ML20214E464

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Forwards Test Results & Summary Re Atmospheric Cleanup Filter Units Per Requirements of Table 5-1 of ANSI N509-1976 & N509-1980 & Reg Guides 1.52 & 1.140.Methyl Iodine Penetration Requirement Exceeded
ML20214E464
Person / Time
Site: Braidwood  Constellation icon.png
Issue date: 11/17/1986
From: Hunsader S
COMMONWEALTH EDISON CO.
To: Harold Denton
Office of Nuclear Reactor Regulation
References
RTR-REGGD-01.052, RTR-REGGD-01.140, RTR-REGGD-1.052, RTR-REGGD-1.140 2401K, NUDOCS 8611240449
Download: ML20214E464 (55)
v • d • e


Text

W

/y One First Nabonal Plaza. Chicago, Illinois m*

/ Address Rept/ L3 Post Omco Box 767 D Chicago, hiinois 60690 0767 November 17, 1986 Mr. Harold R. Denton, Director Office of Nuclear Reactor Regulation U.S. Nuclear Regulatory Commission Washington, DC. 20555

Subject:

Braidwood Station - Units 1 & 2 Atmospheric Clean-up Filter Units Regulatory Guides 1.52 and 1.140 NRC Docket Nos. 50-456 and 50-457

Reference:

(a)

October 21, 1986 A.D. Miosi letter to H.R. Denton In reference (a), Commonwealth Edison provided a commitment to test all carbon, furnished prior to 1985 as part of the original specification for atmospheric clean-up filter units, to the requirements of Table 5-1 of ANSI N509-1976.

Reference (a) also provided a commitment to test all replacement carbon or original carbon furnished in 1985 or later to the requirements of Table 5-1 of ANSI N509-1980 with the exception that the laboratory test for methyl iodine penetration at 300C, 95% relative humidity will be less than 1%.

Table 5-1 of ANSI N509-1976 requires methyl iodine penetration to be less than 1% and ANSI N509-1980 requires methyl iodine penetration to be less than 3%.

The plant Technical Specifications require methyl iodine penetration to be less than 1%.

Attachment A provides the test results which were discussed with representatives of your staff on November 13, 1986.

As shown, the methyl iodine penetration at 300C, 95% RH exceeds 1% in nine (9) of the ten (10) carbon batch samples tested.

Though this requirement has not been met, use of the charcoal is recommended j

based upon the following:

1.

The ANSI N509-1980 requirements have been met.

All of the l

carbon batch samples at 300C, 95% RH meet the 3% methyl I

iodine penetration requirement as stated in this standard.

2.

The Carbon is tested for greater than 99% efficiency to i

receive 95% efficiency credit in the SER.

The Carbon successfully tested for greater than 97% efficiency j

provides an adequate efficiency and margin to earn 95%

credit.

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i In addition, included as Attachment B is a letter from FARR Co. summarizing the test results for the carbon that they have available to fill the last six (6) carbon trays and twenty (20) test canisters under the original Commonwealth Edison purchase order for the Atmospheric Clean-up Filter Units (P.O. 213830).

The material is ANCO Engineers Products Group, Inc. (not North American Carbon, Type G615) and is slightly out of ASTM D4069 requirements for one (1) test value.

The material test data for particle size on the #16 sieve does not comply with the specification requirements.

However, the efficiency of 99.78% is superior and it is not expected that the smaller quantity of carbon on the smaller mesh size will have a significant effect on the efficiency.

As discussed on November 13, 1986, your review and concurrence to use these materials is requested.

If there are any questions, please direct them to this office.

f /

--e w Q S. C. Hunsader Nuclear Licensing Administrator

/klj cc:

J.

Stevens 240lK 9 '

=-

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ATTACHMENT A Summary of Methyl Iodine Penetration Tested at 300C,95% RH Batch 2 2.190% penetration 97.810% efficiency Batch 3 1.962% penetration 98.038% efficiency i

Batch 6 1.484% penetration 98.516% efficiency Batch 7 1.555% penetration 98.445% efficiency Batch 8 1.258% penetration 98.742% efficiency Batch 9 0.986% penetration 99.014% efficiency Batch 10 1.473% penetration 98.527% efficiency Batch 11 1.404% penetration 98.596% efficiency Batch 12 1.279% penetration 98.721% efficiency Batch 14 1.688% penetration 98.312% efficiency Specific test results are presented in the attached report, pages 1-45.

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R A ++a c4 men t A O

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Services, Inc.

PO box 29151 COLUMBUS OHIC 43029 10D1HE-131 REMOVAL EFFICIENCY DETERMINATION OF ADSORBENT SAMPLES PERFORHED ON SAMPLES:

BATCH 2 BATCH 3 BATCH 3 BATCH 6 BATCH 7 PATCH G BATCH 9 BATCH 10 BATCH 11 BA1CH 12 DATCH 14 UATE:

2 OCT 1986 PERFORMED FOR:

COMMONWEALTH EDISON COMPANY, BRAIDWOOD STATION R.R.

41, BOX B1 P.O.

NO. 301798 DISTRIBUTION:

EXTERNAL (4) JOE DEARBACH l

INT ERNAL (1) PROJECT t8 ASTER FILE (1) I-LAB FILE (1) QA FILE NUCON'13CE74Y/01 etECISTERED TRADEMARK OF NltCLEAR CONSULTING SERVICES, INC.

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NUCUN 13CE74'?/01 :

THESE REPOR~I SHEETS CONTAIN THE IODINE. FISSION PRODUCT TEST DATO UDTAINED FROM ADSORiiENT SAMPLES TESTED BY NUCUN.

COUNTING WAS PERFORHED AT 0.364 MEV GollHA LEVEL, IN A 4.0" THALL 1UM ACTIVATED SODIUM IODIDE WELL CRYST AL.

CALIBRATION

()F lilE CullNi1NG CRYSTAL HAS BEEN PERFORMED BY THE USE OF AN NDS 1R ACEAliLE 131-1 STANDARD.

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t HUCON 13CE747/01 TEST REPOR'It HETHYL IODIDE DATE PERFORMED: 29 SEP 1986 SAMPLE:

DATCH 2 SUMMAR Y 0F RESULTS

===============n========r::r

BED No.

RETENTION PENETRA110N STD. DEV.

b_

1 97.010%

2.190%

.0293%

THE RESULTS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OUR BEST KNOWLEDGE.

=

PERFORMED BY 4

V MARK P. KING J NUCLEAR CONSULTING SERVICES, INC.

APPROVED BY A/A971dAA W.

PETER FREEMAN NUCLEAR CONSULTING SERVICES, INC.

1 NUCON 13CE749/01 TEST REPORT: METHYL IUDIDE DATE PERFORMED: 29 SEP 1986 CLIENT:

COMMONWEALTH EDISON COMPANY, BRAIDWOOD STATION R.R.

11, BOX 81 SAMPLE:

BATCH 2 P.O.

NO.:

301790 TEST COND11 IONS:

BED DEPTH 5.08 CM. ( 2.00 IN.)

BED DIAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRE-LOADING 30.0 D

( 86.0

'F )

LOADING 30.0

'C

( 86.0 'F)

POST-LOADING 30.0 D

( 86.0 'F)

RELAllVE HUMIDI'IY 95.0 %

FACE VELOClTY 20.32 CH./SEC (40.0 FPM)

CHALLENGE AGENT CONCENTRATION METHYL IODIDE 1.75 MG./CU.M.

TEST TIMES PRE-LUADING

16. HRS.

LOADING

2. 0 HRS.

POST-LOADING 4.0 HRS.

CAPTURED R ADI0 ACTIVITY

.12 MICR0 CURIES PRESSURE 101.30 kPA.

( 1.00 ATM.)

I

A?

NUCON 13CE749/01 COUNTING DAIA FOR SAMPLE BATCH 2 AIR COUNT DATA

  • PRE-TEST

541.1 STD DEV=

5.4

  • POST-TEST

541.1 S'I D DEV=

5.4 TB1 COUNT DATA

  • PRE-TEST

628.9 STD DEV=

6.3 CPM-AIR =

87.8 STD DEV=

8.3

  • POST-TEST

128,210.0 STD DEV=

410.0 CPM-AIR =

127,670.0 STD DEV=

410.0

  • NET

127,500.0 STD DEV=

410.0 GB1 COUNT DATA

  • PRE-TEST
  • CPHu 613.1 STD DEV=

6.1 CPM-AIR' 72.0 STD DEV=

8.2 KPOST-TEST

3,472.0 STD DEV=

35.0 CPM-AIR =

2,931.0 STD DEV=

35.0 i

  • NET

2,859.0 STD DEV=

36.0 l

I i

1 i

,___m,,

9 NUCON 13CE749/01 COUNTING DATA FOR SAMPLE BATCH 2 i

CD2 COUNT DATA

  • PRE-TEST
  • C P M::-

613.1 STD DEV=

6.1 CPM-AIR =

72.0 STD DEV=

8.2 t

  • POST-TEST
  • CPMe 610.1 STD DEV=

6.1 CPM-AIR =

69.0 STD DEV=

8.2 i

KNET*

NET CPM =

-2.0 STD DEV:=

12.0 i

jo NUCON 13CE749/01 TEST REPORT: METHYL IODIDE DATE PERFORMED: 26 SEP 1996 SAMPLE:

BATCH 3 SUMMAR Y OF RESULTS

=======================

BED No.

RETENTION PENETRATION STD. DEV.

1 98.038%

1.962%

.0254%

THE RESUL1S ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHN10UES AND ACCORDING TO OUR BEST KNOWLEDGE.

PERFORMED BY k

MARK P. KING _

G NUCLEAR CONSULTING SERVICES, INC.

APPROVED BY Mh W.

PETER FREEMAN NUCLEAR CONSULTING SERVICES, INC.

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NUCON 13CE749/01 TEST REPORT: METHYL IUDIDE DATE PERFORMED: 26 SEP 1986 CLIENT:

COMMONWEALTH EDISON COMPANY, BRAIDWOOD STATION R.R.

11, BOX 81 SAMPLE:

BATCH 3 P.O.

NO.:

301798 TEST CONDITIONS:

BED DEPTH 5.00 CM. ( 2.00 IN.)

DED DIAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRE-LOADING 30.0 h

( 86.0

'F )

LOADING 30.0

'C

( 86.0 'F)

POST-LOADING 30.0 D

( 86.0 'F)

RELATIVE HUMIDITY 95.0 %

FACE VELOCITY 20.32 CM./SEC (40.0 FPM)

+

CHALLENGE AGE'4T CONCENTR ATION i' ETHYL 10DIDE 1.75 nG./CU.M.

l TEST TIMES PRE-LOADING

16. HRS.

LOADING 2.0 HRS.

POST-LOADING 4.0 HRS.

CAPTURED RADI0 ACTIVITY

.15 MICR0 CURIES l

PRESSURE 101.30 kPA.

( 1.00 ATM.)

P I

(

[L NUCON 13CE749/01 COUNTING DATA FOR SAMPLE BATCH 3 AIR COUN1 DATA

  • PRE-TEST

541.1 STD DEV=

5.4

  • POST-TEST

541.1 STD DEV=

5.4 TB1 COUNT DATA

  • PRE-TEST

589.6 STD DEV=

5.9 CPM-AIR =

48.5 STD DEV=

8.0

  • POST-TEST

158,730.0 STD DEV=

500.0 CPM-AIR =

158,190.0 STD DEV=

500.0

  • NET

158,140.0 STD-DEV=

500.0 GB1 COUNT DATA

  • PRE-TEST
  • l l

CPM =

613.1 STD DEV=

6.1 CPM-AIR =

72.0 STD DEV=

8.2

  • POST-TEST

3,002.0 STD DEV=

38.0 CPM-AlR=

3,261.0 STD DEV=

38.0 l

  • NET

3,189.0 STD DEV=

39.0 l

l I

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l3 NUCON 13CE749/01 COUN11NG DATA FOR SAMPLE BATCH 3 GB2 COUNT DATA

  • PRE-TEST

61 3.1 STD DEV=

6.1 CPM-AIR =

72.0 STD DEV=

8.2

  • POST-TEST
  • 1 CPM-587.9 STD DEV=

5.9 CPM-AIR =

46.8 STD DEV=

8.0

  • NET
  • NET CPH=

-25.0 STD DEV=

11.0 i

f I

i I

- - - - -. ~ - - - - - - - -

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NUCON 13CE749/01 ~

TEST REPOR1: METHYL 10DIDE DATE PERFORMED: 29 SEP 1986 GANPLE:

BATCH 3

SUMMARY

OF RESUL TS

=========

v====n===

BED No.

RETENTION PENETRATION STD. DEV.

1 99.982%

.018%

.0250%

THE RESUL18 ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHN10UES AND ACCORDING TO OUR BEST KNOWLEDGE.

PERFURMED BY k

MARK P. I(ING (INUCLEARCONSULTINGGERVICES, INC.

APPROVED BY hM dW7 W.

PETER FREEMAN NUCLEAR CONSULTING SERVICES, IAC.

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NUCON 13CE749/01 TEST REPORT: ME1HYL 10DIDE DATE PERFORMED: 29 SEP 1986 CLIENT:

COMMONWEALTH EDISON COMPANY, BRAIDWOOD STATION R.R.

11, BOX 81 BAMPLE:

BATCH 3 P.O.

NO.:

301798 TES1 COND3TIONS:

DED DEPTH 5.08 CM. ( 2.00 IN.)

BED DloMETER 5.08 CH. ( 2.00 IN.)

TEMPERATURES PRE-LOADING 130.0

'C (266.0 'F)

LOADING 130.0

'C (266.0 'F)

POSI-LOADING 130.0 D (266.0

'F )

RELATIVE HUMID 1TY 95.0 %

FACE VELOCITY 20.32 CM./SEC (40.0 FPM)

CHALLENGE AGENT CONCENTRATION METHYL IODIDE 1.70 NG./CU.M.

TEST TIMES PRE-LOADING 2.0 HRS.

l l

LOADING 1.0 HRS.

POSI-LOADING 4.0 HRS.

L

-CAPTURED RADIDACTIVITY

.06 MICR0 CURIES l

PRESSURE 395.07 kPA.

( 3.90 ATM.)

1 l

I il'

~

/s NUCON 13CE749/01 COUN1]NG DATA FOR SAMPLE BATCH 3 AIR COUNT DATA

  • PRE-TEST

528.0 STD DEV=

5.3

  • P OS1 -TEST
  • CPH=

528.0 STD DEV=

5.3 TB1 COUNT DATA

  • PRE-TEST

595.9 STD DEV=

6.0 CPM-A1R=

68.0 STD DEV=

0.0

  • POST-TEST

65,790.0 STD DEV=

210.0 CPM-AIR =

65,260.0 STD DEV=

210.0

  • NET

65,190.0 S1D DEV=

210.0 GB1 COUNT DATA

  • PRE-TEST

605.3 STD DEV=

6.1 CPM-AIR =

77.3 STD DEV=

8.0

  • POST-TEST

633.7 STD DEV=

6.3 CPM-A1R=

105.7 STD DEV=

8.2

  • NET

28.0 STD DEV=

12.0

l1 l

NUCON 13CE749/01 -COUNTING DATA FOR SAMPLE BATCH 3 GB2 COutlT Dolo

  • PRE-TEST

605.3 STD DEV=

6.1 CPM-AIRE 77.3 STD DEV=

8.0 FPOS1-TEST

588.9 STD DEV=

5.9 CPM-AIR =

60.9 STD DEV=

7.9

  • NET
  • NET CPH=

-16.O STD DEV=

11.0 1

e 1

i i

l I

l c

11 NUCON 13CE749/01 TEST REPORT: METHYL IDDIDE DATE PERFORMED: 19 SEP 1986 SAMPLE:

BATCH 6 SUMMAR Y OF RESULTS

_=e=======_======r.===============

BED No.

RElENTION PENETRATION STD. DEV.

I 98.516%

1.484%

.0192%

THE RESULTS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO QUR BEST KNOWLEDGE.

PERFURilED BY A

MARK P.

l(ING NUCLEAR CONSULTING SERVICES, INC.

APPROVED BY

_/M AOMA W.

PETER FREEHAN NUCLEAR CONSULTING SERVICES, INC.

l i

11 NUCUN 13CE749/01 TEST REPORT: METHYL IODIDE DATE PERFORMED: 19 SEP 1986 CLIENT:

COMMONWEAL 1H EDISON COMPANY, BRAIDWOOD STATION R.R.

41, BOX 81 SAMPLE:

BATCH 6 P.O.

NO.:

301798 TEST COND11 IONS:

BED DEPTH 5.08 CM. ( 2.00 IN.)

BED DIAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRE-LOADING 30.0 t

( 86.0 Y)

LOADING 30.0 \\;

( 86.0

'F )

PUST-LOADING 30.0 t

( 86.0

'F )

RELATIVE HUMIDITY 95.0 %

FACE VELOCITY 20.32 CM./SEC (40.0 FPM)

CHALLENGE AGENT CONCENTRATION METHYL IODIDE 1.75 nG./CU.M.

TEST TIMES PRE-LOADING

16. HRS.

LOADJNG

2. 0 HRS.

POST-LOADING 4.0 HRS.

CAPTURED RADI0 ACTIVITY

.24 HICROCURIES PRESSURE 101.30 kPA.

( 1.00 ATM.)

ZO NUCON 13CE749/01 i COUN'IING DoIA FOR SAMPLE BATCH 6 hIR COUNT DATA

  • PRE-TEST

563.1 STD DEV=

5.6

  • POST-TEST

563.1 STD DEV.~2 5.6 TB1 COUNT DATA

  • PRE-TEST

693.0 91D DEV=

6.9 CPM-AIR =

129.9 STD DEV=

8.9 nPOST-TEST

243,900.0 STD DEV=

770.0 CPM-A1R=

243,340.0 STD DEV=

770.0

  • NET
  • NET CPH=

243,210.0 STD DEV=

770.0 CD1 COUNT DATA

  • PRE-TEST

688.2 STD DEV=

6.9 CPM-AIR =

125.2 STD DEV=

0.9

  • POST-TEST

4,386.0 STD DEV=

44.0 CPM-AIR =

3,823.0 STD DEV=

44.0

  • NET

3,698.0 STD DEV=

45.0

J, \\

NUCON 13CE749/01 COUN11NG DATA FOR SAMPLE BATCH 6 GD2 COUNT DATA

  • PRE-TEST

688.2 STD DEV=

6.9 CPM-AIRE 125.2 STD DEV=

8.9

  • POST-TEST

654.0 STD DEV=

6.5 CPM-AIR =

91.0 STD DEV=

8.6

  • NET
  • NET r:PM=

-34.O STD DEV=

12.0 a

i

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HUCON 13CE749/01 TES1 REPOR1: METHYL 10D1DE DATE PERFORMED: 17 SEP 1986 SAMPLE:

BATCH 7

SUMMARY

0F RESULTS n==================r.==============_

BED No.

RETENTION PENETRATION STD. DEV.

1 98.445%

1.555%

.0174%

4 THE RESUL15 ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL 1

TECHNIQUES AND ACCORDING TO OUR BEST KNOWLEDGE.

PERFURMED BY k

] NUCLEAR CONSULTING SERVICES, MARK P.

KING INC.

APPROVED BY

/ M I7 M W.

PETER FREEMAN ~

NUCLEAR CONSULTING SERVICES, INC.

W

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NUCON 13CE749/01 TEST REPORT: HETHYL IDDIDE DATE PERFORMED: 17 SEP 1986 CLIENT:

COMMUNWEAL TH EDISDN COMPANY, BR AIDWOOD STATION R.R.

11, BOX 81 SAMPLE:

BATCH 7 P.O.

NO.:

301798 TEST CONDril0NS:

BED DEPTH 5.08 CM. ( 2. 00 IN. )

BED DIAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRE-LOADING 30.0 h

( 86.0

'F )

LOADING 30.0 h

( 86.0 'F)

POST-LOADING 30.0

'C

( 86.0 'F)

RELATIVE HUMID 1TY

'75.0 %

FACE VELOCITY 20.32 CM./SEC (40.0 FPH)

CHALLENGE AGENT CONCENTRATION METHYL IODIDE 1.75 MG./CU.M.

TEST TIMES PRE-LOADING

16. HRS.

LOADING 2.0 HRS.

POSI-L.0ADING 4.0 HRS.

CAPTURED RADI0 ACTIVITY

.48 MICR0 CURIES PRESSURE 101.30 kPA.

( 1.00 ATH.)

2A NUCON 13CE749/01 COUNIING DATA FUR SAMPLE BATCH 7 AIR COUNI DATA

  • PRE-TEST
  • LPM-549.5 STD DEV=

5.5

  • POST-TEST

549.5 STD DEV=

5.5 TB1 COUNT DATA

  • PRE-TEST

614.6 STD DEV=

6.1 CPM-AIR =

65.2 STD DEV=

8.2

  • POST-TEST

500,000.0 STD DEV=

1,600.0 CPM-AIR =

499,500.0 STD DEV=

1,600.0

  • NET
  • NET CPH=

499,400.0 STD DEV=

1,600.0 GB1 COUNT DATA

  • PRE-TEST

616.1 STD DEV=

6.2 CPM-A1R-66.7 STD DEV=

G.3

  • POST-TEST

8,475.0 STD DEV=

85.0 CPM-AlR=

7,926.0 STD DEV=

85.0

  • NET

7,859.0 STD DEV=

85.0 i

l

\\

l l

i

2f NUCON 13CE749/01.

COUNTING DAlo FOR SAMPLE BATCH 7 GD2 COUN1 Dolo

  • PRE-TEST
  • CPH=

616.1 STD DEV=

6.2 CPM-AIR =

66.7 STD DEV=

8.3

  • POST-TEST

643.1 STD DEV-6.4 CPM-A1R=

93.6 STD DEV=

8.5

  • NET

27.0 STD DEV=

12.0 I

i 1

i i

1 i

. - - _ _ _ _. ~ _ _ _ _.

26 NUCON 13CE749/01 TEST REPORT: METHYL IODIDE DATE PERFOR hki,: 16 SEP 1986 SAMPLE:

Bo1CH B

SUMMARY

0F RESULTS

= = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = =

BED No.

RETENTION PENE1RAlION STD. DEV.

1 98.742%

1.258%

.0151%

9 THE RESUL1S ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHN10UES AND ACCORDING TO QUR BEST KNOWLEDGE.

PERFORHED BY _

w)

NUCLEAR CONSULTING SERVICES, INC.

MARK P. KING APPROVED LiY me W.

PETElf FREEMAN

' NUCLEAR CONSULTING SERVICES, INC.

27 NUCON 13CE749/01 TEST REPORT: METHYL 10DIDE DATE PERFORMED: 16 SEP 1986 CLIENI:

COMMONWEALTH EI)1 SON COMP ANY, BR AIDWOOD STATION R.R.

41, BOX 81 ti AMPLE :

BAICH 8 P.O.

NO.:

301798 TEST COND]TIONS:

DED DEPTH 5.08 CM. ( 2.00 IN.)

BED DIAMElER 5.08 CM. ( 2.00 IN.)

TEMPER A TUR ES PRE-LOADING 30.0 h

( 86.0

'F )

LOADING 30.0

'C

( 86.0 'F)

POST-LOADING 30.0 I:

( B6.0

'F )

RELATIVE HUNID11Y 90.0 %

FACE VELOCITY 20.32 CM./SEC (40. 0 FPM)

CHAL LENGli AGEllT CONCENTR ATION METHYL IODIDE 1.75 MG./CU.M.

TEST 11MES PRE-LOADING

16. HRS.

LO AI)1NG 2.0 HRS.

POST-LOADING 4.0 HRS.

CAP ~ LURED RADIDACTIVITY

.36 HICROCURIES PRESSURE 101.30 kPA.

( 1.00 ATM.)

i

ZY NUCUN 13CE749/01 COUNTING DA1A FOR SAMPLE BATCH 8 AIR COUNT DATA

  • PRE-TEST
  • CPMn 544.7 STD DEU=

5.4

  • POST-TEST

544.7 STD DEV=

5.4 TB1 COUNT DATA

  • PRE-TEST
  • CPMn 619.6 STD DEV=

6.2 CPM-AIR =

74.9 STD DEV=

8.2

  • POST-TEST
  • CPMm 370,400.0 STD DEV=

1,200.0 CPM-A1Hn 369,900.0 STD DEV=

1,200.0

  • NET

369,000.0 STD DEV=

1,200.0 GB1 COUNT DATA

  • PRE-TEST
  • CPH=

613.9 STD DEV=

6.1 CPM-A1Rn 69.2 STD DEV=

8.2 MPOST-TEST

5,348.0 STD DEV=

53.0 CPM-A1R=

4,803.0 STD DEV=

53.0

  • NET
  • NET CPMn 4,734.0 STD DEV=

54.0

,,--,,,---,,,.,-w--

27 NUCON 13CE749/01

-2G-COUNTING DATA FOR SAMPLE BATCH 8 GD2 COUN'I DATA

  • PRE-TEST

613.9 STD DEV=

6.1 CPM-AIR =

69.2 STD DEV=

8.2

  • POST-TEST
  • C P Mr-591.0 STD DEV=

5.9 CPM-AIR =

46.4 STD DEV=

0.0

  • NET
  • HET CPMr-

-22.0 STD DEV=

11.0

30 NUCON 13CE749/01 TEST REPORT: HE1HYL IODIDE DATE PERFORMED: 10 SEP 1986 SAMPLE:

BATCH 9

SUMMARY

OF R ESULTS

= = = =: n n = = = = = = = = = = = = = r: = n n u = = = = = = = = =

DED No.

RETENTION PENETRATION STD. DEV.

1 99.014%

.986%

.0159%

THE RESULTS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHN1 QUES AND ACCORDING TO OUR BEST KNOWLEDGE.

PERFORNED BY l

] NUCLEAR CONSULTING SERVICES, MARK P. KING INC.

APPROVED BY

//A% >

W.

PETER FREEHAl4 NUCLEAR CONSULTING SERVICES, INC.

l l

31 NUCON 13CE749/01 TEST REPORT: METHYL IODIDE DATE PERFORMED 10 SEP 1906 CLIENT:

COMMUNWEALTH EDISON COMPANY, BRAIDWOOD STATION R.R.

11, BOX B1 SAMPLE:

BAICH 9 P.O.

NO.:

301798 TEST CONDITIONS:

DED DEPTH 5.08 CM. ( 2.00 IN.)

BED DIAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRE-LOADING 30.O h

( 86.0

'F )

LOADING 30.0

'C

( 86.0 'F)

POS1-LOADING 30.0 D

( 86.0

'F )

RELATIVE HUMIDITY 95.0 %

FACE VELOC1TY 20.32 CH./SEC (40.0 FPM)

CHALLENGE AGENT CONCENTRATION METHYL 10D1DE 1.75 nG./CU.M.

TEST TIMES P R E-LO ADING

16. HRS.

LOADING 2.0 HRS.

POST-LOADING 4.0 HRS.

CAP 1URED R ADI0 ACTIVITY

.17 HICROCURIES 4

PRESSURE 101.30 kPA.

( 1.00 ATM.)

i

--,-.,,~

])-

NUCON 13CE749/01 COUN' LING DA1A FOR SAMPLE BATCH 9 AIR COUN'l DATA

  • PRE-TEST

519.5 STD DEV=

5.2

  • POST-TEST

519.5 S~ID DEV=

5.2 TD1 COUNT DATA

  • PRE-TEST

598.4 STD DEV=

6.0 CPM-AlR=

79.0 STD DEV=

7.9

  • POST-TEST

178,570.0 STD DEV=

560.0 CPM-AIRa 178,000.0 STD DEV=

560.0

.* NET

177,970.0 STD DEV=

560.0 GB1 COUN1 DA'IA

  • PRE-TEST
  • CPM-594.2 STD DEV=

0.9 CPM-AIR-74.7 STD DEV=

7.9

  • POST-TEST

2,381.0 STD DEV=

24.0 CPM-AlR=

1,862.0 STD DEV=

25.0 l

  • NET
  • NET CPM-1,787.0 STD DEV=

26.0 y

-_..m,--

D NUCON 13CE749/01 COUNTING DAlA FOR SAMPLE BATCH 9 GB2 COUNI DATA

  • PRE-TEST

594.2 STD DEV=

5.9 CPM-A1R=

74.7 STD DEV=

7.9

  • POST-TEST

500.O STD DEV=

0.8 CP M-A1 H r-60.6 STD DEV=

7.8

  • NET

-14.O STD DEV=

11.0 i

t 4

i t

3+

NUCON 13CE749/01 TESI R EP OR ~l : HElHYL IODIDE DATE PERFORHED: 16 SEP 1986 SAMPLE:

BATCH 10 SUMNARY 0F RESULTS

:=======em.=======.um:=n=======

BED No.

HElENTION PENETRATION STD. DEV.

1 98.527%

1.473%

.0171%

THE RESULTS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OUR BEST KNOWLEDGE.

PERFURMED BY l

}NUCLEARCONSULTINGSERVICES, MARK P. KING INC.

APPROVED BY M

///>F7h W.

PE!TER FREEHAN NUCLEAR CONSULTING SERVICES, INC.

3f NUCUN 13CE749/01 TES~I REPORT: NETHYL 10DIDE DATE PERFORMED: 16 SEP 1986 CLIENI:

COHHUNWEALTH EDISDN COMPANY, BRAIDWOOD STATION R.R.

11, BOX B1 GAMPLE:

14A'ICH 10 P.0, NO.:

3017Y8 TEST COND1110NS:

DED DEPiH G. 08 CM. ( 2.00 IN.)

DED DIAMEIER 5.00 CM. ( 2.00 IN.)

TEMPENATURES PRE-LOADING 30.0

'C

( 86.0

'F )

LUADING 30.0 h

( 86.0

'F )

POSI-LOADING 30.0 t

( 86.0

'F )

RELA 11VE HUMIDl'IY 95.0 %

FACE VELOC1'IY 20.32 CH./SEC (40.0 FPH)

CHALLENGE ACENT CONCENTRATION METHYL 10D1DE 1.75 nC./CU.M.

TESI' TIMES PRE-LOADING

16. HRS.

LOADING 2.0 HRS.

POST-LOADING 4.0 HRS.

CAP'IURED R AD10ACTIV11Y

.37 HICROCURIES PRESSURE 101.30 kPA.

( 1.00 ATH.)

I

3t NUCON 13Ch749/01 COUNTING DA'I A FOR SAMPLE BATCH 10 AIR COUN1 DATA

  • PRE-TEST
  • CPH=

S28.5 STD DEV=

5.3

  • POST-TEST

528.5 STD DEV=

5.3 TB1 COUNT DATA

  • PRE-TEST

628.1 STD DEV=

6.3 CPM-AIR =

99.6 STD DEVu 8.2

  • POST-TEST
  • CPMu 384,600.0 STD DEV=

1,200.0 CPM-AIR =

384,100.0 STD DEV=

1,200.0

  • NET
  • NET CPH=

384,000.0 STD DEV=

1,200.0 CB1 COUNi' DATA

  • PRE-TEST
  • CPM" 613.9 STD DEVn 6.1 CPM-AIR =

85.3 STD DEV=

0.1

  • POST-TEST

6,329.0 STD DEV=

63.0 CPM-AIR =

5,800.0 STD DEV=

63.0

  • NET

5,715.0 STD DEV=

64.0

31 NUCON 13CE749/01 1 COUNTING DAT A FOR SAMPLE BATCH 10 GB2 COUNT DA'IA

  • PRE-TEST
  • CPM" 613.9 STD DEV=

61 i

CPM-A1H"'

85.3 STD DEV=

s,1 MPOST-TEST

  • CPM" 637.8 STD DEV*

64 CPM-AIR =

111 3 STD DEV" 8.3

  • NET

26.0 STD DEV:$

12.0 I'

[

)

t I

1

36 NUCON 13CE74'7/ 01.

TEST REPORT: METHYL 10DIDE DATE PERFORMED: 22 SEP 1986 S AMPt.E :

liATCH 11

SUMMARY

0F RESULTS

= = am = = = = = n s. = = = = = = = = = nr = n re = = r.. e= = = = = =

BED No.

RETENTION PENETRATION STD. DEV.

1 98.596%

1.404%

.01*/4%

THE RESUL1B ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OUR BEST KNOWLEDGE.

PERFORMED BY MARK P. KING

} NUCLEAR CONSULTING SERVICES, INC.

APPROVED BY MM W. PETER FREEHAN NUCLEAR CONSULTING SERVICES, INC.

.. - _ _ - _ _, - - - _ =.

5 HUCON 13CE749/01 TEST RE.POR'It METHYL IODIDE DATE PERFORHED: 22 SEP 1986 CLIENT:

CullHONWEALTH EDISDN COMPANY, BRAIDWOOD STATION R.R.

41, BOX 81 SAMPLE:

BATCH 11 P.0.

NO.

301798 TES'l CONDITIONS:

DED DEPTH 5.00 CM. ( 2.00 IN.)

DED DlAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRE-LOADING 30.0

'C

( B6.0 'F)

LDADING 30.0

'C

( 86.0 'F)

POS1-LDADING 30.0 h

( 86.0

'F )

RELATIVE HUMIDI1Y 95.0 %

1 FACE VELOC11Y 20.32 CH./SEC (40.0 FPM)

CHALLENGE ACENT CONCENTRATION METHYL 10D1DE 1.75 nG./CU.M.

TESI TIMES PRE-LDADING

16. HRS.

LOADING 2.0 HRS.

POS1-LOADING 4.0 HRS.

CAPluRED RADIUACTIVITY

.25 H3CROCURIES PRESSURE 101.30 kPA.

( 1.00 ATM.)

.~.-

10 NUCUN 13CE749/01 COUNTING DATA FOR SAMPLE BATCH 11 AIR COUNT DAT A

  • PRE-TEST
  • CP M:a 528.5 STD DEV=

5.3

  • POST-TEST

528.5 STD DEV=

5.3 TB1 COUNT DATA

  • PRE-TEST

568.2 STD DEV=

5.7 CPM-AlR -

39.6 STD DEV=

7.8

  • POST-TEST

263,160.0 STD DEV=

030.0 CPM-AlR=

262,630.O STD DEV:=

830.0

  • NET
  • NET CPil=

262,590.0 STD DEV:=

830.0 GB1 COUNT DATA

  • PRE-TEST

575.4 STD DEV=

5.8 CPM-AIRn 46.8 STD DEV=

7.8

  • POST-TEST

4,310.0 S1D DEV=

43.0 CPM-AIRn 3,781.0 STD DEV=

43.0 4

  • NET
  • NET CPit=

3,735.0 STD DEV=

44.0 l

f(

~

NUCON 13CE74'// 01

_37_

COUNTING DA1A FOR SAMPLE BATCH 11 GB2 COUNT DA1 A

  • PRE-TEST

575.4 STD DEV=

5.8 CPM-A1H" 46.8 STD DEVm 7.8 4

  • POST-TEST
  • CPMu

' 1579.4 S'lD DEV=

5.8 CPM-AIR =

50.8 STD DEV=

7.8 s

  • NET
  • j NET CPM' 4.0 STD DEV=

11.0 l

4 4

f l

1 I

l t

4

f I

W

r (L

e NUCON 13CE749/01 TEST REPOR'I: METHYL 10DIDE DATE PERFORMED: 16 SEP 1906 SAMPl.E BA'ICH 12 4

SUMMARY

0F RESULTS r

-.========_nnn======================

BED No.

RETENTION PENETRATION STD. DEV.

1 98.721%

1.279%

.0158%

THE RESUL'IS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHN10UES AND ACCORDING 10 OUR BEST KNOWLEDGE.

PERFURHED BY MARK P. KING NUCLEAR CONSULTING SERVICES, INC.

APPROVED BY d

h W.

PE'lER FREEHAN NUCLEAR CONSULTING SERVICES, INC.

e 43 NUCON 13CE749/01 1EST REPORT: NETHYL IUD 1DE DATE PERFORMED: 16 SEP 1986 4

CLIEN't: =CulillONWEALTH ED3 SON COMPANY, BRAIDWOOD STATION R.R.

51, DOX 81 SAMPL E s itAICH 12 P.O.

No.:

301790 TEST CONDITIONS:

DED DEP1H

5. 08 CM. ( 2.00 IN.)

BED D1AME1ER 5.08 CM.

( 2.00 IN.)

TEMPERATURES P R E-LU ADI NG 30.0

'C

( 86.0

'F )

LUADING 30.0

'C

( 86.0

'F )

POST-LOADING 30.0 t:

( 86.0

'F )

RELATIVE HUMIDITY 95.0 %

FACE VELOC11Y 20.32 CM./SEC (40.0 FPM)

CHALLENGE AGENT CONCENTRATION METHYL IODIDE 1.75 MG./CU.M.

TEST LIMES PRE-LOADING

16. HRS.

LOADING 2.0 HRS.

POST-LOADING 4.0 HRS.

CAP 1URED RADIDACTIVITY

.29 MICR0 CURIES PRESSURE 101.30 kPA.

( 1.00 ATM.)

N NUCUN 13CE749/01,

COUNTlHG Dol A FOR SAMPLE BATCH 12 AIR COUN1 Dolo

  • PRE-TEST
  • CPMn 579.0 STD DEVn 5.8
  • POST-TEST

579.0 STD DEVm 5.8 TD1 COUN1 DATA

  • PRE-TEST
  • CP Mr-615.0 S1D DEV=

6.2 CP M-A ll?"

36.0 STD DEV=

8.4

  • POST-TEST
  • r CPMr' 303,030.0 STD DEVu 960.0 CPM-A1R=

302,450.0 STD DEVm 960.0

  • NET

302,420.0 S1D DEV=

960.0 CB1 COUNT DATA MPRE-TEST

  • CPM:'

618.0 STD DEV=

6.2 4

CPM-A1R=

39.0 STD DEV=

8.5

  • POST-TEST

4,545.0 STD DEVn 45.0 CPM-AIR =

3,966.0 STD DEV=

45.0 ENET*

NEI CPM =

3,927.0 STD DEV=

46.0

f'[

NUCuli 13CE*/49/ 01 COUNT 3 NG Dolo FOR SAMPLE BATCH 12 GB2 COUNT DATA MPRE-TEST

  • CPHa 618.0 STD DEV=

6.2 CPM-AIRn 39.0 S1D DEV=

8.5 mPOSI-TEST

608.3 STD DEV=

6.1 CPM-AIR =

29.2 STD DEV:=

8.4 WNETM NET CPM =

-9.0 STD DEVm 12.0 4

l 4

e

.,. -, ~... -,,

,. - - ~,,.

N NUCON 13CE749/01 4 TEST R EP OR'1 : METHYL IODIDE DA1E PERFORMED: 19 SEP 1906 SAMPLE:

BA1CH 14

SUMMARY

OF RESULTS

= = = = = = = = = = = = = = = = = = = = = = - = = = = = = = = = =

a DED No.

RETENTION PENETR ATION STD. DEV.

1 98.312%

1.688%

0469%

THE. RESUL1S ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OUR BEST KNOWLEDGE.

PERFUNMED BY 1

MARK P. KING

] NUCLEAR CONSULTING SERVICES, INC.

APPROVED BY 1#7hh W.

PETER FREEMAN NUCLEAR CONSULTING SERVICES, INC.

Al NUCUN 13CE749/01 TEST PEPORT: I1 ETHYL 10D1DE DATE PERFORHED: 19 SEP 1986 CLIENT:

COHHONWEALTH EDISON COMPANY, BR AIDWOOD STATION R.R.

11, BOX 81 UAMPLE:

ItA'ICH 14 P.O.

NO.

301'/98 TESI CONDITIONS:

BED DEPTH 5.08 CM. ( 2.00 IN.)

1 BED DI AMElliR 5.08 CM. ( 2.00 IN.)

TEMPERATURLS PRE-LOADING 30.0 t

( 86.0

'F )

LOADING 30.0

'C

( 86.0 'F)

POST-LOADING 30.0

'C

( 86.0 'F)

RELA'l1VE HUMIDITY 95.0 %

FACE VELOC1'iY 20.32 CH./SEC (40.0 FPM)

CHAI.LENGE AGENT CONCENTRATION METHYL IODIDE 1.75 nG./CU.M.

TEST TIMES PRE-LOADING

16. HRS.

LOAD 3NG 2.0 HRS.

POST-LOADING 4.0 HRS.

CAPTURED R ADIDACTIVITY

.04 MICR0 CURIES PRESSURE 101.30 kPA.

( 1.00 ATM.)

44 NUCON 13CE749/01 COUNTING DATA FOR SAMPLE BATCH 14 AIR COUN1 DATA

  • PRE-TEST

550.1 STD DEV=

5.5 KPOST-TEST

  • CPM:e 550.1 S1D DEV=

5.5 TB1 COUN1 DA1A

  • PRE-1EST*

CPMn 651.5 STD DEV=

6.5 CPM-AIR =

101.4 STD DEV=

0.5

  • POST-TEST

43,860.0 STD DEV=

140.0 CPM-A1R-43,310.0 STD DEV=

140.0

  • NETM NET CPMa 43,210.0 STD DEV=

140,0 CB1 COUN T DATA

  • PRE-TEST
  • CP M:e 656.2 STD DEV=

6.6 CPM-AIRn 106.1 STD DEV=

8.6

  • POST-TEST

1,418.0 STD DEV=

14.0 CP M-A1 Rn 868.0 STD DF'V=

15.0

  • NET

762.0 STD DEV=

17.0

43 NUCON 13CE747/01

-4G-

.i COUNTING DA1A FOR SAMPLE BATCH 14 GB2 COUNT DATA

  • PRE-TEST

656.2 STD DEV=

6.6 CPM-A1Rn 106.1 S1D DEV=

8.6

  • POST-TEST
  • CP He-636.1 STD DEV=

6.4 CPM-AlRn 86.1 STD DEV=

8.4

  • NET

-20.0 STD DEV=

12.0 l

c

6*'

C lii: R *T' :l: l# 3: C A T lii:

C)lr C O M P l.

l
A N C lii:

- PAGE 1 0F 2 -

CLIENT: COMMONWEALTH EDISDN COMPANY, BRAIDWUDD STATIDH R.R.

41, BOX 81 BRACEVILLE, ILLINDIS 60407 DATE: 19 SEP 1986 PROJECT: 13CE749/01 PURCHASE ORDER: 301798 DATE: 25 NOV 1985 NUCull PRODUC1/ SERVICE: IODINE-131 TESTING PERFORMED UN BATCH 2 BATCH 3 BATCH 3 BATCH 6 BATCH 7 BATCH 8 BATCH 9 BA1CH 10 BATCH 11 BATCH 12 BATCH 14 REVIEWED IN ACCORDANCE WITH CHECKLIST OF NUCON PROCEEDURE 95 (QA38 ATTACHED).

3 BY f

FOR QUALITY ASSURANCE DEPT.

ElCOTT F R A'rI Afli NUCLEAR CONSULTING SERVICES, INC.

6I

(.;lir R 'T' :l: IT '.l: C A 'T'lii:

O IT C:C) M P l. *l A N C:lii:

- Po*E 2 OF 2 -

CLIENT: CUMNONWEALTH EDISON COMPANY, BRAIDWOOD STATION R.R.

11, BOX 81 BRACEVILLE, ILLINDIS 60407 DATE: 19 SEP 1986 PROJECT: 13CE749/01 PURCHASE ORDER: 301798 DATE: 25 NOV 1985 THIS IS ~IO CERTIFY THAT PRODUCT / SERVICE CONFORMS TO SPECIFICATION (S) 0F CLIENI:

OF NUCON:

ASTM D3803, NEW CARBON NUCON QA HANUAL AND IS S0 DOCUMEN'IED BY NUCON QUALITY ASSURANCE WITH ANY EXCEPTIONS NOTED.

EXCEP1 IONS:

NONE REVIEWED IN ACCORDANCE WITH CHECKLIST OF NUCD ROCEEDURE 95 (QA38 ATTACHED).

BY

/,,d w

FOR QUALITY ASSURANCE DEPT.

FRATIANN7 NUCLEAR CONSULTING SERVlCES, INC.

g>

OA30 UA CHECKLIST FOR REVIEW OF INSPECTION TEST DOCUMENTS 1.

IS Tile REPORI SIGNED BY PERSON PERFORMING hN INSPECTION UR 1EST?

2.

HAS 'lHE REPORT BEEN REVIEWED AND SIGNED N

DY AN AUTHORIZED PERSON?

3.

IS ACCEPTANCE CRITERIA SPECIFIED?

Y 3a.

1F SO, DOES IT HEET THE CUSTOMERS Y

N/A REQUIREMENTS?

4.

ARE INSPECTIONS OR TEST RESULTS h

N SATISFACTORY?

4a.

IF NOT, WAS A NON-CONFORMANCE REPORT Y

N/4 CENERATED?

5.

IF A NON-CONFORMANCE REPORT WAS NOT GENERATED, EXPLAIN BELOW.

h.

COMMENTS:

SIGNATURE IN REVIEW SECTION OF DOCUMENT INDICATES i

SATISFACTORY REVIEW.

1

CER T IF IC ATrE C1 F C A L I D R A T :l: O N CLILHis COMMONWEALTH EDISON COMPANY BRAIDWOOD STATION RR 91, BOX 81 BRACEVILLE, ILLINDIS 60407 P.O. No.: 301798 NUCUN PROJ ECT No. : 13CE749 DATE: OCT 2, 1986 TES1 EQUIPMENT CALIBRATION STANDARDS LOG No.

CAL. DUE LOG No.

NPS No. (IF APPLICABLE)

LO722 15 NOV 1986 L0350 522/223339

.i,

L0351 226617 LO723 15 NOV 1986 LO350 522/223339 LU351 226617 LO724 15 NOV 1986 LO416 731/220788 LO420 738/227675 LO421 738/227675 LO725 IS NOV 1986 LO416 731/220788 LO420 739/227675 LO421 738/227675 L029Y 8 MAR 1987 LO414 NBS CIRCULAR 4 36 LO485 16 OC1 1986 LO560 NBS SRM 4241-2 THIS IS 10 CERTIFY THAT THE ABOVE LISTED EQUIPMENT HAS BEEN CALIHNATED TRACEABLE TO THE NATIONAL BURFAU OF STANDAhDS, HAS BEEN DERIVED FROM ACCEPTED VALUES OF NATURAL PHYSICAL CONSTANTS, OR HAS BEEN DERIVED BY THE RATIO-TYPE OF SELF CALIBRATION TECHNIQUE AND heels THE REQUIREMENTS OF MIL STD 45662.

B Y _,_ _

_ FRA ANNE s

w_ _,_

FOR QUALITY ASSUR ANCE DEPT.

I A.

NUCLEAR CONSUL 1ING SERVICES, INC.

?

i 9

4 i

I h

?

i e

0 9

k

A + fach Mf 4i O

'VL Y" AL.YLTiL CO3VEP.AL.KTY 2304 RO5 ECH AN 5 AVE., E L S EG UN DO, C ALIF. 90 2 45, PHON E (233) 7 72 -5 2 21 P. O. Es O X O 2 8 8 7, A 4 R OO R T S TAT I O N, LO S A N G E LE S, C A LI F. 90009 TELEX NUMBER 664378 REPty 10. 500 SOUTH MAIN STREET CAVETAL & AKE. ILLih045 60014 PHONE. (8161469 6600 October 8, 1986 Comonwealth Edison Co.

1 South National Plaza P. O. box 76/

Chicago, IL.

60690 Atta: Bill Mamosser

Subject:

Nuclear Grade Carbon Braidwood Station

Dear Bill:

Attached you will find the sumary of the test results for the Carbon that we have available to fill the last six (6) carbon trays and twenty (20) test canisters. The material is not North American Carbon, Type G-615, and is also slightly out of Spec. (Ref ASTM D 6069 particle size).

1 We would like approval to use it and finish your Order 213830.

Yours Truly, (cffek+LL

~

d 1

Ted Kowalski Inspection Supervisor TK/bj l

l l

M ANU F ACTUR ERS OF FILT R ATIO N EQUIPMENT i

l

ANCC ENOlMEERS PAODUCTS O ACUP,INC.

ANCO ENGINEERS PRODUCTS GROUP. INC.

Job #10077, ANPROG Purchase Order #PG-0277 Cameron-Yakima Nuclear Activated Carbon, Type: CY-4089 Lot: CY-NUC-TK-001 ASTM D4089 Carbon Property Requirements frn2nrtr Reauired Actual _

Ignition Temp 3300 3830 Impregnant State KI+TEDA Perticle Size i

On #6 0.1% max 0.1%

On #8 5.04 max 3.0%

On #12 60.0% max 56.4%

On #16 40.04 min 39.0%

Thru #18 5.04 max 0.3%

Thru #18 1.0% max 0.3%

Activity 60.0% min 62%

CH3I, 30C & 954 RH 97.0%

99.78%

I, 1800 99.5%

100.0%

Density 0.38 g/cc min 0.5.55 g/cc Ball Pan Hardness 92.04 min 98.0%

There is one (1) value from the actual. material test data that does not comply with the purchase order and specification requirements, it is in the Particle Size Distribution area.

The amount of material retained on the

  1. 18 sieve (39.0%).is slightly out of tolerance of the 40.04 min allowable.

We recommend that the material be accepted as is because of the excellence of the efficiency test results', and the fact that the slightly smaller quantity of the smaller mesh size carbon in insignificant when compared with the rest of the test data.

l

-

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