ML17158C032

Rev 4, Solid Radwaste Pcp.

ML17158C032
Person / Time
Site:	Susquehanna
Issue date:	01/08/1997
From:	SEIBERT A C, STEFFENAUER D J PENNSYLVANIA POWER & LIGHT CO.
To:
Shared Package
ML17158C031	List: ML17158C030 ML17158C032 PLA-4596, Forwards Susquehanna Steam Electric Station Annual Effluent & Waste Disposal Rept Covering Period Jan-Dec 1996 & Rev 4 to NDAP-QA-0646, Solid Radwaste Pcp
References
NDAP-QA-0646, NDAP-QA-646, NUDOCS 9704030257
Download: ML17158C032 (91)

Text

APPENDIXB REVISIONS TOSSESSOLIDWASTEPROCESSCONTROLPROGRAM(NDAP-QA-0646) 9704030257 97033iPDRADQCK05000387R

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COVERSHEETNUCLEARDEPARTMENT PROCEDURE SOLIDRADIOACTIVE WASTEPROCESSCONTROLPROGRAMNDAP-gA-0646 Revision4Page1of63c'goEFFECTIVE DATE:PERIODICREVIEWFREQUENCY:

PERIODICREVIEWDUEDATE:REVISEDPERIODICREVIEWDUEDATE:PROCEDURE TYPE:OAProgram(Q}YES()NOPlantProcedure (j)YES()NOZ'rd/edco~~g'sag&~i~REVIEWMETHOD:()Alternate

()Expedited (g)POND()ERDPreparedbyReviewedbyRecommended SuperctsonaUn'anager Date3-zz-9'5ApprovedbyPORCCommittee MeetingNo.ERCCottDateDateFORMNDAP-gA-0002-1, Rev.1,Page1of1IMNSttlmllllHNimmtmMIItillS IIllltlmSlIlllllRttll NDAP-gA-0646 Revision4Page2of63PRODURESIONSUMMARSOLIDRADIOACTIVE MASTEPROCESSCONTROLPROGRAMThefollowing changeswillnotreducetheoverallconformance-of thesolidified wasteproducttoexistingcriteriaforsolidwastes.1)Incorporated PCAF1-94-1330 revisingthePCPimplementing procedure matrixtoreflectactualprocedures inuseandchangedtherequirements fordisposalofradioactive wastesamplesafterpackagedradioactive wastehasbeeninitsdesignated storagearea.2)AddedSEGNRCapprovedTopicalReportSTD-P-05-011-P-A toContracted VendorServicestoreflectuseofSEGforwaste'rocessing equipment, methodsandverification ofacceptable wasteformsfordewatering andsolidification.

3)AddedActivated Carbonasanewwaste'type whichisgenerated fromprocessing ofliquidwastesusingvendorprovideddemineralization services.

4)AddedtheSolidification/Dewatering/Services Vendormayperformtestsolidification anddetermination ofmixingratiosforsolidification performed offsite(vendorfacility) 5)AddedRadlok(SEG)typecontainers toHighIntegrity Container approvedforuselist.6)7)AddedSNMinventory requirements duringprocessing perSOOR94-581resolution.

AddedNRCTechnical PositiononConcentration Averaging andEncapsulation toRadioactive MasteAnalysisandClassification toensurethatradionuclide/concentrations areadequately distributed overthevolumeorweightofthewaste.

NDAP-gA-0646 Revision4Page3of63SECTION1.0PURPOSE2;0POLICY/DISCUSSION

3.0REFERENCES

TABOFCONTES4.0RESPONSIBILITIES 4.1EFFLUENTS MANAGEMENT SUPERVISOR 4.2SUPERVISOR

-OPERATIONS TECHNOLOGY 4.3POMERPRODUCTION ENGINEER-EFFLUENTS MANAGEMENT 4.4HEALTHPHYSICIST

-EFFLUENTS HANAGEHENT 4.5RADMASTESUPERVISOR 4.6CHEMISTRY SUPERVISOR 4.7HPFOREMAN-EFFLUENTS MANAGEMENT 4.8MANAGER-NUCLEAR ASSESSMENT SERVICES'.9AUXILIARY SYSTEHSOPERATOR4.10SOLIDIFICATION/DEMATERING/SERVICES VENDOR4.11MANAGER-NUCLEARPROCUREMENT 4.12MANAGER-NUCLEARSYSTEMSENGINEERING 4.13MANAGER-NUCLEARMAINTENANCE 4.14LICENSING SUPERVISOR 4.15MANAGER-NUCLEARTRAINING4.16MANAGER-NUCLEARSECURITY5.0DEFINITIONS

NDAP-gA-0646 Revision4Page4of63~SECION6.0PROCEDURE ABEOFCONTENTSCot'e206.1CONTRACTED VENDORSERVICES6.2MASTETYPES6.3RADIOACTIVE MASTEANALYSISANDCLASSIFICATION 6.4TESTING/TREATHENT OFSOLIDIFIED RADWASTEFORCOMBUSTIBLE GASES6.5RADIOACTIVE WASTESOLIDIFICATION 6.6.RADIOACTIVE WASTEDEWATERING 6.7HIGHINTEGRITY CONTAINERS (HIC)6.8IRRADIATED HARDMAREPROCESSING ANDDEMATERING II6.9CONTAINER INSPECTIONS 6.10WASTECONTAINER SPACEUTILIZATION 6.11STORAGEOFPACKAGEDRADIOACTIVE WASTE6.12TRANSPORTATION, SHIPPINGANDDISPOSALREGULATIONS 6.13SHIPPINGOFRADIOACTIVE WASTE6.14SHIPHENTCONFIRMATION 6.15CHANGESTOTHESOLIDRADIOACTIVE WASTEPROCESSCONTROLPROGRAM6.16EVALUATION OFPROCESSOR.OPERATIONAL CHANGES6.17REPORTING OFHISHAPSINVOLVING LOWLEVELMASTEFORHS6.18PCPINPLEHENTING PROCEDURES 7.0RECORDS20212730304051.52 NOAP-gA-0646 Revision4Page5of63~](CHANTADACHMNTSSolidification RecordSheetDewatering RecordSheetSusquehanna Guaranteed Solidified/Oewatered MasteVolumeRecordPCPImplementing Procedure MatrixMaterials notCompatible withPolyethylene Containers 5559.6063 NOAP-gA-0646 Revision4Page6of631.0f>URPOSEProvideadministrative control,guidanceandrecordsr theprocessing, packaging, transportation, anddisposalofradioactive waste.Thisprocedure istheProcessControlProgramrequiredbySSESTechnical, Specifications.

2.0~PL000000100Thisprocedure isapplicable toLowLevelRadwaste{LLRM)generated asaresultoftheoperation oftheSusquehanna SteamElectricStation(SSES).ThewastestreamsincludesolidandliquidwasteasdefinedintheFSAR,butdonotincludespentfuelorgreaterthanClassCwaste.Efficient generation andprocessing ofradioactive wasteisveryimportant totheoveralloperation ofSSES.Animportant objective withrespecttoradioactive wastegeneration istominimize'the volumeofwastegenerated.

Theprocessing oflargevolumesofwastecanresultintheinability todisposeoforstoreallwastepackaged, thesignificant increased costsassociated withincreased wastegeneration, andthe-potential toover-burden theprocessing systemanddegradeitslongtermreliability.

TheProcessControlProgramdescribes theenvelopewithinwhichprocessing andpackaging ofradioactive wasteisaccomplished toprovidereasonable assurance ofcompliance withLow-Level Radwasteregulations andrequirements.

Thisprocedure isapplicable toSSESinstalled systems,temporary systemsandequipment providedbyvendorsforprocessing, packaging, transportation, anddisposalofapplicable wasteforms.3.0~RFRNCES3.13.23.349CFR100-177,Transportation 10CFR20,Standards forProtection AgainstRadiation 10CFR61,Licensing Requirement forLandOisposalofRadioactive Maste3.43.53.610CFR71,Packaging andTransportation ofRadioactive Material40CFR261, Identification andListingofHazardous MasteSSESTechnical Specifications Section3/4.11.3, SolidRadwasteSystemi3.7SSESTechnical Specifications Section6.13,ProcessControlProgram(PCP)

NOAP-gA-0646 Revision4Page7of633.8NUREG0800,StandardReviewPlan11.4SolidWasteManagement

.Systems3.9Technical PositiononWasteFormRev.1,19913.10Technical PositiononRadioactive WasteClassification, Rev;0,~19833.11Technical PositiononConcentration Averaging andEncapsulation, Rev.0,19953.12Regulatory Guide1.21,Measuring, Evaluating andReporting Radioactive MaterialinSolidWastesandReleaseofRadioactive MaterialinLiquidandGaseousEffluents fromLightMaterCooledNuclearPowerPlants3.13Regulatory Guide1.143,DesignGuidanceofSolidWasteManagement Systems,3.143.153.163.17Regulatory Guide7.1,Administrative GuideforPackaging andTransporting Radioactive MaterialANSI/ANS40.35,VolumeReduction ofLowLevelRadioactive WasteANSI/ANS40.37, MobileRadioactive WasteProcessing SystemsANSI/ANS55.1,SolidRadioactive WasteProcessing SystemforLightWaterCooledReactorPlant3.18.PacificNuclearDewatering SystemTopicalReportNo.TP-02-P-A, Rev.33.19PacificNuclearSolidification ProcessControlProcedure No.PT-51-WS, Rev.40-3.20Scientific EcologyGroupMobileIncontainer Dewatering andSolidification System(HOSS)TopicalReportNo.STD-R-05-011-P-'A, Rev.23.21DisposalSiteCriteriaforBarnwell, S.C.3.22DHEC-HIC-PL-001 SouthCarolinaCertificate ofCompliance forCNSIHighIntegrity Containers 3.23DHEC-HIC-P0-006, SouthCarolinaCertificate ofCompliance forCNSIOverpackHighIntegrity Containers 3.24DHEC-HIC-PL-012, SouthCarolinaCertificate ofCompliance forVectra'Technologies, Inc.HighIntegerityContainer NOAP-QA-0646 Revision4Page8of633.25DHEC-HIC-PL-005, SouthCarolinaCertificate ofCompliance forScientific EcologyGroup,Inc.HighIntegrity Containers 3.26OHEC-HIC-PL-017, SouthCarolinaCertificate ofCompliance forScientific EcologyGroup,Inc,HighIntegrity Containers 3.27PLA-1237, ProcessControlProgram,August17,19823.28ReviewofProcessControlProg}amforSusquehanna, Unit1,Youngblood toCurtis,September 30,19823.29SafetyEvaluation NL-93-008, SolidRadwasteWasteProcessing ServicesUtilizing PacificNuclearProcessing System3.30IEBulletin79-19,Packaging ofLowLevelRadioactive WasteforTransportation andBurial(')3.31NRCInformation NoticeNo.90-50,Minimization ofMethaneGasGeneration inPlantSystemsandRadwasteShippingContainers (z)3.32GenericLetter91-02,Reporting HishapsInvolving LLWFormsPreparedforDisposal()3.33SOOR-1-90-148, BarnwellReceivedContainer Pressurized withFlammable Gas()3.34SOOR1-90-172, Incorrect SamplingMethodUsedonResinLiner()3.35SOOR1-91-322, DoseRatesonContainer HigherThanExpected()3.36SOOR94-581,SpentTIPFoundUnexpectedly inTIPRoom.4.0EEENIBTH4.1Effluents Management Supervisor responsibilities:

4.1.14.1.24.1.3Developing andimplementing programsandprocedures forradioactive wasteprocessing, packaging, transportation anddisposal.

Haintaining theoverallradwasteprogramtoensurecompliance withapplicable radiological andshippingregulations.

Ensuringpersonnel whoperformsupportactivities suchasprocessing, packaging, andtransportation oflowlevelradioactive wasteareavailable andmeetallqualifications andtrainingrequiredbySSESprocedures.

NDAP-gA-0646 Revision4Page9of634.1.4Collecting, maintaining, reviewing andsubmitting accuratedata/information relatedtowastestreamquantityandnuclidecomposition forinclusion intoAnnualRadioactive EffluentReleaseReportandStateDER-BRPquarterly Report.4.2Supervisor

-Operations Technology responsibilities:

4.2.14.2.24.2.3Providing technical assistance toEffluents Management personnel.

Thisincludesinterpretations ofstate,federal,anddisposalfacilityregulations regarding new,imminent, orproposedregulatory changesgoverning processing, packaging, transportation, anddisposal.

Naintaining acurrentcopyoflocal,state,federalanddisposalfacilityregulations pertaining todisposalandtransportation oflowlevelradioactive waste.Coordinating thesubmittal oftheAnnualRadioactive EffluentReleaseReportaspertheSSESTechnical Specifications.

4.3PowerProduction Engineer-Effluents Management responsibilities:

4.3.14.3.24.3.34.3.44.3.5Ensureprocedures areadequatetoprovideforpropersolidification anddewatering ofwaste.Ensuretestdataorrationale isavailable tojustifyapplicable solidification anddewatering functions ofeachwastetype,oranycombinations, toaddressdisposalandregulatory agencies'equirements.

Evaluateservicesprovidedbyvariousvendorstoensurecontracted solidification anddewatering operations areperformed inthemostefficient andeconomical method,asrequiredbytheapplicable regulatory agencies.

PerformthedutiesofRadwasteSupervisor asspecified inthisprocedure inhisabsence.Definewastestreamsbasedongenerator, filtration mediaandmeansofprocessing.

SOAP-gA-0646'evision 4page10of634.3.6Cqllecting, reviewing*

yndsuhoitting datarelatedto'hereporting ofmishapsandresultsofPCPsurveillance specimenexaminations toapplicable regulatory agen'cies.

4;44.4.3HealthPhysicist

-Effluents Hanagement responsibilities:

4.4.1Haintainasamplingandana)ysisprogramtoensurelOCFR61compliance.

4.4.2Ensureprocedures areadequatetoprovideforproperpackaging andshipmentofwastetoensurecompaiance withallapplicable regulations.

Evaluateservicesprovidedbyvariousvendorstoensurecontracted wastepackaging, processing, and.transportation servicesareperformed inthemostefficient andeconomical method,asrequiredbyapplicable regulatory agencies.

4.4.4PerformthedutiesofHPForeman-Effluents Management as'pecified inthisprocedure inhisabsence.4.4.5Coordinate radioactive materialevaluation ofproductacceptability fordisposalatspecificdisposalfacilities.

4.5RadwasteSupervisorresponsibilities:

4.5.1EnsureSolidffication/Dewatering Equipment isoperatedinaccordance withapprovedoperating procedure, including vendorsuppliedequipment.

4.5.24.5.34.5.4Ensureappropriate wastesolidification anddewatering recordsaregenerated.

Interface withstationsupportgroupstoensureproperImplementation ofprocesscontrolprograms.

Providedirection tocontractor personnel involvedinsolidwasteprocessing activities including:

a.Ensuringtestdataisavailable to5ustifyspecificprocessing techniques.

b.Ensuringapplicable vendorprocedures andrevisions areincorporated

.Intoapplicably plantprocedure andapprovedbyPORC.,

~97-DOCS3oF2,INDAP-QA-0646 Revision4Pagellof634.5.54.5.64.5.74.5.84.5.94.5.104.5.ll4.5.124.5.13c..Coordinating pre-processing andpost-processing treatment activities.

..d.Evaluating servicesprovidedtoensureefficient andeconomical methodsareused..EnsureSolidification andDewatering operations arecarriedoutinanALARAmanner.Interface withHPForeman-Effluents Management forlinerandcaskselection forsolidwasteshippingactivities.

Ensurepropermarkingofcontainers priortofilling.Ensuresolidification/dewatering personnel areadequately trainedperNTP-gA-42.6..

Estimateclassification ofwasteforcontainer selection andprocessing method.EnsurethatwastestreamsloadedintoHighIntegrity Containers aresanipledforradionuclide andevaluated forchemical, compatibility applicable totheuseofHighIntegrity Containers.

Ensureproperinspections anddocumentation arecompletepriortouseofaHighIntegrity Container andensurethatconta1ner isproperlyuseduptothepointoftransfertoHPForeman-Effluents Management.

CompleteandprocessHighIntegrity Container UserCertification Statement toensurethecontainer isusedproperly.

EnsurethatradwastetanksarepreparedwithOperations support.4.6Chemistry Supervisor respons1bili ties:4.6.14.6.24.6.34.6.4Performrequiredsamplepreparation andanalysisinaccordance withapprovedchemistry procedures.

Performtestsolidification ifrequired.

Storetestsolidification billet1frequired.

Providedensityofinitialandfinalwasteform.Providetheisotopicmixandconcentration ofisotopesdetectedinthematerialsampledforsolidification ordewatering.

NDAP-gA-0646 Revision4Page12of634.6.64.7.24.6.5CompleteChemistry portionoftheSolidification andDewatering Records.Ensurepersonnel areadequately trainedperNTP-(A-41.2.

4.6.7Providechemicalanalysisand/ortreatment supportasnecessary foruseofHighIntegrity Containers andliners.4.7HPForeman-Effluents Nanag'ement responsibilities:

4.7.1Interface withRadwasteSupervisor forlinerandcaskselection andscheduling forsolidwasteshippingactivities.

Complete, process,andfileradioactive wasteshippingdocumentation.

4.7.34.7.44.7.54.7.64.7.74.7.84.7.94.7.104.7.11Storageofpackagedradioactive wastewithintheradwastefacilities.

Determine wasteclassification anddescription ofsolidified, dewatered, andotherpackagedwaste..Finaldisposition ofsolidified, dewatered andotherpackagedwaste.EnsuresSSESisaregistered userofapplicable HighIntegrity Containers atspecificdisposalfacilities.

.EnsuresHPpersonnel involvedwithradioactive wastehandlinghavereceivedRadwasteMorker.trainingperNTP-gA-42.6.

Evaluatevendorservicesprovidedtoensureefficient andeconomical methodsareused.CompleteandprocessCertification Statement forDisposalofHighIntegrity Containers asrequiredbyapplicable regulatory agencies.

ProcessandpackageCartr'idge Filters,DryActiveHaste,solidsealedsourcesandothernonprocesswastes.Collection ofDAMandnon-process waste(10CFR61) samples.

NDAP-gA-0646 Revision4Page13of634.8Manager-Nuclear Assessment Servicesresponsibilities:

4.8.1~4.8.24.8.3Performperiodicauditofimplementation ofthis.programandreviewofradwasteservicevendor'sgAPrograms.

Inspection ofRadwasteContainers asrequiredbyapplicable procedures.

Ensureprocesscontrolsareadheredtobyinspection oftestsolidification, wastevolumes,solidification agentadditions, productacceptability checks,dewatering processsequence/acceptance criteriaandrecordsreview.4.8.4Inspection ofpackaging, storage,andshippingactivities, asrequiredbyapplicable procedures.

4.9Auxiliary SystemsOperatorisresponsible foroperating theplantsolidandliquidradwasteequipment inaccordance withapprovedoperating procedures asdirectedbytheRadwasteSupervisor andAssistant UnitSupervisor.'.10 Solidification/Dewatering/Services Vendorresponsibilities:

4.10.14.10.24.10.34.10.44.10.5Providesolidification, dewatering and/orvolumereduction servicesinaccordance withavalidcontractforsaidservices.

Providetestdataormakedataavailable forPPLLreviewduringvendorauditstodemonstrate thattheirservicesandequipment meet.theapplicable regulatory anddisposalfacilitylimitations fortheservicetheyareproviding.

Providetrainingdocumentation todemonstrate thatthepersonnel beingprovided, toconducttheapplicable service,areinfacttrainedandknowledgeable intheapplicable services.

Provideprocedures thatareorcanbeplacedintotheSSESprocedure formatfortheservicesbeingprovided.

EnsureanapprovedgualityAssurance Programexiststhatcoverstheservicesbeingprovided.

ThevendorshallworkwithintheSSESgualityAssurance Programwhenapplicable.

NDAP-gA-0646 Revision4Page14of634.10.64.10.74.10.84.10.9Completeapplicable sectionsof.Solidification and-Dewatering Recordsrequiredforeachcontainer processed.

Ensurepre-qualification testdataforeachwasteformshallbesubmitted totheNuclearRegulatory Commission.

Provideadescription oftheequipment/process thatisusedinprocessing waste.Obtainwastesamplesfromprocessing equipment inaccordance withapprovedoperating procedures.

4.10.10Performallpreandposttreatment activities asdetermined byRadwasteSupervisor.

4.11Nanager-NuclearProcurement responsibilities:

4.11.1EnsureHighIntegrity Containers arenotexposedtoultravioletlight(sunlight).

4.11.24.11.3Ensurepropermaterialcertification iscompletepriortoissuanceofHighIntegrity Containers toplantforuse.Receiptinspection ofHighIntegrity Containers anddocumentreviewtoensureconformance.

4.11.4EnsureCertificate ofCompliance (CofC)isreceivedwithHighIntegrity Container.

4.12Hanager-NuclearSystemsEngineering isresponsible forproviding engineering supportasrequiredforoperation ofassignedradwastesystemsandequipment.

4.13Manager-NuclearMaintenance responsibilities:

4.13.1Calibration andmaintenance ofapplicable plantequipment inRadwasteProcessing Systems.4.13.2Providemaintenance personnel tosupportprocessing, packaging andtransportation oflowlevelradioactive waste.4.14Licensing Supervisor responsibilities:

4.14.1Submitting transportation caskuserregistr'ation requeststoNRCperIOCFRTI.12.

NDAP-gA-0646 Revision4Page15of634.14.24.14.3Submitting totheNRCtheAnnualRadioactive EffluentReleaseReport.Coordinating andsubmitting totheNRCthereportsrequiredasaresultofCondition Report(CR)events,investigations, andresolutions.

4.15Man'ager-NucTearTrainingresponsibilities:

4.15.14.15.2Providing trainingandre-training inapplicable regulatory requitementstopersonnel directlyinvolvedintransfer, processing, packaging, storage,andtransport ofradioactive waste.Maintaining arecordoftraining, attendees, andsubjectmaterialforallLowLevelRadioactive

'Hastetraining.

4.16Manager-NuclearSecurityisresponsible fornotifying appropriate lawenforcement agenciesintheeventoflostradioactive materialshipments.

TONS3.0KFFI5.1'.25.35.45.55.6APPROYEOCONTAINERS:

Approvedmeansapprovalissuedorrecognized bytheNRCforuseinshipmentofradioactive material.

BATCH:Thetotalvolumeofwastecontained inaliner,isolated-wastemixingtank-spentresintank-concentrates tankor-phaseseparator thathasbeensampledfor,solidification/dewatering.

BILLSOFLADING:Shippingpapersormanifests servingasimilarpurposeandcontaining theinformation requiredby49CFR172.202,203,and204.CARRIER:Meansapersonengagedinthetransportation ofpassengers orproperty.

(10CFR71.4)

CERTIFICATE OFCOMPLIANCE:

Licenserequirements established bytheNuclearRegulatory Coamission fortheuseofapprovedRadioactive MaterialShippingContainers.

CHELATING AGENT:Achemicalwhichcombineswithametalsoastoformaringstructure heldbycoordination bonds.

NDAP-gA-0646 Revision4Page16of635.75.85.9CHEMICALFORM:ThechemicalcontentoftheRadioactive Materialbeingshipped.CLOSEDTRANSPORT VEHICLE:A.vehicleequippedwithasecurelyattachedexteriorenclosure, whichduringnormaltransport, restricts theaccessofunauthorized personstothecargospace.(49CFR173-403[C])

COMPOSITE SAMPLE:Amixtureofsamplescollected representing conditions attimeofsampling, fromthesamesamplingpoint,atdifferent times.5.10CONSIGNEE:

Theindividual ororganization towhomtheshipmentisconsigned orintended.

5.11CURINGTIME:Thetimeallowedforthesolidified producttosetpriortoitsevaluation forproductacceptability.

5.125.135.14DECAYHEAT:Theheatproducedbyradioactive decay,usually'expressed inMattsorBTU/hr,butcanberelatedtoCurieContent.DEMATERED:

Theremovaloffreeliquidfromsolidmaterialtoapointwherelessthan1'XforHIC'sandlessthan0.5Xforsteellinersbywastevolumeremainsasrequiredbythedisposalfacilitylicense.EXCLUSIVE USEVEHICLE(a/k/a:SoleUseorFullLoad):Shipmentfromasingleconsignor havingtheexclusive useofatransport vehicleandforwhichallinitial,intermediate, andfinalloadingandunloading iscarriedoutby,orunderthedirection oftheconsignor, consignee, orhisdesignated agent.(49CFA173.403[i])

5.15.FREELIQUID:Liquidwhich-isstillvisibleaftersolidification ordewatering iscomplete, orisdrainable fromthelowpointofapunctured container.

5.16HAZARDOUS MATERIAL-Asubstance ormaterial, including ahazardous substance whichhasbeendetermined bytheSecretary ofTransportation tobecapableofposingathreattohealth,safety,'ndpropertywhentransported incommerce, andwhichhasbeensodesignated.

Thetermincludeshazardous substances, hazardous.

wastes,marinepollutants, andelevatedtemperature materials asdefinedin49CFR171.8, materials designated ashazardous under'theprovisions of49CFR172.101 and172.102,andmaterials thatmeetthedefiningcriteriaforhazardclassesanddivisions in49CFR173.

NOAP-QA-0646 Revision4Page17of63IHAZARDOUS WASTE:Wastewhichcontainsmateriallistedin40CFR261,SubpartDand/orexhibitsoneormoreofthefour.characteristics citedin40CFR261,SubpartC,andisnotexcludedfromregulation under40CFR261,SubpartA.HazmatEmployeemeansapersonwhoisemployedbyaHazmatEmployerwhoduringthecourseofemployment:

5.18.1Loads,unloadsorhandleshazardous materials.

5.18.2Prepareshazardous materials fortransportation.

5.18.35.18.4Modifies, marks,orotherwise represents containers, drums,orpackagings asqualified.

foruseintransport ofhazardous materials.

Isresponsible forsafetyoftransporting hazardous material.HIGHINTEGRITY CONTAINER (HIC):Adisposalsiteapprovedcontainer.

thathasanexpectedlifeof300yearsandprovidesthestructural stability tomeetdisposalrequirements.

HIGHWAYROUTECONTROLLED QUANTITY:

Aquantity, theaggregate radioactivity ofwhichexceedsthatspecified in(49CFR173.403[1]).

ISOTOPICANALYSIS:

Theidentification oftheisotopicelementsinvolvedinasampleofRadioactive Material.

LABELING:

Labelsappliedtoacontainer denotingthecontentsofthecontainer anddegreeofhazardassociated withthecontainers.

Thelabelsareidentified asthe'WhiteIlabel,theYellowII,andYellowIIIlabel.AlabelstatingRadioactive

-LSAcanalsobeappliedtoacontainer

.whenappropriate.

(49CFR172,SubpartE)LIHITEDQUANTITYOFRADIOACTIVE MATERIAL:

Meansaquantityofradioactive materialnotexceeding thematerialpackagelimitsspecified in49CFR172.423,andwhichconforms" withrequirements specified in49CFR173.421.(49CFR173.403[m])

LINER:Steelcontainer inwhichdewatered orsolidification productisdeposited.

LOWSPECIFICACTIVITY:

Naterialinwhichtheactivityisessentially uniformly distributed andinwhichtheestimated averageconcentration pergramofcontentsdoesnotexceedthespecification asstatedin49CFR173.403(n).

NDAP-gA-0646

.Revision4Page18of63.LOMLEVEL-RADIOACTIVE MASTE(LLRM):Radioactive wastegenerated asaresultofqperation ofSSES,excluding spentfuelorbyproductmaterial, isclassified bytheNRCaslow-level radioactive waste.LLRMdoesnotinclude"greaterthanclassC"waste.jHIXINGRATIO:Theratioofwastetocementandadditives

• requiredforsatisfactory solidification.

MIXINGRECIPE:Theamountofwaste,cementandadditives mixedto'olidify waste.MIXEDMASTE:Amixtureoflowlevelradioactive andhazardous waste.NORHALFORMRADIOACTIVE MATERIALS:

Meansradioactive materialswhichdonotmeettherequirements ofSpecialFormRadioactive Haterials (49CFR173.403[s]).

PLACARDING:

Alabelaffixedtoallfoursidesofthetransport vehicledenotingthepresenceandlevelofRadioactive materialonthevehicle.(49CFR172,SubpartF)'ROCESS CONTROLPROGRAM(PCP):Programwhichcontainsthesampling,

analysis, andformulation determination bywhichsolidification ofradioactive wastesfromliquidsystemsisassured.RADIOACTIVE HATERIAL:

Forpurposesoftransportation only,materialinwhichtheactivityisessentially uniformly distributed andtheestimated specificactivityexceeds0.002microcuries, pergramofmaterial.

(49CFR173.403[y]

and[aalu)RAOWASTEMORKER:AHazmatEmployeeinvolvedwiththecollection, packaging, andtransportation ofradioactive waste.SEALEDSOURCES:Anyby-product materialthatisencasedinacapsuledesignedtopreventleakageorescapeofby-product material.

SOLIDIFICATION:

Aconversion ofradioactive materials fromliquid'nd solidsystemstoahomogeneous (uniformly distributed) monolithic, immobilized solidwithdefinitevolumeandshape,boundedbyastablesurfaceofdistinctoutlineonallsides(freestanding).

NDAP-gA-0646 Revision4Page19of635.375.385.395.405.415.425.435.445.455.465.47SOLIDIFIED RADWASTE:

Wetwastewhichissolid~fied (e.g.evaporator concentrates, sludge),meetsthefreeliquidcriteria, andsatisfies applicable transportation anddisposalsiterequirements.

Dewatered resinsorfiltersludgesatisfying thetwolattercriteriashallalsobedefinedassolidified radwaste.

SPECIALFORMRADIOACTIVE MATERIALS:

Radioactive materialthatiseitherasinglepiece,oriscontained inasealedcapsule,thatcanbeopenedonlybedestroying thecapsuleandmeetstheadditional requirements specified in49CFRPart173.403(z).

STABLEANDUNSTABLEWASTEFORMS:Shallbedefinedasstatedin10CFRPart 61andothersupporting regulatory documents.

TESTSOLIDIFICATION:

Themixingofwaste(s)andsolidification agentsinthelaboratory tosupportselection ofmixingratiosandprovideinsurance forfinalproductacceptability.

TRANSPORT INDEX(TI):Thedimensionless numberplacedonthelabelofapackagetodesignate thedegreeofcontrol,tobeexercised bythecarrierduringtransportation.

Thetransport indexwillbedetermined inaccordance with49CFR173.403(bb).

TYPE"A"PACKAGING:

Packaging whichisdesignedinaccordance withthegeneralpackaging requirements of49CFR173.24,andwhichisadequatetopreventthelossordispersal oftheradioactive

contents, andtoretaintheefficiency ofitsradiation shielding properties ifthepackageissubjected tothetestdescribed in49CFR173.465or173.466,asappropriate.

{49CFR173.403[gg])

TYPE"A"QUANTITYRADIOACTIVE MATERIAL:

Thatmaterialwhichmaybetransported inType"A"packaging.

{49CFR173.431[a])

TYPE"B"PACKAGING:

Packaging whichmeetsthestandards forType"A"Packaging, andinaddition, meetsthestandards forthehypothetical accidentconditions setforthin10CFR71.(49CFR173.403[hh])

TYPE"B"QUANTITYRADIOACTIVE MATERIAL:

Thatmaterialwhichmaybetransported inType'B"packaging.

(49CFR173.431[b])

WASTESTREAM:Aby-product ofaprocesssystemorcomponent withuniquecharacteristics andmaintained separatefromotherwastestreams.IWASTETYPE:Specificcontentsofalinerortankwhichmaycontainoneormultiplewastestreams,thecategoryofwaste.suitableforaparticular meansofprocessing.

NDAP-qA-0646 Revision4page20of635.48MASTEPRE-CONDITIONING:

Thephysicalorchemicaladjustment of'-thewastetobringitwithinanestablished envelopetoassuresolidification.

6.0JPPocDURE6.1"CONTRACTED VENDORSERVICES6.1.16.1.26.1.36.1.46.1.56.1.6Solidified radwasteprocessing servicesareprovidedbyVectra,Inc.forwastetypesincludedinthisProcessControlProgram.NRCapprovedTopicalReportTP-02-P-A, describes VectraInc.wasteprocessing equipment, methodsandverification ofacceptable wasteformsfordewatering.

/VectraInc.Solidification ProcessControlProcedure PT-5I-MS, describes wasteprocessing equipment, methodsandverif'ication ofacceptable wasteformsforsolidification.

Thisprocedure doesnotprovidestability pertheBranchTechnical PositiononMasteForm,Rev.1.Volumereduction, servicesareprovidedbyScientific EcologyGroup(SEG)forwastetypesincludedintheProcessControlProgram.NRCapprovedTopicalReportSTD-P-05-011-P-A, describes Scientific EcoplogyGroup(SEG)wasteprocessing equipment, methodsandverification ofacceptable wasteformsfordewatering andsolidification.

Selectedsolidified wasteformshavebeenapprovedtoprovidestability pertheBtanchTechnical PositiononMasteForm,Rev.l.Othercontracted vendorserviceswhicharerequiredforsolidification, dewatering andvolumereduction servicesshallbeevaluated totherequirements stated'in thisProcessControlProgramonacasebycasebasis NDAP-gA-0646 Revision4Page21of"636.2MASTETYPESThefollowing wastetypesshallbeprocessed inaccordance withthisprocedure orincombinations asdefined.Thewasteshouldbedewatered wheneverpossibletominimizedisposalvolume.6.2.1Evaporator Concentrates Thefollowing areconcentrated withtheRadwasteEvaporators and.areconsidered Evaporator Concentrates wastestream:(I)Condensate Demineral izerregenerati oneffluent'2)

DeconShopdrains(3)Chemistry Laboratory sinkdrains(4)Auxiliary Boilerblowdowneffluentb.Cid.Theconstituents ofthiswastestreammayincludethefollowing:

(1)Tr'i-Sodium Phosphate

~(2)SodiumSulfate(3)Phosphoric Acid(4)SulfuricAcid(5)SodiumHydroxide (6)Decontamination solutions (7)Negligible amountsofreagentchemicals usedforchemi..try analysisEvaporator Concentrates intherangeof0-24weightpercentsodiumsulfate(equivalent) shallbesolidified forfinaldisposal.

Evaporator Concentrates shallnotbemixedwithanyotherwastetypeinfinalprocessing.

gDAP-qA-0646 Revision4page22of63MixedSolidsaoThefollowing processwastestreamsarecollected either,in.WasteMixTanks,MasteSludgePhaseSeparator ortransferred directlytoaliner/High Integrity Container andareconsidered MixedSolids:(I)LRMFilterMediaanddrainliquid{2)(3)SumpSludgeUltrasonic Resin'Cleaner Maste(URCMaste)b.d.Theconstituents ofthesewastestreamsmay'ncludethefollowing:

{I)Diatomaceous Earth(2)PowderedResins(3)Fibrousmaterial{4)Carbonmaterial(5)Corrosion products(6)Varioussolidsanddirtinsmallconcentrations MixedSolidsmaybesolidified ordewatered forfinaldisposal.

Eachwastestreamshouldbeprocessed separately.

RWCUFilterMediab.TheReactorMaterCleanupSystemandFuelPool'ooling andCleanupSystemfilter/demineralizer wastearecollected intheRWCUPhaseSeparator andshouldbeallowedtodecayfor60days.'his wastestreamisconsidered RWCUFilterMedia.Theconstituents ofthiswastestreammayincludeanionandcationpowderedresin,corrosion andcontaminants removedfromtheprimarycoolant.

NDAP-gA-0646 Revision4Page23of63C.RWCUFilterMediashallbedewatered inHighIntegrity Containers.

Ifthiswastemustbesolidified, Technical Specification 3/4.11.3actionstatement mustbeperformed.

Condensate/Radwaste/Atmospheric Demineralizer BeadResina~b.C.'IResinsfromtheCondensate Oemineralizers, LiquidRadwasteDemineralizer andvendorprovideddemineralization arecollected intheSpentResinTankortransferred directlytoaliner/High Integrity Container.

Thisisconsidered tobe.Condensate/Radwaste/Atmospheric Oemineralizer BeadResin.Theconstituents ofthiswastestreammayincludevarioustypesofanion,cation,mixedbeadresinandcorrosion andcontaminates removedfromliquidwastestreams.BeadResinmaybeusedtodemineralize LiquidWasteineithersteellinersorHighIntegrity Containers.

d.e.Condensate Demineralizer beadresinshouldbeultrasonically cleanedpriortocollection intheSpentResinTank.BeadResinmaybesolidified ordewatered forfinaldisposal.

BeadResinmayalsobeprocessed byvolumereduction methodswhichincludedrying,incineration, compaction, useasfillmaterials orotherevaluated method(s) onacasebycasebasis.Cartridge Filters'a~Cartridge Filterwastetypeconsistsofthefollowing wastestreamsandconstituents:

(I)CRDFilters-CRDorotherfiltersandsmallun-irradiated primarysystemequipment suchasvalves,CRDliftpumpfilters,RinseTankfiltersandothermetalcomponents.

NOAP-gA-0646

..Revision4'Page24of63(2)RNCUSepta-SeptafromRMCUFilte}Demineralizer including septafromFuelPoolCleanupFilterDemineralizer.

(3)RadwasteFilters-including degasifier filtersandotherfiberorpaperfiltersotherthanprimarysystem.{4)Underwater VacuumFilters-non-process filtersgenerated fromwetcleaningactivities.

b.Cartridge Filtersmaybeprocessed bythefollowing methods:{1)Emplacement inacementmatrixinasteeldrum/liner orinaHighIntegrity Container.

(2)Driedtoapointwherenofreeliquidisvisible.Absorbent materialmaybeincludedtoabsorbunintentional andincidental amountsofliquids.{3)Oewatered ifdryingisimpractical.

(4)Incineration orothervolumereduction methods.c.Cartridge Filterstobesolidified forfinaldisposalshallnotbemixedwithanyotherwastetype.d.Eachcartridge filterwastestreamshouldbepackagedseparately unlessanalyzedpriortopackaging inaccordance withtherequirements ofthisprocedure.

Irradiated Hardwarea0Irradiated hardwareisneutronacti'vated metalremovedfromtheinternalareaofthereactorpressurevessel.Thiswastestreamisconsidered Irradiated Hardware.

NDAP-gA-0646 Revision4Page25of63Theconstituents ofthiswastestreammayincludecontrolrodblades,LPRHS's,IRK's,TIP'sandcomponents expendedduringhardwareprocessing andpackaging activities.

Startupsourcesmayalsobeprocessed aspartofthiswastestream.c.Irradiated hardwareispackagedinsteellinersfordisposal.

d.LiquidshallbedrainedtoensurefreeliquidAcceptance Criteriaaremet.e.Irradiated hardwareshallnotbemixedwithanyotherwastetypeinfinalprocessing.

DryActiveWaste(DAM)a.DryActiveWasteisawastestream.b.Theconstituents ofthi'swastestreamconsistofcontaminated paper,plastic,wood,metalandotherdiscarded material.

C.DryActiveMaste,shall beprocessed byvolumereduction methodswhichmayincludeincineration, compaction, decontamination andmetalmelting.d.Ataminimum,DAMshallbepackagedinstrong-tightcontainers fordisposal.

LiquidOilWasteorPetroleum BasedMaterials Theconstituents ofthiswastestreammayincludeturbinelubricating oil,EHCfluidandotherpetroleum basedmaterials.

Contaminated LiquidOilWastegenerated atthefacilityshouldbeprocessed byadecontamination system,solidified forfinaldisposal, volumereducedbyincineration, orotheracceptable methods.

NDAP-gA-0646 Revision4Page26of63CiLiquidOilMasteatconcentrations 1Xandgreatermaybesolidified providedthefollowing areadheredto:k(1)Anemulsification agentisaddedatrequiredconcentrations.

(2)TheLinerisNOTSHIPPEDtoadisposalfacilitywithoutpriordisposalfacilityapproval.

SolidSealedSourcesaob.coSolidSealedSourcesrequiring disposalshallbepackaged.fordisposalasrequested byHealthPhysicsSupervision.

Methodofdisposalisdependent onwasteclassoftheSolidSealedSourceanddisposalfacilityrequirements.

Acceptable methodsofdisposalinclude:(1)Placement withinacontainer consisting ofanotherwastetypeprovided:

(a)Thesourcecontainsisotopics alreadyinthewaste.(b)Thesourceactivityissignificantly lessthanthewasteactivity.

(2)ClassBandCsourcesshallbestabilized withinanapprovedsolidification orencapsulation media.Activated Carbonaob.Activated Carbonfromvendorprovidedliquidwastedemineralization istransferred directlytoaliner/High Integrity Container.

Thiswastestreamisconsidered Activated Carbon.Theconstituents ofthiswastestreammayincludevarioustypesofcharcoal, ionspecificcarbonfiltermediaandcorrosion and.contaminants fromliquidwastestreams.

NDAP-gA-0646 Revision4Page27of63C.Activated Carbonmaybesolidified, dewatetedorprocessed byvolumereduction methodswhichincludedrying,incineration, compaction, useasfillmaterials orotherevaluated methodson'acasebycasebasis.6.2.116.2.126.2.13.AWasteTypethatiscombinedwithaknownamountofhazardous waste'r"MixedWaste"shallbeprocessed

.forfinaldisposalpendingapprovalobtainedfromtheprocessing anddisposalfacilities, Environmental Protection Agency,U.S.NuclearRegulatory Commission andotherregulatory agenciesasrequired.

Wastetypescontaining chelating agentswithintherangeof0.1to8.0percentbyweightshallbeprocessed toastablewasteforminaccordance withandauthorized bydisposalfacilityrequirements and.approvals.

Variousothermaterials notspecifically identified aswastetypeswillbeevaluated forsolidification, dewatering volumereduction orotherprocessing onacasebycasebasis.(")6.3RADIOACTIVE WASTEANALYSISANDCLASSIFICATION 6.3.1Radionuclide concentrations ofradioactive wasteareusedtoclassifywasteforshippinganddisposal.

Radionuclide concentrations shouldbedetermined baseduponisotopicanalysis, volumeandweightoffinalwasteform.6.3.2ThelOCFR61Compliance Programestablishes amethodology forcharacterizing radioactive wastethroughtheuseofcorrelation factors.Thisprogramshallrequireasaminimumthat:a~Samplesrepresentative ofSusquehanna's wastestreamsarecollecte".

andanalyzedsuchthatresultsareobtainedftomadesignated laboratory atleasteverytwoyears(ClassA)fordevelopment ofspecificcorrelation factors.'Wastestreamsknownorsuspected tobeclassified ClassBorClassCshouldbeanalyzedonanannualbasis.

NDAP-gA-0646 Revision4Page28of63b.Technical basisdocumentation andjustification ofcorrelation factorsaredeveloped foreach.wastestreamandareacceptable foruse.Periodicevaluations andnecessary adjustments toestablished ratiosareperformed inatimelymanner.c.Correlation factorsarere-evaluated following significant changes{greaterthanafactorof10)inplantoperations (suchassignificant changesinfuelleakage,radwasteoperations, orequipment).

Determination ofwasteclassification shallbeinaccordance with10CFR61.55, MasteClassification, anditssupplementary BranchTechnical PositiononRadioactive MasteClassification asfollows:b.C.ClassA-Usuallysegregated fromotherwasteclassesatthedisposalfacility.

Physicalformandcharacteristics shallmeettheminimumrequirements specified in10CFR61.56(a).

Ifthestability requirements in10CFR61.56(b) aremet,thewastedoesnothavetobesegregated fordisposal.

ClassS-Physicalformandcharacteristics shallmeetboththeminimumandstability requirements specified in10CFR61.56.

ClassC-Physicalformandcharacteristics shallmeetboththeminimumandstability requirements specified in10CFR61.56.

Inaddition, measuresshallbetakenatthedisposalfacilitytoprotectagainstinadvertent intrusion.

Isotopicanalysismaybeperformed by:a.Gammaspectrometry ofasampleanduseofcorrelation factors.b.C.d.Directgammaspectrometry ofwasteanduseofcorrelation factors.Completeradionuclide analysisofwastesample.DosetoCuriecalculations.

NDAP-QA-0646 Revision4Page29of63e.Activation analysis.

Volumeandweightoffinalwastemaybedetermined by:a~Calculation usinganalytically derivedsampledensities.

b.C~d.Calculation usingstandardwastedensities.

Directmeasurement ofvolumeandweight.Acceptable methodsdescribed intheTechnical PositiononConcentration Averaging andEncapsulation.

Ifsamplesofwasteareusedforclassification, samplingprogramshallinclude:a~b.Samplesshallbeobtainedandanalyzedforeachbatchof.wetwasteifpractical andALARA.Preferentially, samplesshouldbetakenforanalysisfollowing processing intoafinalwasteform.C.Samplestakenpriortofinalprocessing should.enableresultsofsampleanalysistobedirectlytranslated tofinalwasteform.d.e.BeadresinandActivated Carbonusedforchemicaldemineralization shallbesampledafterhavinghasbeendepletedinprocess.Solidification/Dewatering ServicesVendororanotherqualified individual shallobtainrequiredsamples.Preparation ofwasteforsamplingoranalysisa4b.WetWasteCollection tanksshallberecirculated inaccordance withapprovedoperating procedures priortosamplingoranalysis.

Wasteprocessing insolidification liners/High Integrity Containers shallbemixedinaccordance withapprovedprocedures priortosamplingoranalysis.

NDAP-QA-O646 Revision4Page30of636.3.81c.Metwastetobeprocessed mayalsobemixed,recirculated andsampledoranalyzedfrommobileprocessing equipment.

.Finalwasteformcontaining amixtureofwastetypesorstreamsshallbeindividually analyzedtodetermine radionuclide concentrations.

Thesummation ofeachindividual radionuclide concentration shallbeusedtocharacterize thefinalwasteformforshippinganddisposal.

Wastetypesorstreamsofdifferent wasteclasses(estimated byhistorical precedent orprojected analysis) shallnotbemixed.6.3.9Deviations fromsamplingandanalysisrequirements shallbeapprovedbyChemistry Supervisor andEffluents Management Supervision.

6.4TESTING/TREATMENT OFSOLIDIFIED RAOMASTEFORCOMBUSTIBLE GASES6.4.1Solidified wasteshallbetestedand/ortreatedtoensureitisnotcapableofgenerating quantities offlammable ortoxicgases,vaporsorfumeswhichmaybeharmfultopersonstransporting,

handling, storingordisposing ofthewaste.6.5RADIOACTIVE MASTESOLIDIFICATION 6.5.1GeneralRequirements a.WetMasteTypeswhichmaybesolidified inHighIntegrity Containers areEvaporator Concentrates, MixedSolids,Condensate/Radwaste Demineralizer BeadResin,RMCUFilterMediaandLiquidOilWasteorPetroleum BasedMaterial, Cartridge Filters,SolidSealedSourcesandActivated Carbon.b.cd.HighIntegrity Containers shallbeusedtomeetthestability criteriainaccordance withfederalanddisposalfacilityregulations.

Solidification processing shallbeconducted byqualified SSESorSolidification/Dewatering/

ServicesVendorpersonnel.

Thesolidification processshallbeoperatedinaccordance withapprovedprocedures.

Procedures shallspecifywastestream,amountsofsolidification agentandadditives ormethodfordetermination.

NDAP-gA-0646 Revision4Page31of63MastePreconditioning a~b.Mastepreconditioning requirements shallbedetermined by,chemistry analysis.

Preconditioning ofwasteshallbeperformed ifrequiredpriortodetermining mixingratios.c.Mastepreconditioning isrequiredwhenanyofthefollowing conditions exist:(I)AhighorlowpHcondition, asdetermined bychemicalanalysis.

(2)(3)Liquidcontentofthebatchisoutoftheacceptable envelopeforsolidification.

Solidscontentofthebatchisoutoftheacceptable envelopefo}solidification.

(4)Knownpotential problemchemicals andconstituents withinwastethatmayadversely affectsettingandstability ofcement-solidified wasteform.d.~e.Wastepreconditioning shallbeperformed inaccordance withapprovedprocedures toensurewasteiswithintheacceptable envelopeforsolidification.

Uponcompletion ofwastepreconditioning, additional samples,asrequired, shallbeobtainedinaccordance withRadioactive MasteAnalysisandClassification sectionofthisprocedure.

Determination ofHixingRatiosa.Determination ofmixingratiosshallbeperformed foreachwastebatchtobeprocessed.

"-b.Deviation fromtherecommended mixingratiosshallbereviewedbyPlantOperations ReviewCommittee (PORC).c.Chemistry Groupdetermines:

(1)Densityofthewastesamples.

NDAP-gA-0646 Revision4page32of63d.e.(2)SpecificgravityofSodiumSulfateSolutioninEvaporator Concentrates.

Solidification/Dewater ing/Services Vendordetermines ifthefinalmixingratiosarewithintheacceptable envelopeforsolidification.

Forsolidification performed onsite:(2)Chemistry Groupshallperformtestsolidification ofwasteasrequiredbyTestSolidification sectionofthisprocedure.

Chemistry Groupdetermines mixingratiostoensurepr'opersolidification.

Forsolidification performed offsite:(1)Solidification/Dewater ing/Services Vendorshallperformtestsolidification ofwasteasrequiredbyTestSolidification sectionofthisprocedure.

{2)Solidification/Dewatering/Services Vendor,determines mixingratiostoensurepropersolidification.

TestSolidification

'a~Testsolidification shallbeperformed tosupportwastemixingratiosasfoll'ows:

(1)Atleasteverytenth(10th)batchofthesamewastestream.{2)(3)Mhensampleanalysisfalloutsidetheestablished rangeandcriteriaindicating achangeinwastecharacteristics.

Mhenitisbelievedthatsomeunexpected orabnormalcontaminant maybepresent.(4)Mhen'equested byRadwasteSupervisor.

NDAP-0A-0646 Revision4Page33of63(5)Mixingofmaterials shallbeaccomplished inamannerthatduplicates, totheextentpractical, mixingconditions thatareobtainedwithfull-scale mixingincontainer.

b.c~d.e.(6)Curingshallbeperformed under.conditions similartothoseusedinlaboratory qualification testprogram.Uponfailureofatestsolidification, anLCOisentered,additional samplesshallbeobtained,'lternative solidification parameters aredetermined andasubsequent testverifiessolidification.

Testsolidification shallbeperformed oneachsubsequent batchofthesamewaste'streamuntilatleastthree(3)consecutive initialtestsolidification demonstrate acceptability inaccordance withTechnical Specification 3/4.11.3.

gualityControlshallverifytestsolidification acceptability andindicatetheacceptability onthesurveillance documentation.

Theacceptability requirements aredefinedinthePCPSurveillance Specimensectionofthisprocedure.

Extrasamplevolumeforbackuptestingshallbedisposedofafteracceptable container checksarecompleted.

HighIntegrity Container testsolidification billetsshouldbedisposedafteracceptable container checksarecompleted.

Testsolidification shouldbeperformed withsamplesfromwasteobtainedasfollows:(I)Inaccordance withRadioactive WasteAnalysisandClassification sectionofthisprocedure.

(2)'amplingofthesolidsinthec'ontainer andtheliquidsusedforhydration, thenmixedtotheratiosthatexistinthecontainer.

NDAP-gA"0646 Revision4Page34of63g.TestSolidification Procedures shallbedeveloped foreachspecificwastetypeasrequired.

h.Cement,watertypeandadditives tobeusedinactualsolidification shallbeusedinpreparation oftestsolidification.

PCPSurveillance Specimens a.HighIntegrity Container testsolidification billetsshallbeexaminedandtestedforacceptability afterthespecified curetimefor:(1)Liquidonsurfaceofsolidified productlessthat1.0Xbywastevolume.(2)Visibledefects,suchasctacking,spallin'g, ordisintegration.

(3)Strengthbyphysically pokingthesurfaceofsolidified productwitharigidunyielding device.Nominalsurfacedentingisacceptable.

b.Ifcementsolidification insteellinersisNRCapprovedtoprovidestability, PCPsurveillance specimenexamination testingandreporting isrequiredinaccordance withtheBranchTechnical PositiononWasteForm,Rev.l.CuringTimeAminimumof30hoursshallbeallowedforcuringpriortocappingortransporting container.

b.cThecontainer maybemovedduringthefirsthour.aftersolidification butmustremainundisturbed fortheremaining 29hours.Deviations fromminimumrequiredcuringtimeshallbeapprovedbyRadwasteSupervisor'and justifications documented inremarkssectionofSolidification Record.

NDAP-gA-0646 Revision4Page35of63Solidification Productequality'a~b.Solidification productqualityisassuredbyuseofpredetermined mixingratiosofwaste,cementandadditive.

Liquidtobeusedforsolidification shouldbedemineralized water.Pre-qualification mixingratiosarebasedonlaboratory testingusingnon-radioactive wastematerials.

c.Mixingratiosarere-enforced bythefollowing:

(I)Testsolidification performed periodically asstatedinTestSolidification sectionofthisprocedure.

(2)Visuallyandphysically checkingatleasteveryfifth(5th)container ofthesamewastetype.d.Container checksshallconsistof:'(I)Avisualcheckofsolidified productforliquidonsurfaceofproductnottoexceed1.0Xbywastevolume.(2)Physically pokingthesurfaceofsolidified productwitharigidunyielding devicepriortocapping(Nominalsurfacedentingmayoccurandisacceptable).

e.gualityControlshallverifyacceptability ofsolidified productwhencontainers arechecked.f.Deviation fromthecontainer checkingrequirement shallbeapprovedbytheRadwasteSupervisor.

HandlingofUnacceptable Solidified MasteContainers.

a0b.Ifasolidified wastecontainer doesnotmeetacceptability requirements, aCondition Report(CR)shallbeissued.Ifthereasonforunacceptability isfreeliquid:(I)Thefreeliquidwillberemoved;or NDAP-gA-0646 Revision4Page36of63(2)Extracement/additive willbeaddedtosolidifyfreeliquid.Ifportionsoralloftheproductdidnotsolidifyafterthreedays:k(I)Thewastecontainer willbecappedaridplacedinastoragelocationandperiodically checkeduntil'such atimeproductisacceptable; or(2)Additional solidification agentsmaybeaddedtoachievesatisfactory solidification, asdetermined bytheRadwasteSupervisor.

Iftheproductsolidifies prematurely priorto.completing theadditionofrequiredamountofcementandadditive, ascalculated onthesolidification calculation sheetforthespecificprocedure used,thefollowing isrequired:

{I)Atestsolidification shallbeperformed usingtheactualratioofcementandwasteinthecontainer, providedsufficient samplevolumeremainstocompletethisitem.(2)gualityControlshallchecktheproductforacceptability inaccordance with.Container Checkssectionofthisprocedure.

(3)Thecontainer isconsidered tomeetacceptable wasteformcriteriaforshippingprovidedthesubsequent testsolidification and/orcontainer checksare.acceptable togualityControlandconcurrence oftheRadwasteSupervisor is:obtained.

{4)TheaboveapplyonlyiftheEffluents Management Supervisor determines thattheproductcanbeclassified as"ClassAUnstable" orisplacedinaHighIntegrity Container orstructure thatprovidesstability inaccordance withIOCFR61and~thedisposalfacilitycriteria.

NDAP-QA-0646 Revision4Page37of63e.Iftheproductdoesnotsolidifyproperlyinaccordance withthespecificsolidification procedure, thefollowing isrequired:

(I)Anevaluation ofthelinershallbemadebythefollowing personnel:

(a)Effluents Management Supervision (b)Solidification Vendor-Operations (c)Solidification Vendor-Engineering (3)Disposalfacilities shallbecontacted andrequirements forreceiptofthelinerinquestionshallbedefined.Alternative packaging/processing shallbeevaluated.

(4)Recommendations for'finaldisposition shallbemadetothePowerProduction Engineer-Effluents Management.

(5)Finaldisposition shallbereviewedbyPlantOperations ReviewCommittee (PORC).(6)Recordsshallbekeptanddocumentation supportive offinaldisposition attachedtothesolidification recordpackage.'(7)Thelinermaybeshippedafterg.C.reviewofdocumentation iscompleteanddisposalfacilityconcurrence isreceivedinletterform.9-Specificinstructions shallbeestablished forhandlingunacceptable solidified wastecontainer'n acasebycasebasis.gualityControlshallre-verify acceptability ofsolidified productbyperformance ofContainer Checks.CappingofSolidified WasteContainers a.Therequirements ofSolidification Productgualitysectionofthisprocedure shallbemetpriortocappingthecontainer.

NDAP-gA-0646 Revision4Page38'of63b.Ifthecontainer isnotequippedwithapassiveventanditscontentsarewithinthe.requirements ofLowSpecificActivity(LSA)ensureoneofthefollowing:

(1)Thecontainer shouldbeshippedwithin(10)tendaysafter.capping;or(2)Ifacontainer hasbeencappedforlongerthan(10)days,itshallbeopened,vented,andre-capped within(10)tendaysofshipment.

coIfthecontainer exceedsthelimitsforLowSpecificActivityandcontainswaterand/ororganicsubstances whichcouldradiolytically generatecombustible gases,determination mustbemadesuchthatthefollowing criteriaaremetoveraperiodoftimethatistwicetheexpectedshipmenttime:(1)Thehydrogengenerated shal.lbelimitedtoamolarquantitythatwouldbenomorethan5Xbyvolumeofthecontainer gasvold;or(2}Thecontainer andshippingcaskcavitysha11beinertedwithadiluenttoassurethatoxygenislimitedtolessthan5%byvolume.inthoseportionsofthepackagewhichcouldhavehydrogengreaterthan5X.Solidification AgentControla~b.PortlandCement-.ASTMC-150TypeIshallbeusedforthemobilesolidification process.Othersolidification agentsmaybeusedonlyafteracceptable testingoftheagenthasbeencompleted thatdemonstrates acceptable solidification anddisposalfacilityapprovalhasbeenobtained.

NDAP-gA-0646 Revision4Page39of63C.Documented Certification isnotrequiredfor'aterials receivedinbagsprovidedmaterialverification canbeobtainedasfollows:(1)Cementisacceptable providedthebagcontaining thecementindicates thatcementisPortlandTypeI.'2)SodiumSilicateisacceptable providedthebagcontaining theadditiveindicates Anhydrous SodiumHetasilicate.

(3)Otheradditives areacceptable providedthecontainer isclearlymarkedindicating thetypeofadditive.

d.Otheradditives maybeusedforenhancement ofsolidification processasspecified inthesolidification procedure anddocumented inthesolidification records.Radioactive MasteSolidification RecordsASolidification RecordSheet(FormNOAP-gA-0646-1) shallbecompleted foreachcontainer filledwithsolidification products.

Completion oftheSolidification RecordSheetandtherequiredaccompanying documentation shallbeasfollows:a~TheRadwasteSupervisor isresponsible forinitiating thisformandcompleting Parts1and2.b.C.Effluents Management Supervision, Chemistry andSolidification/Oewatering/Services Vendorpersonnel shallprovideandcheckofftherequireddocumentat~:~.

specified inPart3.gualityControlshallprovidereviewasrequiredfottheSolidification Records.

NOAP-gA-0646 Revision4Page40of636.6RADIOACTIVE WASTEDEMATERING 6.6.IGeneralRequirements MasteStreamswhichmaybedewatered ineitherHighIntegrity Containers orsteellinersareLRWFilterMedia,.Ultrasonic ResinCleanerMaste,SumpSludge,RWCUFilteracedia,Condensate/Radwaste Demineralizer BeadResin,Cartridge FiltersandActivated Carbon.Thetypeofcontainer usedshallbebasedonthewasteclassification andstability criteriainaccordance

'withfederalanddisposalfacilityregulations.

b.C.d.e.Dewatering ofRadioactive Masteshallbeperformed byqualified SSESorSolidification/

Dewatering SetvicesVendorpersonnel.

Dewatering ofRadioactive Masteshallbeperformed inaccordance withapprovedprocedures.

Dewatering procedures shallbebasedondocumented testdatathathasdemonstrated theabilitytoachievefreeliquidlimitsasspecified bydisposalfacilities andapplicable regulatory agencies.

Liquidvolumeanddrainagecalculations andactualdrainageverification mayalsobeusedtomeetfreeliquidlimits.HighIntegrity Containers shallbeusedfordisposalwhentheconcentration ofradionuclides withhalf-lives greaterthan5yearsexceedsIpCi/cc.Eachwastestreamwhichmaybedewatered shouldbecharacterized bytheSolidification/

Dewatering ServicesVendortoensuretheoperating parameters andeffectiveness of'thedewatering systemareinaccordance withtheparameters established intheTopicalReport.I4 NDAP-gA-0646 Revision4Page41of63Dewatered ProductControla.Thefinaldewatered productshallcontainlessthan1Xnon-corrosive freeliquidforHighIntegrity Containers and0.5Xforsteelliners.gualityControlchecksshallbeperformed onprocesssteps..b.cIfadewatered wastecontainer doesnotmeetacceptability requirements, aCondition Report(CR)shallbeissued.Specificinstructions shallbeestablished forhandlingunacceptable dewatered wastecontainer onacase-by-case basis.,d.Deviation fromthecontainer checkingrequirement shallbeapprovedbythePowerProduction Engineer-Effluents Hanagement.-

IRadioactive MasteOewatering RecordsADewatetingRecordSheet(FormNDAP-gA-0646-2) shallbecompleted foreachcontainer filledwithdewatered wastestreams.Partsoftheformshallbecompleted bythefollowing responsible individuals orgroups:a.TheRadwasteSupervisor isresponsible forinitiating thisformandcompleting Parts1and2.b.Chemistry GroupshallcompletePart3SamplingandAnalysis.

c~Effluents Management Supervision, Chemistry andSolidification/Dewatering/Services Vendorpersonnel shallprovideandcheckofftherequireddocumentation specified inPart4.d.gualityControlshallprovidereviewasrequiredfortheOewatering Records.

NDAP-gA-0646 Revision4Page'42of636.7HIGHINTEGRITY CONTAINERS (HIC)6.7.1StorageofHighIntegrity Containers a~Yectra,RadlokandCNSIHighIntegrity Containers (HIC)storedindirectsunlightorinareaswherethereisastrongsourceofultraviolet radiation shaTlbefilledanddisposedofwithinoneyearofmanufacturing date.6.7.2b.cUsesa~OncefilledaHighIntegrity Container maybestoredforaperioduntilatotalofone(1)yearofultraviolet radiation isreceived.

Shortexposures (i.e.,severalhours)tosunlight, suchas'occurring duringshipmentandonsitetransferneednotbecountedwhendetermining totalultraviolet exposure.

ofHighIntegrity Containers HighIntegrity Containers maybeusedtopackagethefollowing wastematerials fordisposal:

(1)Oewatered beadresin,powderedresinanddiatomaceous earth.(2)Compressible andnon-compressible solidwastes.(3)Filterelementsandcartridges.

(4)Solidified resins,sludges,andliquidwastes.(5)Incinerator ash,residuals, orequivalent wastewhichhasbeenrenderednon-dispensable inabindingmatrix.(6)Otherdewatered anddrymaterialprovidedconcurrence isreceivedbycontainer vendoranddisposalfacility.

NDAP-gA-0646 Revision4Page43of63Priortousinga.HighIntegrity Container foraspecificwastematerial, procedures shallbeestablished todefinethespecificrequirement thatshallbemetduringuseofthecontainer.

Theprocedures shallcontain:Documentation requirements thatspecificconditions havebeenmetsuchasinspection andexposuretodegrading conditions.

Instructions astohowtohandleandproperlyclosethecontainer.

Instructions foron-sitestorageofloadedcontainers forultimateshipmentfordisposal.

Theprocedures shallprovideamethodfordocumenting requiredinformation relevanttothecontainer frominitialreceipttoshippingfordisposal.

Requiredinformation shall'bebaseduponthecontainer certificate ofcompliance anddisposalfacilityrequirements.

Retention andutilization ofthedocumentation shallbedefinedintheprocedures.

Theprocedures shallestablish specificgualityControlinspection requirements.

PriortothefirstshipmentofaspecifictypeofHighIntegrity Container, authorization shallberequested fromtheapplicable regulatory agencygoverning useofthecontainer inquestionatthedisposalfacilityofconcern.

NDAP-gA-0646 Revision4Page44of63HighIntegrity Container Limitations a.HighIntegrity Containers areapprovedforuseprovidedthefollowing physicallimitations ofthewastearemet:(1)VectraPayloaddensity(2)Loadingtemperature Sl;47gms/ccg170F(3)(4)(5)(6)VectraEL-50N.S.loadedweight:64200lbVectraEL-142N.S.loadedweight:<8250lbVectraEL-142S.loadedweight:611250lbVectraEL-190N.S.loadedweight:gl1950lb(7)VectraEL-190S.loadedweight514800lb(8)VectraEL-210N.S.loadedweight:g13000lb(9)VectraEL-210Sloadedweight{10)CNSISmallloadedweight(ll)CNSIHediumloadedweight(12)CNSILargeloadedweight(13)Radlok179loadedweight(14)Radlok195loadedweight(15)Enduropak 105loadedweight5173001b52500lbg2500lbg2500lbgl8500lbgl8500lbgl700lbb.(16)Enduropak 205loadedweight:g1900lb{17)Enduropak 150loadedweight:g2400'lbThemaximumconcentration ofradionuclides withhalflivesgreaterthan(5)fiveyearsthatmaybedisposedofinaHighIntegrity Container is350pCi/[c.Otherwasteformsshallnotexceed1.0X10radsmaximumintegrated dosetothecontainer.

NOAP-QA-0646 Revision4Page45of63c.Thepolyethylene HighIntegrity Containers shallnotcomeintocontactwithmaterials listedinAttachment E.d.Apassiveventdesignshallbeincorporated intothecontainer torelieveinternalcontainer, pressure.

ClosureofHighIntegrity Containers a.ClosureofHighIntegrity Containers shallbecompleted inaccordance withapprovedprocedures.

b.C.d.Ifthecontainer isnotequippedwithapassiveventanditscontentsarewithinthelimitsofLowSpecificActivityensureoneofthefollowing:

(I)Thecontainer isshippedwithin(10)tendaysafterclosing;-

or(2)Ifthecontainer hasbeenclosedforlongerthan(10)tendays,itshallbeopened,vented,andre-closed withinten.(10)daysofshipment.

Ifthecontainer exceedsthelimitsforLowSpecificActivityorcontainswaterand/ororganicsubstances whichcouldradiolytically generatecombustible gases,determination mustbemadesuchthatthefollowing criteriaaremetoveraperiodoftimethatistwicetheexpectedshipmenttime:(I)Thehydrogengenerated shallbelimitedtoamolarquantitythatwouldbenomorethan5%byvolumeofthecontainer gasvoid;or(2)Thecontainer andshippingcaskcavityshallbeinertedwithadiluenttoassurethatoxygenislimitedtogBXbyvolume,inthoseportionsofthepackagewhichcouldhavehydrogengreaterthan5X.Step6.7.4.band6.7.4.cshallalsoapplytodewatered wasteinsteelliners.

NDAP-gA-0646 Revision4Page46of63P6.8IRRADIATED HARDMAREPROCESSING ANDDEMATERING 6.8.1GeneralRequirements

'.Processing an'ddewater'ing ofIrradiated Hardware~..'hallbeperformed by.qualified SSESorvendor'ersonnel.

b.Processing anddewatering ofIrradiated Hardwareshallbe.performed inaccordance withapprovedprocedures.

CiIrradiated Hardwareconsisting ofnon-fuelSpecialNuclearHaterialshallbeinventoried duringprocessing inaccordance withNDAP-QA-'0337.

6.8.26.8.3d.Dewatering procedures shallbebasedonliquid'olume anddrainagecalculations andactualdrainageverificatios'fo demonstrate the.ability'..toachievefreeliquidlimitsasspecified bydisposal.

facilities and'applicable regulatory agencies.

0Dewatered ProductControl'a.Thefinaldewatered productshallcontainlessthan0.5Xfreeliquidforsteelliners.b.gualityControlchecksshallbeperformed onprocesssteps.Irradiated HardwareProcessing andDewatering Records'..Allrecordsgenerated shallbecompleted andfiledinaccordance withapprovedimplementing procedures.

6.96.9.2CONTAINER INSPECTIONS 6.9.1gualityControlshallinspectcontainers tobeused:fearsolidification, dewatering, andotherpackaging.

fordisposal.

Thisinspection shallassurethatpriortouse,the'ontainers tobeusedforsolidification, dewatering,orotherpackaging are.intactandtheirinternals arefreeof.anyvisualdamagethatwouldpreventthemfrom'.,performing theirintendedfunction.

IIIf p~gJ-f9',/d>7'HDAP-qA-0646 Revision4PQQgX~fN.'age'47of.636.9;3Packagesshallmeet.thegeneralcriter'ia fornormaltransport conditions inaccordance withtherequirements of49'CFR.TypeApackagesshallmeettheadditional designrequirements specified in49CFR.'.10MASTECONTAINER SPACEUTILIZATION 6.10.1Mastevolumeshallbemaximized withintheguidelines ofspecificprocedures tominimize:

'otential voidspaceatthetopofwastecontainer.

afters'olidification ordewatering is'.complete.

6.10.2~6.10.36.10.4~AdcKtional radioactive materialshoul'dbeadded'nly aftertheinitialwastevolumeisinfinalformandsampledandtheaddedwastevolumeisinfinalformandsampled.\b.Theadditional materialmaybedrawnintocontainers abletowithstand higherexternalpressures withoutdegredation bycreatinganareaoflowpressurefnsidethecontainer, suchaswithsteelliners.c.torall'thercontainers, theadditional

~material.

shallbeaddedviamechanital

~processes orbyotherconveyance whichdoesnotexerthigherexteznalpressures.

aMastevolumesshallsectorexceed.disposalsitecriteria.

Ifwastevolume4slessthandisposalfacility'criteria; requirement fordisposalofthecontainer inquestionshallbedefined'by thedisposalfacility.

Specificwastevolumescommitted tobythe.Solidification/Dewatering/Services Vendorshallbemetorotherwise j'ustified astowhywastevolumeswerenot-achieved.

Susquehanna Guaranteed Solidified/Dewatered MasteVolumeRecord,FormNDAP-gA-0646-3; shallbecompleted bytheSolidification/Dewatering/

Servicesvendor'personnel, approvedby.RadwasteSupervisor andshallbeusedtotrack..solidified/dewatered wastevolumes'chieved, ineachindividual container.

6.11STORAGEOFPACKAGEDRADIOACTIVE MASTE6.11.16.11.2RadwasteSupervisor shallprovideSolidification and/orDewatering Recordsheetsthathavebeenreviewedby'gualityControlpersonnel statingthatprocessed wastehasbeensolidified orde-watered

'inaccordance with=theProcessControlProgramandmeetstheapplicable shippinganddisposalcriteria.

So'lidification andDewatering Recordsshall'includetheisotopicmix,isotopicconcentration ofthe',waste thatwaspackaged, thetotalvolumeofthewaste,andtheamountofwater,cementorothersolidification agentused,asappropriate.

NDAP-gA-0646 Revision4.Page48of636.11.36.11.46.11.56.11.6Solidification andDewatering Recordsshallbepariofthepermanent shippingrecordsandadheretorequirements oftheProcessControlProgram.Formaterials packagedinahighintegrity container, documentation shallbemaintained onHIC,storage andpre-shipment checklist information.-

Packagedradioactive wasteshallbestoredinareasdesignated byHPForemanEffluents Management.

Storageofpackagedradioactive wasteintheLowLevelRadwasteHoldingFacility(LLRWHF)shallbeinaccordance withapprovedprocedures.

Aninventory of.stored,packagedwasteshallbemaintained inaccordance withapprovedprocedures.

6.12TRANSPORTATION, SHIPPINGANDDISPOSALREGULATIONS 6.12.1Specificregulatory documents

'shallbemaintained onsiteinastatusthatiscurrent.Specificregulations thatshallbemaintained includebutarenotlimitedtothefollowing:

a.10CFR71Packaging ofRadioactive Materialfortransport andtransportation ofradioactive materialundercertainconditions.

b.c~d.e.949CFR100-199Transportation.

Chem-Nuclear SystemsInc.BarnwellS.C.disposalsiteoperating licensenumber097Stateof.SouthCarolina, asrequired.

Chem-Nuclear SystemInc.NRCMaterialLicense12-13536-01, asrequired.

Chem-Nuclear SystemInc.Barnwell-S.C.disposalsiteoperating procedures andsitecriteria, as.required.

Scientific EcologyGroupLicensesR-73008-E94, R-01052-A91.

CaskManualsforcasksofwhichPPKLisanauthorized user.h.AcopyofthelicenseforeachfacilitytowhichRadioactive Materialissent:

NDAP-gA-0646 Revision4Page49of636.12.26.12.3i.10CFR61Licensing requirements forlanddisposalofRadioactive Waste.Procedures applicable totransportation, shippinganddisposalshallbedeveloped.

a.Procedures shallbeestablished andmaintained toprovidedirections andassureregulatory'ompliance formanifesting, whichincludeapplicable federal,state,anddisposalfacility'egulations, andNRCguidance.

b.Procedures shallcontaincheckofflistswhere'ndwhenapplicable toassurespecificattention ispaidtothecriticalfunctionbeingcontrolled.

c.Procedures shallcontaingualityControlnotifications orholdpoints.IIComputersoftwareusedtoimplement applicable portionsoftheProcessControlProgramshallbeinaccordance withNDAP-gA-0801.

6.13SHIPPINGOFRADIOACTIVE WASTE6.13.16.13.26.13.36.13.4Allradioactive wasteshallbeshippedbyEffluents Management.

Allradioactive wasteshippedfromSSESshallonlybetofacilities licensedtoreceivethewasteandinaccordance with10CFR20,10CFR71and49CFR100-199.

DryActiveWaste{DAW)shouldnormallybeshippedasTypeAquantities andtherefore donotrequirespecificlicensedcontainers.

Wastecontainers shallbeplacedinaUSNRCapproved1'icensed shippingcontainer ifit:ExceedsTypeAquantities b.cExceeds1000mr/hroncontactExceeds1000dpm/100cmloosesurfacecontamination ontheexteriorofthecontainer.

gmp-qA-0646 Revision4Page50of.63Thespecificconditions oftheCertificate ofCompliance foreachapprovedshippingcaskshallbestrictlyadheredto.Packagedwastemaybeshippedunshielded if:a.-Contactdoseratesarelessthan200mrem/hr.anddoseratesat6feetarelessthan10mrem/hr.

b.CuriecontentofthepackageshallbeaTypeAquantity.

c.Container shallbeaminimumofastrongtightcontainer.

.Priortotheshipmentofapackageofradioactive waste,theHPForeman Effluents Hanagement shallassurethecontainer issurveyedforcontactdoseratesandsurfacecontamination.

Decontamination, ifrequired, shallbedoneunderthedirection oftheHP'oremanEffluents management.

Decontamination maybewaivedbaseduponradiological conditions.

Allvehiclesusedtotransport radioactive wasterequiring thevehicletobeplacarded shallbecheckedforadequateoperation andsafetyconditions.

AllRadwasteshipments fromSSESshallnormallybevia"Exclusive Use"vehicles.

Specificinstructions giventothedriverinclude:a.Expectedrouteoftraveltohisfinaldestination.

b.CiMaintaining "Exclusive Use"status.Specificactionstobetakenintheeventofanaccident.

Novehiclecarryingradioactive wastethatisoverweight shallleaveSSESwithoutaPennsylvania overweight permit.a.ADAWshipmentorothershipmentcapableofhavingitsweightadjusted, shallnotbeallowedtoleaveSSESoverloaded.

b.Anoverloaded condition foranyvehicleisbasedontotalweightandweightperaxle.

NOAP-gA-0646 Revision4,Page51of636.13.11In'theeventaccessisdeniedtoSSESatalloperating disposalfacilities, PALwillprovidecarrierwithaletterstatingthatSSESwillmeetallapplicable federal,state,andcompactrequirements forreceiptbackoftheradioactive waste/material incarrier's possession.

6.14SHIPMENTCONFIRMATION Ifdisposalsiteshipmentacknowledgement isnotreceivedwithin18daysfromdeparture fromSSES,Effluents Management Supervision shallconductatraceinvestigation forshipmentlocation.

Ifthedisposalfacilityshipmentreceiptcannotbeconfirmed within20days,aCondition Report(CR)shallbegenerated.

6.15CHANGESTOTHESOLIDRADIOACTIVE NSTEPROCESSCONTROLPROGRAM6.15.1Anychangesasdescribed intheTechnical Specifications, totheSolidRadioactive MasteProcessControlProgramshallbeprovidedintheAnnualRadioactive EffluentReleaseReportfiledwiththeNRC.6.15.2AnychangestotheSolidRadioactive HasteProcessControlProgramshallbeapprovedbyPlantOperations ReviewCommittee (PORC)priortoimplementation.

(")6.16EVALUATION OFPROCESSOROPERATIONAL CHANGES6.16.16.16.2Changesinradioactive wasteprocessing oroperational changesshallbeevaluated todetermine anyimpactsonwastecharacteristics and/orform.Evaluation shouldincludeasaminimum:a.Operational evaluation ofprocessing impacts.b.Chemistry evaluation ofchangestosamplingand.analysismethodology

.-Cid.Effluents Management evaluation ofpackaging and/orshippingimpacts.Effluents Management evaluation for10CFR61compliance.

8 NDAP-gA-0646 Revision4Page52of63e.Solidification/Dewatering ServicesVendorwastestreamcharacteristic evaluation ofthedewatering/solidification systemoperating parameters andeffectiveness.

()6.17REPORTING OFNISHAPSINVOLVING LOWLEVELMASTEFORMS6.17.110CFR61establishes theminimumandstability requirements forLowLevelMaste(LLM)forms.10CFR20requirescertification thattheprocessed wastesatisfies therequirements of10CFR61.MishapswhichmayimpactthefinalwasteformshallbereportedtotheNRC.6.17.2Typesofmishapswhichshouldbereportedinclude:'a~b.C.Failureofhigh-integrity containers usedtoensureastablewasteform.Container failurecanbeevidenced bychangedcontainer dimensions,

cracking, ordamageresulting frommishand'ting (e.g.,droppingorimpacting againstanotherobject).Misuseofhigh-integrity containers, evidenced byaquantityoffreeliquidgreaterthan1percentofcontainer volume,orbyanexcessive

(>1M)voidspacewithinthecontainer.

Production ofacementsolidified ClassBorCwasteformthathasanyofthe-following characteristics:

(1)Containsfreeliquidinquantities exceeding 0.5percentofthevolumeofthewaste.(2)Containswastewithradionuclides inconcentrations exceeding thoseconsidered duringwasteformqualification testingacceptedbytheregulatory agency,whichcouldleadtoerrorsinassessment of-wasteclass.(3)Containsasignificantly different wasteloadingthanthatusedinqualification testingacceptedbytheregulatory agency.

NDAP-gA-0646 Revision4Page53of63d.(4)Containschemicalingredients notpresentinqualification testingacceptedbytheregulatory agency,and.those quantities aresufficient tounacceptably degradethewasteproduct.(5)Showsinstability evidenced bycrumbling,

cracking, spalling, voids,softening, disintegration, non-homogeneity, ordimensional changes.(6)Evidenceofprocessing phenomena thatexceedthelimitingprocessing conditions identified inapplicable topicalreportsorprocesscontrolplans,e.g.,foaming,temperature

extremes, premature orslowhardening, andproduction ofvolatilematerial.

IFailuretoadheretohighintegrity container limitations asrequiredbycontainer certificate ofcompliance.

6.17.36.17.4e.Notification ofviolation bydisposalfacilityregulatory authorities attimeofcontainer

.receiptfordisposal.

'ailureofcement-solidified stablewasteformlongtermPCPsurveillance specimens duetoevidenceofsignificant

cracking, spalling, orbulkdisintegration, compression orpenetrometer strengthandi@version testresults.Requirements forreporting ofmishapsshallapplyonlytoprocessing linersandhighintegrity containers containing radioactive wasteinitsfinalproductform.ACondition Report(CR)shallbegenerated ifoneofthemishapsmentioned occurs.6.18PCPIHPLEHENTING PROCEDURES Procedures requiredforimplementation oftheProcessControlProgramareshowninAttachment D.*

NDAP-gA-0646 Revssion4Page54of637.0~RECODS7.1TheSolidification RecordsorDewatering Recordsandtheattacheddocuments shallbeforwarded tofffluents Management Supervision forretention untilsuchtimeasthecontainer identified onRecordisshippedforfinaldisposition.

7.2Whentheidentified container isshippedtheSolidification RecordsorDewatering Recordsandotherdocuments concerning the.Shipmentshallbefiledwiththeshippingdocumentation andforwarded toDCSforretention.

7.3Documentation ofRadioactive WasteShipments shallberetainedasrequiredbySSESTechnic'al Specifications.

7.4Radioactive wasteshippingdocumentation shallconsistof,butnotlimitedto,thefollowing records:7.4;17.4.27.4.37.4.47.4.57.4.67.4.7Radioactive MaterialShippingNanifestEvaluation ofisotopicmixandconcentration Radiological surveysof:a.Vehicleuponarrivalb.Packagetobeshippedc.LoadedvehiclepriortoshipmentVehicleSafetyinspection Check-off sheetforloadingprocedure Documentation ofadherence toProcessControlProgram(ifapplicable)

Specialinstructions todriver

SOLIDIFICATION RECORDSHEETPARTI:Container identification Information dAttachment ANDAP-gA-0646 Revision.4'age55of631.PPSLLinerNumberNumber'.Container VendorSerial{RWCUFilterMedia.cannotbeentered)(circleone)3.WasteStreamTestSolidification required7 YESNOPART2:Container Selection (RefertoMH-PS-100) 3.ExpectedMasteClassification/Stability l.Estimated LinerContactDoseRatesmR/hrt.P'dt/tttt~tt/d4.Container TypetobeUsed6.ExpectedCaskTypetobeUsedPART3:Documentation Checklist 5.EmptyReightofContainet

'hal.2.3~FormNDAP-gA-0646-1 (original)

WasteFormDocumentation WH-RP-Forms(original)

SC-068-%2 Forms(copy)MasteForm:STABLEUNSTABLE{circleone)~85%LinerVolumeUtilized:

YESNO(circleone)QasteActivityDocumentation CH-RC-.Forms(copy)Isotop>cAnalysis(copy)Compostadded/Log entrymadeonCH-TP-055-1 4,PART4:HealthPhysicsDataLinerRadiological Survey(original)

ActualFilledContainer WeightREMARKS:lb.(Ifavailable ALARA}FORMNDAP-(A-0646-1, Rev.2,Page1of1(FileR69-1)

TNGCOSAttachment BNDAP-gA-0646 Revision4Page56.of63PARTI:Container Identification Information 1.PPKLLinerNumber2.Container VendorSerialNumber3.Maste'tream PART2:Container Selection (RefertoRR-PS-100) 1.Estimated LinerContactDoseRates'R/hr'I2.PtdCiCtt'li/g3.ExpectedMasteClassification/Stability 4.LinerTypetobeUsed6.ExpectedCaskTypetobeUsed5.EmptyMeightofContainer awasteupervlsor ate>meFORMNDAP-(A-0646-2, Rev.3,(DUPLEX),

Page1of3(FileR69-1)

~PRT3:SamplingandAnalysis1.Tank/Container sampled2..SampleNumber3.WasteStream4.IsotopicAnalysisattachedATINGCODS'ttachment BNDAP-gA-0646 Revision4Page57of635.SpecificactivityofDewatered SamplepCi/gm6.a.Dewatered Volumeb.Dewatered Weightc.Sampledensitymlgmgm/ccx62.43lb/ft7.Composite added/Log entrymadeonCH-TP-055-1 Theabovetank/container containing solidshasbeenanalyzedinaccordance withCH-RC-075 andfoundtocontaintheisotopesandspecificactivities asindicated ontheattacheddatasheets.em>stryupervssson ae>meFORMNDAP-(A-0646-2, Rev.3,(DVPLEX)Page2of3(FileR69-I)

ATERNGCODS+gT4:Container ShipmentInformation SummaryAttachment 8NDAP-gA-0646 Revision4Page58of633.4.PPELLinerNumberFormNDAP-gA-0646-2 (original)

MasteFormDocumentation 2.MasteVolumeMM-RP-Forms(original) t~Calculated MasteMeightlb/ft3xftlbPart~ActualFilledContainer Weightlb.(ifavailable ALARA))00x(Dewatered WasteVolume)fts~fts>85%Container VolumeUtilizedYES/NO(Circleone)WasteForm:STABLEUNSTABLE(Circleone)MasteActivityDocumentation CH-RC-Forms(Copy)IsotopicAnalysis(Copy)PART5:REMARKS:awasteupvateeview~ateoremanI~acFORMNDAP-gA-0646-2, Rev.3,(DUPLEX),

Page3of3(FileR69-I)

SUUHANNAGU0SOFEOEWTAttachment CNDAP-gA-0646 Revision4Page59of63STVoU001.DateLinernumber2..WasteType3.4.Container TypeBurialVolumeUseableContainer Volume7.8.Guaranteed MinimumWasteVolumeWasteVolumeAttainedinchesxWasteVolumeContainer Usageftsft>/inch.100x(WasteVol.ft>~Guaranteed Win.WasteVol.ft3)-100DeadbandAssessment VolumeGuaranteed Min.WasteVol.ftk{0.01XGuaranteed Min.WasteVol.ftMinimum{-)

.fttoMaximum(+)

ft10.'Performance Assessment VolumeDeadbandAssessment Vol.ftWasteVol.ftft11.Remarks:12.Signature os1>cationenorepresentatsve 13.Signature awasteuperv~sor FORMNDAP-(A-0646-3, Rev.2,Page1of1(FileR69-1)

MSTPOCSSNGCPPMNGOCDURAttachment DNDAP-qA-0646 Revision4Page60of63vaoratorConcentrates

-Solidified PacificNuclearPT-51-WS'acificNuclearOM-114-NS PacificNuclearOM-104MixedSolids-Solidified PacificNuclearPT-51-MSPacificNuclearON-104PacificNuclearOH-114-NS LRWFilterMediaURCWastWCUFtered'aSSude-Dewatered PacificNuclearOH-43-WSMM-RP-107 Condensate RadwasteDeminera'readesi-SoidifiedPacificNuclearPT-51-MSPacificNuclearON-114PacificNuclearOH-104Condensate RadwasteDemineral'r BeadResin-Dewatered PacificNuclearOH-43-MSWM-RP-106 CartrideFiltersCNSIFO-OP-019 (Overpack)

WM-PS-230 PacificNuclearOH-16-NSMM-RP-)05 SEGSTD-P-22-002 (ResinExpress)WH-RP-104 SEGSTD-P-03-051 MH-RP-108

.Page1of3 CPIMPMNGOCUAttachment DNDAP-gA-0646 Revision4Page61of63rad'atedHardware-Dewatered Ste'rNoneDrctiveWasteDAW-PackaWM-PS-210

'idOilWaste-SolidifedNone'idOilWaste-Decontamination NoneSolidSealedSourcesNoneWASTFANALYSISANDCLASSIFICATION

-OCFR6PacificNuclearOM-45NSWM-RP-008 CH-RC-075 CH-RC-076 CH-TP-055 WM-PS-155 WM-PS-160 WM-PS-170 TSTINGTREATMENT COMBUSTIB GASSWM-RP-009 WM-RP-301 0CTVWASTSOFICTON-PacificNuclearOM-114-.NS SC-068-002 (TestSolidification)

CMNTPage2of3 PCPIPLMENTNGPROCDUAttachment DNDAP-qA-0646 Revision4,Page62of63RADIOACIVEWASTEDEWATERING

-GENERALPacificNuclearOH-60-MSWM-RP-010 HIGHINGRITYCONTAINRSPacificNuclearOM-16-NSPacificNuclearH-18-NSWH-RP-012 ISPOSAFACILITYREUIEMENTSMH-PS-180

~AC@GINGMH-RP-Ol1 WH-PS-401 (LLRMHF)WN-PS-310 WN-PS-311 WH-PS-315 MN-PS-345 WH-PS-351 WM-PS-352 WH-PS-356 (HN-'142)

(LN-142)(SEG3-82)(CNSI14-195)(CNSI21.;300)(CNSI8-120A)MH-PS-354 (CNSI14-215)WM-PS-316 (SEG14-215)WH-PS-318 (Westinghouse TCT)TRANSPORTATION

-49CFOCF7WN-PS-100WH-PS-120 MH-PS-140 WM-PS-180 MH-PS-240 WN-PS-250 Page3of3

ATEISNOTCOMPABEWPOAttachment ENDAP-gA-0646 Revision4Page63of63YNCOINERSAliphatic hydrocarbons (hexane,octahe,bexene,octane,etc.)AcetoneAmylAcetateAmylChlorideAnilineAquaRegiaBenzeneBromineliquidButaneCamphorOilCarbonDisulphide CarbonTetrachloride ChlorineliquidChlorobenzene ChloroformChlorosulfonic acidChromic/sulfuric acidCyclohexanone Dibutylphtalate Dimethylamine DieselfuelEthylacetateEthylbutyrateEthylchlorideEthyletherEthylenechlorideEthylenechlorohydrin Ethylenedichloride FluorineFurfuralFurfurylalcoholFuelOilGasolineIodineMethylbromideMethylChlorideMethylethylketone(MEK)Nethylene ChlorideMoistChlorinegasNitricAcid(50Kweightconcentration)

OrganPeroxides OctylcresolOleicacidOleumPentanePetroleum etherPhenolPropanePropylene dichloride Sulfricacid(60Kweightconcentration)

Tetrahydrofurance Titaniumtetrachloride TouleneTrichloroethylene Turpentine TetralinXylenePageIofI

't'/