ML063400445

Final Status Survey Final Report Phase IV, Appendix A8, Survey Unit Release Record 9106-0008, Discharge Canal

ML063400445
Person / Time
Site:	Haddam Neck File:Connecticut Yankee Atomic Power Co icon.png
Issue date:	11/17/2006
From:	Newson C Connecticut Yankee Atomic Power Co
To:	NRC/FSME
References
9106-0008
Download: ML063400445 (227)

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Final Status Survey Final Report Phase IV Appendix A8 Survey Unit Release Record 9106-0008, Discharge Canal November 2006

CYAPCO FINAL STATUS SURVEY RELEASE RECORD DISCHARGE CANAL SURVEY UNIT 9106-0008 Prepared By: Date:

FSSEnineer~

Reviewed By: Date: j F, ,ngineer Approved By: CAIr Date:"

Technical Support Manager Revision 0

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD TABLE OF CONTENTS

1. SURVEY UNIT DESCRIPTION ................................................................. 3

2. CLASSIFICATION BASIS ...................................................................... 3

3. DATA QUALITY OBJECTIVES (DQO) .................................................... 5

4. SURVEY DESIG N..................................................................................... 8

5. SURVEY IMPLEMENTATION ................................................................ 11

6. SURVEY RESULTS ............................................................................... 12

7. QUALITY CONTROL ............................................................................. 13

8. INVESTIGATIONS AND RESULTS ...................................................... 14

9. REMEDIATION AND RESULTS ............................................................. 14

10. CHANGES FROM THE FINAL STATUS SURVEY PLAN ..................... 14

11. DATA QUALITY ASSESSMENT (DQA) ................................................. 14

12. A NO MA LIES ........................................................................................... 15

13. CO NCLUSIO N ....................................................................................... 15

14. ATTACHM ENTS ..................................................................................... 16 14.1 Attachment 1 - Figures (7 pages including cover) 14.2 Attachment 2 - Sample and Statistical Data (203 pages including covers)

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DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD SURVEY UNIT DESCRIPTION Survey Unit 9106-0008 (Discharge Canal) is designated as Final Status Survey (FSS) Class 2 and consists of approximately 9,763 m2 (2.41 acres) of water covered sediment in an area located approximately 0.92 miles from the reference coordinate system benchmark used at the Haddam Neck Plant (HNP)

(see Attachment 1, Figure 1). The Discharge Canal is a man-made mile long waterway that runs parallel to, and ultimately communicates with the Connecticut River. The Discharge Canal is subdivided into fifteen (15) survey units including two (2) permanent wetland areas for FSS purposes. The survey unit is bounded as follows: Discharge Canal Survey Unit 9106-0007 is to the north (called north as orientated with the north to south flow of the Connecticut River), Survey Area 9523 is to the east, Discharge Canal Survey Unit 9106-0009 is to the south and South Peninsula Survey Area 9531 (formerly a part of 9530) is to the west. The survey unit comprises the canal sediments to the deeper of three feet or the original construction depth and it extends up the canal banks to the mean high water level.

The reference coordinates associated with this survey unit are E019 through E026 by S143 through S153 (refer to License Termination Plan Section 5.4.4).

The reference coordinates provide the maximum dimensions of a rectangle containing this survey unit. Some areas contained in this rectangle may not be part of this survey unit. The boundary of the survey unit was defined using a Global Positioning System (GPS) based on the Connecticut State Plane System North American Datum (NAD) 1927.

2. CLASSIFICATION BASIS The survey unit was classified in accordance with Procedure RPM 5.1-10, "Survey Unit Classification." The historical information, scoping analyses and characterization results provided sufficient data to designate Survey Unit 9106-0008 as Class 2 in May 2006.

The "Classification Basis Summary" conducted for this survey unit consisted of:

a) A review of the 10CFR50.75 (g) (1) database, b) A review of the "Initial CharacterizationReport" and the "HistoricSite Assessment (HSA) Supplement, "

c) Historic and current survey records review, d) Visual inspections and a "walkdown."

e) Formal or informal interviews with cognizant personnel.

A review of the 10CFR50.75(g)(1) database report identified a number of events that may have impacted this survey unit. In 1986, samples were taken from the legacy dredge spoils removed in 1979 dredged spoils area and from recently dredged canal sediment. The sample analyses indicated that the Revision 0 3

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD concentrations of Cs-137, Co-60 and other radionuclides were a small fraction of the DCGLs for those nuclides that could be identified by gamma spectroscopy. (refer to NE-86-RA-1142 dated 11-13-86). None the available historical information reviewed would support a conclusion that any residual activity in this survey unit is likely to be present at concentrations greater than the respective DCGLs.

Additional information was provided by several historical documents, including the "Results of Scoping Survey", (completed 9/1/98), the "Historical Site Assessment", and the HSA Supplement (dated 6-30-00). These documents presented the results of several sediment samples taken in 1997. These sample results indicated concentrations of 0.5 pCi/g for Co-60, 0.024pCi/g for Cs-134 and 0.722 pCi/g for Cs-137.

An initial characterization survey was implemented during April and May of 2004. However, none of the sampling fell inside the footprint of 9106-0008. In an adjacent Survey Unit (9106-0009) six (6) samples from three (3) locations were obtained by biased sampling throughout the area. The samples were analyzed off-site by gamma spectroscopy and with radiochemical analyses for Sr-90 and Tritium. Hard-to-Detect analyses were also conducted on one (1) of the six (6) samples. The only plant-related dosimetrically significant radionuclides identified in the samples were Cs-137, Cobalt-60 and Ni-63. No samples indicated radioactive material in quantities above the ten (10) mrem/yr design DCGL. Cobalt-60 accounted for the majority of the dose in these samples with a maximum concentration of 0.57 pCi/g.

A final characterization was performed by Site Closure personnel in April of 2006. Six (6) sediment samples from six (6) locations were taken. All of the samples were analyzed by gamma spectroscopy. Based on the initial and final characterization results, the radionuclides of concern identified in the sample data for FSS planning purposes were Cesium-137, Cobalt-60 and Ni-63. Since HTD analyses were not performed for all radionuclides of interest during characterization, additional HTD analyses were performed as a part of the FSS.

The statistics for each of the radionuclides of concern are listed in Table 1.

Additionally, since Sr-90 was a radionuclide of concern in an adjacent Survey Unit (9106-0007), it was decided that testing for this isotope was an appropriate conservatism.

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DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD minimum value: -4.YiL-UJ -i ./4L-U4 -I . tLt+UU Maximum Value: 2.5 1E-01 5.87E-01 3.47E+O1 Mean: 1.39E-01 3.28E-01 1.65E+01 Median: 1.42E-01 3.1 OE-01 1.65E+0 I Standard Deviation: 9.84E-02 2.09E-01 2.57E+O1 NOTE: The Operational DCGLs are 6.01 pCi/g for Cs-137, 2.90 pCi/g for Co-60 and 549 for Ni-63; these are used in conjunction with the unity rule to achieve nineteen (19) mnremn/yr TEDE.

The FSS Engineer performed a visual inspection and walk-down during May 2006 to assess the physical condition of the survey unit, evaluate access points and travel paths and identify potentially hazardous conditions.

Based upon the historical information and the results of radiological surveys performed during characterization, it was concluded that there was a low probability for residual radioactivity to be present in this survey unit in concentrations greater than the Operational DCGLs justifying a final survey unit classification of Class 2 (refer to Section 3).

3. DATA QUALITY OBJECTIVES (DQO)

FSS design and planning is based on the Data Quality Objective (DQO) process as described by the LTP, Procedure RPM 5.1-11, "Preparationof FinalStatus Survey Plan," and the "Multi-Agency Radiation Survey and Site Investigation Manual" (MARSSIM). A summary of the main features of the DQO process are provided herein.

The DQO process incorporates hypothesis testing and probabilistic sampling distributions to control decision errors during data analysis. Hypothesis testing is a process based on the scientific method that compares a baseline condition to an alternate condition. The baseline condition is technically known as the null hypothesis. Hypothesis testing rests on the premise that the null hypothesis is true and that sufficient evidence must be provided for rejection. In designing the survey plan, the underlying assumption, or null hypothesis was that residual activity in the survey unit exceeded the release criteria. Rejection of the null hypothesis would satisfy the release criteria objective of the FSS.

The primary objective of the Final Status Survey Plan (FSSP) was to demonstrate that the level of residual radioactivity in Survey Unit 9106-0008 did not exceed the release criteria specified in the LTP and that the potential dose from residual radioactivity is As Low As Reasonably Achievable (ALARA).

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DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD A fundamental precursor to survey design is to establish a relationship between the release criteria and some measurable quantity. This is done through the development of Derived Concentration Guideline Levels (DCGLs). The DCGLs represent the concentration of radioactivity above background, equivalent to a dose-based release criterion and is presented in terms of surface or mass activity concentrations. Chapter 6 of the LTP describes in detail the modeling used to develop the DCGLs for soil (called Base Case Soil DCGL),

for existing groundwater radioactivity and for future groundwater radioactivity that will be contributed by building foundations and footings.

As described in detail in the LTP, the dose model applied to the discharge canal presumes that the canal sediments are dredged to a depth of three (3) feet below the top of the sediment layer and spread for the planting of crops per the Resident Farmer Scenario. Consequently, the soil DCGLs are directly applied to the canal sediment media.

The DCGLs presented in Chapter 6 of the LTP were developed for exposures from three (3) components, that is, residual radioactivity in soil, existing groundwater radioactivity, and future groundwater radioactivity from the burial of concrete foundations or footings from site buildings containing residual radioactivity. Equation 1 shows the mathematical relationship between the three (3) components and the total dose.

Equation 1:

HTotal=Hsoil (sediment) + HExisting GW + HFuture GW The total dose under the LTP criteria is twenty-five (25) mrem/yr TEDE from all three components. The allowable total dose under the Connecticut Department of Environmental Protection (CTDEP) radiological remediation standard for Connecticut Yankee (CY) is nineteen (19) mrem/yr TEDE. To satisfy both the LTP and CY CTDEP criteria, the dose from soil must be reduced when using the groundwater dose values discussed above.

This survey unit is not affected by either existing groundwater or by future groundwater (reference CY memo ISC 06-024). Therefore, dose contribution from both existing and future groundwater is zero (0) mremryr TEDE, based on field data.

Equation 2:

19 mrem/yr 1 otal= 19 mrem/yrsoil+0 mrem/yrExisting GW+O mrem/yrFuture GW The allowable dose for sediment in this survey unit is nineteen (19) mrem/yr TEDE as shown by Equation 2 above. The concentration of residual radioactivity resulting in nineteen (19) mrem/yr TEDE is designated as the Operational DCGL, and has been established for the radionuclides of concern Revision 0 6 Revision 0 6

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD as provided in Table 2. Note: the survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 to conservatively account for the contribution to the total dose from existing and future groundwater which had not been established at the time of planning the FSS.

STable 2 -Radiorniidlide SpecificRseCs Bc SoiCl(( ,Oeaini C~

and Required Minimium Dfetetable Concentrations Radionuclide () BaseCase Soil Operational DCGL Required NDC DCGL (g~i/g) (2) (jpCi/g 3 (3)J(p ci/g)S H-3 4.12E+02 3.13E+02 1.65E+01 C-14 5.66E+00 4.30E+00 2.26E-01 Mn-54 1.74E+01 1.32E+O1 6.96E-01 Fe-55 2.74E+04 2.08E+04 1.1OE+03 Co-60 3.81E+00 2.90E+00 1.52E-01 Ni-63 7.23 E+02 5.49E+02 2.89E+OI Sr-90 1.55E+00 1.18E+00 6.20E-02 Nb-94 7.12E+00 5.41 E+00 2.85E-0 I Tc-99 1.26E+01 9.58E+00 5.04E-0 I Ag- 108m 7.14E+00 5.43 E+00 2.86E-01 Cs- 134 4.67E+00 3.55E+00 1.87E-01 Cs-137 7.91E+00 6.01E+00 3.16E-0 I Eu- 152 1.01E+01 7.68E+00 4.04E-01 Eu-154 9.29E+00 7.06E+00 3.72E-01 Eu- 155 3.92E+02 2.98E+02 1.57E+01 Pu-238 2.96E+01 2.25E+01 1.18E+00 Pu-239/240 2.67E+01 2.03 E+0I 1.07E+00 Pu-241 8.70E+02 6.61E+02 3.48E+0I Am-241 (5) 2.58E+01 1.96E+O1 1.03E+00 Cm-243/244 2.90E+O1 2.20E+O1 1.16E+00 (1) Bold indicates those radionuclides considered to be Hard to Detect (HTD)

(2) The Base Case Soil DCGLs for soil are specified by the LTP in Chapter 6 and are equivalent to twenty-five (25) mrem/yr TEDE (3) The Operational DCGL is equivalent to nineteen (19) mrem/yr TEDE (4) The required MDC is equivalent to one (1) mrem/yr TEDE (5) Americium-241 can be analyzed by gamma and alpha spectroscopy and is considered to be Easy to Detect (ETD). The preferred result is the alpha spectroscopy's when both analyses are performed.

Another important facet of the DQO process is to identify the radionuclides of concern and determine the concentration variability. Characterization was completed in April of 2006 as discussed in Section 2. Cesium-137, Cobalt-60 Revision 0 7 Revision 0 7

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD and Nickel-63 were found to be the predominate radionuclides of concern. The basic statistical quantities (i.e., mean, standard deviation, median) for Cs-137, Co-60 and Ni-63 are provided in Table 1.

Laboratory DQOs and analysis results were to be reported as actual calculated results. Results reported as less than Minimum Detectable Concentration

(<MDC) would not be accepted for FSS. Sample report summaries were to include unique sample identification, analytical method, radionuclide, result, and uncertainty of two standard deviations, laboratory data qualifiers, units, and the required and observed MDC.

4. SURVEY DESIGN The level of effort associated with planning a survey is based on the complexity of the survey and nature of the hazards. To assist the FSS Engineers when preparing survey plans for FSS, guidance is provided in Procedure RPM 5.1-11, "Preparationof Final Status Survey Plans". By design, the FSSP meets the ALARA criteria for soils as specified in Chapter 4 of the LTP. The FSSP uses an integrated sample design that combines scanning surveys and sampling which can be either random or biased.

Characterization was performed by Site Closure personnel in April and May 2006 to determine existing conditions and obtain radiological data for Final Status Survey (FSS). The DQO process determined that Cs-137, Co-60, Sr-90 and Ni-63 would be the radionuclides of concern (refer to Section 3). The sum of fractions or unity rule would be used with the individual Operational DCGLs because multiple radionuclides (Cs-137, Co-60, Sr-90 and Ni-63) were considered in the survey design. Other radionuclides identified during FSS would be evaluated to ensure adequate survey design and compliance with the unity rule.

Surrogate DCGLs were not required for this survey unit based on process knowledge from FSS of nearby adjacent areas and via screening process described in LTP Section 5.4.7.2, "Gross Activity DCGLs". Sr-90 concentrations in sediment and soil were ascertained by direct analysis.

Radionuclide screening or de-selection is a process where an individual radionuclide or aggregate may be considered insignificant and eliminated from the FSS. The criteria for de-selection are concentrations that are less than 5%

for individual radionuclides and that are less than 10% for the aggregate of all radionuclides that are de-selected. This process was applied to analysis data for this survey unit.

The Elevated Measurement Comparison (EMC) did not apply to this survey unit since the survey unit is a Class 2 and discrete, elevated areas of contamination were not expected.

The Sign Test was selected as the non-parametric statistical test. The use of the Sign Test did not require the selection or use of a background reference area, Revision 0 8

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD which simplified survey design and implementation. This approach was conservative since it included background Cs-137 as part of the sample set.

The number of sediment samples for FSS was determined in accordance with Procedure RPM 5.1-12, "Determination of the Number of Samples for Final Status Survey. " The Lower Bound of the Gray Region (LBGR) was set in accordance with Procedure RPM 5.1-11 to 0.5 to maintain the relative shift (A/a) in the range of 1 and 3. The resulting relative shift was 3.0. A Prospective Power Curve was generated using COMPASS, a software package developed under the sponsorship of the United States Nuclear Regulatory Commission (USNRC) for implementation of the MARSSIM in support of the decommissioning license termination rule (10 CFR 20, Subpart E). The result of the COMPASS computer run showed adequate power for the survey design.

This indicates that the survey unit has a high probability of rejecting the null hypothesis, assuming that the characterization data are representative of the FSS results. Survey design specified fourteen (14) sediment core samples for non-parametric statistical testing.

The grid pattern and locations of the sediment samples were determined using Visual Sample Plan (VSP) in accordance with Procedure RPM 5.1-14, "Identifying, and Marking Surface Sample Locations for Final Status Survey. "

Visual Sample Plan was created by Pacific Northwest National Laboratory (PNNL) for the United States Department of Energy. A systematic triangular grid pattern with a random starting point was selected for sample design, which is appropriate for a Class 2 area.

Sample locations were identified using AutoCAD-LT, a commercially available plotting software package with coordinates consistent with the Connecticut State Plane System. These coordinates were integrated with a GPS to locate sample locations in the field. Sample Measurement Locations for the design are listed with the GPS coordinates in Table 3.

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DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Table 3 -Sample MI-asir~enient Locations with Associated GPS Coordinates Designationl Northing ~ Eakstin 9106-0008-001F 234825.31 672724.61 9106-0008-002F 234825.31 672817.80 9106-0008-003F 234744.60 672771.20 9106-0008-004F 234744.60 672864.40 9106-0008-005F 234663.89 672817.80 9106-0008-006F 234663.89 672911.00 9106-0008-007F 234583.17 672864.40 9106-0008-008F 234583.17 672957.60 9106-0008-009F 234502.46 672911.00 9106-0008-01OF 234502.46 673004.20 9106-0008-01 IF 234421.75 672957.60 9106-0008-012F 234421.75 673050.79 9106-0008-013F 234341.04 673004.20 9106-0008-014F 234341.04 673097.39 Four (4) sediment samples were analyzed for the full suite of radionuclides specified in Table 1, exceeding the requirement to analyze 5% of the sample population for HTD analysis specified in procedure RPM 5.1-11. Two (2) of the four (4) samples were randomly selected using the Microsoft Excel "RAND" function. The two (2) samples exhibiting the highest observed radionuclide concentrations by gamma analyses were also selected.

The implementation of survey specific quality control measures as referenced by Procedure RPM 5.1-24, "Split Sample Assessment for FinalStatus Survey, "

included the collection of two (2) sediment samples for "split sample" analysis by the off-site laboratory. These locations were selected randomly using the Microsoft Excel "RAND" function. The number of quality control samples exceeded the 5% requirement.

The LTP specifies that scanning is not required for the FSS of the Discharge Canal. Table 4 provides a synopsis of the survey design.

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DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD survey unit Lana Based on AutoCAD-LT and Visual 9,763 m2 Area Sample Plan calculations Type 1 and Type 2 errors were 0.05, Number of 14 sigma was 0.166 the LBGR was set to Measurements 0.5 to maintain Relative Shift in the range of 1 and 3, Relative Shift was 3.0 Grid Spacing 28.4 m Based on triangular grid 3.16 pCi/g Cs-137 Design DCGL 1.52 pCi/g Co-60 To achieve ten (10) mrem/yr TEDE 0.62 pCi/g Sr-90 289 pCi/g Ni-63 6.01 pCi/g Cs-137 To achieve nineteen (19) mrem/yr Operational 2.90 pCi/g Co-60 TEDE (2)to demonstrate compliance DCGL 1.18 pCi/g Sr-90 with Equation 2 of this Release Record 549 pCi/g Ni-63 Scan Coverage N/A The LTP exempts this area Sediment 6.01 pCi/gCs-137 Investigation 2.90 pCi/g Co-60 The Operational DCGL meets the LTP Level 1.18 pCi/g Sr-90 criteria for a Class 2 survey unit 549 pCi/g Ni-63 (1) The survey design used a much smaller value for investigation than the Operational DCGL provided by Table 2 as the total dose from existing and future groundwater had not been established at the time of planning the FSS

5. SURVEY IMPLEMENTATION Final status survey field activities were conducted under Work Plan and Inspection Record (WP&IR) 2006-0021. The WP&IR package included a detailed FSSP, job safety analysis, job planning checklist and related procedures for reference. Daily briefings were conducted to discuss the expectations for job performance and the safety aspects of the survey. The "Daily Survey Journal" was used to document field activities and other information pertaining to the FSS.

Measurement locations were identified in North American Datum (NAD) 1927 coordinates that were supplied to the sampling vendor, Ocean Survey, Inc.

(OSI) of Old Saybrook, Connecticut. Discharge Canal sampling was accomplished using direct push technology to collect composite samples of bottom and mean high water mark sediments. Sediment cores from the Discharge Canal were obtained by OSI using a vibrating corer that is platform mounted on a sampling vessel. The core barrel was a three (3) inch diameter thin-walled aluminum tube which also served as a core liner (ten (10) feet or less). A core catcher was available to prevent the sample from sliding out of the bottom of the tube. Vessel positioning and the determination of sample Revision 0 I1I Revision 0 11

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD locations were accomplished using a GPS interfaced with a navigation and data logging system.

After extraction, water was drained from above the sample by drilling holes above the sediment. The liner was cut, capped, sealed, labeled and turned over to site personnel who processed and controlled the samples under Chain of Custody (COC) protocols in accordance with procedure RPM 5.1-5, "Chain of Custody for Final Status Survey Samples. " Rinsing of the barrel and associated equipment was performed between sampling events. New aluminum tubes were used for each sample to prevent cross-contamination of subsequent samples.

The Fourteen (14) sediment samples were collected and packaged in accordance with Haddam Neck Plant (HNP) Procedure RPM 5.1-3, "Collection of Sample Media for Final Status Survey". Samples were controlled, transported, stored, and transferred to the off-site laboratory using COC protocols.

Four (4) samples (9106-0008-006F, 9106-0008-007F, 9106-0008-008F and 9106-0008-012F) were selected for HTD radionuclide analysis by the off-site laboratory.

The implementation of survey specific quality control measures included the collection of two (2) split samples at locations 9106-0008-006F and 9106-0008-01 OF for "split sample" analysis by the off-site laboratory.

6. SURVEY RESULTS The off-site laboratory employed for the radiological analyses of samples was General Engineering Laboratories (GEL) - Charleston, South Carolina. The laboratory analyzed the fourteen (14) samples taken for non-parametric statistical testing and the associated duplicates using gamma spectroscopy. Sr-90 was analyzed by gas flow proportional counting. All analyses were performed to the required MDC.

Cesium-137 was identified in nine (9), Co-60 was identified in seven (7), Sr-90 was identified in two (2) and Ni-63 in none of the fourteen (14) samples. The results reported for the remaining sample analyses indicated that activity was present at levels approaching or below the established detection limits in the remaining samples collected and analyzed for non-parametric testing.

Several other radionuclides which were positively identified (i.e., a result greater than two (2) standard deviations uncertainty) could be de-selected or excluded using the 5% and 10% rule described in Section 5.4.7.2 of the LTP.

The off-site laboratory also processed four (4) samples for full HTD analysis as required by the sample plan. The requested analyses included alpha spectroscopy and liquid scintillation depending upon the radionuclide and the Revision 0 12 Revision 0 12

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD measurement method. All analyses were performed to the required MDC. Five (5) of the HTD radionuclides met the acceptance criteria for detection (i.e., a result greater than two standard deviations uncertainty) in more than one (1) sample; however, each of the positive results for HTD radionuclides could be de-selected based on the 5% and 10% rules.

None of the sample results exceeded the Operational DCGL or required further investigation. A summary of the sample results is provided in Table 5.

9106-0008-001 F 3.96E-01 1.33E-01 5.79E-03 2.33E-01 1.17E-01 9106-0008-002F -8.91 E-03 7.77E-03 2.03E-02 -4.84E+00 1.84E-02 9106-0008-003F 2.05E-01 3.24E-0 1 1. 12E-02 -2.74E+00 1.55E-01 9106-0008-004F 4.32E-02 0.00E+00 -6.19E-03 -1.80E+00 1.94E-03 9106-0008-005F 2.66E-01 2.75E-02 8.28E-04 -8.58E-01 5.44E-02 9106-0008-006F 4.92E-01 7.79E-01 5.59E-03 2.28E+00 3.55E-01 9106-0008-007F 2.29E-02 2.68E-02 -8.81E-04 -2.33E+00 1.23E-02 9106-0008-008F 4.72E-01 9.17E-01 -2.69E-03 -4.12E-01 3.92E-01 9106-0008-009F 1.55E-02 -1.08E-02 -5.90E-03 -2.05E+00 -6.15E-03 9106-0008-01OF 3.36E-01 2.46E-0I 3.47E-03 1.23E-01 1.44E-01 9106-0008-01IF 6.76E-02 1.22E-01 1.93E-02 -3.34E+00 6.97E-02 9106-0008-012F 1.84E-01 1.79E-01 -1.92E-02 8.39E-01 7.61 E-02 9106-0008-013F 1.03E-02 2.99E-02 9.80E-03 -2.70E+00 2.03E-02 9106-0008-014F -3.89E-03 -1.45E-02 5.40E-03 -1.72E+00 -1.07E-03 (1) The Operational DCGLs from Table 2 are 6.01 pCi/g for Cs-137, 2.90 pCi/g for Co-60, 1.18 for Sr-90 and 549 for Ni-63; these are used in conjunction with the unity rule to achieve nineteen (19) mrem/yr TEDE.

Biased sampling was not called for in the sample plan.

7. QUALITY CONTROL The two (2) split samples taken for QC were analyzed by the off-site laboratory.

The data were evaluated using USNRC acceptance criteria specified in Inspection Procedure 84750 and as detailed in HNP Procedure RPM 5.1-24, "Split Sample Assessment for FinalStatus Survey. "

Split-sample number 9106-0008-006F/S did not meet the comparison criterion for Co-60. A possible cause for this anomaly could be the presence of Co-60 in the form of discrete particles. Such a physical form does not lend itself to homogenous mixing in a sediment matrix and, therefore, is not necessarily an indicator of inadequate sampling or sample preparation methodology. In this sample, K-40, a natural radioisotope, was found to be present at an acceptable level of agreement, therefore, the comparison was determined to be acceptable.

Additionally, Cs-137 did meet the comparison criteria for the sample results.

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DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD However, Ni-63 and Sr-90 had resolutions of zero (0) and one (1) respectively and values <4 have not been addressed in NRC Inspection Procedure 84750.

Therefore, a determination of the acceptability for resolution values of <4 can not be made.

For the second QC split sample number 9106-0008-O1OF/S there was an acceptable level of agreement between the samples for CO-60 and Cs-137. In this sample, K-40, a natural radioisotope, was found to be present at an acceptable level of agreement, therefore, the comparison was determined to be acceptable. However, Ni-63 and Sr-90 had resolutions of zero (0) and one (1) respectively and resolution values of <4 have not been addressed in NRC Inspection Procedure 84750. Therefore, a determination of the acceptability for values <4 can not be made.

The sample analysis vendor, GEL, maintained quality control and quality assurance plans as part of normal operation. Refer to Attachment 2 for data and data quality analysis results.

8. INVESTIGATIONS AND RESULTS No Investigations were required to be performed since none of the sample results exceeded the investigation levels.

9. REMEDIATION AND RESULTS Historically, no radiological remedial action as described by MARSSIM Section 5.4 was performed in this survey unit prior to or as a result of the FSS. Health Physics TSD BCY-HP-0078, "ALARA Evaluation of Soil Remediation in Support of Final Status Survey, " determined that remediation beyond that required to meet the release criteria to be unnecessary and that the remaining residual radioactivity in sediment was ALARA.

10. CHANGES FROM THE FINAL STATUS SURVEY PLAN The survey was designed to ten (10) mrem/yr TEDE which was conservative and necessary at the time of FSS planning. It is no longer required as the total dose from existing and future groundwater has been established. The dose for sediment used to demonstrate compliance with the LTP criteria is nineteen (19) mremlyr TEDE as discussed in Section 2 of this Release Record.

11. DATA QUALITY ASSESSMENT (DQA)

The DQO sample design and data were reviewed in accordance with Procedure RPM 5.1-23, "Data Quality Assessment. " The sample design had adequate power as indicated by the Retrospective Power Curve. The Sign Test was performed on the data and compared to the original assumptions of the DQOs.

The evaluation of the Sign Test results indicates that the survey unit passes the unrestricted release criterion, thus, the null hypothesis is rejected.

Revision 0 14 Revision 0 14

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Documentation was complete and legible. Surveys and sample collection were consistent with the DQOs and were sufficient to ensure that the survey unit was properly designated as Class 2.

The preliminary data review consisted of calculating basic statistical quantities (e.g., mean, median, standard deviation). The standard deviation was slightly more than the value used for the survey design. This is represented by the shift in the retrospective power curve as shown in Attachment 2f. This would indicate a need to change the original LBGR in order to maintain the number of samples at fourteen (14) to meet the Operational DCGL. However, the value of the LBGR is not a critical issue as the survey unit has passed the statistical test, and the mean and median values are well below the Operational DCGL when used in conjunction with the unity rule. Also, the retrospective power curve shows that a sufficient number of samples were collected to achieve the desired power. Therefore, the survey unit meets the unrestricted release criterion with adequate power as required by the DQOs.

The range of the data, about 3.1 standard deviations, was not unusually large.

The difference between the mean and median was 30% of the standard deviation which indicates some skewness in the data. The data was represented graphically through posting plots, a frequency plot, and a quantile plot. The frequency plot shows some positive skewness as confirmed by the calculated skew of 1.58.

All data, assessments, and graphical representations are provided in Attachment 2.

12. ANOMALIES The anomaly associated with the disagreement between the field splits has been discussed in Section 7. The source of the disagreement for Co-60 was likely due to Co-60 being present in the form of discrete particles. Such a physical form does not lend itself to homogenous mixing in a sediment matrix.

13. CONCLUSION Survey Unit 9106-0008 has demonstrated compliance with the dose based, unrestricted release criterion. The sample data passed the Sign Test and the null hypothesis was rejected. The ALARA criteria for soils as specified in Chapter 4 of the LTP were achieved. Reclassification and remediation of this survey unit was not required.

Graphical representation of data indicates some positive skewness that is probably due to localized differences in particulate deposition rates, hydraulic velocity and sedimentation rates. The Retrospective Power Curve generated using COMPASS shows adequate power was achieved. The survey unit was properly designated as a Class 2 survey unit.

Revision 0 15

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD The dose contribution from sediment is 1.9 mrem/yr TEDE based on the average concentration of the samples used for non-parametric statistical sampling.

This survey unit is not affected by existing groundwater (reference CY memo ISC 06-024). It has been determined that the dose contribution from groundwater sources is bounded by zero (0) mrem/yr TEDE.

This survey unit is also not considered impacted by future groundwater radioactive contamination, as there are no concrete foundations or footings containing residual radioactive material within the groundwater saturated zone in the area (reference CY memo ISC 06-024). The dose contribution from future groundwater, the third dose component is, therefore, zero (0) mrem/yr TEDE.

The average total dose from residual radioactivity in this survey unit, including that from sediment, will not exceed 1.9 mrem/yr Total Effective Dose Equivalent (TEDE).

14. ATTACHMENTS 14.1 Attachment 1 - Figures 14.2 Attachment 2 - Sample and Statistical Data Revision 0 16 Revision 0 16

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Attachment 1 Figures (6 pages)

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DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Attachment 2 Sample and Statistical Data

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Attachment 2a Sample Data (178 Pages)

General Narrative

CASE NARRATIVE For CONNECTICUT YANKEE RE: Sediment PO# 002332 Work Order: 163741 SDG: MSR #06-0743 June 19, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:

2040 Savage Road Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina on May 26, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.

The laboratory received the following sample(s):

Sample ID Client Sample ID 163741001 9106-0008-OOIF 163741002 9106-0008-003F 163741003 9106-0008-004F 163741004 9106-0008-005F 163741005 9106-0008-006F 163741006 9106-0008-006FS 163741007 9106-0008-002F 163741008 9106-0008-007F GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP INC.

Page 2 of 75 P.O. Box 30712

• Charleston, SC 29417

• 2040 Savage Road (29407)

Phone (843) 556-8171 ° Fax (843) 766-1178

• www.gel.com

Sample ID Client Sample ID 163741009 9106-0008-008F 163741010 9106-0008-009F 163741011 9106-0008-OIOF 163741012 9106-0008-OIOFS 163741013 9106-0008-011F 163741014 9106-0008-013F 163741015 9106-0008-014F 163741016 9106-0008-012F Items of Note:

There are no items of note.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.

Analytical Request:

Fourteen sediment samples were analyzed for FSSGAM, Sr-90 and Ni-63.

Two sediment samples were analyzed for FSSALL.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

P.O. Box 30712 ° Charleston, SC 29417 - 2040 Savage Road (29407)

Page 3 of 75 Phone (843) 556-8171

• Fax (843) 766-1178

• www.gel.com

Chain of Custody and Supporting Documentation Page 4 of 75

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Healh Pysis Prcedre PP-GGR-5 104-03-Atacmen B-CY-0 1 ajo SChain of Custody FormN.206037 Connecticut Yankee Atomic Power CompanyCu, No. 2006-00367 362 Injun Hollow Road, East Hampton, CT 06424 860-267-255616374t

/ 3'q,/. _____

Name: Haddam Neck Decommissioning

_roject Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407  ? 0 e 843 556 8171. Attn. Cheryl Jones C .

Container Priority: 0 30 D. Ej 14 D. [] 7 D.

Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0008-OOIF 5/05/06 11:13 SE C BP X X X Transferred from COC # 2006-00324 9106-0008-003F 5/5/06 13:35 SE C BP x x x Transferred from COC # 2006-00325 9106-0008-004F 5/5/06 13:51 SE C BP X X X Transferred from COC # 2006-00325 9106-0008-005F 5/5/06 14:17 SE C BP X X X Transferred from COC # 2006-00325 9106-0008-006F 5/5/06 14:36 SE C BP X X x Transferred from COC # 2006-00325 9106-0008-006FS 5/5106 14:36 SE C BP x x x Transferred from COC # 2006-00325 9106-0008-007F 5/5/06 15:03 SE C BP x Transferred from COC # 2006-00325 9106-0008-002F 5/5/06 13:10 SE C BP x X X Transferred from COC # 2006-00325 NOTES: PO #: 002332 MSR#: 06-7O,3 SSWP#NA Z LTP QA E] Radwaste QA E] Non QA Samples Shipped Via: Internal Container

[ Fed Ex Temp.: - Deg. C El up~s El Hand Custody Sealed?

YEO NO

1) elinqdshe Date/Time 2) e ived ate/Time Custody Seal Intact?

El Other

3) ieinquished By \\J Date/Time 4) Re eive y hate/Time YOI NO Bill of Lading #

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major

~Chain of Custody Form Connecticut Yankee Atomic Power Company No. 2006-00366 362 Injun Hollow Road, East Hampton, CT 06424 o 860-267-2556 S0-oject Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & lPhone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories

• 2040 Savage Road. Charleston SC. 29407 0, 843 556 8171. Attn. Cheryl Jones r Uý Z Priority: Z 30 D. E] 14 D. E] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID

,.? 9106-0008-008F 5/08/06 08:01 SE C BP X x x Transferred from COC # 2006-00327

)10 9106-0008-009F 5/08/06 08:32 SE C BP X X X Transferred from COC # 2006-00327 Oil 9106-0008-01 OF 5/08/06 09:09 SE C BP X X X Transferred from COC # 2006-00327

)11 9106-0008-O1OFS 5/08/06 09:09 SE C BP X X X Transferred from COC # 2006-00327

)It 9106-0008-01IF 5/08/06 09:30 SE C BP X X X Transferred from COC # 2006-00327

,1k 9106-0008-012F 5/08/06 09:53 SE C BP X Transferred from COC # 2006-00327 9106-0008-013F 5/08/06 10:16 SE C BP X x x Transferred from COC #2006-00327 9106-0008-014F 5/08/06 10:47 SE C BP X X x Transferred from COC # 2006-00327 NOTES: PO #: 002332 MSR #: 06- 67 q.3 SSWP# NA Z LTP QA LI Radwaste QA El Non QA Samples Shipped Via: Internal Container

[ Fed Ex Temp.: '41 Deg. C

[] UPS El Hand Custody Sealed?

Y 0 N31

1) Relinquished By Date/Time 2) Received By Date/Time Custody Seal Intact?

C) 10444se By Dt/ e/2 4), Reeie " / a 0l Other

3) Relinquished By Date/Time 4) Received By Date/Time Y5' No Bill of Lading #

Connecticut Yankee 1 37'4I 1 Statement of Work for Analytical Lab Services -CY-ISC-SOW-001 Figure 1. Sample Check-in List Date/lime Received: A5~u1Oto DA? L SDG#: Ae5  % c43 Work Order Number: \( 4 \"

Shipping Container ID: V)0 '1' JOIiP& Chain of Custody # O 0 0OO3 C)o. wq>"

1. *Custody Seals.od shipping container intact? *Yes [V"o (I

2. Custody Seals dated and signed? Yes[ j No [.-

3. Chain-of-Custo.'Jy record present? Yes [-rf"*o I]

4. Cooler temperature / -"

5. Vermiculite/packing materials is: Wet [ I Dry [, ] P 6.' Number of samples in shipping container: t

7. Sample holding times exceeded? Yes [] No

8. Samples have-

-hazard labels

-- ,custody seals /'appropriate sample labels

9. Samples are-."

_2z*1in good condition . leaking

_broken -have air bubbles

10. Were any anomalies identified in sample receipt? Yes [ ] No [, '

11..Description of anomalies (include sample numbers):

Telephoned to:__ __ _ _ __ __ _On _____"__"_"__

By -

.Page7 of 75

0 SAMPLE RECEIPT & REVIEW FORM V on onl 1CClimt: IOASDGIARCOC/WO*I Order-Received: ca 0 , jM(ARev/ew (ensure non-conforming items we resolved prior to siping):

Received By: ____)_

Sample Receipt Criteria CommentslQualiflers (Required for Non-Conforming Items) 1 Shipping containers received intact / icle Awplicable: seals broken damaged comainer leaking container oter (descrb) and sealed?

Samples requiring cold Circle Coolant I ke bags blue ace dry ice jox odher describe) 2 preservation within (4 +1- 2 C)? /

Record preservation method. _.__C Chain of with 3included custody documents shipment?

Sample containers intact and Circle Applicable: seals broken damaged container leaking container ether (descrit) sealed? _ _ _ _ _ _ _ _ _ _

5 Samples requiring chemical / Samp ID's. conainers affected and observed pit preservation at proper pH?

VOA vials free of headspace / In's ciners affected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes. immediately deliver to VOA laboratory)

Samples received within holding 8 time? / Id's and tests affected:

Sample ID's on COC match ID's Sample ID's and comaines affected:

on bottles? /

Date & time on COC match date /sampl ID's afetd

& time on bottles? /_

Number of containers received / ampl ID'i affec*td match number indicated on COG?

COC form is properly signed in 2 relinquished/received sections?_

14 Air Bill ,Tracking #'s, &

Additional Comnents S 6l o?

t k1

• -- ', RSORADReceiptI# -

as 'non ,

.Haurd In o m to Suspected *If > x2 area background is obsered on samples identified Suspected Hazard Information Z) *

• uI regulated/non-radioactiveP, contact the Radiation Safetygroup for further

'_x 1 ,1 investigation.

IA7lRadiologicaI Classification? I ,/ ,..:... r . .. ... - . -,1 ... I P~~CB Regulated? -

• O.,mments: t~-~~

5hippd as DOT L'Hazardous lazard Class Shipped:

C Material? If yes, contact Waste Manager or E-SH Manager..- IN#:

rM (or YMA) view of Hazard classification: Initials (9 cr/6 Date:

ragv 0 U1 /.j

/

Connecticut Yankee Statement of Work for Analytical Lab Services -CY-ISC-SOW-00I Figure 1. Sample Check-in List Date/Time Received: S/!2.Ult *ý 602)

SDG# A _

Work Order Number:-

Shipping Container ID: "19tI Z **_ 1112 Chain of Custody# ' k"*

1. Custody Seals o6 shipping container intact?- Yes k[' o []

2. Custody Seals dated and signed? Yes L,9o []

3. Chaia-of-Custody record present? " es LI,,o [ I

4. Cooler temperature

5. Vermiculite/packing materials is: Wet J'*Dry ['l

6. Number of samples in shipping container:

• hI'h

7. Sample holding times exceeded? Yes-[ ] No

8. Samples have:

tape ___hazard labels

_custody seals _ appropriate sample labels

9. Samples are'

.. "in good condition leaking

-broken -

• have air bubbles

10. Were any anomalies identified in sample receipt? Yes [] No [-j*

11. Description of anomalies. (include sample numbers): .*O Sample Custodian/Laboratory: (oel,24-iC,,7 Date:_ _ _2-______,

Telephoned to: On By Page 9 of 75

ESAMPLE RECEIPT & REVIEW FORM 0"pI' RSAMPLEMus ol Client- Y an kp&SDGIARCOCtWork Order: ho3741 '/

Date Received: jPM(A) Review (ensure non-conforming items are resolved prior to signing):

Sample Receipt Criteria > Z CommentslQualifrers (Required for Non-Conforming Items)

Shipping containers received intact Circle Applicable: seals broken damaged container leaking container other (describe) and sealed? _/_ _I_ _ _ L%

Samples requiring cold Circle Coolant ice bags blue ice dry ice other describe) 2 preservation within (4 +/- 2 C)?

Record preservation method.

3 Chain of custody documents included with shipment?

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking container other (describe) sealed? ________________________________

requiring chemical Sample ID's. containers affected and observed pH:

5 Samples preservation at proper pH?

6 VOA vials free of headspace Sample ID's and containers affected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) 8 Samples received within holding Id's aJ tests affecied:

8 lime? _

9 Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles? "

Date & time on COC match date Sample ID's affected:

0 & time on bottles?

l Number of containers received Sample ID's affected:

match number indicated on COC?

2 COC form is properly signed in relinquished/received sections?

n o4- Kj.,'tiq.1/ I's.d 4 Air Bill ,Tracking #'s,&& L'" 4 p*q /13"5 Additional Comments "V RSO RADReceiptl#

r- *If > x2 area background is observed on samples identified as "non-Suspected Hazard Information V C ,regulated/non-radioactive". contact the Radiation Safety group for further

=- x , investigation.

A Radiological Classification? . Maximum Counts Observed*:

PCB3 Regulated? Comments:

Shipped as DMT Hazardous C Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. IUN#:

PM (or PMA) review of Hazard classification: Initials ) Date:

Page 10 01 75 I

RADIOLOGICAL ANALYSIS Page 11 of 75

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 163741 Method/Analysis Information Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 537411 Prep Batch Number: 534049 Dry Soil Prep GL-RAD-A-021 Batch Number: 534048 Sample ID Client ID 163741008 9106-0008-007F 163741016 9106-0008-012F 1201110207 Method Blank (MB) 1201110208 163741008(9106-0008-007F) Sample Duplicate (DUP) 1201110209 163741008(9106-0008-007F) Matrix Spike (MS) 1201110210 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Page 12 of 75

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163741008 (9106-0008-007F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 13 of 75

Product: Alphaspec Pu, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- 11-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 537412 Prep Batch Number: 534049 Dry Soil Prep GL-RAD-A-021 Batch Number: 534048 Sample ID Client ID 163741008 9106-0008-007F 163741016 9106-0008-012F 1201110215 Method Blank (MB) 1201110216 163741008(9106-0008-007F) Sample Duplicate (DUP) 1201110217 163741008(9106-0008-007F) Matrix Spike (MS) 1201110218 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163741008 (9106-0008-007F).

QC Information All of the QC samples met the required acceptance limits.

Page 14 of 75

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu- I1-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 537417 Prep Batch Number: 534049 Dry Soil Prep GL-RAD-A-021 Batch Number: 534048 Page 15 of 75

Sample ID Client ID 163741008 9106-0008-007F 163741016 9106-0008-012F 1201110229 Method Blank (MB) 1201110230 163741008(9106-0008-007F) Sample Duplicate (DUP) 1201110231 163741008(9106-0008-007F) Matrix Spike (MS) 1201110232 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QCQ Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163741008 (9106-0008-007F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from Page 16 of 75

referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Gamma,Solid-FSS GAM & ALL FSS Analytical Method: EML HASL 300,4.5.2.3 Prep Method: Dry Soil Prep Analytical Batch Number: 534130 Prep Batch Number: 534048 Sample ID Client ID 163741001 9106-0008-0OlF 163741002 9106-0008-003F 163741003 9106-0008-004F 163741004 9106-0008-005F 163741005 9106-0008-006F 163741006 9106-0008-006FS 163741007 9106-0008-002F 163741008 9106-0008-007F 163741009 9106-0008-008F 163741010 9106-0008-009F 163741011 9106-0008-01OF 163741012 9106-0008-01OFS 163741013 9106-0008-01 IF 163741014 9106-0008-013F 163741015 9106-0008-014F 163741016 9106-0008-012F 1201102649 Method Blank (MB) 1201102650 163741001(9106-0008-001 F) Sample Duplicate (DUP) 1201102651 Laboratory Control Sample (LCS)

Page 17 of 75

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-013 REV# 11.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QCQ Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163741001 (9106-0008-001F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments The relative percent difference for Pb-214, in samples 1201102650 (9106-0008-001F) and 163741001 (9106-0008-001F), does not meet the standard requirements. However, when a relative error ratio is calculated, precision is shown at 2.38.

Page 18 of 75

Qualifier information Qualifier Reason Analyte Sample Data rejected due to high Full-Width UI Potassium-40 1201102649 Half-Maximum.

U' Data rejected due to interference. Europium- 155 163741016 Manganese-54 163741004 UI Data rejected due to low abundance. Cesium- 134 163741005 163741007 163741013 163741014 163741016 1201102650 Cobalt-60 163741003 Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 536483 Prep Batch Number: 534049 Dry Soil Prep GL-RAD-A-021 Batch Number: 534048 Page 19 of 75

Sample ID Client ID 163741001 9106-0008-OOIF 163741002 9106-0008-003F 163741003 9106-0008-004F 163741004 9106-0008-005F 163741005 9106-0008-006F 163741006 9106-0008-006FS 163741007 9106-0008-002F 163741008 9106-0008-007F 163741009 9106-0008-008F 163741010 9106-0008-009F 163741011 9106-0008-01OF 163741012 9106-0008-01OFS 163741013 9106-0008-01 IF 163741014 9106-0008-013F 163741015 9106-0008-014F 163741016 9106-0008-012F 1201108056 Method Blank (MB) 1201108057 163741001(9106-0008-001F) Sample Duplicate (DUP) 1201108058 163741001(9106-0008-001 F) Matrix Spike (MS) 1201108059 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 10.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Ouality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163741001 (9106-0008-001F).

QC Information All of the QC samples met the required acceptance limits.

Page 20 of 75

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Samples 163741001 (9106-0008-001F), 163741005 (9106-0008-006F) and 163741011 (9106-0008-01OF) were recounted due to high MDAs.

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from.

referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Tc99, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 536314 Sample ID Client ID 163741008 9106-0008-007F 163741016 9106-0008-012F 1201107610 Method Blank (MB) 1201107611 163741008(9106-0008-007F) Sample Duplicate (DUP) 1201107612 163741008(9106-0008-007F) Matrix Spike (MS) 1201107613 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Page 21 of 75

Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 13.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163741008 (9106-0008-007F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 22 of 75

Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 538969 Prep Batch Number: 534049 Dry Soil Prep GL-RAD-A-021 Batch Number: 534048 Sample ID Client ID 163741008 9106-0008-007F 163741016 9106-0008-012F 1201113887 Method Blank (MB) 1201113888 163741008(9106-0008-007F) Sample Duplicate (DUP) 1201113889 163741008(9106-0008-007F) Matrix Spike (MS) 1201113890 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163741008 (9106-0008-007F).

QC Information Page 23 of 75

All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 538365 Prep Batch Number: 534049 Dry Soil Prep GL-RAD-A-021 Batch Number: 534048 Page 24 of 75

Sample ID Client ID 163741001 9106-0008-001F 163741002 9106-0008-003F 163741003 9106-0008-004F 163741004 9106-0008-005F 163741005 9106-0008-006F 163741006 9106-0008-006FS 163741007 9106-0008-002F 163741008 9106-0008-007F 163741009 9106-0008-008F 163741010 9106-0008-009F 163741011 9106-0008-01OF 163741012 9106-0008-01OFS 163741013 9106-0008-01 IF 163741014 9106-0008-013F 163741015 9106-0008-014F 163741016 9106-0008-012F 1201112555 Method Blank (MB) 1201112556 163741003(9106-0008-004F) Sample Duplicate (DUP) 1201112557 163741003(9106-0008-004F) Matrix Spike (MS) 1201112558 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163741003 (9106-0008-004F).

QC Information All of the QC samples met the required acceptance limits.

Page 25 of 75

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: LSC, Tritium Dist, Solid-HTD2,ALL FSS Analytical Method: EPA 906.0 Modified Analytical Batch Number: 535984 Sample ID Client ID 163741008 9106-0008-007F 163741016 9106-0008-012F 1201106885 Method Blank (MB) 1201106886 163626016(9106-0007-001 F) Sample Duplicate (DUP) 1201106887 163626016(9106-0007-00 IF) Matrix Spike (MS) 1201106888 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 12.

Page 26 of 75

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 163626016 (9106-0007-001F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 27 of 75

Product: Liquid Scint C14, Solid AII,FSS Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 534837 Sample ID Client ID 163741008 9106-0008-007F 163741016 9106-0008-012F 1201104384 Method Blank (MB) 1201104385 162335019(9106-0003-014F) Sample Duplicate (DUP) 1201104386 162335019(9106-0003-014F) Matrix Spike (MS) 1201104387 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 162335019 (9106-0003-014F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for.this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Page 28 of 75

Sample Re-prep/Re-analysis Samples 1201104385 (9106-0003-014F) and 163741016 (9106-0008-012F) were recounted due to high MDAs. Samples were reprepped due to low/high recovery.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

The following data validator verified the information presented in this case narrative:

Reviewer/Date: K4 -9 v-'*t Page 29 of 75

SAMPLE DATA

SUMMARY

Page 30 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOOI Connecticut Yankee Atomic Power Co.

Client SDG: MSR#06-0743 GEL Work Order: 163741 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification ND The analyte concentration is not detected above the reporting limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by Page 31 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-001F Proiect: YANK01204 Sample ID: 163741001 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 38.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM& ALL FSS Actinium-228 0.817 +/-0.177 0.0585 +/-0.177 0.128 pCi/g MJHI 06/15/06 1544 534130 1 Americium-241 U 0.0431 +/-0.0977 0.0813 +/-0.0977 0.168 pCi/g Bismuth-212 0.570 +/-0.292 0.144 +/-0.292 0.309 pCi/g Bismuth-214 0.568 +/-0.0877 0.0366 +/-0.0877 0.0777 pCi/g Cesium-134 U 0.0314 +/-0.0354 0.0253 +/-0.0354 0.0538 pCi/g Cesium-137 0.396 +/-0.0588 0.0193 +/-0.0588 0.0412 pCi/g Cobalt-60 0.133 +/-0.0554 0.0195 +/-0.0554 0.0431 pCi/g Europium-152 U 0.00717 +/-0.0581 0.0513 +/-0.0581 0.108 pCi/g Europium-154 U 0.040 +/-0.0643 0.0578 +/-0.0643 0.127 pCi/g Europium-155 U 0.0854 +/-0.0769 0.0548 +/-0.0769 0.113 pCi/g Lead-212 0.772 +/-0.0707 0.0295 +/-0.0707 0.0615 pCi/g Lead-214 0.585 +/-0.0841 0.0353 +/-0.0841 0.0742 pCi/g Manganese-54 U 0.0123 +/-0.0261 0.0208 +/-0.0261 0.0446 pCi/g Niobium-94 U-0 .000522 +/-0.0212 0.0176 +/-0.0212 0.0375 pCi/g Potassium-40 12.1 +/-0.950 0.178 +/-0.950 0.396 pCi/g Radium-226 0.568 +/-0.0877 0.0366 +/-0.0877 0.0777 pCi/g Silver-108m U 0.00495 +/-0.0195 0.0171 +/-0.0195 0.0361 pCi/g Thallium-208 0.300 +/-0.0497 0.0177 +/-0.0497 0.0379 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.00579 +/-0.0116 0.0116 +/-0.0116 0.0264 pCi/g BXFI 06/22/06 1035 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 0.233 +/-7.56 6.34 +/-7.56 12.9 pCi/g SLNI 06/20/06 0726 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM2 05/28/06 1209 534049 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM1 05/26/06 1530 534048 The following Analytical Methods were performed Method Description Page 32 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-00IF Project: YANK01204 Sample ID: 163741001 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 72 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 33 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificnte of Analvqiq Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-003F Project: YANK01204 Sample ID: 163741002 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 57.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.09 +/-0.203 0.0952 +/-0.203 0.201 pCi/g MJH1 06/15/06 1544 534130 1 Americium-241 U 0.0256 +/-0.140 0.082 +/-0.140 0.169 pCi/g Bismuth-212 0.673 +/-0.467 0.181 +/-0.467 0.382 pCi/g Bismuth-214 0.775 +/-0.123 0.0437 +/-0.123 0.0917 pCi/g Cesium-134 U 0.0459 +/-0.0366 0.0321 +/-0.0366 0.0672 pCi/g Cesium-137 0.205 +/-0.0706 0.0227 +/-0.0706 0.0479 pCi/g Cobalt-60 0.324 +/-0.0774 0.0292 +/-0.0774 0.0625 pCi/g Europium-152 U 0.020 +/-0.073 0.0599 +/-0.073 0.124 pCi/g Europium-154 U 0.00145 +/-0.104 0.0855 +/-0.104 0.182 pCi/g Europium-155 U 0.0192 +/-0.074 0.0571 +/-0.074 0.117 pCi/g Lead-212 1.16 +/-0.083 0.033 +/-0.083 0.0682 pCi/g Lead-214 0.886 +/-0.110 0.0409 +/-0.110 0.0851 pCi/g Manganese-54 U 0.0289 +/-0.0456 0.0244 +/-0.0456 0.0516 pCi/g Niobium-94 U -0.0236 +/-0.0269 0.0208 +/-0.0269 0.0439 pCi/g Potassium-40 16.2 +/-1.14 0.223 +/-1.14 0.487 pCi/g Radium-226 0.775 +/-0.123 0.0437 +/-0.123 0.0917 pCi/g Silver-108m U 0.00754 +/-0.0258 0.0209 +/-0.0258 0.0437 pCi/g Thallium-208 0.337 +/-0.0676 0.0222 +/-0.0676 0.0468 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 L 0.0112 +/-0.0174 0.0173 +/-0.0174 0.0387 pCi/g BXFI 06/18/06 1006 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 L. -2.74 +/-5.74 4.87 +/-5.74 9.92 pCi/g SLN1 06/20/06 0813 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM2 05/28/06 1209 534049 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM1 05/26/06 1530 534048 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 Page 34 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-003F Project: YANK01204 Sample ID: 163741002 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 2 EPA 905.0 Modified 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 71 (25%- 125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 83 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 35 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-004F Proiect: YANKO 1204 Sample ID: 163741003 Client ID: YANKOO I Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 63.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.02 +/-0.200 0.0517 +/-0.200 0.109 pCi/g MJH1 06/15/06 1544 534130 1 Americium-241 U 0.0417 +/-0.0743 0.0608 +/-0.0743 0.125 pCi/g Bismuth-212 0.935 +/-0.288 0.128 +/-0.288 0.269 pCi/g Bismuth-214 0.581 +/-0.112 0.0343 +/-0.112 0.0712 pCi/g Cesium-134 U 0.0381 +/-0.0469 0.0215 +/-0.0469 0.0448 pCi/g Cesium-137 0.0432 +/-0.036 0.016 +/-0.036 0.0334 pCi/g Cobalt-60 UI 0.00 +/-0.0268 0.0258 +/-0.0268 0.0538 pCi/g Europium-152 U -0.00954 +/-0.0498 0.0406 +/-0.0498 0.0841 pCi/g Europium-154 U -0.0501 +/-0.0608 0.0457 +/-0.0608 0.0975 pCi/g Europium-155 U 0.0526 +/-0.0739 0.0508 +/-0.0739 0.104 pCi/g Lead-212 0.937 +/-0.0965 0.0253 +/-0.0965 0.052 pCi/g Lead-214 0.739 +/-0.119 0.0286 +/-0.119 0.0594 pCi/g Manganese-54 U -0.0116 +/-0.0212 0.017 +/-0.0212 0.0357 pCi/g Niobium-94 U 0.00493 +/-0.018 0.0153 +/-0.018 0.0319 pCi/g Potassium-40 13.6 +/-1.14 0.136 +/-1.14 0.295 pCi/g Radium-226 0.581 +/-0.112 0.0343 +/-0.112 0.0712 pCi/g Silver-108m U -0.0039 +/-0.0169 0.0136 +/-0.0169 0.0283 pCi/g Thallium-208 0.234 +/-0.0565 0.0157 +/-0.0565 0.0328 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00619 +/-0.0127 0.0157 +/-0.0127 0.0354 pCi/g BXFI 06/18/06 1006 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -1.8 +/-4.81 4.07 +/-4.81 8.29 pCi/g SLN1 06/20/06 0901 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM2 05/28/06 1209 534049 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/26/06 1530 534048 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 Page 36 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-004F Project: YANKO 1204 Sample ID: 163741003 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 2 EPA 905.0 Modified 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 74 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 78 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 37 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-005F Proiect: YANK01204 Sample ID: 163741004 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 57.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.859 +/-0.224 0.0761 +/-0.224 0.170 pCi/g MJH1 06/15/06 1650 534130 1 Americium-241 U-( 0.000334 +/-0.0393 0.0331 +/-0.0393 0.0687 pCi/g Bismuth-212 0.612 +/-0.380 0.239 +/-0.380 0.512 pCi/g Bismuth-214 0.792 +/-0.157 0.0434 +/-0.157 0.0941 pCi/g Cesium-134 U 0.0388 +/-0.0682 0.0328 +/-0.0682 0.0708 pCi/g Cesium-137 0.266 +/-0.0822 0.0282 +/-0.0822 0.0607 pCi/g Cobalt-60 U 0.0275 +/-0.0345 0.0314 +/-0.0345 0.0696 pCi/g Europium-152 U -0.0306 +/-0.0864 0.0714 +/-0.0864 0.150 pCi/g Europium-154 U 0.0128 +/-0.0977 0.0818 +/-0.0977 0.182 pCi/g Europium-155 U 0.0403 +/-0.0709 0.0602 +/-0.0709 0.125 pCi/g Lead-212 0.757 +/-0.122 0.0365 +/-0.122 0.0764 pCi/g Lead-214 0.677 +/-0.132 0.0501 +/-0.132 0.106 pCi/g Manganese-54 UI 0.00 +/-0.0953 0.0265 +/-0.0953 0.0579 pCi/g Niobium-94 U -0.0242 +/-0.030 0.0222 +/-0.030 0.0482 pCi/g Potassium-40 12.4 +/-1.44 0.265 +/-1.44 0.598 pCi/g Radium-226 0.792 +/-0.157 0.0434 +/-0.157 0.0941 pCi/g Silver-108m U -0.0184 +/-0.0271 0.0214 +/-0.0271 0.0458 pCi/g Thallium-208 0.262 +/-0.0789 0.0219 +/-0.0789 0.0478 pCi/g Rad Gas Flow Proportional Counting GFPC,S90, solid-ALL FSS Strontium-90 U C1.000828 +/-0.0152 0.0169 +/-0.0152 0.0376 pCi/g BXFI 06/18/06 1006 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -0.858 +/-4.37 3.69 +/-4.37 7.51 pCi/g SLNI 06/20/06 0948 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM2 05/28/06 1209 534049 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/26/06 1530 534048 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 Page 38 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-005F Project: YANK01204 Sample ID: 163741004 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 2 EPA 905.0 Modified 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 78 (25%-125%o)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 80 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 39 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analyvis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006F Proiect: YANKO 1204 Sample ID: 163741005 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 30.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.813 +/-0.227 0.0748 +/-0.227 0.160 pCi/g MJH1 06/15/06 1838 534130 1 Americium-241 U 0.0977 +/-0.116 0.0927 +/-0.116 0.191 pCi/g Bismuth-212 0.817 +/-0.336 0.146 +/-0.336 0.311 pCi/g Bismuth-214 0.624 +/-0.109 0.0355 +/-0.109 0.0751 pCi/g Cesium-134 Ut 0.00 +/-0.0387 0.0266 +/-0.0387 0.0562 pCi/g Cesium-137 0.492 +/-0.0725 0.0214 +/-0.0725 0.0452 pCi/g Cobalt-60 0.779 +/-0.098 0.0183 +/-0.098 0.0405 pCi/g Europium-152 U -0.0151 +/-0.0601 0.0488 +/-0.0601 0.102 pCi/g Europium-154 U 0.000763 +/-0.0759 0.0637 +/-0.0759 0.138 pCi/g Europium-155 U 0.0672 +/-0.0612 0.0565 +/-0.0612 0.116 pCi/g Lead-212 0.873 +/-0.0951 0.030 +/-0.0951 0.0622 pCi/g Lead-214 0.720 +/-0.120 0.0351 +/-0.120 0.0735 pCi/g Manganese-54 U 0.0138 +/-0.0283 0.0242 +/-0.0283 0.0511 pCi/g Niobium-94 U -0.00895 +/-0.0211 0.0171 +/-0.0211 0.0363 pCi/g Potassium-40 13.7 +/-1.37 0.145 +/-1.37 0.330 pCi/g Radium-226 0.624 +/-0.109 0.0355 +/-0.109 0.0751 pCi/g Silver-108m U 0.00177 +/-0.0192 0.0168 +/-0.0192 0.0354 pCi/g Thallium-208 0.298 +/-0.0652 0.0195 +/-0.0652 0.0413 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90

• 0.00559 +/-0.013 0.0132 +/-0.013 0.0302 pCi/g BXFI 06/22/06 1035 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 2.28 +/-10.1 8.45 +/-10.1 17.2 pCi/g SLNI 06/20/06 1035 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM2 05/28/06 1209 534049 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/26/06 1530 534048 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 Page 40 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006F Project: YANK01204 Sample ID: 163741005 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 2 EPA 905.0 Modified 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 59 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 54 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 41 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006FS Project: YANK01204 Sample ID: 163741006 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 40.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSS GAM & ALL FSS Actinium-228 1.01 +/-0.284 0.111 +/-0.284 0.236 pCi/g MJHI 06/15/06 1953 534130 1 Americium-241 U 0.0585 +/-0.0523 0.0334 +/-0.0523 0.0689 pCi/g Bismuth-212 0.587 +/-0.428 0.199 +/-0.428 0.427 pCi/g Bismuth-214 0.694 +/-0.162 0.0485 +/-0.162 0.103 pCi/g Cesium-134 U 0.0331 +/-0.0414 0.0374 +/-0.0414 0.0791 pCi/g Cesium-137 0.601 +/-0.100 0.0292 +/-0.100 0.0619 pCi/g Cobalt-60 1.34 +/-0.140 0.024 +/-0.140 0.0539 pCi/g Europium-152 U 0.00817 +/-0.0797 0.0688 +/-0.0797 0.144 pCi/g Europium-154 U -0.0337 +/-0.0957 0.0757 +/-0.0957 0.167 pCi/g Europium-155 U 0.106 +/-0.115 0.0619 +/-0.115 0.128 pCi/g Lead-212 0.866 +/-0.135 0.0461 +/-0.135 0.0951 pCi/g Lead-214 0.763 +/-0.147 0.0479 +/-0.147 0.101 pCi/g Manganese-54 U 0.0198 +/-0.0388 0.0343 +/-0.0388 0.0728 pCi/g Niobium-94 U -0.0228 +/-0.0306 0.0233 +/-0.0306 0.0499 pCi/g Potassium-40 14.9 +/-1.49 0.237 +/- 1.49 0.532 pCi/g Radium-226 0.694 +/-0.162 0.0485 +/-0.162 0.103 pCi/g Silver- 108m U-0.000651 +/-0.0283 0.0239 +/-0.0283 0.0504 pCi/g Thallium-208 0.360 +/-0.073 0.0275 +/-0.073 0.0585 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 t . 0.000875 +/-0.0141 0.0156 +/-0.0141 0.0355 pCi/g BXF1 06/18/06 1007 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 t 0.188 +/-6.10 5.12 +/-6.10 10.4 pCi/g SLNI 06/20/06 1122 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM2 05/28/06 1209 534049 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/26/06 1530 534048 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 Page 42 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006FS Project: YANKO 1204 Sample ID: 163741006 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 2 EPA 905.0 Modified 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 71 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 84 (25%-125o)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below.the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 43 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-002F Project: YANKO 1204 Sample ID: 163741007 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 40.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.20 +1-0.150 0.0467 +1-0.150 0.0976 pCi/g MJHI 06/15/06 1953 534130 1 Americium-241 U -0.0887 +/-0.0966 0.0733 +/-0.0966 0.150 pCi/g Bismuth-212 0.731 +/-0.231 0.102 +/-0.231 0.213 pCi/g Bismuth-214 0.791 +/-0.0864 0.0249 +/-0.0864 0.0516 pCi/g Cesium-134 UI 0.00 +/-0.022 0.0171 +/-0.022 0.0355 pCi/g Cesium-137 U -0.00891 +/-0.0193 0.0132 +/-0.0193 0.0275 pCi/g Cobalt-60 U 0.00777 +/-0.0188 0.0156 +/-0.0188 0.0329 pCi/g Europium-152 U -0.00544 +/-0.0415 0.035 +/-0.0415 0.0722 pCi/g Europium-154 U 0.0213 +/-0.0532 0.0443 +/-0.0532 0.0929 pCi/g Europium-155 U 0.0635 +/-0.0805 0.0424 +/-0.0805 0.0869 pCi/g Lead-212 1.24 +/-0.0603 0.0209 +/-0.0603 0.0429 pCi/g Lead-214 0.965 +/-0.081 0.0252 +/-0.081 0.0519 pCi/g Manganese-54 U 0.0116 +/-0.0185 0.016 +/-0.0185 0.0331 pCi/g Niobium-94 U 0.000167 +/-0.016 0.0129 +/-0.016 0.0268 pCi/g Potassium-40 18.2 +/-0.772 0.121 +/-0.772 0.257 pCi/g Radium-226 0.791 +/-0.0864 0.0249 +/-0.0864 0.0516 pCi/g Silver-108m U -0.00521 +/-0.0142 0.0117 +/-0.0142 0.0242 pCi/g Thallium-208 0.332 +/-0.0409 0.0136 +/-0.0409 0.0281 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 1J 0.0203 +/-0.0201 0.0182 +/-0.0201 0.0413 pCi/g BXF1 06/18/06 1007 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 L -4.84 +/-5.47 4.68 +/-5.47 9.53 pCi/g SLNI 06/20/06 1209 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM2 05/28/06 1209 534049 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/26/06 1530 534048 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 Page 44 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-002F Project: YANK01204 Sample ID: 163741007 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 2 EPA 905.0 Modified 3 DOE RESL Ni-1, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 65 (25%/-,125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 84 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 45 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-007F Proiect: YANK01204 Sample ID: 163741008 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 36.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0. +/-0.0968 0.062 +/-0.097 0.209 pCi/g JXG1 06/16/06 1312 537411 1 Curium-242 U +/-0.0738 0.00 +/-0.0738 0.102 pCi/g Curium-243/244 U 0.0 +/-0.0669 0.0622 +/-0.0669 0.210 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.00 +/-0.110 0.00 +/-0.110 0.151 pCi/g JXGI 06/16/06 0928 537412 2 Plutonium-239/240 U -( ).226 +/-0.163 0.292 +/-0.165 0.734 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 4.08 +/-6.18 5.06 +/-6.19 10.4 pCi/g JXGI 06/20/06 1900 537417 3 Rad Gamma Spec Analysis Gamma,Solid-FSSGAM & ALL FSS Actinium-228 +/-0.175 0.0766 +/-0.175 0.165 pCi/g MJH1 06/15/06 2141 534130 4 Americium-241 U I +/-0.113 0.0936 +/-0.113 0.194 pCi/g Bismuth-212 +/-0.278 0.166 +/-0.278 0.355 pCi/g Bismuth-214 +/-0.095 0.0335 +/-0.095 0.0718 pCi/g Cesium-134 U 0. +/-0.0399 0.0228 +/-0.0399 0.049 pCi/g Cesium-137 U 0. +/-0.0249 0.0227 +/-0.0249 0.0481 pCi/g Cobalt-60 U 0. +/-0.0279 0.0241 +/-0.0279 0.0529 pCi/g Europium-152 U 0. +/-0.0559 0.0502 +/-0.0559 0.106 pCi/g Europium-154 U 0. +/-0.066 0.0605 +/-0.066 0.133 pCi/g Europium-155 U 0. +/-0.107 0.0529 +/-0.107 0.110 pCi/g Lead-212 +/-0.0898 0.0301 +/-0.0898 0.0627 pCi/g Lead-214 +/-0.106 0.035 +/-0.106 0.074 pCi/g Manganese-54 U 0. +/-0.0291 0.0202 +/-0.0291 0.0437 pCi/g Niobium-94 U -0.0 +/-0.0196 0.0158 +/-0.0196 0.0342 pCi/g Potassium-40 +/-1.34 0.166 +/-1.34 0.378 pCi/g Radium-226 ( +/-0.095 0.0335 +/-0.095 0.0718 pCi/g Silver-108m U 0.0 +/-0.0168 0.0149 +/-0.0168 0.032 pCi/g Thallium-208 ( +/-0.0465 0.0196 +/-0.0465 0.0418 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U-0.00 0881 +/-0.0151 0.0171 +/-0.0151 0.038 pCi/g BXFI 06/18/06 1007 536483 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 4.94 +/-6.95 5.56 +/-6.95 11.7 pCi/g NXPI 06/17/06 1609 535984 6 Liquid Scint C14, Solid AllFSS Page 46 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-007F Project: YANK01204 Sample ID: 163741008 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Liquid Scintillation Analysis LiquidScint C14, SolidAllFSS Carbon-14 U -0.015 +/-0.126 0.106 +/-0.126 0.216 pCi/g ATH2 06/04/06 0432 534837 7 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 21.1 +/-18.3 13.0 +/-18.5 27.4 pCi/g SLNI 06/21/06 0813 538969 8 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -2.33 +/-5.91 5.00 +/-5.91 10.2 pCi/g SLNI 06/20/06 1256 538365 9 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.196 +/-0.227 0.184 +/-0.227 0.380 pCi/g SXEI 06/14/06 1714 536314 10 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Ash Soil Prep Ash Soil Prep, GL-RAD-A-021B LXM2 05/28/06 1209 534049 Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM1 05/26/06 1530 534048 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu- 11-RC Modified 4 EML HASL 300, 4.5.2.3 5 EPA 905.0 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 DOE RESL Fe-I, Modified 9 DOE RESL Ni-l, Modified 10 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 83 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 47 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL F5 94 (25%-I125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 79 (25%-I125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 83 (15o/6-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 80 (25%-125%)

Page 47 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-007F Project: YANK01204 Sample ID: 163741008 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 84 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 48 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-008F Project: YANKO 1204 Sample ID: 163741009 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 38.6%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.974 +/-0.257 0.075 +/-0.257 0.161 pCi/g MJH1 06/15/06 2153 534130 1 Americium-241 U 0.0456 +/-0.101 0.0814 +/-0.101 0.169 pCi/g Bismuth-212 0.779 +/-0.439 0.173 +/-0.439 0.368 pCi/g Bismuth-214 0.569 +/-0.134 0.0421 +/-0.134 0.0889 pCi/g Cesium-134 U 0.0547 +/-0.0378 0.0286 +/-0.0378 0.0605 pCi/g Cesium-137 0.472 +/-0.0788 0.023 +/-0.0788 0.0488 pCi/g Cobalt-60 0.917 +/-0.101 0.0202 +/-0.101 0.0446 pCi/g Europium-152 U -0.0108 +/-0.0749 0.056 +/-0.0749 0.118 pCi/g Europium-154 U 0.0271 +/-0.0787 0.0671 +/-0.0787 0.145 pCi/g Europium-155 U 0.00728 +/-0.0765 0.0657 +/-0.0765 0.136 pCi/g Lead-212 0.929 +/-0.106 0.0331 +/-0.106 0.069 pCi/g Lead-214 0.729 +/-0.114 0.0402 +/-0.114 0.0845 pCi/g Manganese-54 U 0.030 +/-0.0293 0.0266 +/-0.0293 0.0564 pCi/g Niobium-94 U 0.026 +/-0.0265 0.0202 +/-0.0265 0.0428 pCi/g Potassium-40 14.5 +1-1.35 0.191 +/-1.35 0.422 pCi/g Radium-226 0.569 +/-0.134 0.0421 +/-0.134 0.0889 pCi/g Silver-108m U 0.00585 +/-0.0218 0.0188 +/-0.0218 0.0398 pCi/g Thallium-208 0.274 +/-0.0702 0.0206 +/-0.0702 0.0439 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U -0.00269 +/-0.0189 0.0216 +/-0.0189 0.0476 pCi/g BXFI 06/18/06 1007 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -0.412 +/-8.90 7.48 +/-8.90 15.2 pCi/g SLNI 06/20/06 1343 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/28/06 1412 534097 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Page 49 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-008F Project: YANKO 1204 Sample ID: 163741009 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 74 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 57 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

U1 Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

• QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 50 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-009F Project: YANKO 1204 Sample ID: 163741010 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 36.8%

Parameter ( :ualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.741 +/-0.207 0.0619 +/-0.207 0.134 pCi/g MJH1 06/16/06 0622 534130 1 Americium-241 U -0.0785 +/-0.124 0.0788 +/-0.124 0.163 pCi/g Bismuth-212 0.596 +/-0.368 0.134 +/-0.368 0.287 pCi/g Bismuth-214 0.667 +/-0.109 0.0311 +/-0.109 0.0663 pCi/g Cesium-134 U 0.0506 +/-0.0431 0.0244 +/-0.0431 0.0516 pCi/g Cesium-137 U 0.0155 +/-0.0231 0.0183 +/-0.0231 0.039 pCi/g Cobalt-60 U -0.0108 +/-0.0254 0.0202 +/-0.0254 0.0443 pCi/g Europium-152 U -0.0723 +/-0.0543 0.0406 +/-0.0543 0.0856 pCi/g Europium-154 U -0.051 +/-0.0695 0.0535 +/-0.0695 0.117 pCi/g Europium-155 U 0.0418 +/-0.0558 0.0512 +/-0.0558 0.106 pCi/g Lead-212 0.813 +/-0.0899 0.0284 +/-0.0899 0.0589 pCi/g Lead-214 0.782 +/-0.120 0.0326 +/-0.120 0.0685 pCi/g Manganese-54 U -0.0123 +/-0.0257 0.0204 +/-0.0257 0.0435 pCi/g Niobium-94 U 0.014 +/-0.0192 0.017 +/-0.0192 0.0361 pCi/g Potassium-40 14.8 +/-1.41 0.147 +/-1.41 0.333 pCi/g Radium-226 0.667 +/-0.109 0.0311 +/-0.109 0.0663 pCi/g Silver-108m U -0.0119 +/-0.0163 0.0135 +/-0.0163 0.0287 pCi/g Thallium-208 0.306 +/-0.0596 0.0159 +/-0.0596 0.0339 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U -0.0059 +/-0.0171 0.0202 +/-0.0171 0.0443 pCi/g BXF1 06/18/06 1101 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -2.05 +/-10.4 8.80 +/-10.4 17.9 pCi/g SLN1 06/20/06 1430 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/28/06 1412 534097 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Page 51 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-009F Proiect: YANKO 1204 Sample ID: 163741010 Client ID: YANKOOl Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 75 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 52 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 52 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-010F Project: YANKO1204 Sample ID: 163741011 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 42.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid FSS GAM & ALL FSS Actinium-228 0.840 +/-0.226 0.0786 +/-0.226 0.168 pCi/g MJHI 06/16/06 0622 534130 1 Americium-241 U 0.0195 +/-0.0317 0.0282 +/-0.0317 0.0579 pCi/g Bismuth-212 0.758 +/-0.371 0.162 +/-0.371 0.345 pCi/g Bismuth-214 0.662 +/-0.138 0.0422 +/-0.138 0.0889 pCi/g Cesium-134 U 0.047 +/-0.0343 0.0272 +/-0.0343 0.0577 pCi/g Cesium-137 0.336 +/-0.0689 0.0223 +/-0.0689 0.0472 pCi/g Cobalt-60 0.246 +1-0.0501 0.0226 +1-0.0501 0.0494 pCi/g Europium-152 U -0.0238 +/-0.0624 0.0526 +/-0.0624 0.110 pCi/g Europium-154 U - -0.00597 +/-0.0975 0.0691 +/-0.0975 0.150 pCi/g Europium-155 U 0.0474 +/-0.0837 0.0461 +/-0.0837 0.0952 pCi/g Lead-212 0.887 +/-0.124 0.0287 +/-0.124 0.0596 pCi/g Lead-214 0.705 +/-0.116 0.0397 +/-0.116 0.0828 pCi/g Manganese-54 U 0.00134 +/-0.0286 0.0245 +/-0.0286 0.0521 pCi/g Niobium-94 U - 0.00916 +/-0.026 0.0207 +/-0.026 0.0439 pCi/g Potassium-40 12.5 +/-1.26 0.187 +/-1.26 0.415 pCi/g Radium-226 0.662 +/-0.138 0.0422 +/-0.138 0.0889 pCi/g Silver-108m U 0.0162 +/-0.0222 0.0196 +/-0.0222 0.0411 pCi/g Thallium-208 0.316 +/-0.0704 0.0195 +/-0.0704 0.0415 pCi/g Rad Gas Flow Proportional Counting GFPC,S90, solid-ALL FSS Strontium-90 U 0.00347 +/-0.0121 0.0128 +/-0.0121 0.0288 pCi/g BXF1 06/22/06 1046 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 0.123 +/-5.98 5.02 +/-5.98 10.2 pCi/g SLN1 06/20/06 1517 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/28/06 1412 534097 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 Page 53 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-OIOF Project: YANKO 1204 Sample ID: 163741011 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 2 EPA 905.0 Modified 3 DOE RESL Ni-1, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 69 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 84 (25%-/125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 54 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-010FS Project: YANK01204 Sample ID: 163741012 Client ID: YANKOO1 Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 41.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis GammaSolid-FSSGAM & ALL FSS Actinium-228 0.834 +/-0.216 0.0744 +/-0.216 0.157 pCi/g MJH1 06/15/06 2338 534130 1 Americium-241 U 0.0216 +/-0.0277 0.0248 +/-0.0277 0.0509 pCi/g Bismuth-212 0.657 +/-0.246 0.145 +/-0.246 0.306 pCi/g Bismuth-214 0.640 +/-0.127 0.0335 +/-0.127 0.0706 pCi/g Cesium-134 U 0.0478 +/-0.0354 0.0239 +/-0.0354 0.0503 pCi/g Cesium-137 0.302 +/-0.0573 0.0214 +/-0.0573 0.0448 pCi/g Cobalt-60 0.328 +/-0.0592 0.0204 +/-0.0592 0.044 pCi/g Europium-152 U 0.0241 +/-0.0519 0.0457 +/-0.0519 0.0952 pCi/g Europium-154 U -0.0192 +/-0.0711 0.0575 +/-0.0711 0.124 pCi/g Europium-155 U 0.0699 +/-0.049 0.0436 +/-0.049 0.0894 pCi/g Lead-212 0.826 +/-0.112 0.0257 +/-0.112 0.053 pCi/g Lead-214 0.705 +/-0.106 0.0338 +/-0.106 0.0704 pCi/g Manganese-54 U 0.014 +/-0.0231 0.0185 +/-0.0231 0.0394 pCi/g Niobium-94 U -0.00643 +/-0.0227 0.0183 +/-0.0227 0.0385 pCi/g Potassium-40 12.7 +/-1.18 0.161 +/-1.18 0.355 pCi/g Radium-226 0.640 +/-0.127 0.0335 +/-0.127 0.0706 pCi/g Silver-108m U-0.000137 +/-0.0191 0.0163 +/-0.0191 0.034 pCi/g Thallium-208 0.257 +/-0.0533 0.0193 +/-0.0533 0.0406 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.00859 +/-0.017 0.0174 +/-0.017 0.0387 pCi/g BXF1 06/18/06 1101 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 L, -1.63 +/-6.69 5.65 +/-6.69 11.5 pCi/g SLNI 06/20/06 1604 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/28/06 1412 534097 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Page 55 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-010FS Project: YANK01204 Sample ID: 163741012 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units - DF Analyst Date Time Batch Mtd 3 DOE RESL Ni-I, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 78 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 81 (25%- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UT Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 56 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-01 IF Proiect: YANKO 1204 Sample ID: 163741013 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 65.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSSGAM & ALL FSS Actinium-228 0.894 +/-0.285 0.121 +/-0.285 0.255 pCi/g MJH1 06/15/06 2338 534130 1 Americium-241 U -0.0065 +/-0.0527 0.043 +/-0.0527 0.088 pCi/g Bismuth-212 U 0.385 +/-0.499 0.263 +/-0.499 0.551 pCi/g Bismuth-214 0.528 +/-0.139 0.0646 +/-0.139 0.135 pCi/g Cesium-134 UI 0.00 +/-0.0499 0.0436 +/-0.0499 0.091 pCi/g Cesium-137 U 0.0676 +/-0.0621 0.038 +/-0.0621 0.079 pCi/g Cobalt-60 0.122 +/-0.0837 0.0368 +/-0.0837 0.0784 pCi/g Europium-152 U -0.0509 +/-0.102 0.0819 +/-0.102 0.170 pCi/g Europium-154 U -0.0134 +/-0.124 0.103 +/-0.124 0.218 pCi/g Europium- 155 0.186 +/-0.145 0.076 +/-0.145 0.156 pCi/g Lead-212 1.01 +/-0.0964 0.0434 +/-0.0964 0.0896 pCi/g Lead-214 0.842 +/-0.147 0.0595 +/-0.147 0.123 pCi/g Manganese-54 U 0.0352 +/-0.0459 0.0393 +/-0.0459 0.0822 pCi/g Niobium-94 U -0.0177 +/-0.0382 0.0309 +/-0.0382 0.0647 pCi/g Potassium-40 16.3 +/-1.25 0.275 +/-1.25 0.598 pCi/g Radium-226 0.528 +/-0.139 0.0646 +/-0.139 0.135 pCi/g Silver-108m U -0.0176 +/-0.0361 0.0285 +/-0.0361 0.0592 pCi/g Thallium-208 0.314 +/-0.0793 0.0353 +/-0.0793 0.0736 pCi/g Rad Gas Flow Proportional Counting GFPC,SO9O, solid-ALL FSS Strontium-90 U 0.0193 +/-0.017 0.0153 +/-0.017 0.0344 pCi/g BXFI 06/18/06 1106 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -3.34 +/-6.23 5.29 +/-6.23 10.8 pCi/g SLN1 06/20/06 1651 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM1 05/28/06 1412 534097 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Page 57 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-01IF Project: YANK01204 Sample ID: 163741013 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE RESL Ni-1, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 77 (25%- 125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 89 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 58 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-013F Project: YANK01204 Sample ID: 163741014 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 61.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 1.21 +/-0.250 0.0775 +/-0.250 0.165 pCi/g MJH1 06/15/06 2354 534130 1 Americium-241 U 0.0448 +/-0.116 0.0842 +/-0.116 0.173 pCi/g Bismuth-212 0.622 +/-0.272 0.166 +/-0.272 0.352 pCi/g Bismuth-214 0.871 +/-0.154 0.0439 +/-0.154 0.0922 pCi/g Cesium-134 UI 0.00 +/-0.0417 0.0281 +/-0.0417 0.0593 pCi/g Cesium-137 U 0.0103 +/-0.0281 0.0232 +/-0.02 81 0.0489 pCi/g Cobalt-60 U 0.0299 +/-0.0305 0.0268 +/-0.0305 0.0573 pCi/g Europium-152 U -0.0772 +/-0.0721 0.0554 +/-0.0721 0.116 pCi/g Europium-154 U 0.0345 +/-0.0915 0.0761 +/-0.0915 0.163 pCi/g Europium-155 U 0.0901 +/-0.087 0.0707 +/-0.087 0.146 pCi/g Lead-212 1.15 +/-0.129 0.0377 +/-0.129 0.0779 pCi/g Lead-214 1.00 +/-0.172 0.041 +/-0.172 0.0856 pCi/g Manganese-54 U 0.0151 +/-0.0301 0.0256 +/-0.0301 0.0541 pCi/g Niobium-94 U 0.0107 +/-0.0253 0.0216 +/-0.0253 0.0454 pCi/g Potassium-40 19.2 +/-1.60 0.185 +/- 1.60 0.408 pCi/g Radium-226 0.871 +/-0.154 0.0439 +/-0.154 0.0922 pCi/g Silver-108m U 0.0111 +/-0.0239 0.0198 +/-0.0239 0.0416 pCi/g Thallium-208 0.313 +/-0.0665 0.0232 +/-0.0665 0.0487 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.0098 +/-0.0158 0.0157 +/-0.0158 0.0353 pCi/g BXFI 06/18/06 1106 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -2.7 +/-5.98 5.07 +/-5.98 10.3 pCi/g SLNI 06/20/06 1738 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM1 05/28/06 1412 534097 The following Analytical Methods were performed Method Description 1 EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Page 59 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-013F Proiect: YANK01204 Sample ID: 163741014 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE RESL Ni-1, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 77 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 83 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 60 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address: 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-014F Project: YANK01204 Sample ID: 163741015 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 54.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.829 +/-0.225 0.0682 +/-0.225 0.147 pCi/g MJHI 06/15/06 2346 534130 1 Americium-241 U -0.00581 +/-0.113 0.089 +/-0.113 0.184 pCi/g Bismuth-212 0.447 +/-0.261 0.161 +/-0.261 0.342 pCi/g Bismuth-214 0.758 +/-0.126 0.0375 +/-0.126 0.0792 pCi/g Cesium-134 U 0.0414 +/-0.0279 0.0252 +/-0.0279 0.0533 pCi/g Cesium-137 U -0.00389 +/-0.0232 0.0189 +/-0.0232 0.0402 pCi/g Cobalt-60 U -0.0145 +/-0.0239 0.0182 +/-0.0239 0.0404 pCi/g Europium-152 U 0.00738 +/-0.0586 0.0474 +/-0.0586 0.0995 pCi/g Europium-154 U -0.0016 +/-0.076 0.0629 +/-0.076 0.137 pCi/g Europium-155 U 0.0316 +/-0.0628 0.0545 +/-0.0628 0.113 pCi/g Lead-212 1.01 +/-0.109 0.0282 +/-0.109 0.0587 pCi/g Lead-214 0.746 +/-0.119 0.0365 +/-0.119 0.0763 pCi/g Manganese-54 U -0.00360! +/-0.027 0.0217 +/-0.027 0.0461 pCi/g Niobium-94 U -0.00521 +/-0.0228 0.0184 +/-0.0228 0.0391 pCi/g Potassium-40 14.7 +/-1.47 0.205 +/-1.47 0.450 pCi/g Radium-226 0.758 +/-0.126 0.0375 +/-0.126 0.0792 pCi/g Silver-108m U 0.000405 +/-0.0194 0.0165 +/-0.0194 0.0348 pCi/g Thallium-208 0.326 +/-0.0564 0.0209 +/-0.0564 0.0441 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr9O, solid-ALL FSS Strontium-90 U 0.0054 +/-0.0153 0.0161 +/-0.0153 0.0357 pCi/g BXFI 06/18/06 1106 536483 2 Rad Liquid Scintillation Analysis Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U -1.72 +/-7.06 5.96 +/-7.06 12.1 pCi/g SLN1 06/20/06 1825 538365 3 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM1 05/28/06 1412 534097 The following Analytical Methods were performed Method Description I EML HASL 300, 4.5.2.3 2 EPA 905.0 Modified Page 61 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-014F Proiect: YANKO 1204 Sample ID: 163741015 ClientID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE RESL Ni-1, Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 82 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 79 (25%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 62 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - wwwgel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-012F Project: YANKO 1204 Sample ID: 163741016 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 26.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0299 +1-0.151 0.144 +1-0.151 0.392 pCi/g JXGI 06/16/06 0803 537411 1 Curium-242 U 0.0126 +/-0.0957 0.089 +/-0.0957 0.300 pCi/g Curium-243/244 U 0.0383 +/-0.218 0.218 +/-0.218 0.540 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.00 +/-0.0633 0.00 +/-0.0633 0.0875 pCi/g JXGI 06/16/06 0928 537412 2 Plutonium-239/240 U 0.0335 +/-0.0944 0.0735 +/-0.0945 0.234 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U -0.179 +/-10.9 9.12 +/-10.9 18.8 pCi/g JXGI 06/20/06 1931 537417 3 Rad Gamma Spec Analysis Gamma,Solid-FSS GAM & ALL FSS Actinium-228 0.685 +/-0.143 0.0394 +/-0.143 0.0829 pCi/g MJHI 06/16/06 0623 534130 4 Americium-241 U-0. 000535 +/-0.0924 0.0773 +/-0.0924 0.159 pCi/g Bismuth-212 0.589 +/-0.310 0.087 +/-0.310 0.182 pCi/g Bismuth-214 0.445 +/-0.0688 0.023 +/-0.0688 0.0477 pCi/g Cesium-134 UI 0.00 +/-0.0301 0.0151 +/-0.0301 0.0313 pCi/g Cesium-137 0.184 +/-0.0341 0.0108 +/-0.0341 0.0226 pCi/g Cobalt-60 0.179 +/-0.0378 0.0132 +/-0.0378 0.028 pCi/g Europium-152 U 0.0299 +/-0.0402 0.0309 +/-0.0402 0.0637 pCi/g Europium-154 U 0.0105 +/-0.0393 0.0338 +/-0.0393 0.0718 pCi/g Europium-155 UI 0.00 +/-0.0573 0.0318 +/-0.0573 0.0653 pCi/g Lead-212 0.723 +/-0.0792 0.0193 +/-0.0792 0.0396 pCi/g Lead-214 0.586 +/-0.0847 0.0213 +/-0.0847 0.0441 pCi/g Manganese-54 U 0.003 +/-0.0149 0.0125 +/-0.0149 0.0261 pCi/g Niobium-94 U 0.00892 +/-0.0123 0.0107 +/-0.0123 0.0223 pCi/g Potassium-40 11.7 +/-0.969 0.0946 +/-0.969 0.205 pCi/g Radium-226 0.445 +/-0.0688 0.023 +/-0.0688 0.0477 pCi/g Silver-108m U -( 0.00372 +/-0.0119 0.0103 +/-0.0119 0.0213 pCi/g Thallium-208 0.221 +/-0.0359 0.0107 +/-0.0359 0.0223 pCi/g Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0. 0192 +/-0.0141 0.0192 +/-0.0141 0.0418 pCi/g BXF1 06/18/06 1109 536483 5 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.839 +/-6.11 5.08 +/-6.11 10.7 pCi/g NXPI 06/17/06 1626 535984 6 Liquid Scint C14, Solid AIIFSS Page 63 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-012F Project: YANK01204 Sample ID: 163741016 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Liquid Scintillation Analysis Liquid Scint C4, SolidAllFSS Carbon-14 U 0. +/-0.117 0.095 +/-0.117 0.193 pCi/g ATH2 06/05/06 2139 534837 7 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U - -3.6 +/-17.5 13.4 +/-17.5 28.2 pCi/g SLN1 06/21/06 0829 538969 8 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U - 2.17 +/-8.55 7.22 +/-8.55 14.7 pCi/g SLNI 06/20/06 1912 538365 9 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.0 182 +/-0.216 0.182 +/-0.216 0.375 pCi/g SXEI 06/14/06 1730 536314 10 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXMI 05/28/06 1412 534097 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EML HASL 300, 4.5.2.3 5 EPA 905.0 Modified 6 EPA 906.0 Modified 7 EPA EERF C-01 Modified 8 DOE RESL Fe-I, Modified 9 DOE RESL Ni-l, Modified 10 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 76 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 89 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 52 (25%-.125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 85 (25%-.125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 63 (25%- 125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 83 (15°-125%)

Page 64 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: June 23, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-012F Proiect: YANK01204 Sample ID: 163741016 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

• QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 65 of 75

I.

QUALITY CONTROL DATA I

Page 66 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: June 23, 2006 Client : Connecticut Yankee Atomic Power Page 1 of 9 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 163741 Pormnomo NO*M Samnie Aiinal OiC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 537411 QC1201110208 163741008 DUP Americium-241 U 0.0496 U 0.0424 pCi/g 16 (0% - 100%) JXGI 06/16/06 08:03 Uncert: +/-0.0968 +/-0.116 TPU: +/-0.097 +/-0.116 Curium-242 U 0.00 U -0.0313 pCi/g 200 (0%- 100%)

Uncert: +/-0.0738 +/-0.0354 TPU: +/-0.0738 +/-0.0357 Curium-243/244 U 0.00883 U -0.0933 pCi/g 242 (0%- 100%)

Uncert: +/-0.0669 +/-0.126 TPU: +/-0.0669 +/-0.126 QCI201110210 LCS Americium-241 13.0 12.7 pCi/g 98 (75%-125%)

Uncert: +/-1.35 TPU: +/-2.20 Curium-242 U 0.0293 pCi/g Uncert: +/-0.0778 TPU: +/-0.0779 Curium-243/244 15.9 15.4 pCi/g 97 (75%-125%)

Uncert: +/-1.50 TPU: +/-2.59 QCI201110207 MB Americium-241 U -0.0328 pCi/g Uncert: +/-0.0912 TPU: +/-0.0914 Curium-242 U -0.0112 pCi/g Uncert: +/-0.022 TPU: +/-0.022 Curium-243/244 U -0.129 pCi/g Uncert: +/-0.123 TPU: +/-0.124 QC1201110209 163741008 MS Americium-241 13.6 U 0.0496 13.4 pCi/g 99 (75%-125%)

Uncert: +/-0.0968 +/-1.46 TPU: +/-0.097 +/-2.36 Curium-242 U 0.00 U 0.0255 pCi/g Uncert: +/-0.0738 +/-0.102 TPU: +/-0.0738 +/-0.102 Curium-243/244 16.7 U 0.00883 16.3 pCi/g 98 (75%-125%)

Uncert: +/-0.0669 +/-1.62 TPU: +/-0.0669 +/-2.79 Batch 537412 QCI201110216 163741008 DUP Plutonium-238 U 0.00 U 0.00 pCi/g 0 (0% - 100%) JXG1 06/16/06 09:28 Page 67 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 163741 Page 2 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 537412 Uncert: +/-0.110 +/-0.0615 TPU: +/-0.110 +/-0.0615 Plutonium-239/240 U -0.226 U 0.0326 pCi/g 267 (0%- 100%)

Uncert: +/-0.163 +/-0.0917 TPU: +/-0.165 +/-0.0918 QCI201110218 LCS Plutonium-238 U 0.0301 pCi/g (75%-125%)

Uncert: +/-0.0797 TPU: +/-0.0798 Plutonium-239/240 12.0 10.9 pCi/g 91 (75%-125%)

Uncert: +/-1.29 TPU: +/-1.77 QCI201110215 MB Plutonium-238 U 0.0798 pCi/g Uncert: +/-0.0991 TPU: +/-0.0995 Plutonium-239/240 U 0.044 pCi/g Uncert: +/-0.0824 TPU: +/-0.0826 QC1201110217 163741008 MS Plutonium-238 U 0.00 U 0.00901 pCi/g (75%-125%)

Uncert: +/-0.110 +/-0.0856 TPU: +/-0.110 +/-0.0856 Plutonium-239/240 12.6 U -0.226 10.7 pCi/g 85 (75%-125%)

Uncert: +/-0.163 +/-1.08 TPU: +/-0.165 +/-1.51 Batch 537417 QC1201110230 163741008 DUP Plutonium-241 U 4.08 U -4.3 pCi/g 0 (0% - 100%) JXG1 06/20/06 20:33 Uncert" +/-6.18 +/-8.53 TPU: +/-6.19 +/-8.54 QC1201110232 LCS Plutonium-241 140 144 pCilg 102 (75%-125%) 06/20/06 21:36 Uncert: +/-10.8 TPU: +/-17.7 QC1201110229 MB Plutonium-241 U -2.16 pCilg 06/20/06 20:02 Uncert: +/-6.46 TPU: +/-6.47 QC1201110231 163741008 MS Plutonium-241 142 U 4.08 129 pCilg 91 (75%-125%) 06/20/06 21:05 Uncert: +/-6.18 +/-9.07 TPU: +/-6.19 +/-14.8 Rad Gamma Spec Batch 534130 QC1201102650 163741001 DUP Actinium-228 0.817 0.702 pCi/g 15 (0% - 100%) MJHI 06/16/06 06:30 Uncert: +/-0.177 +/-0.147

+/-0.147 Page 68 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 163741 Page 3 of 9 Parmname NOM Samole Oual OC Units RPD% REC% Range AnIst Date Time Rad Gamma Spec Batch 534130 TPU: +/-0.177 Americium-241 U 0.0431 U 0.0617 pCi/g 36 (0%- 100%)

Uncert: +/-0.0977 +/-0.0702 TPU: +/-0.0977 +/-0.0702 Bismuth-212 0.570 0.607 pCi/g 6 (0%- 100%)

Uncert: +/-0.292 +/-0.297 TPU: +/-0.292 +/-0.297 Bismuth-214 0.568 0.650 pCi/g 14 (0%- 100%)

Uncert: +/-0.0877 +/-0.103 TPU: +/-0.0877 +/-0.103 Cesium- 134 U 0.0314 UI 0.0349 pCi/g 11 (0%- 100%)

Uncert: +/-0.0354 +/-0.0245 TPU: +/-0.0354 +/-0.0245 Cesium-137 0.396 0.363 pCi/g 9 (0% - 100%)

Uncert: +/-0.0588 +/-0.0539 TPU: +/-0.0588 +/-0.0539 Cobalt-60 0.133 0.105 pCi/g 24 (0%- 100%)

Uncert: +/-0.0554 +/-0.0405 TPU: +/-0.0554 +/-0.0405 Europium- 152 U 0.00717 U -0.0343 pCi/g 306 (0%- 100%)

Uncert: +/-0.0581 +/-0.061 TPU: +/-0.0581 +/-0.061 Europium- 154 U 0.040 U -0.0163 pCi/g 475 (0% - 100%)

Uncert: +/-0.0643 +/-0.0693 TPU: +/-0.0643 +/-0.0693 Europium- 155 U 0.0854 U 0.0232 pCi/g 115 (0%- 100%)

Uncert: +/-0.0769 +/-0.0784 TPU: +/-0.0769 +/-0.0784 Lead-212 0.772 0.808 pCi/g 5 (0%- 20%)

Uncert: +/-0.0707 +/-0.0864 TPU: +/-0.0707 +/-0.0864 Lead-214 0.585 0.742 pCi/g 24 (0%- 20%)

Uncert: +/-0.0841 +/-0.099 TPU: +/-0.0841 +/-0.099 Manganese-54 U 0.0123 U 0.0098 pCi/g 22 (0%- 100%)

Uncert: +/-0.0261 +/-0.022 TPU: +/-0.0261 +/-0.022 Niobium-94 U -0.000522 U 0.00495 pCi/g 247 (0%- 100%)

Uncert: +/-0.0212 +/-0.0175 TPU: +/-0.0212 +/-0.0175 Potassium-40 12.1 12.1 pCi/g 0 (0%- 20%)

Uncert: +/-0.950 +/-1.08 TPU: +/-0.950 +/-1.08 Radium-226 0.568 0.650 pCi/g 14 (0%- 100%)

Uncert: +/-0.0877 +/-0.103 TPU: +/-0.0877 +/-0.103 Silver- 108m U 0.00495 U 0.0141 pCi/g 96 (0% - 100%)

Uncert: +/-0.0195 +/-0.018 Page 69 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 163741 Page 4 of 9 Parmname NOM Samnle Oual QC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 534130 TPU: +/-0.0195 +/-0.018 Thallium-208 0.300 0.295 pCi/g 2 (0%- 100%)

Uncert: +/-0.0497 +/-0.0475 TPU: +/-0.0497 +/-0.0475 QCI201102651 LCS Actinium-228 U 0.235 pCi/g 06/16/06 06:31 Uncert: +/-0.581 TPU: +/-0.581 Americium-24 1 23.4 23.0 pCi/g 98 (75%-125%)

Uncert: +/-2.46 TPU: +/-2.46 Bismuth-212 U 0.778 pCi/g Uncert: +/-1.12 TPU: +/-1.12 Bismuth-214 U -0.171 pCi/g Uncert: +/-0.298 TPU: +/-0.298 Cesium- 134 U 0.0723 pCi/g Uncert: +/-0.160 TPU: +/-0.160 Cesium- 137 9.63 10.5 pCi/g 109 (75%-125%)

Uncert: +/-0.824 TPU: +/-0.824 Cobalt-60 15.0 15.1 pCi/g 101 (75%-125%)

Uncert: +/- 1.08 TPU: +/-1.08 Europium- 152 U 0.042 pCi/g Uncert: +/-0.334 TPU: +/-0.334 Europium- 154 U 0.289 pCi/g Uncert: +/-0.325 TPU: +/-0.325 Europium- 155 U -0.257 pCi/g Uncert: +/-0.387 TPU: +/-0.387 Lead-212 U -0.101 pCi/g Uncert: +/-0.189 TPU: +/-0.189 Lead-214 U 0.233 pCi/g Uncert: +/-0.248 TPU: +/-0.248 Manganese-54 U 0.0621 pCi/g Uncert: +/-0.149 TPU: +/-0.149 Niobium-94 U -0.0598 pCi/g Uncert: +/-0.129 TPU: +/-0.129 Potassium-40 U 0.576 pCi/g Page 70 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 163741 Page 5 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Gamma Spec Batch 534130 Uncert: +/-1.23 TPU: +/-1.23 Radium-226 U -0.171 pCi/g (75%-125%)

Uncert: +/-0.298 TPU: +/-0.298 Silver-108m U -0.0434 pCi/g Uncert: +/-0.123 TPU: +/-0.123 Thallium-208 U 0.144 pCi/g Uncert: +/-0.146 TPU: +/-0.146 QC1201102649 MB Actinium-228 U 0.0712 pCi/g 06/16/06 06:23 Uncert: +/-0.0472 TPU: +/-0.0472 Americium-241 U 0.00139 pCi/g Uncert: +/-0.0249 TPU: +/-0.0249 Bismuth-212 U 0.0152 pCi/g Uncert: +/-0.166 TPU: +/-0.166 Bismuth-214 U 0.0175 pCi/g Uncert: +/-0.0261 TPU: +/-0.0261 Cesium- 134 U 0.00016 pCi/g Uncert: +/-0.0151 TPU: +/-0.0151 Cesium-137 U -0.00376 pCi/g Uncert: +/-0.0123 TPU: +/-0.0123 Cobalt-60 U 0.00528 pCi/g Uncert: +/-0.0137 TPU: +/-0.0137 Europium- 152 U -0.0157 pCi/g Uncert: +/-0.0336 TPU: +/-0.0336 Europium- 154 U -0.0124 pCi/g Uncert: +/-0.0325 TPU: +/-0.0325 Europium- 155 U 0.00213 pCi/g Uncert: +/-0.031 TPU: +/-0.031 Lead-2l2 U 0.000337 pCi/g Uncert: +/-0.0331 TPU: +/-0.0331 Lead-214 U 0.0225 pCi/g Uncert: +/-0.0398 TPU: +/-0.0398 Page 71 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 163741 Page 7 of 9 Parmname NOM Samnle Oual OC Units RPD% REC% Range AnIst Date Time Rad Liquid Scintillation Batch 534837 Uncert: +/-0.125 TPU: +/-0.125 QC1201104386 162335019 MS Carbon-14 7.13 U 0.0228 7.04 pCi/g 99 (75%-125%) 06/04/06 07:36 Uncert: +/-0.110 +/-0.249 TPU: +/-0110 +/-0.272 Batch 535984 QC1201106886 163626016 DUP Tritium U 0.738 U -1.57 pCi/g 0 (0%- 100%) NXP1 06/17/06 17:31 Uncert: +/-6.97 +/-7.27 TPU: +/-6.97 +/-7.27 QCI201106888 LCS Tritium 52.7 55.2 pCi/g 105 (75%-125%) 06/17/06 18:04 Uncert: +/-9.22 TPU: +/-9.27 QC1201106885 MB Tritium U -0.845 pCi/g 06/17/06 17:15 Uncert: +/-5.81 TPU: +/-5.81 QC1201106887 163626016 MS Tritium 53.0 U 0.738 44.6 pCi/g 84 (75%-125%) 06/17/06 17:47 Uncert: +/-6.97 +/-8.62 TPU: +/-6.97 +/-8.66 Batch 536314 QC1201107611 163741008 DUP Technetium-99 U 0.196 U 0.273 pCi/g 0 (0% - 100%) SXEI 06/14/06 18:37 Uncert: +/-0.227 +/-0.233 TPU: +/-0.227 +/-0.233 QC1201107613 LCS Technetium-99 13.1 11.5 pCi/g 87 (75%-125%) 06/14/06 19:11 Uncert: +/-0.471 TPU: +/-0.540 QC0201107610 MB Technetium-99 U 0.090 pCi/g 06/14/06 18:20 Uncert: +/-0.200 TPU: +/-0.200 QC1201107612 163741008 MS Technetium-99 12.7 U 0.196 11.2 pCi/g 88 (75%-125%) 06/14/06 18:54 Uncert: +/-0.227 +/-0.494 TPU: +/-0.227 +/-0.557 Batch 538365 QC1201112556 163741003 DUP Nickel-63 U -1.8 U -2.43 pCi/g 0 (0% - 100%) SLN 1 06/20/06 20:47 Uncert: +/-4.81 +/-6.00 TPU: +/-4.81 +/-6.00 QC1201112558 LCS Nickel-63 356 287 pCi/g 81 (75%-125%) 06/20/06 21:50 Uncert: +/-13.5 TPU: +1-15.5 Page 73 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 163741 Page 6 of 9 Parmname NOM Samnle Oual QC Units RPD% REC% Range AnIst Date Time Rad Gamma Spec Batch 534130 Manganese-54 U -0.00637 PCilg Uncert: +/-0.0124 TPU: +/-0.0124 Niobium-94 U -0.00531 pCi/g Uncert: +/-0.0115 TPU: +/-0.0115 Potassium-40 UI 0.00 pCilg Uncert: +/-0.267 TPU: +/-0.267 Radium-226 U 0.0175 pCi/g Uncert: +/-0.0261 TPU: +/-0.0261 Silver- 108m U -0.00282 pCilg Uncert: +/-0.0119 TPU: +/-0.0119 Thallium-208 U 0.000804 pCi/g Uncert: +/-0.0171 TPU: +/-0.0171 Rad Gas Flow Batch 536483 QC1201108057 163741001 DUP Strontium-90 U 0.00579 U 0.0106 pCi/g 0 (0% - 100%) BXFI 06/18/06 11:09 Uncert: +/-0.0116 +/-0.0165 TPU: +/-0.0116 +/-0.0165 QC1201108059 LCS Strontium-90 1.43 1.41 pCi/g 99 (75%-125%) 06/18/06 10:06 Uncert: +/-0.100 TPU: +/-0.109 QC1201108056 MB Strontium-90 U -0.0118 pCi/g 06/18/06 11:09 Uncert: +/-0.0102 TPU: +/-0.0102 QC1201108058 163741001 MS Strontium-90 1.44 U 0.00579 1.23 pCi/g 86 (75%-125%) 06/18/06 11:09 Uncert: +/-0.0116 +/-0.0952 TPU: +/-0.0116 +/-0.102 Rad Liquid Scintillation Batch 534837 QCI201104385 162335019 DUP Carbon- 14 U 0.0228 U 0.0418 pCi/g 0 (0% - 100%) ATH2 06/05/06 22:40 Uncert: +/-0.110 +/-0.121 TPU: +/-0.110 +/-0.121 QC1201104387 LCS Carbon-14 6.66 6.52 pCi/g 98 (75%-125%) 06/04/06 08:22 Uncert: +/-0.238 TPU: +/-0.259 QC1201104384 MB Carbon- 14 U 0.0371 pCi/g 06/04/06 06:04 Page 72 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 163741 Page 8 of 9 Parm name NOM Samnle Oual OC Units RPD% REC% Ranee Anlst Date Time Rad Liquid Scintillation Batch 538365 QC1201112555 MB Nickel-63 U -1.14 pCi/g 06/20/06 20:00 Uncert: +/-3.95 TPU: +/-3.95 QC1201112557 163741003 MS Nickel-63 413 U -1.8 347 pCi/g 84 (75%-125%) 06/20/06 21:33 Uncert: +/-4.81 +/-16.5 TPU: +/-4.81 +/-19.3 Batch 538969 QC1201113888 163741008 DUP Iron-55 U 21.1 U -1.03 pCi/g 0 (0%- 100%) SLNI 06/21/06 10:23 Uncert: +/-18.3 +/-16.3 TPU: +/-18.5 +/-16.3 QC1201113890 LCS Iron-55 575 529 pCi/g 92 (75%-125%) 06/21/06 10:40 Uncert: +/-44.0 TPU: +/-86.2 QC1201113887 MB Iron-55 U 5.38 pCi/g 06/21/06 09:51 Uncert: +/-26.8 TPU: +/-26.8 QC1201113889 163741008 MS Iron-55 594 U 21.1 546 pCi/g 92 (75%-125%) 06/21/06 10:07 Uncert: +/-18.3 +/-33.8 TPU: +/-18.5 +/-74.0 Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria Result is less than value reported Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL Page 74 of 75

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 163741 Page 9 of 9 Parmname NOM Sample Qual QC Units RPD% REC% Range AnIst Date Time h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

A The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 75 of 75

General Narrative Page 1 of 105

CASE NARRATIVE For CONNECTICUT YANKEE RE: Soil PO# 002332 Work Order: 168404 SDG: MSR #06-0652, 06-0675, 06-0687, 06-0688, 06-0707, 06-0743, 06-0755 August 15, 2006 Laboratory Identification:

General Engineering Laboratories, LLC Mailing Address:

P.O. Box 30712 Charleston, South Carolina 29417 Express Mail Delivery and Shipping Address:

2040 Savage Road Charleston, South Carolina 29407 Telephone Number:

(843) 556-8171 Summary:

Sample receipt The sample(s) for this Project arrived at General Engineering Laboratories, LLC, (GEL) in Charleston, South Carolina on May 5, May 9, May 12, May 17, May 26, June 2, June 8, 2006. All sample containers arrived without any visible signs of tampering or breakage. The chain of custody contained the proper documentation and signatures.

The laboratory received the following sample(s):

Sample ID Client Sample ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01 OF 168404008 9106-0005-014F 168404009 9106-0006-005F GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP,INC.

P.O. Box 30712 - Charleston, SC 29417 ° 2040 Savage Road (29407)

Page 2 of 105 Phone (843) 556-8171 - Fax (843) 766-1178

• www.gel.com

168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OOIF 16840401.5 9106-0010-012F Items of Note:

At the request of Dale Randall on July 20, 2006, GEL analyzed the above samples according to the spreadsheet in the attached email.

Case Narrative:

Sample analyses were conducted using methodology as outlined in General Engineering Laboratories (GEL) Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are listed below by analytical parameter.

Analytical Request:

Seven soil samples were reanalyzed for FSSALL, except gamma and Sr-90.

Four soil samples were reanalyzed for FSSALL, except gamma and Ni-63.

Two soil samples were reanalyzed for FSSALL, except gamma.

Two soil samples were reanalyzed for FSALL, except gamma, Sr-90 and Ni-63.

Internal Chain of Custody:

Custody was maintained for the sample(s).

Data Package:

The enclosed data package contains the following sections: Case Narrative, Chain of Custody and Supporting Documentation and all analytical fractions.

I certify that this data package is in compliance with the SOW, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hard copy data package has been authorized by the Laboratory Manager or a designee, as verified by the following signature.

Cheryl Jones Project Manager GENERAL ENGINEERING LABORATORIES, LLC a Member of THE GEL GROUP INC.

P.O. Box 30712 ° Charleston, SC 29417 ° 2040 Savage Road (29407)

Phone (843) 556-8171

• Fax (843) 766-1178

• www.gel.com Page 3 of 105

. I:

Additional HTD analyses

Subject:

Additional HTD analyses I U 8'4 0 (4'(,

From: "Dale Randall" <randall @cyapco.com>

Date: Thu, 20 Jul 2006 11:04:54 -0400 To: "Cheryl Jones" <cj @gel.corn>

CC: "Clyde Newson" <Newson@CYAPCO.com>, "John McCarthy" <McCarthy@CYAPCO.com>

Cheryl:

Per our earlier discussion, attached is a list of samples that we would like to have analyzed to the FSSALL protocol. I have included a list of test protocols performed on each sample to date. Once you have had an opportunity to determine our options for each sample please call or e-mail me at your convenience.

Thank You, Dale (860) 267-3133 Content-Description: GEL FSSALL analyses request.xls GEL FSSALL analyses request.xls Content-Type: application/vnd.ms-excel Content-Encoding: base64 I of I Page 4 of 105 8/2/2006 7:04 PM

flnnR To be done Previous VGEL ID 164220008 CY sample location IDs FSS xGamn Sr-90 Ni-63 Am Pu Sr9O Pu241 Fe55 Ni63 Tc99 H3 C14 9106-0002-007F x x x x x x x x x 31164220012 9106-0002-011F x x x x x x x x x x U,162335004 9106-0003-004F x x x x x x x x x x

- 162335014 9106-0003-015F x x x x x x x x x x 162832015 9106-0004-005F x x x x x x x x x x 162832009 9106-0004-015F x x x x x x x x x x 162485008 9106-0005-01 OF x x x x x x x x x x 162485011 9106-0005-014F x x x x _ _ x x x x x x 162850014 9106-0006-005F x x x x x x x x x x 163741005 9106-0008-006F x x x x x x x x x x 163741009 9106-0008-008F x x x x x x x x x x 164542008 9106-0009-002F x x x x x x x x x x 164542003 9106-0009-017F x x x x x x x x x x 163105009 9106-0010-001F x x x x x x x _ _x x x 163105016 9106-0010-012F x x x x x--- x x x x

Chain of Custody and Supporting Documentation Page 6 of 105

ev S:q 0 L(

Health Physics Procedure GPP-GGGR-RS 104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00371 362 Injun Hollow Road, East Hampton, CT 06424 0

860-267-2556 _____________________

tJ.

Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones M 5.

Priority: Z 30 D. [] 14 D. [] 7 D. Container Media Type &Type C PL Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0002-OOIF 5/17/06 10:42 SE C BP xx Transferred from COC 2006-003 57 9106-0002-002F 5/18/06 09:43 SE C BP - x - Transferred from CCC 2006-003 61 9106-0002-003F 91i06-0002-004F 5/18/06 10:14 SE C BP X X Transferred from COC 2006-00361 5/18/06 10:39 SE C BP X X Transferred from COC 2006-00361 9106-0002-005F 5/18/06 12:49 SE C BP X X Transferred from COC 2006-00364 9106-0002-006F 5/18/06 13:14 SE C BP X X _ _Transferred fromn C*C 2006-00364 9106-0002-006FS 5/18/06 13:14 SE C BP X X - Transferred from COC 2006-00364 9106-0002-007F 5/18/06 13:37 SE C BP X X Transferred from COC 2006-00364 9106-0002-008F 5/18/06 14:04 SE C BP . x Transferred from COC 2006-00364 NOTES: PO #: 002332 MSR #: 06- SSWP# NA [ LTP QA [] Radwaste QA E Non QA Samples Shipped Via: Internal 9 Fed Ex Container C UPS Temp.:

Deg. C EHand Custody Sealed?

I e uDate/Time 2) 1.ived By Date/Time Custody Seal 1ý"gelintuiiQ BýJ Date/Time 4) Received By Date/Time _ _ YO_ No_

Bill of Lading

5) Relinquished By Date/Time 6)Received By Date/Time 79)" 'YM{5' 57/C)

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-00 I Maj or Heallt Phsc Prcdr GP-GG-510-0 -tahmnI-C-0I ao It' Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00372 CD 001 362 Injun Hollow Road, East Hampton, CT 06424 Project Name:

-ddam Neck Decommissioning Analyses Requested _ Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones n IL Priority: Z 30 D. [] 14 D.E] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID 9106-0002-009F 5/18/06 14:28 SE C BP x Transferred from COC 2006-00364 9106-0002-01OF 5/18/06 14:50 SE C BP X x Transferred from COC 2006-00364 9106-0002-011F 5/19/06 08:10 SE C BP x x Transferred from COC 2006-00365 9106-0002-012F 5/19/06 08:31 SE C BP X x Transferred from COC 2006-00365 9106-0002-013F 5/19/06 09:00 SE C BP x x Transferred from COC 2006-00365 9106-0002-014F 5/19/06 09:58 SE C BP X x Transferred from COC 2006-00365 9106-0002-014FS 5/19/06 09:58 SE C BP X X Transferred from COC 2006-00365 9106-0002-015F 5/19/06 10:29 SE C BP x x Transferred from COC 2006-00365 9106-0002-016F 5/19/06 13:19 SE C BP I 3 Transferrd from CxC 2006-00365 NOTES: PO #: 002332 MSR #: 06- SSWP# NA g LTP QA E] Radwaste QA E] Non QA Samples Shipped Via: Internal 09'57 Fed Ex Container UPS Temp.:

Deg. C E) Hand Custody Sealed?

1 ,Relin! ihe'wi Date/Time 2) Reýived By Data/Time Custody Seal 4 ~ f /~ []..QOther intact?

3)%Kelinquished By Date/Time 4) Received By Date/Time YO NO Bill of Lading #

5) Relinquished By Date/Time 6) Received By Date/Time q9"'V4 7t?

Connecticut Yankee Statement of Work for Analytical Lab Services . .CY-ISC-SOW-001 Figure 1. Sample Check-in List Date/Time Received: to 0:

SDG#: . _ (o -c-'*-(015 Work Order Number: C* '2 O ".

Shipping Cdatainer IDý207 Lf! 5'5 7/ 0 Chain of Custody# O 4, o- 9.

1. Custody Seals oti shipping container intact?. Yes No []

2. Custody Seals dated and signed? Yes No[.

3. Chain-of-Custody record present? Yes j/\No[ "

4. Cooler temperature Vermiculite/packing materials is: Wet [ ] Dry ]

5.

. ,Number of samples in shipping container: t ICA-

7. Sample holding times exceeded? Yes No

8. Sampl&s have:

-tape -hazard labels

-K custody seals - appropriate sample labels

9. Samples are:.*

)Cjin good condition -leaking

-broken .- '" "have air bubbles

10. Were any anomalies identified in sample receipt? Yes'[ ] NoXI

11. .Description of anomalies (include sample numbers):

Saample. Custodian/Laboratory: Date Dam.. . . -D Telephoned to: On By Page 9 of 105

Connecticut Yankee Statement of Work for Analytical Lab Services rv'..j -cy-ISC-SOW-001

.CY-lsC-sow-ool Figure 1. Sample Check-in List DateiTime Receivedý <,f'.*"ý "

SDG#: A LO G 0 Sý Work Order Number: Io.r"" W "

Shipping Cdntainer IDn:ý " LN 5 -59T Chain of Custody'# - O3'_

I. Custody Seals on"shipping container intact? -Yes No [ ]

Yes No []

2. Custody Seals dated and signed?

. Yes No [..

3. .

3. Chain-of-Custody record present? Yes No[

.4. Cooler temperature OP .-

5. Vermiculite/packing materials is: Wet [ ] Dry [, ]

~jy.

6.: Number of samples in shipping container:. __"

7. Sample holding times exceeded? Yes No

8. taSl hazard labels

-custody seals -appropriate sample labels 9, Samples are:'

good condition " leaking

-broken i--_._have air bubbles

10. Were any anomalies identified in sample receipt? Yes [ NoO

11. Description of anomalies (include sample numbers):

Sample Custodian/Laboratory:-./:,j ý i4 Date:_ ___________

Telephoned to: On. By.

Page 10 of105

~SAMPLE RECEIPT & REVIEW F ORM 0 §

~PM use only I

Date Reevd L PM (A)Review (ensure Ron-C011ontimifg items are resolved prior to signing);

eReceived By:0-Sample Receipt Criteria Comments/Qualifiers (Required for Non-Conforming Items) conainer other (descibe)

Circle Applicable: seals broken damaged comainr Shipping containers received intact 1 and sealed? .n ice bags blue ice dry ice none oiler desribe)

Samples requiring cold Circk Coolant #

2 preservation within (4 +1- 2 C)?

Record preservation inethod. /

Chain of custody documents included with shipment? ,1___

Cirkle Applicable-,s broken damaged container leaking container other (descrbie)

Sample containers intact and sealed? ,_

s Samples requiring chemical l iD's. containers affected and observed pH:

if 5preservation at proper pH?- -

Sample ID's and containers affected:

6 VOA vials free of headspace (defined as < 6mm bubble)? ___

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)

Samples received wi 'holding Id's and ei affected:

time? .__,,_

9 Sample ID's COC match ID's Sample ID's ando affected:

- on bottles?.,_

Samp1ID's affected:

10 Date & me on COC match date

- & ti on bottles?

Nu ber of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in 12 relinquished/received sections? Co0__&_ - _ _,

__0_0_(e 14 Air Bill ,Tracking #s, Additional Comments i , RSORADReceipt# ____________

Suspected Hazard Information *If > x2 area background is observed on samples identified as "non-Z to regulated/non-radioactive", contact the Radiation Safety group for further Z investigation.

A Radiological Classification? Maximum Counts Observed*: *p-1 B PCB Regulated? _,/_ Comments:

Shipped as DOI" Hazardous C Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. I/ N#:

PM (or PMA) review of Hazard class tication-: Initials Date: - (

Page 11 of 105

• SAMPLE RECEIPT & REVIEW FORM 0

Client:(o, f (C'* yr" l SDIAlRCOCIWork Order: / .. ..

Review {ere non-onror gI are resolved prior to sipi.,g):

Date Received:"' CA, 0( 0PM(A) o Received BY:

Sample Receipt Criteria i Comments/Quialifiers equired for Non-Conforming Items) damaged container leaking container odier (describe)

Shipping containers received intact Circle Applicable: seals broke and sealed? ..... __

CircleCoolant # i76ags blue ice dry ice none other describe)

Samples requiring cold 2[preservation within (4 +/- 2 Q)?

Reco~rd preservation method. /. ...

3 Chain of custody documents/

included with shipment? *I..

Sample containers intact and Cie pplicable: seals broken damaged container leaking container other (describe) 4sealed? 7 4/......

5 Samples requiring chemical ample ID's. containers affected and observed pH:

preservation at proper pH? ._ ,_.

VOA vials free of headspace Sanple ID's and containers affected:

(defined as < 6mm bubble)? _ _.... .

Are Encore containers present?

7 (If yes, immediately deliver to VOA laborato Samples received within holdin Id's and Testsaffected:

time? _ _._,__

9 Sample ID's on COC ma c ID's Sample ID's and containers affected:

on bottles? r tch date Sample ID's affected:

10 Date & time on COC

& time on bottles?

Number of containe received Sample ID's affected:

match number idic ted on COC?

COC form is pro,-y signed in relinquished/recived sections? Coc- ZOO(,, -- *)' 9(_

Air Bill Tracking #'s, &

Additional Comments

'a V 'a RSO RAD Receipt#

S e Hzr If > x2 area background is observed on samples identified as "non-Suspected Hazard Information .'** * 'regulated/non-radioactive", contact the Radiation Safety group for further

• investigation.

A adiological lassi fcation. Maximum Counts Observed-:

• B Regulated? / Comments:

hippe as 00771 azardous c Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. UN#:

PM (or PMA) review of Hazard classification: ntials Date:

Pg12f15 Page 12 of 105

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 1 Major Chain of Custody Form N.20-01

-,a*

Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 No. 2006-00312

__.......___abUse__l__.""__./" ./.- ', "35 W860-267-2536 _____________________________________________

Project Name: Haddam Neck Decommissioning Analyses Requested L.ab. Use.. Only Contact Name & Phone: 'Com.nnts.

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC, 29407 t 9.

843 556 8171. Attn. Cheryl Jones V Cn Priority: Z 30 D.[] 14 D. [17 D. Container Sample Size- '

Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sam.plei IP.

• 0' 9106-0003-OO1F 4/24/06 14:13 SE C 13P X Transferred from COC2006-00221 I" 9106-0003-002F 4/24/06 14:39 SE C BP X Transferred from COC2006-00221 6'9106-0003-003F 4/24/06 15:01 SE C 1P X Transferred from CoC2006-00221 9106-0003-004F 4/25/06 08:41 SE C 13P X Transferred from COC2006-00223 9106-0003-004FS 4/25/06 08:41 SE C l3P x Transferred from COC2006-00223 9106-0003-005F 4/25/06 09:21 SE C BP X fTransferred from COC2006-00223 9106-0003-006F 4/25/06 09:46 SE C BP X Transferred from COC2006-00223 9106-0003-007F 4/25/06 10:28 SE C BP x Transferred from COC2006-00223 9106-0003-008F 4/25/06 11:15 SE C BP X Transferred from COC2006-00223 NOTES: PO : 002332 MSR #- 0 6 -°O SSWP# NA [ LTP QA (I Radwaste QA l Non QA Samples Shipped Via: 4,tern'1 Co6fi"er Combined samples 9106-0003-003F taken on 4/25/06 @08:19 and 9106-0003-003FB taken on 4/25106@ 08:19 in order to have sufficient sample for ounting. Fed Ex-' Deg,. C' U PS .. : ,...- . ..

.. Hand . "d' tdSealed.,'..'

1)Relinquished By Date/Time 2) iee~ved By 1 Date Time :CUStdy .Seal Intat?

3) Relinquished By Date/Time 4) Received By 110).

Dale/Time Other :1 .-

Bill of Lading # ' .

5) Relinquished By Date/Time 6) Received By Date/Time .9-920- Ž'502o 024 . "

Health Pbysics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Health Physics Procedure GPP-GGGR-R5 104-003 -Attachment B-CY-00 1 Major Chain of Custody FormNo206031 No. 2006-00313 Connecticut Yankee Atomic Power CompanyC CD 362 Injun Hollow Road, East Hampton, CT 06424 / .2iz 860-267-2556 / -,35,'-.

'Z5 04-."

o/

Project Name: Haddam Neck Decommissioning Analyses Requested . -

Contact Name & Phone: ,'origK.*..: <,.-

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 J Ito 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D. El 14 D. D 7 D. Container Sample Size-Media Type &Type . -.

Sample Designation Date Time Code Code Code Comment, Preservation L41 S 9106-0003-009F 4/25/06 13:00 SE C BP x Transferred from COC 2006-00236 9106-0003-01OF 4/25/06 13:23 SE C BP x Transferredfrom COC2006-00236 - .-

9106-0003-01OFS 4/25/06 13:23 SE C BP X Transferred from COC 2006-00236 4/25/06 15:12 SE C BP X Transferred from COC 2006-00236 00 9106-0003-012F 9106-0003-013F 4/25/06 14:21 SE C BP x Transferred from COC 2006-00236 9106-0003-014F 4/25/06 14:48 SE C BP x Transferred from COC 2006-00236 01L 9106-0003-015F 4/26/06 08:16 SE C BP x Transferred from COC 2006-00237 ".

OR-; 9106-0003-016F 4/26/06 09:41 SE C BP X Transferred from COC 2006-00237 I 9106-0003-017F 4/26/06 09:18 SE C BP X Transferred from CVU 2006-00237 to

-9106-0003-018F 4/26/06 08:59 SE IC I BP xI Transferred from COC 2006-00237 oil ~-4-4-4-4~-~ - 4 ~ .. . .. F ... . i 7 .. . .

NOTES: PO #: 002332 MSR#: 0 6 -0 SSWP#NA Z LTPQA [] Radwaste.QA [] Non QA Samples Shipped Via:

[ Fed Ex El uPs 0- Hand S'e'9"Intact?

Y'Teni N I) Relinquished By Date/Time 2) eceived By Date/Time

3) Relinquished By

/Tieo Date/Time 4)Re

4) Received By y eTi

'Date/Time

[] Other Bill of Lading #

7 ZO-012 /7-

Connecticut Yankee Statement of Work for Analytical Lab Services .CY-ISC-SOW-OO

-. Figure 1. Sample Check-in List Date/Time Received: . ) , . 0 "

SDG#: - 4A.-&O)- &(J'-

Work Order Number: I(Z- 35 Shipping Ccntaifer ID: 1UP6 55c1L0 O4 1 Chainof CustodY# AQCQ(o" 605 14.,

0,,. q o03 1.(

.1. Custody Seals od shipping container intact?... Yes. ] No I

2. Custody Seals dated and signed? Yes [ ] No

3. Chain-of-Custody record present? Yesp No [ ]

4. Cooler temperature ) .

5. Vermiculite/packing materials is: Wet [] Dry _I]"Ft-,

6. Number of samples in shipping container: [

7. Sample holding times exceeded? Yes [ No

-tape ----- hazard labels

_ZcUstody seals .appropriate sample labels

9. Samples are-good condition 2 lJeaking

-broken ___have air bubbles

10. Were any anomalies identified in sample receipt? Yes [ ] No Qc2 11.. Description of anomalies (include sample numbers):

Sample Custodian/Laboratory: (Ii)- (4 CC-tCrv; DatewL" Telephoned to: _On By Page 15 of 105

SAMLERECEIPT & REVIEW FORM ICient: 54rRt5%' PM we only! '2 3

[

4 SDG/ARCOC/Work Order:

Date Received: re? 5/1516 Review (ensure non-cont itPM(A) g iems are resolved prior to signing):

Received By: ( i.v c.... -

Sample Receipt Criteria Z Comments/Qualifiers (Required for Non-Conforming Items)

Circl Applicable: seals broken damaged container leaking container otlier (describe)

I Shipping containers received intact

___ __ __Coolant_#_icebagsblueicedryice and sealed?

Samples requiring cold Circl Coolnt I cc bags blue c dy ice noe 2 preservation within (4 +/- 2 C)? de" Record preservation method. Pen"___

Chain of custody documents included with shipment? ,_, _,

Sample containers intact and Circle Applicable: stab broken damaged container leaking conainer other (describe) sealed?

Samples requiring chemical Sample ID's. containers affected and observed pH:

preservation at proper pH? ......... . .

VOA vials free of headspace Sample ID's and containers affected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laborator_)

Samples received within holding Id's and tests affected.

time?

Sample ID's on COC match ID's Sample ID's and containers affected--

on bottles?

Date & time on COC match date ample I's affected:

& time on bottles?

Sampl ID's affected:

Number of containers received match number indicated on COC__?_V_1 COC form is properly signed in relinquished/received sections?

Air Bill ,Tracking #'s, & F9d .'0 Z 1 Additional Comments t b 0 V

"D -4 lRSO RAD Receipt #

Suspected Hazard Information _ *If> x2 area background is observed on samples identified as "wn-Z.&I regulated/non-radioactive", contact the Radiation Safety group for further

_ __ investigation.

Radiological Classification? Maximum Counts Observed*:

Shipped as DUT Haaous C Material? If yes, contact Waste #Hazard Class Shipped:

Manager or ESH Manager. AN1 PM (or PMA) review of Hazard classification: Initials Date: 77t'o Page 16 of 105 61 F' #

I I,

GPP-GGGR-R5 104-003 -Attachment B-CY-00 1 Major Health Physics Procedure Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 I

-ProjectName: Haddamn Neck DecommissiC

-22ontact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: 0 30 D.[] 14 D. L 7 D.

Samples Shipped Via:

[ Fed Ex ri ups El Hand El Other Bill of Lading #

Health Physs Pro6edure GPP-GGGR-R5104-003-Attachment B-CY-00 1 Major

'CQU*. t Yankee Atomic Power Company

": Injun Hollow Road, East Hampton, CT 06424 I

Neck Contact Name & Phone:

Jack McCarthy" 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: M 30 D.E] 14 D. E] 7 D.

Samples Shipped Via:

[ Fed Ex E ups

[] Hand E1 Other Bill of Lading #

Connecticut Yankee Statement of Work for Analytical Lab Services CY-ISC-sOw-001 Figure 1. Sample Check-in List Li-Datc/Timc Reccived: .* - /d . G. . . , CY-ISC-SOW-001 SDG#: 44,5 R:' 4-0-049 Work Order Number: -.

7 Shipping Container ID: 7"14 *31S5 Z- i Chain of Custody # ,x* o. ig- 6 oss -

I. Custody Seals on shipping container intact? Yes No [

2. Custody Seals dated and signed? Yes No []

3. Chain-of-Custody record present? Yes No [J

4. Cooler temperature

5. Vermiculite/packing materials is: Wet Y Dry [ ]

6. Number of samples in shipping container:

7. Sample holding times exceeded? Yes [] No

8. Samples have:

_ tape hazard labels

._,rcustodyseals __ appropriate sample labels

9. Samples are:

in good condition _ leaking broken have air bubbles

10. Were any anomalies identified in sample receipt? Yes No []

Il. Description of anomalies (include sample numbers):

Sample Custodian/Laborato ry: Date: 9'

.By Telephoned to: On By___________

Paqe 45 of 56 Page 19 of 105

. Connecticut Yankee Statement of Work for Analytical Lab Services CY-Isc-SOW-O01 Figure 1. Sample Check-in List.

Date/Time."/i Received: . a 1 " "

• SDG#: J-- -

Work Order Number:-_ I___ ___-._ _ __ __ __

Shipping Cdhtainer ID- Chain ofCustody# _(_._ - _0_ _ 334 1.

!. Custody Seals. odnshipping container intact? Yes [Y No

2. Custody Seals dated and signed? Yes [] .No

3. Chain-of-Custody record present? Yes ' No [1

4. Cooler temperature r*'

5. .Vermiculite/packing materials is: Wet [fPlDiy t\ "

6- Number ofsamples in shipping contain'er

7. Sample holding times exceeded?

8.. Samples have-:

. Weretany amedtdi hazard labels

. .esciptoy seaalise appropriate Sample labels

9. S amples are:anL:t. r - .. . - -.

__7_~~In good conition.,,_ ,*

.- __.* brkem:. " " have air bubbles

1. "

.eci ..ti on a om lies...'

"Tlephrnedt any o:_____ ___________n_ __

r ecei pt .? Yes N Page 20 of 105 . "" .- "

SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM

-Fed F2. oý.-_ )-. ...-. , , -

-(aI ____ -_______ I ( ") S, itv

-l ~qlq 3 5 cmls *a _,-I- o 2,('ao . i-,

cL -u-s_ 5 'QOOZ SAs o n I

Page 21 of 105

SAMPLE RECEIPT & REVIEW FORM a,

PM use only Client: 7rl" SDGIARCOC/Work Order: /: ' 3.-

Date Received: .PM(A) Review (ensure non-conforming items are resolved prior to signing&:

[Received By: *,6 * . 1'./h Sample Receipt Criteria 4 CommentsfQualifiers (Required for Non-Conforming Items) other (describe) containers received intact Circle Applicable: seals broken damaged container leaking container 1 Shipping and sealed? x Samples requiring cold Circle Coolant # ire bags blue ice dry ice none o&ter describe) 2 preservation within (4 +1- 2 C)?

Record preservation method. _ _. ....

3 Chain of custody documents included w ith shipment? _ _seals_ broke _ _ _ _ _ _ _ _ __c_ _ _ _ _ _ _ _ _ _ _ _ _ _

4 Sample containers intact and Ciwle Applicable: seals broken damaged container It oter (describe) sealed? At.<A 910o(- 0oooi- oi0 E 5 Samples requiring chemical Sample UD's. containes affected and observed pH:

preservation at proper pH?

,6 JVOA vials free of headspace Sample ID's and conltainers affected:

(defined as < 6mm bubble)?_ _ _ _ _ _ _ _ _ _ _

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)

Samples received within holding 1d's and tests affected:

time?

9 Sample ID's on COC match ID's Smpl I's a coninr affect:"

on bottles?

time on COC match date S ID's affected:

0&Datetime& on bottles? ,____

Number of containers received 1iD's afecWd:

match number indicated on COC?

12 COC form is properly signed in relinquished/received sections? _eac. X Ao4, Air Bill ,Tracking F's, &

Additional Comments Suspected~

Hmr womton zr9. *If > x2 are background iscontact regulatetnon-radioactiveo, observed on samtples identified as the Radiation Safety group forfurther

_______ investigation.

A Raidio~lognkal CLaissilic.Aton? Mxmum Counts Observed*

7 I as'. Ha-arous C Material? If yes, contact Waste " " /hppd Manager or ESH Manager. UN#:

P/0 t-V9 "'wof Hazard classification: Initials 4_ Date: // (

UI

0 SAMPLE RECEIPT & REVIEW FORM 0

PM use only Cfient- j,'dVo t, 9SDG/ARCOC/Work Order: /LZM-,

Date Receied: ~~ PM(A) Review ¶ ma oufonn ft resolved prior to signing):

amesum 2

ReceivedBy: ( t pe"j c_____

Sample Receipt Criteria Comments/Quali'ers (Required for Non-Conforming Items)

Shipping containers received intact -ircle Applicable: seals broken damaged comainer leaking coalmoer oWier (describe) and sealed? . ... ._ _ _,_,

Samples requiring cold Circle Coolant # ice bags blue ice dry ice (*) aojar descrile) 2 preservation within (4 +/- 2 C)? )

' Record preservation method. .

tv . ...

Chain Of Custody documents 3 included wit*.h shipment?

... .U~ S. 0 N bX q-)U 4

includedwithishieentpV de  : sn ~ damaged container leaking coaitaaer ,odier(decne Sample containers intact and 4 bjen ine ig c -als s Samples requiring chemical mple IDas. conainers affected and observed pH:

preservation at proper pH? .......

VOA vials free of headspace le ID's an cairs .ffecm:

- (defined as < 6mm bubble)? ....

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) _

8 Samples received within holding Id's and ests affected:

time?

Sample ID's on COC match ID's Sample ID's am cnftainms affected:

on bottles?

Date & time on COC match date Sample ID's affecd:"'

& time on bottles?

NNumber of containers received Sample ID's affected:

match number indicated on COC?

COC form is properly signed in " CtGS CLvy., vLi *%ui :V\Ct relinquished/received sections?

14 Air Bill ,Tracking #'s, & i

• u---. ..

Additional Commaents v T R50 RAD ReceiptI ai q *"f> x2 area background is observed on samples identified as .non-Suspected Hazard Information Q 3:

_ _ _ _ _ _ _ ,a 'L regulated/non-radioactive, contact the Radiation Safety group for further investigation.

A Radiological BICB Regulated?Classification? Maximum Counts Observed*:

I iComan.:

iShipped as MIT Hazardous Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. UNI:

PM (or PMA) review of Hazard classification: Initials _ Date: _

• J Y

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-001 Major Healh Pysis Pocedre PP-GGRR5 14-03 -ttahmen B-Y-III ajo Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissic Contact Name & Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority:030 D.[] 14 D.M7D.

Samples Shipped Via:

S Fed Ex El ups M Hand nI Other Bill of Lading # [

7qc 9/9

• Connecticut Yankee Statement of Work for Analytical Lab Services -CY-ISC-SOW-001 Figure 1. Sample Check-in List Date/Time Received- h SD -G#: kkS -- -&

Work Order Number: \ L  %"/

Shipping Cdhtainer ID 'A"

- C .' 5'Jq Chain of Custody#.

1. Custody Seals oii shipping container intact?.. -Yes *kNo[]

2. Custody Seals dated and signed? Yes 'KNo H.

3. Chain-of-Custody record present? Yes L4'No I I

°4. Coolerteprature I '( 1 '1

5. Vermiculite/packing materials is: Wet [,'Dry W i,

6. Number ofsamples in shipping container:

7. Sample holding times exceeded?

Yes[] No

10. Were any anomalies identified insample receipt? " "Yes [] No

11. .Description of anomalies (include sample numbers):

Jude sapl numbers Page 25 of 105

.,r

SAMPLE RECEIPT & REVIEW FORM PM use only CSDG/ARCOCIWork Order. /G 2-(t85 Date Received: PM(A) Review (ensure non-coformlg items are resolved prior to signing):

Received B Vi Sample Receipt Criteria Z Comments/Qualifiers (Required for Non-Conforming Items)

Circle Applicable: seals broken damaged container leaking container other (describe)

N1, Shipping containers received intact ..

al~sealed?

Circle Coolant # blue ice dry ice none other describe)

Samp requiring cold ice bags 2 preservati within (4 +/- 2 C)?

Record preserv *on method.

3IChain of custody d nts included with shipment?

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking comainer other (describe) sealed?

Samples requiring chemical Sample *D*3'containes affected and observed pH:

preservation at proper pH? , _ __ ___IDsanticontainersaffected:

6. VOA vials free of headspace ' aNc S(defined as < 6mm bubble)?

jAre Encore containers present?"6 7 (If yes, immediately deliver to VOA laboratory) 8 Samples received within holding id's and es afeed time?

9 Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles?

Date & time on COC match date Sample ID's affected:

101& time on bottles?

n1lNumber of containers received Sample ID's affected:

match number indicated on COC?

12 COC form is properly signed in relinquished/received sections?

Air Bill ,Tracking #'s, & fd.( "qic ' [ 9 5- 4,-- /7 --

14 Additional Comments 42t493 w-c.-,([

, T RSO RAD Receipt #

S dHaar Information lIf > x2 area background is observed on samples identified as *non-Suspected Hzazard Io a 0 regulated/non-radioactive". contact the Radiation Safety group for further I investigation.

A Radiological Classificatimo - Maximum Counts Observed*:

Cor s IB P'hipped CB Rte gas ted ?

u laDUt Hazardous C Material? If yes, contact Waste Hazard Class Shipped:

Manager or ESH Manager. UN#:

PM (or PMA) review of Hazard classitication. Initials Date:

rav /-Doi.I.. V/

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424

.860-267-2556 iroject Name: Haddam Neck Decommissioning

ýContact Name &Phone:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D. [] 14 D. M 7 D.

Samples Shipped Via:

[ Fed Ex LI uPS El Hand El Other Bill of Lading #

• ?.92 fo- .1el-

Connecticut Yankee Statement of Work for Analytical Lab Services .CY-ISC-SOW-001 Figure 1. Sample Check-in List.

Date/Time Received':-_(I . - ,*"

SDG#: AA Work Order Number.. _"_____________l._"

Shipping CdhtainerlID--t, ~Q~CCt5X Chain of Custqdy# S et ( riý-sk -

I. Custody Seals. owishipping container intact?... -Yes JNof4)

2. Custody Seals dated and signed?

Yes [I No I3. Chin-of-Custody record prýsent? . Yes WANo* [1

.4. Cooler temperature = o1-.

5. Vermiculite/packing materials is:

Wet p) Dry f],

6: Number of samplesin shipping container:. ()

7. Sample holding times cxceded? Yes [] No

.Samples h.ve.

'-hazard label

- custody seals - appropriate sample labels

9. Samples are..

A" good condition -leaking Sbroken * + have air bubbles

10. Were any anomalies identified in sample receipt?

Yes []No *p 11 Description of anomalies (incluesml ubr:______________

Sample CustOdianAa rtory -Dae3 f, 4 ~ J I l" ph' T elep h onn"ed toto:

'-' . ..  :' - ." " ~Date- . Z5.- --

Page 28 of 105

- NG/4;ý SAMPLE RECEIPT & REVIEW FORM 4 ofoon.,yy Client. SDG/ARCOC/Work Order: ((,Zn2 , &(,Z7e5.

Date Received: _PM(A) J-/ Review (ensure nn,-conforin u m reoved prior to uigming):

Received By: C iQ.ev I' cm ,j, I,.,, M, _ -_,_.. .. I_,,___

Sample Receipt Criteria 4 Z Z Comments/Qualiirns (Required for Non-Conforming items) irce* Applkable: scab broken damaged omaine, leaking contae otiler (desabe) 1 Shipping containers received intact and sealed?

Samples requiring cold Circle Coolait # ie bags bte- ice dry ic e aej) oier descrie) 2 preservation within (4 +1- 2 C)?

.0 C_>

Record preservation method.

Chain of custody documents / C£.S oax-o w

• included with shipment? I/ I eeSample containers intact and p/C th damaged coai/er leakit, co-taiq nr oi (dicnribe)

S Samples requiring chemical n/yile iD's. coimn,, affected and oberved pH: a preservation at proper pH? ....

6 VOA vials free of headspace Sample ID's and coainers affected:

(defined as < 6mm bubble)? ......

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory) vd'3 and testsaffected:

Samples received within holding 8 lime?4 9 Sample ID's on COC match ID's Sample S ID's and couainme affected:

on bottles?

10 Date & time on COC match date Samnple ID's allecto:

& time on bottles?

Number of containers received Sml w's affi  :

match number indicated on COC?

COC form is properly signedin in Ct ,s C,.L- VLif'(LUts*'TC1 u

12relinquished/received sections?

Air Bill ,Tracking #'s, & , CiC-,)t*u4$iG ( *IuL*'

Additional Comments IV RSOR AD Receipt SS *If > x2 area background is observed on samples idenified as *non-Suspected HaZard Information -g

.~regulatd/non-radioactive*, contact the Radiation Safety gru for fi rte ad_19 investigation.

A Radiological Classification? - Maximum Counts Observede:

Comments:

B CB Regulated?

Shipped as IX r Hazardous C Material? Ifyes, contact Waste , Hazard Class Shipped:

Manager or ESH Manager. UN#:

PM (or PMA) review of Hazard classification:

Pý, IGQ,, V3 I'Zin"ntal ae 1'7 r,ý %J Y

,-ii,,i Ilh

5 SAMPLE RECEIPT & REVIEW FORM CONTINUATION FORM.

'IAAIkA,7 943 2, 16 Z 50

- ~ 8 6q0 - op (C) nin (4hN 5 ccide-v h ad nkt Page 30 of 105

.1 ;,"in,'

Health Physics Procedure GPP-GGGR-R5104-003 -Attachment B-CY-00 I Major

-c Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00367 362 Injun Hollow Road, East Hampton, CT 06424 0 860-267-2556 .. /[,3-7 Project Name: Haddam Neck Decommissioning -.-. Analyses Requested Lab Use Only 0

Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 843 556 817 1. Attn. Cheryl Jones r * * .

Priority: Z 30 D. [] 14 D. [] 7 D. Container Sample Size-Dae T Media Type &Type on Sample Designation Date Time Code Code Code Comment Preservation Lab Sample ID 9106-0008-OO1F 5/05/06 11:13 SE C BP X x x Transferred from COC #2006-00324 9106-0008-003F 5/5/06 13:35 SE C BP x x x Transferred from COC # 2006-00325 9106-0008-004F 5/5/06 13:51 SE C BP x x x Transferred from COC # 2006-00325 9106-0008-005F 5/5/06 14:17 SE C BP X x x Transferred from COC # 2006-00325 9106-0008-006F 5/5/06 14:36 SE C BP x x X Transferred from COC # 2006-00325 9106-0008-006FS 9106-000.-007F 5/5/06 5/5/06 14:36 15:03 SE C BP X x x Transferred from COC # 2006-00325 SE C BP X TransferredfromCOC#2006-00325 9106-0008-002F 5/5/06 13:10 SE C BP X X X Transferred from COC # 2006-00325 9106-0608-002F_______ 1 5116 1:01S P xx xTanfre rmCC#20-02 NOTES: PO #: 002332 MSR#: 06-0710 SSWP#NA SLTP QA E Radwaste QA E] Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.: __ Deg. C FEUPS

[ Hand Custody Sealed?

1 , I i YO NO Date/Time J~Tme~ Custody Seal Intact?

~-Z6~12'r , .- -P El Other 3)ik mnquished By \J Date/Time D hate/Time YO NO I 4) lideiveZ'*y "

! Bill of Lading #

R 21557 lC2_ /z/6

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-001 Major

~Chain ~No. of Custody Form 2006-00366 C Connecticut Yankee Atomic Power Company W 362 Injun Hollow Road, East Hampton, CT 06424 t* 860-267-2556 163-7 L__IV.

Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & hone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories o m 2040 Savage 817 1.Road.

843 556 Attn.Charleston Cheryl Jones SC. 29407

• ** z Priority: Z 30 D. [] 14 D. ] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID (p 9106-0008-008F. 5/08/06 08:01 SE C BP X x x ___ __ Transferred from COC #2006-00327 010 9106-0008-009F 5/08/06 08:32 SE C BP X X X Transferred from COC #2006-00327 D11 9106-0008-01OF 5/08/06 09:09 SE C BP x x x Transferred from COC # 2006-00327

)oi 9106-0008-010FS 9106-0008-01OF 5/08/06 09:09 SE C BP x x X Transferred from COC #2006-00327 5/08/06 09:30 SE C BP X X X Transferred from COC #2006-00327

)Itf~

)I 9106-0008-012lF

ý 9106-0008-012F 5/08/06 09:530 ... SE 09:53 C B3P BP x X x Transfered Transferred from from COC N2006-00327

1. 2006-00327

)1t 9106-0008-013F 5/08/06 10:16 SE C BP X X X Transferred from COC #2006-00327 05 9106-0008-014F 5/08/06 10:47 SE C BP X X X Transferred from COC # 2006-00327 NOTES: PO #: 002332 MSR #: 06- O"q* SSWP#NA 0 LTP QA [I Radwaste QA [I Non QA Samples Shipped Via: Internal Container M Fed Ex Temp.: -4 1 Deg. C miUPs E Hand Custody Sealed?

Y[0 N)'

1) Relinquished By Date/Time 2) Received By Date/Time Custody Seal Intact?

E Other

3) Relinquished By Date/Time 4) Received By Date/Time Y 9 NO Bill of Lading #

Connecticut Yankee "(0371 4 " /

Statement of Work for Analytical Lab Services -CY-ISC-SOW-001 Figure 1. Sample Check-in List.

Date/Time Received: ]Ii..t .,.

SDG#:

Work Order Number:__

Shipping Cchitainer ID:.. " ' I Chain of Custody# O00 -0C)3 0q

1. Custody Seals.or! shipping container intact?.. -Yes i'TRo []

2. Custody Seals dated and signed? Yes[ ]No [I

3. Chain-of-Custoly record present? Yes [_1o [4]

4. Cooler .temperature

5. Vermiculite/packing materials is: Wet [ Dry -, ] IlVAf 6"' Number of samples in shipping container: "__

Sample holding times exceeded? Yes [ ] No

.8. Samples hav6:*

hazard labels

.Z.-custody seals /appropriate sample labels

9. Samples are:

S .*

.~ good condition "_leaking broken - have air bubbles

10. Were any anomalies identified in sample receipt? Yes [ ] No 1...Description of anomalies (include sample numbers):

Telephoned to:__________________By" On______ __

'Page 33 Of 105

0 SAMPLE RECEIPT & REVIEW FORM a,

& time onCOC match date ne on bottles?

ber of containers received h number indicated on COC? I form is properly signed in 1f x2 area backrground is obevd ;

ADRcep ronaples idestiJfd as noah.

1= 11u=ate~n~dioactjy'. contact the Radiation Safety group for furthe Maxizmm Courits Observed*: ~:

? ifyes, contact Waste lfMd; ssSipped:

, or ESH Manager.

Iniials Page 34 of 105

SAMLERECEIPT & REVIEW FORM ICilent:

Date Received:Y Received By:

an ku&

C .(

12

,'t JSDG/ARCOC/Work PM(A)

Review (ensure Order:

r..tnmonly mon-conforming 5ite are resolved prior to signing):

Sample Receipt Criteria > 4 4 Comments/Qualiners (Required for Non-Conforming Items) leaking container other (describe)

Circle Applicable: seals broken damaged container Shipping containers received intact and sealed? do Samples requiring cold Circle Coolat # ice bags blue ice dry ice odwr describe 2 preservation within (4 +/- 2 C)?

Record preservation method.

Chain of custody documents l included with shipment? ____________________________

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking container odw (describe) sealed?_1 Samples requiring chemical Sample ID's. containers affected and observed pH:

5preservation at proper pH? __________________________

6 VOA vials free of headspace Sample ID's and containers affected:

(defined as < 6mm bubble)? _

Are Encore containers present?

7 (If yes, immediately deliver to .

VOA laboratory)

Samples received within holding Id's and esew affected.

8time? _________________________

9onSamplebsID's on CO match ID's Sample ID's and containers affected:

I&Date & time on COC match date Sample ID's affected:

10;& time on bottles? __________________________

Number of containers received Sample ID's affected:

match number indicated on COC? I COC form is properly signed in ci-F " q Iu.tiA'qt4.1/5,.d 12 relinquished/received sections?

,' te

-I" t2,t

'"r (.. 1L 14 A ir B ill ,Tra ck in g # 's , &

Additional Comments T RSO RAD Receipt #___ ________

SIf > x2 area background is observed on samplesidenifi-d as -non-Suspected Hazard Information 0 - - regulated/non-radioactive'. contact the Radiation Safety group for further

,.. E investigation.

A Radiological Classification? Maximum Counts Observed*:

ipped as DO)1Hazardous Haza Class Shipped:

C Material? If yes, contact Waste ad s d Manager or ESH Manager. N J I PM (or PMA) review of Hazard class iication: Initials e Date:

I I Page 35 of 105

J(~,3-1qI~

Connecticut Yankee Statement of Work for Analytical Lab Services .CY-ISc-Sow-001 Figure 1. Sample Check-in List DatefTime.Received: s"z_4 t3G2 (j, Oti'*"

SDG#:

Work Order Number:

Shipping Cdntainer ID: 1 S57 i 112 Chain of Custody # "C6ao Lajce

1. Custody Seals oui shipping container intact? Yes Fi Io I

2. Custody Seals dated and signed? Yes *,4fo [ ].

3. Chaia-of-Custody record present? Yes Ld,4,o [I

4. Cooler temperature "6

5. Vermiculite/packing materials is: Wet VDry [I1

6. Number of samples in shipping container: C "U.*iihk

7. Sample holding times exceeded? Yes-[ ] No

8. Samples have:

___hazard

-p labels cuody seals ___appropriate sample labels

9. Samples arpe:.

J_ý_in good condition ____leaking broken ___have air bubbles

10. Were any anomalies *identified in sample receipt? Yes [ ] No [-<

1. Description of anomalies (nldsapenumbers):A.

Sample Custodian/Laboratory: tr 'C*b Date.:. -

Telephoned to: . On By Page 36 of 105

" .11 .,

Health Physics Procedure GPP-GGGR-R5104-003-Attachment B-CY-00 I Major 1&45-149 -A I

CD Chain of Custody Form No. 2006-00380 W5 Connecticut Yankee Atomic Power Company 362 Injun Hollow Road, East Hampton, CT 06424 Project Name: Haddam Neck Decommissioning - Analyses Requested LabUse Onl.Y..

Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 (. <

843 556 8171. Attn. Cheryl Jones . Col Priority: Z 30 D. E] 14 D. 0 7 D. Container Media Sample Size-Media Type &Type . I .__

Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID iA 9106-0009-016F 5/15/06 13:28 SE C BP X X Transferred from COC 2006-00352 0 9106-0009-016FS 5/15/06 13:28 SE C BP x x Transferred from COC 2006-00352 9106-0009-017F 5/15/06 14:03 SE C BP X X Transferred from COC 2006-00352 04 9106-0009-01 IF 5/15/06 08:05 SE C BP x Transferred from COC 2006-00351 pq 9106-0009-013F 5/15/06 08:35 SE C BP X X Transferred from COC 2006-00351 V5 9106-0009-013FS 5/15/06 08:35 SE C BP X X - -j- Transferred from COC 2006-00351 Di1 9106-0009-014F 5/15/06 08:59 SE C BP x -- I- Transferred from CCC 2006-00351

¢*t 9106-0009-015F 5/15/06 09:36 SE C BP X X Transferred from COC 2006-00351 I

NOTES: P04:002332 MSR #: 0 6 -0/' SSWP#NA SLTP QA El Radwaste QA El Non QA Samples Shipped Via: Internal Container

[E Fed Ex Temp.: __ Deg. C

[] UPS El Hand Custody Sealed?

YO NO

1) Relinquised By Date/Time 2) R i d Date/Time Custody Seal Intact?

El Other

3) Relinquished By Date/Time 4) ReleiveA By Date/Time YE N-Bill of Lading#

3-lýv-/? 3

Health Physics Procedure 1110-a I - I g-4.1 I

'~' ~ I GPP-GGGR-R5104-003-Attachment B-CY-001 Major C$

Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00381 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 C*

" Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 0, 843 556 8171. Attn. Cheryl Jones Priority: Z 30 D. [] 14 D. E] 7 D. Container Sample Size-Media Type &Type Sample Designation Date Time Code Code Code Comment, Preservation Lab Sample ID

"-9106-0009-OF 5/11/06 13:22 SE C BP x X Transferred from COC 20D6-00347 a'I1 9106-0009-002F 9106-0009-003F 5/11/06 5/11/06 13:46 14:06 SE SE C

C BP BP x

x X

x Transferred from COC 2006-00347 Transferred from COC 2006-00347 9106-0009-004F 5/11/06 14:30 SE C BP X X Transferred from COC 2006-00347 0(it 9106-0009-005F 5/11/06 14:55 SE C BP X X Transferred from COC 2006-00347 1, 9106-0009-007F 5/12/06 07:44 SE C BP X X Transferred from COC 2006-00348 013. 9106-0009-008F 5/12/06 08:16 SE C BP X X Transferred from COC 2006-00348 6( 9106-0009-009F 5/12/06 08:35 SE C BP X X Transferred from COC 2006-00348 0(cf 9106-0009-00F 5/12/06 09:07 SE C BP X X Transferred from COC 2006-00348 NOTES: PO #: 002332 MSR #: 06- SSWP# NA 0 LTP QA El Radwaste QA El Non QA Samples Shipped Via: Internal Container

[ Fed Ex Temp.: __ Deg. C El UPS El Hand Custody Sealed?

YO] N[D

1) Reeinquisned By Custody Seal Intact?

Date/Time /_/*VADate/Time

/,,, od El Other Jft7 r79,,otf 2) Re:cZe* vVe ýy ý I -

Y0 ND 1 3)Relinquished By Date/Time 4) Receiived By / Date/Time Bill of Lading #

tq?1/y- zJ7Yl

I ,'-Pzd-~r~

4-( Ito UV146 1 Y Connecticut Yankee Statement of Work for Analytical Lab Services -CY-ISC-SOW-O01 Figure 1. Sami )le Check-in List Date/rime Received: " - 0 , .Oo(

SDG#: Ma Work Order Number:

2,009 -aO "3 &'L,.

Shipping Container ID:i,-'/-" 3 '* Chain of Custody #

1. Custody Seals o6f shipping container intact?. -Yes LINo [1

2. Custody Seals dated and signed? Yes[ Noo

3. Chain-of-Custody record present? Yes 4 No []

4. Cooler tenmperature

5. Vermiculite/packing materials is: Wet JDry4

6. ,Number of samples in shipping container:

7. Sample holding times ex:eeded? Yes

• No (I

10. Were any anomalies identified in sample receipt? Yes [ No 11., Description of anomalies (include sample numbers):

Sample. Custodian/Laboratory: Date.: -6 -G 2LOC Telephoned to: On By '

Page 39 of 105

Health Physics Procedure GPP-GGGR-RS5104-003-Attachment B-CY-001 Major Connecticut Yankee Atomic Power Company Chain of Custody Form No. 2006-00349 362 Injun Hollow Road, East Hampton, CT 06424 860-267-2556 Project Name: Haddam Neck Decommissioning Analyses Requested Lab Use Only Contact Name & Phone: Comments:

Jack McCarthy 860-267-2556 Ext. 3024 Analytical Lab (Name, City, State)

General Engineering Laboratories 2040 Savage Road. Charleston SC. 29407 .

843 556 8171. Attn. Cheryl Jones C z Priority: Z 30 D. [] 14 D. F1 7 D. Container Media Type &Type Sample Designation Date Time Code Code Code I Comment, Preservation Lab Sample ID

-9106-0010-OOIF 5/04/06 10:49 SE C BP X X Transferred from COC 2006-00321 0 9106-0010-002F 5/04/06 11:12 SE C BP X X TransferredfromCOC 2006-00321 it 9106-0010-004F 5/04/06 12:48 SE C BP X x Transferred from COC 2006-00321 i 9106-0010-006F 5/04/06 13:34 SE C BP X X Transfrred from COC 2006-00321 013 9106-0010-007F 5/04/06 13:21 SE C BP X X Transferred from COC 2006-00321 8it 9106-0010-009F 5/04/06 14:01 SE C BP X x Transferred from COC 2006-00321 9106-0010-OIOF

- 5/04/06 14:21 SE C BP X X Trasfemed from COC 2006-00321 a 9106-0010-012F 9 5/04/06 14:44 SE C BP X X Transferred from COC 2006-00321

'I 9106-0010-013F 5/04/06 15:06 SE C BP X Tramsferred from COC 2006-00321 NOTES: PO #: 002332 MSR#: 06- 0707 SSWP#NA Z LTP QA El Radwaste QA Dl Non QA Samples Shipped Via: Internal Container Z Fed Ex Temp.: /j7Deg. C 0l UPS El Hand CustodySealed?

Y E" N 0 1)RelinquisheBy Date/Ti e 2) Received y Date/Time Custody Seal Intact?

Dl Other 3)Relinquished By DateTime 4) Receved By ate/Time Y 9--N 0 Bill of Lading #

3qo4- 3 )15- g--tf

Connecticut Yankee Statement of Work for Analytical Lab Services cY-lSG-sow-Qol Figure 1. Sample Check-in List Date/Time Received: _L17 /.o b CY-/SC-SOW-001 SDG#: N...to*4p-07/3"7 Work Order Number:

Shipping Cdntainer ID: t 311 SS.,l Chain of Custody#. 2OWL- 60397 I. Custody Seals ori shipping container intact? -Yes

• No []

2. Custody Seals dated and signed? Yesj- No [ J.

3. Chain-of-Custody record present? Yes No 1]

4. Cooler temperature _U7' C

5. Vermiculite/packing materials is: Wet 9. Dry '.

6. Number of samples in shipping container:

7. Sample holding times exceeded? Yes [ ] No p*

8. Samples have'

_tape ----- hazard labels

_z

... ustody seals -appropriate sample labels

9. Samples are:

!.-in good condition . eaking

-broken .have air bubbles

10. Were any anomalies identified in sample receipt? Yes [ No ix]

11...Description of anomalies (include sample numbers): ._

Samnple CustodianLaboratory: -4/s*,- ) Date: *V"--O(

Telephoned to: } On By -

Page 41 of 105-

1111 t SAMPLE RECEIPT & REVIEW FORM OR ' use only Client: 1 aSDG/ARCOC/Work Order:

Date Received: 5- 1Z L PM(A) Review ( 4e 1 g items are resolved prior to signing):

Received By: &uv" [

Sample Receipt Criteria Com ents/Qualifiers (Required for Non-Conforming Items) other (describe)

Shipping containers received intact Circle Applicable: seals broken damaged container leaking coruaincr and sealed? I ice bags blue ice dry ice other decbe)

Samples requiring cold / Circle Coolant #

2 preservation within (4 +/- 2 C)?

Record preservation method.

Chain of custody documents included with shipment?_

4 Sample containers intact and Circle Applicable: seals broken damaged container leaking container other (describe)

.sealed?I Samples requiring chemical Sample ID's. containers affected and observed pH:

preservation at proper pH? .1 6 VOA vials free of headspace Sample ID's and containers affected:

(defined as < 6mm bubble)?

Are Encore containers present?

7 (If yes, immediately deliver to VOA laboratory)

Id's and tests affected:

8 Samples received within holding time?

Sample ID's on COC match ID's Sample ID's and containers affected:

on bottles?

Date & time on COC match date Sample ID's affected:

& time on bottles? _

Number of containers received Sane ID's affected:

match number indicated on COC? _

COC form is properly signed in 1 relinquished/received sections?

Air Bill ,Tracking #'s, & (.r-Ill Additional Comments v* U"* RSO RAD Receipt #

SJ H a I m *If > x2 area background is observed on samples identified as "non-S U U regulated/non-radioactive", contact the Radiation Safety group for further

__ 9 investigation.

A IRadiological Classification?a V Maximum Counts Observed*: in*% 46

-~IPCB Regulated? V Commnents:

Shipped as D01 Hazardous C Material? If yes, contact Waste ""Hazard Class Shipped:

]Manager or ESH Manager. UN#:

PM (or PMA) review of Hazard classification: Initials e -Date: /', .

P. Z Page 42 of 105

List of current GEL Certifications as of 15 August 2006 State Certification Alaska UST-062

-Arizona AZ0668 -

Arkansas 88-0651 CLIA 42D09040k6 California 01151 CA Colorado GenEngLabs Connecticu t.. PH-0169 Dept. of Navy NFESC 413 EPA WG-15J Florida/NELAP Georgia E87156 (FL/NELAP)

Idaho N/A Illinois Indiana C-SC-01 Kansas 10 E-10332 IMaryland Kentucky

. .. .... s -oo29.... ... ,

90129 270 Massachusetts M-SCO12 Michigan Nevada SCI New Jersey New York 11501 North Carolina 233 North Carolina Drinking W North Dakota Oklahoma Pennsylvania ___ 68-485 South Carolina 1012000111658501/10i20002 Tennessee __02934 Texas TX21*3-2006A -.....

S-52597 ....... l U.S. Dept. of Agriculture N/A US Army Corps of Engineer Utah Vermont N/A Virginia 00151 Washington C223 Page 43 of 105

RADIOLOGICAL ANALYSIS Page 44 of 105

Radiochemistry Case Narrative Connecticut Yankee Atomic Power Co. (YANK)

Work Order 168404 Method/Analysis Information Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555696 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201153129 Method Blank (MB) 1201153130 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153131 168340011(9304-01-005C) Matrix Spike (MS) 1201153132 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Page 45 of 105

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 168404003 (9106-0003-004F) was recounted due to high MDA.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Page 46 of 105

Product: Alphaspec Am241, Cm, Solid ALL FSS Analytical Method: DOE EML HASL-300, Am-05-RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 557837 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Sample ID Client ID 168404009 9106-0006-005F 168404010 9106-0008-006F 1201158316 .Method Blank (MB) 1201158317 168404009(9106-0006-005F) Sample Duplicate (DUP) 1201158318 168404009(9106-0006-005F) Matrix Spike (MS) 1201158319 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404009 (9106-0006-005F).

QC Information Page 47 of 105

All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Alphaspec Pu, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu-I -RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555697 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 48 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OO1F 168404015 9106-0010-012F 1201153133 Method Blank (MB) 1201153134 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153135 168340011(9304-01-005C) Matrix Spike (MS) 1201153136 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-01 1 REV# 14.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Page 49 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Pu241, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Pu-1i -RC Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555698 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 50 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 1F 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-01OF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201153137 Method Blank (MB) 1201153138 168340011(9304-01-005C) Sample Duplicate (DUP) 1201153139 168340011(9304-01-005C) Matrix Spike (MS) 1201153140 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-035 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (OC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Page 51 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Manual Integration No manual integrations were performed on data in this batch.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: GFPC, Sr90, solid-ALL FSS Analytical Method: EPA 905.0 Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 556350 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 52 of 105

Sample ID Client ID 168404003 9106-0003-004F 168404004 9106-0003-015F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201154644 Method Blank (MB) 1201154645 168404003(9106-0003-004F) Sample Duplicate (DUP) 1201154646 168404003(9106-0003-004F) Matrix Spike (MS) 1201154647 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-004 REV# 10.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404003 (9106-0003-004F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Page 53 of 105

Chemical Recoveries All chemical recoveries meet the required acceptance limits for this sample set.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Samples 1201154644 (MB), 1201154645 (9106-0003-004F), 1201154646 (9106-0003-004F),

1201154647 (LCS), 168404003 (9106-0003-004F), 168404004 (9106-0003-015F), 168404012 (9106-0009-002F), 168404013 (9106-0009-017F), 168404014 (9106-0010-001F) and 168404015 (9106-0010-012F) were dried and reweighed due to low matrix spike/laboratory control sample recovery.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Tc99, Solid-ALL FSS Analytical Method: DOE EML HASL-300, Tc-02-RC Modified Analytical Batch Number: 554580 Page 54 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201150561 Method Blank (MB) 1201150562 168340012(9304-02-003C) Sample Duplicate (DUP) 1201150563 168340012(9304-02-003C) Matrix Spike (MS) 1201150564 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-005 REV# 13.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Page 55 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Fe55, Solid-ALL FSS Analytical Method: DOE RESL Fe-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555722 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 56 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-O1OF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OO1F 168404015 9106-0010-012F 1201153222 Method Blank (MB) 1201153223 168340012(9304-02-003C) Sample Duplicate (DUP) 1201153224 168340012(9304-02-003C) Matrix Spike (MS) 1201153225 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-040 REV# 3.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (0C0 Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Page 57 of 105

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint Ni63, Solid-ALL FSS Analytical Method: DOE RESL Ni-1, Modified Prep Method: Ash Soil Prep Dry Soil Prep GL-RAD-A-021 Method: Dry Soil Prep Analytical Batch Number: 555723 Prep Batch Number: 554650 Dry Soil Prep GL-RAD-A-021 Batch Number: 554649 Page 58 of 105

Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 1201153226 Method Blank (MB) 1201153227 168340012(9304-02-003C) Sample Duplicate (DUP) 1201153228 168340012(9304-02-003C) Matrix Spike (MS) 1201153229 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-022 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340012 (9304-02-003C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Page 59 of 105

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: LSC, Tritium Dist, Solid-HTD2,ALL FSS Analytical Method: EPA 906.0 Modified Analytical Batch Number: 554582 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-OO1F 168404015 9106-0010-012F 1201150569 Method Blank (MB) 1201150570 168340011(9304-01-005C) Sample Duplicate (DUP) 1201150571 168340011(9304-01-005C) Matrix Spike (MS) 1201150572 Laboratory Control Sample (LCS)

Page 60 of 105

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-002 REV# 12.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168340011 (9304-01-005C).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis Sample 168404010 (9106-0008-006F) was recounted due to high MDA.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Page 61 of 105

Qualifier information Manual qualifiers were not required.

Method/Analysis Information Product: Liquid Scint C14, Solid AII,FSS Analytical Method: EPA EERF C-01 Modified Analytical Batch Number: 554583 Sample ID Client ID 168404001 9106-0002-007F 168404002 9106-0002-01 IF 168404003 9106-0003-004F 168404004 9106-0003-015F 168404005 9106-0004-005F 168404006 9106-0004-015F 168404007 9106-0005-OIOF 168404008 9106-0005-014F 168404009 9106-0006-005F 168404010 9106-0008-006F 168404011 9106-0008-008F 168404012 9106-0009-002F 168404013 9106-0009-017F 168404014 9106-0010-001F 168404015 9106-0010-012F 1201150573 Method Blank (MB) 1201150574 168404003(9106-0003-004F) Sample Duplicate (DUP) 1201150575 168404003(9106-0003-004F) Matrix Spike (MS) 1201150576 Laboratory Control Sample (LCS)

SOP Reference Procedure for preparation, analysis and reporting of analytical data are controlled by General Engineering Laboratories, LLC as Standard Operating Procedure (SOP). The data discussed in this narrative has been analyzed in accordance with GL-RAD-A-003 REV# 8.

Calibration Information:

Calibration Information All initial and continuing calibration requirements have been met.

Standards Information Standard solution(s) for these analyses are NIST traceable and used before the expiration date(s).

Page 62 of 105

Sample Geometry All counting sources were prepared in the same geometry as the calibration standards.

Quality Control (QC) Information:

Blank Information The blank volume is representative of the sample volume in this batch.

Designated QC The following sample was used for QC: 168404003 (9106-0003-004F).

QC Information All of the QC samples met the required acceptance limits.

Technical Information:

Holding Time All sample procedures for this sample set were performed within the required holding time.

Preparation Information All preparation criteria have been met for these analyses.

Sample Re-prep/Re-analysis None of the samples in this sample set required reprep or reanalysis.

Miscellaneous Information:

NCR Documentation Nonconformance reports are generated to document any procedural anomalies that may deviate from referenced SOP or contractual documents. A nonconformance report (NCR) was not generated for this SDG.

Additional Comments Additional comments were not required for this sample set.

Qualifier information Manual qualifiers were not required.

Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative.

Review Validation:

GEL requires all analytical data to be verified by a qualified data validator. In addition, all data designated for CLP or CLP-like packaging will receive a third level validation upon completion of the data package.

Page 63 of 105

The following data validator verified the information presented in this case narrative:

Reviewer/Date: 6--9/Z4§z% z Page 64 of 105

SAMPLE DATA

SUMMARY

Page 65 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for YANKOO Connecticut Yankee Atomic Power Co.

Client SDG: 168404 GEL Work Order: 168404 The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

• • Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

ND The analyte concentration is not detected above the detection limit.

The above sample is reported on a dry weight basis except where prohibited by the analytical procedure.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis.

This data report has been prepared and reviewed in accordance with General Engineering Laboratories, LLC standard operating procedures. Please direct any questions to your Project Manager, Cheryl Jones.

Reviewed by Page 66 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-007F Project: YANK01204 Sample ID: 168404001 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 18-MAY-06 Receive Date: 02-JUN-06 Collector: Client Moisture: 20.9%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0 .0762 +/-0.102 0.00 +/-0.102 0.0956 pCi/g BXLI 08/11/06 1336 555696 1 Curium-242 U 0.00 +/-0.0995 0.00 +/-0.0995 0.138 pCi/g Curium-243/244 U -0.( 10853 +/-0.0717 0.0405 +/-0.0717 0.177 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.199 +/-0.228 0.181 +/-0.229 0.444 pCi/g BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U 0 .0341 +/-0.129 0.120 +/-0.129 0.323 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 10.0 +/-6.64 5.08 +/-6.72 10.7 pCi/g BXLI 08/16/06 1220 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 4.17 +/-6.67 5.28 +/-6.67 11.4 pCi/g DFAI 08/09/06 1128 554582 4 Liquid Scint C14, SolidAllFSS Carbon- 14 U 0 .0813 +/-0.0797 0.0634 +/-0.0797 0.132 pCi/g ATH2 08/09/06 0324 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 9.90 +/-48.1 32.0 +/-48.1 65.9 pCi/g MXPI 08/12/06 1633 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.02 +/-6.39 5.18 +/-6.40 10.6 pCi/g MXPI 08/11/06 0738 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U ).139 +/-0.213 0.173 +/-0.213 0.360 pCi/g EGD1 08/11/06 2027 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu- 11-RC Modified 4 EPA 906.0 Modified Page 67 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-007F Project: YANKO 1204 Sample ID: 168404001 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA EERF C-01 Modified 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 80 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 100 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 98 (25%-/125%/o)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 75 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 74 (15/-,125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 68 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-01IF Proiect: YANKO 1204 Sample ID: 168404002 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 19-MAY-06 Receive Date: 02-JUN-06 Collector: Client Moisture: 17.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.120 +/-0.154 0.0683 +/-0.155 0.251 pCi/g BXLI 08/11/06 1336 555696 1 Curium-242 U -0.0146 +/-0.122 0.0692 +/-0.123 0.303 pCi/g Curium-243/244 U -0.0103 +/-0.0861 0.0487 +/-0.0862 0.213 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.0121 +/-0.125 0.127 +/-0.125 0.344 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0254 +/-0.0675 0.0381 +/-0.0675 0.167 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 6.72 +/-7.02 5.56 +/-7.05 11.7 pCi/g BXLI 08/16/06 1237 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U -0.521 +/-7.03 5.94 +/-7.03 12.8 pCi/g DFAI 08/09/06 1143 554582 4 Liquid Scint C14, SolidAllFSS Carbon- 14 U 0.023 +/-0.0828 0.0685 +/-0.0828 0.143 pCi/g ATH2 08/09/06 0426 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 3.93 +/-47.7 31.9 +/-47.7 65.7 pCi/g MXPI 08/12/06 1649 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.52 +/-5.81 4.68 +/-5.81 9.60 pCi/g MXPI 08/11/06 0825 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.173 +/-0.203 0.164 +/-0.203 0.341 pCi/g EGDI 08/11/06 2043 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-11-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 69 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0002-01IF Project: YANKO 1204 Sample ID: 168404002 Client ID: YANKOOl Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 76 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 100 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 88 (25%-I125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (150/-125%/o)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25%-I125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 79 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 70 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Project: YANKO 1204 Sample ID: 168404003 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 25-APR-06 Receive Date: 05-MAY-06 Collector: Client Moisture: 23.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.027 +/-0.117 0.153 +/-0.117 0.488 pCi/g BXLI 08/13/06 0819 555696 1 Curium-242 U 0.112 +/-0.315 0.245 +1-0.315 0.781 pCi/g Curium-243/244 U 0.0217 +/-0.206 0.205 +/-0.206 0.594 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.061 +/-0.189 0.176 +/-0.189 0.449 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0551 +/-0.103 0.0584 +/-0.103 0.215 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 8.31 +/-5.73 4.40 +/-5.78 9.25 pCi/g BXLI 08/16/06 1253 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00343 +/-0.0203 0.0172 +/-0.0203 0.036 pCi/g BXF1 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.603 +/-8.25 6.87 +/-8.25 14.8 pCi/g DFA1 08/09/06 1159 554582 5 Liquid Scint C14, SolidAll,FSS Carbon-14 U 0.0937 +/-0.0813 0.0642 +/-0.0813 0.134 pCi/g ATH2 08/09/06 0529 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 7.68 +/-51.2 34.2 +/-51.2 70.4 pCi/g MXPI 08/12/06 1706 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 5.74 +/-7.12 6.58 +/-7.13 13.6 pCi/g MXPI 08/11/06 0912 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.0643 +/-0.198 0.169 +/-0.198 0.351 pCi/g EGD1 08/11/06 2059 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified Page 71 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Proiect: YANK01204 Sample ID: 168404003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-I, Modified 9 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 42 (15°/o- 125%/6)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 92 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 113 (25%-/125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 59 (25%/- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 71 (15%/.-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 83 (25%-I125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 76 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded Page 72 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-004F Project: YANKO 1204 Sample ID: 168404003 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd The above sample is reported on a dry weight basis.

Page 73 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Project: YANKO 1204 Sample ID: 168404004 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 25-APR-06 Receive Date: 05-MAY-06 Collector: Client Moisture: 22.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0456 +1-0.155 0.139 +1-0.155 0.387 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.113 +/-0.181 0.0733 +/-0.182 0.321 pCi/g Curium-243/244 U 0.180 +/-0.239 0.181 +/-0.240 0.472 pCi/g Alphaspec Pu, Solid-ALL FSS 0.118 Plutonium-238 U 0.0196 +/-0.121 +/-0.121 0.324 pCi/g. BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0326 +/-0.0639 0.00 +/-0.064 0.0884 pCi/g LiquidScint Pu241, Solid-ALL FSS Plutonium-241 U 6.63 +/-6.19 4.86 +/-6.22 10.2 pCi/g BXLI 08/16/06 1309 555698 3 Rad Gas Flow Proportional Counting GFPC,So9o, solid-ALL FSS Strontium-90 U 0.00477 +/-0.0216 0.0179 +/-0.0216 0.0375 pCi/g BXFI 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 1.03 +/-7.06 5.85 +/-7.06 12.6 pCi/g DFAI 08/09/06 1215 554582 5 Liquid Scint C14, Solid AllFSS Carbon-14 0.156 +/-0.0912 0.0699 +/-0.0913 0.146 pCi/g ATH2 08/09/06 0632 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -9.99 +/-42.7 28.7 +/-42.7 59.2 pCi/g MXP1 08/12/06 1722 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 0.939 +/-10.1 10.3 +/-10.1 21.6 pCi/g MXPI 08/11/06 1001 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.237 +/-0.213 0.170 +/-0.213 0.353 pCi/g EGD1 08/11/06 2115 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified Page 74 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Project: YANKO 1204 Sample ID: 168404004 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-I, Modified 9 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 78 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 94 (150/-1250/%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 101 (25%-/125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 58 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 75 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 62 (250/-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%/-125%/)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded Page 75 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0003-015F Project: YANKO 1204 Sample ID: 168404004 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd The above sample is reported on a dry weight basis.

Page 76 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005F Proiect: YANKO 1204 Sample ID: 168404005 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 15.4%

Parameter Qualifier Reesult Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0 .036 +/-0.123 0.157 +/-0.123 0.437 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0.10169 +/-0.033 0.080 +/-0.0331 0.350 pCi/g Curium-243/244 U -0.10129 +/-0.227 0.247 +/-0.227 0.619 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.10217 +/-0.163 0.181 +/-0.163 0.444 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/2 4 0 U -0.1 0708 +/-0.0791 0.128 +/-0.0795 0.337 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 9.52 +/-6.00 4.57 +/-6.07 9.61 pCi/g BXLI 08/16/06 1326 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.854 +/-5.88 4.87 +/-5.88 10.5 pCi/g DFAI 08/09/06 1231 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 0.347 +/-0.097 0.0674 +/-0.0972 0.141 pCi/g ATH2 08/09/06 0734 554583 5 Liquid Scint Fe55, Solid-ALL FSS lron-55 U - 1.57 +/-46.0 30.7 +/-46.0 63.2 pCi/g MXPI 08/12/06 1738 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 6.39 +/-7.62 7.40 +/-7.62 15.5 pCi/g MXPI 08/11/06 1017 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.( 0198 +/-0.187 0.156 +/-0.187 0.324 pCi/g EGDI 08/11/06 2131 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-1 I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 77 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-005F Project: YANKO 1204 Sample ID: 168404005 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 65 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 95 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 105 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 78 (15%-1 25%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 80 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 80 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier

• QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 78 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-015F Project: YANKO 1204 Sample ID: 168404006 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 03-MAY-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 26.5%

Parameter Qualifier Ri esult Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0. 0823 +/-0.203 0.178 +/-0.203 0.469 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0. 0154 +/-0.0301 0.0729 +/-0.0302 0.319 pCi/g Curium-243/244 U -0. 0994 +/-0.251 0.300 +/-0.251 0.713 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.0466 +/-0.213 0.210 +/-0.213 0.521 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U -0 1.142 +/-0.108 0.191 +/-0.109 0.483 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 6.64 +/-6.53 5.16 +/-6.57 10.8 pCi/g BXLI 08/16/06 1342 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U -2.9 +/-7.59 6.60 +/-7.59 14.2 pCi/g DFA I 08/09/06 1247 554582 4 Liquid Scint C14, SolidA/lFSS Carbon- 14 U 0.'0352 +/-0.0868 0.0713 +/-0.0868 0.149 pCi/g ATH2 08/09/06 0837 554583 5 Liquid Scint Fe55, Solid-ALL FSS lron-55 U 1.88 +/-46.8 31.3 +/-46.8 64.4 pCi/g MXPI 08/12/06 1754 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 3.88 +/-7.46 7.40 +/-7.46 15.5 pCi/g MXPI 08/11/06 1033 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.10894 +/-0.198 0.163 +/-0.198 0.338 pCi/g EGD1 08/11/06 2147 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-11-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 79 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0004-015F Project: YANKO 1204 Sample ID: 168404006 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 72 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 72 (15%-125/%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 94 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 73 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 80 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 78 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 80 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-01 OF Project: YANKO 1204 Sample ID: 168404007 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 56.2%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.128 +/-0.0939 0.142 +/-0.0942 0.385 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U - -0.0115 +/-0.128 0.147 +/-0.128 0.450 pCi/g Curium-243/244 U - -0.0333 +/-0.122 0.149 +/-0.122 0.401 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.0548 +/-0.169 0.158 +/-0.170 0.403 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U 0.0195 +/-0.121 0.117 +/-0.121 0.322 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 10.4 +/-6.89 5.27 +/-6.97 11.1 pCi/g BXL1 08/16/06 1358 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.00 +/-6.86 5.76 +/-6.86 12.4 pCi/g DFAI 08/09/06 1303 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.0636 +/-0.0801 0.0644 +/-0.0801 0.135 pCi/g ATH2 08/09/06 1017 554583 5 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 36.1 +/-44.1 28.7 +/-44.1 59.0 pCi/g MXPI 08/12/06 1811 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.26 +/-10.2 10.0 +/-10.2 20.9 pCi/g MXPI 08/11/06 1049 555723 7 Liquid Scint Tc99, Solid ALL FSS Technetium-99 U -0.05 +/-0.199 0.169 +/-0.199 0.351 pCi/g EGD1 08/11/06 2203 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 81 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-OIOF Project: YANKO 1204 Sample ID: 168404007 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 85 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 92 (25%- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 81 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 64 (25%-.125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 77 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 82 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-014F Proiect: YANKO 1204 Sample ID: 168404008 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 02-MAY-06 Receive Date: 09-MAY-06 Collector: Client Moisture: 32.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0(0591 +/-0.219 0.231 +/-0.219 0.608 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U - 0.04 +/-0.0554 0.134 +/-0.0557 0.494 pCi/g Curium-243/244 U 0.10634 +/-0.261 0.249 +/-0.261 0.646 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.1 0694 +/-0.106 0.160 +/-0.106 0.434 pCi/g BXL1 08/11/06 1633 555697 2 Plutonium-239/240 U -0.1 0287 +/-0.098 0.127 +/-0.0981 0.369 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 4.68 +/-8.01 6.48 +/-8.02 13.6 pCi/g BXLI 08/16/06 1415 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 6.02 +/-6.38 4.90 +/-6.38 10.6 pCi/g DFAI 08/09/06 1319 554582 4 LiquidScint C14, SolidAllFSS Carbon-14 U 0.10892 +/-0.0827 0.0655 +/-0.0827 0.137 pCi/g ATH2 08/09/06 1424 554583 5 Liquid Scint Fe55, Solid-ALL FSS lron-55 U 19.8 +/-46.3 30.6 +/-46.3 62.9 pCi/g MXPI 08/12/06 1827 555722 6 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 5.41 +/-7.91 7.77 +/-7.91 16.2 pCi/g MXPI 08/11/06 1106 555723 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0 .134 +/-0.192 0.167 +/-0.192 0.346 pCi/g EGDI 08/11/06 2218 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-11-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified Page 83 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0005-014F Project: YANKO 1204 Sample ID: 168404008 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 DOE RESL Fe-I, Modified 7 DOE RESL Ni-l, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 50 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 61 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL Fý 74 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 76 (15%-/I25%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 76 (25%-6125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 84 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005F Proiect: YANK01204 Sample ID: 168404009 Client ID: YANKOO I Matrix: SE Vol. Recv.:

Collect Date: 28-APR-06 Receive Date: 12-MAY-06 Collector: Client Moisture: 16.5%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0. 0851 +/-0.136 0.106 +/-0.136 0.390 pCi/g BXLI 08/16/06 0949 557837 1 Curium-242 U -0.' 0253 +/-0.0495 0.120 +/-0.0496 0.525 pCi/g Curium-243/244 U -0. 0479 +/-0.0542 0.131 +/-0.0545 0.443 pCi/g Alphaspec Pu, Solid-ALL FSS 0.303 Plutonium-238 U 0. 0183 +/-0.113 0.110 +/-0.113 pCi/g BXLI 08/11/06 1633 555697 3 Plutonium-239/240 U 0.010122 +/-0.0662 0.0694 +/-0.0662 0.221 pCi/g Liquid Scint Pu241, Solid ALL FSS Plutonium-241 U 4.43 +/-5.83 4.67 +/-5.85 9.82 pCi/g BXLI 08/16/06 1431 555698 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U - 2.02 +/-6.67 5.76 +/-6.67 12.4 pCi/g DFAl 08/09/06 1335 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 0'.142 +/-0.0798 0.061 +/-0.0799 0.127 pCi/g ATH2 08/09/06 1719 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 12.6 +/-47.6 31.7 +/-47.6 65.3 pCi/g MXPI 08/12/06 1843 555722 7 Liquid Scint Ni63, Solid-ALL FSS Nickel-63 U 7.70 +/-9.56 9.31 +/-9.56 19.5 pCi/g MXPI 08/11/06 1122 555723 8 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U -0.0( 0659 +/-0.185 0.156 +/-0.185 0.323 pCi/g EGDI 08/11/062234 554580 9 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-I 1-RC Modified 4 DOE EML HASL-300, Pu-I I-RC Modified 5 EPA 906.0 Modified Page 85 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0006-005F Project: YANKO 1204 Sample ID: 168404009 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE RESL Ni-I, Modified 9 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 76 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 93 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 105 (25%-.125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15%-/125%)

Carrier/Tracer Recovery Liquid Scint Ni63, Solid-ALL FS 64 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 81 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 86 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006F Project: YANKO 1204 Sample ID: 168404010 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 05-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 34.8%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U I +/-0.195 0.0758 +/-0.196 0.332 pCi/g BXLI 08/16/06 0949 557837 1 Curium-242 U I +/-0.202 0.00 +/-0.203 0.280 pCi/g Curium-243/244 U -0. +/-0.0316 0.0766 +/-0.0317 0.335 pCi/g Alphaspec Pu, Solid-ALL FSS pCi/g Plutonium-238 U -0. +/-0.0711 0.0967 +/-0.0712 0.275 BXLI 08/11/06 1633 555697 3 Plutonium-239/240 U 0.0 +/-0.113 0.118 +/-0.113 0.317 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 14.9 +/-6.37 4.64 +/-6.51 9.75 pCi/g BXLI 08/16/06 1447 555698 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.00 +/-6.06 5.09 +/-6.06 10.7 pCi/g DFAI 08/10/06 2150 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 U ).107 +/-0.0846 0.0664 +/-0.0846 0.139 pCi/g ATH2 08/09/06 1822 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 15.1 +/-41.4 27.5 +/-41.4 56.6 pCi/g MXPI 08/12/06 1900 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U ).258 +/-0.225 0.179 +/-0.225 0.373 pCi/g EGDI 08/11/06 2251 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Am-05-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 DOE EML HASL-300, Pu-I I-RC Modified 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified Page 87 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-006F Project: YANK01204 Sample ID: 168404010 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 77 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 94 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 103 (25%-6125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 72 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 71 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

Ul Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 88 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-008F Project: YANK01204 Sample ID: 168404011 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 08-MAY-06 Receive Date: 26-MAY-06 Collector: Client Moisture: 35.7%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0. +/-0.192 0.152 +/-0.193 0.426 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0. +/-0.142 0.132 +/-0.142 0.446 pCi/g Curium-243/244 U -0. +/-0.202 0.240 +/-0.203 0.603 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0. +/-0.096 0.125 +/-0.096 0.328 pCi/g BXLI 08/11/06 1633 555697 2 Plutonium-239/240 U -0. +/-0.114 0.137 +/-0.114 0.353 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 11.5 +/-6.72 5.08 +/-6.80 10.7 pCi/g BXLI 08/16/06 1504 555698 3 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.00 +/-5.92 4.97 +/-5.92 10.7 pCi/g DFAI 08/09/06 1407 554582 4 Liquid Scint C14, SolidAllFSS Carbon-14 U -0. 0238 +/-0.0745 0.0636 +/-0.0745 0.133 pCi/g ATH2 08/09/06 1924 554583 5 Liquid Scint Fe55, Solid-ALL FSS lron-55 U - -10.7 +/-40.9 27.5 +/-40.9 56.8 pCi/g MXPI 08/12/06 1916 555722 6 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0. 0956 +/-0.211 0.174 +/-0.211 0.361 pCi/g EGDI 08/11/06 2307 554580 7 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-1 I-RC Modified 3 DOE EML HASL-300, Pu-I 1-RC Modified 4 EPA 906.0 Modified 5 EPA EERF C-01 Modified 6 DOE,RESL Fe-I, Modified Page 89 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0008-008F Project: YANKO 1204 Sample ID: 168404011 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 7 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALl 65 (15%/-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 98 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 96 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 76 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 74 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 90 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Connecticut Yankee Atomic Power Address 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-002F Project: YANKO 1204 Sample ID: 168404012 Client ID: YANK001 Matrix: SE Vol. Recv.:

Collect Date: 11-MAY-06 Receive Date: 08-JUN-06 Collector: Client Moisture: 33%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U -0.00144 +1-0.155 0.166 +/-0.155 0.458 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.0192 +/-0.145 0.135 +/-0.145 0.455 pCi/g Curium-243/244 U 0.013 +/-0.268 0.281 +/-0.268 0.687 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.00587 +/-0.0493 0.0279 +/-0.0494 0.122 pCi/g BXLI 08/11/06 1632 555697 2 Plutonium-239/240 U 0.0186 +/-0.0492 0.0278 +/-0.0493 0.122 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 13.6 +/-6.90 5.13 +/-7.01 10.8 pCi/g BXLI 08/16/06 1520 555698 3 Rad Gas Flow Proportional Counting GFPC,So9o, solid-ALL FSS Strontium-90 U 0.0151 +/-0.0146 0.0114 +/-0.0146 0.0242 pCi/g BXF1 08/14/06 0834 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 4.12 +/-8.36 6.70 +/-8.36 14.5 pCi/g DFA1 08/09/06 1422 554582 5 Liquid Scint C14, Solid A/lFSS Carbon-14 U 0.046 +/-0.0755 0.0613 +/-0.0755 0.128 pCi/g ATH2 08/09/06 2027 554583 6 Liquid Scint Fe55, Solid ALL FSS Iron-55 U 12.9 +/-40.6 26.8 +/-40.6 55.2 pCi/g MXPI 08/12/06 1932 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.078 +/-0.203 0.168 +/-0.203 0.348 pCi/g EGD1 08/11/06 2323 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified Page 91 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-002F Project: YANKO 1204 Sample ID: 168404012 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 61 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 98 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL F5 94 (25%- 125%o)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 69 (25%-/125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 81 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or.Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 92 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-017F Proiect: YANKO 1204 Sample ID: 168404013 Client ID: YANKOO Matrix: SE Vol. Recv.:

Collect Date: 15-MAY-06 Receive Date: 08-JUN-06 Collector: Client Moisture: 28.4%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.0755 +/-0.242 0.230 +/-0.243 0.574 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.0957 +/-0.220 0.171 +/-0.220 0.509 pCi/g Curium-243/244 U -0.073 +/-0.214 0.256 +/-0.214 0.627 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U -0.00629 +/-0.0529 0.0299 +/-0.0529 0.131 pCi/g BXLI 08/11/06 1632 555697 2 Plutonium-239/240 U 0.0262 +/-0.0513 0.00 +/-0.0514 0.0709 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 13.3 +/-6.66 4.95 +/-6.77 10.4 pCi/g BXLI 08/16/06 1536 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U 0.0205 +1-0.0151 0.0116 +/-0.0151 0.0246 pCi/g BXF1 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.583 +/-7.98 6.65 +/-7.98 14.4 pCi/g DFA I 08/09/06 1438 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.0271 +/-0.0759 0.0625 +/-0.0759 0.131 pCi/g ATH2 08/09/06 2129 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -61.9 +/-150 102 +/-150 210 pCi/g MXPI 08/12/06 1949 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.0628 +/-0.200 0.165 +/-0.200 0.343 pCi/g EGDI 08/11/06 2338 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu- 11-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified Page 93 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0009-017F Project: YANK01204 Sample ID: 168404013 Client ID: YANK001 Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 64 (15%-/125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 96 (25%-125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 72 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 73 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 79 (15%- 125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 94 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-00IF Proiect: YANKO 1204 Sample ID: 168404014 Client ID: YANKOOI Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 17-MAY-06 Collector: Client Moisture: 27.3%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.00677 +/-0.227 0.238 +/-0.227 0.628 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U 0.0854 +/-0.167 0.00 +/-0.168 0.231 pCi/g Curium-243/244 U 0.0361 +/-0.242 0.241 +/-0.242 0.634 pCi/g Alphaspec Pu, Solid-ALL FSS Plutonium-238 U 0.173 +/-0.181 0.143 +/-0.182 0.331 pCi/g BXLI 08/11/06 2250 555697 2 Plutonium-239/240 U -0.0342 +/-0.0865 0.0951 +/-0.0866 0.235 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 13.0 +/-6.44 4.78 +/-6.54 10.0 pCi/g BXLI 08/16/06 1553 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.0128 +/-0.0141 0.0125 +/-0.0141 0.0262 pCi/g BXFI 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.548 +/-7.50 6.25 +/-7.50 13.5 pCi/g DFAI 08/09/06 1454 554582 5 Liquid Scint C14, SolidAllFSS Carbon-14 U 0.0555 +/-0.0809 0.0655 +/-0.0809 0.137 pCi/g ATH2 08/09/06 2232 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U -18.1 +/-47.6 32.3 +/-47.6 66.6 pCi/g MXPI 08/12/06 2005 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.134 +/-0.205 0.167 +/-0.205 0.347 pCi/g EGDI 08/11/06 2354 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description 1 DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I I-RC Modified 3 DOE EML HASL-300, Pu-I I-RC Modified 4 EPA 905.0 Modified Page 95 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-00IF Project: YANK01204 Sample ID: 168404014 Client ID: YANKOOI Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-1, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Test Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 50 (15%-0125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 85 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241 Solid-ALL Fý 99 (25%-125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 74 (25%-125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 70 (15%- 125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15°/o- 125%)

Notes:

The Qualifiers in this report are defined as follows

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 96 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-012F Proiect: YANKO 1204 Sample ID: 168404015 Client ID: YANKOOl Matrix: SE Vol. Recv.:

Collect Date: 04-MAY-06 Receive Date: 17-MAY-06 Collector: Client Moisture: 28.1%

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd Rad Alpha Spec Analysis Alphaspec Am241, Cm, Solid ALL FSS Americium-241 U 0.110 +/-0.184 0.140 +/-0.184 0.386 pCi/g BXLI 08/11/06 1434 555696 1 Curium-242 U -0.0547 +/-0.141 0.192 +/-0.141 0.544 pCi/g Curium-243/244 U -0.126 +/-0.184 0.245 +/-0.185 0.597 pCi/g Alphaspec Pu, Solid-ALL FSS 0.122 Plutonium-238 U -0.00157 +/-0.126 +/-0.126 0.291 pCi/g BXLI 08/11/06 2250 555697 2 Plutonium-239/240 U 0.0867 +/-0.0869 0.0406 +/-0.0872 0.128 pCi/g Liquid Scint Pu241, Solid-ALL FSS Plutonium-241 U 8.31 +/-6.16 4.77 +/-6.21 10.0 pCi/g BXLI 08/16/06 1609 555698 3 Rad Gas Flow Proportional Counting GFPC,Sr90, solid-ALL FSS Strontium-90 U -0.00771 +/-0.0144 0.0124 +/-0.0144 0.0263 pCi/g BXFI 08/14/06 0833 556350 4 Rad Liquid Scintillation Analysis LSC, Tritium Dist, Solid-HTD2,ALL FSS Tritium U 0.896 +/-6.17 5.11 +/-6.17 11.0 pCi/g DFA I 08/09/06 1510 554582 5 Liquid Scint C14, Solid AllFSS Carbon-14 U 0.0162 +/-0.0763 0.0633 +/-0.0763 0.132 pCi/g ATH2 08/09/06 2334 554583 6 Liquid Scint Fe55, Solid-ALL FSS Iron-55 U 23.3 +/-49.3 32.5 +/-49.3 67.0 pCi/g MXPI 08/12/06 2021 555722 7 Liquid Scint Tc99, Solid-ALL FSS Technetium-99 U 0.0577 +/-0.206 0.171 +/-0.206 0.354 pCi/g EGDI 08/12/06 0010 554580 8 The following Prep Methods were performed Method Description Analyst Date Time Prep Batch Dry Soil Prep Dry Soil Prep GL-RAD-A-021 LXM2 08/03/06 1534 554649 The following Analytical Methods were performed Method Description I DOE EML HASL-300, Am-05-RC Modified 2 DOE EML HASL-300, Pu-I 1-RC Modified 3 DOE EML HASL-300, Pu-I 1-RC Modified 4 EPA 905.0 Modified Page 97 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Connecticut Yankee Atomic Power Address : 362 Injun Hollow Rd East Hampton, Connecticut 06424 Report Date: August 21, 2006

Contact:

Mr. Jack McCarthy Project: Soils PO# 002332 Client Sample ID: 9106-0010-012F Project: YANKO 1204 Sample ID: 168404015 Client ID: YANKOO Vol. Recv.:

Parameter Qualifier Result Uncertainty LC TPU MDA Units DF Analyst Date Time Batch Mtd 5 EPA 906.0 Modified 6 EPA EERF C-01 Modified 7 DOE RESL Fe-I, Modified 8 DOE EML HASL-300, Tc-02-RC Modified Surrogate/Tracer recovery Recovery% Acceptable Limits Americium-243 Alphaspec Am241, Cm, Solid ALL 81 (15%-125%)

Plutonium-242 Alphaspec Pu, Solid-ALL FSS 91 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Pu241, Solid-ALL FS 99 (25%-125%)

Carrier/Tracer Recovery GFPC, Sr90, solid-ALL FSS 68 (25%- 125%)

Carrier/Tracer Recovery Liquid Scint Fe55, Solid-ALL FS 74 (15%-125%)

Carrier/Tracer Recovery Liquid Scint Tc99, Solid-ALL FS 75 (15%-125%)

Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported

> Result is greater than value reported A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded The above sample is reported on a dry weight basis.

Page 98 of 105

I.

QUALITY CONTROL DATA Page 99 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: August 21, 2006 Client : Connecticut Yankee Atomic Power Page 1 of 6 362 Injun Hollow Rd East Hampton, Connecticut

Contact:

Mr. Jack McCarthy Workorder: 168404 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time Rad Alpha Spec Batch 555696 QC1201153130 168340011 DUP Americium-241 U -0.000522 U 0.0578 pCi/g 204 (0%- 100%) BXLI 08/11/06 14:34 Uncert: +/-0.0385 +/-0.278 TPU: +/-0.0385 +/-0.279 Curium-242 U 0.00 U -0.0405 pCi/g 200 (0%- 100%)

Uncert: +/-0.0756 +/-0.0562 TPU: +/-0.0756 +/-0.0565 Curium-243/244 U -0.0177 U -0.0517 pCi/g 98 (0%- 100%)

Uncert: +/-0.0764 +/-0.257 TPU: +/-0.0765 +/-0.257 QCI201153132 LCS Americium-241 12.8 12.8 pCi/g 100 (75%-125%)

Uncert: +/-1.84 TPU: +/-2.70 Curium-242 U -0.0328 pCi/g Uncert: +/-0.0454 TPU: +/-0.0457 Curium-243/244 15.5 14.3 pCi/g 92 (75%-125%)

Uncert: +/-1.94 TPU: +/-2.92 QC1201153129 MB Americium-241 U 0.0471 pCi/g Uncert: +/-0.157 TPU: +/-0.157 Curium-242 U -0.0469 pCi/g Uncert: +/-0.0459 TPU: +/-0.0464 Curium-243/244 U -0.00385 pCi/g Uncert: +/-0.210 TPU: +/-0.210 QC1201153131 168340011 MS Americium-241 13.3 U -0.000522 12.0 pCi/g 91 (75%-125%)

Uncert: +/-0.0385 +/-1.38 TPU: +/-0.0385 +/-2.08 Curium-242 U 0.00 U 0.0427 pCi/g Uncert: +/-0.0756 +/-0.0837 TPU: +/-0.0756 +/-0.0839 Curium-243/244 16.1 U -0.0177 15.9 pCi/g 99 (75%-125%)

Uncert: +/-0.0764 +/-1.58 TPU: +/-0.0765 +/-2.61 Batch 555697 QC1201153134 168340011 DUP Plutonium-238 U -0.0155 U 0.0237 pCi/g 956 (0%- 100%) BXLI 08/11/06 22:51 Page 100 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 2 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 555697 Uncert: +/-0.0215 +/-0.0465 TPU: +/-0.0216 +/-0.0466 Plutoniurn-239/240 U 0.0414 U -0.0489 pCi/g 2410 (0%- 100%)

Uncert: +/-0.0934 +/-0.124 TPU: +/-0.0935 +/-0.124 QC1201153136 LCS Plutonium-238 U 0.155 pCi/g (75%- 125%)

Uncert: +/-0.141 TPU: +/-0.142 Plutonium-239/240 11.8 11.5 pCi/g 98 (75%-125%)

Uncert: +/-0.856 TPU: +/-1.32 QC 1201153133 MB Plutonium-238 U 0.0552 pCi/g 08/11/06 22:50 Uncert: +/-0.186 TPU: +/-0.186 Plutonium-239/240 U -0.0978 pCi/g Uncert: +/-0.0892 TPU: +/-0.0899 QC1201153135 168340011 MS Plutonium-238 U -0.0155 U 0.0539 pCi/g (75%-125%) 08/11/06 22:51 Uncert: +/-0.0215 +/-0.112 TPU: +/-0.0216 +/-0.112 Plutoniumn-239/240 12.3 u 0.0414 10.3 pCi/g 84 (75%-125%)

Uncert: +/-0.0934 +/-0.796 TPU: +/-0.0935 +/-1.19 Batch 555698 QC1201153138 168340011 DUP Plutonium-241 U 7.28 U 10.1 pCi/g 0 (0% - 100%) BXLI 08/16/06 16:41 Uncert: +/-6.30 +/-6.39 TPU: +/-6.35 +/-6.46 QCI201153140 LCS Plutonium-241 137 145 pCi/g 106 (75%-125%) 08/16/06 17:14 Uncert: +/-12.5 TPU: +/-19.9 QC1201153137 MB Plutonium-241 U 8.57 pCi/g 08/16/06 16:25 Uncert: +/-6.93 TPU: +/-6.98 QC1201153139 168340011 MS Plutonium-241 138 U 7.28 142 pCi/g 103 (75%-125%) 08/16/06 16:58 Uncert: +/-6.30 +/-12.4 TPU: +/-6.35 +/-19.7 Batch 557837 QC1201158317 168404009 DUP Americium-241 U -0.0851 U 0.167 pCi/g 616 (0%- 100%) BXLI 08/16/06 09:49 Uncen: +/-0.136 +/-0.220 TPU: +/-0.136 +/-0.221 Curium-242 U -0.0253 U 0.241 pCi/g 247 (0%- 100%)

Page 101 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 3 of 6 Parmname NOM Samnle Oual QC Units RPD% REC% Range Anist Date Time Rad Alpha Spec Batch 557837 Uncert: +/-0.0495 +/-0.334 TPU: +/-0.0496 +/-0.335 Curium-243/244 U -0.0479 U 0.0761 pCi/g 879 (0%- 100%)

Uncert: +/-0.0542 +/-0.149 TPU: +/-0.0545 +/-0.149 QC1201158319 LCS Americium-241 24.5 25.4 pCi/g 104 (75%-125%)

Uncert: +/-2.47 TPU: +/-4.16 Curium-242 U 0.0477 pCi/g Uncert: +/-0.127 TPU: +/-0.127 Curium-243/244 29.7 27.0 pCi/g 91 (75%-125%)

Uncert: +/-2.54 TPU: +/-4.38 QC1201158316 MB Americium-241 U 0.234 pCi/g Uncert: +/-0.275 TPU: +/-0.277 Curium-242 U 0.00 pCi/g Uncert: +/-0.152 TPU: +/-0.152 Curium-243/244 U -0.0551 pCi/g Uncert: +/-0.0624 TPU: +/-0.0628 QC1201158318 168404009 MS Americium-241 26.4 U -0.0851 29.1 pCi/g 110 (75%-125%)

Uncerl: +/-0.136 +/-2.97 TPU: +/-0.136 +/-5.01 Curium-242 U -0.0253 U 0.126 pCi/g Uncert: +/-0.0495 +/-0.247 TPU: +/-0.0496 +/-0.248 Curium-243/244 32.4 U -0.0479 31.7 pCi/g 98 (75%-125%)

Uncert: +/-0.0542 +/-3.12 TPU: +/-0.0545 +/-5.39 Rad Gas Flow Batch 556350 QC1201154645 168404003 DUP Strontium-90 U -0.00343 U -0.00637 pCi/g 0 (0% - 100%) BXFI 08/14/06 08:33 Uncert: +/-0.0203 +/-0.0152 TPU: +/-0.0203 +/-0.0152 QC1201154647 LCS Strontium-90 1.56 1.30 pCi/g 83 (75%-125%)

Uncert: +/-0.0563 TPU: +/-0.088 I QC1201154644 MB Strontium-90 U 0.0176 pCi/g Uncert: +/-0.018 TPU: +/-0.018 Page 102 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 4 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range AnIst Date Time Rad Gas Flow Batch 556350 QC1201154646 168404003 MS Strontium-90 1.58 U -0.00343 1.29 pCi/g 82 (75%-125%)

Uncert: +/-0.0203 +/-0.0535 TPU: +/-0.0203 +/-0.0813 Rad Liquid Scintillation Batch 554580 QC1201150562 168340012 DUP Technetium-99 U 0.0338 U 0.266 pCi/g 0 (0% - 100%) EGDI 08/12/06 00:42 Uncert: +/-0.192 +/-0.226 TPU: +/-0.192 +/-0.226 QC1201150564 LCS Technetium-99 13.1 13.6 pCi/g 103 (75%-125%) 08/12/06 01:14 Uncert: +/-0.496 TPU: +/-0.599 QCI201150561 MB Technetium-99 U 0.0311 pCi/g 08/12/06 00:26 Uncert: +/-0.177 TPU: +/-0.177 QC1201150563 168340012 MS Technetium-99 13.0 U 0.0338 12.0 pCilg 92 (75%-125%) 08/12/06 00:58 Uncert: +/-0.192 +/-0.523 TPU: +/-0.192 +/-0.602 Batch 554582 QC1201150570 168340011 DUP Tritium U 1.77 U 1.62 pCi/g 0 (0% - 100%) DFA I 08/09/06 15:42 Uncert: +/-8.20 +/-7.47 TPU: +/-8.20 +/-7.47 QC1201150572 LCS Tritium 68.3 76.2 pCilg Il1 (75%-125%) 08/09/06 16:14 Uncert: +/-14.0 TPU: +/-14.1 QC1201150569 MB Tritium U 0.586 pCilg 08/09/06 15:26 Uncert: +/-8.01 TPU: +/-8.01 QC1201150571 168340011 MS Tritium 61.3 U 1.77 61.8 pCi/g 101 (75%-125%) 08/09/06 15:58 Uncert: +/-8.20 +/-12.2 TPU: +/-8.20 +/-12.3 Batch 554583 QC1201150574 168404003 DUP Carbon- 14 U 0.0937 U 0.0422 pCi/g 0 (0% - 100%) ATH2 08/10/06 01:39 Uncert: +/-0.0813 +/-0.075 TPU: +/-0.0813 +/-0.0751 QC1201150576 LCS Carbon- 14 7.27 7.14 pCi/g 98 (75%-125%) 08/10/06 03:00 Uncert: +/-0.508 TPU: +/-0.520 QC1201150573 MB Page 103 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 5 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time Rad Liquid Scintillation Batch 554583 Carbon- 14 U -0.0315 pCi/g Uncert: +/-0.0776 TPU +/-0.0776 QC1201150575 168404003 MS Carbon-14 15.1 U 0.0937 13.8 pCi/g 92 (75%-125%) 08/10/06 02:43 Uncert: +/-0.0813 +/-1.00 TPU +/-0.0813 +/-1.03 Batch 555722 QC1201153223 168340012 DUP lron-55 U -26.5 U 5.83 pCi/g (0%- 100%) vIxPI 08/12/06 20:54 Uncert: +/-65.1 +/-36.9 TPU +/-65.1 +/-36.9 QC1201153225 LCS Iron-55 641 660 pCi/g 103 (75%-125%) 08/12/06 21:27 Uncert: +/-56.2 TPU +/-67.2 QC1201153222 MB Iron-55 U 18.2 pCi/g 08/12/06 20:38 Uncert: +/-39.6 TPU +/-39.6 QC1201153224 168340012 MS Iron-55 717 U -26.5 688 pCi/g 96 (75%-125%) 08/12/06 21:11 Uncert: +/-65.1 +/-60.2 TPU +/-65.1 +/-71.6 Batch 555723 QC1201153227 168340012 DUP Nickel-63 U 3.79 U 6.68 pCi/g 0 (0% - 100%) viXPI 08/11/06 11:55 Uncert: +/-5.39 +/-7.43 TPU: +/-5.40 +/-7.43 QC1201153229 LCS Nickel-63 512 479 pCi/g 94 (75%-125%) 08/11/06 12:27 Uncert: +/ -22.4 TPU: +/--27.1 QC1201153226 MB Nickel-63 U 15.7 pCi/g 08/11/06 11:38 Uncert: +/- 9.92 TPU: +/--9.93 QC1201153228 168340012 MS Nickel-63 530 U 3.79 511 pCi/g 96 (75%-125%) 08/11/06 12:11 Uncert: +/-5.39 +/- 23.5 TPU: +/-5.40 +/- 28.7 Notes:

The Qualifiers in this report are defined as follows:

• A quality control analyte recovery is outside of specified acceptance criteria

< Result is less than value reported Result is greater than value reported Page 104 of 105

GENERAL ENGINEERING LABORATORIES, LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 168404 Page 6 of 6 Parmname NOM Sample Qual QC Units RPD% REC% Range Anist Date Time A The TIC is a suspected aldol-condensation product B Target analyte was detected in the associated blank BD Results are either below the MDC or tracer recovery is low C Analyte has been confirmed by GC/MS analysis D Results are reported from a diluted aliquot of the sample H Analytical holding time was exceeded J Value is estimated N/A Spike recovery limits do not apply. Sample concentration exceeds spike concentration by 4X or more R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.

UI Gamma Spectroscopy--Uncertain identification X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Y QC Samples were not spiked with this compound A RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more.

• • Indicates analyte is a surrogate compound.

^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptence criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result.

For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.

Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary.

Page 105 of 105

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Attachment 2b Split Sample Assessment Forms (2 Pages)

Connecticut Yankee Decommissioning Project Health 24265-000-GPR-GGGR-R5124-000 Attachment A Physics Procedure Split Sample Assessment Form Survey Area Survey 0008 Survey Discharge Canal

1. 9106 Unit #: Unit Name:

Sample Plan or WPIR#: 2006-021 SML #: 9106-0008-006 Sample

Description:

Comparison of split samples collected from sample measurement location #03 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The standard sample was 9106-0008-006F the comparison sample was 9106-0008-006FS.

STANDARD COMPARISON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable (Y/N)

Value Error Range Value Error Ratio Cs-137 4.92E-01 3.63E-02 14 0.6- 1.66 6.01E-01 5.OOE-02 1.22 Y Co-60 7.79E-01 4.90E-02 16 0.75 - 1.33 1.34E+00 7.OOE-02 1.72 N Sr-90 5.59E-03 6.50E-03 I NONE- 8.75E-04 7.05E-03 0.16 N/A Ni-63 2.28E+00 5.05E+00 0 NONE 1.88E-01 3.05E+00 0.08 N/A K-40 1.37E+01 6.85E-01 20 0.75- 1.33 1.49E+01 7.45E-01 1.09 Y tomments/Correcuve -ActI1os: In consileratlon o1 ,Mr-J0 m, I,4 I able is provideu to snow acceptance criteria used 63 results, guidance for agreement ranges, obtained from to assess split samples.

USNRC Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of Resolution I Agreement Range acceptability for such rations cannot be made. Co-60 has a 4 7 0.50 2.00 likelyhood to be present in the sample matrix in particulate 8 15 0.60 1.66 form, one would not neccassarily expect it to be homogenuously 16 50 0.75 1.33 mixed from processing of the sample-split aliqot. Since Cs-137 51 200 0.80 1.25 and K-40 were found to be present at an acceptable levels of

> 200 0.85 1.18 agreement, no further action is warranted.

Performed By:

WPIR - Work Plan and Inspection Record SML - Sample Measurement Location designation Page I of I

Connecticut Yankee Decommissioning Project Health 24265-000-GPR-GGGR-R5124-000 Attachment A Physics Procedure Split Sample Assessment Form Survey 9106 Survey 0008 Survey Unit Dis Area#: Unit #: Name: charge Canal Sample Plan or WPIR#: 2006-0021 SML #: 9106-0008-010 Sample

Description:

Comparison of split samples collected from sample measurement location #10 and analyzed using gamma spectroscopy by an off-site vendor laboratory. The standard sample was 9106-0008-01OF the comparison sample was 9106-0008-01 OFS.

STANDARD COMPARI SON Radionuclide Activity Standard Resolution Agreement Activity Standard Comparison Acceptable Value Error Range Value Error Ratio (Y/N)

Cs-137 3.36E-01 3.45E-02 10 0.6- 1.66 3.02E-01 2.87E-02 0.90 Y Co-60 2.46E-01 2.51E-02 10 0.6- 1.66 3.28E-01 2.96E-02 1.33 Y Sr-90 3.47E-03 6.05E-03 I NONE 8.59E-03 8.50E-03 2.48 N/A Ni-63 1.23E-01 2.99E+00 0 NONE -1.63E+00 3.35E+00 -13.25 N/A K-40 1.37E+01 6.85E-01 20 0.75 1.33 1.49E+0I 7.45E-01 1.09 Y Comments/Corrective Actions: In consideration of Sr-90 & Ni- Table is provided to show acceptance criteria 63 results, guidance for agreement ranges, obtained from used to assess split samples.

USNRC Inspection Procedure 84750, does not address resolution ratios less than 4, therefore, a determination of Resolution Agreement Range acceptability for such rations cannot be made. Since Cs-137, Co 4 7 0.50 2.00 60 and K-40 were found to be present at an acceptable levels of 8 15 0.60 1.66 agreement, no further action is warranted. 16 50 0.75 1.33 51 200 0.80 1.25

> 200 0.85 1.18 Performed By:

WPIR - Work Plan and Inspection Record SML - Sample Measurement Location designation Page I of I

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Attachment 2c Preliminary Data Form (1 Page)

Health Physics Procedure GPP-GGGR-R5121-001 Attachment B, Rev. CY-001 MAJOR Preliminary Data Review Form - Samples for the Sign Test Survey Unit: 9106- 0008 Survey Unit Name: Discharge Canal Classification: 2 Survey Media: Soil Type of Survey: Final Status Survey Type of Measurement: Radionuclide Specific Number of Measurements: 14 Operational DCGL: 1 BASIC STATISTICAL QUANTITIES Cs-137 Co-60 Sr-90 Ni-63 Minimum Value: -8.91E-03 -1.45E-02 -1.92E-02 -4.84E+00 Maximum Value: 4.92E-01 9.17E-01 2.03E-02 2.28E+00 Mean: 1.78E-01 1.98E-01 3.34E-03 -1.38E+00 Median: 1.26E-01 7.60E-02 4.44E-03 -1.76E+00 Standard Deviation: 1.85E-01 2.95E-01 1.04E-02 1.87E+00 RADIONUCLIDE CONCENTRATION (pCi/g)

NUMBER Cs-137 Co-60 Sr-90 Ni-63 9106-0008-001 F 3.96E-01 1.33E-01 5.79E-03 2.33E-01 9106-0008-002F -8.91 E-03 7.77E-03 2.03E-02 -4.84E+00 9106-0008-003F 2.05E-01 3.24E-01 1.12E-02 -2.74E+00 9106-0008-004F 4.32E-02 O.OOE+00 -6.19E-03 -1.80E+00 9106-0008-005F 2.66E-01 2.75E-02 8.28E-04 -8.58E-01 9106-0008-006F 4.92E-01 7.79E-01 5.59E-03 2.28E+00 9106-0008-007F 2.29E-02 2.68E-02 -8.81 E-04 -2.33E+00 9106-0008-008F 4.72E-01 9.17E-01 -2.69E-03 -4.12E-01 9106-0008-009F 1.55E-02 -1.08E-02 -5.90E-03 -2.05E+00 9106-0008-01OF 3.36E-01 2.46E-01 3.47E-03 1.23E-01 9106-0008-011 F 6.76E-02 1.22E-01 1.93E-02 -3.34E+00 9106-0008-012F 1.84E-01 1.79E-01 -1.92E-02 8.39E-01 9106-0008-013F 1.03E-02 2.99E-02 9.80E-03 -2.70E+00 9106-0008-014F -3.89E-03 -1.45E-02 5.40E-03 -1.72E+00 Performed By: A' Date: 10o-31-0o4 Independent Review: Date: 0// /Oz-J ar

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Attachment 2d Graphical Representation of Data (8 Pages)

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Health Physics Procedure GGGR-R5123-Rev.CY-OO1 Attachment C Quantile Plot For Cesium - 137 Survey Unit: 9106-0008 Survey Unit Name: Discharge Canal Mean: 1.78E-01 pCi/g 6.OOE-01 5.OOE-01 " -

O0. 4.OOE-01 - , --

0 3.OOE-01 .

2.OOE-01

= 1.OOE-01 0

) O.OOE+00 - - - __ "

-1.OOE-01 2'"2 40 60 8 '1 Percentage Cs-1 37 Rank Percentage

-8.91 E-03 1 4 %

-3.89E-03 2 11 %

1.03E-02 3 18 %

1.55E-02 4 25  %

2.29E-02 5 32  %

4.32E-02 6 39 %

6.76E-02 7 46 %

1.84E-01 8 54 %

2.05E-01 9 61 %

2.66E-01 10 68 %

3.36E-01 11 75 %

3.96E-01 12 82 %

4.72E-01 13 89 %

4.92E-01 14 96 %

Prepared By: Date: 31-0 1 Reviewed By: Date: //6"

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Health Physics Procedure GGGR-R5 123-Rev.CY-001 Attachment C Quantile Plot For Cobalt - 60 Survey Unit: 9106-0008 Survey Unit Name: Discharge Canal Mean: 1.98E-01 pCi/g 1.OOE+00-

,_ 8.OOE-01 -

E 6.OOE-01 0

4.00E-01 2.OOE-01

• 0 0.OOE+00 - -,2_ _- -----

20 4 60 80

-2.PcE-01en Percentage Co-60 Rank Percentage

-1.45E-02 1 .4 %

-1.08E-02 2 11 %

O.OOE+00 3 18 %

7.77E-03 4 25 %

2.68E-02 5 32 %

2.75E-02 6 39 %

2.99E-02 7 46 %

1.22E-01 8 54 %

1.33E-01 9 61 %

1.79E-01 10 68 %

2.46E-01 11 75 %

3.24E-01 12 82 %

7.79E-01 13 89 %

9.17E-01 14 96 %

Prepared By: Date:

Reviewed By: 4~4b Date: /1111/ 61K

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Health Physics Procedure GGGR-R5123-Rev.CY-0O1 Attachment C Quantile Plot For Strontium - 90 Survey Unit: 9106-0008 Survey Unit Name: Discharge Canal Mean: 3.34E-03 pCi/g 2.50E-02 2.OOE-02 -- -

1.50E-02

'.) 1.OOE-02 _ -

0.

r-5.00E-03 -,*

• 0 0.0OE+00 ---

-5.OOE-03 - -0 ;L0 -0 --- 0

~-1.00E-02_

0 C3-1.50E -2.OOE-02 -

-2.50E-02 Percentage Sr-90 Rank Percentage

-1.92E-02 1 4 %

-6.19E-03 2 11 %

-5.90E-03 3 18 %

-2.69E-03 4 25 %

-8.81 E-04 5 32 %

8.28E-04 6 39 %

3.47E-03 7 46 %

5.40E-03 8 54 %

5.59E-03 9 61 %

5.79E-03 10 68 %

9.80E-03 11 75 %

1.12E-02 12 82 %

1.93E-02 13 89 %

2.03E-02 14 96 %

Prepared By: Date:

Reviewed By: Date: /1 / :

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Quantile Plot For Nickel - 63 Survey Unit: 9106-0008 Survey Unit Name: Discharge Canal Mean: -1.38E+00 pCi/g 2.50E-02 2.OOE-02 --

1.50E-02

-1.OOE-02 C.

r- 5.OOE-03 O.OOE+02 -

4)

S-5.OOE-03 T~0 - T -@ -40 S-1.OOE-02 - _---

0 0 -1.50E-02 -- - - -- - - -_- -

-2.OOE-02 - _-__ _

-2.50E-02 Percentage Ni-63 Rank Percentage

-4.84E+00 1 4 %

-3.34E+00 2 11 %

-2.74E+00 3 18 %

-2.70E+00 4 25 %

-2.33E+00 5 32 %

-2.05E+00 6 39 %

-1.80E+00 7 46 %

-1.72E+00 8 54 %

-8.58E-01 9 61 %

-4.12E-01 10 68 %

1.23E-01 11 75 %

2.33E-01 12 82 %

8.39E-01 13 89 %

2.28E+00 14 96 %

Prepared By: Date:

Reviewed By: Date:

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Cesium-137 Survey Unit: 9106-0008 Survey Unit Name: Discharge Canal Mean: 0.178 pCi/g 6

5 --

4-4

• 3 22 * .ME 0

0.00 0.10 0.20 0.30 0.40 0.50 Upper End Value (pCilg)

Upper End Observation Observation %

Value Frequency Frequency 0.00 2 14%

0.10 5 36%

0.20 1 7%

0.30 2 14%

0.40 2 14%

0.50 2 14%

Total 14 100%

Prepared By: Date: 10 Vý Reviewed By: Date: / / ,

Z6/1

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Cobalt-60 Survey Unit: 9106-0008 Survey Unit Name: Discharge Canal Mean: 0.198 pCi/g 10 8

G) 6 C" 4-2f 0 i I 0.00 0.25 0.50 0.75 1.00 Upper End Value (pCi/g)

Upper End Observation Observation %

Value Frequency Frequency 0.00 3 21%

0.25 8 57%

0.50 1 7%

0.75 0 0%

1.00 2 14%

Total 14 100%

Prepared By: 61 ýIz Date: /0-3/-o"

~l,4*~2 Reviewed By: Date: 1(1 £

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Strontium-90 Survey Unit: 9106-0008 Survey Unit Name: Discharge Canal Mean: 0.003 pCi/g 6

5 O2 U- 0 i I W .1 I N-L 0.000 0.005 0.010 0.015 0.020 0.025 Upper End Value (pCi/g)

Upper End Observation Observation %

Value Frequency Frequency 0.000 5 36%

0.005 2 14%

0.010 4 29%

0.015 1 7%

0.020 1 7%

0.025 1 7%

Total 14 100%

Prepared By: Date: ,-/-Oý Reviewed By:Dt Date: ///1,

Health Physics Procedure GGGR-R5123-Rev.CY-001 Attachment C Frequency Plot For Nickel-63 Survey Unit: 9106-0008 Survey Unit Name: Discharge Canal Mean: -1.380 pCi/g 5

>4-03 U-0-2

-3.00 -2.00 -1.00 0.00 1.00 2.00 3.00 Upper End Value (pCi/g)

Observatio Observation Upper End n  %

Value Frequency Frequency

-3.00 2 14%

-2.00 4 29%

-1.00 2 14%

0.00 2 14%

1.00 3 21%

2.00 0 0%

3.00 1 7%

Total 14 100%

Prepared By: Date: &f/-/ - o Reviewed By: _D Date: //ZýA/,

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Attachment 2e Sign Test Calculation (1 Page)

Health Physics Procedure 3PP-GGGR-R512 1-000 Attachment A, Rev. CY-00 I MAJOR Health Physics Procedure 3PP-GGGR-R5121-000 Attachment A, Rev. CY-OQi MAJOR Sign Test Calculation Sheet For Multiple Radionuclisdes rvey Unit Numb, 9106-0008 rvey Unit Name: Discharge Canal WP&IR#: 2006-021 Classification : 2 TYPE I (cc error):0.05 TYPE I (3 error):0.05 Radionuclides: Cs-137 Co-60 Sr-90 Ni-63 Survey Design DCGL (pCi/g): 6.01 2.9 1.18 549 Results Cs-137 Results Co-60 Results Sr-90 Results Ni-63 Weighted Sum DCGL-Result Sign (Wi) 3.96E-01 1.33E-01 1.33E-01 1.33E-01 1.17E-01 8.83E-01 1

-8.91E-03 7.77E-03 7.77E-03 7.77E-03 1.84E-02 9.82E-01 1 2.05E-01 3.24E-01 3.24E-01 3.24E-01 1.55E-01 8.45E-01 1 4.32E-02 0.OOE+00 0.OOE+00 0.OOE+00 1.94E-03 9.98E-01 1 2.66E-01 2.75E-02 2.75E-02 2.75E-02 5.44E-02 9.46E-01 1 4.92E-01 7.79E-01 7.79E-01 7.79E-01 3.55E-01 6.45E-01 1 2.29E-02 2.68E-02 2.68E-02 2.68E-02 1.23E-02 9.88E-01 1 4.72E-01 9.17E-01 9.17E-01 9.17E-01 3.92E-01 6.08E-01 1 1.55E-02 -1.08E-02 -1.08E-02 -1.08E-02 -6.15E-03 1.00E+00 1 3.36E-01 2.46E-01 2.46E-01 2.46E-01 1.44E-01 8.56E-01 1 6.76E-02 1.22E-01 1.22E-01 1.22E-01 6.97E-02 9.30E-01 1 1.84E-01 1.79E-01 1.79E-01 1.79E-01 7.61E-02 9.24E-01 1 1.03E-02 2.99E-02 2.99E-02 2.99E-02 2.03E-02 9.80E-01 1

-3.89E-03 -1.45E-02 -1.45E-02 -1.45E-02 -1.07E-03 1.00E+00 1 Number of Positive Differences (S+): 14 Critical Value: 11 Survey Unit: Meets Acceptance Criterion Performed By: ( Date: I9- ?/-061 pendent Review: _ ___ - Date:

Page 1 of I

DISCHARGE CANAL SURVEY UNIT 9106-0008 RELEASE RECORD Attachment 2f COMPASS DQA Surface Soil Report with Retrospective Power Curve (4 Pages)

DQA Surface Soil Report Assessment Summary Site: 9106-0008 (19 mrem/yr)

Planner(s): Dale Randall Survey Unit Name: 9106-0008 Report Number: 1 Survey Unit Samples: 14 Reference Area Samples: 0 Test Performed: Sign Test Result: Not Performed Judgmental Samples: 0 EMC Result: Not Performed Assessment

Conclusion:

Reject Null Hypothesis (Survey Unit PASSES)

Retrospective Power Curve 1

U 0.9 1~

0.8

= iI_

0.7 0.6 ijzi ":_

C, 0.5 ,1T - - _

0.4 0.3 0.2 I. 0.1 0

0.0 0.2 0.4 0.6 0.8 1.0 1.2 Unity Rule Sum-of-Ratios, including background

- - Prospective Power U 1-beta .... Actual Power

- LBGR - - Estimated Power DCGL --- - Retrospective Power COMPASS vi.0.0 111112006 Page 1

~DQA Surface Soil Report Survey Unit Data NOTE: Type = "S"indicates survey unit sample.

Type = "R" indicates reference area sample.

Sample Number Type Co-60 (pCi/g) Cs-137 (pCi/g) Ni-63 (pCilg) 9106-0008-001 F S 0.13 0.4 0.23 9106-0008-002F S 0.01 -0.01 -4.84 9106-0008-003F S 0.32 0.2 -2.74 9106-0008-004F S 0 0.04 -1.8 9106-0008-005F S 0.03 0.27 -0.86 9106-0008-006F S 0.78 0.49 2.28 9106-0008-007F S 0.03 0.02 -2.33 9106-0008-008F S 0.92 0.47 -0.41 9106-0008-009F S -0.01 0.02 -2.05 9106-0008-01 OF S 0.25 0.34 0.12 9106-0008-011 F S 0.12 0.07 -3.34 9106-0008-012F S 0.18 0.18 0.84 9106-0008-013F S 0.03 0.01 -2.7 9106-0008-014F S -0.01 0 -1.72 Sample Number Type SrY-90 (pCi/g) 9106-0008-001 F S 0.01 9106-0008-002F S 0.02 9106-0008-003F S 0.01 9106-0008-004F S -0.01 9106-0008-005F S 0 9106-0008-006F S 0.01 9106-0008-007F S 0 9106-0008-008F S 0 9106-0008-009F S -0.01 9106-0008-01OF S 0 9106-0008-011F S 0.02 9106-0008-012F S -0.02 9106-0008-013F S 0.01 9106-0008-014F S 0.01 COMPASS v1.0.0.P 1111112006 Page 2

DQA Surface Soil Report Modified Data (Unity Rule SOR)

NOTE: Type = "S"indicates survey unit sample.

Type = "R" indicates reference area sample.

Sample Number Type Sum-of-Ratios (SOR) 9106-0008-001 F S 0.12 9106-0008-002F S 0.01 9106-0008-003F S 0.15 9106-0008-004F S 0 9106-0008-005F S 0.05 9106-0008-006F S 0.36 9106-0008-007F S 0.01 9106-0008-008F S 0.39 9106-0008-009F S -0.01 9106-0008-01OF S 0.14 9106-0008-011F S 0.06 9106-0008-012F S 0.08 9106-0008-013F S 0.02 9106-0008-014F S 0 COMPASS vl.0.0 1111112006 Page 3

'K3 DQA Surface Soil Report Basic Statistical Quantities Summary Statistic Survey Unit Background DQO Results Sample Number 14 N/A N=13 Mean (SOR) 0.10 N/A 0.17 Median (SOR) 0.06 N/A N/A Std Dev (SOR) 0.13 N/A 0.09 High Value (SOR) 0.39 N/A N/A Low Value (SOR) -0.01 N/A N/A COMPASS v1.0.0 111/12006 Page 4