ML12227A522

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Calculation 98-ENG-02405D2, Revision 2, Justification for the Table Accuracy Value Used in the Minco RTD Sca Term, Attachment 8, Page 1 of 32
ML12227A522
Person / Time
Site: Millstone Dominion icon.png
Issue date: 08/09/2012
From: Nowlan N
Dominion Nuclear Connecticut
To:
Office of Nuclear Reactor Regulation
References
12-474A 98-ENG-02405D2, Rev 2
Download: ML12227A522 (33)
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Text

Calculation 98-ENG-02405D2, Revision 2 Attachment 8

ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PMPe Page I of 32 EngineeringTechnical Evaluation P,# / a,~ 31 IZ BWT Dominion- Cover Sheet S. S S *.~ .I

1. Stations Doc Type: Sub Type: 2. Document Number 3. Rev # 4. Decomissioning?

[Z MP E] SU 5] NA E] KW [] CO ETE 000 ETE-MP-2012-1135 0 5 Yes f] No (Note: If both SU and NA. then check CO) 5.

Title:

Justification for the Table Accuracy Value Used in the MINCo RTD SCA Term in Calculation No. 98-ENG-02405D2.

6. ETE Level 7. Unit(s)
  • 8. Quality Classification 9. FSRC Approval Req.?

[] Level El] Level 1 1 El Unit1 Ea Unit2 51 Unit3 l ISFSI El SR [] NS 5 NSQ 5 Yes [Z No 10.. Preparation,Review, and Approval Signatures (addor delete rows as needed)

Preparer : (Print) Signature: Date:

Digitally Signed By: . 08/06/2012 Nancy Nowlan 12:03:43 pm Reviewer: (Print) Signature: Date:

Digitally Signed By: 08/06/2012 Konstantine Filippides - "-,, .-- 01:04:08 pm Engineering Supervisor / Designee: (Print) Signature: Date:

Digitally Signed By: 08/06/2012 Keith Deslandes Xý__ z*__ 02:17:27 pm StandardAttachments Attachment # of pages Reviewed/No Not Req.

Impact

11. Design Effects and Considerations (DNES-AA-GN-1003) _ _* F-_
12. Document Impact Summary (DRUL) (DNES-AA-GN-1002) __ *
13. Considerations and Conditions for Document Updates (check N/A F7 if no document updates are noted on the DRUL) 5 All Document updates noted on the DRUL can be initiated immediately 5 Document updates noted on the DRUL are delayed until the following documents/actions are completed:

(e.g., WO, CR etc.) (See DRUL Remarks section) 10CFR5O.59Attachments Attachment # of pages Not Req.

14. 10CFR50.59/72.48 applicability review forms (DNAP-3004 or CM-AA-400) Wk
15. 10CFR50.59/72.48 screen form (DNAP-3004 or CM-AA-400) I*
16. 10CFR50.59/72.48 evaluation form (DNAP-3004 or CM-AA-400) I2
17. Additional Attachments Attachment # of pages Description MET LAB RTD Cal UncertaintyCalc,, 1 MET LAB RTD Cal UncertaintyInforn I CalibrationReport SN 1309.pdf 1 CalibrationReport SN 1269.pdf 1 CalibrationReport SN 1270.pdf 1 MINCoAccuracyStatement.pdf 2 SN_1269,_SN 1270 and SN 1309 C2 12 SN 1269 SN_1270 SN 1309_2009_1V 9 1 Aug 6, 2012 3:06 PM

ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 2 of 32 1'977X61-111460J7- 9.

EngineeringTechnical Evaluation Cover Sheet Domninion-CMA'-T-0 ATTACHMENT l2o .a 18.DDistribution Primary Recipient(s): (Enter the Name I Dept or Location for EACH Primary Recipient in this block.)

Copy To? Other Recipient / Department or Location Copy To? 1Other Recipient/Department or Location

]J Preparer

[]J Reviewer F] Supervisor El Site DCE

[] iffected organization El Program Owners 2.0 Source Document Calculation No. 98-ENG-02405D2, "Millstone Unit 2 Service Water Inlet Temperature-Indicator Accuracy TI-6928, TI-6929 & TI-6930."

4.0 Purpose The purpose of this engineering technical evaluation is to provide justification for the MINCo RTD "Table Accuracy" term used within calculation no. 98-ENG-02405D2. Also, this engineering technical evaluation will contain the calibration tables for the calibrated RTDs TE-6928, TE-6929 and TE-6930.

Aug 6, 2012 3:06 PM

ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 3 of 32 A)*AcJi/I,/y/ 6Jr-*"

.u*,miionEngineering k(6 or 3-ominion"Cover Sheet Technical Evaluation CMAA-T 0 ATTACHMENT 3o .a 7.0 Discussion TE-6928, TE-6929 and TE-6930 are the Vital AC Switchgear Room Cooling Coil (Xl 81A and X811B) Service Water Inlet RTDs. Loops T-6928, T-6929 and T-6930 are used in technical specification surveillance SP 2619A, "Control Room Shift Checks," to record and verify that the "Ultimate Heat Sink" temperature is less than 74.5 degrees F.

TE-6928, TE-6929 and TE-6930 are MINCo. model no. XS7927PKIL76S RTDs, serial nos. S/N 1309, S/N 1270 and S/N 1269, respectively. RTDs S/N 1269 and S/N 1270 were certified by MINCo in 1993 and RTD S/N 1309 was certified by MINCo in 2000.

MINCo certified all three RTDs to a stated accuracy value of+/- 0.025 degrees C (refer to the attached MINCo "Report of Calibrations" and "MINCo Accuracy Statement"). This supported the SCA term used in calculation no. 98-ENG-02405D2, revision no. 0.

A subsequent calibration of these particular serial number RTDs was performed by the Millstone Metrology Lab in 2009. New R vs T tables were generated and used for the calibration of each of the temperature loops (refer to the attached "SN 1269, SN 1270 and SN 1309 Met Lab Calibration Curves"). Information provided by the Millstone Metrology Lab indicates that the standards used by the lab to calibrate these RTDs is +/- 0.0038 degrees C (refer to the attached "Met Lab RTD Cal Uncertainty Cales. And Met Lab RTD Cal Uncertainty Information). This uncertainty value bounds the A:0.025 degrees C used in the SCA term in calculation no. 98-ENG-02405D2.

To ensure the Metrology Lab curves approximated those produced by MINCo, this ETE compared the values of the M]NCo curves to the Metrology Lab curves. The original R vs T tables provided by MINCo were not found. However, within MINCo's website, an RTD Table Generator was used to generate the R vs T tables using the coefficients of the original M1NCo RTD calibration reports. Using EXCEL, R vs T curves were plotted using resistance and temperature values over the 0 to 100 degrees F calibrated span of these temperature loops in 5 degrees F increments (21 data points). Again using EXCEL, R vs T curves were plotted using the 2009 Metrology Lab generated tables for these RTDs. The two curves generated for each serial no. RTD were compared. The worst case error noted and expressed as a percent of span (0 to 100 degrees F span) for S/N 1269, S/N 1270 and S/N 1309 was +/- 0.033 % (+/- 0.033 degrees F), +/-

0.01 % (- 0.01 degrees F) and +/- 0.066 % (+/- 0.066 degrees F), respectively. As stated earlier, S/N 1269 and S/N 1270 were certified by MINCO 16 years prior to the Metrology Lab calibration and S/N 1309 was certified by MINCo 9 years prior to the Metrology Lab calibraion. For S/N 1269 and S/N 1270, a MINCo stated 16 years drift term "root sum of the square" combined with the MINCo repeatability statement for this model no. RTD equates to +/- 0.36 % (0.36 degrees F). For S/N 1309, a MINCo stated 9 years drift term "root sum of the square" combined with the MINCo repeatability statement for this model no. RTD equates to +/- 0.27 % (0.27 degrees F). The worst case error in the curves generated by MINCo as compared to the 2009 Metrology Lab calibrations indicates that these particular serial no. RTDs did not drift very much over their respective 9 year and 16 year period and certainly much less than expected.

8.0 Conclusions The +/- 0.025 degrees C value used in the SCA term for RTD accuracy in calculation no. 98-ENG-2405D2 is valid. This value is used as "Table Accuracy" in revision no. 2 of this calculation.

Aug 6, 2012 3:06 PM

ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 4 of 32 A,7r~c/lA1e,~i-r g EngineeringTechnical Evaluation Cover Sheet

ý) Fominion-CMA-T-0 ATTCHEN 2 e4o
  • 12.0 References All references are attached to this ETE.
1. Calibration Report SN 1269,
2. Calibration Report SN 1270,
3. Calibration Report SN 1309,
4. MET LAB RTD Cal Uncertainty Calcs,
5. MET LAB RTD Cal Uncertainty Information,
6. SN 1269 SN 1270 SN 1309 Met Lab Cal Curves,
7. SN 1269, SN 1270, SN 1309 Calibration Curve Comparisons (EXCEL spreadsheets and charts),
8. MINCo Accuracy Statement.

Aug 6, 2012 3:06 PM

Attachment #1 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 5 of 32

,4/7%6/n'n6A"r a 5-a- 3 2--

MINCO PRODUCTS, INC. REPORT No. 2013 7300 COMMERCE LANE JOB No. 03-30932 FRIDLEY, MN 55432 P.O.# 259053 TELEPHONE: (612) 571-3121 FAX: (612) 571-0927 REPORT OF CALIBRATION

      • CERTIFICATE **T*

FOR PLATINUM RESISTANCE THERMOMETER MODEL XS7927PKIL76S(B) SERIAL No. 1269 PREPARED BY MINCO PRODUCTS, INC.

FOR NORTHEAST NUCLEAR ENERGY CO THE THERMOMETER RESISTANCE WAS MEASURED AT FIXED TEMPERATURE POINTS DEFINED BY ITS-90 OR BY COMPARISON WITH A CALIBRATED PLATINUM RESISTANCE THERMOMETER TRACEABLE TO THE NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY. RESISTANCES WERE MEASURED WITH AN EXCITATION CURRENT OF 1.OmA.

TEMPERATURE IS DERIVED FROM MEASURED RESISTANCE AS FOLLOWS:

FOR TEMPERATURES BELOW 273.16K:

Wref(T) = W(T) - a4*[W(T)-I] - b4*(W(T)-I)lnW(T)

FOR TEMPERATURES AT AND ABOVE 273.16K:

Wref(T) = W(T) - a8*[W(T)-I] - b8*[W(T)-I]-2 WHERE W(T) R(T)/R(273.16K), FOR T IN KELVIN; Wref(T) DEFINES TEMPERATURE ACCORDING TO THE ITS-90 REFERENCE FUNCTION (SEE FOLLOWING PAGE);

AND THE COEFFICIENTS a4, b4, a8, AND b8 ARE UNIQUE TO EACH INDIVIDUAL THERMOMETER.

a8 = -4.0758054D-04 b8 = +8.3733738D-05 a4 = -3.6445181D-04 b4 = -2.8576799D-06 R(OC) = 199.872 OHMS R(100C)/R(OC) = 1.3927 MEASUREMENT DATA TEMP (-C) RESISTANCE (OHMS)

-189.34 43.2061

-38.83 168.742 0.010 199.880 100.00 278.358 231.928 378.273 MEASUREMENTS BY: D. JACOBS CERTIFIED BY: G. ENGELBRECHT DATE CERTIFIED: 10 JUNE 1993 N.I.S.T. TEST REPORT No. 811/250375 DATE OF N.I.S.T. TEST: 4 DECEMBER 1992

Attachment #2 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 6 of 32 A4 7rACI/,'f C,, '-

5-- 6 a MINCO PRODUCTS, INC. REPORT No. 2014 7300 COMMERCE LANE JOB No. '03-30932 FRIDLEY, MN 55432 P.O.# 259053 TELEPHONE: (612) 571-3121 FAX: (612) 571-0927 REPORT OF CALIBRATION

      • C ERT I F I CATE **
  • FOR PLATINUM RESISTANCE THERMOMETER MODEL XS7927PK1L76S(B) SERIAL No. 1270 PREPARED BY MINCO PRODUCTS, INC.

FOR NORTHEAST NUCLEAR ENERGY CO THE THERMOMETER RESISTANCE WAS MEASURED AT FIXED TEMPERATURE POINTS DEFINED BY ITS-90 OR BY COMPARISON WITH A CALIBRATED PLATINUM RESISTANCE THERMOMETER TRACEABLE TO THE NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY. RESISTANCES WERE MEASURED WITH AN EXCITATION CURRENT OF 1.OmA.

TEMPERATURE IS DERIVED FROM MEASURED RESISTANCE AS FOLLOWS:

FOR TEMPERATURES BELOW 273.16K:

Wref(T) = W(T) - a4*[W(T)-I] - b4*[W(T)-I]InW(T)

FOR TEMPERATURES AT AND ABOVE 273.16K:

Wref(T) = W(T) - a8*(W(T)-I] - b8*[W(T)-I]^2 WHERE W(T) = R(T)/R(273.16K), FOR T IN KELVIN; Wref(T) DEFINES TEMPERATURE ACCORDING TO THE ITS-90 REFERENCE FUNCTION (SEE FOLLOWING PAGE);

AND THE COEFFICIENTS a4, b4, a8, AND b8 ARE UNIQUE TO EACH INDIVIDUAL THERMOMETER.

a8 = -5.4864581D-04 b8 = +1.0006569D-04 a4 = -3.3185991D-04 b4 = -2.9061316D-06 R(OC) = 199.904 OHMS R(100C)/R(OC) = 1.3926 MEASUREMENT DATA TEMP (-C) RESISTANCE (OHMS)

-189.34 43.2079

-38.83 168.768 0.010 199.912 100.00 278.392 231.928 378.311 MEASUREMENTS BY: D. JACOBS CERTIFIED BY: G. ENGELBRECHT DATE CERTIFIED: 10 JUNE 1993 N.I.S.T. TEST REPORT No. 811/250375 DATE OF N.I.S.T. TEST: 4 DECEMBER 1992

Attachment #3 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 7 of 32 MINCO Products, Inc. Report No. 3306 7300 Commerce Lane Job No. 3-254185 Fridley, MN 55432 P.O.# 02140472 Tel: (612) 571-3121 t FAX: (612) 571-0927 Report of Calibration

      • CERTIFICATE **
  • for Platinum Resistance Thermometer Model XS7927PKIL76S Serial No. 1309 Prepared by MINCO PRODUCTS, INC.

for NORTHEAST NUCLEAR ENERGY CO.

The thermometer resistance was measured at fixed temperature points defined by ITS-90 or by comparison with a calibrated Platinum Resistance Thermometer traceable to the National Institute of Standards and Technology. Resistances were measured with an excitation current of 1.0mA.

Temperature is derived from measured resistance as follows:

for temperatures below 273.16K:

Wref(T) = W(T) - a4*[W(T)-I] - b4*[W(T)-IjlnW(T) for temperatures at and above 273.16K:

Wref(T) = W(T) - a8*[W(T)-I] - b8*[W(T)-1I]2 1 where W(T) = R(T)/R(273.16K), for T in Kelvin; Wref(T) defines temperature according to the ITS-90 reference function (see following page);

and the coefficients a4, b4, a8, and b8 are unique to each individual thermometer.

a8 = -4.5088398D-04 b8 = +1.4870006D-04 a4 = -6.0597493D-04.

b4 = +3.1314950D-04 R(0 0 C) = 200.008 ohms R(100 0 C)/R(00 C) = 1.3927 Measurement data Temp (OC) Resistance (ohms)

-189.34 43.349

-38.83 168.866 0.010 200.016 100.00 278.546 231.928 378.533 Measurements by: JES Certified by: M. SWENSON Date certified: 14 July 2000 N.I.S.T. Test Report No. 14-HS876-1-1 Date of N.I.S.T. test: 6 May 1999

Attachment #4 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 8 of 32

,47YA!&46Ore-~

Hart Thermometry System Accuracies SPRT + Thermometer Uncertainties Device Temperature Accuracy Combined Uncertainty 1590 -200 to 6610C +/-0.00150C +0.002500 5681 -200to661°C +/-0.0020C Bath Uncertainties Device Parameter Tem erature Specification

-40°C +/-0.0020 C 00C +/-0.0010C 7037 Stability 250C +/-0.00050C

+0.0020C

+/-10000 Uniformity All +/-0.0020C Stability 1000C +/-0.0030C 6022 3000C +/-0.0050C 6022 1000C +/-0.0040C Uniformity 3000C +/-0.0120C

<3000C +/-0.0300C 9260 Stability >3000C +/-0.0500C Uniformity 50 to 6800C +/-0.0200C Fixed Point Fixed Point Cell Temperature Uncertainty 5901 D-Q TPW 0.010C +/-0.0001 0C 5946 MP Zn 429.5270C +/-0.0020C Combined Uncertainties (Bath + 1590 + 5681)

Bath Temperature Combined Uncertainty

-400C +/-0.0038°C 000C +/-0.00340C 250C +/-0.00320C 1000C +/-0.00380C 1000C +/-0.00560C 3000C +/-0.01 320C 9260 <3000C +/-0.03610C

>3000C +0.05390C

=>

0 S

Nancy M Nowlan (Generation - 6) 0, From: Robert J Byrnes (Generation - 4)

Sent: Thursday, August 02, 2012 3:26 PM To: Nancy M Nowlan (Generation - 6)

Subject:

Accuracy of Data Generated by Metrology Laboratory RTD Calibrations

Nancy, Measurement uncertainty for all standards used for calibration of RTDs by the Millstone Metrology Laboratory is +/-0.0038*C. This excludes the uncertainty of the Callendar Van Dusen equation, which generates the Temperature vs. Resistance table and coefficients. The CVD equation, used to generate the table and m

coefficients, contributes such an inconsequential uncertainty, that it is not worthy of consideration.

The RTD data provided by Minco has an uncertainty of 0.0250 C. The calibrations performed by the Millstone Metrology Laboratory are 6.58 times more accurate.

-P bob byrnes Instrument Tech Ill C" Tie Line: 8.759.6229 Phone: 860.447.1791 x6229 0 Fax: 860.444.5317 0 Pager: 860.504.4365 0D "The only stupid question is the one you don't ask." 0 cc O

Attachment #6 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 10 of 32

-Report for Callendar-Van Dusen Coefficients --,-- .

Model: XS7-927PK I Serial: 1309 t-Da~te-: August 04,2009

,5 5-.5 7 C) e7(3 Rekfrence (OC) UUT (Ohms) Residual (QC)

-19:9433 184.0662 0.0000 0.0380 199.9719 0.0000 25.0211 219.8137 -0.0016 50,0 176 239.5121 0.0003 75.0155 259.0611 0.0012 I00.0214 278.4672 -0.0007 Coefficients:

RO = 199.941595 ALPHA = 0.00392657 DELTA = 1.54203 BETA = -9.55746 P'age Iof 3

Attachment #8 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 11 of 32

,f,VrCftAlC'ce&r Model: XS7927PK1 Serial: 1309 Callendar-Van Dusen Temperature vs. Resistance Table OF Resistance dr/dT OF Resistance dr/dT i OF Resistance drldT

-4.00 184.02137 0.4392383 54.00 209.66696 0.4412402 112.00 235.13320 0.4369059

-3.00 184.46076 0.4395457 55.00 210.10817 0.44116551 113.00 235.57007 0.4368311

-2.00 184.90046 0.4398394 56.00 210.54929 0.44109071 114.00 236.00686 0,4367564

-1.00 185.34044 0.4401196 57.00 210.99035 0.4410160 115.00 236.44358 0.4366817 0.00 185.78069 0,4403863 58.00 211.43133 0.44094131 116.00 236.88022 0.4366069 1.00 186.22121 0,44063991 59.00 211.87223 0.44086651 117.00 237.31679 0.4365322 2.00 186.66197 0,4408804 60.00 212.31306 0.4407918 118.00 237.75329 0.4364575 3.00 187.10296 0.44110801 61.00 212.75381 0.4407171 119.00 238.18971 0.4363827 4.00 187.54418 0.4413230 62.00 213.19449 0.4406424 120.00 238.62605 0.4363080 5.00 187.98560 0.4415254 63.00 213.63510 0.4405676 121.00 239.06233 0.4362333 6.00 188.42723 0.4417155 64.00 214.07563 0,4404929 122.00 239.49852 0.4361586 7.00 188.86903 0.4418934 65.00 214.51608 0.4404182 123.00 239.93464 0.4360838 8.00 189.31101 0,4420593 66.00 214.95647 0.4403434 124.00 240.37069 0.4360091 9.00 189.75315 0.4422133 67.00 215.39677 0.4402687 125.00 240.80666 0,4359344 10.00 190.19543 0.4423557 68.00 215.83700 0.4401940 126.00 241.24256 0,4358596 11.00 190.63785 0.4424866 69.00 216.27716 0.4401192 127.00 241.67838 0.4357849 12.00 191.08040 0.4426062 70.00 216.71724 0.4400445 128.00 242.11413 0.4357102 13.00 191.52306 0.4427146 71.00 217.15725 0.4399698 129.00 242.54980 0.4356354 14.00 191,96583 0.4428121 72.00 217.59718 0.4398951 130.00 242.98540 0.4355607 15.00 192.40868 0.4428987 73.00 218.03704 0.4398203 131.00 243.42092 0.4354860 16.00 192.85162 0.44297471 74.00 218.47682 0.4397456 132.00 243.85637 0.4354113 17.00 193.29463 0.4430403 75.00 218.91653 0.4396709 133.00 244.29174 0.4353365 18,00 193.73770 0.4430955 76.00 219.35616 0.4395961 134.00 244.72704 0.4352618 19.00 194.18082 0.4431406 77.00 219.79572 0.4395214 135.00 245.16227 0.4351871 20.00 194.62397 0.44317581 78.00 220.23521 0.4394467 ; 136.00 245.59742 0.4351123 21.00 195.06716 0.4432012! 79.00 220.67462 0.4393719 137.00 246.03249 0.4350376 22.00 195.51037 0.4432170f 80:00 221.11395 0.4392972 138.00 246.46749 0.4349629 23.00 195.95359 0.4432233, 81.00 221,55321 0.4392225 139.00 246.90242 0.4348881 24.00 196.39682 0,4432204! 82.00 221.99240 0.43914781 140.00 247.33727 0.4348134 25.00 196.84003 0.44320841 83.00 222.43151 0,4390730 141.00 247.77205 0.4347387 26.00 197.28323 0.44318751 84.00 222.87054 0,4389983 142.00 248.20675 0.4346640 27.00 197.72640 0.44315781 85.00 223.30950 0,4389236 143.00 248.64137 0.4345892 28.00 198.16954 0.44311961 86.00 223.74839 0.4388488 144.00 249.07592 0,4345145 29.00 198.61264 0.4430729 87.00 224.18720 0.4387741 145.00 249.51040 0.4344398 30.00 199.05569 0.4430180 88.00 224.62594 0,4386994 146.00 249.94480 0.4343650 31.00 199.49867 0.4429551 89.00 225.06460 0.4386246 147.00 250.37913 0.4342903 32.00 199.94159 0.4428843 90.00 225.50319 0.4385499 148.00 250.81338 0.4342156 33.00 200.38444 0.4428095 91.00 225.94170 0.4384752 149.00 251.24756 0,4341408 34.00 200.82721 0.4427348 92.00 226.38014 0.4384005 150.00 251,68167 0,4340661 35.00 201.26991 0.4426601 93.00 226.81850 0.4383257 151.00 252,11570 0.4339914 36.00 201.71253 0.4425853 94.00 227.25679 0,4382510 152.00 252.54965 0.4339167 37.00 202.15508 0.4425106 95.00 227.69500 0.4381763 153.00 252,98353 0.4338419 38.00 202.59756 0.4424359 96.00 228.13314 0.4381015 154.00 253.41733 0.4337672 39.00 203.03995 0.44236111 97.00 228,57120 0.4380268 155.00 253.85106 0.4336925 40.00 203.48228 0.4422864 98.00 229.00919 0.4379521 156.00 254.28472 0.4336177 41.00 203.92453 0,44221171 99.00 229.44711 0.4378773 157.00 254,71830 0,4335430 42.00 204.36670 0.44213701 100.00 229.88495 0.4378026 158.00 255.15180 0.4334683 43.00 204.80880 0.4420622 101.00 230,32271 0.4377279 159.00 255.58524 0.4333935 44.00 205.25083 0.4419875 102.00 230.76040 0.4376532 160.00 256,01859 0.4333188 45.00 205.69278 0.4419128 103.00 231.19802 0.4375784 161.00 256,45187 0.4332441 46.00 206.13465 0.4418380 104.00 231.63556 0.4375037 162.00 256.88508 0.4331694 47.00 206.57645 0.4417633 105.00 232.07303 0.4374290 163.00 257.31821 0.4330946 48.00 207.01818 0.4416886 106.00 232.51042 0.4373542 164.00 257.75127 0.4330199 49.00 207.45983 0,44161381 107.00 232.94774 0.4372795 165.00 258.18425 0.4329452 50.00 207.90141 0.4415391 108.00 233.38498 0.4372048 166.00 258.61716 0.4328704 51,00 208.34291 0.44146441 109.00 233.82215 0.4371300 167.00 259.04999 0.4327957 52.00 208.78433 0.44138971 110.00 234.25924 0.4370553 168.00 259.48275 0.4327210 63.00 209.22569 0.4413149 111.00 234.69626 0.4369806 169,00 259.91543 0.4326462 Page 2 of 3 Date: August 04,2009

Attachment #6 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 12 of 32 Model: XS7927PKI Serial: 1309 Callendar-Van Dusen Temperature vs. Resistance Table OF Resistance drldT 170.00 260.34804 0.4325715 171.00 260.78058 0.4324968 172.00 261.21304 0.4324221 173.00 261.64542 0.4323473 174.00 262.07773 0.4322726 175.00 262.50997 0.4321979 176.00 262.94213 0.4321231 177.00 263.37421 0.4320484 178.00 263.80622 0.4319737 179.00 264.23816 0.4318989 180.00 264.67002 0.4318242 181.00 265.10181 0.4317495 182.00 265.53352 0.4316748 183.00 265.96516 0.4316000 184.00 266.39672 0.4315253.

185.00 266.82821 0.4314506*

186.00 267.25962 0.4313758!

187.00 267.69096 0,4313011!

188.00 268.12222 0.4312264; 189.00 268.55341 0.4311516.

190.00 268,98453 0.4310769-191.00 269.41557 0.4310022:

192.00 269.84653 0.4309275:

193.00 270.27742 0,4308527:

194.00 270,70824 0.4307780 195.00 271.13898 0.4307033, 196.00 271.56964 0.4306285 197.00 272.00023 0.4305538 198.00 272.43075 0.4304791 199.00 272.86119 0.4304044 200.00 273.29156 0.4303296 201.00 273.72185 0.4302549 202.00 274.15207 0.4301802 203.00 274.58221 0.4301054 204.00 275.01228 0.4300307 205.00 275.44227 0.4299560 206.00 275.87219 0.4298812 207.00 276.30204 0.4298065 208.00 276.73181 0.4297318 209.00 277.16150 0.4296571 210.00 277.59112 0.4295823 211.00 278.02066 0.4295076 212.00 278.45014 0.4294329 Page 3 of 3 Date: August 04,2009

Attachment #6 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 13 of 32

,rA(#C A17-e Et Report of Calibration Report No: RU200908073-001 Dominion Page 1 of 3 Rope Ferry Road Bldg 433, Metrology Laboratory Waterford, CT 06385 Model: XS7927PK1 Customer: Dominion Serial: 1270 ' ,1'o Rope Ferry Road

Description:

RTD PLANT INSTALLED Bldg 433, Metrology Laboratory Waterford, CT 06385 Calibration Range: Limited Received Condition: Recalibration Current: 1.0 mA Procedure: MTE 1142E Actual Value UUT (Reference) (Test Sensor) Residuals Method of (C) (Ohms) (C) Realization

-19.92670 183.96920 0.0000 COMP 0.04100 199.93170 0.0000 COMP 25.02490 219.76970 0.0005 COMP 50.01590 239.46400 -0.0003 COMP 75.01290 259.01160 -0.0001 COMP 100.01760 278.41470 0.0001 COMP

'Callendar-Van Dusen Coefficients:

RO = 199.89901 DELTA= 1.53452 ALPHA= 0.00392709 BETA = -0.12847 Test Equipment Manufacturer Model Description Serial Number Recall Date Hart Scientific 1590 Super Thermometer I1 A68350 09/03/2009 Hart Scientific 5681 SPRT, 25 ohm 1466 02/25/2010 Hart Scientific 7037 Bath, Deep Low-Temp 93046 NCR Notes: Initial calibration to establish baseline data.

Acceptance Criteria: RO = 199,8000 to 200.2000 ohms Prerequisitesp/et: Initial: Usage Review Required: Yes __

CR#: 111 - 'inaf Calibration Acceptable: Yes %_ No__

Technician: -17 Calibration Date: 08/17/2009 Recall Date: 08/12/2029 R61~rerI3 Byrne~:

Temperature: 73.OF Humidity: 45% Approved By: -

Customer Order: N/A This reportshahl not be reproducedexcept infull without written approval ofDondnion.

Attachment #6 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 14 of 32 A(f1~416-A'r &

08/18/2009 Temperature vs.'-% tance Table Repoi .o : RJ200908073. -001 Page2of3 F Resistance dr/dT F Resistance dr/dT F Resistance dr/dT 0.00 185.69151 0.4451292 59.00 211.82792 0.4408077 118.00 237.70615 0.4364204 1.00 186.13661 0.4450593 6 0.00 212.26869 0.4407333 119.00 238.14253 0.4363461 2.00 186.58163 0.4449891 61.00 212.70939 0.4406590 120.00 238.57884 0.4362717 3.00 187.02658 0.4449188 62.00 213.15001 0.4405846 121.00 239.01508 0.4361974 4.00 187.47147 0.4448484 6 3.00 213.59056 0.4405102 122.00 239.45124 0.4361230 5.00 187.91628 0.4447777 6 4.00 214.03103 0.4404359 123.00 239.88732 0.4360486 6.00 188.36102 0.4447069 6.5.00 214.47143 0.4403615 124.00 240.32334 0.4359743 7.00 188.80570 0.4446360 6'6.00 214.91175 0.4402872 125.00 240.75927 0.4358999 8.00 189.25030 0.4445648 6 7.00 215.35200 0.4402128 126.00 241.19514 0.4358256 9.00 189.69482 0.4444936 678.00 215.79218 0.4401384 127.00 241.63092 0.4357512 10.00 190.13928 0.4444221 6*9.00 216.23228 0.4400641 128.00 242.06664 0.4356768 11.00 190,58367 0.4443505 7.0.00 216.67231 0.4399897 129.00 242.50228 0.4356025 12.00 191.02798 0.4442788 711.00 217.11226 0.4399154 130.00 242.93784 0.4355281 13.00 191.47223 0.4442069 7E2.00 217.55214 0.4398410 131.00 243.37333 0.4354538 14.00 191.91640 0,4441348 7 3.00 217.99194 0.4397666 132.00 243.80875 0.4353794 15.00 192.36050 0.4440626 714.00 218.43167 0.4396923 133,00 244.24409 0.4353050 16.00 192.80452 0.4439903 755.00 218.87133 0.4396179 134.00 244.67936 0.4352307 17.00 193.24848 0.4439178 766.00 219.31091 0.4395436 135.00 245.11455 0.4351563 18.00 193.69236 0.4438452 777.00 219.75041 0.4394692 136.00 245.54967 0.4350820 19.00 194.13617 0.4437725 788.00 220.18985 0.4393948 137.00 245.98472 0.4350076 20.00 194.57990 0.4436996 79).00 220.62920 0.4093205 138.00 246.41969 0.4349332 21.00 195.02357 0.4436266 800.00 221.06849 0.4392461 139.00 246.85458 0.4348589 22.00 195.46716 0.4435534 8tt.00 221,50770 0.4391718 140.00 247.28941 0.4347845 23.00 195,91067 0.4434802 82,2.00 221.94683 0,4390974 141.00 247.72415 0.4347102 24.00 196.35412 0.4434068 833.00 222.38589 0.4390230 142.00 248,15883 0.4346358 25.00 196,79749 0.4433332 84.00 222.82488 0.4389487 143.00 248,59342 0.4345614 26.00 197.24078 0.4432596 85.00 223.26379 0.4388743 144.00 249.02795 0.4344871 27.00 197.68401 0,4431859 86.00 223.70262 0.4388000 145.00 249.46240 0.4344127 28.00 198.12715 0.4431120 87.00 224.14139 0,4387256 146.00 249.89677 0.4343384 29.00 198.57023 0.4430380 88.00 224.58008 0.4386512 147.00 250.33108 0.4342640 30.00 199.01323 0.4429639 89.00 225.01869 0.4385769 148.00 250.76530 0.4341896 31.00 199.45616 0.4428897 90.00 225.45723 0.4385025 149.00 251.19945 0.4341153 32.00 199.89901 0.4428154 91.00 225.89569 0.4384282 150.00 251.63353 0.4340409 33.00 200.34179 0.4427410 92.00 226.33409 0.4383538 151.00 252.06754 0.4339666 34,00 200.78449 0.4426667 93.00 226.77240 0.4382794 152.00 252.50147 0.4338922 35,00 201.22712 0.4425923 94.00 227.21064 0.4382051 153.00 252.93532 0.4338178 36.00 201.66968 0.4425180 95.00 227.64881 0.4381307 154.00 253.36910 0.4337435 37.00 202,11216 0.4424436 96.00 228.08691 0.4380564 155.00 253.80281 0.4336691 38.00 202.55456 0.4423692 97.00 228.52493 0.4379820 156.00 254.23644 0.4335948 39.00 202.99690 0.4422949 98.00 228.96287 0.4379076 157.00 254.67000 0.4335204 40.00 203.43915 0.4422205 99.00 229.40074 0.4378333 158.00 255.10348 0.4334460 41.00 203.88134 0.4421462 100.00 229.83854 0.4377589 159.00 255.53689 0.4333717 42.00 204.32345 0.4420718 101.00 230.27626 0.4376846 160.00 255.97022 0.4332973 43.00 204.76548 0.4419974 102.00 230.71391 0.4376102 161.00 256.40348 0.4332230 44.00 205,20744 0.4419231 103.00 231.15148 0.4375358 162.00 256.83667 0.4331486 45.00 205,64933 0.4418487 104.00 231.58898 0.4374615 163.00 257.26978 0.4330742 46.00 206.09114 0.4417744 105.00 232.02640 0.4373871 164.00 257.70282 0.4329999 47.00 206.53288 0.4417000 106.00 232.46375 0.4373128 165.00 258.13578 0.4329255 48.00 206.97454 0.4416256 107.00 232.90103 0.4372384 166.00 258.56867 0.4328512 49.00 207.41613 0.4415513 108.00 233.33823 0,4371640 167.00 259.00148 0.4327768 50.00 207.85764 0,4414769 109.00 233.77536 0.4370897 168.00 259.43422 0.4327024 51.00 208.29908 0.4414026 110.00 234.21241 0.4370153 169.00 259.86689 0.4326281 52.00 208.74045 0.4413282 111.00 234.64939 0.4369410 170.00 260.29948 0.4325537 53.00 209.18174 0.4412538 112.00 235.08629 0.4368666 171.00 260.73200 0.4324794 54.00 209.62295 0.4411795 113.00 235.52312 0.4367922 172.00 261.16444 0.4324050 55.00 210.06410 0.4411051 114.00 235.95987 0.4367179 173.00 261.59681 0.4323306

" 56.00 210.50516 0.4410308 115.00 236.39656 0.4366435 174.00 262.02910 0.4322563 57.00 210.94616 0.4409564 116.00 236.83316 0.4365692 175.00 262.46132 0.4321819 58.00 211.38708 0.4408820 117.00 237.26969 0.4364948 176.00 262.89346 0.4321076

Attachment #6 ETE-MP-2012-1135 Report Generated on 816/2012 3:06:09 PM Page 15 of 32

.,, 70CHW1 S R.90-/1"

  • PagZ--of5 08/18/2009 Temperature vs. RL ,tance Table Re poi, . o: RJ200908073-001 Page 3 of 3 F Resistance dr/dT 177.00 263.32553 0.4320332 178.00 263.75753 0,4319588 179.00 264.18945 0.4318845 180.00 264.62130 0.4318101 181.00 265.05307 0.4317358 182.00 265.48477 0.4316614 183.00 265.91639 0.4315870 184.00 266.34794 0.4315127 185.00 266.77942 0.4314383 186.00 267.21082 0.4313640 187.00 267.64215 0.4312896 188.00 268.07340 0.4312152 189.00 268.50458 0.4311409 190.00 268.93568 0.4310665 191.00 269.36671 0.4309922 192.00 269.79767 0.4309178 193.00 270.22855 0.4308434 194.00 270.65935 0.4307691 195.00 271.09008 0.4306947 196.00 271.52074 0.4306204 197.00 271.95133 0.4305460 198.00 272.38183 0.4304716 199.00 272.81227 0.4303973 200.00 273.24263 0.4303229 201.00 273.67291 0.4302486 202.00 274.10313 0.4301742 203.00 274.53326 0.4300998 204.00 274.96333 0.4300255 205.00 275.39331 0.4299511 206.00 275.82323 0.4298768 207.00 276.25307 0.4298024 208.00 276.68283 0.4297280 209.00 277.11252 0.4296537 210.00 277.54214 0.4295793 211.00 277.97168 0.4295050 212.00 278.40115 0.4294306

Attachment #6 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 16 of 32 ff,4 c:/ Ito a//"o Report of Calibration Report No: RJ200908072-001 Dominion Nuclear Connecticut Page 1 of 3 Rope Fenry Road Bldg 433, Metrology Laboratory Waterford, CT 06385

-31n.,OD-2 76~3a Model: XS7927PK1 Customer: Dominion Nuclear Connecticut Serial: 1269 6*730 Rope Ferry Road

Description:

RTD PLANT INSTALLED Bldg 433, Metrology Laboratory Waterford, CT 06385 Calibration Range: Limited Received Condition: New Current: 1.0 mA Procedure: MTE 1142E Actual Value UUT (Reference) (Test Sensor) Residuals Method of (C) (Ohms) (C) Realization

-19.92670 183.91050 0.0000 COMP 0.04100 199.86790 0.0000 COMP 25.02480 219.69950 0.0006 COMP 50.01740 239.38870 -0.0004 COMP 75.01330 258.92880 0.0000 COMP 100.01830 278.32550 0.0001 COMP Callendar-Van Dusen Coefficients:

RO = 199.83522 DELTA'= 1.53631 ALPHA = 0,00392705 BETA = -0.14945 Test Equipment Manufacturer Model Description Serial Number Recall Date Hart Scientific 1590 Super Thermometer II A68350 09/03/2009 Hart Scientific 5681 SPRT 1466 02/25/2010 Hart Scientific 7037 Bath, Deep Low-Temp 93046 NCR Notes: Initial calibration to establish baseline data.

Acceptance Criteria: RO = 19 9 .8 p 200.2 ohms Prerequisites rpet: Initial: Usage Review Required: Yes CR#: Pinal'Cahbration Acceptable: Yes/x_. No _

08/06/2009 Technician:

Calibration Date:

Recall Date: 08/01/2029 Temperature: 73.OF Approved By:

Humidity: 38%

Customer Order: 53M20707631 This reportshall not be reproducedexcept in.fidl without written approval ofDominion Nuclear Connecticut.

Attachment #6 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 17 of 32 1.-rg.C/Y1IhW7- o' 08/07/2009 Temperature vs. Resihance Table Report ,: RJ200908072-001 Page Z of 3 drldT F Resistance drldT F Resistance drldT F Resistance 0.4449825 59.00 211.76038 0.4406680 118.00 237.63026 0.4362771 0.00 185.63222 60.00 212.20101 0,4405936 119.00 238.06650 0.4362027 1.00 186.07716 0.4449132 0.4448437 61.00 212.64157 0.4405191 120.00 238.50267 0.4361282 2.00 186.52204 62.00 213.08205 0.4404447 121.00 238.93876 0.4360538 3.00 186.96685 0.4447740 0.4447041 63.00 213.52246 0.4403703 122.00 239.37477 0.4359794 4.00 187.41159 64.00 213.96279 0.4402959 123.00 239.81072 0.4359050 5.00 187.85626 0.4446340 65.00 214.40305 0.4402215 124.00 240.24658 0.4358305 6.00 188.30086 0.4445637 0.4444932 66.00 214.84324 0.4401470 125.00 240,68238 0.4357561 7.00 188.74539 67.00 215.28334 0.4400726 126.00 241.11810 0.4356817 8.00 189,18984 0.4444226 0.4443517 68.00 215.72338 0.4399982 127.00 241.55374 0.4356073 9.00 189.63423 0.4442807 69.00 216.16334 0.4399238 128.00 241.98931 0.4355329 10.00 190.07855 0.4442095 70.00 216.60323 0.4398493 129.00 242.42481 0.4354584 11.00 190.52279 0.4441381 71.00 217.04304 0.4397749 130.00 242.86023 0.4353840 12.00 190.96697 0.4440666 72.00 217.48278 0.4397005 131.00 243.29558 0.4353096 13.00 191.41107 73.00 217.92244 0.4396261 132.00 243.73085 0.4352352 14.00 191.85510 0.4439948 0.4439229 74.00 218.36203 0.4395517 133.00 244.16605 0.4351607 15.00 192.29906 0.4438509 75.00 218.80154 0.4394772 134.00 244.60117 0.4350863 16.00 192.74295 193.18676 0.4437786 76.60 219'.24098 0,4394028 135.00 245,03622 0.4350119 17.00 0.4437062 77.00 219.68035 0.4393284 136.00 245.47119 0.4349375 18.00 193.63050 0.4436337 78.00 220.11964 0.4392540 137.00 245.90609 0.4348631 19.00 194.07417 0.4435610 79.00 220.55886 0.4391795 138.00 246.34092 0.4347886 20.00 194.51777 0.4434881 80.00 220.99800 0.4391051 139.00 246.77567 0.4347142 21.00 194.96129 0.4434151 81.00 221.43707 0.4390307 140.00 247.21035 0.4346398 22.00 195.40475 0.4433420 82.00 221.87606 0,4389563 141.00 247.64495 0.4345654 23.00 195.84812 83.00 222.31498 0.4388819 142.00 248.07948 0.4344909 24.00 196.29143 0.4432687 0.4431952 84.00 222,75383 0.4388074 143.00 248.51393 0.4344165 25.00 196.73466 0.4431216 85.00 223.19260 0.4387330 144.00 248.94831 0.4343421 26.00 197.17782 0.4430479 86.00 223,63129 0.4386586 145.00 249.38262 0.4342677 27.00 197.62091 0.4429741 87.00 224.06991 0.4385842 146.00 249.81685 0.4341933 28.00 .198.06392 198.50685 0,4429001 88.00 224.50846 0.4385097 147.00 250.25100 0.4341188 29.00 198.94972 0.4428260 89.00 224.94693 0.4384353 148.00 *250.68508 0.4340444 30.00 0.4427517 90.00 225.38533 0,4383609 149.00 251.11909 0.4339700 31.00 199.39251 91.00 225.82365 0.4382865 150.00 251.55302 0.4338956 32.00 199.83522 0.4426774 0,4426030 92.00 226.26190 0.4382121 151.00 251.98688 0.4338211 33.00 200.27786 0.4425285 93.00 226.70008 0.4381376 152.00 252.42067 0.4337467 34.00 200.72043 0.4424541 94.00 227.13818 0.4380632 153.00 252.85438 0.4336723 35.00 201.16292 0.4423797 95.00 227.57620 0,4379888 154.00 253.28801 0.4335979 36.00 201.60533 0.4423053 96.00 228.01416 0.4379144 155.00 253.72157 0.4335235 37.00 202.04768 97.00 228.45203 0.4378399 156.00 254.15506 0.4334490 38.00 202.48994 0.4422309 0.4421564 98.00 228.88984 0.4377655 157.00 254.58847 0.4333746 39.00 202.93214 203.37426 0.4420820 99.00 229.32756 0.4376911 158.00 255.02181 0.4333002 40.00 0.4420076 100.00 229,76522 0.4376167 159.00 255.45507 0.4332258 41.00 203.81630 204.25827 0.4419332 101.00 230,20280 0.4375423 160.00 255.88826 0.4331513 42.00 0.4418587 102.00 230.64030 0.4374678 161.00 256.32137 0.4330769 43.00 204.70017 0.4417843 103.00 231.07773 0.4373934 162.00 256.75441 0.4330025 44.00 205.14199 0.4417099 104.00 231.51509 0.4373190 163.00 257.18738 0.4329281 45.00 205.58374 0.4416355 105.00 231.95237 0.4372446 164.00 257.62027 0.4328537 46.00 206.02541 0.4415611 106.00 232.38958 0.4371701 165.00 258.05309 0.4327792 47.00 206.46701 107.00 232.82671 0.4370957 166.00 258.48583 0.4327048 48.00 206.90853 0.4414866 0.4414122 108.00 233.26377 0.4370213 167.00 258.91849 0.4326304 49.00 207.34998 207.79136 0.4413378 109.00 233.70075 0.4369469 168.00 259.35109 0.4325560 50.00 0.4412634 110.00 234.13766 0.4368725 169.00 259.78361 0.4324815 51.00 208.23266 208.67388 0.4411889 111.00 234.57450 0.4367980 170.00 260.21605 0.4324071 52.00 209,11503 0.4411145 112.00 235.01126 0,4367236 171.00 260.64842 0.4323327 53.00 209.55611 0.4410401 113.00 235.44795 0.4366492 172.00 261.08072 0.4322583 54.00 209.99712 0.4409657 114.00 235.88456 0.4365748 173.00 261.51294 0.4321839 55.00 0.4408913 115.00 236.32110 0.4365003 174.00 261.94508 0.4321094 56.00 210.43804 0.4408168 116.00 236.75756 0.4364259 175.00 262.37716 0.4320350 57.00 210.87890 0.4407424 117.00 237.19395 0.4363515 176.00 262.80915 0.4319606 58.00 211.31968

Attachment #6 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 18 of 32 4 m7-e 08/07/2009 Temperature vs. Resx-tance Table Report j: RJ200908072-001 Page 3 of 3

.F Resistance drldT 177.00 263.24108 0.4318862 178.00 263.67293 0.4318117 179.00 264.10470 0.4317373 180.00 264.53640 0.4316629 181.00 264.96803 0.4315885 182.00 265.39958 0.4315141 183.00 265.83106 0.4314396 184.00 266.26246 0.4313652 185.00 266.69379 0.4312908 186.00 267.12504 0.4312164 187.00 267.55622 0.4311419 188.00 267.98732 0.4310675 189.00 268.41835 0.4309931 190.00 268.84931 0.4309187 191.00 269.28019 0.4308443 192.00 269.71100 0.4307698 193.00 270.14173 0.4306954 194.00 270.57239 0.4306210 195.00 271.00297 0.4305466 196.00 271.43348 0.4304721 197.00 271.86392 0.4303977 198.00 272.29428 0.4303233 199.00 272.72456 0.4302489 200.00 273.15477 0.4301745 201.00 273.58491 0,4301000 202.00 274.01498 0.4300256 203.00 274.44496 0.4299512 204.00 274.87488 0.4298768 205.00 275.30472 0.4298023 206.00 275.73448 0.4297279 207.00 276.16417 0.4296535 208.00 276.59379 0.4295791 209.00 277.02333 0.4295047 210.00 277.45280 0.4294302 211.00 277.88219 0.4293558 212.00 278.31151 0.4292814

Attachment #7 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 19 of 32 Sensor Calculator - Resistance table generator 9,'f'466Il /9 6 Page 1 of 1 PJ c~ R WE Search MINCO Home Products Applications Resources About Us Table Options Select Element Start Over Interchangeability Quick Calc Gen Temperature Vs. Resistance PLATINUM: PIA TCR = 3.93e-3 Ro = 199.872 A4 =-0.00036445181 B4 =-2.8576799E-06 A8 =-0.00040758054 B8 = 8.3733738E-05 Values are in Ohms Temp +0 +1 +2 +3 +4 +5 +6 +7 +8 +9

-F 0 185.6584186.1035186.548 186.9934187.4383187.8831 188.3278188.772 189.2170189.661.

10 190.1059 190.5502190.9945 191.4387 191.882 192.3268192.7708193.2147 193.658 194.102 20 194.5459 194.9895195.4330 195.8765 196.3198196.7631197.2063 197.6495 198.092 198.5355 30 198.9784.199.4213199.8640 200.3067 200.7493 201.1918 201.6343 202.0766 202.5189 202.9611 40 203.40331203.8454 204.2873 204.72931205.1711 205.612 206.0546206.496 206.9377 207.3792 50 207.82061208.2619 208.703 209.14431209.585 210.0265 210.467 210.908 211.3491211.7898 60 212.230 212.6710213.1115213.5520213.9923214.4326214.8728215.312 215.7530216.1929 70 216.63281217.0727 217.5124 217.9521 218.3917 218.8312219.2707 219.7101 220.1494 220.5886 80 -1221.02781221.46681221.905 222.3448222.7837223.222 223.6611224.0998224.5383224.9768 1.90 1225.41521225.8536 226.291 _226.7300 227.1681227.6062 228.0442228.4821 228.919 229.3576 Temp +0 +1 +2 +3 +4 +6 +9 100 229.7953 1 1 1

© 2011 Minco, All Rights Reserved Flexible Heaters I Flex Circuits J Sensors I Instruments I Careers I Privacy Policy I http://www.minco.com/tools/sensorcalc/rtd/display.aspx?action=options 08/06/2012

Attachment #7 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 20 of 32 19 1-M1/14ý0i&A17 e p4wr&z i 01,3--

Serial # 1269 ITS-90 Met Lab Error Error TEMP F R (ohms) R (ohms) Error(ohms)  % Reading %Span 0 185.6584 185.63222 0.02618 0.0141 0.032 5 187.8831 187.85626 0.02684 0.0143 0.032 10 190.1059 190.07855 0.02735 0.0144 0.033 15 192.3268 192.29906 0.02774 0.0144 0.033 20 194.5459 194.51777 0.02813 0.0145 0.033 25 196.7631 196.73466 0.02844 0.0145 0.033 30 198.9784 198.94972 0.02868 0.0144 0.033 35 201.1918 201.16292 0.02888 0.0144 0.033 40 203.4033 203.37426 0.02904 0.0143 0.032 45 205.6129 205.58374 0.02916 0.0142 0.032 50 207.8206 207.79136 0.02924 0.0141 0.032 55 210.0265 209.99712 0.02938 0.0140 0.032 60 212.2305 212.20101 0.02949 0.0139 0.031 65 214.4326 214.40305 0.02955 0.0138 0.031 70 216.6328 216.60323 0.02957 0.0136 0.031 75 218.8312 218.80154 0.02966 0.0136 0.031 80 221.0278 220.998 0.0298 0.0135 0.031 85 223.2224 223.1926 0.0298 0.0133 0.030 90 225.4152 225.38533 0.02987 0.0133 0.030 95 227.6062 227.5762 0.03 0.0132 0.030 100 229.7953 229.76522 0.03008 0.0131 0.030 span 44.1369 Certified by Minco in 1993 Met Lab Cal performed in 2009 16 years between Minco and Met Lab Reports repeatability Drift 16 year drift RSS drift & repeatability 0.01% .05deg C/yr 0.36 0.3604

3 Serial # 1269 ITS-90 VS MET LAB 230 -

225 -

m iq 220

-a IZ 215 E

210 0 C 0D

-ITS TOCaliData0 205 -M LAB Cal Data C 200 195 190 .*

0 10 20 30 40 50 60 70 80 90 100 Temperature (Deg F)

CD 0

(-3 N)

3 Serial # 1269 ITS-90 VS MET LAB

.220 219.8 m

--A 219.6 219.4 CA, 219.2 0

CD

0) 0 219 *~ITS9!0 Cal Data P.

-M LAB Cal Data 218.8 218.6 (C,

218.4 218.2 218 74 74.2 74.4 74.6 74.8 75 75.2 75.4 75.6 75.8 76 Temperature (Deg F)

QI-V CD to (00 w

N3

Attachment #7 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 23 of 32

,,# jrf9-6'41&A/F f Sensor Calculator - Resistance table generator Page 1 of 1 Sý,.,rCNO\ 1-L-)

Search I If MINCO Home Products Applications i Resources i About Us Table Options Select Element Start Over Interchangeability Quick Calc Gen.

Temperature Vs. Resistance PLATINUM: PIA TCR = 3.93e-3 R0 = 199.904 A4 = -0.00033185991 B4 = -2.9061316E-06 A8 = -0.00054864581 B8 = 0.00010006569 Values are in Ohms Temp +0 +1 +2 +3 +4 +5 +6 +7 +8 +9 oF I 0 185.6876186.132 186,577 187,0229187.4679187.9128188.3576188.8023189.2469189.6915 10 190.1360190.5804 191.0248191.4691 191.9133192.3574 192.8014 193.2454193.6893194.1331 20 194.576 195.020 195.4642195.9077196.3511196.7945197.237 197.6810198.1242 198.5673 30 199.0103199.453 199,8960200.3387 200.7813201.2238201.6663202.1087202.5510202.9932 40 203.4354 203.8774 204.3194 204.7614205.2032205.6450206.086 206.5283 206.9699207.4114 50 207.8528 208.2941 208.735 4209.1765 209.6176210.0587 210.4996(210.9405211.3813211.8220 60 212.2627 212.7033 213.1438213.5842214.0246214.4649214,9051215.3452215.7853216.2253 70 216.6652217.105 217.5448217.9845 218.4241218.863 219.30311219.7425220.1818220.6210 80 221.060 221.4993,221.9383 222.3773222.8161223.2549223.6936 224.1323 224.5709 225.0094 90 225.4478 225,8861 *226.3244 226.7626 227.2007 227.63881228.0768 228.5141228.9525 229.3903 Temp +0 +I1 +2 +3 +4 +5 +6 +7 +8 +9 Fo 100 1229.8279

© 2011 Minco, All Rights Reserved Flexible Heaters I Flex Circuits I Sensors I Instruments I Careers I Privacy Policy I http://www.niinco.com/tools/sensorcalc/rtd/display.aspx?action=options 08/06/2012

Attachment #7 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM -Page 24 of 32 Serial # 1270 ITS-90 Met Lab Error Error TEMP F R (ohms) R (ohms) Error(ohms)  % Reading  % Span 0 185.6876 185.69151 -0.00391 -0.0021 -0.005 5 187.9128 187.91628 -0.00348 -0.0019 -0.004 10 190.1360 190.13928 -0.00328 -0.0017 -0.004 15 192.3574 192.36050 -0.0031 -0.0016 -0.004 20 194.5769 194.57990 -0.003 -0.0015 -0.003 25 196.7945 196.79749 -0.00299 -0.0015 -0.003 30 199.0103 199.01323 -0.00293 -0.0015 -0.003 35 201.2238 201.22712 -0.00332 -0.0016 -0.004 40 203.4354 203.43915 -0.00375 -0.0018 -0.004 45 205.6450 205.64933 -0.00433 -0.0021 -0.005 50 207.8528 207.85764 -0.00484 -0.0023 -0.005 55 210.0587 210.06410 -0.0054 -0.0026 -0.006 60 212.2627 212.26869 -0.00599 -0.0028 -0.006 65 214.4649 214.47143 -0.00653 -0.0030 -0.007 70 216.6652 216.67231 -0.00711 -0.0033 -0.007 75 218.8636 218.87133 -0.00773 -0.0035 -0.008 80 221.0602 221.06849 -0.00829 -0.0038 -0.008 85 223.2549 223.26379 -0.00889 -0.0040 -0.009 90 225.4478 225.45723 -0.00943 -0.0042 -0.009 95 227.6388 227.64881 -0.01001 -0.0044 -0.010 100 229.8279 229.83854 -0.01064 -0.0046 -0.010 span 44.1403 Certified by Minco in 1993 Met Lab Cal performed in 2009 16 years between Minco and Met Lab Reports repeatability Drift 16 year drift RSS drift & repeatability 0.01% .05deg C/yr 0.36 0.3604

C)

CD Serial # 1270 ITS-90 VS MET LAB 230.0000 225.0000 M-i 220.0000

-. 215.0000 E

CD 210.0000 C)

C)

- ITS O Cal Data CD 205.0000 M ETLAB Cal Data 0

3 200.0000 0

195.0000 0)

N 190.0000 185.0000 0 10 20 30 40 50 60 70 80 90 100 Temperature (Deg F)

ID C)

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0 N)

LAB METVS ITS-901270

  1. Serial 0

0 Serial # 1270 ITS-90 VS MET LAB 220.0000 219.8000 m

-I 219.6000 m

-u N,

0 219.4000 N, C71 0 219.2000 0 a,

U 0 (0

  • '- ITS! 10Cal Data 00 219.0000 0

a) so- METLAB Cal Data 0 0.

218.8000 0 co N,

0 218.6000 N, Co 0

0) 218.4000 6 CD 218.2000

  • 4, 218.0000 74 74.2 74.4 74.6 74.8 75 75.2 75.4 75.6 75.8 76 Temperature (Deg F)

(D 0

Co N,

Attachment #7 ETE-MP-2012-1135 Report Generated on 816/2012 3:06:09 PM Page 27 of 32 Sensor Calculator - Resistance table generator Page 1 of 1

/'A 1 66 2 -,3Zý Faý Search~

MINCO Home Products I Applications Resources 1 About Us C Table Options Select Element Start Over Interchangeability Quick Calc Genej Temperature Vs. Resistance PLATINUM, PIA TCR = 3.93e-3 Ro = 200.008 A4 =-0.00060597493 B4 = 0.0003131495 AB =-0.00045088398 Ba =0.00014870006 Values are in Ohms emp +0 +1 +2 +3 +4 +5 +6 +7 +8 +9 0

F *_

0 185.7885186.2337186.6789 187.1241187.5691188.0141188.4590188.9038189.3485189.7932 10 190.2378190.6823191.1267191.5711192.015 192.459 192.9038193.3478193.7918194.2358 20 194.6796195.1234195.5671196.0107 196.4543 196.8978 197.3412 197.7845 198.2277 198.6709 30 199.1140,199.55711200.0000 200.4430.200.8859 201.3287.201.7714 202.2140 202.6566 203.0991 40 203.5415 203.9839 204.42621204.8684 205.3105205.7526 206.1945 206.6364 207.0783 207.5200 50 207.9617 208.40331208.8448 209.28631209.7277 210.1690 210.610 211.0514 211.4924 211.9334 60 212.3744 212.8152 213.2560213.6967 214.1374 214.5779 215.0184 215.4588 215.8992 216.339 70 216.7796217.2197 217.65981218.0997 218.5396 218.9794 219.4192219.8588220.298 220.737 80 221.177 221.6168 222.05611222.49532 22.9344 223.3735 223.8125 224.2514 224.6903 225.129 90 225.5677 226.0064 226.444 226.8834 227.3218 227.7601 228.198 228.6366 229.0747 229.512 Temp +0 +1 +2 +3 +4 +5 +6 +7 +8 +9 100 1 229.9507 +1 1 171

@2011 Minco, All Rights Reserved Flexible Heaters I Flex Circuits I Sensors I Instruments I Careers I Privacy Policy J Sit http://www.minco.com/tools/sensorcalc/rtd/display.aspx?action-options 08/06/2012

Attachment #7 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 28 of 32 J9 6Z8 ot 31.

Serial # 1309 ITS-90 Met Lab Error Error TEMP F R (ohms) R (ohms) Error(ohms)  % Reading  % Span 0 185.7885 185.78069 0.00781 0.0042 0.010 5 188.0141 187.98560 0.0285 0.0152 0.034 10 190.2378 190.19543 0.04237 0.0223 0.050 15 192.4596 192.40868 0.05092 0.0265 0.060 20 194.6796 194.62397 0.05563 0.0286 0.065 25 196.8978 196.84003 0.05777 0.0293 0.066 30 199.1140 199.05569 0.05831 0.0293 0.066 35 201.3287 201.26991 0.05879 0.0292 0.066 40 203.5415 203.48228 0.05922 0.0291 0.066 45 205.7526 205.69278 0.05982 0.0291 0.066 50 207.9617 207.90141 0.06029 0.0290 0.066 55 210.1690 210.10817 0.06083 0.0289 0.066 60 212.3744 212.31306 0.06134 0.0289 0.065 65 214.5779 214.51608 0.06182 0.0288 0.065 70 216.7796 216.71724 0.06236 0.0288 0.065 75 218.9794 218.91653 0.06287 0.0287 0.065 80 221.1774 221.11395 0.06345 0.0287 0.065 85 223.3735 223.30950 0.064 0.0287 0.065 90 225.5677 225.50319 0.06451 0.0286 0.065 95 227.7601 227.69500 0.0651 0.0286 0.065 100 229.9507 229.88495 0.06575 0.0286 0.065 span 44.1622 Certified by Minco in 2000 Met Lab Cal performed in 2009 16 years between Minco and Met Lab Reports repeatability Drift 9 year drift RSS drift & repeatability 0.01% .05deg C/yr 0.27 0.2706

0

7 Serial # 1309 ITS-90 VS MET LAB 230.0000 225.0000

,m 220.0000 CD

-t 215.0000 E G)

Co 0

0 210.0000 M

0

-ITS 0 Cal Data CD cz 205.0000 0

=ME" LAB Cal Data C.

0L 200.0000 195.0000 190.0000 185-0000 0 10 20 .30 40 50 60 70 80 90 100 Temperature (Deg F)

"0 (0

0

0 3

Serial # 1309 ITS-90 VS MET LAB 220.0000 219.8000 219.6000 219.4000 0

2.

o 219.2000 U 0b S219.0000

- MT "0Cal Data 0

________ ~~~~~~~

________ ____~~LAB _________ ~ ~ IVE CalI Data 218.8000 218.6000 C-5)

A 218.4000 218.2000 218.0000 I + I +

74 74.2 74.4 74.6 74.8 75 75.2 75.4 75.6 75.8 76 Temperature (Deg F)

(.0 0

0 CD Nancy M Nowlan (Generation - 6)

From: Anderson, Tereasa [tereasa.anderson@minco.com]

Sent: Monday, July 30, 2012 6:25 PM To: Gus J Filippides (Generation - 6)

Cc: Nancy M Nowlan (Generation - 6)

Subject:

Calibrated info reference REQ acc rating to old PO# 932995, Gus from DOM!

Attachments: TS102(N)_L-6.pdf; S7927.pdf

Gus, I just now got it from engineering.

"Somewhere, I seem to have missed the original request for a 0.025°C accuracy guarantee. I have attached an old catalog page that describes the different _*

m calibration tables, and their associated accuracy. Please note that their probe model (57927) is not listed in this table (it had already been discontinued whenT the catalog was published). However, calibration table RT01 is listed as being accurate to +/-0.025°C. I have also attached the S7927 specification drawing that provides repeatability and stability for this model.

You may notice that the model number listed on the calibration certs is "XS7927PK ". The "X" prefix designates an alteration of some sort from the standard

--  :;0 design. In this case, "X" stands for a 200-ohm platinum element. That does not affect table calibration accuracy, nor repeatability, nor stability."

CD Thank you!

TereasaAnderson I Customer Service Representative I Minco Products Tel: 763.586.2920 I Fax: 763-571-0927 Tereasa.anderson@minco.com 0 7300 Commerce Lane I Minneapolis, MN 55432 wwW .rn nc0, corn co From: Gus J Filippides [1]

Sent: Monday, July 30, 2012 10:28 AM To: Anderson, Tereasa Cc: Nancy M Nowlan

Subject:

FW: Calibrated info reference to old PO# 932995, Gus from DOM!

Hello Tereasa, Did you get a response to my follow up question that I sent last week. The calibration reports do not cite any acceptance criteria for the RTDs, ie 0.025 degrees F uncertainty.

What is the accuracy of the RTDs in question that were supplied to us?

CD 1 C.,

0

Attachment #8 ETE-MP-2012-1135 Report Generated on 8/6/2012 3:06:09 PM Page 32 of 32 Ref&nc~1Thiiriieters Calibration furnishes the actual fixed point val- reads 1.77328 at 2001C. A ratio like Minco's fully equipped standards lab ues and the resulting coefficients. this tends to remain more stable over can calibrate and furnish Individual time than an absolute resistance.

tables for any thermometer in this Comparison calibrations You can periodically recheck Rooc in bulletin. All temperatures are based Used for oil filled thermometers, an ice bath and use the latest value on ITS-90. There are two types of comparison calibrations match the for ratio calculation.

calibration: thermometer to be measured against an NIST traceable standard, rather RTD calculations Fixed point calibrations than fixed points. Minco offers two options to create These calibrations use measurements and print RTD tables. You can taken at points derived from physical Absolute vs ratio tables download the DOS PC program constants, such as the triple point of Tables may list either absolute resis- "RTD Cailc" for use on your com-water or the freezing point of tin. tance values (RT vs T) or resistance puter. We also offer "SensorCalc", an The observed values are used to cal- ratios (R-t/Ro vs T) indexed to 1. For on-line tool for creating, printing and culate coefficients for the interpolat- example, if the absolute values of a saving RTD tables. Both are available ing equations of ITS-90. In addition thermometer are 177.47 Q at 200 0 C at www mincn.com/support.

to the comniete R vs T table. Minco and 100.08 9 at 01C, the ratio table Thermometer model (accuracy specifications may vary for other models)

S9688-S9691 S7924, S7928 $7929 S9762 S1059 S7932-S7933 S79253 Type of calibration Fixed point Fixed point Fixed point Fixed point Comparison Fixed point

-189 to -189to -189 to -269 to -189 to -189 to Temperature range 500oM 500OC 660o0 260°0 2600C -100 to 25000 64000 Ordering number for tables RT vs T, 10C Increments RT05 RT05 RT16 RT01 RT09 RT12 ir/R0 vs T, 10C Increments RT06 RT06 RT17 RT02 RTlO RT13 1

RT vs T, O.10C Increments RT07 RT18 RT11 RT03 RT14 Rr/Ro vs T, 0.1 *C Increments RT08 RT19 RT04 RTI5 Table accuracy +/-0.0250C +/-0,02500 +/-0.0250C +/-0.025 +/-0.0250C +/-0.03500 +/-0.0250C Data points supplied

-268.95*C (4.2K): BP helium*

-189.340C : TP of argon2

-50"C, -25°C, 175"*3

-38.830C : TP of mercury2 __*_*

0.01°C :Triple Point of water .

2 100'C: BP water _ _ _

231.928°C : FP tin .....

419.5270C: FP zinc 660.323°C : FP aluminum (+0.05-0) 1 Cryogenic calibrations available on special order. 2 Comparison calibration measurement.

3 S7924, S7925 calibrations based on IEC 751, not ITS-90 The Minco strain-free element Minco precision thermometers rely on a unique element de-sign for superior precision. It consists of a helical coil of plati-num wire, spiraled onto a grooved ceramic bobbin. This con-struction gives more support to the coils than "birdcage" designs, but does not stress the element during thermal ex-pansion. The result is stable and repeatable measurements under a variety of conditions.

1-763-571-0927 Web: www.minoo.com Bulletin TS-102 Page L-6 Page L-6 Mmcv Sales:

Minco 1-763-571-3121 Fax:

Sales: 1-763-571-3121 Fax. 1-763-571-0927 Web: www.minco.com Bulletin TS-102

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