Text

EP-HPT-104, Nasa, Survey Unit Release Record - Part 2
	ML073550692
Person / Time
Site:	Plum Brook File:National Aeronautics and Space Administration icon.png
Issue date:	11/01/2007
From:	; US National Aeronautics & Space Admin (NASA)
To:	; NRC/RGN-III/DNMS/DB
References
	EP-HPT-104
	Download: ML073550692 (85)
	v • d • e

SECTION 7 ATTACHMENT 4 84 PAGES

SUMMARY

RADIATION PROTECTION SURVEY FORM Pagelof 1 e rates in p r h unless otherwise noted H P ~

FldW u v e L 0 - Smear location LAS - Large area smear RP-005 1 1

RADIATION PROTECTION SURVEY FORM Page 1 of \\

RP-005 / 1 Rev. 0

I DCGL,,

I 2.2 I

DCGL 1

3.3 SR-36 SAMPLE RESULTS I

I I

MDA 1

MDA I

Cs-137 1

C0-60 Sample Log #I Sample # I Location I Weight (g) I PC~~I I 20 pcug 1

20 1

% Unlty I Cs:Co r

pcilg PB07-02360-T I SR36-1 I HPT-1 Slice I Top 1

89.0 1

cMDA I

<MDA I

cMDA I

0%

I N/A I 1.90E-02 I 1.30E-02 PB07-07361-T I SR36-1 I Remunt af 2360-T I 89 0 I 379E-01 I

1 64E-01 I cMDA I

cMDA 1

17%

1 NlA I

I PB07-02360-8 SR36-1 HPT-I Slice I Bottom 89.0 5.24E-01 1.55E-01 cMDA cMDA 24%

NIA 1.26E-01 PB07-02362-T SR36-I HPT-1 Slice 2 Top 88.1

<MDA 4 D A cMDA cMDA 0%

NIA 9.9lE-02 l.llE-01 PB07-02362-8 SR36-1 HPT-1 Slice 2 Bottom 88.1

<MDA cMDA cMDA cMDA 0%

N/A 1.18E-01 1.11E-01 I

CS-137 I C0-60 1

Number 40 7

7 2

2 42 2

35 40 Max 258.2 4.93E+00 5.13E-01 6.07E-01 1.60E-01 242%

16.4 l.99E-01 2.20E-01 A v ~

100.0 2.42E+00 2.71E-01 3.91E-01 1.06E-01 19%

12.3 1.15E-01 1.37E-01 SD 37.11 2.09E+00 1.56E-01 3.06E-01 7.63E-02 57%

5.9 3.50E-02 4.57E-02 Conf int +/-

3.96 5.33E-01 3.98E-02 1.46E-01 3.64502 6%

2.8 3.99E-03 4.87E-03

= ~ 5 0 %

Unity

= >I 00% Unity alitative Only analysi

ORTEC g v - i (1087) npp32 G53W3.05 04-ocT-2007 17:10:00 page PBRF spectrum name: ~ ~ 0 7 - 0 3 1 3 1. ~ n l sample description PB07-03131; SR36-3 FROM HPT 104 (CONCAVE);

10/4/07 spectrum ~ilename: \\ \\ ~ b r f - l i b r a r y \\ l i b r a r y data\\Lab\\sA~PLE 0 7 \\ ~ ~ 0 7 - 0 3 1

31. An1

~ c q u i s i ti on i n f o r m a t i o ~

S t a r t time:

Live time:

~ e a l time:

Dead time:

Detector ID:

Detector system

2 DETECTOR (#130) c a l i b r a t i o n F i 1 ename :

P U C ~

73681-773 ( ~ ~ 1 3 0 ) ~ e p t 0 7 Energy Cali b r a t i o n created :

zero o f f s e t :

Gai n :

quadrati c:

~ f f i c i e n c y c a l i b r a t i o n created:

Type :

Uncertai n t y :

c o e f f i c i e n t s :

Library F1:les Ma1 n anal y s i s 1 i brary :

~i brary Match width :

peak s t r i p p i n g :

17-Sep-2007 14:17:46 pol ynomi a1 2.039 %

-0.165998

-4.384815 0.867075

-0.130434 0.008682

-0.000211 plumbrk O l. l i b 0.500 L i brary based npp32 G53w3.05 d S 5 + - 3 % k Z F k V - - j - - - - - -

s t o channel :

I:

8144 ( 2050.66kev )

Pea r e j e c t i o n 1 eve1 :

25.000%

peak search s e n s i t i v i t y :

3 sample Size:

2.5820~+02 A c t i v i t y scaling f a c t o r :

1.0000E+06/(

1.0000E+00*

2.5820E+02)

=

3.8730~+03

~ e t e c t i o n l i m i t method:

Nureg 4.16 and om e r r o r :

systematic e r r o r :

~ r a c t i on L i m i t :

ORTEC g V - i (1087) npp32 G53W3.05 04-OCT-2007 17:10:00 Page Page 1

PBRF PBO7-03131 Spectrum name: PB07-03131.~nl Background width:

best method (based on spectrum).

Hal f 1 i ves decay 1 i m i t :

12.000 A c t i v i t y range factor:

2.000 Min. step backg. energy 0.000 corrections Decay correct t o date:

Decay during acquisition:

Decay during col 1 e c t i on :

True coincidence correction :

peaked background correction:

Absorption (I.nterna1) :

Geometry correction:

Random summi ng :

status YES NO NO NO NO NO NO NO Comments Sep-2007 14 Energy Cali bration Normal i zed d i ff:

S U M M A R Y O F P E A K S I

N R A N G E

+<****

peak Area Uncert FWHM Corrctn

~ u c l i d e Brnch.

Act.

NUC Energy Factor Energy Ratio pCi/g 661.91 1268.

2.90 1.42 3.163E-02 661.66 85.100 4.931E+OO CS137 NO unknown peaks passed s e n s i t i v i t y test.

~ h i s section based on l i b r a r y : plumbrk O l. l i b

- - - - a****** I D E N T I F I E D p E A K s u M M A R y * * * ~ * * *

i r * * * * *

~ u c l i

de Peak centroid ~ackground Net Area I n t e n s i t y Uncert FWHM channel Energy counts counts cts/sec 2 sigma %

kev ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 17:10:00 Page PBRF Spectrum name: P~07-03131.Anl

~ u c l i d e channel Energy

Background

Net area Cnts/sec Uncert EU-154 0.00 1004.72

0.

0.000 0.00 BI-214 0.00 1120.29

0.

0.000 0.00 CO-60 0.00 1173.24

0.

0.000 0.00 Page 2 FWHM 0.000 0.000 0.000

s - Peak f a i l s shape t e s t s.

D - peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E ****"

- Nuclide - Average

peak --------------

Name code ~ c t i v l t y Energy A c t i v i t y code MDA Value PCi /g kev PCi /g PCi /Q COMMENTS CS-137 I

4.9313E+OO 661.66 4.931E+OO

( 8.303E-02 2.90 G K

( - his peak used i n the nuclide a c t i v i t y average.

- Peak i s too wide, but o n l y one peak i n l i b r a r y.

! - Peak i s p a r t o f a m u l t i l e t and t h i s area went negative d u r i ng deconvo u t i on.

? - Peak i s too narrow.

B

@ - Peak i s too wide a t FW25M, but ok a t FWHM.

% - Peak f a i l s s e n s i t i v i t y t e s t.

$ - Peak i d e n t i f i e d, b u t f i r s t peak o f t h i s nuclide f a i 1 ed one o r more qua1 i fi cation t e s t s.

+ - Peak a c t i v i t y higher than counting uncertainty range.

- - peak a c t i v i t y lower than counting uncertainty range.

= - peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o the 1 i brary energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

P - peakbackground subtraction

) - Peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

~ u c l i

de codes :

T - ~ h e r m a l Neutron ~ c t i v a t i o n F - Fast Neutron A c t i v a t i o n I

- ~ i s s i o n product N - Naturally Occurring Isotope P - photon ~ e a c t i o n c - charged P a r t i c l e Reaction M - NO MDA Calcul a t l o n 0

Peak codes:

G - Gamma Ray x - X - ~ a y P - Positron Decay S - Sin l e - ~ s c a p e D - DOU il l e - ~ s c a p e K - Key Line A - Not i n Average

- - - - - - u ~ ~ ~ ~ q ~ - - - i ~ r r p p S L ~. ~ - ~ ~ - 2 6 6 7 - f f : ~ - B a g e - - - - k - -

PBRF Spectrum name: PB07-03131.Anl R - coincidence corrected H - ~ a l f l i f e l i m i t exceeded c - coincidence peak S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

~ i m e of count Time corrected Uncertainty 2 Sigma Nucl i de ti v i t y Act1 v l t y Counting Total PCi /g P C ~

/g PC! /g p c i /g MDA K-40 B<

7.6749E-01 7.6749E-01 Page 3

PB07-03131 CO-60 B<

4.3199E-02 4.3309E-02 Ag-l08mB<

6.3946E-02 6.3948E-02 CS-137 4.929OE+OO 4.9313E+OO 2.8557E-01 EU-152 B<

1.7498E-01 1.7515E-01 EU-154 B<

5.3941E-02 5.4026E-02 PB-212 B<

9.5514E-02 9.5514E-02 PB-214 B<

1.5445~-01 1.5445~-01 BI-212 B<

8.6076E-01 8.6076E-01 BI-214 B<

1.2875E-01 1.2875E-01 RA-226 B<

1.1127E+00 1.1127E+00 TH-234 B<

1.0207E+00 1.0207E+00 U-235 B<

3.5563E-01 3.5563E-01 AM-241 B<

9.5258E-02 9.5261E-02

< - MDA value printed.

A - ~ c t i v i t y printed, but a c t i v i t y < MDA.

B - ~ c t i v i t y

< MDA and f a i l e d t e s t.

c - Area < C r i ti cal l e v e l.

F - Failed f r a c t i o n o r key l i n e t e s t.

H - H a l f l i f e 1 i m i t exceeded S U M M A R Y Total A c t i v i t y (

39.3 t o 2050.7 kev) 4.9290481E+00 pCi/g Total Decayed 2549E+OO pCi /g

~ n a l yzed by :

R ~ V <

ewed by :

R. Case

~aboratory: PBRF Page 4

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 17:12:15 Page 1

PBRF Spectrum name: ~B07-03131-0.~nl sample description PB07-03131-0; SR36-3 FROM HPT 104 (CONVEX);

10/4/07 spectrum Filename: \\ \\ ~ b r f - l i b r a r y \\ l i b r a r y data\\Lab\\SAMPLE 07\\pB07-031 31-O. Anl A C ~ U ~

s i ti on information s t a r t time:

Live time:

Real ti me :

Dead ti me :

Detector ID:

Detector system

2 DETECTOR (#130) cal i b r a t i on

~i 1 ename :

P U C ~

73681-773 (MC130) Sept07 Energy c a l i b r a t i o n Created :

zero o f f s e t :

Gain:

quadratic:

~ f f i c i ency c a l i b r a t i o n created :

Type :

Uncertai nty:

c o e f f i c i e n t s :

Library ~i 1 es Main analysis 1 i brary:

~i brary Match width :

peak stripping:

COPY 17-Sep-2007 13:44:06 0.279 kev 0.252 kev/channel 2.284~-08 kev/channelA2 17-Sep-2007 14:17:46 pol ynomi a1 plumbrk 0 l. l i b 0.500 Library based Anal ysi s parameters Anal y s ~

s engi ne:

npp32 G53W3.05

-tart cnannel:

- 3 9 ? 5 " k p 3 j - -

sto channel:

8144 ( 2050: 66kev )

PeaR r e j e c t i o n 1 eve1 :

25.000%

peak search sensi t ~ v i t y :

3 sample S ~ z e :

2.5820~+02

~ c t i v i t y sca1 i ng f a c t o r :

1.0000~+06/( 1.0000~+00* 2.5820~+02) =

3.8730~t03

~ e t e c t i on 1 i m i t method :

Nureg 4.16 n and om error:

systematic error:

~ r a c t i on L i rnl t :

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 17:12:15 Page 2

Page 1

PBRF PB07-03131-0 spectrum name: ~B07-03131-O.~nl

~ackground width:

~ a 1 f 1 i ves decay 1 i m i t :

A c t i v i t y range f a c t o r :

Min. step backg. energy best method (based on spectrum).

corrections Decay c o r r e c t t o date:

Decay during acqui s i ti on :

Decay during c o l l e c t i o n :

True coi n c i dence correction :

peaked background correction :

~ b s o r p t i o n (Internal) :

Geometry correction:

Random summi ng :

status YES NO NO NO NO NO NO NO comments 27-sep-2007 14:08:00 Energy c a l i b r a t i o n Normalized d i f f :

S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area Uncert FWHM Corrctn Nuclide Brnch.

Act.

Nuc Energy Factor Energy Ratio pCi/g 661.88 735.

3.74 1.35 3.163E-02 661.66 85.100 2.858E+OO CS137 1173.67

37.

16.44 0.63 1.964E-02 1173.24 99.974 1.977E-01 C060 1333.19

26.

24.68 0.61 1.786E-02 1332.50 99.986 1.508E-01 C060 NO unknown peaks passed s e n s i t i v i t y t e s t.

This section based on l i b r a r y : plumbrk 0 l. l i b

n***t+:ana**** I D E N T I F I E D p E A K s u M M A R y * * + r *

f i * * * " * * *

N U C ~ ~

de peak c e n t r o i d Background Net Area I n t e n s i t y Uncert FWHM channel Energy Counts counts Cts/Sec 2 Sigma %

kev ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 17:12:15 page 3

PBRF spectrum name: P~07-03131-O.Anl

~ u c l i d e channel Energy Background Net area Cnts/sec Uncert FWHM EU-154 0.00 723.30

0.

0.000 0.00 0.000 BI-212 0.00 727.33

0.

0.000 0.00 0.000 EU-154 0.00 1004.72

0.

0.000 0.00 0.000 Page 2

s - Peak f a i l s shape t e s t s.

D - Peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E *****

- Nuclide - Average

peak --------------

Name code A c t i v i t y Energy

~ c t i v i t y code MDA Value P C ~

/g kev P C ~

/g P C ~

/g COMMENTS CO-60 CS-137 I

2.8578E+OO 661.66 2.858E+OO

( 4.753E-02

( - This peak used i n t h e nuclide a c t i v i t y average.

- peak i s too wide, but o n l y one peak i n l i b r a r y.

! - peak i s p a r t o f a m u l t i l e t and t h i s area went C

negative d u r i ng deconvo u t i o n.

? - Peak i s too narrow.

@ - Peak i s too wide a t FW25M, but ok a t FWHM.

% - peak f a i l s s e n s i t i v i t y t e s t.

$ - peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i l e d one o r more q u a l i f i c a t i o n t e s t s.

+ - Peak a c t i v i t y higher than counting uncertainty range.

- - Peak a c t i v i t y lower than counting uncertainty range.

= - peak outside analysis energy range.

& - calculated peak c e n t r o i d i s not close enough t o the 1 i brary energy centroid. f o r p o s i t i v e i d e n t i f i c a t i o n.

P - Peakbackground subtraction 3 - peak i s t o o close t o another f o r t h e a c t i v i t y t o be found d i r e c t l y.

~ u c l i

de codes :

peak codes:

T - ~ h e r m a l Neutron A c t i v a t i o n G - Gamma Ray F - Fast Neutron A c t i v a t i o n x - X - ~ a y 0

PBRF ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 17:12:15 Page 4

Spectrum name: PB07-03131-O.Anl I - Fission product P - positron Decay N - ~ a t u r a l l y occurring Isotope s - s i n l e - ~ s c a p e P - photon Reaction D - DOU # l e - ~ s c a p e c - charged p a r t i c l e ~ e a c t i o n K - Key ~ i n e M - NO MDA c a l c u l a t i o n A - ~ o t i n Average R - coincidence corrected C - coincidence peak H - ~ a l f l i

f e l i m i t exceeded S U M M A R Y O F N U C L I D E S I

N S A M P L E **"**

Page 3

PBO7-03131-0 Time o f Count

~ i m e corrected Uncertainty 2 Sigma

~ u c l i

de A c t i v j t y A c t i v i t y counting Total P C ~

/g P C ~

/g MDA

- ~ 1 1 peaks f o r a c t i v i t y calculation had bad shape.

- A c t i v i t y omitted from t o t a l

& - ~ c t i v i t y omitted from t o t a l and a11 peaks had bad shape.

< - MDA value printed.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y < MDA and f a i l e d t e s t.

c - Area < C r i t i c a l 1 eve1.

F - ailed f r a c t i o n o r key 1 i n e t e s t.

H - ~ a l f l i f e l i m i t exceeded S U M M A R Y

~ 0 t a l A c t i v i t y (

39.3 t o 2050.7 kev) 3.0303187E+00 pci/g Total ~ecayed 3 t o 2050.7 kev) 3.0320458E+00 pci/g Anal yzed by :

Revi ewed by :

R. Case

~ a b o r a t o r y : PBRF Page 4

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:39:43 Page 1

PBRF Spectrum name: ~ ~ 0 7 - 0 3 1 1 4. a n l sample description PB07-03114; SR38-58; HPT 104; HOLE 1; 19.5; 10/4/07 spectrum Filename: \\ \\ ~ b r f - l i b r a r y \\ l i b r a r y data\\Lab\\SAMPLE 07\\PB07-031 14.Anl Acquisition information s t a r t time:

Dead time:

Detector ID:

Detector system

3 DETECTOR (#I311 c a l i b r a t i o n F i 1 ename:

250ml #73678-773 (Mc131) Sept07 Energy C a l i b r a t i on created:

Zero o f f s e t :

Gain :

Quadratic:

05-Sep-2007 16:56:38 0.565 kev 0.247 kev/channel 5.022E-08 kev/channelA2 Efficiency C a l i b r a t i o n created:

05-Sep-2007 17:17:39 Type :

pol ynomi a1 uncertainty:

1.204 %

Coefficients:

-0.304311

-4.249899 0.669559

-0.094002 0.005803

-0.000133 Library F i l e s Main analysis l i b r a r y :

plumbrk 0 l. l i b

~i brary Match width:

0.500 peak s t r i p p i n g :

Library based analysis parameters Analysis engine:

npp32 G53~3.05 s t a r t channel :

1 5 5 (

38.83kev )

s t o ~

channel :

8144 ( 2014.22kev )

pea r e j e c t 1 on 1 eve1 ;

25.OOO%

Peak search sensitivity:

3 Sample Size:

4.9610~+02 A c t i v i t y scaling f a c t o r :

1.0000E+06/(

l.OOOOE+OOi:

4.9610E+02) =

2.0157E+03

~ e t e c t i o n 1 i m i t method:

Nureg 4.16 Random e r r o r :

1.0000000E+00 Systematic error:

1.OOOOOOOE+OO Fraction ~ i m i t :

0.000%

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:39:43 Page 2

Page 1

PB07-03114 Spectrum name: ~ ~ 0 7 - 0 3 1 1 4. ~ n l Background width:

best method (based on spectrum).

Half l i v e s decay l i m i t :

12.000 A c t i v i t y range factor:

2.000 Min. step backg. energy 0.000 corrections Decay correct t o date:

Decay during acquisition:

Decay durin collection:

True coinci % ence correction:

Peaked background correction:

~ b s o r p t i o n (Internal) :

Geometry correction:

Random summing:

status YES NO NO NO NO NO NO NO comments 27-Sep-2007 11:30:00 Energy Cali bration Normalized d i ff:

0.1653 S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area uncert FWHM Corrctn Nuclide ~ r n c h.

Act.

NUC Energy Factor Energy Ratio pci/g

- - - - U N I D E N T I F I E D P E A K S U M M A R Y ************

Peak centroid sackground Net Area I n t e n s i t y Uncert FWHM Sus ected channel Energy counts Counts cts/sec 2 Sigma% kev Nucyide s - Peak f a i l s shape t e s t s.

D - peak area deconvoluted.

L - peak w r i t t e n from unknown l i s t.

c - Area < c r i t i c a l 1 eve1.

M - Peak i s close t o a l i b r a r y peak.

This section based on l i b r a r y : plumbrk 0 l. l i b 0

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:39:43 Page 3

PERF spectrum name: ~ ~ 0 7 - 0 3 1 1 4. ~ n l

t**tttit*tf*t I D E N T I F I E D P E A K S U M M A R Y "*****"*****"*

Nuclide Peak centroid Background Net Area I n t e n s i t y Uncert FWHM channel Energy Counts counts Cts/Sec 2 Sigma %

kev AM-241 0.00 59.54

0.

0.000 0.00 0.000 Page 2

s - peak f a i l s shape tests.

D - peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E *****

- Nuclide - Average

peak --------------

Name Code A c t i v i t y Energy A c t i v i t y Code MDA value PC? /g kev P C ~

/g P C ~

/g COMMENTS ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:39:43 Page PBRF spectrum name: PB07-03114.nnl Nuclide AVe a c t i v i t y Energy A c t i v i t y code Peak MDA Comments RA-226 N

2.8167E+00 186.21 2.817~+00 ( 1.279E+00 23.89 G K

( - This peak used i n the nuclide a c t i v i t y average.

- peak i s too wide, but only one peak i n l i b r a r y.

! - Peak i s p a r t, o f a m u l t i l e t and t h i s area went negative duri ng deconvoyution.

? - peak i s too narrow.

@ - peak i s t o o wide a t FW25M, but ok a t FWHM.

% - Peak f a i l s s e n s i t i v i t y t e s t.

$ - peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide Page 3

PB07-03114 f a i l e d one o r more q u a l i f i c a t i o n t e s t s.

+ - peak a c t i v i t y higher than counting uncertainty range.

- - Peak a c t i v i t y lower than counting uncertainty range.

- - peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o t h e l i b r a r y energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

P - Peakbackground subtraction 1 - Peak i s t o o close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

Nuclide codes :

peak codes:

T - Thermal Neutron A c t i v a t i o n G - Gamma Ray F - Fast Neutron A c t i v a t i o n x - x - ~ a y I - Fission product P - positron Decay N - Naturally occurring Isotope s - s i n l e Escape P - photon Reaction D - Dou%leIEscape C - charged P a r t i c l e Reaction K - Key ~ i n e M - NO MDA Calculation A - NO^ i n Average R - Coincidence corrected C - coincidence peak H - H a l f l i f e l i m i t exceeded S U M M A R Y O F N U C L I D E S I

N S A M P L E ***$:*

Time o f Count Time corrected Uncertainty 2 sigma

~ u c l i d e n c t i v i t y a c t i v i t y counting Total MDA PC: /g pci /g pci /g pci /g ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:39:43 Page 5

PERF Spectrum name: PB07-03114.Anl

- a l l peaks f o r a c t i v i t y c a l c u l a t i o n had bad shape.

- a c t i v i t y omitted from t o t a l

& - A c t i v i t y omitted from t o t a l and a l l peaks had bad shape.

< - MDA value p r i n t e d.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y < MDA and f a i l e d t e s t.

c - Area < c r i t i c a l l e v e l.

F - Failed f r a c t i o n o r key l i n e t e s t.

H - ~ a l f l i f e l i m i t exceeded S U M M A R Y

~ o t a l A c t i v i t y (

38.8 t o 2014.2 kev) 0.0000000E+00 pci/g Total Decayed A c t i v i t y (

38.8 t o 2014.2 kev) 0.0000000E+00 pCi/g analyzed by:

Page 4

~607-03114 PERF ~ecommi s s i oni ng Project Reviewed by:

supervisor

~ a b o r a t o r y : PBRF Page 5

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:56:08 Page 1

PERF spectrum name: ~ ~ 0 7 - 0 3 1 1 8. a n l sample description

~807-03118; ~ ~ 3 8 - 6 2 ;

HPT 104; HOLE 2; 19; 10/4/07 Spectrum Filename: \\\\pbrf-library\\library data\\Lab\\SnMP~E 07\\PB07-031 18.An1 acquisition information s t a r t time:

Live time:

Real time:

Dead time:

Detector ID:

Detector system

1 DETECTOR (#I291 calibration F i 1 ename:

250ml #73678-773 (MC129)Sept07 Energy c a l i b r a t i o n created:

zero o f f s e t :

Gain :

Quadrati c:

11-Sep-2007 13:44:33

-0.041 kev 0.250 kev/channel

-7.752E-09 kev/channelA2 Efficiency Cali bration created:

11-Sep-2007 14:04:24 Type :

pol ynomi a1 Uncertainty:

1.649 %

coefficients:

-0.312485

-4.205606 0.662739

-0.094204 0.005970

-0.000141 Library F i l e s

~ a i n analysis 1 i brary:

plumbrk 0 l. l i b

~ i b r a r y Match width:

0.500 peak stripping:

~ i b r a r y based i s oarameters analysis engine:

s t a r t channel :

sto channel:

Pear rejection l e v e l :

peak search sensi t i v i t v :

Sample Size:

~ c t i v i t y scaling factor:

~ e t e c t i o n l i m i t method:

Random error:

systematic.error:

Fraction Limit:

0 Nureg 4.16 ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:56:08 Page 2

Page 1

~~07-03118 Spectrum name: PB07-03118.Anl Background width:

best method (based on spectrum).

Half 1 i ves decay 1 i m i t :

12.000 A c t i v i t y range factor:

2.000 in. step backg. energy 0.000 Corrections status Decay correct t o date:

YES Decay during acquisition :

NO comments 27-Sep-2007 15:43:00

~ e c a y duri n coTlection:

NO True coinci ence correction:

NO Peaked backaround correction:

NO

~ b s o r p t i o n { ~ n t e r n a l ) :

NO Geometry correction:

NO Random summing :

NO Energy Calibration Normalized d i ff:

0.1541 S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area Uncert FWHM Corrctn Nuclide srnch.

Act.

NUC Energy Factor Energy Ratio pci/g

- - fr*i:u*r*** " N I D E N T I F I E D p E A K S U M M A R Y f<h*$<**"***""

Peak centroid Background Net Area Intensity Uncert FWHM Suspected channel Energy Counts Counts Cts/Sec 2 Sigma %

kev Nuclide s - peak f a i l s shape tests.

D - peak area deconvoluted.

L - Peak w r i t t e n from unknown l i s t.

c - Area < c r i t i c a l l e v e l.

M - Peak i s close t o a l i b r a r y peak.

This section based on l i b r a r y : plumbrk O l. l i b 0

ORTEC g v - i (1087) npp32 G53W3.05 04-on-2007 11:56:08 Page 3

PERF spectrum name: ~~07-03118.Anl an************

I D E N T I F I E D p E A K s u M M A R y ******h?:**h***

~ u c l i

de peak Centroid sackground Net Area

~ n t e n s i t y Uncert FWHM Channel Energy Counts counts cts/sec 2 Sigma %

kev AM-241 0.00 59.54

0.

0.000 0.00 0.000 TH-234 0.00 63.29

0.

0.000 0.00 0.000 TH-234 0.00 92.59

0.

0.000 0.00 0.000 EU-152 0.00 121.78

0.

0.000 0.00 0.000 EU-154 0.00 123.07

0.

0.000 0.00 0.000 Page 2

s - peak f a i l s shave tests.

D - Peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E

- tic*

- Nuclide - Average

peak --------------

Name code n c t i v l t y Energy A c t i v i t y code MDA value PC< /g kev pci/g p c i /g COMMENTS PB-212 N

2.8922E-01 238.63 2.892E-01

( 1.508E-01 22.64 G K 0

ORTEC g v - i (1087) npp32 G53W3.05 04-oCT-2007 11:56:08 Page PBRF spectrum name: PB07-03118.nnl Nuclide Ave a c t i v i t y Energy A c t i v i t y code Peak MDA Comments

~

- ~ -.

i120.29 o.oooi+oo 3 5.264~-01 0.00 G

( - This peak used i n the nuclide a c t i v i t y average.

- Peak i s too wide, but only one peak i n l i b r a r y.

! - Peak i s p a r t, o f a m u l t i l e t and t h i s area went negative d u r ~ n g deconvoyution.

? - peak i s too narrow.

@ - peak i s too wide a t FW25M, but ok a t FWHM.

96 - peak f a i l s s e n s i t i v i t y t e s t.

$ - Peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i l e d one o r more q u a l i f i c a t i o n tests.

+ - peak a c t i v i t y higher than counting uncertainty range.

Page 3

~~07-03118

- - Peak a c t i v i t y lower than counting uncertainty range.

= - Peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o the l i b r a r v enerav centroid f o r oositive identification.

P - ~eakbackgrouna subtraction

} - Peak i s too close t o another f o r the a c t i v i t y t o be found directly.

Nuclide codes:

peak codes:

T - ~hermal Neutron Activation G - Gamma Ray F - Fast Neutron Activation x - X - ~ a v I - Fission product P - positron Decay N - Naturally occurring Isotope s - s i n l e Escape P - photon Reaction D - Dou%leIEscape C - charged Particle Reaction K - Key ~ i n e M - NO MDA Calculation A - NO^ i n Average R - coincidence corrected c - Coincidence peak H - H a l f l i f e l i m i t exceeded S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

Time o f count Time corrected Uncertainty 2 sigma

~ u c l i d e n c t i v i t y n c t i v i t y counting Total MDA PC1 /g PC: /g pci /g pci /g ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 11:56:08 Page 5

PBRF spectrum name: PB07-03118.Anl

- a l l peaks f o r a c t i v i t y calculation had bad shape.

- A c t i v i t y omitted from t o t a l

& - A c t i v i t y omitted from t o t a l and a l l peaks had bad shape.

< - MDA value printed.

A - A c t i v i t y printed, but.activity < MDA.

B - A c t i v i t y < MDA and f a i l e d test.

c - Area < c r i t i c a l level.

F - Failed fraction or key l i n e test.

H - ~ a l f l i f e l i m i t exceeded S U M M A R Y Total A c t i v i t y (

38.7 t o 2037.3 kev) 0.0000000E+00 pCi/g Total Decayed A c t i v i t y (

38.7 t o 2037.3 kev) 0.0000000E+00 pCi/g Analyzed by:

PBRF Dec0mmi ssi oni ng Project

~eviewed by:

supervisor Laboratory:

PBRF Page 5

ORTEC g v - i (1087) npp32 G53w3.05 04-oC~-2007 12:01:31 Page 1

PBRF Spectrum name: PB07-03119.An1 sample description

~~07-03119; SR38-63; HPT 104; HOLE 2; 21; 10/4/07 spectrum Filename: \\\\Pbrf-library\\library

~ ~ ~ ~ \\ L ~ ~ \\ s A M P L E 07\\P~07-031 19.nnl ncquisition information s t a r t time:

Live time:

Real time:

Dead time:

Detector ID:

Detector system

3 DETECTOR (#131)

Cali bration F i 1 ename:

2501111 #73678-773 (~C131) Sept07 Energy Cali bration Created:

zero o f f s e t :

Gain :

Quadratic:

05-Sep-2007 16:56:38 0.565 kev 0.247 kev/channel 5.022E-08 kev/channelA2 Efficiency Cali bration created:

05-sep-2007 17:17:39 Type :

pol ynomi a1 uncertainty:

1.204 %

coefficients:

-0.304311

-4.249899 0.669559

-0.094002 0.005803

-0.000133

~i brary Files Main analysis 1 i brary:

Library Match width:

peak stripping:

plumbrk 0 l. l i b 0.500 Library based Analysis parameters nnalysi s engine:

npp32 G53W3.05 s t a r t channel :

155 (

38.83keV )

sto channel:

8144 ( 2014.22kev )

Peat rejection 1 eve1 :

25.OOO%

peak search s e n s i t i v i t y :

3 sample size:

4.2590~t02 n c t i v i t y scaling factor:

1.0000~+06/( 1.0000Et00*

4.2590Et02) =

2.3480~t03

~ e t e c t i o n 1 i m i t method:

Nureg 4.16 Random error:

1.0000000E+00 systematic error:

1.0000000~+00

~ r a c t i o n Limit:

0.000%

0 ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 12:01:31 Page 2

Page 1

PBRF PB07-03119 spectrum name: PB07-03119.Anl Background width:

best method (based on spectrum).

~ a l f l i v e s decay 1 i m i t:

12.000 A c t i v i t y range factor:

2.000 Min. step backg. energy 0.000 corrections status comments oecay correct t o date:

YES 27-Sep-2007 15:48:00 Decay during acquisition :

NO Decay during collection:

NO True coincidence correction:

NO peaked background correction:

NO

~ b s o r o t i o n (Internal) :

NO

~ e o m e t r ~

correction:.

NO ando om summing:

NO Energy c a l i b r a t i o n Normalized d i f f :

0.1602 S U M M A R Y O F P E A K S I

N R A N G E

- - - ?<

peak Area Uncert FWHM Corrctn Nuclide srnch.

Act.

NUC Energy Factor Energy Ratio pCi/g Peak centroid sackground Net Area I n t e n s i t y uncert FWHM Sus ected channel Energy Counts counts cts/sec 2 Sigma% kev NucTide s - Peak f a i l s shape tests.

D - peak area deconvoluted.

L - Peak w r i t t e n from unknown l i s t.

c - ~ r e a

< c r i t i c a l l e v e l.

M - peak i s close t o a l i b r a r y peak.

~ h i s section based on l i b r a r y : plumbrk O l. l i b 0

ORTEC g V - i (1087) npp32 G53W3.05 04-OCT-2007 12:01:31 Page J

PBRF spectrum name: ~~07-03119.Anl

a*a****r*nt**

I D E N T I F I E D p E A K s u M M A R y *""*******"***

~ u c l i d e Peak centroid Background Net Area I n t e n s i t y Uncert FWHM channel Energy counts counts Cts/Sec 2 Sigma %

kev AM-241 0.00 59.54

0.

0.000 0.00 0.000 TH-234 0.00 63.29

0.

0.000 0.00 0.000 TH-234 0.00 92.59

0.

0.000 0.00 0.000 EU-152 0.00 121.78

0.

0.000 0.00 0.000 Page 2

s - Peak f a i l s shape tests.

D - peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E *****

- Nuclide - Average

peak --------------

Name Code A c t i v i t y Energy A c t i v i t y code MDA value P C ~

/g kev PC: /g P C ~

/g COMMENTS ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 12:01:31 Page PERF spectrum name: ~ ~ 0 7 - 0 3 1 1 9. n n l Nuclide AVe a c t i v i t y Energy A c t i v i t y code peak MDA comments RA-226 N

4.9214E+00 186.21 4.921E+00 *(

2.015Et00 21.26 G K

( - This peak used i n the nuclide a c t i v i t y average.

- Peak i s too wide, but only one peak i n l i b r a r y.

! - peak i s Dart o f a m u l t i p l e t and t h i s area went negative. during deconvolution.

? - peak i s too narrow.

@ - Peak i s too wide a t FW25M, but ok a t FWHM.

% - Peak f a i l s sensitivity t e s t.

PB07-03119

$ - Peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i l e d one o r more a u a l i f i c a t i o n tests.

t - Peak a c t i v i t y higher than counting uncertainty range.

- - Peak a c t i v i t y lower than counting uncertainty range.

= - peak outside analysis energy range.

& - calculated peak centroid i s not.close enough t o the l i b r a r y energy centroid f o r p o s ~

t i v e i d e n t i f i c a t i o n.

P - peakbackground subtraction

} - Peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

Nuclide codes :

T - Thermal Neutron Activation F - Fast Neutron Activation I

- Fission product N - Naturally occurring Isotope P - Photon Reaction C - charged P a r t i c l e Reaction M - NO MDA calculation R - Coincidence corrected H - H a l f l i f e l i m i t exceeded Peak Codes:

G - Gamma Ray x - X - ~ a y P - Positron Decay S - s i n l e Escape D - Dou%leIEscape K - Key Line A - NO^ i n Average c - coincidence Peak

"*fc"ir S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

Time o f Count Time corrected Uncertainty 2 Sigma

~ u c l i

de

~ c t i v i t y A c t i v i t y Counting Total MDA pci /g pci /g pci /g P C ~

/g ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 12:01:31 Page 5

PBRF Spectrum name: PB07-03119.Anl

- ~ l l peaks f o r a c t i v i t y calculation had bad shape.

- A c t i v i t y omitted from t o t a l

& - A c t i v i t y omitted from t o t a l and a l l peaks had bad shape.

< - MDA value printed.

A - ~ c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y < MDA and f a i l e d t e s t.

c - Area < c r i t i c a l l e v e l.

F - Failed f r a c t i o n o r key l i n e t e s t.

H - H a l f l i f e l i m i t exceeded S " M M A R Y Total A c t i v i t y (

38.8 t o 2014.2 kev) 0.0000000E+00 pCi/g

~ 0 t a l Decayed A c t i v i t y (

38.8 t o 2014.2 kev) 0.0000000E+00

Analyzed by:

PBRF Dec0mmi ssioni ng project Reviewed by:

supervisor Laboratory:

PBRF Page 5

ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 12:04:52 Page 1

PBRF Spectrum name: ~B07-03120.~nl sample description PBO7-03120; SR38-64; HPT 104; HOLE 2; 24.5; 10/4/07 Spectrum ~ilename: \\\\pbrf-library\\library d a t a \\ ~ a b \\ s A ~ ~ ~ ~

0 7 \\ ~ ~ 0 7 - 0 3 1 20.An1 A C ~ U ~

s i t i o n information s t a r t time:

Live time:

Real ti me :

Dead ti me :

Detector ID:

Detector system

I DETECTOR (#129) cal i b r a t i on F i 1 ename :

250ml #73678-773 (MC129)Sept07 Energy Cal i b r a t i on created:

zero o f f s e t :

Gai n :

Quadrati c:

Efficiency Cali bration created:

Type :

uncertai nty :

c o e f f i c i ents :

Library F i 1 es Main anal y s i s 1 i brary :

Library Match width:

Peak stripping:

11-sep-2007 13:44:33

-0.041 kev 0.250 kev/channel

-7.752~-09 kev/channelA2 pol ynomi a1 1.649 %

-0.312485

-4.205606 0.662739

-0.094204 0.005970

-0.000141 plumbrk Ol.1ib 0.500 Library based

~ n a l ysi s parameters Anal ysi s engine:

npp32 G53W3.05 s t a r t channel :

1 5 5 (

38.74kev )

sto channel :

R 8144 ( 2037.25kev )

Pea rejection 1 eve1 :

2 5.000%

peak search s e n s i t i v i t y :

3 Sample Size:

4.3540~+02 A c t i v i t y scaling factor:

1.0000E+06/(

1.0000E+00*

4.3540E+02) =

2.2967E+03

~ e t e c t i o n 1 i m i t method:

Nureg 4.16 Random error:

systematic error:

Fraction Limit :

ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 12:04:52 Page 2

Page 1

PBRF PB07-03120 spectrum name: PB07-03120.~nl Background width:

Hal f 1 i ves decay 1 i m i t :

~ c t i v i t y range f a c t o r :

Min. step backg. energy best method (based on spectrum).

corrections Decay correct t o date:

Decay d u r i ng acqui s i ti on :

Decay d u r i ng col 1 e c t i on :

True coincidence correction :

Peaked background correction:

Absorption (Internal) :

Geometry correction :

and om summi ng :

status YES N 0 N 0 NO NO N 0 NO NO comments 27-Sep-2007 15:54:00 Energy ca1 i b r a t i on Normal i zed d i f f :

S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area uncert FWHM corrctn

~ u c l i d e Brnch.

Act.

NUC Energy Factor Energy Ratio pci/g

- - - - U N I D E N T I F I E D P E A K S U M M A R Y ************

Peak centroid Background Net Area I n t e n s i t y Uncert FWHM Sus ected channel Energy counts Counts Cts/Sec 2 Sigma %

kev NUC 7 i d e s - Peak f a i l s shape t e s t s.

D - peak area deconvoluted.

L - Peak w r i t t e n from unknown l i s t.

c - Area c C r i t i c a l l e v e l.

M - peak i s close t o a 1 i brary peak.

This section based on l i b r a r y : plumbrk 0 l. l i b 0

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 12:04:52 Page 3

PBRF spectrum name: PB07-03120.An1

- - - - 1 D E N T 1 F 1 E D P E A K S U M M A R Y **************

Nuclide peak centroid ~ackground Net Area I n t e n s i t y uncert FWHM channel Energy counts counts Cts/Sec 2 Sigma %

kev Page 2

EU-152 EU-154 U-235 U-235 RA-226 PB-212 EU-152 PB-214 Ag-108m BI-214 Ag-108m EU-154 BI-212 EU-154 CO-60 EU-154 CO-60 EU-152 K-40 s - Peak f a i l s shape tests.

D - Peak area deconvoluted.

A Derived peak area.

g r "

S U M M A R Y O F L I B R A R Y P E A K U S A G E *****

- ~ u c l i d e - Average

peak --------------

Name code A c t i v i t y Energy A c t i v i t y code MDA Value P C ~

/g kev P C ~

/g P C ~

/g COMMENTS ORTEC g V - i (1087) npp32 G53W3.05 04-OCT-2007 12:04:52 Page 4

PBRF Spectrum name: P~07-03120.Anl

~ u c l i d e Ave a c t i v i t y Energy A c t i v i t y code peak MDA Comments

( - This peak used i n the nuclide a c t i v i t y average.

- peak i s too wide, but only one peak i n l i b r a r y.

! - Peak i s p a r t o f a m u l t i l e t and t h i s area went 7

negative duri ng deconvo u t i on.

? - peak i s too narrow.

@ - Peak i s too wide a t FW25M, but ok a t FWHM.

% - peak f a i l s s e n s i t i v i t y t e s t.

$ - peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i l e d one o r more q u a l i f i c a t i o n tests.

+ - peak a c t i v i t y higher than counting uncertainty range.

Page 3

PB07-03120

- - peak a c t i v i t y lower than counting uncertainty range.

- - Peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o the 1 i brary energy centroid f o r p o s i t i v e i d e n t ~

fi cation.

P - Peakbackground subtraction 3 - Peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

~ u c l i

de codes :

T - Thermal Neutron A c t i v a t i o n F - Fast Neutron ~ c t i v a t i o n I - Fission product N - Naturally Occurring Isotope P - Photon Reaction C - charged P a r t i c l e Reaction M - NO MDA c a l c u l a t i o n R - coincidence corrected H - ~ a l f l i f e l i m i t exceeded Peak Codes:

G - Gamma Ray x - x - ~ a y P - Positron Decay S - Single-~scape D - Double-Escape K - Key Line A - ~ o t i n Average C - Coincidence peak S U M M A R Y O F N U C L I D E S I

N S A M P L E

~ i m e o f Count Time corrected Uncertainty 2 Sigma Nucl i de

~ c t i v i t y A c t i v i t y Counting Total pci /g P C ~

/g P C ~

/g pci /g

*

S t

MDA O R T E C g v - i (1087)npp32 G53W3.05 04-OCT-200712:04:52 Page 5

PBRF spectrum name: PB07-03120.Anl

- ~ l l peaks f o r a c t i v i t y c a l c u l a t i o n had bad shape.

- A c t i v i t y omitted from t o t a l

& - ~ c t i v i t y omitted from t o t a l and a l l peaks had bad shape.

< - MDA value p r i n t e d.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - ~ c t i v i t y < MDA and f a i 1 ed t e s t.

c - Area < C r i ti cal l e v e l.

F - Failed f r a c t i o n o r key l i n e t e s t.

H - H a l f l i f e l i m i t exceeded S U M M A R Y

~ 0 t a l

~ c t i v i t y (

38.7 t o 2037.3 kev) 0.0000000E+00 pci/g

~ 0 t a l Decayed A c t i v i t y (

38.7 t o 2037.3 kev) 0.0000000E+00 pCi/g

~ n a l yzed by :

PBRF ~ecommi s s i oni ng project Page 4

PB07-03120

~ e v i ewed by :

supervi sor Laboratory:

PBRF Page 5

ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 12:00:04 Page PBRF Spectrum name: ~B07-03115.~nl sample description PBO7-03115; SR38-59; HPT 104; HOLE 3; 19; 10/4/07 Spectrum Filename: \\\\Pbrf-library\\library d a t a \\ ~ a b \\ s ~ ~ p ~ E 0 7 \\ ~ ~ 0 7 - 0 3 1 1 5.An1 Acquisi t i o n information s t a r t ti me:

Live time:

Real time:

Dead time:

Detector ID:

Detector system

2 DETECTOR (#130) calibration F i 1 ename :

2501111 #73678-773 (MC130)SeptOi' Energy cal i bration created:

zero offset:

Gai n :

quadrati c :

E f f i c i ency calibration created:

Type :

uncertainty:

coefficients:

Library Files Main analysis l i b r a r y :

Library ~ a t c h width:

Peak stripping :

13-Sep-2007 15:00:31 0.287 kev 0.251 kev/channel 2.324~-08 kev/channelA2 pol ynomi a1 1.626 %

-0.256697

-4.334323 0.664302

-0.092291 0.005686

-0.000130 plumbrk Ol.lib 0.500 Library based

~ n a 1 ysi s parameters Anal ysi s engi ne :

npp32 G53w3.05 s t a r t channel :

1 5 5 (

39.27kev )

sto channel:

R 8144 ( 2049.92kev )

Pea rejection 1 eve1 :

25.OOO%

peak search sensitivity:

3 Sample Size:

3.9410~+02

~ c t i v i t y scaling factor:

1.0000~+06/( 1.0000E+00*

3.9410E+02) =

2.5374~+03

~ e t e c t i o n l i m i t method:

Nureg 4.16 and om error:

systematic error:

Fraction Limit :

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 12:00:04 Page 2

Page 1

PBRF PB07-03115 Spectrum name: P~07-03115.~nl Background width:

best method (based on spectrum).

Hal f 1 i ves decay 1 i m i t :

12.000 A c t i v i t y range factor :

2.000 Min. step backg. energy 0.000 corrections status Decay correct t o date:

YES Decay duri ng acqui s i ti on :

N 0 Decay duri ng col 1 e c t i on :

NO True coincidence correction :

NO peaked background correction:

NO Absorption (Internal) :

NO Geometry correction:

NO Random summing :

N 0 comments 27-Sep-2007 16:35:00 Energy calibration

~ 0 r m a l i zed d i ff :

S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area Uncert FWHM Corrctn Nuclide Brnch.

Act.

Nuc Energy Factor Energy Ratio pCi/g

- - - - a****

u N I D E N T I F I E D P E A K s u M M A R y ************

Peak centroid Background Net Area Intensity Uncert FWHM Sus ected channel Energy Counts Counts Cts/Sec 2 Sigma %

kev NUC 7 i d e s - Peak f a i l s shape tests.

D - peak area deconvoluted.

L - Peak written from unknown l i s t.

c - Area < c r i t i c a l 1 eve1.

M - Peak i s close t o a l i b r a r y peak.

This section based on l i b r a r y : plumbrk 0 l. l i b 0

ORTEC g v - i (1087) npp32 G53W3.05 04-0cT-2007 12:00:04 Page 3

PBRF spectrum name: P~07-03115.Anl P E A K Page 2

Nuclide peak centroid channel Energy 0.00 59.54 0.00 63.29 0.00 92.59 0.00 121.78 0.00 123.07 0.00 143.76 0.00 185.71 737.91 185.87 948.02 238.72 0.00 344.28 1397.83 351.87 0.00 433.94 2420.54 609.15 0.00 614.28 0.00 661.66 0.00 722.91 0.00 723.30 0.00 727.33 0.00 1004.72 0.00 1173.24 0.00 1274.44 0.00 1332.50 0.00 1408.01 5803.84 1460.65 PB07-03115

Background

Net Area counts counts Intensity uncert FWHM cts/sec 2 Sigma %

kev 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.162 33.35 1.515s 0.194 25.85 0.951 0.000 0.00 0.000 0.250 23.14 1.306s 0.000 0.00 0.000 0.147 24.51 1.539 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.000 0.00 0.000 0.267 15.81 1.599 s - peak f a i l s shape tests.

D - Peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E

- ~ u c l i d e - Average

peak --------------

Naffle code A c t i v i t y Energy A c t i v i t y code MDA Value pci /g kev P C ~

/g P C ~

/g COMMENTS ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 12:00:04 Page 4

PBRF spectrum name: ~ ~ 0 7 - 0 3 1 1 5. ~ n l Nuclide AVe a c t i v i t y Energy

~ c t i v i t y code peak MDA Comments RA-226 N

4.6380E+00 186.21 4.638~+00 @(

1.431E+00 16.67 G K

( - his peak used i n the nuclide a c t i v i t y average.

Page 3

PB07-03115

- peak i s too wide, but only one peak i n l i b r a r y.

! - Peak i s p a r t o f a m u l t i l e t and t h i s area went negative during deconvo ution.

? - Peak i s too narrow.

C

@ - Peak i s too wide a t FW25M, but ok a t FWHM.

% - Peak f a i l s s e n s i t i v i t y test.

$ - Peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i 1 ed one o r more qua1 i fi cation tests.

+ - Peak a c t i v i t y higher than counting uncertainty range.

- - peak a c t i v i t y lower than counting uncertainty range.

= - Peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o the l i b r a r y energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

P - Peakbackground subtraction

) - Peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

~ u c l i

de codes :

T - Thermal Neutron Activation F - Fast Neutron Activation I - F

~

S S

~

O

~

Product N - Naturally occurring Isotope P - Photon Reaction c - charged P a r t i c l e Reaction M - NO MDA calculation R - coincidence corrected H - ~ a l f l i f e 1 i m i t exceeded peak codes:

G - Gamma Ray x - x - ~ a y P - Positron Decay S - Sin Ie-Escape il D - DOU l e - ~ s c a p e K - Key Line A - ~ o t i n Average c - coincidence Peak S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

Time o f count Time corrected Uncertainty 2 Sigma Nuclide A c t i v i t y A ~ t i v i t y Counting Total MDA P C ~

/g pci /g P C ~

/g P C ~

/g K-40 1.2204E+01 1.2204E+Ol 1.9296E+OO 1.9686E+OO 5.622E-01 CO-60 B<

5.7747E-02 5.7889E-02 Ag-108mB<

3.8602~-02 3.8603E-02 CS-137 B<

7.9451E-02 7.9485E-02 EU-152 B<

1.8819E-01 1.8837E-01 EU-154 B<

1.2768E-01 1.2787E-01 0

ORTEC g v - i (1087) npp32 G53w3.05 04-on-2007 12:00:04 Page 5

PBRF Spectrum name: PB07-03115.Anl PB-212

5.3315E-01 5.3315E-01 1.3783E-01 1.3851E-01 1.382E-01 PB-214 &

l.O739E+OO l.O739E+OO 2.485OE-01 2.5085E-01 1.998E-01 BI-212 B<

9.5746E-01 9.5746E-01 BI-214

8.2173E-01 8.2174E-01 2.0144E-01 2.036OE-01 1.371E-01 RA-226 &

4.638OE+OO 4.638OE+OO 1.5466E+OO 1.6235E+OO 1.431~+00 TH-234 B<

1.3116E+00 1.3116E+00 U-235 B<

4.1122E-01 4.1122E-01 AM-241 B<

9.4706E-02 9.4709E-02

- ~ 1 1 peaks f o r a c t i v i t y calculation had bad shape.

- A c t i v i t y omitted from t o t a l

& - A

~

t i

~

i t y omitted from t o t a l and a1 1 peaks had bad shape.

< - MDA value printed.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y 5 MDA and f a i l e d test.

c - Area < c r i t i c a l l e v e l.

Page 4

PB07-03115 F - Failed f r a c t i o n o r key l i n e t e s t.

H - ~ a l f l i f e l i m i t exceeded S U M M A R Y Total A c t i v i t y (

39.3 t o 2049.9 kev) 0.0000000E+00 pci/g

~ 0 t a l

~ecayed A c t i v i t y (

39.3 t o 2049.9 kev) 0.0000000E+00 pCi/g

~ n a l yzed by :

PBRF Decommi ssi oni ng Project Revi ewed by :

Supervi sor Laboratory:

PBRF Page 5

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:47:47 Page 1

PBRF Spectrum name: ~ ~ 0 7 - 0 3 1 1 6. ~ n 1 sampl e descri p t i on PB07-03116; SR38-60; HPT 104; HOLE 3; 21; 10/4/07 Spectrum ~ilename: \\ \\ ~ b r f - l i b r a r y \\ l i b r a r y ~ ~ ~ ~ \\ L ~ ~ \\ s A M P L E 0 7 \\ ~ ~ 0 7 - 0 3 1 16.An1 A C ~ U ~

s i t i o n information s t a r t ti me:

Live time:

Real time:

~ e a d time:

Detector ID:

Detector system

1 DETECTOR (#129)

Cali b r a t i o n F i 1 ename :

250ml #73678-773 (Mc129)Sept07 Energy C a l i b r a t i o n created :

zero o f f s e t :

Gai n :

Quadratic:

~ f f i c i ency cal i b r a t i on created :

Type :

uncertainty:

c o e f f i c i ents :

Library F i l e s Main analysis 1 i brary :

L i brary Match width :

Peak stripping:

~ n a l y s i s parameters

~ n a l y s i s engine:

s t a r t channel :

s t o channel:

Pea I: r e j e c t i o n 1 eve1 :

Peak search s e n s i t i v i t y :

sample size:

A c t i v i t y scal i ng f a c t o r :

~ e t e c t i o n 1 i m i t method :

and om e r r o r :

systematic e r r o r :

Fraction ~i m i t :

11-sep-2007 13:44:33

-0.041 kev 0.250 kev/channel

-7.752E-09 kev/channelA2 plumbrk Ol.1ib 0.500 L i brary based npp32 G53w3.05 1 5 5 (

38.74kev )

8144 ( 2037.25kev )

25.OOO%

3 4.0070E+02 l.OOOOE+O6/(

l.OOOOE+OO*

4.0070E+02) =

2.4956~+03 Nureg 4.16 ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:47:47 Page 2

Page 1

PBRF PB07-03116 spectrum name: PB07-03116.Anl Background width:

Half l i v e s decay l i m i t :

A

~

t i

~

i t y range factor:

Min. step backg. energy best method (based on spectrum).

corrections Decay correct t o date:

Decay duri ng acqui s i ti on :

Decay du r i ng col 1 e c t i on :

True coi nci dence correction :

peaked background correction :

Absorption ( ~ n t e r n a l ) :

Geometry correction :

Random summi ng :

Status YES NO NO NO NO NO NO NO Comments 27-Sep-2007 16:46:00 Energy Cal i b r a t i on Normal i zed d i ff :

S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area Uncert FWHM corrctn Nuclide Brnch.

Act.

NUC Energy Factor Energy Ratio pci/g

- - - - U N 1 D E N T 1 F 1 E D P E A K S U M M A R Y

*

f t * * * * ? C ? C *

peak centroid ~ackground Net Area I n t e n s i t y Uncert FWHM Sus channel Energy Counts counts Cts/Sec 2 Sigma %

kev NUC s - peak f a i l s shape tests.

D - Peak area deconvoluted.

L - Peak w r i t t e n from unknown l i s t.

c - Area < c r i t i c a l 1 eve1.

M - Peak i s close t o a l i b r a r y peak.

This section based on l i b r a r y : plumbrk 0 l. l i b 0

ORTEC g v - i (1087) npp32 G53W3.05 04-ocT-2007 11:47:47 Page PBRF spectrum name: ~ ~ 0 7 - 0 3 1 1 6. ~ n 1 fr*fr$<****+*?C***

1 D E N T 1 F 1 E D p E A K S U M M A R y **************

~ u c l i d e peak centroid ~ackground Net Area I n t e n s i t y Uncert FWHM channel Energy Counts counts cts/sec 2 sigma %

kev AM-241 0.00 59.54

0.

0.000 0.00 0.000 TH-234 0.00 63.29

0.

0.000 0.00 0.000 TH-234 0.00 92.59

0.

0.000 0.00 0.000 EU-152 0.00 121.78

0.

0.000 0.00 0.000 EU-154 0.00 123.07

0.

0.000 0.00 0.000 Page 2

U-235 U-235 RA-226 PB-212 EU-152 PB-214 Ag-108m BI-214 Ag-108m CS-137 Ag - 108m EU-154 BI-212 EU-154 CO-60 EU-154 CO-60 EU-152 K-40 s - peak f a i l s shape tests.

D - peak area deconvoluted.

A

~ e r i v e d peak area.

S U M M A R Y

- Nuclide - Average Name code A c t i v i t y pci /g O F L I B R A R Y P E A K U S A G E *****

peak --------------

Energy A c t i v i t y code MDA Value kev P C ~

/g P C ~

/g COMMENTS ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 11:47:47 Page 4

PBRF Spectrum name: PB07-03116.Anl

~ u c l i

de AVe a c t i v i t y Energy A c t i v i t y code peak MDA Comments BI-214 N

1.0388E+00 609.31 1.039E+OO

( 1.235E-01 12.70 G K 1764.49 O.OOOE+OO 8.857E-01 130.17 G 1120.29 O.OOOE+OO %

8.688E-01 32.68 G

( - This peak used i n the nuclide a c t i v i t y average.

- peak i s too wide, but only one peak i n l i b r a r y.

! - peak i s p a r t o f a m u l t i l e t and t h i s area went P

negative during deconvo u t i on.

? - Peak i s too narrow.

@ - Peak i s too wide a t FW25M, but ok a t FWHM.

% - Peak f a i l s s e n s i t i v i t y t e s t.

$ - Peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide failed one o r more qua1 i f i cation tests.

+ - peak a c t i v i t y higher than counting uncertainty range.

- - Peak a c t i v i t y lower than counting uncertainty range.

- - - Peak outside analysis energy range.

page 3

PB07-03116

& - calculated peak centroid i s not close enough t o the l i b r a r y energy centroid f o r p o s i t i v e i d e n t l f i c a t i o n.

P - Peakbackground subtraction

) - peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

Nucl i de codes :

T - Thermal Neutron Activation F - Fast Neutron Activation I

- Fission product N - ~ a t u r a l l y Occurring Isotope P - Photon Reaction C - charged P a r t i c l e Reaction M - NO MDA c a l c u l a t i o n R - coincidence corrected H - H a l f l i f e 1 i m i t exceeded Peak codes:

G - Gamma Ray x - x - ~ a y P - Positron Decay s - s i n 1e-EScape D - DOU E Ie-EScape K - Key Line A - Not i n Average C - coincidence Peak S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

Time o f Count Time corrected Uncertainty 2 sigma Nuclide A c t i v i t y A c t i v i t y Counting Total MDA p c i /g p c i /g P C ~

/g p c i /g ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 11:47:47 Page PBRF spectrum name: Pe07-03116.~n1

- ~ 1 1 peaks f o r a c t i v i t y calculation had bad shape.

- A c t i v i t y omj t t e d from t o t a l

& - A c t i v i t y omitted from t o t a l and a l l peaks had bad shape.

< - MDA value printed.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - ~ ~ t i ~ i t y < MDA and f a i l e d t e s t.

c - Area < c r i t i c a l l e v e l.

F - Failed f r a c t i o n o r key l i n e t e s t.

H - H a l f l i f e l i m i t exceeded S U M M A R Y Total ~ c t i v i t y (

38.7 t o 2037.3 kev) 0.0000000E+00 pci/g Total Decayed A c t i v i t y (

38.7 t o 2037.3 kev) 0.00~0000E+00 pci/g Anal yzed by:

PBRF Decommi ssioni ng Project Revi ewed by :

supervi sor Page 4

~ a b o r a t o r y : PBRF Page 5

ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 11:52:17 Page PBRF Spectrum name: PBOi'-03117.~nl sample description PB07-03117; SR38-61; HPT 104; HOLE 3; 24; 10/4/07 spectrum Filename: \\ \\ ~ b r f - l i b r a r y \\ l i b r a r y data\\Lab\\SAMPLE 0 7 \\ ~ ~ 0 7 - 0 3 1 17.An1 Acquisition information s t a r t time:

Live ti me:

~ e a l ti me :

Dead ti me :

Detector ID:

Detector system

3 DETECTOR (#131) c a l i b r a t i o n F i 1 ename :

250ml #73678-773 (MC131) Sept07 Energy Cal i b r a t i on created :

zero o f f s e t :

Gai n :

Quadratic:

E f f i c i ency c a l i b r a t i on created :

Type :

Uncertai n t y :

c o e f f i c i e n t s :

~i brary Fi 1 es

~ a i n analysis 1 i brary:

Library Match width :

Peak s t r i ppi ng :

Analysi s parameters Anal y s i s engi ne :

s t a r t channel :

s t o channel:

Pea R r e j e c t i o n 1 eve1 :

peak search s e n s i t i v i t y :

Sample Size:

A c t i v i t y s c a l i n g f a c t o r :

Detection l i m i t method:

l and om e r r o r :

systematic e r r o r :

Fraction L i m i t :

05-sep-2007 16:56:38 0.565 kev 0.247 kev/channel 5.022~-08 kev/channel A2 05-sep-2007 17:17:39 POI ynomi a1 plumbrk 0 l. l i b 0.500 L i b r a r y based Nureg 4.16 ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 11:52:17 page Page 1

PBRF PB07-03117 spectrum name: PB07-03117.~n1 Background width:

~ a l f 1 i ves decay 1 i m i t :

A c t i v i t y range factor :

Min. step backg. energy best method (based on spectrum).

corrections Decay correct t o date:

Decay during acqui s i ti on :

Decay duri ng col 1 e c t i on :

True coincidence correction :

Peaked background correction :

Absorption (Internal) :

Geometry correction :

Random summi ng :

Status YES NO NO NO NO NO NO NO Comments 27-Sep-2007 17:00:00 Energy Cal i bration Normal i zed d i ff :

- 9r**

S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area Uncert FWHM Corrctn Nuclide Brnch.

Act.

NUC Energy Factor Energy Ratio pci/g f ~ * * *

f ~ * * * * *

U N 1 D E N T 1 F 1 E D P E A K S U M M A R Y ************

Peak Centroid Background Net Area I n t e n s i t y Uncert FWHM Sus Channel Energy Counts Counts Cts/Sec 2 Sigma %

kev NUC s - Peak f a i l s shape tests.

D - peak area deconvoluted.

L - Peak w r i t t e n from unknown l i s t.

c - Area < c r i t i c a l 1 eve1.

This section based on l i b r a r y : plumbrk 0 1 - l i b 0

ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 11:52:17 Page 3

PBRF Spectrum name: ~B07-03117.Anl

- a***********

1 D E N T 1 F 1 E D P E A K S U M M A R Y **************

~ u c l i d e Peak centroid Background Net Area I n t e n s i t y uncert FWHM channel Energy Counts counts Cts/Sec 2 Sigma %

kev AM-241 0.00 59.54

0.

0.000 0.00 0.000 TH-234 0.00 63.29

0.

0.000 0.00 0.000 TH-234 0.00 92.59

0.

0.000 0.00 0.000 EU-152 0.00 121.78

0.

0.000 0.00 0.000 Page 2

EU-154 U-235 U-235 PB-212 EU-152 PB-214 Ag - 108m BI-214 Ag-108m CS-137 Ag-108m EU-154 BI-212 EU-154 CO-60 EU-154 CO-60 EU-152 K-40 s - peak f a i l s shape tests.

D - peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E *****

- Nuclide - Average

peak --------------

Name code A c t i v i t y Energy A c t i v i t y code MDA Value P C ~

/g kev P C ~

/g P C ~

/g COMMENTS ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 11:52:17 Page 4

PBRF spectrum name: PB07-03117.Anl N U C ~ i de AVe a c t i v i t y Energy A c t i v i t y code Peak MDA Comments BI-214 N

1.1884E+00 609.311.188E+OO

( 1.857E-01 13.27 G K 1764.49 O.OOOE+OO &

9.718E-01 31.62 G 1120.29 O.OOOE+OO 9.562E-01 206.16 G

( - This peak used i n the nuclide a c t i v i t y average.

Peak i s too wide, but only one peak i n l i b r a r y.

peak i s p a r t o f a m u l t i l e t and t h i s area went peak i s too narrow.

P negative d u r i ng deconvo u t i on.

peak i s too wide a t FW25M, but ok a t FWHM.

peak f a i 1 s s e n s i t i v i t y t e s t.

peak i d e n t i f i e d, but fi r s t peak o f t h i s nuclide f a i l e d one o r more q u a l i f i c a t i o n tests.

Peak a c t i v i t y h~ gher than counti ng uncertai n t y range.

peak a c t i v i t y lower #than counting uncertai n t y range.

peak outside analysis energy range.

Page 3

PB07-03117

& - calculated peak centroid i s not close enough t o the l i b r a r y energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

P - Peakbackground subtraction

} - peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

Nucl i de codes :

T - ~ h e r m a l Neutron A c t i v a t i o n F - Fast Neutron A c t i v a t i o n I - Fission product N - Naturally occurring Isotope P - Photon Reaction c - charged p a r t i c l e Reaction M - NO MDA c a l c u l a t i o n R - coincidence corrected H - ~ a l f l i f e l i m i t exceeded Peak codes:

G - Gamma Ray x - X - ~ a y P - Positron Decay s - s i n l e - ~ s c a p e D - DOU 1 e-~scape K - Key Line A - ~ o t i n Average c - coincidence Peak S U M M A R Y O F N U C L I D E S I

N S A M P L E

- - 9r*

Time o f Count Time corrected Uncertainty 2 Sigma

~ u c l i

de

~ c t i v i t y A c t i v i t y Counting Total MDA p c i /g P C ~

/g pci /g pci /g ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 11:52:17 page 5

PBRF spectrum name: PB07-03117.Anl

- ~ l l peaks f o r a c t i v i t y c a l c u l a t i o n had bad shape.

- A c t i v i t y omitted from t o t a l

& - ~ c t i v i t y omitted from t o t a l and a l l peaks had bad shape.

< - MDA value printed.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - ~ c t i v i t y

< MDA and f a i l e d t e s t.

c - Area < C r i t i c a l 1 eve1.

F - ailed f r a c t i o n o r key l i n e t e s t.

H - ~ a l f l i f e l i m i t exceeded S U M M A R Y

~ 0 t a l

~ c t i v i t y (

38.8 t o 2014.2 kev) 0.0000000E+00 pCi/g

~ 0 t a l

~ecayed A c t i v i t y (

38.8 t o 2014.2 kev) 0.0000000E+00 pci/g

~ n a l yzed by :

PBRF Decommi ssi oni ng Project Revi ewed by :

supervi sor Page 4

Laboratory:

PBRF Page 5

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:52:23 Page PBRF spectrum name: PB07-03124.~nl sample description PB07-03124; SR38-65; HPT 104; HOLE 4; 22; 10/4/07 f

spectrum Filename: \\\\Pbrf-library\\library d a t a \\ ~ a b \\ s ~ ~ ~ ~ ~

0 7 \\ ~ ~ 0 7 - 0 3 1

24. An1 Acqui s i ti on information S t a r t time:

Live time:

Real ti me :

Dead ti me :

Detector I D :

Detector system

2 DETECTOR (#130) cal i b r a t i on F i 1 ename :

250m1 #73678-773 (~C130)Sept07 Energy Ca1 i b r a t i on created :

Zero o f f s e t :

Gai n :

quadratic:

E f f i c i ency c a l i b r a t i on created :

Type:

uncertainty:

c o e f f i c i ents :

~i brary F i 1 es Main analysis 1 i brary:

Library Match width :

Peak s t r i ppi ng :

COPY 13-sep-2007 15:00:31 0.287 kev 0.251 kev/channel 2.324E-08 kev/channelA2 plumbrk 0 l. l i b 0.500 Library based Analysis parameters

. - - - - - - - ~ n a l y s i s engi ne:

npp32 G53W3.05

-~ta~t-q-:-

----%5-(---+2*~-)---

~ t o channel:

8144 ( 2049:92kev )

pea[: r e j e c t i o n 1 eve1 :

25.000%

peak search s e n s i t i v i t y :

3 sample size:

4.5530~+02

~ c t i v i t y scaling f a c t o r :

1.0000~+06/( 1.0000~+00* 4.5530E+02) =

2.1964~+03

~ e t e c t i on 1 i m i t method :

Nureg 4.16 n and om error:

systematic-error:

~ r a c t i on L i m i t :

ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 15:52:23 Page Page 1

PBRF PB07-03124 spectrum name: PB07-03124.Anl

~ackground width:

H a l f l i v e s decay l i m i t :

A c t i v i t y range factor:

Min. step backg. energy best method (based on spectrum).

corrections Decay correct t o date:

Decay during acquisition:

Decay duri ng col 1 e c t i on :

True coi nci dence c o r r e c t i on :

Peaked background correction :

~ b s o r p t i o n ( ~ n t e r n a l ) :

Geometry correction:

Random summi ng :

status YES NO NO NO NO NO NO NO Energy cal i b r a t i o n

~0rma1 i zed d i ff :

- 9<**

S U M M A R Y O F P E A K S I

N R A N G E ***"*

peak Area Uncert FWHM Corrctn Nuclide Brnch.

Act.

Energy Factor Energy Ratio pCi/g

- - - - U N I D E N T I F I E D P E A K S U M M A R Y ********"***

peak centroid ~ackground Net Area I n t e n s i t y uncert FWHM Sus channel Energy Counts Counts Cts/Sec 2 Sigma %

kev NUC s - Peak f a i l s shape tests.

- - - - - - - - D - peak area deconvoluted.

~ - - ~ k ~ ~ ~ f r ~ - ~ ' f i ~ t - - - - - - - - - - - - - - - - -

c - Area < c r i t i c a l l e v e l.

M - peak i s close t o a l i b r a r y peak.

~ h i s section based on l i b r a r y : plumbrk 0 l. l i b 0

ORTEC g V - i (1087) npp32 G53W3.05 04-OCT-2007 15:52:23 Page PBRF spectrum name: ~ ~ 0 7 - 0 3 1 2 4. ~ n l

- - - - a****

I D E N T I F I E D p E A K s u M M A R Y ******Qx*****Q Nuclide peak centroid Background Net Area I n t e n s i t y Uncert FWHM Page 2

channel Energy PB07-03124 counts counts

0.

8.

42.

1 2.

57.

0.

6.

60.

0.

46.

0.

17.

0.

16.

0.

0

54.

2 sigma %

kev s - Peak f a i l s shape tests.

D - peak area deconvoluted.

A

~ e r i v e d peak area.

- - - fr S U M M A R Y O F L I B R A R Y P E A K U S A G E *****

- Nuclide - Average

peak --------------

Name code A c t i v l t y Energy A c t i v i t y code MDA Value P C ~

/g kev P C ~

/g P C ~

/g COMMENTS CS-137 I

1.5864E-01 661.66 1.586E-0

?(

6.878E-02 24.25 G K PB-212 N

4.5223E-01 I3 238.63 4.522E-01

( 1.496E-01 16.92 G K

[I O R T E C ~ V - i (1087)npp32 G53W3.05 04-OCT-200715:52:23~age 4

PBRF spectrum name : ~~07-03124.

An1

~ u c l ide AVe a c t i v i t y Energy A c t i v i t y code Peak MDA Comments Page 3

PBO7-03124 186.21 3.418E+00 &(

1.274E+00

( - This peak used i n the nuclide a c t i v i t y average.

jr - peak i s too wide, but only one peak i n l i b r a r y.

! - Peak i s p a r t o f a m u l t i l e t and t h i s area went negative duri ng deconvo u t i on.

? - peak i s too narrow.

P

@ - peak i s too wide a t FW25M, but ok a t FWHM.

% - Peak f a i l s s e n s i t i v i t y t e s t.

$ - peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i l e d one o r more q u a l i f i c a t i o n tests.

+ - peak a c t i v i t y higher than counting uncertainty range.

- - Peak a c t i v i t y lower than counting uncertainty range.

= - peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o the 1 i brary energy centroid f o r p o s i t i v e i dent1 fi cation.

P - peakbackground subtraction

) - peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

Nucl i de codes :

T - Thermal Neutron Activation F - Fast Neutron Activation I

- Fission product N - Naturally occurring Isotope P - Photon Reaction c - charged P a r t i c l e Reaction M - NO MDA calculation R - coincidence Corrected H - Hal fl i f e 1 i m i t exceeded Peak codes:

G - Gamma Ray x - X - ~ a y P - Positron Decay s - s i n l e - ~ s c a p e D - DOU E l e - ~ s c a p e K - Key Line A - Not i n Average c - coincidence Peak ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:52:23 Page PBRF Spectrum name: ~ ~ 0 7 - 0 3 1 2 4. ~ n l S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

Time o f Count Time corrected Uncertainty 2 sigma

~ u c l i

de

~ c t i v i t y A c t i v i t y Counting Total MDA PC! /g pci /g P C ~

/g P C ~

/g

- ~ 1 1 peaks f o r a c t i v i t y ca1 culatlon had bad shape.

- A c t i v i t y omitted from t o t a l

& - A c t i v i t y omitted from t o t a l and a1 1 peaks had bad shape.

< - MDA value p r ~ n t e d.

Page 4

PB07-03124 A - ~ c t i v i t y p r i n t e d, but a c t i v i t y < MDA.

B - ~ c t i v i t y

< MDA and f a i l e d t e s t.

c - Area < C r i t i c a l l e v e l.

F - ailed f r a c t i o n o r key l i n e t e s t.

H - Hal f l i f e 1 i m i t exceeded S U M M A R Y Total A c t i v i t y (

39.3 t o 2049.9 kev) 1.5860933E-01 pCi/g Total Decayed 39.3 t o 2049.9 kev) 1.5864177~-01 pci/g Analyzed by :

Reviewed by:

R. Case Laboratory:

PBRF Page 5

0RTEC.g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:19:50 Page PBRF Spectrum name: PB07-03123.Anl sample description PB07-03123; SR38-66; HPT 104; HOLE 4; 24; 10/4/07 Spectrum Filename: \\ \\ p b r f - l i b r a r y \\ l i b r a r y data\\Lab\\SAMPLE 0 7 \\ ~ ~ 0 7 - 0 3 1 23. ~ n l A C ~ U ~

s i t i o n information s t a r t time:

Live ti me :

Real ti me:

Dead ti me :

Detector ID:

Detector system

I DETECTOR (#129)

COPY c a l i b r a t i on F i 1 ename :

250ml #73678-773 (MC129) ~ e p t 0 7 Energy c a l i b r a t i o n created:

zero o f f s e t :

Gai n :

quadrati c:

~ f f i c i ency c a l i b r a t i on created:

Type :

uncertainty:

c o e f f i c i ents :

L i brary F i 1 es Mai n analysis 1 i b r a r y :

L i brary Match w i d t h :

peak s t r i p p i n g :

11-sep-2007 13:44:33

-0.041 kev 0.250 kev/channel

-7.752E-09 ke~/channelA2 11-sep-2007 14:04:24 POI ynomi a1 1.649 X

-0.312485

-4.205606 0.662739

-0.094204 0.005970

-0.000141 plumbrk 0 l. l i b 0.500 L i b r a r y based

~ n a 1 y s i s parameters Anal y s i s engine :

npp32 G53W3.05

- - - - -- - - - - 1JjJj-f- - +-M-kev-)

s t o channel :

8144 ( 2037125kev)

Pear r e j e c t i on 1 eve1 :

25.000%

peak search s e n s i t i v i t y :

3 sample Size:

4.2570~+02 A c t i v i t y s c a l i n g f a c t o r :

1.0000E+06/(

1.0000~+00* 4.2570~+02) =

2.3491~+03

~ e t e c t i on 1 i m i t method :

Nureg 4.16 n and om e r r o r :

systematic e r r o r :

~ r a c t i on L i m i t :

ORTEC g v - i (1087) npp32 G53w3.05 04-OcT-2007 15:19:50 Page Page 1

PBRF PB07-03123 spectrum name: ~ ~ 0 7 - 0 3 1 2 3. ~ n 1

~ackground width:

~ a l f l i v e s decay l i m i t :

A c t i v i t y range factor:

Min. step backg. energy best method (based on spectrum).

Corrections Decay correct t o date:

Decay during acquisition :

Decay du r i ng col 1 e c t i on :

True coincidence correction:

Peaked background correction:

Absorption ( ~ n t e r n a l ) :

Geometry correction :

and om summi ng :

status YES NO NO NO NO NO NO NO Energy Cali b r a t i on Normal i zed d i ff :

Comments 01-Oct-2007 09:40:00 S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area uncert FWHM Corrctn Nuclide Brnch.

Act.

Energy Factor Energy Ratio pci/g

n******+**n u N I D E N T I F I E D P E A K s u M M A R y *******fi****

peak centroid ~ackground Net Area I n t e n s i t y Uncert FWHM Sus ected channel Energy counts counts cts/sec 2 Sigma %

kev Nucyide s - peak f a i l s shape t e s t s.

D - Peak area deconvoluted.

L - peak w r i t t e n from unknown l i s t.

c - Area < c r i ti ca1 1 eve1.

- - - -- T h i s -semim-.

b e

m-)+bPaV-pqum$&-O$ -I+ - - --- - - - - -- - --- - - - - -- - -- - - -- - - -- - - -- - - - - - - - -

0 ORTEC g v - i (1087) npp32 G53W3.05 04-~CT-2007 15:19:50 Page PBRF Spectrum name: PB07'-03123.~nl

- - - - 1 D E N T 1 F 1 E D P E A K S U M M A R Y **************

~ u c l i

de peak centroid Background Net Area

~ n t e n s i t y Uncert FWHM channel Energy counts counts Cts/Sec 2 Sigma %

kev Page 2

EU-152 EU-154 U-235 U-235 RA-226 PB-212 EU-152 PB-214 Ag-108m BI-214 Ag-108m CS-137 Ag-108m EU-154 BI-212 EU-154 CO-60 EU-154 CO-60 EU-152 K-40 s - peak f a i l s shape t e s t s.

D - peak area deconvoluted.

A

~ e r i v e d peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E ***"*

- Nuclide - Average

- - - - - - - - - m u - -

peak --------------

Name code A c t i v i t y Energy A c t i v i t y code MDA Value P C ~

/g

' kev P C ~

/g P C ~

/g COMMENTS ORTEC g v - i (1087) npp32 G53W3.05 04-0CT-2007 15:19:50 Page PBRF Spectrum name: PB07-03123.Anl

~ u c l i

de AVe a c t i v i t y Energy

~ c t i v i t y code Peak MDA Comments

( - This peak used i n t h e nuclide a c t i v i t y average.

- Peak i s too wide, but o n l y one peak i n l i b r a r y.

! - Peak i s p a r t o f a m u l t i l e t and t h i s area went B

negative during deconvo ution.

? - Peak i s too narrow.

@ - peak i s too wide a t FW25M, but ok a t FWHM.

% - peak f a i l s s e n s i t i v i t y t e s t.

Page 3

PB07-03123.

$ - peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i l e d one o r more q u a l i f i c a t i o n tests.

+ - peak a c t i v i t y higher than counting uncertainty range.

- - peak a c t i v i t y lower than counting uncertainty range.

= - Peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o the l i b r a r y energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

P - peakbackground subtraction

) - peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

~ u c l i

de codes :

T - ~ h e r m a l Neutron Activation F - Fast Neutron Activation I - ~i ssion product N - Naturally occurring Isotope P - Photon Reaction C - charged P a r t i c l e Reaction M - NO MDA Calculation R - coincidence corrected H - H a l f l i f e l i m i t exceeded Peak codes:

G - Gamma Ray x - X - ~ a y P - Positron Decay s - s i n l e - ~ s c a p e D - DOU I! l e - ~ s c a p e K - Key Line A - Not i n Average C - coincidence Peak

- - - ?:

S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

Time o f Count Time corrected Uncertainty 2 sigma Nuclide A c t i v i t y A c t i v i t y counting Total MDA pci /g p c i /g P C ~

/g PC; /g ORTEC g v - i (1087) npp32 G53W3.05 04-on-2007 15:19:50 Page PBRF spectrum name: PB07-03123.Anl

- ~ l l peaks f o r a c t i v i t y calculation had bad shape.

- A c t i v i t y omitted from t o t a l

& - A c t i v i t y omitted from t o t a l ' and a1 1 peaks had bad shape.

< - MDA value printed.

A - ~ c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y < MDA and f a i l e d t e s t.

c - Area < C r i t i c a l 1 eve1.

F - Failed f r a c t i o n o r key l i n e t e s t.

H - H a l f l i f e 1 i m i t exceeded S U M M A R Y Total A c t i v i t y (

38.7 t o 2037.3 kev) 3.4641668E-01 pCi/g

~ 0 t a l Decayed ~ c t i v i t y (

38.7 t o 2037.3 kev) 3.4648734E-01 pci/g Page 4

PBO7-03123

~ n a l yzed by :

~ e v i ewed by :

supervi sor Laboratory:

PBRF R. Case Page 5

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:25:50 Page PBRF spectrum name: PB07-03125..Anl sampl e description PBO7-03125; SR38-67; HPT 104; HOLE 4; 26.5; 10/4/07 spectrum Filename: \\ \\ ~ b r f - l i b r a r y \\ l i b r a r y data\\Lab\\sA~p~E 0 7 \\ ~ ~ 0 7 - 0 3 1 25.An1 A C ~ U ~

s i ti on S nformati on s t a r t time:

L i v e time:

Real time :

Dead ti me :

Detector ID:

Detector system

3 DETECTOR (#131) c a l i b r a t i o n F i 1 ename :

2501111 #73678-773 (MC131)

Sept07 Energy c a l i b r a t i on created:

zero o f f s e t :

Gain :

Quadrati c :

E f f i c i ency c a l i b r a t i o n created :

Type :

uncertainty :

c o e f f i c i e n t s :

Library Fi 1 es Main analysis l i b r a r y :

Library Match width:

peak s t r i p p i n g :

05-Sep-2007 16:56:38 0.565 kev 0.247 kev/channel 5.022~-08 kev/channelA2 05-Sep-2007 17:17:39 pol ynomi a1 1.204 %

-0.304311

-4.249899 0.669559

-0.094002 0.005803

-0.000133 plumbrk 0 1 - l i b 0.500 Library based

~ n a l y s i s parameters

- - - - ~ n a l y s i s engi ne :

npp32 G53~3.05

~ - - - - - - - - * * ~ - - 3 & ~ f s t o channel :

R 8144 ( 2014:22kev )

Pea r e j e c t i o n 1 eve1 :

25.000%

peak search s e n s i t i v i t y :

3 sample size:

4.5350E+02

~ c t i v i t y scaling f a c t o r :

1.0000~+06/( 1.0000E+00*

4.5350~+02) =

2.2051~+03

~ e t e c t i on 1 i m i t method :

Nureg 4.16 Random e r r o r :

systematic e r r o r :

~ r a c t i on L i m i t :

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:25:50 Page Page 1

PBRF PB07-03125 spectrum name: PB07-03125.~nl Background width:

best method (based on spectrum).

~ a l f 1 i ves decay 1 i m i t :

12.000 A c t i v i t y range factor:

2.000 Min. step backg. energy 0.000 corrections Decay correct t o date:

Decay duri ng acqui s i ti on :

Decay during c o l l e c t i on :

True coi nci dence correction :

Peaked background correction:

~ b s o r p t i on ( ~ n t e r n a l ) :

Geometry correction:

Random summi ng :

status YES NO NO NO NO NO NO NO comments 01-Oct-2007 09:48:00 Energy ca1 i b r a t i on Normal i zed d i ff:

S U M M A R Y O F P E A K S I

N R A N G E ****"

peak Area uncert FWHM corrctn Nuclide Brnch.

Act.

NUC Energy Factor Energy Ratio pci/g

9 r > k ~ r * * * * * * *

u N I D E N T I F I E D P E A K s u M M A R y ***x*******Q peak centroid ~ackground Net Area I n t e n s i t y Uncert FWHM Sus ected channel Energy Counts Counts Cts/Sec 2 Sigma %

kev NUC 7 i d e s - Peak f a i l s shape tests.

D - Peak area deconvoluted.

L - Peak w r i t t e n from unknown l i s t.

c - Area < C r i t i c a l 1 eve1.

M - Peak i s close t o a l i b r a r y peak.

This section based on l i b r a r y : plumbrk 0 l. l i b 0

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:25:50 Page PBRF spectrum name: ~ ~ 0 7 - 0 3 1 2 5. ~ n l

- 9r**9r********

1 D E N T 1 F I E D P E A K S U M M A R Y **************

~ u c l i d e peak centroid Background Net Area I n t e n s i t y Uncert FWHM channel Energy Counts counts Cts/Sec 2 Sigma %

kev AM-241 0.00 59.54

0.

0.000 0.00 0.000 TH-234 0.00 63.29

0.

0.000 0.00 0.000 Page 2

TH-234 EU-152 EU-154 U-235 U-235 RA-226 PB-212 EU-152 PB-214 Ag-108m B I - 2 14 Ag-lO8m CS-137 Ag-108m EU-154 BI-212 EU-154 BI-214 CO-60 EU-154 CO-60 EU-152 K-40 s - Peak f a i l s shape t e s t s.

D - peak area deconvoluted.

A Derived peak area.

- - ?;*

S U M M A R Y 0 F L

- ~ u c l i d e - Average Name code A c t i v i t y Energy pci /g kev I B R A R Y P E A K U S A G E ***"*

. - - - - - peak --------------

A c t i v i t y code MDA Value P C ~

/g PC? /g COMMENTS ORTEC g v - i (1087) npp32 G53W3.05 04-Oc~-2007 15:25:50 page PBRF spectrum name: PBoi'-03125.~nl

( - This peak used i n the nuclide a c t i v i t y 'average.

- peak i s too wide, b u t only one peak i n l i b r a r y.

! - Peak i s p a r t o f a m u l t i l e t and t h i s area went C

negative duri ng deconvo u t i on.

? - Peak i s too narrow.

Page 3

PB07-03125 Peak i s too wide a t FW25M, but ok a t FWHM.

peak f a i l s s e n s i t i v i t y t e s t.

peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i l e d one o r more q u a l i f i c a t i o n tests.

peak a c t i v i t y higher than counting uncertainty range.

peak a c t i v i t y lower than counting uncertainty range.

peak outsi de anal y s i s energy range.

calculated peak centroid i s not close enough t o the l i b r a r y energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

peakbackground subtraction Peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

~ u c l i

de codes :

T - Thermal Neutron Activation F - Fast Neutron A c t i v a t i o n I - ~ i s s i o n Product N - Naturally occurring Isotope P - Photon Reaction c - charged P a r t i c l e Reaction M - No MDA Cal G U ~

a t i o n R - coincidence corrected H -. ~ a l f l i f e l i m i t exceeded Peak codes:

G - Gamma Ray x - x - ~ a y P - Positron Decay S - Sin 1e-~scape D - DOU % l e - ~ s c a p e K - Key Line A - Not i n Average C - Coincidence peak S U M M A R Y O F N U C L I D E S I

N S A M P L E *"***

Time o f Count Time Corrected Uncertainty 2 Sigma

~ u c l i

de

~ c t i v i t y A c t i v i t y Counting Total MDA pci /g P C ~

/g pci /g pci /g K-40 1.1831E+01 1.1831E+01 2.6568E+00 2.6794E+00 1.433~+00 CO-60 B<

9.7985E-02 9.8099E-02

~g-108mB<

6.6429E-02 6.6430E-02 cS-137 B<

6.5187E-02 6.520OE-02 EU-152 B<

1.1903E-01 1.1909E-01 EU-154 B<

6.0884E-02 6.0928E-02 0

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:25:50 Page PBRF spectrum name: PB07-03125.Anl PB-212

5.2573E-01 5.2573E-01 2.0467E-01 2.0512E-01 2.091E-01 PB-214 &

1.2179E+OO 1.2179E+OO 2.3771E-01 2.4038E-01 8.549E-02 BI-212 B<

9.1243E-01 9.1243E-01 BI-214

8.6544E-01 8.6545E-01 2.5486E-01 2.5652E-01 1.675E-01

--- --- RA-226 &

3.1197E+OO 3.1198E+OO 1.3171E+OO 1.3583E+OO 1.255E+OO m=234-!3

<--- =+*---2;y&3+*--

U-235 B<

4.9825E-01 4.9825E-01 AM-241 B<

1.8223E-01 1.8223E-01

- ~ l l peaks f o r a c t i v i t y calculation had bad shape.

- A c t i v i t y omitted from t o t a l

& - A c t i v i t y omitted from t o t a l and a1 1 peaks had bad shape.

< - MDA value printed.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y < MDA and f a i l e d t e s t.

C - Area < C r i t i c a l l e v e l.

F - Failed f r a c t i o n o r key l i n e t e s t.

H - H a l f l i f e l i m i t exceeded S U M M A R Y

~ 0 t a 1 A c t i v i t y (

38.8 t o 2014.2 kev) 0.0000000E+00 pCi/g Page 4

PB07-03125

~ 0 t a l

~ e c a y e d A C Z ~ V ~

t y (

38.8 t o 2014.2 kev) 0.0000000E+00 pCi/g Anal yzed by:

~ e v i ewed by :

~aboratory: PBRF Page 5

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:29:03 page PBRF Spectrum name: PB07-03126.~n1 sample description

~ ~ 0 7 - 0 3 1 2 6 ;

SR38-68; HPT 104; HOLE 5; 18.5; 10/4/07 spectrum Filename: \\\\Pbrf-library\\library d a t a \\ ~ a b \\ s ~ ~ p L E 07\\pe07-031

26. An1 Acqui s i ti on i nformation s t a r t time:

Live time:

Real ti me :

Dead ti me:

Detector ID:

Detector system

1 DETECTOR (#129)

COPY c a l i b r a t i o n F i 1 ename :

250ml #73678-773 (Mc129)sept07 Energy Cali b r a t i on created :

zero o f f s e t :

Gai n :

Quadrati c :

11-Sep-2007 13:44:33

-0.041 kev 0.250 kev/channel

-7.752E-09 keV/channelA2

~ f f i c i ency c a l i b r a t i o n created :

11-Sep-2007 14:04:24 Type :

POI ynomi a1 Uncertainty :

1.649 %

c o e f f i c i e n t s :

-0.312485

-4.205606 0.662739

-0.094204 0.005970

-0.000141 Library Fi 1 es Mai n anal y s i s 1 i brary :

Library Match width:

peak s t r i ppi ng :

plumbrk 0 l. l i b 0.500 L i brary based

~ n a l y s i s parameters Anal y s i s engi ne :

npp32 G53w3.05 startc,-&n,+p ------ ---- 355f -

3*7-s t o channel:

8144 ( 2037:25kev )

Pea!

r e j e c t i o n 1 eve1 :

2 5.000%

peak search sensi t-~

v i t y :

3 sample Size:

4.5060E+02 A c t i v i t y scaling f a c t o r :

1.00GO~+06/(

1.0000~+00* 4.5060~+02) =

2.2193E+03

~ e t e c t i on 1 i m i t method :

Nureg 4.16 and om e r r o r :

systematic. e r r o r :

~ r a c t i on L i m i t :

ORTEC g v - i (1087) npp32 G53W3.05 04-oc~-2007 15:29:03 Page Page 1

PBRF PB07-03126 Spectrum name: PB07-03126.An1 Background' width:

H a l f l i v e s decay l i m i t :

A c t i v i t y range factor:

Min. step backg. energy best method (based on spectrum).

Corrections Decay correct t o date:

Decay during acqui s i ti on :

Decay duri n col 1 e c t i on :

True coi nci % ence correction:

peaked background correction:

~ b s o r p t i o n ( ~ n t e r n a l ) :

Geometry correction :

and om summi ng :

Status YES NO NO N 0 NO NO NO NO Energy Cali b r a t i o n Normal i zed d i ff :

comments 01-Oct-2007 10:42:00

"**J'*

S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area Uncert FWHM Corrctn Nuclide ~ r n c h.

Act.

Energy Factor Energy Ratio pCi/g n*i~***~:*nkafr u N I D E N T I F I E D p E A K s u M M A R y *********9:**

peak Centroid ~ackground Net Area I n t e n s i t y Uncert FWHM Sus ected channel Energy counts counts cts/sec 2 Sigma %

kev Nucyide s - peak f a i l s shape t e s t s.

D - Peak area deconvoluted.

L - peak w r i t t e n from unknown l i s t.

c - Area < C r i t i c a l l e v e l.

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:29:03 page PBRF spectrum name: PB07-03126.Anl

- - - - 1 D E N T 1 F 1 E D P E A K S U M M A R Y ******"*******

~ u c l i d e Peak centroid Background Net Area I n t e n s i t y Uncert FWHM channel Energy counts counts cts/sec 2 Sigma %

kev Page 2

EU-152 EU-154 U-235 U-235 RA-226 PB-212 EU-152 PB-214 Ag-108m BI-214 Ag-108m CS-137 Ag-108m EU-154 BI-212 EU-154 BI-214 CO-60 EU-154 CO-60 EU-152 K-40 s - Peak f a i l s shape t e s t s.

D - peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E *"***

- ~ u c l i d e - Average

peak --------------

Name code A c t i v i t y Energy A c t i v i t y Code MDA Value P C ~

/g kev P C ~

/g P C ~

/g COMMENTS ORTEC g V - i (1087) npp32 G53W3.05 04-OCT-2007 15:29:03 Page PBRF spectrum name: P ~ 0 7 - 0 3 1 2 6. ~ n l

~ u c l i d e AVe a c t i v i t y Energy

~ c t i v i t y code peak MDA Comments BI-214 N

9.6346E-01 609.31 9.635E-01

( 1.671E-01 13.75 G K 1764.49 0.000E+00 %

7.876E-01 33.33 G 1120.29 1.797E+OO +

5.518E-01 20.41 G

( - his peak used in t h e nuclide a c t i v i t y average.

- Peak i s too wide, but only one peak i n l i b r a r y.

! - Peak i s p a r t o f a m u l t i l e t and t h i s area went P

negative during deconvo u t i on.

? - Peak i s too narrow.

@ - Peak i s too wide a t FW25M, but ok a t FWHM.

% - Peak f a i l s s e n s i t i v i t y t e s t.

$ - peak i d e n t i f i e d, but fi r s t peak o f t h i s nuclide f a i l e d one o r more qua1 i f i cation tests.

Page 3

PBO7-03126

+ - peak a c t i v i t y higher than counting uncertainty range.

- - Peak a c t i v i t y lower than counting uncertainty range.

= - peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o the l i b r a r y energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

P - peakbackground subtraction

) - Peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

~ u c l i

de codes :

T - ~ h e r m a l Neutron ~ c t i v a t i o n F - Fast Neutron A c t i v a t i o n I

- Fission Product N - ~ a t ~ - r a l l y occurring Isotope P - Photon Reaction c - charged p a r t i c l e Reaction M - NO MDA c a l c u l a t i o n R - coincidence corrected H - H a l f l i f e 1 i m i t exceeded Peak Codes:

G - Gamma Ray x - X - ~ a y P - Positron Decay s - single-~scape D - ~ o u b l e - ~ s c a p e K - Key Line A - ~ o t i n Average C - Coincidence Peak S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

Time o f count Time corrected Uncertainty 2 sigma Nucl i de ti v i t y A c t i v i t y Counting Total MDA P C ~

/g PC? /g pci /g pci /g K-40 1.3388E+Ol 1.3388E+Ol 2.6132E+OO 2.6482~+00 9.397E-01 CO-60 B<

9.587OE-02 9.5981E-02 Ag-108mB<

6.8588~-02 6.8589E-02 CS-137 B<

6.3754E-02 6.3766E-02 EU-152 B<

1.1702E-01 1.1707E-01 EU-154 B<

9.3908E-02 9.3974E-02 PB-212

6.7936E-01 6.7936E-01 2.1188E-01 PB-214

9.8042E-01 9.8042E-01 2.1144E-01 BI-212 B<

9.08IOE-01 9.081OE-01 I

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:29:03 Page 5

PBRF spectrum name: Pe07-03126,~nl BI-214

9.6346E-01 9.6346E-01 2.6503E-01 2.6731E-01 1.671E-01 RA-226 B<

1.8775E+00 1.8775E+00 TH-234 B<

1.5680E+00 1.5680E+00 U-235 B<

5.3336E-01 5.3336E-01 AM-241 B<

1.6023E-01 1.6023E-01

-1 tpea~-foract-&~-Jna&~ad-st+ape----- -- - - - - - --

f f - H

- A c t i v i t y omitted from t o t a l

& - A c t i v i t y omitted from t o t a l and a l l peaks had bad shape.

< - MDA value printed.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y < MDA and f a i l e d t e s t.

c - Area < c r i t i c a l l e v e l.

F -. ailed f r a c t i o n o r key l i n e t e s t.

H - H a l f l i f e 1 i m i t exceeded S U M M A R Y

~ o t a l

~ c t i v i t y (

38.7 t o 2037.3 kev) 0.0000000E+00 pCi/g

~ 0 t a l Decayed ~ H i v i t y (_ 38.7 t o 2037.3 kev) 0.0000000E+00 pCi/g

~ n a 1 yzed by :

J PBRF &commi ssioni ng Project Page 4

~t3v-i ewed by :

~ a b o r a t o r y : PBRF Page 5

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:33:26 Page PBRF spectrum name: PB07-03127.~nl sample description

~ ~ 0 7 - 0 3 1 2 7 ;

SR38-69; HPT 104; HOLE 5; 21.75; 10/4/07 spectrum Filename: \\\\pbrf-library\\library d a t a \\ ~ a b \\ S A ~ p ~ ~

07\\pe07-031 27. ~ n l A C ~ U ~

s i t i o n information s t a r t time:

Live time:

Real ti me :

Dead ti me :

Detector ID:

Detector system

2 DETECTOR (#130) cal i b r a t i on F i 1 ename :

250ml #73678-773 (Mc130)sept07 Energy c a l i b r a t i on created :

zero o f f s e t :

Gai n :

quadrati c:

Efficiency c a l i b r a t i o n created:

Type :

uncertainty:

c o e f f i c i e n t s :

L i brary ~i 1 es

~ a i n analysis l i b r a r y :

~i brary Match width :

peak stripping:

COPY 13-Sep-2007 15:00:31 0.287 kev 0.251 kev/channel 2.324~-08 keV/channelA2 13-Sep-2007 15:22:08 pol ynomi a1 plumbrk 0 l. l i b 0.500 Library based

~ n a l y s i s parameters Analysi s engine:

npp32 G53W3.05

-start *and r-

- --IS- -- - 39.27kev-)- - - - -

s t o channel:

R 8144 ( 2049.92kev )

pea r e j e c t i o n 1 eve1 :

25.000%

peak search s e n s i t i v i t y :

3 sample Size:

4.3800~+02 A c t i v i t y scaling f a c t o r :

1.0000E+06/(

1.0000~+00* 4.3800E+02) =

2.2831E+03

~ e t e c t i on 1 i m i t method :

Nureg 4.16 and om e r r o r :

systematic e r r o r :

~ r a c t i on L i m i t :

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:33:26 Page Page 1

PBRF PB07-03127 spectrum name: ~ ~ 0 7 - 0 3 1 2 7. ~ n 1 Background width:

~ a l f l i v e s decay l i m i t :

A c t i v i t y range f a c t o r :

Min. step backg. energy best method (based on spectrum).

corrections Decay correct t o date:

Decay during acquisition:

Decay during c o l l e c t i on:

True coincidence correction:

Peaked background correction :

Absorption (Internal) :

Geometry correction:

Random summi ng :

Status YES NO NO NO NO NO NO NO Comments 01-Oct-2007 10:55:00 Energy c a l i b r a t i o n

~ 0 r m a l i zed d i ff:

S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area Uncert FWHM Corrctn Nuclide Brnch.

Act.

Nuc Energy Factor Energy Ratio pCi/g n**n**+*nnnn u N I D E N T I F I E D P E A K s u M M A R y ****f:******"

peak centroid Background Net Area I n t e n s i t y uncert FWHM Sus ected Channel Energy counts Counts Cts/Sec 2 Sigma %

kev NUC 7 i d e 295.55 74.61

51.

74.

0.246 42.48 0.954BI-207 M

s - Peak f a i l s shape tests.

D - Peak area deconvoluted.

L - peak w r i t t e n from unknown l i s t.

c - Area < C r i t i c a l l e v e l.

M - peak i s close t o a l i b r a r y peak.

- - - ~ h i s section based on l i b r a r y : plumbrk O l. l i b a

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:33:26 Page 3

PBRF Spectrum name: ~BOi'-03127.~nl

- - - - ?c***n**f:*

1 D E N T 1 F 1 E D P E A K S U M M A R Y ********f:***f;"

~ u c l i d e Peak centroid ~ackground Net Area I n t e n s i t y uncert FWHM channel Energy Counts counts Cts/sec 2 Sigma %

kev Page 2

~g-108m EU-154 61-212 EU-154 BI-214 CO-60 EU-154 CO-60 EU-152 K-40 s - Peak f a i l s -shape t e s t s.

D - Peak area deconvoluted.

A

~ e r i v e d peak area.

fr****

S U M M A R Y O F L I B R A R Y P E A K U S A G E *****

- ~ u c l i d e - Average

peak --------------

~ a m e. code ~ c t i v l t y Energy A c t i v i t y code MDA Value P C ~

/g kev P C ~

/g P C ~

/g COMMENTS ORTEC g v - i (1087) npp32 G53w3.05 04-OCT-2007 15:33:26 Page PBRF spectrum name: ~B07-03127.~!11

~ u c l i d e AVe a c t i v i t y Energy A c t i v i t y code Peak MDA Comments BI-214 N

9.6537E-01

.. - -... - - - - - - - - - - - - - - - - - - - - - - - 6W; 31 -9.654 E - (- -. W%E -

1764.49 O.OOOE+OO 8.34OE-01 1120.29 2.298E+OO +

6.049E-01

( - This peak used i n t h e nuclide a c t i v i t y average.

- peak i s too wide, but only one peak i n l i b r a r y.

! - Peak i s p a r t. o f a m u l t i l e t and t h i s area went 7

negative d u r i ng deconvo u t i on.

? - peak i s too narrow.

@ - peak i s too wide a t FWZSM, but ok a t FWHM.

% - 'peak f a i l s s e n s i t i v i t y t e s t.

$ - peak i d e n t i f i e d, but f i r s t peak o f t h i s nuclide f a i l e d one o r more qua1 i fi c a t i on tests.

+ -. peak a c t i v j t y higher than counting uncertainty range

- - peak a c t i v i t y lower than counting uncertainty range.

Page 3

PB07-03127

= - peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o the 1i brary energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

P - peakbackground subtraction

) - Peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

~ u c l i

de codes :

T - Thermal Neutron Activation F - Fast Neutron Activation I - Fission product N - Naturally occurring Isotope P - Photon Reaction C - charged P a r t i c l e Reaction M - NO MDA calculation R - coincidence corrected H - H a l f l i f e 1 i m i t exceeded Peak codes:

G - Gamma Ray x - X - ~ a y P -. Positron Decay S - Sin l e - ~ s c a p e D - DOU l e - ~ s c a p e K - Key Line A - ~ o t i n Average C - Coincidence peak S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

Time o f count Time corrected Uncertainty 2 Sigma Nuclide Acti v i t y A c t i v i t y Counting Total MDA pci /g pci /g pci /g pci /g K-40 1.8119E+Ol 1.8119E+01 3.154OE+OO 3.2066E+OO 1.012E+00 CO-60 B<

1.0392E-01 1.0404E-01 Ag-108mB<

4.7486E-02 4.7486E-02 CS-137 B<

7.1478E-02 7.1492E-02 EU-152 B<

1.3239E-01 1.3245E-01 EU-154 B<

1.0569E-01 1.0577E-01 PB-212

7.7524E-01 7.7524E-01 2.1123E-01 PB-214 &

1.3542E+OO 1.3542E+OO 2.9298E-01 BI-212 B<

9.9723E-01 9.9723E-01 0

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:33:26 Page 5

PBRF spectrum name: PB07-03127.~nl BI-214

9.6537E-01 9.6537E-01 3.0092E-01 3.0291E-01 2.078E-OJ RA-226 B<

1.6610E+00 1.6610E+00 TH-234 B<

1.4978E+00 1.4978E+00 U-235 B<

5.9727E-01 5.9727E-01 AM-241 B<

2.1355E-01 2.1355E-01

- ~ l l peaks f o r a c t i v i t y calculation had bad shape.

- -. - - - - * - A c t i v i t y omitted from t o t a l

&- =-Acti~ity-omftteCk from total-and-a-'fT -peaks had-bad-shape-.- - - - - - -

< - MDA value printed.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y < MDA and f a i l e d t e s t.

C - Area < ~ r i ti cal 1 eve1.

F - Failed f r a c t i o n o r key l i n e t e s t.

H - ~ a l f l i f e l i m i t exceeded S U M M A R Y

~ 0 t a 1 ~

~

t i

v i t

~ 0 t a l

~ecayed Anal yzed by :

~ e v i ewed by :

supervisor

~ a b o r a t o r y : PBRF Page 5

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:38:24 page PBRF spectrum name: PB07-03128.~n1 sampl e descri p t i o n PB07-03128; SR38-70; HPT 104; HOLE 5; 24.5; 10/4/07 spectrum ~ilename: \\\\Pbrf-library\\library data\\Lab\\SA~p~E 07\\~B07-031

28. An1 A C ~ U ~

s i t i o n information s t a r t time:

Live time:

Real ti me :

Dead ti me :

Detector I D :

Detector system

3 DETECTOR (#131) cal i b r a t i on F i 1 ename :

250ml #73678-773 ( ~ ~ 1 3 1 )

Sept07 Energy c a l i b r a t i o n created:

zero o f f s e t :

Gai n :

quadrati c:

E f f i ciency c a l i b r a t i o n created:

Type :

Uncertainty:

coefficients:

~i brary ~i 1 es Main analysis l i b r a r y :

L i brary Match Width :

peak stripping :

COPY 05-sep-2007 16:56:38 0.565 kev 0.247 kev/channel 5.022~-08 kev/channelA2 05-sep-2007 17:17:39 pol ynomi a1 1.204 %

-0.304311

-4.249899 0.669559

-0.094002 0.005803

-0.000133 p l umbrk 01.1 i b

0.500 L i brary based AtIalysi s parameters

- - - - - - - - - - - ~ n a l ys1 s engi ne:

npp32 G53W3.05

-start-cmF111-----------f5Ef ---%83kw-)-

sto channel:

8144 ( 2014122kev )

Pea[ rejection 1 eve1 ;

2 5. 000%

peak search s e n s i t i v i t y :

3 sample Size:

4.1870~+02 Acti v i t y scal i ng factor:

1.0000E+06/(

1.0000E+00*

4.1870E+02) =

2.3883~+03 Detection 1 i m i t method:

and om e r r o r :

systematic error:

FraCtl on ~i m i t :

Nureg 4.16 ORTEC g v - i (1087) npp32 G53W3.05 04-ocT-2007 15:38:24 Page Page 1

PBRF PBO7-03128 Spectrum name: ~B07-03128.~nl Background w i dth :

~ a l f l i v e s decay l i m i t :

A c t i v i t y range factor:

in. step backg. energy best method (based on spectrum).

corrections Decay correct t o date:

Decay during acqui s i t i o n :

Decay during co1 1 e c t i on :

True coincidence correction:

peaked background correction:

~ b s o r p t i o n (Internal) :

Geometry correction:

Random summi ng :

status YES NO NO NO NO NO NO NO Comments 01-Oct-2007 10:58:00 Energy cal i bration Normal i zed d i ff :

S U M M A R Y O F P E A K S I

N R A N G E *****

peak Area uncert FWHM corrctn Nuclide Brnch.

Act.

Nuc Energy Factor Energy Ratio pci/g

- - f~********

U N 1 D E N T 1 F 1 E D P E A K S U M M A R Y "***********

peak centroid ~ackground Net Area Intensity Uncert FWHM Sus ected channel Energy Counts Counts Cts/Sec 2 Sigma %

kev Nuc 7 i d e s - peak f a i l s shape tests.

D - peak area deconvoluted.

L - Peak written from unknown l i s t.

c - Area < C r i t i c a l 1 eve1.

ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:38:24 page PBRF spectrum name: ~ ~ 0 7 - 0 3 1 2 8. ~ n 1

- - - - 1 D E N T 1 F 1 E D P E A K S U M M A R Y ******"*******

~ u c l ide peak centroid Background Net Area

~ n t e n s i t y Uncert FWHM channel Energy Counts counts Cts/Sec 2 sigma %

kev AM-241 0.00 59.54

0.

0.000 0.00 0.000 TH-234 0.00 63.29

0.

0.000 0.00 0.000 TH-234 0.00 92.59

0.

0.000 0.00 0.000 Page 2

s -.Peak f a i l s shape t e s t s.

D - peak area deconvoluted.

A Derived peak area.

S U M M A R Y O F L I B R A R Y P E A K U S A G E *****

- ~ u c l i d e - Average

- m u - - - - - - - - - -

peak --------------

Name Code

~ c f i v l t y Energy A c t i v i t y code MDA Value P C ~

/g kev P C ~

/g P C ~

/g COMMENTS ORTEC g v - i (1087) npp32 G53W3.05 04-~CT-2007 15:38:24 page PBRF spectrum name: PB07-03128.Anl

~ u c l i d e Ave a c t i v i t y Energy

~ c t i v i t y code peak MDA Comments

- - - - - B I - m - - N - - - l - m + 8 0 609.31 1.289E+00

( 1.952E-01 12.58 G K 1764.49 O.OOOE+OO 8.699E-01 26.73 G 1120.29 1.41OE+OO &(

6.113E-01 24.25 G

( - his peak used i n t h e nuclide a c t i v i t y average.

- peak i s t o o wide, but o n l y one peak i n l i b r a r y.

! - peak i s p a r t o f a m u l t i l e t and t h i s area went 9

negative d u r i ng deconvo u t i on.

? - peak i s t o o narrow.

@ - Peak i s too wide a t FW25M, but ok a t FWHM.

% - Peak f a i l s s e n s i t i v i t y t e s t.

$ - peak i d e n t i f i e d, b u t fi r s t peak o f t h i s nuclide f a i l e d one o r more q u a l i f i c a t i o n tests.

+ - Peak a c t i v i t y higher than counting uncertainty range Page 3

PBO7-03128

- - Peak a c t i v i t y lower than counting uncertainty range.

= - Peak outside analysis energy range.

& - calculated peak centroid i s not close enough t o t h e l i b r a r y energy centroid f o r p o s i t i v e i d e n t i f i c a t i o n.

P - peakbackground subtraction

} - Peak i s too close t o another f o r the a c t i v i t y t o be found d i r e c t l y.

Nucl i de codes :

T - Thermal Neutron A c t i v a t i o n F - Fast Neutron A c t i v a t i o n I - Fission Product N - ~ a t u r a l l y occurring xsotope P - Photon Reaction c - Charged P a r t i c l e ~ e a c t i o n M - NO MDA c a l c u l a t i o n R - coincidence corrected H - H a l f l i f e l i m i t exceeded Peak codes:

G - Gamma Ray x - X - ~ a y P - Positron Decay S - single-~scape D - Doubl e-Escape K - Key Line A - Not i n Average c - coincidence Peak "jr"**

S U M M A R Y O F N U C L I D E S I

N S A M P L E *****

~ i m e o f Count Time Corrected Uncertainty 2 Sigma

~ u c l i

de A c t i v i t y A c t i v i t y counting Total MDA P C ~

/g p c i /g pci /g p c i /g ORTEC g v - i (1087) npp32 G53W3.05 04-OCT-2007 15:38:24 page PBRF spectrum name: PB07-03128.Anl

- - - - - - - - # - ~ l l peaks f o r a c t i v i t y calculation had bad shape.

+

=

~

i t

y

~

d f

~

& - A c t i v i t y omitted f rom. t o t a l and a1 1 peaks had bad shape.

< - MDA value printed.

A - A c t i v i t y printed, but a c t i v i t y < MDA.

B - A c t i v i t y < MDA and f a i l e d t e s t.

c - Area < C r i ti $a1 1 eve1.

F - Failed f r a c t l o n o r key l i n e t e s t.

H - ~ a l f l i f e l i m i t exceeded S U M M A R Y Total A c t i v i t y (

38.8 t o 2014.2 kev) 0.0000000E+00 pCi/g

~ o t a l

~ecayed A c t i v i t o 2014.2 kev) 0.0000000~+00 pCi/g Anal yzed by:

I PBRF &cornmi s s i oni ng project Page 4

~ e v i ewed by :

"7 Laboratory:

PBRF R. Case Page 5

SECTION 7 ATTACHMENT 5 1 PAGE

SUMMARY

DQA Check Sheet Design #

EP HPT-104 Revision #

Original Summary Survey Unit #

EP HPT-104 Preliminary Data Review' Answers to the following questions should be fully documented in the Survey Unit Yes No N,*

Release Record

1. Have surveys been performed in accordance with survey instructions in the Survey Design?

X

2. Is the instrumentation MDC for structure static measurements below the DCGLw for Class 1 and 2 survey units, or below 0.5 DCGLW for Class 3 survey units?

X

3.

Is the instrumentation MDC for embeddedtburied piping static measurements below the DCGLw ?

X

4.

Was the instrumentation MDC for structure scan measurements, soil scan measurements, and embeddedlburied piping scan measurements below the DCGLw, or, if not, was the need for additional X

static measurements or soil samples addressed in the survey design?

5. Was the instrumentation MDC for volumetric measurements and smear analysis < 10% DCGLw ?

X

6. Were the MDCs and assumptions used to develop them appropriate for the instruments and techniques used to perform the survey?

7.

Were the survey methods used to collect data proper for the types of radiation involved and for the media being surveyed?

X

8. Were "Special Methods" for data collection properly applied for the survey unit under review?

X

9. Is the data set comprised of qualified measurement results collected in accordance with the survey design, which accurately reflects the radiological status of the facility?

X Graphical Data Review

1.

Has a posting plot been created?

X

2.

Has a histogram (or other frequency plot) been created?

X

3.

Have other graphical data tools been created to assist in analyzing the data?

X Data Analysis Item 5 is NIA due to speclal methods measurements.

Page 1 of 1

SECTION 7 ATTACHMENT 6 1 DISC

SUMMARY

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