ML20128H082
| ML20128H082 | |
| Person / Time | |
|---|---|
| Issue date: | 09/20/1996 |
| From: | Wiggins E NRC OFFICE OF ADMINISTRATION (ADM) |
| To: | Pryor P PENNSYLVANIA, COMMONWEALTH OF |
| References | |
| CON-FIN-D-2319, CON-NRC-10-96-162 NUDOCS 9610090233 | |
| Download: ML20128H082 (66) | |
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M lt UNITED STATES
.y-j
- j NUCLEAR REGULATORY COMMISSION o
.t WASHINGTON. D.C. 20555 0001
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U.S. Public Health' Service ATTN:
Paul Pryor, M.S., C.I.H.
Division of Federal Occupational Health P.O. Box 13716 3535 Market Street Philadelphia. Pennsylvania 19104
SUBJECT:
INTERAGENCY AGREEMENT NO NRC-10-96-162 ENTITLED
" INDUSTRIAL HYGIENE FOR HEADQUARTERS AND OTHER LOCAL NRC BUILDINGS"
Dear Mr. Pryor:
Pursuant to the Economy Act of 1932. as amended (31 USC 1535), the Nuclear Regulatory Commission (NRC) and the U.S. Public Health Services (PHS).
Division of Federal Occupativnal Health (DF0H) desire to enter into an agreement whereby PHS. DF0H will provide occuptational health program consultation and technical assistance services to the NRC.
Accordingly, upon your agreement as provided below. the terms and conditions of this Interagency Agreement are as follows:
Article I - Statement of Work BACKGROUND:
The Occupational Safety and Health Act of 1970 established requirements for the development and implementation of safety and health programs in both the Federal Government and private sector.
The requirements of this law that pertains to Federal employees were further amplified by Executive Order 12196 of February 26. 1980.
In this Executive Order. the President stated explicitly that Federal employees are to be afforded the same safety. health, and indoor air quality (IAQ) protection as employees in the private sector.
As a result. Title 29 of the Code of Federal Regulations. Part 12960. " Basic Program Elements for Federal Employee Occupational Safety and Health Programs" was promulgated to fulfill this requirement (CFR - Labor 29 Parts 1900 to 1910. Revised as of 7/1/94).
The U.S. Nuclear Regulatory Commission (NRC) has received complaints from g
employees regarding poor IAQ and other forms of physical discomfort that are either actual or perceived as being associated with their immediate
. environment.
Since NRC does not have an industrial hygeniest on staff..an investigation and/or a remedy regarding any discomforts experienced by employees cannot be resolved. therefore scientific capability is required to
{g determine the existence. extent or source of these hazards and/or discomforts.
In addition, the scheduling of periodic inspections will assist the NRC in monitoring the working environment.
Furthermore. NRC requires emergency response service. e.g. analyzing chemical spills.
9610090233 960920 PDR CONTR NRC-10-96-162 PDR
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' OBJECTIVE.
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The objective of this Interagency Agreement is to obtain occupational health program consultation and technical assistance services in establishing the NRC's Occupational Health and Safety Program, which provides the capability for health hazard recognition and evaluation. and recommendations for i
controlling or eliminating those identified health hazards.
In addition. this Agreement shall. ensure compliance with safety and health regulations l
applicable to Federal. State, and local regulations.
a Specific services will be requested through the issuance of individual work l
orders by the NRC Project Officer or alternate Project Officers identified under Article IX of this Agreement, through the DF0H representative.
j TECHNICAL AND OTHER SPECIAL QUALIFICATIONS REQUIRED:
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PHS, DF0H. upon request. shall provide an industrial hygienist (s), who is certified by a nationally recognized certification board such as the American Board of Industrial Hygiene.
A copy of the industrial hygeniest(s) certification shall be available for review by the NRC.
In addition. DF0H shall provide all necessary support services to perform on-i site inspections. sample gathering, sample analysis and subsequent evaluation services using contractor-supplied equipment for the purpose of identifying i
occupational health hazards.
Therefore. DF0H shall provide all technical l
support to include sampling equipment. laboratory services. and administrative
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support services.
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WORK REQUIREMENTS:
Scone of Work The specific tasks under this requirement may include any combination of, but not limited to, the followir.g:
Task 1:
Air Quality Tests DF0H shall conduct air sampling tests and evaluations in order to determine if l
l the environment is hazardous to an employee's health.
Tests performed shall include:
(1) volatile organic compounds (VOC). (2) relative humidity.
l (3) respirable (nuisance) dusts. (4) CO. (5) CO 2. and (6) formaldehyde.
l In addition, screening tests shall be conducted for possible microbial contamination caused by the heating, ventilation and air-conditioning (HVAC) i systems in the building.
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Task 2: Adequacy of Air Flow DF0H shall determine the adequacy of air flow produced by the HVAC systems where NRC employees work.
Determine the ratio of outside air to recirculated air and compare to acceptable levels.
The results of the testing will determine if the HVAC systems have been properly balanced.
NOTE:
The One White Flint BJilding is pending re-balancing after GSA HVAC improvements.
Task 3:
Humidity and Temper ature Readings DF0H shall take humidity and temperature readings throughout the workspace and compare to the acceptable levels, if not acceptable, provide recommendations for corrective actions.
Task 4:
Lead Testing or Bacteria Contamination in the Drinking Water DF0H shall determine the levels of any lead and bacteria in the drinking water systems to ascertain if water is in compliance with accepted EPA standards.
Potential Survey Areas:
Potential survey areas are, but not limited to the following:
1.
Open and partitioned office spaces 2.
Computer rooms 3.
Word processing facilities 4.
Mechanical rooms and systems 5.
Electrical rooms and closets 6.
NRC Daycare Center 7.
Cafeteria facilities 8.
Garage areas 9.
Fresh air intakes
- 10. Public accommodation areas
- 11. Industrial print shop
- 12. Mail room facility
- 13. Smoking lounge
- 14. Warehouses
- 15. Driniking Water Systems Locations and Facilities To Be Surveyed:
Surveys shall be performed for all NRC occupied headquarters buildings in the Washington. DC Metropolitan area listed below:
Current locations One White Flint North Building Two White Flint North Building 11555 Rockville Pike 11545 Rockville Pike Rockville. Maryland 20852 Rockville. Maryland 20852
U.S. Public Health 3ervices 4
Current location (cont'd) l NRC Warehouse.
Gelman Building (PDR) 5000 Boiling Brook Parkway 2120 L Street. NW Rockville Maryland 20852 Washington, DC l
l WORK ORDER PROCUDURES a.
Request for Cost Proposal for Work Orders Individual orders will be issued for specific services required by the NRC in accordance with the terms and conditions of thi.s Agreement.
The NRC Project Officer or alternate Project Officer as identified in this Agreement will transmit to the Government agency a Work Order Request for Cost Proposal which will include the following:
(1) Date of Request (2) Due date of cost proposal (3) Type of service requested (4) Reporting Requirements (5) Period of Performance and Place of Performance (6) NRC contacts: contractual and technical b.
Work Order Proposal By the date specified in the Work Order Request for Proposal. DF0H shall submit to the NRC Project Officer a written estimate of cost for the required services The cost estimate shall include the following:
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(1)
Identify the professional personnel and the number of hours that will be committed to complete the work on the work order.
(2)
Identify support personnel that are needed to assist the professional personnel in completing work on the work order.
I (3) Outline specific work protocol (s) planned to accom31ish the NRC's work order request (air quality testing, lead and 3acteria contamination testing in the drinking water, etc.)
The proposed costs shall be in accordance with the attached rate schedules for labor and laboratory fees (See Attachments B and C. respectively).
The cost estimate must be approved, and a written work order signed / approved by the NRC Project Officer or Alterate Project Officers prior to commencing work.
l The NRC Project Officer or Technical Representative identified in each individual work order may provide technical guidance within the scope of l
this Agreement.
The NRC Project Officer or Technical Representative does not have the authority to change terms or conditions of the agreement or in any way cause an increase or decrease in the total Agreement amount.
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Work Order Award DF0H shall perform the work described in the definitized Work Orders i
Work Orders issued by the NRC Project Officer or his alternate.
Definitized Work Orders-will include the following:
(1) Statement of required services / Meetings / Travel and Deliverables (2) Period of Performance (3)
Identify personnel to perform the work (4) Work Order Amount DF0H may not exceed the approved cost estimate without written approval from the NRC Project Officer or his alternate.
d.
Accelerated Work Order Procedures When a work order request is declared an " emergency", the NRC will give DF0H a verbal description of the task to be performed. and request a cost estimate.
Upon approval of the cost estimate by the NRC Project Officer, the Government agency under this Agreement shall proceed with 3erformance of the required task.
This verbal agreement will be followed
]y a definitized work order, e.
Response Time Requirements for Work Orders For non-emergency testing, on-site response time shall be within 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> after NRC's written approval to comrence work.
For emergency testing. on-site response time shall be one (1) hour upon verbal authorization by the NRC Project Officer or his alternate.
For emergency calls. the NRC may request DF0H to furnish verbal findings.
results and recommendations prior to their written report.
Classification of " emergencies" will be made by the NRC Project Officer.
Article II - Meetinas and Travel At least once per month. DF0H will be required to attend meetings at NRC Headquarters in Rockville. Maryland to provide briefings to NRC management and employees regarding DF0H's findings and recommendations for correcting the reported health hazards.
Article III - NRC Furnished Material No material will be furnished by the NRC.
Article IV - Deliverables Technical Reports A complete analysis of the results of the investigation as well as the conclusions and recommendations to correct all unhealthful conditions shall be submitted in a draft and final report.
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j Technical Renorts (cont'd)
The draft and final report shall evaluate the findings against Federal and accepted industry standards.
This report shall include appropriate tables and charts to present information in a clear and concise manner and floor plans depicting sampling locations.
The DHOF representative signing the report and the laboratory i
performing the. test analysis shall be certified by the American j
Industrial Hygiene Association or an equal organization.
l As requested. DF0H shall provide briefings a NRC management and employees of i
their findings and recommendations.
j One copy of the draft report shall be submitted by DSF0H to the sources listed below within ten (10) workdays after completion of the job test.,
NRC will review the draft report and provide comments to DF0H within ten (10)
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workdays after receipt of the report.
i The final report shall be provided within five (5) workdays from receipt of NRC's comments. The final report shall incorporate all of i
1 NRC's comments.
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If mutually agreed upon, adjustments may be made to the above delivery i
schedule and as stated in individual work orders.
J Fiscal Trackina Screadsheet i
DF0H shall submit a Fiscal Tracking Spreadsheet on a quarterly basis to the NRC Project Officer and Contracting Officer.
The spreadsheet provides billing information per individual task order. Since this is a DF0H generated document, no guidelines for preparing this document are given.
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PLACE OF DEllVERY--REPORTS / FISCAL TRACKING SPREADSHEET All reports to be furnished under this Agreement shall be delivered to:
(a) Project Officer (3 copies) i U.S. Nuclear Regulatory Commission j
ATTN:
Dennis Tarner i
Mail Stop 0-2 B7 Washington. DC 20555 (b) NRC Health and Safety Manager (2 copies) j U.S. Nuclear Regulatory Commission i
ATTN:
Randy Brown Mail Stop T-3 A2 Washington. DC P0555 s
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(c) NRC Contracting Officer'(1 copy) l l
.U.S. Nuclear Regulatory Commission l
ATTN:
Elois Wiggins l
Mail Stop T-712 Washington. DC 20555 Article V - Level of Effort and Period of Performance This Interagency Agreement shall commence on the date of execution of this i
Agreement and end one year thereafter. with four additional one year options.
The Scope of Work set forth in Article I. and the period of performance may be increased as mutually agreed upon by both parties.
Any changes shall be incorporated into this Agreement by the issuance of a negotiated modification by the NRC Contracting Of ficer.
The NRC has the right to terminate this Agreement upon the issuance of a 60 day written notice.
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Article VI - Option to Extend Services The NRC Contracting Officer, by issuance of a negotiated modification to this l
agreement. may exercise an option in accordance with Article I - Scope of Work, at the estimated cost set forth in Article VIII - Estimated Amount.
Article VII - Payment Payment will be made on a reimbursable basis.
DF0H shall submit invoices / vouchers in accordance with Attachment A. " Billing Instructions for Interagency Agreements." upon completion of each work order.
PHS DF0H will be reimbursed for labor (consultation, technical assistance.
sample collection) and laboratory sampling for each specific work order i
ap3 roved by the NRC Project Officer, in accordance with the attached rate L
scledules.
The schedule for labor rates and laboratory fees are attached to this Agreement as Attachments B and C. respectively.
In addition, the Government agency will be reimbursed for any travel and related expenses for each specific work order.
These charges shall be included in the Government agency's cost proposal.
Requests for payment MUST cite the following accounting data:
B&R No.
640-15-32-20-25 FIN:
D2319 BOC:
252A APPN No.
X0200 i
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Article Vlli - Fstimated Amount The total estimated amount of this Agreement for the one year period of performance is $35,000.00.
The estimated amount for each option year is given below:
Option Year 1 - $35.500.00 Option Year 2 - $24,150.00 Option Year 3 - $26.000.00 Option Year 4 - $27.500.00 Article IX - Oblication of Funds The amount presently obligated with respect to this Agreement is $23.000.00.
This obligation amount may be unilaterally increased from time to time by the i
NRC Contracting Officer by written modification to this Agreement.
Article X - Financial Status Report DF0H shall provide a quarterly Financial Status Report to the NRC Project l
Officer and the Contracting Officer.
The report is due within 15 calendar days after the end of the report period and shall identify the title of the project, the contract number, job code, project manager and/or principal investiagor. the contract period of aerformance, and the period covered by the i
report.
Each report shall include t1e following for each discrete task-I a.
Provide total estimated cost (value) of the project as reflected in the contract, the amount of funds available in the contract to date, and the balance of funds rquired to complete the work as follows:
(1) Total Estimated Contract Amount (2) Total Funds Obligated to Date (3) Total Costs Incurred this Reporting Period (4) Total Costs Incurred to Date (5) Balance of Obligations Remaining (6) Balance of Funds Required to Complete Contract b.
Detail of all direct and indirect costs incurred during the reporting period for each task / work order.
Article XI - Points of Contact The PHS contact responsible for the successful completion of this Agreement is Paul Pryor. (215) 596-1416. FAX No.. (215) 596-1426.
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The NRC contacts for this Agreement are:
Techn; cal:
- Dennis Tarner. Project Officer - (301) 415-2283
- Tim Rollins. Alternate Project Officer
- (301) 415-1170
- Don Hall. Alternate Project Officer - (301) 415-3507 Randy Brown. Health and Safety Manager - (301) 415-7111 Contractual:
Anita Hughes. Contract Specialist - (301) 415-6526
- lhese individuals are authorized to issue work orders under this Agreement.
PRIVACY ACT STATEMENT All information (not of a " personally identifiable" medical nature) collected under this Interagency Agreement is the property of and controlled by the NRC.
The decision to disclose any or all of this information (e.g. Freedom of Information Act Requests) is the sole right and responsibility of the NRC.
If this agreement is acceptable to U.S. Public Health Services. DF0H. please so indicate by signing in the space provided below and returning two fully executed copies to me.
You may retain the third copy for your records.
,Since we are rapidly approaching September 30, our fiscal year ending date, you should expedite the execution and return of this document.
Unless the signed documents are returned to me prior to that date. I cannot assure you of
'the continued availability of these funds.
Sincerely.
', EI$
u Elois J. Wiggins.
tracting Officer Technical Acquisition Branch No. 2 Division of Contracts Office of Administration Attachments:
As stated ACCEPTED:
1 BY:
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l Attachment A BILLING INSTRUCTIONS FOR NRC INTERAGENCY AGREEMENT Billings will be provided by DFOH through the "On-Line-Payment-Collection" (OPAC) system each fiscal year to:
Agency Location Code:
31-00-0001 The following information shall be provided by DFOH on the OPAC billing:
1.
OPAC number and date of billing 2.
Interagency Agreement Number 3.
Name and address of agency performing work 5.
NRC Project Officer or Technical Contract 6.
Billing period or beginning/ending dates (day, month, and year) of the period in which costs were incurred and for which reimbursement is requested.
7.
Work Order Number i
8.
Cost detailed by major cost elements:
a.
Direct labor - This consists of salaries and wages paid (or accrued) for direct performance of the contract.
I Indicate labor category and number of hours worked for each labor category b.
Laboratory testing costs, supplies, etc.
c.
Indirect rates, if any d.
Travel cost - airfare, train, local travel by POA -
number of miles times mileage rate Frequency.
The Agency shall submit billings for reimbursement as each task is completed.
Billing of Costs After Expiration of Agreement.
If reimbursable costs are incurred during the agreement period and claimed after the agreement has expired, the period during which these costs were incurred must be cited.
! An original and three copies of your billing must be sent to:
U.S. Nuclear Regulatory Commission Office of the Controller Division of Accounting and Finance General Accounting Branch, T9-E2 Washington, DC 20555 Phone Number:
(301) 415-7520 Payments will be made'by the Office of the Controller, Division of Accounting and Finance, GOV /COM Accounts Section, Washington, DC 20555.
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ATTACHMENT 8 U.S. PUBLIC HEALTH SERVICE DIVISION OF FEDERAL OCCUPATIONAL HEALTH ENVIRONMENTAL HEALTH SERVICES l
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PRICE LIST The information below constitutes a price listing for environmental health consultative services available through this agreement in fiscal year (FY) 1996.
For further information regarding any aspect of ENVIRONMENTAL AND OCCUPATIONAL please call 215/596-1888.
A.
Occupational Health Program Planning and Consultation Services:
1.
DFOli - Project N1anager 47.00 2.
Industrial Hygienist (Certified) 88.00 3.
Professional Engineer (PE) 100.00 4.
llealth Physicist (Certified) 68.00 5.
Microbiologist (EH) 82.00 Microscopist 41.00 6.
Epidemiologist 66.00 7.
Sanitarian 54.00 8.
A HER A-Management Planner / Inspector 39.00 9.
Physician (Certified - Occupational) 119.00 10.
Nurse (Certified - Occupational) 37.00 NOTE:
Professional prices may change by location throughout the country.
B Analytical Services 1.
DFOH National Environmental Reference Laboratories (NERL).
NOTE: See Attached NERL Analytical Services and Price List 2.
Contract Laboratory Services NOTE:
Services are available through DFOH, for reduced cost access to the full range of environmental and industrial hygiene analytical procedures and methods.
Contact DFOH for current price list and analyte / method price quotes (See Attached Services).
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UNITED STATES PUBLIC IIEALTli SERVICE DIVISION OF FEDERAL OCCUPATIONAL IfEALTIf NATIONAL ENVIRONMENTAL REFERENCE LAHORATORIES ANALYTICAL FEE SCifEDULE FISCAL YEAR - 1996 GENERAL A N A LYSIS FEE /S AMPI E 1.
G AS CilROMATOGRAPIIY/ MASS SPECTROSCOPY ANAIYTE TOTAI, IIYDROCARilON QUANTIFICATION 25.00 VOLATil.E ORGANIC COMPOUNDS SCREENING 100.00 CONFIRMATION /QUANTIFICATION 150.00 ALDEllYDES UNKNOWN SCAN (UP TO 12 COMPOUNDS) 50.00 INDIVIDUAL ALDEHYDES QUANTIFICATION 40.00 FORM ALDEllVDE 40.00 2.
TRACE METAL ANALYSES - FLAME AA/GFAA ANALYTE TRACE METALS - ANTIMONY, BERYLLIUM, COPPER SELENIUM, ARSENIC, NICKEL, SILVER, BARIUM CHROMlUM AND THALLIUM (FLAME) 12.00 (FURNACE) 12.00 LEAD PAINT CHIPS 20.00 SURFACE WIPES 20.00 AIR 20.00 i
DRINKING WATER 12.00 j
CONTINUED
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- 3. GENERAL CilEMISTRY ANAIYTE ALKALINITY 10.00 CIIEMICAL OXYGEN DEMAND (COD) 30.00 IIARDNESS 10.00 NITROGEN DIOXIDE 25.00 NITRATE 20.00 p11 5.00 TURBIDITY 10.00 CliLORINE TOTAL RESIDUAL 20.00 FLUORIDE 20.00 IIEXAVALENT CllROMlUM 25.00 NITRIC OX1DE 25.00 NUISANCE PARTICULATE 10.00 TOTAI DISSOLVED SOLIDS 15.00 4.
DRINKING WATER ANAIYTE LEAD / COPPER 22.00 LEAD, COPPER TURBIDITY, pil 35.00 LEAD, COPPER, TURBIDTY, pil. II ARDNESS, 75.00 ALKALINITY, CllLORINE
- 5. OPTICAL MICROSCOPY ANALYTE METilOD MEDI A l
ASBESTOS PCM-NIOSil 7400 MCE FILTER 12.00
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PLM-NIOSli 9002 BULK SAMPLE 16.00 EPA /600/R-93/116 OSHA ID 160 MCE FILTER 20.00 POINT COUNT /
BULK SAMPLE 50.00 EPA /600/M4-82-020 4
CONTLNUED l
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El,ECTRON N11CROSCOPY ANALYTE NIETIIOD N1EDI A ASBESTOS TEN 1-AIIERA PROTOCOL NICE FILTER I15.00 l
(YAN1 ATE LEVEL 11)
TEN 1 - NIOSil 7402 N1CE FILTER 150.00 TEN 1 - CilATFIELD BULK SAN 1PLE 175.00 PRUIDCOL I
UNKNOWN FINE TEN 1-EPA.600/4-84-043 WATER QlDl PARTIC. I.D.
TEN 1,SAED ANDEDXA BULK, WATER OLDIE i
DFOll/NERL SOP-101 DUST AND AIR
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N11CROlllOLOGY AND filOAEROSOI.S ANAL.YTE AIR SAN 1PLES FUNGAL ENUN1ERATION/ IDENTIFICATION 47.00 BACTERIA ENUN1ERATION/GRAA1 STAIN 47.00 l
WIPE / BULK t
SAN 1PLES FUNGlONLY 57.00 l
B ACTERI A ONLY 49.00 BOTH FUNGl AND BACTERIA 70.00 i
TOTAL HETERORPOPPillC COUNT (WATER) 30.00 TOT / L COLIFORN1 B ACTERIA (WATER) 30.00 TOTAL COLIFORN1 B ACTERIA (WIPE) 45.00 i
INDOOR ALLERGENS (DUST N11TES/ CAT DANDER ALLERGENS) 60.00 l
(DUST NilTES Der p-l only) 20.00 (DUST NilTES Der f-l only) 20.00 (CAT ALLERGEN Fel d-l only) 20.00 LEGIONELLA B ACTERI A (WATER) DETECTION 80.00 SPECIATION AFTER DETECTION 95.00 s
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DATA..
CHEM LAB 0RATORIE5 i
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i TABLE OF CONTENTS i
l Page
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introduction.................................................................................................,.,..
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General Information: Te rm s and Condi ti on s............................................
3 t
Index of Environmental Methods................................................................
5 l
EPA 100 Series Tests i
EPA 200 Series Tests
[
EPA 300 Series Tests l
EPA 400 Series Tests EPA 500 Series Tests i
EPA 600 Series Tests EPA 3000 Preparation Procedures EPA 7000 Series Tests i
EPA 8000 Series Tests EPA 9000 Series Tests index of Third Edition NIOSH Met hods..........................................................
15 Inder of Selected OSH A Met hods.................................................................. 21 index of U.S. Army Environmental Center (US AEC) Methods................ 27 Fee Schedule: E n viro n me n t a l A na ly s e s............................................ 31 A.
RC"A Hazardous Waste Analyses B.
Underground Stmage Tank Monitoring i
C.
EPA-CLP Analytical Protocols i
D.
Pesticides /PCBs E.
NPDES Priority Pollutants 1
F.
TSCA Regulations G
Safe Drinking Water H.
Air Sampling /1990 Clean Air Act 1.
Physical Parameters J.
Chemical Parameters K.
Microbiological Parameters in Water L.
Trace Explosives Tests Fee Schedule: Radl oc h emi ca l A na l ys es......................................................... 45 Fee S ched ule : Indu s t rial H y giene A na lyses................................................... 49 A.
Particulates B.
Organic Solvents & Vapors.-Group i C.
Organic Solvents & Vapors.-Group 11 j
D.
Miscellaneous Organic Determinations E.
Passive Organic Vapor Monitors (POVM)
F.
Polynucie.7.r Aromatic Hydrocarbons (PAH) i G
Organics by High Performance Liquid Chromatography H.
Inorganics by Ion Chromatography j
l.
Inorganic Determinations J.
Specialty Gas Chromatography / Mass Spectrometry (GC/MS) Investigations K.
Biological Monitoring l
L.
Other OSHA and NIOSH Methods Fee Schedule: Asboslos Ana1yses................................................................. 59 l
A.
Optical Microscopy.
t B.
Electron Microscopy C.
Asbestos Notes Cliont Reference Gulde...................
63 Environmental: Preservation and Holding Time Requirements l
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Special design features assure the prevention of sample contamination, optimum efficiency, sample security, and safe working conditions.
DataChem Laboratories offers full service analytical capability. State-of-the-Art instrumentation and expertise are available with reference to the following: Gas Chromatography; Gas Chromatography-Mass Spectrometry; Purge-and-Trap Chromatographic Analyses; High Performance Liquid Chromatography; lon Chromatography; Atomic Absorption Spectroscopy; Inductively Coupled Plasma-Atomic Emission Spectroscopy; Optical and Electron Microscopy; IR-UV-Vis Spectrophotometry; Toxicity Characteristic Leaching Procedure; X-ray Diffraction; TOX; TOC; and Automated Colorimetric Analyses.
DataChem Laboratories provides this document as an introduction and guide to the comprehensive services offered. Discussions and requests for discounts and specific proposals are welcome. Client Service representatives and technical experts are available for project definition and the resolution of problems. Documentation including a. comprehensive description of the laboratory's capabilities and qualifications, Quality Assurance manuals, plans, and programs, and Standard Operating Procedures are available upon request.
DataChem Laboratories' standards of excellence emphasize integrity and quality. Please contact us if we can be of service to you.
Sincerely, James H.
elson, Ph.D., CIH President, DataChem Laboratories i
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i GENERAL INFORMATION The following statements describe the terms and conditions under which DataChem Laboratories (DCL) agrees to operate.
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1.
GENERAL 3.3 All analyses will be monitored under the DCL Quabty Assurance /Quahty Control (QA/QC) program. This program includes: instnanent cahbration, the analysts of spiked samples, 1.1 Fee Schedules provide a panial listmg of routine analyses performed by DCL If you have requirernents for analyses not quabty control samples, laboratory blanks, rephcate analyses, beted, special analytical requiremenu, or desire informauor, arnparison of QA/QC data with accepted hmau, and morutonng addressmg sampling and/or analytical prutocols, please contacs a of instrument performance.
member of either our marketing or customer service 3.4 DCL uses QA/QC protocols which are consistent with wrrent department.
industry standards. It is the responsibibry of the customer to i
L2 Upse regnest, DCL wel empply (et east plus shipping charges) desermme if the :.oposed QA/QC protocols meet the project or mampling smeda, assapie battles and preservatives. Shipplag site-specific QArQC requitanents as determined by a perdcular costalmars wts be prov6ded at me ast. Ne credit wul be given regulasory agent.
for returns.
3.5 DCL reserves the nght to refuse to proceed wuh the processing
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l.3 DCL wdl anampt to maintam services at the hsied fee; however, of any sample whidiis judged by DCL to be noncomphant with fees are subjea to change without rotice.
quahty assurance requirements of a requested regulatory analytical protocol. In such an event, the customer shall reimburse DCL for any costs incurred prior to the stop. work ANAL)TICA L SERVICE ORDERS order.
36 DCL wdl attempt to comply with applicable Federal and Sute
. 2.1 Requests for analyncal services may be made by telephone, FAX, or i,i wnting ne customer's authorned representauve requirements for storage, processing, and analytical holding i
times. However, unless samples have been scheduled with a must confirm all requesu for services in wnung DCL Project Manager prior to dehvery, these QA/QC ume Imuu 2.2 DCL reserves the nght to sfuse to proceed with an analytical cannut be guaranteed.
request if the customer fails to penvide an acceptable onnen analytical request or to establish acceptable credit 3.7 Should the QA/QC requirements of a requested regulatory method or protocol spectfy that a sample must be reanalyzed.
i arrangements any additional sample required for the remnalysis will bc 2.3 Pnot to submission of environmental samples, the customer Provided by the customer at the customer's expense, Any i
should develop an appropriate project Quality mutated or requested QA/QC reanalysis which generates data AssuranceJQuahty Control (QA/QC) plan. This plan should consistent with onginal results will be at the customer's expense.
j I
identify, among other items, the antent of the project, sample 3.8 DCL wdl retain any residual sample for a penod of 45 days, collecuan and preservauan n:quirements, types of QC samples that are required (e g., manna spikes, matna sptke duphcates, after which the residual sample will be prope:9 disposed of, field blanks), laborotory analyses / methods to be perfonned, unless a wnnen agreement directing DCL otherwise has been minimum data reporting requirements, and required sample established. DCL reserves the nght to retum unused pomons to tumamund times. his plan should be submined to DCL pnor to the cusunner for disposal.
sample submission. Unless such a plan is subnuned, DCL shall not be responsible for project. specific QA/QC requirements.
d.
ANAL)TICAL RESL'LT3 DCL personnel will assist m the preparauon of projea QA)QC plans.
4.1 DCL reserves the right to determine the appropriate format in
&d Uansas speelal pricing is arranged in advance, all orders for which me analytical results are reported. Reasonable advance entirensnental analytical services are subject to a uninhnusn requests for special formats will be honored. All results are charge of $50 per mothed, and/or $100 per maanple set. Eads provided for the exclusive use of the custorner. DCL accepu no field QC saanple wtl be bleed as a ragwier neld sample, responsibiLty or habihty for the cusiomer's use of such results.
Custeuners wNI not be charged for laboratary QC samspies.
ladustrial Hegiana analviacal nervices are subiect to charges 4.2 When requested, DCL may release verbal or FAX resuhs in fara ' " erfear(4)
' -: for each = = mi ne advance of the written report of resulu. Such results are only regnestad. Mate blanks wtN be b#4ed as saanplan. Asbestes tentative and are subject to subsequent confirmation or
"^'6 dunng standard DCL Q A/QC review procedures.
analytical servlees are not subject to a alnluneen charge.
4.3 DCL will maintain support documentation for analytical resulu
)
3.
SAMPLE RECEll'T AND PROCESSING for a period of three (3) years. If there is a possibility that analytical resulu may be involved in an admuustrative or judicial 3.1 The customer is responsible for all samples prior to receipt, Proceeding, please contact DCL immediately.
j inspecsion, and acceptance by DCL 1
1 5.
PAYMENT ANDTERMS j
3.2 DCL will use analytical methodologies which have been certafied as compliant with sequirements pubbshed or specified 5.1 DCL requires payment for analytical services prior to sample i
by the U.S. Environmental Protection Agency (EPA), State analysis, unless other payment terms have been estabbahed.
l Environmental or Health Agencies, the National Insutute for Occupational Safety and Health (NIOSH), the Occupational 5.2 Any amounts owing DCL by the customer which are not paid l
Safety and Heakh Administration (OSH A), or other regulatory wulun thiny (30) days after invoicing shall accrue interest at the i
agencies. DCL reserves the right to interpret these rate of I 1/2% per month (18% annually).
methodologies when applying them to the analysis of customer's samples based on the reasonable professional judgement of DCL 53 in the event it becomes necessary for DCL to prowed with legal personnel and recognized standards of the industry.
acucm to collect past due amounu, customer agrees to pay coun I
cosu and anorney fees.
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INDEX OF ENVIRONMENTAL METHODS l
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~ MISCELLANEOUS =
/ 7%,,
' EPA (100 TSERIES) TESTS; Method Analyte (s)
Instrumentation Water Price Solid Price 110.2 Color Visual
$7 N/A 120.1 Conductance Conductivity Meter 12 N/A 140.1 Odor Olfactory 12 N/A 150.1 pH Electrode 12 N/A 160.1 Total Dissolved Solids Gravimetry 19 N/A 160.2 Total Suspended Solids Gravimetry 19 N/A 160.3 Total Solids Gravimetry 19 N/A 160.4 Volatile Residue Oven & Gravimetry 29 N/A 160.5 Settleable Solids Volumetric 19 N/A 180.1 Turbidity Nephelometer 21 N/A METALS DETERMINATIONS EPA 200 SERIES TESTS Method Analyte (s) instrumentation Water Price
- Solid Price
- 200.7 Metals (panet)
$215
$215 200.7 Metals (singles)
ICP 65/15 66/15 202.1 Aluminum AA 65/15 65/15 204.2 Antimony GF/AA 70/29 70/28 206.2 Arsenic GF/AA 70/28 70/28 208.1 Barium AA 65/15 65/15 210.1 Beryllium AA 65/15 65/15 210.2 Beryllium GF/AA 70/28 70/28 213.1 Cadmium AA 65/15 65/15 213.2 Cadmium GF/AA 70/28 70/28 215.1 Calcium AA 65/15 65/15 218.1 Chromium AA 65/15 65/15 218.2 Chromium GF/AA 70/28 70/28 219.1 Cobalt AA 65/15 65/15 220.1 Copper AA 65/15 65/15 231.1 Gold AA 65/15 65/15 231.2 Gold GF/AA 70/28 70/28 236.1 Iron AA 65/15 65/15 239.1 Lead AA 65/15 65/15 I
239.2 Lead GF/AA 70/28 70/28 242.'i Magnesium AA 65/15 65/15 243.1 Manganese AA 65/15 65/15 245.1 Mercury Manual CV/AA 42 42 245.5 Mercury in Sediment CV/AA 42 42 246.1 Molybdenum AA 65/15 65/15 246.2 Molybdenum GF/AA 70/28 70/28
'First price includes preparation charge. Additional metals on same digestate are billed at lower charge.
7
EPA 200 SERIES TESTS (Continued)
Instrumentetlon Water Price
$ 65/15
$65/15 255.1 Platinum AA 65/15 65/15 255.2 Platinum GF/AA 70/28 70/28 258.1 Potassium AA 65/15 65/15 270.2 Selenium GF/AA 70/28 70/28 272.1 Silver AA 65/15 65/15 272.2 Silver GF/AA 70/28 70/28 273.1 Sodium AA 65/15 65/15 279.2 Thallium GF/AA 70/28 70/28 282.1 Tin AA 65/15 65/15 282.2 Tin GF/AA 70/28 70/28 283.1 Titanium AA 65/15 65/15 283.2 Titanium GF/AA 70/28 70/28 286.1 Vanadium AA 65/15 65/15 286.2 Vanadium GF/AA 70/28 70/28 289.1 Zinc AA 65/15 65/15 289.2 Zine GF/AA 70/28 70/28
'First price includes preparation charge. Additional metals on same digestate are billed at lower cost.
/
NON METALLIC INORGANICS EPA 300 SERIES TESTS Method Analyte (s)
Instrumentation Water Price Solid Price 300.0 Anions IC
$64/26' 305.1 Acidity Titration 20 310.2 Alkalinity AutoAnalyzer 26 325.2 Chloride AutoAnalyzer 29 335.3 Total Cyanide AutoAnalyzer/UV 52 340.2 Fluoride Electrode 29 350.1 Ammonia AutoAnalyzer 29 351.2 TK Nitrogen AutoAnalyzer 52 353.2 Nitrate AutoAnalyzer 29 353.2 Nitrate & Nitrite AutoAnalyzer 29 353.2 (mod.)
Nitrite AutoAnalyzer 29 365.1 Ortho (filterable) Phosphorus AutoAnalyzer 29 52 365.4 Total Phosphorus AutoAnalyzer 370.1 Silicon, Dissolved AutoAnalyzer 29 375.2 Sulfate Cclorimeter 29 376.1 Sulfide Titration 42
- Fee for first analyte is $64; fee for each additional analyte is $26.
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ORGANCSt
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EPA 400' SERIES TESTSt Method Analyte (s) instrumentation Water Price Solid Price 410.4 COO Colorimeter
$40 413.1 Total Recoverable Oil & Grease Gravimetry 60 413.2 Total Recoverable Oil & Grease infrared 55 415.1 Total Organic Carbon Oxidation / Infrared 55 418,1 Total Recoverable Petroleum Infrared 55 Hydrocarbons 420.2 Phenolics Autoanalyzer 52 425.1 MBAS Colorimeter 75 1
i ORGANICS IN DRINKING WATER EPA 500 SERIES TESTS (FOUR SAWLE MINIMUM FOR DRINKING WATER)
Method Analyte (s)
Instrumentation Water Price Solid Price 501.1 THM P&T/GC
$ 75 N/A 502.2 Volatile Organics P&T/GC 135 N/A 503.1 Volatile Aromatic &
P&T/GC 120 N/A Unsaturated Organics 504 EDB & DBCP GC/ ECD 75 N/A 505 Organohalide GCECD 220 N/A Pesticides & PCBs 507 Nitrogen / Phosphorus Pesticides GC/NPD 175 N/A 508 Chlorinated Pesticides GCECD 175 N/A J
515.1 Chlorinated Acids GCECD 200 N/A j
524.1 Purgeable Organics GC/MS (packed column) 550 N/A 524.2 Purgeable Organics GC/MS (capillary column) 350 N/A 531.1 N Methyl Carbamoylor.imes &
HPLC/PCD 175*
N/A N Methyl Carbamates (10 analytes) 547 Glyphosate fFLC 125 N/A 548 Endothall GC/FID 125 N/A 549 Diquat IPLC 125 N/A 550 PAH FPLC 175 N/A
- Six (6) samples minimum; minimum fee equivalent to fee for six samples.
I
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ORGANICS EPA 600 SERIES TESTS i
Method Analyte (s)
Instrumentation Water Price Solid Price 601 Volatile Halocarbons GCEC 5155 602 Volatile Aromatics GC/FID 120 603 Acrolein / Acrylonitrile GC/FID 120 604 Phenols GC/FID 175 l
606 Phthalate ester GC,EC 120 607 Nitrosamines GC/NP Ouote 608 PCB & Chlorinated Pesticides GCEC 250 608.2 Pesticides in wastewater GCEC 250 610 PNA GC 210 l
610 PNA HPLC 210 611 Haloethers GC/Han 175 I
i 613 Dioxin GC/MS Ouote 614 Organophosphorus Pesticides GCFPD 130 615 Herbicides GC/ ECD 175 618 Halocarbon So! vents GC Direct injection 75 l
622 Organphosphoras Pesticides GC/FPD 180
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624
\\OC GC/ MS 290 625 Semivolatiles GC/MS 550
=
632 Carbamate & Urea Pesticides HPLC Ouote I
S W-8 4 6 EPA 3000 SERIES PREPARATION PROCEDURES i
l Method Analyte (s)
Instrumentation Water Price Solid Price HNO Dgest 535 j
3005 Metals 3
HNO ' hcl Digest 35 3010 Metals 3
i 3015 Metals Microwave / Acid Digest 35 HNO Dgest 35 J
3020 Meta' 3
HNO. H 0. hcl Digest
$35 3050 Metais in Sohds 3 2 2 35 4
3051 Metals in Sohds Microwave / Acid Digest 3
3510 Organics Liquid / Liquid Extraction 50 50 3520 Organics Continuous Extraction 50 50 3540 Semivolatile Organics Soxhlet Extraction 50 50 4
3550 Semivolatile Organics Sonication Extraction 50 50 I
3580A Organics Waste Dilution 50 50 3610 Organics Alumina Cleanup 20 20 3611 Organics Alumina Cleanup &
20 20 4
Petroleum Separation 3620 Organics Florisil Cleanup 20 20 3630 Organics Silica Cleanup 20 20 l
3640 Organics Gel Permeation 50 50 3650 Organics Acid / Base Partition 20 20 J
10
i EPA 3000 SERIES PREPARATION PROCEDURES (Continued)
Method
. Analyte (s) instrumentation Water Price Solid Price 3660 Organics Sulfur Cleanup
$ 20
$ 20 3810 Volatile Organics Headspace GC 155 155 3820 Purgeable Organics Hexadecane Extraction &
120 120 GC Screen
^
METALS DETERMINATIONS
^
SW 846 EPA'7000 SERIES TESTS 1
- ns Method Analyte (s)
Instrumentation Water Price
- Solid Price
$ 6 5/15
$65/15 7041 Tin GF/AA 70/28 70/28 7060 Arsenic GF/AA 70/28 70/28 7080 Barium AA 65/15 65/15 l
7090 Beryllium AA 65/15 65/15 7091 Beryllium GF/AA 70/28 70/28 7130 Cadmium AA 65/15 65/15 7131 Cadmium GF/AA 70/28 70/28 7140 Calcium AA 65/15 65/15 7190 Chromium AA 65/15 65/15 7191 Chromium GF/AA 70/28 70/28 7196 Chromium IV Colorimeter 39 N/A 7200 Cobalt AA 65/15 65/15 7210 Copper AA 65/15 65/15 7380 tron AA 65/15 65/15 7420 Lead AA 65/15 65/15 7421 Lead GF/AA 70/28 70/28 7450 Magnesium AA 65/15 65/15 7460 Manganese AA 65/15 65/15 7470 Mercury (in liquids)
Manual CV/AA 42 7471 Mercury (in solids)
CV/AA 42 7480 Molybdenum AA 65/15 65/15 7520 Nickel AA 65/15 65/15 7610 Potassium AA 65/15 65/15 7740 Selenium GF/AA 70/28 70/28 7760 Silver AA 65/15 65/15 7770 Sodium AA 65/15 65/15 7841 Thallium GF/AA 70/28 70/28 7870 Tin AA 65/15 65/15 7910 Vanadium AA 65/15 65/15 7911 Vanadium GF/AA 70/28 70/28 7950 Zinc AA 65/15 65/15 6010 Metals ICP 65/15**
65/15
- First price includes preparation charge. Additional metals for same dige; state are billed at lower cost.
- lCP panel for Method 6010 consists of 25 metals for $215.
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SW-846 ORGANICS EPA 8000 SERIES TESTS Method Analyte (s) instrumentation Water Price Solid Price 8010A Halogenated Volatile Organics GC/ Hall
$155
$155 8011 1,2 Dibromometnano GCEC 100 100
& 1,2-Dibromo 3 Chloropropane 8015 Nonhalogenated Volatile Organics GCNID 139 139 8015 (Mod.) BETX and TPH GC/ Hall /PID 90 90 8020 Aromatic Volatile Organics GC/PID 120 120 8021 Volatile Organics P&T/GC/EC/PID 250 250 8030 Acrolein, Acrylonitrile, Acetonitrile GC/FID 120 120 8040 Phenols GC/FID 150 150 8060 Phthalate Esters (See Method 8270) 8080 Organochlorine Pesticides PCBs GC/EC 250 300 8100 PNAs GC,FID 210 210 8140 Organophosphorus Pesticides GC'FPD 220 250
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8141 Organophosphorus Pesticide GC.FPD or NPD (cap columq) 250 280 8150 Chlorinated Herbicides GCECD 175 200 8240 Volatne Uganics GC.MS (pacKeg column) 290 310 82S0 Volatile Organics GC/MS (capi!!ary column) 290 310 8270 Semivolatiles GC,MS (capillary column) 550 600 8280 Dioxins, Furans GC Low resolution MS Ouote Quote 8310 PNAs HPLC 210 210 1
8315 Formaldehyde HPLC 150*
8330 Nitroaromatics & Nittamines HPLC Ouote Quote 8318 Carbamate PestwJes HPLC Ouote Quote
- Six (6) samples minimum; minimum fee equivalent to fee for six samples.
MISCELLANEOUS
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SW-846 EPA 9000 SERIES TESTS Method Analyte (s)
Instrumentation Water Price Solid Price 9012 Total Cyanide / Amenable Cyanide AutoAnalyzer/UV
$50/60 9020 Total Organic Halide Microcoulometer 90 9030 Sulfides Distillation / Titration 59
$120 9036 Sulfate AutoAnalyzer/ Colorimeter 29 9040 pH (water)
Electrode 12 9045 pH (solid)
Electrode 15 9050 Conductance Conductivity Meter 12 l
l 9060 Total Organic Carbon IR Analyzer 88 9066 Phenolics AutoAnalyzer Colorimeter 52 9070 Total Recoverable Oil & Grease Gravimetry 60 9076 Total Organic Halide in Organics TOX Analyzer 75 9095 Paint Filter Liquids Paint Filter 14 12
4 SW 446 EPA 9000 SERIES TESTS (Continued)
Method Analyte (s)
Instrumentation Water Price Solid Price l
9251 Chloride AutoAnalyzer
$29 9310 Gross Alpha /Grost. Beta 55 9315 Alpha Isotopes Ouote 1010 Ignitability Pensky. Martin 45 1110 NACE/Corrosivity 180 SW846, 7.3 Reactive Cyanide See 9012 58*
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- Fee for both Reactive Cyanide and Reactive Sulfide: 5115.
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-m-r, INDEX OF THIRD EDITION NIOSH METHODS 1
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INDEX OF THIRD EDITION NIOSH METHOD PRICES (FOUR SAMPLE MINIMUM)
Method Colhod Number Substance Price Number Substance Price 0500 Nuisance Dust, Total
$12 Ethanol 0600 Nuisance Dust, Respirable 12 Isopropyf Alcohol 52 1401 Alcohols 11:
552/15*
1000 Allyl Chloride 1001 Methyl Chlondo 68 n-Butyi Alcohol 1002 Chloroprene 68 sec Butyl Alcohol 1003 Hydrocarbons. Halogerated:
52/15*
isobutyl Alcohol n-Propyl Alcohol Benzyl Chionde 1402 Alcohols Ill:
52/15' Bromoform Carbon Tetrachloride Allyl Alcohol Cyclohexanol Chlorobenzene Diacetone Alcohol Chlorobromomethane Isoamyl Almhol Chloroform o-Dichlorobenzene Methyl Isobutyl Carbanol 1403 Alcohols IV:
52/15*
p-Dichlorobenzene 2.Butoryethanol 1,1 Dichloroethane 2 Ethoxyetnanoi 1,2 Dichloroethylene Ethylene Dichionde Methyl Cellosolve 1450 Esters I:
52/15' Hexachloroethane Methylchloroform n Amyl Acetate sec-Amyl Acetate Tetrachloroethylene 1,1,2 Tnchloroethane n-Butyl Acetate sec-Butyl Acetate 1,2,3-Tnchloropropane 1004 Sym-Dichloroethyl Ether 52 tert-Butyl Acetate 1005 Methylene Chlonde 52 Isoamyl Acetate 1006 Tnchlorofluoromethane 68 isobutyl Acetate 52 Methyl (soamyl Acetate 1007 Vinyl Chlonde 68 n-Propyl Acetate 1008 Ethylene Dibromide 1009 Vinyl Bromide 52 1500 Hydrocarbons, BP 36 - 126 *C:
52/15*
1010 Epichlorohydrin 52 Benzene 1011 Ethyl Bromide 52 Cyclohexane 1012 Dibromodifluoromethane 68 Cycloherene 1013 1,2 Dichloropropane 52 n-Heptsne 68 n Hexane 1014 Methyl lodide 52 Methylcyclohexane 1015 Vinylidene Chlonde 1016 1.1.1,2 Tetrachloro-68/20*
n Octane n-Pontano 2,2-Difluoroethane and Toluene 1,1,2,2 Tetrachloro-1,2-Difluoroethane 1017 Bromotrifluoromethane 68 1501 Hydrocarbons, Aromatic:
52/15*
1018 Dichlorodifluoromethane and 68/20*
Benzene p-tert-Butyl Toluene 1,2-Dichlorotetrafluoroethane 1019 1,1,2,2-Tetrachloroethane 68 Cumene 1020 1,1,2 Trichloro-1,2,2-Triftuoroethane 68 Ethylbenzene 1022 Trichloroethytene 52 a-Methylstyrene 52 Naphthalene 68/20*
1024 1,3-Butadiene 1300 Ketones 1:
52/15*
Styrene 52/15*
Toluene Acetone Vinyl Toluene Cyclohexanone Xylene Diisobutyl Ketone 1550 Naphthas:
Coal Tar Naphthas 68 l
2-Hexanone Methyl isobutyl Ketone 68 Kerosene 2-Pentanone 1301 Ketones 11:
52/15*
Mineral Spints 68 Petroleum Ether 68 Camphor Petroleum Naphtha 68 Ethyt Butyl Ketone Rubber Solvent 68 Mesityl Oxide Stoddard Solvent 68 Methyl (n-Amyl) Ketone 68 1551 Turpentine 1400 Almhots I:
52/15*
1600 Carbon Disulfide 52 5-Methy!-3 Heptanone 1601 1,1-Dichloro 1-Nitroethrano 68 tert-Butyl Alcohot Callar a quoto if fewer fun txa fH sampes are anayzed for te same anays
- Pnoe tar nrst analyte /proe br second anayis; aWoonal anayes on same tube are tdied at lesser pn l
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NIOSH Methods (C ntinued)
M;thod Method Number Substance Price Number Substance Price 1602 Dionane
$52 2528 2 Nitropropane
$ 68
.1603 Acetic Acid 52 2530 Biphenyl 68 1604 Acrylonitrile 52 2531 Glutaraldehyde 68 1606 Acetonitrile 52 2535 Toluene-2,4-Diisocyanate 98 1608 Glycadol 52 2536 Valeraldehyde 68 1609 Tetrahydrofuran 52 2537 Methyl Methacrylate 52 1610 Ethyl Ether 52 2538 Acetaldehyde (GC) 68 16_11 Methylal 52 2539 Aldehydes, Screening 68/20* t 1612 Propylene Orsde 52 2540 Diethylenetriamine, Ethylenediamine & 125/37*
1613 Pyridine 52 Tnethylenetetramine 1614 Ethylene Oxide 95 2541 Formaldehyde (2-HMP) 60 1615 Methyl tert Butyl Ether (MTBE) 75 3500 Formaldehyde (chromotropic acid) 47 2000 Methanol 52 3502 Phenol 68 2001 Cresols 52 3503 Hydrazine 60 2002 Amines, Aromatic:
68/20' 3507 Acetaldehyde (HPLC) 98 Anilsne 3509 Aminoethanol Compounds (by IC) 100/35' N,N-Dimethylanalene 4000 Toluene 52 N,N-Dimethyl-p tolvidine 5000 Cartaon Black 12 o Toluidine 5001 2,4-D and 2,4,5 T 125/35*
2,4 Xylidine 5002 Warfann 98 2003 1,1,2,2 Tetrabromoethane 52 5003 Paraquat 98 2004 Dimethylacetamide and 52/15*
5004 Hydroquinone 98 Demethylformamsde 5005 Thiram 98 2005 Nitrobenzenes:
52/15*
5006 Carbaryl (Sevin) 98 4 Chloronitrobenzene 5007 Rotenone 98 Nitrobenzene 5008 Pyrethrum 98 Nitrotoluene 5009 Benzoyl Peroxide 98 2007 Aminoethanol Compounds:
68/20' 5010 Bromorynil and 98/37' 2 Aminoethanol Bromosynel Octanoate 2-Dibutylaminoethanol 5012 EPN, Malathion, and Parathion 68/20*
2 Diethylaminoethanol 5013 Dyes, Benzidine, o Anisadine, 125/37*
2008 Chloroacetic Aca, (IC) 85 and, o-Tolidine 2010 Amines, Aliphatic 68/20' 5014 Chlorinated Terphenyl 68 Diethylamine 5016 Strychnine 98 Dimethylamine 5018 2,4,7-Trinitrofluoren-9-one 125 2500 2 Butanone 52 5020 Dibutyl Phthalate and 68/20' 2501 Acrolein 68 Di(2-Ethylhexyl) Phthalate 2503 Mevinphos (Phosdnn) 75 5021 o-Terphenyl 68 2504 Tetraethyl Pyrophosphate (TEPP) 68 5023 Coal Tar Pitch Volatiles 47 2505 Furfuryl Alcohol 52 5026 Mineral Oil Mist 52 2506 Acetone Cyanohydrin 68 5027 Ribavinn 125 2507 Nitroclycerin/EGDN 75/30' 5029 4,4 Methylenedianiline (MDA) 98 2508 isophorone 68 5030 Cyanuric Acid 98 2510 1 Octanothiol 68 5031 Aspartame 98 2513 Ethylene Chlorohydrin 52 5500 Ethylene Glycol 68 2514 Anisidino 98 5502 Aldrin and Lindane 75 2515 Diaromethane 68 5503 Polychlorobiphenyls 57 2516 Dichlorofluoromethane 68 5504 Or9anotin Compounds (as Sn) 75 ea.
2517 Pentachloroethane 68 Bibutyttin bis (isooctyl mercaptoacetate) 2518 Hexachloro-1,3-Cyclopentadiene 68 Tetrabutyttin i
2519 Ethyl Chloride 68 Tributyttin Chloride 2520 Methyl Bromide 68 Tricyclohexyltin Hydroxide 2521 Methyl Cyclohexanone 52 5506 Polynuclear Aromatic Hydrocarbons (HPLC)250 j
2523 1,3-Cyclopentadiene 68 5508 Kepone 85 2324 Dimethyl Sulfate 68 5509 Benzidine & 3,3'-Dichlorobenzidine 75/30*
2525 1 Butanothiol 68 5510 Chlordane 75 2526 Nitroethane 68 5512 Pentachlorophenol 98 2527 Nitromethane 68 Cal for a quote if lower tien four IH samples are analyzed for the same anahte
- Pnm for arst analywpnas for smoond analyw, addeonal anaYtos on sarre tube are bilkxf atlesser prre.
tCal laboratity for speahe analytes and exact quae.
Ie
NIOSH Methods (Continued)
Method Method Number Substence Price Number Substence Price 5514 Demeton 5 75 Lithium Vanacium 5515 Polynuclear Aromanc Hydrocarbons (GC) 250 Magnesium Yttrium 5516 2.4 & 2.6-Toluenediamine 98 Manganese Zinc 5517 Polychlorobenzenes:
75/35*
Pentachlorobenzene Molybdenum Zirconium Neckel 1.2.4.5-Totrachlorobenzene 7400 Fibers 1.2,4-Tnchlorobenzene 5.15 7401 Alkahne Dusts 5518 Naphthylamines:
68/20' 7402 Asbestos Fibers 52 1-Naphthylamine 150 7500 Sihca, Crystalkne. Respirable 2 Naphthylamine 78 7501 S4ca, Amorphous 5519 Endnn 345 75 7600 Chromium Hexavaient (UV-VlS) 5521 Isocyanates 125/37' 7901 Arsenic Tnoxide (graphite AAS) 44 6001 Arsine 42 42 7902 Fluondes 6004 Sulfur Dioxide 44/21*
64 7903 Aceds, inorDanic (IC):
52/25' 6005 lodene 64 6006 Deborane Hydrogen Bromide 35 6007 Nickel Carbonyl Hydrogen Chionde 42 6008 Stibine Hydrogen Fluonde 64 6009 Morcury Nitnc Acid 60 Phosphonc Acid 6010 Hydrogen Cyanido 50 6011 Bromine and Chlonne Sulfunc Acid 64/25' 7904 6013 Hydrogen Sulfide Cyanides (Aerosol and Gas) 50 64 7905 Phosphorus 6600 Nitrous Oxide 75 44 8003 Lead in Blood and Urine 6700 Nitrogen Dionsde 35 44 8004 Polychionnated Biphenyls in Serum 165 6701 Ammonia 64 8005 Elements in blood or tissue.
Quote 7013 Aluminum 35/18*
7020 Cak:ium Antimony Molybdenum 35/18' 7024 Chromium Cadmiurn Nickel 35/18' 7027 Cobalt Chromium Platinum 35/18' Copper Silver 7029 Copper (fume and dust) 35/18' 7030 Zinc Iron Strontium 35/18' 7048 Cadmium Lanthanum Thall..a 35/18' Lead Vanadium 7056 Banum. Soluble Compounds 75 Lithium Zinc 7074 Tungsten (Soluble and insoluble) 100 Magnesium Zirconium 7082 Lead (Flame AAS) 35/18*
Manganese 7102 Berylhum 35/18' 8310 Metals in Unne:
7105 Lead (Flameless AAS) 42/35' Quote Aluminum Molybdenum 7200 Welding and Brazing Fume' 35/18' Banum Nickel Cadmium Chromium Cadmium Platinum Chromium Silver Copper Iron Copper Strontium Iron Tin Manganese Lead Titanium Nickel Silver Manganese Zine 9002 Asbestos (bulk) 19 Zinc P& CAM 141 TDI 7300 Elements (ICP):
35/18' P& CAM 142 h01 52 Aluminum Phosphorus P& CAM 266 h0CA 52 Arsenic Platinum P& CAM 339 Ammonia 98 Beryllium Selenium 64 P& CAM 205 Ammonia Cadmium Silver 42 P& CAM 231 NO and NO 2
BB Calcum Sodium S4 Hydrogen Sulfide 45 Chromium Tellurium S8 Ozone Cobalt Thalhum 75 S320 Niirogen Dioxide Copper Tin 44 S321 Nitnc Oxide Iron Titanium 42 S347 Ammonia Lead Tungsten 64 S209 Triorthocresyl Phosphate 75
. i for a qMa if kwer tan totr 1H samples are analyzed kr the same analyh
- hze kr frst anaywpnm tar second anatyle, addeanal analytes on same she are tJkxi at losser pnoe.
/
20
l NIOSH Methods (Continued)
Method Method f
l Humber Subetence Price Number Substance Price 5514 Demeton 5 75 Lithium Vanadium l
5515 Polynuclear Aromatic Hydrocarbons (GC) 250 Magnessum Yttrium 3316 2,4-& 2.6 Toluenediamine 98 Manganese Zinc 5517 Polychlorobenzenes:
75/35*
Molybdenum Ermnium l
Nickel Pentachlorobenzene 1,2,4,5 Tetrachlorobenzene 7400 Fibers 5 15 1.2,4-Tnchlorobenzene 7401 Alkaline Dusts 52 5518 Naphthylaminos:
68/20' 7402 Asbestos Fibers 150 1-Naphthylamine 7500 S4eca Crystaline, Respirable 78 2-Naphthylamine 7501 Salica Amorphous 345 5519 Endnn 75 7600 Chromium Hexavaient (UV.VIS) 44 5521 isocyanates 125/37' 7901 Arsenic Trioxide (graphite AAS) 42 6001 Arsine 42 7902 Fluondes 44/21' 6004 Sulfur Dioxide 64 7903 Acids, Inorganic (IC):
52/25*
I 6005 lodine 64 Hydrogen Bromide 6006 Diborane 35 Hydrogen Chloride 6007 Nickel Carbonyl 42 Hydrogen Fluoride 6008 Stibine 64 Nitric Aced 6009 Mercury 60 Phosphonc Acid 6010 Hydrogen Cyanide 50 Sulfunc Acid 6011 Bromine and Chionne 64/25' 7904 Cyanides (Aerosol and Gas) 50 l
6013 Hydrogen Sulfide 64 7905 Phosphorus 75 G600 Nitrous Onsde 44 8003 Lead in Blood and Unne 35 6700 Nitrogen Dioxide 44 8004 Polychionnated Biphenyfs in Serum
'165 6701 Ammonia 64 8005 Elements in blood or assue:
Quote 7013 Aluminum 35/18*
Antimony Molybdenum 7020 Cakaum 35/18' Cadnium Nackel 7024 Chromium 35/18' Chromium Platinum 7027 Cobalt 35/18*
Copper Silver 7029 Copper (fume and dust) 35/18' fren Strontium 7030 Znc 35/18*
Lanthanum Thall
.1 7048 Cadmium 35/18' Lead Vanadium 7056 Barium, Soluble Compounds 75 Lithium Zinc 7074 Tungsten (Soluble and insoluble) 100 Magnemum Zirconium 7082 Lead (Flame AAS) 35/18*
Manganese 7102 Berythum 35/18' 8310 Metals in Unne:
Quote 7105 Lead (Flameless AAS) 42/35' Aluminum Molybdenum 7200 Welding and Brazing Fume' 35/18' Banum Nickel Ca&nium Platinum Cadmium Chromium Silver Chromium Copper Strantium Copper tron Tin fron Lead Titanium Manganese Manganese Zine Nickel 9002 Asbestos (bulk) 19 Silver 52 P& CAM 141 TDI Zinc 7300 Elements (ICP):
35/18' P& CAM 142 h01 52 Aluminum Phosphorus P& CAM 266 h0CA 98 Arsenic Platmum P& CAM 339 Ammonia 64 Beryllium Selenium P& CAM 205 Ammonia 42 NO and NO 88 Cadmium Silver P& CAM 231 2
45 Celesam Sodium S4 Hydrogen Sulfide Chromium Tellurium SB Ozone 75 44 Cobalt Thaihum S320 Nitrogen Deoxide i
Copper Tin S321 Nitric Oxide 42 fron Titanium S347 Ammonia 64 Lead Tungsten S209 Triorthocresyl Phosphate 75 Cal b a quote if fewer than tour IH samples are analyzed lor tio same analyse
- Pnm lor frst analyta/pnm for second analyte; addeonal analytes on same she are tidied at lesser pnce 19
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l INDEX OF SELECTED OSHA METHODS J
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INDEX OF SELECTED OSHA MEinODS (Four Sample Minimum) niethod Number Price / Sample Analyte 68
$ 68 Acetaldehyde 118 64 Acetic Acid 82 68 Acetic Anhydride 165 52/25*
Acid Mist 52 68 Acrotein 21 104 Acrylamide 1
28 98 Acrylic Acid 37 68 Acrylonitrile 74 85 t
Aldicarb (Tamik) 188 64 Ammonia f
105 42 Arsenic i
12 52 Benzeno 65 75 Benzidine 108 64 Bromine 56 52 1,3 Butadiene 16 52 2-Butanone (MEK) 63 98 Carbaryl (Sevin) 67 85 Chlordane (Technical Grade) 101 50 Chlorine 202 64 Chlorine Dioxide 5
52 Chloroform to 68/20*
bis-Chloromethyl Ether (BCME) 10 68/20*
Chloromethyl Methyl Ether (CMME) 62 68 Chlorpyrifos (Dursban) 47 58 Coal Tar Pitch Volatiles 58 47 Coke Oven Emissions 98/37*
32 Cresol 98 81 Crotonaldehyde 52 1
Cyclohexanone 71 85 o Dianisidine 68 62 65 75/30*
Diazinon Dichlorobenzidine 62 68 DPVP (Dichlorvos) 125 41 Diethylamine 60 125 Diethylenetriamine 18 98 Diisocyanates 66 68 N,N Cimethyl Formamide 34 125 Dimethylamine 44 75/30*
2,4-Dinitrotolueno (DNT)/2,6 DNT 125 22 Diphenylamine 78 125 Diphenylamine 29 68 Enflurane 53 52/15*
2 Ethoxyethanol/2 Ethoxyethyl Acetate 79 52 2-Ethoxyethyl Acetate 79 52 2 Ethoxyethanol 55 98 l
l Ethyl 2 Cyanoacrylate (EC A) 36 125 j
Ethylamine 60 125 Ethylenediamine 2
68 Ethylene Dibromide
' Price for first analyte / price for second analyte; additional analytes on same tube are billed at lesser p Call for a quote it fewer than tour lH samples are analyzed for the same analyte.
3
_ ~ - -
OSHA Methods (C t und) h i
Analyte Method Number Price / Semple l
Ethylene Dichloride 3
$6' Ethylene Glycol Dinitrate 43 98 j
Ethylene Oxide 50 75 l
Fumaldehyde 52 60 l
Formic Acid 112 64 Furfural 72 68 Glutaraldehyde 64 98 Halothane 29 75 1,6-Hexamethylene Diisocyanate 42 98 Hy:frazine 20 Quote Hydrazoic Acid 211 98 isopropylaniline 78 125 Malathion 62 C8 Maleic Anhydride 25 98 Maleic Anhydride 86 98 Mercury Vapor 140 60 Metal Particulates 121 35/18*
2 Methoxyethanol/2 Methoxyethyl Acetate 53 52/15*
2-Methoxyethanol/2-Methoxyethyl Acetate 79 52/15' Methyl 2 Cyanoacrylate (MCA) 55 98 Methyl Ethyl Ketone Peroxide 77 160 Methyl isocyanate 54 98 j
Methyl Mercaptan 26 68 i
Methylamine 40 125 4.4'-Methylene bis (o Chloroaniline) (MOCA) 24 98 4,4' Methylene bis (o Chloroaniline) (MOCA) 71 85 Methylene Bisphenyl Isocyanate (MDI) 47 98 Methylene Chloride 59 52 l
Methylene Chloride 80 52 i
4,4'-Methylene Dianiline 57 85 l
Naphthalene 35 68 Nitric Acid 127 64 j
Nitric Oxide 190 64
~
Nitrogen Dioxide 182 64 Nitroglycerin 43 98 1 Nitropropane 46 52 2-Nitropropane 46 52 l
N Nitrosodiphenylamine 23 125 t
Organic Vapors 7
52/15*
PAHs (selected) 58 47/210**
i l
Parathion 62 68 l
Pentachlorophenol 39 125 Petroleum Distillate Fractions 48 68 Phenol 32 98 Phosphine 180 64 l
Phosphoric Acid 111 52 Pyrethrum 70 85
- Price for first analyte / price for each additional analyte: analytes must be specified.
1 3
"CTPV-547; PAH Scan-$210.
1 Call for a quote if fewer than four lH samples are analyzed for the same analyte.
i 24 l
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OSHA Methods (Continued) i l
Analyte Method Number Price / Sample 142
$78 Quartz 9
52 Styrene 104 64 Sulfur Dioxide (Impinger)
Sulfur Dioxide (Solid Sorbent) 107 64 Sulfur Dioxide (Beaded Carbon) 200 64 Sulfuric Acid 113 52 45 125 2,3,4,6-Tetrachlorophenol 71 85 Tolidine 2,4 Toluenediamine/2,6-Toluenediamine 65 75/35*
Toluene-2,4-diisocyanate (TDI)/2,6 TDI 42 98/37*
o Toluidine /m Toluidine /p-Toluidine 73 85/30*
14 52 1,1,1-Trichloroethane l
11 52 1,1,2-Trichlorcethane 60 125 Triethylenetetramine 44 75 2,4,6 Trinitrotoluene 51 52 Vinyl Acetate 8
52 Vinyl Bromide 4
52 Vinyl Chloride 19 52 Vinylidene Chloride 125 35/18*
Welding Fumes and Particulates
- Price for first analyte / price for each additional analyte; analytes must be specified.
Call for a quote if fewer than four lH samples are analyzed for the same analyte.
I 25
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INDEX OF U.S. ARMY ENVIRONMENTAL CENTER (USAEC)
METHODS 4
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1 SOlt WATER Certified Certified Method Unit Method Unit l
USAEC Analyte Number Price Number Price l
Ammonia M
TF30
$ 55 Anbns KT07
$150 TT09 145 l
Arsenic (GFAA) 89 55 AX8 55 Cyanide KF15 60 TF34 60 Fluoride m
TUO2 55 Hexavalent Chromium JYO3 85 SF01 75 ICP Metals JS12 190 SS12 175 l
Lead (GFAA)
JD21 55 SD18 55 Mercury (CVAA)
Y9 75 CC8 75 Nitrate / Nitrite KF17 55 LL8 55 i
Nitrite m
TF31 55 Selenium (GFAA)
JD20 55 SD25 55 j
Silver (GFAA)
JD22 55 SD26 55 Sulfide m
TY15 60 T-Phosphorus KF18 75 TF29 75
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TF28 90 Vanadium (GFAA)
JD23 55 SD29 55 DBCP S9 125 AY8 115 LW23 335 UW25 325 Explosives Herbicides LH18 210 UH10 205 Nitrocellulose LF05 170 UF05 170 Nitrogen / Phosphorus Pesticides LH15 190 UH11 180 Nitroglycerin /PETN LW27 300 UW27 300 Nitroguanidine LW30 240 UW29 230 Nitrosamines M
UM34 275 Organochlorine Pesticides /PCBs LH17 325 UH2O 310 i
Organosulfur Compounds LLO6 210 AAA8 200 Tetrazene LW28 170 UW30 170 Thiodiglycol LL9 190 in Review 180 Volatile Aromatics AA9 125 AV8 120 Volatile Halocarbons NN9 175 N8 165 GC/MS Semivolatiles LM25 595 UM25 590 GC/MS Volatiles LM23 300 UM21 290 1
1 29
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i STANDARD USAEC METHOD PRICING (Continued)
SOIL WATER i
i l
Methods Performed Under USAEC USAEC l
t the Auspices of the Method Unit Method Unit 1993 USAEC Guidelines Designation Price Designation Price Antimony (GFAA)
GSB1-SO
$ 55 GSB1-WA
$ 55 i
Arsenic (GFAA)
GASI-SO 55 GAS 1-WA 55 l
Lead (GFAA)
GPB1 SO 55 GPB1-WA 55 Mercury (CVAA)
HGC1-SO 75 HGC1-WA 75 l
Metals (ICP)
ICP1-SO 190 ICP1-WA 175 Selenium (GFAA)
GSE1-SO 55 GSE1 WA 55 i
Thallium (GFAA)
GTL1-SO 55 GTL1-WA
.55 I
Agent Breakdown Products '
In Review 195 in Review 190 (IMPA, MPA, Chloroacetic 3
Acid & Fluoroacetic Acid) 4 DIMP/DMMP in Review 170 In Review 170 Organochlorine Pesticides PST1-SO 325 PST1-WA 310 l
Semivolatile Organic j
Compounds by GC,MS SMV1-SO 585 SMV1-WA 575
{
Volatile Organic i
Compounds by Purge-l
- and-Trap and GC/MS VMS1-SO 300 VMS1-WA 290 VMS2 SO 395 i
(High Level) 1 i
All prices are based upon standard deliverables, turn-around schedules, and minimum of four (4) samples.
j Alternative or additional requirements, as well as factors such as matrix and sample load, may j
warrant discounts or supplemental costs.
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ENVIRONMENTAL ANALYSES i
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ENVIRONMENTAL CHEMISTRY ANALYSES A. 'RCRNYNAZARDOUSl WASTE ANALYSES (40 CFR 261)
- (Per Resource Conservation afxi Recovery-Act)'
SW-84 6 '
Method Fee 2 Analysis 1.
Toxicity Characteristic Leaching Procedure (TCLP) a.
Toxicity Characteristic (TC)
(Leaching plus full panel of 39 analytes) 1.
Leaching Procedure & Analysis Panel (c.1.-c.5 below)
EPA Methods
$ 1,3 4 5 2.
Matrix Spike for Analysis Panel (c.1.-c.5.3 below) 505 3.
Leaching Procedure & Analysis Panel, Multi phase EPA Methods Ouote d
4 Difficult matrices EPA Methods Quote b.
TC Leaching Procedures (TCLP)S these include:
1.
ZHE (Volatiles Only)
EPA 13116 150 2.
Organics & Metals
-Single-Phase EPA 13116 100
-Multi-Phase EPA 13116 Ouote c.
TC Analyses ^5 3
these include:
1.
Volatiles (10)
EPA 8240 230 2.
Semi Volatiles (13)
EPA 8270 480 3.
Pesticides (6)
EPA 8080 250 4.
Herbicides (2)
EPA 8150 200 5.
Metals (8)
EPA 6010/7000 187 7
d.
'CCWE' Analyses for
- Listed
- Wastes:
1.
Treated Waste Extractable(s)
EPA Method (s)
Quote Fee 2 Analysis SW 8461 Instrument Soll Water Method 2.
Organic Analyses a.
Volatile Organics 8240 GC/MS
$310
$290 b.
Semi-Volatile Organics 8270 GC/MS 600 550 c.
Pesticides and PCBs 8080 GC 300 250 d.
Pesticides 8080 GC 275 235 3.
Total Metals a.
Acid Digestion Procedure 3010/3050 38 38 b.
Metals Scan: including:
6010/7000 ICP 185 185 As, Ba, Cd, Cr, Pb, Se, Ag and digestion c.
Metals Scan (27 metals) including digestion 6010 ICP 215 215 d.
Mercury 7471/7470 CVAA 42 42 e.
Metals: low level detection 7000 GFAA (See page 41)
(per analyte) 33
A.
RCRA HAZARDOUS WASTE ANALYSES (Continued)
Fee Analyste SW-8461 Instrument Weste Method 4.
Ignitability 1010 Pensky-Martens S 46 (closed cup) 5.
Corroelvity a.
Electrode (pH) 9040/9045 Electrode 12 b.
NACE Test 1110 Gravimetry 180 6.
Reactivity (S=, CN-)
Section 7.3 115 7.
Colvent identification (organic components >1%)
GC/MS 400 8.
Cellfornle Weste Extraction Test (WET)
Quote I
Methods from: EPA Manual. " Test Methods for Evaluating Soled Waste.' SW-846. Third Edition; analyses according to the Second Edition methods are tvailable wth pnar arrangements.
2 Fee is for rouhne water and soil samples. Addnional charges may appty to heavily contaminated soil or water and to other matrices. The fee indudes analysas of laboratory qualdy control samples (e g, laboratory blanks, replicate analyses., surrogates). Field quality centrol samples (e g., field blanks.
trip blanks. equpment blanks. matnx spokes. matnx spike dupiscales) will be charged as separate samples.
EPA Method 1311 (TCLP) eequires a metnad matrix spike for each 20 same-mainx samples; thes spike sample will be analyzed and billed at additional 3
cost.
Whenever the TC leaching procedure produces two sampio preparations, one miscible with water and one non truscble with water, EACH of the sample preparassons must be analyzed and anvcuced as an independent sample.
5 The swervidual *TC* leectung procedures (TCLP) and *TC* Analyses are pnced separately.
6 The TCLP, Method 1311. leaciung promdures are not identical wnh those fourx! in the EP toxicity test. Method 1310.
Determination of 'Conshtuent Concentration in Waste Estract* iCCWE) in most cases, requires that an extrad (Leachate) of the waste be prepared 7
unang EPA 1311 (TCLP). The
- Waste E.itrad* is then analyzed for a specdic hazardous constituent by the appropriate EPA Method. The customer must determane whicti consteuent(s) and analytical s.ethod(s) are
- required" by the regutator who will review the analytical data.
1 Ft BdUNDERGROUND S10HAGE TAdK MONITORING NOTE: Analytical requirements vary among states. Contact the appropriate State agency for requirements prior to submitting samples to the laboratory.
Analysis Method Instrument Fee 1.
Volatile Liquid Leekage (e.g., gasoline) a.
BTEXN (benzene, toluene, ethyl-Modified 8015/
GC/HS/PID/FID
$ 90 benzene, xylenes, and naphthalene) 80201 and TPH for gasoline: C4 to C12 in soil b.
BTEX in Water 80201 GC/PID or HS 120 c.
Lead, Total 7421 1 GFAA 65 Organic Cal 2 AA 75 d.
Ignitability 10101 Pensky. Martens 46 (c!osed cup)
- 2. - S:Imivolatile Liquid Leekage (e.g.,
diesel / fuels)
Cal 2 Modified 8015 Extraction & GC/FID 139 a.
TPH for fuels: C8 to C25
/
b.
TPH Total Recoverable 418.13 IR 55 c.
Ignitability 10101 Pensky Martens (closed cup) 46 34
B. UNDERGROUND STORAGE TANK MONITORING (Continued)
Method instrument Fee Analysis Halogenated Organic Solvents (e.g., ethylene dichloride its gasoline) 3.
a.
Halogenated Organics 8010' GC/PT/ Hall
$155 4.
Unified Soll Classification Test a.
Visual estimate 20 45 b.
Sieve Analysis Quote
)
S.
Unknown Content of Storage Tanks See Section A-RCRA HAZARDOUS WASTE ANALYSES.
Methods from EPA Manual,
- Test Methods for Evaluatog Solaf Waste' SW446. Thrd Edden.
I 3
Methods from Califerna Departrnent of HeaRh Seruces Methods from EPA Manual,
- Methods for Cherrucal Analyss of Water and Wastes.* EPA 600/4JS420. Reesed March 1983.
3 NNEN!
U ~'*
1 C, EPA-CLPf ANALYTICAL PROTOCOLS jg3 Fee Method Instrument Soll Water Analysis OLM01.8 (SOW /3-90)
GC/MS
$350
$310 1.
Volatiles 3.
Semi-Volatiles OLM01.8 (SOW /3 90)
GC/MS 600 550 j
3.
Pesticides and PCBs OLM01.8 (SOW /3 90)
GC/EC 300 250 ILM01.0 (SOW /3-90)
AAllCP 325 325 4.
Metals ILM01.0 (SOW /3 90)
Autoanalyzer 55 55 5.
Cyanide Methods, analytes, and reporting requirements for EPA 4LP protocols depend on the specdat slarement of work (SOW) issu I
if specahe EPA 4LP protoco6s are required. p6 ease contad oCL for arrangements.
contract I
q y js D,l PESTICIDES /PCBs :
Fee Method instrument Solli Water i
Analysis 1.
Organochlorine Pesticides 8080 /6083 GC/EC
$300
$250 2
and PCBs 2
4 5
GC 250 220 8150 /615 /515.1 2.
Herbicide Acids 3.
Organophosphorus Pesticides 81412 GC 250 230 614'6224 GC N/A 130/180 d
4.
Organophosphorus Pesticides 35
PESTICIDES /PCBS (Continued)
Fee Analysis Method Instrument Solli Water 1 5
d 4
GC Ouote Quote 507 /627 /629 5.
Nitrogen / Phosphorus Pesticides 531.1, 632 WLC NA
$1608 5
4 6.
Corbamate/Ursas Quote Quote 7.
Others (e.g., organot.'n, mercurials, ersonicals, dithiocarbamates) 8.
Gti Permeetion Chromatography
$50 50 (GPC) cleanup, if required Additional charges may apply to heavdy contaminated sod, wager or other matrims.
EPA Manual. " Test Methods for Evalueling Sok! Weste." SW-846. TNrd Ede,on.
40 CFR. Part 136, Revised July 1,199o.
Test Methods for Nonconventional Postodos. Chemcal Analyses of Industnal and Muncpal Wastewater, EPA 440/1-83/079C..'anuary.1983 (NTIS Document No. PB 83 176636).
Methods for the Delermination of Organic Compounds in Dnnking Water. EPA 400/448439.1988.
Six (6) samples monimum; minimum fee equivalent to fee for six samples.
'N..'4-NPDESf PR.lORITY POLLUTANTS (40 CFR, Part 136, Revised July 1.- 1990).1 (National: Pollutant Discharoe' Elimination System)
Analysis Methodi instrument f
Was Wr 1.
Toxic (Priority) Pollutants (40 CFR, Part 122, Appendix D Table ll, Revised July 1,1990) a.
Volatiles (+ 5 unknowns) 6245 GC/MS
$290 b.
Semi Volatiles (+ 10 unknowns) 6255 GC/MS 550 c.
Identification of each additional GC/MS 16 unknown found during analysis 2.
Other Toxic Pol utants (40 CFR, Part 122, Appendix D Tabte til, Revised July 1,1990) a.
Metals (total):
200 Series AAllCP 275 Sb, As, Be, Cd, Cr, Cu, Pb, Hg, Ni, Se, Ag, TI, Zn b.
Phenols (total) 420.2 Autoanalyzer 52 c.
Cyanide (total) 335.3 Autoanalyzer 52
. Csnv:ntional Pollutants (40 CFR, Part 122 Appendix D Table IV Revised July 1,1990) a.
Chlorine, Total Residual Performed on site b.
Color 110.2 Visual 12 c.
Fluoride 340.2 Electrode 29 d.
Nitrate-Nitrite 353.2 Autoanalyzer 29 e.
Nitrogen, Total Organic 351.2 and 350.1 Autoanalyzer 78 f.
Oil and Grease 413.1 Gravimetric 60 g.
Phosphorus, Total 365.4 Autoanalyzer 52 h.
Sulfate 375.2 Autoanalyzer 29
- i. Sulfide 376.1/90302 Titration / Distillation 59
- j. Sulfite 377.1 Titration 42 36 i
_.____.._____________.._._.____._.__.._.__________.m.._
l i
i E. NPDES PRIORITY POLLUTANTS (Continued)
Fee r
Method 1 instrument i
Analysis g,
k.
Surfactants 425.1 Autoanalyzer
$75 l
1.
Aluminum, Total 200.7 iCP 65/15 4 3
n.
J p.
Molybdenum, Total 200.7 CP s.
Manganese, Total 200.7 iCP t.
Titanium, Total 200.7 iCP 4.
Purgeable Halocarbons 6015 GC/PT 155 5.
Purgeable Aromatics 6025 GC/P T 120 601 /6025 GC/PT 250 5
a.
PANEL: Items 4 and 5 above 6.
Phenols 6045 GC 150 7.
Pesticides and PCBs 6085 GC 250 8.
Nitrosamines 6075 GC Ouote 9.
Polynuclear Aromatic Hydrocarbons 610 GC 210 5
- 10. Extraction / Preparation / Cleanup for items 6,
7, 3,
9 a.
Liquid / Liquid Extraction 40 b.
Continuous Extraction 50 c.
Soxhlet Extraction 40 d.
Acid / Base Cisanup 60 I
Methods from EPA Manual. "Methoos for Chemical Analysis of Water and Wasies." EPA 600/4-79-020 Rowsed March 1983, unless indicated otherwse 2
EPA Manual. " Test Methods for Evaluanng Sohd Waste." SW-846. Third Eddeon Fee per sample: 1st analyte-$65: 2nd to 10th analytes on same samph$15 each 3
0 Includes digeshon.
40 CFR 136. Appendix A. Revised July 1,1990.
F[TSCA{ REGULATIONS l(40$,CFR) Parts (700 799h~ Revised [Julyd j;;1988)}.
_jm)-;p y.;
Analysis Method Instrument Fee 1.
Polychlorinated Blphenyls (PCBs) a.
Transformer Oil EPA 1 GC/EC
$ 45 b.
Soil / Solids 80802 GC/EC 150 c.
GPC Cleanup, if required 36402 GC/EC 50 2.
Other Analytes Quote j
Method from: "The Determination of Polychionnaled B@nyls in Transformer Fluid and Waste Oils." EPA-600/441045 2
Method from EPA Manual:
- Test Methods for Evaluahng Solid Waste." SW 846. Third Edition.
37
G.
SAFE DRINKING WATER (40 CFR, Parts 141-143, Revised July 1,1992)
(A minimum of four drinking water samples is required for these prices to apply. If fewer samples are submitted, please call for quote.)
Analysis Method 1 Instrument Fee 1
Complete Chemical Analysis
$375 (39 parameters for new sources) 2.
- a. Inorganic MCLs (existing sources) 290 required in 1992
]
As. Ba, Cd, Cr. F. Pb Hg, NO. Se 3
3.
Asbestos 600/4 83-0043 TEM
'7C 4
VOC 502 2 GC PID Han
- 35 5.
THM 501 1 GCha'
'i 6.
EDB-DBCP 504 GC. EC
'5 7.
Chlorinated Acids 5'5' GC EC 2
8.
Carbamates 53' HPLC 7
9.
Glyphosate 547 HPLC
- 25
- 10. Diquat 549 HPLC
'25
- 11. PAH 550 HPLC
'75
- 12. Endothall 548 GC FID 125
- 13. Organochlorine Pesticides 508 GC.EC
'75
- 15. Radionuclides:
Gross Alpha: Gross Beta 55 Radium 226 15 Radium 228
'20 Radon Phase ill 95 Uranit,m Phase til 85 E PA Mvhods ufuess ottierwt5e sited i<
}
H/ AIR'iSAMPLING/1990 CLEAN AIR: ACT Analysis Method 1 Instrument Fee 1.
Volatlle Organic Compounds TO1 GC/MS Ouote (Tenax tube, Thermal desorption) 2.
Volatile Organic Compounds TO2 GC/MS Ouote (Carbon sieve, Thermal desorption) 3.
Volatile Organic Compounds TO2 GC/MS
$450 (Modified to use solid sorbent (Modified) i media with thermal desorption-screens for TO1, TO2, and TO3 analytes) 4.
Blanks for above TO2 GC/MS 100 (Modified) l 5,
NOx 7D 64 l
TACB27 64 6.
SO2 l
I EPA Compendium of Methods for the Determination of Tosic Organic Compounds in Amtwent Air EPA 600 4-84 041,1984 Additional Clean Air Ad MethodWI for a quote l
I. PHYSICAL PARAMETERS Fee 2 Wastewater /
Analysis Method 1 Instrument Groundwater 1.
Acidity 305.1 Titration
$ 20 2.
Alkallnity 310.2 Autoanalyzer 26 3.
Chemical Oxygen Demand 410.4 Colorimetric 40 (COD) 4.
Color 110.2 Visual 12 5.
Corrosivity (N ACE) 11103 Gravimetric 180 6.
Flash Point 10103 Pensky Martens 46 (closed cup) 7.
Herdneea 2340B4 Calculation 29 (Requires Ca and Mg)
(80) 39
i l
l PHYSICAL PARAMETERS (Continued)
Fee 3 i
Westewater/
Analysis Method 8 instrument Groundwater 8.
Methylene Blue Active 425.1 Cowimator
$75 l
Substance (MBAS) l 9.
% Molsture Karl Fischer Titration 50 1
l 12 l
10.
Odor 140.1 l
11.
Oli and Grease 413.2 IR 55 12.
Petroleum Hydrocarbons -
418.1 IR 55 150.1 Electrode 12 13.
pH 1
3 115 l
14.
Reactivity (S". CN')
SW 846, Sec. 7.3 15.
Solids:
a.
Total Dissolved (Filterable) 160.1 Gravimetric 19 Gravimetric 19 b.
Suspended (Nonfilterable) 160.2 c.
Total 160.3 Gravimetric 19 d.
Volatile 160.4 Gravimetric 29 e.
Settleable 160.5 Gravimetric 19 i
16.
Specif!c Conductance 120.1 Wheatstone Bridge 12
)
(Conductivity) 17.
Duplicate analysis 415.1 Oxidation /lR 55 i
b.
Quadruplicate analysis 90603 Oxidation /lR 88 5
129 c.
TOC in soil Modified Mebius d.
TOC in soil Modified Lloyd Kahn 129 18.
Total Organic Hallde (TOX) a.
Single analysis 90203 (Modified)
Microcoulometer 90 b.
Duplicate analysis 90203 Microcoulometer 180 19.
Total Halldes in Organics 90763 Microcoulometer 75 20.
Total Halldes in Solids 600/4-84-008 Microcoulometer 75 21.
Turbidity 180.1 Nephelometric 21
\\
I Methods from EPA Manual, " Methods for Chemical Analysis of Water and Wastes.* EPA 600/4-79-o2o. Revised March 1983. unless noted otherwise.
Fee stoes not melude protect-specdic quainy control sarnpies.
EPA Manual.
- Test Methods for Evaluatog Sohd Waste, sW-846. Thrd Edason.
l APHA.AWWA-WPCF. " Standard Methods for the Exammaton of water and Wastewater.* 17th Editen.1989 Methods of Sop Analysis Part 2. Agronomy Monograph Number 9 l
40
Jk (dHEMICAd PARAMETERS.
Feet Wastewater /
Method 1 Instrument Groundwater Analysla Inorganic Procedures 1.
Anlons 41103 IC (Br, Cl, F, NO, NO, PO -3,SOI) 300.0 IC 2
3 4
$ 64 a.
First anion 26 b.
Each additional anion 185 c.
PANEL: All 7 anions (above) 2.
Perchlorate DCL Method IC 70
(+ $100 setup) 3.
Carbonate 310.2 Autoanalyzer 29 (CO = and HCO 'a )
23203 Titration 40 3
4.
Chloride 325.2 Autoanalyzer 29 a.
Free 4500-CN F3 GE 40 5.
Cyanide b.
Total 335.3 Autoanalyzer 52 c.
Weak Acid Dissociable 4500-CN 13 Autoanalyzer 37 d.
Amenable (requires Total CN, also) 4500.CN H3 Autoanalyzer 60 6.
Fluorlde 340.2 Electrode 29 7.
Hydrazine (water)
ASTM-D 1385 Colorimeter 554 Fee 2 Solids / Wastewater /
7000 Seriess or 200 Seriess Methods) instrument Groundwater Metals (by 8.
(Fee per sample: ICP 1st ana!yte-$65; 2nd to 10th analytes on same sample-$15 each; additional analytes - see below: ICP scan-af. GFAA 1st analyte-$70; additional analytes on same sample-$28 each) a.
$ 6 5 /15
- b.
Antimony (Sb) 200.7 (CP 204.2/7041 GF A A 70/28*
c.
Arsenic (As) 200.7 (CP 206.2/7061 GF A A d.
Beryllium (Be) 200.7 iCP 210.2/7091 GFAA f.
Boron (B) 200.7 iCP g.
Cadmium (Cd) 200.7 ICP 213.2/7131 GFAA h.
Calcium (Ca) 200.7 iCP
- i. Chromium (Cr) 200.7 iCP
- j. Chromium, Hexavalent (Cr+6) 7196 TAA 58/39 k.
l J. CHEMICAL PARAMETERS (Continued)
Feez Wastewaterl Anelysis Method 8 instrument Groundwster 1.
Copper (Cu) 200.7 iCP
- m. Iron (Fe) 200.7 iCP n.
Lead (Pb) 200.7 iCP 239.2/7421 GFA A o.
Lithium (Li) 200.7 iCP p.
Manganese (Mn) 200.7 iCP r.
Mercury (Hg) 245.1 CVAA
$42' s.
Molybdenum (Mo) 200.7 iCP t.
Nickel (Ni) 200.7 iCP u.
Potassium (K) 200.7 iCP
- v. Selenium (Se) 200.7 iCP 270.2/7741 GFA A
Strontium (Sr) 200.7 iCP z.
Tellurium (Te) 200.7 iCP aa. Thallium (TI) 200.7 iCP 279.2/7841 GFAA ab. Tin (Sn) 200.7 ICP 282.2 GFA A ac. Titanium (Ti) 200.7 ICP ad. Vanadium (V) 200.7 ICP 286.2/7911 GFAA ae. Zinc (Zn) 200.7 ICP af. ICP Scan 200.7 ICP 215*
Pnce ricaudes digestion. A requred-9.
Nitrogen as N a.
Ammonia (NH )
350.1 Autoanalyzer 29 3
b.
Nitrite 353.2 Autoanalyzer 29 c.
Nitrate + Nitrite (Nitrates) 353.2 Autoanalyzer 29 d.
Nitrate 353.2 Autoanalyzer 52 (c minus b) c.
Total Kjeldahl 351.2 Autoanalyzer 52
- 10. Phosphorus as P a.
Total 365.4 Autoanalyzer 52 b.
Ortho (Filterable) 365.1 Autoanalyzer 29 c.
Organic 365.1 Autoanalyzer 65
- 11. Total Phenols 420.2 Autoanalyzer 52
- 12. Sulfite (SO =)
377.1 Titration 42 3
- 13. Sulfate (SO ")
375.2 Autoanalyzer 29 4
42
i J. CHEMICAL PARAMETERS (Continued)
Feen Wastewater /
i Method 1 Instrument Groundwater Analysis Org:nic Procedures
- 14. Phenols 80405 GC
$175
- 15. Formaldehyde 83155 FPLC 1508 Methods from EPA Manual,
- Methods for Chermcal Analyses of Water and Wasles.* EPA 600/4-79'020. Revned March 1983, unless noted otherw 2 Fee does not include protect-specdc qualty control samples.
APHA AWWA WPCF. " Standard Methods for the Examination of Water and Wastewater.* 17th Ednaon.1989.
Six (6) samples minimum for hydrazme; mennnum fee equivalent to fee for sa samples.
d 5 EPA Manual. ' Test Methods for Evaluating Solid Waste.' SW446. Thrd Eddaon.
Six (6) samples minimum for formaldehyde; minimum fee equivalent to fee for six svnpies.
6 K. MICROBIOLOGICAL' PARAMETERS IN WATER (caution: short holdirid times)-
Fee Analysis Quote 1.
Total Plate Count 2.
C ollf o rm Quote a.
Total Quote b.
Fecal Ouote 3.
Fecal Streptococci Quote 4.
Blochemical Oxygen Demand (BOD)
LUTRACE EXPLOSlVES TESTS Fee Method Instrument
,j g, g,
Analysis 1.
Explosives Panel: HMX,RDX, 83301 FPLC
$240/250 TNB, DNB, Tetryl, NB, TNT, 2.4-DNT 2,Q-D NT 2.
Item 1. (plus 2-Am-DNT, 2-NT, 83301 FPLC 350/375 4 NT, 3 NT)
USAEC FPLC 200/210 3.
Nitroglycerin /PETN USAEC FPLC 125/125 4.
Nitroguanidine 43
. _ _ _ _.. ~ _ _ _. _
l t
' TRACE EXPLOSIVES TESTS (Continued)
]
Fee Method Instrument Water /Soll Anclysis b
15.
Plcric Acid USAEC HPLC
$125/125 i
i USAEC WLC 160/160 6; Totrazene l
7.
Nitrocellulose USAEC Autoanalyzer 130/150 i
if required, second-column confirmahons are $100/sampie.
EPA Manual, ' Test Methods for Evaluating Scw Waste." SW-846. Thrd Eddeon.
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f D WASTE SAMPLES RADIOCHEMICAL ANALYSESE ' ENVIRONMENTA 2
Detectable Minimum Cost Concentration (MDC) 1 Solid (pCl/g)
Method Water (pCl/L)
Annlysis
$ 55 5
2 110 0.1 PC 103 85 Gross Alpha / Gross Beta GS 0.2 gg/g 0.8 g/L 120 Gamma Spectrometry KPA 0.4 1.0 120 Uranium (Total)
AS 0.4 Uranium-234, 235/236, 238 1.0 120 AS 0.4 1.0 305 Thorium 228, 230, 232 AS 8.0 Plutonium 238, 239/240 20 120 PC 0.4 1.0 120 Plutonium-241 AS 0.4 1.0 120 Americium-241 AS 0.4 1.0 120 Curium 244, 245, 246 AS 0.2 20 130 Nrptunium-237 LSC 0,3 1.0 115 Technelium 99 AS 0.3 1.0 120 Radium-226 RE.GS 0.5 3.0 145 Radium 226 (EPA Method)
PC, GS 0.5 2.0 120 Radium 228 PC 0.5 2.0 175 Strontium 90 (Total)
PC 0.8 3.0 120 Strontium 89, 90 PC 0.3 0.5 120 Load-210 PC 0.1 10 120 Polonium 210 GS 0.1 Cesium-134, 137 10 120 GS 1.0 150 75 Coba!!-60 GS N/A 500 Ruthenium-106 LSC 30 Hydrogen-3 (Tritium) 95 Radon (in ambient air by GS N/A 4
50 25 EPA charcoat canister)
LSC Radon (Dissolved in water) 25 s
Sample Preparation 25 6
Sample Preparation 9
7 Sample Screening tsat:on cou ting n
P A). aya spectrometry {AS), radon eaa-apon (RE).1.owd scin Radiologcal techniques snclude ionate pnosphorescence ana'ysis (Kon 'evel at d<scemible from the PC)
(LSC). gamma spectrometry (GS). and proportonat cou tng (
n 1
henimum detectable concentrations (MDCs) are def ned as a pn 2
reagent tWanks (at 95% confidence level).
m 137 energy hne s (a8 hours) ater sampong mental radioactmry (e o soit. vegetation.
Gamma spectrometry MDC is based on the Cesiu Radon samp+es must be received at the laboratory no later than two caymatnces commonly conecte 3
samp'e d
A sample preparation charge is apveed for all sammeair Afters, trssue. etc ). No
- g. construction materiais, studges. cas. etc ) in ace t water samples S
(
expected actmties above 0 01 A samp6e preparation charge is appied for as mixed waste matnces etamenated e preparaton charges to cover the cost of waste handhng.A sample screenin er is reached Arst.
6 7
pCvsamp6e gross alpha,0.1 pChample gross tota. nts w'll be performed for PC or AS analyses. whichev prefer DCL to handle the Standard costa guarantee that eether the MDC wdl be met or 1000 mmute cou#e t
An add +bonal fee may be cfiarged if mixed wastes. both sam NIA:Not Apphcable 1.5 6.sposal of eqaste and preparations.
14 30 der tar: Mattipfy by 5 day TAT.Witipsy by 2 5 J day TAT: Multiply by 3 $
al analyses.
In addrtion.
Normal TATS are considered to be 30 a5 days for radiochemec a4ow prescreenmg of radeocher'ucafly contammated s 20-35 mL of aqueous or 1 gram of sohd sample must be sent toThis must be done taefore actual s NOTE:
pease send a copy of radioactive materials beense VOLUME DISCOUNTS ARE AVAILABLE instructions.
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1 INDUSTRIAL HYGIENE ANALYSES A.
PARTICULATES Analysis Method (s)
Instrumentation Sampling Medium Fee
$12
Bulk 115
- b. Cristobalite
- c. Tridymite Metals 4.
Inductively Coupled Plasma NIOSH 7300 ICP MCE Filter (37-mm; O 8 m) 180
( Al. As. Be. Cd, Ca. Cr.
Scan (27 elements)
Co. Cu Fe, Pb, Mg Mn Mo. Ni, K. Se, Ag Na, U, P.
Pt. Te, Tl. Ti, W, V. Zn)
- 5. Atomic Absorption Various Fiame AAS ICP MCE Futer (37.mm: 0.8-gm) 35 18' Various Graph:te Furnace AAS MCE F4 iter (37 mm; 0.8 m) 42 35' Fee per sample: 1st analyte by flame AAS.lCP-$35, eacn additonal ana'y'e on same samp;e-St8. 1st ana;yte ty GFAA-$42;
~
1 each additional anayte on same samp'e-535 B.
ORGANIC SOLVENTS & VAPORS - GROUP l (Fe*e por tubet 1st analyte-$52; each aedit eal analyte-$15i Analysis Method (s) instrumentation Sampling Medium Fee
- 1. a Acetone NIOSH 13M GCFO Chareca T.te
$ 52 15 b, MO<
v<eter'es
- See Acc.e
- c. 2 Hexanone
- 2. Acetonitrile NIOSH 16C=5 GCFO Charcoal Tuee 62
- 3. Alcohols NIOSH t400 GCFO Charccal Tube 52 ' E NIOSH 1401 GCFO Cnarcoal Tube NIOSH 1402 GCFO Charcoal Tube NIOSH 1403 GGTO Charcoal Tube
- 4. a Benzene NIOSH 1501 GGFO Charcoal Tube 52n 5
- b. Styrene (Aromatic Hydrocarbons)
- c. Toluene
- d. Xylenes
- 5. 2 Butanone (MEK)
NIOSH 2500 GCFO Ambersorb Tube 52 OSHA 16 GCFO Silica Get Tube
- 6. Butyl Acetate NIOSH 1450 GC.FO Charcoal Tube 52 (Esters I) casi tor a quote d sewer than tour IH sarnpies are anawed for the same anaire
$t
d
}
B.
ORGANIC SOLVENTS & VAPORS -- GROUP l (continu:d) i l
Anclysis Method (s)
Instrumentation Sampling Medium Fee j
- 7. 1 Butyl Cellosolve NIOSH 1403 GCED Charcoal Tube
$52/15 I
- b. Cellosolve (Almhols IV)
GCED Charcoal Tube c Methyl Cellosolve OSHA 07
i 4
- b. Chlorobenzene (Halogenated Hydrocarbons) c Chloroform OSHA 07 GCED Charcoaf Tube l
- c. Tetrachloroethylene i
l i
- f. Trkhloroethane j
- g. Trichloroethylona NIOSH 1022 GCFD Charcoal Tube
- 10. & Cydohexane NIOSH 1500 OGFD Charcoal Tube 52/15
- b. Heptano (Hydrocarbons) c Hexane OSHA 07 GCED Charcoal Tube
- d. Octane
- e. Pantano
? 11. Epichlorohydrin NIOSH 1010 GCED Charcoal Tube 52
- 12. Ethyl Acetate OSHA 07 GCFD Charcoal Tube 52 l
Special Sorbent Tube 95
{
t i 14. Froon 112 NIOSH 1016 GCED
_ Charcoal Tube 52 1l 15. f q 113 NIOSH ;020 GGFD Charcoal Tube 52 13 Isobutyl Amtate NIOSH 1450 (Esters I)
GLND Charcoal Tube 52/15 D. Tetrahydrofuran NIOF" 1609 GCED Charcoal Tube r
c Vinyl Toluene NIOSH 1501 GCED Charcoal Tube f
- 17. M:thanol NIOSH 2000 GCFD Silica Get Tube 52 68
- 18. n M thyl 2.Pyrrotidone GC
OSHA 32 HPLC XAD.7 See HPLC Pricing
- 20. Sulfw Compounds /Mercaptans Chemiluminescence GC Air Bag 100/35
- 21. Sulfur Compunds/ Mercaptan GC Air Bag 300 Screen for 8 Compounds
- 22. Vinyl Acetate OSHA 51 GCED Ambersorb Tube 52
\\
I Call for e quote d fewer than tour lH samples are anatyred for the same analyte 52 l
l l
C. ORGANIC SOLVENTS & VAPORS - GROUP ll l
Analysis Method (s)
Instrumentation Sampling Medium Fee 1.
Acrotein NIOSH 2501 GCFD Special Sorbent Tube 5 68 OSHA 52 GCNPD Special Sorbent Tube l
- 2. Aldehyde Screen (11)
NIOSH 2539 GCFD Special Sorbent Tube 188
- 3. Amines, Aromatic NIOSH 2002 GCFD Sikca Get Tube 68/20' Aminoethanols. Aliphatic NIOSH 2007,2010 GCFD Silica Gel Tube Quote Amines i
4.
Anesthetic Gases N1003 GCFD Charcoal Tube 75/25 l
S. Formaldehyde NIOSH 2541 GCFD Special Sorbent Tube 60 OSHA 52 GCNP l
6 Glutaraldehyde NIOSH 2531 GCFD Special Sorbent Tube 68 OSHA 64 HPLC Treated Glass Fiber Fiber See HPLC Pncing 7 Kerosene NiOSH 1550 GCFD Charcoal Tube 68
- 8. Methyl Mercaptan OSHA 26 GCFPD Treated Glassfiber Fitter 68
' 9.
Naphthas NIOSH 1550 GCFD Charcoal Tube 68 2
- 10. Nicotine NIOSH S293 GC XAD-2 Tube 69 3
- 11. Nitroglycerin /EGDN NIOSH 2507 GCEC Tenax Tube 75/30
- 12. Stoddard Solvent 2 NIOSH 1550 GCFD Cnarcoal Tube 68 13 Total Hydrocarbons NIOSH 1550 (moo.t ed) GCFD Cnarecal Tube 68 1
3
- 14. 2.4 DNT; 2.6 DNT; TNT OSH A 44 GCEC Tenax 75/30/30 Fee per sample: 1st analyte-568; each ada.tronal analyte on same sampie-520.
1 2 Requires bu* standard to be supphed by customer. shipped in separate package Fee per sample: 1st analyte-$75; each additional analyte on same sample-530 3
]
D. MISCELLANEOUS ORGANIC DETERMINATIONS Analysis Method (s) instrumentation Sampling Medium Fee
- 1. Aminoethanol Compounds NIOSH 3509 non Chromatography Impinger
$100/35 (ME A. DE A. TEA)
- 2. Benzene Solubles NIOSH 5023 Gravimetry Filter 47 60 (Coal Tar Pitch Volatiles)
OSHA 58
- 3. Formaldehyde NIOSH 3500 Colorimetry Impinger 47 4 Isocyanates a MDI P& CAM 142 Co;or; metry Impinger 52
- b. TDI P& CAM 141 Colorimetry Impinger 52
- 5. Lowdevel indoor Air Thermal Desorption GCMS Carbotrap 300 450 Quakty Scan for Organics 100 Blank for above Call for a quote # tewer than four IH samples ara anatyred for the same analyte 53
D. MISCELLANEOUS ORGANIC DETERMINATIONS (Continusd)
Analysis Method (s) instrumentation Sampling Medium Fee
$ 52 (37-mm; 0.0- m)
- 7. P:stidde Screen a Carbamato panel HPLC OVS Tube 125/371
- b. Organochlorine panel GC OVS Tube 85/371 j
- c. Organophosphorus panel GC OVS Tube 85/371
)
- d. Organochlorine /organophos GC Samiquant. San GC OVS Tube 350
- 8. Polychlorinated biphenyls (PCBs) a Oil 600/4 81 045 GCEC Bulk 45 1
- b. Solid sorbent NOSH 5503 Florisil Tube 57
- c. Soil, wipes, water 8080 Bulk 150
- d. Wipes NIOSH 5503 100
)
- o. Blood GCEC Blood 150 l
- 9. 4,4 M:thylenedianiline (MDA)
OSHA 57 GCEC Filter or Wipe 85 NIOSH 5029 HPLC Filter (acid treated)
See HPLC Prices 1
Fee per sample: oost for 151 analyte / cost for each additional analyte.
2 Requirss bulk standard to be supplied by customer, shipped in separate package.
E. PASSIVE ORGANIC VAPOR MONITORS (POVM) (Fee per sample: 1st analyte-$52: each additional analyte on same sample-.sts)-
Anolysis Method (s)
Instrumentation Sampling Medium Fee t.
Formaldehyde 3M#4E Colorimetry 3M 3721
$47
- 2. Organics 3M GC 3M 3500 52/15 (See Above)
- 3. Total Hydrocarbons 3M GC 3M 3500 68
- 4. Othtr Fassive Monitors Quote F. POLYNUCLEAR AROMATIC HYDROCARBONS (PAH) (Fee per sample: GC 1st arnlyte-$79: each additional rnalyte on same sample.-$31. HPLC 1st analyte-598: each additional analyte on same sample-537)
Analysis Method (s) instrumentation Sampling Medium Fee
- 1. Quantitation of individual PAHs: multi-point calibration; OC Ac naphthene NIOSH 5506 or HPLC PTFE Filter or XAD 2 Tube
$98/37 Ac naphthylene NIOSH 5515 GCSD 79/31 Anthracene Filter and Tube Combined (See Above)
Benz (a) anthracene Benzo (b)fluoranthene Benzo (k)fluoranthene Benzo (a) pyrene Benzo (s) pyrene Benzo (ghi)perylsne Chrysene Dibenz(a.h) anthracene Fluoranthene Fluorene Indono(1,2,3 cd) pyrene N:phthalene Phenanthrone Pyrene cast for a quote d sewer than tour tH sampnes are analyzed for the same analyte 54
F. POLYNUCLEAR AROMATIC HYDROCARBONS-PAH (Continued)
Analysis Method (s)
Instrumentation Sampling Medium Fee
- 2. PAH Panel (mutti-point NIOSH 5506 or HPLC Filter or Tube
$210 calibration for 17 PAHs)
NIOSH 5515 GCED Filter and Tube combined 210 j
Il Gi CRGANICSLB HIGH PERFORMANCE Ll0UID CHROMATOGRAPHY (Fee per sample; f at =_',2 '*aa: each adamanal v_'.r an same samd: M7}
Anolysis Method (s) instrumentation Sampling Medium Fee
- 1. Cerbaryl HPLC
$ 98
- 2. Explosives GC/HPLC Quote (Nitrobenzene:
Nitroglycerin; Tetryt; 1,3,5-TNB; 1,3-DNB; PETN;2,4,6 TNT; 2,4-DNT; 2,6-DNT:
HPLC HMX;RDX)
- 3. Glutaraldehyde OSHA 64 HPLC Treated Gl ass Fiber Filter 98 4.
Isocyanates a 2,4-TDl; T.S TCi NIOSH 2535 HPLC Treated Glasswool Tube 98/37
- b. 2,4 TD,2,6 TDI OSHA 42 HPLC Treated Glass Fiber Filter 98/37
- d. hO OSHA 47 HPLC Treated Glass Fiber Filter 98
- e. IPDI OSHA 47 HPLC Treated Glass Fiber Filter 98 i
f.
Isocyanates NIOSH 5521 HPLC Impinger 125 l
S. MEK Peroxide OSHA 77 HPLC XAD 4 160
- 6. 4,4.Methylenedianiline (MDA)
NIOSH 5029 HPLC Filter (acid treated) 125
- 7. MOCA P& CAM 236 HPLC Glass Fiber Filter &
98 Silca Gel Tube
- 8. Pentamidine HPLC Quote j
- 9. Phenol OSHA 32 HPLC XAD-7 98
- 10. Ribavirin NIOSH 5027 HPLC Glass Fiber Filter 125 11, Individual Pesticides OSHA HPLC OVS 98/37 (See Above)
... %-u
. xk%.
+
HEINORGANICS BYllON CHROMATOGRAPHYT iW w
~ m:
Analysis Method (s)
Instrumentation Sampling Medium Fee 1
1, a Bromine Nf0SH 6011 lC Special Filter
$64/25
- b. Chlorine
- 3. Iodine NIOSH 6005 IC Can for a quase a lower than tour IH samples are anatyred for the same ana>rie.
55
H. INORGANICS BY ION CHROMATOGRAPHY (Cantinued)
Anolysis Method (s)
Instrumentation Sampling Medium Fee 4 Mineral Aods NIOSH 7903 IC Silica Get Tube
$52/252 a Hydrofluoric (Inorganic Acids)
- b. Hydrochloric c Phosphoric
- d. Nitric
- o. Sulfuric 110
- f. Panel {a. thru o.)
- 5. Sulfur Dioxide NIOSH 6004 IC Treated Filter 64 OSHA 104 IC Fitter & Impinger 64 Fee per sample: 1st analyte-464; each additional analyte on same sample-$25.
1 2
Fee per sample: 1st analyte-$52; each additional analyte on same sample-525.
4 l',jiNORGANidiDETERMINATIONS):
Anolysis Method (s)
Instrumentation Sampling Medium Fee
$52'
- 2. Ammonia NIOSH S 347 (mod.)
Colorimetry Treated Silica Gel 52 P& CAM 205 Colorimetry Impinger 42 Special Sorbent Tube 50 OSHA 188 (mod.)
Colorimetry e
Chromium VI NIOSH 7600 Colorimetry PVC Filter 44
- 6. Fluoride a Gaseous NIOSH 7902 Electrode Treated Back up Pad 44
- b. Particulate NIOSH 7902 Electrode Filter 44 c Gaseous & Particulate NIOSH 7902 Electrode Filter and Treated Back up Pad 65
- 7. Hydrazine OSHA 20 (Modified)
Colonmetry Special Sorbent Tube Quote
- 8. Hydrogen Sulfide NIOSH S4 Colorimetry Impinger 451 NIOSH 6013 IC PTFE and Charcoal Tube 70 (400/200 mg)
- 10. Oxides of Nitrogen a Nitric Oxide (NO)
S 321 Colorimetry TEA Tube 44
- b. Nitrogen Dioxide (NO )
NIOSH S 320 Colorimetry TEA Tube 44 2
c NO and NO P & CAM 231 Colorimetry TEA Tube 88 2
- 11. Phosphine OSHA 180 ton Chromatography Special Sorbent Tube 64
- 12. Phosphorus NIOSH 7905 GC/FPD Tenax Tube 75 i Six (6) samples rninimum; minimum fee equivalent to fee for six samples.
Call for a quase a fewer than tour IH samples are anatyred for the same arwpe.
56
J.
SPECIALTY GAS CHROMATOGRAPHYlMASS SPECTROMETRY (GC/MS) INVESTIGATIONS (Custom analyses at an hour'y rate are ottered by quote, Custom analyset for compound confirmation or identification are offered by ouote.)
1.
GC/MS Scan for Volatile Organics by Thermal Desorpt.on (EPA TO3 - Modihed) 5450 100 Blank for above Ovate 2.
Custom GC.MS Spocia:ty Analyses (e g. odors, unknown organic vapors, organics on charcoal tubes, waste maracten2ation, gas ana!ysis)
Ovote 3.
Pyrofysis GC,MS Specialty Analyses (e g., resins, polymers, plastict)
K.
BIOLOGICAL MONITORING Biological monitoring using (for example) blood, unne or hair is available to assess the consequences of indus', rial hygiene exposures to lead and other metals, solvents. PCBs, pesticides or other matenals. Please call for method information and piice quote.
f L.
~
Most OSHA and NIOSH methods are o!!ered t'y DCL The f aboratory has extensive expenence with modhmg and acapting standard methods to special sampkng requiremerts. P: ease call for r"ethod info'rnation and pnce Quote.
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ASBESTOS ANALYSES i
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ASBESTOS ANALYSIS A.
OPTICAL MICROSCOPY Analysis Method instrumentation Sampling Medium Fee 1.
Asbestos NIOSH 7'00 PCM Air Filter
$15 PCM Air Filter (<24 hr.)
21 PCM Blanks N/C NIOSH 9002 PLM1 Bulk, Friab's 19 Bulk, Friable (<24 hr )
27 Bulk, Non friable 2 pg Bulk, Non-friable 2 (<48 hr.)
39 Soil 29 EP A 600/M4-82 020 PLM3 (point count)
Bulk, Friable 100 (December 1982)
Bulk, Friable (<24 hr.)
150 Bulk, Non friable 2 11o Bulk, Non friable 2 (<48 hr.)
165 1
Estimated percentage analysis 2
Non friable materials: (o g., vinyl asbestos file (VAT), roofng materials. plaster, cement) i Point counting samples range. <1% to 9%
f 3
For multi phase PLM bulk sampies, add 50. for each additional pnase f
EPA poini-counting samples range. < t% to 9% asbestos, not recommended for non friable materiaf (e p. vinyl asbestos fiie.
rooting rnaterial)
B.
ELECTHON MICROSCOPY Analysis Method InstrumenteHon Sampling Medium Fee 1.
Asbestos EPA AHERA Protocol TEM Air fdter (4 or more samples)
(Yamate. Level 11)
Same day or 8 AM next day
$110 5 PM next day 100 90 3 5 days Air filter (13 samples) 12 hours1.388889e-4 days <br />0.00333 hours <br />1.984127e-5 weeks <br />4.566e-6 months <br /> (3 days) t00 NIOSH 7402 TEM Air filter 2 5 days 135 Same day 150 150 EPA 600/4 83 043 TEM Drinking water 170 ELAP NY TEM Drinking water DCL SOP based on TEM Waste water EPA 600/4 78 011 Fibers ato m long 150 Fibers 2 5 m long 300 0
Sediment in waste water 20*
DCL SOP 025 TEM Bulk visual estimate 40 2 5 days 60 Same day ELAP NY Chatfield PLM + TEM Bulk non friable 110 Gravimetric Reduction (Max 20 samples. 5 days)
Where waste water contains large amounts of sediment, there is this add #tional charge for the separate sediment analysis.
61
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ASSESTOS NOTES 1.
Optical Microscopy L
PCM results are usually reported in 2 3 days.
DataChem Laboratories must be notified for sample sets greater than 50.
Result will be telephoned or faxed on request, i
Late night, weekend or holiday service can be arranged.
Additional layers in bulk samples are analyzed, reported and billed separately, i
2.
Electron Microscopy s
A field blank is strongly recommended for all sample sets.
Rush samples received no later than 10 a.m. are processed in the next turnaround category.
Late night, weekend or holiday service can be arranged.
AHERA air sampling cassettes are available.
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a CLIENT REFERENCE GUIDE Environmental: Preservation and Holding Time Requirements The following information pertains to three Federal regulatory programs: RCRA, Safe DrinkinD Water Act (SDWA), and NPDES, The tables presented below list the parameters; reference method; analytical techniques; container types, number and volume; preservation and storage requirements; and maximum holding times prior to extraction and analysis.
- 1. SOLID / WASTE SAMPLES Reference Preservation Holding Time Parameter Method Technioue Container and Storage Extractl Analyze 2 Volatile Organics EPA 8240 GC/MS (2) 40-mL Refrigerated at 4'C N/A 14 days" VOA vials Ssmivolatile EPA 8270 GC/MS (1) 250-mL Refrigerated at 4*C 14 days 40 days Extrretable Organics glass jar Hilogenated EPA 8010 GC/HSD (2) 40-mL Refrigerated at 4'C N/A 14 days" Volstile Organics VOA vials Aromatic Volatile EPA 8020 GC/PID (2) 40-mL Refrigerated at 4'C N/A 14 days" Organics VOA vials Phonols EPA 8040 GC/FID (1) 250 mL Refngerated at 4'C 14 days 40 days glass jar Organochlorine EPA 8080 GC/ ECD (1) 25r'-mL Refrigerated at 4'C 14 days 40 days Posticides & PCBs glass jar Polynuclear Aromatic EPA 8100 GC/FID (1) 250 mL Refrigerated at 4*C 14 days 40 days Hydrocarbons or EPA 8310 HPLC glass jar Chlorinated EPA 8120 GCiECD (1) 250-mL Refrigerated at 4'C 14 days 40 days Hydrocarbons glass jar Metals: Cd,Cr,Pb, Mn.
EPA 6010 ICP Atomic (1) 250-mL Refrigerated at 4'C N/A 6 months Ba,Si,Fe, Al,Sb,Be,Co, Emission plastic jar Cu,Mo,Ni, Ao.TI.V,Zn Soectroscopy Arssnic EPA 7060 Furnace AA (1) 250 mL Refrigerated at 4*C N/A 6 montns Silsnium EPA 7740 Furnace AA plastic jar N/A 6 months Marcury EPA 7471 Cold Vapor AA N/A 28 days Lead EPA 7421 Furnace AA N/A 6 months Organic Lead ASTM 3237 AA after (1) 250 mL Refrigerated at 4'C 14 days 14 days" extraction glass jar Oil and Grease EPA 9070/ Gravimetric (1) 250 mL3 Refrigerated at 4*C N/A 28 days 9071 glass jar
% Solids SM 209F Gravimetric (1) 250-mL3 Refrigerated at 4'C N/A 7 days plastic jar FH EPA 9045 Electrometric (1) 250-mL3 Refrigerated at 4*C N/A Analyze plastic jar immediately ignitability EPA 7.1.2.2 Torch (1) 250 mL3 Refrigerated at 4'C N/A As soon as glass jar possible" Rxactive Cyanide EPA 7.3 &
Colorimetric (1) 250-mL3 Refrigerated at 4*C N/A As soon as EPA 9012 glass jar possible" Rractive Sulfide EPA 7.3 &
Titration (1) 250-mL Refrigerated at 4*C N/A As soon as 3
EPA 9030 glass jar possible" Fluoride EPA 340.2 Electrode (1) 2! mLa Refngerated at 4*C N/A 28 days plastic jar 1.
From field collection to extraction.
2.
From extraction to complete an& lysis.
3.
Can be analyzed from same 250-mL bottle.
"These samples must be shipped within 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> of collection.
HSD = Halogen Specific Detector SM = Standard Methods (APHA)
N/A = Not apphcable 65 i
f
- 2. WATER SAMPLES Reft,rence Preservation Holding Time 2
Parameter Method Techniaue Container and Storage Extract 1 Analyze Volatile Organics EPA 8240* GC/MS (2) 40 mL Refrigerated at 4*C N/A 14 days"t EPA 624 VOA vials hcl pH<2 Samivolatile EPA 8270* GC/MS (2) l L Refrigerated at 4*C 7 days" 40 days Extractable Organics EPA 625 glass bottles; TFE-lined cap Polychlorinated EPA 8280* GC/MS (1) 1-L Refrigerated at 4'C 7 days 40 days dibenzo-dioxins (PCDD),
amber glass l
polychlorinated dibenzo-furans bottle TFE.
l (PCDF) lined cap EPA 613 7 days" 40 days Halog 2nated Volatile EPA 8010 GCMSD (2) 40-mL Refrigerated at 4'C N/A 14 days" Organics EPA 601 VOA vials Aromatic Volatile EPA 8020 GC/PID (2) 40-mL Refrigerated at 4*C; N/A 14 days"t Oroanics EPA 602 VOA vials hcl pH < 2 Phanois EPA 8040 GC/FID (1) 1 L Refrigerated at 4*C 7 days" 40 days EPA 604 glass bottle; TFE lined cap l
Organochlorine EPA 8080* GC/ ECD (1) 1 L Refrigerated at 4*C 7 days" 40 days Pasticides and PCBs EPA 608 amber glass bottle; TFE-lined cap PCBs EPA 608 GC/MS (1) 1-L Refrigerated at 4*C 7 days" 40 days amber glass bottle; TFE-lined cap Chlonnated EPA 8120 GC/ ECD (1) 1-L glass Refrigerated at 4*C 7 days" 40 days Hycrocarbons (modified) bottle;TFE-lined cap Organophosphate EPA 8140' GC/FPD (1) 1-L amber Refrigerated at 4*C 7 days" 40 days Pesticides glass bottle; TFE-lined cap Chlorinated Herbicides EPA 8150' GC/ ECD (1) 1 L amber Refrigerated at 4*C 7 d ay s**
40 days glass bottle; TFE lined cap Polynuclear Aromatic EPA 8310 HPLC (1) 1 L Refrigerated at 4*C 7 days" 40 days Hydrocarbons glass bottle; TFE-lined cap I
1.
From field collection to extraction.
2.
From extraction to complete analysis.
- 40 CFR Part 261, Appendix IX List, July 1,1989.
" These samples must be shipped within 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> of collection.
- t. Preserve for Aromatics only; 7 rfays if no hcl.
HSD = Halogen Specific Detector SM = Standard Methods (APHA)
N/A Not applicable 66
E HNO pH < 2 N/A 6 months Mstals EPA 6010' ICPES (1) 500-mL 3
EPA 200.7 plastic bottle HNO pH < 2 N/A 6 months Arsenic EPA 7060* Furnace AA (1) 500 mL 3
EPA 206.2 plastic bottle HNO pH < 2 N/A 6 months Salsnium EPA 7740' Furnace AA (1) 500-mL 3
EPA 270.2 plastic bottle 3P <2 N/A 38 days-gias.
H 4
Mercury EPA 7470* Cold Vapor AA (1) 500 mL HNO EPA 245.1 glass bottle 13 days--piastic HNO pH < 2 N/A 6 months Lead EPA 7421* Furnace AA (1) 500-mL 3
EPA 239.2 plastic bottle Chromium (VI)
EPA 7196 Colorimetric (1) 125-mL Refrigerated at 4'C N/A 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br />" J
SM 3128 plastic bottle Organic Lead ASTM 3237 AA after (1) 500 mL Refrigerated at 4*C 14 days 30 days extraction glass bottle Sulfide EPA 9030' Titration (1) 500-mL Refrigerated at 4'C; N/A 7 days" EPA 376.1 plastic bottle add 2 mL of zine acetate and NaOH to pH > 9 Cyanide (CN)
EPA 9012' Colorimetric (1) 1 L Refrigerated at 4'C; N/A 14 days" EPA 335.3 plastic bottle NaOH pH>12
)
Fluoride EPA 340.2 E!ectrode (1) 500-mL3 N/A N/A 28 days plastic bot'!e Chloride, Nitrate, EPA 300.0 IC (1) 125 mL N/A N/A 28 days Sulfate plastic bottle Nitrate / Nitrite EPA 353.1 Colonmetric (1) 125 mL Refngerated at 4*C; N/A 28 days H SO4 pH<2 EPA 353.2 plastic bottle 2
Total Phenolics EPA 9066 Colorimetric (1) 1 L Refrigerated at 4*C; N/A 28 days H SO4 pH<2 EPA 420 2 glass only 2
Total Organic Carbon EPA 415.1 Oxidation /
(1) 125 mL Refrigerated at 4'C; N/A 28 days H SO pH<2 EPA 9060 NDIR amber glass 2 4 bottle Petroleum EPA 418.1 IR (1) 1 L Refngerated at 4'C; N/A 28 days H SO pH<2 Hydrocarbons glass bottle 2
4 Total Organic EPA 450.1 Dontmann (1) 500 mL Refrigerated at 4*C; N/A 28 days H SO pH<2 Halogens EPA 9020 DX-20 amber glass 2 4 bottle pH EPA 9040 Electrometric (1) 500-mL3 Refrigerated at 4*C N/A Analyze EPA 1501 plastic bottle immediately" Conductance EPA 9050 Wheatstone (1) 500 mL3 Refngerated at 4*C N/A 28 days EPA 120.1 Bndge plastic bottle Chimical Oxygen EPA 410.4 Colorimetnc (1) 125-mL3 Refrigerated at 4*C.
N/A 28 days SO pH<2 Demand plastic bottle H2 4
Oil & Grease EPA 413.1 Gravimetnc (1) l L Refrigerated at 4'C; N/A 28 days H SO4 pH<2 EPA 413.2 lR glass bottle 2
Total Dissolved EPA 160.1 Gravimetnc (1) 500-mL3 Refrigerated at 4'C N/A 7 days" Solids plastic bottle Total Suspended EPA 160.2 Gravimetric (1) 500-mL3 Refngerated at 4'C N/A 7 days" Solids plastic bottle Alkalinity EPA 310.2 Colorimetnc (1) 500 mLa Refrigerated at 4 C N/A 14 days" plastic bottle 1.
From field collection to extraction.
2.
From extraction to complete analysis.
3.
Can be analyzed from same 500 mL botne.
- 40 CFR, Part 261, Appendix IX List, July 1.1989.
"These samples must be shipped within 24 hours2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> of collection.
HSD = Halogen Specific Detector SM = Standard Methods (APHA)
N/A = Not apphcable 67
- 3. TOXICITY CH ARACTERIST t.EACHit4G PROCEDUP.E (TCLP) L IPLES Reference Preservate-Hfe q T e Parameter Memod Tecnniave Container and Storace E c ict' Ara,re-Votatue Organ,cs (VOCs) EPA 131' leroHead (2) 40 mL pett'ge' rec a 4'C
1ays
'4 cays teacrmg Space VOA via s Procecure E x tractabte Rotary (1) 250 - l.
Ra'rgy atec m 4'C
'4 days 40 cays i
Organics Evracoce glass ;ar Mercury 28 days 28 ca s r
Other Metals 180 days 180 cays VOCs EPA 8240 GC MS (2) 40 mL Refrigerated at 4^C N'A 14 days VOA vials Semi-volatiles EPA 8270 GC MS (1) 500-mL Refrigerated at 4'C 7 days 40 cays Pesticides EPA 8080 GCEC glass jar Heroicides EPA 8150 GCEC t
HtO pH<2 N/A 180 cays Ag.Ba,Cd.
EPA 6010 ICP Em:ssion (1) 250 mL 3
Cr. Po Soectrosccoy clastic cottie Arsenic EPA 7060 Fu'" ace A A (1 ) 250 mL HNO3 pHe2 N.A ISO cays Se'on,um EPA 7740 F
ace A A p.ast c oc" et t NA 80 caps Merc rv E P A 7.:70 C 0 'aco' A A NA 28 ca,s MINIMUM SAMPLE VOLUMES REQUIRED FOR TCLP EXTRACTION M a t r. a Me t a i r, Vc at es Se votat es Pestic ces He'o c ces Fe !TCLP Ac ac,s 61n 500 -L i C -L
'er
'e' 3
te's
<0 5% soi cs Solvent Oil' 2 '.ters 50; L 2
ers 2 ters 6
te's Slucge, Sod 500 ~L 125 -L
'e' ler 2 de's
(<0 5;. schds)
Sohd'*
150 g 5: ;
'50 g 150 g 200 ;
' Depending upon the *. sohds. te s samp'e at' i may 'esutt m a mu't p e pnase eachate j
"This category would incr ce any non f te ao e wave n e. rags or cag f.iters) u 1.
From field collection to extraction.
2.
From extraction to complete analysis.
"These samples must be shipped ethin 24 hou s Of ccuecon.
r f tMay be taken from ICP sample container HSD Halogen Specific Detector SV = Sta-ca'a VePocs t APH A)
N A = Not appocatie n*
. CERTIFICATION 51 LICE 0' 5URES
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