75E02 8.10E02 3.87E+00 3.64E03 1.24E02 0.00E+00 7.11E02 8.76E02 1.18E02 1.05E02 4.75E01 2.53E02 3.05E01 9.89E01 3.42E02 1.66E01 5.41E02 3.82E02 5.21E02 1.03E01 6.18E02 4.38E02 1.09E01 3.31E02 5.95E02 2.51E01 5.39E02 4.32E02 7.31E02 7.52E02 7.23E02 1.35E+00 2.74E02 3.28E02 3.21E+00 2.82E02 1.34E01 1.36E01 1.17E+01 3.28E02 3.13E02 1.26E01 6.98E02 7.39E02 4.10E02 6.08E02 8.34E01 5.71E02 6.04E01 1.81E+00 5.80E02 3.25E01 1.00E01 3.59E02 1.02E01 4.49E02 1.49E01 9.47E02 1.84E01 4.99E02 1.15E01 4.82E01 1.02E01 8.01E02 1.69E01 1.33E01 7.16E02 2.49E+00 4.59E02 5.90E02 6.05E+00 4.80E02 2.31E01 2.69E01 2.20E+01 6.04E02 6.14E02 1.80E01 1.58E01 1.44E01 7.30E02 1.13E01 1.00E01 U
3,U U
U U
U U
UI U
3 3,U U
U U
U U
U U
U U
UI U
U U
U U
U U
U U
U UI 3,U 3,U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 46 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614015 Misc Solid TLG Services, Inc.
August 09, 2013 October 03, 2013 SU 1.2 #1 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 6.93E02 3.05E02 1.03E01 1.95E02 3.21E01 1.93E02 1.91E01 1.91E01 9.73E01 7.21E03 9.73E01 6.25E02 1.11E02 3.84E02 4.45E+00 7.95E02 6.58E02 4.37E01 6.84E02 1.96E01 1.96E01 1.13E+00 1.32E01 1.13E+00 2.94E01 1.28E01 4.98E02 8.25E+00 1.11E01 1.05E01 8.50E01 1.19E01 2.86E01 2.86E01 2.05E+00 2.49E01 2.05E+00 4.92E01 2.38E01 3
U 3,U U
U U
U U
U U
U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 47 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614015 Misc Solid TLG Services, Inc.
August 09, 2013 October 03, 2013 SU 1.2 #1 Analyte Activity Gamma Spec Co60 Tl208 9.51E01 6.93E02 pCi/g pCi/g Units
% Abundance 093.201 006.799 Total Activity:
1.02E+00 Total % Abundance:
100.00 Page 48 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614016 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.2 #2 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.27E01 1.12E02 1.65E01 2.53E01 8.71E03 1.66E02 8.19E04 0.00E+00 9.84E03 7.72E01 6.18E03 1.36E02 4.56E02 7.29E04 2.90E02 8.65E02 6.88E03 1.07E02 8.43E02 4.70E03 1.05E03 1.66E01 1.56E02 1.78E03 1.49E01 9.71E03 2.45E02 6.75E02 4.98E+00 1.85E02 1.29E03 4.81E01 2.01E02 9.47E03 5.37E03 2.83E02 2.75E01 1.50E02 2.27E01 4.53E01 2.46E02 9.77E02 3.25E02 3.51E02 3.05E02 7.27E02 6.44E02 2.20E02 5.53E02 1.80E02 3.24E02 1.76E01 3.38E02 2.52E02 5.48E02 4.22E02 2.11E02 6.07E01 1.77E02 1.78E02 1.48E+00 1.38E02 7.19E02 9.23E02 4.34E+00 1.81E02 1.83E02 8.76E02 4.26E02 4.21E02 2.12E02 3.10E02 4.94E01 3.26E02 1.98E01 8.79E01 3.93E02 1.81E01 6.28E02 3.85E02 5.77E02 3.83E02 1.05E01 5.02E02 1.17E01 3.54E02 6.77E02 3.16E01 6.35E02 5.18E02 5.89E02 8.23E02 4.09E02 1.19E+00 3.02E02 3.60E02 2.88E+00 2.88E02 1.33E01 1.74E01 7.38E+00 3.26E02 3.62E02 7.79E02 8.98E02 8.82E02 4.22E02 6.35E02 1.00E01 U
U U
U U
U U
UI U
3 U
U U
U U
U U
U U
U U
U U
U U
U U
U U
U U
3 U
U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 49 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614016 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.2 #2 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 4.23E02 3.53E01 2.63E01 5.76E03 2.98E01 6.28E02 1.37E01 1.37E01 3.22E02 3.81E03 3.22E02 4.73E02 2.05E02 3.83E02 2.65E+00 5.56E02 3.51E02 3.28E01 5.09E02 9.33E02 9.33E02 1.65E+00 8.26E02 1.65E+00 1.77E01 8.09E02 3.09E02 5.25E+00 4.99E02 6.82E02 4.87E01 7.34E02 1.85E01 1.85E01 1.31E+00 1.53E01 1.31E+00 3.32E01 1.62E01 3
U 3
U U
3,U 3,U 3,U U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 50 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614016 Misc Solid TLG Services, Inc.
August 15, 2013 October 03, 2013 SU 1.2 #2 Analyte Activity Gamma Spec Co60 Eu152 Pb212 Tl208 7.72E01 4.81E01 2.63E01 4.23E02 pCi/g pCi/g pCi/g pCi/g Units
% Abundance 049.568 030.855 016.865 002.712 Total Activity:
1.56E+00 Total % Abundance:
100.00 Page 51 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614017 Misc Solid TLG Services, Inc.
August 16, 2013 October 03, 2013 SU 1.2 #3 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 2.41E02 3.51E05 7.96E02 4.51E02 1.51E02 1.43E02 1.49E02 1.06E02 9.20E03 8.68E01 5.94E02 4.27E03 5.11E04 6.84E03 1.18E02 6.95E02 2.89E02 8.22E03 4.81E02 1.59E02 8.92E03 1.79E01 5.18E03 9.52E03 9.07E01 2.90E03 1.84E02 1.99E02 5.94E01 9.44E03 1.62E03 0.00E+00 3.98E04 2.15E02 8.66E03 7.74E03 2.08E01 1.71E02 1.50E01 3.91E01 1.77E02 8.05E02 2.67E02 1.02E02 2.75E02 6.23E02 5.48E02 2.11E02 4.55E02 1.63E02 2.80E02 1.35E01 2.62E02 2.15E02 4.64E02 3.55E02 1.77E02 5.07E01 1.47E02 1.74E02 1.16E+00 1.33E02 5.64E02 7.81E02 3.69E+00 1.44E02 1.56E02 6.02E02 4.74E02 3.57E02 1.98E02 2.75E02 4.03E01 2.73E02 2.91E01 7.42E01 3.42E02 1.40E01 5.15E02 2.14E02 5.03E02 2.32E02 7.58E02 3.96E02 8.62E02 2.55E02 5.10E02 2.71E01 5.21E02 4.11E02 7.27E02 6.69E02 3.44E02 9.74E01 2.90E02 2.87E02 2.06E+00 2.51E02 1.12E01 1.51E01 6.90E+00 2.88E02 3.04E02 7.32E02 7.53E02 6.97E02 3.66E02 5.40E02 1.00E01 U
U U
U U
U U
3,U U
3 U
U U
U U
U 3,U U
U U
U U
U U
U U
U U
U U
U UI U
U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 52 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614017 Misc Solid TLG Services, Inc.
August 16, 2013 October 03, 2013 SU 1.2 #3 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 3.46E02 9.69E02 1.59E01 4.08E02 1.69E01 5.52E02 1.20E01 1.20E01 3.88E01 7.61E03 3.88E01 2.75E02 4.90E02 2.48E02 2.11E+00 5.65E02 5.63E02 2.12E01 5.91E02 1.35E01 1.35E01 1.16E+00 7.97E02 1.16E+00 1.44E01 6.90E02 2.70E02 4.02E+00 3.98E02 5.92E02 4.22E01 6.95E02 1.50E01 1.50E01 1.08E+00 1.38E01 1.08E+00 2.84E01 1.40E01 3
U 3
U U
U U
U U
U U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 53 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614017 Misc Solid TLG Services, Inc.
August 16, 2013 October 03, 2013 SU 1.2 #3 Analyte Activity Gamma Spec Co60 Pb212 Tl208 8.68E01 1.59E01 3.46E02 pCi/g pCi/g pCi/g Units
% Abundance 081.792 014.949 003.259 Total Activity:
1.06E+00 Total % Abundance:
100.00 Page 54 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614018 Misc Solid TLG Services, Inc.
August 16, 2013 October 03, 2013 SU 1.2 #4 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 6.36E02 4.30E03 4.10E03 6.11E02 3.89E03 6.00E02 5.93E03 0.00E+00 1.33E02 7.64E01 2.11E02 5.98E03 2.33E02 4.71E03 2.17E02 7.56E02 3.51E03 1.07E02 5.20E04 2.29E02 1.17E02 1.47E01 5.95E03 1.75E02 9.56E02 8.92E05 0.00E+00 1.52E02 5.98E01 1.71E02 5.12E03 0.00E+00 1.10E02 2.99E02 5.55E03 2.28E02 2.17E01 1.35E02 1.78E01 5.97E01 2.04E02 7.76E02 2.84E02 2.79E02 2.45E02 5.60E02 4.38E02 1.90E02 5.12E02 1.41E02 2.69E02 1.40E01 2.88E02 2.41E02 4.99E02 3.60E02 1.81E02 4.58E01 1.42E02 1.86E02 1.15E+00 1.39E02 2.71E01 8.26E02 3.50E+00 1.50E02 1.76E02 8.83E02 3.75E02 3.91E02 2.39E02 5.15E02 4.18E01 2.46E02 2.27E01 8.47E01 3.16E02 1.36E01 5.19E02 2.22E02 4.38E02 2.58E02 8.40E02 3.81E02 9.70E02 2.60E02 5.32E02 2.78E01 4.48E02 4.48E02 9.69E02 6.55E02 3.52E02 8.42E01 2.74E02 2.85E02 2.22E+00 2.72E02 1.13E01 1.63E01 6.94E+00 3.05E02 3.39E02 9.50E02 6.87E02 8.23E02 3.97E02 5.47E02 1.00E01 U
U U
U U
U U
UI U
3 U
U U
U U
U U
U U
U U
U U
U U
U UI U
U 3,U U
UI U
U U
U 1
2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 55 of 72
GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.
- 2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
- 3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:
Matrix:
Geometry Received:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614018 Misc Solid TLG Services, Inc.
August 16, 2013 October 03, 2013 SU 1.2 #4 Report Date: October 28, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 10/15/13 0.00E+00 4.72E01 0.00E+00 1.34E02 6.26E02 1.30E02 0.00E+00 0.00E+00 1.74E01 0.00E+00 1.74E01 1.23E01 2.29E02 2.73E02 3.32E+00 5.90E02 3.21E02 2.04E01 3.32E02 1.47E01 1.47E01 5.54E01 3.31E01 5.54E01 1.87E01 5.93E02 2.72E02 2.92E+00 6.75E02 5.18E02 3.92E01 6.04E02 1.58E01 1.58E01 1.12E+00 1.49E01 1.12E+00 3.16E01 1.15E01 UI U
UI U
U U
UI UI U
UI U
U U
1 2
pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 56 of 72
GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:
Matrix:
Client:
Collect Date:
Receive Date:
Client Sample ID:
334614018 Misc Solid TLG Services, Inc.
August 16, 2013 October 03, 2013 SU 1.2 #4 Analyte Activity Gamma Spec Co60 7.64E01 pCi/g Units
% Abundance 100.000 Total Activity:
7.64E01 Total % Abundance:
100.00 Page 57 of 72
QC Summary Page 58 of 72
QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1336621 Batch Actinium-228 Americium-241 Antimony-124 Antimony-125 Barium-133 Barium-140 Beryllium-7 Bismuth-212 Bismuth-214 Cerium-139 Cerium-141 Cerium-144 Cesium-134 Cesium-136 Cesium-137 Chromium-51 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Parmname Mr. Jay Adler
Contact:
TLG Services, Inc.
148 New Milford Rd. East Bridgewater, Connecticut October 28, 2013 Report Date:
Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 10/15/13 14:40 QC 1.16 0.0743
-0.0372 0.0329
-0.00507
-0.355 0.274 1.14 1.24
-0.0016
-0.11 0.0983 0.00 0.153
-0.0226
-0.615 0.00341 0.00 0.00 0.0624 NOM Sample 1.47 0.0677 0.0916 0.0728
-0.0127 2.93
-0.132 1.15 1.11
-0.0155 0.0525 0.0633 0.00
-0.318
-0.00567 0.152
-0.0171 0.00
-0.031 0.107 Range (0%-20%)
N/A N/A N/A N/A N/A N/A (0% - 100%)
(0%-20%)
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A (0% - 100%)
Qual U
U U
U U
U U
U U
UI U
U U
U UI UI QC1202961675 334614002 23.6 N/A N/A N/A N/A N/A N/A 1.31 10.9 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 52.5 REC%
DUP 334614 Workorder:
U U
U U
U U
U U
U UI U
U U
U UI U
+/-0.217
+/-0.161
+/-0.104
+/-0.0751
+/-0.0377
+/-3.02
+/-0.460
+/-0.744
+/-0.140
+/-0.0301
+/-0.157
+/-0.183
+/-0.0755
+/-0.968
+/-0.0283
+/-1.03
+/-0.0482
+/-0.0395
+/-0.0505
+/-0.0489
+/-0.265
+/-0.0948
+/-0.101
+/-0.0724
+/-0.040
+/-3.14
+/-0.473
+/-0.743
+/-0.136
+/-0.0297
+/-0.143
+/-0.201
+/-0.0534
+/-1.14
+/-0.0359
+/-1.04
+/-0.0555
+/-0.0491
+/-0.152
+/-0.0536 RPD%
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 1 of 8 Page 59 of 72
QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1336621 Batch Europium-152 Europium-154 Europium-155 Iridium-192 Iron-59 Lead-210 Lead-212 Lead-214 Manganese-54 Mercury-203 Neodymium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Promethium-144 Promethium-146 Radium-228 Ruthenium-106 Silver-110m Sodium-22 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 10/15/13 14:40 QC 0.660
-0.0213
-0.00966 0.0154
-0.0141 3.28 1.43 1.48
-0.00235
-0.0124
-6.01
-0.103 0.000281 0.0322 19.1 0.00715
-0.00326 1.16
-0.0578
-0.0332
-0.00734 NOM Sample 0.615
-0.00225 0.0282
-0.0215 0.0351 0.924 1.44 1.53 0.0234 0.0752
-2.34
-0.301 0.0128
-0.0271 19.3 0.00658 0.0242 1.47 0.404
-0.0459
-0.000815 Range (0% - 100%)
N/A N/A N/A N/A (0% - 100%)
(0%-20%)
(0%-20%)
N/A N/A N/A N/A N/A N/A (0%-20%)
N/A N/A (0%-20%)
N/A N/A N/A Qual U
U U
U U
U U
U U
U U
U U
U U
7.00 N/A N/A N/A N/A 88.0 0.418 3.20 N/A N/A N/A N/A N/A N/A 1.09 N/A N/A 23.6 N/A N/A N/A REC%
334614 Workorder:
U U
U U
U U
U U
U U
U U
U U
U U
+/-0.123
+/-0.0935
+/-0.0883
+/-0.0414
+/-0.184
+/-4.21
+/-0.104
+/-0.169
+/-0.0354
+/-0.0679
+/-8.44
+/-0.384
+/-0.0265
+/-0.0724
+/-1.32
+/-0.0284
+/-0.0316
+/-0.217
+/-0.540
+/-0.0422
+/-0.0338
+/-0.129
+/-0.108
+/-0.0843
+/-0.0456
+/-0.167
+/-2.90
+/-0.104
+/-0.131
+/-0.0343
+/-0.0731
+/-10.0
+/-0.367
+/-0.0298
+/-0.0669
+/-1.21
+/-0.0346
+/-0.0403
+/-0.265
+/-0.282
+/-0.048
+/-0.039 RPD%
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 2 of 8 Page 60 of 72
QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1336621 Batch Thallium-208 Thorium-234 Tin-113 Uranium-235 Uranium-238 Yttrium-88 Zinc-65 Zirconium-95 Actinium-228 Americium-241 Antimony-124 Antimony-125 Barium-133 Barium-140 Beryllium-7 Bismuth-212 Bismuth-214 Cerium-139 Cerium-141 Cerium-144 Cesium-134 Cesium-136 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 10/15/13 14:40 10/15/13 14:41 QC 0.370 2.78 0.00799 0.038 2.78
-0.0103 0.00
-0.0255 1.75 565
-0.19
-0.0307 0.0333
-1.68
-2.65 2.19
-0.185 2.40 0.0139 0.0487 0.504 0.0663 NOM Sample 0.380 3.86
-0.0113 0.205 3.86 0.00123 0.0606 0.0596 Range (0%-20%)
(0% - 100%)
N/A N/A (0% - 100%)
N/A N/A N/A (75%-125%)
Qual U
U U
UI U
U U
U U
U U
U U
U U
U U
QC1202961676 2.67 32.4 N/A N/A 32.4 N/A N/A N/A REC%
115 491 LCS 334614 Workorder:
U U
U U
U
+/-0.0791
+/-2.39
+/-0.0487
+/-0.235
+/-2.39
+/-0.0288
+/-0.142
+/-0.102
+/-0.0711
+/-1.98
+/-0.0477
+/-0.163
+/-1.98
+/-0.0312
+/-0.115
+/-0.110
+/-2.44
+/-8.40
+/-0.438
+/-1.25
+/-0.518
+/-1.64
+/-3.90
+/-6.55
+/-0.853
+/-0.415
+/-0.400
+/-1.93
+/-0.565 RPD%
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 3 of 8 Page 61 of 72
QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1336621 Batch Cesium-137 Chromium-51 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Europium-152 Europium-154 Europium-155 Iridium-192 Iron-59 Lead-210 Lead-212 Lead-214 Manganese-54 Mercury-203 Neodymium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 10/15/13 14:41 QC 184 1.21
-0.59 15.7 0.266 220 0.512 0.694
-0.30
-0.399 0.625 5490 0.0886
-0.419
-0.36
-0.181 2.18 0.640 0.245 0.0959 0.221 NOM Sample Range (75%-125%)
(75%-125%)
Qual U
U U
U U
U U
U U
U U
U U
U U
U U
REC%
95.8 92.8 192 237 334614 Workorder:
+/-0.836
+/-1.87
+/-3.13
+/-0.547
+/-0.540
+/-0.507
+/-2.30
+/-1.19
+/-0.852
+/-1.06
+/-0.369
+/-1.19
+/-158
+/-0.596
+/-0.894
+/-0.525
+/-0.345
+/-3.14
+/-4.42
+/-0.418
+/-0.471
+/-2.04 RPD%
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 4 of 8 Page 62 of 72
QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1336621 Batch Promethium-144 Promethium-146 Radium-228 Ruthenium-106 Silver-110m Sodium-22 Thallium-208 Thorium-234 Tin-113 Uranium-235 Uranium-238 Yttrium-88 Zinc-65 Zirconium-95 Actinium-228 Americium-241 Antimony-124 Antimony-125 Barium-133 Barium-140 Beryllium-7 Bismuth-212 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 10/15/13 14:41 10/15/13 14:39 QC
-0.279
-0.37 1.75
-4.38
-0.124 0.236 0.0373
-43.9 1.33 0.686
-43.9 1.38 49.6 1.11
-0.0156 0.0537 0.0076 0.0185 0.0024
-0.0097 0.00758 0.112 NOM Sample Range Qual U
U U
U U
U U
U U
U U
U U
U U
U U
U U
QC1202961674 REC%
MB 334614 Workorder:
+/-0.418
+/-0.619
+/-2.44
+/-4.61
+/-0.821
+/-0.298
+/-0.442
+/-20.6
+/-0.694
+/-1.70
+/-20.6
+/-0.451
+/-2.65
+/-0.923
+/-0.0512
+/-0.0799
+/-0.0304
+/-0.0288
+/-0.0156
+/-0.0396
+/-0.099 RPD%
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 5 of 8 Page 63 of 72
QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1336621 Batch Bismuth-214 Cerium-139 Cerium-141 Cerium-144 Cesium-134 Cesium-136 Cesium-137 Chromium-51 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Europium-152 Europium-154 Europium-155 Iridium-192 Iron-59 Lead-210 Lead-212 Lead-214 Manganese-54 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 10/15/13 14:39 QC
-0.00775 0.00151 0.00433 0.00
-0.00466 0.00572 0.000936 0.00972
-0.00281
-0.0018
-0.00495
-0.0107
-0.0272
-0.00512
-0.0181 0.00201
-0.00625
-1.72 0.0111
-0.0311 0.00843 NOM Sample Range Qual U
U U
UI U
U U
U U
U U
U U
U U
U U
U U
U U
REC%
334614 Workorder:
+/-0.174
+/-0.0271
+/-0.00934
+/-0.0367
+/-0.129
+/-0.0114
+/-0.0177
+/-0.0177
+/-0.0838
+/-0.0109
+/-0.00747
+/-0.0111
+/-0.0147
+/-0.035
+/-0.0329
+/-0.0316
+/-0.00978
+/-0.0252
+/-3.08
+/-0.0409
+/-0.0306
+/-0.0103 RPD%
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 6 of 8 Page 64 of 72
QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1336621 Batch Mercury-203 Neodymium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Promethium-144 Promethium-146 Radium-228 Ruthenium-106 Silver-110m Sodium-22 Thallium-208 Thorium-234 Tin-113 Uranium-235 Uranium-238 Yttrium-88 Zinc-65 Zirconium-95 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 10/15/13 14:39 QC
-0.00558 0.0865 0.00651
-0.0065 0.00527 0.140
-0.00589 0.00216
-0.0156
-0.0547
-0.000892
-0.000374 0.00121
-0.141
-0.00656 0.0184
-0.141 0.00392
-0.00685 0.000959 NOM Sample Range Qual U
U U
U U
U U
U U
U U
U U
U U
U U
U U
U The Qualifiers in this report are defined as follows:
REC%
334614 Workorder:
+/-0.0115
+/-0.130
+/-0.126
+/-0.0126
+/-0.0109
+/-0.159
+/-0.014
+/-0.0141
+/-0.0512
+/-0.105
+/-0.0131
+/-0.0112
+/-0.0128
+/-0.704
+/-0.0137
+/-0.156
+/-0.704
+/-0.0101
+/-0.0257
+/-0.0188 RPD%
Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Notes:
Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).
Page 7 of 8 Page 65 of 72
QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Parmname Page 8 of 8 Units Anlst Date Time QC NOM Sample Range Qual REC%
334614 Workorder:
BD FA H
J K
L M
M N/A N1 ND NJ Q
R U
UI UJ UL X
Y
^
h Analyte is a Tracer compound Result is less than value reported Result is greater than value reported Results are either below the MDC or tracer recovery is low Failed analysis.
Analytical holding time was exceeded Value is estimated Analyte present. Reported value may be biased high. Actual value is expected to be lower.
Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M if above MDC and less than LLD REMP Result > MDC/CL and < RDL RPD or %Recovery limits do not apply.
See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Other specific qualifiers were required to properly define the results. Consult case narrative.
RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.
- Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.
RPD%
Page 66 of 72
Chain of Custody Page 67 of 72
Page 68 of 72
Page 69 of 72
Page 70 of 72
Laboratory Certifications Page 71 of 72
State Certification Alaska Arkansas CLIA California NELAP Colorado Connecticut Delaware DoD ELAP/ ISO17025 A2LA Florida NELAP Foreign Soils Permit Georgia Georgia SDWA Hawaii Idaho Chemistry Idaho Radiochemistry Illinois NELAP Indiana Kansas NELAP Kentucky Louisiana NELAP Louisiana SDWA Maryland Massachusetts Michigan Mississippi Nebraska Nevada New Hampshire NELAP New Jersey NELAP New Mexico New York NELAP North Carolina North Carolina SDWA Oklahoma Pennsylvania NELAP Plant Material Permit South Carolina Chemistry South Carolina GVL South Carolina Radiochemi Tennessee Texas NELAP Utah NELAP Vermont Virginia NELAP Washington Wisconsin UST110 880651 42D0904046 01151CA SC00012 PH0169 SC00012201310 2567.01 E87156 P3301200283, P3301200284 SC00012 967 SC00012201310 SC00012 SC00012 200029 CSC01 E10332 90129 03046 (AI33904)
LA130005 270 MSC012 9976 SC00012201310 NEOS2613 SC0001220132 2054 SC002 SC00012 11501 233 45709 9904 6800485 PDEP1200260 10120001 23611001 10120002 TN 02934 T104704235138 SC00012201310 VT87156 460202 C78012 999887790 List of current GEL Certifications as of 28 October 2013 Page 72 of 72