ML20237L246

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Advises That NRC Attendance Not Necessary at 860709 Meeting Since NRC Met W/Kirner on 860625 to Discuss Asphalt Issue. Agreement That Backfilling Would Be Acceptable Approach for Providing Stability for Waste Reached
ML20237L246
Person / Time
Issue date: 06/25/1986
From: Johnson T
NRC OFFICE OF NUCLEAR MATERIAL SAFETY & SAFEGUARDS (NMSS)
To: Day J
ASSOCIATED TECHNOLOGIES, INC.
Shared Package
ML20237L079 List:
References
REF-WM-91 NUDOCS 8709080305
Download: ML20237L246 (57)


Text

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/[ ge,a ucy*'o, UNITED STATES

~j NUCLEAR REGULATORY COMMISSION O PAa

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JUN 2 5 1985 Mr. J. E. Day Assor eted Technologies, Inc.

d Suite 300, 212 South Tryon Street Charlotte, NC 28281

Dear Mr,

. Day:

Thank you very much for your invitation to attend the July 9,1986 meeting between your organization and the State of Washington. As you know we met with Ms. Kirner from the State of Washington on June 25, 1986 to discuss the asphalt issue.

In this meeting we reviewed the draft backfill evaluation the NRC had previously prepared. 'We'also reached a basic agreement'that'

.backfilling would be'an' acceptable approach for providing stability for asphalt wastes. As a result of our discussion and agreements, I do not consider it necessary for me to meet with you in Olympia.

If you have any questions, please contact me at 301-427-4088.

Sincerely, 4///

mothy son

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Engineering Branch Division of Waste Management Office of Nuclear Material Safety and Safeguards 1

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k 9709080305 870019 PDR WASTE PDR WM-91 l

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S200 Semenvte hood, Sune 300

- l P.o. Som 7216 Lassvee. Komucay 40207 602 426 7160 l

USEcology en Amencen Econogy company November 19, 1986 Mr. Earl Ingersol Radiation Control Section DSES, Health Services Division Mail Stop LF-13 Olympia, Washington 98504

Dear Mr. Ingersol:

Per discussion with Mr. Ed Day of Associated Technology Inc. (ATI) and as a follow-up to his discussion with you concerning the disposal of Class B and C stabilized bitumen waste at our Richland facility, we have draf ted this letter.

By this letter,. US Ecology is commi tting to following the administration procedures f or the : disposal of bitumen waste recommended in -

the NRC's. Draf t paper titled ' Staff Recommendations' on Soil Backfill for LLW Land Disposal Excavations,' except as hereaf ter modified with respect to the 12% limitation on fines.

As you know, this paper is in draft form and one comment that we have submitted to the NRC deals with the maximum 12% fines (passing a 200 sieve) that they specify for backfill material.

The soils at the Richland facility can be described as unconsolidated sands and silts through the depths normally excavated for the disposal units.

Samples taken from a typical trench have been f ound to be sandy soils in layers consisting of fine sand, coarse sand, and fine sand, progressing.from the surface downward to the trench flocr.

Tne percent of material p'assing a 200 sieve ranges from 4 to 20%.-

'Because of the arid conditions at the site, limiting the percentage of fines to 12% should not be required as long as the soile are dry, f ree flowing and noncohesive.

We had discussed this with the Imc and they have agreec.

We wanted to bring this issue to your attention because in our commitment to follow the Draf t recommendations, we will be utilizing only site soils for backfilling, and do not feel that any separation of backfill material is warranted.

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Mr. Earl Ingersol November 19, 1986 Page 2 We hope that thi s commitment to utilize administrative controls for the disposal of Class B and c bitumen solidified wastes will satisfy the states requirements in their approval of this waste form.

If you have any questions please contact us.

Sincerely,

' N(

Richard E. Sauer Manager, Engineering RES:cch cc:

Ed Day, ATI Nancy Kirner, DSHS l

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q.m ot u wwaos DEPARTMENT Of SOCIAL AND HLALTH SERVICES on mou n.ahe c o, w n e d l

December 11,.1986 1

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l Sic V. Wright, Jr.

Vice President Radiological Division US Ecology, Inc.

9200 Shelbyville Road, Suite 526 P.O. box 7246 Louisville, Kentucky 40207 1

Dear Mr. Wright; This is in response to Richard E. Sauer's letter cated hovember 19, 1986 relevant to the acceptance and disposal of Class B and C waste, stabilized i

j with citumen.

In oroer to fully achieve the stability requirements for J

Class B anc C wastes as outlined in Title 10 CFR 61 anc,'since the NRC branch Technical Pc.

ion Paper dated May 11,.1983 coes not provice com-plete guidance for bitumenous waste forms, administrative controls must l

1 be relied upon.

Interim approval is granted for the. acceptance and disposal of wastes stabili2eo with bitumen, provioed that the bitumen _ stabilized wastes are processed in accordance with a prescribed Quality Assurance procedure

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that results in a free l standing monolith. ' Additionally, these: wastes. must be. disposed of-and' backfilled according tolthe-procedur-es recommended in the NRC oraf t paper titled."NRC Staff Recommendations on Soil Backfill for LLW Lano: Disposal Excavations" and procedures submitted by US Ecology, Inc. in correspondence cated November 19, 1986.

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i 51d V. Wright, Jr.

December 11, 1986 Page 2 All shipments must conform in all other respects to the requirements and regulations of DDT, NRC, state of Washington as well as US Ecology, Inc.'s license conditions.

If you should have any questions, do not hesitate to contact this office.

Sincerely, b,5*.)

Clacete.e'E. Ingersoll, Acting Head I

Waste Management Section Office of Radiation Protection Mail Stop LE-13 (206) 753-3353 0/Yfg/

l Mikel J. Eisen Radiation Health Physicist (206) 753-1116 CEI:MJE:pm cc:

Bob Biostrup - DSHS, Site Inspector US Ecology, Inc. - Ricnlanc, WA David N. Enegess - Weste Cnem Z E. Day - ATI Donald Nusseaumer - USNRC 1

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LAW ENGINEERING TESTING COMPANY geemm enevomwem & conewueton mewees connunems t:

t-601 MINVET LANE P.O. Box 11297

  • CHARLOTTE. NORTH CARoUNA 28220 (704)523 2022 February 20, 1985 I

l Duke Powe.r Company Nuclear Production P.O. Box 33189 Charlotte, North Carolina. 28242 Attention:

Mr. Russell Propst

Subject:

Laboratory Testing Bituminous Mixtures Duke Power Company Charlotte, North Carolina l

P.O. Number K-54427-74 LETCo. Job No. CHG 5219 Gentlemen:

WS-y As requested, Law Engineering Testing Company has completed compressive strength

'W testing on two samples delivered to our office.

j 1

These samples were tested by a method similar to that described in ASTM D 1074,

" Compressive Strength of Bituminous Mixtures". It should be noted however, that the samples were cooled to a temperature of 55 F12 and that t he s amp l e's original test height was not equal to the diameter as specified.

It should be further noted that these samples have no true failure point at which the load does not continue to increase.

This is due at least in part to the plastic nature of these samples.

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The results of these tests are shown on the attached " Report of Compressive strength of Bituminous Mixtures". If you have any questions concerning this l

report or if we can be further assistance, please contact this office.

Respectfully submitted, 1

L/S ENGINEERING TESTING COMPANY d.,2 Allen J.

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n REPORT OF COMPRESSIVE STRINCTE OF BITUMINDOUS MIITURES.

Duke Power Co=pany Charlotte, North Carolina LETCo. Job No. CEG 5219 February 20, 1985 Sample 2ype:

422 Solids, 582 Bitumen Date Sampled: 1/11/85 Date 2ested: 2/14/85 Original Diameter: 2.85 in. Area

6. 83 Sq. In, original Height: 2.10 in.

Final Diameter: 5.60 in.

Deflection _

Total Load (Lbs.)

Cottressive Streerth, Ipsi)

LINCht})

.05 234.1 36.7

.10 253.6 39.7

.15 323.3 50.7

.20 359_.5_

Q

.30 404.1 63.3

.40 434.8 68.2

.50 471.0 73,g E)$

.60 526.7 82.6

.70 602.0 94,4

.80 705.2 110.5

.90 864.0 135.4 1.00 1081.0 169.4 1.10*

1142.7 179.1 1.20 1845.1 289.2 1.30 24'89.0 390,1 l

1.40 3180.2 498.5

  • Compressive strengths vere calculated based on the original ar specimen's actual area increased as the load increased.

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PIPORT OF COMPPISSIVE STPECTE OF BITUMINDOUS MIITUPIS Duke Power Company Charlotte, North Carolina LETCo. Job No. CEG 5219 Feb; uary 20, 1985 Sample Type:

422 Solids, 58% Eitu=en Date Sampled:

1/11/85 Date Tested: 2/14/85 Original Diameter: 2.85 in. Ar ea 6.36 sq. In.

Original Height: 2.4 5 in.

Tinal Diameter: 3.60 in.

Deflection Total Load libs.)_

Compressive Strencth, (Psi)

(i,a c s < > )

.05 41.8 6.6

.10 75.3 11.8 h

.15 100.3 15.7

.20 133.8 211,0J

.30 170.0 26.6,1 40 211.8 33.2

.50 231.3 36.3

.60 253.6 39.7

.70 278.7 43.7

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.80 295.4 46.3

.90 320.5 50.2 1

1.00 348.4 54.6 1.10 3B4.6 60.3 1.20 429.2 67.3 1.30 485.0 76.0 1.40 5,57.4 87.4.

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

Rote: The top of this sample was concave and chipped on the sides.

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$01 MINUET LANE P o. Box 11297 + CHARLOTTE NORTH CAROUNA 28220 (7041 523 2022 March 5, 1985 Duke Power Company Nuclear Production P.O. Box 33189 Charlotte, North Carolina 28242 Attention:. Mr. Russell Propst

Subject:

Laboratory Testing Bituminous Mixtures Duke Power Company Charlotte, North Carolina P.O.

Number K-54427-74 LETCo. Job No. CHG 5219 Gentlemen:

As requested, Law Engineering Testing Company has completed compressive strength testing on two samples delivered to our office.

These samples were tested by a method similar to that described in ASTM D 1074,

" Compressive Strength of Bituminous Mixtures". It should be noted however, that the samples were cooled to a temperature of 55 32 and that the sampl e's 0

original test beight was not equal to the diameter as specified.

It should be further noted that these samples have no true failure point at which the load does not continue to increase.

This is due at least in part to the plastic nature of these samples.

The results of these tests are shown on the attached " Report of Compressive strength of Bituminous Mixtures". If you have any questions concerning this report or if we can be further assistance, please contact this office.

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Respectfully submitted, IR ENGINEERING TESTING COMPANY Allen J. Hu es, C.

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Laboratory - pervisor

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.i, REPOET OF COMPRESSIVE STRENGTE OF BITUMINDOUS MIITURES Duke Power Company Charlotte, lierth Carolina LETCo. Job lio. CBG 5219 Sample Type: EDTA 40% Solids, 60 Bitumen Date Sampled: 2/22/85 Date Tested: 2/27/85 Original Diameter: 3.77 in. Area 11.16 Sq. In.

Original Height: 2.75 in.

Final Diameter: 3.09 in.

Deflect,. ion _ 9e Total Lead (Lbs.)

Ce=vressive Strenrth. (Psi) v-.

.05 l' 2 174.3 15.6

.10 2A 316.4 28.4

.15 L ~-

445.2 39.9

.20

7. 3 560.0 50.2 l

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656.6 D3 l

.30

/0 7 749.0 67.1/-

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/J. 7 827.'4 7.1

.*0 143 907.9 81.4

.45

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980.0 87. 8 w

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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3.h an 4f REPORT OF COMPRESSIVE STRENGTE OF BITUMINUOUS MIITURES Duke Power Company Charlotte, North Carolina LETCo. Job No. CEG 5219 Sample Type: EDIA 35 Solids, 65% Bitumen Date Sampled: 2/22/85 Date Tested: 2/27/85 Original Diameter:

3.88 in. Area 11.79 Sq. In.

Original Height: 2.79 in.

Final Diameter: 4.14 in.

Deflection 9c Total Lead (Lbs.)

Coceressive Strenrth. (Psi) ve.)

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.05 1 82.0 15.4

.10 36 329.0 27,9

.15

f. p 448.7 38.1 l

.20

7. 2.

556.5 47.2

.25 9.O 654.5 J5.5 i

.30

/O.g 742.7 113. D.*,

.35

/2.,5 820.4 69.6

.40 14.J 888.3 75.3

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.45

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945.0 80.2

.50 n.c 987.0 83.7

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Compressive strengths vere calculated based on the original areas.

The specimen's actual area increased as the load increased.

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O RIPDRI 0F COMPRESSIVE STRINGTE OF BITUMINUOUS MIXTUPJ.S Duke Power Company Charlotte, North Carolina LITCo. Job No. CHG 5219 Sample Type: IDIA 402 Solids, 602 Bitumen Date Sampled: 2/22/ 85 Date Tested: 2/27/85

' original Diameter: 2.85 in. Area 6.38 Sq. In.

Original Height: 2.00 in.

Final Diameter: 3.24 in.

t Deflection h

. Total Load (Lbs.)

Co=pressive Strenrth, ! Psi)

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.05 161.7 25.3

.10 278.6 43.7

.15 7,5 363.2 56.9

.20

/0. c '

434.0 T6 8.0 H

.25

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490.0 76.8

.30

/5, c 535.5 S3.9

.35 r/,3 569.8

.40 89.3 y,c, o 598.5 93.8

.45 4,J 623.7 97.8

.50 23.o 647.5 101.5

  • Compressive strengths were calculated based on the original specimen's actual area inert.ased as the load increased.

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.u-c REPORT OF COMPRESSIVE STRINGTE OT BITUMINUOUS HIITURE Duke Power Company Charlotte, North Carolina LETCo. Job No. CBC 5219 Sample Type: IDIA 42.5% Solids, 57.5% Bitumen Date Sampled: 2/22/85 Date 2ested: 2/27/85 Original Diameter:

3.87 in. Area 11.76 Sq. In.

Original Height: 3.19 in.

Final Diameter: 3.92 in.

Deflection ko Total Lead ILbs.)

Coetressive Strenrth. (Psi)

(J e.)

.05

/'S 75.6

.10 3/

6.4 149.1

.15 S7 12.7 227.5 19.3

.20

(:2. 3 302.4

.25 7.f 371.0 25.7 31.5

.30 9, ep 437.5 27.2

.35

/ /, C 499.1 yp.

42.4

.40

. /2 3 560.0 47.6

.45

/SI 617.4

.50.

/57 52.5 670.0 57.0

  • Compressive strengths were calculated based on the original areas.

specimen's actual area increased as the load increased.

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REPORT OF COMPRESSIVE STRENGTH OT BITUMINUOUS MIXTURES 4

Duke Power Company Charlotte, North Carolina LETCo. Job No. CBG 5219 i

Sample Type: EDIA 352 Solids, 652 Bitumen Date Sampled: 2/22/85 Date Tes:ed: 2/27/85 Original Diameter: 3.88 in. Area 11.82 Sq. In.

Original Eeight: 3.15 in.

Final Diameter: 4.12 in.

Deflectionfd Total Lead (Lbs.)

Compressive Strenrth. (Psi)

.05 144.9 12.3

.10 264.6 22.4

.15 364.7 30.9

.20 455.0 38.5 1

.25 539.7 45.7

.30 6 23.0

/ 52.7?

.35 700.0

~59.2

.40 770.7 65.2 9"r

.45 833.0 70.5 886.0 75.0

  • Compressive strengths were cal'culated based on the original areas l

The specimen's actual area increased as the load increased.

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REPORT OF COMPRESSIVE STRENOK OI 2ITUMINUOUS MIITURES Duke Powt[ Company Charlotte, North Carclina 1,ITCo. Job No. CHG 5219 d

Sample Type: EDIA45% Soli'ds,55%Bitumrin Date Sampled: 2/22/83

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Late Tested: 2/27/85 t:

Original Diameter: 3.92 in. Area Il.99-Sq'. In.

Original Height: 3.2 in.

Final Diameter: 4.13 in.

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Deflection /la).il; Iotal Load (Lbs.)

j.Cnxo essive Streneth, ! Psi)

.05

-98.0

.10 8.2 v.. US.6 18.0

.15 325.5 y

.s 27.1 35.5 H

.20

.25 425.6 x

515.0 4 2 J

.30 605.5 50.5 -

.35 689.5

.40 57.5 770.0 64.2

.45 848.4

.50 70.8 916.3 76.4

  • Co=pressive strengths were calculated based on the original areas.

specimen's actual area increased as the load increased.

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REPORI 0F COMPRESSIVE STRDIGTH OT EITJETNDOUS IITURES l

Duke Power Conpany Charlotte, North Carolina LETCo. Job No. CHG 5219 e

Sample Type: IDIA 42.5% Solids, 57.5% Bitumen Date sampled: 2/02/85 Date Tested: 2/27/85 Original Ditmeter:

3.89 in. Area 11.8B Sq. In.

Original Height: 3.1 in.

' final Dianecer: 4.15 in.

Defis;1ionO")

Total Lead (Lbs.)

Convressive Streerth (Psi)

.05 133.7 11.3

.10 219.8 18.5

.15 294.0 24.7

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.20 364.0 30.6

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.25 422 1 35.5

.30 4 81.6 40.5'

.35 525.7

.3

.40 574.0 4E.3 g@

.45

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6 16.0 51.9

. 5 0.

658.0 55.4

  • Compressive 'streng bs were ca.lculated based on the original areas.

The specimen's actual area. increased as the load increased.

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REPORT OT COMPRESSIVE STRDiCTE OT 51TUMINUOUS MIITURIS Duke Power Company Charlotte, North Carolina LETCo. Job No. CEG 5219 Sample Type: IDIA 452 Solids, 552 Eitumen Date Sampled: 2/22/85 Date Tested: 2/27/85 Original Diameter: 2.92 in. Area 6.71 Sq. In.

Original Eeight: 3.11 in.

Final Diameter: 4.15 in.

De# ec!iet 9e Total Lead ILbr.)

co eressive s:renrth, M

.05

/* l 175,7 ys,3 10

?E 315.7 47,o

.15 42 427.7 63.7

.20 g.p 527.8 7g,7

.25 f, o 626.7 92.9

.30 f.4 6 96.5 Fjo3,gp

.35

//,3 760.9 713,4 40 fy,9 819,0 122.1

.45 pf,;

s70,1 339,7 a

.50

/4. /

915.6 136.5

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the lead increased.

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March 21, 1985 e.

Duke Power Company Nuc liat' Noduetion P.O.[ Bo2 33189 Chatlettek North Carolisi 28242 Attention:

M;. Rursell Propst Fabject:

Laboratory'7ettio.g Bituminour. Mixtures Duke Povez'Oempany Cherlottei krth Carolin.t P.O. Number K-54427-74 LETCo. J eb Ho. CBG S219 N

G en t.".cmen :

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As requested, l.sv Engineering Testing Compaoy has, cortpleted cer.pressive strength h

testing on tut.nty-two samples delivered to our office.

These samples were tested by a' method similar to that described;in ASTM D 1074,

" Compressive Strength of Bituminous Mixtures". It should be noted however, that the sa=ples vere. cooled to a temperature of 55.t2 with the exceptic.n of samples fl9 an6 20, which were tested at room temperature (72 ) and also the original 0

height was not en ctly equal to the criginal diameter as specified.

It should be further noted that these sample.' have no true failure point at which the load does not continue to ines ease. This is due at least in part to the plastic nature of these samples.

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The reruits of thest tests are shown en the attached " Report of Compressive strength of Bitutincua Mixtu:res". If you have any questions concerning this report or if we can be ivrther assistance, please c'entact. this office.

Respectfu1]y submitted, LW ENGINEERING TESTING C MPANY J

Allen J.

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s RAPORT OF COMPRESSIVE STRENGTH OF BITUMINUOUS MIITURES Duke Power Company l

Charlotte, North Carolina LETCo. Job No. CBG 5219 Sample Type:

35: Solids, 65 : Bitumen Date Sampled: 3/15/85 Date Tested: 3/22/85 Sample No. f3 Original Diameter: 3.90 in. Area 11.94 sq. In.

Original Height: 3.50 in.

Final Diameter: 4.50 in.

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, De f' e e t ion (jv.)

Total Lead (Lbs.)

Compressive Str,eneth _(Psi)

.05 208.9 17.5

.10 '

328.9 27.5

.15 429.0 35.9

.20 514.8 43.1 l

.25 586.3

'49.1

.30 646.4 54.1

.35 749.3 f 62.7 7

~ i6. 8

.40 7 97.9 6

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.45 835.1 69.9

.50 906.6 75.9

.60 958.1 80.2

.70 1023.9 85.8

.80 1058.2 88.6

.90 1092.5 91.5 1.00 1112.5 93.2 j

  • Compressive strengths were calculated based on the original areasI The specimen's actual area increased as the load increased.

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REPORT OF COMPPISSIVE STPINGTE OF BITUMINUOUS HIITUPIS Duke Tover Company Charlotte, North Carolina LETCo. Job No. CEG 5219 Sample Type:

35% Solids, 65% Bitumen I

Date Sampled: 3/15/85 Date Tested: 3/22/85 l

Sample No. (4 Original Diameter:

3.94 in. Area 12.19 Sq. In.

Original Height: 3.51 in.

Final Diameter: 4.53 in.

. Deflection ([N-)

Total Lead (Lbs.)

Compressive Strencth, (Psi)

]

.05 220.2 18.1

.10 337.5-27.7

.15 440.4 36.1

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.20 523.4 42.9

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.25 594.9 48.8 i

.30 657.8

.3 5 '

715.0

~8.

.40 763.6 h

.45 806.5 66.2

.50 843.7 69.2

.60 912.3 74.8

.70 966.7 79.3

.80 1029.6 84.5 I

.90 1081.1 88,7-1.00 1132.6 92.9

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  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased, l

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'l REPORT OF COMPRESSIVE STRENGTH OF BITUMINDOUS MIITURES Duke Power Company Charlotte, North Carolina LETCo. Job No. CHG 5219 l

1 Sample Type:

40 % Solids, 60 Bitumen

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Date Sampled: 3/15/85 Date Tested: 3/22/85 l

Sample No. #5 i

Original Diameter:

3.88 in. Area 11.82 Sq. In.

Original Height: 3.59 in.

l Final Diameter: 4.47 in.

. De fle ct i onUND Total Lead (Lbs.)

Compressive Strength. (Psi)

.05 251.7 21.3

.10.

.383.2 32.4

.15 471.9 39.9

.20 543.4 46.0

.25 600.6 50.8

.30 646.4 51,.7

.35 6 92.1 (58.6)

.40 737.9 6E4 d?

45 769.3 65.1 G

.50 800.8 67.7

.60 829.4 70.2 l

.70 863.7 73.1 i

.80 900.9 76.2 l

.90 958.1

'81.1 1.00 1009.6 85.4 i

1

  • Compressive strengths were calculated based on the original areas.

The specimen's' actual area increased as the load increased.

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REPORT OF COMPRESSIVE STRENGTH OF BITUMINDOUS MIITURES j

Duke Power Company 1

Charlotte, North Carolina LETCo. Job No. CEG 5219 Sample Type:

40 2 Solids, 60 Bitumen l

Date Sampled: 3/15/85 Date Tested: 3/22/85 Sample No. #6 Original Diameter:

3.83 in. Area -

11.52 sq. In.

Original-Height: 3.32 in.

Final Diameter: 4.44 in.

. De fle et i onO^'-)

Tetal Lead (Lbs.)

_ Compressive Strenrth. (Psi)

.05,

165.9 14.4

.10 277.4 24.1

.15 371.8 32.3

.20 463.3 40.2

.25 537.7 46.7

.30 600.6 52 1

.35 660.6 (57.3')

.40 712.1 6E5

.45 755.0 65.5

.50 792.2 68.8

.60 855.1 74.2

.70 909.5 78.9

.80 950.1 83.2

+-

.90 1006.7 87.4 1.00 1055.3 91.6

  • Co=pressive strengths were calculated based on the original areas.

The specimen's actual aret increased as the lead increased.

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l REPORT OF COMPRESSIVE STRENGTE OF EITUMINUOUS MIITURES.

Duke Power Company Charlotte, North Carolina l

LETCo. Job No. CBG 5219 I

i i

Sample Type:

4 2.5% Solids, 57.5% Bitumen Date Sampled: 3/15/85 Date Tested: 3/22/85 l

Sample No. #7 l

Original Diameter:

3.89 in. Area 11.88 sq. In.

Original Height: 3.98 in.

Final Diameter: 4.28 in.

.DeflectionOMU Iotal Lead (Lbs.)

Compressive Strencth. (Psi)-

4

.05 *

'194.5 16.4

{

.10 328.9 27.7 j

.15 451.9 38.0 l

.20 540.5 45.5

.25 614.9 51.8

.30 686.4 57.8 I

.35 749.3 63.1 '

h-)

40 812.2

/65.4 l

.45 869.4 73.2 i

.50 915.2 77.0

.60 1001.0 84.3

.70 1063.9 89.6 l

.80 1124.0 94.6

.90 1175.5 98.9 1.00 1224.1 103.1

  • Compressive strengths were calculated based on the e iginal areas.

The specimen's actual area increased as the load increased.

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h' REPORT OF COMPRESSIVE STRENGTE OF BITUMINUOUS MIITURES Duke Power Company Charlotte, North Carolina LETCo. Job No. CBG 5219 l

Sample Type:

42.5% Solids, 57.52 Bitumen Date Sampled: 3/15/85 Date Tested: 3/22/85 Sample No. (8 Original Diameter:

3.89 in. Area 11.88 sq. In.

Original Height:

3.85 in.

Final Diameter: 4.39 in.

. De fl e c t ion (lu.)

Totsi Lead (Lbs.)

Compressive Strencth, (Psi)

.05 268.8 22.6

.10 449.0 37.8'

.15 577.7 48.6

.20 672.1 56.6

.25 760.8 64.0

.30 835.1 70.3

.35 098.0 75.6

.40 952.4 L80.2 /

.45 992.4 8f.5 C..m p b~'

.50 1035.3 87.1

.60 1109.7 93.4 l

.70 1166.9 98.2

.80 1204.1 101.4

.90 1249.8 105.2 i

1.00 1292.7 108.8

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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+OMPRESSIVE STRENGTE OF BITUMINDOUS MIITURES Duke Power Company Charlotte, North Carolina j

LITCo. Job No. CHG 5219 4e l

Sample Type:

45 2 Solids, 55 2 Bitumen Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No. #9 Original Diameter: 3.99 in. Area 12.50 sq. In.

Original Eeight: 3.67 in.

l Final Diameter: 4.51 in.

i l

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.DeflectionONd Total Load (Lbs.)

Compressive Strencth, (Psi)

.05 -

174.5 14.0

.10 291.7 23.3

.15 377.5 30.2

.20 457.6 36.6 I

. 2'S 526.2 42.1 l

.30 586.3 4_64

.35 637.8

(,51. 0' (th

~~

40 689.3 55.1

.45 735.0 58.8 l

l

.50 777.9 62.2

.60 834.7 67.5 l

.70 892.3 71.4

.80 932.4 74.6

.90 97 5.3 78.0 1.00 1018.2 81.5 l

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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/f REPORT OF COMPRESSIVE STRENGTH OF BITUMINUOUS MIITURES Duke Power Company Charlotte, North Carolina j

LETCo. Job No. CHG 5219 1

l Sample Type:

45 % Solids, 55 % Eitumen Date Sanpled: 3/18/85 Date Tested: 3/22/85 Sample No. #10 Original Diameter:

3.88 in. Area 11.82 sq. In.

Original Height: 4.01 in.

i Final Diameter: 4.51 in.

1

. Deflection (!ud Total Load (Lbs.)

Compressive Strength, (Psi) l

.05

. 100.1 8.5 4

.10 251.7 21.3

.15 409.0 34.6

~

.20 486.2 41.1

.25 566.3 47.9

.30 623.5 52.7

.35 666.4 58.1 g

.40 743.6

/ 62.97 d

.45 7 95.1 67.3

.50 835.1 70.7 i

.60 915.2

-77.4

.70 978.1 82.7

.80 1023.9 86.6

.90 1066.8 90.3 1.00 1104.0 93.4

  • Co=pressive strengths were calculated based on the original areas.

The

'speci=en's actual area increased as the load increased, g p q.*

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/9 REPORT OF COMPRESSIVE STRENGTH OF BITUMINUOUS MIXTURES Duke Tower Company Charlotte, North Carolina LETCo. Job No. CBG 5219 47.5 Sample Type:

6976% Solids, 52.5% Eitumen Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No. fil Original Diameter:

3.88 in. Area 11.82 sq. In.

Original Beight: 3.72 in.

Final Diameter: 4.48 in.

. De fle c t ion (/N)

Total Load (Lbs.1 Coceressive Streerth, (Psi)'

. 05' 257.4 21.8

.10 414.7 35.1

.15 543.4 46.0

.20 637.8 54.0

.25 726.4 61.5

.30 800.8 67.7

.35 866.6

~73.3 4

a.ib

.40 923.8

_78.2

.45 981.0 83.0

.50 1029.6 87.1

.60 1109.7 93.9

.70 1184.0 100.2

.80 1233.0 104.3

.90 1272.7 107.7 1.00 1324.2 112.0 ee l

l

  • Co=pressive streng.hs were calculated based on the original areas The specimen's actual area increased as the load increased.

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J REPORT OF COMPRESSIVE STRENGTH OF BITUMINUOUS MIXTURES Duke Power Company Charlotte, North Carolina 1

LETCo. Job No. CBG 5219

)

Sample Type:

47.5 2 Solids, 52.52 Bitumen J

Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No. #12 j

Original Diameter: 3.84 in. Area 11.58 sq. In.

Original Height: 3.71 in.

Final Diameter: 4.40 in.

1

, Deflection ( M)

Total Load (Lbs.-)

Compressive Streneth, (Psi)

.05 234.5

'20.3

.10'

'357.5 30.9

.15 466.2 40.3

.20 563.4 48.7

.25 637.8 55.1

.30 703.6 60.8_

.35 818.0 70.6

.40 869.4 7.

h)

.45 912.3 78.8

.50 949.5 82.0 3

.60 986.7 85.2

'l

.70 1052.5 90.9 j

.80 1086.8 93.9

.90 1129.7 97.6 1.00 1166.9 100.8

  • Compressive strengths were calculated based on the original areas.

The

{

specimen's actual area increased as the load increased.

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REPORT OF COMPRESSIVE STRENGTH OF EITUMINDOUS MIITURIS i

Duke Power Co=pany I

Charlotte, North Carolina LETCo. Job No. CBG 5219 l

Sample Type:

52.5% Solids, 47.5" Eitumen 122 Boric Acid Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No. #13 1

Original Diameter: 3.90 in. Area 11.95 Sq. In.

Original Height: 3.83 in.

I Final Diameter: 4.45 in.

. Deflection (lad Total Load (Lbs.)

Compressive Strencth. (Psi) i 1

.05 343.2 28.7 I

.10 552.0 46.2

.15 703.6 58.9 I

.20 823.7 68.9

.25 915.2 76.6

.30 1006.7 84.2

.35 1083.9 90.7 g')

40 1152.6 IV6.5 /

l

.45 1206.9 101.0

.50 1249.8 104.6

.60 1338.5 112.0

.70 1401.4 117.3

.80 1447.2 121.1

.90 1484.3 124.2 1.00 1507.2 126.1

  • Compressive strengths were calculated based on the original areas.

The

)

' specimen's actual area increased as the load increased.

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REPORT OF COMPRESSIVE STRENGTE OF EITUMINUOUS MIITUPIS Duke Power Company Charlotte, North Carolina LETCo. Job No. CBG 5219 Sample Type:

52.5* Solids,47.5 % Eitumen Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No.~#14 1

l Original Diameter:

3.90 in. Area 11.95 Sq. In.

Original Height: 3.91 in.

Final Diameter: 4.46 in.

. Deflection [/M.)

Total Lead (Lbs.)

Compressive Strength, (Psi)

.05 286.0 23.9 I

.10 457.6 38.3

.15 586.3 49.1 l

.20 700.7 58.6

.25 795.1 66.5

.30 878.0 73.5

.35 946.7 79.2

.40

~1006.7 I 84.2_J l

.45 1063.9 89.0 l

.50 1109.7 92.9

)

.60 1195.5 100.0 l

.70 1258.4 105.3 1 -

.80 1312.7 109.8

.90 1358.5 113.7 1.00 1395.7 116.8 i

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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"EPORT OF COMPPISSIVE STPINGTH OF BITUMINDOUS MIXTURES Duke Power Company Charlotte, North Carolina LETCo. Job No. CEG 5219 Sample Type:

55 2 Solids, 45 % Eitumen Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No, f15 Original Diameter: 3.90 in. Area 11.95 Sq. In.

Original Height: 3.81 in.

Final Diameter: 4.45 in.

.DeflectionIlad Total Lead (Lbs.)

Cemnressive Strencth, (Psi)

.05 4 23.3 35.4

.10 743.'6 62.2 l

.15 934.8 79.0 i

.20 1144.0 95.7 l- -

.25 1301.3 108.9

.30 1421.4 118.9

.35 1521.5 1 27.3

.40 1598.7

! 133.8 /

(g 45 1661.7 139.1 l

.50 1716.0 13 9.1

.60 1796.1 150.3

.70 1856.1 155.3 i

.80 1907.6 159.6

.90 1953.4 163.5 1.00 1996.3 167.1 9=

l

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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h REPORT OF COMPRESSIVE STRENGTE OF EITUMINUOUS MIITURES Duke Power Company Charlotte, North Carolina LETCo. Job No. CEG 5219 Sample Type:

55: Solids, 45% Eitumet 12% Boric Acid Date Sampled: 3/18/85 (1545)

Date Tested: 3/22/85 Sample No. f16 j

i Original Diameter: 3.89 in. Area 11.88 Sq. In.

Original Height: 3.58 in.

I Final Diameter: 4.39 in, i

i Deflection (/a.)'

Total Lord (Lbs.)

Compressive Strencth, (Psi)

{

.05 417.9 39.7 l

.10 780.8 65.7 i

.15 1009.6 85.0

.20 1189.8 100.1

.25 1310.0 110.3

.30 1435.7 120.9

.35 1535.8

[ETE2[]

.40 1624.5 136.7

.45 1690.3 142.3

{~$

.50 17 44.6 146.9 j

.60 1816.1 152.9 I

l

.70 1841.8 155.0 l

.80 1873.3 157.7 l

.90 1913.3 161.1 1.00 1964.8 165.4 i

  • Co=pressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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REPORT OF COMPRESSIVE STRENCTU OF BITUMINDOUS MIITURES

{

I Duke Power Company Charlotte, North Carolina LETCo. Job No. CBG 5219 l

Sample Type:

45 % Solids, 55 % Eitumen I

Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No. #17 1

1 Original Diameter:

3.82 in. Area 11.46 Sq. In.

Original Eeight: 4.17.in.

Tinal Diameter: 4.34 in.

I l

DulectionUN)

Total Lead (Lbs.)

Compressive Strenrth, (Psi)

I

. )5 243'.1 21.2

.10 300.3 26.2

.15 411.8 35.9 I

.20 509.1 44.4

.25 592.0 51.7

.30 669.2 58.4 1

.35 743.6 64.9 Q*

.40 815.1 1 71.1]

45 878.0

^K. 6

.50 923.4 81.4

.60 1038.2 90.6

.70 1121.1 97.8-

.80 1192.6

'104.1

.90 1258.4 109.8 1.00 1301.3 113.6 I

, *Compressiv'e strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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1 REPORT OF COMPRESSIVE STRINGTE OF BITUMINUOUS riIITURES j

1 Duke Power Company j

Charlotte, North Carolina i

LETCo. Job No. CHG 5219 Sample Type:

745% Solids, 55 % Eitumen Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No.'f18 l

Original Diameter: 3.92 in. Area 12.07 Sq. In.

Original Height: 3.93 in.

Final Diameter: 4.41 in.

J DeflectionUud Total Lead (Lbs.)

Cernressive Strencth, (psi)

.05 225.9 18.7

.10 383.2 31.8

.15 509.1 42.2

~

.20 614.9 50.9 l

.25 712.1 59.0 J

.30 797.9 66.1 I

.35 875.2 72.5

.40 943.8 T 78.2 7

.45 2003.9 83.2

.50 1063.9 88.1

.60 1172.6 97.1

.70 1267.0 105.0

.80 1344.2-111.4

.90 1407.1 116.6 1.00 1452.9 120.4

  • Compressive strengths were calculated based on the original a::eas.

The specimen's actual area increased as the load increased.

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REPORT OF COMPPISSIVE STPINGTE OF BITUMINUOUS MIITURES Duke Power Company Charlotte, North Carolina LETCo. Job No. CHG 5219 Sample Type:

45 : Solids, 55 % Bitumen 12% Eoric Acid Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No. #19 original Diameter:

3.97 in. Area 12.38 sq. In.

Original Height: 3.84 in.

Final Diameter: 4.47 in.

1 Deflectionfl~).

Total Lead (Lbs.)

Compressive Streneth, (Psi)

.05 91.5, 7.4

.10 151.6 12.2

.15 1 97.3 15.9

.20 234.5 18.9

.25 268.8 21.7 j

.30 297.4 24.0

{

.35 323.3-26.1

.40 348.9 T28.2]

h, 45 371.8-

~

30.0

.50 3 91.8 31.6

.60 417.6 33.7 l

.70 437.6 35.3 I

.80 457.6 37.0 l

.90-477.6 38.6 1.00 497.6 40.2 Note: This sample was tested at 72 8 0

  • Compressive strengths were calculated based on the originG areas.

The specimen's actual area increased as the load increased.

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ZJem L8 REPORT OF COMPRESSIVE STRENGTH OF BITUMINUOUS MIKTURES

)

Duke Power Company Charlotte, North Carolina 4

LETCo. Job No. CBG 5219 l

,.i Sample Type:

45 % Solids, 55 % Eitumen

)

Date Sampled: 3/18/85 Date Tested: 3/22/85 Sample No. #20

]

original Diameter: 3.88 in. Area 11.82 sq. In.

Original Height: 3.89 in.

Final Diameter: 4.46 in.

Deflection (/4)

Total Loed (Lbs.)-

Cocoressive Strencth. (Psi)

.05 9,1. 5 7.7

.10 14$.7 12.6-

.15 194.5 16.5

.20 231.7 19.6

.25 260.3 22.0

.30 286.0 24.2

.35 311.7 26,4 j

l

.40 334.6 28.33 (p)

.45 360.4 3'd'. 5

?

.50 383.2 32.4

.60 414.7 35.1

.70 434.7 36.8

.80 454.7 38.5

.90 474.8 40.2 1.00 491.9 46.1 Note: This sample was tested at 72 [

Me 0

l

  • Compressive strengths were calculated based on the original areas.

The

. specimen's actual area increased as the load increased.

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  • ).a REPORT OF COMPRESSIVE STRENGTH OF BITUMINUOUS HIXTURES Duke Power Company Charlotte, North Carolina LETCo. Job No. CHG 5219 Sample Type:

~45% Solids, 55 " Bitumen 12% Boric Acid, 10% Evaporated Date Sampled: 3/20/85 Date Tested: 3/22/85 Capacity Sample No. #21 Original Diameter: 3.88 in. Area 11.82Sq. In.

Original Height: 3.56 in.

Final Diameter: 4.57 in.

.DeflectionhN.)

Total Load (Lbs.)

Compressive Strenrth, (Psi) l 1

.05 300.3, 25.4

.10 480.5 40.7

.15 617.8 52.7

.20 737.9 62.4

~

.25 829.4 70.2 I

.30 906.6 76.7

.35 966.7 l81.8]

.40 1023.9 86.6 3

.45 1066.8 90.3 4

.50 1109.7 93.9

.60 1181.2 99.9

.70 1232.6 104.3

.80 1292.7 109.4

.90 1315.6 111.3

{

1.00 1344.2 113.7

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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REPORT OF COMPRESSIVE STRENGTH OF BITUMINUOUS MIXTURES l

Duke Power Company Charlotte, North Carolina l

LETCo. Job No. CEG 5219 Sample Type:

45 % Solids, 55 % Bitumen 12% Boric Acid Date Sampled: 3/20/85 Date Tested: 3/22/85 Sample No. (22 l

Original Diameter:

3.88 in. Area 11.82 Sq. In.

Original Height: 3.46 in.

l l

Final Diameter: 4.52 in.

l

.DeflectietDad Total Lead (Lbs.)

Compressive Streneth, (Psi) l

.05 263.1 22.3 l

.10 414.7 35.1 I

.15 532.0 45.0

.20 629.2 53.2

.25 712.1 60.2 l

.30 783.6 66.3 I

.35 849.4

t. 71. 9 l l

h) 40 903.8

~76.5

.45 949.5 80.3

.50 995.3 84.2

.60 1061.1 89.8 l

.70 1095.4 92.7

~

I

.80 1132.6 95.8

.90 1164.0 98.5 1.00 1204.1 101.9

  • Co=pressive strengtas were calculated based on the original areas.

The specimen's actual area increased as the load increased.

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/""h LAW ENGINEERING TESTINO COMPANY penwennca erworrnarns & construenon enames connunarus 501 MINUET LANE P o. sox 11297 e CHARLOTTE, NORTH CAROLINA 28220 (7041523-2022 November 30, 1984 Associated Technologys, Inc.

212 South Tryon Street Charlotte, North Carolina 28281 Attention:

Mr. Steve Simpson

Subject:

Laboratory Testing Bituminuous Mixtures Associated Technologys, Inc.

Charlotte, North Carolina LETCo. Job No. CHG 5219 Gentlemen:

As requested, Law Engineering Testing Company has completed compressive strength testing on two samples delivered to our office.

These samples were tested by a method similar to that described in ASTM D 1074, " Compressive Strength of Bituminous Mixtures".

It should be noted however, that the samples ver.e_ cooled to a temperature of 550 i 20 and F

that the sample's original test. height was not equal to the diameter as specified. It should be further noted that these samples have no true failure point at which the load does not continue'to increase.

This is'due at least in part to the plastic nature of these samples.

The specific gravity of each sample was also checked and from this the unit weight after compression was calculated.

The results of these tests are shown on the attached " Report of Compressive Strength ~of Bituminous Mixtures".

If you have any questions concerning thi's report or if we can be further assistance, please contact this office.

Respectfully submitted, LAW ENGINEE NG COMP "Y

e Allen J.. ghes [.E.T.

y&

Laboratory SupeTvisor

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%w REPORT OF COMPRESSIVE STRENGTH OF BITUMINUOUS MIXTURES Associated Technologys, Inc.

Charlotte, North Carolina LETCo. Job No. CHG 5219 November 30, 1984 Sample Type:

50/50 Borate / ype I Date Tested:

11/27/84 Original Diameter: 2.865 In.

Area:

6.45 Sq. In.

Original Height: 2.33 In.

Specific Gravi *y: 1.28 Unit Weight 79.9 lb/Cu.Ft.

Deflection (IN)

Total Load (Lbs.)

Compressive Strength, (Psi)*

.05 70.0 10.9

.10 182.7 28.3

.15 245.0 38.0

.20 418.6 64.9

.30

-544.6-~~-~~~

~ 84.4

.40 600.6 93.1

.50 629.3 97.6

.60 651.0 100.9

.70 679.0 105 3

.80 709.1 109.9

.90

^

746.2 115.7 1 00 795 2 123.3 1.20 852.6 132.2 1.40 929 6 144.1 1.60 1012.0 156.9

  • Compressive strengths were calculated based on the original areas.

The specimen's actual area increased as load the increased.

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e L.AW ENGINEERING TESTING COMP %NY

. gootecnacat erwwonrnenta a construenon matenate conauriants 501 MINUET LANE P O BOX 11297 e CHARLOTTE. NORTH CAROUNA 28220 (704) $23-2022 December 23, 1986 Jan ua ry 6, 19 87 -

i 1

Associated Technologies, Inc.

Suite 300 l

212 South Tryon Street Charlotte, North Carolina 28281 Attention: Mr. Steve Simpson

Subject:

ATI Bituminized Specimens ATI Test Plan Issued 8/5/86 Ass ociated Technologies, Inc.

Charlotte, North Carolina LETCo. Job No. CHG 5219, Corrected January 6,1987 I,

Gen t1eme n :

l As authorized by your acceptance of our Proposal No. 234M6, Law Engineering has c omplet ed laborat ory t es ting o n bituminiz ed s pecimen s submitted to our i

lab oratory by Mr. Steve Simpson.

Requested testing was outlined in the a p pro pr ia t e s ec tion s of the A.T. I.- Tes t Plan is sued o n Augus t. 5, 1986.

Numerical specimens designations were established by Mr. Simpson.

Requested test procedures and exceptions were as f ollows:

A.

A.T.I. Test Plan issued August 5,1986, Section 1.0 Cesium nitrate and cobalt nitrate used in specimen preparations were furnished by A.T.I.

Sorption of glass leach test vessels was not determined.

Electrical conduc tivity and tot al organic content of leachate solution was analyzed three times during testing.

Leachate tes t vessel rinse was disregarded as entire tes t vessel was used in analysis process.

Chemical analysis f or s pecified materials in leachate s olution were made.

Other c alc ula tions ac cording t o ASN 16.1 to be performed by A.T.I.

pe rs o nn el.

3.

A.T.I. Test Plan issued August 5,1986, Section 2.0 Test s pecimens f er compres sive strength were conditioned at 5 5 +

20 F.

Stress-strain calculations were made at 0.05 inch increments up t o 1.0 inch def orma tion or sample f ailure, wh icheve r occ urr ed first.

Stress calculations were based on original specimen geometry.

1 s

Associated Technologies, Inc.

LETCo. Job No. CHG 5219 l

Decembe r 23, 1986 l '

C.

A.T.I. Tes t Plan is sued August 5,1986, Section 3.0 Radia tion t es ting was performed by o thers.

Penetration testing was performed according to Sections 8.1 and

)

9 of ASTM D 5

" Standard Tes t Method for Pe n e t ra t io n of Bituminous Materials ".

Test temperatures of 77 + 30 F were used.

l Only four specimens of six specimens prepared were returned for f inal t es ting.

Photographs were only taken af ter specimen irradiation.

Compres sive strength tes ting was performed under same conditions as stated in above "B".

D.

A.T.I. Tes t Plan issued Augus t 5,19 86, Section 4.0 Testing included in this section was performed by others.

Compres sive strength tes ting of expos ed s pecimen s to be 3

per' formed by Law Etigineering at a later date.

l E.

A.T.I. Tes t Plan issued Augus t 5,19 86, Section 5.0

)

Cold portion of thermal cycling was performed on protected s pecimen s in a N-Pro pyl Alcohol bath.

l Compressive strength testing was performed under same conditions j

as stat ed in above "B".

J

+

Test results and photographs are included in the attached " Summary of i

Laboratory Tes ting" sheets.

{

Law Engineering appreciates the opportunity to provide its professional l

se rvice s a t this time.

If you have any ques tions concerning this report, or if ue may be of further assistance, please contact this of fice.

f Ve ry L ruly yours,

j l

LAW ENGINEERING TESTING COMPANY I

l M

D Micha el 0. Hamlet t, C. E. T.

Senior Engineering Technician l

Robe r t E. Sm ith, Jr., P. E.

Chief Etigineer MOH :RES :jk f

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OF LABORA't0RY TESTING T

b.

Asst:ciated Technologies Inc.

Charlotte, North Carolina p

Test Plan Issued August 8,1986 L_

LETCo. Job No. CHG 5219 Immersion Tes ting (Section 7.M Ecodex/ Type I Materiill' 1

Compressive Load (esi).

I i

Deflection Specimen Nur.ber Specimen Number

/

L Inch e s (Or it inal Condi t ion) i Af t e r 9,Q D ev Imtne r s ion k

i r

12 M

14_

U M

c.l 0

0 0

0 0

0 0.05 6.9

' 6.3 40.4 11.3 15.8 f

0.10 15.8 28.4 20;4 22.7 32.2 0.15 34.4 29.2 29.7 31.5 46.5 0.20 52.4 38.1 38.0 38.2 58.1 r~n 0.25 66.8 45.5 44.6 43.9 68.'2 LJ 0.30 (78.87 51.6 49.9 48.9 77.5 0.35 89.0 Q

LM MI

/84.2/

0.40 97.6 61.7 59.5 57.5 93.6 0.45 106.7 70.2 63.7 61.3

'98.1

' ' ^ "

0.50 117.8 77.8 67.6 64.7 104.5 0.55 124.3 76LJ 71.4 67.6 108.5 F

0.60 126.5 7E.3 75.0 70.6 113.1 k

0.65 130.9 79.9 78.4 73.5 117.9 0.70 135.4 82.S 81.8 76.2 122.8 0.75 140.9 86.1 85.0 79.0 127.4 0.80 14 5.3 89.5 88.2 81.9 131.8 0.85 150.5 92.9 91.6 84.0 135.4 0.90 154.9 95.S 95.0 87.0 139.9 y

0.95 159.3 98.7 98.8 89.5 144.7 1.00 1 64.9 102.1 102.0 92.4 14 8.5

{

Note: Leading Rate: 0.16 inches per minute Conditioning Temp. : 550 F w

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OF LABORATORY TESTING As sociat ed Technologies, Inc.

Charlotte, North Carolina 4

Tes t Plan Issued 8/5/86

.i LETCo. Job No.. CHG 5219

/

4 Radiation Tes ting (Section 3.0)

Ecodex/ Type I Material Comores sive Load (osi)

Def lec tio r:.

Specimen Number Specimen Number (Inches)

(Oricinal Condition)

(After Irradiation)*

11 11 12 10 1

I O

0 0

0 0

0.05 6.9 6.3 3.9 3.0 0.10 15.8 18.4 7.5 6.3 0.15 34.4 29.2 11.3 9.5 0.20 52.4 38.1 15.2 12.8 C.2 5 66.8 45.5 18.2 15.5 0.30 f 78.8 /

51.6 _

f7ITTl 17.9 0.35 89.0 E14,.1) 24.1 J 20.s /

0.40 97.6 61.7 26.3 22 7 0.45 106.7 70.2 29.1 25.4 0.50 117.8 77.8 31.3 27.6 0.55 124.3 78.1 34.8 30.1 0.60 126.5 78.3 41.0 35.2 0.65 130.9 79.9 43.1 33.6 0.70 135.4 82.8 42.1 33.9 0.75 140.9 86.1 41.8 35.4 0.80 145.3 89.5 43.5 37.0 0.85 150.5 92.9 45.4 38.8 4

0.90 154.9 95.8 47.5 40.9 l

0.95 159.3 98.7 49.7 42.8 1.00 164.9 102.1 51.7 44.3 l

Note: Loading Rate: 0.16 inch e s pe r-m inute.

l Conditioning Tempera ture: 550 F l

l

  • Corrected 1/6/87 I

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OF LABORATORY TESTING j

l Associated Technologies Inc.

Charlotte, North Carolina Tes t Plan Issued Augus t 8,1986 LETCo. Job No. CHG 5219 Thermal Cycle Tes ting (Section 5.0)

Ecodex / Type I Material l

i comeres sive Load (e si)

Def lectio n Specimen Number Specimen Number I

Inches (Orininal Condition)

(After Therrnt Ovelin,1*

12.

1.1 E.Q 2.1, '

21 I

O 0

0 0

0 0

l 0.05 6.9 6.3 5.0 9.7 10.7 l

l 0.10 15.8 18.4 13.7 21.3 21.2 0.15 34.4 29.2 22.2 30.7 29.6 0.20 32.4 38.1 29.3 39.0 39.8

'I 0.25 66.8 45.5 37.8 47.3 48.2 0.30 T737El 51.6 Lal,1j 54.9 54.9 0.35 89.0 T56.53 53.6 ITI~T1 l_60.51~

j 0.40 97.6 61.7 59.5 69 3 66.1 0.45 106.7 70.2 65.2 74.5 71.2 0.40 117.8 77.8 70.6 79.2 75.7 l

0.55 124.3 78.1 74.2 83.7 79.6 1

0.60 126.5 78.3 78.2 89.4 83.3 0.65 130.9 79.9 82.4 93.4 87.5 0.70 135.4 82.8 86.0 97.0 91.3 0.75 140.9 86.1 88.8 100.3 94.5 0.80 145.3 89.5 92.3 103.8 98.0 0.85 150.5 e2.9 94.5 107.4 101.3 0.90 154.9 95.S 98.0 110.9 103.8 l

0.95 159.3 98.7 100.6 114.0 107.1 1.00 164.9 102.1 108.4 116.8 110.6 Note: Loading Rat e: 0.16 inches pe r m in ut e Conditioning; Temp: 550 F f

  • Corrected 1/6/87 l

l I.Av ENGNEERING TELTING CCWANY

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OF LABORATORY TESTING Ass ociat ed Tec.bol; 3 es Inc.

i Charlotte, North Carolina 1'

Tec t Plan Iss ued Augus t 8,19E6 I

I.ETCc. Job No. C!!0 5219

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Imme rsion Tes ting (Section 2.0)-

Bead Resin / Type I Materiu

?-

Cem e-as si ve I o n d j,p,s i )

Deflection Specimen Numb /.r Specimen Number IUP.h_.f.E :

LOjig,irial Conditic;11 (After 40-Day Tree re i en}

l 1

1 1

1 0

0 0

0 0

0 0.05 5 4.2J O.10 112.1 7,

51.0 39.5 68.8 86.9 107.1 85.9 135.9 120.0 0,15 1 72.3

,' 176.6 118.5 192.9 166.8 e

0.20 252.4 249.2 178.3 244.0 206.2

) 1 0.25 285.3..

313.3 a

220.0' 285.8 235.4 0.30

}335.8]

3_61.5

' T2 44.B T318. 8'!-

L237d.J 0.35 3 75. 7 1391.31 257.8 34 2.5

'.7 2. 0 0.40; 402.1 411.8 263.6 356.5-280.3 0.45 Failur e

- 616.9 2 64.1 362.5 285.2 O.50 Failure Failure 362.7 N 5. $

0.55 3411ure s Failure 0.60 0.65 1

l' G.70 0.75 0.80,

{

0.85 '

T

.0.90f l

0.95 l

1.00 r

Note: Loading Rate: 0.16 inches per minute J

l j

Condit io ning Tempera tur e : 55s F 1

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SUMMARY

OF LABORATORY TESTING Ass ociat ed Technologies, Inc.

)

Charlotte, North Carolina Tes t Plau Issued 8/5/86 LETCo. Job No. C11G 5213 l

Radia tion Tes ting (Section 3.0) j Bead Resin / Type I Material

]

i Comores sive Load (e si) i Def lectio n Specimen Numbe r Specimen Number I

(Inches)

(Oricinal Condi tion)

(After Irradiation)

I i

1 la Lt 0

0 0

0 0

0.05 54.2 31.0 35.5 55.2 -

3 l

0.10 112.1 107.1 69.1 91.5 l

0.15 172.3 176.6 99.4 105.7 0.20 252.4 249.2 134.2 137.9 2

0.25 285.3 313.3 165.0 165.5 l

0.30 F335.&1 361.5__

F190.11 f l85.0 /

j 0.35 375.7 f_391 RI 213.4 200.0 j

0.40 402.1 411.8 230.1 210.3 j

0.45 Fa ilur e 41 6.9 241.8 218.3 0.50 Failure 249.0 223.2 0.55 251.4 226.2 0.60 Failure 226.6 j

0.65 226.8 O.70 Failure 0.73 0.80 0.85 0.90 1

0.95 I

1.00 l

1 Note: Loading Rate: 0.16 inches per minute Conditioning Tempera ture: 550 F 1

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SUMMARY

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Associated Technologies Inc.

l Charlotte, North Carolina Tes t Flan issued Augus t 8,1986 LETCo. Job No. CHG 5219 Thermal Cycle Tes ting (Section 5.0)

Bead Resin / Type I Material Comores sive Load (p si)

Def lec tio n Specimen Number Specimen Number

]

Inches (Oricinal Condition)

(Af ter Thermal Cveline)*

j i

1 1

1 4

1 O

O O

O O

O j

0.05

~

54.2 51.0 13.7 13.4 13.2 i

0.10 112.1 107.1 30.3 28.0 41.3 0.15 172.3 176.6 51.2 44.5 77.0 0.20 252.4 249.2 77.1 66.6 118.3 0.25 285.3 313.3 104.6 89.7 156.3 0.30

{335.87f 361.5_

137.7_

119.2_

186.5 0.35 375.7 L391.8I

[169.11 l_148.91 1215.11 0.40 402.1 411.8

~187.0 169.9 235.3 0.45 Fa ilur e 416.9 194.5 186.0 245.2 0.50 Failure Failure 192.3 Failure 0.55 Failure 0.60 0.65 0.70 0.75 0.80 0.85 0.90 0.95 1.00 Note: Loading Rate: 0.16 inches per minute Conditioning Temp: 550 F

  • Corrected 1/6/87 I

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LAW ENGINEERING TESTING CO9WIPANY peowc, vicat er=worvraww a conswucton mmeras cxneunarns 501 MINUET LANE P.O. Box 11297 e CHARLOTTE. NORTH CAROUNA 28220 (704) 52>2022 March 23, 1987 Associated Technologies Inc.

Suite 300 l

212 South Tryon Street Charlotte, North Carolina 28281 Attention: Mr. Steve Simpson Subj ect:

Rep ort of Laboratory Testing ATI Bituminized Specimens i

ATI Test Plan Issued 8/5/86 l

Section 4.0 - Compressive Strength 5

l Associated Technologies, Inc.

Charlotte, North Carolina LAW Job No. CHG 5219 Gentiemen:

As authorized by your acceptance of our Proposal No. 234M6, Law Engineering has completed laboratory testing on six bituminized specimens subnitted to us by J

Mr. Steve Simpson, Compressive strength testing was performed on specimens l

after biodegradation testing was completed by others.

Testing war. performed according tc Section 8.0 of ASTM D 1074, " Standard Test Method f or Compressive Strength of L uminous Mixtures".

The results of our laboratory testing are tabulated on the attached " Summary of Laboratory Testing" sheets.

If you have any questions concerning this report, or if we may be of further l

l assistance, please contact this of fice.

'l i

Very truly yours, LAW ENGI1EERING 4

Michael 0. Hamlett, C. E. T.

f Senior EngineerigTechnician C

Robert E.

Smith, J

, P. E.

Chief Engineer MOH:RES:j k Attachments

sn

SUMMARY

OF LABOPATORY TESTII:0 Associated Technologies Inc.

Charlotte, North Carolina A.T.I. Test Plan Issued August 5,1986 LAW Job No. CHG 5219 Section 4.0 Specimen Dimensions After Biodegradation Testing Specimen Material Average Average Weight

._ Numbe r Type Diameter (in)

' Height (in)

(gms) 30 Bead Resin 2.195 2.292 146.5 31 Bead Resin 2.189 2.425 153.3 32 Bead Resin 2.186 2.565 164.3 36 Bead Resin 2.180 2.287 141.4 37 Bead Resin 2.179 2.668 163.6 38 Bead Resin 2.187 2.199 135.9 4

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SUMMARY

OF LABORATORY TESTING AssoEiated Technologies Inc.

Charlotte, North Carolina i

A.T.I. Test Plan Issued August 5,1986 LAW Job No. CRG 5219 Section 4.0 Compressive Strength After Biodegradation Testing Compressive Lead (psi)

Deflection Specimen Numbers (inche s )

30 31 32 36 37' 38 l

0 0

0 0

0 0

0 i

0.05 202.5 1 65.9 202.7 189.3 206.3 213.8 0.10 323.3 304.7 357.7 393.9 344.8 413.3 1

0.15 388.6 393.8 462.1 534.5 420.9 582.5 0.20 414.1_

433.7._

485.6 568.8 53 0.6 7675.4/

0.25 L417.11 /445.El /:490.91 f544.4] / 559.5/

682.2 0.30 405.1 438.3 480.3 482.1 479.6 615.7 0.35 384.1 418.6 456.8 395.4 392.0 482.8 0.40 35 2.6 389.2 420.5 311.0 320.5 384.6 0.45 3 15.1 355.3 380.4 263.9 176.6 328.7 d

0.50 286.5 324.4 340.3 237.2 15 2.2 300.7 0.55 268.5 295.7 310.1 225.1 141.6 275.8 0.60 255.0 27 7.6 291.2 220.5 13 1.7 259.9 0.65 247.5 267.8 276.1 2 17.5 121.0 249.3 0.70 240.8 264.0 260.2 215.9 114.2 241.8 0.75 240.8 260.2 251.9 213.7 1 08. 9 235.0 0.80 241.5 258.0 248.1 211.4 104.3 231.2 0.85 243.8 258.0 245.8 2 05.3 101.2 230.4 0.90 243.0 262.5 243.5 197.7 99.0 231.2 0.95 244.5 265.5 242.8 191.6 98.2 234.2 1.00 249.0 267.0 245.8 18 8.6 96.7 239.5 NOTES:

1. Loading Rate: 0.16 inches per minute
2. Conditioning Temperature: 5 50F.
3. Compressive load calculations based on original average diameters.

p LM ENGNEERING TESTNG CCMRWf

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LAW ENGINEEMNG l

GE0 TECHNICAL ENVIRONMENTAL April 27, 19 87

$0"$[ANs' ""

"' t 3ut Associated Technologies. Inc.

Suit e 300 l

212 South Tryon Street l

Charlotte. North Carolina 28281 Attention:. f r. Steve Simpson Subj ect:

1.eport of Laboratory Tes ting ATI Bitu=inized Specimens JGC/ Virginia Power Pilot Plant Test Associated Technologies. Inc.

Charlotte. North Carolina LAW Job No. CHG 5 219 Gentleme n:

-As-suthorized by your. ac ceptance 'of our Proposal No. 234M6 and your letter ~ ~ ~ ~ ~ ~ ~

dat ed April 7, 1987. Law Engineering has completed requested laboratory testing on bituminized specimens submit ted to our 2 aboratory by Mr. St eve Simp s on o n April 7 19 87.

Request ed tes ting was performed according t o the appropriat e sections of the following test s tandards:

. ASTM D 5 "atandard Test Method for Penetration of Bituminous Materials".

. ASTM D 2726. " Standard Test Method for Bulk Specific Gravity and Density of Compacted Bituminous Mixtures Using Saturated Surface-Dry Specimens".

ASTM D 1074

" Standard Test Method for Compressive Strength of Bituminous Mixtur es".

ASTM D 3 6. " Standard Test Method for Sof t ening Point of Bitumen (Ring-And-E s11 Apparatus)".

ASTM D 2172 " Standard Test Methods for Quantit ative Extraction of Bitumen f rom Bituninous Paving Mixtures".

The result s of our laboratory t esting are tioulated on the attached " Summary.

of Laboratory Testing" sheets.

=-

P.O. BOX 11297 CHARLOTTE. NC 28220 591 MINUTE LANE CHARLOTTE. NC 2B217 704 523 2022 L________-_-__--________-_-____-_--------__--_-_-

1 Associated Technologies Inc.

l LAW Job No. CHG 5219 I

April 27.19 87 f

~2-

\\

2 If you have any ques tions conceming this report, or if we may be of further I

assistance, please contact this office.

Vezy truly yours.

LAW ENGINEERING Michael 0. Hamle tt, C. E. T.

j Principal Engineering Technician j

i Robert E. Smith, Jr.,

Chief Engineer 4

MOH:RES:jk At t achme nts 4

l LM ENGINEERNG TESTNG CO# ANT I

1

1 4

i SLHMARY OF LABORATORY TESTING i

Associated Technologies Inc.

Charlotte. North Caroline JGC/ Virginia Power Pilot Plant Test LAW Job No. CHG 5 219 Den sity Tes ting ASTM D 2726 i

Specimen Material pesigna tion Typ e Density (per) 052 Powder Resin 78.2 053 Powder Resin 78.2 055 Powder Resin 78.0 l

060 Bead Resin 75.2 061 Bead Resin 74.3 062 Bead Resin 75.8 l

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SLMMARY OF LA30RATORf TESTING Associated Technologies Inc.

Charlotte, North Carolina JGC/ Virginia Power Pilot Plant Test LAW Job No.' CHG 5 219 Compres sive Strength ASTM D 1071 Compres sive Load (psi)

D eflection Specimen Designation (in ches) 052 053 055 060

061, 062 0

0 0

0 0

0 0

0.05 14.0 12.1 12.1 9.3 13.4 11.5 0.10 30.0 25.0 26.1 19.1 24.1 24.6 0.15 49.2 36.8 38.5 27.3 34.3 36.1 0.20 63.8 46.7 48.3 34.7 44.5 46.7 0.25 74.8 55.0 56.6 41.0 48.3 55.5 0.30 83.3 61.9 63.7 46.4 53.6 62.8 0.35 90.7 68.7 70.9 51 9 58.2 68.1 0.40 l_96.8 75.3 76.4 56.0 62.0 72.1 I

s.

0.45 102.3 80.6 81.0 60.6~

65.4 75.6 0.50 107.2 84.4 84.9 65.0 68.4 78.2 O.55 111.4 87.7 87.3 68.3 71.1 80.1 l

0.60 114.7 91.0 90.6 71.0 73.5 81.7 f

0.65 117.4 93.8 93.4 73.2 75.1 83.3 j

0.70 120.4 96.0 95.9 75.1 76.4 84.7 0.75 123.2 97.6 97.8 76.8 77.8 85.5 0.80 125.9 99.5 99.2 78.1 79.1 86.8 0.85 1 27. 8 101.7 101.1 79.2 80.5 88.1 0.90 129.8 103.9 103.3 80.9 81.5 89,5 I

0.95 132.0 105.6 105.7 81.9 82.6 90.8 l

1.00 134.4 107.2 107.4 83.3 83.4 92.1 1

2 NOTES:

A. Loading Rate: 0.16 inches per minut e.

B. Conditioning Temperature: 55 F.

C. Compres cive lo ad calc ula tions based on original specimen diame ter.

J D. No free water was found in specimen centers after testing.

t LM ENGINEERING TESTWG CCNPANY

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. [* Y L.aW ENO6 NEEM 9NO TEST 1MO CO8u9PIMfY go.onocevuca, artisemisruni4 cxmswucoce muista.s exmmsissus 5016A8NVET LANE P.o. Box 11297 = CMARLOTTE. NORTH CAROL *NA 28220 (704)62 1 2022 November 30, 1981.

Associated Technologys, Inc.

212 South Tryon Street Charlotte, North Carolina 28281 Attention:

Mr. Steve Simpson

Subject:

Laboratory Testing Bituminuous Mixtures Associated Technologys, Inc.

Charlotte, North Carolina LETCo. Job No. CEG 5219

- -.. Gentlemen:

-'-' ' - ~ ~ ~ ~

l As requested, Law Engineering Testing Company has completed compressive I

strength testing on two samples delivered to our office.

l These samples were tested by a method sim.ilar to that described in ASTM D,

  • Compressive Strength of Bitu=inous Mixtures".

It should le noted

1074, however, that the samples ver.e_ cooled to a temperature of 550 '

2 and T

that the sample's original test. height was not equal to the diameter as l

l specified. It should be further noted thai: -these sa:ples have no true failure point at which the load does not continue'to increase.

Inis it"due at least in part to the plastic nature of these samples.

The specific gravity of each sa=ple was also checked and from this the unit i

veight after compression was calculated.

The results of these tests are shown on the attached " Report of Compressive Strength bf Bituminous Mixtures *.

If you have any questions concerning thn report or if we can be further assistance, please contact this office.

1 Respectfully submitted, LAW INGINE m NG CDMFANY j

l Allen J. Ighes C.I.T.

j y

Laborato;d SupeYvisor l

%2'

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REPORT OF COMPRESSIVE STRENGTH OF BITUMItGOUS MIXTURES Associated Technologys, Inc.

Charlotte, North Carolina LETCo. Job No. CHG 5219 November 30, 1984 Sample Type: Type I, Bit. 100%

Date Tested:

11/27/84 Original Diameter 2.86 In.

Area:

6.42 Sq. In.

Original Height:

2.33 In, Specific Gravity:

1.03 Unit Weight:

64.3 Lb/cu.ft.

Deflection [lud Total Load (Lbs.)

Compressive Strength (Psi)*

.05 20.1 3.1

.10 42.0 6.5

.15 69.5 10.8

.20 94.6 M

.30 138.4 21.6

.40 179.7 27.9 g-

.50 ~

2" S.1 34.0 v

.60 254.2 39.6

.70 290.0 45.2

.80 324.4 50.5

.90 358.4 55.8 1.00 394.0 61.4

  • Compressive strengths were calculated based on the original areas.

The

. specimen's actual area increased as the load increased.

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