ML14080A195

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Letter from Erin Trent Radiochemistry Analysis Work Order: 337774
ML14080A195
Person / Time
Site: 05000134
Issue date: 12/06/2013
From: Trent E
GEL Labs
To: James Adler
TLG Services
References
337774
Download: ML14080A195 (30)
v • d • e


Text

December 06, 2013 Mr. Jay Adler TLG Services, Inc.

148 New Milford Rd. East Bridgewater, Connecticut 06752 Re: Radiochemistry Analysis Work Order: 337774

Dear Mr. Adler:

GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on November 19, 2013. This original data report has been prepared and reviewed in accordance with GELs standard operating procedures.

Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4504.

Sincerely, PM_SIGN_HERE Erin Trent Project Manager Purchase Order: Signed Quote GELP13-1296 Enclosures Page 1 of 30

Certificate of Analysis Page 2 of 30

Reviewed by USER_SIGN_HERE GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Certificate of Analysis Report TLGS001 TLG Services, Inc.

Client SDG: 337774 GEL Work Order: 337774 Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the U qualifier above.

This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Erin Trent.

The Qualifiers in this report are defined as follows:

  • A quality control analyte recovery is outside of specified acceptance criteria
    • Analyte is a Tracer compound
    • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification for Page 3 of 30

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:

Geometry Received:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774001 Misc Solid TLG Services, Inc.

August 14, 2013 November 19, 2013 SU 1.4 #3 (1530 cm)

Report Date: December 06, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 1.87E01 1.40E02 1.52E+01 1.97E01 9.06E04 3.80E01 4.92E02 0.00E+00 6.95E02 1.52E01 2.95E01 2.62E02 4.07E02 8.19E03 1.35E01 1.15E01 4.63E02 1.37E03 3.04E02 3.11E02 7.16E02 1.97E01 1.93E02 9.48E03 1.43E+00 2.31E02 2.75E02 1.70E01 5.65E+01 6.18E03 2.88E03 2.66E01 3.69E02 0.00E+00 3.61E02 1.16E01 8.32E01 3.63E02 1.16E+00 2.01E+00 3.61E02 2.79E01 8.38E02 4.24E02 7.02E02 4.43E02 1.49E01 4.61E02 1.45E01 2.88E02 1.09E01 3.09E01 4.94E02 5.57E02 1.32E01 7.04E02 5.23E02 6.75E+00 3.22E02 3.65E02 1.81E+01 3.32E02 2.65E01 1.77E01 8.25E+01 3.38E02 3.38E02 1.33E01 9.87E02 8.98E02 5.10E02 1.07E01 1.34E+00 6.52E02 4.42E01 3.74E+00 6.64E02 4.32E01 1.22E01 5.52E02 1.18E01 5.56E02 1.73E01 7.97E02 2.74E01 5.35E02 1.49E01 5.67E01 8.26E02 1.02E01 2.52E01 1.24E01 7.36E02 1.23E+01 5.43E02 5.95E02 3.30E+01 5.77E02 4.73E01 3.01E01 1.41E+02 6.16E02 6.17E02 1.31E01 1.78E01 1.22E01 9.04E02 1.87E01 1.00E01 U

U 3

U U

U U

UI U

3 U

U U

U 3,U U

U U

U U

3,U U

U U

U U

U U

U U

U 3

U UI U

3,U 1

2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 4 of 30

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:

Geometry Received:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774001 Misc Solid TLG Services, Inc.

August 14, 2013 November 19, 2013 SU 1.4 #3 (1530 cm)

Report Date: December 06, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 2.54E01 1.23E+00 9.24E01 6.41E01 0.00E+00 4.61E01 8.46E01 8.46E01 7.71E01 7.49E02 7.71E01 1.33E02 1.53E02 5.22E02 7.25E01 7.88E02 1.10E01 6.63E01 9.95E02 2.27E01 2.27E01 6.68E01 1.47E01 6.68E01 3.02E01 4.19E02 5.00E02 6.02E01 7.79E02 1.86E01 9.47E01 9.75E02 1.89E01 1.89E01 7.17E01 2.56E01 7.17E01 4.84E01 7.10E02 3

3 3

3 UI 3

3 3

3 U

3 U

U 1

2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 5 of 30

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:

Matrix:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774001 Misc Solid TLG Services, Inc.

August 14, 2013 November 19, 2013 SU 1.4 #3 (1530 cm)

Analyte Activity Gamma Spec Ac228 Bi214 Co60 Eu152 Pb210 Pb212 Pb214 K40 Ra228 Tl208 Th234 U238 8.46E01 4.61E01 1.52E01 2.66E01 1.23E+00 9.24E01 6.41E01 1.52E+01 8.46E01 2.54E01 7.71E01 7.71E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units

% Abundance 003.780 002.061 000.681 001.186 005.487 004.130 002.863 068.007 003.780 001.134 003.445 003.445 Total Activity:

2.24E+01 Total % Abundance:

100.00 Page 6 of 30

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:

Geometry Received:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774002 Soil TLG Services, Inc.

October 22, 2013 November 19, 2013 SU 4.2 #1 Report Date: December 06, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 1.84E02 1.78E04 1.61E+00 1.89E01 8.79E03 5.01E02 1.50E02 7.50E02 1.06E02 1.09E01 1.04E01 1.61E03 4.74E02 5.28E03 2.27E02 7.07E02 1.78E03 1.85E02 4.58E02 2.38E02 3.97E03 1.01E01 4.07E+00 5.50E03 4.62E02 6.74E04 1.97E02 2.95E02 1.55E01 7.96E03 2.61E02 1.19E01 6.44E03 4.95E02 1.30E02 2.00E02 4.80E01 2.83E02 5.90E01 4.34E01 2.86E02 7.93E02 3.41E02 2.87E02 3.08E02 6.00E02 8.40E02 3.65E02 6.08E02 2.49E02 3.70E02 2.49E01 3.69E02 4.82E02 9.89E02 9.52E02 3.15E02 1.60E01 1.75E01 3.84E02 4.44E01 2.00E02 5.02E02 1.12E01 1.18E+00 2.58E02 5.26E02 1.24E01 8.10E02 6.56E02 3.10E02 3.45E02 8.54E01 5.55E02 5.33E01 8.28E01 5.14E02 1.69E01 5.99E02 2.70E02 6.18E02 6.58E02 1.33E01 7.38E02 1.03E01 4.84E02 6.40E02 4.59E01 7.32E02 8.54E02 1.78E01 1.75E01 6.02E02 2.81E01 4.96E02 6.13E02 8.59E01 3.66E02 9.09E02 2.13E01 2.21E+00 4.71E02 9.07E02 1.73E01 1.61E01 9.62E02 5.62E02 6.54E02 1.00E01 U

U 3

U U

U U

3 U

3 U

U U

U U

U U

U U

U U

U 3

U U

U U

U U

U U

U U

U U

U 1

2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 7 of 30

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:

Geometry Received:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774002 Soil TLG Services, Inc.

October 22, 2013 November 19, 2013 SU 4.2 #1 Report Date: December 06, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 1.18E01 2.01E+00 2.50E01 4.17E01 4.04E01 3.59E01 0.00E+00 0.00E+00 6.60E01 4.95E02 6.60E01 3.12E01 1.83E02 5.22E02 4.32E01 8.25E02 1.42E01 5.11E01 1.10E01 1.75E01 1.75E01 4.87E01 1.28E01 4.87E01 3.08E01 2.66E02 4.92E02 4.77E01 7.19E02 1.12E01 8.33E01 1.01E01 3.02E01 3.02E01 4.91E01 2.18E01 4.91E01 3.62E01 4.87E02 3

3 3

3 U

3 UI UI 3

U 3

U U

1 2

pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 8 of 30

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:

Matrix:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774002 Soil TLG Services, Inc.

October 22, 2013 November 19, 2013 SU 4.2 #1 Analyte Activity Gamma Spec Bi214 Cs137 Co57 Co60 Pb210 Pb212 Pb214 K40 Tl208 Th234 U238 3.59E01 4.07E+00 7.50E02 1.09E01 2.01E+00 2.50E01 4.17E01 1.61E+00 1.18E01 6.60E01 6.60E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units

% Abundance 003.477 039.354 000.726 001.055 019.440 002.421 004.030 015.579 001.137 006.390 006.390 Total Activity:

1.03E+01 Total % Abundance:

100.00 Page 9 of 30

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:

Geometry Received:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774003 Misc Solid TLG Services, Inc.

August 22, 2013 November 19, 2013 SU 1.3 #1 (1530 cm)

Report Date: December 06, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 5.14E01 2.48E02 1.59E+01 3.70E02 3.85E03 6.82E02 4.99E02 1.34E01 3.54E02 4.06E02 2.50E02 7.80E04 1.12E01 3.95E03 7.89E02 1.84E01 1.81E02 1.21E02 2.67E02 2.16E02 5.46E02 6.06E+00 8.12E03 2.59E02 1.30E+01 1.59E02 6.97E02 1.28E01 1.17E+00 2.25E02 9.35E03 2.31E01 5.76E02 5.27E02 3.23E02 4.87E03 1.08E+00 5.19E02 1.32E+00 2.75E+00 5.77E02 3.45E01 9.40E02 7.42E02 1.03E01 6.49E02 1.49E01 5.12E02 1.96E01 4.05E02 1.23E01 4.54E01 7.37E02 8.16E02 2.18E01 1.10E01 6.42E02 6.34E+00 4.46E02 5.98E02 1.75E+01 4.88E02 3.39E01 2.40E01 7.92E+01 5.13E02 5.14E02 2.11E01 1.43E01 1.05E01 7.85E02 1.32E01 1.87E+00 9.77E02 5.62E01 5.02E+00 9.35E02 6.18E01 1.75E01 5.70E02 1.79E01 9.45E02 2.35E01 1.01E01 3.68E01 7.28E02 2.21E01 8.06E01 1.29E01 1.46E01 4.07E01 1.99E01 9.16E02 1.07E+01 8.02E02 9.07E02 3.09E+01 8.65E02 6.08E01 4.47E01 1.40E+02 9.48E02 9.28E02 2.39E01 2.68E01 1.91E01 1.41E01 2.42E01 1.00E01 U

U 3

U U

U U

3 U

U U

U U

U U

U U

U U

U U

U U

U U

U U

U U

U U

3,U U

U U

U 1

2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 10 of 30

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:

Geometry Received:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774003 Misc Solid TLG Services, Inc.

August 22, 2013 November 19, 2013 SU 1.3 #1 (1530 cm)

Report Date: December 06, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 2.70E01 1.84E+00 1.15E+00 6.83E01 0.00E+00 7.16E01 1.21E+00 1.21E+00 0.00E+00 1.47E01 0.00E+00 5.68E02 4.19E02 9.24E02 9.22E01 1.16E01 1.71E01 1.02E+00 1.59E01 2.94E01 2.94E01 1.37E+00 2.15E01 1.37E+00 4.50E01 6.80E02 7.24E02 9.09E01 1.14E01 1.57E01 1.33E+00 1.61E01 3.11E01 3.11E01 1.14E+00 3.73E01 1.14E+00 7.31E01 1.10E01 3

3 3

3 UI 3

3 3

UI U

UI U

U 1

2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 11 of 30

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:

Matrix:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774003 Misc Solid TLG Services, Inc.

August 22, 2013 November 19, 2013 SU 1.3 #1 (1530 cm)

Analyte Activity Gamma Spec Ac228 Bi214 Co57 Pb210 Pb212 Pb214 K40 Ra228 Tl208 1.21E+00 7.16E01 1.34E01 1.84E+00 1.15E+00 6.83E01 1.59E+01 1.21E+00 2.70E01 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units

% Abundance 005.243 003.095 000.579 007.963 004.979 002.956 068.777 005.243 001.166 Total Activity:

2.31E+01 Total % Abundance:

100.00 Page 12 of 30

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:

Geometry Received:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774004 Misc Solid TLG Services, Inc.

August 22, 2013 November 19, 2013 SU 1.3 #3 (1531 cm)

Report Date: December 06, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Gamma Spec Be7 Na22 K40 Cr51 Mn54 Fe59 Co56 Co57 Co58 Co60 Zn65 Y88 Zr95 Nb94 Nb95 Ru106 Ag110m Sn113 Sb124 Sb125 Cs134 Cs136 Cs137 Ba133 Ba140 Ce139 Ce141 Ce144 Nd147 Pm144 Pm146 Eu152 Eu154 Eu155 Ir192 Hg203 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 2.32E01 1.77E02 1.40E+01 0.00E+00 3.75E02 3.59E01 3.72E02 1.54E01 4.45E03 7.31E02 2.12E01 2.46E02 1.89E01 1.45E02 5.48E02 7.90E02 9.33E02 3.75E02 4.62E02 9.93E02 7.43E02 4.71E+00 1.38E02 8.16E03 6.90E+00 2.33E02 1.06E02 2.29E01 8.58E+00 4.04E02 0.00E+00 0.00E+00 9.31E02 4.58E02 7.13E02 1.59E01 9.70E01 5.22E02 1.42E+00 4.48E+00 5.00E02 3.72E01 1.02E01 6.60E02 1.11E01 6.61E02 1.92E01 5.09E02 2.12E01 4.36E02 1.27E01 4.38E01 1.10E01 8.47E02 2.47E01 1.15E01 5.22E02 6.71E+00 4.17E02 5.36E02 1.99E+01 4.47E02 3.59E01 2.81E01 7.40E+01 4.61E02 6.11E02 1.63E01 1.48E01 9.54E02 8.46E02 2.39E01 1.71E+00 9.35E02 5.45E01 4.63E+00 8.14E02 6.09E01 1.73E01 5.29E02 1.78E01 8.31E02 2.74E01 1.22E01 4.20E01 8.23E02 2.15E01 8.30E01 1.51E01 1.58E01 5.06E01 1.91E01 1.10E01 1.17E+01 7.53E02 8.72E02 3.62E+01 7.67E02 5.69E01 4.23E01 1.38E+02 7.79E02 9.91E02 2.53E01 2.54E01 1.78E01 1.24E01 2.12E01 1.00E01 U

U 3

UI U

U U

3 U

3,U 3,U U

U U

U U

U U

U U

3,U U

U U

U U

U U

U U

UI UI U

U U

U 1

2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 13 of 30

GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com Note(s): 1. Calculated MDAs are aposteriori values at the 95% confidence level.

2. Activity is reported on a dry weight basis unless otherwise indicated in the case narrativeand is decay corrected to the sample collect date.
3. Results are statistically positive at the 95% confidence level. (activity is greater than or equal to the two sigma uncertainty)

U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma SpectroscopyUncertain identification 10 CFR Part 50/61 Certificate of Analysis GEL Sample ID:

Matrix:

Geometry Received:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774004 Misc Solid TLG Services, Inc.

August 22, 2013 November 19, 2013 SU 1.3 #3 (1531 cm)

Report Date: December 06, 2013 Analyte Run Date Activity MDA Qualifier 2 Sigma Uncertainty RL Tl208 Pb210 Pb212 Pb214 Bi212 Bi214 Ra228 Ac228 Th234 U235 U238 Np239 Am241 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 11/20/13 2.57E01 1.10E+00 8.97E01 6.68E01 1.10E+00 5.72E01 9.10E01 9.10E01 1.69E+00 1.97E01 1.69E+00 1.06E01 1.85E02 9.49E02 9.86E01 1.11E01 1.64E01 8.89E01 1.51E01 3.12E01 3.12E01 1.56E+00 3.04E01 1.56E+00 4.43E01 8.50E02 7.65E02 1.14E+00 1.18E01 1.49E01 1.41E+00 1.69E01 3.08E01 3.08E01 1.32E+00 3.58E01 1.32E+00 7.03E01 1.37E01 3

3,U 3

3 3,U 3

3 3

3 U

3 U

U 1

2 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units Page 14 of 30

GEL LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 (843) 5568171 www.gel.com 10 CFR Part 50/61 Isotope Abundance Report GEL Sample ID:

Matrix:

Client:

Collect Date:

Receive Date:

Client Sample ID:

337774004 Misc Solid TLG Services, Inc.

August 22, 2013 November 19, 2013 SU 1.3 #3 (1531 cm)

Analyte Activity Gamma Spec Ac228 Bi214 Co57 Pb212 Pb214 K40 Ra228 Tl208 Th234 U238 9.10E01 5.72E01 1.54E01 8.97E01 6.68E01 1.40E+01 9.10E01 2.57E01 1.69E+00 1.69E+00 pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Units

% Abundance 004.191 002.635 000.711 004.132 003.075 064.327 004.191 001.183 007.777 007.777 Total Activity:

2.17E+01 Total % Abundance:

100.00 Page 15 of 30

QC Summary Page 16 of 30

QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1347774 Batch Actinium-228 Americium-241 Antimony-124 Antimony-125 Barium-133 Barium-140 Beryllium-7 Bismuth-212 Bismuth-214 Cerium-139 Cerium-141 Cerium-144 Cesium-134 Cesium-136 Cesium-137 Chromium-51 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Parmname Mr. Jay Adler

Contact:

TLG Services, Inc.

148 New Milford Rd. East Bridgewater, Connecticut December 6, 2013 Report Date:

Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 11/20/13 15:07 QC 0.836 0.0804

-0.0558

-0.059

-0.012

-14.8

-0.313 0.386 0.423 0.0181 0.0821 0.00807 0.0408 2.71

-0.0267

-1.2 0.000757 0.00582 0.00617 0.111 NOM Sample 0.846 0.0153

-0.0304

-0.0311 0.00948 1.43 0.187 0.00 0.461

-0.0231 0.0275 0.170 0.0716 0.197

-0.0193 0.197

-0.0492 0.00

-0.0695 0.152 Range (0% - 100%)

N/A N/A N/A N/A N/A N/A N/A (0% - 100%)

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A (0% - 100%)

Qual U

U U

U U

U U

U U

U U

U U

U U

U U

QC1202989167 337774001 1.18 N/A N/A N/A N/A N/A N/A N/A 8.78 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A 31.9 REC%

DUP 337774 Workorder:

U U

U U

U U

UI U

U U

U U

U U

U UI U

+/-0.227

+/-0.0419

+/-0.132

+/-0.0704

+/-0.0365

+/-18.1

+/-0.832

+/-0.663

+/-0.0995

+/-0.0332

+/-0.265

+/-0.177

+/-0.0523

+/-6.75

+/-0.0322

+/-2.01

+/-0.0838

+/-0.0424

+/-0.0702

+/-0.0443

+/-0.213

+/-0.0855

+/-0.157

+/-0.0699

+/-0.0335

+/-16.9

+/-0.657

+/-0.578

+/-0.103

+/-0.0305

+/-0.257

+/-0.180

+/-0.036

+/-6.35

+/-0.0286

+/-2.16

+/-0.0608

+/-0.062

+/-0.0639

+/-0.0496 RPD%

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 1 of 8 Page 17 of 30

QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1347774 Batch Europium-152 Europium-154 Europium-155 Iridium-192 Iron-59 Lead-210 Lead-212 Lead-214 Manganese-54 Mercury-203 Neodymium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Promethium-144 Promethium-146 Radium-228 Ruthenium-106 Silver-110m Sodium-22 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 11/20/13 15:07 QC 0.369

-0.0478

-0.0335

-0.00185

-0.0641 0.00 0.918 0.524

-0.00925 0.0517 11.5

-0.076

-0.0122 0.0489 13.5

-0.000987 0.00838 0.836

-0.0497

-0.0326

-0.0145 NOM Sample 0.266

-0.0369 0.00

-0.0361

-0.38 1.23 0.924 0.641 0.000906 0.116

-56.5

-0.0133 0.00819 0.135 15.2

-0.00618 0.00288 0.846 0.115

-0.0463

-0.014 Range (0% - 100%)

N/A N/A N/A N/A (0% - 100%)

(0%-20%)

(0%-20%)

N/A N/A N/A N/A N/A N/A (0%-20%)

N/A N/A (0% - 100%)

N/A N/A N/A Qual U

U U

U UI U

U U

U U

U U

U U

U U

32.7 N/A N/A N/A N/A 114 0.651 20.0 N/A N/A N/A N/A N/A N/A 12.1 N/A N/A 1.18 N/A N/A N/A REC%

337774 Workorder:

U UI U

U U

U U

U U

U U

U U

U U

+/-0.133

+/-0.0987

+/-0.0898

+/-0.051

+/-0.279

+/-0.725

+/-0.0788

+/-0.110

+/-0.0361

+/-0.107

+/-82.5

+/-0.302

+/-0.0288

+/-0.109

+/-1.16

+/-0.0338

+/-0.0338

+/-0.227

+/-0.309

+/-0.0494

+/-0.0363

+/-0.119

+/-0.0993

+/-0.0828

+/-0.0518

+/-0.247

+/-3.19

+/-0.0852

+/-0.110

+/-0.0334

+/-0.151

+/-73.6

+/-0.318

+/-0.0268

+/-0.0912

+/-1.09

+/-0.0303

+/-0.0304

+/-0.213

+/-0.260

+/-0.0507

+/-0.0359 RPD%

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 2 of 8 Page 18 of 30

QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1347774 Batch Thallium-208 Thorium-234 Tin-113 Uranium-235 Uranium-238 Yttrium-88 Zinc-65 Zirconium-95 Actinium-228 Americium-241 Antimony-124 Antimony-125 Barium-133 Barium-140 Beryllium-7 Bismuth-212 Bismuth-214 Cerium-139 Cerium-141 Cerium-144 Cesium-134 Cesium-136 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 11/20/13 15:07 11/20/13 15:07 QC 0.280 1.24

-0.0323

-0.021 1.24 0.0029 0.106

-0.0266 1.22 533

-0.0637

-0.664 0.278

-0.328 7.69 3.87

-0.0671 2.05

-0.225

-0.372 0.103

-0.228 NOM Sample 0.254 0.771 0.00137

-0.0749 0.771

-0.0262

-0.295 0.0407 Range (0%-20%)

(0% - 100%)

N/A N/A (0% - 100%)

N/A N/A N/A (75%-125%)

Qual U

U U

U U

U U

U U

U U

U U

U U

U U

U QC1202989168 9.68 46.9 N/A N/A 46.9 N/A N/A N/A REC%

108 491 LCS 337774 Workorder:

U U

U U

U

+/-0.0522

+/-0.668

+/-0.0557

+/-0.147

+/-0.668

+/-0.0461

+/-0.149

+/-0.145

+/-0.0531

+/-1.15

+/-0.0555

+/-0.146

+/-1.15

+/-0.0384

+/-0.125

+/-0.125

+/-2.61

+/-2.76

+/-0.545

+/-1.28

+/-0.487

+/-1.63

+/-4.62

+/-7.25

+/-0.911

+/-0.347

+/-0.338

+/-1.58

+/-0.672 RPD%

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 3 of 8 Page 19 of 30

QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1347774 Batch Cesium-137 Chromium-51 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Europium-152 Europium-154 Europium-155 Iridium-192 Iron-59 Lead-210 Lead-212 Lead-214 Manganese-54 Mercury-203 Neodymium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 11/20/13 15:07 QC 193

-1.1 0.331 15.7

-0.573 229 0.0962

-0.0973

-0.781 0.0795

-0.596 6360

-0.098

-0.247

-0.281 0.0911 0.0952 1.37

-0.0589

-0.136 1.42 NOM Sample Range (75%-125%)

(75%-125%)

Qual U

U U

U U

U U

U U

U U

U U

U U

U U

REC%

101 97.8 191 234 337774 Workorder:

+/-0.963

+/-2.15

+/-2.83

+/-0.655

+/-0.410

+/-0.606

+/-2.71

+/-1.12

+/-0.980

+/-0.704

+/-0.334

+/-1.47

+/-27.1

+/-0.535

+/-0.841

+/-0.634

+/-0.313

+/-3.07

+/-3.26

+/-0.480

+/-0.547

+/-2.42 RPD%

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 4 of 8 Page 20 of 30

QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1347774 Batch Promethium-144 Promethium-146 Radium-228 Ruthenium-106 Silver-110m Sodium-22 Thallium-208 Thorium-234 Tin-113 Uranium-235 Uranium-238 Yttrium-88 Zinc-65 Zirconium-95 Actinium-228 Americium-241 Antimony-124 Antimony-125 Barium-133 Barium-140 Beryllium-7 Bismuth-212 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 11/20/13 15:07 11/20/13 15:06 QC 0.547

-0.134 1.22

-0.128 0.210

-0.0341 0.157

-3.89 1.33 0.393

-3.89 1.43 47.3

-0.122 0.0521

-0.00656

-0.00379

-0.00674

-0.0108 0.0345

-0.0319 0.230 NOM Sample Range Qual U

U U

U U

U U

U U

U U

U U

U U

U U

U U

QC1202989166 REC%

MB 337774 Workorder:

+/-0.468

+/-0.717

+/-2.61

+/-4.24

+/-0.960

+/-0.343

+/-0.473

+/-6.77

+/-0.621

+/-1.46

+/-6.77

+/-0.450

+/-2.84

+/-0.964

+/-0.0855

+/-0.0207

+/-0.0342

+/-0.043

+/-0.0217

+/-0.0577

+/-0.113 RPD%

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 5 of 8 Page 21 of 30

QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1347774 Batch Bismuth-214 Cerium-139 Cerium-141 Cerium-144 Cesium-134 Cesium-136 Cesium-137 Chromium-51 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Europium-152 Europium-154 Europium-155 Iridium-192 Iron-59 Lead-210 Lead-212 Lead-214 Manganese-54 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 11/20/13 15:06 QC

-0.00297 0.00413 0.00295

-0.0195 0.00511 0.0187 0.0152 0.0113 0.00757

-0.000507 0.00579

-0.00723

-0.00701 0.0278 0.0202 0.000769 0.0153 0.0331 0.00184

-0.0285 0.0092 NOM Sample Range Qual U

U U

U U

U U

U U

U U

U U

U U

U U

U U

U U

REC%

337774 Workorder:

+/-0.197

+/-0.0408

+/-0.0102

+/-0.0182

+/-0.0676

+/-0.0174

+/-0.0193

+/-0.018

+/-0.0969

+/-0.0161

+/-0.00866

+/-0.0145

+/-0.0169

+/-0.0363

+/-0.0418

+/-0.0323

+/-0.0118

+/-0.0272

+/-0.331

+/-0.0525

+/-0.0363

+/-0.0184 RPD%

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Page 6 of 8 Page 22 of 30

QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Rad Gamma Spec 1347774 Batch Mercury-203 Neodymium-147 Neptunium-239 Niobium-94 Niobium-95 Potassium-40 Promethium-144 Promethium-146 Radium-228 Ruthenium-106 Silver-110m Sodium-22 Thallium-208 Thorium-234 Tin-113 Uranium-235 Uranium-238 Yttrium-88 Zinc-65 Zirconium-95 Parmname Units pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g pCi/g Anlst Date Time MXR1 11/20/13 15:06 QC 0.0106

-0.0438 0.00967

-0.00866 0.00378 0.216 0.00989 0.00257 0.0521 0.0629

-0.000438 0.00973 0.00335 0.0597

-0.00715

-0.0692 0.0597

-0.0163 0.0122

-0.00233 NOM Sample Range Qual U

U U

U U

U U

U U

U U

U U

U U

U U

U U

U The Qualifiers in this report are defined as follows:

REC%

337774 Workorder:

+/-0.0111

+/-0.0878

+/-0.129

+/-0.0221

+/-0.0158

+/-0.186

+/-0.0163

+/-0.0166

+/-0.0855

+/-0.132

+/-0.0185

+/-0.0147

+/-0.0193

+/-0.359

+/-0.0177

+/-0.0808

+/-0.359

+/-0.0168

+/-0.0349

+/-0.0257 RPD%

Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Uncertainty Notes:

Counting Uncertainty is calculated at the 95% confidence level (1.96-sigma).

Page 7 of 8 Page 23 of 30

QC Summary GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com Parmname Page 8 of 8 Units Anlst Date Time QC NOM Sample Range Qual REC%

337774 Workorder:

BD FA H

J K

L M

M N/A N1 ND NJ Q

R U

UI UJ UL X

Y

^

h Analyte is a Tracer compound Result is less than value reported Result is greater than value reported Results are either below the MDC or tracer recovery is low Failed analysis.

Analytical holding time was exceeded Value is estimated Analyte present. Reported value may be biased high. Actual value is expected to be lower.

Analyte present. Reported value may be biased low. Actual value is expected to be higher.

M if above MDC and less than LLD REMP Result > MDC/CL and < RDL RPD or %Recovery limits do not apply.

See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER.

Sample results are rejected Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.

Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Other specific qualifiers were required to properly define the results. Consult case narrative.

RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.

Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike conc. by a factor of 4 or more.

^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

  • Indicates that a Quality Control parameter was not within specifications.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

RPD%

Page 24 of 30

There are no "Data Exception Reports" associated with this analytical report.

Page 25 of 30

Chain of Custody Page 26 of 30

Page 27 of 30

Page 28 of 30

Laboratory Certifications Page 29 of 30

State Certification Alaska Arkansas CLIA California NELAP Colorado Connecticut Delaware DoD ELAP/ ISO17025 A2LA Florida NELAP Foreign Soils Permit Georgia Georgia SDWA Hawaii Idaho Chemistry Idaho Radiochemistry Illinois NELAP Indiana Kansas NELAP Kentucky Louisiana NELAP Louisiana SDWA Maryland Massachusetts Michigan Mississippi Nebraska Nevada New Hampshire NELAP New Jersey NELAP New Mexico New York NELAP North Carolina North Carolina SDWA Oklahoma Pennsylvania NELAP Plant Material Permit South Carolina Chemistry South Carolina GVL South Carolina Radiochemi Tennessee Texas NELAP Utah NELAP Vermont Virginia NELAP Washington Wisconsin UST110 880651 42D0904046 01151CA SC00012 PH0169 SC00012201310 2567.01 E87156 P3301200283, P3301200284 SC00012 967 SC00012201310 SC00012 SC00012 200029 CSC01 E10332 90129 03046 (AI33904)

LA130005 270 MSC012 9976 SC00012201310 NEOS2613 SC0001220132 2054 SC002 SC00012 11501 233 45709 9904 6800485 PDEP1200260 10120001 23611001 10120002 TN 02934 T104704235138 SC00012201311 VT87156 460202 C78012 999887790 List of current GEL Certifications as of 06 December 2013 Page 30 of 30

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