ML22349A200
| ML22349A200 | |
| Person / Time | |
|---|---|
| Site: | Columbia  |
| Issue date: | 12/01/2022 |
| From: | Schmitt M Energy Northwest Environmental Services Laboratory |
| To: | Graves R Office of Nuclear Reactor Regulation, US Dept of Commerce, National Oceanographic and Atmospheric Administration |
| References | |
| GO-22-118 | |
| Download: ML22349A200 (145) | |
Text
From:
Schmitt, Marshall A. <maschmitt@energy-northwest.com>
Sent:
Thursday, December 1, 2022 12:13 PM To:
Ritchie Graves - NOAA Federal Cc:
Briana Arlene; EndangeredSpecies Resource; Barfuss, Brad C.; Ramos, Mary Joy.; Hildman, Cynthia M.; Byers, Kristopher R.
Subject:
[External_Sender] Energy Northwest Columbia Generating Station 2022 Priority Pollutant Discharge Monitoring Report Attachments:
GO2-22-118.pdf Mr. Graves, Condition 2.9.4(4)(a) of the Endangered Species Act 7(a)(2) Biological Opinion requires Energy Northwest to send a copy of reports submitted pursuant to NPDES Permit WA002515-1 to National Marine Fisheries Service (NMFS) and copy to the Nuclear Regulatory Commission (NRC). Please find the attached Columbia Generating Station Annual 2022 Priority Pollutant Discharge Monitoring Report (DMR). This letter and enclosed report are being provided as an electronic transmittal and the DMR has been submitted electronically to the State of Washington Department of Ecology (Ecology) via Ecologys Online Reporting System.
If you have any questions about this report, please contact me at (509) 372-5334 or maschmitt@energy-northwest.com Sincerely, Marshall Schmitt l Environmental Scientist Energy Northwest Environmental and Regulatory Programs 509-372-5334 l maschmitt@energy-northwest.com
Hearing Identifier:
NRR_DRMA Email Number:
1863 Mail Envelope Properties (SA0PR09MB69699627BA0D7AA7BE7CADDD90149)
Subject:
[External_Sender] Energy Northwest Columbia Generating Station 2022 Priority Pollutant Discharge Monitoring Report Sent Date:
12/1/2022 12:12:50 PM Received Date:
12/1/2022 12:13:59 PM From:
Schmitt, Marshall A.
Created By:
maschmitt@energy-northwest.com Recipients:
"Briana Arlene" <briana.arlene@nrc.gov>
Tracking Status: None "EndangeredSpecies Resource" <EndangeredSpecies.Resource@nrc.gov>
Tracking Status: None "Barfuss, Brad C." <bcbarfuss@energy-northwest.com>
Tracking Status: None "Ramos, Mary Joy." <mjoyramos@energy-northwest.com>
Tracking Status: None "Hildman, Cynthia M." <cmhildman@energy-northwest.com>
Tracking Status: None "Byers, Kristopher R." <krbyers@energy-northwest.com>
Tracking Status: None "Ritchie Graves - NOAA Federal" <ritchie.graves@noaa.gov>
Tracking Status: None Post Office:
SA0PR09MB6969.namprd09.prod.outlook.com Files Size Date & Time MESSAGE 961 12/1/2022 12:13:59 PM GO2-22-118.pdf 6875081 Options Priority:
Normal Return Notification:
Yes Reply Requested:
No Sensitivity:
Normal Expiration Date:
P.O. Box 968 / Richland, WA 99352-0968 / (509) 372-5000 / www.energy-northwest.com INTEROFFICE MEMO GO2-22-118 DIC: 1316.20 DATE:
November 17, 2022 TO:
Columbia Generating Station, (CGS)
FROM:
Jane LePage, (1025)
SUBJECT:
COLUMBIA GENERATING STATION NPDES 2022 ANNUAL PRIORITY POLLUTANT DISCHARGE MONITORING REPORT
REFERENCE:
NPDES Permit No. WA 002515-1 Condition S3.A On September 6, 2022, Columbia Generating Station collected a 24-hr composite sample and grab samples of the circulating water blowdown (CWBD) water for annual priority pollutant testing in accordance with special condition S2.A of Permit No.
WA002515-1. Please find attached the NPDES Discharge Monitoring Report (DMR) for 2022 annual priority pollutant analysis. The report will be submitted electronically to the State of Washington Department of Ecology (Ecology) via Ecologys Online Reporting System.
If you have any questions concerning this information, please contact MA Schmitt at (509) 372-5334.
Enclosures:
1-Discharge Monitoring Report (DMR) for annual sample 2-Reports of Analysis NPDES annual priority pollutant sample 3-Edge Analytical, Burlington WA Scope of Accreditation 4-Anatek Labs, Inc., Moscow ID Scope of Accreditation 5-Pace Analytical, MN Scope of Accreditation CC:
National Marine Fisheries Service (NMFS)
Richie.Graves@noaa.gov Columbia Hydropower Branch National Marine Fisheries Service 1201 NE Lloyd Blvd, Suite 1100 Portland, OR 97232
Columbia Generating Station (CGS)
Page 2 of 2 November 17, 2022 Columbia Genertaing Station NPDES 2022 Annual Priority Pollutant Discharge Monitoring Report Briana.Grange@nrc.gov, and EndangeredSpecies.Resource@nrc.gov U.S. Nuclear Regulatory Commission Document Control Desk Washington, DC 20555-0001 JTL I certify under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
Prepared by:
Jane T. LePage, Environmental Scientist, Environmental Services Reviewed by:
Kristopher Byers, Environmental Scientist, Environmental Services Reviewed by:
Marshall Schmitt, Environmental Scientist, E&RP Reviewed by:
Matthew Turner, Manager, Environmental Services Approved by:
Brad C. Barfuss, Manager, Environmental & Regulatory Programs DISTRIBUTION LIST:
INTERNAL DISTRIBUTION:
M Schmitt (via email)
Docket File PE20 J LePage (via email)
Regulatory (via email)
K Byers (via email)
Document Control (via APW)
Monitoring Period:01/01/2022 - 12/31/2022 Facility County: Benton WA0025151 Permit Number:
Permittee:
Receiving Waterbody:
Outfall: 001 Energy Northwest Columbia Generating Station Version:
1 Monitoring Point Parameter Fraction Units Sample Qualifier Code Required Detection Level Required Quantitation Level Actual Detection Level Actual Quantitation Level CWB Antimony Total Micrograms/L (ug/L) 0.6 0.3 1.0 0.4 1
CWB Arsenic Total Micrograms/L (ug/L) 2.8 0.1 0.5 0.5 0.5 CWB Beryllium Total Micrograms/L (ug/L)
< 0.028 U
0.1 0.5 0.028 0.3 CWB Cadmium Total Micrograms/L (ug/L)
< 0.04 U
0.05 0.25 0.04 0.25 CWB Chromium, Hexavalent Total Micrograms/L (ug/L)
M*
NAF 0.3 1.2 CWB Chromium Total Micrograms/L (ug/L) 1.4 0.2 1
0.36 0.5 CWB Copper Total Micrograms/L (ug/L) 9.0 0.4 2
0.073 2
CWB Lead Total Micrograms/L (ug/L) 0.2 0.1 0.5 0.091 0.5 CWB Mercury Total Nanograms/L (ng/L) 3.88 0.2 ng/L 0.5 ng/L 0.2 0.5 CWB Nickel Total Micrograms/L (ug/L) 6.6 0.1 0.5 0.1 0.5 CWB Selenium Total Micrograms/L (ug/L) 1 1
1 0.22 1
CWB Silver Total Micrograms/L (ug/L)
< 0.19 U
0.04 0.2 0.19 0.2 CWB Thallium Total Micrograms/L (ug/L)
< 0.04 U
0.09 0.36 0.04 0.36 CWB Zinc Total Micrograms/L (ug/L) 11.4 0.5 2.5 0.79 2.5 CWB Cyanide Total Micrograms/L (ug/L)
M*
NAF 5
10 CWB Phenolics (Total Phenols)
Total Micrograms/L (ug/L)
M*
NAF 50 CWB 2-Chlorophenol Micrograms/L (ug/L)
< 0.1 U
1 2
0.1 1
CWB 2,4-Dichlorophenol Micrograms/L (ug/L)
< 0.2 U
0.5 1
0.2 1
CWB 2,4-Dimethylphenol Micrograms/L (ug/L)
< 0.4 U
0.5 1
0.4 1
CWB 4,6-Dinitro Methylphenol (4,6 dinitro-o-cresol)(2-methyl-4,6-dinitrophenol)
Micrograms/L (ug/L)
< 0.3 U
1 2
0.3 1
CWB 2,4-Dinitrophenol Micrograms/L (ug/L)
< 0.5 U
1 2
0.5 1
CWB 2-Nitrophenol Micrograms/L (ug/L)
< 0.2 U
0.5 1
0.2 1
CWB 4-Nitrophenol Micrograms/L (ug/L)
< 0.3 U
0.5 1
0.3 1
CWB 4-Chloro-3-Methylphenol (Parachlorometa cresol)
Micrograms/L (ug/L)
< 0.2 U
1 2
0.2 1
CWB Pentachlorophenol Micrograms/L (ug/L)
< 0.2 U
0.5 1
0.2 0.4 CWB Phenol Micrograms/L (ug/L)
< 0.1 U
2 4
0.1 1
CWB 2,4,6-Trichlorophenol Micrograms/L (ug/L)
< 0.1 U
2 4
0.1 1
CWB Acrolein Micrograms/L (ug/L)
< 0.42 U
5 10 0.42 2
Sample Date: 9/6/2022 Washington State Department of Ecology Discharge Monitoring Report (DMR)
Page: 1 of 5
CWB Acrylonitrile Micrograms/L (ug/L)
< 0.56 U
1 2
0.56 2
CWB Benzene Micrograms/L (ug/L)
< 0.23 U
1 2
0.23 0.4 CWB Bromoform Micrograms/L (ug/L)
< 0.26 U
1 2
0.26 0.4 CWB Carbon Tetrachloride Micrograms/L (ug/L)
< 0.24 U
1 2
0.24 0.4 CWB Chlorobenzene Micrograms/L (ug/L)
< 0.28 U
1 2
0.28 0.4 CWB Chloroethane Micrograms/L (ug/L)
< 0.34 U
1 2
0.34 0.4 CWB 2-Chloroethylvinylether Micrograms/L (ug/L)
< 0.46 U
1 2
0.46 2
CWB Chloroform Micrograms/L (ug/L) 2.2 1
2 0.25 0.4 CWB Dibromochloromethane (chlorodibromomethane)
Micrograms/L (ug/L)
< 0.28 U
1 2
0.28 0.4 CWB 1,2-Dichlorobenzene Micrograms/L (ug/L)
< 0.31 U
1.9 7.6 0.31 0.4 CWB 1,3-Dichlorobenzene Micrograms/L (ug/L)
< 0.29 U
1.9 7.6 0.29 0.4 CWB 1,4-Dichlorobenzene Micrograms/L (ug/L)
< 0.29 U
4.4 17.6 0.29 0.4 CWB Dichlorobromomethane Micrograms/L (ug/L)
< 0.28 U
1 2
0.28 0.4 CWB 1,1-Dichloroethane Micrograms/L (ug/L)
< 0.32 U
1 2
0.32 0.4 CWB 1,2-Dichloroethane Micrograms/L (ug/L)
< 0.38 U
1 2
0.38 0.4 CWB 1,1-Dichloroethene (1,1-dichloroethylene)
Micrograms/L (ug/L)
< 0.25 U
1 2
0.25 0.4 CWB 1,2-Dichloropropane Micrograms/L (ug/L)
< 0.22 U
1 2
0.22 0.4 CWB 1,3-Dichloropropene (1,3 Dichloropropylene)
Micrograms/L (ug/L)
< 0.31*
U 1
2 0.31 0.4 CWB Ethylbenzene Micrograms/L (ug/L)
< 0.29 U
1 2
0.29 0.4 CWB Bromomethane (methyl bromide)
Micrograms/L (ug/L)
< 0.37 U
5 10 0.37 0.4 CWB Chloromethane (methyl chloride)
Micrograms/L (ug/L)
< 0.28 U
1 2
0.28 0.4 CWB Methylene Chloride Micrograms/L (ug/L)
< 0.28 U
5 10 0.28 0.4 CWB 1,1,2,2-Tetrachloroethane Micrograms/L (ug/L)
< 0.37 U
1.9 2
0.37 0.4 CWB Tetrachloroethene (tetrachloroethylene)
Micrograms/L (ug/L)
< 0.24 U
1 2
0.24 0.4 CWB Toluene Micrograms/L (ug/L)
< 0.24 U
1 2
0.24 0.4 CWB 1,2 Trans-Dichloroethylene OR Trans 1,2 Dichloroethene (Ethylene dichloride)
Micrograms/L (ug/L)
< 0.34 U
1 2
0.34 0.4 CWB 1,1,1-Trichloroethane Micrograms/L (ug/L)
< 0.26 U
1 2
0.26 0.4 CWB 1,1,2-Trichloroethane Micrograms/L (ug/L)
< 0.28 U
1 2
0.28 0.4 CWB Trichloroethene (Trichloroethylene)
Micrograms/L (ug/L)
< 0.29 U
1 2
0.29 0.4 CWB Vinyl Chloride Micrograms/L (ug/L)
< 0.28 U
1 2
0.28 0.4 CWB Acenaphthene Micrograms/L (ug/L)
< 0.04 U
0.2 0.4 0.04 0.4 CWB Acenaphthylene Micrograms/L (ug/L)
< 0.07 U
0.3 0.6 0.07 0.4 Washington State Department of Ecology Discharge Monitoring Report (DMR)
Page: 2 of 5
CWB Anthracene Micrograms/L (ug/L)
< 0.05 U
0.3 0.6 0.05 0.4 CWB Benzidine Micrograms/L (ug/L)
< 9 U
12 24 9
10 CWB Butyl benzyl phthalate (Benzyl butyl phthalate)
Micrograms/L (ug/L)
< 0.03 U
0.3 0.6 0.03 0.4 CWB Benzo(a)anthracene Micrograms/L (ug/L)
< 0.05 U
0.3 0.6 0.05 0.4 CWB Benzo(b)fluoranthene (3,4
-Benzofluoranthene)
Micrograms/L (ug/L)
< 0.08 U
0.8 1.6 0.08 0.4 CWB Benzo(j)fluoranthene Micrograms/L (ug/L)
< 0.4 U
0.5 1
0.4 1
CWB Benzo(k)fluoranthene (11,12-benzofluoranthene)
Micrograms/L (ug/L)
< 0.08 U
0.8 1.6 0.08 0.4 CWB Benzo(r,s,t)pentaphene (dibenzo(a,i) pyrene)
Micrograms/L (ug/L)
< 0.3 U
0.5 1
0.3 1
CWB Benzo(a)pyrene Micrograms/L (ug/L)
< 0.05 U
0.5 1
0.05 0.4 CWB Benzo(ghi)perylene Micrograms/L (ug/L)
< 0.05 U
0.5 1
0.05 0.4 CWB Bis(2-Chloroethoxy)Methane Micrograms/L (ug/L)
< 0.06 U
5.3 21.2 0.06 0.4 CWB Bis(2-Chloroethyl)Ether Micrograms/L (ug/L)
< 0.06 U
0.3 1
0.06 0.4 CWB Bis(2-chloro methylethyl)Ether Micrograms/L (ug/L)
< 0.06*
U 5.7 17.1 0.06 0.4 CWB Bis(2-Ethylhexyl)
Phthalate Micrograms/L (ug/L)
< 0.1 U
0.1 0.5 0.1 0.4 CWB 4-Bromophenyl phenyl ether Micrograms/L (ug/L)
< 0.04 U
0.2 0.4 0.04 0.4 CWB 2-Chloronaphthalene Micrograms/L (ug/L)
< 0.05 U
0.3 0.6 0.05 0.4 CWB 4-Chlorophenyl-Phenylether Micrograms/L (ug/L)
< 0.04 U
0.3 0.5 0.04 0.4 CWB Chrysene Micrograms/L (ug/L)
< 0.06 U
0.3 0.6 0.06 0.4 CWB Dibenzo (a,h)acridine Micrograms/L (ug/L)
< 0.4*
U 2.5 10 0.4 1
CWB Dibenzo (a,j)acridine Micrograms/L (ug/L)
< 0.4*
U 2.5 10 0.4 1
CWB Dibenzo(a,h)anthracene Micrograms/L (ug/L)
< 0.05 U
0.8 1.6 0.05 0.4 CWB Dibenzo(a,e)pyrene Micrograms/L (ug/L)
< 0.5*
U 2.5 10 0.5 1
CWB Dibenzo(a,h)pyrene Micrograms/L (ug/L)
< 0.3*
U 2.5 10 0.3 1
CWB 3,3'-Dichlorobenzidine Micrograms/L (ug/L)
< 0.2 U
0.5 1
0.2 0.2 CWB Diethyl phthalate Micrograms/L (ug/L)
< 0.06 U
1.9 7.6 0.06 0.4 CWB Dimethyl phthalate Micrograms/L (ug/L)
< 0.05 U
1.6 6.4 0.05 0.4 CWB Dibutyl phthalate (Di-n-butyl phthalate)
Micrograms/L (ug/L)
< 0.07 U
0.5 1
0.07 0.4 CWB 2,4-Dinitrotoluene Micrograms/L (ug/L)
< 0.07 U
0.2 0.4 0.07 0.4 CWB 2,6-Dinitrotoluene Micrograms/L (ug/L)
< 0.09 U
0.2 0.4 0.09 0.4 CWB Di-N-Octyl Phthalate Micrograms/L (ug/L)
< 0.02 U
0.3 0.6 0.02 0.4 CWB 1,2-Diphenylhydrazine Micrograms/L (ug/L)
< 0.06*
U 5
20 0.06 0.4 CWB Fluoranthene Micrograms/L (ug/L)
< 0.05 U
0.3 0.6 0.05 0.4 CWB Fluorene Micrograms/L (ug/L)
< 0.05 U
0.3 0.6 0.05 0.4 Washington State Department of Ecology Discharge Monitoring Report (DMR)
Page: 3 of 5
Reporting Codes Used: B - Below Detection Limit/No Detection, M - Monitoring Is Conditional/Not Req This MP Outfall: 001 -
Monitoring Point Parameter Sample Date/
Statistical Base Value Notes/Comment CWB Bis(2-chloro methylethyl)Ether Micrograms/L (ug/L) 9/6/2022 Bl< 0.06 Permit references CAS 39638-32-9 CWB Dibenzo (a,h)acridine Micrograms/L (ug/L) 9/6/2022 Bl< 0.4 Method 625.1 used CWB Dibenzo (a,j)acridine Micrograms/L (ug/L) 9/6/2022 Bl< 0.4 Method 625.1 used CWB Dibenzo(a,e)pyrene Micrograms/L (ug/L) 9/6/2022 Bl< 0.5 Method 625.1 used CWB Dibenzo(a,h)pyrene Micrograms/L (ug/L) 9/6/2022 Bl< 0.3 Method 625.1 used CWB 1,2-Diphenylhydrazine Micrograms/L (ug/L) 9/6/2022 Bl< 0.06 Method 625.1 used CWB Chromium, Hexavalent Total Micrograms/L (ug/L) 9/6/2022 MlM Analysis not required CWB Cyanide Total Micrograms/L (ug/L) 9/6/2022 MlM Analysis required only 1/permit cycle.
CWB Hexachlorobenzene Micrograms/L (ug/L)
< 0.06 U
0.3 0.6 0.06 0.4 CWB Hexachlorobutadiene Micrograms/L (ug/L)
< 0.09 U
0.5 1
0.09 0.4 CWB Hexachlorocyclopentadie ne (hexachloropentadiene)
Micrograms/L (ug/L)
< 0.2 U
0.5 1
0.2 0.4 CWB Hexachloroethane Micrograms/L (ug/L)
< 0.09 U
0.5 1
0.09 0.4 CWB Indeno(1,2,3-cd)pyrene Micrograms/L (ug/L)
< 0.09 U
0.5 1
0.09 0.4 CWB Isophorone Micrograms/L (ug/L)
< 0.07 U
0.5 1
0.07 0.4 CWB 3-Methyl cholanthrene (1,2-dihydro-3-methyl-Benz[j]aceanthrylene)
Micrograms/L (ug/L)
< 0.4 U
2 8
0.4 1
CWB Naphthalene Micrograms/L (ug/L)
< 0.06 U
0.3 0.6 0.06 0.4 CWB Nitrobenzene Micrograms/L (ug/L)
< 0.05 U
0.5 1
0.05 0.4 CWB N-Nitrosodimethylamine Micrograms/L (ug/L)
< 0.3 U
2 4
0.3 0.4 CWB N-Nitrosodi-n-propylamine Micrograms/L (ug/L)
< 0.1 U
0.5 1
0.1 0.4 CWB N-Nitrosodiphenylamine Micrograms/L (ug/L)
< 0.05 U
0.5 1
0.05 0.4 CWB Perylene Micrograms/L (ug/L)
< 0.6 U
1.9 7.6 0.6 1
CWB Phenanthrene Micrograms/L (ug/L)
< 0.06 U
0.3 0.6 0.06 0.4 CWB Pyrene Micrograms/L (ug/L)
< 0.05 U
0.3 0.6 0.05 0.4 CWB 1,2,4-Trichlorobenzene Micrograms/L (ug/L)
< 0.05 U
0.3 0.6 0.05 0.4 CWB TCDD - Dioxin Picograms/L
< 1.2 U
1.3 pg/L 5 pg/L 1.2 5
Washington State Department of Ecology Discharge Monitoring Report (DMR)
Page: 4 of 5
CWB Phenolics (Total Phenols)
Total Micrograms/L (ug/L) 9/6/2022 MlM Analysis required only 1/permit cycle CWB 1,3-Dichloropropene (1,3 Dichloropropylene)
Micrograms/L (ug/L) 9/6/2022 Bl< 0.31 cis-1,3-dichloropropene and trans-1,3-dichloropropene I certify under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
Brad Barfuss Signature Date 11/17/2022 2:20:14 PM Washington State Department of Ecology Discharge Monitoring Report (DMR)
Page: 5 of 5
Burlington, WA Corporate Laboratory (a) 1620 S Walnut St - Burlington, WA 98233 - 800.755.9295
- 360.757.1400 Bellingham, WA Microbiology (b) 805 Orchard Dr Ste 4 - Bellingham, WA 98225 - 360.715.1212 Corvallis, OR Microbiology/Chemistry (d) 1100 NE Circle Blvd, Ste 130 - Corvallis, OR 97330 - 541.753.4946 Bend, OR Microbiology (e) 20332 Empire Blvd Ste 4 - Bend, OR 97701 - 541.639.8425 Portland, OR Microbiology/Chemistry (c) 9725 SW Commerce Cr Ste A2 - Wilsonville, OR 97070 - 503.682.7802 October 12, 2022 Page 1 of 1 Jane LePage 350 Hills St #107 Richland, WA 99354 Energy Northwest All samples were analyzed within the accepted holding times and were appropriately preserved and analyzed according to approved analytical protocols, unless noted in the data or QC reports. The quality control data was within laboratory acceptance limits, unless specified in the data or QC reports.
Your project: Priority Pollutants, was received on Thursday September 08, 2022.
Dear Jane LePage,
RE: 22-30019 - Priority Pollutants Respectfully If you have questions phone us at 800 755-9295.
Director of Laboratories, Vice President Lawrence J Henderson, PhD Chain of Custody QC Reports Data Report
Enclosures:
FORM: COVER Rev 2
Page 1 of 1 Burlington, WA Corporate Laboratory (a) 1620 S Walnut St - Burlington, WA 98233 - 800.755.9295
- 360.757.1400 Bellingham, WA Microbiology (b) 805 Orchard Dr Ste 4 - Bellingham, WA 98225 - 360.715.1212 Bend, OR Microbiology (e) 20332 Empire Blvd Ste 4 - Bend, OR 97701 - 541.639.8425 Corvallis, OR Microbiology/Chemistry (d) 1100 NE Circle Blvd, Ste 130 - Corvallis, OR 97330 - 541.753.4946 Portland, OR Microbiology/Chemistry (c) 9725 SW Commerce Cr Ste A2 - Wilsonville, OR 97070 - 503.682.7802 Data Report Energy Northwest Client Name:
22-30019 Reference Number:
Project: Priority Pollutants Report Date: 10/12/22 350 Hills St #107 Richland, WA 99354 Date Received:
Approved by:
9/8/22 ljh Authorized by:
Lawrence J Henderson, PhD Director of Laboratories, Vice President Sample
Description:
Lab Number: 58274 230214-01 CW 24hr Composite Sample Date: 9/6/22 8:30 am Jane LePage Collected By:
Sample Comment:
Matrix WW Analyzed Parameter Result PQL Units Comment Method Analyst Batch CAS ID#
DF MDL Lab BERYLLIUM ug/L 0.3 ND 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-41-7 1.0 0.028 a
CHROMIUM ug/L 0.5 1.4 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-47-3 1.0 0.36 a
NICKEL ug/L 0.5 6.6 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-02-0 1.0 0.1 a
COPPER ug/L 2
9.0 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-50-8 1.0 0.073 a
ZINC ug/L 2.5 11.4 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-66-6 1.0 0.79 a
ARSENIC ug/L 0.5 2.8 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-38-2 1.0 0.5 a
SELENIUM ug/L 1
1.0 200.8/TR 9/29/22 BJ 200.8_220929B2 7782-49-2 1.0 0.22 a
SILVER ug/L 0.2 ND 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-22-4 1.0 0.19 a
CADMIUM ug/L 0.25 ND 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-43-9 1.0 0.04 a
ANTIMONY ug/L 1
0.6 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-36-0 1.0 0.4 a
THALLIUM ug/L 0.36 ND 200.8/TR 9/29/22 BJ 200.8_220929B2 7440-28-0 1.0 0.04 a
LEAD ug/L 0.5 0.2 200.8/TR 9/29/22 BJ 200.8_220929B2 7439-92-1 1.0 0.091 a
If you have any questions concerning this report contact us at the above phone number.
Form: cRslt_2.rpt PQL = Practical Quantitation Limit is the lowest level that can be achieved within specified limits of precision and accuracy during routine laboratory operating conditions.
Notes:
ND = Not detected above the listed practical quantitation limit (PQL) or not above the Method Detection Limit (MDL), if requested.
D.F. - Dilution Factor
DATA REPORT WSDOE Lab C567 Page 1 of 4 Burlington, WA Corporate Laboratory (a) 1620 S Walnut St - Burlington, WA 98233 - 800.755.9295
- 360.757.1400 Bellingham, WA Microbiology (b) 805 Orchard Dr Ste 4 - Bellingham, WA 98225 - 360.715.1212 Portland, OR Microbiology/Chemistry (c) 9725 SW Commerce Cr Ste A2 - Wilsonville, OR 97070 - 503.682.7802 Bend, OR Microbiology (e) 20332 Empire Blvd Ste 4 - Bend, OR 97701 - 541.639.8425 Corvallis, OR Microbiology/Chemistry (d) 1100 NE Circle Blvd, Ste 130 - Corvallis, OR 97330 - 541.753.4946 Energy Northwest Client Name:
350 Hills St #107 Richland, WA 99354 22-30019 Reference Number:
Project: Priority Pollutants Lab Number:
Matrix:
Sample Date:
Extraction Date:
Sample
Description:
Field ID: 230214-01 CW 24hr Composite 9/6/22 Report Date:
Date Analyzed:
Analyst:
Approved By:
10/12/22 58274 Extraction Method:
Wastewater 9/9/22 3510C NML 625.1 Analytical Method:
9/23/22 Batch: 625_220909 pdm Authorized by:
Lawrence J Henderson, PhD Director of Laboratories, Vice President COMMENT UNITS MDL QL RESULT Compound CAS Flag D.F.
Lab Lab Acid Extractables 88-06-2 2,4,6-TRICHLOROPHENOL ND ug/L 1
0.1 1.00 a
120-83-2 2,4-DICHLOROPHENOL ND ug/L 1
0.2 1.00 a
105-67-9 2,4-DIMETHYLPHENOL ND ug/L 1
0.4 1.00 a
51-28-5 2,4-DINITROPHENOL ND ug/L 1
0.5 1.00 a
95-57-8 2-CHLOROPHENOL ND ug/L 1
0.1 1.00 a
88-75-5 2-NITROPHENOL ND ug/L 1
0.2 1.00 a
534-52-1 4,6-DINITRO-2-METHYLPHENOL ND ug/L 1
0.3 1.00 a
59-50-7 4-CHLORO-3-METHYLPHENOL ND ug/L 1
0.2 1.00 a
100-02-7 4-NITROPHENOL ND ug/L 1
0.3 1.00 a
87-86-5 PENTACHLOROPHENOL ND ug/L 0.4 0.2 1.00 a
108-95-2 PHENOL ND ug/L 1
0.1 1.00 a
Base/Neutral Extractables 120-82-1 1,2,4-TRICHLOROBENZENE ND ug/L 0.4 0.05 1.00 a
122-66-7 1,2-DIPHENYLHYDRAZINE ND ug/L as Azobenzene 0.4 0.06 1.00 a
121-14-2 2,4-DINITROTOLUENE ND ug/L 0.4 0.07 1.00 a
606-20-2 2,6-DINITROTOLUENE ND ug/L 0.4 0.09 1.00 a
91-58-7 2-CHLORONAPHTHALENE ND ug/L 0.4 0.05 1.00 a
91-94-1 3,3-DICHLOROBENZIDINE ND ug/L 0.2 0.2 1.00 a
101-55-3 4-BROMOPHENYL PHENYL ETHER ND ug/L 0.4 0.04 1.00 a
7005-72-3 4-CHLOROPHENYL PHENYL ETHER ND ug/L 0.4 0.04 1.00 a
83-32-9 ACENAPHTHENE ND ug/L 0.4 0.04 1.00 a
208-96-8 ACENAPHTHYLENE ND ug/L 0.4 0.07 1.00 a
120-12-7 ANTHRACENE ND ug/L 0.4 0.05 1.00 a
56-55-3 BENZ[A]ANTHRACENE ND ug/L 0.4 0.05 1.00 a
92-87-5 BENZIDINE ND ug/L screening method 10 9.
1.00 a
50-32-8 BENZO(A)PYRENE ND ug/L 0.4 0.05 1.00 a
205-99-2 BENZO[B]FLUORANTHENE ND ug/L unresolved w/
Benzo(J)Fluoranthene 0.4 0.08 1.00 a
ND - indicates the compound was not detected above the PQL or MDL.
Flags are data qualifiers. If there are data qualifiers on your report definitions can be found on an accompanying sheet.
Form: c608.rpt Lab QL = Laboratory Quantitation Limit is the lowest level that can be achieved within specified limits of precision and accuracy during routine laboratory operating conditions.
D.F. - Dilution Factor.
Notes:
If you have any questions concerning this report contact us at the above phone number.
Permit QL = Quantitation Limt required by permit (listed in Appendix A) or other regulatory requirement.
Page 2 of 4 Reference Number:
Lab Number:
Report Date: 10/12/22 22-30019 58274 Lab Number:
Matrix:
Sample Date:
Extraction Date:
Sample
Description:
Field ID: 230214-01 CW 24hr Composite 9/6/22 Report Date:
Date Analyzed:
Analyst:
Approved By:
10/12/22 58274 Extraction Method:
Wastewater 9/9/22 3510C NML 625.1 Analytical Method:
9/23/22 Batch: 625_220909 pdm COMMENT UNITS MDL QL RESULT Compound CAS Flag D.F.
Lab Lab 191-24-2 BENZO[G,H,I]PERYLENE ND ug/L 0.4 0.05 1.00 a
207-08-9 BENZO[K]FLUORANTHENE ND ug/L 0.4 0.08 1.00 a
85-68-7 BENZYL BUTYL PHTHALATE ND ug/L 0.4 0.03 1.00 a
108-60-1 BIS(2-CHLORO-1-METHYLETHYL)ETHE R
ND ug/L 0.4 0.06 1.00 a
111-91-1 Bis(2-CHLOROETHOXY)METHANE ND ug/L 0.4 0.06 1.00 a
111-44-4 BIS(2-CHLOROETHYL)ETHER ND ug/L 0.4 0.06 1.00 a
218-01-9 CHRYSENE ND ug/L 0.4 0.06 1.00 a
117-81-7 DI(2-ETHYLHEXYL)PHTHALATE ND ug/L 0.4 0.1 1.00 a
53-70-3 DIBENZO[A,H]ANTHRACENE ND ug/L 0.4 0.05 1.00 a
84-66-2 DIETHYL PHTHALATE ND ug/L 0.4 0.06 1.00 a
131-11-3 DIMETHYL PHTHALATE ND ug/L 0.4 0.05 1.00 a
84-74-2 DI-N-BUTYL PHTHALATE ND ug/L 0.4 0.07 1.00 a
117-84-0 DI-N-OCTYL PHTHALATE ND ug/L 0.4 0.02 1.00 a
206-44-0 FLUORANTHENE ND ug/L 0.4 0.05 1.00 a
86-73-7 FLUORENE ND ug/L 0.4 0.05 1.00 a
118-74-1 HEXACHLOROBENZENE ND ug/L 0.4 0.06 1.00 a
87-68-3 HEXACHLOROBUTADIENE ND ug/L 0.4 0.09 1.00 a
77-47-4 HEXACHLOROCYCLOPENTADIENE ND ug/L 0.4 0.2 1.00 a
67-72-1 HEXACHLOROETHANE ND ug/L 0.4 0.09 1.00 a
193-39-5 INDENO[1,2,3,C,D]PYRENE ND ug/L 0.4 0.09 1.00 a
78-59-1 ISOPHORONE ND ug/L 0.4 0.07 1.00 a
91-20-3 NAPHTHALENE ND ug/L 0.4 0.06 1.00 a
98-95-3 NITROBENZENE ND ug/L 0.4 0.05 1.00 a
62-75-9 N-NITROSODIMETHYLAMINE ND ug/L 0.4 0.3 1.00 a
621-64-7 N-NITROSODI-N-PROPYLAMINE ND ug/L 0.4 0.1 1.00 a
86-30-6 N-NITROSODIPHENYLAMINE ND ug/L as Diphenylamine 0.4 0.05 1.00 a
85-01-8 PHENANTHRENE ND ug/L 0.4 0.06 1.00 a
129-00-0 PYRENE ND ug/L 0.4 0.05 1.00 a
Ecology Priority Toxic Chemicals 56-49-5 3-METHYL CHOLANTHRENE ND ug/L 1
0.4 1.00 a
205-82-3 BENZO(J)FLUORANTHENE ND ug/L unresolved w/
Benzo(B)Fluoranthene 1
0.4 1.00 a
189-55-9 BENZO(R,S,T)PENTAPHENE ND ug/L 1
0.3 1.00 a
192-65-4 DIBENZO(A,E)PYRENE ND ug/L 1
0.5 1.00 a
226-36-8 DIBENZO(A,H)ACRIDINE ND ug/L 1
0.4 1.00 a
189-64-0 DIBENZO(A,H)PYRENE ND ug/L 1
0.3 1.00 a
224-42-0 DIBENZO(A,J)ACRIDINE ND ug/L 1
0.4 1.00 a
198-55-0 PERYLENE ND ug/L 1
0.6 1.00 a
ND - indicates the compound was not detected above the PQL or MDL.
Flags are data qualifiers. If there are data qualifiers on your report definitions can be found on an accompanying sheet.
Form: c608.rpt Lab QL = Laboratory Quantitation Limit is the lowest level that can be achieved within specified limits of precision and accuracy during routine laboratory operating conditions.
D.F. - Dilution Factor.
Notes:
Permit QL = Quantitation Limt required by permit (listed in Appendix A) or other regulatory requirement.
Page 3 of 4 Reference Number:
Lab Number:
Report Date: 10/12/22 22-30019 58275 Lab Number:
Matrix:
Sample Date:
Extraction Date:
Sample
Description:
Field ID: 230214-02 CW Grab 9/6/22 Report Date:
Date Analyzed:
Analyst:
Approved By:
10/12/22 58275 Extraction Method:
Wastewater 9/9/22 5030B NML 624(pH4)
Analytical Method:
9/9/22 Batch: 624_220909 pdm COMMENT UNITS MDL QL RESULT Compound CAS Flag D.F.
Lab Lab 107-02-8 ACROLEIN ND ug/L 2.0 0.42 1.00 a
107-13-1 ACRYLONITRILE ND ug/L 2.0 0.56 1.00 a
ND - indicates the compound was not detected above the PQL or MDL.
Flags are data qualifiers. If there are data qualifiers on your report definitions can be found on an accompanying sheet.
Form: c608.rpt Lab QL = Laboratory Quantitation Limit is the lowest level that can be achieved within specified limits of precision and accuracy during routine laboratory operating conditions.
D.F. - Dilution Factor.
Notes:
Permit QL = Quantitation Limt required by permit (listed in Appendix A) or other regulatory requirement.
Page 4 of 4 Reference Number:
Lab Number:
Report Date: 10/12/22 22-30019 58275 Lab Number:
Matrix:
Sample Date:
Extraction Date:
Sample
Description:
Field ID: 230214-02 CW Grab 9/6/22 Report Date:
Date Analyzed:
Analyst:
Approved By:
10/12/22 58275 Extraction Method:
Wastewater 9/9/22 5030B NML 624.1 Analytical Method:
9/9/22 Batch: 624_220909 pdm COMMENT UNITS MDL QL RESULT Compound CAS Flag D.F.
Lab Lab 71-43-2 BENZENE ND ug/L 0.4 0.23 1.00 a
75-27-4 BROMODICHLOROMETHANE ND ug/L 0.4 0.28 1.00 a
75-25-2 BROMOFORM ND ug/L 0.4 0.26 1.00 a
74-83-9 BROMOMETHANE ND ug/L 0.4 0.37 1.00 a
56-23-5 CARBON TETRACHLORIDE ND ug/L 0.4 0.24 1.00 a
108-90-7 CHLOROBENZENE ND ug/L 0.4 0.28 1.00 a
75-00-3 CHLOROETHANE ND ug/L 0.4 0.34 1.00 a
110-75-8 2-CHLOROETHYL VINYL ETHER ND ug/L 2.0 0.46 1.00 a
67-66-3 CHLOROFORM 2.2 ug/L 0.4 0.25 1.00 a
74-87-3 CHLOROMETHANE ND ug/L 0.4 0.28 1.00 a
124-48-1 CHLORODIBROMOMETHANE ND ug/L 0.4 0.28 1.00 a
95-50-1 1,2-DICHLOROBENZENE ND ug/L 0.4 0.31 1.00 a
541-73-1 1,3-DICHLOROBENZENE ND ug/L 0.4 0.29 1.00 a
106-46-7 1,4-DICHLOROBENZENE ND ug/L 0.4 0.29 1.00 a
75-34-3 1,1 - DICHLOROETHANE ND ug/L 0.4 0.32 1.00 a
107-06-2 1,2 - DICHLOROETHANE ND ug/L 0.4 0.38 1.00 a
75-35-4 1,1 - DICHLOROETHYLENE ND ug/L 0.4 0.25 1.00 a
156-60-5 T - 1,2 - DICHLOROETHYLENE ND ug/L 0.4 0.34 1.00 a
75-71-8 DICHLORODIFLUOROMETHANE ND ug/L 0.5 0.21 1.00 a
78-87-5 1,2 - DICHLOROPROPANE ND ug/L 0.4 0.22 1.00 a
10061-01-5 CIS - 1,3 - DICHLOROPROPENE ND ug/L 0.4 0.31 1.00 a
10061-02-6 TRANS-1,3 - DICHLOROPROPENE ND ug/L 0.4 0.24 1.00 a
100-41-4 ETHYLBENZENE ND ug/L 0.4 0.29 1.00 a
75-09-2 METHYLENE CHLORIDE ND ug/L 0.4 0.28 1.00 a
79-34-5 1,1,2,2 - TETRACHLOROETHANE ND ug/L 0.4 0.37 1.00 a
127-18-4 TETRACHLOROETHYLENE ND ug/L 0.4 0.24 1.00 a
108-88-3 TOLUENE ND ug/L 0.4 0.24 1.00 a
71-55-6 1,1,1 - TRICHLOROETHANE ND ug/L 0.4 0.26 1.00 a
79-00-5 1,1,2 - TRICHLOROETHANE ND ug/L 0.4 0.28 1.00 a
79-01-6 TRICHLOROETHYLENE ND ug/L 0.4 0.29 1.00 a
75-69-4 TRICHLOROFLUOROMETHANE ND ug/L 0.5 0.18 1.00 a
75-01-4 VINYL CHLORIDE ND ug/L 0.4 0.28 1.00 a
ND - indicates the compound was not detected above the PQL or MDL.
Flags are data qualifiers. If there are data qualifiers on your report definitions can be found on an accompanying sheet.
Form: c608.rpt Lab QL = Laboratory Quantitation Limit is the lowest level that can be achieved within specified limits of precision and accuracy during routine laboratory operating conditions.
D.F. - Dilution Factor.
Notes:
Permit QL = Quantitation Limt required by permit (listed in Appendix A) or other regulatory requirement.
Page 1 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Calibration Check 200.8_220929B2 ANTIMONY 0.00093 0.001 mg/L 200.8 93 80-120 CAL 0
ARSENIC 0.00101 0.001 mg/L 200.8 101 80-120 CAL 0
BERYLLIUM 0.001 0.001 mg/L 200.8 100 80-120 CAL 0
CADMIUM 0.00099 0.001 mg/L 200.8 99 80-120 CAL 0
CHROMIUM 0.00101 0.001 mg/L 200.8 101 80-120 CAL 0
COPPER 0.00103 0.001 mg/L 200.8 103 80-120 CAL 0
LEAD 0.001 0.001 mg/L 200.8 100 80-120 CAL 0
NICKEL 0.00102 0.001 mg/L 200.8 102 80-120 CAL 0
SELENIUM 0.00098 0.001 mg/L 200.8 98 80-120 CAL 0
SILVER 0.001 0.001 mg/L 200.8 100 80-120 CAL 0
THALLIUM 0.00101 0.001 mg/L 200.8 101 80-120 CAL 0
ZINC 0.00104 0.001 mg/L 200.8 104 80-120 CAL 0
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 2 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Laboratory Fortified Blank 200.8_220929B2 ANTIMONY 0.0119 0.0125 mg/L 200.8 95 85-115 LFB 0
ARSENIC 0.0123 0.0125 mg/L 200.8 98 85-115 LFB 0
BERYLLIUM 0.0129 0.0125 mg/L 200.8 103 85-115 LFB 0
CADMIUM 0.0124 0.0125 mg/L 200.8 99 85-115 LFB 0
CHROMIUM 0.0132 0.0125 mg/L 200.8 106 85-115 LFB 0
COPPER 0.0135 0.0125 mg/L 200.8 108 85-115 LFB 0
LEAD 0.0124 0.0125 mg/L 200.8 99 85-115 LFB 0
NICKEL 0.013 0.0125 mg/L 200.8 104 85-115 LFB 0
SELENIUM 0.0115 0.0125 mg/L 200.8 92 85-115 LFB 0
SILVER 0.0056 0.00625 mg/L 200.8 90 85-115 LFB 0
THALLIUM 0.0123 0.0125 mg/L 200.8 98 85-115 LFB 0
ZINC 0.0128 0.0125 mg/L 200.8 102 85-115 LFB 0
624_220909 1,1 - DICHLOROETHANE 8.8 10 ug/L 624.1 88 70-130 LFB 0
1,1 - DICHLOROETHYLENE 8.6 10 ug/L 624.1 86 50-150 LFB 0
1,1,1 - TRICHLOROETHANE 8.7 10 ug/L 624.1 87 70-130 LFB 0
1,1,2 - TRICHLOROETHANE 8.8 10 ug/L 624.1 88 70-130 LFB 0
1,1,2,2 - TETRACHLOROETHANE 9.9 10 ug/L 624.1 99 60-140 LFB 0
1,2 - DICHLOROETHANE 9.1 10 ug/L 624.1 91 70-130 LFB 0
1,2 - DICHLOROPROPANE 8.5 10 ug/L 624.1 85 35-165 LFB 0
1,2-DICHLOROBENZENE 10.6 10 ug/L 624.1 106 65-135 LFB 0
1,3-DICHLOROBENZENE 10.6 10 ug/L 624.1 106 70-130 LFB 0
1,4-DICHLOROBENZENE 10.7 10 ug/L 624.1 107 65-135 LFB 0
2-CHLOROETHYL VINYL ETHER 7.8 10 ug/L 624.1 78 1-225 LFB 0
BENZENE 8.8 10 ug/L 624.1 88 65-135 LFB 0
BROMODICHLOROMETHANE 9.1 10 ug/L 624.1 91 65-135 LFB 0
BROMOFORM 10.9 10 ug/L 624.1 109 70-130 LFB 0
BROMOMETHANE 8.2 10 ug/L 624.1 82 15-185 LFB 0
CARBON TETRACHLORIDE 8.7 10 ug/L 624.1 87 70-130 LFB 0
CHLOROBENZENE 9.8 10 ug/L 624.1 98 65-135 LFB 0
CHLORODIBROMOMETHANE 9.2 10 ug/L 624.1 92 70-135 LFB 0
CHLOROETHANE 9.2 10 ug/L 624.1 92 40-160 LFB 0
CHLOROFORM 9.5 10 ug/L 624.1 95 70-135 LFB 0
CHLOROMETHANE 8.1 10 ug/L 624.1 81 1-205 LFB 0
CIS - 1,3 - DICHLOROPROPENE 9.2 10 ug/L 624.1 92 25-175 LFB 0
DICHLORODIFLUOROMETHANE 6.8 10 ug/L 624.1 68 60-140 LFB 0
ETHYLBENZENE 10.2 10 ug/L 624.1 102 60-140 LFB 0
METHYLENE CHLORIDE 8.8 10 ug/L 624.1 88 60-140 LFB 0
T - 1,2 - DICHLOROETHYLENE 8.5 10 ug/L 624.1 85 70-130 LFB 0
TETRACHLOROETHYLENE 8.9 10 ug/L 624.1 89 70-130 LFB 0
TOLUENE 8.6 10 ug/L 624.1 86 70-130 LFB 0
TRANS-1,3 - DICHLOROPROPENE 9.2 10 ug/L 624.1 92 50-150 LFB 0
TRICHLOROETHYLENE 8.9 10 ug/L 624.1 89 65-135 LFB 0
TRICHLOROFLUOROMETHANE 9.2 10 ug/L 624.1 92 50-150 LFB 0
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 3 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Laboratory Fortified Blank 624_220909 VINYL CHLORIDE 7.9 10 ug/L 624.1 79 5-195 LFB 0
ACROLEIN 8.0 10 ug/L 624.1 80 60-140 LFB 0
ACRYLONITRILE 8.8 10 ug/L 624.1 88 60-140 LFB 0
625_220909 2 - FLUOROBIPHENYL (Surr) 78 625.1 53-140 LFB 0
2 - FLUOROPHENOL (Surr) 53 625.1 29-140 LFB 0
2,4,6 - TRIBROMOPHENOL (Surr) 90 625.1 39-140 LFB 0
d5-NITROBENZENE (Surr) 78 625.1 50-140 LFB 0
d5-PHENOL (Surr) 34 625.1 23-140 LFB 0
p-TERPHENYL-d14 (Surr) 87 625.1 60-140 LFB 0
2,4,6-TRICHLOROPHENOL 7.8 10 ug/L 625.1 78 52-129 LFB 0
2,4-DICHLOROPHENOL 7.4 10 ug/L 625.1 74 53-122 LFB 0
2,4-DIMETHYLPHENOL 5.5 10 ug/L 625.1 55 42-120 LFB 0
2,4-DINITROPHENOL 4.9 10 ug/L 625.1 49 1-173 LFB 0
2-CHLOROPHENOL 6.9 10 ug/L 625.1 69 36-120 LFB 0
2-NITROPHENOL 7.3 10 ug/L 625.1 73 45-167 LFB 0
4,6-DINITRO-2-METHYLPHENOL 7.6 10 ug/L 625.1 76 53-130 LFB 0
4-CHLORO-3-METHYLPHENOL 8.2 10 ug/L 625.1 82 41-128 LFB 0
4-NITROPHENOL 3.1 10 ug/L 625.1 31 13-129 LFB 0
PENTACHLOROPHENOL 4.9 10 ug/L 625.1 49 38-152 LFB 0
PHENOL 3.4 10 ug/L 625.1 34 17-120 LFB 0
1,2,4-TRICHLOROBENZENE 6.7 10 ug/L 625.1 67 57-130 LFB 0
1,2-DIPHENYLHYDRAZINE 7.3 10 ug/L 625.1 73 71-125 LFB 0
2,4-DINITROTOLUENE 8.6 10 ug/L 625.1 86 48-127 LFB 0
2,6-DINITROTOLUENE 8.2 10 ug/L 625.1 82 68-137 LFB 0
2-CHLORONAPHTHALENE 7.3 10 ug/L 625.1 73 65-120 LFB 0
3,3-DICHLOROBENZIDINE 0.9 1
ug/L 625.1 90 8-213 LFB 0
4-BROMOPHENYL PHENYL ETHER 8.2 10 ug/L 625.1 82 65-120 LFB 0
4-CHLOROPHENYL PHENYL ETHER 8.4 10 ug/L 625.1 84 38-145 LFB 0
ACENAPHTHENE 8.0 10 ug/L 625.1 80 60-132 LFB 0
ACENAPHTHYLENE 7.9 10 ug/L 625.1 79 54-126 LFB 0
ANTHRACENE 8.3 10 ug/L 625.1 83 43-120 LFB 0
BENZ[A]ANTHRACENE 9.0 10 ug/L 625.1 90 42-133 LFB 0
BENZIDINE 10.0 25 ug/L 625.1 40 1-125 LFB 0
BENZO(A)PYRENE 7.6 10 ug/L 625.1 76 32-148 LFB 0
BENZO[B]FLUORANTHENE 15.1 20 ug/L 625.1 76 42-140 LFB 0
BENZO[G,H,I]PERYLENE 6.8 10 ug/L 625.1 68 1-195 LFB 0
BENZO[K]FLUORANTHENE 8.7 10 ug/L 625.1 87 25-146 LFB 0
BENZYL BUTYL PHTHALATE 8.0 10 ug/L 625.1 80 1-140 LFB 0
BIS(2-CHLORO-1-METHYLETHYL)ETHER 7.1 10 ug/L 625.1 71 63-139 LFB 0
Bis(2-CHLOROETHOXY)METHANE 7.6 10 ug/L 625.1 76 49-165 LFB 0
BIS(2-CHLOROETHYL)ETHER 7.0 10 ug/L 625.1 70 43-126 LFB 0
CHRYSENE 9.1 10 ug/L 625.1 91 44-140 LFB 0
DI(2-ETHYLHEXYL)PHTHALATE 6.4 10 ug/L 625.1 64 29-137 LFB 0
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 4 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Laboratory Fortified Blank 625_220909 DIBENZO[A,H]ANTHRACENE 5.2 10 ug/L 625.1 52 1-200 LFB 0
DIETHYL PHTHALATE 8.2 10 ug/L 625.1 82 1-120 LFB 0
DIMETHYL PHTHALATE 7.1 10 ug/L 625.1 71 1-120 LFB 0
DI-N-BUTYL PHTHALATE 8.7 10 ug/L 625.1 87 8-120 LFB 0
DI-N-OCTYL PHTHALATE 5.5 10 ug/L 625.1 55 19-132 LFB 0
FLUORANTHENE 8.4 10 ug/L 625.1 84 43-121 LFB 0
FLUORENE 8.0 10 ug/L 625.1 80 70-120 LFB 0
HEXACHLOROBENZENE 8.5 10 ug/L 625.1 85 8-142 LFB 0
HEXACHLOROBUTADIENE 6.1 10 ug/L 625.1 61 38-120 LFB 0
HEXACHLOROCYCLOPENTADIENE 6.2 10 ug/L 625.1 62 14-170 LFB 0
HEXACHLOROETHANE 5.9 10 ug/L 625.1 59 55-120 LFB 0
INDENO[1,2,3,C,D]PYRENE 6.8 10 ug/L 625.1 68 1-151 LFB 0
ISOPHORONE 8.0 10 ug/L 625.1 80 47-180 LFB 0
NAPHTHALENE 7.0 10 ug/L 625.1 70 36-120 LFB 0
NITROBENZENE 7.3 10 ug/L 625.1 73 54-158 LFB 0
N-NITROSODIMETHYLAMINE 5.3 10 ug/L 625.1 53 20-116 LFB 0
N-NITROSODI-N-PROPYLAMINE 7.6 10 ug/L 625.1 76 14-198 LFB 0
N-NITROSODIPHENYLAMINE 8.8 10 ug/L 625.1 88 65-137 LFB 0
PHENANTHRENE 8.4 10 ug/L 625.1 84 65-120 LFB 0
PYRENE 8.9 10 ug/L 625.1 89 70-120 LFB 0
3-METHYL CHOLANTHRENE 7.4 10 ug/L 625.1 74 57-119 LFB 0
BENZO(J)FLUORANTHENE 15.8 20 ug/L 625.1 79 42-140 LFB 0
BENZO(R,S,T)PENTAPHENE 7.3 10 ug/L 625.1 73 1-172 LFB 0
DIBENZO(A,E)PYRENE 6.8 10 ug/L 625.1 68 1-199 LFB 0
DIBENZO(A,H)ACRIDINE 9.1 10 ug/L 625.1 91 60-131 LFB 0
DIBENZO(A,H)PYRENE 6.4 10 ug/L 625.1 64 4-160 LFB 0
DIBENZO(A,J)ACRIDINE 8.9 10 ug/L 625.1 89 55-136 LFB 0
PERYLENE 6.5 10 ug/L 625.1 65 57-125 LFB 0
Laboratory Reagent Blank 200.8_220929B2 ANTIMONY ND mg/L 200.8 0-0 LRB 0
ARSENIC ND mg/L 200.8 0-0 LRB 0
BERYLLIUM ND mg/L 200.8 0-0 LRB 0
CADMIUM ND mg/L 200.8 0-0 LRB 0
CHROMIUM ND mg/L 200.8 0-0 LRB 0
COPPER ND mg/L 200.8 0-0 LRB 0
LEAD ND mg/L 200.8 0-0 LRB 0
NICKEL ND mg/L 200.8 0-0 LRB 0
SELENIUM ND mg/L 200.8 0-0 LRB 0
SILVER ND mg/L 200.8 0-0 LRB 0
THALLIUM ND mg/L 200.8 0-0 LRB 0
ZINC ND mg/L 200.8 0-0 LRB 0
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 5 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Method Blank 200.8_220929B2 ANTIMONY ND mg/L 200.8 0-0 MB 0
ARSENIC ND mg/L 200.8 0-0 MB 0
BERYLLIUM ND mg/L 200.8 0-0 MB 0
CADMIUM ND mg/L 200.8 0-0 MB 0
CHROMIUM ND mg/L 200.8 0-0 MB 0
COPPER ND mg/L 200.8 0-0 MB 0
LEAD ND mg/L 200.8 0-0 MB 0
NICKEL ND mg/L 200.8 0-0 MB 0
SELENIUM ND mg/L 200.8 0-0 MB 0
SILVER ND mg/L 200.8 0-0 MB 0
THALLIUM ND mg/L 200.8 0-0 MB 0
ZINC ND mg/L 200.8 0-0 MB 0
624_220909 1,1 - DICHLOROETHANE ND ug/L 624.1 0-0 MB 0
1,1 - DICHLOROETHYLENE ND ug/L 624.1 0-0 MB 0
1,1,1 - TRICHLOROETHANE ND ug/L 624.1 0-0 MB 0
1,1,2 - TRICHLOROETHANE ND ug/L 624.1 0-0 MB 0
1,1,2,2 - TETRACHLOROETHANE ND ug/L 624.1 0-0 MB 0
1,2 - DICHLOROETHANE ND ug/L 624.1 0-0 MB 0
1,2 - DICHLOROPROPANE ND ug/L 624.1 0-0 MB 0
1,2-DICHLOROBENZENE ND ug/L 624.1 0-0 MB 0
1,3-DICHLOROBENZENE ND ug/L 624.1 0-0 MB 0
1,4-DICHLOROBENZENE ND ug/L 624.1 0-0 MB 0
2-CHLOROETHYL VINYL ETHER ND ug/L 624.1 0-0 MB 0
BENZENE ND ug/L 624.1 0-0 MB 0
BROMODICHLOROMETHANE ND ug/L 624.1 0-0 MB 0
BROMOFORM ND ug/L 624.1 0-0 MB 0
BROMOMETHANE ND ug/L 624.1 0-0 MB 0
CARBON TETRACHLORIDE ND ug/L 624.1 0-0 MB 0
CHLOROBENZENE ND ug/L 624.1 0-0 MB 0
CHLORODIBROMOMETHANE ND ug/L 624.1 0-0 MB 0
CHLOROETHANE ND ug/L 624.1 0-0 MB 0
CHLOROFORM ND ug/L 624.1 0-0 MB 0
CHLOROMETHANE ND ug/L 624.1 0-0 MB 0
CIS - 1,3 - DICHLOROPROPENE ND ug/L 624.1 0-0 MB 0
DICHLORODIFLUOROMETHANE ND ug/L 624.1 0-0 MB 0
ETHYLBENZENE ND ug/L 624.1 0-0 MB 0
METHYLENE CHLORIDE ND ug/L 624.1 0-0 MB 0
T - 1,2 - DICHLOROETHYLENE ND ug/L 624.1 0-0 MB 0
TETRACHLOROETHYLENE ND ug/L 624.1 0-0 MB 0
TOLUENE ND ug/L 624.1 0-0 MB 0
TRANS-1,3 - DICHLOROPROPENE ND ug/L 624.1 0-0 MB 0
TRICHLOROETHYLENE ND ug/L 624.1 0-0 MB 0
TRICHLOROFLUOROMETHANE ND ug/L 624.1 0-0 MB 0
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 6 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Method Blank 624_220909 VINYL CHLORIDE ND ug/L 624.1 0-0 MB 0
ACROLEIN ND ug/L 624.1 0-0 MB 0
ACRYLONITRILE ND ug/L 624.1 0-0 MB 0
1,1 - DICHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,1 - DICHLOROETHYLENE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,1,1 - TRICHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,1,2 - TRICHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,1,2,2 - TETRACHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,2 - DICHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,2 - DICHLOROPROPANE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,2-DICHLOROBENZENE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,3-DICHLOROBENZENE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,4-DICHLOROBENZENE ND ug/L 624.1 0-0 MB TB 22-29690 1
2-CHLOROETHYL VINYL ETHER ND ug/L 624.1 0-0 MB TB 22-29690 1
BENZENE ND ug/L 624.1 0-0 MB TB 22-29690 1
BROMODICHLOROMETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
BROMOFORM ND ug/L 624.1 0-0 MB TB 22-29690 1
BROMOMETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
CARBON TETRACHLORIDE ND ug/L 624.1 0-0 MB TB 22-29690 1
CHLOROBENZENE ND ug/L 624.1 0-0 MB TB 22-29690 1
CHLORODIBROMOMETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
CHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
CHLOROFORM ND ug/L 624.1 0-0 MB TB 22-29690 1
CHLOROMETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
CIS - 1,3 - DICHLOROPROPENE ND ug/L 624.1 0-0 MB TB 22-29690 1
DICHLORODIFLUOROMETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
ETHYLBENZENE ND ug/L 624.1 0-0 MB TB 22-29690 1
METHYLENE CHLORIDE ND ug/L 624.1 0-0 MB TB 22-29690 1
T - 1,2 - DICHLOROETHYLENE ND ug/L 624.1 0-0 MB TB 22-29690 1
TETRACHLOROETHYLENE ND ug/L 624.1 0-0 MB TB 22-29690 1
TOLUENE ND ug/L 624.1 0-0 MB TB 22-29690 1
TRANS-1,3 - DICHLOROPROPENE ND ug/L 624.1 0-0 MB TB 22-29690 1
TRICHLOROETHYLENE ND ug/L 624.1 0-0 MB TB 22-29690 1
TRICHLOROFLUOROMETHANE ND ug/L 624.1 0-0 MB TB 22-29690 1
VINYL CHLORIDE ND ug/L 624.1 0-0 MB TB 22-29690 1
ACROLEIN ND ug/L 624.1 0-0 MB TB 22-29690 1
ACRYLONITRILE ND ug/L 624.1 0-0 MB TB 22-29690 1
1,1 - DICHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
1,1 - DICHLOROETHYLENE ND ug/L 624.1 0-0 MB TB 22-30019 2
1,1,1 - TRICHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
1,1,2 - TRICHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
1,1,2,2 - TETRACHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
1,2 - DICHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 7 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Method Blank 624_220909 1,2 - DICHLOROPROPANE ND ug/L 624.1 0-0 MB TB 22-30019 2
1,2-DICHLOROBENZENE ND ug/L 624.1 0-0 MB TB 22-30019 2
1,3-DICHLOROBENZENE ND ug/L 624.1 0-0 MB TB 22-30019 2
1,4-DICHLOROBENZENE ND ug/L 624.1 0-0 MB TB 22-30019 2
2-CHLOROETHYL VINYL ETHER ND ug/L 624.1 0-0 MB TB 22-30019 2
BENZENE ND ug/L 624.1 0-0 MB TB 22-30019 2
BROMODICHLOROMETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
BROMOFORM ND ug/L 624.1 0-0 MB TB 22-30019 2
BROMOMETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
CARBON TETRACHLORIDE ND ug/L 624.1 0-0 MB TB 22-30019 2
CHLOROBENZENE ND ug/L 624.1 0-0 MB TB 22-30019 2
CHLORODIBROMOMETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
CHLOROETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
CHLOROFORM ND ug/L 624.1 0-0 MB TB 22-30019 2
CHLOROMETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
CIS - 1,3 - DICHLOROPROPENE ND ug/L 624.1 0-0 MB TB 22-30019 2
DICHLORODIFLUOROMETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
ETHYLBENZENE ND ug/L 624.1 0-0 MB TB 22-30019 2
METHYLENE CHLORIDE ND ug/L 624.1 0-0 MB TB 22-30019 2
T - 1,2 - DICHLOROETHYLENE ND ug/L 624.1 0-0 MB TB 22-30019 2
TETRACHLOROETHYLENE ND ug/L 624.1 0-0 MB TB 22-30019 2
TOLUENE ND ug/L 624.1 0-0 MB TB 22-30019 2
TRANS-1,3 - DICHLOROPROPENE ND ug/L 624.1 0-0 MB TB 22-30019 2
TRICHLOROETHYLENE ND ug/L 624.1 0-0 MB TB 22-30019 2
TRICHLOROFLUOROMETHANE ND ug/L 624.1 0-0 MB TB 22-30019 2
VINYL CHLORIDE ND ug/L 624.1 0-0 MB TB 22-30019 2
ACROLEIN ND ug/L 624.1 0-0 MB TB 22-30019 2
ACRYLONITRILE ND ug/L 624.1 0-0 MB TB 22-30019 2
625_220909 2 - FLUOROBIPHENYL (Surr) 43 625.1 53-140 SA MB 0
2 - FLUOROPHENOL (Surr) 36 625.1 29-140 MB 0
2,4,6 - TRIBROMOPHENOL (Surr) 48 625.1 39-140 MB 0
d5-NITROBENZENE (Surr) 51 625.1 50-140 MB 0
d5-PHENOL (Surr) 21 625.1 23-140 SA MB 0
p-TERPHENYL-d14 (Surr) 48 625.1 60-140 SA MB 0
2,4,6-TRICHLOROPHENOL ND ug/L 625.1 0-0 MB 0
2,4-DICHLOROPHENOL ND ug/L 625.1 0-0 MB 0
2,4-DIMETHYLPHENOL ND ug/L 625.1 0-0 MB 0
2,4-DINITROPHENOL ND ug/L 625.1 0-0 MB 0
2-CHLOROPHENOL ND ug/L 625.1 0-0 MB 0
2-NITROPHENOL ND ug/L 625.1 0-0 MB 0
4,6-DINITRO-2-METHYLPHENOL ND ug/L 625.1 0-0 MB 0
4-CHLORO-3-METHYLPHENOL ND ug/L 625.1 0-0 MB 0
4-NITROPHENOL ND ug/L 625.1 0-0 MB 0
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 8 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Method Blank 625_220909 PENTACHLOROPHENOL ND ug/L 625.1 0-0 MB 0
PHENOL ND ug/L 625.1 0-0 MB 0
1,2,4-TRICHLOROBENZENE ND ug/L 625.1 0-0 MB 0
1,2-DIPHENYLHYDRAZINE ND ug/L 625.1 0-0 MB 0
2,4-DINITROTOLUENE ND ug/L 625.1 0-0 MB 0
2,6-DINITROTOLUENE ND ug/L 625.1 0-0 MB 0
2-CHLORONAPHTHALENE ND ug/L 625.1 0-0 MB 0
3,3-DICHLOROBENZIDINE ND ug/L 625.1 0-0 MB 0
4-BROMOPHENYL PHENYL ETHER ND ug/L 625.1 0-0 MB 0
4-CHLOROPHENYL PHENYL ETHER ND ug/L 625.1 0-0 MB 0
ACENAPHTHENE ND ug/L 625.1 0-0 MB 0
ACENAPHTHYLENE ND ug/L 625.1 0-0 MB 0
ANTHRACENE ND ug/L 625.1 0-0 MB 0
BENZ[A]ANTHRACENE ND ug/L 625.1 0-0 MB 0
BENZIDINE ND ug/L 625.1 0-0 MB 0
BENZO(A)PYRENE ND ug/L 625.1 0-0 MB 0
BENZO[B]FLUORANTHENE ND ug/L 625.1 0-0 MB 0
BENZO[G,H,I]PERYLENE ND ug/L 625.1 0-0 MB 0
BENZO[K]FLUORANTHENE ND ug/L 625.1 0-0 MB 0
BENZYL BUTYL PHTHALATE ND ug/L 625.1 0-0 MB 0
BIS(2-CHLORO-1-METHYLETHYL)ETHER ND ug/L 625.1 0-0 MB 0
Bis(2-CHLOROETHOXY)METHANE ND ug/L 625.1 0-0 MB 0
BIS(2-CHLOROETHYL)ETHER ND ug/L 625.1 0-0 MB 0
CHRYSENE ND ug/L 625.1 0-0 MB 0
DI(2-ETHYLHEXYL)PHTHALATE ND ug/L 625.1 0-0 MB 0
DIBENZO[A,H]ANTHRACENE ND ug/L 625.1 0-0 MB 0
DIETHYL PHTHALATE ND ug/L 625.1 0-0 MB 0
DIMETHYL PHTHALATE ND ug/L 625.1 0-0 MB 0
DI-N-BUTYL PHTHALATE ND ug/L 625.1 0-0 MB 0
DI-N-OCTYL PHTHALATE ND ug/L 625.1 0-0 MB 0
FLUORANTHENE ND ug/L 625.1 0-0 MB 0
FLUORENE ND ug/L 625.1 0-0 MB 0
HEXACHLOROBENZENE ND ug/L 625.1 0-0 MB 0
HEXACHLOROBUTADIENE ND ug/L 625.1 0-0 MB 0
HEXACHLOROCYCLOPENTADIENE ND ug/L 625.1 0-0 MB 0
HEXACHLOROETHANE ND ug/L 625.1 0-0 MB 0
INDENO[1,2,3,C,D]PYRENE ND ug/L 625.1 0-0 MB 0
ISOPHORONE ND ug/L 625.1 0-0 MB 0
NAPHTHALENE ND ug/L 625.1 0-0 MB 0
NITROBENZENE ND ug/L 625.1 0-0 MB 0
N-NITROSODIMETHYLAMINE ND ug/L 625.1 0-0 MB 0
N-NITROSODI-N-PROPYLAMINE ND ug/L 625.1 0-0 MB 0
N-NITROSODIPHENYLAMINE ND ug/L 625.1 0-0 MB 0
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 9 of 9 SAMPLE INDEPENDENT QUALITY CONTROL REPORT Reference Number:
10/12/22 Report Date:
22-30019 Batch Analyte Result True Value Units Method Recovery Limits* Qualifier Comment QC Type QC Method Blank 625_220909 PHENANTHRENE ND ug/L 625.1 0-0 MB 0
PYRENE ND ug/L 625.1 0-0 MB 0
3-METHYL CHOLANTHRENE ND ug/L 625.1 0-0 MB 0
BENZO(J)FLUORANTHENE ND ug/L 625.1 0-0 MB 0
BENZO(R,S,T)PENTAPHENE ND ug/L 625.1 0-0 MB 0
DIBENZO(A,E)PYRENE ND ug/L 625.1 0-0 MB 0
DIBENZO(A,H)ACRIDINE ND ug/L 625.1 0-0 MB 0
DIBENZO(A,H)PYRENE ND ug/L 625.1 0-0 MB 0
DIBENZO(A,J)ACRIDINE ND ug/L 625.1 0-0 MB 0
PERYLENE ND ug/L 625.1 0-0 MB 0
Quality Control Sample 200.8_220929B2 ANTIMONY 0.039 0.04 mg/L 200.8 98 90-110 QCS 0
ARSENIC 0.0397 0.04 mg/L 200.8 99 90-110 QCS 0
BERYLLIUM 0.0395 0.04 mg/L 200.8 99 90-110 QCS 0
CADMIUM 0.0395 0.04 mg/L 200.8 99 90-110 QCS 0
CHROMIUM 0.0407 0.04 mg/L 200.8 102 90-110 QCS 0
COPPER 0.0404 0.04 mg/L 200.8 101 90-110 QCS 0
LEAD 0.0392 0.04 mg/L 200.8 98 90-110 QCS 0
NICKEL 0.0401 0.04 mg/L 200.8 100 90-110 QCS 0
SELENIUM 0.0393 0.04 mg/L 200.8 98 90-110 QCS 0
SILVER 0.021 0.02 mg/L 200.8 105 90-110 QCS 0
THALLIUM 0.0389 0.04 mg/L 200.8 97 90-110 QCS 0
ZINC 0.0364 0.04 mg/L 200.8 91 90-110 QCS 0
- Notation:
% Recovery = (Result of Analysis)/(True Value)
- 100 NA = Indicates % Recovery could not be calculated.
Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QCIndependent4.rpt
Page 1 of 5 Reference Number: 22-30019 Report Date: 10/12/2022 SAMPLE DEPENDENT QUALITY CONTROL REPORT Duplicate, Matrix Spike/Matrix Spike Duplicate and Confirmation Result Report Duplicate Type
%RPD Limits Qualifier Comments Result Result Units Sample Analyte Batch QC Duplicate 200.8_220929B2 52725 ARSENIC 0.0024 mg/L 0.0024 0.0 0-20 DUP 7440-38-2 52725 CADMIUM 0.0003 mg/L 0.0003 0.0 0-20 DUP 7440-43-9 52725 CHROMIUM 0.0052 mg/L 0.0052 0.0 0-20 DUP 7440-47-3 52725 COPPER 0.0713 mg/L 0.0645 10.0 0-20 DUP 7440-50-8 52725 LEAD 0.0017 mg/L 0.0017 0.0 0-20 DUP 7439-92-1 52725 NICKEL 0.0047 mg/L 0.0044 6.6 0-20 DUP 7440-02-0 52725 SELENIUM 0.0018 mg/L 0.0015 18.2 0-20 DUP IEV 7782-49-2 52725 ZINC 0.285 mg/L 0.280 1.8 0-20 DUP 7440-66-6 57694 COPPER 0.0030 mg/L 0.0029 3.4 0-20 DUP 7440-50-8 58615 COPPER 0.0004 mg/L 0.0006 40.0 0-20 DUP IEV 7440-50-8 62035 COPPER 0.0373 mg/L 0.0388 3.9 0-20 DUP 7440-50-8 62035 LEAD 0.0035 mg/L 0.0042 18.2 0-20 DUP 7439-92-1 62035 ZINC 0.297 mg/L 0.300 1.0 0-20 DUP 7440-66-6 Matrix Spike (MS)/Matrix Spike Duplicate (MSD) analyses are used to determine the accuracy (MS) and precision (MSD) of a analytical method in a given sample matrix. Therefore, the usefulness of this report is limited to samples of similar matrices analyzed in the same analytical batch.
NA = Indicates %RPD could not be calculated
%RPD = Relative Percent Difference Only Duplicate sample with detections are listed in this report Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QC Dependent2.rpt
Reference Number:
Report Date:
Page 2 of 5 10/12/2022 22-30019 Laboratory Fortified Matrix (MS)
Batch/CAS Analyte Sample Result Result Result Conc Units Limits*
%RPD MS MSD Limits*
Qualifier Type Comments QC Percent Recovery Spike Spike Duplicate 200.8_220929B2 52725 ARSENIC 0.0150 mg/L 0.0024 0.0125 101 70-130 NA 0-20 LFM 7440-38-2 52725 CADMIUM 0.0128 mg/L 0.0003 0.0125 100 70-130 NA 0-20 LFM 7440-43-9 52725 CHROMIUM 0.0183 mg/L 0.0052 0.0125 105 70-130 NA 0-20 LFM 7440-47-3 52725 COPPER 0.0829 mg/L 0.0645 0.0125 147 70-130 NA 0-20 LFM IS 7440-50-8 52725 LEAD 0.0142 mg/L 0.0017 0.0125 100 70-130 NA 0-20 LFM 7439-92-1 52725 NICKEL 0.0172 mg/L 0.0044 0.0125 102 70-130 NA 0-20 LFM 7440-02-0 52725 SELENIUM 0.0120 mg/L 0.0015 0.0125 84 70-130 NA 0-20 LFM 7782-49-2 52725 ZINC 0.333 mg/L 0.280 0.0125 424 70-130 NA 0-20 LFM IS 7440-66-6 57694 COPPER 0.0154 mg/L 0.0029 0.0125 100 70-130 NA 0-20 LFM 7440-50-8 58615 COPPER 0.0136 mg/L 0.0006 0.0125 104 70-130 NA 0-20 LFM 7440-50-8 62035 COPPER 0.0905 mg/L 0.0388 0.050 103 70-130 NA 0-20 LFM 7440-50-8 62035 LEAD 0.0535 mg/L 0.0042 0.050 99 70-130 NA 0-20 LFM 7439-92-1 62035 ZINC 0.340 mg/L 0.300 0.050 80 70-130 NA 0-20 LFM 7440-66-6 624_220909 57667 1,1 - DICHLOROETHANE 3.6 ug/L ND 4
3.8 90 95 59-155 5.4 0-40 LFM 75-34-3 57667 1,1 - DICHLOROETHYLENE 3.9 ug/L ND 4
4.0 98 100 1-234 2.5 0-32 LFM 75-35-4 57667 1,1,1 - TRICHLOROETHANE 3.7 ug/L ND 4
3.9 93 98 52-162 5.3 0-36 LFM 71-55-6 57667 1,1,2 - TRICHLOROETHANE 3.2 ug/L ND 4
3.4 80 85 52-150 6.1 0-45 LFM 79-00-5 57667 1,1,2,2 - TETRACHLOROETHANE 3.7 ug/L ND 4
4.1 93 103 46-157 10.3 0-61 LFM 79-34-5 57667 1,2 - DICHLOROETHANE 3.4 ug/L ND 4
3.6 85 90 49-155 5.7 0-49 LFM 107-06-2 57667 1,2 - DICHLOROPROPANE 3.2 ug/L ND 4
3.4 80 85 1-210 6.1 0-55 LFM 78-87-5 57667 1,2-DICHLOROBENZENE 3.9 ug/L ND 4
4.4 98 110 18-190 12.0 0-57 LFM 95-50-1 57667 1,3-DICHLOROBENZENE 4.1 ug/L ND 4
4.4 103 110 59-156 7.1 0-43 LFM 541-73-1 57667 1,4-DICHLOROBENZENE 4.1 ug/L ND 4
4.5 103 113 18-190 9.3 0-57 LFM 106-46-7 57667 2-CHLOROETHYL VINYL ETHER 6.2 ug/L ND 10 8.0 62 80 2-305 25.4 0-71 LFM 110-75-8 57667 ACROLEIN 6.1 ug/L ND 10 7.9 61 79 40-160 25.7 0-60 LFM 107-02-8 57667 ACRYLONITRILE 8.7 ug/L ND 10 9.9 87 99 40-160 12.9 0-60 LFM 107-13-1 57667 BENZENE 3.6 ug/L ND 4
3.7 90 93 37-151 2.7 0-61 LFM 71-43-2 57667 BROMODICHLOROMETHANE 3.4 ug/L ND 4
3.7 85 93 35-155 8.5 0-56 LFM 75-27-4 57667 BROMOFORM 3.9 ug/L ND 4
4.3 98 108 45-169 9.8 0-42 LFM 75-25-2 57667 BROMOMETHANE 2.8 ug/L ND 4
3.1 70 78 1-242 10.2 0-61 LFM 74-83-9 57667 CARBON TETRACHLORIDE 3.9 ug/L ND 4
4.0 98 100 70-140 2.5 0-41 LFM 56-23-5 57667 CHLOROBENZENE 3.7 ug/L ND 4
4.0 93 100 37-160 7.8 0-53 LFM 108-90-7 57667 CHLORODIBROMOMETHANE 3.3 ug/L ND 4
3.5 83 88 53-149 5.9 0-50 LFM 124-48-1 57667 CHLOROETHANE 3.9 ug/L ND 4
4.0 98 100 14-230 2.5 0-78 LFM 75-00-3 Matrix Spike (MS)/Matrix Spike Duplicate (MSD) analyses are used to determine the accuracy (MS) and precision (MSD) of a analytical method in a given sample matrix. Therefore, the usefulness of this report is limited to samples of similar matrices analyzed in the same analytical batch.
NA = Indicates %RPD could not be calculated
%RPD = Relative Percent Difference Only Duplicate sample with detections are listed in this report Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QC Dependent2.rpt
Reference Number:
Report Date:
Page 3 of 5 10/12/2022 22-30019 Laboratory Fortified Matrix (MS)
Batch/CAS Analyte Sample Result Result Result Conc Units Limits*
%RPD MS MSD Limits*
Qualifier Type Comments QC Percent Recovery Spike Spike Duplicate 57667 CHLOROFORM 4.8 ug/L 1.1 4
5.0 93 98 51-138 5.3 0-54 LFM 67-66-3 57667 CHLOROMETHANE 3.6 ug/L ND 4
3.6 90 90 1-273 0.0 0-60 LFM 74-87-3 57667 CIS - 1,3 - DICHLOROPROPENE 3.3 ug/L ND 4
3.5 83 88 1-227 5.9 0-58 LFM 10061-01-5 57667 DICHLORODIFLUOROMETHANE 3.0 ug/L ND 4
3.0 75 75 70-130 0.0 0-20 LFM 75-71-8 57667 ETHYLBENZENE 4.3 ug/L ND 4
4.5 108 113 37-162 4.5 0-63 LFM 100-41-4 57667 METHYLENE CHLORIDE 3.4 ug/L ND 4
3.5 85 88 1-221 2.9 0-28 LFM 75-09-2 57667 T - 1,2 - DICHLOROETHYLENE 3.6 ug/L ND 4
3.7 90 93 54-156 2.7 0-45 LFM 156-60-5 57667 TETRACHLOROETHYLENE 3.9 ug/L ND 4
3.9 98 98 64-148 0.0 0-39 LFM 127-18-4 57667 TOLUENE 3.6 ug/L ND 4
3.7 90 93 47-150 2.7 0-41 LFM 108-88-3 57667 TRANS-1,3 - DICHLOROPROPENE 3.1 ug/L ND 4
3.6 78 90 17-183 14.9 0-86 LFM 10061-02-6 57667 TRICHLOROETHYLENE 3.7 ug/L ND 4
3.9 93 98 70-157 5.3 0-48 LFM 79-01-6 57667 TRICHLOROFLUOROMETHANE 6.6 ug/L ND 4
4.3 165 108 17-181 42.2 0-84 LFM 75-69-4 57667 VINYL CHLORIDE 3.3 ug/L ND 4
3.7 83 93 1-251 11.4 0-66 LFM 75-01-4 625_220909 57667 2 - FLUOROBIPHENYL (Surr) 67 53 44 NA 53-140 NA 0-20 LFM SA 321-60-8 57667 2 - FLUOROPHENOL (Surr) 42 37 29 NA 29-140 NA 0-20 LFM 367-12-4 57667 2,4,6 - TRIBROMOPHENOL (Surr) 78 68 49 NA 39-140 NA 0-20 LFM 118-79-6 57667 d5-NITROBENZENE (Surr) 66 58 47 NA 50-140 NA 0-20 LFM SA 98-95-3 57667 d5-PHENOL (Surr) 30 25 22 NA 23-140 NA 0-20 LFM SA 108-95-2 57667 p-TERPHENYL-d14 (Surr) 71 63 38 NA 60-140 NA 0-20 LFM SA 1718-51-0 57667 1,2,4-TRICHLOROBENZENE 6.1 ug/L ND 10 4.4 61 44 44-142 32.4 0-50 LFM 120-82-1 57667 1,2-DIPHENYLHYDRAZINE 7.3 ug/L ND 10 4.9 73 49 67-127 39.3 0-40 LFM M2 122-66-7 57667 2,4,6-TRICHLOROPHENOL 7.3 ug/L ND 10 4.5 73 45 37-144 47.5 0-58 LFM 88-06-2 57667 2,4-DICHLOROPHENOL 7.0 ug/L ND 10 4.9 70 49 39-135 35.3 0-50 LFM 120-83-2 57667 2,4-DIMETHYLPHENOL 7.2 ug/L ND 10 5.1 72 51 32-120 34.1 0-58 LFM 105-67-9 57667 2,4-DINITROPHENOL 2.4 ug/L ND 10 1.1 24 11 1-191 74.3 0-132 LFM 51-28-5 57667 2,4-DINITROTOLUENE 7.6 ug/L ND 10 4.9 76 49 39-139 43.2 0-42 LFM R4 121-14-2 57667 2,6-DINITROTOLUENE 7.2 ug/L ND 10 5.0 72 50 50-158 36.1 0-48 LFM 606-20-2 57667 2-CHLORONAPHTHALENE 6.8 ug/L ND 10 4.4 68 44 60-120 42.9 0-24 LFM R1 M2 91-58-7 57667 2-CHLOROPHENOL 6.3 ug/L ND 10 4.5 63 45 23-134 33.3 0-61 LFM 95-57-8 57667 2-NITROPHENOL 7.1 ug/L ND 10 4.8 71 48 29-182 38.7 0-55 LFM 88-75-5 57667 3,3-DICHLOROBENZIDINE 0.3 ug/L ND 1
0.5 30 50 1-262 50.0 0-108 LFM 91-94-1 57667 3-METHYL CHOLANTHRENE 6.7 ug/L ND 10 3.6 67 36 5-125 60.2 0-40 LFM R4 56-49-5 57667 4,6-DINITRO-2-METHYLPHENOL 5.1 ug/L ND 10 2.5 51 25 1-181 68.4 0-203 LFM 534-52-1 57667 4-BROMOPHENYL PHENYL ETHER 7.5 ug/L ND 10 4.9 75 49 53-127 41.9 0-43 LFM M2 101-55-3 57667 4-CHLORO-3-METHYLPHENOL 7.8 ug/L ND 10 4.9 78 49 22-147 45.7 0-73 LFM 59-50-7 Matrix Spike (MS)/Matrix Spike Duplicate (MSD) analyses are used to determine the accuracy (MS) and precision (MSD) of a analytical method in a given sample matrix. Therefore, the usefulness of this report is limited to samples of similar matrices analyzed in the same analytical batch.
NA = Indicates %RPD could not be calculated
%RPD = Relative Percent Difference Only Duplicate sample with detections are listed in this report Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QC Dependent2.rpt
Reference Number:
Report Date:
Page 4 of 5 10/12/2022 22-30019 Laboratory Fortified Matrix (MS)
Batch/CAS Analyte Sample Result Result Result Conc Units Limits*
%RPD MS MSD Limits*
Qualifier Type Comments QC Percent Recovery Spike Spike Duplicate 57667 4-CHLOROPHENYL PHENYL ETHER 7.8 ug/L ND 10 4.8 78 48 25-158 47.6 0-61 LFM 7005-72-3 57667 4-NITROPHENOL 3.2 ug/L ND 10 1.5 32 15 1-132 72.3 0-131 LFM 100-02-7 57667 ACENAPHTHENE 6.9 ug/L ND 10 4.4 69 44 47-145 44.2 0-48 LFM M2 83-32-9 57667 ACENAPHTHYLENE 7.0 ug/L ND 10 4.6 70 46 33-145 41.4 0-74 LFM 208-96-8 57667 ANTHRACENE 7.3 ug/L ND 10 4.7 73 47 27-133 43.3 0-66 LFM 120-12-7 57667 BENZ[A]ANTHRACENE 7.6 ug/L ND 10 4.2 76 42 33-143 57.6 0-53 LFM R4 56-55-3 57667 BENZIDINE ND ug/L ND 25 ND NA 1-59 NA 0-40 LFM P
92-87-5 57667 BENZO(A)PYRENE 6.7 ug/L ND 10 3.6 67 36 17-163 60.2 0-72 LFM 50-32-8 57667 BENZO(J)FLUORANTHENE 14.1 ug/L ND 20 8.0 71 40 21-123 55.2 0-40 LFM R4 205-82-3 57667 BENZO(R,S,T)PENTAPHENE 6.4 ug/L ND 10 4.0 64 40 1-156 46.2 0-40 LFM R4 189-55-9 57667 BENZO[B]FLUORANTHENE 13.4 ug/L ND 20 7.5 67 38 24-159 56.5 0-71 LFM 205-99-2 57667 BENZO[G,H,I]PERYLENE 6.6 ug/L ND 10 3.4 66 34 1-219 64.0 0-97 LFM 191-24-2 57667 BENZO[K]FLUORANTHENE 7.4 ug/L ND 10 3.6 74 36 11-162 69.1 0-63 LFM R4 207-08-9 57667 BENZYL BUTYL PHTHALATE 7.4 ug/L ND 10 4.5 74 45 1-152 48.7 0-60 LFM 85-68-7 57667 BIS(2-CHLORO-1-METHYLETHYL)ETHER 6.1 ug/L ND 10 4.5 61 45 36-166 30.2 0-76 LFM 108-60-1 57667 Bis(2-CHLOROETHOXY)METHANE 7.0 ug/L ND 10 4.9 70 49 33-184 35.3 0-54 LFM 111-91-1 57667 BIS(2-CHLOROETHYL)ETHER 6.0 ug/L ND 10 4.3 60 43 12-158 33.0 0-108 LFM 111-44-4 57667 CHRYSENE 7.5 ug/L ND 10 4.2 75 42 17-168 56.4 0-87 LFM 218-01-9 57667 DI(2-ETHYLHEXYL)PHTHALATE 5.2 ug/L ND 10 2.2 52 22 8-158 81.1 0-82 LFM 117-81-7 57667 DIBENZO(A,E)PYRENE 6.6 ug/L ND 10 3.1 66 31 1-154 72.2 0-40 LFM R4 192-65-4 57667 DIBENZO(A,H)ACRIDINE 8.5 ug/L ND 10 5.0 85 50 25-133 51.9 0-40 LFM R4 226-36-8 57667 DIBENZO(A,H)PYRENE 5.9 ug/L ND 10 2.9 59 29 4-160 68.2 0-40 LFM R4 189-64-0 57667 DIBENZO(A,J)ACRIDINE 8.8 ug/L ND 10 5.3 88 53 31-139 49.6 0-40 LFM R4 224-42-0 57667 DIBENZO[A,H]ANTHRACENE 7.7 ug/L ND 10 4.0 77 40 1-227 63.2 0-126 LFM 53-70-3 57667 DIETHYL PHTHALATE 7.7 ug/L ND 10 5.0 77 50 1-120 42.5 0-100 LFM 84-66-2 57667 DIMETHYL PHTHALATE 7.0 ug/L ND 10 4.4 70 44 1-120 45.6 0-183 LFM 131-11-3 57667 DI-N-BUTYL PHTHALATE 7.5 ug/L ND 10 4.9 75 49 1-120 41.9 0-47 LFM 84-74-2 57667 DI-N-OCTYL PHTHALATE 4.6 ug/L ND 10 2.0 46 20 4-146 78.8 0-69 LFM R4 117-84-0 57667 FLUORANTHENE 7.5 ug/L ND 10 4.7 75 47 26-137 45.9 0-66 LFM 206-44-0 57667 FLUORENE 7.3 ug/L ND 10 4.5 73 45 59-121 47.5 0-38 LFM R1 M2 86-73-7 57667 HEXACHLOROBENZENE 7.2 ug/L ND 10 4.7 72 47 1-152 42.0 0-55 LFM 118-74-1 57667 HEXACHLOROBUTADIENE 5.4 ug/L ND 10 3.6 54 36 24-120 40.0 0-62 LFM 87-68-3 57667 HEXACHLOROCYCLOPENTADIENE 2.7 ug/L ND 10 2.0 27 20 1-142 29.8 0-40 LFM 77-47-4 57667 HEXACHLOROETHANE 4.9 ug/L ND 10 3.6 49 36 40-120 30.6 0-52 LFM M2 67-72-1 57667 INDENO[1,2,3,C,D]PYRENE 7.2 ug/L ND 10 3.8 72 38 1-171 61.8 0-99 LFM 193-39-5 57667 ISOPHORONE 6.9 ug/L ND 10 4.8 69 48 21-196 35.9 0-93 LFM 78-59-1 Matrix Spike (MS)/Matrix Spike Duplicate (MSD) analyses are used to determine the accuracy (MS) and precision (MSD) of a analytical method in a given sample matrix. Therefore, the usefulness of this report is limited to samples of similar matrices analyzed in the same analytical batch.
NA = Indicates %RPD could not be calculated
%RPD = Relative Percent Difference Only Duplicate sample with detections are listed in this report Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QC Dependent2.rpt
Reference Number:
Report Date:
Page 5 of 5 10/12/2022 22-30019 Laboratory Fortified Matrix (MS)
Batch/CAS Analyte Sample Result Result Result Conc Units Limits*
%RPD MS MSD Limits*
Qualifier Type Comments QC Percent Recovery Spike Spike Duplicate 57667 NAPHTHALENE 6.2 ug/L ND 10 4.2 62 42 21-133 38.5 0-65 LFM 91-20-3 57667 NITROBENZENE 6.3 ug/L ND 10 4.7 63 47 35-180 29.1 0-62 LFM 98-95-3 57667 N-NITROSODIMETHYLAMINE 4.4 ug/L ND 10 3.1 44 31 19-109 34.7 0-40 LFM 62-75-9 57667 N-NITROSODI-N-PROPYLAMINE 6.7 ug/L ND 10 4.8 67 48 1-230 33.0 0-87 LFM 621-64-7 57667 N-NITROSODIPHENYLAMINE 7.6 ug/L ND 10 5.0 76 50 61-139 41.3 0-40 LFM R1 M2 86-30-6 57667 PENTACHLOROPHENOL 2.4 ug/L ND 10 1.4 24 14 14-176 52.6 0-86 LFM 87-86-5 57667 PERYLENE 5.4 ug/L ND 10 3.0 54 30 18-114 57.1 0-40 LFM R4 198-55-0 57667 PHENANTHRENE 7.4 ug/L ND 10 4.7 74 47 54-120 44.6 0-39 LFM R1 M2 85-01-8 57667 PHENOL 3.0 ug/L ND 10 2.1 30 21 5-120 35.3 0-64 LFM 108-95-2 57667 PYRENE 8.0 ug/L ND 10 5.1 80 51 52-120 44.3 0-49 LFM M2 129-00-0 Matrix Spike (MS)/Matrix Spike Duplicate (MSD) analyses are used to determine the accuracy (MS) and precision (MSD) of a analytical method in a given sample matrix. Therefore, the usefulness of this report is limited to samples of similar matrices analyzed in the same analytical batch.
NA = Indicates %RPD could not be calculated
%RPD = Relative Percent Difference Only Duplicate sample with detections are listed in this report Limits are intended for water matrices only. These criteria are for guidance only when reported with soils/solids.
FORM: QC Dependent2.rpt
Page 1 of 1 10/12/22 QUALITY CONTROL REPORT Report Date:
Reference Number:
SURROGATE REPORT 22-30019 Result Limit Units Method Analyte Lab No Qualifier 625_220909 58274 2,4,6 - TRIBROMOPHENOL (Surr) 625.1 31 SA 2 - FLUOROBIPHENYL (Surr) 36 SA 2 - FLUOROPHENOL (Surr) 18 SA d5-PHENOL (Surr) 16 SA p-TERPHENYL-d14 (Surr) 41 SA d5-NITROBENZENE (Surr) 38 SA 624_220909 58275 1,2 - DICHLOROETHANE-d4 (SURR) 624.1 102 Acceptance Limit 70-130%
4-BROMOFLUOROBENZENE (Surr) 96 Acceptance Limit 70-130%
d8-TOLUENE (Surr) 91 Acceptance Limit 70-130%
- Notation:
The Acceptance Limits (or Control Limits) approximate a 99% confidence interval around the mean recovery.
Page 1 of 1 Qualifier Definitions Reference Number:
Report Date:
10/12/22 22-30019 Qualifier Definition IEV Acceptance criteria do not apply to estimated values IS The ratio of the spike concentration to sample background was too low to meet performance criteria M2 Matrix bias indicated, the LFB is within acceptance limits. Results for this compound is suspect as biased high.
P The Laboratory Fortified Blank was within limits. Little or No recovery of the MS/MSD indicates matrix effects. Detection at the reported amount may not have been achieved.
R1 RPD/RSD exceeded the method acceptance limit. See case narrative.
R4 MS/MSD RPD exceeded the method acceptance limit. Recovery met acceptance criteria.
SA Surrogate recovery outside method acceptance limits. CCV target compound recovery meets method requirements.
FORM: QualifierDefs Note: Some qualifier definitions found on this page may pertain to results or QC data which are not printed with this report.
Anatek Labs, Inc.
1282 Alturas Drive - Moscow, ID 83843 - (208) 883-2839 - Fax (208) 8829246 - email moscow@anateklabs.com 504 E Sprague Ste. D - Spokane, WA 99202 - (509) 838-3999 - fax (509) 838-4433 - email spokane@anateklabs.com Client:
Work Order:
Project:
Reported:
Energy Northwest 350 Hills St Suite 107 Richland, WA 99354 9/26/2022 16:28 Attn:
Address:
Environmental Services MCI0323 230214 Analytical Results Report Result Analyte PQL Analyzed Method Units 230214-02 (CW Grab)
Analyst Qualifier Date Received:
Lab/Sample Number:
MCI0323-01 Collect Date:
09/09/22 12:54 Sample Location:
Collected By:
09/07/22 11:55 Wastewater Matrix:
Mercury Mercury ug/L EPA 1631 E 9/20/22 15:40 BSM 0.000500 0.00388 Page 1 of 5
Anatek Labs, Inc.
1282 Alturas Drive - Moscow, ID 83843 - (208) 883-2839 - Fax (208) 8829246 - email moscow@anateklabs.com 504 E Sprague Ste. D - Spokane, WA 99202 - (509) 838-3999 - fax (509) 838-4433 - email spokane@anateklabs.com Analytical Results Report (Continued)
Result Analyte PQL Analyzed Method Units 230214-05 (Field Blank)
Analyst Qualifier Date Received:
Lab/Sample Number:
MCI0323-02 Collect Date:
09/09/22 12:54 Sample Location:
Collected By:
09/07/22 11:55 Wastewater Matrix:
Mercury Mercury ug/L EPA 1631 E 9/20/22 15:47 BSM U
0.000500 ND
[TOC_1]Quality Assurance Results[TOC]
Authorized Signature, Justin Doty For Todd Taruscio, Laboratory Manager The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
J Compound was analyzed for but not detected U
PQL Practical Quantitation Limit ND Not Detected MCL EPA's Maximum Contaminant Level Dry Sample results reported on a dry weight basis Not a state-certified analyte RPD Relative Percent Difference
%REC Percent Recovery Source Sample that was spiked or duplicated.
This report shall not be reproduced except in full, without the written approval of the laboratory The results reported related only to the samples indicated.
Page 2 of 5
Anatek Labs, Inc.
1282 Alturas Drive - Moscow, ID 83843 - (208) 883-2839 - Fax (208) 8829246 - email moscow@anateklabs.com 504 E Sprague Ste. D - Spokane, WA 99202 - (509) 838-3999 - fax (509) 838-4433 - email spokane@anateklabs.com Result Reporting Limit Units Spike Level Source Result
%REC
%REC Limits RPD RPD Limit Qual Analyte Quality Control Data Mercury Batch: BCI0556 - Hg Trace Prepared: 9/19/2022 Analyzed: 9/20/2022 Blank (BCI0556-BLK1)
U ND 0.000500 ug/L Mercury Prepared: 9/19/2022 Analyzed: 9/20/2022 LCS (BCI0556-BS1) 0.00491 0.000500 0.00500 77-123 98.2 ug/L Mercury Prepared: 9/19/2022 Analyzed: 9/20/2022 Source: MCI0329-01 Matrix Spike (BCI0556-MS1) 0.00591 0.000500 0.00500 0.00140 71-125 90.1 ug/L Mercury Prepared: 9/19/2022 Analyzed: 9/20/2022 Source: MCI0329-01 Matrix Spike Dup (BCI0556-MSD1) 0.00590 0.000500 0.00500 0.00140 24 71-125 89.9 0.203 ug/L Mercury Page 3 of 5
Page 4 of 5
Page 5 of 5
SampleNumber Matrix Test Method Customername CustomerContact CustomerAddress CustomerCityStateZip Units Qualifier AnalysisTime Analyst Dilution Param CAS Result DetectionLimit RDL RepLimit SampleType ExtractDate Location CollectDate CollectTime ReceiveDate CustomerSampleNumber Orders_Comment OrderProjectName MCL MCI0323-01 Water Hg 1631 EPA 1631 E Energy Northwest Environmental Services 350 Hills St Suite 107 Richland, WA 99354 ug/L 9/20/2022 3:40:02 PM BSM 1
Mercury 7439-97-6 0.00388 0.000200 0.000200 0.000500 9/19/2022 10:11:00 AM 09/07/2022 11:55 9/9/2022 12:54:00 PM 230214-02 (CW Grab)
MCI0323-02 Water Hg 1631 EPA 1631 E Energy Northwest Environmental Services 350 Hills St Suite 107 Richland, WA 99354 ug/L U
9/20/2022 3:47:40 PM BSM 1
Mercury 7439-97-6 <0.000200 [2] 0.000200 0.000200 0.000500 9/19/2022 10:11:00 AM 09/07/2022 11:55 9/9/2022 12:54:00 PM 230214-05 (Field Blank)
Sample 230214-02 grab sample.
Excerpt from Anatek EDD file for mercury grab sample and field blank; EDD shows detection limit.
Thisreportshouldnotbereproduced,exceptinfull, withoutthewrittenconsentofPaceAnalyticalServices,Inc.
Theresultsrelateonlyt othesamplesincludedinthisreport.
Report of Laboratory Analysis www.pacelabs.com Pace Analytical Services, LLC.
1700 Elm Street Minneapolis, MN 55414 Phone: 612.607.1700 Fax: 612.607.6444 Jane LePage Energy Northwest Environmental Ser 76 N Power Plant Loop Richland WA 99354 REPORT OF LABORATORY ANALYSIS FOR TCDD This report has been reviewed by:
Invoicing & Reporting Options:
Report Information:
Report Prepared Date:
September 23, 2022 PaceProject#:10624694 SampleReceiptDate:09/08/2022 Client Project #: 230214, NPDES Priority Client Sub PO #: N/A The report provided has been invoiced as a Level 2 2,3,7,8-TCDD Report. If an upgrade of this report package is requested, an additional charge may be applied.
Please review the attached invoice for accuracy and forward any questions to Carolynne Trout, your Pace Project Manager.
State Cert #: C486 Report Prepared for:
Page 1 of 14 Report No.....10624694_1613TCDD_DFR September 27, 2022 Carolynne Trout, Project Manager (612) 607-6351 (612) 607-6444 (fax)
Carolynne.Trout@pacelabs.com
Pace Analytical Services, LLC.
1700 Elm Street Minneapolis, MN 55414 Phone: 612.607.1700 Fax: 612.607.6444 REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
This report presents the results from the analysis performed on one sample submitted by a representative of Energy Northwest. The sample was analyzed for the presence or absence of 2,3,7,8-tetrachlorodibenzo-p-dioxin (2,3,7,8-TCDD) using USEPA Method 1613B. The estimated detection limits (EDLs) were based on signal-to-noise measurements.
The isotopically-labeled TCDD internal standard in the sample extract was recovered at 27%. Except for one low value, which was flagged "R" on the results table, the labeled standard recoveries obtained for this project were within the target ranges specified in Method 1613B. Also, since the quantification of the native TCDD was based on isotope dilution, the data were automatically corrected for recovery and accurate values were obtained.
A laboratory method blank was prepared and analyzed with the sample batch as part of our routine quality control procedures. The results show the blank to be free of 2,3,7,8-TCDD at the reporting limit.
Laboratory spike samples were also prepared using clean reference matrix that had been fortified with native standard material. The results show that the spiked native TCDD was recovered at 105-114% with a relative percent difference of 8.2%. These results were within the target ranges for the method. Matrix spikes were not prepared with the sample batch.
DISCUSSION Page 2 of 14 Report No.....10624694_1613TCDD_DFR
REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, LLC 1700 Elm Street - Suite 200 Minneapolis, MN 55414 Tel: 612-607-1700 Fax: 612-607-6444 Report No.....10624694 Minnesota Laboratory Certifications Authority Certificate #
Authority Certificate #
Mississippi MN00064 Missouri 10100 A2LA 2926.01 Montana CERT0092 Alabama 40770 Nebraska NE-OS-18-06 Alaska-DW MN00064 Nevada MN00064 Alaska-UST 17-009 New Hampshire 2081 Arizona AZ0014 New Jersey MN002 Arkansas - WW 88-0680 New York 11647 Arkansas-DW MN00064 North Carolina-27700 California 2929 North Carolina-530 Colorado MN00064 North Dakota R-036 Connecticut PH-0256 Ohio-DW 41244 Florida E87605 Ohio-VAP (170 CL101 Georgia 959 Ohio-VAP (180 CL110 Hawaii MN00064 Oklahoma 9507 Idaho MN00064 Oregon-rimary MN300001 Illinois 200011 Oregon-Second MN200001 Indiana C-MN-01 Pennsylvania 68-00563 Iowa 368 Puerto Rico MN00064 Kansas E-10167 South Carolina 74003 Kentucky-DW 90062 Tennessee TN02818 Kentucky-WW 90062 Texas T104704192 Louisiana-DEQ AI-84596 Utah MN00064 Louisiana-DW MN00064 Vermont VT-027053137 Maine MN00064 Virginia 460163 Maryland 322 Washington C486 Michigan 9909 West Virginia-D 382 Minnesota 027-053-137 West Virginia-D 9952C Minnesota-Ag via MN 027-053 Wisconsin 999407970 Minnesota-Petr 1240 Wyoming-UST via A2LA 2926.
Page 3 of 14 Report No.....10624694_1613TCDD_DFR
Pace Analytical Services, LLC 1700 Elm Street, Suite 200 Minneapolis, MN 55414 Phone: 612.607.1700 Fax: 612.607.6444 www.pacelabs.com Appendix A Sample Management REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Page 4 of 14 Report No.....10624694_1613TCDD_DFR
Page 5 of 14 Report No.....10624694_1613TCDD_DFR
9/12/22 Page 6 of 14 Report No.....10624694_1613TCDD_DFR Carolynne Trout
Page 7 of 14 Report No.....10624694_1613TCDD_DFR
Pace Analytical Services, LLC 1700 Elm Street, Suite 200 Minneapolis, MN 55414 Phone: 612.607.1700 Fax: 612.607.6444 www.pacelabs.com A =
B =
C =
D =
E =
I =
J =
L =
Nn =
P =
R =
S =
U =
V =
X =
Y =
- =
Reporting Limit based on signal to noise (EDL)
Less than 10x higher than method blank level Result obtained from confirmation analysis Result obtained from analysis of diluted sample Exceeds calibration range Isotope ratio out of specification Estimated value Suppressive interference, analyte may be biased low Value obtained from additional analysis PCDE Interference Recovery outside target range Peak saturated Analyte not detected Result verified by confirmation analysis
%D Exceeds limits Calculated using average of daily RFs See Discussion Reporting Flags REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Page 8 of 14 Report No.....10624694_1613TCDD_DFR
Pace Analytical Services, LLC 1700 Elm Street, Suite 200 Minneapolis, MN 55414 Phone: 612.607.1700 Fax: 612.607.6444 www.pacelabs.com Appendix B Sample Analysis Summary REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Page 9 of 14 Report No.....10624694_1613TCDD_DFR
REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, LLC 1700 Elm Street - Suite 200 Minneapolis, MN 55414 Tel: 612-607-1700 Fax: 612-607-6444 Lab Sample ID Injected By Filename Total Amount Extracted
% Moisture Dry Weight Extracted ICAL ID CCal Filename(s)
Method Blank ID Client's Sample ID 230214.01 10624694001 L220921A_07 MS4 NA 984 mL NA L220811 L220920A_18 BLANK-101187 Matrix Dilution Collected Received Extracted Analyzed Water NA 09/06/2022 08:30 09/08/2022 13:30 09/13/2022 12:56 09/21/2022 05:39 Client - Energy Northwest Environmental Services Lab Method 1613B Sample Analysis Results Native Isomers Conc pg/L pg/L Internal Standards Added ng's Percent Recovery EMPC pg/L EDL 2,3,7,8-TCDD ND 1.2 2,3,7,8-TCDD-13C 2.00 27 R
Recovery Standard 1,2,3,4-TCDD-13C 2.00 NA Cleanup Standard 2,3,7,8-TCDD-37Cl4 0.20 73 Conc = Concentration (Totals include 2,3,7,8-substituted isomers).
EMPC = Estimated Maximum Possible Concentration ND = Not Detected NA = Not Applicable NC = Not Calculated R = Recovery outside target range E = Exceeds calibration range EDL = Estimated Detection Limit Page 10 of 14 Report No.....10624694_1613TCDD_DFR
REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, LLC 1700 Elm Street - Suite 200 Minneapolis, MN 55414 Tel: 612-607-1700 Fax: 612-607-6444 Lab Sample ID Injected By Filename Total Amount Extracted ICAL ID CCal Filename(s)
BLANK-101187 F220919A_09 MS4 992 mL F220529 F220919A_02 Matrix Dilution Extracted Analyzed Water 09/13/2022 12:56 09/19/2022 16:28 NA Method 1613B Blank Analysis Results Lab Sample Name DFBLKGN Native Isomers pg/L Conc EMPC pg/L pg/L Internal Standards Added ng's Percent Recovery EDL 2,3,7,8-TCDD ND 0.90 2,3,7,8-TCDD-13C 2.00 45 Recovery Standard 1,2,3,4-TCDD-13C 2.00 NA Cleanup Standard 2,3,7,8-TCDD-37Cl4 0.20 76 Conc=Concentration(Totalsinclude2,3,7,8-substitutedisomers).
EMPC=EstimatedMaximumPossibleConcentration J = Estimated value I = Isotope ratio out of specification EDL = Estimated Detection Limit Page 11 of 14 Report No.....10624694_1613TCDD_DFR
REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, LLC 1700 Elm Street - Suite 200 Minneapolis, MN 55414 Tel: 612-607-1700 Fax: 612-607-6444 Method 1613B Laboratory Control Spike Results Lab Sample ID Injected By Filename Total Amount Extracted ICAL ID CCal Filename LCS-101178 F220919A_04 MS4 998 mL F220529 F220919A_02 Matrix Dilution Extracted Analyzed Water 09/13/2022 12:56 09/19/2022 12:40 NA Method Blank ID BLANK-101187 Compound Cs Cr Lower Upper Limit Limit Rec.
2,3,7,8-TCDD 10 11 7.3 14.6 105 2,3,7,8-TCDD-37Cl4 10 7.3 3.7 15.8 73 2,3,7,8-TCDD-13C 100 25 25.0 141.0 25 Cs = Concentration Spiked (ng/mL)
Cr = Concentration Recovered (ng/mL)
Rec. = Recovery (Expressed as Percent)
Control Limit
Reference:
Method 1613, Table 6, 10/94 Revision R = Recovery outside of control limits Nn = Value obtained from additional analysis
- =SeeDiscussion Page 12 of 14 Report No.....10624694_1613TCDD_DFR
REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, LLC 1700 Elm Street - Suite 200 Minneapolis, MN 55414 Tel: 612-607-1700 Fax: 612-607-6444 Method 1613B Laboratory Control Spike Results Lab Sample ID Injected By Filename Total Amount Extracted ICAL ID CCal Filename LCSD-101179 F220919A_05 MS4 999 mL F220529 F220919A_02 Matrix Dilution Extracted Analyzed Water 09/13/2022 12:56 09/19/2022 13:26 NA Method Blank ID BLANK-101187 Compound Cs Cr Lower Upper Limit Limit Rec.
2,3,7,8-TCDD 10 11 7.3 14.6 114 2,3,7,8-TCDD-37Cl4 10 8.5 3.7 15.8 85 2,3,7,8-TCDD-13C 100 53 25.0 141.0 53 Cs = Concentration Spiked (ng/mL)
Cr = Concentration Recovered (ng/mL)
Rec. = Recovery (Expressed as Percent)
Control Limit
Reference:
Method 1613, Table 6, 10/94 Revision R = Recovery outside of control limits Nn = Value obtained from additional analysis
- =SeeDiscussion Page 13 of 14 Report No.....10624694_1613TCDD_DFR
REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.
Pace Analytical Services, LLC 1700 Elm Street - Suite 200 Minneapolis, MN 55414 Tel: 612-607-1700 Fax: 612-607-6444 Client Spike 1 ID Spike 1 Filename F220919A_04 LCS-101178 Energy Northwest Environmental Services Lab Spike Recovery Relative Percent Difference (RPD) Results Spike 2 ID Spike 2 Filename F220919A_05 LCSD-101179 Method 1613B Spike 1 Spike 2 Compound
%REC
%REC
%RPD 2,3,7,8-TCDD 105 114 8.2
%REC = Percent Recovered RPD = The difference between the two values divided by the mean value Page 14 of 14 Report No.....10624694_1613TCDD_DFR
is accredited for the analytes listed below using the methods indicated. Full accreditation is granted unless stated otherwise in a note. EPA is the U.S. Environmental Protection Agency. SM is "Standard Methods for the Examination of Water and Wastewater." SM refers to EPA approved method versions. ASTM is the American Society for Testing and Materials. USGS is the U.S. Geological Survey. AOAC is the Association of Official Analytical Chemists. Other references are described in notes.
Edge Analytical, Incorporated Burlington, WA WASHINGTON STATE DEPARTMENT OF ECOLOGY SCOPE OF ACCREDITATION ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM Matrix/Analyte Method Notes Air Benzene EPA 325B 1
Drinking Water pH EPA 150.1_1982 1
Turbidity EPA 180.1_2_1993 1
Chromium, Hexavalent EPA 218.6_3.3_1994 1
Fluoride EPA 300.0_2.1_1993 1
Nitrate EPA 300.0_2.1_1993 1
Nitrate + Nitrite EPA 300.0_2.1_1993 1
Nitrite EPA 300.0_2.1_1993 1
Orthophosphate EPA 300.0_2.1_1993 Sulfate EPA 300.0_2.1_1993 1
Bromate EPA 300.1_1_1997 1
Bromide EPA 300.1_1_1997 1
Chlorate EPA 300.1_1_1997 1
Chlorite EPA 300.1_1_1997 1
Cyanide, Available OIA 1677 Color SM 2120 B-2011 1,88 Alkalinity SM 2320 B-2011 1
Hardness (calc.)
SM 2340 B-2011 1,88 Specific Conductance SM 2510 B-2011 1
Solids, Total Dissolved SM 2540 C-2011 1
Chlorine (Residual), Free SM 4500-Cl G-2011 1,5 Chlorine Dioxide SM 4500-ClO2 D-93 5
pH SM 4500-H+ B-2011 1,88 Nitrate SM 4500-NO3-F-2011 1
Page 1 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Drinking Water Nitrate + Nitrite SM 4500-NO3-F-2011 1
Nitrite SM 4500-NO3-F-2011 1
Orthophosphate SM 4500-P F-2011 1
Dissolved Organic Carbon SM 5310 B-2011 1
Total Organic Carbon SM 5310 B-2011 1
UV Absorbing Organics SM 5910 B-00 1
Beryllium EPA 200.7_4.4_1994 1
Hardness, Total (as CaCO3)
EPA 200.7_4.4_1994 Iron EPA 200.7_4.4_1994 1
Magnesium EPA 200.7_4.4_1994 1
Manganese EPA 200.7_4.4_1994 1
Silica EPA 200.7_4.4_1994 Silver EPA 200.7_4.4_1994 1
Aluminum EPA 200.8_5.4_1994 Antimony EPA 200.8_5.4_1994 1
Beryllium EPA 200.8_5.4_1994 1
Manganese EPA 200.8_5.4_1994 1
Page 2 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Drinking Water Total Uranium EPA 200.8_5.4_1994 1
1,2,3-Trichloropropane EPA 504.1_1.1_1995 1
1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA 504.1_1.1_1995 1,2 Dibromochloropropane EPA 504.1_1.1_1995 1,2 4,4'-DDD EPA 508.1_2_1995 1
4,4'-DDE EPA 508.1_2_1995 1
4,4'-DDT EPA 508.1_2_1995 1
Aldrin EPA 508.1_2_1995 1
alpha-BHC (alpha-Hexachlorocyclohexane)
EPA 508.1_2_1995 1
Aroclor-1016 (PCB-1016)
EPA 508.1_2_1995 1
Aroclor-1221 (PCB-1221)
EPA 508.1_2_1995 1
Aroclor-1232 (PCB-1232)
EPA 508.1_2_1995 1
Aroclor-1242 (PCB-1242)
EPA 508.1_2_1995 1
Aroclor-1248 (PCB-1248)
EPA 508.1_2_1995 1
Aroclor-1254 (PCB-1254)
EPA 508.1_2_1995 1
Aroclor-1260 (PCB-1260)
EPA 508.1_2_1995 1
beta-BHC (beta-Hexachlorocyclohexane)
EPA 508.1_2_1995 1
Chlordane (tech.)
EPA 508.1_2_1995 1,2 delta-BHC EPA 508.1_2_1995 1
Dieldrin EPA 508.1_2_1995 1
Endosulfan I EPA 508.1_2_1995 1
Endosulfan II EPA 508.1_2_1995 1
Endosulfan sulfate EPA 508.1_2_1995 1
Endrin EPA 508.1_2_1995 1
Endrin aldehyde EPA 508.1_2_1995 1
gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 508.1_2_1995 1
Heptachlor EPA 508.1_2_1995 1
Heptachlor epoxide EPA 508.1_2_1995 1
Methoxychlor EPA 508.1_2_1995 1
PCBs EPA 508.1_2_1995 1,2 Toxaphene (Chlorinated camphene)
EPA 508.1_2_1995 1,2 2,4,5-T EPA 515.4_1_2000 1,2 2,4-D EPA 515.4_1_2000 1,2 2,4-DB EPA 515.4_1_2000 1
3,5-Dichlorobenzoic acid EPA 515.4_1_2000 1
Page 3 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Drinking Water Acifluorfen EPA 515.4_1_2000 1
Bentazon EPA 515.4_1_2000 1
Dacthal (DCPA)
EPA 515.4_1_2000 1,2 Dalapon EPA 515.4_1_2000 1,2 Dicamba EPA 515.4_1_2000 1
Dichloroprop (Dichlorprop)
EPA 515.4_1_2000 1
Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
EPA 515.4_1_2000 1,2 Pentachlorophenol EPA 515.4_1_2000 1,2 Picloram EPA 515.4_1_2000 1,2 Silvex (2,4,5-TP)
EPA 515.4_1_2000 1,2 3-Hydroxycarbofuran EPA 531.2_1_2001 1
Aldicarb (Temik)
EPA 531.2_1_2001 1
Aldicarb sulfone EPA 531.2_1_2001 1
Aldicarb sulfoxide EPA 531.2_1_2001 1
Carbaryl (Sevin)
EPA 531.2_1_2001 1
Carbofuran (Furaden)
EPA 531.2_1_2001 1
Methiocarb (Mesurol)
EPA 531.2_1_2001 1
Methomyl (Lannate)
EPA 531.2_1_2001 1
Oxamyl EPA 531.2_1_2001 1
Propoxur (Baygon)
EPA 531.2_1_2001 1
Glyphosate EPA 547_1990 1,2 Diquat EPA 549.2_1_1997 1,2 Paraquat EPA 549.2_1_1997 1
Bromoacetic acid (MBAA, BAA)
EPA 552.3 Rev 1 (2003) 1,2 Bromochloroacetic acid (BCAA)
EPA 552.3 Rev 1 (2003) 1 Chloroacetic acid (MCAA, CAA)
EPA 552.3 Rev 1 (2003) 1,2 Dibromoacetic acid (DBAA)
EPA 552.3 Rev 1 (2003) 1,2 Dichloroacetic acid (DCAA)
EPA 552.3 Rev 1 (2003) 1,2 Trichloroacetic acid (TCAA)
EPA 552.3 Rev 1 (2003) 1,2 1,1,1,2-Tetrachloroethane EPA 524.2_4.1_1995 1
1,1,1-Trichloroethane EPA 524.2_4.1_1995 1,2 1,1,2,2-Tetrachloroethane EPA 524.2_4.1_1995 1
1,1,2-Trichloroethane EPA 524.2_4.1_1995 1,2 1,1-Dichloroethane EPA 524.2_4.1_1995 1
1,1-Dichloroethylene EPA 524.2_4.1_1995 1,2 1,1-Dichloropropene EPA 524.2_4.1_1995 1
1,2,3-Trichlorobenzene EPA 524.2_4.1_1995 1
Page 4 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Drinking Water 1,2,4-Trichlorobenzene EPA 524.2_4.1_1995 1,2 1,2,4-Trimethylbenzene EPA 524.2_4.1_1995 1
1,2-Dichlorobenzene EPA 524.2_4.1_1995 1,2 1,2-Dichloroethane (Ethylene dichloride)
EPA 524.2_4.1_1995 1,2 1,2-Dichloropropane EPA 524.2_4.1_1995 1,2 1,3,5-Trimethylbenzene EPA 524.2_4.1_1995 1
1,3-Dichlorobenzene EPA 524.2_4.1_1995 1
1,3-Dichloropropane EPA 524.2_4.1_1995 1
1,4-Dichlorobenzene EPA 524.2_4.1_1995 1,2 2,2-Dichloropropane EPA 524.2_4.1_1995 1
2-Chlorotoluene EPA 524.2_4.1_1995 1
4-Chlorotoluene EPA 524.2_4.1_1995 1
4-Isopropyltoluene (p-Cymene)
EPA 524.2_4.1_1995 1
Benzene EPA 524.2_4.1_1995 1,2 Bromobenzene EPA 524.2_4.1_1995 1
Bromochloromethane EPA 524.2_4.1_1995 1
Bromodichloromethane EPA 524.2_4.1_1995 1,2 Bromoform EPA 524.2_4.1_1995 1,2 Carbon tetrachloride EPA 524.2_4.1_1995 1,2 Chlorobenzene EPA 524.2_4.1_1995 1,2 Chlorodibromomethane EPA 524.2_4.1_1995 1,2 Chloroethane (Ethyl chloride)
EPA 524.2_4.1_1995 1
Chloroform EPA 524.2_4.1_1995 1,2 cis-1,2-Dichloroethylene EPA 524.2_4.1_1995 1,2 cis-1,3-Dichloropropene EPA 524.2_4.1_1995 1
Dibromomethane EPA 524.2_4.1_1995 1
Dichlorodifluoromethane (Freon-12)
EPA 524.2_4.1_1995 1
Dichloromethane (DCM, Methylene chloride)
EPA 524.2_4.1_1995 1,2 Ethylbenzene EPA 524.2_4.1_1995 1,2 Hexachlorobutadiene EPA 524.2_4.1_1995 1
Isopropylbenzene EPA 524.2_4.1_1995 1
m+p-xylene EPA 524.2_4.1_1995 1
Methyl bromide (Bromomethane)
EPA 524.2_4.1_1995 1
Methyl chloride (Chloromethane)
EPA 524.2_4.1_1995 1
Naphthalene EPA 524.2_4.1_1995 1
n-Butylbenzene EPA 524.2_4.1_1995 1
n-Propylbenzene EPA 524.2_4.1_1995 1
Page 5 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Drinking Water o-Xylene EPA 524.2_4.1_1995 1
sec-Butylbenzene EPA 524.2_4.1_1995 1
Styrene EPA 524.2_4.1_1995 1,2 tert-Butylbenzene EPA 524.2_4.1_1995 1
Tetrachloroethylene (Perchloroethylene)
EPA 524.2_4.1_1995 1,2 Toluene EPA 524.2_4.1_1995 1,2 Total Trihalomethanes EPA 524.2_4.1_1995 1,2 trans-1,2-Dichloroethylene EPA 524.2_4.1_1995 1,2 Trichloroethene (Trichloroethylene)
EPA 524.2_4.1_1995 1,2 Trichlorofluoromethane (Freon 11)
EPA 524.2_4.1_1995 1
Vinyl chloride EPA 524.2_4.1_1995 1,2 Xylene (total)
EPA 524.2_4.1_1995 1,2 4,4'-DDD EPA 525.2_2_1995 1
4,4'-DDE EPA 525.2_2_1995 1
4,4'-DDT EPA 525.2_2_1995 1
Acenaphthylene EPA 525.2_2_1995 1
Alachlor EPA 525.2_2_1995 1
Aldrin EPA 525.2_2_1995 1
Ametryn EPA 525.2_2_1995 1
Anthracene EPA 525.2_2_1995 1
Atrazine EPA 525.2_2_1995 1,2 Benzo(a)anthracene EPA 525.2_2_1995 1
Benzo(a)pyrene EPA 525.2_2_1995 1,2 Benzo(g,h,i)perylene EPA 525.2_2_1995 1
Benzo(k)fluoranthene EPA 525.2_2_1995 1
Benzo[b]fluoranthene EPA 525.2_2_1995 1
bis(2-Ethylhexyl) phthalate (DEHP)
EPA 525.2_2_1995 1
Bromacil EPA 525.2_2_1995 1
Butachlor EPA 525.2_2_1995 1
Butyl benzyl phthalate EPA 525.2_2_1995 Butylate EPA 525.2_2_1995 1
Chlorobenzilate EPA 525.2_2_1995 1
Chloroneb EPA 525.2_2_1995 1
Chloropropham EPA 525.2_2_1995 1
Chlorothalonil EPA 525.2_2_1995 1
Chlorpyrifos EPA 525.2_2_1995 1
Chrysene EPA 525.2_2_1995 1
Page 6 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Drinking Water cis-Permethrin EPA 525.2_2_1995 1
Cyanazine EPA 525.2_2_1995 1
Cycloate EPA 525.2_2_1995 1
Dacthal (DCPA)
EPA 525.2_2_1995 1
Di(2-ethylhexyl)adipate EPA 525.2_2_1995 1,2 Di(2-ethylhexyl)phthalate EPA 525.2_2_1995 1,2 Dibenz(a,h) anthracene EPA 525.2_2_1995 1
Dieldrin EPA 525.2_2_1995 1
Diethyl phthalate EPA 525.2_2_1995 1
Dimethyl phthalate EPA 525.2_2_1995 1
Di-n-butyl phthalate EPA 525.2_2_1995 1
Diphenamid EPA 525.2_2_1995 1
Endosulfan I EPA 525.2_2_1995 1
Endosulfan II EPA 525.2_2_1995 1
Endosulfan sulfate EPA 525.2_2_1995 1
Endrin EPA 525.2_2_1995 1,2 Endrin aldehyde EPA 525.2_2_1995 1
EPTC (Eptam, s-ethyl-dipropyl thio carbamate)
EPA 525.2_2_1995 1
Ethoprop EPA 525.2_2_1995 1
Etridiazole EPA 525.2_2_1995 1
Fenarimol EPA 525.2_2_1995 1
Fluoranthene EPA 525.2_2_1995 Fluorene EPA 525.2_2_1995 1
gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 525.2_2_1995 1,2 Heptachlor EPA 525.2_2_1995 1,2 Heptachlor epoxide EPA 525.2_2_1995 1,2 Hexachlorobenzene EPA 525.2_2_1995 1,2 Hexachlorocyclopentadiene EPA 525.2_2_1995 1,2 Hexazinone EPA 525.2_2_1995 1
Indeno(1,2,3-cd) pyrene EPA 525.2_2_1995 1
Methoxychlor EPA 525.2_2_1995 1,2 Metolachlor EPA 525.2_2_1995 1
Metribuzin EPA 525.2_2_1995 1
Mevinphos EPA 525.2_2_1995 1
MGK-264 EPA 525.2_2_1995 1
Molinate EPA 525.2_2_1995 1
Napropamide EPA 525.2_2_1995 1
Page 7 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Drinking Water Norflurazon EPA 525.2_2_1995 1
Pebulate EPA 525.2_2_1995 1
Phenanthrene EPA 525.2_2_1995 1
Prometryn EPA 525.2_2_1995 1
Pronamide (Kerb)
EPA 525.2_2_1995 1
Propachlor (Ramrod)
EPA 525.2_2_1995 1
Propazine EPA 525.2_2_1995 1
Pyrene EPA 525.2_2_1995 1
Simazine EPA 525.2_2_1995 1,2 Simetryn EPA 525.2_2_1995 1
Terbacil EPA 525.2_2_1995 1
Terbutryn EPA 525.2_2_1995 1
trans Permethrin EPA 525.2_2_1995 1
Triademefon EPA 525.2_2_1995 1
Trifluralin (Treflan)
EPA 525.2_2_1995 1
Vernolate EPA 525.2_2_1995 1
Endothall EPA 548.1_1_1992 1,2 Total coli/E.coli - detect SM 9223 B Colilert 18 (PA)
Non-Potable Water Cyanide, Total ASTM D7511-12 3
n-Hexane Extractable Material (O&G)
EPA 1664A_1_1999 Turbidity EPA 180.1_2_1993 Chromium, Hexavalent EPA 218.6_3.3_1994 Chloride EPA 300.0_2.1_1993 Fluoride EPA 300.0_2.1_1993 Nitrate EPA 300.0_2.1_1993 Nitrate + Nitrite EPA 300.0_2.1_1993 Nitrite EPA 300.0_2.1_1993 Orthophosphate EPA 300.0_2.1_1993 Sulfate EPA 300.0_2.1_1993 Bromate EPA 300.1_1_1997 Bromide EPA 300.1_1_1997 Chlorate EPA 300.1_1_1997 Alkalinity EPA 310.2_1974 Ammonia EPA 350.1_2_1993 Nitrogen, Total Kjeldahl EPA 351.2_2_1993 Dissolved Oxygen Hach 10360 rev 1.2 Page 8 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Non-Potable Water Cyanide, Available OIA 1677 Color SM 2120 B-2011 Acidity SM 2310 B-2011 Alkalinity SM 2320 B-2011 Hardness (calc.)
SM 2340 B-2011 Specific Conductance SM 2510 B-2011 Salinity SM 2520 B-2011 Solids, Total SM 2540 B-2011 Solids, Total Dissolved SM 2540 C-2011 Solids, Total Volatile SM 2540 E-2011 9
Solids, Settleable SM 2540 F-2011 Chlorine (Residual), Free SM 4500-Cl G-2011 5
Chlorine (Residual), Total SM 4500-Cl G-2011 5
Chlorine Dioxide SM 4500-ClO2 D-93 5
Cyanide, Weak Acid Dissociable SM 4500-CN-I-97 pH SM 4500-H+ B-2011 Nitrate SM 4500-NO3-F-2011 Nitrate + Nitrite SM 4500-NO3-F-2011 Nitrite SM 4500-NO3-F-2011 Orthophosphate SM 4500-P F-2011 Phosphorus, Total SM 4500-P F-2011 Sulfide SM 4500-S2-F-2011 Sulfite SM 4500-SO3-B-2011 Biochemical Oxygen Demand (BOD)
SM 5210 B-2011 Chemical Oxygen Demand (COD)
SM 5220 D-2011 Total Organic Carbon SM 5310 B-2011 Solids, Total Suspended USGS I-3765-85 Aluminum EPA 200.7_4.4_1994 Antimony EPA 200.7_4.4_1994 Arsenic EPA 200.7_4.4_1994 Barium EPA 200.7_4.4_1994 Beryllium EPA 200.7_4.4_1994 Boron EPA 200.7_4.4_1994 Cadmium EPA 200.7_4.4_1994 Calcium EPA 200.7_4.4_1994 Chromium EPA 200.7_4.4_1994 Cobalt EPA 200.7_4.4_1994 Page 9 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Non-Potable Water Copper EPA 200.7_4.4_1994 Hardness, Total (as CaCO3)
EPA 200.7_4.4_1994 3
Iron EPA 200.7_4.4_1994 Lead EPA 200.7_4.4_1994 Magnesium EPA 200.7_4.4_1994 Manganese EPA 200.7_4.4_1994 Molybdenum EPA 200.7_4.4_1994 Nickel EPA 200.7_4.4_1994 Phosphorus EPA 200.7_4.4_1994 Potassium EPA 200.7_4.4_1994 9
Selenium EPA 200.7_4.4_1994 Silica EPA 200.7_4.4_1994 Silver EPA 200.7_4.4_1994 Sodium EPA 200.7_4.4_1994 Strontium EPA 200.7_4.4_1994 Thallium EPA 200.7_4.4_1994 Tin EPA 200.7_4.4_1994 Titanium EPA 200.7_4.4_1994 Zinc EPA 200.7_4.4_1994 Aluminum EPA 200.8_5.4_1994 Antimony EPA 200.8_5.4_1994 Arsenic EPA 200.8_5.4_1994 Barium EPA 200.8_5.4_1994 Beryllium EPA 200.8_5.4_1994 Cadmium EPA 200.8_5.4_1994 Chromium EPA 200.8_5.4_1994 Cobalt EPA 200.8_5.4_1994 Copper EPA 200.8_5.4_1994 Lead EPA 200.8_5.4_1994 Manganese EPA 200.8_5.4_1994 Molybdenum EPA 200.8_5.4_1994 Nickel EPA 200.8_5.4_1994 Selenium EPA 200.8_5.4_1994 Silver EPA 200.8_5.4_1994 Strontium EPA 200.8_5.4_1994 Thallium EPA 200.8_5.4_1994 Thorium EPA 200.8_5.4_1994 Page 10 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Non-Potable Water Tin EPA 200.8_5.4_1994 Titanium EPA 200.8_5.4_1994 Total Uranium EPA 200.8_5.4_1994 Vanadium EPA 200.8_5.4_1994 Zinc EPA 200.8_5.4_1994 Mercury EPA 245.1_3_1994 4,4'-DDD EPA 608.3 14 4,4'-DDE EPA 608.3 14 4,4'-DDT EPA 608.3 14 Alachlor EPA 608.3 14 Aldrin EPA 608.3 14 alpha-BHC (alpha-Hexachlorocyclohexane)
EPA 608.3 14 alpha-Chlordane EPA 608.3 14 Aroclor-1016 (PCB-1016)
EPA 608.3 14 Aroclor-1221 (PCB-1221)
EPA 608.3 14 Aroclor-1232 (PCB-1232)
EPA 608.3 14 Aroclor-1242 (PCB-1242)
EPA 608.3 14 Aroclor-1248 (PCB-1248)
EPA 608.3 14 Aroclor-1254 (PCB-1254)
EPA 608.3 14 Aroclor-1260 (PCB-1260)
EPA 608.3 14 Atrazine EPA 608.3 14 beta-BHC (beta-Hexachlorocyclohexane)
EPA 608.3 14 Chlordane (tech.)
EPA 608.3 14 delta-BHC EPA 608.3 14 Dieldrin EPA 608.3 14 Endosulfan I EPA 608.3 14 Endosulfan II EPA 608.3 14 Endosulfan sulfate EPA 608.3 14 Endrin EPA 608.3 14 Endrin aldehyde EPA 608.3 14 gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 608.3 14 gamma-Chlordane EPA 608.3 14 Heptachlor EPA 608.3 14 Heptachlor epoxide EPA 608.3 14 Methoxychlor EPA 608.3 14 Metribuzin EPA 608.3 14 Propachlor (Ramrod)
EPA 608.3 14 Page 11 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Non-Potable Water Simazine EPA 608.3 14 Toxaphene (Chlorinated camphene)
EPA 608.3 14 Trifluralin (Treflan)
EPA 608.3 14 2,4,5-T EPA 615 2,4-D EPA 615 2,4-DB EPA 615 Dalapon EPA 615 Dicamba EPA 615 Dichloroprop (Dichlorprop)
EPA 615 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
EPA 615 MCPA EPA 615 3,8 MCPP EPA 615 3,8 Silvex (2,4,5-TP)
EPA 615 Trichlopyr EPA 615 Diesel range organics (DRO)
WDOE NWTPH-Dx_(1997) 4,17,18 Gasoline range organics (GRO)
WDOE NWTPH-Gx_(1997) 4,17,19 1,1,1,2-Tetrachloroethane EPA 624.1 13 1,1,1-Trichloroethane EPA 624.1 13 1,1,2,2-Tetrachloroethane EPA 624.1 13 1,1,2-Trichloroethane EPA 624.1 13 1,1-Dichloroethane EPA 624.1 13 1,1-Dichloroethylene EPA 624.1 13 1,2,3-Trichlorobenzene EPA 624.1 13 1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA 624.1 13 1,2-Dichlorobenzene EPA 624.1 13 1,2-Dichloroethane (Ethylene dichloride)
EPA 624.1 13 1,2-Dichloropropane EPA 624.1 13 1,3-Dichlorobenzene EPA 624.1 13 1,4-Dichlorobenzene EPA 624.1 13 2-Butanone (Methyl ethyl ketone, MEK)
EPA 624.1 13 2-Chloroethyl vinyl ether EPA 624.1 13 2-Picoline (2-Methylpyridine)
EPA 624.1 13 4-Isopropyltoluene (p-Cymene)
EPA 624.1 13 Acetone EPA 624.1 13 Acrolein (Propenal)
EPA 624.1 13 Acrylonitrile EPA 624.1 13 Benzene EPA 624.1 13 Page 12 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Non-Potable Water Bromodichloromethane EPA 624.1 13 Bromoform EPA 624.1 13 Carbon tetrachloride EPA 624.1 13 Chlorobenzene EPA 624.1 13 Chlorodibromomethane EPA 624.1 13 Chloroethane (Ethyl chloride)
EPA 624.1 13 Chloroform EPA 624.1 13 cis-1,3-Dichloropropene EPA 624.1 13 Dibromochloropropane EPA 624.1 13 Dichloromethane (DCM, Methylene chloride)
EPA 624.1 13 Diethyl ether EPA 624.1 13 Epichlorohydrin (1-Chloro-2,3-epoxypropane)
EPA 624.1 13 Ethylbenzene EPA 624.1 13 Methyl bromide (Bromomethane)
EPA 624.1 13 Methyl chloride (Chloromethane)
EPA 624.1 13 Methyl tert-butyl ether (MTBE)
EPA 624.1 13 Methylene chloride (Dichloromethane)
EPA 624.1 13 p-Dioxane EPA 624.1 13 Styrene EPA 624.1 13 Tetrachloroethylene (Perchloroethylene)
EPA 624.1 13 Toluene EPA 624.1 13 trans-1,2-Dichloroethylene EPA 624.1 13 trans-1,3-Dichloropropylene EPA 624.1 13 Trichloroethene (Trichloroethylene)
EPA 624.1 13 Trichlorofluoromethane (Freon 11)
EPA 624.1 13 Vinyl chloride EPA 624.1 13 1,2,4-Trichlorobenzene EPA 625.1 15 1,2-Diphenylhydrazine EPA 625.1 15 2,3,6-Trichlorophenol (4C)
EPA 625.1 15 2,4,5-Trichlorophenol EPA 625.1 15 2,4,6-Trichlorophenol EPA 625.1 15 2,4-Dichlorophenol EPA 625.1 15 2,4-Dimethylphenol EPA 625.1 15 2,4-Dinitrophenol EPA 625.1 15 2,4-Dinitrotoluene (2,4-DNT)
EPA 625.1 15 2,6-Dinitrotoluene (2,6-DNT)
EPA 625.1 15 2-Chloronaphthalene EPA 625.1 15 Page 13 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Non-Potable Water 2-Chlorophenol EPA 625.1 15 2-Methylnaphthalene EPA 625.1 15 2-Nitrophenol EPA 625.1 15 3,3'-Dichlorobenzidine EPA 625.1 15 3-Methylcholanthrene EPA 625.1 15 4,4'-DDD EPA 625.1 15 4,4'-DDE EPA 625.1 15 4,4'-DDT EPA 625.1 15 4,6-Dinitro-2-methylphenol EPA 625.1 15 4-Bromophenyl phenyl ether (BDE-3)
EPA 625.1 15 4-Chloro-3-methylphenol EPA 625.1 15 4-Chlorophenol EPA 625.1 15 4-Chlorophenyl phenylether EPA 625.1 15 4-Nitrophenol EPA 625.1 15 Acenaphthene EPA 625.1 15 Acenaphthylene EPA 625.1 15 Aldrin EPA 625.1 15 alpha-BHC (alpha-Hexachlorocyclohexane)
EPA 625.1 15 alpha-Terpineol EPA 625.1 15 Anthracene EPA 625.1 15 Benzidine EPA 625.1 15 Benzo(a)anthracene EPA 625.1 15 Benzo(a)pyrene EPA 625.1 15 Benzo(g,h,i)perylene EPA 625.1 15 Benzo(j)fluoranthene EPA 625.1 15 Benzo(k)fluoranthene EPA 625.1 15 Benzo(r,s,t)pentaphene EPA 625.1 15 Benzo[b]fluoranthene EPA 625.1 15 Benzoic acid EPA 625.1 15 beta-BHC (beta-Hexachlorocyclohexane)
EPA 625.1 15 bis(2-Chloroethoxy)methane EPA 625.1 15 bis(2-Chloroethyl) ether EPA 625.1 15 bis(2-Chloroisopropyl) ether EPA 625.1 15 bis(2-Ethylhexyl) phthalate (DEHP)
EPA 625.1 15 Butyl benzyl phthalate EPA 625.1 15 Carbazole EPA 625.1 15 Chrysene EPA 625.1 15 Page 14 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Non-Potable Water delta-BHC EPA 625.1 15 Di(2-ethylhexyl)adipate EPA 625.1 15 Dibenz(a,h) acridine EPA 625.1 15 Dibenz(a,h) anthracene EPA 625.1 15 Dibenz(a,j) acridine EPA 625.1 15 Dibenzo(a,e) pyrene EPA 625.1 15 Dibenzo(a,h) pyrene EPA 625.1 15 Dibenzofuran EPA 625.1 15 Dieldrin EPA 625.1 15 Diethyl phthalate EPA 625.1 15 Dimethyl phthalate EPA 625.1 15 Di-n-butyl phthalate EPA 625.1 15 Di-n-octyl phthalate EPA 625.1 15 Endosulfan I EPA 625.1 15 Endosulfan II EPA 625.1 15 Endosulfan sulfate EPA 625.1 15 Endrin EPA 625.1 15 Fluoranthene EPA 625.1 15 Fluorene EPA 625.1 15 gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 625.1 15 Heptachlor EPA 625.1 15 Heptachlor epoxide EPA 625.1 15 Hexachlorobenzene EPA 625.1 15 Hexachlorobutadiene EPA 625.1 15 Hexachlorocyclopentadiene EPA 625.1 15 Hexachloroethane EPA 625.1 15 Indeno(1,2,3-cd) pyrene EPA 625.1 15 Isophorone EPA 625.1 15 Methoxychlor EPA 625.1 15 Naphthalene EPA 625.1 15 n-Docosane EPA 625.1 15 n-Dodecane EPA 625.1 15 n-Eicosane EPA 625.1 15 n-Hexadecane EPA 625.1 15 Nitrobenzene EPA 625.1 15 n-Nitrosodimethylamine EPA 625.1 15 N-Nitroso-di-n-propylamine EPA 625.1 15 Page 15 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Non-Potable Water n-Nitrosodiphenylamine EPA 625.1 15 n-Octadecane EPA 625.1 15 n-Tetradecane EPA 625.1 15 Pentachloroethane EPA 625.1 15 Pentachlorophenol EPA 625.1 15 Perylene EPA 625.1 15 Phenanthrene EPA 625.1 15 Phenol EPA 625.1 15 Pyrene EPA 625.1 15 Pyridine EPA 625.1 15 Ignitability ASTM D93-02 Solid and Chemical Materials Ammonia EPA 350.1_2_1993 Nitrogen, Total Kjeldahl EPA 351.2_2_1993 9
Sulfide, Acid-Soluble EPA 9034_1996 Aluminum EPA 6010D_(7/14) 10 Antimony EPA 6010D_(7/14) 10 Arsenic EPA 6010D_(7/14) 10 Barium EPA 6010D_(7/14) 10 Beryllium EPA 6010D_(7/14) 10 Boron EPA 6010D_(7/14) 9,10 Cadmium EPA 6010D_(7/14) 10 Calcium EPA 6010D_(7/14) 10 Chromium EPA 6010D_(7/14) 10 Cobalt EPA 6010D_(7/14) 10 Copper EPA 6010D_(7/14) 10 Iron EPA 6010D_(7/14) 10 Lead EPA 6010D_(7/14) 9,10 Magnesium EPA 6010D_(7/14) 10 Manganese EPA 6010D_(7/14) 10 Molybdenum EPA 6010D_(7/14) 10 Nickel EPA 6010D_(7/14) 10 Phosphorus, Total EPA 6010D_(7/14) 10 Potassium EPA 6010D_(7/14) 10 Selenium EPA 6010D_(7/14) 10 Silver EPA 6010D_(7/14) 9,10 Sodium EPA 6010D_(7/14) 10 Page 16 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials Strontium EPA 6010D_(7/14) 10 Thallium EPA 6010D_(7/14) 9,10 Tin EPA 6010D_(7/14) 10 Titanium EPA 6010D_(7/14) 10 Vanadium EPA 6010D_(7/14) 10 Zinc EPA 6010D_(7/14) 10 Aluminum EPA 6020B_(7/14) 10 Antimony EPA 6020B_(7/14) 10 Arsenic EPA 6020B_(7/14) 10 Barium EPA 6020B_(7/14) 10 Beryllium EPA 6020B_(7/14) 10 Cadmium EPA 6020B_(7/14) 10 Chromium EPA 6020B_(7/14) 10 Cobalt EPA 6020B_(7/14) 10 Copper EPA 6020B_(7/14) 10 Lead EPA 6020B_(7/14) 9,10 Manganese EPA 6020B_(7/14) 10 Molybdenum EPA 6020B_(7/14) 10 Nickel EPA 6020B_(7/14) 10 Selenium EPA 6020B_(7/14) 10 Silver EPA 6020B_(7/14) 10 Strontium EPA 6020B_(7/14) 10 Thallium EPA 6020B_(7/14) 9,10 Titanium EPA 6020B_(7/14) 10 Vanadium EPA 6020B_(7/14) 10 Zinc EPA 6020B_(7/14) 10 Mercury EPA 7470A_1_1994 Mercury EPA 7471B_(1/98)
Aroclor-1016 (PCB-1016)
EPA 600/4-81-045 Aroclor-1221 (PCB-1221)
EPA 600/4-81-045 Aroclor-1232 (PCB-1232)
EPA 600/4-81-045 Aroclor-1242 (PCB-1242)
EPA 600/4-81-045 Aroclor-1248 (PCB-1248)
EPA 600/4-81-045 Aroclor-1254 (PCB-1254)
EPA 600/4-81-045 Aroclor-1260 (PCB-1260)
EPA 600/4-81-045 4,4'-DDD EPA 8081B_(2/07) 4,4'-DDE EPA 8081B_(2/07)
Page 17 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials 4,4'-DDT EPA 8081B_(2/07)
Aldrin EPA 8081B_(2/07) alpha-BHC (alpha-Hexachlorocyclohexane)
EPA 8081B_(2/07) alpha-Chlordane EPA 8081B_(2/07) beta-BHC (beta-Hexachlorocyclohexane)
EPA 8081B_(2/07)
Captafol EPA 8081B_(2/07)
Chlordane (tech.)
EPA 8081B_(2/07)
Chlorobenzilate EPA 8081B_(2/07)
Chloroneb EPA 8081B_(2/07)
Chloropropylate EPA 8081B_(2/07)
Chlorothalonil EPA 8081B_(2/07)
Dacthal (DCPA)
EPA 8081B_(2/07) delta-BHC EPA 8081B_(2/07)
Diallate EPA 8081B_(2/07)
Dichlone EPA 8081B_(2/07)
Dicofol EPA 8081B_(2/07)
Dieldrin EPA 8081B_(2/07)
Endosulfan I EPA 8081B_(2/07)
Endosulfan II EPA 8081B_(2/07)
Endosulfan sulfate EPA 8081B_(2/07)
Endrin EPA 8081B_(2/07)
Endrin aldehyde EPA 8081B_(2/07)
Endrin ketone EPA 8081B_(2/07)
Etridiazole EPA 8081B_(2/07) gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 8081B_(2/07) gamma-Chlordane EPA 8081B_(2/07)
Halowax-1000 EPA 8081B_(2/07)
Halowax-1001 EPA 8081B_(2/07)
Halowax-1013 EPA 8081B_(2/07)
Halowax-1014 EPA 8081B_(2/07)
Halowax-1051 EPA 8081B_(2/07)
Halowax-1099 EPA 8081B_(2/07)
Heptachlor EPA 8081B_(2/07)
Heptachlor epoxide EPA 8081B_(2/07)
Isodrin EPA 8081B_(2/07)
Methoxychlor EPA 8081B_(2/07)
Mirex EPA 8081B_(2/07)
Page 18 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials Nitrofen EPA 8081B_(2/07)
Permethrin (total)
EPA 8081B_(2/07)
Perthane EPA 8081B_(2/07)
Strobane EPA 8081B_(2/07)
Toxaphene (Chlorinated camphene)
EPA 8081B_(2/07) trans-Nonachlor EPA 8081B_(2/07)
Aroclor-1016 (PCB-1016)
EPA 8082A_(2/07)
Aroclor-1221 (PCB-1221)
EPA 8082A_(2/07)
Aroclor-1232 (PCB-1232)
EPA 8082A_(2/07)
Aroclor-1242 (PCB-1242)
EPA 8082A_(2/07)
Aroclor-1248 (PCB-1248)
EPA 8082A_(2/07)
Aroclor-1254 (PCB-1254)
EPA 8082A_(2/07)
Aroclor-1260 (PCB-1260)
EPA 8082A_(2/07) 2,4,5-T EPA 8151A_(1/98) 2,4-D EPA 8151A_(1/98) 2,4-DB EPA 8151A_(1/98) 3,5-Dichlorobenzoic acid EPA 8151A_(1/98) 4-Nitrophenol EPA 8151A_(1/98) 5-Hydroxydicamba EPA 8151A_(1/98)
Acifluorfen EPA 8151A_(1/98)
Bentazon EPA 8151A_(1/98)
Chloramben EPA 8151A_(1/98)
Dacthal (DCPA)
EPA 8151A_(1/98)
Dalapon EPA 8151A_(1/98)
DCPA di acid degradate EPA 8151A_(1/98)
Dicamba EPA 8151A_(1/98)
Dichloroprop (Dichlorprop)
EPA 8151A_(1/98)
Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
EPA 8151A_(1/98)
MCPA EPA 8151A_(1/98) 8 MCPP EPA 8151A_(1/98) 8 Pentachlorophenol EPA 8151A_(1/98)
Picloram EPA 8151A_(1/98)
Silvex (2,4,5-TP)
EPA 8151A_(1/98)
Trichlopyr EPA 8151A_(1/98)
Diesel range organics (DRO)
WDOE NWTPH-Dx_(1997) 4,17,18 Gasoline range organics (GRO)
WDOE NWTPH-Gx_(1997) 4,17,19 Azinphos-methyl (Guthion)
EPA 8141B_2_(2/07) 7 Page 19 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials Bolstar (Sulprofos)
EPA 8141B_2_(2/07) 7 Chlorpyrifos EPA 8141B_2_(2/07) 7 Coumaphos EPA 8141B_2_(2/07) 7 Demeton EPA 8141B_2_(2/07) 7 Diazinon EPA 8141B_2_(2/07) 7 Dichlorovos (DDVP, Dichlorvos)
EPA 8141B_2_(2/07) 7 Dimethoate EPA 8141B_2_(2/07) 7 Disulfoton EPA 8141B_2_(2/07) 7 EPN EPA 8141B_2_(2/07) 7 Ethoprop EPA 8141B_2_(2/07) 7 Fensulfothion EPA 8141B_2_(2/07) 7 Fenthion EPA 8141B_2_(2/07) 7 Malathion EPA 8141B_2_(2/07) 7 Merphos EPA 8141B_2_(2/07) 7 Methyl parathion (Parathion, methyl)
EPA 8141B_2_(2/07) 7 Mevinphos EPA 8141B_2_(2/07) 7 Monocrotophos EPA 8141B_2_(2/07) 7 Parathion, ethyl EPA 8141B_2_(2/07) 7 Phorate EPA 8141B_2_(2/07) 7 Ronnel EPA 8141B_2_(2/07) 7 Sulfotepp EPA 8141B_2_(2/07) 7 Tetrachlorvinphos (Stirophos, Gardona)
EPA 8141B_2_(2/07) 7 Tokuthion (Prothiophos)
EPA 8141B_2_(2/07) 7 Trichloronate EPA 8141B_2_(2/07) 7 1,1,1,2-Tetrachloroethane EPA 8260D_4_(6/18) 1,1,1-Trichloro-2,2,2-trifluoroethane EPA 8260D_4_(6/18) 1,1,1-Trichloro-2-propanone EPA 8260D_4_(6/18) 1,1,1-Trichloroethane EPA 8260D_4_(6/18) 1,1,2,2-Tetrachloroethane EPA 8260D_4_(6/18) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
EPA 8260D_4_(6/18) 1,1,2-Trichloroethane EPA 8260D_4_(6/18) 1,1,2-Trichlorofluoroethane EPA 8260D_4_(6/18) 1,1-Dichloro-1-fluoroethane EPA 8260D_4_(6/18) 1,1-Dichloroethane EPA 8260D_4_(6/18) 1,1-Dichloroethylene EPA 8260D_4_(6/18) 1,1-Dichloropropene EPA 8260D_4_(6/18) 1,2,3,4-Diepoxybutane EPA 8260D_4_(6/18)
Page 20 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials 1,2,3-Trichlorobenzene EPA 8260D_4_(6/18) 1,2,3-Trichloropropane EPA 8260D_4_(6/18) 11 1,2,3-Trimethylbenzene EPA 8260D_4_(6/18) 1,2,4-Trichlorobenzene EPA 8260D_4_(6/18) 1,2,4-Trimethylbenzene EPA 8260D_4_(6/18) 1,2-Dibromo-3-chloropropane (DBCP)
EPA 8260D_4_(6/18) 11 1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA 8260D_4_(6/18) 11 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
EPA 8260D_4_(6/18) 1,2-Dichloro-1,1,2-trifluoroethane EPA 8260D_4_(6/18) 1,2-Dichlorobenzene EPA 8260D_4_(6/18) 1,2-Dichloroethane (Ethylene dichloride)
EPA 8260D_4_(6/18) 1,2-Dichloropropane EPA 8260D_4_(6/18) 1,2-Dimethoxyethane EPA 8260D_4_(6/18) 1,3,5-Trimethylbenzene EPA 8260D_4_(6/18) 1,3-Butanediol EPA 8260D_4_(6/18) 1,3-Dichloro-2-propanol EPA 8260D_4_(6/18) 1,3-Dichlorobenzene EPA 8260D_4_(6/18) 1,3-Dichloropropane EPA 8260D_4_(6/18) 1,3-Dichloropropene EPA 8260D_4_(6/18) 1,4-Butanediol EPA 8260D_4_(6/18) 1,4-Dichloro-2-butene EPA 8260D_4_(6/18) 1,4-Dichlorobenzene EPA 8260D_4_(6/18) 1,4-Difluorobenzene EPA 8260D_4_(6/18) 1,4-Dioxane (1,4-Diethyleneoxide)
EPA 8260D_4_(6/18) 11 1-Butene EPA 8260D_4_(6/18) 1-Chloro-1,2,2-trifluoroethane (Freon 133)
EPA 8260D_4_(6/18) 1-Chlorobutane EPA 8260D_4_(6/18) 1-Heptene EPA 8260D_4_(6/18) 1-Hexene EPA 8260D_4_(6/18) 1-Methyl-2-n-propylbenzene EPA 8260D_4_(6/18) 1-Propene EPA 8260D_4_(6/18) 2,2,4-Trimethylpentane EPA 8260D_4_(6/18) 2,2-Dichloro-1,1,1-trifluoroethane (Freon 123)
EPA 8260D_4_(6/18) 2,2-Dichloropropane EPA 8260D_4_(6/18) 2,2-Dimethylbutane EPA 8260D_4_(6/18) 2,2'-Oxybis(1-chloropropane)
EPA 8260D_4_(6/18) 2,3,4-Trimethylpentane EPA 8260D_4_(6/18)
Page 21 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials 2,3-Dichloropropene EPA 8260D_4_(6/18) 2,3-Dimethylbutane EPA 8260D_4_(6/18) 2,3-Dimethylpentane EPA 8260D_4_(6/18) 2,4-Dimethylpentane EPA 8260D_4_(6/18) 2-Bromofluorobenzene EPA 8260D_4_(6/18) 2-Butanone (Methyl ethyl ketone, MEK)
EPA 8260D_4_(6/18) 2-Chloro-2-methybutane (tert-Amyl chloride)
EPA 8260D_4_(6/18) 2-Chloroethanol EPA 8260D_4_(6/18) 2-Chloroethyl vinyl ether EPA 8260D_4_(6/18) 11 2-Chlorotoluene EPA 8260D_4_(6/18) 2-Ethylhexanol (2-Ethyl-1-hexanol)
EPA 8260D_4_(6/18) 2-Ethyltoluene EPA 8260D_4_(6/18) 2-Hexanone EPA 8260D_4_(6/18) 2-Hexene EPA 8260D_4_(6/18) 2-Hydroxypropionitrile EPA 8260D_4_(6/18) 2-Methoxyethanol (Methyl cellosolve)
EPA 8260D_4_(6/18) 2-Methyl-1,3-dioxolane EPA 8260D_4_(6/18) 2-Methyl-2-Butene EPA 8260D_4_(6/18) 2-Methylaniline (o-Toluidine)
EPA 8260D_4_(6/18) 2-Methylbutadiene (Isoprene)
EPA 8260D_4_(6/18) 2-Methylbutane (Isopentane)
EPA 8260D_4_(6/18) 2-Methylheptane EPA 8260D_4_(6/18) 2-Methylhexane EPA 8260D_4_(6/18) 2-Methylpentane (Isohexane)
EPA 8260D_4_(6/18) 2-methylpropane (Isobutane)
EPA 8260D_4_(6/18) 2-Nitropropane EPA 8260D_4_(6/18) 2-Pentanone EPA 8260D_4_(6/18) 2-Picoline (2-Methylpyridine)
EPA 8260D_4_(6/18) 3-Bromofluorobenzene EPA 8260D_4_(6/18) 3-Butene-1-ol EPA 8260D_4_(6/18) 3-Chloropropionitrile EPA 8260D_4_(6/18) 3-Ethyltoluene EPA 8260D_4_(6/18) 3-Methyl-1-Butene EPA 8260D_4_(6/18) 3-Methylheptane EPA 8260D_4_(6/18) 3-Methylhexane EPA 8260D_4_(6/18) 3-Methylpentane EPA 8260D_4_(6/18) 4-Bromofluorobenzene EPA 8260D_4_(6/18)
Page 22 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials 4-Chlorotoluene EPA 8260D_4_(6/18) 4-Ethyltoluene EPA 8260D_4_(6/18) 4-Isopropyltoluene (p-Cymene)
EPA 8260D_4_(6/18) 4-Methyl-1-Pentene EPA 8260D_4_(6/18) 4-Methyl-2-pentanone (MIBK)
EPA 8260D_4_(6/18) 4-Methylaniline (p-Toluidine)
EPA 8260D_4_(6/18)
Acetamide EPA 8260D_4_(6/18)
Acetone EPA 8260D_4_(6/18)
Acetylene EPA 8260D_4_(6/18)
Acrolein (Propenal)
EPA 8260D_4_(6/18)
Acrylamide EPA 8260D_4_(6/18)
Acrylic acid EPA 8260D_4_(6/18)
Acrylonitrile EPA 8260D_4_(6/18) 11 Adsorbable Organic Halides (AOX)
EPA 8260D_4_(6/18)
Allyl alcohol EPA 8260D_4_(6/18)
Allyl chloride (3-Chloropropene)
EPA 8260D_4_(6/18) alpha-Methylstyrene EPA 8260D_4_(6/18)
Benzene EPA 8260D_4_(6/18) 11 beta-Propiolactone EPA 8260D_4_(6/18) bis(2-Chloroethyl) sulfide EPA 8260D_4_(6/18) bis(Chloromethyl)ether EPA 8260D_4_(6/18)
Bromoacetone EPA 8260D_4_(6/18)
Bromobenzene EPA 8260D_4_(6/18)
Bromochloromethane EPA 8260D_4_(6/18)
Bromodichloromethane EPA 8260D_4_(6/18)
Bromoethane (Ethyl Bromide)
EPA 8260D_4_(6/18)
Bromoethene EPA 8260D_4_(6/18)
Bromoform EPA 8260D_4_(6/18)
Butyl acetate EPA 8260D_4_(6/18)
Carbon disulfide EPA 8260D_4_(6/18)
Carbon tetrachloride EPA 8260D_4_(6/18)
Chloral hydrate EPA 8260D_4_(6/18)
Chloroacetonitrile EPA 8260D_4_(6/18)
Chlorobenzene EPA 8260D_4_(6/18)
Chlorodibromomethane EPA 8260D_4_(6/18)
Chlorodifluoromethane (Freon-22)
EPA 8260D_4_(6/18)
Chloroethane (Ethyl chloride)
EPA 8260D_4_(6/18)
Page 23 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials Chloroform EPA 8260D_4_(6/18)
Chloromethyl methyl ether EPA 8260D_4_(6/18)
Chloropicrin EPA 8260D_4_(6/18)
Chloroprene (2-Chloro-1,3-butadiene)
EPA 8260D_4_(6/18) cis & trans-1,2-Dichloroethene EPA 8260D_4_(6/18) cis-1,2-Dichloroethylene EPA 8260D_4_(6/18) cis-1,3-Dichloropropene EPA 8260D_4_(6/18) cis-2-Butene EPA 8260D_4_(6/18) cis-2-Hexene EPA 8260D_4_(6/18) cis-2-pentene EPA 8260D_4_(6/18)
Cycloate EPA 8260D_4_(6/18)
Cyclohexanol EPA 8260D_4_(6/18)
Cyclopentane EPA 8260D_4_(6/18)
Cyclopentene EPA 8260D_4_(6/18)
Decanal EPA 8260D_4_(6/18)
Dibromochloropropane EPA 8260D_4_(6/18)
Dibromofluoromethane EPA 8260D_4_(6/18)
Dibromomethane EPA 8260D_4_(6/18)
Dichlorodifluoromethane (Freon-12)
EPA 8260D_4_(6/18)
Dichlorofluoromethane (Freon 21)
EPA 8260D_4_(6/18)
Dichlorotetrafluoroethane EPA 8260D_4_(6/18)
Dicyclopentadiene EPA 8260D_4_(6/18)
Diethyl ether EPA 8260D_4_(6/18)
Diethylamine EPA 8260D_4_(6/18)
Diethylene glycol EPA 8260D_4_(6/18)
Dimethyl disulfide EPA 8260D_4_(6/18)
Dimethyl sulfoxide EPA 8260D_4_(6/18)
Epichlorohydrin (1-Chloro-2,3-epoxypropane)
EPA 8260D_4_(6/18)
Ethane EPA 8260D_4_(6/18)
Ethene EPA 8260D_4_(6/18)
Ethyl acetate EPA 8260D_4_(6/18)
Ethyl acrylate EPA 8260D_4_(6/18)
Ethyl methacrylate EPA 8260D_4_(6/18)
Ethylbenzene EPA 8260D_4_(6/18) 11 Ethylene glycol EPA 8260D_4_(6/18)
Ethylene oxide EPA 8260D_4_(6/18)
Ethylene thiourea EPA 8260D_4_(6/18)
Page 24 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials Ethyleneimine EPA 8260D_4_(6/18)
Fluorobenzene EPA 8260D_4_(6/18)
Fluoromethane (Freon 41)
EPA 8260D_4_(6/18)
Heptanal EPA 8260D_4_(6/18)
Hexachlorobutadiene EPA 8260D_4_(6/18)
Hexachloroethane EPA 8260D_4_(6/18)
Iodomethane (Methyl iodide)
EPA 8260D_4_(6/18)
Isopropyl acetate EPA 8260D_4_(6/18)
Isopropyl alcohol (2-Propanol, Isopropanol)
EPA 8260D_4_(6/18)
Isopropylbenzene EPA 8260D_4_(6/18) m+p-xylene EPA 8260D_4_(6/18) 11 Malononitrile EPA 8260D_4_(6/18)
Methacrylonitrile EPA 8260D_4_(6/18)
Methane EPA 8260D_4_(6/18)
Methanol EPA 8260D_4_(6/18)
Methyl acrylate EPA 8260D_4_(6/18)
Methyl bromide (Bromomethane)
EPA 8260D_4_(6/18)
Methyl chloride (Chloromethane)
EPA 8260D_4_(6/18)
Methyl formate EPA 8260D_4_(6/18)
Methyl methacrylate EPA 8260D_4_(6/18)
Methyl tert-butyl ether (MTBE)
EPA 8260D_4_(6/18)
Methylcyclopentane EPA 8260D_4_(6/18)
Methylene chloride (Dichloromethane)
EPA 8260D_4_(6/18) n, n-Dimethylformamide EPA 8260D_4_(6/18) n-Amyl acetate EPA 8260D_4_(6/18) n-Amyl alcohol EPA 8260D_4_(6/18)
Naphthalene EPA 8260D_4_(6/18) n-Butane EPA 8260D_4_(6/18) n-Butyl alcohol (1-Butanol, n-Butanol)
EPA 8260D_4_(6/18) n-Butylbenzene EPA 8260D_4_(6/18) n-Butylcyclopentane EPA 8260D_4_(6/18) n-Heptane EPA 8260D_4_(6/18)
Nitrobenzene EPA 8260D_4_(6/18) n-Nitroso-di-n-butylamine EPA 8260D_4_(6/18) n-Nonane EPA 8260D_4_(6/18) n-Octane EPA 8260D_4_(6/18) n-Pentane EPA 8260D_4_(6/18)
Page 25 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials n-Propane EPA 8260D_4_(6/18) n-Propanol (1-Propanol)
EPA 8260D_4_(6/18) n-Propylamine EPA 8260D_4_(6/18) n-Propylbenzene EPA 8260D_4_(6/18) o-Xylene EPA 8260D_4_(6/18) 11 p-Diethylbenzene EPA 8260D_4_(6/18)
Pentachloroethane EPA 8260D_4_(6/18)
Pentafluorobenzene EPA 8260D_4_(6/18)
Propargyl alcohol EPA 8260D_4_(6/18)
Propyne EPA 8260D_4_(6/18)
Purgeable Organic Halides EPA 8260D_4_(6/18)
Pyridine EPA 8260D_4_(6/18)
Sec-Amyl Alcohol (2-Pentanol)
EPA 8260D_4_(6/18) sec-Butylbenzene EPA 8260D_4_(6/18)
S-Methyl thioacetate (S-Methyl etanethioate)
EPA 8260D_4_(6/18)
Styrene EPA 8260D_4_(6/18) 11 tert-Amyl ethyl ether (TAEE)
EPA 8260D_4_(6/18) tert-Butylbenzene EPA 8260D_4_(6/18)
Tetrachloroethylene (Perchloroethylene)
EPA 8260D_4_(6/18)
Tetrahydrofuran (THF)
EPA 8260D_4_(6/18)
Toluene EPA 8260D_4_(6/18)
Total Trihalomethanes EPA 8260D_4_(6/18)
Total Volatile Petroleum Hydrocarbons (VPH)
EPA 8260D_4_(6/18) trans-1,2-Dichloroethylene EPA 8260D_4_(6/18) trans-1,3-Dichloropropylene EPA 8260D_4_(6/18) trans-1,4-Dichloro-2-butene EPA 8260D_4_(6/18) trans-2-Butene EPA 8260D_4_(6/18) trans-2-Hexene EPA 8260D_4_(6/18) trans-2-pentene EPA 8260D_4_(6/18)
Trichloroethene (Trichloroethylene)
EPA 8260D_4_(6/18)
Trichlorofluoromethane (Freon 11)
EPA 8260D_4_(6/18)
Triethylamine EPA 8260D_4_(6/18)
Trifluoromethane (Freon 23)
EPA 8260D_4_(6/18)
Vinyl acetate EPA 8260D_4_(6/18)
Vinyl bromide EPA 8260D_4_(6/18)
Vinyl chloride EPA 8260D_4_(6/18) 11 Xylene (total)
EPA 8260D_4_(6/18)
Page 26 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials 1,2,4-Trichlorobenzene EPA 8270E_6_(6/18) 1,2-Dibromo-3-chloropropane (DBCP)
EPA 8270E_6_(6/18) 1,2-Dichlorobenzene EPA 8270E_6_(6/18) 1,2-Dinitrobenzene EPA 8270E_6_(6/18) 1,2-Diphenylhydrazine EPA 8270E_6_(6/18) 1,3-Dichlorobenzene EPA 8270E_6_(6/18) 1,4-Dichlorobenzene EPA 8270E_6_(6/18) 1,4-Dinitrobenzene EPA 8270E_6_(6/18) 1,4-Phenylenediamine EPA 8270E_6_(6/18) 1-Acetyl-2-thiourea EPA 8270E_6_(6/18) 2,3,4,6-Tetrachlorophenol EPA 8270E_6_(6/18) 2,4,5-Trichlorophenol EPA 8270E_6_(6/18) 2,4,5-Trimethylaniline EPA 8270E_6_(6/18) 2,4,6-Trichlorophenol EPA 8270E_6_(6/18) 2,4-Diaminotoluene EPA 8270E_6_(6/18) 2,4-Dichlorophenol EPA 8270E_6_(6/18) 2,4-Dimethylphenol EPA 8270E_6_(6/18) 2,4-Dinitrophenol EPA 8270E_6_(6/18) 2,4-Dinitrotoluene (2,4-DNT)
EPA 8270E_6_(6/18) 2,6-Dichlorophenol EPA 8270E_6_(6/18) 2,6-Dinitrotoluene (2,6-DNT)
EPA 8270E_6_(6/18) 2-Aminoanthraquinone EPA 8270E_6_(6/18) 2-Chloronaphthalene EPA 8270E_6_(6/18) 2-Chlorophenol EPA 8270E_6_(6/18) 2-Cyclohexyl-4,6-dinitrophenol EPA 8270E_6_(6/18) 2-Methylnaphthalene EPA 8270E_6_(6/18) 2-Methylphenol (o-Cresol)
EPA 8270E_6_(6/18) 2-Nitrophenol EPA 8270E_6_(6/18) 3-(Chloromethyl) pyridine hydrochloride EPA 8270E_6_(6/18) 3,3'-Dichlorobenzidine EPA 8270E_6_(6/18) 3,3'-Dimethoxybenzidine EPA 8270E_6_(6/18) 3-Amino-9-ethylcarbazole EPA 8270E_6_(6/18) 4,4'-DDD EPA 8270E_6_(6/18) 4,4'-DDE EPA 8270E_6_(6/18) 4,4'-DDT EPA 8270E_6_(6/18) 4,4'-Methylenebis(2-chloroaniline)
EPA 8270E_6_(6/18) 4,4'-Methylenebis(n, n-dimethylaniline)
EPA 8270E_6_(6/18)
Page 27 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials 4,4'-Oxydianiline EPA 8270E_6_(6/18) 4,6-Dinitro-2-methylphenol EPA 8270E_6_(6/18) 4-Chloro-1,2-phenylenediamine EPA 8270E_6_(6/18) 4-Chloro-1,3-phenylenediamine EPA 8270E_6_(6/18) 4-Chloro-3-methylphenol EPA 8270E_6_(6/18) 4-Chlorophenol EPA 8270E_6_(6/18) 4-Chlorophenyl phenylether EPA 8270E_6_(6/18) 4-Dimethyl aminoazobenzene EPA 8270E_6_(6/18) 4-Nitrobiphenyl EPA 8270E_6_(6/18) 4-Nitrophenol EPA 8270E_6_(6/18) 5,5-Diphenylhydantoin EPA 8270E_6_(6/18) 5-Chloro-2-methylaniline EPA 8270E_6_(6/18) 5-Nitroacenaphthene EPA 8270E_6_(6/18) 5-Nitro-o-anisidine EPA 8270E_6_(6/18)
Acenaphthene EPA 8270E_6_(6/18)
Acenaphthylene EPA 8270E_6_(6/18) alpha-Terpineol EPA 8270E_6_(6/18)
Aminoazobenzene EPA 8270E_6_(6/18)
Anilazine EPA 8270E_6_(6/18)
Anthracene EPA 8270E_6_(6/18)
Aramite EPA 8270E_6_(6/18)
Barban EPA 8270E_6_(6/18)
Benzidine EPA 8270E_6_(6/18)
Benzo(a)anthracene EPA 8270E_6_(6/18)
Benzo(a)pyrene EPA 8270E_6_(6/18)
Benzo(g,h,i)perylene EPA 8270E_6_(6/18)
Benzo(k)fluoranthene EPA 8270E_6_(6/18)
Benzo[b]fluoranthene EPA 8270E_6_(6/18)
Benzoic acid EPA 8270E_6_(6/18)
Benzyl alcohol EPA 8270E_6_(6/18) bis(2-Chloroethoxy)methane EPA 8270E_6_(6/18) bis(2-Chloroethyl) ether EPA 8270E_6_(6/18) bis(2-Chloroisopropyl) ether EPA 8270E_6_(6/18)
Bromoxynil octanate EPA 8270E_6_(6/18)
Butyl benzyl phthalate EPA 8270E_6_(6/18)
Captafol EPA 8270E_6_(6/18)
Captan EPA 8270E_6_(6/18)
Page 28 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials Carbazole EPA 8270E_6_(6/18)
Carbophenothion EPA 8270E_6_(6/18)
Chrysene EPA 8270E_6_(6/18)
Di(2-ethylhexyl)adipate EPA 8270E_6_(6/18)
Di(2-ethylhexyl)phthalate EPA 8270E_6_(6/18)
Dibenz(a,h) acridine EPA 8270E_6_(6/18)
Dibenz(a,h) anthracene EPA 8270E_6_(6/18)
Dibenz(a,j) acridine EPA 8270E_6_(6/18)
Dibenzo(a,e) pyrene EPA 8270E_6_(6/18)
Dibenzofuran EPA 8270E_6_(6/18)
Dibenzothiophene EPA 8270E_6_(6/18)
Dichlone EPA 8270E_6_(6/18)
Diethyl phthalate EPA 8270E_6_(6/18)
Diethyl sulfate EPA 8270E_6_(6/18)
Diethylstilbestrol EPA 8270E_6_(6/18)
Dihydrosafrole EPA 8270E_6_(6/18)
Dimethyl phthalate EPA 8270E_6_(6/18)
Di-n-butyl phthalate EPA 8270E_6_(6/18)
Dinocap EPA 8270E_6_(6/18)
Di-n-octyl phthalate EPA 8270E_6_(6/18)
Diphenylamine EPA 8270E_6_(6/18)
Fluchloralin EPA 8270E_6_(6/18)
Fluoranthene EPA 8270E_6_(6/18)
Fluorene EPA 8270E_6_(6/18)
Hexachlorobenzene EPA 8270E_6_(6/18)
Hexachlorobutadiene EPA 8270E_6_(6/18)
Hexachlorocyclopentadiene EPA 8270E_6_(6/18)
Hexachloroethane EPA 8270E_6_(6/18)
Hexamethylphosphoramide (HMPA)
EPA 8270E_6_(6/18)
Hydroquinone EPA 8270E_6_(6/18)
Indeno(1,2,3-cd) pyrene EPA 8270E_6_(6/18)
Isophorone EPA 8270E_6_(6/18) m+p Cresol EPA 8270E_6_(6/18)
Mestranol EPA 8270E_6_(6/18)
Mexacarbate EPA 8270E_6_(6/18)
Mirex EPA 8270E_6_(6/18)
Naphthalene EPA 8270E_6_(6/18)
Page 29 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Solid and Chemical Materials n-Hexadecane EPA 8270E_6_(6/18)
Nicotine EPA 8270E_6_(6/18)
Nitrobenzene EPA 8270E_6_(6/18)
Nitrofen EPA 8270E_6_(6/18)
Nitroquinoline-1-oxide EPA 8270E_6_(6/18) n-Nitrosodimethylamine EPA 8270E_6_(6/18)
N-Nitroso-di-n-propylamine EPA 8270E_6_(6/18) n-Nitrosodiphenylamine EPA 8270E_6_(6/18) n-Tetradecane EPA 8270E_6_(6/18) o-Anisidine EPA 8270E_6_(6/18)
Octamethyl pyrophosphoramide EPA 8270E_6_(6/18) p-Benzoquinone EPA 8270E_6_(6/18) p-Cresidine EPA 8270E_6_(6/18)
Pentachlorophenol EPA 8270E_6_(6/18)
Phenanthrene EPA 8270E_6_(6/18)
Phenobarbital EPA 8270E_6_(6/18)
Phenol EPA 8270E_6_(6/18)
Phosalone EPA 8270E_6_(6/18)
Phosmet (Imidan)
EPA 8270E_6_(6/18)
Phosphamidon EPA 8270E_6_(6/18)
Phthalic anhydride EPA 8270E_6_(6/18)
Piperonyl sulfoxide EPA 8270E_6_(6/18)
Propylthiouracil EPA 8270E_6_(6/18)
Pyrene EPA 8270E_6_(6/18)
Pyridine EPA 8270E_6_(6/18)
Resorcinol EPA 8270E_6_(6/18)
Strychnine EPA 8270E_6_(6/18)
Sulfallate EPA 8270E_6_(6/18)
Terbufos EPA 8270E_6_(6/18)
Tetraethyl dithiopyrophosphate EPA 8270E_6_(6/18)
Thiophenol (Benzenethiol)
EPA 8270E_6_(6/18)
Toluene diisocyanate EPA 8270E_6_(6/18)
Trifluralin (Treflan)
EPA 8270E_6_(6/18)
Trimethyl phosphate EPA 8270E_6_(6/18)
Tri-p-tolyl phosphate EPA 8270E_6_(6/18) tris-(2,3-Dibromopropyl) phosphate (tris-BP)
EPA 8270E_6_(6/18) 4-Bromophenyl phenyl ether (BDE-3)
EPA 8270E_6_(6/18) SIM Page 30 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Matrix/Analyte Method Notes Edge Analytical, Incorporated Authentication Signature (1) Accreditation based in part on recognition of Oregon NELAP accreditation. (2) Accreditation based in part on recognition of EPA Region 10 certification. (3) Method not approved for NPDES testing. (4) Washington Department of Ecology Analytical Methods for Petroleum Hydrocarbons, Publication Number ECY 97-602, June 1997. (5) Approved for compliance testing only when holding time is met. (7) Method modified to determine this analyte. (8) Results for MCPP and MCPA reported from GC/MS SIM data. (9) Provisional accreditation pending submittal of additional, acceptable Proficiency Testing (PT) results (WAC 173-50-110). (10) Provisional accreditation pending completion of update to SW 846 Update V. (11) Includes SIM (13) Provisional status pending completion of update to EPA Method 624.1 (14) Provisional status pending completion of update to EPA Method 608.3 (15) Provisional status pending completion of update to EPA Method 625.1 (17) Interim accreditation pending the successful completion of an on-site audit to verify method capabilities (WAC 173-50-100). (18)
Provisional accreditation pending acceptable SOP. (19) Provisional accreditation pending submittal of acceptable SOP and IDC. (88) Interim Washington accreditation pending receipt of an updated Scope from your other recognized accreditor (Oregon NELAP). This accreditation is based in part on recognition of your currently held accreditations for previous method versions.
Accredited Parameter Note Detail Date Rebecca Wood, Lab Accreditation Unit Supervisor 01/31/2022 Page 31 of 31 Washington State Department of Ecology Effective Date: 1/19/2022 Laboratory Accreditation Unit Scope Expires: 1/18/2023 Scope of Accreditation Report for Edge Analytical, Incorporated C567-22
Anatek Labs, Inc - Moscow Moscow, ID has complied with provisions set forth in Chapter 173-50 WAC and is hereby recognized by the Department of Ecology as an ACCREDITED LABORATORY for the analytical parameters listed on the accompanying Scope of Accreditation. This certificate is effective March 21, 2022 and shall expire March 20, 2023.
Witnessed under my hand on April 22, 2022 Rebecca Wood Lab Accreditation Unit Supervisor Laboratory ID C595
is accredited for the analytes listed below using the methods indicated. Full accreditation is granted unless stated otherwise in a note. EPA is the U.S. Environmental Protection Agency. SM is "Standard Methods for the Examination of Water and Wastewater." SM refers to EPA approved method versions. ASTM is the American Society for Testing and Materials. USGS is the U.S. Geological Survey. AOAC is the Association of Official Analytical Chemists. Other references are described in notes.
Anatek Labs, Inc - Moscow Moscow, ID WASHINGTON STATE DEPARTMENT OF ECOLOGY SCOPE OF ACCREDITATION ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM Matrix/Analyte Method Notes Drinking Water Turbidity EPA 180.1_2_1993 1,8 Bromide EPA 300.0_2.1_1993 9
Fluoride EPA 300.0_2.1_1993 1,8 Nitrate EPA 300.0_2.1_1993 1,8 Nitrate + Nitrite EPA 300.0_2.1_1993 1
Nitrite EPA 300.0_2.1_1993 1,8,9 Orthophosphate EPA 300.0_2.1_1993 1
Sulfate EPA 300.0_2.1_1993 1
Perchlorate EPA 331.0_1.0_2005 1,9 Cyanide, Total EPA 335.4_1_1993 1,8 Color SM 2120 B-2011 1,9 Alkalinity SM 2320 B-2011 1
Hardness (calc.)
SM 2340 B-2011 1
Specific Conductance SM 2510 B-2011 1
Solids, Total Dissolved SM 2540 C-2011 1
Cyanide, Weak Acid Dissociable SM 4500 CN-I-2011 pH SM 4500-H+ B-2011 1,6 Nitrate SM 4500-NO3-F-2011 1,8 Nitrate + Nitrite SM 4500-NO3-F-2011 1
Nitrite SM 4500-NO3-F-2011 1,8 Total Organic Carbon SM 5310 B-2011 1,9 Anionic Surfactants (MBAS)
SM 5540 C-2011 1
Barium EPA 200.7_4.4_1994 1,8 Beryllium EPA 200.7_4.4_1994 1
Page 1 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Drinking Water Boron EPA 200.7_4.4_1994 Cadmium EPA 200.7_4.4_1994 1
Chromium EPA 200.7_4.4_1994 1,8 Copper EPA 200.7_4.4_1994 1,8 Iron EPA 200.7_4.4_1994 1
Magnesium EPA 200.7_4.4_1994 1
Manganese EPA 200.7_4.4_1994 1
Nickel EPA 200.7_4.4_1994 1,8 Potassium EPA 200.7_4.4_1994 1
Sodium EPA 200.7_4.4_1994 1,8 Zinc EPA 200.7_4.4_1994 Aluminum EPA 200.8_5.4_1994 1
Antimony EPA 200.8_5.4_1994 1,8 Arsenic EPA 200.8_5.4_1994 1,8 Barium EPA 200.8_5.4_1994 1,8 Beryllium EPA 200.8_5.4_1994 1,8 Cadmium EPA 200.8_5.4_1994 1,8 Chromium EPA 200.8_5.4_1994 1,8 Copper EPA 200.8_5.4_1994 1,8 Lead EPA 200.8_5.4_1994 1,8 Manganese EPA 200.8_5.4_1994 1
Mercury EPA 200.8_5.4_1994 1,8 Nickel EPA 200.8_5.4_1994 1,8 Selenium EPA 200.8_5.4_1994 1,8 Silver EPA 200.8_5.4_1994 1
Thallium EPA 200.8_5.4_1994 1,8 Total Uranium EPA 200.8_5.4_1994 1,8 Zinc EPA 200.8_5.4_1994 1
1,2,3-Trichloropropane EPA 504.1_1.1_1995 1
1,2-Dibromo-3-chloropropane (DBCP)
EPA 504.1_1.1_1995 1,8 1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA 504.1_1.1_1995 1,8 Aldrin EPA 505_2.1_1995 1
Aroclor-1016 (PCB-1016)
EPA 505_2.1_1995 1,8 Aroclor-1221 (PCB-1221)
EPA 505_2.1_1995 1,8 Aroclor-1232 (PCB-1232)
EPA 505_2.1_1995 1,8 Aroclor-1242 (PCB-1242)
EPA 505_2.1_1995 1,8 Page 2 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Drinking Water Aroclor-1248 (PCB-1248)
EPA 505_2.1_1995 1,8 Aroclor-1254 (PCB-1254)
EPA 505_2.1_1995 1,8 Aroclor-1260 (PCB-1260)
EPA 505_2.1_1995 1,8 Chlordane (tech.)
EPA 505_2.1_1995 1,8 Dieldrin EPA 505_2.1_1995 1
Endrin EPA 505_2.1_1995 1,8 gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 505_2.1_1995 1,8 Heptachlor EPA 505_2.1_1995 1,8 Heptachlor epoxide EPA 505_2.1_1995 1,8 Methoxychlor EPA 505_2.1_1995 1,8 Toxaphene (Chlorinated camphene)
EPA 505_2.1_1995 1,8 2,4,5-T EPA 515.4_1_2000 1
2,4-D EPA 515.4_1_2000 1,8 2,4-DB EPA 515.4_1_2000 1
3,5-Dichlorobenzoic acid EPA 515.4_1_2000 Acifluorfen EPA 515.4_1_2000 1
Bentazon EPA 515.4_1_2000 Chloramben EPA 515.4_1_2000 Dacthal Acid Metabolites EPA 515.4_1_2000 1
Dalapon EPA 515.4_1_2000 1,8 Dicamba EPA 515.4_1_2000 1
Dichloroprop (Dichlorprop)
EPA 515.4_1_2000 1
Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
EPA 515.4_1_2000 1,8 Pentachlorophenol EPA 515.4_1_2000 1,8 Picloram EPA 515.4_1_2000 1,8 Silvex (2,4,5-TP)
EPA 515.4_1_2000 1,8 3-Hydroxycarbofuran EPA 531.2_1_2001 1
Aldicarb (Temik)
EPA 531.2_1_2001 1
Aldicarb sulfone EPA 531.2_1_2001 1
Aldicarb sulfoxide EPA 531.2_1_2001 1
Carbaryl (Sevin)
EPA 531.2_1_2001 1
Carbofuran (Furaden)
EPA 531.2_1_2001 1,8 Methiocarb (Mesurol)
EPA 531.2_1_2001 1
Methomyl (Lannate)
EPA 531.2_1_2001 1
Oxamyl EPA 531.2_1_2001 1,8 Propoxur (Baygon)
EPA 531.2_1_2001 1
Glyphosate EPA 547_1990 1,8 Page 3 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Drinking Water Diquat EPA 549.2_1_1997 1,8 Bromoacetic acid (MBAA, BAA)
SM 6251 B-05 1,8 Bromochloroacetic acid (BCAA)
SM 6251 B-05 1
Chloroacetic acid (MCAA, CAA)
SM 6251 B-05 1,8 Dibromoacetic acid (DBAA)
SM 6251 B-05 1,8 Dichloroacetic acid (DCAA)
SM 6251 B-05 1,8 Total haloacetic acids (HAA5)
SM 6251 B-05 1,8 Trichloroacetic acid (TCAA)
SM 6251 B-05 1,8 1,1,1,2-Tetrachloroethane EPA 524.3_1.0_2009 1
1,1,1-Trichloroethane EPA 524.3_1.0_2009 1
1,1,2,2-Tetrachloroethane EPA 524.3_1.0_2009 1
1,1,2-Trichloroethane EPA 524.3_1.0_2009 1
1,1-Dichloroethane EPA 524.3_1.0_2009 1
1,1-Dichloroethylene EPA 524.3_1.0_2009 1
1,1-Dichloropropene EPA 524.3_1.0_2009 1
1,2,3-Trichlorobenzene EPA 524.3_1.0_2009 1
1,2,3-Trichloropropane EPA 524.3_1.0_2009 1
1,2,4-Trichlorobenzene EPA 524.3_1.0_2009 1
1,2,4-Trimethylbenzene EPA 524.3_1.0_2009 1
1,2-Dichlorobenzene EPA 524.3_1.0_2009 1
1,2-Dichloroethane (Ethylene dichloride)
EPA 524.3_1.0_2009 1
1,2-Dichloropropane EPA 524.3_1.0_2009 1
1,3,5-Trimethylbenzene EPA 524.3_1.0_2009 1
1,3-Dichlorobenzene EPA 524.3_1.0_2009 1
1,3-Dichloropropane EPA 524.3_1.0_2009 1
1,4-Dichlorobenzene EPA 524.3_1.0_2009 1
2,2-Dichloropropane EPA 524.3_1.0_2009 2-Chlorotoluene EPA 524.3_1.0_2009 1
4-Chlorotoluene EPA 524.3_1.0_2009 1
4-Isopropyltoluene (p-Cymene)
EPA 524.3_1.0_2009 1
Benzene EPA 524.3_1.0_2009 1
Bromobenzene EPA 524.3_1.0_2009 1
Bromochloromethane EPA 524.3_1.0_2009 1
Bromodichloromethane EPA 524.3_1.0_2009 1,8 Bromoform EPA 524.3_1.0_2009 1,8 Carbon disulfide EPA 524.3_1.0_2009 1
Carbon tetrachloride EPA 524.3_1.0_2009 1
Page 4 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Drinking Water Chlorobenzene EPA 524.3_1.0_2009 1
Chlorodibromomethane EPA 524.3_1.0_2009 1,8 Chloroethane (Ethyl chloride)
EPA 524.3_1.0_2009 Chloroform EPA 524.3_1.0_2009 1,8 cis-1,2-Dichloroethylene EPA 524.3_1.0_2009 1
cis-1,3-Dichloropropene EPA 524.3_1.0_2009 1
Dibromomethane EPA 524.3_1.0_2009 1
Dichlorodifluoromethane (Freon-12)
EPA 524.3_1.0_2009 1
Diethyl ether EPA 524.3_1.0_2009 1
Ethylbenzene EPA 524.3_1.0_2009 1
Hexachlorobutadiene EPA 524.3_1.0_2009 1
Iodomethane (Methyl iodide)
EPA 524.3_1.0_2009 1
Isopropylbenzene EPA 524.3_1.0_2009 1
m+p-xylene EPA 524.3_1.0_2009 1
Methyl bromide (Bromomethane)
EPA 524.3_1.0_2009 1
Methyl chloride (Chloromethane)
EPA 524.3_1.0_2009 1
Methyl tert-butyl ether (MTBE)
EPA 524.3_1.0_2009 1
Methylene chloride (Dichloromethane)
EPA 524.3_1.0_2009 1
Naphthalene EPA 524.3_1.0_2009 1
n-Butylbenzene EPA 524.3_1.0_2009 1
n-Propylbenzene EPA 524.3_1.0_2009 1
o-Xylene EPA 524.3_1.0_2009 1
sec-Butylbenzene EPA 524.3_1.0_2009 1
Styrene EPA 524.3_1.0_2009 1
tert-Butylbenzene EPA 524.3_1.0_2009 1
Tetrachloroethylene (Perchloroethylene)
EPA 524.3_1.0_2009 1
Toluene EPA 524.3_1.0_2009 1
Total Trihalomethanes EPA 524.3_1.0_2009 1,8 trans-1,2-Dichloroethylene EPA 524.3_1.0_2009 1
trans-1,3-Dichloropropylene EPA 524.3_1.0_2009 1
Trichloroethene (Trichloroethylene)
EPA 524.3_1.0_2009 1
Trichlorofluoromethane (Freon 11)
EPA 524.3_1.0_2009 1
Vinyl chloride EPA 524.3_1.0_2009 1,8 Xylene (total)
EPA 524.3_1.0_2009 1
2,4-Dinitrotoluene (2,4-DNT)
EPA 525.2_2_1995 1
2,6-Dinitrotoluene (2,6-DNT)
EPA 525.2_2_1995 1
4,4'-DDD EPA 525.2_2_1995 1
Page 5 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Drinking Water 4,4'-DDE EPA 525.2_2_1995 1
4,4'-DDT EPA 525.2_2_1995 1
Acenaphthylene EPA 525.2_2_1995 1
Acetochlor EPA 525.2_2_1995 1
Alachlor EPA 525.2_2_1995 1,8 alpha-BHC (alpha-Hexachlorocyclohexane)
EPA 525.2_2_1995 1
alpha-Chlordane EPA 525.2_2_1995 1
Anthracene EPA 525.2_2_1995 1
Atrazine EPA 525.2_2_1995 1,8 Benzo(a)anthracene EPA 525.2_2_1995 1
Benzo(a)pyrene EPA 525.2_2_1995 1
Benzo(g,h,i)perylene EPA 525.2_2_1995 1
Benzo(k)fluoranthene EPA 525.2_2_1995 1
Benzo[b]fluoranthene EPA 525.2_2_1995 1
beta-BHC (beta-Hexachlorocyclohexane)
EPA 525.2_2_1995 1
bis(2-Ethylhexyl) phthalate (DEHP)
EPA 525.2_2_1995 1,8 Bromacil EPA 525.2_2_1995 1
Butachlor EPA 525.2_2_1995 1
Butyl benzyl phthalate EPA 525.2_2_1995 1,8 Chrysene EPA 525.2_2_1995 1
Cyanazine EPA 525.2_2_1995 1
delta-BHC EPA 525.2_2_1995 1
Di(2-ethylhexyl)adipate EPA 525.2_2_1995 1,8 Diazinon EPA 525.2_2_1995 1
Dibenz(a,h) anthracene EPA 525.2_2_1995 1
Diethyl phthalate EPA 525.2_2_1995 1,8 Dimethyl phthalate EPA 525.2_2_1995 1,8 Di-n-butyl phthalate EPA 525.2_2_1995 1,8 EPTC (Eptam, s-ethyl-dipropyl thio carbamate)
EPA 525.2_2_1995 1
Fluorene EPA 525.2_2_1995 1
gamma-Chlordane EPA 525.2_2_1995 1
Hexachlorobenzene EPA 525.2_2_1995 1,8 Hexachlorocyclopentadiene EPA 525.2_2_1995 1,8 Indeno(1,2,3-cd) pyrene EPA 525.2_2_1995 1
Metolachlor EPA 525.2_2_1995 1
Metribuzin EPA 525.2_2_1995 1
Molinate EPA 525.2_2_1995 1
Page 6 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Drinking Water Phenanthrene EPA 525.2_2_1995 1
Prometon EPA 525.2_2_1995 1
Propachlor (Ramrod)
EPA 525.2_2_1995 1
Pyrene EPA 525.2_2_1995 1
Simazine EPA 525.2_2_1995 1,8 Terbacil EPA 525.2_2_1995 1
trans-Nonachlor EPA 525.2_2_1995 1
11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
EPA 533 1
1H,1H,2H,2H,-Perfluorodecanesulfonic acid (8:2 FTS)
EPA 533 1
1H,1H,2H,2H,-Perfluorooctansulfonic acid (6:2 FTS)
EPA 533 1
1H,1H,2H,2H-Perfluorohexanesulfonic acid (4:2 FTS)
EPA 533 1
4,8-Dioxa-3H-perfluorononanoic acid (ADONA)
EPA 533 1
9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
EPA 533 1
Hexafluoropropylene oxide dimer acid (HFPO-DA)
EPA 533 1
Nonafluoro-3,6-dioxaheptanoic acid (NFDHA)
EPA 533 1
Perfluoro(2-ethoxyethane)sulfonic acid (PFEESA)
EPA 533 1
Perfluoro-3-methoxypropanoic acid (PFMPA)
EPA 533 1
Perfluoro-4-methoxybutanoic acid (PFMBA)
EPA 533 1
Perfluorobutane sulfonic acid (PFBS)
EPA 533 1
Perfluorobutanoic acid (PFBA)
EPA 533 1
Perfluorodecanoic acid (PFDA)
EPA 533 1
Perfluorododecanoic acid (PFDoA)
EPA 533 1
Perfluoroheptane sulfonic acid (PFHpS)
EPA 533 1
Perfluoroheptanoic acid (PFHpA)
EPA 533 1
Perfluorohexane sulfonic acid (PFHxS)
EPA 533 1
Perfluorohexanoic acid (PFHxA)
EPA 533 1
Perfluorononanoic acid (PFNA)
EPA 533 1
Perfluorooctane sulfonic acid (PFOS)
EPA 533 1
Perfluorooctanoic acid (PFOA)
EPA 533 1
Perfluoropentane sulfonic acid (PFPeS)
EPA 533 1
Perfluoropentanoic acid (PFPeA)
EPA 533 1
Perfluoroundecanoic acid (PFUnA)
EPA 533 1
11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
EPA 537.1 revison 2 (3/20) 10 4,8-Dioxa-3H-perfluorononanoic acid (ADONA)
EPA 537.1 revison 2 (3/20) 10 9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
EPA 537.1 revison 2 (3/20) 10 Hexafluoropropylene oxide dimer acid (HFPO-DA)
EPA 537.1 revison 2 (3/20) 10 N-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
EPA 537.1 revison 2 (3/20) 10 Page 7 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Drinking Water N-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
EPA 537.1 revison 2 (3/20) 10 Perfluorobutane sulfonic acid (PFBS)
EPA 537.1 revison 2 (3/20) 10 Perfluorodecanoic acid (PFDA)
EPA 537.1 revison 2 (3/20) 10 Perfluorododecanoic acid (PFDoA)
EPA 537.1 revison 2 (3/20) 10 Perfluoroheptanoic acid (PFHpA)
EPA 537.1 revison 2 (3/20) 10 Perfluorohexane sulfonic acid (PFHxS)
EPA 537.1 revison 2 (3/20) 10 Perfluorohexanoic acid (PFHxA)
EPA 537.1 revison 2 (3/20) 10 Perfluorononanoic acid (PFNA)
EPA 537.1 revison 2 (3/20) 10 Perfluorooctane sulfonic acid (PFOS)
EPA 537.1 revison 2 (3/20) 10 Perfluorooctanoic acid (PFOA)
EPA 537.1 revison 2 (3/20) 10 Perfluorotetradecanoic acid (PFTeDA)
EPA 537.1 revison 2 (3/20) 10 Perfluorotridecanoic acid (PFTrDA)
EPA 537.1 revison 2 (3/20) 10 Perfluoroundecanoic acid (PFUnA)
EPA 537.1 revison 2 (3/20) 10 N-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
EPA 537_1.1_2009 1
N-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
EPA 537_1.1_2009 1
Perfluorobutane sulfonic acid (PFBS)
EPA 537_1.1_2009 1
Perfluorodecanoic acid (PFDA)
EPA 537_1.1_2009 1
Perfluorododecanoic acid (PFDoA)
EPA 537_1.1_2009 1
Perfluoroheptanoic acid (PFHPA)
EPA 537_1.1_2009 1
Perfluorohexane sulfonic acid (PFHxS)
EPA 537_1.1_2009 1
Perfluorohexanoic acid (PFHxA)
EPA 537_1.1_2009 1
Perfluorononanoic acid (PFNA)
EPA 537_1.1_2009 1
Perfluorooctane sulfonic acid (PFOS)
EPA 537_1.1_2009 1
Perfluorooctanoic acid (PFOA)
EPA 537_1.1_2009 1
Perfluorotetradecanoic acid (PFTeDA)
EPA 537_1.1_2009 1
Perfluorotridecanoic acid (PFTrDA)
EPA 537_1.1_2009 1
Perfluoroundecanoic acid (PFUnA)
EPA 537_1.1_2009 1
Endothall EPA 548.1_1_1992 1,8 Total coli/E.coli - detect SM 9223 B Colilert 18 (PA) 8 Non-Potable Water n-Hexane Extractable Material (O&G)
EPA 1664A_1_1999 1
n-Hexane Extractable Material (O&G)
EPA 1664B -10 (HEM) 1 Turbidity EPA 180.1_2_1993 1
Fluoride EPA 300.0_2.1_1993 1
Nitrate EPA 300.0_2.1_1993 1
Nitrate + Nitrite EPA 300.0_2.1_1993 1
Page 8 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Non-Potable Water Nitrite EPA 300.0_2.1_1993 1
Orthophosphate EPA 300.0_2.1_1993 1
Sulfate EPA 300.0_2.1_1993 1
Perchlorate EPA 331.0_1.0_2005 7
Cyanide, Total EPA 335.4_1_1993 1
Phenolics, Total EPA 420.1_1978 1
Perchlorate EPA 6850-07 1
Alkalinity SM 2320 B-2011 1
Hardness (calc.)
SM 2340 B-2011 1
Specific Conductance SM 2510 B-2011 1
Solids, Total Dissolved SM 2540 C-2011 1
Solids, Total Suspended SM 2540 D-2011 1,9 Cyanide, Weak Acid Dissociable SM 4500 CN-I-2011 Cyanides, Amenable to Chlorination SM 4500-CN-G-2011 pH SM 4500-H+ B-2011 1,6 Ammonia SM 4500-NH3 G-2011 1
Nitrate SM 4500-NO3-F-2011 1
Nitrate + Nitrite SM 4500-NO3-F-2011 1
Nitrite SM 4500-NO3-F-2011 1
Nitrogen, Total Kjeldahl SM 4500-Norg C-2011 1,9 Orthophosphate SM 4500-P F-2011 1
Phosphorus, total SM 4500-P F-2011 1
Sulfide SM 4500-S2-F-2011 9
Total Organic Carbon SM 5310 B-2011 1
Phenolics, Total SM 5530 D-2010 1
Beryllium EPA 200.7_4.4_1994 1
Page 9 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Non-Potable Water Magnesium EPA 200.7_4.4_1994 1
Manganese EPA 200.7_4.4_1994 1
Molybdenum EPA 200.7_4.4_1994 1
Beryllium EPA 200.8_5.4_1994 1
Calcium EPA 200.8_5.4_1994 Chromium EPA 200.8_5.4_1994 1
Iron EPA 200.8_5.4_1994 Lead EPA 200.8_5.4_1994 1
Magnesium EPA 200.8_5.4_1994 Manganese EPA 200.8_5.4_1994 1
Molybdenum EPA 200.8_5.4_1994 1
Potassium EPA 200.8_5.4_1994 Selenium EPA 200.8_5.4_1994 1
Sodium EPA 200.8_5.4_1994 Strontium EPA 200.8_5.4_1994 Thallium EPA 200.8_5.4_1994 1
Tin EPA 200.8_5.4_1994 Titanium EPA 200.8_5.4_1994 Total Uranium EPA 200.8_5.4_1994 1
Page 10 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Non-Potable Water Mercury EPA 245.7_2005 1
4,4'-DDD EPA 608.3 1
4,4'-DDE EPA 608.3 1
4,4'-DDT EPA 608.3 1
Aldrin EPA 608.3 1
alpha-BHC (alpha-Hexachlorocyclohexane)
EPA 608.3 1
Aroclor-1016 (PCB-1016)
EPA 608.3 1
Aroclor-1221 (PCB-1221)
EPA 608.3 1
Aroclor-1232 (PCB-1232)
EPA 608.3 1
Aroclor-1242 (PCB-1242)
EPA 608.3 1
Aroclor-1248 (PCB-1248)
EPA 608.3 1
Aroclor-1254 (PCB-1254)
EPA 608.3 1
Aroclor-1260 (PCB-1260)
EPA 608.3 1
beta-BHC (beta-Hexachlorocyclohexane)
EPA 608.3 1
Chlordane (tech.)
EPA 608.3 1
delta-BHC EPA 608.3 1
Dieldrin EPA 608.3 1
Endosulfan I EPA 608.3 1
Endosulfan II EPA 608.3 1
Endosulfan sulfate EPA 608.3 1
Endrin EPA 608.3 1
Endrin aldehyde EPA 608.3 1
Endrin ketone EPA 608.3 1
gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 608.3 1
Heptachlor EPA 608.3 1
Heptachlor epoxide EPA 608.3 1
Methoxychlor EPA 608.3 1
Toxaphene (Chlorinated camphene)
EPA 608.3 1
1,1,1,2-Tetrachloroethane EPA 624.1 1,1,1-Trichloroethane EPA 624.1 1
1,1,2,2-Tetrachloroethane EPA 624.1 1
1,1,2-Trichloroethane EPA 624.1 1
1,1-Dichloroethane EPA 624.1 1
1,1-Dichloroethylene EPA 624.1 1
1,1-Dichloropropene EPA 624.1 1
1,2,3-Trichlorobenzene EPA 624.1 1
1,2,3-Trichloropropane EPA 624.1 1
Page 11 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Non-Potable Water 1,2,4-Trimethylbenzene EPA 624.1 1
1,2-Dibromo-3-chloropropane (DBCP)
EPA 624.1 1
1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA 624.1 1
1,2-Dichlorobenzene EPA 624.1 1
1,2-Dichloroethane (Ethylene dichloride)
EPA 624.1 1
1,2-Dichloropropane EPA 624.1 1
1,3,5-Trimethylbenzene EPA 624.1 1
1,3-Dichlorobenzene EPA 624.1 1
1,3-Dichloropropane EPA 624.1 1
1,4-Dichlorobenzene EPA 624.1 1
2,2-Dichloropropane EPA 624.1 1
2-Butanone (Methyl ethyl ketone, MEK)
EPA 624.1 2-Chloroethyl vinyl ether EPA 624.1 1
2-Chlorotoluene EPA 624.1 1
2-Hexanone EPA 624.1 4-Chlorotoluene EPA 624.1 1
4-Isopropyltoluene (p-Cymene)
EPA 624.1 1
4-Methyl-2-pentanone (MIBK)
EPA 624.1 Acrolein (Propenal)
EPA 624.1 1
Acrylonitrile EPA 624.1 1
Benzene EPA 624.1 1
Bromobenzene EPA 624.1 1
Bromochloromethane EPA 624.1 1
Bromodichloromethane EPA 624.1 1
Bromoform EPA 624.1 1
Carbon disulfide EPA 624.1 Carbon tetrachloride EPA 624.1 1
Chlorobenzene EPA 624.1 1
Chlorodibromomethane EPA 624.1 1
Chloroethane (Ethyl chloride)
EPA 624.1 1
Chloroform EPA 624.1 1
cis-1,2-Dichloroethylene EPA 624.1 1
cis-1,3-Dichloropropene EPA 624.1 1
Dibromomethane EPA 624.1 1
Diethyl ether EPA 624.1 1
Ethylbenzene EPA 624.1 Iodomethane (Methyl iodide)
EPA 624.1 1
Page 12 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Non-Potable Water Isopropylbenzene EPA 624.1 1
m+p-xylene EPA 624.1 1
Methyl bromide (Bromomethane)
EPA 624.1 1
Methyl chloride (Chloromethane)
EPA 624.1 1
Methyl tert-butyl ether (MTBE)
EPA 624.1 1
Methylene chloride (Dichloromethane)
EPA 624.1 1
n-Butylbenzene EPA 624.1 1
n-Propylbenzene EPA 624.1 1
sec-Butylbenzene EPA 624.1 1
Styrene EPA 624.1 1
tert-Butylbenzene EPA 624.1 Tetrachloroethylene (Perchloroethylene)
EPA 624.1 1
Toluene EPA 624.1 1
trans-1,2-Dichloroethylene EPA 624.1 1
trans-1,3-Dichloropropylene EPA 624.1 1
trans-1,4-Dichloro-2-butene EPA 624.1 1
Trichloroethene (Trichloroethylene)
EPA 624.1 1
Trichlorofluoromethane (Freon 11)
EPA 624.1 1
Xylene (total)
EPA 624.1 1
1,2,4-Trichlorobenzene EPA 625.1 1
1,2-Dinitrobenzene EPA 625.1 1,2-Diphenylhydrazine EPA 625.1 1
1,3-Dinitrobenzene (1,3-DNB)
EPA 625.1 1-Methylnaphthalene EPA 625.1 2,3,4,6-Tetrachlorophenol EPA 625.1 1
2,3,5,6-Tetrachlorophenol EPA 625.1 2,4,5-Trichlorophenol EPA 625.1 1
2,4,6-Trichlorophenol EPA 625.1 1
2,4-Dichlorophenol EPA 625.1 1
2,4-Dimethylphenol EPA 625.1 1
2,4-Dinitrophenol EPA 625.1 1
2,4-Dinitrotoluene (2,4-DNT)
EPA 625.1 1
2,6-Dinitrotoluene (2,6-DNT)
EPA 625.1 1
2-Chloronaphthalene EPA 625.1 1
2-Chlorophenol EPA 625.1 1
2-Methylnaphthalene EPA 625.1 1
Page 13 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Non-Potable Water 2-Methylphenol (o-Cresol)
EPA 625.1 2-Nitroaniline EPA 625.1 1
2-Nitrophenol EPA 625.1 1
3,3'-Dichlorobenzidine EPA 625.1 1
3-Nitroaniline EPA 625.1 1
4,6-Dinitro-2-methylphenol EPA 625.1 1
4-Bromophenyl phenyl ether (BDE-3)
EPA 625.1 1
4-Chloro-3-methylphenol EPA 625.1 1
4-Chloroaniline EPA 625.1 1
4-Chlorophenyl phenylether EPA 625.1 1
4-Methylphenol (p-Cresol)
EPA 625.1 4-Nitroaniline EPA 625.1 1
4-Nitrophenol EPA 625.1 1
Acenaphthene EPA 625.1 1
Acenaphthylene EPA 625.1 1
Aniline EPA 625.1 Anthracene EPA 625.1 1
Benzidine EPA 625.1 1
Benzo(a)anthracene EPA 625.1 1
Benzo(a)pyrene EPA 625.1 1
Benzo(g,h,i)perylene EPA 625.1 1
Benzo(k)fluoranthene EPA 625.1 1
Benzo[b]fluoranthene EPA 625.1 1
Benzyl alcohol EPA 625.1 1
bis(2-Chloroethoxy)methane EPA 625.1 1
bis(2-Chloroethyl) ether EPA 625.1 1
bis(2-Chloroisopropyl) ether EPA 625.1 1
bis(2-Ethylhexyl) phthalate (DEHP)
EPA 625.1 1
Butyl benzyl phthalate EPA 625.1 1
Carbazole EPA 625.1 Chrysene EPA 625.1 1
Dibenz(a,h) anthracene EPA 625.1 1
Diethyl phthalate EPA 625.1 1
Dimethyl phthalate EPA 625.1 1
Di-n-butyl phthalate EPA 625.1 1
Di-n-octyl phthalate EPA 625.1 1
Fluoranthene EPA 625.1 1
Page 14 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Non-Potable Water Fluorene EPA 625.1 1
Hexachlorobenzene EPA 625.1 1
Hexachlorobutadiene EPA 625.1 1
Hexachlorocyclopentadiene EPA 625.1 1
Hexachloroethane EPA 625.1 1
Indeno(1,2,3-cd) pyrene EPA 625.1 1
Isophorone EPA 625.1 1
m+p Cresol EPA 625.1 Naphthalene EPA 625.1 1
Nitrobenzene EPA 625.1 1
N-Nitrosodimethylamine EPA 625.1 1
N-Nitroso-di-n-propylamine EPA 625.1 1
N-Nitrosodiphenylamine EPA 625.1 1
Pentachlorophenol EPA 625.1 1
Phenanthrene EPA 625.1 1
Phenol EPA 625.1 1
Pyrene EPA 625.1 1
Pyridine EPA 625.1 Fecal coliform-count SM 9221 B+E1+C (LTB/BGB/EC-MPN)
Total coliforms-count SM 9221 B+E1+C (LTB/BGB/EC-MPN)
E.coli-count SM 9221 B+F+C (LTB/BGB/EC Mug-MPN)
Total coliforms-count SM 9221 B+F+C (LTB/BGB/EC Mug-MPN)
Solid and Chemical Materials Nitrate EPA 300.0_2.1_1993 Cyanide, Total EPA 335.4_1_1993 Phenolics, Total EPA 420.1_1978 4
Cyanide, Total EPA 9012 B-04 Cyanide, Total SM 4500-CN-E-2011 Cyanides, Amenable to Chlorination SM 4500-CN-G-2011 4,9 Ammonia SM 4500-NH3 G-2011 Nitrogen, Total Kjeldahl SM 4500-Norg C-2011 Phosphorus, total SM 4500-P F-2011 Sulfide SM 4500-S2-F-2011 9
Antimony EPA 6010D_(7/14) 4,9 Barium EPA 6010D_(7/14)
Page 15 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials Cadmium EPA 6010D_(7/14)
Cobalt EPA 6010D_(7/14) 4 Copper EPA 6010D_(7/14)
Lead EPA 6010D_(7/14) 4 Magnesium EPA 6010D_(7/14)
Molybdenum EPA 6010D_(7/14)
Strontium EPA 6010D_(7/14) 4 Thallium EPA 6010D_(7/14) 4 Titanium EPA 6010D_(7/14) 4 Vanadium EPA 6010D_(7/14)
Molybdenum EPA 6020B_(7/14)
Page 16 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials Silver EPA 6020B_(7/14)
4,4'-DDD EPA 8081B_(2/07) 4,4'-DDE EPA 8081B_(2/07) 4,4'-DDT EPA 8081B_(2/07)
Alachlor EPA 8081B_(2/07)
Aldrin EPA 8081B_(2/07) alpha-BHC (alpha-Hexachlorocyclohexane)
EPA 8081B_(2/07) beta-BHC (beta-Hexachlorocyclohexane)
EPA 8081B_(2/07)
Chlordane (tech.)
EPA 8081B_(2/07)
Dacthal (DCPA)
EPA 8081B_(2/07) delta-BHC EPA 8081B_(2/07)
Diallate EPA 8081B_(2/07)
Dieldrin EPA 8081B_(2/07)
Endosulfan I EPA 8081B_(2/07)
Endosulfan II EPA 8081B_(2/07)
Endosulfan sulfate EPA 8081B_(2/07)
Endrin EPA 8081B_(2/07)
Endrin aldehyde EPA 8081B_(2/07)
Endrin ketone EPA 8081B_(2/07) gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 8081B_(2/07)
Heptachlor EPA 8081B_(2/07)
Heptachlor epoxide EPA 8081B_(2/07)
Isodrin EPA 8081B_(2/07)
Methoxychlor EPA 8081B_(2/07)
Toxaphene (Chlorinated camphene)
EPA 8081B_(2/07)
Aroclor-1016 (PCB-1016)
EPA 8082A_(2/07)
Aroclor-1221 (PCB-1221)
EPA 8082A_(2/07)
Aroclor-1232 (PCB-1232)
EPA 8082A_(2/07)
Aroclor-1242 (PCB-1242)
EPA 8082A_(2/07)
Aroclor-1248 (PCB-1248)
EPA 8082A_(2/07)
Page 17 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials Aroclor-1254 (PCB-1254)
EPA 8082A_(2/07)
Aroclor-1260 (PCB-1260)
EPA 8082A_(2/07)
Azinphos-ethyl (Ethyl guthion)
EPA 8141B_2_(2/07)
Azinphos-methyl (Guthion)
EPA 8141B_2_(2/07)
Bolstar (Sulprofos)
EPA 8141B_2_(2/07)
Carbophenothion EPA 8141B_2_(2/07)
Chlorfenvinphos EPA 8141B_2_(2/07)
Chlorpyrifos EPA 8141B_2_(2/07)
Coumaphos EPA 8141B_2_(2/07)
Demeton EPA 8141B_2_(2/07)
Demeton-o EPA 8141B_2_(2/07)
Demeton-s EPA 8141B_2_(2/07)
Diazinon EPA 8141B_2_(2/07)
Dichlorovos (DDVP, Dichlorvos)
EPA 8141B_2_(2/07)
Dimethoate EPA 8141B_2_(2/07)
Dioxathion EPA 8141B_2_(2/07)
Disulfoton EPA 8141B_2_(2/07)
EPN EPA 8141B_2_(2/07)
Ethion EPA 8141B_2_(2/07) 4 Ethoprop EPA 8141B_2_(2/07)
Famphur EPA 8141B_2_(2/07)
Fensulfothion EPA 8141B_2_(2/07)
Fenthion EPA 8141B_2_(2/07)
Hexamethylphosphoramide (HMPA)
EPA 8141B_2_(2/07)
Malathion EPA 8141B_2_(2/07)
Merphos EPA 8141B_2_(2/07)
Methyl parathion (Parathion, methyl)
EPA 8141B_2_(2/07)
Mevinphos EPA 8141B_2_(2/07)
Monocrotophos EPA 8141B_2_(2/07) 4 Naled EPA 8141B_2_(2/07)
Parathion, ethyl EPA 8141B_2_(2/07)
Phorate EPA 8141B_2_(2/07)
Phosmet (Imidan)
EPA 8141B_2_(2/07) 4 Ronnel EPA 8141B_2_(2/07)
Sulfotepp EPA 8141B_2_(2/07)
Terbufos EPA 8141B_2_(2/07)
Tetrachlorvinphos (Stirophos, Gardona)
EPA 8141B_2_(2/07)
Page 18 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials Tetraethyl pyrophosphate (TEPP)
EPA 8141B_2_(2/07)
Tokuthion (Prothiophos)
EPA 8141B_2_(2/07)
Trichloronate EPA 8141B_2_(2/07) 2,4,5-T EPA 8151A_(1/98) 2,4-D EPA 8151A_(1/98) 2,4-DB EPA 8151A_(1/98) 5-Hydroxydicamba EPA 8151A_(1/98)
Acifluorfen EPA 8151A_(1/98)
Bentazon EPA 8151A_(1/98)
Chloramben EPA 8151A_(1/98)
Dacthal (DCPA)
EPA 8151A_(1/98)
Dalapon EPA 8151A_(1/98)
DCPA di acid degradate EPA 8151A_(1/98)
Dicamba EPA 8151A_(1/98)
Dichloroprop (Dichlorprop)
EPA 8151A_(1/98)
Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
EPA 8151A_(1/98)
MCPA EPA 8151A_(1/98)
MCPP EPA 8151A_(1/98)
Pentachlorophenol EPA 8151A_(1/98)
Picloram EPA 8151A_(1/98)
Silvex (2,4,5-TP)
EPA 8151A_(1/98) 1,3,5-Trinitrobenzene (1,3,5-TNB)
EPA 8330B_(10/06) 4 1,3-Dinitrobenzene (1,3-DNB)
EPA 8330B_(10/06) 4 2,4,6-Trinitrobenzene EPA 8330B_(10/06) 4 2,4,6-Trinitrotoluene (2,4,6-TNT)
EPA 8330B_(10/06) 4 2,4-Dinitrotoluene (2,4-DNT)
EPA 8330B_(10/06) 4 2,6-Dinitrotoluene (2,6-DNT)
EPA 8330B_(10/06) 4 2-Amino-4,6-dinitrotoluene (2-am-dnt)
EPA 8330B_(10/06) 4 2-Nitrotoluene EPA 8330B_(10/06) 4 3-Nitrotoluene EPA 8330B_(10/06) 4 4-Amino-2,6-dinitrotoluene (4-am-dnt)
EPA 8330B_(10/06) 4 4-Nitrotoluene EPA 8330B_(10/06) 4 Methyl-2,4,6-trinitrophenylnitramine (tetryl)
EPA 8330B_(10/06) 4 Nitrobenzene EPA 8330B_(10/06) 4 Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX)
EPA 8330B_(10/06) 4 RDX (hexahydro-1,3,5-trinitro-1,3,5-triazine)
EPA 8330B_(10/06) 4 Tetryl (methyl-2,4,6-trinitrophenylnitramine)
EPA 8330B_(10/06) 4 Page 19 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials 1,1,1,2-Tetrachloroethane EPA 8260D_4_(6/18) 1,1,1-Trichloroethane EPA 8260D_4_(6/18) 1,1,2,2-Tetrachloroethane EPA 8260D_4_(6/18) 1,1,2-Trichloroethane EPA 8260D_4_(6/18) 1,1-Dichloroethane EPA 8260D_4_(6/18) 1,1-Dichloroethylene EPA 8260D_4_(6/18) 1,1-Dichloropropene EPA 8260D_4_(6/18) 1,2,3-Trichlorobenzene EPA 8260D_4_(6/18) 1,2,3-Trichloropropane EPA 8260D_4_(6/18) 1,2,4-Trichlorobenzene EPA 8260D_4_(6/18) 1,2,4-Trimethylbenzene EPA 8260D_4_(6/18) 1,2-Dibromo-3-chloropropane (DBCP)
EPA 8260D_4_(6/18) 1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA 8260D_4_(6/18) 1,2-Dichlorobenzene EPA 8260D_4_(6/18) 1,2-Dichloroethane (Ethylene dichloride)
EPA 8260D_4_(6/18) 1,2-Dichloropropane EPA 8260D_4_(6/18) 1,3,5-Trimethylbenzene EPA 8260D_4_(6/18) 1,3-Dichlorobenzene EPA 8260D_4_(6/18) 1,3-Dichloropropane EPA 8260D_4_(6/18) 1,4-Dichlorobenzene EPA 8260D_4_(6/18) 2,2-Dichloropropane EPA 8260D_4_(6/18) 2-Butanone (Methyl ethyl ketone, MEK)
EPA 8260D_4_(6/18) 2-Chlorotoluene EPA 8260D_4_(6/18) 2-Hexanone EPA 8260D_4_(6/18) 4-Chlorotoluene EPA 8260D_4_(6/18) 4-Isopropyltoluene (p-Cymene)
EPA 8260D_4_(6/18) 4-Methyl-2-pentanone (MIBK)
EPA 8260D_4_(6/18)
Acetone EPA 8260D_4_(6/18)
Acrylonitrile EPA 8260D_4_(6/18)
Benzene EPA 8260D_4_(6/18)
Bromobenzene EPA 8260D_4_(6/18)
Bromochloromethane EPA 8260D_4_(6/18)
Bromodichloromethane EPA 8260D_4_(6/18)
Bromoform EPA 8260D_4_(6/18)
Carbon disulfide EPA 8260D_4_(6/18)
Carbon tetrachloride EPA 8260D_4_(6/18)
Chlorobenzene EPA 8260D_4_(6/18)
Page 20 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials Chlorodibromomethane EPA 8260D_4_(6/18)
Chlorodifluoromethane (Freon-22)
EPA 8260D_4_(6/18)
Chloroethane (Ethyl chloride)
EPA 8260D_4_(6/18)
Chloroform EPA 8260D_4_(6/18) cis-1,2-Dichloroethylene EPA 8260D_4_(6/18) cis-1,3-Dichloropropene EPA 8260D_4_(6/18)
Dibromochloropropane EPA 8260D_4_(6/18)
Dibromomethane EPA 8260D_4_(6/18)
Dichlorodifluoromethane (Freon-12)
EPA 8260D_4_(6/18)
Diethyl ether EPA 8260D_4_(6/18)
Ethylbenzene EPA 8260D_4_(6/18)
Hexachlorobutadiene EPA 8260D_4_(6/18)
Iodomethane (Methyl iodide)
EPA 8260D_4_(6/18)
Iodomethane (Methyl iodide)
EPA 8260D_4_(6/18)
Isopropylbenzene EPA 8260D_4_(6/18) m+p-xylene EPA 8260D_4_(6/18)
Methyl bromide (Bromomethane)
EPA 8260D_4_(6/18)
Methyl chloride (Chloromethane)
EPA 8260D_4_(6/18)
Methyl tert-butyl ether (MTBE)
EPA 8260D_4_(6/18)
Methylene chloride (Dichloromethane)
EPA 8260D_4_(6/18)
Naphthalene EPA 8260D_4_(6/18) n-Butylbenzene EPA 8260D_4_(6/18)
Nitrobenzene EPA 8260D_4_(6/18) n-Nitroso-di-n-butylamine EPA 8260D_4_(6/18) n-Propylbenzene EPA 8260D_4_(6/18) o-Xylene EPA 8260D_4_(6/18) p-Xylene EPA 8260D_4_(6/18)
Pyridine EPA 8260D_4_(6/18) sec-Butylbenzene EPA 8260D_4_(6/18)
Styrene EPA 8260D_4_(6/18) tert-Butylbenzene EPA 8260D_4_(6/18)
Tetrachloroethylene (Perchloroethylene)
EPA 8260D_4_(6/18)
Toluene EPA 8260D_4_(6/18)
Total Trihalomethanes EPA 8260D_4_(6/18)
Total Volatile Petroleum Hydrocarbons (VPH)
EPA 8260D_4_(6/18) trans-1,2-Dichloroethylene EPA 8260D_4_(6/18) trans-1,3-Dichloropropylene EPA 8260D_4_(6/18)
Page 21 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials trans-1,4-Dichloro-2-butene EPA 8260D_4_(6/18)
Trichloroethene (Trichloroethylene)
EPA 8260D_4_(6/18)
Trichlorofluoromethane (Freon 11)
EPA 8260D_4_(6/18)
Vinyl chloride EPA 8260D_4_(6/18)
Xylene (total)
EPA 8260D_4_(6/18) 1,2,4-Trichlorobenzene EPA 8270E_6_(6/18) 1,2-Dibromo-3-chloropropane (DBCP)
EPA 8270E_6_(6/18) 1,2-Dichlorobenzene EPA 8270E_6_(6/18) 1,2-Dinitrobenzene EPA 8270E_6_(6/18) 1,2-Diphenylhydrazine EPA 8270E_6_(6/18) 1,3,5-Trinitrobenzene (1,3,5-TNB)
EPA 8270E_6_(6/18) 1,3-Dichlorobenzene EPA 8270E_6_(6/18) 1,3-Dinitrobenzene (1,3-DNB)
EPA 8270E_6_(6/18) 1,4-Dichlorobenzene EPA 8270E_6_(6/18) 1,4-Dinitrobenzene EPA 8270E_6_(6/18) 1-Methylnaphthalene EPA 8270E_6_(6/18) 2,3,4,6-Tetrachlorophenol EPA 8270E_6_(6/18) 2,3,5,6-Tetrachlorophenol EPA 8270E_6_(6/18) 2,4,5-Trichlorophenol EPA 8270E_6_(6/18) 2,4,6-Trichlorophenol EPA 8270E_6_(6/18) 2,4-Dichlorophenol EPA 8270E_6_(6/18) 2,4-Dimethylphenol EPA 8270E_6_(6/18) 2,4-Dinitrophenol EPA 8270E_6_(6/18) 2,6-Dinitrotoluene (2,6-DNT)
EPA 8270E_6_(6/18) 2-Chloronaphthalene EPA 8270E_6_(6/18) 2-Chlorophenol EPA 8270E_6_(6/18) 2-Methylnaphthalene EPA 8270E_6_(6/18) 2-Methylphenol (o-Cresol)
EPA 8270E_6_(6/18) 2-Naphthylamine EPA 8270E_6_(6/18) 2-Nitroaniline EPA 8270E_6_(6/18) 2-Nitrophenol EPA 8270E_6_(6/18) 3,3'-Dichlorobenzidine EPA 8270E_6_(6/18) 3-Nitroaniline EPA 8270E_6_(6/18) 4,6-Dinitro-2-methylphenol EPA 8270E_6_(6/18) 4-Bromophenyl phenyl ether (BDE-3)
EPA 8270E_6_(6/18) 4-Chloro-3-methylphenol EPA 8270E_6_(6/18) 4-Chloroaniline EPA 8270E_6_(6/18)
Page 22 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials 4-Chlorophenyl phenylether EPA 8270E_6_(6/18) 4-Methylphenol (p-Cresol)
EPA 8270E_6_(6/18) 4-Nitroaniline EPA 8270E_6_(6/18) 4-Nitrophenol EPA 8270E_6_(6/18)
Acenaphthene EPA 8270E_6_(6/18)
Acenaphthylene EPA 8270E_6_(6/18)
Aniline EPA 8270E_6_(6/18)
Anthracene EPA 8270E_6_(6/18)
Azinphos-methyl (Guthion)
EPA 8270E_6_(6/18) 3 Benzidine EPA 8270E_6_(6/18)
Benzo(a)anthracene EPA 8270E_6_(6/18)
Benzo(a)pyrene EPA 8270E_6_(6/18)
Benzo(g,h,i)perylene EPA 8270E_6_(6/18)
Benzo(k)fluoranthene EPA 8270E_6_(6/18)
Benzo[b]fluoranthene EPA 8270E_6_(6/18)
Benzyl alcohol EPA 8270E_6_(6/18) beta-BHC (beta-Hexachlorocyclohexane)
EPA 8270E_6_(6/18) 3 bis(2-Chloroethoxy)methane EPA 8270E_6_(6/18) bis(2-Chloroethyl) ether EPA 8270E_6_(6/18) bis(2-Chloroisopropyl) ether EPA 8270E_6_(6/18)
Butyl benzyl phthalate EPA 8270E_6_(6/18)
Carbazole EPA 8270E_6_(6/18)
Carbophenothion EPA 8270E_6_(6/18)
Chlorpyrifos EPA 8270E_6_(6/18) 3 Chrysene EPA 8270E_6_(6/18)
Coumaphos EPA 8270E_6_(6/18) 3 Demeton-s EPA 8270E_6_(6/18)
Di(2-ethylhexyl)adipate EPA 8270E_6_(6/18)
Di(2-ethylhexyl)phthalate EPA 8270E_6_(6/18)
Dibenz(a,h) anthracene EPA 8270E_6_(6/18)
Dibenzofuran EPA 8270E_6_(6/18)
Dichlorovos (DDVP, Dichlorvos)
EPA 8270E_6_(6/18) 3 Diethyl phthalate EPA 8270E_6_(6/18)
Dimethoate EPA 8270E_6_(6/18) 3 Dimethyl phthalate EPA 8270E_6_(6/18)
Di-n-butyl phthalate EPA 8270E_6_(6/18)
Di-n-octyl phthalate EPA 8270E_6_(6/18)
Page 23 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials Dioxathion EPA 8270E_6_(6/18) 3,4 Disulfoton EPA 8270E_6_(6/18) 3 EPN EPA 8270E_6_(6/18)
Famphur EPA 8270E_6_(6/18)
Fensulfothion EPA 8270E_6_(6/18) 3 Fenthion EPA 8270E_6_(6/18) 3 Fluoranthene EPA 8270E_6_(6/18)
Fluorene EPA 8270E_6_(6/18)
Hexachlorobenzene EPA 8270E_6_(6/18)
Hexachlorobutadiene EPA 8270E_6_(6/18)
Hexachlorocyclopentadiene EPA 8270E_6_(6/18)
Hexachloroethane EPA 8270E_6_(6/18)
Indeno(1,2,3-cd) pyrene EPA 8270E_6_(6/18)
Isophorone EPA 8270E_6_(6/18) m,p Cresol EPA 8270E_6_(6/18)
Malathion EPA 8270E_6_(6/18) 3 Methyl parathion (Parathion, methyl)
EPA 8270E_6_(6/18) 3 Mevinphos EPA 8270E_6_(6/18) 3 Monocrotophos EPA 8270E_6_(6/18) 3,4 Naled EPA 8270E_6_(6/18) 3 Naphthalene EPA 8270E_6_(6/18)
Nitrobenzene EPA 8270E_6_(6/18) n-Nitrosodimethylamine EPA 8270E_6_(6/18) n-Nitroso-di-n-butylamine EPA 8270E_6_(6/18)
N-Nitroso-di-n-propylamine EPA 8270E_6_(6/18) n-Nitrosodiphenylamine EPA 8270E_6_(6/18)
Parathion EPA 8270E_6_(6/18) 3 Pentachlorophenol EPA 8270E_6_(6/18)
Phenanthrene EPA 8270E_6_(6/18)
Phenol EPA 8270E_6_(6/18)
Phorate EPA 8270E_6_(6/18) 3 Phosmet (Imidan)
EPA 8270E_6_(6/18) 3,4 Pyrene EPA 8270E_6_(6/18)
Pyridine EPA 8270E_6_(6/18)
Sulfotepp EPA 8270E_6_(6/18) 3 Terbufos EPA 8270E_6_(6/18) 3 Tetrachlorvinphos (Stirophos, Gardona)
EPA 8270E_6_(6/18) 3 Page 24 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Matrix/Analyte Method Notes Anatek Labs, Inc - Moscow Solid and Chemical Materials Diesel range organics (DRO)
WDOE NWTPH-Dx_(1997) 2 Gasoline range organics (GRO)
WDOE NWTPH-Gx_(1997) 2 Authentication Signature (1) Accreditation is based in part on recognition of Florida Department of Health NELAP accreditation. (2) Analytical Methods for Petroleum Hydrocarbons, Publication No. ECY 97-602, June 1997. (3) Tributyl phosphate used for internal standard and normal 8270 surrogates used. (4) Accreditation is limited to water only. (5) Anatek Labs, Inc.
SOP for determination of methamphetamine by HPLC-MS. (6) Approved for compliance testing only when holding time is met.(7) Method not approved for NPDES testing. (8)Accreditation based in part on recognition of Idaho Department of Health and Welfare accreditation. (9) Provisional accreditation pending submittal of acceptable Proficiency Testing (PT) results (WAC 173-50-110).(10) Interim accreditation pending the successful completion of an on-site audit to verify method capabilities (WAC 173-50-100).
Accredited Parameter Note Detail Date Rebecca Wood, Lab Accreditation Unit Supervisor 07/13/2022 Page 25 of 25 Washington State Department of Ecology Effective Date: 7/13/2022 Laboratory Accreditation Unit Scope Expires: 3/20/2023 Scope of Accreditation Report for Anatek Labs, Inc - Moscow C595-22b
Pace Analytical Services, LLC - Minneapolis MN Minneapolis, MN has complied with provisions set forth in Chapter 173-50 WAC and is hereby recognized by the Department of Ecology as an ACCREDITED LABORATORY for the analytical parameters listed on the accompanying Scope of Accreditation. This certificate is effective February 19, 2022 and shall expire February 18, 2023.
Witnessed under my hand on February 16, 2022.
Rebecca Wood Lab Accreditation Unit Supervisor Laboratory ID C486
is accredited for the analytes listed below using the methods indicated. Full accreditation is granted unless stated otherwise in a note. EPA is the U.S. Environmental Protection Agency. SM is "Standard Methods for the Examination of Water and Wastewater." SM refers to EPA approved method versions. ASTM is the American Society for Testing and Materials. USGS is the U.S. Geological Survey. AOAC is the Association of Official Analytical Chemists. Other references are described in notes.
Pace Analytical Services, LLC - Minneapolis MN Minneapolis, MN WASHINGTON STATE DEPARTMENT OF ECOLOGY SCOPE OF ACCREDITATION ENVIRONMENTAL LABORATORY ACCREDITATION PROGRAM Matrix/Analyte Method Notes Air Carbon dioxide EPA 3C 1
Methane EPA 3C 1
1,2,4-Trimethylbenzene EPA TO-3 1
Benzene EPA TO-3 1
Ethane EPA TO-3 1
Ethene EPA TO-3 1
Ethylbenzene EPA TO-3 1
m+p-xylene EPA TO-3 1
Methane EPA TO-3 1
Methyl tert-butyl ether (MTBE)
EPA TO-3 1
n-Hexane EPA TO-3 1
o-Xylene EPA TO-3 1
Toluene EPA TO-3 1
Total Hydrocarbons C1-C4 EPA TO-3 1
Total Hydrocarbons C6-C10 EPA TO-3 1
Xylene (total)
EPA TO-3 1
1,1,1-Trichloroethane EPA TO-15 Rev. 2 (1999) 1 1,1,2,2-Tetrachloroethane EPA TO-15 Rev. 2 (1999) 1 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
EPA TO-15 Rev. 2 (1999) 1 1,1,2-Trichloroethane EPA TO-15 Rev. 2 (1999) 1 1,1-Dichloroethane EPA TO-15 Rev. 2 (1999) 1 1,1-Dichloroethylene EPA TO-15 Rev. 2 (1999) 1 Page 1 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Air 1,2,3-Trimethylbenzene EPA TO-15 Rev. 2 (1999) 1 1,2,4-Trichlorobenzene EPA TO-15 Rev. 2 (1999) 1 1,2,4-Trimethylbenzene EPA TO-15 Rev. 2 (1999) 1 1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA TO-15 Rev. 2 (1999) 1 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
EPA TO-15 Rev. 2 (1999) 1 1,2-Dichlorobenzene EPA TO-15 Rev. 2 (1999) 1 1,2-Dichloroethane (Ethylene dichloride)
EPA TO-15 Rev. 2 (1999) 1 1,2-Dichloropropane EPA TO-15 Rev. 2 (1999) 1 1,3,5-Trimethylbenzene EPA TO-15 Rev. 2 (1999) 1 1,3-Butadiene EPA TO-15 Rev. 2 (1999) 1 1,3-Dichlorobenzene EPA TO-15 Rev. 2 (1999) 1 1,4-Dichlorobenzene EPA TO-15 Rev. 2 (1999) 1 1,4-Dioxane (1,4-Diethyleneoxide)
EPA TO-15 Rev. 2 (1999) 1 1-Propene EPA TO-15 Rev. 2 (1999) 1 2,2,4-Trimethylpentane EPA TO-15 Rev. 2 (1999) 1 2-Butanone (Methyl ethyl ketone, MEK)
EPA TO-15 Rev. 2 (1999) 1 2-Hexanone EPA TO-15 Rev. 2 (1999) 1 4-Ethyltoluene EPA TO-15 Rev. 2 (1999) 1 4-Isopropyltoluene (p-Cymene)
EPA TO-15 Rev. 2 (1999) 1 4-Methyl-2-pentanone (MIBK)
EPA TO-15 Rev. 2 (1999) 1 Acetone EPA TO-15 Rev. 2 (1999) 1 Acrolein (Propenal)
EPA TO-15 Rev. 2 (1999) 1 Acrylonitrile EPA TO-15 Rev. 2 (1999) 1 Allyl chloride (3-Chloropropene)
EPA TO-15 Rev. 2 (1999) 1 Benzene EPA TO-15 Rev. 2 (1999) 1 Benzyl chloride EPA TO-15 Rev. 2 (1999) 1 Bromodichloromethane EPA TO-15 Rev. 2 (1999) 1 Bromoform EPA TO-15 Rev. 2 (1999) 1 Carbon disulfide EPA TO-15 Rev. 2 (1999) 1 Carbon tetrachloride EPA TO-15 Rev. 2 (1999) 1 Chlorobenzene EPA TO-15 Rev. 2 (1999) 1 Chlorodibromomethane EPA TO-15 Rev. 2 (1999) 1 Chlorodifluoromethane (Freon-22)
EPA TO-15 Rev. 2 (1999) 1 Chloroethane EPA TO-15 Rev. 2 (1999) 1 Chloroform EPA TO-15 Rev. 2 (1999) 1 cis-1,2-Dichloroethylene EPA TO-15 Rev. 2 (1999) 1 cis-1,3-Dichloropropene EPA TO-15 Rev. 2 (1999) 1 Page 2 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Air Cyclohexane EPA TO-15 Rev. 2 (1999) 1 Dichlorodifluoromethane (Freon-12)
EPA TO-15 Rev. 2 (1999) 1 Di-isopropylether (DIPE)
EPA TO-15 Rev. 2 (1999) 1 Ethanol EPA TO-15 Rev. 2 (1999) 1 Ethyl acetate EPA TO-15 Rev. 2 (1999) 1 Ethylbenzene EPA TO-15 Rev. 2 (1999) 1 Ethyl-t-butylether (ETBE)
EPA TO-15 Rev. 2 (1999) 1 Hexachlorobutadiene EPA TO-15 Rev. 2 (1999) 1 Isopropyl alcohol (2-Propanol)
EPA TO-15 Rev. 2 (1999) 1 Isopropylbenzene EPA TO-15 Rev. 2 (1999) 1 m+p-xylene EPA TO-15 Rev. 2 (1999) 1 Methyl bromide (Bromomethane)
EPA TO-15 Rev. 2 (1999) 1 Methyl chloride (Chloromethane)
EPA TO-15 Rev. 2 (1999) 1 Methyl methacrylate EPA TO-15 Rev. 2 (1999) 1 Methyl tert-butyl ether (MTBE)
EPA TO-15 Rev. 2 (1999) 1 Methylcyclohexane EPA TO-15 Rev. 2 (1999) 1 Methylene chloride (Dichloromethane)
EPA TO-15 Rev. 2 (1999) 1 Naphthalene EPA TO-15 Rev. 2 (1999) 1 n-Butylbenzene EPA TO-15 Rev. 2 (1999) 1 n-Heptane EPA TO-15 Rev. 2 (1999) 1 n-Hexane EPA TO-15 Rev. 2 (1999) 1 n-Propylbenzene EPA TO-15 Rev. 2 (1999) 1 o-Xylene EPA TO-15 Rev. 2 (1999) 1 sec-Butylbenzene EPA TO-15 Rev. 2 (1999) 1 Styrene EPA TO-15 Rev. 2 (1999) 1 tert-amylmethylether (TAME)
EPA TO-15 Rev. 2 (1999) 1 tert-Butyl alcohol EPA TO-15 Rev. 2 (1999) 1 tert-Butylbenzene EPA TO-15 Rev. 2 (1999) 1 Tetrachloroethylene (Perchloroethylene)
EPA TO-15 Rev. 2 (1999) 1 Tetrahydrofuran (THF)
EPA TO-15 Rev. 2 (1999) 1 Toluene EPA TO-15 Rev. 2 (1999) 1 Total Hydrocarbons C1-C4 EPA TO-15 Rev. 2 (1999) 1 Total Hydrocarbons C6-C10 EPA TO-15 Rev. 2 (1999) 1 trans-1,2-Dichloroethylene EPA TO-15 Rev. 2 (1999) 1 trans-1,3-Dichloropropylene EPA TO-15 Rev. 2 (1999) 1 Trichloroethene (Trichloroethylene)
EPA TO-15 Rev. 2 (1999) 1 Trichlorofluoromethane (Freon 11)
EPA TO-15 Rev. 2 (1999) 1 Page 3 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Air Vinyl acetate EPA TO-15 Rev. 2 (1999) 1 Vinyl bromide EPA TO-15 Rev. 2 (1999) 1 Vinyl chloride EPA TO-15 Rev. 2 (1999) 1 Xylene (total)
EPA TO-15 Rev. 2 (1999) 1 Drinking Water Turbidity EPA 180.1_2_1993 1
Bromide EPA 300.0_2.1_1993 1
Fluoride EPA 300.0_2.1_1993 1
Nitrate EPA 300.0_2.1_1993 1
Nitrite EPA 300.0_2.1_1993 1
Sulfate EPA 300.0_2.1_1993 1
Nitrate EPA 353.2_2_1993 1
Nitrite EPA 353.2_2_1993 1
Alkalinity SM 2320 B-2011 1
Specific Conductance SM 2510 B-2011 1
Solids, Total Dissolved SM 2540 C-2011 1
Chlorine (Residual), Total SM 4500-Cl G-2011 1
Cyanide, Total SM 4500-CN-E-2011 1
Fluoride SM 4500-F-C-2011 1
pH SM 4500-H+ B-2011 1,3 Nitrite SM 4500-NO2-B-2011 1
Beryllium EPA 200.8_5.4_1994 1
Manganese EPA 200.8_5.4_1994 1
Page 4 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Drinking Water Total Uranium EPA 200.8_5.4_1994 1
2,3,7,8-Tetrachlorodibenzo-p-dioxin (TCDD)
EPA 1613B_1994 1
11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
EPA 537.1_(11/18) 1 4,8-Dioxa-3H-perfluorononanoic acid (ADONA)
EPA 537.1_(11/18) 1 9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
EPA 537.1_(11/18) 1 Hexafluoropropylene oxide dimer acid (HFPO-DA)
EPA 537.1_(11/18) 1 N-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
EPA 537.1_(11/18) 1 N-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
EPA 537.1_(11/18) 1 Perfluorobutane sulfonate (PFBS)
EPA 537.1_(11/18) 1 Perfluorodecanoic acid (PFDA)
EPA 537.1_(11/18) 1 Perfluorododecanoic acid (PFDoA)
EPA 537.1_(11/18) 1 Perfluoroheptanoic acid (PFHpA)
EPA 537.1_(11/18) 1 Perfluorohexane sulfonate (PFHxS)
EPA 537.1_(11/18) 1 Perfluorohexanoic acid (PFHxA)
EPA 537.1_(11/18) 1 Perfluorononanoic acid (PFNA)
EPA 537.1_(11/18) 1 Perfluorooctane sulfonate (PFOS)
EPA 537.1_(11/18) 1 Perfluorooctanoic acid (PFOA)
EPA 537.1_(11/18) 1 Perfluorotetradecanoic acid (PFTeDA)
EPA 537.1_(11/18) 1 Perfluorotridecanoic acid (PFTrDA)
EPA 537.1_(11/18) 1 Perfluoroundecanoic acid (PFUnA)
EPA 537.1_(11/18) 1 Non-Potable Water Sulfate ASTM D516-11 1
Specific Conductance EPA 120.1_1982 1
Solids, Total Volatile EPA 160.4_1971 1
non-Polar Extractable Material (TPH)
EPA 1664B (SGT-HEM) 1 n-Hexane Extractable Material (O&G)
EPA 1664B -10 (HEM) 1 Turbidity EPA 180.1_2_1993 1
Bromide EPA 300.0_2.1_1993 1
Fluoride EPA 300.0_2.1_1993 1
Nitrate EPA 300.0_2.1_1993 1
Nitrite EPA 300.0_2.1_1993 1
Sulfate EPA 300.0_2.1_1993 1
Ammonia EPA 350.1_2_1993 1
Nitrate EPA 353.2_2_1993 1
Page 5 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water Nitrate + Nitrite EPA 353.2_2_1993 1
Nitrite EPA 353.2_2_1993 1
Chemical Oxygen Demand (COD)
EPA 410.4_2_1993 1
Alkalinity SM 2320 B-2011 1
Hardness (calc.)
SM 2340 B-2011 1
Specific Conductance SM 2510 B-2011 1
Solids, Total SM 2540 B-2011 1
Solids, Total Dissolved SM 2540 C-2011 1
Solids, Total Suspended SM 2540 D-2011 1
Solids, Settleable SM 2540 F-2011 1
Chromium, Hexavalent SM 3500-Cr B-2011 1
Cyanide, Total SM 4500-CN-E-2011 1
Cyanides, Amenable to Chlorination SM 4500-CN-G-2011 1
Fluoride SM 4500-F-C-2011 1
pH SM 4500-H+ B-2011 1,3 Nitrite SM 4500-NO2-B-2011 1
Nitrate + Nitrite SM 4500-NO3-H-2011 1
Phosphorus, Total SM 4500-P F-2011 1
Orthophosphate SM 4500-P G-2011 1
Chemical Oxygen Demand (COD)
SM 5220 D-2011 1
Beryllium EPA 200.7_4.4_1994 1
Magnesium EPA 200.7_4.4_1994 1
Manganese EPA 200.7_4.4_1994 1
Molybdenum EPA 200.7_4.4_1994 1
Page 6 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water Nickel EPA 200.7_4.4_1994 1
Potassium EPA 200.7_4.4_1994 1
Beryllium EPA 200.8_5.4_1994 1
Magnesium EPA 200.8_5.4_1994 1
Manganese EPA 200.8_5.4_1994 1
Molybdenum EPA 200.8_5.4_1994 1
Palladium EPA 200.8_5.4_1994 1
Potassium EPA 200.8_5.4_1994 1
Strontium EPA 200.8_5.4_1994 1
Page 7 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water Thallium EPA 200.8_5.4_1994 1
Diesel range organics (DRO)
WDOE NWTPH-Dx_(1997) 2,5 Gasoline range organics (GRO)
WDOE NWTPH-Gx_(1997) 2,5 11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
ENV-SOP-MIN4-0178 5
1H,1H,2H,2H,-Perfluorodecanesulfonic acid (8:2 FTS)
ENV-SOP-MIN4-0178 5
1H,1H,2H,2H,-Perfluorooctansulfonic acid (6:2 FTS)
ENV-SOP-MIN4-0178 5
1H,1H,2H,2H-Perfluorododecane sulfonic acid (10:2-FTS)
ENV-SOP-MIN4-0178 5
1H,1H,2H,2H-Perfluorohexanesulfonic acid (4:2 FTS)
ENV-SOP-MIN4-0178 5
4,8-Dioxa-3H-perfluorononanoic acid (ADONA)
ENV-SOP-MIN4-0178 5
9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
ENV-SOP-MIN4-0178 5
Hexafluoropropylene oxide dimer acid (HFPO-DA)
ENV-SOP-MIN4-0178 5
N-Ethylperfluorooctane sulfonamide (EtFOSA)
ENV-SOP-MIN4-0178 5
N-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
ENV-SOP-MIN4-0178 5
N-Ethylperfluorooctanesulfonamidoethanol (EtFOSE)
ENV-SOP-MIN4-0178 5
N-Methylperfluorooctane sulfonamide (MeFOSA)
ENV-SOP-MIN4-0178 5
N-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
ENV-SOP-MIN4-0178 5
N-Methylperfluorooctanesulfonamido ethanol (MeFOSE)
ENV-SOP-MIN4-0178 5
Perfluorobutane sulfonic acid (PFBS)
ENV-SOP-MIN4-0178 5
Perfluorobutanoic acid (PFBA)
ENV-SOP-MIN4-0178 5
Perfluorodecane sulfonic acid (PFDS)
ENV-SOP-MIN4-0178 5
Perfluorodecanoic acid (PFDA)
ENV-SOP-MIN4-0178 5
Perfluorododecane sulfonic acid (PFDoS)
ENV-SOP-MIN4-0178 5
Perfluorododecanoic acid (PFDoA)
ENV-SOP-MIN4-0178 5
Perfluoroheptane sulfonic acid (PFHpS)
ENV-SOP-MIN4-0178 5
Perfluoroheptanoic acid (PFHpA)
ENV-SOP-MIN4-0178 5
Perfluorohexadecanoic acid (PFHXDA)
ENV-SOP-MIN4-0178 5
Perfluorohexane sulfonic acid (PFHxS)
ENV-SOP-MIN4-0178 5
Perfluorohexanoic acid (PFHxA)
ENV-SOP-MIN4-0178 5
Perfluorononane sulfonic acid (PFNS)
ENV-SOP-MIN4-0178 5
Perfluorononanoic acid (PFNA)
ENV-SOP-MIN4-0178 5
Perfluorooctadecanoic acid (PFODA)
ENV-SOP-MIN4-0178 5
Page 8 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water Perfluorooctane sulfonamide (PFOSA)
ENV-SOP-MIN4-0178 5
Perfluorooctane sulfonic acid (PFOS)
ENV-SOP-MIN4-0178 5
Perfluorooctanoic acid (PFOA)
ENV-SOP-MIN4-0178 5
Perfluoropentane sulfonic acid (PFPeS)
ENV-SOP-MIN4-0178 5
Perfluoropentanoic acid (PFPeA)
ENV-SOP-MIN4-0178 5
Perfluorotetradecanoic acid (PFTeDA)
ENV-SOP-MIN4-0178 5
Perfluorotridecanoic acid (PFTrDA)
ENV-SOP-MIN4-0178 5
Perfluoroundecanoic acid (PFUnA)
ENV-SOP-MIN4-0178 5
1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)
EPA 1613B_1994 1
1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
EPA 1613B_1994 1
1,2,3,4,6,7,8-Hpcdd EPA 1613B_1994 1
1,2,3,4,6,7,8-Hpcdf EPA 1613B_1994 1
1,2,3,4,7,8,9-Hpcdf EPA 1613B_1994 1
1,2,3,4,7,8-Hxcdd EPA 1613B_1994 1
1,2,3,4,7,8-Hxcdf EPA 1613B_1994 1
1,2,3,6,7,8-Hxcdd EPA 1613B_1994 1
1,2,3,6,7,8-Hxcdf EPA 1613B_1994 1
1,2,3,7,8,9-Hxcdd EPA 1613B_1994 1
1,2,3,7,8,9-Hxcdf EPA 1613B_1994 1
1,2,3,7,8-Pecdd EPA 1613B_1994 1
1,2,3,7,8-Pecdf EPA 1613B_1994 1
2,3,4,6,7,8-Hxcdf EPA 1613B_1994 1
2,3,4,7,8-Pecdf EPA 1613B_1994 1
2,3,7,8-TCDD EPA 1613B_1994 1
2,3,7,8-TCDF EPA 1613B_1994 1
Hpcdd, total EPA 1613B_1994 1
Hpcdf, total EPA 1613B_1994 1
Hxcdd, total EPA 1613B_1994 1
Hxcdf, total EPA 1613B_1994 1
Pecdd, total EPA 1613B_1994 1
Pecdf, total EPA 1613B_1994 1
TCDD, total EPA 1613B_1994 1
TCDF, total EPA 1613B_1994 1
2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl (BZ-206)
EPA 1668C_2010 1
2,2',3,3',4,4',5,5'-Octachlorobiphenyl (BZ-194)
EPA 1668C_2010 1
2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl (BZ-207)
EPA 1668C_2010 1
2,2',3,3',4,4',5,6-Octachlorobiphenyl (BZ-195)
EPA 1668C_2010 1
Page 9 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water 2,2',3,3',4,4',5,6'-Octachlorobiphenyl (BZ-196)
EPA 1668C_2010 1
2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ-170)
EPA 1668C_2010 1
2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl (BZ-208)
EPA 1668C_2010 1
2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ-172)
EPA 1668C_2010 1
2,2',3,3',4,5',6,6'-Octachlorobiphenyl (BZ-201)
EPA 1668C_2010 1
2,2',3,3',4,5,6'-Heptachlorobiphenyl (BZ-174)
EPA 1668C_2010 1
2,2',3,3',4,5',6-Heptachlorobiphenyl (BZ-175)
EPA 1668C_2010 1
2,2',3,3',4,5',6'-Heptachlorobiphenyl (BZ-177)
EPA 1668C_2010 1
2,2',3,3',4,5'-Hexachlorobiphenyl (BZ-130)
EPA 1668C_2010 1
2,2',3,3',4,6,6'-Heptachlorobiphenyl (BZ-176)
EPA 1668C_2010 1
2,2',3,3',4,6-Hexachlorobiphenyl (BZ-131)
EPA 1668C_2010 1
2,2',3,3',4,6'-Hexachlorobiphenyl (BZ-132)
EPA 1668C_2010 1
2,2',3,3',4-Pentachlorobiphenyl (BZ-82)
EPA 1668C_2010 1
2,2',3,3',5,5',6,6'-Octachlorobiphenyl (BZ-202)
EPA 1668C_2010 1
2,2',3,3',5,5',6-Heptachlorobiphenyl (BZ-178)
EPA 1668C_2010 1
2,2',3,3',5,5'-Hexachlorobiphenyl (BZ-133)
EPA 1668C_2010 1
2,2',3,3',5,6,6'-Heptachlorobiphenyl (BZ-179)
EPA 1668C_2010 1
2,2',3,3',5-Pentachlorobiphenyl (BZ-83)
EPA 1668C_2010 1
2,2',3,3',6,6'-Hexachlorobiphenyl (BZ-136)
EPA 1668C_2010 1
2,2',3,3',6-Pentachlorobiphenyl (BZ-84)
EPA 1668C_2010 1
2,2',3,4,4',5,5',6-Octachlorobiphenyl (BZ-203)
EPA 1668C_2010 1
2,2',3,4,4',5,6,6'-Octachlorobiphenyl (BZ-204)
EPA 1668C_2010 1
2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ-181)
EPA 1668C_2010 1
2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ-182)
EPA 1668C_2010 1
2,2',3,4,4',5-Hexachlorobiphenyl (BZ-137)
EPA 1668C_2010 1
2,2',3,4,4',6,6'-Heptachlorobiphenyl (BZ-184)
EPA 1668C_2010 1
2,2',3,4',5,5',6-Heptachlorobiphenyl (BZ-187)
EPA 1668C_2010 1
2,2',3,4,5,5'-Hexachlorobiphenyl (BZ-141)
EPA 1668C_2010 1
2,2',3,4',5,5'-Hexachlorobiphenyl (BZ-146)
EPA 1668C_2010 1
2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ-186)
EPA 1668C_2010 1
2,2',3,4',5,6,6'-Heptachlorobiphenyl (BZ-188)
EPA 1668C_2010 1
2,2',3,4,5,6-Hexachlorobiphenyl (BZ-142)
EPA 1668C_2010 1
2,2',3,4,5',6-Hexachlorobiphenyl (BZ-144)
EPA 1668C_2010 1
2,2',3,4',5,6'-Hexachlorobiphenyl (BZ-148)
EPA 1668C_2010 1
2,2',3,4,6,6'-Hexachlorobiphenyl (BZ-145)
EPA 1668C_2010 1
2,2',3,4',6,6'-Hexachlorobiphenyl (BZ-150)
EPA 1668C_2010 1
2,2',3,4,6'-Pentachlorobiphenyl (BZ-89)
EPA 1668C_2010 1
Page 10 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water 2,2',3,4'-Tetrachlorobiphenyl (BZ-42)
EPA 1668C_2010 1
2,2',3,5,5'-Pentachlorobiphenyl (BZ-92)
EPA 1668C_2010 1
2,2',3,5,6,6'-Hexachlorobiphenyl (BZ-152)
EPA 1668C_2010 1
2,2',3,5,6'-Pentachlorobiphenyl (BZ-94)
EPA 1668C_2010 1
2,2',3,5',6-Pentachlorobiphenyl (BZ-95)
EPA 1668C_2010 1
2,2',3,6,6'-Pentachlorobiphenyl (BZ-96)
EPA 1668C_2010 1
2,2',3,6'-Tetrachlorobiphenyl (BZ-46)
EPA 1668C_2010 1
2,2',3-Trichlorobiphenyl (BZ-16)
EPA 1668C_2010 1
2,2',4,4',5,6'-Hexachlorobiphenyl (BZ-154)
EPA 1668C_2010 1
2,2',4,4',5-Pentachlorobiphenyl (BZ-99)
EPA 1668C_2010 1
2,2',4,4',6,6'-Hexachlorobiphenyl (BZ-155)
EPA 1668C_2010 1
2,2',4,5',6-Pentachlorobiphenyl (BZ-103)
EPA 1668C_2010 1
2,2',4,5-Tetrachlorobiphenyl (BZ-48)
EPA 1668C_2010 1
2,2',4,6,6'-Pentachlorobiphenyl (BZ-104)
EPA 1668C_2010 1
2,2',4-Trichlorobiphenyl (BZ-17)
EPA 1668C_2010 1
2,2',5,5'-Tetrachlorobiphenyl (BZ-52)
EPA 1668C_2010 1
2,2',6,6'-Tetrachlorobiphenyl (BZ-54)
EPA 1668C_2010 1
2,2',6-Trichlorobiphenyl (BZ-19)
EPA 1668C_2010 1
2,2'-Dichlorobiphenyl (BZ-4)
EPA 1668C_2010 1
2,3,3',4,4',5,5',6-Octachlorobiphenyl (BZ-205)
EPA 1668C_2010 1
2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ-189)
EPA 1668C_2010 1
2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ-190)
EPA 1668C_2010 1
2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ-191)
EPA 1668C_2010 1
2,3,3',4,4',6-Hexachlorobiphenyl (BZ-158)
EPA 1668C_2010 1
2,3,3',4,4'-Pentachlorobiphenyl (BZ-105)
EPA 1668C_2010 1
2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ-192)
EPA 1668C_2010 1
2,3,3',4,5,5'-Hexachlorobiphenyl (BZ-159)
EPA 1668C_2010 1
2,3,3',4',5,5'-Hexachlorobiphenyl (BZ-162)
EPA 1668C_2010 1
2,3,3',4,5,6-Hexachlorobiphenyl (BZ-160)
EPA 1668C_2010 1
2,3,3',4',5',6-Hexachlorobiphenyl (BZ-164)
EPA 1668C_2010 1
2,3,3',4,5',6-Hexachlorobiphenyl (BZ-161)
EPA 1668C_2010 1
2,3,3',4,5-Pentachlorobiphenyl (BZ-106)
EPA 1668C_2010 1
2,3,3',4',5'-Pentachlorobiphenyl (BZ-122)
EPA 1668C_2010 1
2,3,3',4,6-Pentachlorobiphenyl (BZ-109)
EPA 1668C_2010 1
2,3,3',4-Tetrachlorobiphenyl (BZ-55)
EPA 1668C_2010 1
2,3,3',4'-Tetrachlorobiphenyl (BZ-56)
EPA 1668C_2010 1
2,3,3',5,5',6-Hexachlorobiphenyl (BZ-165)
EPA 1668C_2010 1
Page 11 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water 2,3,3',5,5'-Pentachlorobiphenyl (BZ-111)
EPA 1668C_2010 1
2,3,3',5,6-Pentachlorobiphenyl (BZ-112)
EPA 1668C_2010 1
2,3,3',5-Tetrachlorobiphenyl (BZ-57)
EPA 1668C_2010 1
2,3,3',5'-Tetrachlorobiphenyl (BZ-58)
EPA 1668C_2010 1
2,3',4,4',5,5'-Hexachlorobiphenyl (BZ-167)
EPA 1668C_2010 1
2,3,4,4',5-Pentachlorobiphenyl (BZ-114)
EPA 1668C_2010 1
2,3',4,4',5-Pentachlorobiphenyl (BZ-118)
EPA 1668C_2010 1
2,3',4,4',5'-Pentachlorobiphenyl (BZ-123)
EPA 1668C_2010 1
2,3,4,4'-Tetrachlorobiphenyl (BZ-60)
EPA 1668C_2010 1
2,3',4,4'-Tetrachlorobiphenyl (BZ-66)
EPA 1668C_2010 1
2,3',4,5,5'-Pentachlorobiphenyl (BZ-120)
EPA 1668C_2010 1
2,3',4,5',6-Pentachlorobiphenyl (BZ-121)
EPA 1668C_2010 1
2,3,4',5-Tetrachlorobiphenyl (BZ-63)
EPA 1668C_2010 1
2,3',4,5'-Tetrachlorobiphenyl (BZ-68)
EPA 1668C_2010 1
2,3',4,5-Tetrachlorobiphenyl (BZ-67)
EPA 1668C_2010 1
2,3,4',6-Tetrachlorobiphenyl (BZ-64)
EPA 1668C_2010 1
2,3,4'-Trichlorobiphenyl (BZ-22)
EPA 1668C_2010 1
2,3',4-Trichlorobiphenyl (BZ-25)
EPA 1668C_2010 1
2,3',5,5'-Tetrachlorobiphenyl (BZ-72)
EPA 1668C_2010 1
2,3',5',6-Tetrachlorobiphenyl (BZ-73)
EPA 1668C_2010 1
2,3,5-Trichlorobiphenyl (BZ-23)
EPA 1668C_2010 1
2,3',5'-Trichlorobiphenyl (BZ-34)
EPA 1668C_2010 1
2,3,6-Trichlorobiphenyl (BZ-24)
EPA 1668C_2010 1
2,3',6-Trichlorobiphenyl (BZ-27)
EPA 1668C_2010 1
2,3-Dichlorobiphenyl (BZ-5)
EPA 1668C_2010 1
2,3'-Dichlorobiphenyl (BZ-6)
EPA 1668C_2010 1
2,4',5-Trichlorobiphenyl (BZ-31)
EPA 1668C_2010 1
2,4',6-Trichlorobiphenyl (BZ-32)
EPA 1668C_2010 1
2,4-Dichlorobiphenyl (BZ-7)
EPA 1668C_2010 1
2,4'-Dichlorobiphenyl (BZ-8)
EPA 1668C_2010 1
2,5-Dichlorobiphenyl (BZ-9)
EPA 1668C_2010 1
2,6-Dichlorobiphenyl (BZ-10)
EPA 1668C_2010 1
2-Chlorobiphenyl (BZ-1)
EPA 1668C_2010 1
3,3',4,4',5,5'-Hexachlorobiphenyl (BZ-169)
EPA 1668C_2010 1
3,3',4,4',5-Pentachlorobiphenyl (BZ-126)
EPA 1668C_2010 1
3,3',4,4'-Tetrachlorobiphenyl (BZ-77)
EPA 1668C_2010 1
3,3',4,5,5'-Pentachlorobiphenyl (BZ-127)
EPA 1668C_2010 1
Page 12 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water 3,3',4,5-Tetrachlorobiphenyl (BZ-78)
EPA 1668C_2010 1
3,3',4,5'-Tetrachlorobiphenyl (BZ-79)
EPA 1668C_2010 1
3,3',4-Trichlorobiphenyl (BZ-35)
EPA 1668C_2010 1
3,3',5,5'-Tetrachlorobiphenyl (BZ-80)
EPA 1668C_2010 1
3,3',5-Trichlorobiphenyl (BZ-36)
EPA 1668C_2010 1
3,3'-Dichlorobiphenyl (BZ-11)
EPA 1668C_2010 1
3,4,4',5-Tetrachlorobiphenyl (BZ-81)
EPA 1668C_2010 1
3,4,4'-Trichlorobiphenyl (BZ-37)
EPA 1668C_2010 1
3,4,5-Trichlorobiphenyl (BZ-38)
EPA 1668C_2010 1
3,4',5-Trichlorobiphenyl (BZ-39)
EPA 1668C_2010 1
3,5-Dichlorobiphenyl (BZ-14)
EPA 1668C_2010 1
3-Chlorobiphenyl (BZ-2)
EPA 1668C_2010 1
4,4'-Dichlorobiphenyl (BZ-15)
EPA 1668C_2010 1
4-Chlorobiphenyl (BZ-3)
EPA 1668C_2010 1
Coelution - Dichlorobiphenyls (BZ-12-+13)
EPA 1668C_2010 1
Coelution - Heptachlorobiphenyls (BZ-171 + BZ-173)
EPA 1668C_2010 1
Coelution - Heptachlorobiphenyls (BZ-180 + BZ-193)
EPA 1668C_2010 1
Coelution - Heptachlorobiphenyls (BZ-183 + BZ-185)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-128 + BZ-166)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-129 + BZ138 + BZ-163)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-134 + BZ-143)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-135 + BZ-151)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-139 + BZ-140)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-147 + BZ-149)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-153 + BZ-168)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-156 + BZ-157)
EPA 1668C_2010 1
Coelution - Octachlorobiphenyls (BZ-197 + BZ-200)
EPA 1668C_2010 1
Coelution - Octachlorobiphenyls (BZ-198 + BZ-199)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-107 + BZ-124)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-110 + BZ-115)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-85 + BZ-116 + BZ-117)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-88 + BZ-91)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-90 + BZ-101 + BZ-113)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-40 + BZ-41 + BZ-71)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-44 + BZ-47 + BZ-65)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-45 + BZ-51)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-49 + BZ-69)
EPA 1668C_2010 1
Page 13 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water Coelution - Tetrachlorobiphenyls (BZ-50 + BZ-53)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-59 + BZ-62 + BZ-75)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-61 + BZ-70 + BZ-74 + BZ-76)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-70 + BZ-74 + BZ-76)
EPA 1668C_2010 1
Coelution - Trichlorobiphenyls (BZ-18 + BZ-30)
EPA 1668C_2010 1
Coelution - Trichlorobiphenyls (BZ-20 + BZ-28)
EPA 1668C_2010 1
Coelution - Trichlorobiphenyls (BZ-21 + BZ-33)
EPA 1668C_2010 1
Coelution - Trichlorobiphenyls (BZ-26 + BZ-29)
EPA 1668C_2010 1
Decachlorobiphenyl (BZ-209)
EPA 1668C_2010 1
PCBs, as congeners EPA 1668C_2010 1
1,1,1-Trichloroethane EPA 624.1 1
1,1,2,2-Tetrachloroethane EPA 624.1 1
1,1,2-Trichloroethane EPA 624.1 1
1,1-Dichloroethane EPA 624.1 1
1,1-Dichloroethylene EPA 624.1 1
1,2-Dichlorobenzene EPA 624.1 1
1,2-Dichloroethane (Ethylene dichloride)
EPA 624.1 1
1,2-Dichloropropane EPA 624.1 1
1,3-Dichlorobenzene EPA 624.1 1
1,4-Dichlorobenzene EPA 624.1 1
2-Butanone (Methyl ethyl ketone, MEK)
EPA 624.1 1
4-Methyl-2-pentanone (MIBK)
EPA 624.1 1
Acetone EPA 624.1 1
Acrolein (Propenal)
EPA 624.1 1
Acrylonitrile EPA 624.1 1
Benzene EPA 624.1 1
Bromodichloromethane EPA 624.1 1
Bromoform EPA 624.1 1
Carbon tetrachloride EPA 624.1 1
Chlorobenzene EPA 624.1 1
Chlorodibromomethane EPA 624.1 1
Chloroethane (Ethyl chloride)
EPA 624.1 1
Chloroform EPA 624.1 1
cis-1,3-Dichloropropene EPA 624.1 1
Ethylbenzene EPA 624.1 1
Isopropylbenzene EPA 624.1 1
m+p-xylene EPA 624.1 1
Page 14 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water Methyl bromide (Bromomethane)
EPA 624.1 1
Methyl chloride (Chloromethane)
EPA 624.1 1
Methylene chloride (Dichloromethane)
EPA 624.1 1
o-Xylene EPA 624.1 1
Tetrachloroethylene (Perchloroethylene)
EPA 624.1 1
Tetrahydrofuran (THF)
EPA 624.1 1
Toluene EPA 624.1 1
trans-1,2-Dichloroethylene EPA 624.1 1
trans-1,3-Dichloropropylene EPA 624.1 1
Trichloroethene (Trichloroethylene)
EPA 624.1 1
Trichlorofluoromethane (Freon 11)
EPA 624.1 1
Xylene (total)
EPA 624.1 1
1,2,4-Trichlorobenzene EPA 625.1 1
2,2'-Oxybis(1-chloropropane)
EPA 625.1 1
2,4,5-Trichlorophenol EPA 625.1 1
2,4,6-Trichlorophenol EPA 625.1 1
2,4-Dichlorophenol EPA 625.1 1
2,4-Dimethylphenol EPA 625.1 1
2,4-Dinitrophenol EPA 625.1 1
2,4-Dinitrotoluene (2,4-DNT)
EPA 625.1 1
2,6-Dinitrotoluene (2,6-DNT)
EPA 625.1 1
2-Chloronaphthalene EPA 625.1 1
2-Chlorophenol EPA 625.1 1
2-Methyl-4,6-dinitrophenol EPA 625.1 1
2-Nitrophenol EPA 625.1 1
3,3'-Dichlorobenzidine EPA 625.1 1
4-Bromophenyl phenyl ether (BDE-3)
EPA 625.1 1
4-Chloro-3-methylphenol EPA 625.1 1
4-Chlorophenyl phenylether EPA 625.1 1
4-Nitrophenol EPA 625.1 1
Acenaphthene EPA 625.1 1
Acenaphthylene EPA 625.1 1
Anthracene EPA 625.1 1
Benzidine EPA 625.1 1
Benzo(a)anthracene EPA 625.1 1
Benzo(a)pyrene EPA 625.1 1
Page 15 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Non-Potable Water Benzo(g,h,i)perylene EPA 625.1 1
Benzo(k)fluoranthene EPA 625.1 1
Benzo[b]fluoranthene EPA 625.1 1
bis(2-Chloroethoxy)methane EPA 625.1 1
bis(2-Chloroethyl) ether EPA 625.1 1
Butyl benzyl phthalate EPA 625.1 1
Chrysene EPA 625.1 1
Di(2-ethylhexyl)phthalate EPA 625.1 1
Dibenz(a,h) anthracene EPA 625.1 1
Diethyl phthalate EPA 625.1 1
Dimethyl phthalate EPA 625.1 1
Di-n-butyl phthalate EPA 625.1 1
Di-n-octyl phthalate EPA 625.1 1
Fluoranthene EPA 625.1 1
Fluorene EPA 625.1 1
Hexachlorobenzene EPA 625.1 1
Hexachlorobutadiene EPA 625.1 1
Hexachlorocyclopentadiene EPA 625.1 1
Hexachloroethane EPA 625.1 1
Indeno(1,2,3-cd) pyrene EPA 625.1 1
Isophorone EPA 625.1 1
Naphthalene EPA 625.1 1
Nitrobenzene EPA 625.1 1
N-Nitrosodimethylamine EPA 625.1 1
N-Nitroso-di-n-propylamine EPA 625.1 1
N-Nitrosodiphenylamine EPA 625.1 1
Pentachlorophenol EPA 625.1 1
Phenanthrene EPA 625.1 1
Phenol EPA 625.1 1
Pyrene EPA 625.1 1
Ethane EPA RSK-175 1
Ethene EPA RSK-175 1
Methane EPA RSK-175 1
n-Propane EPA RSK-175 1
Solid and Chemical Materials pH EPA 9045D_2002 1
Bromide EPA 9056A_(02/07) 1,4 Page 16 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Chloride EPA 9056A_(02/07) 1,4 Fluoride EPA 9056A_(02/07) 1,4 Nitrate EPA 9056A_(02/07) 1 Nitrite EPA 9056A_(02/07) 1 Sulfate EPA 9056A_(02/07) 1,4 n-Hexane Extractable Material (O&G)
EPA 9071 B_2_1999 1
Paint Filter Liquids EPA 9095 B-04 1
Molybdenum EPA 6010D_2018 1
Natural uranium EPA 6010D_2018 1
Phosphorus, Total EPA 6010D_2018 1
Page 17 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Zinc EPA 6010D_2018 1
Aluminum EPA 6020B_(7/14) 1 Antimony EPA 6020B_(7/14) 1 Arsenic EPA 6020B_(7/14) 1 Barium EPA 6020B_(7/14) 1 Beryllium EPA 6020B_(7/14) 1 Bismuth EPA 6020B_(7/14) 1,4 Boron EPA 6020B_(7/14) 1 Cadmium EPA 6020B_(7/14) 1 Calcium EPA 6020B_(7/14) 1 Chromium EPA 6020B_(7/14) 1 Cobalt EPA 6020B_(7/14) 1 Copper EPA 6020B_(7/14) 1 Iron EPA 6020B_(7/14) 1 Lead EPA 6020B_(7/14) 1 Lithium EPA 6020B_(7/14) 1 Magnesium EPA 6020B_(7/14) 1 Manganese EPA 6020B_(7/14) 1 Mercury EPA 6020B_(7/14) 1 Molybdenum EPA 6020B_(7/14) 1 Nickel EPA 6020B_(7/14) 1 Palladium EPA 6020B_(7/14) 1,4 Platinum EPA 6020B_(7/14) 1 Potassium EPA 6020B_(7/14) 1 Selenium EPA 6020B_(7/14) 1 Silicon EPA 6020B_(7/14) 1 Silver EPA 6020B_(7/14) 1 Sodium EPA 6020B_(7/14) 1 Strontium EPA 6020B_(7/14) 1 Sulfur EPA 6020B_(7/14) 1 Thallium EPA 6020B_(7/14) 1 Thorium EPA 6020B_(7/14) 1 Tin EPA 6020B_(7/14) 1 Titanium EPA 6020B_(7/14) 1 Uranium EPA 6020B_(7/14) 1 Vanadium EPA 6020B_(7/14) 1 Zinc EPA 6020B_(7/14) 1 Page 18 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Mercury EPA 7470A_1_1994 1
Mercury EPA 7471B_(1/98) 1 1,2-Dibromo-3-chloropropane (DBCP)
EPA 8011-92 1,4 1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA 8011-92 1,4 Diesel range organics (DRO)
EPA 8015D_4_(6/03) 1 Gasoline range organics (GRO)
EPA 8015D_4_(6/03) 1 4,4'-DDD EPA 8081B_(2/07) 1 4,4'-DDE EPA 8081B_(2/07) 1 4,4'-DDT EPA 8081B_(2/07) 1 Aldrin EPA 8081B_(2/07) 1 alpha-BHC (alpha-Hexachlorocyclohexane)
EPA 8081B_(2/07) 1 alpha-Chlordane EPA 8081B_(2/07) 1 beta-BHC (beta-Hexachlorocyclohexane)
EPA 8081B_(2/07) 1 Chlordane (tech.)
EPA 8081B_(2/07) 1 delta-BHC EPA 8081B_(2/07) 1 Dieldrin EPA 8081B_(2/07) 1 Endosulfan I EPA 8081B_(2/07) 1 Endosulfan II EPA 8081B_(2/07) 1 Endosulfan sulfate EPA 8081B_(2/07) 1 Endrin EPA 8081B_(2/07) 1 Endrin aldehyde EPA 8081B_(2/07) 1 Endrin ketone EPA 8081B_(2/07) 1 gamma-BHC (Lindane, gamma-Hexachlorocyclohexane)
EPA 8081B_(2/07) 1 gamma-Chlordane EPA 8081B_(2/07) 1 Heptachlor EPA 8081B_(2/07) 1 Heptachlor epoxide EPA 8081B_(2/07) 1 Methoxychlor EPA 8081B_(2/07) 1 Toxaphene (Chlorinated camphene)
EPA 8081B_(2/07) 1 Aroclor-1016 (PCB-1016)
EPA 8082A_(2/07) 1 Aroclor-1221 (PCB-1221)
EPA 8082A_(2/07) 1 Aroclor-1232 (PCB-1232)
EPA 8082A_(2/07) 1 Aroclor-1242 (PCB-1242)
EPA 8082A_(2/07) 1 Aroclor-1248 (PCB-1248)
EPA 8082A_(2/07) 1 Aroclor-1254 (PCB-1254)
EPA 8082A_(2/07) 1 Aroclor-1260 (PCB-1260)
EPA 8082A_(2/07) 1 Aroclor-1262 (PCB-1262)
EPA 8082A_(2/07) 1 Aroclor-1268 (PCB-1268)
EPA 8082A_(2/07) 1 Page 19 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Diesel range organics (DRO)
WDOE NWTPH-Dx_(1997) 2,5 Motor Oil WDOE NWTPH-Dx_(1997) 2,5 Gasoline range organics (GRO)
WDOE NWTPH-Gx_(1997) 2,5 11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
ENV-SOP-MIN4-0178 5
1H,1H,2H,2H,-Perfluorodecanesulfonic acid (8:2 FTS)
ENV-SOP-MIN4-0178 5
1H,1H,2H,2H,-Perfluorooctansulfonic acid (6:2 FTS)
ENV-SOP-MIN4-0178 5
1H,1H,2H,2H-Perfluorododecane sulfonic acid (10:2-FTS)
ENV-SOP-MIN4-0178 5
1H,1H,2H,2H-Perfluorohexanesulfonic acid (4:2 FTS)
ENV-SOP-MIN4-0178 5
4,8-Dioxa-3H-perfluorononanoic acid (ADONA)
ENV-SOP-MIN4-0178 5
9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
ENV-SOP-MIN4-0178 5
Hexafluoropropylene oxide dimer acid (HFPO-DA)
ENV-SOP-MIN4-0178 5
N-Ethylperfluorooctane sulfonamide (EtFOSA)
ENV-SOP-MIN4-0178 5
N-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
ENV-SOP-MIN4-0178 5
N-Ethylperfluorooctanesulfonamidoethanol (EtFOSE)
ENV-SOP-MIN4-0178 5
N-Methylperfluorooctane sulfonamide (MeFOSA)
ENV-SOP-MIN4-0178 5
N-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
ENV-SOP-MIN4-0178 5
N-Methylperfluorooctanesulfonamido ethanol (MeFOSE)
ENV-SOP-MIN4-0178 5
Perfluorobutane sulfonic acid (PFBS)
ENV-SOP-MIN4-0178 5
Perfluorobutanoic acid (PFBA)
ENV-SOP-MIN4-0178 5
Perfluorodecane sulfonic acid (PFDS)
ENV-SOP-MIN4-0178 5
Perfluorodecanoic acid (PFDA)
ENV-SOP-MIN4-0178 5
Perfluorododecane sulfonic acid (PFDoS)
ENV-SOP-MIN4-0178 5
Perfluorododecanoic acid (PFDoA)
ENV-SOP-MIN4-0178 5
Perfluoroheptane sulfonic acid (PFHpS)
ENV-SOP-MIN4-0178 5
Perfluoroheptanoic acid (PFHpA)
ENV-SOP-MIN4-0178 5
Perfluorohexadecanoic acid (PFHXDA)
ENV-SOP-MIN4-0178 5
Perfluorohexane sulfonic acid (PFHxS)
ENV-SOP-MIN4-0178 5
Perfluorohexanoic acid (PFHxA)
ENV-SOP-MIN4-0178 5
Perfluorononane sulfonic acid (PFNS)
ENV-SOP-MIN4-0178 5
Perfluorononanoic acid (PFNA)
ENV-SOP-MIN4-0178 5
Perfluorooctadecanoic acid (PFODA)
ENV-SOP-MIN4-0178 5
Perfluorooctane sulfonamide (PFOSA)
ENV-SOP-MIN4-0178 5
Perfluorooctane sulfonic acid (PFOS)
ENV-SOP-MIN4-0178 5
Perfluorooctanoic acid (PFOA)
ENV-SOP-MIN4-0178 5
Perfluoropentane sulfonic acid (PFPeS)
ENV-SOP-MIN4-0178 5
Perfluoropentanoic acid (PFPeA)
ENV-SOP-MIN4-0178 5
Perfluorotetradecanoic acid (PFTeDA)
ENV-SOP-MIN4-0178 5
Page 20 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Perfluorotridecanoic acid (PFTrDA)
ENV-SOP-MIN4-0178 5
Perfluoroundecanoic acid (PFUnA)
ENV-SOP-MIN4-0178 5
2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl (BZ-206)
EPA 1668C_2010 1
2,2',3,3',4,4',5,5'-Octachlorobiphenyl (BZ-194)
EPA 1668C_2010 1
2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl (BZ-207)
EPA 1668C_2010 1
2,2',3,3',4,4',5,6-Octachlorobiphenyl (BZ-195)
EPA 1668C_2010 1
2,2',3,3',4,4',5,6'-Octachlorobiphenyl (BZ-196)
EPA 1668C_2010 1
2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ-170)
EPA 1668C_2010 1
2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl (BZ-208)
EPA 1668C_2010 1
2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ-172)
EPA 1668C_2010 1
2,2',3,3',4,5',6,6'-Octachlorobiphenyl (BZ-201)
EPA 1668C_2010 1
2,2',3,3',4,5,6'-Heptachlorobiphenyl (BZ-174)
EPA 1668C_2010 1
2,2',3,3',4,5',6-Heptachlorobiphenyl (BZ-175)
EPA 1668C_2010 1
2,2',3,3',4,5',6'-Heptachlorobiphenyl (BZ-177)
EPA 1668C_2010 1
2,2',3,3',4,5'-Hexachlorobiphenyl (BZ-130)
EPA 1668C_2010 1
2,2',3,3',4,6,6'-Heptachlorobiphenyl (BZ-176)
EPA 1668C_2010 1
2,2',3,3',4,6-Hexachlorobiphenyl (BZ-131)
EPA 1668C_2010 1
2,2',3,3',4,6'-Hexachlorobiphenyl (BZ-132)
EPA 1668C_2010 1
2,2',3,3',4-Pentachlorobiphenyl (BZ-82)
EPA 1668C_2010 1
2,2',3,3',5,5',6,6'-Octachlorobiphenyl (BZ-202)
EPA 1668C_2010 1
2,2',3,3',5,5',6-Heptachlorobiphenyl (BZ-178)
EPA 1668C_2010 1
2,2',3,3',5,5'-Hexachlorobiphenyl (BZ-133)
EPA 1668C_2010 1
2,2',3,3',5,6,6'-Heptachlorobiphenyl (BZ-179)
EPA 1668C_2010 1
2,2',3,3',5-Pentachlorobiphenyl (BZ-83)
EPA 1668C_2010 1
2,2',3,3',6,6'-Hexachlorobiphenyl (BZ-136)
EPA 1668C_2010 1
2,2',3,3',6-Pentachlorobiphenyl (BZ-84)
EPA 1668C_2010 1
2,2',3,4,4',5,5',6-Octachlorobiphenyl (BZ-203)
EPA 1668C_2010 1
2,2',3,4,4',5,6,6'-Octachlorobiphenyl (BZ-204)
EPA 1668C_2010 1
2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ-181)
EPA 1668C_2010 1
2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ-182)
EPA 1668C_2010 1
2,2',3,4,4',5-Hexachlorobiphenyl (BZ-137)
EPA 1668C_2010 1
2,2',3,4,4',6,6'-Heptachlorobiphenyl (BZ-184)
EPA 1668C_2010 1
2,2',3,4,5,5'-Hexachlorobiphenyl (BZ-141)
EPA 1668C_2010 1
2,2',3,4',5,5'-Hexachlorobiphenyl (BZ-146)
EPA 1668C_2010 1
2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ-186)
EPA 1668C_2010 1
2,2',3,4',5,6,6'-Heptachlorobiphenyl (BZ-188)
EPA 1668C_2010 1
2,2',3,4,5,6-Hexachlorobiphenyl (BZ-142)
EPA 1668C_2010 1
Page 21 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials 2,2',3,4,5',6-Hexachlorobiphenyl (BZ-144)
EPA 1668C_2010 1
2,2',3,4',5,6'-Hexachlorobiphenyl (BZ-148)
EPA 1668C_2010 1
2,2',3,4,6,6'-Hexachlorobiphenyl (BZ-145)
EPA 1668C_2010 1
2,2',3,4',6,6'-Hexachlorobiphenyl (BZ-150)
EPA 1668C_2010 1
2,2',3,4,6'-Pentachlorobiphenyl (BZ-89)
EPA 1668C_2010 1
2,2',3,4'-Tetrachlorobiphenyl (BZ-42)
EPA 1668C_2010 1
2,2',3,5,5'-Pentachlorobiphenyl (BZ-92)
EPA 1668C_2010 1
2,2',3,5,6,6'-Hexachlorobiphenyl (BZ-152)
EPA 1668C_2010 1
2,2',3,5,6'-Pentachlorobiphenyl (BZ-94)
EPA 1668C_2010 1
2,2',3,5',6-Pentachlorobiphenyl (BZ-95)
EPA 1668C_2010 1
2,2',3,6,6'-Pentachlorobiphenyl (BZ-96)
EPA 1668C_2010 1
2,2',3,6'-Tetrachlorobiphenyl (BZ-46)
EPA 1668C_2010 1
2,2',3-Trichlorobiphenyl (BZ-16)
EPA 1668C_2010 1
2,2',4,4',5,6'-Hexachlorobiphenyl (BZ-154)
EPA 1668C_2010 1
2,2',4,4',5-Pentachlorobiphenyl (BZ-99)
EPA 1668C_2010 1
2,2',4,4',6,6'-Hexachlorobiphenyl (BZ-155)
EPA 1668C_2010 1
2,2',4,5',6-Pentachlorobiphenyl (BZ-103)
EPA 1668C_2010 1
2,2',4,5-Tetrachlorobiphenyl (BZ-48)
EPA 1668C_2010 1
2,2',4,6,6'-Pentachlorobiphenyl (BZ-104)
EPA 1668C_2010 1
2,2',4-Trichlorobiphenyl (BZ-17)
EPA 1668C_2010 1
2,2',5,5'-Tetrachlorobiphenyl (BZ-52)
EPA 1668C_2010 1
2,2',6,6'-Tetrachlorobiphenyl (BZ-54)
EPA 1668C_2010 1
2,2',6-Trichlorobiphenyl (BZ-19)
EPA 1668C_2010 1
2,2'-Dichlorobiphenyl (BZ-4)
EPA 1668C_2010 1
2,3,3',4,4',5,5',6-Octachlorobiphenyl (BZ-205)
EPA 1668C_2010 1
2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ-189)
EPA 1668C_2010 1
2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ-190)
EPA 1668C_2010 1
2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ-191)
EPA 1668C_2010 1
2,3,3',4,4',6-Hexachlorobiphenyl (BZ-158)
EPA 1668C_2010 1
2,3,3',4,4'-Pentachlorobiphenyl (BZ-105)
EPA 1668C_2010 1
2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ-192)
EPA 1668C_2010 1
2,3,3',4,5,5'-Hexachlorobiphenyl (BZ-159)
EPA 1668C_2010 1
2,3,3',4',5,5'-Hexachlorobiphenyl (BZ-162)
EPA 1668C_2010 1
2,3,3',4,5,6-Hexachlorobiphenyl (BZ-160)
EPA 1668C_2010 1
2,3,3',4',5',6-Hexachlorobiphenyl (BZ-164)
EPA 1668C_2010 1
2,3,3',4,5',6-Hexachlorobiphenyl (BZ-161)
EPA 1668C_2010 1
2,3,3',4,5-Pentachlorobiphenyl (BZ-106)
EPA 1668C_2010 1
Page 22 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials 2,3,3',4',5'-Pentachlorobiphenyl (BZ-122)
EPA 1668C_2010 1
2,3,3',4,6-Pentachlorobiphenyl (BZ-109)
EPA 1668C_2010 1
2,3,3',4-Tetrachlorobiphenyl (BZ-55)
EPA 1668C_2010 1
2,3,3',4'-Tetrachlorobiphenyl (BZ-56)
EPA 1668C_2010 1
2,3,3',5,5',6-Hexachlorobiphenyl (BZ-165)
EPA 1668C_2010 1
2,3,3',5,5'-Pentachlorobiphenyl (BZ-111)
EPA 1668C_2010 1
2,3,3',5,6-Pentachlorobiphenyl (BZ-112)
EPA 1668C_2010 1
2,3,3',5-Tetrachlorobiphenyl (BZ-57)
EPA 1668C_2010 1
2,3,3',5'-Tetrachlorobiphenyl (BZ-58)
EPA 1668C_2010 1
2,3',4,4',5,5'-Hexachlorobiphenyl (BZ-167)
EPA 1668C_2010 1
2,3,4,4',5-Pentachlorobiphenyl (BZ-114)
EPA 1668C_2010 1
2,3',4,4',5-Pentachlorobiphenyl (BZ-118)
EPA 1668C_2010 1
2,3',4,4',5'-Pentachlorobiphenyl (BZ-123)
EPA 1668C_2010 1
2,3,4,4'-Tetrachlorobiphenyl (BZ-60)
EPA 1668C_2010 1
2,3',4,4'-Tetrachlorobiphenyl (BZ-66)
EPA 1668C_2010 1
2,3',4,5,5'-Pentachlorobiphenyl (BZ-120)
EPA 1668C_2010 1
2,3',4,5',6-Pentachlorobiphenyl (BZ-121)
EPA 1668C_2010 1
2,3,4',5-Tetrachlorobiphenyl (BZ-63)
EPA 1668C_2010 1
2,3',4,5'-Tetrachlorobiphenyl (BZ-68)
EPA 1668C_2010 1
2,3',4,5-Tetrachlorobiphenyl (BZ-67)
EPA 1668C_2010 1
2,3,4',6-Tetrachlorobiphenyl (BZ-64)
EPA 1668C_2010 1
2,3,4'-Trichlorobiphenyl (BZ-22)
EPA 1668C_2010 1
2,3',4-Trichlorobiphenyl (BZ-25)
EPA 1668C_2010 1
2,3',5,5'-Tetrachlorobiphenyl (BZ-72)
EPA 1668C_2010 1
2,3',5',6-Tetrachlorobiphenyl (BZ-73)
EPA 1668C_2010 1
2,3,5-Trichlorobiphenyl (BZ-23)
EPA 1668C_2010 1
2,3',5'-Trichlorobiphenyl (BZ-34)
EPA 1668C_2010 1
2,3,6-Trichlorobiphenyl (BZ-24)
EPA 1668C_2010 1
2,3',6-Trichlorobiphenyl (BZ-27)
EPA 1668C_2010 1
2,3-Dichlorobiphenyl (BZ-5)
EPA 1668C_2010 1
2,3'-Dichlorobiphenyl (BZ-6)
EPA 1668C_2010 1
2,4',5-Trichlorobiphenyl (BZ-31)
EPA 1668C_2010 1
2,4',6-Trichlorobiphenyl (BZ-32)
EPA 1668C_2010 1
2,4-Dichlorobiphenyl (BZ-7)
EPA 1668C_2010 1
2,4'-Dichlorobiphenyl (BZ-8)
EPA 1668C_2010 1
2,5-Dichlorobiphenyl (BZ-9)
EPA 1668C_2010 1
2,6-Dichlorobiphenyl (BZ-10)
EPA 1668C_2010 1
Page 23 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials 2-Chlorobiphenyl (BZ-1)
EPA 1668C_2010 1
3,3',4,4',5,5'-Hexachlorobiphenyl (BZ-169)
EPA 1668C_2010 1
3,3',4,4',5-Pentachlorobiphenyl (BZ-126)
EPA 1668C_2010 1
3,3',4,4'-Tetrachlorobiphenyl (BZ-77)
EPA 1668C_2010 1
3,3',4,5,5'-Pentachlorobiphenyl (BZ-127)
EPA 1668C_2010 1
3,3',4,5-Tetrachlorobiphenyl (BZ-78)
EPA 1668C_2010 1
3,3',4,5'-Tetrachlorobiphenyl (BZ-79)
EPA 1668C_2010 1
3,3',4-Trichlorobiphenyl (BZ-35)
EPA 1668C_2010 1
3,3',5,5'-Tetrachlorobiphenyl (BZ-80)
EPA 1668C_2010 1
3,3',5-Trichlorobiphenyl (BZ-36)
EPA 1668C_2010 1
3,3'-Dichlorobiphenyl (BZ-11)
EPA 1668C_2010 1
3,4,4',5-Tetrachlorobiphenyl (BZ-81)
EPA 1668C_2010 1
3,4,4'-Trichlorobiphenyl (BZ-37)
EPA 1668C_2010 1
3,4,5-Trichlorobiphenyl (BZ-38)
EPA 1668C_2010 1
3,4',5-Trichlorobiphenyl (BZ-39)
EPA 1668C_2010 1
3,5-Dichlorobiphenyl (BZ-14)
EPA 1668C_2010 1
3-Chlorobiphenyl (BZ-2)
EPA 1668C_2010 1
4,4'-Dichlorobiphenyl (BZ-15)
EPA 1668C_2010 1
4-Chlorobiphenyl (BZ-3)
EPA 1668C_2010 1
Coelution - Dichlorobiphenyls (BZ-12-+13)
EPA 1668C_2010 1
Coelution - Heptachlorobiphenyls (BZ-171 + BZ-173)
EPA 1668C_2010 1
Coelution - Heptachlorobiphenyls (BZ-180 + BZ-193)
EPA 1668C_2010 1
Coelution - Heptachlorobiphenyls (BZ-183 + BZ-185)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-128 + BZ-166)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-129 + BZ138 + BZ-163)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-134 + BZ-143)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-135 + BZ-151)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-139 + BZ-140)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-147 + BZ-149)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-153 + BZ-168)
EPA 1668C_2010 1
Coelution - Hexachlorobiphenyls (BZ-156 + BZ-157)
EPA 1668C_2010 1
Coelution - Octachlorobiphenyls (BZ-197 + BZ-200)
EPA 1668C_2010 1
Coelution - Octachlorobiphenyls (BZ-198 + BZ-199)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-107 + BZ-124)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-110 + BZ-115)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-85 + BZ-116 + BZ-117)
EPA 1668C_2010 1
Coelution - Pentachlorobiphenyls (BZ-88 + BZ-91)
EPA 1668C_2010 1
Page 24 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Coelution - Pentachlorobiphenyls (BZ-90 + BZ-101 + BZ-113)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-40 + BZ-41 + BZ-71)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-44 + BZ-47 + BZ-65)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-45 + BZ-51)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-49 + BZ-69)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-50 + BZ-53)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-59 + BZ-62 + BZ-75)
EPA 1668C_2010 1
Coelution - Tetrachlorobiphenyls (BZ-61 + BZ-70 + BZ-74 + BZ-76)
EPA 1668C_2010 1
Coelution - Trichlorobiphenyls (BZ-18 + BZ-30)
EPA 1668C_2010 1
Coelution - Trichlorobiphenyls (BZ-20 + BZ-28)
EPA 1668C_2010 1
Coelution - Trichlorobiphenyls (BZ-21 + BZ-33)
EPA 1668C_2010 1
Coelution - Trichlorobiphenyls (BZ-26 + BZ-29)
EPA 1668C_2010 1
Coelution-Hexachlorobiphenyls (BZ-129+BZ-138+BZ-160+BZ-163)
EPA 1668C_2010 1
Coelution-Pentachlorobiphenyls (BZ-93 + BZ-98 + BZ-100 + BZ-102)
EPA 1668C_2010 1
Decachlorobiphenyl (BZ-209)
EPA 1668C_2010 1
PCBs, as congeners EPA 1668C_2010 1
1,1,1,2-Tetrachloroethane EPA 8260D_4_(6/18) 1 1,1,1-Trichloroethane EPA 8260D_4_(6/18) 1 1,1,2,2-Tetrachloroethane EPA 8260D_4_(6/18) 1 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
EPA 8260D_4_(6/18) 1 1,1,2-Trichloroethane EPA 8260D_4_(6/18) 1 1,1-Dichloroethane EPA 8260D_4_(6/18) 1 1,1-Dichloroethylene EPA 8260D_4_(6/18) 1 1,1-Dichloropropene EPA 8260D_4_(6/18) 1 1,2,3-Trichlorobenzene EPA 8260D_4_(6/18) 1 1,2,3-Trichloropropane EPA 8260D_4_(6/18) 1 1,2,3-Trimethylbenzene EPA 8260D_4_(6/18) 1 1,2,4-Trichlorobenzene EPA 8260D_4_(6/18) 1 1,2,4-Trimethylbenzene EPA 8260D_4_(6/18) 1 1,2-Dibromo-3-chloropropane (DBCP)
EPA 8260D_4_(6/18) 1 1,2-Dibromoethane (EDB, Ethylene dibromide)
EPA 8260D_4_(6/18) 1 1,2-Dichlorobenzene EPA 8260D_4_(6/18) 1 1,2-Dichloroethane (Ethylene dichloride)
EPA 8260D_4_(6/18) 1 1,2-Dichloropropane EPA 8260D_4_(6/18) 1 1,3,5-Trimethylbenzene EPA 8260D_4_(6/18) 1 1,3-Dichlorobenzene EPA 8260D_4_(6/18) 1 1,3-Dichloropropane EPA 8260D_4_(6/18) 1 Page 25 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials 1,4-Dichlorobenzene EPA 8260D_4_(6/18) 1 1,4-Dioxane (1,4-Diethyleneoxide)
EPA 8260D_4_(6/18) 1 2,2-Dichloropropane EPA 8260D_4_(6/18) 1 2-Butanone (Methyl ethyl ketone, MEK)
EPA 8260D_4_(6/18) 1 2-Chloroethyl vinyl ether EPA 8260D_4_(6/18) 1 2-Chlorotoluene EPA 8260D_4_(6/18) 1 2-Hexanone EPA 8260D_4_(6/18) 1 2-Methylnaphthalene EPA 8260D_4_(6/18) 1 4-Chlorotoluene EPA 8260D_4_(6/18) 1 4-Isopropyltoluene (p-Cymene)
EPA 8260D_4_(6/18) 1 4-Methyl-2-pentanone (MIBK)
EPA 8260D_4_(6/18) 1 Acetone EPA 8260D_4_(6/18) 1 Acrolein (Propenal)
EPA 8260D_4_(6/18) 1 Acrylonitrile EPA 8260D_4_(6/18) 1 Allyl chloride (3-Chloropropene)
EPA 8260D_4_(6/18) 1 Benzene EPA 8260D_4_(6/18) 1 Bromobenzene EPA 8260D_4_(6/18) 1 Bromochloromethane EPA 8260D_4_(6/18) 1 Bromodichloromethane EPA 8260D_4_(6/18) 1 Bromoform EPA 8260D_4_(6/18) 1 Carbon disulfide EPA 8260D_4_(6/18) 1 Carbon tetrachloride EPA 8260D_4_(6/18) 1 Chlorobenzene EPA 8260D_4_(6/18) 1 Chlorodibromomethane EPA 8260D_4_(6/18) 1 Chloroethane (Ethyl chloride)
EPA 8260D_4_(6/18) 1 Chloroform EPA 8260D_4_(6/18) 1 cis & trans-1,2-Dichloroethene EPA 8260D_4_(6/18) 1 cis-1,2-Dichloroethylene EPA 8260D_4_(6/18) 1 cis-1,3-Dichloropropene EPA 8260D_4_(6/18) 1 Cyclohexane EPA 8260D_4_(6/18) 1 Dibromomethane EPA 8260D_4_(6/18) 1 Dichlorodifluoromethane (Freon-12)
EPA 8260D_4_(6/18) 1 Dichlorofluoromethane (Freon 21)
EPA 8260D_4_(6/18) 1 Diethyl ether EPA 8260D_4_(6/18) 1 Di-isopropylether (DIPE)
EPA 8260D_4_(6/18) 1 Ethylbenzene EPA 8260D_4_(6/18) 1 Hexachlorobutadiene EPA 8260D_4_(6/18) 1 Page 26 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Iodomethane (Methyl iodide)
EPA 8260D_4_(6/18) 1 Isopropylbenzene EPA 8260D_4_(6/18) 1 m+p-xylene EPA 8260D_4_(6/18) 1 Methyl bromide (Bromomethane)
EPA 8260D_4_(6/18) 1 Methyl chloride (Chloromethane)
EPA 8260D_4_(6/18) 1 Methyl tert-butyl ether (MTBE)
EPA 8260D_4_(6/18) 1 Methylene chloride (Dichloromethane)
EPA 8260D_4_(6/18) 1 Naphthalene EPA 8260D_4_(6/18) 1 n-Butylbenzene EPA 8260D_4_(6/18) 1 n-Hexane EPA 8260D_4_(6/18) 1 n-Propylbenzene EPA 8260D_4_(6/18) 1 o-Xylene EPA 8260D_4_(6/18) 1 sec-Butylbenzene EPA 8260D_4_(6/18) 1 Styrene EPA 8260D_4_(6/18) 1 tert-Butylbenzene EPA 8260D_4_(6/18) 1 Tetrachloroethylene (Perchloroethylene)
EPA 8260D_4_(6/18) 1 Tetrahydrofuran (THF)
EPA 8260D_4_(6/18) 1 Toluene EPA 8260D_4_(6/18) 1 trans-1,2-Dichloroethylene EPA 8260D_4_(6/18) 1 trans-1,3-Dichloropropylene EPA 8260D_4_(6/18) 1 trans-1,4-Dichloro-2-butene EPA 8260D_4_(6/18) 1 Trichloroethene (Trichloroethylene)
EPA 8260D_4_(6/18) 1 Trichlorofluoromethane (Freon 11)
EPA 8260D_4_(6/18) 1 Vinyl acetate EPA 8260D_4_(6/18) 1 Vinyl chloride EPA 8260D_4_(6/18) 1 Xylene (total)
EPA 8260D_4_(6/18) 1 1,2,4-Trichlorobenzene EPA 8270E_6_(6/18) 1 1,2-Dichlorobenzene EPA 8270E_6_(6/18) 1 1,2-Diphenylhydrazine EPA 8270E_6_(6/18) 1 1,3-Dichlorobenzene EPA 8270E_6_(6/18) 1 1,3-Dinitrobenzene (1,3-DNB)
EPA 8270E_6_(6/18) 1 1,4-Dichlorobenzene EPA 8270E_6_(6/18) 1 1,4-Dioxane (1,4-Diethyleneoxide)
EPA 8270E_6_(6/18) 1,4 1-Methylnaphthalene EPA 8270E_6_(6/18) 1 2,2'-Oxybis(1-chloropropane)
EPA 8270E_6_(6/18) 1 2,4,5-Trichlorophenol EPA 8270E_6_(6/18) 1 2,4,6-Trichlorophenol EPA 8270E_6_(6/18) 1 Page 27 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials 2,4-Dichlorophenol EPA 8270E_6_(6/18) 1 2,4-Dimethylphenol EPA 8270E_6_(6/18) 1 2,4-Dinitrophenol EPA 8270E_6_(6/18) 1 2,4-Dinitrotoluene (2,4-DNT)
EPA 8270E_6_(6/18) 1 2,6-Dinitrotoluene (2,6-DNT)
EPA 8270E_6_(6/18) 1 2-Chloronaphthalene EPA 8270E_6_(6/18) 1 2-Chlorophenol EPA 8270E_6_(6/18) 1 2-Methylnaphthalene EPA 8270E_6_(6/18) 1 2-Methylphenol (o-Cresol)
EPA 8270E_6_(6/18) 1 2-Nitroaniline EPA 8270E_6_(6/18) 1 2-Nitrophenol EPA 8270E_6_(6/18) 1 3,3'-Dichlorobenzidine EPA 8270E_6_(6/18) 1 3-Methylcholanthrene EPA 8270E_6_(6/18) 1 3-Methylphenol (m-Cresol)
EPA 8270E_6_(6/18) 1 3-Nitroaniline EPA 8270E_6_(6/18) 1 4,6-Dinitro-2-methylphenol EPA 8270E_6_(6/18) 1 4-Bromophenyl phenyl ether (BDE-3)
EPA 8270E_6_(6/18) 1 4-Chloro-3-methylphenol EPA 8270E_6_(6/18) 1 4-Chloroaniline EPA 8270E_6_(6/18) 1 4-Chlorophenyl phenylether EPA 8270E_6_(6/18) 1 4-Methylphenol (p-Cresol)
EPA 8270E_6_(6/18) 1 4-Nitroaniline EPA 8270E_6_(6/18) 1 4-Nitrophenol EPA 8270E_6_(6/18) 1 5-Methylchrysene EPA 8270E_6_(6/18) 1 5-Nitroacenaphthene EPA 8270E_6_(6/18) 1 6-Nitrochrysene EPA 8270E_6_(6/18) 1 7,12-Dimethylbenz(a) anthracene EPA 8270E_6_(6/18) 1 7h-Dibenzo(c, g) carbazole EPA 8270E_6_(6/18) 1 Acenaphthene EPA 8270E_6_(6/18) 1 Acenaphthylene EPA 8270E_6_(6/18) 1 Anthracene EPA 8270E_6_(6/18) 1 Benzidine EPA 8270E_6_(6/18) 1 Benzo(a)anthracene EPA 8270E_6_(6/18) 1 Benzo(a)pyrene EPA 8270E_6_(6/18) 1 Benzo(e)pyrene EPA 8270E_6_(6/18) 1 Benzo(g,h,i)perylene EPA 8270E_6_(6/18) 1 Benzo(j)fluoranthene EPA 8270E_6_(6/18) 1 Page 28 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Benzo(k)fluoranthene EPA 8270E_6_(6/18) 1 Benzo[b]fluoranthene EPA 8270E_6_(6/18) 1 Benzoic acid EPA 8270E_6_(6/18) 1 Benzyl alcohol EPA 8270E_6_(6/18) 1 bis(2-Chloroethoxy)methane EPA 8270E_6_(6/18) 1 bis(2-Chloroethyl) ether EPA 8270E_6_(6/18) 1 bis(2-Chloroisopropyl) ether EPA 8270E_6_(6/18) 1 Butyl benzyl phthalate EPA 8270E_6_(6/18) 1 Carbazole EPA 8270E_6_(6/18) 1 Chrysene EPA 8270E_6_(6/18) 1 Di(2-ethylhexyl)phthalate EPA 8270E_6_(6/18) 1 Dibenz(a,h) acridine EPA 8270E_6_(6/18) 1 Dibenz(a,h) anthracene EPA 8270E_6_(6/18) 1 Dibenz(a,j) acridine EPA 8270E_6_(6/18) 1 Dibenzo(a,e) pyrene EPA 8270E_6_(6/18) 1 Dibenzo(a,h) pyrene EPA 8270E_6_(6/18) 1 Dibenzo(a,i) pyrene EPA 8270E_6_(6/18) 1 Dibenzo(a,l)pyrene EPA 8270E_6_(6/18) 1 Dibenzofuran EPA 8270E_6_(6/18) 1 Diethyl phthalate EPA 8270E_6_(6/18) 1 Dimethyl phthalate EPA 8270E_6_(6/18) 1 Di-n-butyl phthalate EPA 8270E_6_(6/18) 1 Di-n-octyl phthalate EPA 8270E_6_(6/18) 1 Fluoranthene EPA 8270E_6_(6/18) 1 Fluorene EPA 8270E_6_(6/18) 1 Hexachlorobenzene EPA 8270E_6_(6/18) 1 Hexachlorobutadiene EPA 8270E_6_(6/18) 1 Hexachlorocyclopentadiene EPA 8270E_6_(6/18) 1 Hexachloroethane EPA 8270E_6_(6/18) 1 Indeno(1,2,3-cd) pyrene EPA 8270E_6_(6/18) 1 Isophorone EPA 8270E_6_(6/18) 1 m+p Cresol EPA 8270E_6_(6/18) 1 Naphthalene EPA 8270E_6_(6/18) 1 Nitrobenzene EPA 8270E_6_(6/18) 1 n-Nitrosodimethylamine EPA 8270E_6_(6/18) 1 N-Nitroso-di-n-propylamine EPA 8270E_6_(6/18) 1 n-Nitrosodiphenylamine EPA 8270E_6_(6/18) 1 Page 29 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials Pentachlorophenol EPA 8270E_6_(6/18) 1 Perylene EPA 8270E_6_(6/18) 1 Phenanthrene EPA 8270E_6_(6/18) 1 Phenol EPA 8270E_6_(6/18) 1 Pyrene EPA 8270E_6_(6/18) 1 Pyridine EPA 8270E_6_(6/18) 1 Quinoline EPA 8270E_6_(6/18) 1 1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)
EPA 8280B_2_(2/07) 1 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
EPA 8280B_2_(2/07) 1 1,2,3,4,6,7,8-Hpcdd EPA 8280B_2_(2/07) 1 1,2,3,4,6,7,8-Hpcdf EPA 8280B_2_(2/07) 1 1,2,3,4,7,8,9-Hpcdf EPA 8280B_2_(2/07) 1 1,2,3,4,7,8-Hxcdd EPA 8280B_2_(2/07) 1 1,2,3,4,7,8-Hxcdf EPA 8280B_2_(2/07) 1 1,2,3,6,7,8-Hxcdd EPA 8280B_2_(2/07) 1 1,2,3,6,7,8-Hxcdf EPA 8280B_2_(2/07) 1 1,2,3,7,8,9-Hxcdd EPA 8280B_2_(2/07) 1 1,2,3,7,8,9-Hxcdf EPA 8280B_2_(2/07) 1 1,2,3,7,8-Pecdd EPA 8280B_2_(2/07) 1 1,2,3,7,8-Pecdf EPA 8280B_2_(2/07) 1 2,3,4,6,7,8-Hxcdf EPA 8280B_2_(2/07) 1 2,3,4,7,8-Pecdf EPA 8280B_2_(2/07) 1 2,3,7,8-TCDD EPA 8280B_2_(2/07) 1 2,3,7,8-TCDF EPA 8280B_2_(2/07) 1 Hpcdd, total EPA 8280B_2_(2/07) 1 Hpcdf, total EPA 8280B_2_(2/07) 1 Hxcdd, total EPA 8280B_2_(2/07) 1 Hxcdf, total EPA 8280B_2_(2/07) 1 Pecdd, total EPA 8280B_2_(2/07) 1 Pecdf, total EPA 8280B_2_(2/07) 1 TCDD, total EPA 8280B_2_(2/07) 1 TCDF, total EPA 8280B_2_(2/07) 1 1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)
EPA 8290A_1_(2/07) 1 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)
EPA 8290A_1_(2/07) 1 1,2,3,4,6,7,8-Hpcdd EPA 8290A_1_(2/07) 1 1,2,3,4,6,7,8-Hpcdf EPA 8290A_1_(2/07) 1 1,2,3,4,7,8,9-Hpcdf EPA 8290A_1_(2/07) 1 Page 30 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a
Matrix/Analyte Method Notes Pace Analytical Services, LLC - Minneapolis MN Solid and Chemical Materials 1,2,3,4,7,8-Hxcdd EPA 8290A_1_(2/07) 1 1,2,3,4,7,8-Hxcdf EPA 8290A_1_(2/07) 1 1,2,3,6,7,8-Hxcdd EPA 8290A_1_(2/07) 1 1,2,3,6,7,8-Hxcdf EPA 8290A_1_(2/07) 1 1,2,3,7,8,9-Hxcdd EPA 8290A_1_(2/07) 1 1,2,3,7,8,9-Hxcdf EPA 8290A_1_(2/07) 1 1,2,3,7,8-Pecdd EPA 8290A_1_(2/07) 1 1,2,3,7,8-Pecdf EPA 8290A_1_(2/07) 1 2,3,4,6,7,8-Hxcdf EPA 8290A_1_(2/07) 1 2,3,4,7,8-Pecdf EPA 8290A_1_(2/07) 1 2,3,7,8-TCDD EPA 8290A_1_(2/07) 1 2,3,7,8-TCDF EPA 8290A_1_(2/07) 1 Hpcdd, total EPA 8290A_1_(2/07) 1 Hpcdf, total EPA 8290A_1_(2/07) 1 Hxcdd, total EPA 8290A_1_(2/07) 1 Hxcdf, total EPA 8290A_1_(2/07) 1 Pecdd, total EPA 8290A_1_(2/07) 1 Pecdf, total EPA 8290A_1_(2/07) 1 TCDD, total EPA 8290A_1_(2/07) 1 TCDF, total EPA 8290A_1_(2/07) 1 Authentication Signature (1) Accreditation based in part on recognition of Minnesota NELAP accreditation. (2) Washington Department of Ecology Analytical Methods for Petroleum Hydrocarbons, Publication Number ECY 97-602, June 1997. (3)
Approved for compliance testing only when holding time is met. (4) Accreditation limited to water. (5) Accreditation based in part on recognition of Oregon NELAP accreditation.
Accredited Parameter Note Detail Date Rebecca Wood, Lab Accreditation Unit Supervisor 06/10/2022 Page 31 of 31 Washington State Department of Ecology Effective Date: 6/10/2022 Laboratory Accreditation Unit Scope Expires: 2/18/2023 Scope of Accreditation Report for Pace Analytical Services, LLC - Minneapolis MN C486-22a