ML20129E098

Guide for Preparation of Application for Use of Radioactive Matls in Well-Logging Operations

ML20129E098
Person / Time
Issue date:	01/31/1984
From:	NRC OFFICE OF NUCLEAR MATERIAL SAFETY & SAFEGUARDS (NMSS)
To:
Shared Package
ML20129E079	List: ML20129E098
References
FOIA-84-729 PROC-840131, NUDOCS 8507160732
Download: ML20129E098 (37)

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ce, t ~ GUIDE FOR THE DREPARATION OF APPLICATIONS FOR THE USE OF RADI0 ACTIVE MATERIALS IN WELL-LOGGING OPERATIONS JANUARY 1984 Nuclear Regulatory Commission Division of Fuel Cycle and Material Safety Material Certification and Procedures Branch Washington, DC 20555 sa e 9 I t i {. d\\ 8507160732 850405 PDR FOIA CARMAN 84-729 PDR t m

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TABLE OF CONTENTS _Page No. A. INTRODUCTION I l. Purpose of Guide 1 2. Applicable Regulations 1 3. ALARA (As Low As Reasonably Achievable) 1 B.. LICENSE FEES 2 C. FILING AN APPLICATION 2 D.' CONTENTS OF APPLICATION 3 Item 2 - Applicant's Name and Address 3 Item 3 - State and Address (for possession and use) 3 Item 4 - Person To Be Contacted About Application 4 Item 5 - Radioactive Material 4 Item 6 - Purpose for Which Licensed Material Will Be Used 5 Item 7 - Individual (s) Responsible for Safety Program-Training and Experience 5 (1) Radiation Protection Officer - 5 (2) Other user-Supervisory Personnel 6 Item 8 - Training of Individuals Working in or Frequenting Restricted Areas 8 Item 9 - Facilities and Equipment 8 A. Radiation Detection Instruments and Calibration 8 B. Personnel Monitoring 10 C. Physical Facilities and Equipment 11 1. Plant-Field Station Facilities 11 2. Storage Facilities 12 3. Transport Containers 12 4 Remote Handling Tools 12 5. Tracer Facilities and Equipment 12 6. Tracer Storage Facilities 13 7. General Safety Equipment-Tracers 13 Item 10 - Radiation Safety Program 13 10.1 PR0HIBITION. 14 10.2 EQUIPMENT CONTROL 14 10.2.1 Limits on Levels of Radiation 14 10.2.2 Storage Precautions 14 10.2.3 Transport Precautions 15 10.2.4 Radiation Survey Instruments 15 L

C ,8 c. Page No. 10.2.5 Leak Testing af Seaked Sources 15 10.2.6 Periodic Inventory of Sources of Radiation 17 10.2.7 Utilization Records 17 10.2.8 Labeling Requirements 17 10.2.9 Inspection and Maintenance 18 10.3 REQUIREMENTS FOR PERSONNEL SAFETY 19 10.3.1 Training Requirements 19 10.3.2 Operating and Emergency Procedures 20 10.3.3 Personnel Monitoring 21 10.4 PRECAUTIONARY PROCEDURES IN LOGGING ANC SUBSURFACE TRACER OPERATIONS 22 10.4.1 Security 22 10.4.2 Handling Tools 22 10.4.3 Subsurface Tracer Studies 23 10.4.4 Particle Accelerators 23 10.5 RADIATION SURVEYS AND RECORDS 23 10.5.1 Radiation Surveys 23 10.5.2 Documents and Records at Field Stations 24 10.5.3 Documents and Records at Temporary Job Sites 2J 10.6 NOTIFICATION 25 10.6.1 Notification of Incidents, Abandonment and Lost Sources 25 Item 11 - Waste Management 29 Item 12 - Certificate 30 E. AMENDMENTS TO LICENSE 30 F. RENEWAL OF LICENSE 31 ATTACHMENTS: Appendix A In-House Calibration of Survey Instruments 34 _y

s GUIDE FOR THE PREPARATION OF APPLICATIONS FOR THE USE OF RADI0 ACTIVE MATERIALS IN WELL-L'0GGING OPERATIONS A. INTRODUCTION 1. Purpose of the Guide This guide describes the type of information that the NRC staff needs to evauate an application for the use of radioactive materials in oil, gas, and mineral well-logging operations. Thewell-ldlbingoperationscoveredbythis guide are: (1) the use of the electronic well-logging tools containing sealed sources in wellbores, and (2) the use of radioactive materials to conduct tracer studies in a wellbore or adjacent formation. 2. Applicable Regulations In addition to 10 CFR Part 30, other regulations pertaining to this type of license are found in 10 CFR Part 19, " Notice, Instructions, and Reports to Worke nspections"; 10 CFR Part 20, " Standards for Protection Against Rad ,10 CFR Part 71, " Packaging of Radioactive Material for Transport and Transportation of Radioactive Materials Under Certain Conditions"; and 10 CFR Part 170, " Fees for Facilities and Material Licenses and Other Regu-latory Services Under the Atomic Energy Act of 1954, As Amended." 3. As Low As Is Reasonably Achievable (ALARA) Paragraph 20.1(c) of 10 CFR Part 20 states, in part, "...rersons engaged in activities under licenses issued by the Nuclear Regulatory Commission pursuant to the Atomic Energy Act of 1954, as amended, and the Energy Reorganization Act of 1974 should, in addition to complying with the requirements set forth in this part, make every reasonable effort to maintain radiation exposures, an releases of radioactive materials in effluents to unrestricted areas, as low as is reasonably achieveable." Regulatory Guide 8.10, " Operating Philosophy 1

e-for Maintaining Occupational Radiation Exposures As Low As Reasonably Achievable," provides the NRC staff position of this important subject. License applicants should give consideraton to the ALARA philosphy, as described in Regulatory Guide 8.10, in the development of plans for work with licensed radioactive materials. B. LICENSE FEES A license fee is required for most types of licenses and amendments to i licenses. The applicant should refer to Section 170.31, " Schedule of Fees for Materials Licenses and Other Regulatory Services," of 10 CFR Part 170, to determine the amount of fee that must accompany the application. Review of the application will not begin until the proper fee is received by the NRC. Checks should be made payable to the U.S. Nuclear Regulatory Commission. C. FILING AN APPLICATION An application for a new license to possess and use byroduct material in well-logging operations should be filed on Form NRC-313, " Application for Material License." Since the space provided on the application form is limited, you should append additional sheets to provide complete information. Rapid evaluation and handling of the application can be facilitated by submitting the information on ccnsecutively numbering pages, 8-1/2 x 11 inches, identifying all drawings or diagrams submitted. Three copies of the application should be completed. The original and one copy should be mailed to the NRC regional office in which your home office or corporate headquarters is located. The mailing addresses of the NRC regional offices are listed in the 313 Form. Since the license will require, as a condition, that you follow the statements and representations set forth in the application and any supplements *to it, one copy of the application with all attachments should be retained for your use. The information submitted should pertain to the specific activities for which authorization is requested and should be as complete as possible. Submissions 2

• r of incomplete information will result in delays because of the' correspondence necessary to obtain supplemental information. The submitted information must be sufficient to allow the Commission to determine that the proposed equip-ment, facilities, trained personnel, procedure ~s, and controls'are adequate to protect health and minimize danger to life and property.

The following discussion in Item D, CONTENTS OF APPLICATION, applies to specific terms on Form NRC-313. Each specific item in the guide must be addressed in your application, and when a specific item is not applicable to your proposed program, it must be so stated and your reasons for non-applicability fully explained. D. CONTENTS OF APPLICATION Except for Item 1, which is self explanatory, the following guidance applies to the separate items of Form NRC-313 as indicated: Item 2 Applicant's Name The applicant corporation or other legal entity should be specified by name in Item 2 along with the complete mailing address. Individuals should be desig-nated as applicant in Item 2 only if they are acting in a private capacity and the use of byproduct material is not connected with their employment with a corporation or other legal entity. Item 3 State and Addresses Where Licensed Material Will Be Possessed or Used The actual location (s) where the radioactive materials will be possessed, stored and/or used should be specified in Item 3. Permanent facilities such as field stations or storage areas where licensed material will be stored or used, from wich equipment is dispatched to temporary job sites, should be identified by location (street address, route or highway no., etc.) city and state. An example of a rural location might be "15 miles East, Highway 30, Townville, Montana." Field locations of wells should be specified as "and at temporary job sites." 3

r. 2.- Item 4.Name and telephone number of Person to be Contacted about the Application The individual named in Item 4 is normalJy the' person whom management designates to be responsible for the day-to-day operation of the proposed program and is authorized to speak for management regarding any questions that may arise concerning the application or the proposed program. Item 5 Radioactive material ([a] element and mass number, [b] chemical and/or physical form and [c] maximum amount which will be possessed at any one time). Under this item, the applicant needs to identify the radioactive materials to be possessed and used under the license. The following are examples of the kinds of listings of licensed material. Element & Mass No. Chemical and Physical Form

• Maximum activity / source

[a] [b] [c] (Manufacturer and Model No. of Sources) A. Americium-241:Be A. Sealed sources (XYZ Inc A. Not to exceed Model ABC-34) 3 curies per source. B. Cesium-137 B. Sealed sources (Mesa B. Not to exceed Blanch, Inc. Model 1. 3 curies per source. C. Iodine-131 C. Sodium Iodide C. 30 millicuries total 4 (10 millicuries per study). D. Tridium-192 D. Baked on glass beads D. 60 millicuries total (15 millicuries per study).

• Note:

The manufacturer and Model number of the sealed sources needs to be listed under subitem [b]. Under subitem [c] it is not necessary to state the number of sources you intend to possess. You need only list the maximum activitity per source as in the example. For the tracer materials, list the total quantity to be possessed in [c] and in addition specify the maximum amount of material that will be used for each study as in the above examples. e 4

r. Item 6 Purpose for which Ticensed material will be used Under this item you will need to state the purpose for which each licensed material listed in Item 5 will be used.. In pa'rticular, you should specify the type of wells in which the material 1 will be used (for example, gas, oil, mineral). The following is an example of the listings for the radionuclides listed in Item 5 above. A. For use in oil and gas well logging. ~ B. For use in oil and gas well logging. C. For use in cement top and cement ch'nnel locations in oil and gas wells. a D. For use as perforation markers in oil and gas wells. Item 7 Individual (s) responsible for safety program - training and experience (S 30.33(a)(3), 10 CFR 30) Under this item you should list: (1) The name of the individual responsible for your day-to-day radiation protection program and for assuring compliance with NRC Regulations and the terms and conditions of the license (e.g., your Radiation Protection Officer). The individual designated as Radiation Protection Officer (RPO) is normally an individual user, supervisor or other individual who will maintain the license and have overall responsibility for the radiation protection program. You should detail the named individual's duties and responsibilities uner this item, along with the named individual's training and experience. The RPO is expected to coordinate the safe use of the licensed materials and to ensure compliance with the requirements of Title 10, Code of Federal Regulations, Parts 19, 20, 30, and 71. The minimum duties of the RPO are considered to include the following: (a) To ensure that licensed materials that are possessed or used by the applicant are limited to those materials specified in the license. 5

e (b) To ensure that the licensed materials are used only by those individuals authorized by the license. (c) To ensure that all users wear personnel monitoring equipment, such as film badges or thermoluminescence dosimeters (TLD). (d) To ensure that licensed material is properly secured againt unauthorized removal at all times. (e) To supervise leak testing of sealed sources and instrument' calibrations. (f) To develop operating and emergency procedures and to assist in personnel training and orientation on these procedures. (g) To is a point of contact and give assistance in case of emergency, for s ple, well-logging tool damage, theft of licensed materials, fire, etc., and to ensure that proper authorities, for example, NRC, local police, and State personnel, are notified promptly in case of accidents or other incidents that may involve the release of licensed material. (h) To ensure that the terms and conditions of the license, such as periodic leak tests, are met; and that the required records, such as personnel exposure records, leak test records, etc., are periodically reviewed for compliance with NRC regulations and the license conditions as listed on the license. (i) To conduct radiation safety inspections of licensed activity periodically to ensure compliance with the regulations and license conditions. (2) The names of other personnel who will use or directly supervise the use of the licensed material in the performance of well-logging operations under the license (for example, logging supervisors). The training and experience resume of each individual listed in accordance with the above should be submitted and should include formal academic training 6

- e I and on-the-job training. The following are considered the subjects that should be included in formal training courses along with the minimum duration of formal training courses and on-the-job training. SUBJECTS TO BE INCLUDED IN TRAINING COURSES FOR LOGGING SUPERVISORS I. Fundamentals of Radiation Safety. A. Characteristics of radiation. B. Units of radiation dose and quantity of radioactivity. 4 C. Hazards of exposure to radiation. D. Levels of radiation from licensed material. E. Methods of centrolling radiation dose. 1. Working time. 2. Working distances. 3. Shielding. II. Radiation Detection Instrumentation To Be Used. A. Use of radiation survey instruments. 1. Operation. 2. Calibration. 3. Limitations. B. Survey techniques. C. Use of personnel monitoring equipment. III. Equipment to be Used. A. Handling equipment and remote handling tools. B. Licensed materials. C. Storage control, and disposal of equipment and licensed materials. 1 0. Operation and control of equipment and licensed materials. E. Maintenance of equipment. IV. The Requirements of Pertinent Federal and State Regulations. I 7 1 .. - -,.., -,. _ -. _,,.-., -, _., _,-- -.~...,. -,- --- . -. ~ ~ - -.

e e. V. The Licensee's Written Operating and Emergency Procedures,. VI. The Licensee's Recordkeeping Procedures. VII. Case Histories and Potential Consequences of Accidents in Well-Logging Operations. MINIMUM REQUIREMENTS Formal training should encompass all of the above subjects and should be, as a minimum, approximately 24 hours duration. The trainee should show evidence of Eb satisfactory completion of this training by a written or oral test. Formal on-the-job training should be, as a minimum, approximately three months duration working under the direct supervision of an approved user who has been specifically named on an NRC or Agreement State license. Following the on-the-job training period, the trainor should be able to attest to the fact that the trainee has demonstrated a clear and concise understanding of the duties and responsibilities of the job. Item 8 Training of individuals working in or frequenting restricted areas. (Pursuant to requirements of S 19.12, 10 CFR 19.) For this item, you will need to specify that all employees (including ancillary employees) who frequently any restricted area (e.g., your storage and use areas, field use areas and temporary job sites) will be given periodic instruc-tion in basic radiation safety principles and be instructed in your own radia-tion safety program. Item 9 Facilities and equipment. (S 30.33, (a), (2), 10 CFR 30) A. Radiation Detection Instruments and Instrument Calibration (for perform-ance of surveys required pursuant to S 20.201, 10 CFR 20). Section 20.201 of 10 CFR 20 requires each licensee to make surveys as necessary to evaluate the extent of radiation hazards that may be present during 8

e ~. e, I possession and use of licensed material. Therefore, you need to provide information on the instrumentation to be used for performing surveys. Well-logging licensees are required,to maintain calibrated and operable radiation survey instruments at each field station to make radiation surveys at the field station and at each temporary job site as required by the regulations. The radiation survey instruments must be capable of measuring beta gamma exposure from 0-20 milliroentgens per hour. List the radiation survey instruments available for use in performing the required surveys. List by (a) type of instrument, (b) number available, (c) radiation's detected and (d) sensitivity range. An example of such a li' ting is as follows: s RADIATION DETECTION INSTRUMENTS NUMBER RADIATION SENSITIVITY TYPE AVAILABLE DETECTED RANGE Portable Thin Window 2

beta, 0-500 mr/hr GM survey meter gamma You will need to specify how the listed instruments will be periodically calibrated. Well-logging licensees are required to have their survey instruments calibrated:

(1) At intervals not to exceed six (6) months and after each instrument servicing. (2) At energies and radiat, ion levels appropriate for use. (3) So that accuracy within 20 percent of the true radiation level can be demonstrated on each scale. 9

' f.' Calibration records for each survey meter shall be maintained for a period of two (2) years from the date of calibration of inspection by the Commission. Usually, calibration services are obtained from either the instrument manufacturer or a licensed service company. If you plan to use this method, you will need to only specify this. If, however, you intend to establish your own in-house survey meter calibration program, you should so state and provide the additional information as outlined in the attached Appendix A. B. Personnel Monitoring (pursuant to S 20.202, 10 CFR 20) Section 20.202, 10 CFR 20, specifies the requirement for personnel monitoring. Film badges or thermoluminescence dosimeters (TLD) are normally required for personnel engaged in well-logging operations. These devices are available from commercial suppliers. Monthly exchange and evaluation for film badge devices is an acceptable practice. Quarterly exchange is acceptable for TLD. Note that it is no longer necessary to specify the name of the commercial service company providing your personnel monitoring devices. However, it is important to note that if americium-beryllium or other neutron sources are used in your program, your service company must provide neutron dosimetry service to your personnel. Records of personnel monitoring shall be maintained in accordance with Section l 20.401, 10 CFR 20. An acceptable example for the completion of this Item l is in the following: l l i i 10 1

..-. -~_ - i e PERSONNEL MONITORING DEVICES 4 TYPE SUPPLIER EXCHANGE FREQUENCY (Check and/or complete as (Service Company) appropriate.) A B C O(1) FILM BADGE Service will be obtained from a (maximum) commercial service company. Neu- 0 MONTHLY for film or O(2) THERM 01.UMINESCENCE tron monitoring will be provided badges DOSIMETER (TLD) if Americium-241:Be neutron a QUARTERLY for O(3) OTHER (Specify): sources are authorized o OTHER (Specify): t Well-logging licensees must not permit an individual to.use licensed material (i.e., to act as a logging supervisor or logging assistant) unless the indivi-dual wears, at all times during operation, either a film badge or a thermolumi- ) nescence dosimeter (TLD) that is capable of r.easuring radiation exposure from the licensed material in use. Each film badge or TLD dosimeter must be assigned to and worn by only one individual. i C. Physical Facilities and Equipment (Pursuant to S 30.33[a][2] 10 CFR 30) Well-logging licensees are required to maintain sufficient facilities and equipment adequate to protect health and minimize danger to life or property. Therefore, you should provide the information on your facilities as indicated below. INFORMATION ON FACILITIES AND EQUIPMENT TO BE INCLUDED 1. Sketch (es) and/or description (s) of your field station (s) and facilities r where radioactive materials are stored or used, and from which equipment is dispatched to temporary job sites. Sketches should include, where e 5 11 i ..---,._-,__.~m ..,_,,___,_.._,-,,_.y_-,,_.~_,,,..__,_--_.,.m7-_,,_-,__._m.._

e e applicable: building (s), boundary lines, security fences, designated areas, locked storage areas and distances to accessible areas not under the applicants control. Sketches should be to rough scale and all dimensions indicated. 2. Sketch (es) and/or descriptions of your locked storage containers or underground storage pits maintained at your facility. Methods of preventing unauthorized removal and/or use of licensed material should be indicated on the' sketch or otherwise specified. 3. Sketch (es) and/or descriptions of transport containers to be used for transporting both gamma and neutron logging sources to and from temporary job sites. You should specify the maximum activity that will be transported in each type transport container that you include in this submission. Furthermore, descriptions and/or sketches should clearly indicate how the transport contains are to be locked and physically secured to the transport-ing vehicle to prevent accidental loss, tampering, or unauthorized removal of the licensed material from the vehicle. 4. Sketch (es) and/or descriptions of the remote tools you will use to transfer source to and from storage containers and well-logging tools and for handling tracer shipments. CAUTION - SOURCES MUST NOT BE HANDLED WITH BARE HANDS. NOTE: The following additional information is to be supplied by the applicant only if the applicant requests the use of radioactive tracer materials (unsealed radionuclides such as iodine-131, iridium 192, etc.) in the well-logging operations. 5. Facilities and equipment for tracer injection sample preparation. If tracer samples are not to be purchased in ready to use form, laboratory or field office facilities that are to be maintained as restricted areas for sample preparation sould be described. Sketches are helpful.

Hoods, sinks, trays with absorbent materials, remote handling tools, rubber gloves, etc., that will be available at these lahoratory sites should also be described.

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e' 6. Storage provisions. The description of storage facilities should include drawings or sketches of the rooms, building, pits, etc., showing shielding materials (concrete, steel, lead, earth, etc.) and means for securing materials from unauthorized removals Stohage facilities should be designed and materials positioned so that radiation levels do not normally exceed 2 mR per hour at 18 inches from the exterior surface of the storage facility. 7. General safety equipment. A description of protective clothing (such as rubber gloves, coveralls, respirators, and face shield), auxiliary shielding, absorbent materials, injection equipment, secondary containers, plastic bags for storing contaminated clothing, tissue, handling tools, etc., that will be available at well sites should be submitted. Item 10 - Radiation Safety Program The following are considered radiation safety requirements that need to be addressed.by you in making application for a license to engage in well-logging (wireline) service operations and subsurface tracer studies. ' Each specific subitem of Item 10 discusses requirements to which you must agree to abide by in your operations, or explain precisely why you do not ' agree by offering a reasonable alternative. If, for example, you feel that a particular item does not apply to your proposed operation, you should say so and offer a full explanation and/or your alternative (s). You will need to provide the information for Item 10 on additional 81/2 by 11 inch paper, properly keyed to this item and its respective subitems. It is requested that you address each subitem of Item 10 in the or. der presented in this section of the cuide in order to facilitate the application review process. e B \\ 13

4 Item 10.'. PROHIBITION You must agree not to perform wireline service operations with a sealed source (s) in any well or wellbore unless, prior to commencement of the operation, you have a written agreement with the well operator, well owner, drilling contractor, or land owner that: (a) In the event a sealed source is lodged downhole, a reasonable effort at recovery will be made. (b) In the event a decision is'made to abandon the sealed source downhole, therequirementsofItem10.6.1ofthisapplicatiokbshall be met. Item 10.2 EQUIPMENT CONTROL Item 10.2.1 - Limits on Levels of Radiation You must agree that sources of radiation shall be used, stored and transported in such a manner that the transportation requirements of 10 CFR 71, and the dose limitation of Sections 20.101-20.106 of 10 CFR 20, as applicable, are met. Item 10.2.2 - Storage Precautions You must agree that: (a) Each source of radiation, except accelerators, shall be provided with a storage and/or transport container. The container shall be provided with a lock (or tamper seal for calibration sources) to prevent unauthorized renioval of or exposure to the sources of radiation. (b) Sources of radiation shall be stored in a manner which will minimize danger from explosion and/or fire. 14

Item 10.2.3 - Transport Precautions You must agree that transport containers shall be physically secured to the transport vehicles to prevent accidental loss,' tampering, or unauthorized removal. Item 10.2.4 - Radiation Survey Instruments (a) You must agree to maintain sufficient calibrated and operable ra'diation survey instruments at each field station to make physical radiation surveys as required by Section 20.201, 10 CFR 20, and the commitment made in Section 10,5.1 of this application. Instrumentation shall be capable of measuring 0.1 milliroentgen per hour thourgh at least 20 milliroentgens per hour. (b) You must agree that each radiation survey instrument shall be calibrated: 1. At intervals not to exceed six months and after each instrument servicing. 2. At energies and radiation levels appropriate for use. 3. So that accuracy within plus or minus 20 percent of the true radiation level can be demonstrated on each scale. (c) You should further agree that calibration records shall be maintained for a period of two years for inspection by the NRC. Item 10.2.5 - Leak Testing of Sealed Sources You must agree that each sealed. source of radioactive material shall be tested for leakage in accordance with the items listed below. Records of leak tests results will be kept in units of microcuries and maintained for six (6) months after the next required leak test is performed or until transfer or disposal of the sealed source. 15

e. (a) Method of Testing Tests for leakage shall be performed only by personnel specifically authorized to perform such tests by the U.S. Nuclear Regulatory Commission or an Agreement State. The test sample shall be take,n from the surface of the source, source holder, or from the surface of the device in which the source is stored or mounted, and on which one might expect contamination to accumulate. The test sample shall be analyzed for radioactive contami-nation, and the analysis shall be capable of detecting the presence of 0.005 microcurie of radioactive material on the test sample. (Note that if you prooose to use an approved leak test kit to perform leak tests, you will need to state this and provide the name of the manufacturer of the leak test kit and the manufacturer's model number of the kit.) (b) Interval of Testing Each sealed source of radioactive material shall be tested at intervals not to exceed six months. In the absence of a certificate from a transferor indicating that a test has been made prior to the transfer, the~ sealed source shall not be put into use until tested. If, for any reason, it is suspected that a sealed source may be leaking, it shall be removed from service immediately and tested for leakage as soon as practical. (c) Leaking or Contaminated Sources If the test reveals the presence of 0.005 microcurie or more of leakage of contamination, then you shall agree to immediately withdraw the source from use and shall cause it to be decontaminated, repaired, or disposed of in accordance with Section 20.301, 10 CFR 20. A report describing the equipment involved, the test results, and the corrective action taken shall be filed with the appropriate NRC Region in which the license is issued. 16

4 Item 10.2.6 - Periodic Inventory of Sources of Radiation You must agree to conduct a periodic physical inventory (at intervals not to exceed six [6] months) to account for all sourices of radiation possessed under the license. Records of inventories shall be maintained for two (2) years from the date of inventory for inspection by the NRC and shall include the quantities and kinds of sources of radiation, the location where sources are assigned, the date.of the inventory, and the name of the individual conducting the inventory. Item 10.2.7 - Utilization Records You must agree to maintain current records, which shall be kept available for inspection by the agency for two years from the date of the recorded event, showing the following information for each source of radiation: (a) Make, model number, and a serial number or a description of each source of radiation used. (b) The identity of the well-logging supervisor or field unit to whom assigned. (c) Locations where used and dates of use. (d) In the case of tracer materials and radioactive markers, the utilization record shall indicate the radionuclide and activity used in a particular well. Note that a copy of or facsimile of your utilizaticn log should be submitted also under this section. Item 10.2.8 - Labeling [ pursuant to 10 CFR 20.203(f)] You must agree to abide by the following labeling requirements: 17

s' s (a) Each source, source holder, or logging tool containing radioactive material shall bear a durable, legible, and clearly visible marking or' label, which has, as a minimum, the standard radiation caution symbol, without the conventional color requirement,,and the following wording: DANGER (OR CAUTION) RADI0 ACTIVE This labeling shall be on the smallest component transported as a separa'te piece of equipment. (b) Each transport container shall have permanently attached to it a durable, legible, and clearly visible label which has, as a minimum, the standard radiation caution symbol and the following wording: DANGER (OR CAUTION) RADI0 ACTIVE NOTIFY CIVIL AUTHORITIES (OR NAME OF YOUR COMPANY) Item 10.2.9 - Inspection and Maintenance (a) You must agree to conduct, at intervals not to exceed six months, a program of inspection and maintenance of source holders, logging tools, source handling tools, storage containers, transport containers, and injection tools to assure proper labeling and physical condition. Records of inspection and maintenance shall be maintained for a period of two years for inspection by the NRC. (b) You must lurther agree that if any inspection conducted pursuant to the above reveals damage to labeling or components critical to radiation safety, the device shall be removed from service until repairs have been made and that... (c). 18

e. (c) The repair, opening, or modification of any sealed source, or the non-routine servicing

• and maintenance of equipment such as the removal of source capsules from source holders, repair and replacement of seals on source holder / pressure housings, etc.

shall be performed only by persons specifically authorized to do so by the U.S. Nuclear Regulatory Commis-sion or an Agreement State. Item 10.3 REQUIREMENTS FOR PERSONNEL SAFETY Item 10.3.1 - Training Requirements (a) You must agree not to permit an individual to use byproduct material until such individual has: 1. Received, in a course recognized by the U.S. Nuclear Regulatory Commission or an Agreement State, instruction in the subjects out-lined in Item 7 cf this guide and demonstrated an understanding thereof. 2. Read and received instruction in the commitments contained in your application and the applicable regulations contained in 10 CFR 19, 20, 30, and 71, and conditions of the NRC issued license, and your operating and emergency procedures, and demonstrated an understanding thereof. 3. Demonstrated competence to use sources of radiation, related handling tools, and radiation survey instruments which will be used on the job.

• Note:

If wish to request authorization to perform such non-routine services as indicated in 10.2.9(c) above, you will need to describe the specific services you wish to perform and provide' step-by-step procedures for the performance of these non-routine services, including a description of any special tools that will be used to minimize personnel exposure. Sources and source holder / pressure housings should never be handled with the bare hands. You are reminded that where specific approval for non-routine servicing of source holders or pressure housings containing the source have not been requested and subsequently granted under the license, you will be required to return the. items to the device manufacturer or other persons specifically licensed to perform such non-routine services. 19

s t; (b).You must agree that no individual shall be permitted to assist in the handling of sources of radiation until such individual has: 1. Read or received instruction in our ' operating and emergency procedures -~ and demonstrated an understanding thereof. 2. Demonstrated competence to use, under the personal supervision of the logging surpervisor, the sources of radiation, related handling tools and radiation survey instruments which will be used on the job. l (c) You must further agree that you shall maintain employee training records for inspection by the NRC for two years following termination of employment. Item 10.3.2 - Operating and Emergency Procedures I You must agree that each individual who will use or supervise the use of licensed material will be provided with a set of operating and emergency I procedures. These procedures shall include instruction in at least the ( l following: (a) Handling and use of sources of radiation to be employed so that no individual is likely to be exposed to radiation doses in excess of the limits established in the appropriate Sections of 20.101-20.106, 10 CFR 20. j (b) Methods and occasions for conducting radiation surveys. (See also 10.5.1.) (c) Methods and occasions of locking and securing sources of radiation. (d) Personnel monitoring and the use of personnel monitoring equipment. ,(e) Transportation to temporary jobsites and field stations, including the packaging and placing of sources of radiation in vehicles, placarding of vehicles, and securing sources of radiation during transportation. I 20 l

s' s (f) Minimizing exposure of individuals in the event of an accident. (g) Procedures for notifying proper personnel in the event of an accident. (h) Maintenance of records. (i) Inspection and maintenance of source holders, logging tools, source handling tools, storage containers, transport containers, and injection tools. (j) Procedure to be followed in the event a sealed source is lodged downhole. db (k) Procedures to be used for picking up, receiving, and opening packages containing radioactive material pursuant to Section 20.205, 10 CFR 20. (1) The procedures to be used for site and equipment surveys and decontamination following tracer studies. It is not necessary that you submit copies of your operating and emergency procedures. You need only state that will provide a set of procedures as required by 10.3.2 and restate the elements which will be included in them as specified above. Item 10.3.3 - Personnel Monitoring (as required by S 20.202) (a) Film badges / Thermoluminescence dosimeters. You must agree not to permit an individual to use licensed material or to assist in the handling of sources of radiation unless each individual wears, all times during operation, either a film badge or a thumoluminescence dosimeter (TLD) that is capable of measuring radiation exposure from the leiensed material. This implies that where both gamma and neutron well-logging sources are used, the film badges or TLD dosimeters must be capable of measuring both gamma and neutron radiation exposure. Each film badge or TLD dosimeter shall be assigned to and worn by only one 21

,mpsm o. s s individual. Film badge or TLD processing is required at.no longer than monthly intervals for film badges and quarterly intervals for TLD dosimeters. (b) Bioassay services required for use of tracer materials (pursuant to the requirements of S 20.108, 10 CFR 20) Where your proposed program requires the use of large amounts of radio-active material in uncontained form, for example, well tracers, you will need to address under this section of your application what provisions will be made for the performance of bioassays on your user personnel. A typical example is that if you will require the use of iodine-131 in your proposed program and the maximum activity to be handled by any one of you rpersonnel will exceed 50 millicur'ies per week, you will need to address under this section of the application what provisions you will make to perform appropriate bioassays on these individuals as specified in Regulatory Guide 8.20. A copy of Regulatory Guide 8.20 may be obtained from any of the NRC regional offices listed in Appendix D of 10 CFR 20. (c) You must agree that your personnel monitoring records will be maintained for inspection until the NRC authorizes disposition (pursuant to the requirement of S 20.401(c)(1), 10 CFR 20). Item 10.4 PRECAUTIONARY PROCEDURES IN LOGGING AND SUBSURFACE TRACER OPERATIONS Item 10.4.1 - Security You must agree tht during each logging or tracer application, the logging supervisor or other designated employee shall maintain d'irect surveillance of the operating to protect against unauthorized and/or unnecessary entry into a i restricted area, as defined in Section 20.3(a)(14), 10 CFR 20. Item 10.4.2 - Handling Tools You must agree to provide and require the use of tools that will assure remote handling of sealed sources other than the low activity calibration sources. ~ 22

-_+,t s' s Item 10.4.3 - Subsurface Tracer Studies ~ 1 (a) You must agree to require the use of protective gloves and other protective clothing and equipment by all personnel h'andling radioactive tracer material. Precautions shall be taken to avoid ingestion or inhalation of radioactive material. (b) You must agree to not cause the injection of radioactive material into potable water aquifers without prior written authorization from the NRC. o Item 10.4.4 - Particle Accelerators (Note: This item may be disregarded as not applicable if tritium as targets and/or accelerator tubes containing tritium are not required under Item 5, Radioactive Material, of your application.) If particle accelerators containing tritium targets are required in your program, you must agr'ee to not permit above ground testing of particle accelerators, designed for use in well-logging, which results in the production of radiation, except in areas or facilities controlled or shielded

o that the requirements of Section 20.101 and 20.105,10 CFR 20, are met.

Item 10.5 RADIATION SURVEYS AND RECORDS Item 10.5.1 - Radiation Surveys (required pursuant to Sections 20.201 and 20.401, 10 CFR 20) You must agree to perform radiation surveys and maintain records as indicated below: (a) Padiation surveys and/or calculations shall be made and recorded for each area where radioactive materials are stored. (b) Radiation surveys and/or calculations shall be made and recorded for the radiation levels in occupied positions and on the exterior of each vehicle used to transport radioactive material. Such suryeys and/or calculations shall include each source of radiation or combination of sources to be transported in the vehicle. 23 ,-,,_,m_-m_.. .,__y ,,.-.-m-- -n- - - - - + - -

e (c) After removal of the sealed source from the logging tool and before departing the jobsite, the logging tool detector shall be energized, or a survey meter used, to assure that the' logging tool is free of contamination. (d) Radiation surveys shall be made and recorded at the jobsite or wellhead for each tracer operaticn, except those using hydrogen-3, carbon-14, and sul fur-35. These surveys shall include measurements of radiation levels before and after the operation. (e) Records required pursuant to (a) through (d) above shall include the dates, the identification of individual (s) making the survey, the identi-fication of survey instrument (s) used, and an exact description of the location of the survey. Records of these surveys shall be maintained for inspection by the agency for two years after completion of the survey. Item 10.5.2 - Documents and Records at Field Stations Listed in Item 3 You must agree to maintain, for inspection by the NRC, the following documents and records for the specific devices and sources used at your field station listed in Item 3 of your application: (a) Copy of the NRC license. (b) Operating and emergency procedures. (c) Applicable regulations. (d) Records of the latest survey instrument calibrations you specified in Item 9.A. (e) Records of the latest leak test resu'lts you specified in Item 10.2.5. (f) Inventories required in accordance with Item 10.2.6. (g) Utilization records requird in accordance with Item 10.2.7. 24

o (h) Records of inspection and maintenance required in accordance with Item 10.2.9. (1) Survey records required in accordance with Item 10.5.1 of your application. Item 10.5.3 - Documents and Records at Temporary Job Sites You must agree that, when conducting operations at a temporary jobsite, you shall have the following documents and records available at that site for inspection by the NCR: (a) Operating and emergency procedures. (b) Survey records required in accordance with Item 10.5.1 of your application for the period of operation at the site. (c) Evidence of current calibration for the radiation survey instruments in use at the site. (d) When operating in an Agreement State under reciprocity, a copy of your NRC license. Item 10.6 NOTIFICATION Item 10.6.1 - Notification of Incidents, Abandonment, and Lost Sources You must agree to abide by the notification procedures and precautions outlined in (a) through (e) below: (a) Notification of incidents and sources lost in other than downhole logging operations shall be made in accordance with appropriate provisions of Sections 20.403 and 20.405, 10 CFR 20. 25

E e (b) Whenever a sealed source or device containing radioactive material. is 1 i lodged downhole you shall: 1. Provide the drill rig operator and the fishing service company with a complete description of the tool and the location of the source in i the tool. 2. Advise the drill rig operator and fishing service company against using any fishing techniques which may damage the source in the tool. 3. Continuously monitor the wellhead and any w~ll circulating fluids e (drilling mud, etc.) during all fishing operations to check for any surface contamination rasulting from downhole source damage. This monitoring should be accomplished utilizing a sensitive beta gamma survey meter. The sensitive gamma scintillation detector that is contained in a well-logging tool may also be used and may be prefer-able for this surface contamination monitoring. Any instrument readings above background should be considered evidence of source damage. 4. .n the event of any evidence of downhole source damage, immediately notify the drill rig operator and fishing service company to cease all operations, restrict the flow of drilling fluids through the ' downhole fluid circulatory system, and make attempts to separately isolate and contain the fluids coming from the wellhead. The well-logger should also notify the Radiation Protection Officer who should then immediately notify the nearest NRC, Regional Office listed in Appendix D, 10 CFR 20, of the situation. (c) When it becomes apparent that efforts to recover the radioactive source will not be successful, you shall: 1. Advise the well-operator of requirements for abandonment and an appropriate metod of abandonment, which shall include: 26 1

e (i) The immobilization and sealing in place of the radioactive source with a cement plug. (ii) The setting of a whipstoq.k or other deflection device. (iii) The mounting of a permanent identification plaque, at the surface of the well, containing the appropriate information required by (d) below. 2. Notify the appropriate Region listed in Appendix D,10 CFR 20, by telephone, giving the circumstances of the loss, and request approval of the proposed abandonment procedures. Ib 3. File a written report with the Region within 30 days of tLe abandon-ment, setting forth the following information: (i) Date of occurrence and a brief description of attempt to recover the source. (ii) A description of the radioactive source involved, including radionuclide, quantity, and chemical and physical form. (iii) Surface location and identification of well. (iv) Results of efforts to immobolize and set the source in place. (v) Depth of the radioactive source. (vi) Depth of the top of the cement plug. ~ (vii) Depth of the well.. (viii) Information contained on the permanent identification plaque. 27

(d) Whenever a sealed source containing radioactive material-is abandoned downhole, you shall provide a permanent plaque for posting the well or wellbore. This plaque shall: 1. Be constructed of long-lasting material, such as stainless steel or monel. 2. Contain the following information engraved on its face: (i) The word " CAUTION." (ii) The radiation symbol without the conventional color requirement. (iii) The date of abandonment. (iv) The name of the well operator or.well owner. (v) The well name and well identification number (s) or other designtion. (vi) The sealed source (s) by radionuclide and quantity of activity. (vii) The source depth and the depth to the top of the plug. (viii) An appropriate warning, depending of the specific circumstances of each abandonment. (Note that appropriate warnings may include: (a] "Do not drill below plug back depth;" (b] "Do not enlarge casing;" or (c) "Do not re-enter,the hole," followed by the words, "before contacting the Nuclear Regulatory Commission.") (e) You shall immediately notify the agency by telephone and subsequently by confirming letter if you know of, or have reason to believe that, radio-active material has been lost in, or to an underground potable water source. Such notice shall designate the well location and shall describe the magni-tude and extent of loss of radioactive material,, assess the consequences 28

~ r i of such loss, and explain efforts planned or being taken to mitigate these consequences. Item 11 - Waste Management The applicant is required to dispose' of licensed material pursuant to Section 20.301, 10 CFR 20. (a) Sealed Sources Sealed sources containing licensed material should be transferred only to a licensee authorized to possess the specific quantity and form being transferred. (b) Tracer Materials and Wastes Wastes from tracer operations such as unused materials (material not injected into wells), contaminated tissues, gloves, tools, clothing, con-4 tainers, etc., shall be disposed of in accordance with the requirements of Sections 20.301-20.306 of 10 CFR 20. Short half-life materials (e.g., iodine-131) may be stored to allow decay to background levels prior to disposal by ordinary means. The licensee is required to provide security during storage so that radiation levels outside the restricted storage area do not exceed the levels specified in Section 20.105, 10 CFR 20. Prior to disposal of material in ordinary trash, the licensee must monitor each waste package in a low background area (away from other radioactive 1 materials), deface all radioactive label markings on each package and make a record of such disposals showing that the specific package did not register above background levels on an appropriate beta gamma survey meter. A commonly used method of disposal is transfer to a commercial firm licensed to accept radi.1 active wastes. Lists of these firms are available from the Commis-sion on request. In dealing with these firms, prior contact is recommended to determine the specific services that will be provided. 29 -,,_._.,.___---.,,__m-._.. -,__,7-, m_..

o 4, d'. s The applicant may complete Item 11 by agreeing to dispose of all radioactive waste in the following manner and so stating under this section of'the application. Waste Management (a) Sealed sources will be disposed of by return to the manufacturer or by transfer to a commercial. waste disposal service specifically licensed by -the NRC or an Agreement State. l (b) Tracer material wastes will be disposed of by transfer to a commercial waste disposal service specifically licensed by the NRC or an Agreement State. Short half-life waste may be held for decay to background levels, as measured by a beta gamma GM survey meter, prior to disposal as regular trash. (c) Records of waste disposal will be maintained pursuant to Section 20.401(c)(3), 10 CFR 20. Shipment manifests will be prepared and maintained in accordance -with 5 20.311, 10 CFR 20. Item 12 - Certificate You should have an official representative, e.g President, Department or Division Head, or other person you have authorized to sign official documents, sign and date your appifcation, to certify that your application contains information that is true and correct to the best of your knowledge and belief. 'We will return applications that you have not signed, for proper signature. I E. AMENDMENTS TO LICENSES Licensees are required to conduct their programs in accordance with statements, representations, and procedures contained in the license application and supportive documents. The ifcense must therefore be amended if you plan to make any changes or modifications in facilities, equipment, procedures, personnel, or licensed material to be used. 30 l

o .r s. Applications for license amendments may be filed either on the~ application form or in letter form. Your application for amendmeat should identify the license by number, and should clearly describe the exact nature of the changes, modifications, additions, or deletions.. References to previously submitted information and do:uments should be clear and specific and should identify the pertinent information by date, page, and paragraph. The appropriate fee for license amendment, as listed in 10 CFR Part 170, must accompany your application. F. RENEWAL OF A LICENSE Byproduct material licensees are normally issued for a period not to exceed five years. An application for renewal may be submitted in its entirety without reference to previously submitted information. As an alternative, you may do the following: 1. Review your current license to determine that the information concerning your sealed sources, tracer materials, places of use, etc., accurately represents your current and anticipated program. Identify any additions, deletions, or other changes. For additions or other changes, you must* prepare information appropriate for the required additions or changes. 2. Review the documents you have submitted in the past to determine that the information in them is up-to-date and accurately represents your management control program, facilities, equipment, personnel, radiation safety proce-dures, location (s) of use, and any other information pertinent to your program. The documents which you consider to be those which represent your current program, should be identified by date. Any out-of-date and superseded documents should also be identified. (Those documents which f 31

e a,t you have submitted in the past which are part of your license are refer-enced in your current license.) Changes should be made in the documents, as necessary, to reflect your current program. 3. Review NRC regulations to assure that any changes in the regulations are appropriately covered in your program description. 4. Af ter you have completed your review, you should submit a letter, in dupli-cate, with proper fee, which requests renewal of your license and which l provides the information specified in Items 1, 2, and 3, as necessary. 5. Include the name and telephone number of the person who may be contacted concerning your renewal application, and include your correct mailing address if it is not indicated correctly on your license. If your application for license renewal is filed at least thirty (30) days before the expiration date of your license and the application is accom-panied by the appropriate fee for license renewal, your license will auto-matica11y remain in effect until final action is taken on your application. However, if your application is filed less than thirty (30) days before the expiration date and it cannot be processed before that date, you could be without a valid license when the license expires. It is important that the appropriate fee for license renewal accompany' your application for license renewal. In accordance with Section 170.12 of 10 CFR Part 170, no application will be accepted for filing or will be processed before the proper fee is paid. If you do not wish to renew your license, you must dispose of all licensed radioactive material in your possession in a manner authorized in 10 CFR i Part 20; complete Form NRC-314 " Certificate of Dispostion of Materials," l and return it before the expiration date of your Ifcense with a request that your license be terminated. If you cannot dispose of all Itcensed radioactive material in your possession before the expiration date, you l j 32 i l l l [

,,.~o

1. ,.4,; '[

must request a 1,icense renewal for storage only for the radioactive mate-rial to avoid violations of possessing licensable material without a valid license. ATTACHMENTS: (1) Appendix A In-House Calibration of Survey Instruments e0 e 5 4 4 4 33

,:.-: :y I d'(\\/ . : ;2 a:

• E l #

APPENDIX A i',r/ SURVEY INSTRUMENT CALIBRATIONS If.you have indicated in Item 9. A. that survey instruments will be calibrated in-house then the following outlines the additional information that must be i ..provided on your proposed galibration program: Additional Information For Item lib 1. Calibration source (s) to be used: (Provide the following information on each source to be possessed and used for calibration purposes.) o Radionuclide: J Manufacturer's name: Model No: Activity (for example, millicuries): , and Output (for, example, R/hr at 1 meter): Accuracy

• of the source (s):

2. Frequency of calibration: months 3. Specific procedure to be used (include radiation safety procedure to be followed during handling and use of source [s]). 4. An example of your calibration record form. 5. Calibrations will be performed by: 6. Pertinent training and experience of person (s) named ab' ve. o " Note that the accuracy is the maximum deviation of the nominal value of the source from the true value. This information is usually provided by the manufacturer of the source (s) along with a statement on the traceability to a national standard. e 34 o

..-, e Wq - D ) rn ' .n 6 NRC Form 3131 U.S. NUCLEAR REGULATORY COMMISSION

1. APPLICATION FOR:

(1241 (Check and/or complete as appropriate) 10 CFR 30 APPLICATION FOR BYPRODUCT MATERIAL LICENSE n INDUSTRIAL

8. NEW LICENSE See attached onstructions for detallL

b. AMENDMENT TO:

LICEN5E NUMBER Completed applications are filed in duplica'te with the Division of fuel Cycle and Material Safety. Offace of Nuclear Material Safety, and Safeguards, U.S. Nuclear Regulatory Commission, Washington, DC 20555 or applications may be filed in person at the Commission's office at

• ],'

gu,g 1717 H Street NW, Washington, D. C. or 1915 Eastern Avenue, Silver Spring. Maryland.

2. APPLICANT'S NAME (Instituteon, firm, person, etc./

3. NAME AND TITLE OF PERSON TO BE CONTACTED REGARDING THIS APPLICATION UNITED WIRELINE SERVICE,INC.

CARL W HUBBARTT, PRES.& MANAGER EL PHON N SE : ARE A CODE - NUMBER EXTENSION T P O MBER: ARE A CODE - NUMBER EXTENSION

4. APPLICANT'S MAILING ADDRESS (incluoelsa Codel

5. STREET ADDRESS WHERE LICENSED MATERIAL WILL SE USED (Address to which NRC correspondence, notices, bulletins, etc.,

(Include Zip Code) should be sent.) P.O. Box W (oVL 1925 Maple Ave. Fairfield, Illinois 62837 Mattoon, Illinois 61938 (lF MORE SPACE IS NEEDED FOR ANY ITEM. USE ADDITIONAL PROPERLY KEYED PAGESJ

6. INDIVIDUAL (S) WHO WILL USE OR DIRECTLY SUPERVISE THE USE OF LICENSED MATERIAL (see items 16 and 11 for required training and esperoence of each indirnfuelnamed bebow)

FULL N AME TITLE Carl W Hubbattt President & General Manager e. rs h U3 t.U 5 T L P M s6 S / $f'ftlf0PMI /// [. l.- /( /l/! / i k ] 7]j ONCCN N3. Q hY' c,

1. RADIAT1ON 9ROTECTION OFF1CEW. '

A ttWt;closume of person's training ~end esparoe'nce as cuttoned in Items Car 1 W Hubbalc'ttt W[ /M !'D' *P"' I CC. [W./ M."C". '. 4.** !5. "' U *"" **ic h'*

• • ""d*'

-G / d'**** I n,;., r,, / l / 'f h 8. LICENSED MATERIAL MtC'd' 'Y88d 7 L ELEMENT"#"'*/T* CHEMICA1g NAME OF MANUF ACTU6ER MAXIMUM NUM8ER OF IltGBlV80 8)l4ND. r.'!','g MIL,LlyURIES AND/OR SE ALED M// 'M ANDIOR 8 i AND N M ASS NUMSE R* mran mL rur M "^"ELJd uMSE R SOURC,ES AND MAXIMUM ACTI. E (t/ Sealed Source) VIT Y PER SOURCE WHICH WILL SE POSSESSED AT ANY ONE TIME N O. A e C D Ii t to exceed 11: Americium 241 Sealed Source Gulf Nuclear,Inc. 5 curies / source c,we.s. m m Cesium 137 Sealed Source iulf huclear,Inc. Not to exceed tri g q q,.3 _ uf m 2 curies / source g, Iodine 131 any Gulf Nuclear,Inc. 25 mil 11 curies ni Iridium 192 any Gulf Nuclear,Inc. 25 mil 11 curies DESCRIBE USE OF LICENSED MATERIAL E g i, Lines # 1&2 to be used for 011 well logging ~ services 12 Lines # ]&4 to be used for tracer studies in oil & Gas 'Well's. - p

r. = = a (4

U $ $ $oM 040702 Control No. {g97 12-24320-01 PDR ]D f, 'M f

C C

9. STORAGE OF SEALED SOURCES y

CONTAINER AND/OR DEVICE IN WHICH EACH SEALED NAME OF MANUFACTURER MODEL NUMBER N SOURCE WILL BE STORED OR USED. NO. A. S. -C. Gearhart 3&5 Curie Neutron Shield b1f>M ""O% g rie Lead shield ni (31 (4)

10. RADIATION DETECTION INSTRUMENTS TYPE M ANU F ACTU R E R'S MODEL NUMBER RADIATION SENSITIVITY

{ OF NAME NUM8ER AVAILABLE DETECTED MANGE N INSTRUMENT (alpha, bets, (mlillroentgens/ hour t gamme, neutron) or counts / minute) un, A B C D E F ~ fli Survey Meter Victoreen 493 2 Gamma-Neutron Ok/ Neutron (2) Film Badge Gulf Nuclec r 833 leak test Gulf Nuclez r LTK-1 all source s GR/N (4)

11. CALIBRATION OF INSTRUMENTS LISTED IN ITEM 10 Ga. CAL 10 RATED BY SERVICE COMPANY Ob. Call 8 RATED BY APPLICANT NAME, ADDRESS, AND FREOUENCY A ttach a separate sheet describing method, frequency and stendeMs Gulf Nuclear TNC.

us*d for c*!*br* tone instruments. a 100 NASA RD. Suite #1 Webster, Texas 77598 every 6 mos.

12. PERSONNEL MONITORING DEVICES (Check and/or to !$te as appropriate.)

(ServYce C$ pony) "C"# Gulf Nuclear, Inc. Of MONTHLY Q(H) FILM BADGE 202 Medical Center Blvd. Webster, Texas 77598 O OUARTERLY O t2) TH E R MOLUMINESCENCE DOSIMETER (TLD) O t31 OTHE R ISpecotyl: O OTHER (Specoty): ,13. FACILITIES AND EQUIPMENT (Check were appropriate and attach annotated sketch (es) and description (s). O a. LABORATORY FACILITIES, PLANT FACILITIES, FUME HOODS (Include filtration,itenyl, ETC. [R b. STOR AGE F ACILITIES, CONTAINERS, SPECI AL SHIELDING (/omed and/or temporary), ETC. Qe REMOTE H ANDLING TOOLS OR EOUIPMENT, ETC. Od RESPIR ATORY PROTECTIVE EOUIPMENT, ETC.

14. WASTE DISPO_ SAL a.NAME OF COMME RCI AL WASTE DISPOSAL SERVICE EMPLOYED Gulf Nucleat INC. WEBSTER, TEXAS b.lF COMMERCIAL WASTE DISPOSAL SERVICE IS NOT EMPLOYED, SUBMIT A DETAILED DESCRIPTION OF METHODS WHICH WILL BE USED FOR DISPOSING OF RADIOACTIVE WASTES AND ESTIMATES OF THE TYPE AND AMOUNT OF ACTIVITY INVOLVED.lF THE APPLICATION IS FOR SEALED SOURCES AND DEVICES AND THEY WILL BE RETURNED TO THE MANUFACTURER,50 STATE.

NMC FORM 313 t it2 sti

INFORMATION REQUIRED FOR ITEMS 15,16 AND 17 e Describe in detail the infortnation required for items 15,16 and 17. Begin each item on a separate page and key to the application as follows: a

15. RADIATION PROTECTION PROGRAM. Describe the radiation protection program as appropriate for the material to be used including the duties and responsibilities of the Radiation Protection Officer, control measures, bioassay procedures (If needed), day to< fay general safety instruction to be followed, etc. If the application is for sealed source's also submit leak testing procedures, or if leak testing will be performed using a leak test kit, specify manufacturer and model number of the leak test kit.

16. FORMAL TRAINING IN RADIATION SAFETY. Attach a resume for each individual named in items 6 and 7.

Describe individual's formal training in the following areas where applicable. Include ] the name of person or institution providing the training, duration of training, when training was received, etc. l

a. Principles and practims of radiation protection.

b. Radioactivity measurement standardization and monitoring techniques and instruments.

c. Mathematics and calculations basic to the use and measurement of radioactivity.

d. Biological effects of radiation.

17. EXPERIENCE, Attach a resume for each individual named in items 6 and 7. Describe individual's work experience with radiation, including where experience was obtained. Work experience or on-the-job training should be commensurate with the proposed use. include list of radioisotopes and maximum activity of each used.

18. CERTIFICATE (This item must be completed by applicant) i The applocant and any official esecuting this certificate un behalf of the applicant named in Item 2, certsfy that this application is prepared in conformity with Totle 10, Code of federal Regulations, Part 30, and that all information contained herein, includmg any supplements attached hereto, is true and correct to the best of our knowneke and belief.

WARNING.-18 US.C., Section 1001: Act of June 25,1948; 62 Stat. 749; makes it a criminal offense to make a willfully falso statement or repeasentat6on to any deportment or seency of the United States as to any matter wt.hin its jurisdiction, I

a. LICENSE FEE REQUIRED

($' b.CERTI YING OFFICI AL (5,aneture) Isoe section 170.31,10 CFR 170) % U. ~ y l_

c. NAME IType or pronti Carl W llubbartt (1) LICENSE FEE CATEGORY: Well Logging & Surv$y General Manager & President e.DATE 12: LICENSE FEE ENCLOSED: S NEW 460.00 March 23, 1984

,.nc eonu sia siis en po en an j

{ { Resume of applicant Name Carl W Hubbartt Address P.O. Box 734 Fairfield, Illinois 62837 Birth Date April 14,1955 Occupation Oil Well Logging Engineer Formal training in Radiation Safety I have attended the three day Oil well radiation training school provided by Gulf Nuclear,Inc., completed March 24, 1982.My Certificate is attached. After such training I have been involved as general manager & Radiation Safety Officer at Mid-States Logging & Perforating Co. in Fairfield,Ill., for the past 2 years. I am familiar with items a,b,c,d, under Item 16 of the Radiation application form 313. These items were discussed and covered during my schooling in Radiation with Gulf Nuclear, Inc. Item # 15 I have outlined in my Radiation Manual, appendix A, RADIATION PROGRAM MANAGEMENT AND RESPONSIBILITY,which I Have initiated as my new companys daily procedures. EXPIRENCE-ITEM 17 of application My experience includes the use of the following radio-isotopes: Americium 241,3 & 5 curie Neutron sealed sources,2 curie Cesium 137 sealed source, & Liquid Iodine 131,& Iridium 192, for the purpose of 011 Well Logging & Tracer studies with my company. These radioisotopes are the same isotopes I plan to use under my one truck logging company in the near future.

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evised Addition for Materi s Liscence United Wirelino Services Inc. Submitted by Carl W. Hubbartt 1. Item #5 of application Street address the same. Liscenced material will be used at any remote area or temporary job sites within the complying NRC states in the U.S. for Logging purposes only'. Description of shop area is as follows, including designated storage area. N mwhe t w e. t ~ . C~ gv 6 9% q ii DCOT UJ%, Espo$jvf f I E bv G w I o % c.c. g N-(L oo sq \\ t 8' ~ ,a% e. M Stem q q9 q s34 Nt % 0 bJtbT W 33 cesw (t>6 s a go w e %ts:M.i t'Ow 5' _ y iR A R EC EIV E D tu s ' ' t e. % i JUN 2 81984 g.___. a o ' y E"' kVe GuNet shw 4 g MN IU t.oem e b g c o' ~ s 4 ' *4 wn e a m.,

( ( The survelance of all RA materials will,be handled by myself i at all times during the use of the' material at temporary job sites, es well as in the shops and transporting to an from the job sites. i All incoming and out going source shipments to an from the j supplier will be scheduled and handled by myself at my convience, j so that I may monitor excess RA levels, check into or out of inven-tory, the proper paper work is in order, etc. Under Item 8 of application the following Model numbers will be used ~AmBe source'241 71-1 not to exceed 5 curies Cesium source 137 CSV not to exceed 2 curies I will assure they will not be altered in any way, nor will the i i Radioactive pill be tampered with or removed, while in my possession I es the designated uses of such source. All sealed sources will remain'in their respective shields under l lock and key while not in use, either in the shop designed area or on the truck during transporting. 4 A routine inspection of all'RA material containers and equipment will be performed an a monthly basis to assure proper conditions such as condition of source, proper labeling, workable source handling tools, etc. any equipment found defective will be replaced immediately. ' And records of such inspection maintained for a period of at least 2 . years.. -Fishing operations All fishing operations will at all times be under my supervision, ajunk-basket or: an overshot will be used to fish for the source if deemed feasable. The following prce'edure will be used: A. Clear area of all unauthorized personell and post restricted area E. Make a RA survey of the well an surrounding area. C. Notify the NRC and local authorities D. Proceed with fishing: operations' if possible E. If attempts are unsuccessful, the source will be cemented in permenatley, including a deflection device.

F.

' Identification plaque placed at the well head, with the information as-outlined in section D page 28 of NRC well logging operations. G. File report with NRC containing information in section C, item 3 page 27 i i-,

of F:RC wall logging o(perations. ( D.O.T. Regulations At all times all employees will follow D.O.T. regulations, as they will keep Regulation Log books, survey sheets, the proper plackarding,etc. Utilization Records I will agree to maitain current records which will be kept available for a period of 2 years containg information as, A. Make,model, and serial number of each source used and dates. B. The identity of well logged or supervising user assigned. C. Locations where used and dates D. Tracer materials will include the radionclide and activity used in each well. Documents and Records at field stations; I will agree to maintain for inspection by the NRC the following documents and records. A. Copy of the NRC liscence B. Operating and emergency procedures manuel C. Applicable regulations D. Record of latest survey instrument calibrations E. Record of leak test results F. Inventories required in accordance with item 10.2.6. G. Utilization records required in item 10. 2. 7 H. Records of inspection and maintenance required in item 10.2.9 I. Survey records required in accordance with item 10 5 1. Documents and records at temporary job sites I will agree that while conducting operations at a temporary job site, the following records will be made available foe inspection; A. Operating and emergency procedures manual B. Survey records in accordance with item 10,5.lof app]ication.

( ( C. Evidence of current calibration for the survey instruments in use at site. D. When operating in an agreement state under reciprocity, a copy of my NRC liscence. Facilities and Equipment We will be using 3 survey meters with a scale of 0-100 MR/h, which will be sent to Gulf Nuclear every 6 months for calibration. The survey meter calibration will be spaced 3 months apart so there will be at least 2 meters available at all times, one in the shop area, and one for job site and truck use. brut 3 %ew m& nutsuo % % %.ted M wite me - C,ww Personnel Monitoring o - 1 R, All personnel directly related to activity involving radioactive materials will wear a TLD badge or a suitable acceptable dosimeter. Film badge records will be quarterly and monitoring will be at least on a quarterly basis. Leak Procedures Leak tests will be performed every 6 months by Radiation safety officer, myself. I will be using the LTK-1 leak test kit supplied by Gulf Nuclear. The source will be swab tested, using 4 i t. the source handling tool to minimize exposure time during the test. Once the test is completed, a survey of the leak test kit will be made before sending the test to Gulf Nuclear for analysis, the readings will also be recorded for our files the same day. I myself will be the only classified user of RA materials at the time. I intend to initiate 2 types of training programs as follows. A. Program 1 will be designed to familarize the hazards of radiation, its, affects, the use of the film badges, survey meters, etc. This program will be directed to non users associated with the company such as sales personnel and servicemen under my supervision at all times.

( ( Program 2 will be directed to potential users as engineers B. who will be required to attend at least 24 hours of instructions in well logging safety through a qualified institution such as Gulf Nuclear to be certified. (section 10 3 1 of instr'uction manual) All employees classified as users or non users will be required to take an annual refresher course on a regular basis either written or orally. Individuals responsible for safety program; I agree to follow the items under item 7, page 5 and 6 of RA logging guidelines, under my position of Radiation protection officer, especially items d,e.g,h,. To ensure that liscenced material is properly secured D. against unauthorized removal at all times. To supervise leak testing of sealed sources and instrument E. calibration To serve as a point of ' contact and give assistance in case G. of emergency. To ensure that the terms and conditions of the liscence H. such as periodic leak tests, are met and that,the 2 required records such as personel exposure records, leak test records, etc. are periodicalJy reviewed for compliance with URC regulations and the liscence conditions as listed on the liscence. I l t

( A temporary shop facility will be set up in Industrial Park located in Fairfield Illinois to also house our Ra and explosives materials until our permanent office is completed in Whittington, Illinois on Route 37 south of Mt. Vernon Illinois appioximetly 12 miles south. This will then be our only permanent shop and office NOU under construction. We will purchase only 1 AmBe 241 sealed source at this time until our permanent shop facility or the Fairfield facility, so I anticipate no problems in the monitoring of this source. I have enclosed a diagram of the tenporary facility in Fairfield as well. Respectfully submitted, $& Gu /WN Carl W. Hubbartt h e 4

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( h7.C Form 313 I U.S. NUCLEAR REGULATORY COMMISSION

1. APPLICATION FOR:

(Check rnd/or comphts es appropri3t:) (12C1) 10 CFR 30 APPLICATION FOR BYPRODUCT MATERIAL LICENSE X) a. NEW LICENSE INDUSTRIAL

b. AMENDMENT TO:

See attached instructions for details. LICENSE NUMBER Completed applications are filed in duplicate with the Division of fuel Cycle and Material Safety. Oflice of Nuclear Material Safety, and Safeguards, U.S. Nuclear Regulatory Commission,

c. RENEWAL OF:

Washington, DC 20SSS or applications may be filed in person at the Commission's office at g, 1717 H Street, NW, Washington, D. C. or 7915 Eastern Avenue,. Silver Spring, Maryland.

2. APPLIC ANT'S NAME (Institution, firm, person, etc.)

3. NAME AND TITLE OF PERSON TO BE CONTACTED REGARDING THIS APPLICATION UNITED WIRELINE SERVICE,INC.

CARL W HUBBARTT, PRES.& MANAGER EL PH N BE : ARE A CODE - NUMBER EXTENSION T P O MBER: ARE A CODE - NUMBER EXTENSION

4. APPLICANT'S MAILING ADDRESS (include Zip Code)

5. STREET ADDRESS WHERE LICENSED MATERIAL WILL BE U3ED (Address to which NRCcorrespondence, notices, bulletins, etc.,

(include Zip Code) sToouid be'serit.[ ~ P.O. Box "5$ W 1925 Maple Ave. Fairfield, Illinois 62837 Mattoon, Illinois 61938 (IF MORE SPACE IS NEEDED FOR ANY ITEM. USE ADDITIONAL PROPERLY KEYED PAGES

s. INDIVIDUAL.(S) WHO WILL USE OR DIRECTLY SUPERVISE THE USE OF LICENSED MATERIAL (See items 16 and 17 for required training and experience of each individualnamed below)

TITLE FULL NAME Carl W Hubbartt President & General Manager b. c. " Attach a resume of person's training and experience as outlined in items

1. R ADIATION PROiECTION OFFICER Car 1 W Hubbartt l '6 *"" U *"d d**c'ib' bi' 'p"*ibi'i'i'* ""d h*m 15-l

8. LICENSED MATERIAL L

ELEMENT CHEMICAL NAME OF MANUFACTURER M AXIMUM NUMBER OF AND MILLICURIES ANDIOR SE ALED I AND ANDIOR MODEL NUMBER SOURCES AND MAXIMUM ACTI-N MASS NUMBER PHYSICAL FORM VITY PER SOURCE WHICH WILL lifSealedSource) E BE POSSESSED AT ANY ONETIME NO. A B C D Not to exceed Gulf NuclIa~r',Inc. 5 curies / source tu Americium 241 Sealed Source c, w e.s - m u Cesium 137 Sealed Source lulf Nuclear,Inc. Not to exceed (2) q _ x_ _eM n 2 curies / source [g Iodine 131 any Gulf,N,uclear,Inc. 25 millicuries Gulf Nuclear,Inc. 25 millicuries Iridium 192 any g3 DESCRIBE USE OF LICENSED MATERIAL E Lines # 1&2 to.be used for Oil well logging services (n (2) Lines 77 3&4 to be used for. tracer studies in oil & Gas Wells. (3) (4) N HC F C HM 313 I (12 81)

N

9. STOR AGE OF SEALED SOURCL.

k CSNTAINER AND/OR DEVICE IN WHICH E ACH SEALED NAME OF M ANUFACTURER MODEL NUMBER o ~ p SOURCE WILL BE STORED OR USED. No. A. 8. -C. M-Gearhart 3&5 Curie Neutron Shield Gulf Nuc, lear &,.ving ggrie ti) anarhar Tnan c: Lead shield (3) (4)

10. RADIATION DETECTION INSTRUMENTS TYPE MANU F ACTURE R'S MODEL NUMBER RADIATION SENSITIVITY y

OF NAME NUMBER AVAILABLE DETECTED RANGE N INSTRUMENT fofpha, beto, (millircontpens/ hour

• • • • • "*"""I
• *""'*I""I No.

A B C D E F (Il Survey Meter Victoreen 491 3 Gamma-Neutz on 7bb all employ ees/ Neutron GR

12) EJ-M Badge Gulf Nucle 2 r (33 leak test Gulf Nucles r LTK-1 all source s GR/N 14)

11. CAllBRATION OF INSTRUMENTS LISTED IN ITEM 10 Ga. CAllBRATED BY SERVICE COMPANY Ob. CAllBRATED BY APPLICANT A ttach a separate sheet describing method, frequency and stamferds N AME, ADDRESS, AND FREQUENCY Gulf Nucleara 1NC.

used for ca!!brating instruments. 100 NASA RD. Suite #1 Webster, Texas 77598 every 6 mos.

12. PERSONNEL MONITORING DEVICES TYPE SUPPLIER EXCHANGE FREQUENCY (Check and/or complete as appropriate.1 (Service Company) g A

B Gulf Nuclear, Inc. g ugg7 gly Q({ ti FILM BADGE 202 Medical Center Blvd. 1ebster, Texas 77598 O QUARTERLY O (2) TH E RMOLUMINESCENCE DOSIMETER (TLD1 O l3) OTH E R (Speco!y1: O OTHER (Specify):

13. FACILITIES AND EQUIPMENT (Check were appropriate and attach annotated sketch (es) and description (s).

O a. LABORATORY FACILITIES, PLANT F ACILITIES, FUME HOODS (/nclude filtration,if anyl, ETC. Q b. STOR AGE FACILITIES, CONTAINERS, SPECI AL SHIELDING (fixed and/or temporary), ETC. Q c. REMOTE H ANDLING TOOLS OR EQUIPMENT, ETC. O d. RESPIR ATORY PROTECTIVE EQUIPMENT, ETC.

14. WASTE DISPOSAL a.NAME OF COMMERCI AL WASTE DISPOSAL SERVICE EMPLOYED Gulf Nucleat INC. WEBSTER, TEXAS b.lF COMMERCI AL WASTE DISPOSAL SERVICE IS NOT EMPLOYED, SUBMIT A DETAILED DESCRIPTION OF METHODS WHICH WILL BE USED FOR DISPOSING OF R ADIOACTIVE WASTES AND ESTIMATES OF THE TYPE AND AMOUNT OF ACTIVITY INVOLVED. lF THE APPLICATION IS FOR SEALE D SOURCES AND DEVICES AND THEY WILL BE RETURNED TO THE MANUFACTURER,SO STATE.

NRCFORM 313 1112 41) Control No. 76597,

INFORMATION REQUIRED FOR ITEMS 15,16 AND 17 Describe in detail the information required for items 15,16 and 17. Begin each item on a separate page and key to the application as follows: 15. RADIATION PROTECTION PROGRAM _. Describe the radiation protection program as appropriate fo,r thei material to be used including the duties and responsibilities of the Radiation Protection Officer, control measures, bioassay procedures I/f needed), day to< fay general safety instruction to be followed, etc. If the application is for sealed source's also submit leak testing procedures, or if leak testing will be performed using a leak test kit, specify manufacturer and model number of the leak test kit.

16. FORMAL TRAINING IN RADIATION SAFETY. Attach a resume for each individual named in items 6 and 7.

Describe individual's formal training in the following areas where applicable. Include the name of person or institution providing the training, duration of training, when training was received, etc.

a. Principles and practices of radiation prote:: tion.

b. Radioactivity measurement standardization and monitoring techniques and instruments.

c. Mathematics and calculations basic to the use and measurement of radioactivity.

I

d. Biological effects of radiation.

17. EXPERIENCE. Attach a resume for each individual named in items 6 and 7. Describe individual's work experience with radiation, including where experience was obtained. Work experience or on-the job training should be commensurate with the proposed use, include list of radioisotopes and. maximum activity of each used. 9

18. CERTIFICATE (This item must be completed by applicent) l a

The applicant and asy official executing this certificate on behalf of the applicant named in item 2, i certify that this application is prepared in conformity with Totle 10. Code of Federal Regulations, l Part 30, and that all information contained herein, including any supplements attached hereto, is true and correct to the best of our knowntdpe and belief. WARNING.-18 US.C., Section 1001: Act of June 25,1948: 62 Stat. 749 makes it e criminal offense to make a willfully false statement or representation to any department or agency of the United States as to any matter wi.hin its jurisdiction, i

s. LICENSE FEE REQUIRED gi.

b.CERTI YING OFFICIAL (Signature) (See Section 110.31,10 CFR 170) $C y

c. NAME (Type or print)

Carl W Hubbartt

d. TITLE 01 LICENSE FEE CATEGORY: Well Logging & Survey General Manager & President

e. D ATE (2) LICENSE FEE ENCLOSED: s NEW 460.00 March 23, 1984 Control No. 7639Ti

• ee romu aia ina.au o -o a '"

(.~ UNITFD "IRELI:'F. SERV TCES, INCORPOPATED P.TDICACTIVE 3'ATERIALS STORAGE,OPERATIMG AND EMERGENCY PROCFDURES MANUAL I l I I l 8408210624 840702 NMS LIC30 l 12-24320-01 PDR r

.sr A?E'NDIX A-I. Radiation Pro.: ram Manacement and ResDonsibility A. Com.tane Oraanization Chart Safety Officer II. F.adiatic. ... r.. o _., c, 7 7 a n_ a ...c ~

+

n p e.- s c.. e. 4-. 2 g*. .c ". C ". 4 3 '~ A ".' 4 .C " '.'. U. r _.r. 3...-s d..# ^. m~ ~. * ". e.i.ac- $ _.- 4 a l s 4 s. g. .: v, q + 2.c - !.<_.-.._._'__-...c_y-e y. V~. F.ecord ..r.a g er.e n t _.. - C '1 O a C l i V '3 h.B t e r i a J. S . r O CC-G u r:.;C :-or '2 Th::SDo rt inc. ....Yji. r f

G APPENDIX A I. RADI ATIO:: PROGRAM MANAGEMENT AND RESPONFIBILIY;

a. The radiation Protection officer is to be designated overall manaaer for the radiation program.

b. The duties of the nadiation Protection Officer included the delegaticn of authority to persons responsible for carrying out the duties such as that of Radiation Tafety Officer, Overall responsibility for records, surveys, the forming of corrittees where necessery and in general the administrative procedures for the entire radiation prograr.

The Radiation Protection Of ficer is CARL F ITUEHARTT. IT. The Radiation Fafety Officer is responsible to the Radiation Protection Officer and in aeneral is to conduct or cause to be conducted the programs and responsibility delegated by the Radiation Protecticn Officer. These duties might include; a. Site surveys b. Records, personnel nonitorina rccords and compilation

c. -Vehicle sur"ey records d.

Training & qualifyino personnel e. Cr.nducts prriodic cafety check.s to as.'.ure the radiatien protection prograr. The Radiatior Fafety Of ficer is CAPL F !!UBPARTT. III. .ERFONNEL '.inP FORT"G rPCCEDUREF ALL personc] directly related to acti"ity involving radioactive raterials will uear a filr> badge or a suitable acceptable dosireter. Fi.!r hadce recort.s will be quarterly and ronitorinI will be at least on a cuarterly basis.

e ( It ir clearly understood that maximun. acceptable dose levels are not to exceed 1.25 Rem per calendar quarter or no more than 5.0 Rem per calendar year, It is also clearly understood that in the event these -doses are greater than those listed above that proper notification will be posted with the licensing autho-rity. Also reports of desages will be maintained on at.inast a cuarterly 'rasic. IV. Storing and Securing r.adioactive Materials Upon receipt of the racicactive materials the receiving records will be placed in a properly marked file. The materials will be placed in a secure area that is pro- .cerly marked with appropriate signs around the perim'eter. This area vill be either a room, a storage area or a storage bunker but will in any case contain a door or lock type top. Materials when not in use will_ remain in the storage area properly locked and secured. V. Pcstinc Restricted Area, Vehicles and I,abelling Containers estine restricted arear-storace area and areas where a. r 2 mR/hr will raciation levels are expected to achieve be labelled with signs stating " Caution-Radiation Area" " Caution Eadioact ive Materials". These signs will or bear the. radiation rymbol and be magenta and safety yellow ir. color. The signs will be conspicuous and obvious f rom all dir ect ions. In the event that the levels exceed 5 mR/hr then a sign stating " Caution P.ich Radicticr Area', riacenta and safctv vellow in color will be ccnspicueusly postec. A pro,rer ';o: ice to Emp3oyees will a3sc be posted i wt.ere it is cbvious to e.plcyees. All vehicles t.ranspo'rLing or b. Vehicle 3ar5: ding. con t a ini n; r t :1c act ive

• r.a r e ri als wil,_ hear a pl a-

. ides t ".a t bears the pre r labelling card on four = according c .he D.O.T. sp.rci fi ca ti on s the word RADI CAC'h J E '. This piacard mproximately 10 3/4" . 10 3/4" will : e pl ac -a on the cehicle only when transporting or storing radioactive .ne venic,ie s - ~ r.ateria r. Th plaind is bia n 3 et -ring on a rafety yellow o_. <- i n. n l.. T- .d e r r t e o d ".a t this' a ,.. d i f ' ' i t- -h i r'l e is c 'c . :.: 1 2.

t ( c. All containers carrying or "t oring or used for trans-porting radioactive materials will bear a tag with the identification of the radioactive material,'the quar.tity of the radioactive materials-and the date that the radioactive material was that particular quantity. The tag will also state " Caution-Radio-active Matetials." ..ecords Management VI. a. Utilization Loc-This log will contain the master file on each type or shipment of radioactive material received and the distribution of each such shipment. This master file will be maintained at the facility. b. Receipt anc trans:er recorcs will be mal:.tainec in files to shcw at all times where material is to be located or -if it is disposed of. Personnel exposure records-film badge, TLD or dosimeter c. reports-will be maintained in a separate file a3cng with

o. ro.ner c.uarterlv rer. orts on each person using radioact2.ve materials.

d. Leak Test records on a31 s.u3ed sources will be main-tained on each sealed source. These records will in-dicate leak testing at six month intervals. e. durvey recorcs wn2cn ine,_uce br lc..ing or storage areas survev.s on a c.uarter3v. basis will be maintained in a filc. These survcys will. reflect in milliroentgens re ad ir.g s at a pcin on each side and the top of the storage arca. f. Vehicic surecys vill be conducted at monthly intervals and 'he c surveys will be icintained in a file. will he cend.r -d by r.onitoring a well bore at c. Su. <e ;c tne sur: ace prar to tre c:. any rac:cactive materlal and remonitoring.h2 we '.1 hore upon comp.3iet. ton or-

a.. e m

work. Th ; s e nu--h:- r c w i : 2

e recor de-d.

A survey meter or t.on1 which is.c a p:.ble vill be used for the moni- - "c.rds of t.h i s nurvey performed on toring rc .proce <acn ,.c o w i t,.t..2 ,a r.t a. :mc in a f a. 3 e. VI!. trocedu: es for Tra:.. parting :ndi active Matcrials c t -lO ~ "i v ..:

• Thnsported by CO%canV I

h. N.I i s'.. *- t iV O '*J.~. g g

.r i i r

rc-

[ L_

d-( pcrly' pac). aged and mnried. 1.n identification will'be on each container transpo;. ud and the vehicle will be .lacarded with the proper D.C.T. markinc.s. p b. The vehicle transporting radioactive materials will be clearly placarded with a 10 3/4" x 10 3/4", dia-m:nd shaped sign with 'c2ach letters that read " RADIO-r.r. a : s = Fachape;s transported will :3e packaged.as received from c. the supplier. These packiges generally bear a diamond shaped Yellow III label. It is clearly ur.derstood, hat signs will be removed when vehicle does not trensport radioactive materials.

O - APPE.NDIX B-I. Procedures for Storage a. Storace b. Transport II. Procedures for Use of Fadioactive Sources !II. Radiation Survev.s IV. Leak Test Procedares V. Procedures for Lost Source D: .':ici c V~. E ergency Procedures VII. St.ferv Cu rve for AmBe Sources N

IJ> r, v.,.D,d-. r. Procedures for Storing Scaled Sources of Radioactive I. .aterials c-o ac,a = ~ -. w. .:ec in t.nelr snaelc. , or. ,De nacicactive sources mus: anc i. e.ot in a loc ;ec s tor.:ce, t ruck c'a-. par trient, cabinet, pit or chained and-locked t.o an integral g _... o. . h c.. .a _ i..., -n e.

r.,

..._,,o_. e . or ositionec .etcra:e rac1,_ r.ies .ust.e r: c e s i c. n ec. so :na no person in an u:cor. ro,. ec erea can re-ceive :mor e than 2 n.R in cny cne hour or more than 10 0 r.E in any seven cor necut _ve days. (1) Storage Pits (Downhe'n} (a) Mini::.um of two feet of carth, concrete c... m_ c. o _

1 1 o e,_,....,.

. -; c. c . c. (b) Pits to be a minir.ur of four feet deep. (c) Lids to be screwed cn or recessed in, cesac_aec to exc.uce.ater and ecui.c.oed w 2 t.n a l oc,i: i n c. c.m ce. ... ~. -.; "s c.e, y. ! '.) ~. 6 g .p ...p. .....c_..

y.....i...*.:

g g.,. $. c.. -s .u.

w......

p.. a -.

..C ""'L" ".> ~w w a.. b s^. Y. 1 7. _........e. r. +.,., c. ) g.,-. c.:. ...3eg .c. .e .u. L.. .i n *w 3,.. 7 9... o." l'.'.'"". .. - c C. l a g__ .w, (., .c.>......u... w. A. ..; 91. e. D.. '._%; 3.......ic..--c. .. i.. C a i F,.. CcL: .; s. ...,C*, c 4 c. Le CELaD31Shec .1 : t..". e .~4.. . & *s' e 3. 9 ( m. ', . a. .ny i

• y y. m j cs -

.. r_ % c. ......._ s,:.. t 1 ,3..c s e 3.< a ;; u. .c. .c..... .e .....: aC.,.. s .-(.3 r...,*. . s: c. 6, e.

r...._.:

u -e .....,At n c,:- .y.< :. 2,. ., L+.- ,., 3 i...<.--.-.. u.1 e,,,, 6... r... s.. *. 1 .3 ..,c C o a.2 .t ...t i t o . ~ r. s. . a,. c ..n. s.. e.... t e

( ( be chain locked to an integral part of the vehicle. Vehicle will then oc placarded with D.O.T. specifi.- cation RADIOACTIVE" _ signs on all four-sides. II. Procedure for Use of Radioactive Sources Compan personnel c..irectiv. in charce c:. loocine. coerations utilizing radioactive sources are resp:nsible for the health pro.ection of all personnel aest.ciated with the sources and the general public wh may be associated at all times. The above personnel (company) must personally i su,rervise all source.handl.ing ooerations-transportation < storage and shipping according to the following regulations. (1) Company personnel who have been trained in handling sealed sources shall be the only ones who perfor:n c.oc r a ti ons involvinc., the sources. All customer oer-s c r.n el shall be recuired to be remote to these opera-tions. ( ) Oni. the com.nanv. a provec handline tools will be used. e

e. l. s c.u c e s are to be t r a r.. o r r e n. in tne approvec anc

(,, lockcd source shipping con:siners. () U. sing t.ne remote hano...:ing tools the source is re-moved from -he shipping or transport container. The sc.urce is attached to the lcncina tool and olaced in-s:ce cf t.ne well, h*nen logging operat1on is fin 2snec tne cr2 Aer v1. return source to sur., ace tne

occinc, o

op.ratcr ill r en.ov e tool f r c.T well, utilizing remote he.ndl nc tool, the source will be removed from the tool e.nd..:.: cad hack into the s:vrage container. The time-din snee fac. ors must be ut.a# a~# Actively when working v i t' rad.icactive sources t o i.eep cxposure to a minim =. .C.un ut;. ing the remote h:.nd13 ne tools a safe distance is provided but ea:e and practice are neede6 to decrease the h u.dling experure time. iL)

ny sourcer that you e.re not funiliar with, in handling

.nd urace c ont ;ct the a :

.s enc' n -er or the Radiation Fsiety 6fhicer before using them in a logging job. m III. F.e lilt * '.(". urveys j '. 't .it

t.. U ! c C L ' f.t.290 b.M :}. +. :

.G V e O101 :90 cT ^I3nC- ?.r: ~ ;.' a .P? r f ; r.. - hu j..v. .MTh por able l o*.t - l e V e l - <ix i:.:: g f:cr av..rce. -r Control No. 7 6 5 9 T. e

1 Place source in vehicle. Record on Job Log Sheet. secure position. (Loci:ed containment) Survey Record en Job Log Sheet. .Invehicle on all four sides. Arrival at well site-using low level' survey meter,

.. s Record '

monitor the area before cc:mnencing job.Af ter job is finish sketch of area. d to determine there is no contamination aroun on After arriving area site. Record on Job Log Sheet. storage site monitor vehicle to show free of con-w?ll attamination. The f ollowing.han_diling equipment Jr.ust be present and Gloves, handling tools, protec-used on well sites: tive clothing. IV. Le ak Te s t Procedures intervals sources must be preformed at h'i pe tests on all not exceeding six month. Inc. Model Source vill be wipe tested wi th Gulf Nuc1 car, (pr o-edures enclosed) L'IE-1 '<. i. Test rit. Inc. at kits will be mailed .o Gulf nucle.tr, Leak ' Test Houston, Texas f or cour. ting. sent back to licensee with lesh test E -ports.cill be certificate. V. F:onedure for ',ost sou: ce zwnnole netify the well ow..ar or his (1) h' :e r. a rource ic Josta source is s 'ch in the well. that .e ae: ntative . a n c... nim a orawing ti.ere*1 t er as POCrih3 0 n 7his wil3 enable r.? F O n Scu r ce (:nd nour. ; n:- DDCel. Of *he

sning operation

. e: tre he c '-a rts the t.ype of .,dioactive material and the . ::i. t.o..now r. t5. e.;u an t i ty, and toO1 CCDF*.! uction of the CapsOlft r.chaniCal involved. Crate Radiation Control Ag<encv.

.=ed i c.tely no:, f.'

theNuclear Regu3 atory Cort nission. _ :.volv ed und the U.S. anc.eep tnem inr crmac

o' rce..a s ' acon lost t..c t ow.a r d 2 ecovery of the source.

c' -he.Iv9rerE (2) '"... n t - : c '. e r., ' - f ;,..., . y ;

r t d t o 5

11 ! i g,..- r,c n:cs 1

) rr w'I; t. ' '. e,.. r r V I l ". v a t;i' r r 0 9

( ( that these are for their protection and intended primarily for a record of trivial or no exposures to his employees. s. c. (4) Durino the critical fishing operations the mud beine. -circulatec. shoulc. be monitorec..usine. c.amma ray equipment with the downhole tool in the mud. (c.) ..cu have only tu:.e anc c1 stance tactors available 2 to reduce the radiation field and personnel exposure while the source is being fished out. .*here prac-r tical everyone exce.pt the driller and enough per-sonnel to cover the hole should remain in the area. All handling of the drilline. rio. co.uie~nent should be handled by the custo.mer and actual handling of the source shall be done by the licensee. VI. Emergency Proredures Enerc. enci es var}- c.reativ in their res.oective harr.rds. These are sometimes in the fer:n of spills, fires, ex-picsions or vehicle wrecks which consecuently result

n :s..e spreac c:. rac cact.ve r.a t erial conta: tina tion.

The ! ational Sureau of Standards Handbook !;u:nber 4 8, Emercency Guides, are used as a cuide for the procedures. These t.rocedurer are ceneral and anv specific emergenev wou}c c e: : n i n1.v -nvolve accational.orocedures not covered in the outline. (1) Vehi r1e W: eck In t ;- -

4. v e n t of an acri~ :.t while transportine radio-r h ou.. be n.a c.e to minirnize te ac::ve ater:aar, er : o: t s thc c x;. :.: e r e cf any 3.cr uns.

Thic would include r rr,- i n g c f f th-c.rta,

,.

:. f f.:a ti on of the investi3ating ef'icer, a r..:. Tadiation F:fety Officer at the ho:re r e f i :- c '. r r. d 'r e ne, :f'-J

..d i z. t e ly, aking ::t re t :,a t - he arca ir no-inft u:,a t t e nd ed. This wil'. enable the .adiation rafety Gf fice: to notify the proper g r.. : : -.-n t a l a = - n c y. 1) Fi r- . d 0:.her E.w. r g e: - r li; ' M.. i f.

e. 3 2 :... r..

.n c i.:. the arot.. ::.:ied i a t ely 'b3 .: : e.:.pt to

.t out nil !irest if a :. dia ti on

.. :' ~s r 0 if D:c t

i'.:.. :

'. y _ r e:D 614 % . u..c.

r. :., -

s.

u y ( '. -' ' '

r i .r

( ( APPENDIX C PROCEDURES FOR TRACER APPLICATIONS 1 I. OIL FIELD TRACER APPLICATION II. SAFETY PRECAUTIONS III. Health Physics Regarding Actual Field Studies A. Monitoring Job Sites B. Handling Equipment C. Pocket Dosir.eters D. FILM Badges VI. Tracer Packagino V. Handling & Field Equiprent chech lis: VI. Operating Procedures VII. EMERGENCY PROCEDURFS A. Energency Procedures Report VIII. Monitorina Techniques for Personnel IX. Transportation & Disposition of Radioactive Faste Safety Procedures for !!andlinq Radioactive Tracers A. Introducticn B. !!andling Procedures C. CONTAMINATION Survey Techniques D. Decentar.ination Proceduren XI. CHARTS A. Iland Exposure fror Radioactive Tracers E. Radia tion Levels at 1 foot 'rer unshielded Radioactivo tracer L'. Radiation leveln at ' feet fror un:; hie]ded radinactive tracer.

e \\ \\.. \\.N. - t , ' N.:c. - g ...~.. m .;.. : ;.m.~ m,. .g.- :.. c ; - c. h ~ -iZ I. Oil Field Tracer Applications i Selection of the isotope depends en the study to be perIormec. L:..stec..celow are the critical isotopes and some injection techniques. Io,ine-lal Irid iu: -192 The method of injection depends on the t.pe of equip-e ment avad'iable and the presrure and condition of the well. The fol]owin-are descriptions of applicable e techniques. A. Liquid anc gas tracers can be inserted by means of a sampling bomb. A creater.oressure can be exerted beyond.the bomb than that of the item on anc the material is pushec. into ceing workec. the well head. Very frequently used on gas wells.

• .ater # als are placed in breakable vessels and 3.

attached to a logging device. h~nen in the well the.v are exoloded bv. use of a sc.uibb charc. e. C. The..n._ rial can be poured or inserted by using Used a syr.ge directly into the well head. i where no pressure is involved. D. h.ere ranc :s concernec the ranc.1s general.y 2 hiended nt the riurry hc..pe r. pi e S..:. i s i c... .-d .rao the well end by E. The so,aenoic. utc....u c. t o e. us:ng n u:ning :cv:ce. .nto :ne :2cw. T.,e enter:al :s re.. a r ca so:cre is cdded to ?. An ;,r pr opr i a t e., u u n t of 2.- an.n ecticn torl which i :: controlled from the tr uci. jar.el bo -rd p< nd t :.ng limited quantities of 2: erta!c tc he in j e c c-d.

~ Studies covered are ar follows: acidizing operations, cement top loce.tions, cement channel locations, casing seat channel locations, water flood. directional flew,W ~ ~ inter' face markers, f l ok..'- ~ ~ ~ i oil injection profiles, calibrations, oil slurry cement locations, gas flow-.. calibrations, gas channel locations behind-casing, gas i injection profiles, gas flooding, recovery projects, re:1nerv anc enemical clan: caseous oroduct tracinc, ~

racturing, muc car.e cetermir.a:1on and per.meability surveys.

II. Safety Precautions Generally, the followinc. safety facts should be known and observed when utilizing radioactive tracer materials. e 1 A. Saf ety through Distance-Distance can be an effective safety measure from a source. Safe distances should be known for the amounts of radioactive material being handled. ~ D:ancles of extesure rates at various distar-es from ~ ICi; millicurie scurce: a i Radioactive Material 3 Feet 6 Feet 9 Teet mR mR mR I r i di= -19 2 C1 15.25 6.8 Iodine-131 25 6.25 2.8 E. Safety through Shielding-Ce:tain materials are effective chie36s agr. inst radiation. The half-layer l value is the amount of shield necessary to reduce i the radiation :nc-half. ialf-La.v.er value for vcmc cc.nion materials: ,t -- -..i. o a.c.t i v e - : h t.e.. r.i. a l-Le : d.. S.te..el Concrete .ad.-. i Ctbal -60 C'. 4 5 " 0.87" 5.0" O.6E" 2.1" Ce r i um-137 0. ; i ". 2.,1 c.:.... ~ e...>. c... e,. O.seu 1.oe -~ ~

O ( 0 ~ Saf ety Thrciugh St'af Midb--Thi sa f etv. of an ' individual:- C. may be gained by contro11in the amount of time he w is exposed to radiation. If exposure attains an unsafe limit, personnel shoulc be rotated.

21.

Health Physics Regarding Actual Field studies. .ir._tia:1cn or..ork anc. . n A. h.onitoring Jo.n Site _me: ore on Completion to assure no Cent.2n.ination Left at the k' ell Site 1. Using a low level survey meter, and before work Initiation, monstor'the area. r.ecorc. t.ne observations on a sketch of the area. 2. Certify the area cican before commencina the 3Ob. E. Handlin: Ecuiement-The followine items shall be worn at all u.ne unen nand...11 n g nne rr.closctave material while health physics problems are present: 1. G1cres* 2. F a c e m a r~r. s *

• 3.

Han:12.::g Tcng s' 4. Prc tec tive cl ot.l.i ng

• C.

Poc%ct Losimeters can be worn by personnel who are handling the radicactive v.a' rials. If, howev er, personnel aisc carr.v. pers<na: :: 11 acc.es, t.ne oction l. is precent as to unether the .i e t d e s ir.:.t er be worn. The edvantage to the pocke de.u u,: :: is direct rcading, and if :he radiation level i ::. r.ot a:ce s r i ve (Generally 1 to IC :Ci. of I o d i n e - 1 3 1 w i :' '. i.e handit-d per injection), then ii uh uld be *he ep'icn of :b field ca fecy of ficer is to h.eth t: poc. a des:- : .r 'r e worn. ~ . ril 17,g rc,di r. :c t ive I r. c q i., e :.:,- w1,1 c., } y.,,y s, b.y win ' - 'r ' i ty o f cor.t.:mir.a ti on

• Ori;I5,

.:.. r t- ' e !. * * *. g t '*. r. IadiobrtiVL .athr.al. 0 ..~ l'

• . '. Y 4.

.. Face masks shal'_ be worn at all - ne when a gaseous racioactive material is Deing usec. 2. : e l a. study. O.ne . 1: ~ face mask shall be a tvoe approved by .he National Bureau o:. Mines anc shoul o. contain an excel',ent organic r12ter 89ent. . ;...r

.c. 2i..;'.

.ma D. Filn. Ladc.es-It will be mandator.v for all b.ersonnel working in the restricted area (an area greater than 2 mR/hr) to wear a film badge. ... =.. IV. Tracer Packaging

• All oackaces received f rom the secoliers containinc racaoactive materials snail.ne monitorec prior to t.oelr leaving their facilities.

The 6c%ge limits shall comply to t.ne DOT s a : n..o i n ~3 regu ations wn:cn are a ma:cmum o, 200 mRfnr at the surf ace of a shipping container and a maximum of 10 mR/hr at a distance of one meter from the surface of the container. V. Handline. and Field Ecui.nment Check List The s;ecific a.c.clication vill :eculre additional radiation detection ecuipment than that listed below, but, generally the field (-cu i p ment will consist of the following,Fi t en.s : -First aid hit -Fim-v:ipes (industrial type) -s.nonc.es -La r c. e and c:.a ll o. c '.v. ethv. l ene stor a c. e bac. s f or ~ containing contaminated equipn.ent, sponges, e t c "..... ~ -Prot.ective ciething -nc r eme te 1.andl ing tongs -::a z i :.nc anc p;astic e w e t. r i ca,2

a.ne

.not:2es -?..astic wasn -hubber gloves -Labels for the return of radicacti. e.wa ste -30simeter and charger -F5.1:. had ge s -C.,nzent ra t ed w<.r.h colution. -Lew Lcve1 surve;ic meter (o* - 50~Ar[.'r'! . #,/ e b f r.

L 4 Operating Proeecures %.=~.f. =..v =.. ..~..... a..R o r;:,. VI. .e...... Pre-job knowledge and planning-the Radiological . - ~....' ',.: ~, := A. Fafety Supervisor must know: 1. Types of radiation involved. 2. Intensity o:. raciation. 3. Relative hazard of each type of radiation. 4. h'n a t the "stav time" (ma>:imum allowable e>:cesure t:.. .me 1s. 5. Knat the possible contamiration problems arc. 6. Any internal contamination problems. 7. i,,.na t incustr1a,. nuisance removac.te conta:n na-tion vill create. E. VTna t controls must be dictated to protect personnel. 9. Plan methods for controlling access to rac1ographic area. ne incivicual Specir:c procecures w111 vary witn t. E. .ich ar..oli ca ticns. In cenern!, the followinc Orc- - ~ cedures. should be f011cwed: 1. Plan the job in advc.nc2. Monitor the area and mcarure the backg:cund 2. radiation level. Optimum r.i>:ing location thould be selected. 3. Radioactive material sheuld be mi>:ed with iniection fluid as close to well head as ecEsible. 4. befine the area which is p:chibited to unau-horized per sonnel. .(2 mr/hr is the ma>:i num alicwnble radiation t o pt-nple not wearing fil ': s:5::Qs). I u'p 3 5. Vi; : 3dic.het;VC mai.e:lal wit.a :njeCt10n w A i *. ';. f r. : - 1 a l c C n E l c L-r b t i C ;. 91VQn to SplaSHin9s Vihd,l'. D d i t i o n s, hnd any Other out%20e in!iuenCe /hi ;; could interre:c wi-- the safe handling or . =. c. E.- 1.

• .i

?1d ; ! Or ;al'her C 3 C/.* ? F 70C2C De k-! r n a t a3, L'h i 'a O '-ndling ' h eli ! ' t i v C' mcLUrials. II* .t i n.1 *.* r 1 W i 27 is E u f f 5 C i ~4 t i o Cv i.M .~ l *.; W i n c, -e e s O Control No.

7. o 59 @

1 .- p._. J ::.

a (<. c Ex.oo sure time"s. b.. uld.~.b.e. :' control ~ led. If e x o. c su r e ". '.1-:.-. ~ ' * ~ " ~' 7. ~ ac.oroaches the maximum.u. e r ni ssible limit >. per-sonnel should'be fotated.' E. Allow no' eating, smoking, or drinking in the restricted area. 9. Followino the comoletion of the ooeration, the entire ar"ea shou 3c..ce monitorec. 10. Radioactive Contamination Inspection Data Sheet 2. ,112ec out anc c:.ven to cus omer. snou.ac be . t.

.**., t. ;.

V:I. Emergency Procedures Emergencies vary creatly in their respective hazards. . Sometimes these emergencies are in'the form-of spills, fires or exolosions which consecuentiv, result in the spread or. racloactive contaminat.on. Emergency proce-dures contained in the National Bureau of Standards, Handbook !!o. 4Er are civen_here as a guide. It must be-recognized t.nat. s..ese procedures are general and any snec1fic cmercencv wou.c certa 1n.3v i nv o,. ve a c c i t i on a,_. procecures ..ot spec 1:1 cal.ly coverec i n t..nis outline. 1. Spills..nvolving no raciation.r.a n a r c to personne,: a. 1;otif.v all.oerso. nei i r. :Se area at once. only a minimum nta.:,er of personnel ^ in b. Permit the vicinity of the spill. Confine the spill immediately.' c. d. I;otify th: Radiation Prote etion Officer. - e. Der ntaminatc. f. "c-r. ; ;. all pe sor.nel in.c'ved in the spill

a.. c: caning.

c.,

Pera.it ac person to re: - work in the area until 1: har been surveyed und -pp;cred by one of the app:eved individual nst.~ -.~*-i.fied on the U.S. ICC ar.d/ur 1 gret: ment State Rai!c.ictive Material License. -,-m a

( s 2. Spills involving radiation har.ard to personnel: ~ 5 5' ~ Notify all' pei'sonnel riot involved in the' spill a. to vacate the area at once. . :.. e s o. l.,.1 1 s 3_2 c.u 2 c anc t.ne banc.s are .c. 2 pr;.e::ed, right the container. c. If the spill is on the skin, flush thoroughlv.a discard outer d. If the s. nill is on.the.c1cthine,.. ~ or protective clothino at once. e. Switch off all fans. Vacata the room. ~ f. Notify the Radiation Prctection Officer as soon as persicae.

c..

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u. .ermit no.perron to resume work in the area i. the until a suivev. is made and ac..croval of. E a c..: ol or. a. ca2. Safer.v. 0:..12cer 2s securec. T r e.c.a r e a c cmo. l et e h i s t e : v. of the accident, s -.q c. r...;...*C,e 7. " V, .U " o C e C " e. e. _.3 ,.J...- Ac..J.1e A 4 . o' 's i o n s a u* ~.'.*.* ~ # ~ ~. b .m... f,

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.~ C C ?. 2 : 2. T e" ' J. ; * ..O person 'nVCivrc in a 76clation inj i:Ty tC WCrh Wi'.Isout the approval of the l e t'; r ". iC %.q s e : C. 6 *. 's. q. x. p. 1. .t~~ all r;sC'.nt.:On ..ct'..'. n t s (k'Ound S, o v 'S r ..t Q.

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n j e. P:epare a ccmp2ete hintcry cf the accident and give the details in the Dae:gency Procedures Report. Fire and other m'[o[A[r.ergencies: ~ -'T'- 4. a ~2-: i ' '- a. Notify all per sonnel in the area at once. h. A t t ' m. t to put out all fir es if radiation hazard is not immediately present. ,; c... y. . > = .m_ - c. r.n,. ...... u.. .s u 6. Notify the Radiological Caf5ty Officer. ~ c. Govern the fire fighting or other emercenc1-- activity by the restrictions of the Radiological Safety Officer. f-. Follo, ring the emergency, monitor the area and determine the emergency devices necessary for safe decontamination. c. _... _. _.. e. =.. .i r ..a.....c. h. Fernit no per son to re sume work without approval cf the Radio 20gical Safety Officer.

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4 Control No. 7650% 4

.r. c.. D Lw.. .c =.., O n, T - ru..,- _.c...<t,.=h,Cv. A. i e 1. Customer: 2. Customer's Supervisor: 3. Comoan.y su.perv1 sor :. - 4. Cause of Emercency: . ~ _ _ _ _ _ _. e E. 30..rce cr i r.o t o.ne : __ _ _ _ -... _ _ _ _ _.. _ _ .oeen sp112ec: g e,l : i. + c to.n r. v e a mtc.oe (curier) i. '....a n t i tv. of r A ,,. g... L a L ..e.~

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n h. An additionel sterage facility of suitable con-struction will be provided for the storage of. empty containers which have contained radioactive _ 2 material's?icint'dmnsted"obj6 cts 'such"ad' fooliB '/(~ @;f D.- ~ rags, clothing, etc.[ This stor' age fccility'shal1: ~ remain locked at all times. Suitable markings vill be placed at the location. 1. Waste Disposal Disposal by release into sanitary sewage systems-a. No licensee shall_ discharge radioactive materials into a sanitary scwace svrtem, unless, it is readily soluble in water and does not exceed the. .PC as specified in 10 CFR or applicable State M regulations. b. Discosal bv burial-no licensee shall dispose of racaoactive mater 2als.y.our al v2.thout a permit-m obtained from the Federal or State authorities.- ~ Dispcsal by incineration-no licensee shal1 dispesc c. c: raa2oactive materialr.c3 means or. incineraticn. c. 1 :. 1: becomes necessarv to als. pose o, anv racio-active' material, contact Gulf Nuclear, Inc. for .aro.ner steos to be taken. 4. Markine.s: a. 53n.bols prescribed by this section.shall use the conventional radiation caution colors (magenta or purple on yellow background). The symbol is the e enve n ti on al three blaied design. b. c r. e of rigns-a sign or signs bearing t.ne raciation c;nbol t.c AU'I I ON.rJ-D : GP..'r '. VE :U.TERI ALS ) shs.ll'be us< i in the following antrances: (..; s.3C;at3on Artis radi oactive mater:a.3 s r.ocms or are.:n whr- .~. e. u, . in are storec. quar,t ir :ec exceeo _ng those t.pec2 fed in 10 CFR or applicabe State re-gulations. (2) Centa;ners in wn.en :.iiinactive material .c d: ornd. a t:1 oac.i ; ve .6 eri al s. . h1O is ! !.~2 7; " ! v ' J ,.hg.

The al'.cuable handling time is determined as the maximum time in minutes ner week that a person - can work with his hands [(rubber gloved) in direct contact with unshielded tracer units. The allowable handling time as indicated on Chart 1 is not additive-that is, you cannot, for example work for 1E minutes with 10 millicuries of Iridium-192 and 42 minutes with an equal amount of ~ Iodine-131 in one week. If several hand bxposures to both types of tracer materials are received during one week, the exposurec must be rationed. If in one calendar week a person directly Example: handler 20 millicuries of Iodine-131 for 3 minutes, 10 millicuries of Iridium-192 for 3 minutes and 15 millicuries of Iodine-131 f or 4 minutes, these exposures are totaled as follows: From the chart the allewable handl3ng time for 20 millicuries of Iodine-131 is 21 minutes. Hence the exposure to the hands fer 20 millicuries of Iodine-131 ir 3 divided by 21, or.143 or the weekly allowable handline time. Similar1v, the exoosure for the 10 millicuries of Iridium-192 is 3 d$ivided by 18, or .167; and that for the 15 millicuries of Iodine-131 is 4, divided by 28, or.143. Adding these three fracticas,.143 +.367 +.143 ecuals.453,'or a ~ little Icts than half the total allowable handling time for that particular calendar week. W}iEN THE VARIOUS EXPOSURES ADD TO A TOTAL OF MORE T}iAN 1.000 THE WrEKLY ALLO'.;AELE liANDLING TIME HAS EEEN EXC}MDED AND THE FOLLOWING WEEK ' S WORK MUST EE LIMI'.~ED ACCORDINGLY. Charts : c. n d 3 indicate th e r a d i a ti on levels that for various amountc of the tracer are p;cr.ent " a ;.c r. a '. s c. t c.n c and - F.: ee b-f rom the u nnhielded t.ra:sr ur1:n. Control W. T659T-

x-Saf et, Troredures for i.ar,di ng F.adioactive Tracers A. T.troduction-In ordc te give pren.er safety consi-deration to the various radicactive materials used, in tracer surveys, the ic13 owing inf ormation shoul.:=. ' - be understood by all field uners. The relatively tracer units allow some low activity levels of the y atituce in..ancline. techn2c.ues suen taat mocerate y saf ety.trecautions are sufficient. The.aj:r safety probicm is the prevention of acc-lation of radioactive material in the body. The activities tv..oically used are from 100 to 10r000 times the tolerable. lim.it for internal accumulatior_ The degree of this particular hazard 6epends on them biological activity of the isotope, its half-life and the r.ature of the tracer pre.caration. E. Handling Procedures-The large variety of tracer .crecarat 2 cn usec, or ava13e., ale :or use, is suen that no dixed procedures can be specified for each. tracer unit. In general though, the majority of tracerr may be handiec :or a :ew minutes without tha use of extension tools. Charts 1, 2 and 3 indica:.e the relat:.ve hazardr of working with various amounts of ten tracer u.aterials. Chari 1.gives the allowable handling time in minu .r.... : 1 &- . c c..ine-3 1,

er.eek :...or varacut amounts o,_

.i 2 "192, Scandit:7.-46 and Eirconium-95. This is based actuu rt asur.c ents r.ade by i uclear Enviror. mental Inc., our tracer suc.olier anc a max:nr Inc. ineerine.,.... a;; ewer.e rac at cr exposure o,_

).C rems per year c

(IE.75

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( i 4 i s for t -N Please remember that tolerances are not meant working levels 'out as maximum safe levels only, and that the obiective should be to obtain a T..nis curing tracer operations. 4 rinimum exrOsure. ve. at rac. 2 cly, ace:m,_ snec oy worxinc 1. can ce carefully, as poss!':1c with the tracer uni.ts and also by distributing the actual direct handling .i of the unshielded materials among as many qualified oeople as cossible.. C. Cont amination Survev. Technic.uer Surveying of Area and Ec.ui-sent e 1. The ideal mixing and injection operation would have no stills-and leave no residue of tracer naterial in any of the vessels or pipes through ^ which the tracer was injected. In practice such an ideal may not be realized, and a survey of the arca is nececsary so that the proper .crocedures nay be follosed to assure that no remaininc contaminant can cause harm to ccmpany personnei, the customer 's personnel, or the

c. en er a l tsubl i c.

i be used with the beta survey neter must '~: e chicid o, en to survey the entire area where r has been 5cnc, and the pipes'and mixit.c a soci c::ed ccmpenents th:cugh which the mix ren3ucted to the well, to be.sure that no was co..c...t ra : l en : 4-mainc that may cauce harm, e th.r by c:..ternal radiarion or by possible cen:c.:r.i na. ien of f ood or wat er supplies. ~ Ct. t.-ina: ion or the probe must be avoided c c:r.pl e tel :. If any contact rurvey is mace, the .rcts is to be t.rotected wit.h a sheet of

aen the object.'. n d pr obe.

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( 2.' >O'c4"", .y,w.6 'a*e C'a w- >A, 2 c. 4. c. ,1 u .yin4ected into the well with the main tracer unit. The' area Of the sp:ll should then be surveved with the pr.Obe a =. rO>:ima t elv. " one inch above the surfaces. .. n v. areas Or : : e:t s O f e c.u ;.C. a e n t wn1Cn incicate . 8,:. _4 G.s,. 1\\74 1, c J v-, c. e.-..,.w. ca... ~.v_ C_ a:. e - c:. 4.ac-u.~ . s. n e.2 con..i.- ew 2 .cC., C..,2, e.. c-3. ;. -D c.. C v.. : was .. ". D O. *:w O., :.: :. U. a c n.: a,. ; O r,.. :

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r( 1. Rubber gloves, shall be worn during decontamination procedures involvinc~ personal contact with the ec.ui.nment. 2. Ford, cigare::s, etc., shall be i.ept outside the cleen-u: arca. Ocantities c f radic active n.aterial which prescnt no harard cutside the body can be very dangercur if the r.ame amount is internal. 3. The wasli' wa't' r 'shal.1 be treated as radicactive e waste. If wash water is discharced into sanitarv sewerage system, the dilution of the activity by the sewerage must be such that the tolerance established for such discesal by the AEC and Agreement States are not exceeded. .,,,a. Since we do not have the capability of assaying the wash water for the ccacentration of contaminant in :r.icrocurier per ::illi2 iter, we must use the of tracer ::aterial actually used on the '.2ob .:unt .:nd I.e average daily water consur.ption at the base I n a e t e rmir.in e. .nat we are not exceecinc. tolerances. .ne wasn water :s cisenarc.ec into a se.ntic tank, 2 :. thcn the surface of the fluid in the septic tank sra,.1 be sur vevec a: t..r . a cn sucn cecemtamina,.icn c.. ration, anc 1:.. -any ac. vity above bae.r.cround is pested wit.na racIntion notec, tne tanr. s..212.:e warning sign alerting everycne concerned of the -ecsi51e hazard. If c i mie r d i <-t o n. a mi n a '. j o n e f ic< r t e -re unsucccr'rful, -J..--,- ' r. - h. : : s te be fe'ic d shall d.epend on the

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f( (s .- r. <e.. ' *E~T- ~ 4. If "the " fixed" cbbtamiriati~on mea sures less than 0.2 mR/hr at one centimeter, the item of equip-ment, article of clothing, etc., can be returned tc ns:- al use. 2. _ :. :ne

.x e c.. cc.ntamina:2cn measure more tw..an C.2 1R/*:r at one centimeter, the item or items in cuestion shall be treated as radioactive vaste anc cirposeo of accoro..inalv 6.

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u a-( (. ~ t .s .. ~ en s Y'. l n+ i / w A s t y r W ', m.u b 4 ? p e ( r / ' -APPEt4 DIX i / r PROCEDO.215'7,0R LOST SOURCE DOIJNHOLE / I t A. Decicion cn F.ecevery of n Source: 5. The Cc.T.psny'c F.cEpontibi35tiet l C. Eecovery or Abandant:.ent of.a Scurce W 9% D. 6 LII".*Tih Q' f r l l 1 Y g. ~, W 4=" a 9 1 1 7

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a ( .z_r.m....v. D This arca is an ex.pansion of part i' c f An..oendix-3.". 2 512 0encinC_.ne cec:slon CL recoVCry o,a source JactorF... A. s... _2. o...- ..,.3, . m.. 4 ,.c. __ _4..a. %.

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4 n. m._. - e.- .co,_ s_.._... s. .t a cCSt ADC'prool-Je U.aximum cost Of recovery. u. drill stem and fishinc. 2. The risk of stickino a tools, especially if all cones of interest are above the tool. 1. Interference of the tool wlth.notential oro- . cu ct :.o.. an c. neepe : cr:111ng. ncu e lor acS1tional,locs. 4. \\,i.,t u e o _, c.: e ari:ag .,n s. 3. Knen a radioactive s c.u r c e ir u s.ociated with stuck 4 a c t. ". e l y _4.".vc P. #. . s., e s_._..... _,. -.... _... m. r.- u........, 3. m c... _ u..,. r. 4.. :,. ...........,.,. c.. 1. F.emain in contact with the client and offer our best ac.vice and reco:renenc.an ons regarcing sa.,.e

1shing procecures.

1. Tai.h ' care to.recogni ze th:- possibility that a

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n ( a dry hcid in simple. 2. 7.b u.d x.cie n t of a_rource : r. a All records, including these of the state agency ril ing. 2ssuing permits for or controlling the c L of oil and gas wells, should contain information regarding the depth', date, type and cuantity of radioactive materials. The well head, if'left above the surf ace, should centain the same in-f rr:r.ation on an engraved 6trable. etal placard. v 1. A source left belew a producing ::ene presents li ttle dif fic-ulty. I r. s.e s t cases the normal cementine of the.croduction strinc. of casine. or tubine will. isola.te.t. h.o sou rce (Ficure 1). If the well is to be produced: from open hole com-pletion, cement should be spotted around and/or above it to prevent the movement of fluids past the capsule and eventual 6estruction of the cap-sule through abrasion (Ficure 2). 4.. In questionable cases the life of the capsule and the solubility of radioactive materials might in- -fluence the acceptance of the proposal. (The Com-

=.nv's source carsules have an estimated life of

..r. uncisturoec salt water. T.ne solu-

n... fears s.s...._:.ty c:. t.ne rac oact ve n.a:.eria,is ir an t.ne o:cer a: unc cart v e r m,_,. : c n o e r w a c k.

5. . : odu ct ion of g ac, wa :.e or oil past a source s n o u 2 :. e.urer.t o_ tec. un.tess the ca.rsu..t e 2s. orc-tectrd from abrasion. Casing or tubing should be adequate. The spott ing of cement, if oratical

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ear r,:c, accs t., tne protection ( r_ a. gure.3).

,... s.+, c.ul d.... o en in :;etting casing past the

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.:c i. ;r.c. - r a.v. survov tun after the caring is below the

c.e will civa arsurance that the tool and source wi2_ :.ct :.i-e r. :: r - n e r t d.nd dam:.g=d at a Io.:er level.

C. In t.he

e. vent a E..arce

.r 1 -f: in a producing zone it should be :.-me n t e d '. p'.nce if persible. Ex-

.rc me cautica e noule..

n -n sace tracking to t. e.:id rcentering the orie - =1 hole and damaging . :. 2 .ource a ntainer W.g. e 4). Normally, the .. : t-ir at e r ne a r t.he 1. - oT. of the tool. If to piece ce;mn t .-re

.~icient cic -

.we m ueI dd, in :icst cases,

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Dw t:*.* t'? r, .ht d r i l li ng Fu d 'i.~a'ill d .t-

U a probably harden in a shor: time to prevent nonreci:ble flow of fluide by the source. In aShi ion, the' separation between the, new and q. origi nal hole would' r. educe the rate ' of' flow at: ">;. '",,: - the to:1 to a very small figure. It is recom-

. ended. hat the new a.nd cid holes be sept. rated h.e a;.eas: 15 feet to r:'e:S ude any possibility c.i d -c. a ;: e tc the source 'ry T err oratine.

A ga:r..a-ray source abandc.nad in a well cannot  :..n c u c e,, racl oactivit.v. in car, oil, water, or other mater. ials.. For. all practical.our.coses .~ th e s ame may be s.. _, 2 curie, 5 curie anc alo o. 20 curie Am3e neutron sources. Although neutron . flux at one foot from a 3 curie, 5 curie or 20 curie source is necli.gible in this respect. For cxample, the flux in a reae cr used to activate a echalt-60 ?ip" tag to I C :ri crocuries is hun-dreds of...illi cas times grca.er that that at one-foot from a 5 curie source. A3though it is not creci r.ely ec-rrect to sa: that there is no activa tion, incucec rad 20activ:t-. wou3d be a.a.m o s t im-r.earurable initially and threagh decay woulc be ic tally obscured by natural background radiz. tion lonc before.the material reached the surface. ,9m.-

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D. Fummary 1. All prc-cauti ons should be taken to avoid rupture . rishina. operat2on. of a rac:cactive source our:nc. ..t.nougn each source.nas r.-^n inolvicually pres-r.re *rried to 25,000,rni, i t. it s m a '.1 and will' not wit.ns:an

n,. i n e i: : 3 3. ;. n c. u or pouncine.

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-cisi on as ' o wh ethe r I

..-.,p. 6 '.st. ' n.'. < :. on ... o., ..3, e. .a the a <. ce: red considere:i r.c for abandoninc any c4wer v.ue tool. A c..c r-c.ain aanes are tne safetv t l

so.ec, the orener el.:ca rd-::,c of the we31 and en-

r. :.c rmn. l on 2 n : n e we ll r e co.:d s.

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_ e s con s l.n a ; V. al. reports it. t.ne Co.- .m u n c.rn a n: I n c. a c. enc 2 e s ~ e .Danv s. ~~. ,, cc 5. It is the client's responsi'oi 3 ity to deal with the State agencies issuing permits for drilling e..,.,

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h ~/Vf cW"6/ SLAY 10184 Mid States Logging and Perforating Co. I License No. 12-19985-01 ATTN: Mr. Donald Gherardini Manager North Route 45 Box 39 Fairfield, Illinois 62837 Gentlemen: This refers to the telephone conversation between Mr. Donald Gherardini and Messrs. W. L. Axelson and D R. Gibbons of my staff on May 9,1984, regarding t the arrangements for an enforcement conference between members of our respec-tive organizations. The meeting is scheduled for 1:00 p.m. (CDT), Friday, May 18, 1984, in the Region III office at 799 Roosevelt Road, Glen Ellyn, . Illinois. The purpose of this meeting is to discuss the findings of the routine inspec-tion ccnducted April 30 through May 2,1984, your corrective actions, and enforcement options available to the NRC. If you have any questions related to this meeting, please contact Mr. Gibbons at (312) 790-5736. Sincerely, k k-J.A. hind, Director Division of Radiological and Materials Safety Programs cc: DMB/ Document Control Desk (RIDS) 3 0 O r i / / n g/ ) 7 (YA I T Y ( J) N fe f F RIII RIII RII h l Gibbons /rr Wie n A hih H 05/10/84 .Sp ff D

1. g.aH44k NUCLEAR REGULATORY COMMisslON UNITED STATES

[- G REGIONIll j 7se noostvELT noAo 'e GLEN ELLYN, ILLINOIS 60137 NOTICE OF SIGNIFICANT LICENSEE MEETING 1 Name of Licensee: Mid States Logging and Perforating Company License No. 12-19985-01 Date and Time of Meeting: May 18, 19Ed. 1:00 p.m. (CDT) ~ Location of Meeting: NRC Region III Office 799 Roosevelt Road Glen Ellyn, Illinois Purpose of Meeting: Tc discuss NRC findings during a recent routine inspec-tion,. licensee's corrective actions, and enforcement options available to the NRC. i Region III Attendees: 4 A. B. Davis, Deputy Regional Administrator J. A. Hind, Director, Division of Radiological and Materials Safety Programs S. H. Lewis, Regional Counsel W. H. Schultz, Enforcement Coordinator W. L. Axelson, Chief, Materials and Safeguards Branch D. G. Wiedeman, Chief, Materials Radiation Protection Section 1 D. R. Gibbons, Radiation Specialist, MRPS 1 B. S. Mallett, Chief, Materials Licensing Section Licensee Attendees: A. J. Pitcher, Owner 1' L. D. Pitcher, Owner Donald Gherardini, Manager j Aaron P. Settles, User, Radiation Safety Officer l NOTE: Attendance by NRC personnel at this Region III licensee meeting should t be made known by 9:00 a.m. (CDT), May 17, 1984, via telephone call to D. R. Gibbons, Region III, FTS 388-5736. Distribution: L. I. Cobb, Chief, Safeguards and Materials Program Branch, IE J. Nelson Grace, Director, Division of Quality Assurance, Safeguards, and Inspection Programs, IE Vandy Miller, Chief, Materials Licensing Branch, NMSS Jane Axelrad, Director, Enforcement Staff, IE James Lieberman, ELD, HQ James G. Keppler, Regional Administrator, Region III A+ 4 ---sr--w 2-r- umw--*o* --s -w--% v v w-- 7-

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6' 8 d JUN 141984 Mid-States Logging & Perforating Co. ATTN: Donald A. Gherardini General Manager Rt. 45 N., Box 39 Fairfield, IL 62283 Gentlemen: Enclosed is Amendment No. 02 to your NRC License (No. 12-19985-01), which authorizes your new places of use at Fairfield and Albion, Illinois; D. Gherardini, E. Beyers, T. Keylon, and S. Daley as authorized users; new source model numbers; and changes in your Radiation Safety Program. Please note the following: 1. As discussed in a telephone conversation between Donald Gherardini of your staff and me on June 1,1984, we have added a condition to your license requiring you to instruct all authorized users in your operating and emergency procedures prior to initiating work and on a refresher basis. 2. We have authorized Steve Daley for the use of sealed sources and not iodine-131 or iridium-192 as unsealed sources. In order to obtain this authorization, you will need to submit documentation of his training and/or experience in the use of these materials for tracer operations. This training should bc under an authorized user listed on an NRC or Agreement State license performing tracer operations and for a duration of at least 3 months. 3. We have not authorized Larry Oliver or Robert Childers as users as requested. In order to obtain this authorization, you will need to submit documentation indicating that their on-the-job trainor, Tony Keylon, was and/or is on an NRC and/or Agreement State License for the use of sealed and unsealed sources in well logging operations. 4. We have not authorized Michael Clayton, Carroll Wiles, or Samuel Vandever as users as requested. In order to obtain this authorization for the use of sealed sources, you will need to submit documentation of their formal training equivalent to that specified in Item 7. of the enclosed guide. In order to obtain this authorization for unsealed sources, you will need to submit documentation of the training each individual has received in the use of the materials'for tracer operations. A7 6 4t 840601 NMS LIC30 11 12-19985-01 PDR T[*

Mid-States Logging & Perforating 2 5. Your May 3, 1984 letter included a request to add cesium-137 as a Gulf Nuclear, Inc. Model No. RL-1 sealed source. We have not authorized this model number, since the NRC and Gulf Nuclear, Inc. do not have such a model number in their registries. However, we have authorized you for a Gulf Nuclear, Inc. Model No. VL-1 based upon the assumption that this is the source desired. 6. We have modifed Condition 14. on your license to prohibit you from removing sealed sources from source holders. If you wish authorization to perform such a service, you will need to submit the information requested in Item 10.2.9.(c) of the enclosed guide. If you have any questions or require clarification on any of the information stated above, you may contact us at (312) 790-5625. Sincerely, Bruce S. Mallett, Ph.D., Chief Materials Licensing Section

Enclosures:

1. Amendment No. 1 2. Guide For Preparation of Applications for Well Logging Operations (pvhf3di Mallett/bm 06/05/84

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REQUEST FOR AMENDMENTS TO MATERIALS LICENSE # 12-19985-01... 'a i-RE D BY LFM8 -Date..).flf d.[d[ Amendment to Condition #2 Rt. 45 N. Box 39, Fairfield, II. 62837 Log. .kIl' / Amendment to Condition #7 By. . 6f Orig. To. .<. /~ A. Sealed Neutron Source (Gulf Nuclear Model 71-1; Mian Compi. (Gammatron Model AN-HP) B. Sealed Source (Gulf Nuclear Model CSV) (Gulf Nuclear Model RL-1) C. Any D. Any Amendment to Condition f 10 Licensed material may be used and stored at Rt. 45 N. Box 39, Fairfield, II., and Rt. 130 N. Albion, II., and used at temporary job sites of the licensee anywhere in the United States where the U.S. Nuclear Regulatory Commission maintains jurisdiction for regulating the use of licensed material. Amendment to Condition # 12 Licensed material shall be used by, or under the supervision and in the physical presence of Aaron.P. Sejtles g, Steve Daley RECEIVED Larry Oliver-Tony Keylon Don Gherardini Ed Beyers MAY 0 71984 Samual Vandever Robert Childers Micheal Clayton Carroll Files REGION III i Yb 7 y '[ kk M b genwnl blo. 12-19905-01 PDR c,s j i

_,._:..www .--..n- .s 1 MI S ~ 8 m ...---~:~ .w 3 Amendment to Supporting Material Mid-States Logging and Perforating Radioactive Mater-ials Storage, Operating and Emergency Procedures Manual. Appendix A Section II The Radiation Saftey Officers Are: Steven Daley Larry Oliver ADDITIONAL SUPPORTING MATERIAL Building in use at present is Rt. 45 N., Fairfield, II. There will be no transport of sources between buildings, as when new location is completed, the entire operation of licensee will be moved to Rt.130 N., Albion, II., and lease on present building will be terminated. A close-out survey will be performed at time o'l re-location and submitted for approval by the Commission. l l l Control No. 76720

Source room concrete block construction with voids in blocks filled with cement. Steel door double locked and access keys controlled by R/A safyy officer. Sources stored inside within D.O.T.7A carriers. Placarded accordingly/ / M' .l f8' pms l .y l l .~ 2 , 0' ' 5' -f i I .? )

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I PART I i.s ACER TECENOLOGY SERVICES, INC. WELL LOGGING RADIATION SAFETY TRAINING (t e d f$ ) NAME N g,t h.i t b. hodcx $b, [khb DATE w l a Circle the T if the statement is true, if false circle the F (1/2 point each) ,l. (f) F A survey meter sha21 be used during any radiation acivity or source manipulations. \\. (f(hHalf-life: the time in which half the atoms in a radio-2 active substance disintegrates.

3. h) F Af ter seven (7) half-lives, you have less than 1% of the radioactivity left.

h) F Radioactivity is the spontaneous disintegration of unstable 4. nuclei with the resulting emission of nuclear radiation. 10 5. @) F 3.7 x 10 disintegration per second is one curie of radioactivity. h)F The unit of quantity of any radioactivity substance is '%- 6. the curie. () A millicurie is one millionth of a curie. ' 7. T

8. lh F The Nuclear Regulatory Commission (NRC) and agreement states specify that survey meters used by loggers measures as high as 20 mR/hr.

9 lh F Survey meters are mandatory on your vehicles while transporting radioactive materials. Q{)Geigercountersarethemostefficientoftheprinciple 10 T types of counters.

11. f?) F HVL is the symbol for half value layer in radiation shielding.

12. $$)F REM is a notation for Roentgen equivalent man.

@j) The genetic ef fects of radiation are well documented 13. T and it is possible to predict such effects with great accuracy.

14. kh F In the formula 5 (n-18), N is the age.

hf F The yearly allowable occupational dose is 5 Rem. 15.

...fi d k3.,.... .., I A s.v. 67.v..y,. (. r... 9 p.;r-S.L.e-to.y . %J e ) Ve f, .a w.9 a i$i'i.L LGGGI::G SA T.TY T Ih'ING - PriRT I Pure 2 rI T F Diological ::>.l f li fe in the amount of time that it takes 16. to excrete c:.e half of a radicsetive aubstance from the body. @ The body will repair all ti.e damage done to it by radiation. 17. T

18. hF The basic philosophy in ar.necsing the public health aspects of radiation exposure can be uxpressed by the following statement:

Any u.n<cessary exposure to radiation should be avoided. ) h For storage of radioactive materials, 19. a sign statinc y " Caution Radioactive 'ca t erials'- must be posted on the storage container and t.he entrance to the storage area room. 20. F " Radioactive" must b<a posted on four(4) sides on all vehicles transporting radioa'ctive materials with " yellow III" labels. h 2 mr/llr. 21. in the i.ading that distir.guishes betwecn a ' restricte 1 area ar.d a nor.-Icstricted area. hF 22. The inverue square law n ans that if the source in twice as far away.2n 'crurr, t.h e intennity is one fourth as great. i

23. @F Time-Distance-Shielding i.re inportant f actors ir. rad ia t. ion safety.

( An acute dose of 750 F.em ik a. lethal dose of radiation. 24.

25. @F Radiation in pres.nt in the.amouphere at all times.

26. T T8 The film hadge is u cd for gar.ma radiation only. hF A TLD badge l' efficient at r.;oni toring neutrons. 27. @F Leak testing of scalrid radioactive sources is required 28. every 180 dayn or six noat hs. h Dyproduct materials are 29. T Tir;ionable. [] F Speci fi c a.-' ivi ty in not.::pt r t... !. t in (:.'rerming the 30. physical size of a neuree of r..d ic..ac t i ve ma teri a l. 4 Control No. 7672I

• PAitT II.

TF ER TECHNOLOGY SERVICES, 2 WELL LOGGERS SAFETY TRAINING NAME _ Mr.jpn - (c_v 'DATE 3c.%. I3 A t ( (#1 thru 14 - 5 points each) (!15 - 10 points) (#16 - 15 points) 1. One curie of Iodine-131 yields L. t. (' R/hr at one foot. One curie of Iridium-192 yields g, 9 R/hr at one foot. One curie of Cesium-137 yields 4, A R/hr at one foot. A three curie AmBe source yields gf mrem at two feet. A five curie AmBe source yields , q g-mrem at two feet. 2. Calculate the radiation from 12 millicuries of Iridium-192. E ,a) at a distance of four(4) feet. n IU E 8 ( - u.

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If,f' .$..,l i3 ! 1-C'1 [x ! 'llq5W Yfr I/ l L ** IfeJE:. 5 t. 9 ~ g'*, r 3 .U 13 !. n. L// 5,& lh ae 4. State the radiation levels indicated by a survey meter when the meter needle points to: 0.12 on the X10 Range /, 2 mR/hr. 0.50 on the X10 Range g. mR/hr. 0.45 on the X1 Range y s mR/hr. 0.20 on the X1 Range , s. o mR/hr. 0.35 on the X100 Range _ gg mR/hr. l

Mt. CER TLCHNOLOGY SEPVICES, INC. $. Dd e. y - WEL'L LOGGE1tS SAF ETY To.INING - PART II PAGE -2 5. Give three requirements placed on the calibration of survey i) pt,.,4 g, s e,d in ~+/u d souy Ln ~fx +o a la s I,ke. &,lf R/u.e.fe sr \\ .2) L t. % 4.. ~ d b s M fd +~"" * ~ '+ d

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TRACER TECHNOLOGY SERVICES, INC. 5 hd.c_y

• WEL1 LOGGERS SAFETY TR NING - PART II I

.Page - 3 10. Define and explain cause for: (a) Radiation sickness k dk M g N h r4 h eg p Ap (b)' Radiation injury /2,,, k (Q uW A'dd - % 4 As e A. W Q w = 8, e k % L K rL A/A M 3

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There exists in the transportation of radioactive materials a terminology called a " transport index" (TI). Explain what this is. k~k ~ m, //,' = A% y% 13. What information should appear on job site monitoring sheet? y,,.e a 1.y s m. - eer-p* ,,, V.1 a L n u m L er-f -f c & f, .s. ~ r.v ~ ~ L e r-he [,'g L lo ad. ~ Y\\ S,ul.y $,4, ~ a nr-vey d r-14. Certain records must be inaintained for inspectors f rom the licensing agencies. List thrase records. ichlad.. /~.s4r /A-+

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[ l Control No. 76720

TRACER TECHNOLOGY SERVICES, INC. g, hi(c y WE5L LOGGERS SM'ETY TJ .HING - PSRT II '[ l Page 4 C 15. In your own words, (a) what procedure would you follow in ~ consolidating several partially filled cans of sand into one larger can; and (b) How would you determine the millicuries in the can; and (c ) -Host would you indicate this on your utilization / master log? A).rnsed.ry den.IiL% :p fr.c.ed R ,) m i x m ~ 5 d. p.A. J. + u d *= 4+ - > ^ * * * '"^ #^ ' a) +d<e. 6.e y..md -g,-.4 ~. - A 'to ' (,, ~ A /4 - M-i / s) 41 -. tI, t~,-..s. Ay u, y, w.,3 m d, ?,. r,,.,e,- J e. s p,. m I.s u t!I t m e 4 ';& m A,. p q s a s + a / ' 'l) M h~r+ La.sk p 4 M ee.,nfh a d ay 3 c) %. Lo C F er..~ r, sda. ~ Ad n a ~ sk ~ ws *- d yw l y

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G~s \\a 1(MH6.gr8p&T A:T.wES l o g g. g a_ gftp. =srforat..... .u .,wc u in spg 3 Donald Gherardini: Three years field experience as senior engineer with' Burgener Services in Olney, Il. Responsible for source handling in respect to well logging and RA tracer surveys. Experience includes handling of CS 137, AmBe 241, Iridium 192, and field experience in fishing for tools lost in hole. Attended safety classes in'structed by Hubert Rennert, and personally instructed by him in the field. Previously employed by Dresser Atlas and completed course of instruction for RA source handling for operators written by Dresser Atlas Company, supervised and counseled by Company Radiation Safety Officer and company engineers. Ed Beyers: Three years field experience as senior engineer with Burgener Services in Olney, Il. Supervised handling of sources and other RA materials used in well logging and tracer surveys, including CS 137 and AmBe 241 logging sources and Iridium 192. Experience includes overseeing of fishing operations for tools lost in open hole. Attended well logging course and RA safety course in-structed by Hubert Rennert. Was also under Mr. Rennert's personal supervision during training period. Steven Daley: Three years experience with Woodell Logging in Mattoon, II. Supervised the handling of CS 137 and AmBe 241 in mineral and oil well logging. Successfully completed Rad-iation Safety course instructed by John Hamley of Tracer l Technology Services, Inc., Fort Worth, Tx., after.one year-experience at Hooddell Logging. l Administered leak wipe tests in compliance with NRC l regulations. Was trained by Dennis Fathauer, Radiation l Safety Officer, to be able to deal with any necessary proct.dures in handling radioactive materials. l l k l ) l Rn'ita d4 N

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• Fairfielrl 11 A7837
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.t: 4% ,il ..gg-.. rating 3 I i ) SSy: 412-19-569I+ D03: 8 25-58 l DOE: 6183 i Tony Alan Keylon Rt. 1 Mountain Springs, Ky. ~ Employed by Basin Surveys, Inc., trained by C.M. Bower, Marshall Mic!csan, and Fred Staggs. 5 years of on the lob training in handling of CS 137, hbe-241, and Iodine-131. Including monthly safat,y meetings with classroom type instruction. Gulf buclear. Inc. Radiation Safety training course was successfally com.nleted on April 14, 1932. Instructed by Frank Malok. Have received Kentucky License for 1." McCullough-Easin Surveys Shop in Paintsville, Ky. with reself as orimary Radiation Safety Officer. Mid States Logging G Perforatin;; by Aaron Settics. 4 months of on the job training in handling of CS 137 and k:be-241. Certificate included i l l l 1 i 1 l i l I l ( j Route 45 N

• Box 39
• Fairfield, il 62837
• Phone: 618-842-9156 l

.~o = .. m u.r> g b ' V-J , ~.-~.. Tony A.. Ke lott - ~~.- - - u n -- w,-... f 3. u-.w.... J..../ 1/ n.ul >?l&J 1 l T Control No. 76720

( ,j ( viD-ST"E3 N. A'1 ST M E B%. &p,e... fora.e.. a.."i;ES . f,b ~1 us ll lo.,.g. sng ~.. r ting g y SS7: 407-%-1471 D03 6-25 60 DOE 1-16 84 Larry Dean Oliver Rt. 1 Mountain Springs, Ky. Employed by Basin Surveys, Inc. Trained by Tony Keylon. 1 Year on the job C -137, Ambe-241, and Iodine-131 Including monthly training in handling of S safety meetings with classroon type instruction. Gulf 'suelear, Inc. Radiation S'.foty Training course was successfully completed on Septer.ber 1,1932. Instructed by Frank Malek. Certificate included l l l 1 l L J Route 45 N

• Box 39
• Fairfie!d, il 62837
• Phone: 618-842-9156

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s3h 337-28-5533 Dos: 7-7-36 Carroll Ray viiles Rt. 1 Mountain Springs, Ky. p> F Employed by Basin Surveys, Inc. Trained by. Mike Dinsmore.t,On the job trainir. in handling of CS-137, Asbe S1, arti Iodine-131. Mid States Logging and Perforating; Trained by Aaron Settles. On the job training in har.dling of CS 137, Ambo 31. l l l l I l l t Control NO-YO72 Route 45 N

• Box 39
• Fairfield. Il 62837
• Phone: 618-842 9156

i 1 MRD;$.5S%tFji.wES rn rers F.~.I igm 32 5 h n.., J C.2. + u 5 *.r.- 1999199._ 9-_ gra (pg pa SSf: 411-70 8919 DOS: 2 18 43 DOE: 4-16 83 '41111am Samuel Vandover Rt. 1 Mountain Springs, Ky. Daployed by Ensin Surveys, Inc. Trained by Tony Keylon. 4}yearsofonthe job training in -handling of CS-137, Ambe 241, and Iodine-131 including monthly safety :r.eetings with classroom type instruction. Mid Statos Logging & Forforating, trained by Aaron Settles. 1 year of on the job training in handling of CS-137 r.nd.bbo-241. I 1 l l I Control No. 76720' ) Route 45 N

• Box 39
• Fairfield, il 62837
• Phone: 618-842-9156

.w ' r..!D 3T 3 ~ IT NE! > El fMHDRS T,_ M E E S 1 .,$[#sggTFpe,rfo; rating 4 en a z..w j 99 SSf: 335-56 4242 DOB: 7-16-57 DOS: 7-28 S2 Michael Lee Clayton St. 3 Box 434 Stanton, Ky. 40330 Fooloyad by Basin Surveys Inc. Trained by Mike Dinsmore 6 months of on the job training in hardling of CJ 137 and Anbo 241 ~ Mid States Logging and Perforating: 2 years of on the job training in handling of CS 137 and Ambe 241 by Asron 3ettles. Illini by Bill Dent: 4 months of on the job t*aining in handling of CS-137 and ArPa-241. l l l L- ) Route 45 N

• Box 39
• Fairfield, ll 62837
• Phone: 618-842-9156

t1 .4 .n,n 3- -r<- s.V W f 1 M I D ?:. Q~Q S24 O Cht. -TS T w.f .... =. in xa t. l IOQQ}QQ' 3 ing SSf: 402- % -3353 Dos: 6-19 60 doe: 1-16 84 Robert Earl Childers Rt. 1 Mountain Springs, Ky. Employed by dasin Surveys, Inc. Trained by Tony Keylon. 1 year on the job training in handling of C3 137, Ambe 241, and Iodine 131. Including monthly Safety meetins;s with classroom type training. tontrol No. '7 6 7 2 6 Route 45 N

• Box 39
• Fairfield, il 62837
• Phone: 618-842-9156

. PMID,g,S, TATES Q lo,.. e.gging & perfdraiting u 3 Amendment to Supporting Material Mid-States Lcpging and Perforating Radioactive Materials Storage, Operating and Emergency Procedures Manual. Appendix A Section I The Radiation Protection Officer is: Aaron Settles Appendix A Section II The Radiation Safety Officers are: Steven Deley Larry Oliver Appendix B Section I Paragraph C Receiving of Radioactive Material by designated persons reporting to the Radiation Safety Officer, who shall perforc inspection of said material and docureniation, then material to be placed in storage facility until needed. Unsealed sources shal] remain in shipping container, inside storage facility, until required. Appendix C Section I All tracer material preparations will be made in the field, where inmediate use of the material will be made. Precautions will be taken in the handling of natorial, according to Section III of this part and to manufacturer's recommendations concerning loading of injection tools, if such tools are used. k J Route 45 N

• Box 39
• Fairfield, il 62837
• Phone: 618-842-9156

% 730

~ d / 1 .rN MI6 ESTATES 00 rig & perfdrating Jo lo. i T Appendix C Section III Paragraph D Equipment for field preparation of Radioactive Material for tracer studies shall include a plastic tray lined with an absorbant material, whereby the handling of all liquid Radioactive Material shall be done in such a manner that if any spills should occur they shall be contained. ADDITIONAL SUPPORTING MMTRIAL Building in use at present is Rt. 45 N., Fairfield, II. There will be no transport of sources between buildings, as when new location is completed, the entire operation of licensee will be mcVed to Rt. 130 N., Albion, II., and lease on present building will be terminated. A close-out survey will be performed at time of relocation and submitted for approval by the Comt.ission. I hereby testify that these procedures will be followed accordingly, and that supporting material is, to the best of my knowledge, correct. I then request that these anendments to Materials License number 12-19985-01 in the name of Mid -States Logging & Perforating Co. be ratified. Respectfully submitted, / wk lY b N* ~ Donald A. Gherardini General Manager Q J Route 45 N

• Box 39
• Fairfield, il 62837
• Phone: 618-842-9156

) ! go.sg Y,' ' qMig~^~._-=y S _.i-- n n -a-- ~ 3 Carroll Ray Wiles Rt. 1 Mountain Springs, KY SS#: 337-28-5533 DOB: 7-7-36 c Employed by Basin Surveys, Inc., Trained by Mike Dinsmore. On the job training in handling of CS-137, AMBE-241, and Iodine-131. Employed 2 years. Mid-States Logging and Perforating: Trained by Aaron Settles. On the job training in handling of CS-137, AMBE-241. Employed 1 years. t s l L J Route 45 N

• Box 39
• Fairfield, 1162837
• Phone: 618-842-9156

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