Text

Radiological Survey for Equestrian Ctr Harkness State Park Waterford,Ct
	ML20199G809
Person / Time
Site:	Millstone
Issue date:	11/30/1997
From:	; NORTHEAST NUCLEAR ENERGY CO.
To:	;
Shared Package
ML20199G796	List: B16973, Provides Summary Info Re Offsite Baseball Field Survey Results from Various Recreational Ballfields Located in Waterford,Ct; ML20199G803; ML20199G809;
References
	NUDOCS 9802040348
	Download: ML20199G809 (140)
	v • d • e

{{#Wiki_filter:3.-___-_-..__---__-_._-_.--_____- l Radiological Survey 1 L EQUESTRIAN CENTER l HARKNESS STATE PARK l Waterford, Connecticut c i I l . u,. 3," l cp-[. - e ( e _N ..,5 l~ i i i 4

n.-

1 g%g .;}, ,,3, i l i November 1997 4 d 9802040348 900115 PDR ADOCK 0*000245,..; p PDR.,

L Summary Information 1 Radiological Survey Maps 2 Soil Sample Gamma Spectroscopy Results 3

) - Northeast I Utilities System Memo December 22,1997 TO: William Nevelos Director Nuclear Work Services - FROM: Ronald Sachatello Manager-Site Characterization

SUBJECT:

CAMP HARNESS EQUESTRIAN CENTER, WATERFORD CT, RADIOLOGICAL SURVEY RESULTS BACKGROUND INFORMATION: During the month of November 1997 the Millstone Station Health Physics department performed a series of radiological surveys on the Harkness State Park Equestrian Riding Center in Waterford CT. This survey was performed in response to public concern for potential radiological contamination from soll materials donated by Northeast Utilities to private citizens and municipalities in the past 25 year time period. In the approximate 1980 time frame Millstone Station donated approximately 1'),000 cubic yards of fill material to the Harkness State Park for facility site grading improvements. SURVEY RESULTS: The results of the Millstone Station survey at the Camp Harkness Equestrian Center indicate that this area is free of radioactive materials from Millstone .i ~ related activities. The Harkness State Park Equestrian facility has radiation levels similar to other locations in Connecticut consistent with natural background levels found in New England. . SURVEY METHODOLOGY: The Harkness Equestrian riding facility is a fenced in oval shaped area with a grass /soll surfaced riding arena measuring approximately 176 long on the long axis and 100 feet long on the lesser axis. Surveys were performed in both the defined riding arena area (fenced in oval area), and the surrounding area (30' by 176') on the west portion of the site that was described by the Harkness Park - managers as receiving Millstone donated soll material for elevation leveling _ purposes. The entire survey area was approximately 22,000 square feet. o m aava + (

i f This site was surveyed using sensitive beta / gamma field instrumentation and soll-sampling techniques. Approximately 600 individual measurement locations were used to take direct field radiation measurements. These surveys were taken on contact with the grass /soll area and at a wa.st level height from the soll level plane using a Eberline SPAR-3 gamma scintillator. This survey was repeated with at the same locations with both a Ludlum Model 12-S micro-R meter and an Eberlin,e E-140/260 instrument for a total of 1800 field radiation measurements. All field radiation measurements indicated normal expected background levels for Connecticut outdoor geographical areas. Interestingly the highest radiation levels found at this survey location, by an approximate 10 times increase, is from natural granite rock outcroppings on the facility, rather than soll material transferred from the Millstone Station site, t-Additionally a total of 23 soll samples were taken at the Harkness Equestrian riding facility. These samples were taken from a depth ranging from 12-30 inches, using shovels and hand auger penetrations specimens. These soll samples were counted in 1000 ml Marinelli geometries on a 39% relative efficiency gamma multi channel analyzer. All soil samples results show environmentally related activity attributed to naturally occurring radioactivity - present in soils throughout Connecticut. No plant related activity such as cobalt 60 were present in any soil sample. Traces of Cs-137, an isotope attributed to nuclear weapons fallout, were observed in the normal expected values found in Connecticut with concentrations ranging from none detected (N.D.) to a maximum value of 0.5 picoeuries (pCl) per gram. C cc: Arlene Sherman-Coordinator Harkness Equestrian Center Tony Sheridan-Waterford, CT First Selectman Kevin McCarthy-State of CT, DEP

MILLSTONE NUCLE AR POWER STATION - RADIATION SURVEY FIEURE NO. O UNIT 3

c...ry.< a. u.............................i ~ ~ e< w t4 i'DAoutes

< o' - < o> ii,2im Ef** iOOO' ri, clow/w Richmond /r. salamone/R. Sachatello ! N/A

DAWP8 Type Instrument Type Senel % mter i

UENcency l

Background

Cahbeatior Due DS N/A t N/A y N/A I N/A 1 N/A N/A N i N/A N/A i N/A N/A t N/A l N/A N/A l N/A N/A a s, Radiological Survey Data for Camp Ilarkness Equestrian Center SOIL SAMPLE LOCATIONS W0ods C Swale @ Mil Area .@g) M: 4 %, )I Gate pw. lR$ b @Akhh, j m..~. $b fRf NIkN Fenced ?QJd in Riding VM q Enclosure [ jM h gQ M ll$$ .c.T,ky h h A total of 23 soil samples were n EJ: 4 r h Qi taken. The sample depth ranged 5a Platform f' m -12 to 30". AH samples $.gg were prepared by B. Clow. j tjk:n, if. % ge3

73:er$

O - soli sampie tocations ( 4 b LQQ gamma (y) at waist levelin mmrrVhr 100+. gamma (y) contact in mrem'hr 25n neutron (o y)in mienyhr r @. contamination surveypoint 50 mrad. beta (p) reading in mrad'hr

MILLSTONE NUCLEAR POWER STATION - RAC)l3Tj0N SURVEY FIGURE NO. o UNIT 3 4 i /26/97 D31 5Wwey By k Typ. Oi Wrvey t s.onai,.,,,,,, _,,, _,,, g' ,,,,,, I rywwsa By RdM g n,,, og 3,,,,, ivr:s Pnni Nam. (% Reactor Powor 1100 R. Sachatello / F.T. Perr) I N/A ORWP# Type i instiwn.nt typ. i serei Ner C./ vEnconcy j Bacyround caudrenon om osi. y Eberline SPAR.3 1215/72443 j N/A -9,000 cpm 10/98 .m' N/A N/A I N/A NiA l N/A a l N/A l N/A N/A j N/A l N/A N/A l N/A J N/A 3y i E 140N/itP260 i 1910 i N/A 1 =80 cpm i 1/98 Radiological Survey Data for Camp Ilarkness Equestrian Center gg,, I.;/ @cly ',( ' RADIATION READINGS t ..s s *.. :g.:,l - - -]. 4 \\ '. Te $ i } f 9 Highest Reading with Large . h. A WOODS 3$'[ M 3 I' I k Conuct Rahn N - l. /,- 9, A - 100 cpm 129h

.,;Y.f

? 'I N S e .~ B 20 pR/hr I [ ,e C 35.000 50.000 cpm 1, i,m ,, kt j]l[., Area Swale g: J. y\\,kh^lf

i -

3 H Ga' 3 l . h ';'[f A. 80 cpm I Q[N Q. to pR/hr l i0[T C 10.000 rpm ' " * / Q. 80 cpm p, O 10pR/hr A. 80 cpm ,1

.h

- 10,000 cpn' B 9 pR/hr ML c 9.000 com Fenced / D. 80 cp, in RidinD hM Enclosure ./ f a,J Q.10,000 cpm pi% s.io pRfa, i ~.? ?'O 3 ,., gkd / MOj A 100 cpm ? / [ h,@: E 10 pRlhr g. .. ' ?? f'*e> g k' f' .e{ C - 9.000 cpm g, g3,e, a q '.$'iY.9 - 0 9pR/he hh*j C a.500 cpm v3 h(v Platform q A.so epm 4 Qa 0 10 pR/hr 80 cpre $I',b C 9.500 cpm g,g , ww 1,j W. ; C. I t,000 cpm NOTE: p-"d } All readmp taken at contact ~ wuh soil and at 3' above soll INSTRDIENT LIDGEND Sgd;glh lucktvrneed C11. Due fue A E 140VilP260 1910 =H0 cpm 1/98 B Micro-R Meter 80530 =10 pR,11r IW C SPAR-3 Meter 1211/72443 = 9,000 cpm IV)H

A, MILLSTONE NUCLE AR POWEFi STATION - RADI, ION SURVEY FIGURE NO. 0 UNIT 3 o.ie ! s~, e, g h. nmm. e,Qu,b,M a,p. m., 11/26/97 sonature O novine E sre ci imo i Pnnt tvame % Reactor Po*er 1100 R. Sachstello / I'.T. Fe rr3 N/A ORWPe Type l Instfwment Type se'ial Number V t/E ficoney i

Background

i Cahbrahon Due Date 1:berline SPART 1215 /72443 N/A j =9,000 cpm 10/98 .y N/A N/A N/A N/A I N/A a N/A l N/A 1 N/A l N/A l N/A l N/A l N/A N/A B .y L i 'ON/Ill'260 i 1910 i N/A 1/98 =80 cpm Radiological Survey Data for Camp llarkness Equestrian Center RADIKfl0N READINGS O i Highcu Raing wuh large WOOD 5 = 300 lbs. fyelb g. r-. -;; ; g Caa'"' RnA.,ng pg, O A 100 cpm g

it'^ - ~ ^

7 g__ B. 20 pR/hr C. 35,000 50.000 cpm peg j soll.: Swale Ali readmp iaken at contaci l with s il and ai 3' above soil Mea ,_3 t: : %q' Gate j A A. no cpm ,1 w.' (,, E - 10 pR/hr h< E.10,000 cpm I Q. 80 cpm ,. D i0 rRehr ,.,0,,, j' '" _1 @.10,000 cpn' B9A Y'] C. 9,000 cem Fenced in Riding m-A - 80 cpn, Enclosure kj B - 10 pR/hr y C 10,000 cpm g B 10 pR/hr }, C. 9,000 cpm A. 80 cpm q Id E 9 pR/hr iW C. 8,500 cpm Lf. p,.yf < t y; a.80 cpm Platform (i;plN B 10 pR/hr - 80 com C - 9,$00 cpm O,. 1 g,, 4M*9 C. I1,000 cpm U$b INSTRD1ENT IIDGl3D krulNo. Hrkenund 61 fine Inte A E 140Vilp260 1910 -m) cpm 1/'M B. Micro R Meter R830 =l0 pR/hr 12/9? G SPAR 3 Meter 121M2443 = 9,000 cpm 10/9H

lj 1< 41 1g$q o ggc h ..! y. \\ r 'i j .i j ,eer r-m mp.: v. 3$4L,. u$!:( ,d)'- 'i f mm. m !~[ j f$fv 4 owd d 1; y; '\\ %e p b ( I Tl O J.

h l?.l'.;

ji i n;.t )s L, s g; w% y of ) r f is 0 k J h ~ $r M J'9 %y% le 1 f 1 .W mu ew hkh ,,h vljahh92ar$(h" l b 3t p 3; yp '.Q[ y jf m.sw + v u. E '1 o x ce w n ~ ( g.gl> Ms. 3;

i q.- i,i ' ' ( ( taarin e

.nigugy k'

cf !g whg4 j ,c . p c iK.7 j c t S 1 9 1 j e ~j ?c{)$$(1L 1;KJ_ q ,g). 3 I' 8 d() m l f .s I ~ q 15, i,2. ~ i 7.: = gg 'ih(fl f, 'l i l L t

y 3. ff

4 M j I

.'h *

.[,h(1%' <, f b 4 dk ubn,.w;g#'p.Jn, M. /vn. @. fy U h y,, s., J,,qa@#tp:w.w%"4(W69h6by./y.3\\3 J.1, ik &, d qq% s, %. g, v u e, h fa uar $$ a ~ s I4i ' X $gi,@w

%o %j i4O.

.4 y p F m% hp MFCd,.$5_h:; ;s.Mi4[Wg a hm hug.i M]y yg.u4. a d

m. W W.., y. : ? J plf.,f 2, ~; Y'.% ; -

~ . 9:. - n.c a:c e.~.e' &

w,..:PX

., GT ~~r e gg rev^o eds..x. g. p.2:g.. %6 a.: we W 2~~

~~y..way~~
~ ,%v g;;;, fin.. + 4.,.j , y-l,fA red. - aw.. .q. - g. g' c.,: w,.- r..,,g,, m ~. e .s .Pd
== ag Eh k f*,[
D.
~~se&.D f ' 'ig s '?fk' ,Y ^h~~
~~L.xhabt :. *2Ct :m. ek s~~
Yv,, A m .*.+.: h,y N s Whrbh hg ~ g m( h h.4 ~; g-Q g.. y
g, 7 , y$ gr 5 .t' 't.. s y L T ? )a gj ..a gc g ,.fd,*,gy M 4.. N M .t ( v x.- 14 4 '.4 . x.:fn ,1 's '.:' .e .F,1,, 6. D.. M .a. e i g {5 .w w :.s.
~~% ':<'% Q '~~
~~i ,m ..i k,' b .m ~ ~~'"'- O -W* }4.c n o t.. ~ h. s;,. n a w., t $3 N i$ e,. ~ M.i~~
~~,s E,~~
~~t n-A> a ,.m$'l( ' JE }~K.' .f$ Y( ~1~ -e.c O -y e c.,36~~
~~3 g~~
~~r, y 5,.3, c 4~~
~~. <.1 n~~
t 8L ew
,l y g 4 3 l ~, m ,s, 2 O K" R; ~. 3 7 r, T, .,S - Jr,m,94,"t .m T W Mi. m' *N N v n 5 1. a ,I NQ4fS :{ g 4, u
~~.,a~~
~~\\ ' ':~ n~~
~~..rA y o4:~~
~~' h',; 'l i Rj.4~~
~~<%,LJ W~~
~~~.g, .. g3, .a s4 . q g y, o ~ c g y n.~~
~~q,,~~
Yi<- t3 T. '. "I e,r(' . s s I ~ }lf ., l g u dif jge +: y w i e.4 7 g h; 7 ~
gh.,.'r.ylf,'g[o/4 I j ( Ah. Y ? -ly:r s ) I* p(' O y y a \\( A. k_$$2%_.g_.k$)_k, .;2.s~.
~~,,q y,f x;3:; ;;;.,+QupwNOP~~
~~$. :,0@5ES.E,kM%A22 h...p.:.,n.,iAx j~. hJ,< d .n.=. ,,aa a ~ x~ h 9E9=[ g s dis 56%iGW: %=%,sewnn%s:.~~
~~,umw&.:en+ar., u~~
~~= n. s~ y..-s.sp=,%ggr.pJ;.v si mA y.9,A. G (?'y?.C@XiE.%+pjQ,t -~~
~~h,+f w %'? % C ;;y c~~
= L 2 p';7, 4.WYhv.M(@ 5'$e'62$fyf G R Ef2? SW r.Wi&74in, n a., f... # y. v. 4 7 _ * ~ w; : , m. ue -. m.. b) n ~. i 9 1 e 3 3 w]'e'. 3 bak$' '.;*t:$ w'f.. Y' .Yb? O g&. ~ * *
~~9 ms 7~~
~~w my a,, Yz'*s h sc3 Qi;~~
~~mavhp~~
~~~ o ?f? $l:. h}] Y'T' ^ll) ~h'kkf y,k[g;;k,%g f . th. 7.br;Ja.9k.-tW ..~7 2n n% + v ,r:,1: r.'~~
~~t.,c, h,$$ Y-Ybh $h.~~
~~up-eg ir~~
..~r.

.9.%.. h,
~~mr 4 L o -x ~ _ [i .g~~
~~m. g w Nl'~~
,t&%s; ' ^ +%,.4 Wt qma l. ,e. fl I 'J ? 4 ,y Cy ~ g 1 t
ggt s ~ .sn ya: 5 o f,.j ~
~~$,;h g ~." d g 4~~
~~^\\ . s s.. y b }f; m a ,ty $7. B Mhffh.j!~~
~~3) g,,. y s.,;cgN y~~
~~,3, 4 u /. W t'd Y !'h 3,.- ?) ,e;,%gt,f' 4 0 i. 4 = C p. '}( 's~~
~~g..~~
~~s 4 Y. g)$c* u s y' 'h~, u, t. m. g.... m 'L \\, .w .'.6 3 $g.- p; f..+.jts s .x e .gm ,}- r~~
~~..r g,,.~~
.s 'r NS a
s. i \\ !O tp , p. '3 r i 3 3:, 3 w, !:.t t e I; . ; ;3 i l v: $M &:f {.j, ' " > r y' J .e
~~( d;Hf~~
~~,Ud i f..l , b ]G ' l. } l w, -e 4.jpg ,j f A I- 'i, 3 m!, su 'a~~
~~:$ k i~~
~~( .;.l,f * :: q ., f ^^ ( 1 ^2 I Gu l l I ,g m, m _L.J. l +=~~
~~'?"IT*;_,~~
~~1 -:.wb ~ k l g ,.en.~~
)
~~Q: . ?) w 3 "M i w l ~ N;~~
~~w..u.,~~
\\ .Q [. ^ ,= -= y q,/ 'J "d l _4 ^ ^ g f i ' ',.,) " Qfj ^ j dhi 2': .:'+ .y'g L ~ f j .,e f(-
N: g 7 e
~~e f~~
~~+ :t l u . ; ;.. ? .., *id o \\ is ,[; ) I-9 j 'S[~ t;!' l w z~. l W[ s' I Ol L t I u.~_.. L ~ "( .e l~~
~~--;;;qy;p;;;;;gg - - - -~~
~~- - ^ - - - - - - m y 4 J ',~~
w.
~~,: ~. v u e( \\ .. y ;- .yy.7(, l ~ 3... s .i. i. - ? .7 p..#g 2:L2~~
xn

.za.:.
~~~ , [.,, I,-I-[ } ; ; ..*,k -~~
~~#.c~~
~~.$% } +, 'aq _ ,3 .z. 7 3,/fi. 1, l +. ;;; 1 ff i e [.'" ~;T{" ]! ~ .ityfr45 ~ ,. -% $U; ;,$ ' l ^ j ~ v. l .y.; ., ~ l ~ bi) l~~
6
~~.} j i 1s ( 1 J [P y l 4.V~~
f. (,;g'

i. f.:.
~~,e 9 4 x,. i 4~~
~~I t~~
}~ ? _{f[ i f { v 9 L .t ) i - - Us 's \\!
a &n k tw<n aw a >gamppAg$If. k $.a ~g e an. s w e g! gf r h. p p 1 _e w. Y. ;c - g YJ%hjhn c.] % a )$@gn~? O ts,iesQgbr v. f \\ w p.y .,p,.. =w%. .c. kfhjk' WMml_. d
~~> g g,g~~
= at?. ,r.. s 4ub %e t . o.g g(. '3?pg g:c.. ---'4 j g
3 J b r {} l '9 k ' ft 5 ^ ,. yf e hh ,(J,.% o r P.fWk 4. A ' :,
~~y..~~
~~tp. p?M41.;b:. %g ) b.gr 9,a.. e~~
fi
~~,k*', m e e (,;.a h Yf.*.. i. lr. y'- J =~~
~~ygg -~~
.r' , 43 g.
/,[ E$[ h.3dlId)i?.'1$5;h.' .m ~ j p-.. g- / s ...j.m
~~a........., ;,,. 2, s 1.>~~
~~851~,'[,* h*dh.,* * * . ('...'F ) ~ N E M M N. @d @.?.. h @ i O $, %v ' # y' ;- o? s..,-> ,.: ~ :.,.~~
~~s w~~
~~g ..a W: ,i s i d,s ?... y lsS.,5.. 3. 5. M,..D,, n y.0 %s:..,. g.' a 1.v~~
~~?.v!~~
~~E. ) ! W is ? g':n 2.+.,e Q, m 2,* %'~~
~~i h t *J f. o N l L.~~
~~min 4.g y~~
l

~'*
~~y eW.i;sm;r .3~~
~~...R~~
~~...,,. p.. ' q.'.-,..:.y ?* 4 ,5 e ' N, .- 7 s'*?.; g,;<v.. ~3.,. ,s. h e,.tt ::.**lf.y+f* *;. w2.'ff; 2;C ~ fiV~~
~~A.// r o n : m'M,f. a#4 s,i.e :fM.*.<. if~~
~~. d.,~~
~~N. :%pp'iv 3~~
~~a vn a ,1 f W a.t.4E...s f'..u'7" O. \\G1Q,b.&t:$y.wff,.;& N . :.7. v ' ' ' l'N.jigf.,)' %x y*. Q W m2'm .;d+MQ,>;F.if'j',R'A;9,$ f-s& r;~~
~~n. % 5;r:y~~
~~~#rs-;a:_fEfN..w;yyQ y~a:*m'Lp? ih'I' //.B.! [hhh20 .Yb!Y;t'h. Q.a.,+. 79 g&j%.:, ...s .:w c%9'c r"-%. Mi-qy,.4'6;ln i .r..~~
~~.'.vi~~
~~\\ w gg.>g*;.w: %,.,, u. t.a S c. y~~
~~an fa~~
~~y 0 (y t m 3.':,' y f'..'y @ h,7W.~~
~~X. P~~
.h ph bNb.d,vm4 ,;. 3. g r A r 2 6,:. 6 ~ %. 5r in.5,...g% t 4 ay 53 ize f MO hh e 5 k ff, Nk W$$ ht#qg$1%w@' k!g$kaN =lh 97 hkghE t a s-Q,_c ge.sgg; +. _ g, ! r. .. $'4 7w fw.. 8 V 6 g' n .%9 a i "r m [d . N ' 'fp'g s; \\,, .( 0 g '----m '*'"'~n,~ m,_.
ws MI. STONE HEALTH PHYSICS-ENVIRONMENTAL 21-NOV-1997 14:22:31 \\

~~Sample Information ----~~

~~Samplo ID~~
Harkness #1 Sample Quantity

1.00000E+03 gm Scmplo Number

37462 Spctrm Collector : HP Environmental Sample Analyst

HP Environmental

~~Sample Deposition Information ----~~

~~No Dep. Duration Dap. Correction?~~
~~Dopocition Start : Deposition End~~
~~21-NOV-1997 14:11:01~~

~~Sample Decav/ Count Information ----~~

~~Scmplo Date~~
~~21-NOV-1997 14:11: 01 Acquisition date : 21-NOV-1997 14:11:29 caccy time 0 00:00:28.23~~
~~% dead time~~
~~0.0%~~
~~Elapood live times 0 00:10:00.00 Elapsed real time 0 00:10:00.30 I~~

~~Detector Parameters ----~~

~~Enargy cal. time : 19-JUL-1995 08:05:48 Energy cal. oper.: HP Support Datoctor name~~
~~Environmental Counting geometry: 1 Liter Soil Effic. cal. time : 19-JUL-1995 08:56:03 Effic. cal, oper.: HP Support~~

~~Processing Parameters ----~~

~~Stcrt channel~~
100 End channel

3700 S0nr,itivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No Empirical Eff?

Yes Libran-based eff: No Enargy tolerance : 1.00000 Half life ratio

8.00000 Abundance limit 80.00000 WTM error limit

3.00000 pnA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
1...-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 3 74.98 72 117 0.86 1$0.03 146 31 24.4 2.34E+00 PB214 PB212 3 77.24 147 119 0.98 154.55 ' 146 13 14.3 PB214 PB212 0 86.88 55 122 1.34 173.85 172 7 35.7 PB214 PB212 5 90.01 57 56 1.01 180.12 178 13 22.2 1.74E+00 PB214 5 93.06 84 137 1.61 186.22 178 13 28.5 TH234 5 TH234 0 185.82 35 113 1.21 371.87 367 11 61.9 RA226 5 238.64 430 51 1.02 477.57 471 17 5.5 1.76E+00 PB212 5 341.48 63 61 1.63 483.24 471 17 37.6 PB214 0 295.21 87 55 0.74 590.78 585 10 19.2 PB214 0 300.40 25 24 1.29 601.16 597 8 39.6 PB212 0 338.26 68 40 0.86 676.93 673 9 20.4 AC228 0 351.97 172 25 1,44 704.35 699-13 9.7 PB214 0 511.47 31 46 1.17 1023.51 1017 14 50.1 TL208 0 562.69 14 6-1.41 1126.00 1123 6 37.3 0 583.25 158 26 1.45 1167.14 1161 14 10.6 TL208 0 609.14 125 17 1.42 1218.94 1213 12 11.2 BI214 0 709.06 15 14 0.94 1418.86 1414 9 52.7 0 860.61 34 0 1.70 1722.06 1717 11 17.1 TL208 CO?Y
'PCct-NID Pock Soorch Report (continued) Pago : 2 C mplo ID : Harkneso #1 Acquisition date : 21-NOV-1997 14:11:29 f ( Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 911.11 88 12 1.89 1823.09 1815 16 13.8 AC228 1 964.72 19 4 1.95 1930.33 1928 16 26.9 1.10E+00 AC228 1 968.73 62 10 1.71 1938.36 1928 16 15.5 AC228 0 1119,70 35 0 1.35 2240.34 2233 13 16.9 BI214 O 1460.62 240 3 2.30 2922.25 2916 13 6.6 K40 Intorference Report Interfering Interfered Nuclide Line Nuclide Line 0 PB214 241.92 RA224 241.00 TL208 510.72 ANN-RD 511.00 t + i
r* Summary of Nuclido Activity Pega i 3 Scmple ID : Harkness #1 Acquisition date : 21-NOV-1997 14:11:29 ( '*cl number of lines in spectrum 23 ( =ber of unidentified lines 1 Humber of lines tentatively identified by NID 22 95.65% Nuclide Type : natural Corr Decay Corr 1-Sigma Uncorrected Decay /gm 1-Sigma Error % Error Flags Nuclide Hlife Decay uCi/gm uCi K40 1.28E+09Y 1.00 1.429E-05 1.429E-05 0.095E-05 6.65 TL208 3.10M 2.78 5.505E-07 1.532E-06 0.163E-06 10,62 A PB212 10.64H 1.01 1.581E-06 1.591E-06 0.087E-06 5.46 A BI214 19.90M 1.20 8.389E-07 1.010E-06 0.113E 11.22 A PB214 26.00M 1.15 9.473E-07 1.088E-06 0.106E-06 9.74 A RA226 1600.00Y 1.00 1.478E-06 1.478E-06 0.915E 06 61.87 AC228 6,13H 1.01 1.312E-06 1.326E-06 0.183E-06 13.82 A 1 TH234 24.10D 1.00 4.511E-06 4.511E-06 1.286E-06 28.52 KA Total Activity : 2.551E-05 2.683E-05 Grand Total Activity i 2.551E-05 2.683E-05 Flcgs:
~~K" = Keyline not found "M" = Manually accepted "E"~~
= Manually edited "A" = Nuclide specific abn. limit .1 9
Nuclidh Lino Error Propogotion Roport Pcg3 4 ,Shraple' ID : Harkness #1 Acquicition dcto : 21-NOV-1997 14:11:29 I hw 41de Types natural Corr 1-Sigma Uncorrected Decay /gm uCi/gm uCi % Error Status Nuclide Energy %Abn %Eff K40 1460.75 10 70* 7.058E-01 1.429E-05 1.429E-05 6.65 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 6.65%) Absent Line Not Found TL208 277.36 6.50 2.596E+00 510.72 22.50 1.669E+00 3.773E-07 1.050E-06 50.12 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 50.12%) 583.14 86.00* 1.505E+00 5.505E-07 1.532E-06 10.62 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 10.62%) 860.47 12.00 1.093E+00 1.168E-06 3.249E-06 17.15 OK ( 0.0%) ( 5.61%) (Decay 0.00%) (Area 17.15%) PB212 74.81 9.60 1.994E+00 1.691E-06 1.701E-06 24.40 OK ( 0.0%) ( 4.15 % ) (Decay 0.00%) (Area 24.40%) 77.31 17.50 2.115E+00 1.787E-06 1.798E-06 14.28 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 14.28%) 97.20 6.30 2.562E+00 1.530E-06 1.539E-06 35.67 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 35.67%) 238.63 43.10* 2.845E+00 1.581E-06 1.591E-06 5.46 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.46%) 300.09 3.27 2.463E+00 1.392E-06 1.401E-06 39.56 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 39.56%) DI214 609.32 46.09* 1.454E+00 8.389E-07 1.010E-06 11.22 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 11.22%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.754E-01 1.197E-06 1.442E-06 16.90 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 16.90%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PD214 74,81 6.33 1.994E+00 2.564E-06 2.946E-06 24.40 OK ( 0.0%) ( 4.15 % ) (Decay 0.00%) (Area 24.40%) 77.11 10.70 2.115E+00 2.923E-06 3.358E-06 14.28 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 14.28%) 87.20 3.70 2.562E+00 2.605E-06 2.993E-06 35.67 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 35.67%) 89.80 1.03 2.683E+00 9.30BE-06 1.069E-05 22.16 OK 1 ( 0.0%) ( 4.07%) (Decay 0.00%) (Area 22.16%) 241.92 7.47 2.826E+00 1.337E-06 1.536E-06 37.56 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 37.56%) 295.22 19.20 2.492E+00 8.180E-07 9.398E-07 19.24 OK ( 0.0%) ( 5.09%) (Decay 0.00%) (Area 19.24%) 351.99 37.10* 2.207E+00 9.473E-07 1.088E-06 9.74 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 9.74%) Absent Line Not Found 785.95 1.09 1.180E+00 RA226 185.99 3.28* 3.213E+00 1.478E-06 1.478E-06 61.87 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 61.87%) Absent Line Not Found AC228 209.40 4.55 3.050E+00 Absent Line Not Found 270.30 3 77 2.639E+00
. ~ - Nhcli4bLinoErrorPropcgotionRoport (continusd) Pcgo : 5 Actf;ple ID : Harkness #1 Acquisition date : 21-NOV-1997 14:11:29 vu.41de Types natural Corr 1-Sigma Uncorrected Decay /gm uCi/gm uCi % Error Status Nuclide Energy %Abn %Eff Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.270E+00 1.130E-06 1.142E-06 20.36 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 20.36%) Absent Line Not Found 409.40 2.23 1.977E+00 Absent Line Not Found 463.00 4.64 1.802E+00 Absent Line Hot Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1,62 1.197E+00 Absent Line Not Found 794.00 4.84 1.169E+00 Absent Line Not Found 835.60 1,82 1.121E+00 911.07 29.00* 1.042E+00 1.312E-06 1.326E-06 13.82 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 13.82%) 964 60 5.45 9.926E-01 1.550E-06 1.566E-06 26.87 OK ( 0.0%) ( 5.44%) (Decay 0.00%) (Area 26.87%) 968.90 17.46 9.892E-01 1.618E-06 1.635E-06 15.55 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 15.55%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.789E+00 5.266E-06 5.266E-06 28.52 OK 4 ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 28.52%) 92.80 3.00 2.789E+00 4.511E-06 4.511E-06 28,52 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 28,52%) Absent Line Not Found 112.81 0.25 3.240E+00 - Keyline i o e
i e. s
~~MI$LSTONE HEALTH PHYSICS-ENVIRONMENTAL 22-NOV-1997 14:28:09~~
~~/ \\~~

~~Sample Information - --~~

~~SOmple ID~~
Harkness #2 Sample Quantity-

1.00000E+03 g Scmple-Number 37518 Spctrm Collector : HP Environmental Sample Analyst HP Environmental

~~Sample Deposition Information ----~~

~~Dop. Correction? : No Dep. Duration Dsposition Start : Deposition End~~
~~22-NOV-1997 14:17:27~~

~~Sample Decay / Count Information ----~~

~~Sample Date~~
~~22-NOV-1997 14:17:27 Acquisition date : 22-NOV-1997 14:17:33 Doccy time 0 00:00:06.19~~
~~% dead time~~
~~0.0%~~
~~Elepced live times 0 00:10:00.00 Elapsed real times 0 00:10:00.27 l-~~

~~Detector Parameters ----~~

~~Enorgy cal, time 19-JUL-1995 08:05:48 Energy cal oper.: HP Support Datoctor name~~
~~Environmental Counting geometry: 1 Liter Soil Effic cal. time : 19-JUL 1995 08:56:03 Effic, cal. oper.: HP Support~~
~~-- - Processing Parameters ---- -Start channel-t 100 End-channel~~
3700

Sansitivity

4.50000 Gaussian Sens.
~~10.00000 Critical level?~~
Yes Propagate Errors?: No Empirical Eff?

Yes Library-based eff: No Energy tolerance : 1.00000 Half life ratio

8.00000 Abundance limit i 80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000.%
. NID Peak Search Report -It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 3 74.82 91 90 1.28 149.72 144 17 21.2 1.67E+00 PB214 .PB212 3 77.28 150 72 1.28 154.64. 144 17 13.5 PB214 PB212 0 93.22 59 117 1.39 186.54 183 10 36.8 TH234 TH234 0 129.92 62 149 3.70 259.99 253 16 45.8 0 186.03 71 82 1.15' 372.27 368 0 26.8 RA226 0 209.85 29-66 1.35 419.95 415 8-51.8 AC228 g 0 238.58 304-43 1.18 477.44-474 7 6.7 PB212 0 241.60 30 39 1.47 483.49 481 7 48.7 RA224 0 270.48 44 33 0.96-541.28 537 9 28.3 AC228 0 295.18-80 49 0.85 590.72 586 10 19.9 PB214 0 299.98 25 30 1.11 600.31 596 8 42.7 PB212 0 338.41 77 24 1.19 677.21 673 11 16.9 AC228 0 .351.73 174 31-1.47 703.87 697 15 10.2 PB214 0 510.63 21 19 1.01 1021.84 1018 7 41.8 TL208 0 -- 583.14 99 5 1.79 1166.93 1162 13 11.3 TL208 0 609.17 125 8 1,54 1218.99 1213 11 10.0 BI214 '0-728.37 18-16 1,54 1457.48 1449 113 52.5 0. 795.16 20 3 0.59 1591.12 1585 10 26.8 AC228 0 910.84- -85 3 1.48-1822.54 1816 13 11.7 AC228 COPY
~~l.,~~
Port-HID P0ck Socrch Report (continu0d) Pcg3 2 SCmplo ID : Harknesp #2 Acquisition dato : 22-NOV-1997 14:17:33 k , Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides i 0 964.39 19 4 1.96 1929.67 1925 9 31.0 AC228 0 969.04 40 10 2.14 1938.97 1934 10 21.7 AC228 0 1120.11 13 9 1.13 2241.18 2237 7 45.9 BI214 0 1460.54 219 0 2.19 2922.09 2915 13 6.8 K40 Intorference Report Interfering Interfered j Nuclide Line Nuclide Line PB214 241.92 RA224 241.00 ( TL208 510.72 Mai-RD 511.00 e 9 't
t 6, a Summ3ry of Nuclido Activity Pcgo 3 Sample 3D : Harkness #2 Acquisition date : 22-NOV-1997 14:17:33 / "cl number of lines in spectrum 23 A.. ber of unidentified lines 2 Number of lines tentatively identified by NID 21 91.30% t Nuclide Type i natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclido Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags X40 1.2BE+09Y 1.00 1.3062-05 1.306E-05 0.088E-05 6.76 TL300 3.16M 2.56 3.432E-07 8.846E-07 0.998E-07 11.28 A PB212 10,64H 1.01 1.118E-06 1.124E-06 0.076E-06 6.74 A BI214 19.90M 1.19 8.377E-07 9.957E-07 0.997E-07 10.02 A PB214 26.80M 1.14 9.583E-07 1.091E-06 0.111E-06 10.22 A 3A224 3.66D 1.00 1.223E 06 1.223E-06 0.595E-06 48.65 RA226 1600.00Y 1.00 3.020E-06 3.0'8E-06 0.810E-06 26.76 IAC228 6.13H 1.01 1.264E-06 1.276E-06 0.149E-06 11.71 A TH234 24.10D 1.00 3.167E-06 3.167E-06 1.165E-06 36.78 KA Total Activity i 2.500E-05 2.585E-05 Grand Total Activity : 2.500E-05 2.585E-05 Flage: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit ~ e
l s. .-Nuclida Lino Error Propogotion Report Pcg3 : 4
~~Sample ID : Harkness #2 Acquisition date : 22-NOV-1997 14:17:33 r~~
( Nuclide Typer natural Uncorrected Decay corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status 4 K40 1460.75 10.70* 7.058E-01 1.306E-05 1.306E-05 6.76 OK l ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 6.76%) l Absent Line Not Found TL208 277.36 6.50 2.596E+00 510.7.2 22.50 1.671E+00 2.457E-07 6.298E-07 41.85 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 41.85%) 583.14 86.00* 1.505E+00 3.452E-07 8.846E-07 11.28 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 11.28%) Absent Line Not Found 860.47 12.00 1.093E+00 PB212 74.81 9.60 1.985E+00 2.148E-06 2.160E-06 21.19 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 21.19%) 1 77.11 17.50 2.11?E+00 1.824E-06 1.834E-06 13.48 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 13.48%) Absent Line Not Found 87.20 6.30 2.575E+00 238.63 43.10* 2.845E+00 1.118E-06 1.124E-06 6.74 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 6.74%) 300.09 3.27 2.466E+00 1.404E-06 1.412E-06 42.68 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 42.68%) EI214 609.32 46.09* 1.453E+00 8.377E-07 9.957E-07 10.02 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 10.02%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.751E-01 4.558E-07 5.418E-07 45.87 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 45.87%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PD214 74.81 6.33 1.985E+00 3.258E-06 3.707E-06 21.19 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 21.19%) 77.11 10.70 2.117E+00 2.983E-06 3.395E-06 13.48 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 13.48%) Absent Line Not Found 87.20 3.70 2.575E+00 Absent Line Not Found 89.80 1.03 2.675E+00 Line Not Found

~~<< INT Reject 241.92 7.47 2.823E+00 295.22 19.20 2.492E+00 7.535E-07 8.574E-07 19,91 OK 1~~

( 0.0%) ( 5.09%) (Decay 0.00%) (Area 19.91%) 351.99 37.10* 2.208E+00 9.583E-07 1.091E-06 10.22 OK ( 0.0%) ( 4.59%) (Decay 0.00%) (Area 10.22%) Absent Line Not Found 785.95 1.09 1.180E+00 Absent Line Not Found RA324 83.78 0.21 2.430E+00 241.00 3.90* 2.825E+00 1.223E-06 1.223E-06 48.65 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 48.65%) RA226 185.99 3.28* 3.212E+00 3.028E-06 3.028E-06 26.76 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 26.76%) AC228 209.40 4.55 3.047E+00 9.534E-07 9.626E-07 51.77-OK ( 0.0%) ( 4.93%) (Decay 0.00%) (Area 51.77%) . 270.30 3.77 2.638E+00 2.011E-06 2.031E-06 28.31 OK ( 0.0%) ( 5.16%) (Decay 0.00%) (Area 28.31%) 4 -,-,----n- .c
iluelide Line Error Propagation Report (continued) Pcg2 5 Scmple ID : Harkaeas #2 Acquisition date : 22-!!OV-1997 14:17:33 ( A Nuclide Types natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.269E+00 1.271E-06 1.283E-06 16.91 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 16.91%) Absent Line Not Found 409.40 2.23 1.977E+00 Absent Line Hot Found 463.00 4.64 1.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 794.80 4.84 1.168E+00 1.607E-06 1.623E-06 26.81 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 26.81%) Absent Line Not Found ( 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 1.264E-06 1.276E-06 11.71 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 11.71%) 964.60 5.45 9.929E-01 1.5%JE-06 1.560E-06 31.00 OK ( 0.0%) ( 5.44%) (Decay 0.00%) (Area 31.00%) 968.90 17.46 9.889E-01 1.044E-06 1.054E-06 21.65 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 21.65%) Absent Line Not Found 1587.90 3.71 6.633E 01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.794E+00 3.696E-06 3.697E-06 36.78 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 36.78%) 92.80 3.00 2.794E+00 3.167E-06 3.167E-06 36.78 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 36.78%) Absent Line Not Found 112.81 0.25 3.240E+00 Flag "** = Keyline
_ _ _ ~.__ _. _ _ _ _ _ _.. _ _ _ _ __ _ _, eg 'HILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 22-NOV-1997 14:59:06 t l f (

~~Sample Information ----~~

~~Semple IC~~
~~Harkness #3 Sample Quantity 1.00000E+03 g Semple Number 37519 Spctrm Collector : HP Environmental i~~
~~Sample Analyst~~
~~HP Environmental~~

~~Sample Deposition Information ----~~

~~? No Dep. Duration D p. Correction?~~
~~22-NOV-1997 14:48:22 i~~
~~Deposition End D3pocition Start - -- Sample Decay / Count Information ---- i Sample Date~~
~~22-NOV-1997 14:48:22 Acquisition date : 22-NOV 1997 14:48:29 D0ccy time 0 00:00:06.29~~
~~% dead time~~
~~0.0%~~
~~i Elepsed live time: 0 00:10:00.00 Elapsed real times 0 00:10:00.27 ]~~

~~Detector Parameters ----~~

Enorgy cal time : 19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Datoctor name-Environmental Counting geometry: 1 Liter Soil i Effic. cal time : 19-JUL-1995 08:56:03 Effic, cal. oper.: HP Support

~~Processing Parameters ----~~

~~Start channel~~
100 End channel

3700 Sanoitivity

4.50000 Gaussian Sens.
~~10.00000 Critical level?~~
Yes Propagate Errors?: No Empirical Eff?

Yes Library-based eff No Inargy tolerance : 1.00000 Half life ratio

8.00000 t
~~Abundance limiu~~
80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
..-HID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 3-74.78 93 93 1.28 149.63 143 19 21.5 1.02E+00 PB214 PB212 3 77.17 135 76 1.02 154.42 - 143 19 13.5 PB214 PB212 0 87.25 71 76 1.04 174.59 172 6 22.9 PB214 PB212 0-93.45 84 110 1,56 187.00 183 9 25.3 0 186.10 91 63 1.12 372.42 368 10 19.4 RA226 4 4_ l238.64 360 56 1.07 477.56 472 18 6.1 1.30E+00 PB212 4 241.42 58 69 1.77 483.13 472 18 41.6 PB214 -0 294.83 131 25 1.19 590.01 583 12 11.5 PB214 3 0 300.29 35 30 0.78 600.94 596 10 33.8 PB212 0 328.54 30 30 2.72 657.47-652 -10 38.7 AC228 0 338.43 56 48 1.26 677.26 673 9 25.7 AC228 0 351.99 131 38 1.11 704.39 697 14 13.3 PB214 0 510.77 33 22 1.53 1022.11 1018 8 30.0 TL208 0 583.16 123 11 1.42 1166.95 -1161 14-10.6 TL208 0 609.02 112 21 -1,24-1218.69 1212.=14 12.9-BI214 1F 661.11 29 5 1.10 1322.91' 1319 7 22.7 CS137 0 699.51-12 0 1.50.1399.75 1397 6 28.9 01 727.40 16 ~ 22 0.81 1455.55 1451 13 65.1 BI212 0 910.92 -77 5 2.26 1822.69 1818 10 12.6-AC228 ~ CO?Y
7 test-NID Pock Socrch Roport (continu0d) POg3 2 .S mple ID : Harkness #3 Acquisition date : 22-NOV-1997 14:48:29 ( ( Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 968.82 48 6 2.05 1938.54 1934 11 17.4 AC228 i 0 1120.78 20 20 0.71 2242.51 2236 13 51.9 BI214 0 1460,59 233 4 1.97 2922 19' 2915 15 6.8 K40 O 1764.34 11 5 1.06 3529.64 3524 10 48.5 BI214 Intorference Report ? Inte.fering Interfered Nuclide Line Nuclide Line-PB214 241.92 RA224 241.00 t TL208 510.72 ANN-RD 511.00 1 i 4 4 .y
l Su'mmary of Nuclida Activity Pcgo 3 .Scmple ID : Harkness #3 Acquisition date : 22-NOV-1997 14:48:29 e **tol number of lines in spectrum 23 ,n tur of unidentified lines 1 b s Number. cf lines tentatively identified by NID 22 95.65% l f Nuclide Type : natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags X40 1.28E+09Y 1.00 1.392E-05 1.392E-05 0.095E-05 6.79 TL208 3.10M 2.56 4.280E-07 1.097E-C6 0.117E-06 10.62 A BI212 60.55M 1.06 4.932E-07 5.226E-07 3.402E-07 65.11 A PB212 10.64H 1.01 1.324E-06 1.332E-06 0.082E-06 6.13 A BI214 19.90M 1.19 7.511E-07 8.928E-07 1.148E-07 12.86 A r PB214 26.80M 1.14 7.190E-07 8.182E-07 1.091E-07 13.34 A RA226 1600.00Y 1.00 3.877E-06 3.877E-06 0.753E-06 19.43 1 AC228 6.13H 1.01 1.155E-06 1.166E-06 0.146E-06 12.55 A Total Activity 2.267E-05 2.363E-05 Nuclide Type i fission l' Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uci/g uci/g 1-Sigma Error % Error Flags CS137 30.10Y 1.00 1.132E-07 1.132E-07 0.257E-07 22.72 Total Activity : 1.132E-07 1.132E-07 Grand Total Activity 2.278E-05 2.374E-05 Flags: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit. w 1 ,-,9--

~~v.-m,~~

-.g---- -,n- -, -- +- g,,
i 3-Nuclido Lino Error Propogetion Report pega 4 Semple ID : Harkness #) Acquisition date : 22-NOV-1997 14:48:29 ? \\.. Nuclide Type: natural Uncorrected Decay corr 1-Sigma Nuclide Eneroy %Abn tEff uC1/g uCi/g % Error Status K40 1460.55 10.70* 7.058E-01 1.392E-05 1.3922-05 6.79 OK 1 ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 6.79%) Line Not Found Absent TL208 277.36 6.50 2.596E+00 510.72 22.50 1.671E+00 3.979E 07 1.020E-06 29.96 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 29.96%) 583.14 86.00* 1.505E+00 4.280E-07 1.097E-06 10.62 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 10.62%) Absent Line Not Found 860.47 12.00 1.093E+00 DI212 727.17 11.80* 1.258E+00 4.932E-07 5.226E-07 65.11 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 65.11%) Absent Line Not Found I 785.42 2.00 1.180E+00 Absent Line Not Found 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 PD212 74.81 9.60 1.983E+00 2.208E-06 2.220E-06 21.54 OK ( 0.0M ( 4.15%) (Decay 0.00%) (Area 21.54%) 77.11 17.50 2.111E+00 1.645E-06 1.654E-06 13.53 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 13.53%) 87.20 6.30 2.577E+00 1.963E-06 1.974E-06 22.87 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 22.87%) 238.63 43.10* 2.845E+00 1.324E-0G 1.332E-06 6.13 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 6.13%) 300.09 3.27 2.464E+00 1.957E-06 1.968E-06 33.81 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 33.81%) 4 609.32 46.09* 1.454E+00 7.511E 07 8.928E-07 12.86 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 12.86%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E400 1120.28 15.04 8.747E-01 6.677E-07 7.937E-07 51.89 OK ( 0.0%) ( 4.61%) (Decay 0.00%) (Area 51.89%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent 1377.65 4.02 7.387E-01

~~' Line Not Found Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 1764.51 15.92 6.174E-01 5.042E-07 5.993E-07 48.53 OK~~

~~( 0.0%) i 1.80%) (Decay 0.00%) (Area 48.53%) PB214 74.81 6.33 1.983E+00 3.348E-06 3.810E-06~~
~~21..~~
OK 1 ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 21.54%) l 77.11 10.70 2.111E+00 2.690E-06 3.061E-06 13.53 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 13.5)%) 87.20 3.70 2.577E+00 3.342E-06 3.803E-06 22.87 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 22.87%) Absent Line Not Found 89.80 1.03 2.675E+00 241.92 7.47 2.826E+00 1.232E-06 1.402E-06 41.65 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 41.65%) 295.22 19.20 2.494E+00 1.232E-06 1.402E-06 11.53 OK ( 0.0%) ( 5.09%) (Decay 0.00%) (Area 11.53%) 351.99 37.10* ' 2.207E+00 7.190E-07 8.182E-07 13.34 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 13.34%) -Absent Line Not Found 785.95 1.09 1.180E+00 -k 'L w r.-., en-- 4 r <,y.
g. Nuclida Lino Error Propogotion Roport (continuod) Pcgo : 5 Scmple ID : Harkneso #3 Acquisition date : 22-NOV-1997 14:48:29 ( Nuclide Types natural Uncorrected Decay corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status RA226 185.99 3.28* 3.211E+00 3.877E-06 3.877E-06 19.43 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 19.43%) Line Not Found Absent AC228 209.40 4.55 3.050E+00 Line Not Found Absent 270.30 3.77 2.639E+00 328.00 3.36 2.317E+00 1.734E-06 1.751E-06 38.73 OK ( 0.0%) ( 4.82%) (Decay 0.00%) (Area 38.73%) 338.40 12.01 2.269E400 9.334E-07 9.4.4E-07 25.68 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 25.68%) Line Not Found Absent 409.40 2.23 1.977E+00 Line Not Found Absent 463.00 4.64 1.802E+00 Line Not Found Absent 1 478.20 0.24 1.758E+00 Line Not Found Absent 772.10 1.62 1.197E+00 Line Not Found Absent 794.80 4.84 1.169E400 Line Not Found Absent 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 1.155E-06 1.166E-06 12.55 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 12.55%) Line Not Found Absent 964.60 5.45 9.927E-01 968.90 17.46 9.891E-01 1.239E-06 1.251E-06 17.38 OK ( 0.0%) ( 6.43%) (Decay 0.00%) (Area 17.38%) Line Not Found Absent 1587.90 3.71 6.633E-01 Line Not Found Absent 1630.40 1.95 6.510E-01 'ide Typer fission Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status CS137 661.62 84.62* 1.360E+00 1.132E-07 1.132E-07 22.72 OK ( 0.0%) ( 5.10%) (Decay 0.00%) (Area 22.72%) = Keyline Fleg: i
e o*.
~~MILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 22-NOV 1997 06:12:18 I~~

~~Sample Information (Sample ID~~

Harkness #4 Sample Quantity i 1.00000E+03 g S mple Number 37491 Spetrm Collector : HP Environmental Sample Analyst

HP Environmental

~~Sample Deposition Information ----~~

~~D:p. Correction? : No Dep. Duration D3pooitjon Start : Deposition End~~
~~22-NOV-1997 06:01:33~~

~~Sample Decay / Count Information ----~~

~~Sampic Date~~
~~22-NOV-1997 06:01:33 Acquisition date : 22-NOV-1997 06:01:39 D]ccy time 0 00:00:06.15~~
~~% dead time~~
~~0.0%~~
~~ElCpced live times 0 00:10:00.00 Elapsed real times 0 00:10:00.22 )~~

~~Detector Parameters ----~~

~~Energy cal. time i 19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Datoctor name~~
~~Environmental Counting geometry: 1 Liter Soil Effic. cal time : 19-JUL-1995 08:56: 03 Effic, cal. oper.: HP Support~~

~~Processing Parameters ----~~

~~Stort channel~~
100 End channel

3700 S:noitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No

Yes Library-based eff: No Empirical Eff?
~~Enorg i 1.00000 Half life ratio~~
8.00000 Abund,y tolerance ance limit i 80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 3.00000 MDA Confid Level : 3.00000 %

-NID Peak Search Report it Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0
76.32 170 113 0.96 152.71 147 11 14.4 PB214 PB212 1 87.42 56 77 1.03 174.93 168 16 26.8 2.05E+00 PB214 PB212 1 90.05 37 73 1.09 180.20 168 16 43.2 PB214 0 93.12 73 71 1.20 186.33 183 8 23.4 TH234 TH234 0 186.54 31 64 1.33 373.31 369 9 50.2 RA226 g 6 238.64 221 34 1.02 477.57 473 18 7.9 9.01E-01 PB212 6 241.79 41 58 2.00 483.87 473 lb 52.1 RA224 0 295.29 89 32 1.24 590.94 584 14 17.0 PB214 0 300.48 17 13 1.07 601.32 598 7 43.9 PB212 0 338.58 56 36 1.12 677.55 673 12 25.3 AC228 0 352.03 89 30 0.97 704.47 703 8 16.9 PB214 0 510.U2 30 13 2.68 1021.60 1014 13 35.6 ANN-RD 0 583.57 61 21 0.88 1167.77 1160 14 20.4 TL208 0 609.55 28 7 1.48 1219.76 1214 14 12.4 BI214 0 661.80 68 16 1,51 1324.30 1319 9 16.1 CS137 0 726.71 17 5 1.93 1454.18 1448 10 34.6 BI212 0 860.34 17 2 1.55 1721.51 1717 8 27.9 TL208 0 911.19 58 0 1,79 1823.24 1819 10 13.1 AC228 0 969.37 20 14 0.58 1939.63 1932 12 44.1 AC228 / CO?Y
Pdst-NID Pock Socrch Roport (continu0d) Paga : 2 . Semple ID-Harkness #4 Acquisition date : 22-NOV-1997 06:01:39 f Area Bkgnd FWHM Channel L6ft Pw % Err Fit Nuclides g. Energy _ 0 1460.95 184 3 2.22 2922.91 2916 14 7.7 K40 I Intorference Report Interfering Interfered Nue) !de-Line Nuclide Line PB214 241.92 RA224 241.00 TL200 510.72 ANN-RD 511.00 t 0 I l e 4 i + 1h@-__.
g. Summ3ry of Nuclido Activity pogo 3 .Scmple ID : Harkness #4 Acquisition dSto 22-40V-1997 06:01:39 /
tol number of lines in spectrum

20
( ber of unidentified lines 0 Nu'ber of, lines-tentatively identified by NID 20 100.00% m Nuclide Type i natural Uncorrected Decay Corr Decay corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags X40 1.20E+09Y 1.00 1.095E-05 1.095E-05 0.084E-05 7.69 TL208 3.10M 2.56 2.124E-07 5.442E-07 1.113E-07 20.44 A BI212 60.55M 1.06 5.155E-07 5.463E-07 1.887E-07 34.55 A PB212 10.64H 1.01 8.116E-07 8.161E-07 0.644E-07 7.89 A DI214 19.90M 1.19 5.920E-07 7.037E-07 0.874E-07 12.42 A PB214 26.80M 1.14 4.872E-07 5.544E-07 0.935E-07 16.86 A RA224 3.66D 1.00 1.674E-06 1.676E-06 0.873E-06 52.10 g RA226 1600.00Y 1.00 1.326E-06 1.326E-06 0.666E-06 50.20 AC228 6.13H 1.01 8.648E-07 8.732E-07 1.147E-07 13.13 A TH234 24.10D 1.00 3.909E-06 3.910E-06 0.913E-06 23.36 KA Total Activity : 2.134E-05 2.190E-05 Nuclide Type : fission Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags CS137 30.10Y 1.00 2.655E-07 2.655E-07 0.428E-07 16.12 Total Activity i 2.655E-07 2.655E-07 ide Type : other Uncorrected Decay Corr Decay Corr 1-Sigma. Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags ANN-RD 109.74M 1.03 4.218E-08 4.355E-08 1.552E-08 35.64 Total Activity : 4.218E-08 4.355E-08 Grana Total Activity 2.165E-05 2.221E-05 Flcgo: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit
I l T i' t Nu'elido Lino Error Propagation Roport Pogo : 4 i
~~Jample ID~~

~~t. Harkness #4 Acquisition date : 22-NOV-1997 06:01:39 l 't l~~
\\

Nuclide Types natural i
~~Uncorrected Decay Corr 1-Sigma l Nuclide Energy %1.bn %Eff uCi/g uCi/g % Error Status~~
K40 1460.75 10.70*
~~7.057E-01 1.095E-05 1.095E-05 7.69 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 7.69%) i Absent Line Not Found ' TL208 277.36-6.50 2.596E+00 Line Not Found~~

<< INT Reject 510.72 22.50 1.671E+00 583.14 86.00*

1.504E+00 2.124E-07 5.442E-07 20.44 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 20.44%) 860.47 12.00 1.093E+00 5.909E-07 1.514E-06 27.87 OK-( 0.0%) ( 5.61%) (Decay-0.00%) (Area'27.87%) BI212-727.17 11.80* 1.259E+00 5.155E 07 5.463E-07 34.55 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 34.55%) Absent-Line Not Found 785.42 2.00 1.180E400 Absent Line Not Found 1078.62 0.97 -9.033E 01 Absent -Line Not Found 1620.56-2.75 6.538E-01 Absent-Line Not Found PB212 74.81 9.60 1.965E+00 77.11 17.50 2.066E+00 2.114E-06 2.126E-06 14.44 OK ( 0.0%) ( 4.12%) (Decay 0.00%) (Area 14.44%) 87.20 6.30 2.583E+00 1.554E 06 1.563E-06 26.80 OK-( 0.0%) ( 4.05%) (Decay 0.00%) (Area 26.80%) 238.63 43.10* 2.345E+00 8.116E-07 8.161E-07 7.89 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 7.89%) 300.09 3.27 2.463E+00 9.397E 07 9.449E-07 43.94 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 43.94%) .B1214 609.32 46'.09* 1.453E+00 5.920E 07 7.037E-07 12.42 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 12.42%) Absent Line Not Found 768.36 ' 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 Absent Line Not Found 1120.28 15.04 8.750E-01 Absent Line Not Found 1238.11 5.92 8.052E-01. Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Lina Not Found 1729.60 3.05 6.254E 01 Absent Line Not Fou.d 1764.51 15.92 6.173E-01 Absent Line Not Found PB214 74.81 6.33 1.985E+00 77.11 10.70 2.066E+00 3.458E-06 3.935E-06 14.44 OK -( 0.0%) ( 4.12 % ) (Decay 0.00%) (Area 14.44%) 87.20-3.70 2.583E+00 2.646E-0( 3.011E-06 26.80 OK -( 0.0%) -( 4.05%) (Decay 0.00%) (Area 26.80%) 89.80 1.03 2.684E+00 5.999E-06 6.826E-06 43.22 OK-( 0.0%) ( 4.07%) (Decay 0.00%) (Area 43.22%) Line Not Found

~~<< INT Reject 241.92.~~

7.47 2.823E+00 295.22 19.20 2.492E+00 8.42:E-07 9.583E-07 17.00 OK ('O.0%) (-5.09%) (Decay 0.00%) (Area 17.00%) 351.99 37.10* 2.207E+00 -4.872E-07 5.544E-07 16.86 OK ( 0.0%) ( 4.Sti) -(Decay 0.00%) (Area 16.86%) . Absent Line Not Found <785.95 1.09 1.180E+00~ Absent RA224 83.78 0.~ 21 = 2.430E+00

~~--Line Not'Found.~~

241.00 3.90* 2.823E+00 1.614E-06 1.676E-06 52.10 OK -( 0.0%) ( 5.05%) (Decay 0.00%) (Area 52.10%) RA326 185.99. 3.28* 3.208E+00 1.326E-06 1.326E-06 50.20 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 50.20%) If (
d Nu*clida Lino Error Propogotion Report (continued) Pcgo 5 ) . Sample ID : Harkness #4 Acquisition date 22-NOV-1997 06:01:39 l o N Nuclide Type natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status Line Not Found Absent AC228 209.40 4.55 3.050E+00 Absent Lina Not Found 270.30 3.77 2.639E+00 Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.269E+00 9.258E-07 9.347E-07 25.25 OK ( 0.0%) ( 4.72%) (Decay 0.00%) (Area 25.25%) Absent Line Not Found 409.40 2.23 1.977E+00 Absent Line Not Found 463.00 4.64 1.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 Absent Line Not Found 794.00 4.84 1.169E+00 Absent Line Not Found i 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 8.648E-07 8.732E-07 13.13 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 13.13%) Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 9.886E-01 5.265E-07 5.316E-07 44.05 OK 0.0%) ( 5.42%) (Decay 0.00%) (Area 44.05%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.791E+00 4.563E-06 4.564E-06 23.36 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 23.36%) 92.80 3.00 2.791E+00 3.909E-06 3.910E-06 23.36 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 23.36%) Absent Line Not Found 112.81 0.25 3.240E+00 Nuclide Types fission Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status CS137 661.62 84.62* 1.359E+00 2.655E-07 2.655E-07 16.12 OK (Decay 0.00%) (Area 16.12%) ( 0.0%) ( 5.10%) Nuclide Types other Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status ANN-RD $11.00 193.40* 1.671E+00 4.218E-08 4.355E-08 35.64 OK g ( 0.0%) ( 4.61%) (Decay 0.00%) (Area 35.64%) Flcg
~~" = Keyline~~
~~N e.- ,s J4!LLSTONE HEALTH PHYSICS-ENVIRONMENTAL 21-NOV-1997 20:06:55 /~~

~~Sample Information ----~~

~~bemple ID Harkness #5 Sample Quantity~~
~~1.00000E+03 g i~~
~~Sample Number~~
37479 Spctrm Collector : HP Environmental Sample Analyst

HP Environmental
)

~~Sample Deposition Information ----~~

~~No Dep. Duration l~~
~~D:p. Correction? D3 position Start : Deposition End~~
~~21-NOV-1997 19:56:09 i~~

~~Sample Decay / Count Information ----~~

~~Sample Date~~
~~21-NOV-1997 19:56:09 Ac@isition date : 21-NOV-1997 19:56:17 Docay time 0 00:00:08.29~~
~~% dead time~~
~~0.0%~~
~~Elepoed live time: 0 00:10:00.00 Elapsed real times 0 00:10:00.25 j~~

~~Detector Parameters ----~~

~~g Energy cal, time : 19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Detector name-~~
~~Environmental Counting geometry: 1 Liter Soil Effic, cal, time : 19-JUL-1995 08:56:03 Effic. cal. oper.: HP Support~~

~~Processing Parameters ----~~

~~Start-channel~~
100 End channel

3700

4.50000 Gaussian Sens.

10.00000 icnoitivity Critical level?

Yes Propagate Errors?: No Empirical Eff?

Yes Library-based eff: No Energy tolerance : 1.00000 Half life ratio

8.00000 Abundance limit 80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
.-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 2 74.92 61 71 0.90 149.91 146 15 23.6 2.83E+00 PB214 PB212 2 77.26 122 81 1.17 154.59 146 15 15.4 PB214 PB212 0 88.84 71 143 4.11 177.77 171 13 37.2 PB214 0 92.97 64 69 1.71 186.05 183 8 26.3 TH234 TH234 1 186.00 51 46 1.26 372.33 366 15 28.9 2.28E+00 RA226 1 187.50 27 45 1.26 375.20 366 15 53.5 1 0 210.20 48 83 3.84 420.65 412 14 42.9 AC228 4 238.56 276 40 1. 40 8 477.41 470 21 7.0 8.12E-01 PB212 4 241.48-49 68 1.78 483.26 470 21 42.9 PB214 0 '295.46 68-43 1.04 591.27 586 9 21.1 PB214 0 318.32 56 28 1.36-677.04 671 10 21.9-AC228 0 351.95 127 13 1.40 704.31 699 12 10.4 PB214 0 463.40 18 19 3.22 927.32 920 11 53.2 AC228 0 510.39. 33_ 33 2.09 1021.34 :1015.13~40.0 TL208 =0 582.87 99 6 1.77 1166.37 1159 13 11.3 TL208 0' 609.32 89 9 1,04 1219.31 1213 12 12.6 BI214 0 661.62 72-19 1.17'1323.95 1319 12 16.7 CS137-O. ~727.29 23 5 1.09 1455.33 1450 10 27.4 BI212 0. 794.93-16 4 1.62 1590.66 1586 9 34.5' AC228 l s CO "
~. -..... - - - {, Pcg3 1 2 (continued) );t-NID Peak Soorch Roport Acquisition date : 21.NOV-1997 19:56:17 Jcmplo ID : Harkness #5 ( 11 Energy Area Bkgnd FWRM Chbinel Left Pw % Err Fit Nuclides A 1 0 911.05 63 9 1.00 1822.95 1817 10 15.7 AC228 l 0 970.49 24 22 2.28 1941.87 1931 12 44.4 0 1120.02 23 8 1.52 2240.99 2236 9 31.7 BI214 O 1460.70 243 0 1.37 2922.40 2916 13 6.4 K40 l 0 1764.68 19 0 1.52 3530.32 3523 12 22.9 BI214 Intorforence RepErt i Interfering-Interfered Nuclide Line Nuclide Line PB214-241.92 PA224 241.00 3 TL208 510.72 ANN-RD 511.00 i 4 1 9 t 9
7.. Summary.of Nuclide Activity Pcgo 3 . Sample ID : Harkr.ess #5 Acquisition dato 21-NOV-1997 19:56:17 f *ntal number of lines in spectrum 24 6er of unidentified lines 2 ( Number of lines tentatively identified by NID 22 91.67% Naclide Type : natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags X40 1.28E+09Y 1.00 1.449E-05 1.449E-05 0.093E-05 6.41 TL208 3.10M 2.58 3.456E-07 8.928E-07 1.009E-07 11.30 A BI212 60.55H 1.06 7.0448-07 7.467E-07 2.047E-07 27.41 A FB212 10.64H 1.01 1.013E-06 1.019E-06 0.071E-06 6.98 A BI214 19.90M 1.19 5.984E-07 7.122E-07 0.895E-07 12.57 A PB214 26.80M 1.14 7.010E-07 7.985E-07 0.831E-07 10.41 A RA226 1600.00Y 1.00 2.172E-06 2.172E-06 0.627E-06 28.86 g AC328 6.13H 1.01 9.3498-07 9.440E-07 1.483E-07 15.71 A TH234 24.10D 1.00 3.462E-06 3.463E-06 0.877E-06 25.34 KA Total Activity : 2.443E-05 2.524E-05 Nuclide Type i fission Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags CS137 30.10Y 1.00 2.820E-07 2.820E-07 0.471E-07 16.72 Total Activity : 2.820E-07 2.820E-07 Jrand Total Activity 2.471E-05 2.552E-05 Flege: "K" = Keyline not found "M" = Manually accepted "E" - Manually edited "A" = Nuclide specific abn. limit I ( 1
q.. Nuclida* Lino Error Propcgetion Rcport Pcgo : 4 Scmple ID : Harkness #5 Acquisition deto : 21-NOV-1997 19:56:17 f Nuclide Type natural Uncorrected Decay Corr 1-Sigma 4 Huclide Energy %Abn %Eff uCi/g uCi/g % Error Status i K40 1460.75 10.70* 7.058E-01 1.449E-05 1.449E-05 6.41 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 6.42%) Absent l Line Hot Found TL208 277.36 6.50 2.596E+00 510.72 22.50 1.672E+00 3.919E-07 1.012E-06 40.03 OK i ( 0.0%) ( 4.61%) (Decay 0.00%) (Area 40.03%) 583.14 86.00* 1.506E+00 3.456E-07 8.92BE-07 11.30 OK ( 0.0%) ( 4.87%) (Decay 0.00%) (Area 11.30%) Absent Line Not Found 860.47 12.00 1.093E+00 DI212 727.17 11.80* 1.258E+00 7.044E-07 7.467E-07 27.41 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 27.41%) Line Not Found Absent 785.42 2.00 1.180E+00 Absent Line Not Found 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 FB212 74.81 9.60 1.991E+00 1.448E-06 1.456E-06 23.60 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 23.60%) 77.11 17.50 2.116E+00 1.486E-06 1.494E-06 15.43 OK ( 0.0%) ( 4.10 % ) (Decay 0.00%) (Area 15.43%) Absent Line Not Found 87.20 6.30 2.575E+00 238.63 43.10* 2.845E+00 1.013E-06 1.019E-06 6.98 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 6.98%) Absent Line Not Found 300.09 3.27 2.465E+00 3I214 609.32 46.09* 1.453E+00 5.984E-07 7.122E-07 12.57 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 12.57%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.752E"Oi 7.739E-07 9.209E-07 31.66 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (A:ea 31.66%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Lino Not Found 1729.60 3.05 6.254E-01 1764.51 15.92 6.173E-01 8.709E-07 1.036E-06 22.94 OK ( 0.0%) ( 4.80%) (Decay 0.00%) (Area 22.94%) PD214 '4.81 6.33 1.991S+00 2.196E-06 2.501E-06 23.60 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 23.60%) 77.11 10.70 2.116E+00 9.430E-06 2.768E-06 15.43 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 15.43%) q Absent Line Not Found 87.20 3.70 2.575E+00 89.80 1.03 2.639E+00 1.179E-05 1.343E-05 37.18 OK ( 0.0%) ( 4.06%) (Decay 0.00%) (Area 37.18%) 241.92 7.47 2.825E+00 1.050E-06 1.196E-06 42.87 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 42.87%) 295.22 19.20 2.491E+00 6.439E-07 7.334E-07 21.06 OK ( 0.0%) ( 5.08%) (Decay 0.00%) (Area 21.06%) 351.99 37.10* 2.207E+00 7.010E-07 7.985E-07 10.41 OK ( 0.0%) ( v.58%) (Decay 0.00%) (Area 10.41%) Absent Line Not Found 785.95 1.09 1.180E+00 RA226 185.99 3.2C 3.212E+00 2.172E-06 2.172E-06 28.86 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 28.86%) i
_ - - - - - ~ _ _ _ _ Ndolid3* Lina Error Propagation R3 port (continuod) Pcga i 5 .Scmple ID : Harkness #5 Acquisition date : 21-NOV-1997 19:56:17 kNuclide Types natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status AC228 209.40 4.55 3.044E+00 1.562E-06 1.577E-06 42.90 OK ( 0.0%) ( 4.93%) (Decay 0.000 (Area 42.90%) Line Not Found Absent 270.30 3.77 2.639E+00 Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.270E+00 9.310E-07 9.401E-07 21.93 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 21.93ti Absent Line Not Found 409.40 2.23 1.977E+00 463.00 4.64 1.801E+00 9.615E-07 9.709E-07 53.17 OK ( 0.0%) ( 4.42%) (Decay 0.00%) (Area 53.17%) Absent Line Not Found 478.20 0.14 1.758E+00 Absent Line Not Found ( 772.10 1.62 1.197E+00 794.80 4.84 1.168E+00 1.267E-06 1.279E-06 34.52 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 34.52%) Absent Line Not Found 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 9.349E-07 9.440E-07 15. */1 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 15.71%) Absent Line Not Found 964.60 5.45 9.927E-01 Absent Line Not Found 968.90 17.46 9.890E-01 Absent Line Not Foun6 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.786E+00 4.042E-06 4.042E-06 25.34 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 25.34%) 92.80 3.00 2.786E+00 3.462E-06 3.463E-06 25.34 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 25.34%) Absent Line Not Found 112.81 0.25 3.240E+00 Nuclide Types fission Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status CS137 661.62 84.62* 1.360E+00 2.820E-07 2.820E-07 16,72 OK ( 0.0%) ( 5.10%) (Decay 0.00%) (Area 16.72%) Fleg: "*" = Keyline 0
r* t' 6 'Hl3LSh0NEHEALTHPHYSICS-ENVIRONMENTAL 21-NOV-1997 17:51:48 $.(

~~Sample Information ----~~

~~Scmple ID~~
Harkness #6 Sample Quantity

1.00000E+03 g Scmple Number

37473 Spetrm Collector : HP Environmental Sample Analyst i HP Environmental

~~Sample Deposition Information ----~~

~~l D:p. Correction? : No Dep. Duration l D3 position Start : Deposition End i 21-NOV-1997 17:40:43 1~~

~~Sample Decay / Count Intformation ----~~

~~l Scter'.e Date~~
~~21-NOV-1997 17:40:43 A:quisition date : 21-NOV-1997 17:41:09 i~~
~~'rme~~
~~0.0%~~
C D0chy time 0 00:00:26.17 % det* Elepsed live time:~0 00:10:00.0 Elapse 4eal times 0 00:10:00.30 --- Detector Parameters ---- ( Enorgy cal. time : 19-JUL-1995 08:05:48 Energy cal. oper.: HP Support Datector name
~~Environmental Counting geometry: 1 Liter Soil Effic. cal. time : 19-JUL-1995 08:56:03 Effic. cal, oper.: HP Support~~

~~Processing Parameters ----~~

~~Stort channel~~
100 End channel

3700 Soncitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No Empirical Eff?

Yes Library-based eff No Enorgy tolerance : 1.00000 Half life ratio

8.00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level 3.00000 %
..-HID Peak Search Report It Energy. Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 2 74.97 107 108 1.17 150.02 143 17 19.1 8.09E-01 PB214 PB212 2-77.26 161 87 1.07 154.59 - 143 17 12.6 PB214 PB212 0 187.04 44 138 1.54 374.31 369 13 58.8 13 238.64 380 52 0.97 477.57 473 15 5.9 2.15E+00 9B212 3 241.56 43 52 1.61 483.41 473 15 38.7 RA224 -0 270.15 39 61 0.9P 540.63 535 11 42.0 AC228 0 0 281.34 76 135 6.71 563.02 551 33 48.9 0 295.08 100 23 1.23 590.50 586 10 13.4 PB214 0 338.47 79 51 1.33 677.34 671 13 21.8 AC228 0 351.96 110 35 1.20 704.33 700 8 13.0 PB214 .0 510,22 30 29 1.15 1021.02 1014 14 49.5 ANN-RD 0 583.16 122 12 1.25 1166.95 1162 9 10.3 -TL208 0 609.26~ -116 9 1.96 1219.17 1213 12-10.6 BI214 .0 661.27 50 10- 1.14 1323.25 1316 14 19.9 CS137 0. 727.32 .35 9 1,54 1455.39 1448 12 24'3 BI212 0 862.42-25 18 4.32 1725.67 1716 19 45.7 0 911.35 85 13 1.67 1823.55 1818 13 14.4 AC228 + 0 965.'02 15 9 1.77-1930.93 1921 13 49.9 AC228 O 968.98 50 7 1.54,1938.86 1934 10 17.5 AC228 ~0 1120.24 26 15 0.96 2241.43 2232 14 37.1 BI214 + + CO?Y ,...--m. +.,, ~,,,m.,, .,,.n.,,Q,..,y-r ,v.m..v.,y - -,,m. w,.r.c .m,
PQst-NZD Peak Search Report (continued) Page : 2 Lampl6 ID : Harkness #6 Acquisition date : 21-NOV-1997 17:41:09 ( Energy Area Bkgnd FhP1 Channel Left Pw % Err Fit Nuclides 0 1460.66 322 0 1.84 2922.33 2916 13 5.f K40 0 1764.48 23 0 2.02 3529.91 3523 12 20. BI214 Interference Report Interfering Interfered .......s.......... Nuclide Line Nuclide Line PB214 241.92 RA224 241.00 c; TL208 510.72 ANN-RD 511.00 1y i \\ E
O I g'^~ 4 -Summary;of;Nuclids Activity- -Page :- ; 'Scmp16 ID:r Harkness #6 Acquisition date s.21-NOV-1997.17:41:09 j 4 ( 'Al number ofilines:in spectrum 22' 3 lA. bar of-unidentified lines '19-86.~36% , -Numbar ofilinesLtentatively identified by-NID Nuclide TypeL:? natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide. Hlife' Decay uCi/g .uCi/g 1-Sigma Error % Error Flags >:K40 1.28E+09Y- -1.00 1.921E-05 1.921E-05 0.107E-05 5.57 TL208 . 3310M -2.76 4.260E-07 1.176E-06' O.121E-06 -10.31-A ,i BI2121 60.55M 1.06 1.053E-06 1.120E 0.272E-06. 24.29 A 'PB212- .10.64H 1.01 1.394E-06 1.403E-00 0.083E-06 5.95. A BI214
~~19. 90M 1.20 -7.811E-07 9.392E-0?~~
0.997E-07 10.62 A 41-PB214 26.80M 1.-15 6.075E-07 6.973E-07 0.9042-07 12.96 A RA224 .3.66D-1.00 1.758E-06 1.760E-06 0.680E.06 38.67 d AC228 6.13H 1.01 1.270E-06 1.284E-06 0.185E-06 14.41 A . Total Activity : 2.650E-05 2.758E-05 1 NuclideDType' fission Uncorrected Decay Corr Decay Corr 1-Sigma , Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags E CS13't-30.10Y 1.00 1.938E-07 1.938E-07 0.38EE-07 19.86 4 Total Activity : 1.938E-07' 1.938E /Nuclide Type-: other Uncorrected Decay Corr Decay Corr 1-Sigma yNuclide Hlife-Decay uCi/g uCi/g 1-Sigma Error % Error Flags ANN-RD-109.74M 1.03 4.150E-08 4.294E-08 2.127E-08 49.52 2. Total Activity : 4.150E-08 4.294E-08 Grand: Total Activity : 2.673E-05 2.782E-05 >. cFlagsi "K" = Keyline not.found "M" = Manually accepted "E"E--Manually: edited "A" = Nuclide specific abn. limit ) 'i e d d J -. = -
Nucli49 Lina Error Propagation Kaport Pcgo : 4 Simple ID : Harknesc #6 Acquisition date : 21-NOV-1997 17:41:09 ( Nuclide Type: natural Uncorrected Decay corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status K40 1460.75 10.70* 7.058E-01 1.921E-05 1.921E-05 5.57 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 5.57%) Absent Line Not Found TL208 277.36 6.5C 2.596E+00 Line Not Found

<< INT Reject 510.72 22.50 1.671E+00 583.14 86.00*

1.505E+00 4.260E-07 1.P;6E-06 10.31 OK ( 0.0%) ( 4.88%) (Docay 0.00%) (Area 10.31%) Absent LJne Not Found 860.47 12.00 1.093E+00 BI212 727.17 11.80* 1.258E+00 1.053E-06 1.120E-06 24.29 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 24.29%) Absent Line Not Found 785.42 2.00 1.180E+00 Absent Line Not Found i 1078.62 0.97 9.033E-01 Absent Line Not Found 1520.56 2.75 6.538E-01 PB212 74.81 9.60 1.994E+00 2.524E-06 2.539E-06 19.08 OK ( 0.0%) ( 4.15 % ) (Decay 0.00%) (Area-19.08%) 77.11 17.50 .2.116E+00- 1.965F-06 1.976E-06 12.58 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 12.58%) Absent Line Not Found 87.20 6.30 2.575E+00 238.63 43.10* 2.845E+00 1.394E-06 1.403E-06 5.95 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.95%) Absent Line Not Found 300.09 3.27 2.465E+00 bI214 609.32 46.09* 1.453E+00 7.811E-07 9.392E-07 10.62 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 10.62%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.750E-01 8.711E-07 1.047E-06 37.07 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 37.07%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 1764.51 15.92 6.173E-01 1.054E-06 1.268E-06 20.85 OK ( 0.0%) ( 4.80%) (Decay 0.00%) (Area 20.85%) PB214 74.81 6.33 1.994E+00 3.827E-06 4.393E-06 19.08 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 19.08%) 77.11 10.70 2.116E+00 3.213E-06 3.688E-06 12.58 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 12.58%) Absent Line Not Found { 87.20 3.70 2.575E+00 Absent Line Not Found 89.80 1.03 2.675E+00 Line Not Found

~~<< INT Reject 241.92 7.47 2.823E+00 295.22 19.20 2.493E+00 9.407E-07 1.080E-06 13.39 OK~~

( 0.0%) ( 5.09%) (Decay 0.00%) (Area 13.39%) 351.99 37.10* 2.207E+00 6.075E-07 6.973E-07 12.96 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 12.96%) Absent Line Not Found 785.95 1.09 1.180E+00 Absent Line Not Found RA224 83.78 0.21 2.430E+00 241.00 3.90* 2.825E+00 1.758E-06 1.760E-06 38.67 OK ( 0.0%) (-5.05%) (Decay 0.00%) (Area 38.67%) . Absent Line Not Found AC228 209.40 4.55 3.050E+00 270.30 3.77 2.640E+00 1.761E-06 1.779E-06 41.96 OK ( 0.0%) ( 5.15%) (Decay 0.00%) (Area 41.96%) w
4 Nuglidg Lino Error Propagation Rcport '(continued) Pcgo : 5 Stk.pid ID : Harkness #6 Acquieition dato : 21-NOV-1997 17:41,19 'Nuclide Type natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.269E+00 1.308E-06 1.322E-06 21.85 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 21.85%) Absent Line Not Found 409.40 2.23 1.977E+00 Absent Line Not Found 463.00 4.64 1.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 Absent Line Not Found 794.80 4.84 1.169E+00 Absent Line Not Found 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 1.270E-06 1.284E-06 14.41 OK g ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 14.41%) 964.60 5.45 9.924E-01 1.246E-06 1.259E-06 49.89 OK ( 0.0%) ( 5.44%) (Decay 0.00%) (Area 49.89%) 968.90 17.46 9.889E-01 1.295E-06 1.308E-06 17.53 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 17.53%) Absent Line Not Found 1587,90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Nuclide Type: fission Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status CS137 661.62 84.62* 1.360E+00 1.938E-07 1.938E-07 19.86 OK ( 0.0%) ( 5.10%) (Decay 0.00%) (Area 19.86%) Nuclide Type: other Unco.rected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status ANN-RD 511.00 193.40* 1.672E+00 4.150E-08 4.294F-08 49.52 OK ( 0.0%) ( 4.61%) (Decay 0.00%) (Area 49.52%) = Keyline -Flag:
\\
~~i ' 'e'. .4- < MILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 21-NOV-1997 17:33:47 (Sam'plo ID -: Harkness #7 Sample Quantity~~
~~1.00000E+03 g-~~

~~Sample Information ----~~

~~Semple Number~~
37472 Spetrm Collector : HP Environmental Sample Analyst

HP Environmental

~~Sample Deposition Information ----~~

~~No Dep. Duration Dep. Correction?~~
~~Deposition Start : Deposition End~~
~~21-NOV-1997 17:22:59 Sample Decay / Count Information ----~~
~~Sample Date~~
~~21-NOV-1997 17:22:59 Acquisition date : 21-NOV-1997 17:23:09 Dscay time 0 00:00:10.33~~
~~% dead time~~
~~0.0%~~
~~Elapsed live time: 0 00:10:00.00 Elapsed real times 0 00:10:00.27~~

~~Detector Parameters ----~~

~~19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Energy cal, time~~
~~-Dotoctor name~~
~~Environmental Counting geometry: 1 Liter Soil Effic. cal. time-: 19-JUL-1995 08:56:03 Effic cal. oper.: HP Support~~

~~Prec,essing Parameters ----~~

~~Start channel~~
100 End channel

3700 Sensitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No

Yes Library-based eff: No Empirical Eff?
~~Energy tolerance : 1.00000 Half life ratio~~
8.00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
t .-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left PW % Err Fit Nuclides 2 74.95 62 97 0.89 149.97 146 13 26.2 1.88E+00 PB214 PB212 2-77.15 ~107 84 0.90 154.37 146 13 16.0 PB214 PB212 3 87.42 48 73 0.93 174.94 171 19 31.2 1.29E+00 PB214 PB212 3 89.85 32 82 1.09 179.80 171 19 49.6 PB214 3 92.78 67 90 1.33 185.66 171 19 27.3 TH234 TH234 l 0 209.70 36-60 0.94 419.66 415 9 42.4 AC228 O-238.43 274 120 1.03 477.14 471 10 9.0 PB212 0 241.84 36 49 0.86-483.98 482 7 39.6 PB214 O' 270.06, 40 36 1.92 540.44 536 8 30.4 AC228 0 295.46 56 35- 0.86 591.27-587 9 23.3 PB214 0 328.14l 17 19 1.20 656.67 652 7 49.6 AC228 Oc 338.17 58 53 1.04 676.74 671 12 27.8 AC228 0 352.03 104 36 0.91 704.48 700 9 14.4 PB214 . Ct 510.34-40 36 1.37 1021.26 1014 16 37.5 TL208 0-583.48 112 33-1.66 1167.59 1161 16 15.2 TL208 609.78-55 35 1.33 1220.23 -1212 14 26.5 BI214 0. 661.64 68 12 1.51 1323.97 1319' 11 15.3 CS127' 795.15; 13 3 14 1.50 1591.09 1584 14 29.7 AC228 Co e x
,.c r[ Post-NID Pock Socrch Report --(continuad)- Pcgo:n-.
2-

Scmple

ID F Harkness'#7 Acquisition date.: 21-NOV-1997 17:23:09-k Energy =
iArea._ -Bkgnd-FWHM Channel Left Pw % Err: Fit-Nuclides- .. g O. ~860118 22-2 1.28i1721.19 1716 10 25.5: TL208: 0- .911.02- ~52 15 1.09 1822.91 1818 10 19.5 AC228 0.- 965.41/ 24 - 17__- '1.94 1931.71 1922 13-40.6-AC228 4 4 ~ 0: 969.00 42 14-1.49 1938.89 1935 12 22.7 AC228 1 0 1119.82 24-5- 3'.23 2240.60- 2236 10 27.3 BI214 j -0L 1460.61 337-0 1.88 2922.23 2913 16 5.4 K40 Interference Report-Interferir.g ' Interfered 1-1 Nuclide~ Line Nuclide Line -i PB214 241,92 RA224 241.OC p -- TL208 510.72 ANN-RD 511.00 h i 5 3 + E 4 i 4 f: N s a t 9 S.' % ,. -i 4 ~,l-- ,m, .., - ~ ~ 4 L h y.-, 's.. -,--.4
" Summary of Nuclids Activity P c g e _:. -3 " Semple ID1:-: Harkness #7 Acquisition date_ 21-NOV-1997 17:23:09
~~[0 301 number of lines in spectrum 24 3..Aber of unidentified-lines-24; 100.00%~~
0 Number of> lines tentatively identified by NID Nuclide: Type :-natural _ Uncorrected - Corr Decay corr 1-Sigma Decay /g 1-Sigma Error % Error Flags uCi 1Nuclide Hlife Decay uCi/g- - K4 0 - -1.28E+09Y 1.00 2.010E-05 2.010E 0.109E-05 5.45 TL208 3.1'OM-2.60 3.883E-07 1.011E-06 0.154E-06 15.24 A
~~PB2121 10.64H-1.01 1.008E-06 1.013E-06 0.091E-06 9.02' A~~
_BI214 19;90M-1.19 3.701E-07 4.410E-07 -1.169E-07 26.50 A PB214-26.80M-1.14 5.739E-07 6.542E-07 0.943E-07 14.41 A -AC228 6.13H 1.01 7,804E-07 7.880E-07 -1.539E-07 19.53 A TH234 24.10D 1.00 3.597E-06 3.598E-06 0.983E-06 27.32 KA~ (- Total Activity 2.682E-05 2.760E-05
Nuclide--Type-: fission Uncorrected Decay Corr Decay Corr 1-Sigma-

Nuclide,
-Hlife-Decay uci/g uCi/g 1-Sigma Error % Error Flags 1.00- 2.681E-07 -2.681E-07 0.411E-07 15.34 CS137 -30.10Y; 1 Total Activity : 2.681E 2.681E-07 Grand Total Activity i 2.709E-05 2.787E-05 i..-3s : K" =.Keyline not found "M" = Manually accepted E" - Manually edited "A" = Nuclide-specific abn. limit I 9 I .T y
?v 7 3. Nuclids-Lino Error Pro agetion Report Pcga 4 ? semple ID's--Harkness #
~~Acquisition date : 21-NOV-1997 17:23:09~~
[- Nuc'lide Typen natural ^ Uncorrected Decay Corr 1-Sigma %Abn %Eff uCi/g uCi/g- % Error Status Nuclide-. Energy. . 10.-70* 7.058E-01 2.010E-05' 2.010E 5.45 ~OK - X40 1460.75 (-_0. 0% ) ( 4.45%)- (Decay 0.00%) (Area 5.45%) Absent Line Not Found TL208 277.36-6.50-2.596E+00 510.77 -22.50 1.672E+00 4.731E-07 1.231E 37.54 OK-( 0.0%) ( 4.61%) (Decay 0.00%) (Area 37.54%) 583.14 86.00* 1.504E+00 3.883E-07 1.011E-06 15.24 OK -( 0.0%) ( 4.88%) (Decay 0.00%)- (Area 15.24%)' 860.47 12.00 1.094E+00 7.409E-07 1.928E 25.48 OK ( 0.0%) ( 5.61%) (Decay 0.00%) (Area 25.48%) PB212 74.81 9.60 1.992E+00 1.457E-06 1.465E-06 26.19 OK 1: ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 26.19%) 77.11 17.50 2.110E+00 1.306E-06 1.314E-06 15.97 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 15.97%)_ 87.20 6.30 2.584E+00 1.323E-06 1.330E-06 31.15 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 31.15%). 238.63 43.10* 2.846E+00 1.008E-06 1.013E 9.02 OK ( 0.0%) (-5.04%) (Decay 0.00%) (Area 9.02%)~ Absent Line Not Found 300.09 3.27 2.465E+00 BI214 609.32 46.09* 1.452E+00 3.701E-07 4.410E-07 26.50 OK-( 0.0%) ( 4.96%) (Decay 0.00%) (Area 26.50%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.753E-01 8.082E-07 9.630E-07 27.27 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 27.27%) r Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02. 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PB214 74.81 6.33 1.992E+00 2.210E-06 2.519E-06 26.19 OK ( 0.0%) ( 4.15%) (Decay.0.00%) (Area 26.19%) 77.11 -10.70 2.110E+00 2.137E-06 2.436E-06 15.97 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 15.97%) 87.20 3.70-2.584E+00 2.252E-06 2.568E-06 31.15 -OK ( 0 0%) ( 4.05%) (Decay 0.00%) (Area 31.15%)- 89.80 1.03 2.677E+00 5.225E-06 5.956E-06. 49.64 OK 1 _ ( 0. 0%)- ( 4.07%) (Decay 0.00%) (Area 49.64%) -241.92' 7.47 2.823E+00 7.709E-07 8.788E-07 39.62 OK ( 0.0%) (.5.05%) (Decay 0.00%) (Area 39.62%) -295.22 19.20 2.491E+00 5.300E-07 6.042E-07 23.31 - OK ( 0.0%)' ( 5.08%)- (Decay 0.00%) (Area 23.31%) 351.99 37.10*- 2.207E+00 5.739E-07 6.542E-07 14.41 OK. ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 14.41%) Absent Line Not Found 785.95 1.09 1.180E+00 AC228; 209.'40 . 4.55 3.048E+00 1.167E-06 1.178E-06 42.45 OK (Decay 0.00%)- (Area 42.45%) _( 0. 0%): -( 4. 93%) _1.810E 1.828E-06 30.41-OK 3.77 2.640E+00-270.30 - ( 0.0%)- (~5.15%)- (Decay 0.00%) (Area 30.41%) 328.00 3.36 2.319E+00 9.720E-07 9.815E-07 49.59 ~OK . (E 0. 0%) (- 4. 83%) _ (Decay 0.00%) (Area 49.59%) T t
I ~[ , e Nuclida Lino Error Propagation Roport (continusd) Pcga : 5 .Stmple ID : Harkness #7 Acquisition date : 21-NOV-1997 17:23:09 k -Nuclide Type natural Uncorrected Decay Corr-1-sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status 338.40 12.01 2.271E+00 9.657E-07 9.751E-07 27.79 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 27.79%) Line Not Found Absent 409.40 2.23 1.977E+00 Line Not Found Absent 463.00 4.64 1.802E+00 Line Not Found Absent 478 2D 0.24 1.758E+00 Line Not Found Absent 772.10 1.62 1.197E+00 794.80 4.84 1.168E+00 2.629E-06 2.655E-06 29.69 OK ( 0.0%) .( 5.48%) (Decay 0.00%) (Area 29.69%) Absent Line Not Found 835.60 1.82 1.121E+00 911.07. 29.00* 1.042E+00 7.804E-07 7.880E-07 19.53 OK 1 ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 19.53%) 964.60 5.45 9.920E-01 1.987E-06 2.007E-06 40.60 OK ( 0.0%) ( 5.44%) (Decay 0.00%) (Area 40.60%) 968.90 17.46 9.889E-01 1.101E-06 1.112E-06 22.72 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 22.72%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.779E+00 4.199E-06 4.200E-06 27.32 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 27.32%) 92.80 3.00 2.779E+00 3.597E-06 3.598E-06 27.32 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 27.32%) Abuent Line Not Found 112.81 0.25 3.240E+00 Nuclide Type: fission Uncorrected Decay Corr 1-Sigma Nuclide Energy- %Abn %Eff uCi/g uCi/g % Error Status CS137 661.62 84.62* 1.359E+00 2.681E-07 2.681E-07 15.34 OK ( 0.0%) ( 5.10%) (Decay 0.00%) (Area 15,34%) = Keyline Flag: t 4
3 MILLSiONE HEALTH PHYSICS-ENVIRONMENTAL ~ 25-NOV-1997 14:56:01 r .c

~~Sample Information ----~~

~~[ le ID Harkness #8 Sample Quantity~~
~~1.00000E+03 g~~
~~( le Number~~
37515 Spctrm Collector i HP Environmental Sample Analyat

HP Environmental

~~Sample Deposition Information --- :~~

~~No Dep. Duration Dap. Correction?~~
~~Deposition End~~
~~22-NOV-1997 11:34:37 Daposition Start~~

~~Sample Decay / Count Information ----~~

~~Scmple Date~~
~~22-NOV-1997 11:34 37 Ac@isition date : 22-NOV-1997 11:34:43 Dacsy time 0 00:00:06.20~~
~~% dead time~~
~~0.0% '~~
~~Elepsed live times 0 00:10:00.00 Elapsed real time 0 00:10:00.30~~

~~Detector Parameters ----~~

~~19-JUL-1995 08:05:48 Energy cal, oper.: HP Support EnDrgy cal. time 1~~
~~Datector name~~
~~Environmental Counting geometry: 1 Liter Soil Effic, cal. time : 19-JUL-1995 08:56:03 Effic. cal. oper.: HP Support~~

~~Processing Parameters ----~~

~~Start channel~~
100 End channel

3700 Sensitivity

4.50000 Gaussian Sens.

10.00000 Critical-level?

Yes Prupagate Errors?: No
~~- Empirical Eff?~~
Yes Libra n-based eff: No

1.00000 Half life ratio

8.00000 Energy tolerance Abundance limit i 80.00000 WTM error limit

3.00000 MDA Width _ (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
De-*-NID Peak Search Report Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 3 74.87 142 120 1.28 149.81 145 13 16.0 3.15E+00 PB214 PB212 3 77.18 156 86 0.99 154.43 145 13 12.9 PB214 PB212 1 87.39 56 98 0.93 174.88 172 12 30.5 3.91E+00 PB214 PB212 1 89.85 70 95 1.09 179.80 172 12 25.6 PB214 0 93.26 79 106 1.41 186.61 183 6 25.0 TH234 TH234 0 186.24 84 117 1.35 372.70 366 12 27,9 RA226 4 0 209.05 67 79 1.62 418.35 412 12 29.2 AC228 0 238.50 386 133 1.09 477.30 471 11 7.8 PB212 0 242.11 52 84 1.19 484.51 482 10 38.5 PB214 0-277.12 33 27 1.50 554.57 551 7 31.9 TL208 0 295.39-96 46 1.09 591.14 587 9 16.5 PB214 0 299.88 51 32 1.23 600.11 596 8 23.6 PB212 0-338.68 68 82 1.03 677.77 673 11 28.3 AC228 0 351.97 159 35 1.12 704.34 699 11 10.7 PB214 0-462.60 36 10 1.03 925.72 920 10 23.2 AC228 0 510.94 53 .19 2.10 1022.45-1016 13 21.9 TL208 0 583.06 132 16 1.01 1166.75 1163 10 10.3 TL208 0 609.09 130 '20 1.33 1218.85 1213 12 11.3-BI214 ~ CO Y
' Post.NID Pack Sacrch Report (continusd) Pcga : 2 Sh.mplo ID : Harkneso #8 Acquisition dato : 22-NOV-1997 11:34:43 4 T* Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 727.71 27 29 0.90 1456.17 1449 16 47.3 BI212 910.92 101 0 1.94 1822.70 1817 11 10.0 AC228 0 968.90 51 7 1.38 1938.69 1934 11 17.5 AC228 0 1119.80 31 6 3.43 2240.56 7234 13 24.6 BI214 0 1460.65 239 0 2.24 2922.31 2916 13 6.5 K40 0 1764.24 30 0 1.44 3529.43 3523 12 18.3 BI214 Intorference Report Interfering Interfered Nuclide Line Nuclide Line TL208 510.72 ANN-RD 511.00 g 4
Summary of Nuclido Activity Paga : 3 Sample ID : Harkness #8 Acquisition date : 22-NOV-1997 11:34:43 s - 4 Total number of lines in spectrum 24 0 i (.. Number of-unidentified linesd r of lines tentatively identi'fied by NID 24 100.00% w. h ide Type : natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags K40 1.28E+09Y 1.00 1.426E-05 1.426E-05 0.092E-05 6.47 TL208 3.10M 2.56 4.590E-07 1.176E-06 0.121E-06 10.33 A BI212 60.55M 1.06 8.316E-07 8.812E-07 4.170E-07 47.32 A P3212 10.64H 1.01 1.418E-06 1.425E-06 0.111E-06 7.76 A BI214 19.90M 1.19 8.710E-07 1.035E-06 0.117E-06 11.27 A PB214 26.80M 1.14 8.759E-07 9.968E-07 1.070E-07 10.74 A RA226 1600.00Y 1.00 3.599E-06 3.599E-06 1.005E-06 27.92 AC228 6.13H 1.01 1.506E-06 1.520E-06 0.151E-06 9.95 A TH234 24.10D 1.00 4.268E-06 4.268E-06 1.065E-06 24.95 KA 0 Total Activity : 2.808E-05 2.916E-05 Grand Total Activity : 2.808E-05 2.916E-05 Flags: "F" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit ( \\ 6
~~Nuc1ida Lin3 Error Prop getion Report Page :~~
4 Sample ID : Herkness-#8-Acquisition date : 22-NOV-1997,11:34:43 (= -lide Type natural L A: Uncorrected Decay Corr 1-Sigma l h ide Energy %Abn %Eff uCi/g uCi/g % Error Status K4v 1460.75 10.70* 7.058E-01 1.426E-05 1.426E 6.47 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 6.47%) TL208 277.36 6.50 2.597E+00 8.725E-07 2.236E-06 31.93 oOK i ( 0.0%) ( 5.18%) (Decay 0.00%) (Area 31.93%). 510.72 22.50 1.670E+00 6.362E-07 1.631E-06 21.92 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 21.92%) 583.14 86.00* 1.505E+00 4.590E-07 1.176E-06 10.33 OK ( 0.0%) _( 4.88%) (Decay 0.00%) (Area 10.33%) Line Not Found Absent 860.47 12.00 1.093E+00 BI212 727.17 11.00* 1.257E+00 8.316E-07 8.812E-07 47.32 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 47.32%) Line Not Found Absent 785.42 2.00 1.180E+00 Absent Line Not Found "( 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 PB212 74.81 9.60 1.988E+00 3.359E-06 3.377E-06 16.04 OK ( 0.0%) ( 4.15%) (Dechy 0.00%) (Area 16.04%) 77.11 17.50-2.111E+00 1.897E-06 1.907E-06 12.93 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 12.93%) 87.20 6.30 2.582E+00 1.538E-06 1.547E-06 30.51 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 30.51%) 4 238.63 43.10* 2.846E+00' 1.418E-06 1.425E-06 7.76 OK ( 0.0%) ( 5.04%) (Decay-0.00%) (Area 7.76%) 300.09 3.27 2.466E+00 2.867E-06 2.883E-06 23.62 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 23.62%) BI214 609.32 46.09* 1.454E+00 8.710E-07 1.035E-06 11.27 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 11.27%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.753E-01 1.061E-06 1.261E-06 24.59 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 24.59%) + Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 2377.65 4.02 7.387E-01 Absent Line Not Found -1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 1764.51 15.92 6.174E-01 1.375E-06 1.634E-06 18.26 OK ( 0.0%) ( 4.80%) (Decay 0.00%) (Area 18.26%) .PB214 74.81 6.33 1.988E+00 -5.094E-06 5.797E-06 16.0< OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 16.04%) 77.11 10.70 2.111E+00 3.102E-06 3.530E-06 12.93-OK 4 ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 12.93%) 87.20 3.70 2.582E+00- 2.619E-06 2.980E-06 30.51 - OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 30.51%) 89.80 1.03 2.677E+00 1.150E-05 1.309E-05 25.61 OK ( 0.0%) ( 4.07%) (Decay-0.00%) (Area 25.61%) 241.92 7.47 2.821E+00 1.109E-06 1.262E-06 38.49 OK ( 0.0%) ( 5.06%) (Decay 0.00%) -(Area 38.49%) '295.22 19.20 2.491E+00- 9.007E-07 3.025E-06 16.48-OK ( 0.0%) (-5.08%) (Decay 0.00%) (Area 16.48%) 351.99 37.-10* - 2.207E+00.8.759E-07 9.968E-07-- 10.74 -OK ( 0.0%). ( 4.58%) (Decay 0.00%) (Area 10.74%) r _ + m
Nuclid3 Lino Error Prop.getion ROport (continuod) pega : 5 Samplo ID : Harknoso #8 Acquicition dato : 22-NOV-1997 11:34:43
~~3. a a~~
natural (.alideTyper Uncorrected Decay Corr 1-Sigma h ide Energy %Abn %Eff uCi/g uCi/g % Error Status Line Not Found Absent 785.95 1.09 1.180E+00 RA226 185.99 3.28* 3.210E+00 3.599E-06 3.599E-06 27.92 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 27.92%) AC228 209.40 4.55 3.052E+00 2.187E-06 2.208E-06 29.23 OK ( 0.0%) ( 4.93%) (Decay 0.00%) (Area 29.23%) Line Not Found Absent 270.30 3.77 2.639E+00 Line Not Found Absent 328.00 3.36 2.320E+00 338.40 12.01 2.268E+00 1.124E-06 1.134E-06 28.28 OK ( 0.0%) ( 4.72%) (Decay 0.00%) (Area 28.28%) Line Not Found Absent 409.40 2.23 1.977E+00 463.00 4.64 1.803E+00 1.959E-06 1.978E-06 23.15 OK ( 0.0%) ( 4.41%) (Decay 0.00%) (Area 23.15%) Line Not Found Absent ( 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 Absent Line Not Found 794.80 4.84 1.169E+00 Absent Line Not Found 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 1.506E-06 1.520E-06 9.95 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 9.95%) Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 9.890E-01' 1.341E-06 1.354E-06 17.47 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 17.47%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2,795E+00 4.982E-06 4.982E-06 24.95 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 24.95%) 92.80 3.00 2.795E+00 4.268E-06 4.268E-06 24.95 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 24.95%) Absent Line Not Found 112.81 0.25 3.240E+0? Flag: "*" = Keyline i
t 2 '.i , MILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 25-NOV-1997 14:57:20 f

~~Sample Information ----~~

~~k. e ID~~
Harkness #9 Sample Quantity 1.00000E+03 g Sh..,1e Number

37516-Spctrm Collector HP Environmental Sample Analyst

-HP Environmental

~~Sample Deposition.Information ----~~

~~D3p. Correction? :-No Dep. Duration D3pocition Start : Deposition End~~
~~22-NOV-1997 12:53:24~~

~~Sample Decay / Count Information ----~~

~~Sample Date~~
~~22-NOV-1997 12:53:24 Ac@isition date : 22-NOV-1997 12:53:30 Dacoy time 0 00:00:06.22~~
~~% dead time~~
~~0.1%~~
~~Elepced live time: 0 00:10:00.00 Elapsed real time: 0 00:10:00.31~~

~~Detector Parameters ----~~

J
19-JUL-1995 08:05:48 EnerW cal, oper.: HP Support Energy cal. time Datoctor name

-Environmental Counting geometry: 1 Liter Soil Effic cal time : 19-JUL-1995 08:56:03 Effic. cal. oper.: HP Support

~~Processing Parameters ----~~

~~Start channel~~
100 End channel

3700 Sensitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No Empirical Eff?

Yes Libra n-based eff: No Energy tolerance : 1.00000 Half life ratio

8.00000
~~- Abundance limit~~
80.00000 WTM error limit

3.00000 MDA' Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nucli, des 3 75.02 127 126 1.00 150.11 146 13 16.4 5.76E-01 PB214 PB212 '3 77.14 153 109 1.02 154.36. 146 13 14.2 PB214 PB212-5 ~ 87.45 73 102 1.33 175.00 172. 11 24.3 8.82E-01 PB214 PB212 5 90.04 50 90 1.04 180.18 172 11 33.9 PB214 0 93.08 105 131 1.38-186,26 183 9 22.0 TH234 TR234 I0 185.95 88 95 0.99 372.12 366 12 24.5 RA226 5 238.61 419 54 1.08 477.51 474 14 5.6 1.46E+00 PB212 5 241.53 72 75 1.62 483.36 474 14 24.3 PB214 0 277.57 59 57-1.61' 555.48 549 15 30.5 TL208 0. 295.16 112 43 1.14 590.67 586 10 14.4 PB214 .0 300.41 21 44 0.73 601.18 597 8 57.6 PB212 -0 327.89 35 27 1,64 656.16 651 9 31.6 AC228 .- 0 338.15 81 44 1.21 676.69 671 11 19.3 AC228 0 351.81 155
~~47. U.92 704.03 699 11 11.7 PB214 0~~
511'27 28 30 1.73 1023.11 1015 12 43.9 TL208 0 583.24 137 26 1.46-1167.12 1161 13 11.5 TL208 0 609.33 140 15 1.55 1219.33 1214 14 10.2 BI214 0 727.38-37 14 1.68 1455.51 1448 14 27.0 BI212 ~ C 0" 3
Pdst-NID POOk Scorch R3 port (continu3d) P0ga : 2
~~Harkness #9 Acquisition date : 22-NOV-1997 12:53:30~~
.S2mple ID ( Energy _ Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 869.31 14 3 1.42 1739.50 1734 11 34.8 0 911.03 102 11 1.49 1822.93 1816 15 12.2 AC228 0 933.96 19 3 1.44 1868.80 1865 8 29.5 BI214 0 968.01 61 41 5.13 1938.51 1923 22 28.9 AC228 0 1121.29 28 15 1.49 2243.52 2236 16 36.6 0 1460.66 255 0 1.81 2922.33 2915 16 6.3 K40 Intorference Report Interfering Interfered Nuclide Line Nuclide Line 1 PB214 241.92 RA224 241.00 TL208 510.72 ANN-RD 511.00
l 'SummrfofNuclidsActivity pago : - 3 i Harknees #9= Acquisition date : 22-NOV-1997 12:53:30- .I . Sample ID : Total number of 11'nes in spectrum 24 ,_I ber of unidentified lines 1 < \\-
~~)erlof lines tentatively identified by NID 23 95.83%~~
~~i ' LNuclide Type _ natural-Uncorrected-Decay Corr Decay Corr' 1-Sigma Nuclide-Hlife Decay-uCi/g uCi/g 1-Sigma Error % Error Flags 1.K40 1.28E+09Y 1.00 1.521E-05 1.521E-05 0.095E-05 6.26 I 7L208.~~
~~3. TOM-2.56 4.768E-07 1.222E-06 0.140E-06 11.48 A~~
BI212 60.55M 1.06. 1.123E-06 1.190E-06 0.322E-06 27.03 A PD212 10.64HL 1.01 1.540E-06 1.549E-06 0.087E-06 5.60 A ~BI214- - 19.90M 1.19 9.388E-07 1.116E-06 0.114E-06 10.23 A PB214 26.80M 1.14 8.525E-07 9.701E-07 1.138E-07 11.73 A RA226 1600.00Yt 1.00 3.780E-06 3.780E-06 0.928E-06 24.54 I AC228 6.13H 1.01 1.523E-06 11.537E-06 0.188E-06 12.20 A TH234 24.10D 1.00 5.636E-06 5.637E-06 1.239E-06 21.98 KA -Total-Activity : -3.108E-05 3.221E-05 l s t Grand Total Activity.: 3.108E-05 3.221E-05 f Flagst- ' K" = Keyline not found "M"-= Manually accepted "E" = Manually edited "A" - Nuclide specific abn. limit t k-4 i. f W .t .-4, ., _,..~
1 ' e. ' 'g N6clida Lino Error Propagetion Report Pcga : 4 Scmple ID : Harkness #9-Acquisition date : 22-NOV-1997 12:53:30 f\\ Nt 'de Type natural Uncorrected Decay Corr 1-Sigma Uuclide Energy %Abn %Eff uCi/g uCi/g % Error Status X40 1460.75 10.70* 7.058E-01 1.521E-05 1.521E-05 6.26 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area-6.26%) TL208 277.36 6.50 2.594E+00 1.584E-06 4.060E-06 30.49 OK ( 0.0%) ( 5.18%) (Decay 0.00%) (Area 30.49%) 510.72 22.50 1.670E+00 3.312E-07 8.516E-07 43.91 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 43.91%) 583.14 86,00* 1.505E+00 4.768E-07 1.222E-06 11.48 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area l' 48%) Line Not Found 860.47 12.00 1.093E+00 Absen. BI212 727.17 11.80* 1.258E+00 1.123E-06 1.190E-06 27.03 OK ( ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 27.03%) Line Not Found 785.42 2.00 1.180E+00 Absent-Line Not Found 1078.62 0.97 9.033E-01 Absent 1620.56 2 75 6.538E-01 Line Not Found Absent PB212-74.81 3,60 1.996E+00 2.978E-06 2.994E-06 16.36 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 16.36%) 77.11 17.50 2.110E+00 1.862E-06 1.872E-06 14.23 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 14.23%) 87.20 6.30 2.585E+00 2.016E-06 2.027E-06 24.29 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 24.29%) 238.63 43.10* 2.845E+00 1.540E-06 1.549E-06 5.60 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.60%) 300.09 3.27 2.463E+00 1.200E-06 1.207E-06 57.63 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 57.63%) 1 609.32 46.09* 1.453E+00 9.388E-07 1.116E-06 10.23 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 10.23%) Line Not Found 768.36 4.89 1.202E+00 Absent 934.05 3,16 1.020E+00 2.587E 06 3.075E-06 29.53 OK ( 0,0%) ( 5.56%) (Decay 0.00%) (Area 29.53%) Line Not Found 1120.28 15.04 8.750E-01 Absent 1238.11 5.92 8.052E-01 Line Not Found Absent 1377.65 4.02 7.387E-01 Line Not Found Absent Line Not Found 1509.19 2.19 6.885E-01 Absent 1729.60 3.05 6.254E-01 Line Not Found Absent-Line Not Found 1764.51 15.92 6.173E-01 Absent PB214 74.81 6.33 1.996E+00 4.516E-06 5.140E-06 16.36 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 16.36%) 77.11 10.70 2.110E+00 3.045E-06 3.465E-06 14.23 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 14.23%) 87.20 3.70 2.585E+00 3.432E-06 3.906E-06 24.29 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 24.29%) 89.80 1.03 2.684E+00 8.164E-06 9.291E-06 33.89 OK ( 0.0%) ( 4.07%) (Decay 0.00%) (Area 33.89%) 241.92 7.47 2.825E+00 1.529E-06 1.740E 06 24.26 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 24.26%) 295.22 19.20 2.492E+00 1.053E-06 1.199E-06 14.45 OK ( 0.0%) ( 5.09%) (Decay 0.00%) (Area 14.45%) 351.99 37.10* 2.208E+00 8.525E-07 9.701E-07 11.73 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 11.73%) k
i '
a I'*
Nuclido Lino--Error-Propagation Report (continued) Page : 5 'Acmple-ID.:-Harkness #9 AcquisitionLdate : 22-NOV-1997 12:53:30 q ? f fi -k ~'de. Types natural Uncorrected Decay Corr 1-Sigma Nuclide= ' Energy -%Abn .%Eff_ uCi/g uCi/g, % Error' Absent Status Line Not Found. 785.95 1.09 1.180E+00 RA326 185.99 -3.28* 3.212E+00 3.780E-06 3.780E 24.54-OK ( 0.0%) . ( 4.85%) (Decay 0.00%) (Area 24.54%) Line Not Found , AC228-209.40 4.55 3.050E+00 Absent Line Not Found 270.30 3.77 ~ 2.639E+00 -Absent 328.00 3.36 _ 2.320E+00 2.022E-06 2.041E-06 31.63 OK ( 0.0%) ( 4.83%) (Decay 0.00%) (Area 31.63%) 4 G .338.40 12.01 2.271E+00 1.343E-06 1.356E-06 19.29 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 19.29%) ) Line Not Found Absent 409.40 2'.23 1.977E+00 Line Not Found' Abri;t q 463.00 4.64 1.802E+00

~~- Line-Not Found 478.20 0.24 1.758E+00 Absent-Line Not Found Absent 772.10 1.62 1.197E+00 794.80 4.84 1.169E+00.-----~~

Line Not-Found Absent Line Not-Found 835.60 . 1.82 1.121E+00 Absent' 911.07 29.00*- 1.042E+00 1.523E-06 1.537E-06 12.20 - .OK i ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 12.20%) l-964.60 5.45 _ 9.927E-01 Line-Not Found Absent 968.90 -17.46 9.891E-01 1.599E-06 1.614E-06 28.90 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 28.90%) Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found Absent 1630.40. 1.95 6.510E-01 FTH234-63.29 3.90* 1.299E+00. . Line-Not Found Absent f 92.38 2.57 2.789E+00 6.579E-06 6.580E-06 21.98 OK ( 0. 0%)- ( 4.10%)- (Decay 0.00%) (Atea 21.98%) 92.80 3.00 __2.789E+00 5.636E-06 54637E-06 21.98 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area-21.98%) Line Not Found 4' Absent 112.81 0.25 3.240E+00
~~Flagt~~
"*a~= Keyline-e e t 5 ,j_ ' l\\ h-p .~ t 4- ~ v = t r~ -vr-rw '- w,-- --.y m- -w. -=
..F.. MILLSTONE HEALTH PHYSICS-ENVIRONMENTAL ~ 21-NOV-1997 23:52:20

~~Sample Information ----~~

~~7 ple ID~~
Harkness #10 Sample Quantity

1.00000E+03 g

37487 Spetrm Collector : HP Environmental udmple-Number Sample Analyst

HP Environmental

~~Sample Deposition Information ----~~

~~D:p. Correction? No Dep. Duration Deposition End~~
~~21-NOV-1997 23:41:26 Dsposition Start~~

~~Sample Decay / Count Information ----~~

~~21-NOV-1997 23:41:26 Acquisition date : 21-NOV-1997 23:41:33 Sample.Date Dacey time 0 00:00:07.55~~
~~% dead time~~
~~0.0%~~
~~Elepsed live time: 0 00:10:00.00 Elapsed real time: 0 00:10:00.22~~

~~Detector Parameters ----~~

19-JUL-1995 08:05:48 Energy cal. oper.: HP Support Ensrgy cal. time g Datoctor name

Environmental Counting geometry: 1 Liter Soil Effic. cal, time : 19-JUL-1995 08:56:03 Effic. cal, oper.: HP Support

~~Processing Parameters ----~~

~~Stoit channel .: 100 End channel~~
3700 Sansitivity

4.50000 Gaussian Sens.

10.00000
~~-Critical level?~~
Yes Propagate Errors?: No

Yes Library-based eff: No Empirical Eff?
~~Enargy tolerance : 1.00000 Half life ratio~~
8.00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FNHM) : 5.00000 MDA Confid Level : 3.00000 %
"--t-NID Peak Search Report at Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 4 74.79 70 84-1.13 149.65 146 13 24.8 1.33E+00 PS214 PB212 4 77.14 86 81 1.10 154.35 146 13 21.4 PB214 PB212 4 92.91 74 48 1.46 185.93 183 13 19.5 2.56E+00 TH234 TH234 4 94.62 30 45 1.34 189.34 '. J 3 13 53.5 0-186.26 38 58 1.50 372.75 368 9 40.6 RA226 5 238.62 -251 33 1.05 477.53 473 15 7.2 3.09E-01 PB212 5 -241.36 47 39 1.95 483.01 473 15 39.6 PB214 I .0 295,35 60 36 0.78 591.05 586 8 21.6 PB214 0' 338.31 51 33 1.26 677.02 672 12 26.7 AC228 0-352.10- "97 24 1.42 704.62 700' 12 14.3 PB214 0 510.42 33 13 1.08 1021.42 1016 11 27.5 TL208 0 583.01. 80 23 1.10 1166.65 1162 12 16,0 TL208 .0 609.31 77 9 1.73 1219.29 1213 12 13.8 BI214 0 -661.57 138 14 1.12 1323.84 1318 13 10.1 CS137 0 839.58 11 9 0.52 1679.98 1671 11 61.5 911.44 -35 18 1.21 1823.75 1818 11 29.6 AC228 0- -968.74 28 13 2.11.1938.37 1933 12 30.9 AC228 0 1460.81 265 0 1.64 2922.62 2916 13 6.1 K40 Intorference Report COPi
~. . y,. IntorfGronco ROport (c~ont inL*d) Pcg3 : 2 'Snmplo ID : Horknaec #10 Acquicition dato : 21-NOV-1997 23:41:33 Interfering Interfered ( Nuclide Line Nuclide Line 1 PB214 241.92 RA224 241,00 TL208-510.72 ANN-RD 511.00 e 4 I l '.
4.. Summary of-Nuclida Activity pega 3 Scmplo ID : Harknoos #10 Acquisition date : 21-NOV-1997 23:41:33 Total number of lines in spectrum 18 ' wber of unidentified lines 2 /.( mber of lines tentatively identified by NID 16 88.09% Nuclide Type : natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags - K40 1.28E+09Y 1.00 1.581E-05 1.581E-05 0.097E-05 6.14 TL208 3 10M 2.58 2.799E-07 7.209E-07 1.155E-07 16.02 A PB212 10.64H 1.01 9.212E-07 9.263E-07 0.668E-07 7.21 A B1214 19.90M 1.19 5.184E-07 6.167E-07 0.850E-07 13.79 A PB214 26.80M 1.14 5.337E-07 6.077E-07 0.870E-07 14.32 A RA226 1600.00Y i.00 1.606E-06 1.606E-06 0.653E-06 40.63 AC228 6.13H 1.01 5.183E-07 5.234E-07 1.550E-07 29.61 A TH234 24.10D 1.00 4.000E-06 4.001E-06 0.781E-06 19.52 KA ( Total Activity : 2.419E-05 2.483E-05 Nuclide Type : fission Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags CS137 30.10Y 1.00 5.420E-07, 5.420E-07 0.546E-07 10.07 Total Activity : 5.420E-07 5.420E-07 Grand Total Activity : 2.473E-05 2.535E-05 .gs: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit ( e W -t
_ _ _ _ ~. _. _. _ -... Pags-: 4 -Nuclida Lins Error:Propogotion Report ! Sample ID : Harkness #10 Acquisition date.: 21-NOV-1997.23:41:33 f (- - lide Typet natural ) Uncorrected Decay Corr 1-Sigma 1 Nuclide Energy. %Abn %Eff uCi/g' uCi/g % Error Status i K40 1460.75 10.70*. 7.057E-01 1.581E-05 1.581E-05 6.14 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 6.14%) 1 Absent 1 Line Not Found =TL208 277.36 6.50 2.596E+00 510.72 22.50 1.672E+00 3.991E-07 1.028E-06 27.47 OK ( 0.0%) ( 4.61%) (Decay 0.00%) (Area 27.47%) ) 583.14 d6.00* 1.505E+00 2.799E-07 7.209E-07 16.02 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 16.02%) Line Not Found Absent 860.47 12.00 1.093E+00 PB212 74.81 9.60 1.984E+00 1.656E-06 1.665E-06 24.78 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area-24.78%) 77.11 17.50 2.109E+00 1.043E-06 1.049E-06 21.41 OK ~1 ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 21.41%) Absent Line Not Found 87.20 6.30 2.575E+00 238.63 43.10* 2.845E+00 9.212E-07 9.263E-07 7.21 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 7.21%) Absent Line Not Found 300.09 3.27 2.465E+00 BI214L 609.32 46.09* 1.453E+00 5.184E-07 6.167E-07 13.79 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 13.79%) Absent Line Not Found 768.36 4.89 -1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00-Absent Line Not Found 1120.28 15.04 8.750E-01 Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E ----- Absent-Line Not Found 1509.19 2.19 6.885E-01 Absent. Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PB214 74.81 6.33 1.984E+00 2.511E-06 2.860E-06 24.78 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 24.78%) 77.11 10.70 2.109E+00 1.706E-06 1.943E-06 21.41 OK ( 0.0%) ( 4.10%; (Decay 0.00%) (Area 21.41%) Absent Line Not Found 87.20 3.70 2.575E+00 Absent 89.80 '1.03 2.675E+00 Line Not Found -241.92 7.47 -2.826E+00 1.000E-06 1.139E-06 39.62 OK 4 ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 39.62%) 295.22 19,20 2.491E+00 5.648E-07 6.430E-07 21.61 OK ( 0.0%) ( 5.08%) (Decay 0.00%) (Area 21.61%) 351.99 37.10* 2.207E+00 5.337E-07 6.077E-07 34.32' OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 14.32%) Absent Line Not-Found-II 785.95 1.09 1.180E+00 RA226 185.99 3.28* 3.210E+00 1.606E-06 1.606E-06 40.63 OK l ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 40.63%) Absent Line Not1Found AC228 -209.40 4.55 3.050E+00 Absent Line Not Found 270;30 3.77 2.639E+00-Absent Line Not Found 328'00 1.36-2.320E+00 338.40 12.01 2.270E+00 8.358E-07 8.439E-07 26.74 OK .(-0.0%) ( 4~.73%) (Decay 0.00%) (Area 26.74%) Absent Line Not Found' -400.40- .2.23 1.977E+00 Absent Line Not Found 463.00 -4. 64-11.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 4 b ~
1 Nuclid3' Lina Error Propagation Report (continued) Pcga : 5 Sample ID : Harkneco #10 Acquicition dato : 21-NOV-1997 23:41:33 \\ lide Type natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status Line Not Found Absent 772.10 1.62 1.197E+00 Line Not Found Absent 794.80 4.84 1.169E+00 Line Not Found Absent 835.60 1.82 1.121E+00 911.07 29.00* 1.041E+00 5.183E-07 5.234E-07 29.61 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 29.61%) Line Not Found Absent 964.60 5.45 9.927E-01 968.90 17.46 9.891E-01 7.417E-07 7.489E-07 30.86 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 30.86%) Line Not Found Absent 1587.90 3.71 6.633E-01 Line Not Found Absent 1630.40 1.95 6.510E-01 Line Not Found Absent TH234 63.29 3.90* 1.299E+00 1 92.38 2.57 2.784E+00 4.670E-06 4.670E-06 19.52 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 19.52%) 92.80 3.00 2.784E+00 4.000E-06 4.001E-06 19.52 OK ( 0.0%) ( 4.10% ) (Decay-0.00%) (Area 19.52%) Line Not Found Absent 112.81 0.25 3.240E+00 Nuclide Type: fission ' Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status CS137 661.62 84.62* 1.360E+00 5.420E-07 5.420E-07 10.07 OK ( 0.0%) ( 5.10%) (Decay 0.00%) (Area 10.07%)
~~g: "*" = Keyline t.~~
~~/.i g 2 MILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 22-NOV-1997 13:38:21 t' Sample Information ---- S;mple ID~~
Harkncss #11 Sample Quantity

1.00000E+03 g

37517 Spctrm Collector : HP Environmental S mple Number Sample Analyst HP Environmental

~~Sample Deposition Information ----~~

~~D:p Correction? : No Dep. Duration Leposition End~~
~~22-NOV-1997 13:27:43 reposition Start :~~
~~Sample Decay / Count Information ---- Scmple Date~~
~~22-NOV-1997 13:27:43 Acquisition date : 22-NOV-1997 13:27:49 Decay time 0 00:00:06.11~~
~~% dead time~~
~~0.0%~~
~~Elepsed live time: 0 00:10:00.00 Elapsed real time: 0 00:10:00.28~~
I

~~Detector Parameters ----~~

~~Enorgy cal. time : 19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Datoctor name~~
~~Environmental Counting geometry: 1 Liter Soil Effic.- cal, time : 19-JUL-1995 08:56:03 Effic. cal, oper.: HP Support~~

~~Processing Parameters ----~~

~~Stort channel~~
100 End channel

3700

4.50000 Caussian Sens.

10.00000 Sancitivity Critical level?

Yes Propagate Errors?: No

Yes Libra n-based eff: No Empirical Eff?

1.00000 Half life rat 13

8.00000 Inargy tolerance Abundance limit

80.00000 WTM error limi~

3.00000 Width (FWRM) : 5.00000 MDA Confid Leve'J : 3.00000 %
Post-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclid'es 2 74.92 65 104 0.92 149.92 146 13 27.1 1.18E+00 PB214 PB212 2 77.15 117 87 1.06 154.39 146 13 16.1 PB214 PB212 0-87.17 41 89 0.81 174.43 172 6 39.8 PB214 PB212 4 90.06 42 72 1.11 180.22 178 19 33.2 6.97E-01 PB214 4 '92.91 47 111 1.4G 185.93 178 19 43.9 TH234 e TH234 0 186.14 52 76 1.33 372.50 367 8 32.0 RA226 D 238.58 308 110 1.05 477.44 473 9 8.4 PB212 0 294.73 86 26 1.42 589.81 583 13 16.3 PB214 0 338.25 62 45 0.80 676.89 672 10 23.7 AC228 0 351.95 121 30 1.06 704.32 699 11 12.7 PB214 0 463.13 25 11 0.88 926.79 923 9 32.8 AC228 0 583.03 99 5 1.52 1166.70 1162 9 10.7 TL208 0 609.34 97 20 1.20 1219.34 1212 13 13.8 BI214 0 727.75 19 15 0.79 1456.25 1449 10 44.1 BI212 0 911.09 66 22 1.52 1823.05 1817 11 18.4 AC228 0 969.07 48 15 1.45 1939.03 1933 11 21.9 AC228 0 1460.52 364 0 2.08 2922.04 2916 13 5.2 K40 0 1763.90 16 0 1.54 3528.75 3522 11 25.0 BI214 / -.rference Report CO*Y
is h4oine.erferencecorrectionperformed f( 9 5 i I t:-
/.. ,,~ Summary of Nuclida Activity Pcga : 2
~~22-NOV-1997 13:27:49 SOmplo ID : Harkness #11 Acquisition date~~
(. autbar of unidentified lines 21 number of lipes in spectrum 18 0 Numb 3r of lines tentatively identified by NID 18 100.00% Nuclide Type i natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags K40 1.28E+0pY 1.00 2.171E-05 2.171E-05 0.114E-05 5.24 TL208 3.10M 2.56 3.459E-07 8.863E-07 0.952E-07 10.74 A BI212 60.55M 1.06 5.822E-07 6.169E-07 2.720E-07 44.09 A PB212 10.64H 1.01 1.130E-06 1.136E-06 0.095E-06 8.39 A DI214 19.90M 1.19 6.540E-07 7.773E-07 1.074E-07 13.81 A PB214 26.80M 1.14 6.652E-07 7.569E-07 0 958E-07 12.65 A RA226 1600.00Y-1.00 2.235E-06 2.235E-06 0.716E-06 32.03 1AC228 6.13H 1.01 9.857E-07 9.952E-07 1.834E-07 18.43 A TH234 24.10D 1.00 2.522E-06 2.522E-06 1.108E-06 43.95 KA Total Activity : 3.083E-05 3.163E-05 Grand Total Activity t 3.083E-05 3.163E-05 Flags: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn, limit l 3 m
~ f.e 'w.* Nuclida Lina Error Propngetion Roport Paga 3 1 Semple ID : Harkness #11 Acquisition date
~~22-NOV-1997 13:27: 49~~
!A Nuclide Type: natural Uncorrected Decay Corr 1-Sigma Nuclide Eneray Area %Abn %Eff uCi/g uCi/g % Error K40 1460.75 364 10.70* 7.059E-01 2.171E-05 2.171E-05 5.24 ( 5.24%) ( 0.0%) ( 4.45%) (Decay 0.00%) Line Not Found 6.50 2.596E+00 TL208 277.36 Line Not Found 22.50 1.671E+00 510.72 581.14 99 86.00* 1.505E+00 3.459E-07 8.863E-07 10.74 (10.74%) ( 0.0%) ('4.88%) (Decay 0.00b Line Not Found 12.00 1.093E+00 860.47 BI212 727.17 19 11.80* 1.257E+00 5.822E-07 6.169E-07 44.09 (44.09%) ( 0.0%) ( 5.30%) (Decay 0.00%) Line Not Found 2.00 1.180E+00 785.42 Line Not Found 0.97 9.033E-01 1 1078.62 Line Not Found 2.75 6.538E-01 1620.56 PB212 74.81 65 9.60 1.991E+00 1.533E-06 1.542E-06 27.10 (27.10%) ( 0.0%) ( 4.15%) (Decay 0.00%) 77.11 117 17.50 2.110E+00 1.426E-06 1.434E-06 16.07 (16.07%) ( 0.0%) ( 4.10%) (Decay 0.00%) 87.20 41 6.30 2.573E+00 1.133E-06 1.139E-06 39.76 (39.76%) ( 0.0%) ( 4.05%) (Decay 0.00%) 238.63 308 43.10* 2.845E+00 1.130E-06 1.136E-06 8.39 ( 8.39%) ( 0.0%) ( 5.04%) (Decay 0.00%) Line Not Found 3.27 2.465E+00 300.09 BI214 609.32 97 46.09* 1.453E+00 6.54CE-07 7.773E-07 13.81 (13.81%) ( 0.0%) ( 4.96%) (Decay 0.00%) Line Not Found 4.89 1.202E+00 768.36 Line Not Found 3.16 1.020E+00 934.05 Line Not Found 15.04 8.750E-01 1120.28 Line Not Found 5.92 8.052E-01 1238.11 Line Not Found 4.02 7.387E-01 1377.65 Line Not Found 2.19 6.885E-01 1509.19 Line Not Found 3.05 6.254E-01 1729.60 1764.51 16 15.92 6.175E-01 7.332E-07 8.714E-07 25.00 (25.00%) ( 0.0%) ( 4.80%) (Decay 0.00%) PB214 74.81 65 6.33 1.991E+00 2.325E-06 2.646E-06 27.10 (27.10%) ( 0.0%) ( 4.15%) (Decay 0.00%) 77.11 117 10.70 2.110E+00 2.332E-06 2.653E-06 16.07 (16.07%) ( 0.0%) ( 4.10%) (Decay 0.00%) 87.20 41 3.70 2.573E+00 1.929E-06 2.195E-06 39.76 g (39.76%) ( 0.0%) ( 4.05%) (Decay 0.00%) 89.80 42 1.03 2.684E+00 6.814E-06 7.754E-06 33.19 (33.19%) ( 0.0%) ( 4.07%) (Decay 0.00%) Line Not Found 7.47 2.823E+00 241.92 295.22 86 19.20 2.495E+00 8.088E-07 9.203E-07 16.30 (16.30%) ( 0.0%) ( 5.09%) (Decay 0.00%) 351.99 121 37.10* 2.207E+00 6.652E-07 7.569E-07 12.65 (12.65%) ( 0.0%) ( 4.58%) (Decay 0.00%) Line Not Found 1.09 1.180E+00 785.95 RA226 185.99 52 3.28* 3.211E+00 2.2351-J6 2.235E-06 32.03 (32.03%) ( 0.0%) ( 4.85%) (Decay 0.00%) Line Not Found 4.55 3.050E+00 AC228 209.40
I ' j s Nuclido Lino Error Prop 0gotion R0 port (continuod) P0go 4 ' Sample ID Narkness #11 Acquisition date : 22 NOV-1997 13:27:49 Nuclide Type natural Uncorrected Decay Corr 1' a Nuclide Energy Area %Abn %Eff uC1/g uCi/g %J;10r Line Not Found 3.77 2.639E+00 270.30 Line Not Found 3.30 2.320E+00 328.00 338.40 62 12.01 2.270E+00 1.031E-06 1.041E-06 23.75 ( 2 3. '/ 5 % ) ( 0.0%) ( 4.73%) (Decay 0.00%) Line Not Found 2.23 1.977E+00 409'.40 463.00 25 4.64 1.802E+00 1.338E-06 1.351E-06 32.81 (32.81%) ( 0.0%) ( 4.42%) (Decay 0.00%) Line Not Found 0.24 1.758E+00 478.20 Line Not Found 1.62 1.197E+00 772.10 Line Not Found 4.84 1.169E+00 794.80 Line Not Found 1.82 1.121E+00 I 835.60 911.07 66 29.00* 1.042E+00 9.857E-07 9.952E-07 18.43 (18.43%) ( 0.0%) ( 5.64%) (Decay 0.00%) Line Not Found 5.4L 9.927E-01 964.60 968.90 48 17.46 9.889E-01 1.242E-06 1.254E-06 21.86 (21.86%) ( 0.0%) ( 5.43%) (Decay 0.00%) Line Not Found 3.71 6.633E-01 1587.90 Line Not Found 1.95 6.510E-01 1630.40 Line Not Found 3.90* 1.299E+00 TH234 63.29 92.38 ,7 2.57 2.784E+00 2.944E-06 2.944E-06 43.95 (43.954) ( 0.0%) ( 4.10%) (Decay 0.00%) 92.80 47 3.00 2.784E+00 2.522E-06 2.522E-06 43.95 (43.95%) ( 0.0%) ( 4.10 % ) (Decay 0.00%) Line Not Found 0.25 3.240E+00 112.t1 Keyline Flags "*" - ) t f e J-4
r
~~MILLS ONE HEALTH PHYSICS-ENVIRONMENTAL 22-NOV-1997 08:55:22 (bcmpleID~~

~~Sample Information ----~~

Harkness #12 Sample Quantity 1.00000E+03 g Semple Number

37504 Spetrm Collector : HP Environmental Sample Analyst

HP Envircr' ental

~~Sample Deposition Information ----~~

~~Dap. Correction? : No Dep. Duration Dopo0ition Start : Depnsition End~~
~~22 NOV-1997 08:44:38~~

~~Sample Decay / Count Information ----~~

~~Scmple Date~~
~~22-NOV-1997 08:44:38 AcWisition date : 22-NOV-1997 08:44:44 Daccy time 0 00:00:06.14~~
~~% dead time~~
~~0.1%~~
~~Elepoed live times 0 00:10:00.00 Elapsed real time 0 00:10:00.36~~

~~Detector Parameters ----~~

~~0 19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Enorgy cal. time Datoctor name Environmental Counting geometry: 1 Liter Soil Effic. cal. time : 19-JUL-1995 08:56:03 Effic. cal, oper.: HP Support~~

~~Processing Parameters ----~~

~~Sturt channel~~
100 End channel

3700 Sonsitivity

4.50000 Gaussian Sens.
~~10.00000 Critical level?~~
Yes Propagate Errorn?: No Empirical Eff?

Yes Library-based eff: No Enorgy tolerance : 1.00000 Half life ratio

8.00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level ? 3.00000 %
. -NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 3 74.96 135 142 1.17 150.01 144 17 16.7 2.65E+00 PB214 PB212 2 77.16 188 117 1.09 154.41 - 144 17 12.6 PB214 PB212 0 87.51 44 169 0.94 175.11 171 8 53.9 PB214 PB232 0 93.21 66 131 1.19 186.53 183 7 31.7 TH234 TH234 g 0 128.83 48 151 0.77 257.81 254 9 48.8 1 238.75 539 75 1.33 477.78 473 17 5.0 8.88E+00 PB212 1 242.35 37 43 1.21 485.00 473 17 42.0 PB214 0 295.34 75 74 0.P9 591.04 587 10 24.6 PB214 0 328,49 25 30 1.k3 657.37 652 8 42.6 AC228 0 338.25 99 67 1.10 676.89 672 10 18.5 AC228 0 351.89 126 31 1.39 704.20 700 9 12.0 PB214 0 462.66 47 14 1.46 925.85 920 11 20.9 AC228 0 510.56 34 26 1.29 1021.69 1015 13 43.0 ANN-RD 0 583.'15 175 17-1.26 1166.94 1161 13 8.9 TL208 0 609.29 124 8 1.21 1219.24 1213 11 10.0 BI214 0 727.39 68 13 1.81 1455.53 1449 13 16.3 BI212 0 794.96 34 11 1.10 1590.72 1586 10 25.9 AC228 0 911.19 99 17 1.50 1823.25 1816 14 13.5 AC228 CO?Y
Poeg-NTD Pock Socrch Roport (continued) Paga 2 Scmplo ID : Horkneso #12 Acquisition dato 22-NOV-1997 08:44 44 ( E ier.Jy . Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 2 9bc e4 34 11 2.14 1930.38 1923 21 24.0 1.04E+00 AC228 2 968.87 80 4 1.81 1938.64 1923 21 12.9 AC228 0 1119.79 24 10 1.27 2240.54 2236 10 32.0 BI214 0 1460.66 395 3 2.09 2922.32 2914 14 5.1 K40 Interferer:ce Report Interfering Interfered Nuclide Line Nuclide Line TL208 510.72 ANN-RD 511.00 I 4 ( y.
Summary of Nuclida Activity pag 3 : 3 J mplo ID : Horknoso #12 Acquisition dato 22-NOV-1997 08:44:44 ol number of lines in spectrum 22 , -*ber of unidentified lines 1 Number of lines tentatively identified by NID 21 95.45%
~~natural Nuclide Type Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error~~
% Error Flags K40 1.28E+09Y 1.00 2.357E-05 2.357E-05 0.121E-05 5.13 TL208 3.10M 2.56 6.106E-07 1.565E-06 0.140E-06 8.92 A BI212 60.55M 1.06 2.072E-06 2.196E-06 0.357E-06 16.26 A PB212 10.64H 1.01 1.980E-06 1.991E-06 0.099E-06 4.99 A BI214 19.90M 1.19 8.344E-07 9.917E-07 0.994E-07 10.02 A PB214 26.80M 1.14 6.925E-07 7.881E-07 0.945E-07 11.99 A AC228 6.13H 1.01 1.469E-06 1.484E-06 0.200E-06 13.51 A gTH234 24.10D 1.00 3.545E-06 3.545E-06 1.122E-06 31.65 KA Total Activity : 3.477E-05 3.613E-05 Nuclide Type : other Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uti/g 1-Sigma Error % Error Flags ANN-RD 109.74M 1.03 4.768E-08 4.924E-08 2.116E-08 42.07 Total Activity : 4.768E-08 4.924E-08 ' rand Total Activity : 3.482E-05 3.618E-05 Flags: "K" = Keyline not found "M" - Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit. I
[Nuclid.3LinoErrorPropogotionRcport 22-NOV-1997$ai pc 4 scmplo ID : Harknaso #12 Acquisition dato : 8:44:44 t Nuclide Type: natural Uncorrected Decay Corr 1-Sigma > Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status K40 1460.75 10.70* 7.058E-01 2.357E-05 2.357E-05 5.13 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 5.13%) Absent Line Not Found TL208 277.36 6.50 2.596E+00 Line Not Found

<< INT Reject 510.72 22.50 1.671E+00 583.14 86.00*

1.505E+00 6.106E-07 1.565E-06 8.92 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 8.92%) Absent Line Not Found 860.47 12.00 1.093E+00 DI212 727.17 11.80* 1.258E+00 2.072E-06 2.196E-06 16.26 OK ( 0.01' ( 5.30%) (Decay 0.00%) (Area 16.26%) Absent Line Not Found 785.42 2.00 1.180E+00 Absent Line Not Found 1078.62 0.97 9.033E-01 g Absent Line Not Found 1620.56 2.75 6.538E-01 PD212 74.81 9.60 1.993E+00 3.184E-06 3.202E-06 16.68 OK ( 0.0%) ( 4.15 % ) (Decay 0.00%) (Area 16,68%) 77.11 17.50 2.111E+00 2.288E-06 2.301E-06 12.58 OK ( 0.0%) ( 4.10 % ) (Decay 0.00%) (Area 12.58%) 87.20 6.30 2.587E+00 1.206E-06 1.212E-06 53.90 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 53.90%) 238.63 43.10* 2.844E+00 1.980E-06 1.991E-06 .4.99 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 4.99%) Absent Line Not Found 300.09 3.27 2.465E+00 DI214 609.32 46.09* 1.453E+00 8.344E-07 9.917E-07 10.02 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 10.02%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.753E-01 8.212E-07 9.761E-07 32.00 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 32.00%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PB214 74.81 6.33 1.993E+00 4.829E-06 5.495E-06 16.68 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 16.68%) 77.11 10.70 2.111E+00 3.742E-06 4.258E-06 12.58 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 12.58%) 87.20 3.70 2.587E+00 2.053E-06 2.336E-06 53.90 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 53.90%) Absent Line Not Found 89.80 1.03 2.675E+00 241.92 7.47 2.820E+00 7.835E-07 8.893E-07 41.97 OK ( 0.0%) ( 5.06%) (Decay 0.00%) (Area 41.97%) 295.22 19.20 2.491E+00 7.092E-07 8.070E-07 24.58 OK ( 0.0%) ( 5.08%) (Decay 0.00%) (Area 24.58%) 351.99 37.10* 2.200E+00 6.925E-07 7.881E-07 11.99 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 11.99%) Absent .Line Not Found 785.95 1.09 1.180E+00 Absent Line Not Found AC228 209.40 4.55 3.050Et00 Absent Line Not Found 270.30 3.77 2.639E+00 328.00 3.36 2.317E+00 1.455E-06 1.469E-06 42.59 OK ( 0.0%) ( 4.82%) (Decay 0.00%) (Area 42.59%) i ,~
Nuclido Lino Error Propogotion Report (continued) Pogo 5 ,Scmple ID : Harknoos #12 Acquisition dato 22-NOV-1997 08:44:44 I' uclide Types natural 'N Uncorrected Decay Cort 1-Sigma Nuclide Energy %Abn %Eff uC1/g uCi/g % Error Status 338.40 12.01 2.270E+00 1.630E-06 1.646E-06 18.54 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 18.54%) Absent Line Not Found 409.40 2.23 1.977E+00 463.00 4.64 1.803E+00 2.555E-06 2.580E 06 20.95 OK ( 0.0%) ( 4.41%) (becay 0.00%) (Area 20.95%) Absent Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1,62 1.197E+00 794.80 4.84 1.168E+00 2.682E-06 2.708E-06 25.94 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 25.94%) Absent Line Not Found 835.60 1.82 1.121E+00 J 911.07 29.00* 1.042E+00 1.469E-06 1.484E-06 13.51 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 13.51%) 964.60 5.45 9.926E-01 2.816E-06 2.843E-06 24.05 OK ( 0.0%) ( 5.44%) (Decay 0.00%) (Area 24.05%) 968.90 17.46 9.890E-01 2.088E 06 2.108E-06 12.87 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 12.87%) Absent Line Not Found 1587.90-3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.794E+00 4.130E-06 4.138E-06 31.65 OK ( 0.0%) ( 4 11%) (Decay 0.00%) (Area 31.65%) 92.80 3.00 2.' %CN SO 3.545E-06 3.545E-06 31.65 OK ( 0.0%) i 4 \\tte (Decay 0.00%) (Area 31.65%) Absent Line Not Found 112.81 0.25 3. ; '. f.' J4 Nuclide Types other Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status ANN-RD 511.00 193.40* 1.671E+00 4.768E-08 4.924E-08 42.97 OK (Decay 0.00%) (Area 42.97%) ( 0.0%) ( 4.61%) Fleg: "*" = Keyline f 3-
e MILLSTONE HEALTH PHYSICS-ENVIRO! MENTAL 22-NOV-1997 11:07:51 is

~~Sample Information ----~~

~~Scmplo ID~~
Harkness #13 Sample Quantity

1.00000E+03 g Scmplo Number

37512 Spetrm Collector : HP Environmental Sample Analyst

HP Environmental

~~Sample Deposition Information ----~~

~~No Dep. Duration D:p. Correction?~~
~~D pooition Start : Deposition End~~
~~22-NOV-1997 10:57:10~~

~~Sample Decay / Count Information ----~~

~~Scmplo Date 22-NOV-1997 10:57:10 Acquisition date : 22-NOV-1997 10:57:17 D3ccy time 0 00:00:06.77 % dead time~~
~~0.0%~~
~~ElapOd live times 0 00:10:00.00 Elapsed real times 0 00:10:00.28 I~~

~~Detector Parameters ----~~

19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Enorgy cal, time Datcetor name

Environmental Counting geometry: 1 Liter Soil Effic. cal, time i 19-JUL-1995 08:56:03 Effic, cal. oper.: HP Support

~~Processing Parameters ----~~

~~Stcrt channel~~
100 End channel

3700 Scncitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No Empirical Eff?

Yes Libran-based eff: No Enorgy tolerance : 1.00000 Half llfe ratio

0.00000 Abundtnce limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
o-NID Peak Search Report 4 It Energy Area Bkgnd FWHM Channel Left PW % Err Fit Nuclides 7 74.82 57 52 1.23 149.72 148 10 20.1 2.90E+00 PB214 PB212 7 77.09 124 96 1.03 154.26 148 10 15.5 PB214 PB212 0 87.28 60 77 1.40 174.66 172 6 26.6 PB214 PB212 0 89.95 58 60 1.02 180.00 178 5 24.0 PB214 0 93.16 66 105 1.40 106.43 183 9 30.8 TH234 TH234 0 186.23 32 68 0.98 372.67 369 8 48.5 RA226 0 209.14 33 46 1.34 418.52 415 7 38.6 AC228 2 238.59 343 40 1.17 477.47 472 17 6.2 1.84E+00 PB212 2 240.60 31 30 1.07 491.48 472 17 55.8 RA224 241.87 49 42 1,47 484.02 472 17 31.5 PB214 0 295.43 78 27 1.28 591.20 587 11 16.8 PB214 0 300.69 23 37 1.17 601.75 598 9 50.7 PB212 0 328.08 38 24 1.00 656.55 652 9 28.7 AC228 0 339.45 48 70 0.72 679.30 671 15 41.8 0 351.91 88 42 0.97 704.24 698 10 17.4 PB214 0 510.86 28 13 1.02 1022.29 1017 11 39.4 ANN-RD 0 583.05 97 22 0.95 1166.74 1162 10 13.7 TL208 0 609.39 81 16 1.47 1219.44 1212 11 14.3 BI214 CO?Y 4
r 'o o Po0t-NID Pack Socrch Rcport (continu0d) Pogo : 2 'S mplo ID : Har'* ness #13 Acquisition date : 22-NOV-1997 10:57:17 4 i Energy Area _ Bksnd FWHM Channel Left PW % Err Fit Nuclides 0 727.34 26 7 1,46 1455.42 1452 7 25.9 BI212 0 911.19 75 17 1.47 1823.24 1818 10 15.5 AC228 0 969.10 45 9 1.89 1939.09 1934 10 19.8 AC228 0 1460.50 344 7 2.01 2922.01 2915 14 5.6 K40 0 1764.54 18 3 1.39 3530.04 3522 13 30.4 DI214 Intorference Report Interfering Interfered Nuclide Line Nuclide Line 1 TL208 510.72 ANN-RD 511.00 e e t-
_m,_ l. Subm3ry'ofNuclidaActivity pago 3 . Sample ID : Harkness #13 Acquisition dato : 22-NOV-1997 10:57:17 01 number of lines in spectrum 23 k..a'ber of unidentified lines 1 Humber of lines tentatively identified by HID 22_ 95.65% Nuclide Type natural Uncorrected Decay corr Decay Corr 1-Sigma i Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags K40 1.28E+09Y 1.00 2.052E-05 2.052E-05 0.116E-05 5.63 TL208 3.10M 2.51 3.364E-07 8.640E-07 1.183E-07 13.69 A BI212 60.55M 1.06 7.890E-07 8.361E-07 2.163E-07 25.87 A PB212 10.64H 1.01 1.262E-06 1.269E-06 0.078E-06 6.16 A BI214 19.90M
~~1. 3 ',~~
5.477E-07 6.513E-07 0.929E-07 14.26 A PB214 26.80M 1.14 4.062E-07 5.535E-07 0.962E-07 17.39 A RA224 3.66D 1.00 1.263E-06 1.264E-06 0.705E-06 55.79 j RA226 1600.00Y 1.00 1.368E-06 1.368E-06 0.663E-06 48.45 AC228 6.13H 1.01 1.121E-06 1.132E-06 0.175E-06 15.50 A TH234 24.10D 1.00 3.529E-06 3.529E-06 1.088E-06 30.82 KA Total Activity : 3.122E-05 3.198E-05 Nuclide Type : other Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags ANN-RD 109.74M 1.03 3.903E-08 4.031E-08 1.588E-08 39.39 Total Activity : 3.903E-08 4.031E-08 Grand Total Activity : 3.126E-05 3.202E-05 Flago: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit 3 y w w,- ,--,e

~~.e r~~

-ua-+------n 3
r g Nuclido Lino Error Prop 0gotion RGport pega : 4 Semple ID : Harkness #13 Acquisition date : 22-NOV-1997 10:57:17 .( i Nuclide Types natural Uncorrected Decay Corr 1-Sigma i Huclide Energy %Abn %Eff uCi/g uCi/g % Error Status K40 1460.75 10.70* 7.059E-01 2.052E-05 2.052E-05 5.63 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 5.63%) Line Hot Found Absent TL208 277.36 6.50 2.596E+00 Line Not Found

<< INT Reject 510.72 22.50 1.671E+00 583.14 86.00*

1.505E+00 3.364E-07 8.640E-07 13.69 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 13.69%) Absent Line Not Found 860.47 12.00 1.093E+00 BI212 727.17 11.80* 1.258E+00 7.890E-07 8.361E-07 25.87 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 25.87%) Absent Line Not Found 785.42 2.00 1.180E+00 Absent Line Not Found i 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 PB212 74.81 9.60 1.985E+00 1.342E-06 1.349E-06 20.09 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 20.09%) 77.11 17.50 2.107E+00 1.509E-06 1.518E-06 15.45 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 15.45%) 87.20 6.30 2.578E+00 1.663E-06 1.672E-06 26.58 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 26.58%) 238 63 43.10* 2.845E+00 1.262E-06 1.269E-06 6.16 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 6.16%) 300.09 3.27 2.462E+00 1.310E-06 1.318E-06 50.71 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 50.71%) DI214 609.32 46.09* 1.453E+00 5.477E-07 6.513E-07 14.26 OK ( 0 0%) ( 4.96%) (Decay 0.00%) (Area 14.26%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 Absent Line Not Found 1120.28 15.04 8.750E-01 Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 1764.51 15.92 6.173E-01 8.469E-07 1.007E-06 30.41 OK ( 0.0%) ( 4.80%) (Decay 0.00%) (Area 30.41%) PB214 74.81 6.33 1.985E+00 2.035E-06 2.317E-06 20.09 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 20.09%) 77.11 10.70 2.107E+00 2.469E-06 2.810E-06 15.45 OK 3 ( 0.0%) ( 4.10 % ) (Decay 0.00%) (Area 15.45%) ~ 87.20 3.70 2.578E+00 2.832E-06 3.223E-06 26.58 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 26.58%) 89.80 1.03 2.680E+00 9.463E-06 1.077E-05 23.95 OK ( 0.0%) ( 4.07%) (Decay 0.00%) (Area 23.95%) 241.92 7.47 2.823E+00 1.055E-06 1.201E-06 31.53 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 31.53%) -295.22 19.20 2.491E+00 7.369E-07 8.388E-07 16.81 OK ( 0.0%) ( 5.08%) (Decay 0.00%) (Area 16.81%) 351.99 37.10* 2.207E+00 4.862E-07 5.535E-07 17.39 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 17.39%) Absent Line Not Found 785.95 1.09 1.180E+00 Absent Line Not Found RA224 83.78 0.21 2.430E+00 f ^ i-
r . ~ Nuclido Lino Error Propagation Report (continuod) Pcga 5 Scmple ID : Harkness #13 Acquisition date : 22-NOV-1997 10:57:17 / Nuclide Typei natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status 241.00 3.90* 2.832E+00 1.263E-06 1.264E-06 55.79 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 55.79%) RA226 185.99 3.28* 3.211E+00 1.368E-06 1.368E-06 48.45 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 48.45%) AC228 209.40 4.55 3.052E+00 1.054E-06 1.064E-06 38.63 OK ( 0.0%) ( 4.93%) (Decay 0.00%) (Area 38.63%) Absent Line Not Found 270.30 3.77 2.639E+00 328.00 3.36 2.319E+00 2.184E-06 2.205E-06 28.68 OK ( 0.0%) ( 4.83%) (Decay 0.00%) (Area 28.68%) Absent Line Not Found 330.40 12.01 2.269E+00 Absent Line Not Found { 409.40 2.23 1.977E+00 Line Not Found Absent 463.00 4.64 1.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 Line Not Found Absent 772.10 1.62 1.197E+00 Absent Line Not Found 794.80 4.84 1.169E+00 . Absent Line Not Found 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 1.121E-06 1.132E-06 15.50 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 15.50%) Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 9.888E-01 1.170E-06 1.182E-06 19.82 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 19.82%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found 4 63.29 3.90* 1.299E+00 92.38 2.57 2.792E+00 4.119E-06 4.120E-06 30.82 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 30.82%) 92.80 3.00 2.792E+00 3.529E-06 3.529E-06 30.82 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 30.82%) Absent Line Not Found 112.81 0.25 3.240E+00 Nuclide Types other Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status ANN-RD 511.00 193.40* 1.671E+00 3.903E-08 4.031E-08 39.39 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 39.39%) I Flog: "*" = Keyline w
I . MILLSTONE HEALTH FHYSICS-ENVIRONMENTAL 21-NCV-1997 21:33:43 [ Sample Information ---- . t..nple ID
Harkness #14 Sample Quantity

1.00000E+03 g Scmple Number

37403 Spctrm Collector : HP Environmental Sample Analyst

HP Environmental

~~Sample Deposition Information ----~~

~~Dap. Correction?~~
No Dep. Duration D3 position Start Deposition End

21-NOV-1997 21:22:57

~~Sample Decay / Count Information ----~~

~~Semple Date~~
~~21-NOV-1997 21:22:57 Acquisition date : 21-NOV-1997 21:23:06 D2 coy time 0 00:00:09.33~~
~~% dead time~~
~~0.0%~~
~~Elepsed live times 0 00:10:00.00 Elapsed real time: 0 00:10:00.28~~

~~Detector Parameters ----~~

~~5 Enargy cal. time 19-JUL-1995 08:05:48 Energy cal. oper.: HP Support-I Counti.1 1 Liter Soil Datoctor name~~
~~Environmental Effic. g geometry:~~
~~Effic. cal, time : 19-JUL-1995 08:56:03 cal. oper.: HP Support~~

~~Processing Parameters ----~~

~~l Start channel~~
100 End-channel

3700 Sonsitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate. Errors?: No Empirical Eff?

Yer Libran-based eff: No Ensrgy tolerance : 1.00000 Half life ratio

8.00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 4 74.78 81-12A 1.13 149.64 145 20 24.8 1.37E+00 PB214 PB212 4 77.24 133 115 1.10 154.56 145 20 16.2 PB214 PB212 1 90.05 47 88 1.03 180.20 169 24 33.6 2.51E+00 PB214 1 93.03 61 71 1.10 186.17 169 24 29.8 TH234 TH234 0-186.24 49 93 1.48 372.71 368 9 38.6 RA226 0 209.39 35 62 1.48 419.03 415 9 43.8 AC228 i5 238.66 359 40 1.03 477.61 473 16 6.0 6.15E-01 PB212 5 -241.49 45 SS 1.68 483.28 473 16 51.1 RA224 'l 295.32 133 20 1.40 591.00 586 20 10.0 3.41E+00 PB214 1 300.19 36 14 1.40 600.?4 586 20 28.0 PB212 0 338.44 57 60 1.36 677.28 6'70 15 32.4 AC228 0 352.08 160 41 1.11 704.58 -698 14 11.6 PB214 'O 463.72 44 .3 1.52 927.98 921 15R28.2 AC228 0 510.73-24 '4 1.48 1022.03 1016 15 55.6 ANN-RD 0 583.08-111 1.14.1166.80 1161 12111.8 TL208 'O 609.26 144 1.37 1219.19 11212 -13 8.7 BI214 0 646.33 14 9' 1.40 1293.35 1289 7 47.3 0 727.21-27 14 0.81 1455.16.1450' 13 34.4 BI212 1 0 794.85 19 5 1.40 1590.49 1586 10 32.5 AC228 '(:) DY I a e
'e< Post-HID Pock Socrch Roport (continucd) Pego : 2 ,Scmple ID : Harknoco #14 Acquisition dato : 21-NOV-1997 21:23:06 ( Energy Area Bkgnd FWHM Channel Left PW % Err Fit Nuclides 0 910.92 80 4 1.43 1822.71 1815 16 12.5 AC228 0 969.66 35 28 0.73 1940.22 1932 13 36.4 AC228 0 1119.88 38 0 1.20 2240.71 2235 12 16.2 BI214 0 1460.73 255 10 1.90 2922.46 2915 14 6.8 K40 0 1764.19 15 0 1.25 3529.33 3523 11 25.8 BI214 Interference Report Interfering Interfered Nuclide Line Nuclide Line ] PB214 241.92 RA224 241.00 TL208 510.72 ANN-RD 511.00 i t e e 7 [.
l Summ3ry of Nuclido Activity Pega 3 i .Scmplo ID : Horknaso #14 Acquioition dato : 21-NOV-1997 21:23:06 f -*cl number of lines in spectrum 24 I .tber of unidentified lines 0 l ' A' umber of lines tentatively identified by NID 24 100.00% Nuclide Type natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife-Decay uCi/g uCi/g 1-Sigma Error % Error Flags K40 1.28E+09Y 1.00 1.519E-05 1.519E-05 0.104E-05 6.82 TL208 3.10M 2.59 3.869E-07 1.003E-06 0.118E-06 11.76 A l BI212 60.55M 1.06 8.048E-07 8.533E-07 2.935E-07 34.40 A PB212 10.64H 1.01 1.319E-06 1.327E-06 0.079E-06 5.96 A B1214 19.90M 1.19 9.714E-07 1.157E-06 0.101E-06 8.72 A PB214 26.80M 1.14 8.822E-07 1.005E-06 0.117E-06 11.63 A RA224 3.66D 1.00 1.835E-06 1.836E-06 0.938E-06 51.09 g RA226 1600.00Y 1.00 2.085E-06 2.085E-06 0.806E-06 38.64 AC228 6.13!I 1.01 1.192E-06 1.203E-06 0.151E-06 12.51 A TH234 24.10D 1.00 3.276E-06 3.277E-06 0.978E-06 29.85 KA Total Activity 2.795E-05 2.894E-05 Nuclide Type : other Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags ANN-RD 109.74M 1.03 3.354E-08 3.464E-08 1.925E-08 55.58 Total Activity : 3.354E-08 3.464E-08 Grand Total Activity 2.798E-05 2.89. -05 .Flego: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit 'l 1 y e- ~-..ey ,-3.,. y -c-y =
Nuclida Lino Error Prop 0gation Roport Pcga : 4 ,Scmplo ID : Harkness #14 Acquisition dato : 21-NOV-1997 21:23:06 / huclide Typer natural Uncorrected Decay Corr 1-Sigma Nuclide Eneroy %Abn %Eff uCi/g uCi/g % Error Status K40 1460,95 10.70* 7.058E-01 1.519E-05 1.519E-05 6.82 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 6.82%) Lir.e Not Found Absent TL208 277.36 6.50 2.596E400 Line Not Found

<<IhT Reject 510.72 22.50 1.671E+00 583.1.4 86.00*

1.500E+00 3.869E-07 1.003E-06 11.76 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 11.76%) Absent Line Not Found 860.47 12.00 1.093E+00 BI212 727.17 11.80* 1.258E+00 8.048E-07 8.533E-07 34.40 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 34.40%) i Absent Line Not Found 785.42 2.00 1.180E+00 Absent Line Not Found 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 4 + PD212 74.81 9.60 1.983E+00 1.912E-06 1.923E-06 24.81 OK ( 0.0%) ( 4.15 % ) (Decay 0.00%) (Area 24.81%) 77.11 17.50 2.115E+00 1.619E-06 1.628E-06 16.18 OK ( 0 0%) ( 4.10%) (Decay 0.00%) (Area 16.18%) Absent Line Not Found 87.20 6.30 2. 5'/ S E + 0 0 238.63 43.10* 2.845E+00 1.319E-06 1.327E-06 5.96 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.96%) 300.09 3.27 2.464E+00 2.005E-06 2.017E-06 28.01 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 28.01%) BI214 609.32 46.09* 1.453E+00 9.714E-07 1.157E-06 8.72 OK ( 0.0%) ( 4.96%) . (Decay 0.00%) (Area 8.72%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.753E-01 1.300E-06 1.548E-06 16.22 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 16.22%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 1764.51 15.92 6.174E-01 6.874E-07 8.186E-07 25.82 OK ( 0.0%) ( 4.80%) (Decay 0.00%) (Area 25.82%) PB214 74.81 6.33 1.983E+00 2.900E-06 3.305E-06 24.81 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 24.81%) 77.11 10.70 2.115E+00 2.648E-06 3.017E-06 16.18 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 16.18%) Absent Line Not Found 1 87.20 3.70 2.575E+00 89.80 1.03 2.684E+00 7.687E-06 8.760E-06 33.57 OK ( 0.0%) ( 4.07%) (Deca', 0. 00%) (Area 33.57%) Line Not Found

~~<< INT Reject 241.92 7.47 2.823E+00 295.22 19.20 2.491E+00 1.251E 06 1.425E-06 9.96 OK~~

( 0.0%) ( 5.08%) (Decay 0.00%) (Area 9.96%) 351.99 37.10* 2.207E+00 8.822E-07 1.005E-06 11.63 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 11.63%) Absent Line Not Found 785.95 1,09 1.180E+00 Absent Line Not Found RA224 83.78 0.21 2.430E+00 241.00 3.90* 2.825E+00 1.835E-06 1.836E-06 51.09 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 51.09%)
Nuclido Lino Error Propegotion Roport (continuod) Pcga : S Somplo ID : Horknoco #14 Acquisition dcto : 21-NOV-1997 21:23:06 i .uclide Type: natural Uncorrected Decay Corr 1 Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status RA226 185.99 3,28* 3.210E+00 2.085E 06 2.085E-06 38.64 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 38.64%) AC228 209.40 4.55 3.050E+00 1.133E-06 1.144E-06 43.77 OK ( 0.0%) ( 4.93%) (Decay 0.00%) (Area 43.77%) Absent Line Not Found 270.3.0 3.77 2.639E+00 Absent Line Not Found 328.00 3.36 2.320E+00 338.9 12.01 2.269E+00 9.421E-07 9.513E-07 32.44 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 32.44%) Absent Line Not Found 409,40 2.23 1.977E+00 463.00 4.64 1.800E+00 2.346E-06 2.369E-06 28.19 OK ( 0.0%) ( 4.42%) (Decay 0.00%) (Area 28.19%) Absent I 478.20 0.24 1.758E400 Line Not Found Absent Line Not Found 772.10 1.62 1.197E+00 794.80 4.84 1.168E+00 1.480E-06 1.495E-06 32.51 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 32.51%) s Absent Line Not Found 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 1.192E 06 1.203E-06 12.51 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 12.51%) Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 f 884E-01 9.022E-07 9.110E-07 36.37 OK ( 0.0%) ( 5.42%) (Decay 0.00%) (Area 36.37%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found
' " 14 63.29 3.90*
1.299E+00 92.38 2.57 2.788E+00 3.825E-06 3.825E-06 29.85 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 29.85%) 92.80 3.00 2.788E+00 3.276E-06 3.277E-06 29.85 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 29.85%) Absent Line Not Found 112.81 0.25 3.240E+00 4 Nuclide Types other Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status ANN-RD 511.00 193.40* 1.671E+00 3.354E-08 3.464E-08 55.58 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 55.58%) i Fleg: "*" = Keyline n
r s e I4!LLSTONE HEALTH PHYSICS-ENVIRONMENTAL 21-NOV-1997 22 04:31 (

~~Sample Information ----~~

~~$emplo ID~~
Harkness #15 Sample Quantity 1.00000E+03 g

37485 Spetrm Collector : HP Environmental S mplo Number Sample Analyst

HP Environmental Sample Deposition Information ----
~~Dap. Correction? : No Dep. Duration Deposition End i 21-NOV 1997 21:53:44 Dopocition Start :~~

~~Sample Decay / Count Information ----~~

~~S:mplo Date~~
~~21-HOV-1997 21:53:44 Acquisition date : 21-NOV-1997 21:53454 Docoy time 0 00:00:09.51~~
~~% dead time~~
~~0.0%~~
~~Elepood live times 0 00:10:00.00 Elapsed real time 0 00:10:00.24~~

~~Detector Parameters ----~~

~~Enorgy cal. time : 19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Datoctor name~~
~~Environmental Counting geom.ry: 1 Liter Soil Effic. cal, time i 19-JUL-1995 08:56:03 Effic, cal. oper.: HP Support~~

~~Processing Parameters ----~~

~~Start channel~~
100 End channel

3700 Sanoitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No Empirical Eff?
~~Yes Library-based eff No~~
1.00000 Half life ratio

8.00000 Enorgy tolerance Abundance limit

80.00000 WTM error limit

3.00000
~~dDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %~~
.-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left PW % Err Fit Nuclides 3 74.89 76 87 0.92 149.86 145 16 21.9 1.14E+00 PB214 PB212 3 77.19 132 83 1.00 154.46 ' 145 16 14.0 PB214 PB212 0 93.54 92 88 1.54 187.18 183 11 22.9 0 186,00 51 105 1.13 372.23 366 11 42.0 RA226 4 238.66 263 34 1.00 477.60 472 17 7.1 8.40E-01 PB212 4 241.88 45 43 1.77 484.06 472 17 35.4 RA224 1 295,20 109 18 1.40 590.75 587 21 10.8 2.52E+00 PB214 1 299.95 30 14 1.40 600.26 587 21 30.1 PB212 1 302.27 17 11 1.18 604.91 587 21 48.0 0 338.32 63 30 1.02 677.03 673 10 20.2 AC228 0 351.91 123 36 1.50 704.23 697 11 13.1 PB214 0 462.98 33 10 2.56 926.48 922 10 25.3 AC228 0 511.52 35 21 1.42 1023.62 1016 13 32.2 TL208 0 583.42 89 21 1.53 1167.48 1161 12 14.8 TL208 0 609.20 81 18 1.25 1219.06 1214 12 15.3 BI214 0 661.76 110 26 1,61 l's24.22 1316 17 14.2 CS137 0 727.74 16 14 1,53 1456.23 1451 8 47.5 BI212 0 860,91 13 12 1.64 1722.66 1716 12 62.4 TL208 0 911,07 68 5 2.13 1823.01 1817 11 13.8 AC228 0 968.98 34 2 1.90 1938.85 1935 8 18.6 AC228 AaO3 3
4. Post NID Pock Socrch Report (continusd) POg3 2 Scmple ID : Harkness #15 . Acquisition date : 21-NOV-1997 21:53:54 ( Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 1120.92 11 6 2.24 2242.79 2236 9 53.1 BI214 l 0 1460.75 221 0 2.31 2922.51 2916 13 6.7 K40 0 1764.79 17 0 1.49 3530.53 3524 12 24.3 BI214
~~Intorference Report Interfering Interfered Nuclide Line Nuclide Line i~~
PB214 241.92-RA224 241.00 TL208 510.72 ANN.RD 511.00 il ~ r 5 b 2 1 4 b 'l -3 a;
t Summary of Huelida Activity Pego : 3 ccmplo ID : Harkness #15 Acquisition date : 21-NOV-1997 21:53:54 l 131 number of lines in spectrum 23 ~ ( tbar of unidentified lines 0. Numb 3r of lines tentatively identified by NID 23 100.00%
~~natural Nuclide Type Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error~~
% Error Flags i X40 1.28E+09Y 1.00 1.318E-05 1.318E-05 0.089E-05 6.73 TL208 3.10M 2.59 3.098E-07 8.038E-07 1.188E-07 14.78 A BI212 60.55M 1.06 4.868E-07 5.161E-07 2.452*d-07 47.50 A FB212 10.64H 1.01 9.651E-07 9.705E-07 0.686E-07 7.07 A BI214 19.90M 1.19 5.447E-07 6.486E-07 0.991E-07 15.27 A PB214 26.80M 1.14 6.751E-07 7.693E-07 1.005E-07 13.07 A RA224 3.66D 1.00 1.835E-06 1.836E-06 0.651E-06 35.43 gRA226 1600.00Y. 1.00 2.159E-06 2.159E-06 0.907E-06 42.00 AC228 6.13H 1.01 1.014E-06 1.024E-06 0.141E-06 13.81 A Total Activity 2.117E-05 2.191E-05 EuclideLType : fission Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags CS137 30.10Y 1.00 4.288E-07 4.288E-07 0.611E-07 14.25 Total Activity : 4.288E-07 4.288E-07 arand Total Activity : 2.160E-05 2.234E-05 F1 cgs: "K" = Keyline not found "M" = Manually accepted "E" - Manually edited "A" = Nuclide specific abn. limit 7 c
Nuclida Lino Error Propogotion Roport Pcgo : 4 ' semple ID : Harkness #15 Acquisition date : 21-NOV-1997 21:53:54 f Nuclide Type natural Uncorrected Decay corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status K40 1460.75 10.70* 7.058E-01 1.318E-05 1.318E-05 6.73 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 6.73%) Line Not Found Absent TL208 277.36 6.50 2.596E+00 510.72 22.50 1.669E+00 4.251E-07 1.103E-06 32.17 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 32.17%) 583.14 86.00* 1.505E+00 3.098E-07 8.038E-07 14.78 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 14.78%) 860.47 12.00 1.093E+00 4.301E-07 1.116E-06 62.38 OK ( 0.0%) ( 5.61%) (Decay 0.00%) (Area 62.38%) DI212 727.17 11.80* 1.257E+00 4.868E-07 5.161E-07 47.50 OK g ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 47.50%) Absent Line Not Found 785.42 2.00 1.180E+00 Absent Line Not Found 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 PB212 74.81 9.60 1.989E+00 1.795E-06 1.805E-06 21.95 OK ( 0.0%) ( 4.15 % ) (Decay 0.00%) (Area 21.95%) 77.11 17.50 2.112E+00 1.614E-06 1.623E-06 14.03 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 14.03%) Absent Line Not Found 87.20 6.30 2.575E+00 238.63 43.10* 2.845E+00 9.651E-07 9.705E-07 7.07 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 7.07%) 300.09 3.27 2.466E+00 1.689E-06 1.698E-06 30.14 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 30.14%) 4 609.32 46.09* 1.453E+00 5.447E-07 6.486E-07 15.27 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 15.27%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.746E-01 3.656E-07 4.354E-07 53.14 OK ( 0.0%) ( 4. 61%) (Decay 0.00%) (Area 53.14%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 1764.51 15.92 6.173E-01 7.793E-07 9.280E-07 24.25 OK ( 0.0%) ( 4.80%) (Decay 0.00%) (Area 24.25%) PB214 74.81 6.33 1.989E+00 2.722E-06 3.102E-06 21.95 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 21.95%) I 77.11 10.70 2.112E+00 2.639E-06 3.008E-06 14.03 OK ( 0.0%) ( 4.10%) (Decay 0.000 (Area 14.03%) Absent Line Not Found 87.20 3.70 2.575E+00 Absent Line Not Found 89.80 1.03 2.675E+00 Line Not Found

~~<< INT Reject 241.92 7.47 2.823E+00 295.22 19.20 2.492E+00 1.029E-06 1.173E-06 10.78 OK~~

( 0.0%) ( 5.09%) (Decay 0.00%) (Area 10.78%) 351.99 37.10* 2.207E+00 6.751E-07 7.693E-07 13.07 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 13.07%) Absent Line Not Found 785.95 1.09 1.180E+00 Absent Line Not Found RA224 83.78 0.21 2.430E+00 241.00 3.90* 2.823E+00 1.835E-06 1.836E-06 35.43 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 35.43%) b
e sa Nuclido Lino Er4*or Propogotion Roport (continued) Pogo : 5 Scmplo ID Harkness #15 Acquisition date : 21-NOV 1997 21:53:54 .uclide Types natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status l RA226 185.99 3.28* 3.212E+00 2.159E-06 2.159E-06 42.00 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 42.00%) Absent Line Not Found AC228 209.40 4.55 3.050E+00 Absent Line Not Found 270.30 3.77 2.639E+00 Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.. 2.270E+00 1.042E-06 1.052E-06 20.17 OK ( 0.s ( 4.73%) (Decay 0.00%) (Area 20.17%) Absent Line Not Found 409.40 2.23 1.977E+00 463.00 4.64 1.802E+00 1.758E-06 1.775E-06 25.27 OK ( 0.0%) ( 4.42%) (Decay 0.00%) (Area 25.27%) Absent Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 Absent Line Not Found 794.80 4.84 1.169E400 Absent Line Not Found 835.60 1.82 1.121E+00 911,07 29.00* 1.042E+00 1.014E-04 1.024E-06 13.81 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 13.81%) Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 9.889E-01 8.848E 07 84934E-07 18.65 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 18.65%) Absent Line Not Found 1587.90 3 71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 P ide Types fission Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uC1/g uCi/g % Error Status 'S137 661.62 84,62* 1.359E+00 4.288E-07 4.288E-07 14.25 OK ( 0.0%) ( 5.10%) (Decay 0.00%) (Area 14.25%) Flag Keyline k
U
~~,n 6~~
~~. MILLSTONE HEALTH PHYSICS ENVIRONMENTAL 21-NOV-1997 19:15:25 -- - Sample Information ---- \\.nple ID~~
Harkness #26 Sample Quantity

1.00000E+03 g Sample Number

37476 Spetrm Collector HP Environmental Sample Analyst HP Environmental

~~Sample Deposition Information ----~~

~~No Dep. Duration Dap. Correction?~~
~~D3pocition Start Deposition End 21-NOV-1997 19:04:33~~

~~Sample Decay / Count Information ----~~

~~Semple Date~~
~~21-NOV 1997 19:04:33 Acquisition date : 21-NOV-1997 19:04:43 Dacoy time 0 00:00:09.67~~
~~% dead time~~
~~0.1%~~
~~Elepsed live time 0 00:10:00.00 Elapsed real times 0 00:10:00.34~~

~~Detector Parameters ----~~

~~Energy cal. time : 19-JUL-1995 08:05:48 Energy cal, oper.: HP Support 4 --Datoctor name~~
~~Environmental Counting geometry: 1 Liter Soil Effic.. cal. time 19-JUL-1995 08:56:03 Effic, cal. oper, HP Support~~

~~Processing Parameters ----~~

~~Start channel~~
100 End channel 3700

4.50000 Gaussian Sens.

10.00000 Sanoitivity Critical level?

Yes Propagate Errors?: No Empirical Eff?

Yes Libran-based eff: No Energy tolerance : 1.00000 Half life ratio

8.00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM)' : 5.00000 MDA Confid Level : 3.00000 %
-NID Peak search Report It' Energy Area Bkgnd FWHM Channel Lt!: Pw % Err Fit Nuclides 3 74.85 114 98 0.88 149.77 144 16 16.0 1.45E+00 PB214 PB212 3 77.20 161 117 0.97 154.47. 144 16 13.0 PB214 PB212 2 87.25 62 142 1.11 174.60 170 14 32.9 1.44E+00 PB214 PB212 2 89.96 59 106 1.20 180.01 170 14 34.2 PB214 0 93.42 83 137 2.81 186.95 183 9 27.4 0 129.05 39 124 0.68 258.24 254 8 52.4 1 0 209.70 37 115 0.64-419.64 413 11 59.1 AC228 4 238.64 498 60 1.13 477.56 473 16 5.1 1.23E+00 PB212 4 241.41 51 69 1.70 483.11 473 16 49.1 RA224 0 270.31 49 46 1.04 540.95 537 9 29.1 AC228 0 295.21 69 48 1.11 590.77 586 10 22.4 PB214 0-300.50 31 48 1.47 601.35 597 9 44.6 PB212 0 338.60 .134
~~27. 1.36 677.60 673 13 12.1 AC228 0~~
352.11-113 47 0.95 704.64 700 11-14.8 PB214 0< .510.80 _ 59 28 1.36 1022.17 1016 11 21.4 TL208 0 .583.06 167 -24 1.33 1166.75 1162 13 9.5 TL208 0-609.13-94 12 1.81 1218.91 1213 12 12.7 BI214. 0 768.19 20-10 1.29.1537.16 -1531 10 36.2 BI214 0. 785.82 15 6 1.16.1572.43 1569 8 39.2 P"214 =
f' .e Post-HID Pock Sacrch Roport (continued) Pcgo 2 scmple ID : Horknoco #16 Acquisition dato : 21-NOV-1997 19:04s43 l .( Energy Area Bkgnd FWlD4 Channel Left PW % Err Fit Huclides 0 795.50 16 -17 1.77 1591.79 1583 11 55.1 AC228 0 860.94 38 17 1.57 1722.71 1715 17 29.7 TL208 O 911.04 123 6 1.53 1822.93 1818 11 9.8 AC228 0 958.97 9 2 1.42 1918.82 1916 6 38.9 0 969.16 52 21 1.65 1939.21 1933 11 22.3 AC228 0 1210.22 19 9 4.28 2421.42 2415 13 41.5 i 0 1460.69 375 4 1.81 2922.39 2915 15 5.3 K40 { Interference Report Interfaring Interfered j y Nuclide Line Nuclide Line PB214 241.92 RA224 241.00 TL208 510.72 ANN-RD 511.00 i + ~ .m -y
f. e ' summary of Nuclida Activity P ga 3 ,S mple ID : Harkness #16 Acquisition dato : 21-NOV-1997 19:04:43 ( um.cl number of lines in spectrum . ne 26 Der of unidentified linea 3 ber of lines tentatively identified by NID 23 88.46% Nuclide Type : natural Uncorrected Decay Co2r Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uC1/g 1-Sigma Error % Error Flags K40 1.28E+09Y 1.00 2.238E-05 2.238E-05 0.118E-05 5.28 TL208 3.10M 2.60 5.826E-07 1.513E-06 C.144E-06 9.53 A PB212 10.64H 1.01 1.830E-06 1.840E-06 0.095E-06 5.14 A BI214 19.90M 1.19 6.320E-07 '/.528E-07 0.954E-07 12.68 A PB214 26.80M 1.14 6.245E-07 7.118E-07 1.051E-07 14.77 A RA224 3.66D 1.00 2.097E-06 2.099E-06 1.031E-06 49.14 AC228 6.13H 1.01 1.826E-06 1.844E 06 0.180E-06 9.77 A Total Activity a bbb7bbb bkk4bbb I Grand Total Activity : 2.997E-05 3.11<E-05 Flego: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit / I
i I i.. Nuclido Lino Error Fropagation Report pe 4 , Semple ID : Herknoco #16 Acquioition dato 21-NOV-1997$a9:04:43 i i b elide Types natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uC1/g uCi/g % Error Status X40 1460.75 10.70* 7.058E-01 2.238E-05 2.238E-05 5.28 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 5.28%) Line Not Found Absent TL208 277.36 6.50 2.596E+00 510.72 22.50 1.671E+00 7.125E-07 1.850E-06 21.45 OK - ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 21.45%) 583.14 86,00* 1.505E+00 5.826E-07 1.513E-06 9.53 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 9.53%) 860.47 12.00 1.093E+00 1.305E-06 3.389E-06 29.69 OK ( 0.0%) ( 5.62%) (Decay 0.00%) (Area-29.69%) FB212 74.81 3.60 1.987E+00 2.701E-06 2.716E-06 _15.95 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 15.95%) I 77.11 17.50 2.112E+00 1.960E-06 1.971E-06 13.03 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area-13.03%) 87.20 6.30 2.577E+00 1.724E-06 1.734E-06 32.89 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 32.89%) 238.63 43.10* 2.845E+00 1.830E-06 1.840E-06 5.14 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.14%) 3LV 09 3.27 2.463E+00 1.732E-06 1.741E-06 44.57 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 44.57%) BI214 609.32-46.09* 1.454E+00 6.320E-07 7.528E-07 12.68 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 12.68%) 768.36 4.89 1.202E400 1.570E-06 1.870E-06 36.24 OK ( 0.0%) ( 5.41%) (Decay 0.00%) (Area 36.24%) Absent Line Not Found 934.05 3.16 1.020E+00 Absent Line Not Found 1120.28 15.04 8.750E-01 Absent Line Not'Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3,05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PB214 74.81 6.33 1.987E+00 4.096E-06 4.669E-06 15.95 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 15.95%) 77.11 10,70 2.112E+00 3.206E-06 3.654E-06 13.03 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 13.03%) 87.20 3.70-2.577E+00 2.935E-06 3.345E-06 32.89 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 32.89%) 89.80 1.03 2.681E+00 9.572E-06 1.091E-05 34.16 OK (-0.0%) ( 4.07%) (Decay 0.00%) (Area 34.16%) Line Not Found

~~<< INT Reject 241.92 7.47 2.823E+00~~

=---- 295.22 19.20 2.492E+00 6.465E-07 7.368E-07 22.36 OK - ( 0.0%) ( 5.09%) (Decay 0.00%) (Area 22.36%) 351.99 37.10*. 2.207E+00 6.245E-07 -7.118E-07 14.77 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 14.77%) '785.95 1.09-1.180E+00 5.130E-06 5.846E-06 39.23 OK ( 0,0%); ( 5.46%) (Decay 0.00%) (Area 39.23%) Absent Line Not Found RA2241 83.78 0.21 2.430E+00 241.00 3;90* 2.826E+00 -2.097E-06. 2.099E-06 49.14 OK ( 0.0%)- ( 5.05%) (Decay 0.00%) (Area 49.14%) AC228 209.40 4.55 -3.048E+00 1.191E 06 1.202E-06 59.08 OK (,0.0%) _ ( - 4. 93 %) '(Decay 0.00%)_ (Area 59.08%) L _ := 2 - ~
- - - - ~ t ' Nu'elido Lina Error Propogotion Roport (continu9d) POg3 : 5 ,Scmple ID : Harkness #16 Acquisition date : 21-NOV-1997 19:04:43 k.uclideTypesnatural 4 Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff UCi/g uCi/g % Error Status 270.30. 3.77 2.639E+00 2.210E-06 2.231E-06 29.07 OK ( 0.0%) ( 5.16%) (Decay 0.00%) (Area 29.07%) Line Not Found Absent 328.00 3.36 2.320E+00 338.40 12.01 2.269E+00 2.223E-06 2.245E-06 12.14 OK ( 0.0%) ( 4.72%) (Decay 0.00%) (Area 12.14%) Absent Line Not Found 409.40 2.23 1.977E+00 Absent Line Not Found 463.00 4.64 1.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 794.80 4.84 1.168E+00 1.280E-06 1.293E-06 55.12 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 55.12%) I 835.60 1.82 1.121E+00 Absent Line Not Found 911.07 29.00* 1.042E+00 1.826E-06 1,844E-06 9.77 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 9.77%) Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 9.888E-01 1.349E-06 1.363E-06 22.34 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 22.34%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 = Keyline Flcg m 1
u
~~r. -~~
~~KILf9 TONE HEALTH PHYSICS ENVIRONMENTAL 21-NOV-1997 19:15:25~~

~~Sample Information ----~~

~~wnple ID -~~
Harkness #16 Sample Quantity 1.00000E+03 g Scmple Number

37476 Spctrm Collector : HP Environmental l
~~Sample Analyst~~
~~HP Environmental~~

~~Sample Deposition Information ----~~

~~l Dop. Correction?_i No Dep. Duration a Doposition Start : Deposition End~~
~~21-NOV-1997 19:04:33 4~~

~~Sample Decay / Count Information ----~~

~~Sample Date~~
~~21-NOV-1997 19:04:33 Acquisition date : 21-NOV-1997 19:04:43 Dacey time 0 00:00:09.67~~
~~% dead time~~
~~0.1%~~
~~Elepoed live time 0 00:10:00.00 Elapsed real times.O 00:10:00.34~~

~~Detector Parameters ----~~

~~, Energy cal, time 19-JUL-1995 08:05:48 Energy cal. oper.: HP Support Datoctor name~~
~~Environmental Counting geometry: 1 Liter Soil Effic, cal, time : 19-JUL-1995 08:56:03 Effic, cal, oper.: HP Support~~

~~Processing Parameters ----~~

~~Start channel~~
100 End channel

3700 Ssnsitivity

4.50000 Gaussian Sens.
~~i 10.00000 Critical level?~~
Yes Propagate Errors?: No Empirical Eff?

Yes Lioran-based eff No

En3rgy tolerance 1.00000 Half life ratio

8.00000 Abundance limit i 80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
i -HID Peak Search-Report It Energy Area Bkgnd FWHM Channel ' Left Pw % Err Fit Nuclides 3 74.85 114 98 0.88 149.77 144 16 16.0 1.45E+00 PS214 PB212 3 -77.20 161 117 0.97 154.47. 144 ~6 13.0 PB214 PB212 2-87.25 62 142 1.11 174.60 l'i 0 14 32.9 1.44E+00 PB214 PB212 2 89.96 59 106-1.20 180.01 170 14 34.2 PB214 0 93.42 83 137 2.81 186.95 183 9 27.4 0 129.05 39 124 0.68 258.24. 254 8 52.4 0-209.70 37 115 0.64 419.64 413 11 59.1 AC228 4 238.64 498 60 1.13 477.56 473 16 5.1 1.23E+00 PB212 '4 241.41 51 69 1.70' 483.11 413 16 49.1 RA224 O_ 270.31 49 46 1.04 540.95 537 9 29.1 AC228 0 295.21 69 48 .1.11 590.77 586 10 22.4 PB214 0' 300.50 31 48 1.47 601.35 597 9 44.6 PB212 0 338.60 134-27 1.36 677.60 673 13 1:2.1 AC228 4 0-352.11 113 47 0.95 704.64 700 11 14.8 PB214 - (L 510.80 59 28-1.36 1022.17~ 1016 11 21.4 TL208-O' 583.06: 167 24 -1.33 1166.75 1162 13 9.5 TL208 0-609.13 94 12 1.81'1218.91 1213-12.12.7 BI214 0. 768.19 -20 10 1.29 1537.1f 1531-10 36.2 BI214 0' 785.82 15 1.16 1572.43 1569 8 39.2 -PB214 y CC?T m 4 ,,e- .m m ---w-+,. ~r .r-
(. PostsyID. Pock Search Rcport (continued) Pago : 2 Scmpid.TD : Harknoco #16 Acquioition dsto : 21-NOV-1997 19:04:43 ( Energy Area Skgnd FWHM Channel Left Pw % Err Fit Nuclides 0 795.50 16 17 1.77 1591.79 1583 11 55.1 AC228 0 860.94 38 17 1.B7 1722.71 1715 17 29.7 TL208 0 911.04 123 6 1.53 1822.93 1818 11 9.8 AC228 0 958.97 9 2 1.42 1918.82 1916 6 38.9 0 969.16 52 21 1.65 1$39.21 1933 li 22.3 AC228 0 1210.22 19 9 4.28 2421.42 2415 13 41.5 0 1460.69 3'S 4 1.81 2922.39 2915 15 5.3 K40 Intorference Report Interfering Interfered 3 - Nuclide Line Nuclide Line PB214 241.92 RA224 241.00 TL208 510.72 ANN-RD 511.00 I
10, 'I Su 27 Qf Nuclide Activity Paga-3 .Scmp o'ID:-Harkna.is,#16 Acquisition dote : 21-NOV-1997 19: 04:43= 3" t.11-number of-lines in spectrum 26 ber of unidentified--lines 3 'humbar.of11fnes1 tentatively identified by NID 23 88.46% -Nuclide Type-: natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g-uCi/g-Sigma Error % Error Flags-K40-1.28E+09Y 1.00 2.238E-05 2.238E-05 0.118E-05 5.28 TL208 3.10M 2.60 -5.826E-07 1.513E-06 0.144E-06 9.53 A PB212-10.64H 1.01 1.830E-06 1.840E-06 0.095E-06 5.14. - A BI214 19.90M .1.19 6.320E-07 7.528E-07 0.954E-07 12.68 A- -PB214 26.80M 1.14 6.245E-07 7.118E-07 1.051E-07 14.77 A-RA224 3.66D 1.00 2.097E-06 2.099E-06 1.031E-06 49.14 AC228 6.13H 1.01 1.826E-06 -1.844E-06 0.180E-06 9.77 A I Total. Activity : h$hh7bbh 3$kk4bhh 4 p Grand Total' Activity-: 2.997E-05 3.114E-05 .Flago "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit t L. ( '1 ~ .._m___
q Nucadda -Line Error Propagstion Report - Pago : 4' ,S:mple ID : _Harkness-#16 Acquisition dato_: 21-NOV-1997f19:04:43 .fi -\\-huclide Type nacural Uncorrected Decay Corr 1-Sigma Energy. %Abn %Eff uCi/g uCi/g % Error Status Nuclide.-1460.75 -10.70* 7.058E-01 -2,238E-05 2.238E-05 5.28 OK X40 -(- 0.0%) -( 4.45%) (Decay 0.00%) (Area 5.28%) Line Not Found Absent TL208 277.36 6.50 2.596E+00 510.72 22.50 1.671E+00 7.125E-07 1.850E-06 21.45 OK ( 0.0%) ( 4.62%)- (Decay 0.00%) (Area 21.45%) 583.14 86.00* 1.505E+00 5.826E-07 1.513E-06 9.53 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 9.53%) 860.47. 12.00 1.093E+00 1.305E-Ou 3.389E-06 29.69 OK ( 0.0%) ( 5.62%) (Decay 0.00%) (Area 29.69%) PB212 74.81 9.60 1.987E+00 2.701E-06 2.716E-06 15.95 OK i -( 0.0%) ( 4.15%) (Decay 0,.4 ') (Area 15.95%) -l g 77.11-17.50 2.112E+00 1.960E-06
~~1. 9 71E .~~
13.03 OK _( 0.0%) ( 4.10%) (Decay 0.So o (Arca 13.03%) 87.20 6.30 2.577E+00 1.724E-06 1.734E-06 32.69-OK ( 0,0V) ( 4.05%) (Decay 0.00%) -(Area 32.89%) 238.63 43.10* 2.845E+00 1.830E-06 1.840E-06 5.14-OK-( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.14%) 300.09 3.27 2.463E+00 1.732E-06 1.741E-06 44.57 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 44.57%) -BI214 609.32 46.09* 1.454E+00 6.320E-07 7.528E-07 12.68 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 12.68%) 768.36 4.89 1.202E+00 1.570E-06 1.870E-06 36.24 OK ( 0.0%) ( 5.41%) (Decay 0.00%) (Area 36.24%) Absent Line'Not Found 934.05 3.16 1.020E+00 Absent Line Not Found 1120.28 15.04 8.750E-01. Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Fcund 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PB214 74.81-6.33 1.987E+00 4.096E-06 4.669E-06 15.95 OK _( 0.0%) ( 4.15 % ) (Decay 0.00%) (Area 15.95%) 77.11 10.70 2.112E+00 3.206E-06 3.654E-06 13.03 OK ( 0.0%) ( 4.10% ) _ -(Decay 0.00%) (Area 13.03%) 07.20 3.70 2.577E+00 2 935E-06 3.345E-06 32.89 OK ( 0.0%) ( 4.05%) (Decay 0,00%) ( Area ' 2. 8 9%)- 89.80 1.03 2.681E+00 9.572E-06 1.091E-05 34.16 OK ( 0.0%)- - ( - 4. 07%) (Decay-0.00%) (Area 34.16%) Line ' Not Foud - ----- << INT Rej ect 241.92 7.'47 2.823E+00-295.22 19.20 2.492E+00 6.465E-07 7.368E-07 22.36 OK (-0.0%) ( 5.09%) (Decay 0.00%) (Area 22.36%) 351.991 37.10* 2.207E+00. 6.245E-07 7.118E-07 14.77 OK ( 0. 0 %)- . ( 4.58%) - (Decay 0.00%)- (Area 14.77%)' 785.95 - 1. 10 9 1.180E+00 5.130E-06 5.846E-06 '39.23 OK .( 0.0%)- ( 5.46%). (Decay 0.00%) (Area 39.23%)' Absent Line Not-Found .RA224 83.78 0.21 2.430E+00 241'.00 3.90* 2.826E+00' 2.097E 2.099E-06 49.14 OK. ( 0.0%): ( 5.05%) (Decay 0.00%) (Area 49.14%) 'AC226 209.40-14.55 3.048E+00 1.191E-06 1.202E-06 59.08 OK ,10.0%) ( 4.93%) (Decay 0.00%) (Area 59.08%) ( .t I.
r , Sam}plo' ID :Uuc ida, Lina Error Propagotion Roport (continuad) Pcga : 5 Horknaco #16 Acquisition dato : 21-NOV-1997 19:04:43 I haclide Type natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status 270.30 3.77 2.639E+00 2.210E-06 2.231E-06 29.07 OK ( 0.0%) ( 5.16%) (Decay 0.00%) (Area 29.07%) Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.269E+00 2.223E-06 2.245E-06 12.14 OK ( 0.0%) ( 4.72%) (Decay 0.00%) (Area 12.14%) Absent Line Not Found 409.40 2.23 1.977E+00 Absent Line Not Found 463.00 4.64 1.802E+00 Absent Line Not Found 470.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 794.80 4.84 1.168E+00 1.280E-06 1.293E-06 55.12 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 55.12%) g Absent Line Not Found 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 1.826E-06 1.844E-06 9.77 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 9.77%) Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 9.888E-01 1.349E-06 1.363E-06 22.34 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 22.34%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Fleg: "*" = Keyline "I
, MILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 21-NOV-1997 17:03:49
~~y g~~

~~Sample Information ----~~

~~f T plo ID.~~
-Harkness #17 Sample Quantity

1.00000E+03 g Simplo: Number _

37470 Spctrm Collector : HP Environmental Sample Analyst

HP Envirormental

~~Sa'mple Deposition Informati'on ----~~

~~Dap. Correction? : No Dep.- Duration Daposition. Start : Deposition End~~
~~21-NOV-1997 16:53:07~~

~~Sample Decay / Count Information ----~~

~~. Simple Date~~
~~21-NOV 4997 16:53:07 Acquisition date : 21-NOV-1997 16:53:14 Dacay time 0 00:00:07.60~~
~~% dead-time~~
~~0.1%~~
~~Elepsed live. time: 0 00:10:00.00 Elapsed real times 0 00:10:00.36~~

~~Detector Parameters ----~~

~~] Enorgy cal. time : 19-JUL-1995 08:05:48 Energy cal. oper.: HP Support Datoctor name~~
~~Environmental Counting geometry: 1 Liter Soil Effic.z cal. time : 19-JUL-1995 08:56:03 Effic, cal, oper.: HP Support~~

~~Processing Parameters.----~~

~~Start channel~~
100 End channel

3700 Sannitivity

4.50000 Gaussian Sene.

10.00000-Critical level?

-Yes Propagate Errors?: No Empirical Eff?

Yes Library-based eff: No
~~-Energy tolerance : 1.00000 Half life ratio~~
8,00000 Abundance limit- : 80.00000 WTM error limit

3.00000 MDA Width (FWHM)- : 5.00000 MDA Confid Level : 3.00000 %
-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 .74.66 93 148 1.07 149.39 146 7 24.0 PB214 PB212 0 77.37-137 153 1.01 154.81 152 7 17.3 PB214 PB212 4 92.81 49 62 0.96 185.73 184 8 27.3 3.43E+00 TH234 TH234 4 -93.95 50 93 1.00 188.00 184 8 36.0 0 186.08 84 88 1.78 372.38 367 10 23.7 RA226 0 209.47 47 108 0.96 419.18 414 10 44.3 AC228 3 238.61 506 39 1.20 477.50 474 1-6 4.9-1.81E+00 PB212 I 3 241.26. 67 46 1.51-482.80 474 16 35.2 -RA224 0 269.88 65 72. 1.83 540,07 534 13 29.6 AC228 0, 295.43 85 51 1.03-'591.21 587-9 18.7 PB214 0 '327.76 53 42 1.40 655.92 650 13 28.7 AC228 0 338.29 117 34 0.85 676.97 672 10 13.2 AC228 0, 352.12
~~112 60 1.28--~~
704.66 699 10 16.0 PB214 0 510.41 16 6 - 45-1.45 1021.39 1013 15 25.3 TL208 0 583.10~ 157 13' 1.55 1166.84 1160 12 9.1 TL208 0 609.18 - 114 19 1,72 1219.02 1213 11 12.0 BI214 0 727.18 1304 15 -1.57 1455.11 1450.10 30.1 BI212 0 .795.04 17 22-1.04 1590.88 1586 11 58.7 AC228 0 861.21 27 11 1,69 1723.25 1714 15 33.3 TL208 V u o [
Post-NID Pack Search Report (continued) Paga : 2 ,S:mplo ID : Harknoso #17 Acquisition date : 21-NOV-1997 16:53:14 ~ Energy-Area Bkgnd FWHM Channel Left PW % Err Fit Nuclides .(V 911.00 126 4 1.59 1822.86 1815 15 9.5 AC228 0 964.71 25 9 1.24 1930.32 1925 9 29.5 AC228 0 968.97 68 14 1.72 1938.83 1934 11 16.1 AC228 0 1119.73 30 13 2.46 2240.41 2233 14 32.4 BI214 0 1460.67 460 3 1.92 2922.33 2916 14 4.7 K40 Interference Report Interfering Interfered Nuclide Line Nuclide Line PB214 241.92 RA224 241.00 g TL208 510.72 ANN-RD 511.00 4 4 e
Summary of Nuclide Activity Pcga : 3 ,Sen1plc ID : Harkness #17 Acquisition dato : 21-NOV-1997. 16:53:14 4 -Total number of lines in spectrum 24 ter of unidentified lines 1 ,( aber of lines tentatively identified by NID 23 95.83% Nuclide Type : natural Uncorrected Decay corr Decay Corr 1-Sigma P 'lide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags K.*! 1.28E+09Y 1.00 2.743E-05 2.743E-05 0.130E-05 4.74 TL2b8 3.10M 2.58 5.476E-07 1.411E-06 0.129E-06 9.12 A BI212 60.55M 1.06 9.143E-07 9.691E-07 2.921E-07 30.14 A PB212 10.64H 1.01 1.859E-06 1.869E-06 0.091E-06 4.89 A B1214 19.90M 1.19 7.634E-07 9.081E-07 1.091E-07 12.01 A PB214 26.80M 1.14 6.167E-07 7.022E-07 1.124E-07 16.01 A RA224 3.66D 1.00 2.719E-06 2.721E-06 0.959E-06 35.23 RA226 1600.00Y 1.00 3.599E-06 3.599E-06 0.852E-06 23.63 g AC228 6.13H 1.01 1.885E-06 1.903E-06 0.181E-06 9.49 A TH234 24.10D 1.00 2.666E-06 2.666E-06 0.729E-06 27.33 KA Total Activity : 4.300E-05 4.418E-05 Grand Total Activity : 4.300E-05 4.418E-05 Flags: "K" = Keyline not found "M" = Manually accepted "E" - Manually edited "A" = Nuclide specific abn. limit i b p e
I Nuc1'ida Lina Error Propagation Report Pega : 4 n,S:qple ID : Harkneso #17 Acquisition date.: 21-NOV-1997 16:53:14 4. 41de; Types natural Uncorrected Decay Corr 1-Sigma Nuclide. Energy %Abn
~~%Eff~~
-uCi/g uCi/g % Error Status .K40-1460.751 10.70* 7.058E-01' 2.743E-05 2.743E-05 4.74-OK-( 0.0%) ( 4.45%) (Decay 0.00%) (Area 4.74%) Line Not Found Absent TL208 277.36 6.50 2.596E+00' 510.72 22.50 1.672E+00 7.904E-07 2.037E-06 25.34 OK ( 0.0%) ( 4.61%) (Decay 0.00%) (Area 25.34%) 583.1'4 86.00* _ 1.505E+00 5.476E-07 1.411E-06 9.12 OK ( 0.0%) ( 4.08%) (Decay 0.00%) (Area 9.12%) 860.47 12.00 1.092E+00 9.232E-07 2.379E-06 33.33 OK ( 0.0%) ( 5.62%) (Decay 0.00%) (Area 33.33%) BI212 727.17 11.80* 1.258E+00 9.143E-07 9.691E-07 30.14 -OK-g- 785.42 '( 0.0%) ( 5.30%) (Decay 0.00%) (Area 30.14%) Absent Line Not Found 2.00 1.180E+00 Absent Line Not Found -1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 PB212 74.81 9.60 - 1.976E+00 2.206E-06 -2.219E-06~ 24.02 OK: ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 24.02%) 77.11 17.50. 2.121E+00 1.665E-06 1.674E-06 17.28 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 17.28%) Absent Line Not Found 87.20 6.30 2.575E+00 238.63 43.10*- 2.845E+00 1.859E-06 1.869E-06 4.89 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 4.89%) Absent Line Not Found 300.09 3.27 2.465E+00 BI214-609.32 46.09*. 1.453E+00 7.634E-07 9.081E-07 12.01 OK ( 0.0%) ( 4.96%) (Decay 0.00%) -(Arca 12.01%) Absent. Line Not Found -768.36 4 89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28-15.04 8.754E-01 1.012E-06 1.204E-06 32.42 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 32.42%) Absent Line Not Found 1238.11 '5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found -1509.19 2.19 6.885E-Ci Absent Line Not Found 1729.Er 3.05 6.254E-01 Absent Line Not Found '1764.51 15.92 6.173E-01 -PB214 74.81 6.33 1.976E+00 3.346E-06 3.810E-06 24.02 OK ( 0.0%) - ( 4.15 % ) (Decay-0.00%) (Area 24.02%) 77.11 10.70 2.121E+00- 2.723E-06 3.101E-06 17.28 OK ( 0.0%) ( 4.10%) (. Decay 0.00%) (Area 17.~28%) Absent i Line Not Found 87.20 3.70 2.575E+00 I 89.80 1.03 2,675E+00 Absent Line Not Found Line Not Found

~~<< INT Reject 241 92 7.47; 2.823E+00 295,22 19.20 2.491E+00 8.017E-07' 9.129E-07 18.67 OK~~

( 0.0%) (=5.08%) (Decay 0.00%) -(Area.18.67%) 351.99 37.10*- 2.206E+00 6.167E-07. 7.022E-07 16.01 OK' (10.0%) ( 4.58%) (Decay 0.00%)- (Area 16.01%) -Absent. Line Not Found 785'.95 1'.09 1.180E+00 Absent Line Not Found RA224 83.78 0.21 --2.430E+00 241.00 3.90* -2.827E+00 -2.719E-06 2.721E 35.23 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 35.23%) -RA226= 185.99-13.28* _ 3.211E+00- 3.599E-06 3.599E-06 23~.68-OK (;0.0%) (-4.85%)' -(Decay 0.00%)- (Area 23.68%) i p w tz 1
.... ~. .. -. -. _ - _ -. -... ~ _ o. Nuclida Lino Error' Propagation. Report (continued) Page : 5 =, Semple,L ID : Harkness #17 - Acquisition date : 21-NOV-1997 16:53:14 4... 4' aide Type ' natural: Uncorrected Decay' Corr 1-Sigma-Nuclide Energy %Abn -%Eff uCi/g uCi/g % Error Status L -AC228 209.40 4.55 -3.049E+00 -1.520E-06 1.534E-06 44.27 OK- ~ ( 0.0%) ( 4.93%) (Decay 0.00%) (Area 44.27%) 270.30~ 3.77 2.641E+00 2.937E-06 2.966E-06 29.60 OK ( 0.0%) ( 5.15%) (Decay 0.00%) '(Area 29.60%) 328.00 3.36 2.321E+00 3.069E-06 3.099E-06 28.65 OK ( 0.0%) ( 4.83%) (Decay 0.00%) (Area 28,65%) ~ 338.40 12.01 2.270E+00 1.934E-06 1.953E-06 13.19 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 13.19%) Line Not Found - Absent 409.40 2.23 1.977E+00 Absent Line Not Found 463.00-4.64 1.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 Absent 772.10 1.62 1.197E+00 ' Line Not Found -794.80 -4.84 1.168E+00 1.354E-06 1.367E-06 58.68 OK ( 0.0%) (- 5.4 8%)- (Decay 0.00%) (Area 58.68%) Absent Line Not-Found 835.60 1.82 1.121E+00. 911.07 29.00* 1.042E+00- 1.885E-06 1.903E-06 9.49 OK (-0.0%) ( 5.64%) (Decay 0.00%) (Area 9.49%) 964.60 c.45 9.926E-01 2.082E-06 2.102E-06 29.46 OK ' s.0%) ( 5.445) (Decay 0.00%) (Area 29.46%) 968.90 17.46 9.889E-01 1.773E 1.790E-06 16.10 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 16.10%) t Absent Line Not Found 1587.90-3.71 6.633E-01 Absent Line Not Found 1630.40 1.'95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 .9:2.38 2.57 2.781E+00 3.112E-06 3.112E-06 27.33 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 27.33%) 92.80 3.00 2.781E+00 2.666E-06 2.666E-06 27.33 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 27.33%)- Absent Line Not Found 112.81 0.25 3.240E+00 = Keyline
~~Flag~~

A t i 4 9 4 s v e r-y y-y q w-,- e v --g .-%r
I n.sy... .)4ILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 21-NOV-1997 15:07:42 -( mple ID Sample Information ----
Harkness-#18-Sample Quantity- : 1.00000E+03 g Sample Number

37467 Spctrm Collector : HP Environmental Sample Analyst

HP Environmental

~~Sample Deposition Information ----~~

~~Dap. Correction? : No Dep. Duration Deposition End~~
~~21-NOV-1997 14:57:00 Dapasition Start~~

~~Sample Decay / Count Information ----~~

~~Scmple Date~~
~~21-NOV-1997 14:57:00 Ac@isition date : 21-NOV-1997 14:57:06 D3 cay time 0 00:00:06.14~~
~~% dead tire~~
~~0.1%~~
~~Elepeed live time: 0 00:10:00.00 Elapsad I.al time: 0 00:10:00.32~~

~~Detector Parameters ----~~

~~Energy cal. time : 19-JUL-1995 08:05:48 Energy cal. oper.: HP Support Countin 1 Liter Soil Detector name~~
~~Environmental Effic, g_ geometry:~~
~~cal.- oper.: HP Support Effic, cal. time : 19-0UL-1995 08:56:03~~

~~Processing Parameters ----~~

~~Start channel~~
100 End channel

3700 Soncitivity.

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No Empirical Eff?

Yes
~~' Libra g-based eff: No Energy tolerance : 1.00000 Half life ratio~~
8.00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width fFWHM) : 5.00000 MDA Confid Level : 3.00000 %
-NID Peak Search Report It Energy Area Bkynd FWHM Channel Left Pw %".rr Fit Nuclides 0 77.72 124 225 0.88 155.52 151 10 26.3 PB214 PB212 0 89.83 71 99 1.43 179.75 178 6 25.3 PB214 0 93.25 89 126 0.89 186.61 184 8 24.2 TH234 TH234 0 -209.36 82 90 1.31 418.97 414 11 25.4 AC228 5 238,57 502 37 1.12 477.42-473 23 4.9 1.45E+00 PB212 5 241.79 80 48 1.85 483.87 473 23 29.7 . RA224 2 270.10-56 41 1.51 540.52 534 25 25.4 1.40E+00 AC228 1 2 277.19 25 41 1.52 554.71 534 25.49.7 TL208 0 295.58-68 58 1.26 591.51 588 10-24.3 PB214 0-338.34 90 48 1.03 677.07 672 10 17.8 AC228 0 352.10 100 63 1.31 704.61 699 13 19.1 PB214 0 462.78. 23 18 1.25 v26.09 920-9 39.3 AC228 0 510.88' 53 25 1.58 1022.33 1017 14 24.2 TL208 0 582.18 .76 18 1.43 1167.00 1162 13 9.1 TL208 0. -609.67 75 35 0.91 1219.99' 1212 17 22.0 BI214 0 727.41 44 6 1.26 1455.57 1450 11 18.4 BI212 0 794.82 25 9 1,56 1590.43 1583 12 31.5 AC228 0- '860.07 22 8 2.26 1720.98 1715 11 33.2 TL208 0- -911.06. 102 17 1.56 1822.99 1814 17 13.5 AC228 0 969.00 64 20 1.46 1938.89 1934 13 19.7 AC228 u: Co 1
..Po2t-NID Pcck Sacrch Raport- (continu0d) Pcg3 a 2 ,Srmplo ID : Herkncoo #18 AcquiGition dato-: 21-NOV-1997 14:57:06 Energy Area. Bkgnd FWHM Channel Left Pw'% Err-Fit Nuclides -0 1460,55 343 3= 1.57 2922.10 2916-14 5.5 K40 Intorference Report Interfering Interfered Nuclide. Line Nuclide Line PB214 241.92 RA224 241.00-TL208 510.72 ANN-RD 511.00 i 1 4 2
.l-; '/Shmmsr'y'of Nuclide-Activity - Paga.:- 3. .., Sample ID :-Harkness #18 Acquisition date : ~21-NOV-1997 14:57:06 P tal number of lines in spectrum 21 0 ciber-of unidentified.-lines 21- '100.00% '( umber of lines tentatively identified by NID n Ruclide-Type-: natural Uncorrected Decay Corr Decay-Corr 1-Sigma-Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags -K40 1.28E+09Y-1.00 2.046E-05 2.046E 0.113E 5.52 TL208-3.10M 2.56 6.127E-07 1.570E-06 0.143E-06 9.11 A-BI212-60.55M 1.06 1.320E-06 1.399E-06 0.258E-06 10.41 A PB212 --10.64H 1.01 1.845E-06 1.855E-06 0.091E-06 4.89 A BI214 19.90M 1.19 5.045E-07 5.996E-07
~~1. 3 2 0 E-O'i 22.02 A~~
P3214 26.80M 1.14 5.491E-07 6.249E-07 1.194E-07 19.11 A RA224 3.66D 1.00 3.279E-06 3.282E-06 0.973E-06 29.66 AC228-6.13H 1.01-1.526E-06 1.541E-06 0.208E-06 13.51 A I TH234 24.-10D' 1.00 4.805E-06 4.805E 1.161E-06 24.16 KA Total Activity : 3.490E-05 3.613E-05 Grand Total Activity : 3.490E-05 3.613E-05 Flags: "K" - Keyline not found "M" = Manually accepted "E" = Manually edited "A" - Nuclide specific abn. limit i t 1 a 4 4 W 4 .,e -e t-a- r n- 's-- m ,-->-.----r-w .~~.-,.-.n+~- .-w., --.~,v ne
l ie: ~ENudlid3' Lino Error' Propagation Report ~ PCga : 4 ~,Scmpla ID: -Harkness #18 Acquisition date : _21-NOV-1997 14:C7:06-J c ? c =h 1 l imc11de Type r natural Uncorrected Decay Corr 1-Sigma Nuclide. ' Energy %Abn %Eff uCi/g uCi/g-1% Error Status -K40 1460.75 10.70* 7.058E-01 2.046E-05 2.046E-05 5.52-OK ( 0.0%) ( 4.45%) (Decay 0.00%). (Area 5.52%) 1 TL208-277.36 6.50 2.597E+00 6.603E-07 1.692E-06 49.69 OK 1 ( 0.0%) ( 5.18%) ..(Decay 0.00%) -(Area 49.69%) 510.72 22.50 -1.670E+00 6.330E-07 1.622E-06 24.23 OK ' ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 24.23%) 583.14 86.00* 1.505E+00 6.127E-07 1.570E-06 9.11 OK ( 0.0%) ( 4.88%) (Decay-0.00%) (Area 9.11%) -860.47 12.00 1.094E+00 7.505E-07 1.923E-06 33.19-OK ( 0.0%) ( 5.61%) (Decay 0.00%) -(Area 33.19%) BI212-727.17 11.80* 1.258E+00 1.320E-06 1.399E-06 18.41 OK I ( 0.0%) ( 5.30%) -(Decay 0.00%) (Area 18.41%) Absent Line Not Found 785.42 2.00 .1.180E+00 Absent Line Not Found 10'78.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 -6.538E-01 ' Absent-Line Not Found PB212e 74.81 9.60 1.985E+00 77.11= 17.50 2.140E+00 1.488E-06 1.496E-06 26.27 OK ( 0.0%) ( 4.09%) (Decay 0.00%) (Area 26.27%) Absent: Line Not Found 87.20 6.30 2.575E+00 238.63 43.10* 2.845E+00 1.845E-06 1.855E-06 4.89 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 4.89%) Absent Line Not Found -300.09 3.27 2.465E+00 BI214 .609.32-46.09* 1.453E+00 5.045E-07 5.996E-07 22.02 OK F ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 22.02%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Nct Found 934.05 3.16 1.020E+00 Absent Line Not'Found 1120.28 15.04 8.750E-01 Absent
Line Noa Found 1238.11 5.'92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent' Line Not Found 1764.51--
15.92 6.173E-01 ' Absent-Line Not Found PB214' 74.81 6.33 1.985E+00-77.11 10.70 2.140E+00 2.433E-06 2.769E-06 26.27 OK ( 0.0%) ( 4.09%) (Decay 0.00%) (Area 26.27%) Absent Line Not Found -87.20 3.70 2.575E+00 89.80 1.03 2.676E+00 1.157E-05 1.316E-05 25.31 OK ~. ( 0.0%) ( 4 ~. 07 % ) (Decay 0.00%) (Area 25.31%) Line-Not Found

~~<< INT: Reject 241.92~~

_7. 4 7 - 2.823E+00 295.22 19.20 2.490E+00 6.442E-07 7.330E-07 24.30 OK (-3,0%) ( 5.08%) .(Decay 0.00%) (Area 24.30%) 351.99 37.10* 2.207E+00 5.491E-07 6.249E-07 19.11 OK (: 0.0S) ( 4.58%) (Decay 0.00%) (Area 19.11%) Absent-Line Not:Found 785.95-11.09 1.180E+00 Absent Line Not Found RA224 83.78 0.21-2.430E+00 241.00 .3.90*. 2.823E+00 3.279E-06 3.282E 29.66 OK ( 0.0%) ( 5.05%) _ (Decay 0.00%)- (Area 29.66%) AC228 209.40 ~4.55 _ 3.050E+00 2.650E-06 2.676R-06 25.35: OK ( 0.0%) ( 4.93%) (Deca; .00%) (Area 25.35%) 7.. - f
L".he' lido Lino-Error Propagation:Roport -~ (continuad) Paga :- S-N _, Semple-ID : Harkness #18 Acquisition date-21-NOV-1997 14:57: 06
i.ciide-. Type ' natural Uncorrected Decay Corr 1-Sigma-

Nuclide Energy.
%Abn %Eff-uCi/g uCi/g % Error Status- --270.30 3.77 2.640E+00 2.518E-06 2.542E 25.37-OK ( 10. 0 % )_ '(.5.15%) (Decay 0.00%) (Area 25.37%) Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.270E+00 1.490E-06 1.505E-06 17.77-OK. (- 0.0%) ( 4.73%) (Decay'O.00%) (Area 17.77%) Absent-Line Not Found 409.40 2.23 1.977E+00 463.00 4.64 1.803E+00 1.239E-06 1.251E-06 39.25 OK ( 0.0%) (-4.41%) (Decay 0.00%) (Area 39.25%) Abrant Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10' 1.62 1.197E+00 794.80 4.84 1.169E+00 1.972E-06 1.991E-06 31.54 OK I ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 31.54%) Absent Line Not Found 835.60 1.82 1.121E+00 E 911.07 29.00* 1.042Ee00 1.526E-06 1.541E-06 13.51 'OK ( 0.0%) ( 5.64%) (Decay-0.00%) \\A ta 15.51%) Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 9.889E-01 1.663E-06 1.679E-06 19.71-OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 19.71%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line-Not Found 1630.40' '1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.795E+00 5.609E-06 5.609E-06 24.16-OK ( 0.0%) ( 4.11%) (Decay 0.00%) .(Area 24.16%) 92.80 3.00 2.795E+00 4.805E 4.805E-06 24.16 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 24.16%) Absent Line Not Found 112.81 0.25 3.240E+00 = Keyline Flag: t' s
g.* I )41LLSTONE HEALTH PHYSICS-ENVIRONMENTAL 22-NOV-1997 09:46:14 (

~~Sample Information ----~~

~~..mple ID~~
Harkness #19 Sample Quantity

-1.00000E+03 g

37507 Spctrm Collector : HP Environmental Scmple Number Sample Analyst

HP Environmental Sample Deposition Information ----

No Dep. Duration Dap. Correction?
~~Deposition End~~
~~22-NOV-1997 09:35:30 D; position Start~~

~~Sample Decay / Count Information ----~~

~~22-NOV-1997 09:35:30 Acpisition date : 22-NOV-1997 09:35:36 Scmple Date 0 00:00:06.17~~
~~% dead time~~
~~0.0%~~
~~Deccy time Elepaed live time: 0 00:10:00.00 Elapsed real time: 0 00:10:00.30~~

~~Detector Parameters ----~~

19-JUL-1995 08:05:48 Energy cal. oper.: HP Support Energy cal. time Datoctor name

Environmental Counting geometry: 1 Liter Soil Effic. cal. time : 19-JUL-1995 08:56:03 Effic, cal, oper.: HP Support

~~Processing Parameters ----~~

~~Start channel~~
100 End channel

3700

4.50000 Gaussian Sens.

10.00000 Sensitivity Critical level?
~~Yes Propagate Errors?: No~~
~~Yes Libra n-based eff: No Empirical Eff?~~
~~Energ tolerance : 1.00000 Half life ratio~~
8,00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
a-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 2 74.88 102 113 1.14 149.83 145 14 19.6 2.47E+00 PB214 PB212 2 77.29 164 108 1.17 154.66 145 14 13.3 PB214 PB212 1 87.35 57 127 1.09 174.80 171 12 35.6 8.89E-01 PB214 PB212 1 90.00 33 98 1.00 180.09 171 12 51.3 PB214 0 92.78 62 79 1.42 185.65 183 6 26.1 TH234 TH234 I O 128,74 45 85 1.23 257.62 254 7 37.0 0 185.74 64 111 1.59 371.69 365 12 35.3 RA226 0 238.71 402 146 1.14 477.70 473 12 7.7 PB212 0 270.23 40 38 1.41 540.78 537 10 32.8 AC228 0 295.12 84 35 1.07 590.58 585 10 17.1 PB214 0 338.26 108 55 1.36 676.91 670 13 17.1 AC228 0 351.90 109 34 0.79 704.22 699 9 13.6 PB214 0 433.25 16 23 0.84 867.00 862 9 60.7 0 511.00 44 30 0.92 1022.57 1017 12 29.1 TL208 0 583.18 136 29 1.26 1156.99 1161 13 11.9 TL208 0 609.57 82 33 1.65 1219.80 1214 13 19.0 BI214 0 727.66 25 15 1.00 1456.07 1450 10 35.1 BI212 0 $10.90 82 2 1.32 1822.66 1817 10 11.6 AC228 C0? l
w. Pcga i 2 00t-NID Peak Search P.eport (continund) 22-NOV-1997 09:35:36 Acquisition date icmplo-ID : Harkness #19 (t - Enargy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 964.96 16 2 1,49 1930.81 1927 8 29.5 AC228 0 969.08 .75 2 1.69 1939.06 1934 13 12.6 AC228 0 1120.44 13 13 0.85 2241.83 2235 10 56.2 BI214 0 1460.73 368 0 2.09 2922.46 2915 14 5.2 K40 (ntorforence Report Interfered Interfering Nuclide Line Nuclide Line TL208 510.72 ANN-RD 511.00 l e I
t. s Summary of Nuclida Activity Pcge : 3 . sample ID : Harkness #19 Acquisition date : 22-NOV-1997 09: 35:36 si number of lines in spectrum 22 / ...mer of unidentified lines 2 i t Number of lines tentatively identified by NID 20 90.91% -Nuclide Type : natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags K40 1.28E+09Y 1.00 2.195E-05 2.195E-05 0.214E-05 5.21 TL208 3.10M 2.56 4.735E-07 1.214E-06 0.144E-06 11.85 A BI212 60.55M 1.06 7.605E-07 8.058E-07 2.832E-07 35.14 A PB212 10.64H 1.01 1.477E-06 1.485E-06 0.115E-06 7.72 A BI214 19.90M 1.19 5.496E-07 6.532E-07 1.243E-07 19.03 A PB214 26.80M . 14 5.983E-07 6.808E-07 0.926E-07 13.60 A RA226 1600.00Y 1.00 2.732E-06 2.732E-06 0.963E-06 35.25
~~AC228 6.13H 1.01 1.220E-06 1.231E-06 0.143E-06 11.61 A~~
TH234 24.10D 1.00 3.355E-06 3.355E-06 0.875E-06 26.09 KA Total Activity : 3.312E-05 a.411E-05 h Grand Total Activity : 3.312E-05 3.411E-05 Flags: "K" = Keyline not found "M" = Manually accepted "E" = Panually edited "A" = Nuclide specific abn. limit L GJ.
I*Nuclid$ Lino Error Propogction Rcport Pcgo : 4 Semplo ID : Harknoco #19 Acquicition dato : 22-NOV-1997 09:35:36 / h e11de Types natural Uncorrected Decay Corr icSigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status K40 1460.75 10.70* 7.058E-01 2.195E-05 2.195E-05 5.21 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 5.21%) Line Not Found Absent TL208 277.36 6.50 2.596E+00 510.72 22.50 1.670E+00 5.274E-07 1.352E-06 29.11 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 29.11%) 583.14 86.00* 1.505E+00 4.735E-07 1.214E-04 11.85 OK ( 0.0%) ( 4.88%) (Decay 0.Ost) (Area 11.85%) Absent Line Not Found 860.47 12.00 1.093E+00 BI212 727.17 11.80* 1.257E+00 7.605E-07 8.058E-07 35.14 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 35.14%) Absent Line Not Found 785.42 2.00 1.180E+00 Absent Line Not Found I 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 PB212 74.81 9.60 1.989E+00 2.409E-06 2.423E-06 19.56 OK ( 0.0%) ( 4.15 % ) (Decay 0.00%) (Area 19.56%) 77.11 17.50 2.117E+00 1.989E-06 2.000E-06 13.32 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 13.32%) 87.20 6.30 2.581E+00 1.566E-06 1.575E-06 35.58 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 35.58%) 238.63 43.10* 2.844E+00 1.477E-06 1.485E-06 7.72 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 7.72%) Absent Line Not Found 300.09 3.27 2.465E+00 BI214 609.32 46.09* 1.453E+00 5.4967.-07 6.532E-07 1s.03 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 19.03%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1,020E+00 1120.28 15.04 8.749E-01 4.608E-07 5.477E-07 56.21 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 56.21%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PB214 74.81 6.33 1.989E+00 3.654E-06 4.158E-06 19.56 OK ( 0.0%) ( 4.15%) (Decay 0,00%) (Area 19.56%) 77.11 10.70 2.117E+00 3.253E-06 3.702E-06 13.32 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 13.32%) i 87.20 3.70 2.581E+00 2.666E-06 3.034E-06 35.58 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 35.58%) 89.80 1.03 2.682E+00 5.422E-06 6.170E-06 51.29 OK ( U.0%) ( 4.07%) (Decay 0.00%) (Area 51.29%) Absent Line Not Found 241.92 7.47 2.823E+00 295.22 19.20 2.493E+00 7.900E-07 8.990E-07 17.12 OK ( 0.0%) ( 5.09%) (Decay 0.00%) (Area 17.12%) 351.99 37.10* 2.207E+00 5.983E-07 6.808E-07 13.60 OK ( 0.0%) ( 4.58%)- (Decay 0.00%) (Area 13.60%) Absent Line Not Found 785.95 1.09 1.18CE+00 RA226 185.99 3.28* 3.214E+00 2.732E-06 2.732E-06 35.25 OK ( 0.0%) (. 4.85%) (Decay 0.00%) (Area 35.25%) r 't
{+ puclida Lino Error Propagation Rcport-(continued) Pcg3 : 5 .Scmple ID : Harkness #19 Acquicition dato : 22-NOV-1997 09:35:36 (huclide Typer natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uC1/g uCi/g % Error Status Absent Line Not Found AC228 209.40 4.55 3.050E+00 270.30 3.77 2.639E+00 1.810E-06 1.828E-06 32.78 OK ( 0.0%) ( 5.15%) (Decay 0.00%) (Area 32.78%' Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.270E+00 1.788E-06 1.806E-06 17.10 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 17.10%) Absent Line Not Found 409.40 2.23 1.977E+00 Absent Line Not Found 463.00 4.64 1.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 Absent Line Not Found 794.80 4.84 1.169E+00 g Absent Line Not Found 835.60 1.82 1.121E+00 911.07 29.00* 1.042E+00 1.220E-06 1.231E-06 11.61 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 11.61%) 964.60 5.45 9.924E-01 1.323E-06 1.336E-06 29.52 OK ( 0.0%) ( 5.44%) (Decay 0.00%) (Area 29.52%) 968.90 17.46 9.889E-01 1.944E-06 1.963E-06 12.56 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 12.56%) Absent Line Not Found 1587.90 3,71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.779E+00 3.916E-06 3.917E-06 26.09 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 26.09%) 92.80 3.00 2.779E+00 3.355E-06 3.355E-06 26.09 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 26.09%) Absent Line Not Found 112.81 0.25 3.240E+00 = Keyline Fleg: 1 4 ' ~
4 -( + d4ILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 22-NOV-1997 07:46:49 i 4

~~Sample Information ----~~

~~4 Lumple ID~~
Harkness #20 Sample Quantity

1.00000E+03 g

HP Environmental Scmple Number

37496 Spctrm. Collector Sample Analyst

HP Environmental

~~Sample Deposition Information ----~~

~~No Dep. Duration Dap. Correction?~~
~~D:pocition Start : Deposition End~~
~~22-NOV-1997 07:36:03~~

~~Sample Decay / Count Information ----~~

~~Scmple Date~~
~~22-NOV-1997 07:36:03 Acquisition date : 22-NOV-1997 07:36:11 D3 cay time 0 00:00:08.45~~
~~% dead time~~
~~0.0%~~
~~Elepaed live time: 0 00:10:00.00 Elapsed real time: 0 00:10:00.30~~

~~Detector Parameters ----~~

g
19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Energy cal, time Detoctor name

Environmental Counting geometry: 1 Liter Soil Effic. cal, time : 19-JUL-1995 08:56:03 Effic cal, oper.: HP Support

~~Processing Parameters ----~~

~~Start channel~~
100 End cnannel

3700 Sanoitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No

Yes Libran -based ef f : No Empirical Eff?
~~Energy tolerance : 1.00000 Half llfe ratio~~
8.00000 Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
..-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 3 74.93 90 86 0.85 149.94 145 13 18.7 1.73E+00 PB214 PB212 3 77.19 131 86 1.06 154.46 145 13 14.8 PB214 PB212 0 37.23 55 74 1.18 174.55 172 6 28.5 PB214 PB212 0 186.38 31 58 1.11 372.98 370 6 43.1 RA226 0 209.95 56 67 1.12 420.15 416 11 31.6 AC228 5 238.64 393 46 1.09 477.57 470 22 5.8 1.07E+00 PB212 5 241.59 74 55 1,81 483.47 470 22 31.3 PB214 5 295.08 85 22 1.54 590.51 585 21 15.5 1.98E+00 PB214 5 299.79 42 38 -2.06 599.93 585 21 32.5 PB212 0 327.94 42 19 1.19 656.27 651 11 25.4 AC228 0 338.46 79 52 1.37 677.32 669 15 23.0 AC228 0. 352.15 122 53 1.09 704.71 699 12 15.0 PB214 0 409.21 35 13 0.63 818.89 812 13 27.1 AC228 0 510.68 53 7 1.67 1021.93 1015 14 22.3 ANN-RD 0 583.04 123 19 1,49 1166.72 1160 15 11.9 TL208 0 609.59 89 21 1.77 1219.84 1215 14 15.8 BI214 0 661.18 58 12 1.23 1323.07 1317 12 17.8 CS137 0 911.18 72 12 1.53 1823.22 1818 10 15.0 AC228 0 968.94 52 6 1.17 1938.78 1935 8 16.1 AC228 COPY
Rodt-RIDibck'SocrchReport (continued). ~ Pcga 1 _ 2 1 Scmplo_ID; Harkness-#20; Acquisition-dato 22-NOV-1997 07:36:11 Energy. Area -Bkgnd= FWHM Channel Left Pw % Err . Fit Nuclides! ' -- O 980.39 9-5- 0.76 1961.69. 1958 -7 56.2 0-1120;83 21 12-1.87-2242.62 2233 16 42.9' BI214 1 -0 u54.28-17- '2-- 1.21-2309.52 2305-8 28.4-1 0 1460,81 283. 0-2.10 2922.62 2915-14 5.9 K40 Intorference. Report-- -Interfering Interfered I Nuclide Line Nuclide Line PB214 '241.92 'RA224 241.00' TL208-510.72 ANN-RD 511.00 L I e -4 C ,-/ I s ... m
Sum 6ary df Nuclido Activity Pcga : 3 Snmplo ID : Harknose #20 Acquisition dato : 22-NOV-1997 07:36:11
*cl number of lines in spectrum 23
/ ..n er of unidentified lines 2 b \\.. umber of lines tentatively identified by NID 21 91.30% Nuc' Aide Type : natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags K40 1.28E+09Y 1.00 1.688E-05 1.688E-05 0.100E-05 5.94 TL208 3.10M 2.58 4.275E-07 1.105E-06 0.131E-06 11.86 A PB212 10.64H 1.01 1.442E-06 1.450E-06 0.084E-06 5.78 A BI214 19.90M 1.19 5.966E-07 7.101E-07 1.120E-07 15.78 A PB214 26.90M 1.14 6.728E-07 7.664E-07 1.151E-07 15.02 A RA226 1600.00Y 1.00 1.336E-06 1.336E-06 0.576E-06 43.12 AC228 6.13H 1.01 1.068E-06 1.078E-06 0.162E-06 14.99 A I Total Activity : 2.242E 05 2.333E-05
~~fission Nuclide Type Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error~~
% Error Flags CS137 30.10Y 1.00 2.270E-07 2.270E-07 0.403E-07 17.75 Total Activity : 2.270E-07 2.270E-07 Nuclide Type : other Uncorrected Decay Corr Decay Corr 1-Sigma .ide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags nan-RD 109.74M 1.03 7.338E-08 7.579E-08 1.688E-08 22.27 Total Activity : 7.338E-08 7.579E-08 Grand Total Activity : 2.272E-05 2.363E-05 Flags: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit 1 4
.Nucl(daLinaErrorProp0getionRoport Pcgo : 4 Semplo ID : Harknaco #20 Acqui0ition doto : 22-NOV-1997 07:36:11-I( 211de Type natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status K40 1460.75 10.70* 7.057E-01 1.688E-05 1.688E-05 5.94 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 5.94%) Line Not Found Absent TL208 277.36 6.50 2.596E+00 << INT Reject Line Not Found 510.72 22.50 1.671E+00 583.14 86.00* 1.505E+00 4.275E-07 1.105E-06 11.86 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 11.86%) Line Not Found Absent 860.47 12.00 1.093E+00 PB212 74.81 9.60 1.991E+00 2.128E-06 2.140E-06 18.69 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 18.69%) 77.11 17.50 2.112E+00 1.601E-06 1.610E-06 14.82 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 14.82%) 1 87.20 6.30 2.576E+00 1.513E-06 1.521E-06 28.51 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 28.51%) 238.63 43.10* 2.845E+00 1.442E-06 1.450E-06 5.78 OK ( 0.0%) ( 5. 04 f. ) (Decay 0.00%) (Area 5.78%) 300.09 3.27 2.467E+00 2.362E-06 2.375E-06 32.50 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 32.50%) BI214 609.32 46.09* 1.453E+00 5.966E-07 7.101E-07 15.78 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 15.78%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 1120.28 15.04 8.746E-01 7.186E-07 8.552E-07 42.89 OK ( 0.0%) ( 4.61%) (Decay 0.00%) (Area 42.89%) Absent Line Not Found 12;8.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PB214 74.81 6.33 1.991E+00 3.228E-06 3.677E-06 18.69 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 18.69%) 77.11 10.70 2.112E+00 2.618E-06 2.903E-06 14.82 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 14.82%) 87.20 3.70 2.576E+00 2.576E-06 2.934E-06 28.51 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 28,51%) Absent Line Not Found 89.80 1.03 2.675E+00 241.92 7.47 2.825E+00 1.586E-06 1.807E-06 31.34 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 31.34%) 295.22 19.20 2.493E+00 8.044E-07 9.163E-07 15.51 OK ( 0.0%) ( 5.09%) (Decay 0.00%) (Area 15.51%) 351.99 37.10* 2.206E+00 6.728E-07 7.664E-07 15.02 OK ( 0.0%) ( 4.58%)- (Decay 0.00%) (Area 15.02%) Absent Line Not Found 785.95 1.09 1.180E+00 RA226 185.99 3.28* 3.209E+00 1.336E-06 1.336E-06 43.12 OK -( 0.0%) ( 4.85%) ' Decay 0.00%) (Area 43.12%) AC228 209.40 4.55 3.046E+00 1.814E-06 1.831E-06 31.63 OK ( 0.0%) ( 4.93%) s'2 cay 0.00%) (Area 31.63%) Absent Lint Not Found 270.30 3.77 2.639E+00 328.00 3.36 2.320E+00 2.424E-06 2.448E-06 25.41 OK ( 0.0%) ( 4.83%) (Decay 0.00%) (Area 25.41%) c l'
N. L puclida/41no Error Propagation Report (continuad) Paga 5 Stmplo ID : Harknoos #20 Acquicition dato : 22-NOV-1997 07:36:11 f( 411de Type: natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status 338.40 12.01 2.269E+00 1.299E-06 1.312E-06 23.04 OK ( 0.0%) ( 4.73%) (Decay 0.00%)- (Area 23.04%) 409.40 2.23 1.978E+00 3.570E-06 3.605E-06 27.14 OK ( 0.0%) ( 4.16%) (Decay 0.00%) (Area 27.14%) 463.00 4.64 1.802E+00 Line Not Found Absent 478.2'O 0.24 1.758E+00 Line Not Found Absent 772.10 1.62 1.197E+00 Line Not Found Absent 794.80 4.84 1.169E+00 Line Not Found Absent 835.60 1.82 1.121E+00 Line Not Found Absent 911.07 29.00* 1.042E+00 1.068E-06 1.078E-06 14.99 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 14.99%) I 964.60 5.45 9.927E-01 Line Not Found Absent 968.90 17.46 9.890E-01 1.352E-06 1.366E-06 16.14 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 16.14%) Line Not Found 1587.90 -3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Nuclide Type: fission Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status CS137 661.62 84.62* 1.360E+00 2.270E-07 2.270E-07 17.75 OK ( 0.0%) ( 5.10%) (Decay 0.00%) (Area 17.75%) o.J11de Types other ) Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error ' Status ANN-RD 511.00 193.40* 1.671E+00 7.338E-08 7.579E-08 22.27 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 22.27%) Flag: "*" = Keyline .f. ~~
4. t ,'i ' MILLSTONE HEALTH PHYSICS-ENVIRONMENTAL 21-NOV-1997 21:49:42 (

~~Sample Information ----~~

~~bcmple ID~~
Harkness #21 Sample Quantity

1.00000E+03 g Sample Number

37484 Spctrm Collector : HP Environmental Sample Analyst

HP Environmental Sample Deposition Information ----
~~Dap. Correction? : No Dep. Duration Daposition Start : Deposition End~~
~~21-NOV-1997 21:38:58~~

~~Sample Decay / Count Information ----~~

~~Scmple Date~~
~~21-NOV-1997 21:38:58 Ac@isition date : 21-NOV-1997 21:39:07 Daccy time 0 00:00:08.50~~
~~% dead time~~
~~0.1%~~
~~Elcpced live time: 0 00:10:00.00 Elapsed real time: 0 00:10:00.32 1~~

~~Detector Parameters ----~~

19-JUL-1995 08:05:48 Energy cal, oper.: HP Support Enorgy cal. time D0toctor name

Environmental Counting geometry: 1 Liter Soil Effic, cal, time : 19-JUL-1995 08:56:03 Effic, cal. oper.: HP Support

~~Processing Parameters ----~~

~~Stort channel~~
100 End channel

3700 Sanoitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No

Yes Library-based eff: No Empirical Eff?

1.00000 Half life ratio

8.00000 Enargy tolerance Abundance limit

80.00000 WTM error limit

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
.c-NID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 76.21 207 277 3.06 152.49 144 14 18.4 PB214 PB212 O 89.92 46 86 0.73 179.93 ' 178 5 33.7 PB214 0 185.37 C8 103 3.65 370.95 365 12 31.9 RA226 3 238.65 409 50 1.09 477.59 471 17 5.7 1.12E+00 PB212 3 241.45 43 56 1.57 483.20 471 17 52.3 RA224 0 270.88 36 70 0.94 542.08 537 11 49.9 AC228 0 277.16 23 33 0.95 554.65 551 7 47.3 TL208 0 295.62 111 71 1.56 591.58 583 15 19.0 PB214 I O 300.23 28 46 0.77 600.81 597 8 46.0 PB212 0 338.16 103 39 1.15 676.71 672 12 15.3 AC228 0 352.08 105 57 1.09 704.57 699 11 17.1 PB214 0 409.41 29 30 1.47 819,29 813 11 41.3 AC228 0 510.98 38 45 1.56 1022.54 1017 15 39.2 TL208 0 583.21 165 18 1.25 1167.06 1160 11 9.1 TL208 0 609.44 77 36 1.13 1219.55 1213 14 19.8 BI214 0 727.64 34 19 1.93 1456.04 1450 9 28.1 BI212 0. 795.08 31 11 1.07 1590.95 1586 11 27.3 AC228 0 860.29 24 12 1.38 1721.41 1714 11 33.6 TL208 0 911.04 105 14-1.78 1822.94 1815 18 12.8 AC228 0 969.54 38 38 1.70 1939.97 1931 13 37.4 AC228 -Q 1121.02 17 16 1.54 2243.00 2238 10 51.4 BI214 L ~ Co V 4
-. - _ ~. -.. _. -.. -... ~ _ _,.... __-_.. -..... - + -s 'A; " PoDt-NID Pock Saarch Report.(continued)- Pcga -- : 2 '- Acquisition:date-21-NOV-1997 21:39:07. .Scmple ID :-Harkness #21: 7 -[ Energy.. - Area -. Bkgnd I FWHM' Channel Left PW % Err-Fit Nuclides-0- 1460.76 1362 9 1.88-2922.52 - 2913 17 -5.6 -K40 + 0 1764.55 16: 'O 1.49 3530.06-3524 11:-25.0 BI214' l Interference Report l terfering Interfered l n Nuclide-Line . Nuclide- 'Line PB214 241,92 RA224 241.00 TL208 510.72 ANN-RD 511.00 1 Y i _.f n-J + a d a 4 1 f b fN
~~1. -~~
7 t'- ~,.- + J-m,- g .s rw.<- t.wyw W .cy yvt 'r-w vt
j A . Summary of Nuclida Activity pcge : 3 S mple ID : Harkness #21 Acquisition date : 21-NOV-1997 21:39:07 i cl number of lines in spectrum 23. A amber of unidentified lines 0 Number of lines tentatively identified by NID 23 100.00% Nuclide Type natural Uncorrected Decay Corr Decay Corr 1-Sigma 5 Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags K40 3.28E+09Y 1.00 2.157E-05 2.157E-05 0.120E-05 5.58 TL208 3.1'OM 2.59 5.751E-07 1.487E-06 0.136E-06 9.15 A BI212 60.55M 1.06 1.044E-06 1.106E-06 0.311E-06 28.13 A PB212 10.64H 1.01 1.504E-06 1.512E-06 0.087E-06 5.72 A BI214 19.90M 1.19 5.201E-07 6.150E-07 1.229E-07 19.85 A PB214 26.80M 1.14 5.768E-07 6.571E-07 1.123E-07 17.09 A RA224 3.66D 1.00 1.771E-06 1.772E-06 0.926E-06 52.28 i RA226 1600.00Y 1.00 2.923E-06 2.923E-06 0.933E-06 31.90 AC228 6.13H 1.01 1.566E-06 1.582E-06 0.202E-06 12.76 A Total. Activity : 3.205E-05 3.323E-05 Grand Total Activity : 3.205E-05 3.323E-05 Flegs: "K" = Keyline not found "M" = Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit 9 b wx

~~_-.----_-___--______-____.-.___._______-____---_._________J~~

~~h 6~~
~~3 Tyuhlid$LL' ins Error Propagation Report Paga :~~
~~4 'Scmple_IDL: Harkness:#21 Acquisition date : 21-NOV-1997 21:39:07 Nuclide Typen natural-Uncorrected Decay Corr 1-Sigma -Nuclide-Energy _ %Abn %Eff uCi/g uCi/g % Error Status-~~
~~X40~~
-1460.75 10.70* 7.058E-01' 2.157E-05 2.157E-05 5.58 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 5.58%) TL208 '277.36 6.50 2.597E+00 6.004E-07 1.552E-06 47.28 OK ( 0.0%) ( 5.18%) (Decay 0.00%) (Area 47.28%) 510.72 22.50 1.670E+00 4.569E-07 1.181E-06 39.23 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 39.23%) 583.14 86.00* 1.505E+00 5.751E-07 1.487E-06 9.15 OK ( 0.0%). ( 4.88%) (Decay 0.00%) (Area 9.15%) 860.47 12.00 1.093E+00. 8.315E-07: 2.150E-06 33.60 OK ( 0.0%) ( 5.61%) (Decay 0.00%) (Area 33.60%) OB1212 727.17 11.80* 1.257E+00 1.044E-06 1.106E-06 28.13 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 28.13%) Absent Line Not-Found 785.42 2.00 1.180E+00 Absent Line Not Found -1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 Absent Line Not Found PB212 74.81 9.60 1.905E+00 77.11 17.50 2.060E+00 2.587E-06 2.601E-06 18.40 OK l ( 0.0%) ( 4.12%) (Decay 0.00%) (Area 18.40%) Absent Line Not Found 87.20 6.30 2.575E+00 238.63 43.10* 2.845E+00 1.504E-06 1.512E-06 5.72 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.72%) 300.09 3.27 2.464E+00 1.565E-06 1.574E-06 46.01 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 46.01%) 4 609.32 46.09* 1.453E+00 5.201E-07 6.190E-07 19.85 OK (_0.0%) ( 4.96%) (Decay 0.00%) (Area-15. 3%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934,05 3.16 1.020E+00 1120.28 15.04 8.745E 5.838E-07 6.948E-07 51.40 OK ( 0.0%) ( 4.61%) (Decay 0.00%) (Area 51.40%) Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line-Not Found 1509.19 2.19 6,885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 1764.51 15.92 6.173E-01 7.334E-07 8.729E-07 25.00 OK ( 0.0%) _ ( 4.80%) (Decay 0.00%) (Area 25.00%) Absent 1 Line Not Found PB214 74.81 6.33-1.985E+00 77.11 10.70-2.060E+00 4.231E-06 4.819E-06 18.40 OK-I ( 0.0%) ( 4.12%). (Pecay 0.00%) (Area 18.40%) Absent Line Not Found 87.20 13.70 2.575E+00 89.80 1.03 2.679E+00 7.442E-06 8.478E-06 33.74 OK ( 0.0%)- (-4.07%) (Decay 0.00%) (Area 33.74%) << INT Reject Line Not Found. 241.92 7.47 2.823E+00 1.195E-06 19.04 OK 295.22-19.20 2.490E+00 1.049E (Decay - 0. 0 0%). (Area 19.04%)= (10;0%) -( 5.08%) -351.99 37.10* 2.207E+00 5.768E-07 6~.571E-07 17.09 OK (10.0%) ( 4.58%) (Decay 0.00%)_ (Area 17.09%) Absent Line Not Found 785.95. 1.09 1.180E+00 Absent Line Not Found RA2241 83.78 0.' 21 - 2.430E+00 241.00 3.90* 2.826E+00. 1.'771E-06 1.772E-06 52.28 OK ( 0.0%)- -(.5 d5%) (Decay 0.00%) (Area 52.28%)
-4. I (continu0d) Pcga : 5 l 'Ndelidt Lina Error Propngation Report Stmplo ID : Hnrknoss #21 Acquicition date : 21-NOV-1997 21:39:07 4melide Type: natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status RA226 185.99 3.28* 3.216E+00 2.923E-06 2.923E-06 31.90 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 31.90%) Line Not Found AC228 209.40 4.55 3,050E+00 Absent 270.30 3.77 2.635E+00 1.621E-06 1.637E-06 49.87 OK ( 0.0%) ( 5.16%) (Decay 0.00t) (Area 49.07%) Line Not Found Absent 328.00 3.36 2.320E+00 338.40 12.01 2.271E+00 1.704E-06 1.721E-06 15.32 OK ( 0.0%) ( 4.73%) (Decay 0.00%) (Area 15.32%) 409.40 2.23 1.977E+00 2.945E-06 2.974E-06 41.31 OK ( 0.0%) ( 4.17%) (Decay 0.00%) (Are-41.31%) Line Not Found Absent 463.00 4.64 1.802E+00 I Line Not Found Absent 478.20 0.24 1.758E+00 Line Not Found Absent 772.10 1.62 1.197E+00 794.80 4.84 1.168E+00 2.477E-06 2.501E-06 27.34 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 27.34%) Line Not Found Absent 835.60 1.82 1.121S+00 911.07 29.00* 1.042E+00 1.566E-06 1.582E-06 12.76 OK ( 0.0%) ( S.64%) (Decay 0.00%) (Area 12.76%) Line Not Found Absent 964.60 5.45 9.927E-01 968.90 17.46 9.885E-01 9.946E-07 1.004E-06 37.37 OK ( 0.0%) ( 5.42%) (Decay 0.00%) (Area 37.37%) Line Not Found Absent 1587.90 3.71 6.633E-01 Line Not Found Absent 1630.40 1.95 6.510E-01 s: = Keyline 1 ( l 1
i * *,.
s
~~, MILLSTONE HEALTH FHYSICS ENVIRONMENTAL 21-NOV-1997 20:39:40~~

~~Sample Information ----~~

~~g . ample ID~~
Harkness #22 Sample Quantity

1.000i SE+03 g Sem;,e Number 37480 Spctrm Collector : HP EnN ronmental Sample Analyst HP EnvAronmental

~~Sample Deposition Information ----~~

~~Dop. Correction? : No Dep. Duration D3 position Start : Deposition End~~
~~21-NOV-1997 20:28:57 l~~

~~Sample Decay / Count Information ----~~

~~Scmple Date~~
~~21-NOV-1997 20:28:57 Acwisition date : 21-NOV-1997 20:29:05 t'~~
Daccy time 0 00:00:07.61 % dead time-t 0.1% Elepcod live times- 0 00:10:00.00 Elapsed real times 0 00:10:00.31 ---. Detecter Parameters ---- I Enargy cal. time : 19-JUL-1995 08:05:48 Energy cal. oper.: HP Support Letoctor name
~~Environmental Counting geomutry: 1 Liter Soil Effic. cal, time : 19-JUL-1995'08:56:03 Effic. cal, opar.: HP Support-~~

~~Processing Parameters ----~~

~~Start channel~~
100 End channel-3700 Sonsitivity

4.50000 Gaussian Sens.

10.00000 Critical level?

Yet Propagate Errors?: No Empirical Eff' Yes Library-based eff: No En3rgy tolerance i 1.00000 Half life ratio

8.00000 Abundance limit

80.00000 WTM error lin't

3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %
e t .-NTD Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 76.10 239 204 3.14 152.28 146 13 13.0 0 93.23 83 96 1.47 186.57 183 8 23.3 TH234 TH234 0 185.80 32 92 1.62 371.82 368 8 55.5 RA226 0 209.68 37 51 0.92 419.61 416 7 35.9 AC228 3 238.62 388 57 1.03 477.53 473 15 5.8 2.81E+00 PB212 3 241.38 58 45 1.61 483.05 473 15 39.5 PB214 2 295.06 70 28 1.54 590.47 585 22 18.0 2.25E+00 PB214 2 300.19-45 11 1.55 600.73 585 22 23.7 PB212 O 351.93 142 36 1.14 704.28 699 11 11.7 PB214 0 463.03 20 27 0.96 926.59 921 11 54.1-AC228 0-C10.82 35 20 2.94 1022.22 1017 15 38.1 ANN-RD 0-583.21 134 18 1.20 1167.06 1161 12 10.7 TL208-0 609.19 96 13 1.20 1219.04 1213 13 12.9 BI214 ' 727.92 37 14 0.78 1456.59 1451 13 27.7 BI212 0 768.19 17 2 0.99 1537.16 1534 8 28.4 - BI214 ~0 784,78. 31 0 4.88 1570.35 1564 12-18.0 BI212 0 795.35-16 6 1,54 1591.49 1585 12 38.4 AC228 0 860.66-21 -2 1.08 1722.15 1718 8 24.7-TL200 0 911.87 72 43 0.88 1824.59 1815-19 24.8 AC228 0 969.18 46 5 0;97 1939.25 1935 10 17.3 AC228 0 1460,62-374 4 1.04 2922.25 2914 16 3.3 K40 in6irference Report [3 kdI 0^ L ,-L.+ <,-,~L +.-ne + ,-,m,-, v n e,e y,e_.----- -,y--,,n- .n,,- ,e>k- ~,--vn-- ? w n, ~
1 1 I'n' tor drenco X: port (continu;d) Pcg3 : 2 S taplo ID : HOrknoco #22 Acquisition dnto 21-NOV-1997 20:29:05 Interfering Interfered l. Nucijde Line Nuclide Line j PB214 241.92 RA224 241.00 TL208 510.72 ANN-RD 511.00 l l ? I 4 i
Summary of Nuclido Activity Pcgo 3 (,cmplo ID : Harknoos #22 Acquicition dato 21-NOV-1997 20:29:05 I T**.cl number of lines in spectrum 21 ber of unidentified lines 1 ( amber of linen tentatively identified by HID 20 95.24% i Nuclide Type natural Uncorrected Decay Corr Decay Corr 1-Sigma l Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags i K40 1.28E+09Y 1.00 2.230E-05 2.230E-05 0.118E-05 5.31 TL208 3.10M 2.58 4.660E-07 1.201L 06 0.129E-06 10.72 A BI212 60.55M 1.06 1.118E-0G 1.185E 06 0.328E-06 27.67 A PB212-10.64H 1.01 1.427E-06 1.435E-06 0.083E-06 5.81 A DI214 19.90M
~~1. 19 6.433E 07 7.652E-07 0.984E-07 12.86 A~~
PB214 26.80M 1.14 7.808E-07 8.891E-07 1.041E-07 11.71 A RA226 1600.00Y 1.00 1.352E-06 1.352E-06 0.750E-06 55.49 AC328 6.13H 1.01 1.073E-06 1.083E-06 0.269E-06 24.81 A I TH234 24.10D 1.00 4.436E-06 4.437E-06 1.035E-06 23.33 KA Total Activity : 3.360E-05 3.465E-05 Nuclide Type : other Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uC1/g 1-Sigma Error % Error Flags ANN-RD 109.74M 1.03 4.937E-08 5.098E-08 1.941E-08 38.07 Total Activity : 4.937E-08 5.098E-08 rand Total Activity : 3.365E-05 3.470E-05 Flags: "K" - Keyline not found "M" = Manually accepted i "E" = Manually edited "A" = Nuclide specific abn. limit I -1 ,e t i 4 Y --V+ +w ey-- ,,e\\.
~. Nuclida Lino Error Prepngotion R0 port Pega 4 semple ID : Harknoos #22 Acquioition dcto : 21-NOV-1997 20:29:05 alide Type natural Uncorrected Decay corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uC1/g % Error Status K40 1460.75 10.70* 7.058E-01 2.230E-05 2.230E-05 5.31 OK ( 0.0%) I 4.45%) (Decay 0.00%) (Area 5.31%) Line Not Found Absent TL208 277.36 6.50 2.596E+00 << INT Reject Line Not Found 510.72 22.50 1.671E+00 583.14 86.00* 1.505E+00 4.660E-07 1.201E-06 10.72 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 10.72%) 860.47 12.00 1.093E+00 7.227F 07 1.862E-06 24.69 OK ( 0.0%) ( 5.61%) (Decay 0.00%) (Area 24.69%) BI212 727.17 11 804 1.257E+00 1.118E-06 1.185E-06 27.67 OK i 0.0%) ( 5.30%) (Decay 0.00%) (Area 27.67%) 785.42 2.00 1.181E+00 5.912E-06 6.266E-06 17.96 OK I ( 0.0%) ( 5.45%) (Decay 0.00%) (Area 17.96%) Absent Line Not Found 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 Line Not Found Absent PB212 74.81 9.60 1.985E+00 Absent Line Not Found 77.11 17.50 2.108E+00 Absent Line Not Found 87.20 6.30 2.575E+00 238.63 43.10* 2.845E+00 1.427E-06 1.435E-06 5.81 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.81%) 300.09 3.27 2.464E+00 2.543E-06 2.557E-05 23.74 OK / 0.0%) ( 5.05%) (Decay 0.00%) (Area 23.74%) DI214 609.32 96.09* 1.453E+00 6.433E-07 7.652E-07 12.86 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 12.86%) 768.36 4.89 1.202E+00 1.266E-06 1.506E-06 28.43 OK ( 0.0%) ( 5.41%) (Decay 0.00%) (Area 28.43%) Line Not h and Absent 934.05 3.16 1.020E+00 Absent Line Not Found 1120,2< 15.04 8.750E-01 Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 Absent Line Not Found PB214 74.81 6.33 1.985E+00 Absent Line Not Found 77.11 10.70 2.108E+00 Absent Line Not Found 87.20 3.70 2.575E+00 Absent Line Not Fout-1 89.80 1.03 2.675E+00 241.92 7.47 2.826E+00 1.235E-06 1.407E-06 39.47 OK j ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 39.47%) 295.22 19.20 2.493E+00 6.632E-07 7.551E-07 17.99 OK ( 0.0%) ( 5.09%) (Decay 0.00%) (Area 17.99%) 351.99 37.10* 2.207E+00 7.808E-07 8.891E-07 11.71 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 11.71%) Absent Line Not Found 785.95 1.09 1.180E+00 RA226 185.99 3.28* 3.213E+00 1.352E-06 1.352E-06 55.49 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 55.49%) AC228 209.40 4.55 3.04BE+00 1.201E-06 1.212E-06 35.95 OK ( 0.0%) ( 4.93%) (Decay 0.00%) (Area 35.95%) Absent Line Not Found 270.30 3.77 2.639E+00 Absent Line Not Found 328.00 3.36 2.320E+00 r h o l
)
Nuclido Lino Error Propogstion Raport (continuod) Pcgo : 5 l 1 Sample ID : Harknoco #22 Acquiaition dcto : 21-NOV-1997 20:29:05 L i ( 11de Type natural Uncorrected Decay Corr 1-$1gma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status Line Not Found Absent 338.40 12.01 2.269E+00 Line Not Found Absent 409.40 2.23 1.977E+00 463.00 4.64 1.802E+00 1.103E-06 1.113E-06 54.10 OK 4 ( 0.0%) ( 4.42%) (Decay 0.00%) (Area 54.10%) Line Not Found Absent 478.20 0.24 1.758E+00 Line Not Found Absent 772.10 1.62 1.197E+00 794.80 4.84 1.168E+00 1.311E-06 1.324E-06 38.44 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 38.44%) Absent Line Not Found 835.60 1.62 1.121E+00 911.07 29.00* 1.041E+00 1.073E-06 1.083E-06 24.81 OK ( 0.0%) ( 5.63%) (Decay 0.00%) (Area 24.81%') Absent Line Not Found 964.60 5.45 9.927E-01 968.90 17.46 9.888E-01 1.200E-06 1.212E-06 17.32 OK ( 0.0%) ( 5.43%) (Decay 0.00%) (Area 17.32%) Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1530.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.794E+00 5.179E-06 5.179E-06 23.33 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 23.33%) 92.80 3.00 2.794E+00 4.436E-06 4.437E-06 23.33 OK ( 0.0%) ( 4.11%) (Decay 0.00%) (Area 23.33%) Absent Line Not Found 112.81 0.25 3.240E+00 ide Types other Uncorrected Decay corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status ANN-RD 511.00 193.40* 1.671E+00 4.937E-08 5.098E-08 38.07 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 38.07%) = Keyline Flag: t i f'
i, 43 % i NILLSTONEHEALTH-PHYSICS-ENVIRONMENTAL-21-NOV 1997 18:36:13 l Sample Information ---- c-.aple ID
Harkness #23 Sample Quantity

1.00000E+03 g Semple Number

37475 Spctrm Collector : EP Environmental e
~~Sample Analyst~~
~~HP Environmental~~

~~Sample Depooition Information ----~~

~~D3p. Correction? : No Dep. Duration Deposition End 21-NOV-1997 18:25:30 Deposition Start :~~

~~Sample Decay / Count Information ----~~

~~- Dscay time- . : '21-NOV-1997 18:25:30 Acquisition date : 21-NOV-1997 18:25:38 Samplo Date t 0 00:00:08.16 % dead time~~
~~0.1%~~
~~Elepood live times 0 00:10:00.00 Elapsed real times 0.00:10:00.34~~

~~Detector Parameters ----~~

~~)Enorgy cal. time : 19-JUL-1995 08:05:48 Energy cal. oper.: HP Support D3tector name~~
~~Environmental Counting geometry: 1 Liter Soil Effic. cal. time : 19-JUL-1995 08:56:03 Effic, cal, oper.: HP Support~~

~~Process ag Parameters ----~~

~~Start channel~~
100 End channel

3700 L
~~Soncitivity~~
4,50000 Gaussian Sens.

10.00000 Critical level?

Yes Propagate Errors?: No

Yes Libran-cased eff: No Empirical Eff?
~~Energy tolerance : 1.00000 Half life ratio~~
~~8.00000 Abundance limit i 80.00000 WTM error limit i 3.00000 MDA Width (FWHM) : 5.00000 MDA Confid Level : 3.00000 %~~
-HID Peak Search Report It Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 2 74.98 106 113 0.04 150.03 146 13 18.1 1.38E+00 PB214 PB212 2-77.16-190 111 1.15 154.40, 146 13 12.1 PB214 PB212 0 87.01 51 116 0.91 174.12 171 7 38.0 PB214 PB212 0 -93.09 46 173 1.02 186.29 182. 9 54.1 TH234 TH234 0 185.86 45 131 1.42 371.94 367 10 50.3 RA226 L0 208.97 27 85 0.84 418.19 415 7 60.0 AC228 4 238.61 436 41 1.03 477.51 470 24 5.3 1.58E+00 PB212 4 241.42 75' 58 1.72 483.13 470 24 30.6 PB214 0 270.55 33 68 0.84 541.42 537 9 48.8 AC228 0 '295.35 95 26 1.08 591.05 587 10 14.2 PB214 0-299.98 38 29 1.14 600.'2 597 7 28.1 PB212 4 0 338.69 72-59 1.46 677.78 671 13 24.9 AC228 0 '351.88 114 51 0.94 704.17 698 12'15.6. PB214 0
~~511.14'~~
~~.60 -35 1.36 1022.86-1015 16 25.7 TL208 0 583.08 159 28 1.21--1166.81 1160 14 10.0 TL208- - 10 609.60 82 ' 41 - 0.96 1219.86 1214 12.19.2 BI214 OL~~
~~727.~93' 50:~~
20- 1.-43 1456.60. lo is-16'24.3 BI212 0' 795.21~ 20 13 1.56-1591.22 _1586 9 40.2 AC228 Co " r,- w
en % Port-NID Pock Socrch Roport (continued) Pogo 2 drmplo ID : Harkness #23 Acquicition dcto : 21-NOV-1997 18:25:38 ~ l Energy Area Bkgnd FWHM Channel Left Pw % Err Fit Nuclides 0 860.28 20 10 2.14 1721.40 1716 10 37.3 TL208 0 911.01 124 11 2.04 1822.88 1816 14 10.5 AC228 0 1460.59 415 0 1.97 2922.18 2915 15 4.9 K40 Intorference Report Interfering Interfered Nuclide Line Nuclide Line PB214 241.92 RA224 241.00 TL208 510.72 ANN-RD 511.00 l 1-(- 4 l_
a t d. 'Summ32;y of Nuclido Activity Pago 3 IScmplo ID : Harp.noso #23 Acquisition dcto 21-NOV-1997 18:25:38 Tntal number of lines in spectrum 21 bar of unidentified lines 0 '..cmbar of lines tentatively identified by NID 21 100.00% Nuclide Type : natural Uncorrected Decay Corr Decay Corr 1-Sigma Nuclide Hlife Decay uCi/g uCi/g 1-Sigma Error % Error Flags K40 1.20E+09Y 1.00 2.475E-05 2.475E-05 0.122E-05 4.91 TL208 3.10M 2.58 5.518E-07 1.425E-06 0.152E-06 10.64 A BI212 60.55M 1.06 1.529E-06 1.620E-06 0.394E-06 24.33 A PB212 10.64H 1.01 1.601E-06 1.610E-06 0.085E-06 5.28 A BI214 19.90M 1.19 5.528E-07 6.579E-07 1.263E-07 19.20 A PB214 26.80M 1.14 6.268E-07 7.1402-07 1.117E-07 15.65 A RA226 1600.00Y 1.00 1.915E 06 1.915E-06 0.963E-Od 50.27 6.13H 1.01 1.855E-06 1.873E-06 0.197E-06 10.53 A ) AC228 TH234 24.10D 1.00 2.465E-06 2.465E-06 1.334E-06 54.11 KA Total-Activity : 3.585E-05 3.703E-05 -Grand Total Activity : 3.585E-05 3.703E-05 Flago: "K" = Keyline not found "M" - Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit a 4 I e a
c. Nuclido Lino Error Propagation Report Pego 4 'Scmple ID : Harknoso #23 Acquisition date : 21-NOV-1997 18:25:38 (w.. elide Types natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g % Error Status K40 1460.75 10.70* 7.058E-01 2.475E-05 2.475E-05 4.91 OK ( 0.0%) ( 4.45%) (Decay 0.00%) (Area 4.91%) Absent Line Not Found TL208 277,36 6.50 2.596E+00 510.72 22.50 1.670E+00 7 #19E-07 1.864E-06 25.67 OK ( 0.0%) ( 4.62%) (Decay 0.00%) (Area 25.67%) 583.14 86.00* 1.505E+00 5.518E-07 1.425E-06 10.64 OK ( 0.0%) ( 4.88%) (Decay 0.00%) (Area 10.64%) 860.47 12.00 1.093E+00 6.820E-07 1.761E-06 37.33 OK ( 0.0%) ( 5.61%) (Decay 0.00%) (Area 37.33%) BI212 727.17 11.80* 1.257E+00 1.529E-06 1.620E-06 24.33 OK ( 0.0%) ( 5.30%) (Decay 0.00%) (Area 24.33%) Absent Line Not Found 3 785.42 2.00 1.180E+00 Absent Line Not Found 1078.62 0.97 9.033E-01 Absent Line Not Found 1620.56 2.75 6.538E-01 PB212 74.81 9.60 1.994E+00 2.503E-06 2.517E-06 18.14 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 18.14%) 77.11 17.50 2.110E+00 2.318E-06 2.331E-06 12.12 OK ( 0.0%) ( 4.10%) (Decay 0.00%J (Area 12.12%) 87.20 6.30 2.567E+00 1.407E-06 1.414E-06 37.99 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 37.99%) 238.63 43.10* 2.845E+00 1.601E-06 1.610E-06 5.28 OK ( 0.0%) ( 5.04%) (Decay 0.00%) (Area 5.28%) 300.09 3.27 2.465E+00 2.140E-06 2.152E-06 28,12 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 28.12%) .4 609.32 46.09* 1.453E+00 5.528E-07 6.579E-07 19.20 OK ( 0.0%) ( 4.96%) (Decay 0.00%) (Area 19.20%) Absent Line Not Found 768.36 4.89 1.202E+00 Absent Line Not Found 934.05 3.16 1.020E+00 Absent Line Not Found 1129.28 15.04 8.750E-01 Absent Line Not Found 1238.11 5.92 8.052E-01 Absent Line Not Found 1377.65 4.02 7.387E-01 Absent Line Not Found 1509.19 2.19 6.885E-01 Absent Line Not Found 1729.60 3.05 6.254E-01 Absent Line Not Found 1764.51 15.92 6.173E-01 PB214 74.81 6.33 1.994E+00 3.796E-06 4.323E-06 18.14 OK ( 0.0%) ( 4.15%) (Decay 0.00%) (Area 18.14%) 77.11 10.70 2.110E+00 3.791E-06 4.317E-06 12.12 OK I ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 12.12%) 87.20 3.70 5.567E+00 2.395E 2.728E-06 37.99 OK ( 0.0%) ( 4.05%) (Decay 0.00%) (Area 37.99%) Absent Line Not Found 89.00 1.03 2.675E+00 241.92 7.47 2.826E+00 1.601E-06 1.823E-06 30.55 OK ( 0.0%) ( 5.05%) (Decay 0.00%) (Area 30.55%) 295.22 19.20 2.491E+00 8.954E-07 1.020E-06 14.25 OK ( 0.0%) ( 5.08%) (Decay 0.00%) (Area'14.25%) 351.99 37.10* _2.200E+00 6.268E-07 7.140E-07 15.65 OK ( 0.0%) ( 4.58%) (Decay 0.00%) (Area 15.65%) Absent Line Not Found 785.95 1.09 1.180E+00 RA226 .185.99 3.28* 3.213E+00 1.915E-06 1.915E-06 50.27 OK ( 0.0%) ( 4.85%) (Decay 0.00%) (Area 50.27%) i J
,,o.. Nuclida Lino Error Propcgntion R port (continund) Pogo : 5 $2mplo ID : Harknaso #23 Acquicition dato : 21-NOV-1997 18:25:38 ...Lide Types natural Uncorrected Decay Corr 1-Sigma Nuclide Energy %Abn %Eff uCi/g uCi/g %Errcr Status AC228 209,40 4.55 3.053E+00 8.692E-07 8.777E-07 60.00 OK ( 0.0%) ( 4.93%) (Decay 0.00%) (Area 60.00%) 270.30 3.77 2.637E+00 1.472E-06 1.487E-06 48.83 OK ( 0.0%) ( 5.16%) (Decay 0.00%) (Area 48,83%) Absent Line Not Found 328.00 3.36 2.320E+00 338.40 12.01 2.268E+00 1.190E-06 1.202E-06 24.89 OK ( 0.0%) ( 4.72%) (Decay 0.00%) (Area 24.89%) Absent Line Not Found 409.40 2.23 1.977E+00 Absent Line Not Found 463.00 4.64 1.802E+00 Absent Line Not Found 478.20 0.24 1.758E+00 Absent Line Not Found 772.10 1.62 1.197E+00 ( 794.80 4.84 1.168E+00 1.579E-06 1.574E-06 40.17 OK ( 0.0%) ( 5.48%) (Decay 0.00%) (Area 40.17%-) Absent Line Not Found 835.60 1,82 1.121E+00 911.07 29.00* 1.042E+00 1.855E-06 1.873E-06 10.53 OK ( 0.0%) ( 5.64%) (Decay 0.00%) (Area 10.53%) Absent Line Not Found 964.60 F.45 9.927E-01 Absent Line Not Found 968.90 17.46 9.890E-01 Absent Line Not Found 1587.90 3.71 6.633E-01 Absent Line Not Found 1630.40 1.95 6.510E-01 Absent Line Not Found TH234 63.29 3.90* 1.299E+00 92.38 2.57 2.790E+00 2.877E-06 2.877E-06 54.11 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 54.11%) 92.80 3.00 2.790E+00 2.465E-06 2.465E-06 54.11 OK ( 0.0%) ( 4.10%) (Decay 0.00%) (Area 54.11%) Absent Line Not Found 112,81 0.25 3.240E+00 Keyline Flag: "*" = l l l [ =}}

ML20199G809

Contents

Text

SUBJECT:

Background

Background

Navigation menu