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Forwards Application for Renewal of NPDES Permit MI0005827, as Sent to State of Mi Water Resources Commission,Per Amends 54 & 40 to Licenses DPR-58 & DPR-74,respectively
	ML20128F662
Person / Time
Site:	Cook
Issue date:	05/10/1985
From:	Will Smith; INDIANA MICHIGAN POWER CO. (FORMERLY INDIANA & MICHIG
To:	James Keppler; NRC OFFICE OF INSPECTION & ENFORCEMENT (IE REGION III)
References
	NUDOCS 8505290700
	Download: ML20128F662 (143)
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,5 INDIANA & MICHIGAN ELECTRIC _ COMPANY Ml?hf gag {A DONALD C. COOK NUCLEA!! PLANT i y p I P.O. Box 458, Bridgman, Michigan 49106 (616) 465-5901 g2 4_ p >I f f Tt -{

n,4 May 10, 1985 Mr. J. G. Keppler, Regional Administrator United States Nuclear Regulatory Comission Region III i

799 Roosevelt Road Glen Ellyn, IL 60137 f Operating License DPR-58/74 Docket Nos. 50-315/50-316 I

Dear Mr. Keppler:

( Pursuant to the requirements of Appendix B, Part II - Nonradiological Environmental Protection Plan, Section 3.2, a copy of the application sent to the Michigan Water Resources Commission for renewal of National Pollutant Discharge Elimination. System Permit No. MI0005827 is attached. L This application is forwarded in accordance with Amendment No. 54 to [ Facility Operating License No. DPR-58 and Amendment No. 40 to Facility Operating License No. DPR-74 dated May 6, 1982. [ Sincerely, t I l LAY W. G. Smith, r. Plant Manager cc: John E. Dolan M. P. Alexich R. F. Kroeger H. Brugger NRC Resident Inspector R. C. Callen, MPSC G. Charnoff, Esq. J. M. Hennigan H. R. Denton, NRC J. F. Stietzel Dottie Sherman, ANI Library Q N INP0 PNSRC All cc without attachments gg 8505290700 850510 PDR ADOCK 0500031S P PDR MAY151985

s Docket Nos. 50-315/50-316 Page 2 bec: T. A. Kriesel J. E. Fryer D. Fitzgerald-Stuart T. P. Beilman

O [ a } L LINDIANA & MICHIGAN ELECTRIC COMPANY oNE SUMaet souARE. P O SOX 40. FORT WAYNL IN 40001 Teepnene (219) 425 2111 April 26, 1985 Mr. Paul D.' Zugger, Executive Secretary ' Water Resources Commission Department of Natural Resources P. O. Box 30028 Lansing, MI 48909

Dear Mr. Zugger:

Re: Donald C. Cook Nuclear Plant NPDES Permit No. MI0005827 Michigan Permit No. M00064 i Enclosed is an updated Industrial and Commercial Wastewater Discharge Application, which you requested. Two complete copies are enclosed since the Donald C. Cook Nuclear Plant has both surface water and groundwater discharges. A hydrogeologic evaluation of.the Cook Plant is being completed and will be forwarded as soon as it becomes available. Please forward one ' copy of the permit application to the Groundwater Quality Division. You also requested the Company's determination of applicable categorical effluent limitations. Attached please find a table listing - the proposed _ effluent limits and bases for limitations. During the past six years since the first permit renewal application was submitted to i the Michigan WRC, three drafts of the new permit were proposed;- l negotiations between the Company and the Permit Writer have resulted in the deletion of several monitoring requirements. Also U.S. EPA has revised the " Effluent Guidelines for the Ste'sm Electric Generating Point Source Category" eliminating monitoring of some previously required parameters. Following is a summary of discussion relative to those past monitoring requirements which have not been included in the table of proposed affluent limitations. OUTFALLS 00A, 00B, and 00C Internal outfalls 00A, 00B, and OOC are the effluents of the Unit 1 l steam generator blowdown, Unit 2 steam generator blowdown, and plant heating boiler blowdown, respectively. The Company proposes to delete monitoring requirements for iron and copper since the new Steam Electric Power Industry Effluent Limitations Guidelines now consider boiler blowdown a low-volume vaste which has no iron and copper limitations. l

r; Mr. Ptul D. Zuggar s April 26, 1985 Page'2 U.S. EPA determined that the concentrations af iron and copper are below the level of treatability and in such smal'. quantity that they will not cause toxic effects l(45 FR 68339). Moreover, in March 1979 the Michigan Water Resources Commission approved a permit modification which would delete iron and copper effluent limits for these discharges. An effluent limit for pH has not been included since the steam generator and boiler chemistry require that the blowdown.p'H be close to, or in excess of, 9.0. Also, the volume of blowdown is so small compared to the volume of cooling water into which it is discharged (see flow diagram attached), and since the cooling water pH naturally ranges between 6 and 9, little purpose is served by regulating the steam generator or boiler blowdown pH. Also, an effluent limit for Oil and Grease (0&G) has not been included since the existence of O&G in the steam generator or boiler blowdown is highly unlikely. No O&G materials are allowed to be fed into the steam generators / boiler since such materials, if introduced, would deposit on heat transfer surfaces, be decomposed to leave a char - deposit, thereby interfering with heat transfer causing a loss of efficiency and an increase in operating and maintenance costs. Furthermore, even if O&G materials were accidently introduced into the steam generator / boiler, their decomposition therein would prevent passage of any O&G into the blowdown. OUTFALL 003 Outfall 003 is a deicing discharge and is used on a very limited. basis. Furthermore Outfall 003 effluent consists of either Outfalls 001 and 002 effluents which are regularly monitored. Therefore, monitoring requirements for Outfall 003 are redundant and an unnecessary operating expense and the Company proposes to delete Outfall 003 monitoring requirements. ESSENTIAL SERVICE WATER Essential service water is pumped from the intake forebay for the purpose of non-contact cooling of miscellaneous small equipment (as opposed to the main turbine condensers) and is discharged to the circulating water discharge bay. The maximum design temperature rise is l 16*F. Since no water treatment additives are used in this system, heat ( is the only pollutant added'to Lake Michigan. The essential service water system maximum design flow is 28.8 MGD for each unit. Therefore, compared to the 1277 MGD discharge from Unit I and the 1718 MGD discharge from Unit 2, this additional heat load to Lake Michigan is insignificant. Furthermore, the D. C. Cook Plant 316(a) Demonstration approved by the Michigan Water Resources Commission on 5/27/77 shows that the total heat load from D. C. Cook Plant (including the heat discharged through the essential service water I discharge) ~did not adversely affect the aquatic environment. Therefore, I-

b Mr. Paul D. Zuggar April 26, 1985 Page 3 j no monitoring requirements have been proposed for the essential service water discharge. PCBs ~ The Company proposes that the BAT effluent guideline be adopted, "There shall be no net' discharge of polychlorinated biphenyl compounds such as those commonly used for transformer fluid." However, it is very unlikely for a net discharge of PCBs to occur since all PCB equipment is contained within the main plant building, and within enclosures designed to contain oil spills. Moreover, an extensive PCB survey conducted by the Michgian DNR Hazardous Waste Division on September 7, 1983 found that the PCB " transformers and overall the facility, appeared to be in very good condition, clean. and orderly. -more so than average." The Company proposes that monitoring for PCBs not be required unless a spill of PCBs to a waterway occurs. COMPLIANCE RECORD Two additional questions which you requested to be addressed are: 1) Is Donald C. Cook Nuclear Plant capable of complying with existing federal regulations without construction, 2) . Indicate the Company's assessment of compliance with the - existing permit.' Donald C. Cook Nuclear Plant has a good. history of compliance with . the existing NPDES permit and with existing federal regulations. Construction is not needed to comply with the existing regulations. PLANNED EQUIPMENT MODIFICATION Additional demineralization equipment is planned to be installed in 1985 as a-part of the discharge treatment system. These demineralizers will be used in lieu of existing evaporators. The install.?. tion of the demineralizers will result in an increase in the amount of boron discharged to Lake Michigan. The total yearly maximum amount estimated to be discharged is 13.477 pounds of boron. On the basis of the total-annual discharge of circulating water from Units 1 and 2, the concentration of baron in the discharge should increase to between 0.0015 ppm and 0.002 ppm. Since this equipment is not yet in service, additional NPDES screening data for boron will be provided when a representative sample of the discharge can be taken. I hope you find the attached information helpful in preparing the Donald C. Cook Nuclear Plant NPDES permit. Please call me if you require additional information or if you have any questions regarding the information enclosed. We believe that a meeting with the people responsible for draf ting the permit would aid them in understanding our

P--. i Mr. Ptul D. Zuggar April 26, 1985 Page 4 facility. Therefore, we propose a meeting either at the D. C. Cook Plant or in your office at your convenience. Very truly yours. ^ } n k/Wd $ ' Jack A. Druckemiller Manager of Environmental Affairs JAD/CEH/cak Enclosures c: W. G. Smith bc: T. A. Miskimen/T. E. Webb/C. E. Hawk R. E. Zahler R. W. Reeves - w/o enclosures i l l l L

DONALD C. COOK NUCLEAR PLANT NPDES PERMIT APPLICATION PROPOSED EFFLUENT LIMITS Out-Type of Parameter and Measurement Sample fall Description Discharge Effluent Limit Frequency Type Basis of Limitation 001 Unit 1 Surface pH: 6.0 to 9.0 Weekly Grab 40 CFR 423.12 & 423.13 Condenser Water PCBs: No net NA NA Non-Contact discharge Cooling Water

- TRC: 0.2 mg/l Daily Grab' Cl Application 2

Rate: 2 Hrs / Unit / Day Flow (MGD): 1,406 Daily Calculated Design capacity (Unit I condenser non-contact cooling water, Unit I steam generator blowdown, heating boiler blowdown) Temperature (OF)

The Company's 316(a) demonstration was Daily Continuous approved on 5/27/77 and showed that the Intake:
Discharge:

Daily Continuous discharges of 001, 002, and 003 would not increase the temperature of Lake Michigan at the edge of-a mixing zone, described as an area equivalent to 570 acres (a defined area equivalent to that of a circle of radius of 2811 feet) more than 30F above the existing natural temperature or above the following monthly maximum temperature: Jan 45 Feb 45 Mar 45 Apr 55 May 60 Jun 70 Jul 80 Aug 80 Sep 80 Oct 65 Nov 60 Dec 50 Heat Addition Daily Calculation (BTU /HR)

- Applicable when chlorinatin

) 1/5 l I

DONALD C. COOK NUCLEAR PLANT NPDES PERMIT' APPLICATION PROPOSED EFFLUENT LIMITS Out-Type of Parameter and Measurement Sample fall Description Discharge Effluent Limit Frequency Type Basis of Limitation 002 Onit 2 Surface pH: 6.0 to 9.0 Weekly Grab 40 CFR 423.12 & 423.13 Condenser Water PCBs: No net NA NA Non-Contact discharge Cooling Water

- TRC: 0.2 mg/l Daily Grab C12 Application Rate:

2 Hrs / Unit / Day Flow (MGD): 1,892 Daily Calculation Design Capacity (Unit 2 condenser. non-contact cooling water, Unit 2 steam generator blowdown, heating boiler blowdown) Temperature (DF) Daily Continuous

The Company's 316(a) demonstration was Intake:
Discharge:

Daily Continuous approved on 5/27/77 and showed that the discharges of 001, 002, and 003 would not increase the temperature of Lake Michigan at the edge of a mixing zone, described as an area equivalent to 570 acres.(a defined area equivalent to ti;3t of a circle of radius of 2811 feet) more than 30F above the existing natural temperature or above the following monthly maximum temperature: Jan 45 Feb 45 Mar 45 Apr 55 May 60 Jun 70 Jul 80 Aug 80 Sep 80 Oct 65 Nov 60 Dec 50 Heat Addition Daily Calculation (BTU /HR)

- Applicable when chlorinating 2/5

DONALD C. COOK NUCLEAR PLANT NPDES PERMIT APPLICATION PROPOSED EFFL6ENT LIMITS Out-Type of Parameter and Measurement Sample fall Description Discharge Effluent Limit Frequency Type Basis of Limitation 003 De-icing Surface Flow (MGD): 1,892 Daily

Calculation Design Capacity Discharge Water 00A Unit 1 Internal PCBs: No net 40 CFR 423.12 & 423.13 Steam Generator discharge Blowdown TSS: 30 mg/l Avg. Once/24 Hrs Grab 100 mg/l Max.

Flow (MGD): 0.864 Once/24 Hrs Calculated Unit Start-up, Design Capacity 00B Unit 2 Internal PCBs: No net 40 CFR 423.12 & 423.13 Steam Generator discharge Blowdown TSS: 30 mg/l Avg. Once/24 Hrs Grab 100 mg/l Max. Flow (MGD): 0.864 Once/24 Hrs Calculated Unit Start-up, Design Capacity 00C Heating Boiler Internal PCBs: No net Blowdown discharge 40 CFR 423.12 & 423.13 TSS: 30 mg/l Avg. Once/24 Ers Grab 100 mg/l Max. Flow (MGD): 0.019 Once/24, Hrs Calculated Design Capacity

During De-icir g operations 3/5

DONALD Ca COOK NUCLEAR PLANT NPDES PERMIT" APPLICATION PROPOSED EFFLUENT LIMITS Out-Type of Parameter and Measurement Sample fall Description Discharge Effluent Limit Frequency Type Basis of Limitation 000 Utility Ground-Flow (MGD): 2.5 Continuous Measurement Michigan Permit No. M00064 and previous Wastewater Water C0D (mg/1) Weekly Composite agreement between the Company and State-Discharge TDS (mg/1) Daily Composite authorities. Sulfate (mg/1) Daily Composite l Chloride (mg/1) Weekly _ Composite Note: Sample to be_taken prior to Phosphorous (mg/l) Weekly Composite. discharge to the on-site Cadmium (pg/l) Composite absorption pond. O&G (mg/l) Weekly. Grab l, pH: 5.5 to 9.0. Daily Composite-Weekly-Visual j Ob ervation i. 00E Sanitary Ground-Flow (MGD): 0.031 Daily Measurement Design Capacity Sewage Water Seepage Area Used List date i when areas are i alternated t 1 + i ]

During-bo iler cleanin!

1 4 9 4/5

DONALD C. COOK _ NUCLEAR PLANT NPDES PERMIT APPLICATION PROPOSED EFFLUENT LIMITS Type of Parameter and Measurement . Sample Out-Discharge' Effluent Limit Frequency Type Basis of Limitation fall Description 110400 Groundwater. N.A. Prior to' Michigan Permit M00064 and previous Static Elevation. Quarterly Monitoring Sampling agreement between the Company and State 4 110401 Wells pH Quarterly Grab authorities. 11040? Chromium Quarterly Grab 110403 Copper Quarterly-Grab l' Sulfate Quarterly Grab Chloride Quarterly Grab Hardness Quarterly Grab i Nitrate-Nitrogen Quarterly Grab Sodium Quarterly Grab j PCBs' Quarterly Grab l C00 Quarterly Grab i Boron Quarterly Grab Phosphorous Quarterly Grab T D solved Quarterly Grab g 1 Cadmium Quarterly Grab Oil & Grease Quarterly Grab i e 4 A 5/5

INDUSTRIAL AND COMMERCIAL WASTEWATER OISCHARGE APPilCAll0N OF MICh/ 44 9 ! g '. 'A o wenon $g i N E w 4 'W- %a

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i SECTION I penuiT + OTIOOOS837 NUMBER SEE INSTRUCTIONS ON REVERSE SIDE A. P90vt0E A BRIEF IfSCRIPTICH 40 LIE DIAGP,v1904t% THE HATER FLOW THROLEM YotR FACILITY FROt INTAKE TO DISCHARGE. SK)W Ad MRATIOr6 CDeiRIBUTING WASTD=ATER, INCLIEllG FROCESS MO PR03JCTICN AREAS, SANITARY FLOWS, CDOL!?G WATER, 40 StopfteATER RiksfF. YOU MAf GROUP lTEM SIMILAR CPOLATIONS INTO A SINGLI LAli. TE WATER BAL# ACE SHOULD SKM AVERAGE FLOWS. SHOW ALL SIGNIFICANT LOSSES OF WATER TO P903ETS, ATK!SPt(RE, 40 DISOSRGE. YOU 90AJ USE ACTUAL MEASSE?f.NTS te{hEVER AVAILABLE; OTERWISE TEE YOLR BEST ESTIMATE. DESCRIPTION SEE LinE DAdeAm oN Fou_owsNc pA M DIAGRAM i i l l lt i o G l

T ,f W W'II DD-I Visitor's r Center n r Potable and l 31.000 CPD Outfall 00E (MI 341) Sanfrary h ter ; N [atended WNel Absotption Field, From Unit I or 2 Make-up Water Plan d Aeration STP Operated Alternately 4 Plant weil ao. 2 0 40.000 lb/hr Sanitary 0.015 MG0 Avg. ---e Back-Up Ht. 0.031 MG0 Max 8 " Internal Outfall 00C (MI 3%) 0.014 MGD Avg. l Internal Outfall 00A (MI 397) 0.112 MGD Avg., 0.2 M MGD Max gitorwn.a ter d' North Catch Basir. 50s [ssential Start-up Service Water Normal = Flash 78.8 MGD Flash 4f Outfall 001 (MI 393) Unit I Unit 1 Circulating Water Discharge g 3200' Offshore usche Bay T-Steam rnna,nser l unit 15tm. Gen.l 1118 MCD Avg., 1277 NGO Man j a s6 I m , Emeraenew Overf be l ir ] u Unit 1 Make-Up Water Plant Regeneration Outfall 000 C ) Intake Cribs [ Intake Non-Essential Service Erter Pumnt BI H - m Turbi"' 3 O 423 MGD Ava. m (MI 374) Outfall 003* g (2250' Offshore Forebay Unit 2 Make-Up 2.4 MGD Max " On-Site (MI395) e-b Water Plant Absorption Pond d i In-Plant Sumps E isc Floor Drains-- Outfall 002 (Mt 394) Unit 2 Circulating Water Olscharge C 4 ";- Steam 1 1200* Offshore Dschg hy condenser i J 1425 MGD Avg., 1718 MGD Max A Normal m m Start-up tssential Flash Tank " flash Tank Service Water 28.8 MGD 3 m ir i, internal Outfall 006 (Mi 398) 0.109 MGD Avg. 0.282 MGD Max

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stormwater Lake Michigan .pSouth Catch Basin Wastewater Flow Diagram,1984 502 Donald C. Cook huclear Plant C. E. Hawk - 2/20/85

Outfall 003 De-icing Oschg was used 42 days In 1984 -- 224 MGD Avg., 839 MGD Max

MI0005827 Section I, Item 6 cont'd. OUTFALL. DESCRIPTIONS / OUTFALL 001 - Unit 1 Circulating Water Discharge Outfall 001 is a noncontact condenser cooling water discharge which 'is. continuous during periods of Unit 1 operation. The Outfall also contains steam generator blowdown from Unit 1 (internal Outfall 00A described-below) and sometimes plant heating boiler blowdown.(internal Outfall OOC described below). Condenser cooling water is withdrawn from Lake Michigan, screened to remove trash, routed through the Unit 1 surface condensers to condense steam, and routed back to Lake Michigan at a slightly elevated temperature. No water treatment chemicals or biocides are added; therefore, the discharged cooling water quality is essentially the same as the intake water. OUTFALL 002 - Unit 2 Circulating Water Discharge Outfall 002 is a noncontact condenser cooling water discharge which -is continuous during periods of Unit 2 operation. The Outfall also contains steam generator blowdown from Unit 2 (internal Outfall 00B described below) and sometimes plant heating boiler blowdown (internal Outfall 000 described below). Condenser cooling water is withdrawn from Lake Michigan, screened to remove trash, routed through the Unit 2 surface condensers to condense steam, and routed back to Lake Michigan , at a slightly elevated temperature. No water treatment chemicals or biocides are added; therefore, the discharged cooling water quality is essentially the same as the intake water. OUTFALL 003 - Deicing Discharge Outfall 003 is a deicing discharge which is used on a very limited basis.- A portion of the flow from Outfall 001 or Outfall 002 is directed through the middle one of the three intake structures to prevent ice buildup which would restrict intake flow. Use of this discharge is generally required only during the period from January 1 through April 5. OUTFALL 00A - Unit 1 Steam Generator Blowdown The steam generator requires ultra high purity water for its operation.- Make-up water used in the steam generator is withdrawn from the intake forebay and essentially all of the natural impurities are removed in demineralizers. Blowdown from the steam generator is directed through a series of three demineralizers prior to discharge back into the intake forebay. Impurities contained in the steam generator blowdown consist primarily of insoluble iron and copper. Boiler treatment additives consist of ammonia for pH adjustment and hydrazine for oxygen scavenging.~ These additives are either consumed

MI0005827 during the steam generator operation or removed in demineralizers prior l to discharge. OUTFALL 008 - Unit 2 Steam Generator Blowdown 'The steam generator requires ultra high purity water for its operation. Make-up water used in the steam generator is withdrawn from the intake. forebay and essentially all of the natural impurities are removed in demineralizers. Blowdown from the steam generator is directed through a series of three demineralizers prior to discharge back into the intake forebay. Impurities contained in the steam generator. blowdown consist primarily of insoluble iron and copper. Boiler treatment additives consist of ammonia. for pH adjustment and hydrazine for oxygen scavenging. These additives are either consumed during the steam generator operation or removed in damineralizers prior to discharge. '0UTFALL 00C - Plant Heating Boiler One main heating boiler (150,000 lb/hr capacity) and one back-up heating boiler (40,000 lb/hr capacity) operate to supply heating and miscellaneous steam only when Unit 1-and Unit 2 steam generators are out of service. Impurities from the boiler water, consisting primarily of insoluble iron and copper, are discharged to the intake forebay. The boiler is fired once per month for testing purposes to insure its availability. Due to its infrequent use and the fact that the boiler seldom. achieves steady-state operation, the plant heating boiler blowdown generally contains somewhat greater concentrations of iron and copper.than the steam generator blowdowns. OUTFALL 000 - Utility Wastewater Discharge Utility wastewaters from within the plant are discharged to an~ on-site absorption pond. The ultimate disposition of these wastes is to the groundwater and then to Lake Michigan. These wastewaters include wastes from the boiler. water treatment systems (water softeners, clarifiers, make-up demineralizers) and periodically " boiler lay up water" (water containing 200 ppm hydrazine and 6 ppm ammonia used to scavenge oxygen and protect equipment during long unit outages). Other chemicals present in the discharge include dilute sodium sulfate (the chemical product of neutralizing sulfuric acid and sodium hydroxide) and alum. This discharge is monitored quarterly by a network of 4 groundwater monitoring wells. OUTFALL 00E - Sanitary Waste Discharge Sanitary wastes are segregated and routed to an activated sludge treatment plant. The treated wastewater is then directed to an on-site absorption pond for subsequent discharge to the groundwater.

SECTION i PERMir w MIO00$837 NUMBER r SEE INSTRUCTIONS ON REVERSE SIDE A. P90Vf0E A P%P & THE TREATMENT FACILITY 1,0CATith sost?G TE LOCAfl0N & TE DISOMEE POINT (S) NO OTKR IfECAMATION R8XESTED ITEM ON ROUSE SIOE & PEE. 7 c^tSN SEE To po yy1AP oN FoLLOWINC FACE EAP I 4 i i 21

su u it uuu us as-i ns i.h .Y j"a' i i ^* = S=

== == sis " ~, ' ' '".'s-",,,,4',,, , *. i note: BRIDOM AN. MICH. i .I 00A Unit 1 Steam Generator Blowdown e 8 8 8 8 8 8 8 8 8 3 [. 8 NE e TM6E E Oah$ iS QuaDeaNCgg CONIOUR IN1ERVAt 10 FEET 008 Unit 2 Steam Generator Blowdown N 4152.5-wa630/ 7. 5 ( 3. 87 h f 00C Air Heating Boiler Elowdown gg70 'W ! [ f )I Are all discharp.ed thru 001 or 002 k / ,. I M**~ [h*2 \\ [f de AMS 3667 I NE-SERIES V862 33

.'.f-l y

I \\,, ~, ';, v, o g .- i ,[ II'ik W') j' f 'li Waverland Beach ( / ,l. e . o s,,, 2 i l - (. l ' ~ i .. { s' Drinking Water Wells at Residences--- ,_ J.y f.' y

',,j- [: p e -- --v-iss

) 1,, s Plant Drinking Water Wells j f 1 501 STORMWATER DISCHARGE NORTH osemary Be ch - )~ * ' . ;)h, 7 { '.,.;[g,. Y l 'll l-001 UNIT 1 NONCONTACT COOLING f' *.e '. k-g s.>, c-3' / ).? i o j i l 003 UNITS 1 & 2 DEICING '6

y'

/ h l2 E*a ~ i ~~ 3 002 UNIT 2 NONCONTACT COOLING / pf 00D ONSITE ABSORPTION POND 00E SEWAGE ABSORPTION FIELDS i i.'p, '{ 502 STORMWATER DISCHARGE SOUTit ,,Vj Pr.ai" 4*, ,2 -. [ _. " Groundwater Monitoring Wells rico y h' 'l )I ). .i / Groundwater Monitoring Wells h. '[ / l .). 1 .. y. ( /" l }' 'y f," ... ' )' - j, pf"" d.h, Drinking Water We'lls at Residences s. /. Iivianuoa r -( p -.c g

.pf r.: ' s.... g '. s.'-.

E DESIGro SAFETY FACTOR FOR THIS CDNTROL SYSTDt? A. LIST M W MIN. l' e E 8. GIVE DE POSER CF THIS TYPE OF ANIR IN OPEN CDFireENT. I t f f f I I t t t -l C. GIW THE tusER OF THIS TYPE OF AN!% IN FOUSED COPFIPeeG. I f f I f I f f f I t TYPE c B. GIVE THE NtteER OF THIS TYPE OF ANIMAL IN OPEN g'3 CEFFINEPENT. I f f I f f I f f j i OF C. GIVE DE PO9ER CF THIS TYPE OF AN1% IN HOUSED cw f *een. A. LIST TYPE OF AN!%. ,,,,, t,,,,,,, t t,,,,,, I CPEN E B. GIVE DE PUGER CF THIS TYPE OF AN1% IN OPEN >M CDFl? CENT. I f f f f f I f I f j AND i C. GI HOUSED ce,V,E DE FUSER OF THIS TYPE OF AN!% IN POUSED , peguy, .e e i t f I i t I e CONFINEMENT A. L!$f TYPE OF AN! %. ,,,,,,,,,, g ,,,,,,,,, a E 8. GivE THE fuSER OF THIS TYPE OF Mt% IN CPEN f CorstreENT. I f I f f f f i i I C. GIW THE FUSER OF THl3 TYPE OF ANIE IN FOUSED PFt'etW. A. LIST TYPE OF AN! %. l t t t t t t t I e t i f f I f f I t i I I B. GivE THE PueER CF THIS TYPE OF ANIR IN OPEN coppgpe gur, e I t t i e i e I s C. GIVE THE t&SER OF This TYPE OF AN!% IN HOUSED.. entstnn c W. A. LIST TYPE OF AN!%. l t [ t t t I i i I f f f f i f f f I t f i N 8. GINE DE MPSER CF THIS TYPE CF AN1% IN OPEN g CCFF Ue06. C. GIVE DE fueER CF THIS TYPE OF ANIR IN 00USED CCtFifDENT. I l I I f I ' I I -} A. LIST TYPE CF ANIN. t I t t t t i f f f I t f f f I f I f f f E, 3. GIW DE POSER OF THIS TYPE OF AN!% IN OPEN $p frwFt'ofW. C. GivE THE 7020t OF THIS TYPE OF AN!% IN HOUSG CONFD D O G. ' I ' ' I I ' ' ' I A. LlST TYPE OF ANI%. t, i t i i t f f f f f f f I f I f f f I E'D d. GI4 Dt fuiEA M THIS frFE OF ANL% IN WEN n CCFFINVENT. E f f t t t f I t I e C. GtW DE POSER OF THIS TYPE OF Ahl% IN 90USED

cargpegg, i 1 1 1 1 1 1 1 I I i

23 --w-, ,,--n,, - -.., -, - -, -,. .n-- ..w ,-n ,,,.-m---. -,,, -..,. _ _ _,, _ -, ..---.-,.n._ 9 _- \\ l 200 *attre dairy cNtle (thether milked or dry coun). 2. 4 1' 3. 750 seine each weighing over 25 kilogrsas (approximately 55 pounds). 14 ISO horses. 5. 3.000 sheep or Imos.

6. '16.500 turbevs.

' 7. 30,000 laying hans or eroliers (if the f acility has continuous overficw watering). 8.. 9,000 taylm; hans or trollers (if the facility has a Ifquid menure handling system). t 9. 1,500 ducks. -l

50. 300 animat. units.

AND

Elther one of the folicwing conditions are mots pot tutants are discharged into waters of the United States through a d

manrece altch, flushing system or other similar manmade device (" manmade

means constructed by man and used for the purpose of transportirg wastes); or pollutants are discharged directly into waters of the United States which originate outside of ans pass over, across, or through the f acility or otherwise cee into direct contact with ine animals confined in tne operation.

I Provided. however, that no animal feeding operation is a concentrated animal feeding operation as defined above if such j animas feeding coeration disenerges aniy la the event of a 25 year 24 hour storm event. g The permittee shal t continue with Section 11 and address items I, 2, a, and 5 on pages 33, 33, and 35. .s f I I. 6 I u s-e i a. .I s I i - i. 25 SECTION I PERMIT M1000$D7 l NUMBER SEE INSTRUCTIONS ON REVERSE SIDE A. QD 10U CPERATE AN AQunTIC AN!mL PHODUCTION FACILITY? LIF ND. CDNTINIK TD !TDI M ITEM 10 - i-M -T- - -- - STRUCTWIES AT V0Wt FACILITY. t_, ' '. -S r i # . RACEMYS AQUATIC AmAt yEctFv i e ' i n e e ' ' ' ' ' ' ' ' ' '. Onet POODUTION C. If0!CATE IN *!O1 CALDENt PONTH 7%XIMLPI FEEDING OCCWtS. p i t t t t t I l e ,ENTUt M TOTAL NLPSER OF POWOS OF FOOD _ FED DtJt!NG THIS D. 7 I i f t t e e e r e pry,eg A. !$ THIS SPECIE A hMM OR COLD MTUt SPECIE? 3. G!vE THE MPE OF THIS SPECIE. E C. ENTER M TOTAL HNtVESTAaLE MIGHT OF THIS SPECIE 11 M PDCDUCED BY THIS FACILITY PER YEAR IN POWOS. I I f I f f f f f I PtMOS 0. ENTER M NIMWt WIGHT PitESENT FOR TH!$ SPECIE *!O1 wuD REmESENT 10Wt NORMAL OPERATION. I I I f f f I f I f POWOS SPECIES ,g, g;g OF m COLD 8. G!vE M hmME OF THis SPECIE. g PRODUCED E C. ENTUt 'HE TOTAL HMtVESTAg!g E!GHT OF THIS SPECIE e N00uCID W m!S FACILm M M IN M. I l I I f f I f f fM AT THIS FACILITY D. ENTER M NIM WIM MESN FOR m!$ SPECIE *!CH NXA.D REPRESENT Yout 70M4L OPERATION. I i i I f f I f I POLDOS A. IS TH!$ SPECIE A e OR COLD *TER SPECIE? g g us 8. G!vE THE NME OF THl3 SPECIE. Un E C. ENTER DE TOTAL HMtVESTABLE WE!GHT OF THIS SPECIE en PornrED BY WIS FACILfTY PER YEAR TN A0Lf03. I f f I f f I f f f PulACE D. ENTER THE WIPU1 WE!GHT PRESENT FOR THIS SPECIE *!CH l PfM OS etD PEP #ESE*.T YOtJi PUNAL CPERATION. I f f A. IS THIS SPECIE A hMN OR COLD MTUt SPECIE? t g g h B. GIVE M PWE OF THl3 SPECIE. U, E C. ENTUt M TOTAL HMtvESTABLE WE!GHT OF THIS SPECIE M P90DitED BY THf S FACfLITY PER YENt f N POWOS. I f f I f f f f I I POLDOS D. ENTUt DE Pnx!Put WE!GHT PRESENT FOR THIS SPECIE *!CH WIAD REPRESENT V0tJi PORMAL OPERATION. I l f f f f f I f POWOS A. IS THIS SPECIE A HARM OR Cm3 *TER SPECIE? { { COLD e l y 8. CIVE DE FWE OF THIS SPECIE. U+ E C. ENTER THE TOTAL HNtVESTAJILE hE!CHT OF THIS SPECIE o PMoutED BY Nf 3 FACfLITY PER VF)P IN PO'JOS. I I f I I f I f f f POWOS D. ENTDI DE W!*Vt WIGHT PRESENT FOR THl3 SPECIE *!CH WM.D REPRESENT Y(1Jt PIDM4L OPERAT!(N. ' f f f f I f l PtlfCS f A. IS THIS SPECIE A hAAM OR COLD MTER SPECIE? wup pages 8. G!vt M rape OF THIS SPECIE. I C. ENTER DE TOTAL tSRVESTABLE WIGHT OF THIS SPECIE M perOKED BY mf 5 FACftf fv efo VFAP TN Pnifts. ' ' ' ' ' ' ' ' ' ' PUl#0S D. ENTER M MAAl*U9 HEIGHT PRESENT FOR THIS SPECIE *!CH WALD REPRESENT YOIR PONAL CPEPATION. a e i f f I f f I f P0lf0$ f f I l 27 .-w

m. -.

-.-w..,-~w~..-,..--~-.---.m -..------,..-,..,-c-,-- .-,n,-.-- 1-SECTION I QR l{p A grooos%27 ust we me mruNG AERESS OF AU, PROPEm OMSS AaMGfr TO T)E TREAvtNT FACILITY Ate OR DISOMIE/ DISPOSAL AREA. ITEM 12 nom casum EDWAr.D P. CAPARO l] GSO ~50 DAN LAYE DR. Not.T4 List Soum B e N o, I n. 4 G 6 3 5' OF ADJACENT mitry Sount OWNEas LAYE ToWNSHif c/o GegAi o L, WAsgo ToWM5 Hip SupERNiSoR lLlt o SHAWNEE R. D. BEiocEMAw, Mr. 9 9 t o 6, W EST_ LAEE Mic-HiCA M EAST Reo ARR.ow HicawAy 29 . - _ ~ _ _ _ i SECTION 11 gER NIO00SEM7 E INSTRUCTIONS REVERSE SIDE OO/ 0)TFALL lMER i iii ITEM A. -i-Di-fulw, t is wt t unm.o tsi. m t o.5 5.. wu.i 19 tw, md RECEIVi% *TG (IE. GiufWTG CR - 0F UrACE,f.,, A, K, g,, y, p, C, g, p ig, A,g, B. =Ar G. You DISCMEE SEASCMLLfl g 3' "' # # OISCHARGE LOCATION D. IF YES, LIST DISch4EE PERIODS NA "o / D"Y 'S / cay e SCHEDULE i ,r e i i THROUGH I t i t i t o FLOW ' t i W TwurH I I I I 8 i CATE ' ' ' ' ' 8 WASTEWATER s'"'U'u m TYPE CODE _ E. LAND APPLICAT!m RATE NA i i i iu i i y WASTDaTER TYPE COCE L.J U3 t_J LJ LJ L.J 1 CONTACT F. W M E COOLING 2 NONCONTACT G. DISCHAEE SOCAI (YEMLY AVERAGE) g gfgg, gJg /g 7 ,3,4, y, A CoOuNo 3 PROCESS H. DISOWGE FLCH RATE 6 ASIS

EA/EctfD Flow RATES

,y,4,4,f,o,g,

yCCM

,a7 4 SANITARY DAILY MIN!PS 1 i i I t t i fOi h 5 STORMWATER ItAt7f98 LEJ U"lLY Wl'* I f f I I UNIT CODE tIIN10 lbl 1 MGY I. M MMIM DISchsMi FLOM RATE TO BE Au!KRIZED IN PEM'IT. AUD Ri2ED I I 1 I 2 MCO W CEDE ,f g g,4, J. MMIS DESIGN DISCH4EE FLCH RATE. g 3 CPO A. C3 You USE MAITA TEEAIMENT A:0ITivES TO TREAT Y0tR DISCHARrt? (IF No, CCNTINIK 70 ITEM 3) YES NO 8. Nkt FtfCTION, 40 CelCAL C2PC$iTION OF TI(SE G1T!WS. 2 WATER TPEATMENT NA ADDITIVES C. N#1E NO ADCRESS OF PW4fACTURERS OF M SE G ITIVES. UNITS CODE 1 Mg/l 2 Ug/' NA D. EMECTED DISONGE CDCENTRATION OF AIDIT!vES. MQ t L_;,. t .. u o iT m m t;,. AmtTgyg m i e a e i L,j ; e i t I f I J;I I f f I LJ GITivt m ,,,,, gg ;,,,, i L,,j j i i e i L_j O,o E. 00 YOU TREAT M DISO#rd TO Roc 4 GIT!WS? NA "S n'~"'"" r. T is M RemL Err:Ciocy um DisO*GE rRExeCv? NA 1Rpov4L teS./ DAY CAv5/wt. atTm m i i i L1J 13 AztTivt m i r i L._L J LJ i i i i t i L.J atityt m G. AS AN ATTAOfiENT TO ThlS APPLICATIM FMvl2 SFTCIFIC Mt All4N CR AG ATIC TUXICWF.! CAL CATA CR REFESCCE WHICH ARE AVAILA& INFCsfiATICn CN M RATE CF DECMDAfim 0F M F9X1ETS FCft EKH Ax!TivE. 31 l SECTION 11 EU5'dR M 000 5D 7 SEE INSTRUCTIONS ON REVERSE SIDE ILTIM.l. Mff6 IOtO [t f I EM A. N E w Pe0 CESS CDNuirsurim to mE DismARGE ,O, ,;,, r,o,o it, ,W, A, r,6,R i i /,Q, /, /, TH4DLD4 THIS OUTFALL Ato $tC COCE t 8. P4 CESS SOEIRA.E (YEstLY AVERAGd N VDAY l I I DAYVvrAft I I #l I C. PIIOCESS WLuf FLDs RATE '5'B'7'!'* TUTA YEAAY STREAMS b" M b g b DAILY MINIMlft I f I ' ' f f ' I CONTRtSOTING TO I/t717tM b DAILY WrM i f f I ' t S Pm D TION RATE DISCH KjA A. NME OF PROCESS CDemt!BUTING TO TE DISOdRGE THIDLDI THIS OUTFh 40 SIC CGE N b* a, I f I f f I I I I I I I I I I ' I I I I 8. Pn0 CESS SOEDIA.1 (YEMILY AWRAGd MDAY l f I DAYVW l I t I my PROCESS WI.UE FLDr RATE An Ga C. OTA YEAAY I I I I I I I I I ' kd a DAILY MINI M I I ' ' I I I I ' ' UNITS CODE 1 POUNDS I'# "I" 2 GALLONS Ut!TS /T!?E D. PROCESS PRODUCTION RATE I f I e i e i I i wL! A. NME OF P40 CESS (DNTitlBUTlfG TO TE DISOWIGE YARDS THt0Use THis CUTFE NO $!C CDDE NA i i i e i i i i t i i i e i i i i i 8. PROCESS SOEDIAE (YEMLY AVERAGd mVMY f I I DAYVyEM l f f I e mlT GJ C. PRDCESS WLiff FLD# RATE TOTA YEAALY I i i t i I I f 1 i L! g DA!LY MINIM I I I I I I I ' I I U' DAILY WIMs, I t I t I I I't t I LJ ~ b~ D. PROCESS Pf00A' TION RATE ,,,, -,, e p l- - 1 HOUR ! A. NME OF PPOCESS CDPmt!8UTING TO TE DISch4RGE },~, ',[A A g., wouse futs Oufratt Arc ste CroE 2 DAY 3 WEEK I' 38 HOURS / DAY I I I DAYS /YIM ! I ! I o MONTH mif m 5 YEAR TOTAL YEAALY l I ' ' ' ' ' ' ' ' U 8' E DAILY MINIM I I I I I I I I ' ' L! DATLY WiM l I I I I ' ' ' ' ' Id D. Pf0 CESS Pm0DITIGs RATE etTS /TIPE i t t t t t t t t LJ/t_J A. NAff CF PROCESS CDPmt!BUTING TO l'E DISOWIGE THI0tne THIS OUTFALL AND SIC CGE g I I I I ' I f ' I I I ' I ', ',,,, 3. PROCESS SOEDLLE (YEMLY AVERAGd MXRS/ DAY t t i DAYS /YEMt i I I I eo C. MIOCESS M FLOW RATE W17 C2 TOTA YMY 8 I I I I I ' ' I I Ld 8* g DAILY MINIM 71 I I ! I I I ' ! I ' gg[Ly Mgy[Mpq t f f f f I I I f LJ D. PIOCESS P500UCTION RATE UhlTS / TI*E , g,,,,,,, L _y t._, ; l t SECTION 11 PERMIT C NEO00SD? NUMBER SEEINSTRUCTIONS j ON REVERSE SIDE Ed IM [ gO,O A. IS TM DI FM THis OUTFALL DIREC TO THE GROLFO OR Grot #Od'ERS. IF PC, CONT!NIA 70 ITEM D YES ao 8. HAS A HYDROGE0 LOGICAL STI.CY OR ITS EQJIVALENT BEEN POlF0frfD Ot IS TMRE StFFICIENT CJRRENT HY30GEOLQGICAL INF0fMATION AVAll>BLE AS REQUIRED LY TLWATER RESOURCES SES NO CDelSSICN PART H CROLFOdTER RIA.E OF AL&uST 114, $O R.w.RU/ (PAGE M) FOR GROUNOWATER THIS alSTIE CR PROPUSED DISO#GE IF YES ATTACH A COPY OF THE REPORT. DISCHARGE C. ARE YOU T!?G El CCPTION FROt SLB91TT!rG A HYDROGECLOGICAL REPORT LPOER INFORMATION (@33 (5) (PACE 19) 0F Tm PART a RULES.(PAGE l6) OR FROM GROLPOdTLR MONITORING gEQUjRO(NT VES to RULE R. i .c IF YES ATTACs. IJ.0ER RULE R. DOCLtOTS RO OLPIA.ATION TO DOONSTRATE THAT YOUR DISO#GE W3ULD OUALIFY FOR NA u, ven. ARE YOU #E2KSTIM A VARIANCE FROt RILE 32.3.M (PAGE $. )IF YES, ATTACH SUCH (mtOEGRADAT!30 0F D. YES =O THE WATER RESOURCES C3 HISS 10N PART H GROLFOdTER RULES DOCif'ENTS As hECESSARY TO TRATE THE NEED FOR A VARI #rE IN TEfNS OF TE CRITERIA SPECIFIED IN RULK ) 0 (PAGE M) OF THE PART 22 rules. g E. LIST Al,L ChejlCAL StBSTANCES mlCH ARE IN MICHIGAN'S CRITICAL MAT { RIALS REGISTER TABLE IV (PAGE b) AND/OR U.S. EPA'S PRICRITY POLLUTANT LIST TABLE V [PAGE /) OR ANY OTMR StBSTANCES NOT MIME!EVED ASSENT WICH ARE CR MAY BECCPE IPLIURIQJS TO TE DESIGNATED USES OF TE CROL70dTER OR TO THE PUBLIC KALTH THAT ARE DISo#GED OR EXPECTED TO BE DISOMGED TO TM GROLDOdTERJY THIS FACILITY. EST! FATE THE Ftr.AL EFFLUE# CONCENTRATION WO RECCRD ALL DATA IN ITEM / OF SECT!31 !! IN TH15 BOCit.ET. PRESENT, DATA PROVIDED IN ITD9 7 TM APPLICANT r%Y BE RE3JIRED TO DO ADDITIOiAL WASTE ANALYSES. g A. DISOWGE CHARACTERISTICS CONCENTRATION L741TS CODE # ANALYSES SAMPLE TYPE ITEM 5

' " ~ ' " " ' ' ' "" 6'" '

(3] W l_.} 'CDD (O(NICAL OXYGu DEN #0) I I I I*I I I I I l l I

I_

l l I I ' ' '.I f f ' ' ' ' 8 8 ' I I Llj i ' ' L_ J

TOC (TOTAL ORGm!C CARaw)

WASTE A ER CHARAC* '#tiONIA NITROGD (AS h) I I I I1 I I I I I ' I.I I I I dW L! TERISTICS ( ).)

TOTAL SUSPEED SOLIDS I

I I I.I I I I ' I f I i I f f I f I L_J e UNITS CODE TOTAL PK)SPK9US (AS P) l I f I eI f f I I I I I e i f f I da f I U 1 Mg/l t IJ l ' I L- ! 2 Ug / l TOTAL RESIDUAL ot4RlhE = 3 COUNTS / I I I I.' I I ' 8 I I l.I I I I b' I 8 U 100 mi DISSOLVED 0xYGEN Mgg 4,S. U. .pg i I f,U w,y g w y S F d1 6 LBS/ DAY I I f 1 I I I I I f f I L_J FECAL COLIFORM BACTEAIA

TEMPERATURE (SLPfER)

L l. I a L! L-.1- !. L J LJ ' ' ' LI 'rENPERATURE (wlNTER) ' ' '* LJ L L._.!. L J LEl 8 L_J B. OTHER WASTDdTER CHARACTERISTICS 1 0,I L # Eg r., R p t, A, S, E, g 3,,,,,,, g,,,,,i g,, g l g $AMPy I f I f I f f I f f I I f f I i 1 I t f I i i I.I t i 1 L,,_j l i f U TYPE I I I I i f I l t i I l l t t i.1 I t I t i 1 f.I I t I L,,,) I f f L,,,,,,j 2 24 HOW ' ' ' ' ' ' I l ' ' I I I ' ' '.' I i I I ' ' f.' L_J ' ' I L.J COMPOSITC i f f f f f f I f f I t i t I 1.t I f f f I i l.I f I i U i t i U t f I I f 1 t if I t i i t f f ,t i f f i f I 1.I f 1 i U l i I U f I f I t I t t f i t t t a t t .I I I i i t t t.l l t ] (,_,J l t t U See attached sheets for data. Note: Results for triary1 phosphate esters and hydrazine in Attach!nent I. l 7 REMf7 TO: Laboratory Services Division Park West Two j 5350 Campbells Run Road Cliff Mine Road { Pittsburgh, PA 15205 Pittsburgh, PA 15275 ( 412-786-1000 I I._ A B ANAL _YSIS REPQRT CLIENT NAME: INDIANA 6 MICHIGAN ELECTRIC CO. NUS CLIENT NO: 010904 ADDRESS: P. O. BOX 60 NUS SAMPLE NO: 15021634 FORT WAYNE, - IN 46801 VENDOR NO: REPORT DATE: 03/26/85 WORK ORDER NO: 55830 ATTENTION: MR. JOHN HUGHEY DATE RECEIVED: 02/27/85 SAMPLE IDENTIFICATION: UNIT 1 DISCHARGE 02/26 TEST DETERMINATION RESULTS UNITS 1361 NPDES PART V-B M010 Aluminua ( A1) < 0.1 ag/l 1040 Borium (Bo) < 0.1 ag/l M150 Cobalt (Co) < 0.01 ag/l 1190 Iton, total (Fe1 0.05 mg/l M230 Mogreesium (Mg) 12 ag/1 1240 Mongonese (Mn) < 0.01 ag/l M260 Molybdenua(Mo) < 0.03 ag/l 1340 Tin (Sn) <1 ag/l M350 Titanius (Ti) < 0.5 mg/1 1055 Boron (B) < 0.2 ag/l WO60 Broeide (Br) <2 ag/l 1225 Color,True 110 Pt-Co W310 W Fluoride, total (F) ,, R -e o S ag/l 1390 Mitrate (N) 0.5 mg/l W410 Nitrite (N) < 0.01 ag/l 1435 Nitrogen, Kjeldahl (N) < 0.1 ag/l W440 Nitrogen, Organic (N) < 0.1 ag/l 1540 Phosphorus, total (P) 0.02 ag/l W730 Sulfate, turbidinetric (504) 27 ag/l 1740 Sulfide (S) < 0.1 ag/l W760 Sulfite (S03) <2 mg/1 1770 Surfactants (MPAS) < 0.1 ag/l l M362 HnDES PART V-C 10XIC METALS 11020 Antimony (Sb) <0.1, ag/l M030 Arsenic ( As) < 0.001 ag/l 1050 Beryllium (Be) < 0.002 ag/l M090 Codaium (Cd) < 0.005 mg/l 1140 Chreatus (Cr) < 0.01 ag/l M160 Copper (Cu) < 0.01 ag/l 1200 Leod (Pb) < 0.03 ag/l M250 Mercury (Hg) < 0.0002 ag/l

A recheck of the same sample was made by NUS.

PAT NO: 1 The first reported result was in error. $ A Halliburton Company CLtIMT ORIGINAL REastT T O: % SerWes DMelon Park West Two 5360 CampboHs Run Road Cliff Mine Road PHtaburgh. PA 15205 PHtaburgn. PA 15275 gg 412-736 1030 LAB ANALYSIS REPORT CLIENTllAME: IllDIAllA & MICH18All ELECTRIC CO. NUS CLIENT NO: 010904 ADDRESS: P. O. 30X 60 NUS SAIPLE NO: 15021684 FORT UAYlE, Ill 46001 YENDOR NO: REPORT MTE: 03/26/95 n10RK ORDER NO: 55830 ATTENTION: Ist. J0lti IRIGIEY DATE RECEIVED: 02/27/85 Salt 1E IDENTIFICATION: LAIIT 1 DISCHARDE 02/26 TEST DETERMIllATI0ll RESLLTS LBIITS ltDO Mickel (Ili) <0.03 ag/l 18290 Seleniva (Se) < 0.004 ag/l 1300 Silver ( Ag) < 0.01 og/1 M330 Thelline (TI) < 0.1 ag/l 5390 Zinc (In) < 0.01 ag/l U270 Cyenide, total (CN) < 0.005 mg/l 1500 Phenolics ( 0.02 ag/l M220 Lithine (Li) <0.01 ag/l 1110 VOLATILES-PP Ill liATER OY01 Acrolein ( 100 ug/l WO2 Acrylonitrile ( 100 ug/l OY03 Benzene (5 og/l WO5 3roeofore <5 og/1 OY06 Carbon Tetrachloride <5 ug/l WO7 Chlorobenzene <5 og/l OYo8 Chlorodibronomethere <5 ug/1 WO9 Chlorcethane ( 10 ug/l OY10 2-Chloroethylvirgl Ether ( 10 mg/l W11 Chlorofors (5 ug/l OY12 Dichlorobronomethane <5 ug/l W14 1,1-Dichloroethene (5 ug/l DV15 1,2-Dichloroethene <5 og/l W16 1,1-Dichloroethylene (5 og/l DV17 1,2-Dichloropropone <5 ug/l W18 1,3-Dithloropropylene (5 ug/l OVit Ethylbenzene <5 ug/l W20 Methyl Broeide < 10 ug/l OY21 Methyl Chloride < 10 mg/l W22 Methylere Chloride <5 mg/l OY23 1,1,2,2-Tetrachloroethene (5 ug/l W24 Tettochloroethyler4(Perchloro) <5 mg/l OY25 Toluene <5 mg/l PAE NO: 2 h A Halliburton Company CLIENT ORIGINAL REelfT TO: % Services DMsion Park West Two NUS 5350 Carvtsells Run Road Cliff Mine Road Nrgh, PA 15206 Pittsburgh, PA 15275 mg 412-7a8-10e0 LAB ANALYSIS REPORT CLIENT NAIE: INDIANA & NICHI6All ELECTRIC CO. NUS CLIENT NO: 010904 ADDRESS: P. O. 301 60 11US SAlfLE NO: 15021684 FORTliAYME, IN 44001 VENDOR 110: REPORT BATE: 03/26/95 nl0RK ORDER NO: 55830 T1ENTION: IWt. J0101 HUGIEY DATE RECEIVED: 02/27/85 SAIFLE IENTIFICATION: LAIIT 191SCHAR0E 02/26 TEST KTERNIIIATION ESLA.TS LpllTS W26 1,2-Trens-Dichloroethylene <5 mg/l DV27 1,1,1-Trichloroethane (5 og/1, IV28 1,1,2-Trichloroethene <5 ug/l OY29 Trichloroethylene (5 mg/l IV31 Vinyl chloride <5 mg/l 0120 ACIDS - PP IN niATER 0401 2-Chlorophenol ( 10 ug/l 0402 2,4-Bichlorophenol ( 10 ug/l IA03 2,4-Dimethylphenol < 10 ug/l OA04 4,6-Dinitro-o-cresol ( 50 mg/l IA05 2,4-Dinittophenol ( 50 og/1 0406 2-Nitrophenol ( 10 ug/l lA07 4-Nitrophenol ( 50 ug/l DA0S p-Chloro-a-cresol < 10 ug/l IA09 Pentechlorophenol ( 50 ug/l 0410 Phenol ( 10 og/l lAll 2,4,6-Trichlorophenot < 10 ug/l DE30 Acid Extraction-lister 0130 BASE NEUTRALS - PP IN liATER OM1 Acenophthene ( 10 ug/l 1902 Acenophthylene < 10 ug/l 0903 Anthrecone ( 10 ug/l IB04 Denzidine < 50 ug/l 0805 Benzo (s)Anthrecene ( 10 ug/l 1906 Senzo(ePyrene ( 10 ug/l 0007 3,4-lenzofluorenthene ( 10 ug/l 1908 Benzo (ghiPerylene ( 10 ug/l 0009 Benzo (kFluorenthene < 10 ug/l 1910 lis(2-Chloroethoxy) Methene < 10 ug/l 0811 lis(2-ChloroethylEther < 10 mg/l 1912 Fis(2-ChloroisoprepylEther < 10 mg/l 0813 31s(2-EthylhexylFhthelete ( 10 ug/l PAE NO: 3 i A Mhdon Company CLIENT ORIGINAL I REtstT TO: Laboratory Services Division Park West Two NUS S350 Campbelts Run Road Cliff Mine Road Pittsburgh, PA 15205 Ptttsburgh, PA 15275 412-788-1000 LAB ANALYSIS-REPORT CLIDif IIAIE: IllBIAlle & NICHI6All ELECTRIC CO. NUS CLIENT 110: 010904 ABORESS: P. O. BOX 40 NUS SAIFLE 110: 15021684 FORT MAYlE, Ill 46001 YD80R 110: REPORT MTE: 03/26/85 UORK ORK R 110: 55830 ATTDITIOll: Ist. Jolti illOlEY DATE RECEIYEtt 02/27/95 SAlfLE IKNTIFICATION: 1811T 1 DISCHARiiE 02/24 TEST KTERNillATIO11 MSIA.TS UNITS 314 4-Brosophenyl Phenyl Ethet < 10 eg/l 0915 Butyl Benzyl Ph h lete < 10 mg/l 1916 2-Chlotonoph h lene < 10 ug/l 0817 4-Chlorophenyl Phenyl Ethet < 10 ug/l l318 Chrysene < 10 ug/l 0919 Dibenzo(o,h)Antheocene < 10 ug/1 8320 1,2-Bichlorobenzene < 10 ug/l 0521 1,3-Dichlorobenzene < 10 mg/l IB22 1,4-91 chlorobenzene < 10 og/1 0B23 3,3'-Bichlorobenzidine ( 10 mg/l 1924 Diethyl Phthalate < 10 mg/l 0325 Dioethyl Ph h lete < 10 ug/l ll26 Di-N-lutyl Phtholote < 10 eg/l 0327 2,4-Dinittstoluene < 10 ug/l i IB28 2,6-Dinittotoluene ( 10 mg/l 0829 Di-N-Octyl Ph h lete < 10 ug/l 1830 1,2-Diphengthydeazine(Azobz) < 20 ug/1 0831 Fluotenthene ( 10 ug/l 1932 Fluotene < 10 ug/l 0833 Hexachlorbenzene < 10 ug/l 1934 Hexachlorobutodiene ( 10 mg/l 0835 Hexachloro-cyclopentadiene ( 10 ug/l 1836 Hexachloroethane ( 10 ug/l 0837 Indeno(1,2,3 cd) Pyrene < 10 ug/l 133B !sophotone ( 10 ug/l j 0839 Iloph h lene < 10 ug/l ll40 Nitrobenzene < 10 ug/l 0841 N-Nitrosodieethylaeine ( 10 ug/l 9942 N-Nitrosodi-N-Propylonine ( 10 ug/l 0943 N-Nitrosodiphenyleine ( 10 ug/l i 1944 Pher4nthrene < 10 ug/l OH5 Pyrene ( 10 ug/l PAE 100: 4 h A Ha!!! burton Company CLIENT ORIGINAL IIEtelT TO: Laboratory Services Dhrision Park West Two hNUS 5360 Campbelle Run Road Cliff MineCoed a Pittsburgh, PA 15206 f%ttsburgh, PA #275 g 412-788-1000 l._ A B ANALYSIS REPORT CLIDIT 11AfE: INDIANA & MICHIGAN ELECTRIC CD. NUS CLIDif 110: 010904 ABIRESS: P. O. 30X 60 NUS SAlfLE NO: 15021684 FORT WAYE, IN 46001 YDS 3R 110 EPORT DATE: 03/26/05 UORK ORDDt 110: 55830 ATTENTIWl 1st. J0181 IRIGIEY DATE RECEIVE 3: 02/27/95 SAIFLE IDDITIFICATION: lRIIT 1 DISCHARGE 02/26 TEST DETERMIllATI0lt RESIA.TS UNITS 3 46 1,2,4-Trichlorobenzene < 10 mg/l OE25 Base lieutrel Extraction-Veter 0141 PRIORITY POLLUTANT PCB'S OE11 PCB Extraction - Water IP19 PCI-1016 ( 0.5 mg/l DP20 PCI-1221 ( 0.5 ug/l lP21 PCB-1232 ( 0.5 ug/l DP22 PCB-1242 ( 0.5 ug/l IP23 PCB-1248 ( 0.5 ug/l DP24 PCB-1254 < 1.0 ug/l IP25 PCB-1260 ( 1.0 ug/l R450 RADIUM 226 AND 228 19 04 Rodium-226 < 0.4 pCi/1 R805 Radium-228 <1 pCi/1 R800 Gross Alphe <4 pCi/1 R801 Gross Bett 5.0 t/-1.2 pC1/1 1032 Aneonia os M (distillation) < 0.1 ag/l W050 BOD, 5-dog (02) <1 ag/l 1100 Carbon, organic (C) 24.6 og/1 W120 C0D (02) <5 mg/l l 1610 Solids, suspended at 103 C 2 og/l 1 ComOITS: Reviewed and Approved by: PM PAGE NO: 5 $ A Halliburton Company CLIENT ORIGINAL REterT TO: Laboratory Services DMeion Park West Two NUS 5360 CampboHs Run Road CHff Mine Road Pittsburgh, PA 15205 Pittsburgh, PA 15275 mg 412-7as-toso 4 LAB ANALYSIB REPORT CLIDif IIAIE: 15:A114 & NIDl!8All ELECTRIC CD. NUS CLIDif NO: 610904 AISRESS: P. O. DOX 40 NUS SAlfLE NO: 15021685 FORT WAYlE, IN 46001 VDIDOR 110: REPORT DATE: 03/26/85 WORK ORDER 110: 55830 ATTDITI0lls IEt. J0101 tilGIEY DATE RECE!YES: 02/27/85 SAltLE IDDITIFICATION: UllIT 1 DISCHARGE - GRAB 01 02/25 0825 1EST BETERNIllAT10ll RESLLTS UNITS 3A32 l'ecal Califore - 1F91 15 co1/100e1 W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 8.1 W680 Oil, extrtction gravinetric 1.0 eg/l ColflENTS: Reviewed and Approved by:.31C @ A Halliburton Company CLIENT ORIGINAL RESIIT TO: Laboratory Services DMelon Park West Two NUS 5360 Campbsite Run Road Cliff Mine Road Pittstwrgh, PA 15206 Pittsburgh, PA 15275 412-788-1000 gg LAB ANALYSIS REPORT CLIDIT IWE: IMBIAllA 6 MICHIGAll ELECTRIC CO. IlUS CLIENT NO: 010904 ABORESS: P. O. 30X 40 WS SAIFLE NO: 15021686 Folti ilAYIE, IN 46001 YDSOR 110: I D 0lti M TE: 03/26/85 ll0RK ORMR 110: 55630 ATTENT10ll IEt. 10181 HUEEY DATE RECEIYER: 02/27/95 SAlfLE IDDITIFICAT10ll: UllIT 191SCHAlt0E - GRAB 82 02/25 1420 TEST MTERMIllAT10ll RESLLTS 1AITS 3A32 Fecal Califors - 1F11 <3 col /100e1 W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 8.1 W680 Oil, extrettion grevisettic 3.2 ag/l l C0leENTS: Reviewed end Approved by: JIC $ A Halliburton Company CLIENT ORIGINAL. ReestT To: l aboratory Serdose Division Park West Two NUS 5360 Wie Run Mood Cliff Mine Road M r9h,PA 15206 Pittsburgh, PA 15275 Ng 412-788 1000 j l LAB ANALYSIS REPORT CLIDIT IWE IllDIAllA & MICHIGAll ELECTRIC CO. NUS CLIENT NO: 010904 ABORESS: P. O. DOX 40 NUS SAlfLE NO: 15021687 FORI liAYlE, IN 44001 YDIDOR110: REPORT NTE: 03/26/85 UORK ORDER 110: 55830 ATTENTI0ll: Itt. JOHil MUGHEY DATE ItECEIVED: 02/27/95 1 SAltLE IDENTIFICATION: UllIT 1 DISCHARGE - GRAB 43 02/25 2021 i TEST DETERMIllATI0li RESULTS UNITS 1A32 Fecol Califors - IPN 4 col /100e1 U150 Chlorine, residuel DPD (C12) < 0.1 ag/l i 1490 pH 8.1 9600 Oil, extraction gttvisettic 1.8 ag/l 0019ENTS: Reviewed and Approved by:.mC h A Halliburton Company CLIENT ORIGINAL i REteff TO: l.aboratory Services Division Park West Two NUQ' 5300 Campbelle Run Road Cliff Mine Road Mttsburgh PA 15206 Pittsburgh, PA 15275 gg 412-788 1000 LAB A N A L. Y B "E S REPORT CLIDIT MANE: ISIANA & NICHI6All ELECTRIC CO. IlUS CLIENT NO: 010904 ABORESS: P. O. 30X 40 NUS SAWLE NO: 15021688 FORT WAY E, IN 44001 YDSOR NO: EPORT MTE: 03/26/95 WORK ORDER NO: 55830 ATTENTION: lWt. Jolti HUGEY MTE RECEIVED: 02/27/85 l SAMLE IKMTIFICATION: UNIT 1 DISCHARGE - GRAB H 02/26 0225 TEST DETERNIllATI0ll RESLLTS UNITS 1432 Fecol Colifore - IFil (3 col /100e1 W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1 I490 pH 8.1 W680 Oil, extraction gravinetric 1.8 og/l i l (20LENTS: Reviewed and Approved by: JIC h A Halliburton Company CLIENT ORIGINAL t a 4 SECTION 11 PERMIT NMN F SEE INSTRUCTIONS NUMBER ON REVERSE SIDE asu. m ,o,o,/, ITEM ~E PEW USE DISCnvGERS ML;, PROVIM EerECTED VALLES FW DE QUANTITATIVE NO -STG -r- -ESSE = =. - =-5. W QJALITATIVE INFORmilJe REuutSTED BELOW. jS THis FACILITY A PRIPWtY If0USTRY? (REFER TO TABd !A PK4 N) A. YES to i f F.e, r4 70 E) ( rF VES, 00 To g) P^10RITY 3. Le!CATE TYPE OF PR!$RY IrOUSTRY AS LISTED IN TA83 IA PEE d!1. POLLUTANTS WN wf m M I TIM fbfblbfOl IP ut RI ANO C. DCES THIS OUTFE DISCHARGE C34TAIN ANY PROCESS WASTEWATER? fir N, o TO E) (tr vES, GO TO 0) YES NO ADDITIO N INF@RMATION D. IPCICATE MelCH GC/MS FRACTIONS MUST BE TESTED FOR. (REFER To TABLE [A PEE 41) NULATILE FOR NQIE! FCR EAOf GC/MS FRACTION OECKED,EACH SPECIFIC ORGANIC T0x!C POLLUTANT WITHIN SURFACE EACH FRACTION M BE AieALYZED FOR (SEE TABLE I1A rare '!2. IN ADDITICW, E PRIP*ARY BASEhEUTRAL WATER troJSTRY APPLIC#.TS w TH A PROCESS WASTEWATER DISCHARGE t3dI PROVIDE QUANTITATIVE DATA M ACH MANT IN TABLE It!A NE @ DISCHARGE h CID ONI.Y RECWD E DATA ON FCfMS PROVICQ (ITEM d IN THIS B00NLET. (CONT!PAE WITH E-K BELOW) PESTICIIE E. IF /jg SWFACE aATER DISotARGE APPLICANT (PRIMARY OR SCCOOARY IN0USTRY), REGARDLESS OF TnE TYPE CF DISihARGE, CD4 OR HAS REASON TO BELIEVE THAT AtN POLLUTANT LISTED NOT APPLICABLE /BELIEVG ABSENT IN TABLE IIA AND IVA PAGES d-M 15 DISOtARGED FROt ANY Q:TFALL,T)E QJANTITATIVE I 3EI BE PROVICED. RECORD h DATA ON F0mS PROVIDED (ITEM 7) IN TH15 BOOKLET. PRE / IS MM F. IF ## SWFACE HATER DISOtARGE APPLICANT (PRIMtY OR SECDOARY INDUSTRY), REG #tDLESS OF TYPE OF DISO)VtGE, ROfS OR HAS REASON TO BELIEVE ANY Pot 1UTANTS LISTED IN NOT APPLICABLE /8ELIEVED ABSENT TABLE VA PEE M ARE DISCHAMED FRP ANY OUTFALL TE APPLICANT taaI DESCRIEE REASONS FOR TM POLLUTANT BElfG PRESENT #D PROVIDE ANY AVAILABLE QUANTITATIVE DATA. RECDtD E DATA CN FOMS PROVICQ (ITEN 7) 1N THIS BOOKLET. G. E SWFACE HATER DISOWGE APPLICANTS (PRimRY Ato SECONDARY ltOJSTRIES) MO: 1 OR PwuACTsES 2, 4, - TRIOuR0p>EroxY ACETr ACr (2, 4, 5-T); , 4. FTRIOuROPEP0xY PROPN4fC ACID (SILVEX,, 4, , TP)$'; 0, DirETHYL Ome, 4, FTRiouR0PHENYL)2-DIOuROPROP 0NA 4, yty p eR0pteoxY ETHYL 2, Rs0N PtOSPHDROTHICATE (R0r#EL); 4, VTRIOtCe0PHE?OL (TCP); OR HEXAOLOROPHEFE (tCP); (ALL DATA FOR THE ABOVE PtJST BE GEfERATED UStrG STAPO#tD ANALYTICAL CALIBRATION PROCEDWES) OR NFCWS OR HAS REASON TO BELIEVE THAT TCDD IS OR PHY BE PRESENT IN T)flR DISOdRGE. M,jl PEPCRT ftJALITATIVE DATA, GE?ERATED MilOj uiD A SCREEN!PG PROCEDtFE NOT PRESENT/CATA IS ATTACHED .CAuBRATED WITH 4tALYT! CAL STNCARDS, FOR 2, 2, / )8, - TETRAOLORODIBENZD-P-DIOx!N (TCCD). RECCRD E DATA ON F0m$ PROVIDED (ITEM / IN THIS In0KLET. J. IF M SURFACE MATER DISCHARGE APPLIC#dT Kf06 OR HAS REASON 70 BELIEVE THAT PCT APPLICABLE BIOLOGI T0x! CITY TESTS hERE MADE IN THE LAST TWEE (3) YEARS CN ANY OF T4 APPLICNdT S DISOtARGES OR De A RECElvlPG MATER IN RE1ATION TO A DISOWGE, PROVIDE THl3 If.70Rh4 TION AS #1 ATTAOfENT TO This APPLICATION. APPLICABLE /SEEATTACHED K. IF A CordTRACT LAllmAT3tY OR COdSLA.T!?G FIRN PERFCRr0 ANY OF TE #4.AYSES REQUIRED fCT APPLICABLE BY THIS APPLICATICN, PROVIDE THE feer

AND ADWESS OF EAOt LABOPATORY Ot FIRPt 40 THE #eALYSES FERFQPMD AS #4 ATTAOfsNT OF THIS APPLICATION.

Qw APPLICAad/SEE ATTACHG L. 00 YOU DISOWG[ ANY OTMR TCxic OR IPULft! ICAL SLSSTANCES NOT LISTED IN TASLES IV PEE D #D IIA T40Ur44 VA Parts (-fa. IF YES, T'EN IDENTl'Y TM '0I APPLICA8LI OelCAL SLSSTAtCES NO ESitMATE M FINAL EFFLUENT CDCENTRATIONS. SLDtli THis IWMATION AS #4 ATTAQt1ENT TO THIS APPLICATION. APPLICABLE /SEE ATTAGED l 1 9 ] SECTION ll pERuir m MW%M NWBER 7 SEE INSTRUCTIONS ON REVERSE SIDE t td t /t ITEM A. USE THIS DATA 9EET TO RECORD !WORMATION AS REWIRED IN: (OECX APPROPRIATE BOX FOR WICH IN80RMATION THIS DATA SHEET REPRESD:TS.)

1. SECTION II, ITDt '4-E.

GRoupenTet DisotNr4 !*aomAff0N (PAGE 55) CRITICAL

2. SECTION !!, ITEM 6. Pol 0RITY POLLUTANTS IN SUtFACE MTUt DISOtWE (PAGE 37) 3.

8. BELON: CRITICAL MATellALS (TARE fv) !N St#tFACE MTUt DISOtNIGE (PAGE 39)

POLLUTANTS e HAZARDOUS SU8 STANCES 8. LIST ANY CRITICAL MATERIAL (TAst.E IV PAGE 6) NOT ADWESSE IN SECTION !! (TEM 6 *RIORITY 10T APPLICA8LE POLLUTANTS WlCH YOU ICKW OR HAVE REASON Tn BELIEVE TO BE PRESENT IN T}E DISCHARGE. SEE W REVERSE SIDE OF TNis PAGE FOR F@M.R DIRECTIONS. DISCHARGE ' APPLICABLE (SEE BELOW) .J A. WPE OF CRiflCAL MATUt!AL OR PRIORITY POLLUTANT g g g g g g g g 5 I 8. AVERAGE CONCENTRATION; SAMPLE TYPE; I 0F ANALYSES g g g g_g g g g g 3

I
W CODE C.

MAXIM 79 CDCDmtATION NO FASS A. IWE OF CRITICAL MATERIAL OR PR!Gt!TY PEUTANT g g g g g g g g 8 # #'*"'#IE8 8. AVERAGE COCCmtATION; SAMPLE TYPE; # OF ANALYSES l g g g,g g g g 2 C. MAxle CahCDmtATION APO MASS Wlf CO[E Wlf CODE t t t 1,f I f a y e, t e,f ,,, W UNITS CODE A. NAME OF CRITICAL MATERIAL W PRIQtITY POLLUTANT t l l l l l [ l h 9 g /g wtT CODE SAP 9LE TYPE # M ANALYSES g y S. AVERAGE COPCENTRATION; SAMPLE TYPE; P OF NtALYSES l l g g,l g g g g y 4 WIT GDE Wii CD0ti 3 LBS/ DAY 3 C. Mx!M C0tCENTRATION WO MASS g,,, g,,, g,,, g,s , t, y 4 MG/ DAY A. fWE OF CRITICAL MATERIAL Gt PRIORITY POLLUTANT l l l g g g g g III 3. AVERAGE C0tCCITRATION; SAMPLE TYPE; # OF ANALYSES g g g g,g g g g W1 CODE, W1 m 2 C. pax!M CottemtATION AFC MASS SAMPLE TYPE A. ftAPE CF CRITICAL PATUt!AL OR PRIORITY POLLUTANT g g g g g g g g cRA8 2 24 HR. COMP 8. AvEPEE CCPCCITRATIONJ SAlfLE TYPE; # CF ANALYSES ' g g g

,l g g g W W - f,0F YSES WI WI C00E C.

MAxt%79 C0tCE*tTRATION AtO MASS CODE, A. ftAFE OF CRIT! CAL MATERIAL OR PRIORITY POLLUTANT t l l 1 l t l [ g 8. AVERAGE COCENTRATION; SAMPLE TYPE; I 0F ANALYSES l l 9 l ,l l g g g 2 b C. %xfitM CDCD(TRATION AtO MASS g 4. NAtt OF CRITICAL MATERIAL OR PRIORITY Pat 1UTANT i I I f f I l l g Lftli N SAPPLE TYPE # W #AvsES 7 8. AvDIAGE CONCDmtATICN; $ AMPLE TYN; # OF hhALYSES l l g gg g I I U U l f l g t#41T C00E W4I W C. max!M COCENTRATION Ate MASS I I f f .I f f f L_J l I t i.I t ,, Lg A. WPT W CRITICAL MATERIAL OR PRIORITY POLWTANT g g g g g g g g g so

3. AVEPNI CC'CDmtAtl0N; SAMPLE TYPE; # W ANALYSES g g g g,g g g g

,g,,,,,,,,, yy A = C. Mo n,, m en., Tim O MASS A00 TranAL Pact $ OF tnt 3 tret 7 APE Afteos FOR T>< REST OF TH CRITICAL M YEs MrUt Au uc/OR PR!aRITY PuuTANTS REWIRC 70 BE REPORTD. O NO I n SECTION 11 PERMIT 000 78M NUMBER 7 EE INSTRUCTI NS N REVERSE St E GE4J. UTER io>o A i ITEM A. == - D - e, w, t is,wi s. une loa;. =,o 41 s.. wa.i '9 w. 1 .. wai- -T= o c. - -

s F=

,t 4,x,e, .".1 u, e.4.", ,,.,, I C. YOU DISCMRfA SEASWA&.LYl IF No, um TO El m 5 DISCHARGE LOCATION D. IF YES, List DISCHAAGE Put!@$ NA 5/ mv m./ mv SCHE 0t,tE w e i e TwtoucH i

1 r i o

FLOW L._1_J t i i THa0tcH I ' e i l i RI.TE e i t i t I nere i f I t t I WASTEWATER IN./4. W./0Af IN./W%. TYPE COOE_ I' LA'O "ICAN " 1 I faLJ l 8 I L_J l f Ie U M I F. TYPE & HASTEhATER DISO WIGE h d y U 2 NONCONTACT G. O!50990E SO{DtA2 (YUPl.Y AVERVA) MDAY l !Ql DAv/YUR I f-1 i 4 i3i ), o i 1io i mbl CODE 3 PROCESS H. OlSCHMGE FLOW RATE %!' MD FM MTE ~ a m, i e 4 SANITARY 5 STORMWATER DAILY MIN! M i i t t I t tgi t/t71IthI h DAILY PWEIM i i t I UNIT CODE 1 MGY 1. 7)( MAxlMi>9 DISCHAPGE FLOW RATE TO BE AUTHORIZED IN PER4lT. AUTWW I.'H) I i f I l I l I 2 MGD m!I.ccDE Iff IT ' 8 L'J# J. MxlFU1 CESIGN DISCHARGE FLOd RATE. Ot$lGN I I i f 3 CPD IO VGU USE MATY.R TREATMt. T ADDITIVES TO TREAT Y0tJt DISCHUtr47 N A. (IF NO, COdTtNIK 70 ITD9 3) YES 'O .. h4E FLPCTION, Ato CHEMICAL C01 POSITION OF Tf4SE ACCITI W S. 2 WATER TREATMENT gg AMITIVES C. 4V1E Ato ATRESS & MAfAEACTWERS OF M SE ACCITIVES. UNITS CODE 1 Mg/l 2 Ug/l NA MINIPt.71 tAITS AWRK4 I. NITS MAA!PtPt WI TS 0. E)aPECTED DISchAJIGE CDCENTRAfl0N OF GIT!WS. NA mu

cme cer i e t

I i L_J J' ' i ' ' LJ G ITIVE h4T e e ie 1 L,,,,j j AICIT!W Pwt t ' ' 8 L!J t ' ' I i LIJ' ' ' ' ' LJ AECIII4 M t i e i I L_J J t i ' I i t._.J J ' ' ' ' ' L.J E. 00 YOJ TREAT TIE DISOME TO RDtM GlTIVES7 gg YES Pc F. W1AT 15 NE RDovAL EFFICIDCY AND D150#1 FRE'ACCY7 QQ D1?M M ""' IRDovAL $$./ DAY M't at. ADDITIVE NVE I I f 1 I I L.3 ADDITIVE he1E I i i I l i L.J i i e i f I l_ ) A0!T!vt WT G. A5 AN ATTAottNT TO THIS ATM.!CAflJ. F'CVIDE SS'ECIFIC M#t'ALI AN rp A0 Afic TONICOLTICAL [ATA @ DEFE9CdCE sA410e APE AVAIVIAI AND INFCaf9713e Od f>( RATE & CECAACAfl38 UF T4 f5*00ff $ FOI EACH KEilflW. 31 l SECTION 11 gR g greco Sp7 I p - SEE INSTRUCTIONS ON REVERSE SIDE (UTFALL fifRR ioioi A ITEM A. wE Or Pn0 CESS CCnTRrBuTim To mE OtSOwiGE , g),,4, C, o,o, L, , W, A,7,E,g,,Q,9, /, /, De0UG4 ml5 atMM #D 1IC ("CCE B. PROCESS SOEDLLE (YENtLY AM) MDAY f I I Days /yr3p I3 f d iIf C. PROCESS % Cuff FLDW RATE ' 5 ' H' 7' / ' "I ' PROCESS TOTA YENtLY STREAMS 94$)$ ! j'l84 8 LOW 04I4 m !LY e t e 8 ' ' f I I ' f IOf L.h CONTRt8UTING TO DAILY WIM I I I I ' I f {8 f 13I o[c A c,E "' " ' '58'"*"'"*" "^ Ys M ' ' ' ' ' ' ' ' I A. MME OF P40 CESS CONTRIBUTIm TO DE DISOWIGE D90Ur44 D413 OUTFE #D SIC CODE I I I I I I I I I ' ' I I I I I I I I I B. PROCESS SOEDt1E (YEARLY AVERAGE) M DAY l i t DAYS /vtMt i i l I ey PROCESS NOL1fE FLDW RATE mir w.A C. OTA Y m y I I l I I f I I ' I L--.I 8" [ DA!LY MINte I ' I I I I ' I ' ' tJNITS CODE 1 POUNDS I" "I" 2 CALLONS D. PROCESS PEDUCTICN RATE 3 CU8tC A. nee OF PROCESS CDNTRIBUTim TO DE DISOARGE YARDS DetouGt m!S OUTFM Arc SIC CDCE ,,,,,,,,,,, f f f I I f f f f T0

s. PROCESS SOEXAE (YEARLY AVERAGd HDLRS/ CAY I I I OAYI!YEMI 6 MGD gg C.

PROCESS VQ.LPE FLOW RATE w TOTAL YENtLY I I I I I I ' ' ' ' g DAILY MINIMM i I i I f f f I ' ' U DA!LY WIM I I I ' I f ' ' ' I U D. Mt0 CESS PRODUCTION RATE TIME ,, i t t t t t I 1 HOUR A. NAME OF PROCESS CDNTRIBUTING TO DE DISOdRGE NA IU 2 DAY 3 WEEK B. SS N (YEARLY AM) muPS/ DAY I I I DAYS / YEAR I f f I W1 CODE C. PrRESS NULLfE, FLOW RATE y E 8' [ DAILY MINIMM i f f f f 1 I f f f L_.J D4 fly Wie I I I I I ' f ' f t t-- j IAITS /TIPE D. PROCESS PEDUCTION RATE t t t I t t I f t t _V L_J A. MNE OF P90 CESS CONTRIBUTING TO DE DISOdRGE DF0lfH ik!S OtMM NO SIC CCCI I I I ! " f ',,,,,,,,,,,,, B. PROCESS SOCALE (YENtLY ANERAGd M CAY I t I DAYS /YENt i f f f g tr4lT C2 g C. PROCESS WLifE FLOW RATE TOTE YMY l ' I I I ' ' ' ' ' I Oc [ DAILY MINIMM I I I I I I I I i t U De rLY Pdx!MN I t I f f f I t f f L _.J D. PROCESS P'00UCTION RATE UNITS / TIPE i i i t t t t t t LVU 5 [ SECTION 11 PERMIT W VI0000807 E NUM'ER SEEINSTRUCTIONS ON REVERSE SIDE 1 (LTFML !UfG ,d,o,a ITEM " - o' - ~iS - T - ca GROUhDeATmERS.IF PC, C3dTINUE TO ITEMw$ A-YES Po 8. NAS A HYDR 0 GEOLOGICAL STOCY OR ITS EQUlVALENT BEEN PERF0fMD OR 15 THRE StFFICIENT CURRENT HYDf0GEOLQGICAL INFGNATION AVAll.AaLE AS REQUIRED RLT(WATER RESOURCES YES. NO CONISSIOe PART d GROL70 EATER RULE OF AUGUST 14,193) R.5Z5 uur (PEE 43) FOR GROUNOWATER THIS EXISTING OR PROPOSED DISchMGE !F YFS ATTACH A COPY OF THE REPORT. DISCHARGE C. ARE YOJJP T!?G #4 EXDff!CN FRO 1 SUBMITT!!G A HYD OGE0 LOGICAL REPORT Lt0ER INFORMATION RtA.E R. >c. 7 (10) (PACE %) at FRot GR0t70e4TL4 70NITORING 3EQUjREMENTS YES to Ur.CER pule R. 25.E03 (5) (PEE 47) 0F TW P4tT H RtLES. IF YES ATTACH DLCIOTS A O EXPLNeATIOt TO CEOeSTRATE THAT YOUR DISChMGE WolA.D OUALIFY FOR xe D E'97 !^m D. ARE YOU REQUEST!rG A VARIANCE FRoi RgE 323.205 (PAGE If DOCEGRADATION) 0F TII IO TM WATER RESOURCIS CONISS[0N PAJef R GR0lf DWATER RtLES. IF YES, ATTACH SUCH DOC #ENTS AS NECESSARY TO TRATE THE NEED FJI A VAR! MICE IN TE7NS OF T4 q CRt!ERIA SPECIFIED IN RULE ) 0 (PAGE 41) & THE PART 22 RULES. E. LIST Al.L O*EMICAL SLESTANCES WHICH APE De MICHIG;W S CRITICAL MATERIALS REGISTER TABLE IV (PEE h) AND/OR U.S. EPA'S PRI0tlTY PtXLUTANT LIST TABLE V (PAGE /_) OR ANY OTWR StBSTANCES NOT APPLICABLE / BELIEVED ABSENT 44fCH ARE Ot MAY BECOT INJURIOUS TO T4 MSIGNATED USES OF TE GROLPOdTER OR TO THE PUBLIC HEALTH ThkT ARE DISCHMGED CR EXPECTD TO EE DISCHUGED TO TM GR0tPO*ATERJY THIS FACILITY. ESTIMATE THE FlhAL EFFLUENT CONCENTRATIO8 NO RECORD ALL DATA IN ITEM / OF SECTION !! IN THIS 90C4.ET. PRESENT, DATA PROVIDED IN ITEM E TK APPLICANT MAY BE REQJIRED TO DO ACDITIOdL HASTE AIAYSES. M A. DISchMGE CHAPACTERISTICS CONCENTRATION L74173 CODE # #dLYSES SAM'LE ^" ~ ITEM ' ' ' ' ' ' ' I ' I* U '80E5 (FIVE DAY BIO 0GICAL OXYGEN CO%ND) 'CCD (OEMICAL CXYGEN ImVC) l I I I*8 ' I I l f I I.8 f I I L. ) L L.) L! ' E=, u; u-> u TOC (T01 _, _, C RAc. . _,A,,, _ (AS,) a u_, a TERISTICS

TOTAL SUSPCCCD SOLIDS I I I I.I f f I I I ' II I I l L13

[._1 J U UNITS CODE TOTAL PH;SPHORUS (AS P) I I i _f .1 I f f I I l !. I f f I di! ' L! 1 Mg/l d' ' ' L-J 2 Ug / l TOTAL RESIDIAL 04.ORIP.E 3 COUNTS / 100 mi CIISCLVED ON MIN o S.U. .pg I l I, L,J ,,,y ggj w y 5 'F l}l I ' ' LJ 6 LBS/ DAY I I I I I I I I I ' I I FE COLIFORM BACTERIA I f I.Lj ' I I L! ' ' I l J

TefERAT1.lRE (SitttR) a y

8 ' '. L_J l ' '. LJ Lb' lJ 'TUPERanpE (ntuTER) B. OTHER WASTEWLTER CHARACTERISTICS ,0 t t,L,1 9 6,R ! E,A,S,E, y gg_g g J AMPLE. t I r i t i i e i ' 1 i i I 8.' 1 ' ' ' ' ' 8.8 8 ' i U 1 I f L.) I t f I t t t i I i f i i t t i.I f f I I i 1 I.I I f I L_j i f I L_) 2 24 HOUR y y COMPOSITC i i i i f f f i i f 1 i I f I i.I f f I i f f.I 1 1 1 L,,,J t i f LJ I I I t t t t I I f t I f i f f.I i f f i 1 I 1. I f f f U W L) e i i r e i i i e e t i l i r I.i 1 i i i f i 1.t t i I L_1 t i L.J See attached sheets for data. Note: Results for triary1 phosphate esters and hydrazine in Attachment I. l 7 REtefT 70: Laboratory Services DMeion Park West Two 5380 CampeeHe Run Road Cliff Mine Road Ptttetwrgh. PA 15206 Pittsburgh, PA 15275 i g 412-788 1000 l J LAB ANALYSIS REPORT CLIDif IIAE IllBIANA & MICHIGAN ELECTRIC CO. NUS CLIENT 110: 010904 ADDRESS: P. O. 90X 60 110S SAWLE 110: 15021704 l F0ftf WAYE, IM 46001 YDIDOR110: 1 EPORT DATE: 03/26/85 UORK OR90t 110: 55830 ATTENTION: let. Jolti HUGEY DATE RECEIYED: 02/27/85 SAWLE IDDITIFICATION: UllIT 2 BISCHARK 02/26 TEST DETERMIllATI0lt ESLA.TS UllITS 1361 W K S PART Y-3 11010 Aluminus ( A1) < 0.1 ag/l 10 # lerius (le) < 0.1 ag/l M150 Cobelt (Co) < 0.01 ag/l 1190 tron, total (Fe1 0.06 ag/l M230 Magnesius (llg) 12 ag/l 1240 Mengenese (IIn) 0.01 ag/l M260 Molybdenue (Mo) < 0.03 og/l 1340 Tin (Sn) <1 og/1 M350 Titenius (Ti) <0.5 og/l 1055 Boron (3) <0.2 og/l 9060 Broeide (Br) <2 og/l 1225 Color,True 30 Pt-Co W310 Fluotide, total (F) < 0.5 ogIl 1390 Nitrate (11) 0.6 ag/l W410 Mitrite (N) < 0.01 og/l 1435 Mitrogen, Kjeldehl (II) < 0.1 og/l W440 Nitrogen, Organic (N) < 0.1 og/l 1540 Phosphorus, total (P) 0.03 og/l W730 Sulfate, turbiditetric (SO4) 28 og/l 1740 Sulfide (S) < 0.1 ag/l if/60 Sulfite (903) <2 og/l 1770 Surfectents (MBAS) < 0.1 og/l l M362 MPMS PMT V4: T0XIC METALS 11020 Ardisony (Sb) < 0.1 og/l l 11030 Arsenic ( As) < 0.001 ag/l 8050 Seryllius (le) < 0.002 og/l M090 Codeium(C4) < 0.005 mg/l 1140 Chroeius (Cr) < 0.01 ag/l M160 Copper (Cu) < 0.01 ag/l 1200 Leed (Pb) < 0.03 ag/l M250 Mercury (Hg) < 0.0002 ag/l PA E NO: 1 h A Halliburton Company CLIEf1T ORIGif1AL REsttf 70: WN Park West Two I NUS 5360 C C : Run Road Cliff Mme Road Pittsburgh, PA 15206 Pittsburgn, PA 15275 mg 412-7es.toso l l 't i LAB ANALYSIS REPORT l CLIDif IIAIE: IllBIAllA & MICHIGAll ELECTRIC CO. MVS CLIENT 110: 010904 AIORESS: P. O. 30X 60 NUS SAIFLE 110: 15021704 l FORT MYIE, Ill 46001 VENDOR 110: IEPORT BATE: 03/26/95 110lX ORDut 110: 55830 l ATTENTION: IIt. J0lti IRiglEY DATE RECTIVED: 02/27/85 SAltLE IDDITIFICATI0ll WIT 2 DISCHARGE 02/26 1EST KTEPHIllATI0ll RESULTS UNITS l lG70 llickel (Ni) < 0.03 ag/l M290 Selenius (Se) < 0.004 ag/l 1300 Silver ( Ag) <0.01 30/1 N330 Thellius (T1). < 0.1 ag/l 1390 Zinc (Zn) < 0.01 ag/l W270 Cyonide, total (CN) < 0.005 mg/l l l 1500 Phenolics 0.03 ag/l l l M220 Lithius(Li) < 0.01 ag/l l l 1110 VOLATILES-PP IN li4TER l OY01 krolein ( 100 ug/l 1902 krylonitrile ( 100 mg/l i OY03 Benzene (5 ug/l l905 Brosofore <5 mg/l OYO6 Carbon Tetrochloride <5 og/l IV07 Chlorobenzene (5 og/l OY00 Chlorodibronomethane <5 ug/l IV09 Chloroethene < 10 og/1 l OY10 2-Chloroethylvinyl Ether < 10 ug/l IV11 Chlorofors (5 ug/l OY12 Dichlorobronomethane (5 ug/l IV14 1,1-Dichloroethane <5 ug/l OY15 1,2-Dichloroethene <5 ug/l IV16 1,1-Dichloroethylene (5 ug/l DV17 1,2-Dichloropropane <5 ug/l IV18 1,3-Dichloropropylene <5 ug/l OY19 Ethylbenzene <5 ug/l IV20 Methyl Broeide < 10 ug/l OY21 Methyl Chloride < 10 ug/l IV22 Methylene Chloride <5 mg/l l OY23 1,1,2,2-Tetrochloroethene og/l IV24-Tetrechloroethylene(Perchloro) <5 og/l OY25 Toluene (5 ug/l PAE NO: 2 h A Halliburton Company CLIENT ORIGINAL REnffT TO: WWN Park West Two NUS 5300 Cr7__.; Run Road Cliff MineQoed Pittsburgh, PA 15206 Pittsburgh, PA 15275 } mg 412-786-1000 i LAB ANALYSIS. R E P C3 R T CLIDIT llAfE INDIANA 6 NICHIGAN ELECTRIC CO. NUSCLIENTNO: 010904 ABIRESS: P. O. 301 60 IlUS SAMPLE 110: 15021704 F0iti WAYE, IN 46001 YENDOR 110: 1 REPORT DATE: 03/26/95 WORK ORDER NO: 55830 l ATTENTI0lla let. J01811U110 DATE RECEIVED: 02/27/85 SAlfLE IENTIFICATION: iglIT 2 BISCHARGE 02/26 l l TEST DETERMillATI0ll RESILTS UNITS l 0/X 1,2-Trans-Dichloroethylene (5 ug/l DV27 1,1,1-Trichloroethene <5 mg/l IV28 1,1,2-Trichloroethene <5 mg/l l OY29 Trichloroethylene <5 mg/l IV31 Virgl chloride <5 mg/l 0120 ACIDS - PP IN WATER 0A01 2-Chlorophenol < 10 ogil 0402 2,4-Dichlorophenol < 10 ug/l l 1A03 2,4-Binethylphenol ( 10 eg/l l 0404 4,6-Dinitro-o-cresol ( 50 mg/l l lA05 2,4-Dinitrophenol ( 50 ug/l 0A06 2-Nitrophenol ( 10 ug/l IA07 ,4-Nitrophenol < 50 mg/l l 0A08 p-Chloro-a-cresol < 10 ug/1 l lA09 Pentechlorophenol < 50 ug/l 0410 Phenol ( 10 ug/l lAll 2,4,6-Trichlorophenol < 10 ug/l DE30 Acid Extraction-Water l 0130 BASE NEUTRALS - PP IN WATER 0801 Acenophthene ( 10 eg/l l 1902 Acenophthylene < 10 ug/l l 0803 Anthrocene < 10 ug/l 1904 Benzidine < 50 og/l 0B05 Benzo (a) Anthracene < 10 ug/l 1906 Benzo (oPyrene ( 10 ug/l l 0007 3,4-Benzofluoronthene ( 10 ug/l 1908 Denzo(ghi) Perylene ( 10 ug/l 0D09 Benzo (k)Fluorenthene < 10 mg/l IB10 31s(2-Chloroethoxy) Methane ( 10 ug/l 0311 lis(2-Chloroethyl) Ether ( 10 ug/l 6312 list 2-Chloroisoptopyl) Ether < 10 og/1 0B13 bis (2-Ethylhexy1Phthelete < 10 mg/l PAE NO: 3 h A Hall! burton Company CLIENT ORIGINAL RElefT TO: %hN Park West Two ~ M W Run Road CHff Mine Road ~ Pittsburgh. PA 15206 Pittsbutgh. PA 15275 mg 412-786-1000 l AB ANALYSIS REPORT CLIENT IIAE: INDIANA & NICHI6All ELECTRIC CO. NUS CLIDff NO: 010904 ADDitESS: P. O. BOX 40 NUS SAIRE NO: 150217H FORT WATE, IN 46001 VOIDolt 110: ItEPORT DATE: 03/26/85 UOltK OR90t 110: 55630 ATTENTION: lWt. JOHN HUGET DATE RECEIVED: 02/27/85 SAltLE IDENTIFICATION: UNIT 2 DISCHAltGE 02/26 1EST KTDtMIllATION RESIA.TS UNITS 3 14 4-tronophenyl Pheryl Ether < 10 ug/l. 0B15 h tyl Benzyl Phtholote < 10 mg/l 9316 2-Chloronoph W 1ene ( 10 ug/l 0B17 4-Chlorophenyl Phenyl Ether < 10 ug/l ll18 Chrysene < 10 ug/l 0919 Dibereo(e,h)Anthrocene < 10 ug/l 1820 1,2-Dichlorobenzene < 10 ug/l 0521 1,3-Dithlorobenzene < 10 mg/l 1822 1,4-Dichlorobenzene < 10 ug/l 0923 3,3'-Dichlorobenridine < 10 mg/l l IB24 Diethyl Phtholote < 10 ug/l l OB25 Dimethyl Phtholote < 10 ug/l 1826 Di-N-Butyl Phtholote < 10 ug/l 0B27 2,4-Dinitrotoluene < 10 ug/l 1328 2,6-Dinitrotoluene < 10 ug/l 0829 Di-N-Octyl Phtholote < 10 ug/l IB30 1,2-Dipherglhydrozine( Azobz) < 20 ug/l 0531 Fluorenthene < 10 ug/l 1332 Fluorene < 10 mg/l 0B33 Her.achlorbergene

10 eg/l IB34 Hexechlt.robutodiene

<10 vg/l 0835 Hexachloro-cyclopentodiene < 10 ug/l 1936 Hexachloroethane < 10 ug/l 0837 Indeed1,2,3 cd)Pyrere < 10 ug/l IB3B Isophotone ( 10 ug/l 0839 Neph W lene < 10 ug/l lH0 Nitrobenzene ( 10 ug/l 0841 N-Nitrosodisethylonine < 10 ug/l IB42 N-Nitrosodi-N-Propylonine ( 10 ug/l l 0943 N-Nitrosodiphenyleire ( 10 ug/l 1844 Phenanthrene ( 10 ug/l 0345 Pyrene ( 10 ug/l PAE NO: 4 h A Ha!!! burton Company CLIENT ORIGINAL REANT TO: Lalporatory W Mico Park West Two l 5360 ComptieNe Run Road Cliff Mine Road - '2 Pettelpurgh, PA 15206 %rgh, PA 15275 mg 412-7as-toso i l LAB ANALYSIS REPORT l CLIDIT llAlfr I R IANA & MICHIGAN ELECTRIC CD. NUS CLIENT 110: 010904 ADIRESS: P. O. 30X 60 IRIS SAlfLE 110: 15021704 FORT WAYlE, IN 46001 VENDOR 110: REPORT NTE: 03/26/85 UORK ORDER 110: 55830 AT1ENTIOll M. Jolti IRililEY DATE RECEIYED: 02/27/85 l SAlfLE IENTIFICATIOll: Ull!T 2 DISCHARDE 02/26 TEST KTERMIllATI0li KSLLTS UNITS 3 46 1,2,4-Trichlorobenzene < 10 ug/l OE25 lose Neutral Extraction-Veter 0141 PRIORITY POLLUTANT Kl'S DE11 KB Extr4ction - Water 1P19 KB-1016 ( 0.5 ug/l GP20 PCB-1221 < 0.5 ug/l IP21 KB-1232 ( 0.5 ug/l OP22 KB-1242 ( 0.5 ug/l j IP23 PCI-1248 ( 0.5 ug/l 1 OP24 PCB-1254 < 1.0 ug/l DP25 PCI-1260 ( 1.0 ug/l R450 RADIUM 226 AllD 228 2 04 Rodium-226 <0.5 pCi/1 R805 Rodium-228 <2 9C1/1 R800 Gross Alphe <2 pCi/1 R801 Gross Dete <4 pCi/1 1032 Aeoonie os 11 (distillation) < 0.1 ag/l WO50 900, 5-dog (02) <1 ag/l 1100 Carbon, organic (C) 23.2 ag/l W120 CCD (02) <5 mg/l J 1610 Solids, suspended at 103 C <1 ag/l j i C019lDITS: Reviewed and Approved hs PM PAGE NO: 5 h A Halliburton Company CLIENT ORIGINAL ) OttatfT TO: Latweboey Serv 6ces N Fark West Two l - NUS 5300 Campbelle Run Road Cliff Mine Road Plttetugh.PA 15206 Pittsburgh, PA 15275 mg 412-7ss-ioso LAB ANALYSIS R E P C3 R T CLIDif IIAIE: IllBIAllA & MICHI6All ELECTRIC CO. IlUS CLIDif 110 010904 ADDRESS: P. O. BOX 60 IIUS SAlfLE NO: 15021705 FORT MYlE, Ill 46001 YOIDOR 110: REPORT DATE: 03/24/85 liORK ORDut 110: 55830 AT1EllT10ll Itt. Jolti IIUBIEY MTE RECEIVED: 02/27/85 SAltLE IllDITIFICATIt31: ISIIT 2 DISCHAltGE - GitAt 41 02/25 0645 TEST KTEltMIllATIOlt ItESIA.TS UllITS 3A32 Fecel Califore - IFil 15 col /100el W150 Chlorine, residual DPD (C12) < 0.1 og/l I490 pli 7.9 ISSO 011, extraction gravinetric 1.3 ag/l 6 Gl91ENTS: Reviewed end Approved by: Jet h A Halliburton Company CLIENT OF.lGINAL REI8tT TO: %WN Park West Two NUS 5380 CampbeNe Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 mg 412-78e-10e0 LAB ANALYSIS REPORT CLIDIT llAIE: ISIANA & MICH16All ELECTRIC CD. IlUS CLIDIT 110: 010904 ADDRESS: P. O. 30X 60 IlUS SAlfLE 110: 15021706 FORT UfmE, Ill 46801 VDIDOR 110: ItEPORT BATE: 03/26/85 UORK ORBDt 110: 55830 ATTDITI0ll IWt. J0ltl HUGIEY DATE RECEIVED: 02/27/85 SAIPLE IDDITIFICATI0lls (plIT 2 BISCHARGE - GitAB 42 02/25 1500 TEST DETERMINATION RESULTS UNITS IA32 Fecal Califore - 1911 9 col /100a1 U150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 81 9600 011, extraction grevisetric < 1.0 ag/l 4 OMIENTS: Reviewed ard AppW by: JIC h 'A Halliburton Company CLIENT ORIGINAL RE88f7 TO: Laboratory Services DMolon Park West Two ~"2 NUS h 5360 Camptoile Run Road Cliff Mine Road Mttstugh, PA 1520$ PW.aburgh, PA 15275 mg 412-708-1000 LAB ANALYSIS REPORT CLIDIT IWE ISIAllA & MICHIGAN D.ECTRIC CO. NUS CLIDIT 110: 010904 ADBRESS: P. O. BOX 40 110S SAIFLE 110: 15021707 FORT WATIE, IN 44001 YDIDOR 110: IU ORT MTE: 03/26/95 UORK OR90t 110: 55830 ATTDITION: ltt. JOM HUBIEY MTEItECEIVE3: 02/27/85 SAIFLE 190lTIFICATIOll: LIIIT 2 BISQWtGE - GRAB 93 02/25 2100 TEST KTDtMIllATIOlt RESULTS UNITS IA32 Fecal Colifore - 1911 4 co1/100e1 V150 Chlorine, resideal DPD (Cl2) <0.1 ag/l I490 pH 8.1 W680 Oil, extraction grevisettic 2.3 ag/l 1 O M ENTS: ) Reviewed end Approved by: E h A Halliburton Company CLIENT ORIGINAL i REMIT TO: Latwatory Sorwkus N Park West Two l LNUS h 5300 CampboNe Run Road Cliff Mine Road Plttelugh PA 16206 Pittsburgh, PA 15275 412 788-1000 g LAB ANALYSIS REPORT CLIDIT llAE: 111D1A114 6 MICHIliell ELECTRIC CD. IluS CLIDIT 110: 010904 AggItESS: P. O. 30X 60 IluS SAlfLE NO: 15021706 FORTliAYIE, Ill 46001 VDIDOR 110: IUelti MTE: 03/26/85 iloitK ORDER 110: 55830 i ATTENTIDII: 10t. Jolti tilliEY MTE ItECEIVED: 02/27/85 SAIFLE IDDITIFICATI0ll LIIIT 2 DISCHAltGE - GItAB 44 02/26 0303 1EST DETERMIllATIOll ItESLA.TS UllITS BA32 Fecol Colifore - 1991 21 col /100e1 W150 Chlorine, residual DPD (C121 < 0.1 ag/l 1490 pH 8.1 li480 Oil, extraction gravinetric 2.8 ag/l ) OttENTS: Reviewed end Approved by: E $ A Halliburton Company CLIENT ORIGINAL ~ t =. c SECTION 11 PERMIT y , gg gp SEE INSTRUCTIONS NUMBER ON REVERSE SIDE O 0 A, 0, TALL fUTER i

i Tv4 FOLLOWING REQUESTED IVCmATION i,g.LJ,5 ADWESSED EZ ALL SWFACE WATER DISchAAGERS.

tHE. HEW USE DISOMRGERS 2&Ll, PROVLft f.vECTED VALLES M M OUANT!TATIVE 40 GidL] TAT [VE Irfomatt0N GEQutsTED BELLw.

A. is mis rACit:TY A PRinARY trotsTRv? (REFER TO TABLE rA Pre sil) hr o, co To O (in vts, eo To ej YES NO PRIORITY 8. INDICATE TYPE OF PRIPWtY IPOUSTRY AS LISTED IN TABLE IA PF418.1.

5tTtHe seitiE Ci iPiw,R, POLLUTANTS

'Nt'a E wtm c.) AND C. DCES This CUTFE DISCHMGE CONTAIN ANY PROCESS hASTEWATER? f F YES. GO TO D) YES NO (It *C, GO TO E) INF!RMATION D. !!CICATE seelCn GC/MS FRACTIONS PtJST BE TESTED FOR. (REFER TO TABLE lA Pv4 El VOLATILE FOR tcIE,! FCR EA04 GC/MS FRACTION OECKED EACH SPECIFIC OEANIC 70Xtc POLLUTANT WITHIN gAo FRACTION f.15I BE AidLYZED FOR (SEE TA'lLE llA Pr.E #2, IN ADotTION, ALL PRIP9dtY BASE / NEUTRAL SURFACE VmTER trCUSTRY APPLICAhTS WITH A PROCESS WASTEWATER DISOdRGE E PROVIDE QuM4TITATIVE

*

IIIA '*# O
DISCHARGE

@ ACID ONLy RECDRD ALL DATA ON FORMS PROVIDQ (ITEM 7) !N THIS BOOKLET. (CONT!NUE wtTH E-K BELOW) PESTICIDE E. IP c $@ FACE HATER DISOMRGE APPLICANT (PRIP%RY OR SECONDARY IN[1JSTRY), REGAR!1.ESS OF M TYPE OF DISCHAEE, xtCWS OR tdS REASON TO BELIEVE T>dT ANY POLLUTANT LISTED NOT APPLICABLE / BELIEVED ABSENT IN TABLE IlA M.D IVA PAGES 4231 IS DISOdEED FRCM ANY CUTFAL1,TE QunNTITATIVE 2151 SE PROVIDED. RECDRD E DATA ON FGNS PROVIDED (ITEM 7) IN THIS BOOKLET. PPESENT/ DATA IS ATTAO(D F. IF ANY $$ FACE HATER DISCHARGE APPLICANT (PRIMARY OR SECDPCARY IPOUSTRY), REGARDLESS h NOT APPLICABLE /8ELIEVO ASSENT OF TYPE OF DIS E, ANDWS OR HAS REASGe TO BELIEVE ANY POLLUTANTS LISTED IN 4 TABLE VA PK4 3 ARE DISCHARr,ED FRrM ANY CUTFALL TPE APPLICANT 5&I DESCRIEE REASONS FOR THE POLLUTANT BElfG PRESLNT #C PROVIDE ANY AVAll>8LE QbANTITATIVE DATA. RECDRD E DATA CN F0m$ PROVIDED (ITEM 7) IN THIS 900MLET. G. E $$ FACE HATER DISOtARGE APPLICANTS (PRIMARY #C SECONDrJtY INIAJSTRIES) MO: ~ OR MANifACTWES 2, 4, - TRIOA.OROPKNOXY ACETI ACI (2, 4, 5-7), TRICHi.OROPENDXY PR0PM (C ACID ($1LVEX,, 4, , TP)h' 0, pr ETHvt 2-DIO4LCR0PROPtDa e DitETWL W(gHLcR0necxY4, di, kTRIOLOROPHENYL) PtOSPt0ROTH! (ROPfaEL)J , 4, MTRIOtGt0P>(*0L (TCP)J OR HEXAOLORCP(PE ( (ALL DATA FOR T>E ABOVE MJST BE GDdERATED USING STANCMD ANALYTICAL CALIBRATICri PROCEDWES) OR NF0WS OR HAS REASON TO BELIEVE THAT TCDD is OR P%Y BE PRESENT IN T>EIR DISOdEE. tL.T, REPORT '1UALITATIVE DATA, GDERATED WHIOj UQED A SCREENING PROCEDtFE PCT PRESENT/ DATA 15 ATTAOED CALLBRATED WITH NdLYTICAL STWCARDS, FOR 4, ), /c 8,

TETRAOLDR00! BENZO-P-Ol0X1N (TCDD). RECORD ALL DATA ON F0FMS PROVIDED (ITEM /) IN THIS ECOMLET.

J. IF M SWFACE HATER DISO*TE APPLIC#4T KtOWS Ot NAS REASON TO BELIEVE THAT 3 pey ggg k BIOLOGICAL T0x! CITY TEITS hERE NADE IN THE LAST T>dEE (3) YEARS ON ANY OF T5E APPLIC#4T,3 DISodRGES OR ON A RECElvtrG NATER IN RELAT[0N TO A DISOMEE, PROVIDE THis trfuhTION #3 #4 ATTAOfEdT TO THis APPLICATION. APPLICABLE /SEE ATTACHED K. IF A C3dTRACT LAWATORY OR CCf64.LTI'G FIRP9 PERFORMED #ff 0F T F #4.AYSES PEQUl#ED NOT APOLICAAE BY THl3 APP ICAfiCN, PROVIDE T4 reE #C ACORESS CF EAO4 LA1CAATORY Ut Fim #C L M ArdLYSES PERFORMED AS #s ATTAOff_NT OF THIS APPLICATICh. APPLICABLE /SEEATTACHO L. DO You DISOwr4 ANY OMR 70xlC ut IFUmforG plCAL SLSSTANCES PCT LISTED IN TAPLES IV PM4 tp ED !!A itMrH VA FV4S 8h4 IF VES, T'fN IDENT!rY T4 PCT APPLICABLE O(MICAL SLE!TANCES 40 EST!'dTE M Fl% EFFLUENT COPdCENTRATIONS. SJPt!T THis IMOPATION AS AN ATTAofENT TO THIS ATPLICATIGt. APPLICA8LE/SEE ATTAGED 9 ..t' SECTION 11 PERMIT C M.E 000 3D7 NUMBER v SEE INSTRUCTIONS ON REVERSE SIDE um N toio1A ITEM A. USE THIS DATA SEET TO RECORD INFGNAT!ON AS RE3JIRQ IN: (CECK APPROPRIATE BOX FOR W4tCH INFORMATICri THIS DATA SHEET REPRESFETS.) 7

1. SECTION !!, ITDi l-E.

CRouOaATER DTSO4 AVE INFOP*ATION (PAGE $5) l CRITICAL

2. SECTION II, ITD16. PRIORITY RWTMTS IN SWFACE NATER DISchariE (PAGE 57) 3.

8. BELON: CRITICAL MATERIALS (TAILE fv) IN SURFACE HATER DISOiARGE (PAGE M) toxic POLLUTANTS e

HAZARDOUS SUBSTANCES 8. LtST ANY CRITICAL MATERIAL (TABLE IV P/4E 6) NOT ADSESSED IN SECTION ll ! TEM 6 8RIORITY NOT APPLICABLE - PQ.LUTMTS M41CH VOU ICE"w OR HAVE REASON Tn BELIEVE TO BE PRESENT IN TE DISOinRGE. SEE M REVERSE SIDE CF TH15 PEE FOR FURM.R DIRECTIONS. DISCHARGE APPLICABLE (SEE BELOW) A. NAME OF CRITICAL MATERIAL OR PR!CRITY POLLUTANT

,,, g,

mii M N ME # OF ANat YSES $a B. AVDAGE CONCENTRATION; SMPLE TYPE; I 0F ANALYSES l I l i l I l l L] LJ l f I Q2 m!T COOL mlT COE C. MAXIV C3 CENTRATION NO MASS s e t t. e i t a y a < r

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t i y A. NAME CF CRITICAL MATERIAL OR PRIORITY POLLUTANT g g g g g g y

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AVERAGE CONCCCRATION; SAMPLE TYPE; # OF ANALYSES g g g g,g l l [ I C. MAXI?tPt CONCENTRATION #O MAS 3 mlT C00E mli COT I t t t.I I t e y i I t t.t t I f (J A. NAME OF CRITICAL PATERIAL OR PRIORlW POLURANT l l l l l I l l UNITS CODE -J5 i II Ecs E. AVERAGE COPCENTRATION; SAMPLE TYPE; f 0F ANALYSES ] l ] l,j j j j U y i, a ud!T CG)E MW DPF # M MALYSES 2 Ug/l y 3 LBS/ DAY 2 .gr a .3, m C. MAxt'tN C0tCENTRAtl0N #C MASS g,, ,,g [_j i t i f,e f f I tJ 4 KG/ DAY A. NAME & CRITICAL MATERIAL CR PRIORITY POLWTANT l l l l l l t l 4 S. AVERAGE CONCClTRAT!ON; SAMPLE TYPE; # OF ANALYSES g g g l,g g g g C. MAXtPtM CorCENTRAT!as NO MASS SAMPLE TYPE A. Nrdt CF CRITIC 4. "ATERIA6., OR PRIORlW POL 1UTMT g g ;, 9 g g, 1 GRAS g CM SMPLE TYPE # OF NAYSES 8. AVEREE C0rCUiTRATION; SA;ftf TYPE; # OF ANALYSES ' l g g g,g l l l 2 24 HR. COMP { m!T CODE WIT CODE C. MAXIM.74 C3CETRATION NO MASS I t i e.I t t t L_; t I i j.s t

j u

-J A. NAFE OF CRITICAL MATERIAL CA PRIGttTY PQ.Lt/ TANT t t I i l l l l 5 tr utti CODE S#fLE TYPE # OF NAYSES g4 S. AVEPACE COCEWRATION; SAMPLI TYPE; I 0F ANALYSES 1 I l l.I l I J L_J tJ f f I <2 I , #b C.

1Axt*1M cCrCc(TRATION Mc MASS 3,,

,, eg,,, ! A. 41tT OF CRITICAL MATERIAL OR PR!GRITY POLLUTANT f f I t i I f I g E m&T CCCE 5#FLE TYPE # OF ANALYSES 7 8. AvDtEE CONCENTE.ATION; SAMPLE TYiY: # OF ANALYSES Ll l l,U l J U y e i i mir C00E mil WJE C. MAxle COPCENTRATICN #O MASS r t t t.e t t t t_ _j t ? I f.I I I I IJ A. Niet OF CRITICAL MATERIAL OR PRICRITY POLUJTMT l l l g g g g, g 3. A/EPACE CCPCD.19Atl0N; SAMPLE TYPE; # OF M.ALYSES g g g g,g g g C. MAxlv WC4MATION #O 6 g,,,,,,,, Arm:TIONAL. PAGES OF THIS ITU9 7 #E ATTAOC FOR M REST OF M CRITICAL YES mATEa!ALs uc/OR PR!ai!TY POLucANTS RE2J1RO TO BE Ap0RTED. O ro I 11 $4 3 2 1 I T I U S N W L D F C O I T U AR 321 T T O T A 2 1 IN DE GMM IN O SPC N CC Y S S W T D A T R AROC OO P T # L H C C E. S I T A T T P GG MINOOOON E E Oo Ee A H U M C I ME 2E T NE D I A DDY C CL N LT NT I A CW W U O R O WT g M g O V E R E AE I NC OA L NG M / RI D A RS G A l l/ D E N T E E T GT D E S E YS C E EN T E T E R V R S .F E. G IO D C. .A J G F E. D. C. S. .A E H T w R A A G A A A I D I A TI D L D C I T ~ w ( f D D T T t I I T ( I 3' 0A 4 !T I W D I t t E WM W-im M M F Y O !T I X INS 4 E T Y x ( S S P F I S e r, O o E D Y Y V P W W E E V Tt T . 0 ST O t E "U y W P 2 M f FN O C H A ,S u II M N T EA 4 ,eo A N V M M 1 U M DO E-X WE I N F S S I LI "D I D M E St S G G P I E W m EN AA D Eo r 1 u 1 E E M T M L R e M T TT M LM t E CS S T .R T I3A H C S C C A e O E A I AA T D S L O T A T E S s N I O C M IT IM i D ID X ir-D T S )D E G D t I S P D R V at R O lTE D R A T N I "M I R I ee vT O IS T. O T S TT C E M t !W-I O A E C G N VS I R R M IS H V G E M T T S M o-f ET A D E SW S. E A O A ( D T A O L I C G D I E G I5 T i M g Y R S E C I AT E O D M S E 0 ER t A E IR .M A O TH F G F e, O I P A E1 F A E L W E t L 5 E E G f I( O L g Y FA I M N C A 3T F W T O l E. R C ) L P O R V D ML r 3 I W o t A E S G P D T A T T g i R E T S 9 R 9I Y A O tC R O E n A DY P O N R G AA A W E T T S E e E. O TC G C W ) Ai C g 4 s B CIh D A A u E s T NP I A m A S 0 U E I C0 O C 1T I g FVI W I T T O O R i e TT G I I e g t ,v T R V ) E .S M N { E V E i S E Z S P ? 0 D f PP XC 0 W I g 1 vf E 0 w 1 N F IIF E II J D C' @ g g I P O g N TC S E S Y N F t M ? W I g A FCe AC T M, g R*tA N E i 3 Et s Q 1 Al CA HN g t D" D ,.o IO i i I L I g f 3 ,A T@ A A A M 3 L L IT? Y Y i N Nl I i

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Y M I W W 1 L t I t D F t. A N i f i bh t o 9 f A J I i t hD C M C C 1 A D O i i In s L Y i I i D M L. L. C S / E J J .J W Ct L U E! g Dh j J T S ,ll l: SECTION ll PERMIT Flr o00 SD.7 NUMBER r SEE INSTRUCTIONS ON REVERSE SIDE (IJTM.L fGTER O O,33 I t ~U{U Ie IVI NVE OF P50 CESS CONTRIMIPG TO THE DISOWtGE , D, E,, ;, c, #, NiG, A. woum mis ouTFut we Sic Cem ,,,,, i i,,,, 3 .. PROCESS SOe1E (YE~iLv ave-Go Ai4i - S/o4Y eAYs '4,2, C. PROCESS VOLuf FLOW RATE '3'9' 7' W PROCESS "8 TOTAL YENtLY STREAMS QA$l$ll989 kl4N DATM gaggy ggggy i e , i,,, iO, M CONTRIBUTING Q-TO IS 13 i9 i 4 DA!LY MAxt e I i i f ' I o['[,,,c, D. P= CESS emuuCT:Cu uTE MM gg A. Nve or PROCESS murRIButtNG 70 nf DISOWtGE mouw twis cinFR140 $fC CTE NA i i r i i i ' i ' ' ' ' ' ', B. PROCESS SOGtLE (YEARLY AVERAGd HoutS/ DAY I f I DAYS / YEAR I ' I I @li at. C. PROCESS VOLitt FLOW RATE TOTA MY l I ' ' ' ' I l3 On I ' ' I I ' ' ' ' ' DAILY MINIPut UNITS CODE DAILY MAXtrut ' ' ' I f f I ' U uttTS T!PE 2 GALLONS D. PROCES$ PRODUCTICN RATE I I I f I I ' I I l-- I I-3 A. NME OF Pfl0 CESS CONTRIBUTING TO T4 DIM YARDS Moum THIS CUTF41 #C SIC C00E NA i i i e i i i i ' i i ' ' ',,,,,, B. PROCESS SOct11 (YEARLY AVEMGd Y g g/ggy g, 3 DAYS / I 'I I h 6 MGD WII CM C. PROCESS VOLLPE FIDW RATE TOTA YE#tLY l I I I I I I I I I b- - S 7 GPD p DAtLY MIN!*Ut I I ! ' ' ' ' ' ' ' DAILY MAXI M l I I I I I I I ' I U D. PROCESS PSCDLET!ON RATE t#41TS /TIPE TIME 1 i t t t t t I t_ V L ) 1 HOUR A. NVE OF Pr1 CESS CCrmt!BUTIPG TO DE DISCHARCE gg TWD4 Tufs CUTratt RO SIC C00E ,,;,,,,,ie i ,e i 2 DAY 8' 3 WEEK tours / day i I I DAYS / WAR l I ' ' C. PROCESS WLIFE FLDd RATE TOTAL MY I I ' ' I ' ' ' ' I v e DA!LY MIN!PtPt i I ' ' I ' ' I I I kd c. DAfW MAXfM I f I f f f f 8 t i L""J t#tl TS TIPE D. PROCESS PRODUCTICN RATE L_t t t I t t I _t Ld A. Nitf CF PROCESS CONTRIBttfirG TO DE DISChMGE uA DNourai NIS OUTT4140 51C CCLE M P4 t_ _.1. I L ' f I I I I I f I ' I I I I I E. Pf(4ESS SOfDL1E (VEp_' Y A(ped gypg/yy g g j DAyL' FEAR I t, I Ij ur41T C2 C. PROCESS VULut FLDW RATE TOTA YEARLY I I I I I I I t t f II us DAILY MINIMlft b I ! I I I ' ' ' ' DAILY MAXIV ' ' ' ' ' ' I ' ' f l1 UN!TS It'E D. PROCESS ProwCTION RATE e t t t l I t t i l-J 5 l SECTION 11 PERMIT 00 NN NUMBER F SEEINSTRUCTIONS ON REVERSE SIDE QRFitt !U18 ,6,O i3 i /EOM THl5 OUTFALL DIREC TO THE GROL#O CA IS THE Dly IF % CONTINLE TO ITE?9 A. yES po GROLFOeATER3. B. HAS A HCROGECLOGICAL STLEY OR ITS EQUIVALENT BEEN PERFOAPED OR IS MRE StFFICIENT CURRENT HYDR 0GECLQGICAL INFORMAfl0N AVAILABLE A$ REQUIRED (v TLwATER RESOURCES '43 to C099tSS10N PART U Grot #0dTER RLAI 0F ALLUST $,19lD R.ao.LU/ (PEE 4j) FOR GROUPeDWATER THIS EXISTING Ot PRGPCSQ DISCHMGE IF YES ATTAot A CCFY OF THE REPORT. DISCHARGE C. ARE YOU M T!% A*8 EXENTION FR09 SLRi!TTl*G A HYDROGE0 LOGICAL REPORT L?OER INFORMATION VES to ($a(PEE 46) OR FRGt GROLFOdTLR MONITORIPG $EQUjRDTNTS RULE R.3D. .Lu (5) (PxE 47) 0F M PART R RLLES. IF YES ATTACH LtcER WULE R.) DO,CitOTS A D EXPLN4AT10N TO COON 57 RATE THAT YCL7t DISCHMGE WXAD QLALIFY FOR NA r oentm. ARE YOU RE2ESTI!G A VARIANCE FRO 1 Rjf 323.M (PAGE y IF YES, ATTACH SUCH (Not0EGRACATION) 0F D. ygg ,O THE MATER RESCURCES L379155!O6 PART H GROLFOeATER RtA.ES. DOCit'ENTS AS NECESSARY TO M NE D FOR A VARIAf IN TEfV'S OF M CRITERIA SPECIFIED IN RLA1 ). PAGE 4 0F THE PART 2LA.ES. g E. LIST AL,L CHCdlCAL 51.LSTAtCES WHICH APE IN NCHIGAN'S CRITICAL MAT (RIALS REGISTER TABLE IV (PAGE b) A@;Gt U.S. EPA'S PRIORITY POLLUTANT LIST TABLE V (PAGE /) OR ANY OMR SLBSTANCES NOT M!CABLI/ BELIEVED ABSENT

!CH ARE CR MAY BECOE INJURIOUS TO M DESIGATO USES OF M G40lPOdT0t CR TO M PUBLIC HEALTH THAT ARE CISOdRGED OR EXPECTO TO PE DISCHMGED TO M GROL70dTER_SY THl$

FACILITf. ESTIMATE THE FINAL EFFLLENT CDrCENTRAfl0N Ato RECDC ALL DATA IN ITEM / G SECTION II IN THIS B00ftET. RESENT, DATA Pt0V!CED IN ITD17 M APPLICANT MAY BE RECIJIRED TO DO ACDITIONAL WTE ANALYSES. M A. DISOiMGE CHARACTERISTICS CONCENTRATION t#41TS CODE # ANALYSES SAreLE TYPE ~ ITEM 5 "5"*'""'""'-"*'

a (ogrtgCAL cryce; me)

I t i I.I f I t i I i 1.I t I f Ll.J W LJ EXPECTED ,,,,,,,,,,,, i,,,,, gl,3 g,,,,g_j g,,3 ,,gg { g ) WASTEWATER CHARAC-

MI A PITROGEN (AS N)

! I I II I I I I I I !.I ! I I Lk,3 I I I U TERISTICS

TOTAL SUSPE'EED SOLIDS I ' I I

.I I f I ' ' ' ' t LJ ' ' ' L_; UNITS CODE TOTAL PICSPHORUS (AS P) I f 'I f .I i f I I f f f.I I f f L}J t f f U 1 Mg/l ' ' ' ' e' ' ' I LI 2 Ug/l TOTAL RE$ttt1AL Ot.ORINE 3 COUNTS / L!) I I I I.' I I ' ' I I I *I ' I I U 100 mi DISSOLVED OXYGEN mig 4 S.U. .pg 1 l l.L!

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Tc9PEUTURE (StrtER)
TeeEuTust (a:NTER) i '

'.LJ l ' '. LI LEJ L_J E. OTHER NASTE%ETER CHMACTERISTICS ,0,!,L,%,A,8 t t,A,S;E, ,,,,,,,, i,,,,,,,, i g (_g g SAMPLE i f f i I e I i ' ' I i f I.8 ' f f i f f f.1 I LJ f 1 ' L.) TYPE i f ' ' ' ' ' r t ' f I f I i 1.8 I f I i i 1 J.' t f I LJ 8 ' 1 LJ 1 cRAs 2 24 HOUR y,,, y COMPOSITC i e t t 1 t t t i t e i e t i i.e t t s a t i 1.t t i ! E,_J t t i L.J i i 1 e i i i e t - i t i r i e.: i I i e i i n. i i i L_f f i 1 L i i i e i i i t i t i e i.t I t 1 i i i e.I 1 i I L,,,j i i I L! % SEE NOTE O N pac.E 9, cowAu. co3 I 7 I I SECTION ll PERMIT y , gog SEE INSTRUCTIONS NUMBER ON REVERSE SIDE MFid.L 'LTR ,0,o,3, ITEM - -To -Ti- -SSEo -- -TT o-RS. M;TE NEW U2 DISCHr#GERS 2&L FiDIR t#ECTED VALdS 6At DE OLANTITATIVE A;O - QuAttTATIVE INFCMST!4.f4 REQASIED BEL.W. A. IS THIS FACILITY A M1? wry !!OUSTRY? (PEFER TO TABLE [A PK4 Ljl) h t ir % ro 70 E) ( f F vE9, r,o to g) & YES to P;10RITY 8. INDICATE TYPE OF Po!NRY 1700STRY AS LISTED IN TABLE !A PEE 181. POLLUTANTS 'r**JTW W~ ra i iPM A AND C. D;ES THIS OUTFM DISChMGE CONTAIN ANY PROCESS WASTEhATER! (IFNo,G3 TOE) (f F YES, GO TO 0) YES PC gg LNFCRMATION D. !!CICATE 4+1CH GdMS FRACT!0r43 MUST BE TESTED FOR. (REFER TO TABLE !A PEE L.i.1) h VOLATILE FOR N011,! FOR EACH CdMS FRACTION O(CKED,EACH SPECIFIC ORGANIC TCXfC POLLUTANT WITHIN SURFACE gjo ppACTION N BE A'dLYZED FOR (SEE TABLE IIA Par,E M. IN AD0lfim ALL PRlPARY BASE / NEUTRAL WATER If0USTRY APPLICAt.TS WITH A PROCESS WASTEWATER DISCHARGE g PROVIDE QUANTITATIVE O* DISCHARGE y ACID ONLY RECORD E DATA GN FORMS PROY!XD (ITEM 7) IN THIS B00:417. (CONil?CE WITH E*K BELCW) PESTICIDE E. IF L2 St.RFACE MATER DISCHARGE APPLICANT (PRIMARY OR SECOfCARY INDJSTRY), REGARD ESS OF !< TYPE CF DISCHARGE, Mov$ CR *ns REASON TO BELIEVE THAT ANY P0t.LUTANT LISTED NOT APPLICABLE / BELIEVED ASSENT IN TABLE I!A A'.D IVA PAGES MM IS DISOdRGED F901 ANY OUTFAti,DE QUANTITATIVE IIM BE PROVIDED. RECORD ALL DATA ON F05 Pts PRWIDED (ITEM 7) IN THIS BOOKLET. p, j gg g F. IF ANY St.RFACE WATER DISCHARGE APPLICANT (PRIMARY OR SECONDARY IPOUSTRY), REGARDLESS OF TYPE OF DISOS%E, cods OR HAS REASON TO BELIEVE ANY POLLUTANTS LISTED IN NOT APPLICABLE /8ELIEVED At .T TA8d VA Pr{ 'Q A3E DISCHAprG FRnM ANY CUTFALL Tif APPLICANT M DESCpitE REASch$ FOR THE POLLUTANT BElfG PRESENT #C PROVIDE ANY AVAILABd QUANTITATIVE DATA. RECCRD ALL DATA Cr4 F0ftts PROVIDED (ITEM 7) IN THIS 800xLIT. PRESENT/ DATA l$ ATTAOdD G. Id.L SLRFACE HATER DISCHMGE APPLICANTS (PRIMARY NO SECOPOARY INDUSTRIES)

0:

l ( 907 APPLICABLE / BELIEVED ABSENT OR PNATACTURES 2, 4, 5 - TRIOuROPHEfCXY ACET!Q ACI (2, 4, 5-T); ,4,bTRipATRICHLOROPHEfOXYf PROPN1IC ACID (SILVEX, 4, 4,2-DIOwom0ProaTE EPSONi; 0, , 4, ,TP) DITTWYL 0-te, ~RCae exv ETHYL 4, 5-TRIO 4!OR0fHENYL) PDCSP>0p0TH10 ATE (RottaEL); , 4, 'rTR!CHLCROPt(NOL (TCP); OR HEXAOt.OROPHEPE (HCP); (ALL DATA FOR THE A50VE PtJST BE GENEAATED USING STNOARD ANALYTICAL CALIBRATION PROCEDIRES) OR MiodS CR HAS PEASON TO EELIEVE THAT TCDD IS OR MAY BE PRESENT IN THE!R D!$ CHARGE. t%I REPCRT '1JALITATIVE DATA, GDERATED WICy UitED A SCREENING PGOCEDLRE NOT PRESENT/ DATA IS ATTACHED UtahPATED m!TH #eALYTICAL SINCMDS, FOR 2, x / 8, - TETRAO(ORODiBENzD-P-P!OXtN t (TCDD). PECCRD ALL DATA ON FOPMS PROVIDED (ITEM /) IN THIS BOOKLET. J. IF D( SURFACE aATER DISOdPGE APPLICANT KroWS OR HAS REASON TO BELIEW THAT N NOT WCA8d 81CLOGIC/4 TCxlCITr TESTS WEGE MADE IN Di LAST TWEE (3) YEARS ON ANY OF Ttt APPLICMT S DISCHAPGES OR ON A RECELVING MATER IN RELATION TO A DISOSRGE, PRWIDE THIS stEO,1hATIOr AS M ATTAOfE.T TO THIS APPLICATICN. APPLICABLE /SEE ATTAOG t. IF A C31 TRACT L/,ICRATJRY OR Cur. SLAT!?6 FIRM PERF0FFTD ANY OF T E AIAlvSES REQUIRED pof MICABd 6f THIS AFPLICATKN, FR0vlDE Di fereE AiO ADDRESS OF FACH LABORATORY OR F191 NO D( At:ALrSES PEVOP!TD AS AN ATTA9ffMT OF THIS AP'LICATIVN. APPLkCABd/SEE ATTACHED L. D) Voti DISCWG( #lf OTHER T0XIC CP !PUURI ICAL SLESTANCES NOT LISTED IN TAPLES IV PV4 O ND !!A TWOTM VA PW45 LkU. IF VEs. TVN IDENTl*Y DE FOT WCABd O(MICAL SdSTANCES NeD EST!*uTE THE FINAL EFFuiNT COJCENTEATIONS. $dPflf TMIS IJUN4 TION AS ke ATTAOftNT TO THIS APPLICAT!Wd. APPLICA&LE/SEE ATTAOG % WATER DISC HARCED FoR DE-ICIN G j5 THE SA MG AS o oT/Auf oo/ AND 002, 742EFofE, Ino,4nA ( 01 cHicAN ELecRic. cerqANY R6QOESTS PERMIS5lo u To USE WE ScmWC OATA Mom OuTFAU. 00I ol O uTf4L 002 Tb CHARACTE29 2E TW$ p/SCHARG, 1 9 .'l. SECTION 11 PERMIT , K 000 SSM NUMBER SEE INSTRUCTIONS ON REVERSESIDE. j.. ME N ,did,3i ITEM A. USE THIS DATA SEET TO RECORD INFCRMATION AS REQ;1RQ IN: (OECK APPROPRIATE BOX FOR *!CH INFOR9710N THl$ CATA SHEET *EPRESF.NTS.) 7

1. SECTION 11, ITEM k. GROWDMTER DISCHARGE INFOR*ATION (PE4 35)

CRiflCAL

2. SECTIOe !!, ITDt 6. Prim!TV #0LLUTMR$ IN SlMACE Me DISCWE (PAGE 37) b 3.

8. BELON: CRITICAL MATERIALS (TABE fv) IN SURFACE MTER CISCHARGE (PAGE 39)

POLLUTANTS e HAZARDOUS i SUBSTANCES 8. LIST ANY CRITICAL PATER!AL (TABtJE IV PAGE 6) NOT ADmESSED IN SECT!m !! ITD9 6 *RIORm PCT MICAmi PRLUTndTS WICH YOU ICDS OR HAVE REASON fn BELIEVE TO BE PRESD6 IN TIE DISCMRCE. SEE IN REVERSE S!OE OF THIS PAGE FOR FURT)fR DIRECTIONS. h 'AP5t! CABLE (SEE EELO8) OtSCHARGE A. Mf( OF CRITICAL MAfD!AL OR PRIORITY POLLUTANT ,,g 8. AVDAGE COdCENTRATION; SMRE TYPE; I CF AN4 LYSES ~ g g g g g g g g

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= C. .m, moum 0,. ue MSS ACX3ITIChAL PAGES OF TH!$ ITD17 APE ATTAo(D FOR T){ REST OF T){ CRITICAL YES MTERIALS #c/Ot PR!CRITY POLuffANTS RE2;tRD TO BE PEPORTC. L., NO -N SEE NOTE on pact 9, ooTFALL oo3 l 11 SECTION 11 j gER MIOoo SD 7 SEE INSTRUCTIONS ' ON REVERSE SIDE GMALL tlttER ,0,0 n A n ITEM A. =Te Di= iN iWi t tSM t ma ioiG. m ioiaib, wu i h% 1 S. - RE=i- -T= ur - = = = = = .t.4,o c. a i u 'i c a,* ..,, I m 4TO C. vou Of SOWIGE SEA 50MLLYl I' *' # # DISCHARGE LOCATION D. IF YES, LIST DISOWEE PDICOS NQ MO. / DLY PC. / DAY e $CHE M E ,, w Twaxy w w e FLOW L L_1 W Twi0mH 1 L.J l I l CATE t t l t i 1 TWICEM l l I I I I WASTEWATER IN.ha. Ht./ DAY IN./Wi(. TYPE CODE E. L4 0 M ICATION RATE Nk l 3 l, (,,,,j [ t t, g_j l t t L,,,,,) 1 CONTACT NASTDdTER TYPE CEE F. TYPE OF NASTEMTER DISOWIGE U U LJ L_J U 2 NONCONTACT G. DISOWIGE SOEDL11 (YEMILY AVERAGE) g3,, i 2,Q, 3,f, ,3,4,g, COOLING lit CDCE DISO WIGE FLDv RATE g g g g g g g g g gg, g 3 PROCESS H. 4 SANITARY 'O Lb S STORMWATER DAILY MINI U 8 i '4 ' J lb 0"ILY *I" UNIT CODE AUT>oRf:ED 1 1 I 10 i. iS iG s y,

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I I A. Do YOU USE MATIJt TREATMENT ADDITIVES TO TREAT YOLR DISOWIr(') (IF #0, CONTINIK TO IT09 3) YES PC S. N#f FLPsCTION, APO O(NICAL CD1 POSIT 10N OF TfESE AICITtWS. 2 WATER TREATMENT NQ ADDITIVES C. Natt APO ACERESS OF MMAFACTlflERS OF MSE AMITIVES. UNITS CODE 1 Mg/l 2 Ug/l g4 D. EXPECTED DISOWIGE CCNCENTRATION OF A2tTIVES. NA E ^" E E 8 i f ' U ACCITIVE Natt e i e i t__] ; e e s e i t__l ; I G ITIVE hitT I ' ' ' ' t !J' l. l J ' ' ' ' ' I-I GIT!W M ,, i t,,,,j y (,_ e i e n [_J L_) j L, OO E. DO YOU TREAT M DISOWird TD flDOVE ADDITIVES? NA YES F. WST IS THE RDOVAL EFFICICCY MD DISOWE FRE'JJDiCV7 QQ g$cWCE FWiM 1gegvg HR$./ DAY DAYS /W. AmlTIVE PWf f I I I I I lI A:08TIVE PeME I t i ' ' I

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ADDIT!W WE I t i l i I L._J G. AS AN ATTAOtENT TO THIS APPLICATION Movi:E $PECIFIC M#eALINe OR A'3ATIC Toxic 0Lfr.lCAL DATA Ot REFERENCE *MICH ARE AVAILABLE AND thFGMATICh 06 M RATE & WJtADAflGt OF T>E PRODITS FCR LACH ATCITIVE. NA 31 l SECTION 11 QRMl M OOOIOM7 BER SEE INSTRUCTIONS ON' REVERSE SIDE amu. ruta

ioioi4, ITEM A.

MPE OP PROCESS C=RisuTim 70 mE dis =GE ,f, , 5, r, ri,,c; y,u, ,8, t,o,N 4/,9, /, /, De0UG4 THIS OJTFALL 40 SfC M*t i i B. PROCESS SCHEDA.E (YEARLY AVEMGd IAihI f.31 hd ggy ggfyg N C. PROCESS wu,E ra uTE , i 3iB i., / 4.3, *F PROCESS wTAc YEA,tY BASIS : 1984 Flow DATA STREAMS ,,,,,,,,o,4 , ty n,x CONTRIBUTING Q-TO t O t.17. i[s ib ((g ) mity m;u I t t i D. PROCESS PRODUCTION RATE g g,,,,, g, g A. MPE OF P% CESS C0tmt!BUTING TO DE DISQARGE Df0 UGH Tkl$ QUTFALL NO $1C CM NA i ' i f ' ' ' ' ' ' ' ' ' ' ' ' I I' N (YNY A'N peutS/gy i I I DaygygAR t f 1 1 m wit Gs4 C. PROCESS WUIE Flow RATE TOTA YEARLY I I I I I I I I I I k3 es I I I ' I I I I DAILY MIN!Ptf1 UNITS CODE DAILY max!PtM f f 1 f ft i I f f (_ ] 2 GALLONS D. PROCESS PRODUCTION RATE I f I I I f I I I l ! A. FWE OF PIUCESS CONTRIBUT!rG TO DE DISOdRGE YARDS DeOuGi THIS cuinu. Ato SIC CECE Nk i i I f I f f I I I I I I I ' ' ' ' I I B. PROCESS SOCULE (YEARLY AVEMGd gggy , g f NYS/ YEAR I ' ' I w

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C. Pf0 CESS WLiff Ft.fW RATE GPD TOTA YEARLY I I I I I I I I I I U { ggty mgnge i f I I f f i 1 ' I l_.] DAILY MAxt e i f f I I I I ' ' I L-I bb D. PROCESS PR03 JCT!ON RATE g, t t t t, i e TIME 1 HOUR A. NME OF PROCESS emitBUTim M DE DISCMRGE gg ,,,,,,,,,,,,,, e ,, r i nsoucH Nf s Mmu 40 S!C CM B. NSS N MY AM 3 WEEK soups / DAY I ' 8 NYS/vEAR l I I ' O MONTH m mIT m y C. PROCESS WLt!E FLOW RATE TOTE YEARLY 8 ' ' ' ' ' I ' ' I lI 8' g DAILY MINIPtM i f I f f I f f I I U a. gggty g g g I t f f f I I I I I (! mlTS TIPt D. Pf0 CESS Pf00UCTION RATE I 1 t I f f f I t LJ A. NME OF PROCESS CONTRIButtrG TO DE DISOARGE D@One THis CUTYAU_ 40 SIC CTE g f f I f f I, I,,,,,,,,, ;,, B. Pf0 CESS SOCI.LE (YEARLY AVEREd p$/gy p g g myS/ YEAR Lf f f y, mlT C2 g C. PROCESS WLttE FLOW RATE g3gygy i, e t i t i t f f U um DAILY MINlatf1 I I ! ! I I I ' ' ' LAILY max!Ptf9 8 I I I f f I i I ' LJ WITS / TI4 D. PFOCESS PRODUCTION RATE , i i i t ! I t t J L._J SECTION 11 PERMIT C IIIOOO5877 NUMBER 7 SEEINSTRUCTIONS ON REVERSE SIDE EE IN t O,d, t !$ M CIS Fatt9 THIS OUTFALL l;tREC TO THE GROLfD OR A. GROUPDeATEy45.IF 'O, CON'!4)E TO ITD9 YES to 8. HAS A HYtROGE0 LOGICAL ST!EY OR tTS EQUlvALENT BEEN PERFORtD OR !$ THEPE StFFICIENT CURRENT HYCROGE - ICAL INFOPATICN AVAILJ3LE AS REQU GED Y t=ATER RESOURCES YES po COfi!SSICN PMT ) GRotJO=ATER RULE OF A LUST ll4, 1 R. (PAGE @)FOR GROUNDWATER THIS O!$TIPG CR PRCPOSQ DISCHMGE IF YES ATTACH A C&Y & THE REPGtT. DISCHARGE ARE Ya; R& ST! AN DEMPTICN FRO 9 SLEM!TTI'G A HYDROGEOLOGICAL REPORT Ur0ER C. RULE R.38.1/ y(.0) (PACE M) CR FRO 1 GRotJOi4TH MONITCRlrG PEQJfDOTS INFORMATION VES to UFCER FULE 4.J2.3.Cu,3 (3) (PME 47) 0F M PMT d RULES. IF YES ATTACH aX7DTS #D DP;.ANATION TO CDONSTRATE THAT Y0t.R DISCHARGE WOLAD QUALIFY FOR N A's t> evTt: a. D. ' ARE YOU RE1EST!!G A VAAl# ACE FRCH Rgy E.3 (PAGE lfi ) (NorCE;RADATICrt) 0F YES to THE asATER PESCURCES C7tilSSION PART d GR0(FOsATER RULES'. !F YES. ATTACH SUCH DOCLP'OTS AS AECESSMY TO TRATE T){ D Fat A VARI IN TERMS OF M q' CRITERIA SPECIFIED IN RULI . 0 (PAGE 4 ) & THE PART RULES. 1,lST A;J). CHEMICAL SthST# ICES teitCH ME lN P'ICHIGAN'S CRITICAL 7"A E. RfALS REGISTER TABLE IV (PAGE 0 AC/OR U.S. EPA'S PRI'RITY P0l1UTANT L!$f TABLE V (PAGE OR ANY OTIER SLSSTkJCES NOT APPLICABLE / BELIEVED ABSENT i+#ICH ARE CR MAY BECOT IPUURICUS TO T)E u!SIOdTD USES OF T>E TER OR TO T)E PU2LIC HEALTH THAT ARE CISCHMGED OR EXPECTED TO EE DISOWtGO TO T>E CHClfOeATER_SY THl3 FACILITY. EST!PATE THE FIP.4L EFFLUDT CONCENTRATION WO RECDID ALL DATA IN ITEM / OF SECTIO 4 II IN THIS BOCMLET. RESENT, DATA N!S IN ITm 7 Th( APPLICANT MAY BE RECIJ!RO TO DO ADDITIO4AL MSTE #dLYSES. g A. DISOMCE ChMACTERISTICS CChCENTRATION LNITS CODE # #dLYSES S#fti TYPE ^# ITEM " " " ' ' " ' ' " " ' ' ' ' """ 6"*' '1' " 5 ' COD (OL'1tCAL OnUEN CDwo) I ' ' l*I I I ' I f ' '8 f ' ' L1.1 1 ' f LJ b W U OC 6TAL ORG#itC WsOn) WASTE A R m!A Nlm (AS h) l I ' 'I I=' I I I l II ' ' ' W CHARAC-e TERaSTICS ' TOTAL SUSPOW SOLICS I ' ' ' *I ' ' ' l ' ' I I ' ' ' l.l I W e UNITS CODE TOTAL PteSPHORUS (AS P) I t f f .I I t i i t f I. I I I t L}.] f f I LJ 1 Mg/l ' ' ' I *' ' I I I I ' ' ' I ' I k3 2 Ug/1 TOTAL RESIDUAL 01LCRINE = 3 COUNTS / I ' ' ' *' ' ' ' ' ' ' 8.' ' ' ' d8 U 100 ml DIS $0LW D c e ngN 4 S. U. .pg l l l,U ,,,,y g,,,,g,g g,,j 5 'F 6 LBS/ DAY I ' ' ' ' ' ' ' ' ' I ' kJ FM COL FW BACTERIA 'TDfERATWE (SMR) ' ' I

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TDfERATURE (WINTER)

'*L-J I I '. I. J LE.1 I i ' LJ OTHER 4 STEhATER CHARACTERISTICS B. 1 i t 0,I,L,R,6,RgE,A,S,E, g y Lg,y g SAMPLE t t t i i e i t e i i i t.I i t t i i i I.I I t i L_.J t t I LJ 1.1EL U ' ' ' W 1 cRAs 2 24 woun ,,,,,,,,,,,,,,,,, J LJ r i i u COMPOSITr. I i t i ! t t i i e t i t e i 1.I i t i t i i 1.I t i I LJ t tJ t i e t t i i e i e i 1 e i i t. e t i t e i s.: I e i LJ i e t L; i i t i t i i i t i t i i i t i.i i t i i t i e.t I i I LJ l i I LJ See attached sheets for data. Note: Results for triarylphosphate esters and hydrazine in Attachraent I. 7 REnffT TO: Laboratory Services DMeiort Park Wes? Two ,L, 5360 Campbene Mutt Road Cliff Mine Road -.I Mttsburgh, PA 15206 Mttsburgh, PA 15275 412-788-1080 l AB A N Al._ Y S I S R E P C3 R T CLIDIT llAlf: IllDIANA & MICNIGAN ELECTRIC CO. NUS CLIDIT NO: 010904 AMRESS: P. O. 30X 40 NUS SAWLE 110: 15021689 FORT llAYlE, IN 44001 VDIDOR 110: REPORT DATE: 03/24/85 ll0RK ORMR NO: 55830 ATTENTION: Itt. Jolti itililEY DATE RECEIVED: 02/27/85 SAMLE IDDITIFICATION: LplIT 1 S6 BLOO0lill 02/26 TEST KTERM!rdTIOll RESULTS UllITS 1361 IIPKS PAlti V-l M010 Aluminus ( A1) < 0.1 ag/l 1040 Serius (le) < 0.1 og/l M150 Cobelt (Co) < 0.01" og/l 1190 Iron, total (Fe) < 0.01 ag/l M230 Megresius (Mg) < 0.001 ag/l 12 # Mangerese (Mn) <0.01 og/1 M2# Molybdenue (Mo) < 0.03 ag/l 1340 Tin (Sn) <1 ag/l M350 Titanius (Ti) < 0.5 ag/l 1055 Boron (3) < 0.2 og/l il060 Broeide th) <2 ag/l l 1225 Color,True 120 Pt-Co W310 Fluoride, total (F) < 0.1 ag/l 1390 Mitrate (N) < 0.1 ag/l li410 Nitrite (N) < 0.01 ag/l 1435 Nitrogen, Kjeldehl (N) 0.2 og/l W440 Nitrogen, Organic (N) 0.2 ag/l 1 15 # Phosphorus, total (P) < 0.01 ag/l Il730 Sulfate, turbidieetric (SO4) <1 og/l 17 # Sulfide (S) < 0.1 ag/l i ll760 Sulfite (S03) <2 og/l 1770 Surfectents (MBAS) < 0,1 ag/l j M362 MPMS PART V-C T0XIC METALS i M020 Antimony (SD) < 0.1 og/l h030 Arsenic ( As) < 0.001 ag/l 1050 Beryllius (le) < 0.002 og/l M090 Codnium (Cd) < 0.005 ag/l 11 # Chroelue (Cr) < 0.01 ag/l M160 Copper (Cu) < 0.01 ag/l 1200 Leed (Pb) < 0.03 ag/l M250 Mercury (Hg) < 0.0002 ag/l PA E NO: 1 h A Halliburton Company CLIENT ORIGINAL REaffT TO: Laboratory So, vices Division Park West Two N U' S 5350 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgn, PA 15275 412-788-1000 IAB ANAL _YSIS REPQRT CLIENT llAE: IllDIANA & MICHIGAN ELECTRIC CO. IlUS CLIENT NO: 010904 ABORESS: P. O. DOX 60 NUS SAlfLE 1101 15021689 FORT liAYE, IN 46001 VDIDOR 110: ItEPORT DATE: 03/26/85 il0RK ORDER 110: 55830 ATTENTI0lls IWt. Jolti HUGET DATE RECEIVEls 02/27/85 SAlfLE IDENTIFICATION: 13 TIT 1 S6 BLOWDOWN 02/26 TEST KTERMlllATIOll RESLLTS UllITS It270 Nititel (Ni) <0.03 ag/l M290 Selenium (Se) < 0.004 ag/l 1300 Silver (Ag) < 0.01 ogIl M330 hllius (TI) < 0.1 ag/l 1390 Zirs (In) < 0.01 ag/l V270 Cyanide, total (CN) < 0.005 ag/l 1500 Phenolics < 0.02 ag/l M220 Lithium (Li) < 0.01 ag/l 1110 VOLATILES-PP IN llATER OY01 Acrolein ( 100 ug/l IV02 Acrylonitrile < 100 mg/l DV03 Benzene <5 ug/l IV05 Brosofora <5 ug/l OYO6 Carbon Tetrochloride <5 ug/l 1907 Chlorobenzene (5 ug/l DV00 Chlorodibronomethane (5 ug/l IV09 Chlotoe W ne < 10 vg/1 DV10 2-Chloroethylvinyl Ether < 10 ug/l IV11 Chlorofors (5 ug/l DV12 Dithlorobronomethane <5 ug/l IV14 1,1 Dichlorcethane <5 ug/l 0V15 1,2-Dichloroeshone <5 ug/l IV16 1,1-lii:hloroethylere <5 ug/l CV17 1,2-Dichloropro;wne <5 ug/l W18 1,3-Dichloropropylene <5 og/l OY19 Ethyltenzene <5 ug/l IV20 Methyl Broeide < 10 ug/l OU21 Methyl Chloride < 10 mg/l IV22 Methylenechloride <5 ug/l DV23 1,1,2,2-Tettothloroethane <5 ug/1 IV24 Tetrochloroethylene(Perchloro) (5 vg/l DV25 Toluene <5 og/l PAE 110: 2 h A Ha!!iburton Company CLIENT ORIGINAL REldfT TO: NUS Laboratory Services Diviskm Parit West Two 5360 Campbells Run Road Chtf Mine Road Pittsburgh, PA 16206 Pittsburgn, PA 15275 412-788-1000 l._ A B ANALYSIS REPORT CLIENTllAE 1HDIANA % MICHIGAN ELECTRIC CO. MUS CLIENT NO: 010904 ADORESS: P. O. tot 60 NUS SAlfLE NO: 15021689 FORT WAYE, IN 44001 VENDOR NO: REPORT DATE: 03/26/85 WORK OR KR MO: 55830 ATTENTION: IWt. JOHN HUGEY DATE ECEIVEB 02/27/95 SAlfLE IDENTIFICATION: UNIT 1 SG BLOUDOWN 02/26 TEST NTERMINATION RESULTS UNITS Om 1,2-Trans-Dicnloroethylene <5 ug/l DV27 1,1,1-Trichloroethane <5 mg/l IV29 1,1,2-Trichloroethane <5 ug/1 OV29 Trichloroethylene (5 ug/l IV31 Vinylchloride <5 ug/l 0120 ACIDS - PP IN WATER i 0401 2-Chlorophenol <10 ug/l 0A02 2,4-Dichlorophenol < 10 ug/l lA03 2,4-Dimethylphenol < 10 ug/l 0404 4,6-Dinitro-o-cresol ( 50 ug/l lA05 2,4-Binitrophenol ( 50 ug/l DA06 2-Nitrophenol < 10 ug/l lA07 4-Nitrophenol < 50 ug/l 0406 p-Chloro-e-cresol ( 10 ug/l lA09 Pentochlorophenol < 50 ug/l 0410 Phenol ( 10 ug/l lAll 2,4,6-Trichlorophenol ( 10 ug/l DE30 Acid Extraction-Water 0130 BASE NEUTRALS - PP IN WATER 0901 Acenophthene ( 10 ug/l 1902 Acenophthylene < 10 ug/l 0903 Anthrocene < 10 i.g/1 8304 Benzidine < 50 ug/l 0805 Benzo (s)Anthrocene < 10 ug/l 1906 Penzo(o)Fyrene ( 10 ug/l 0807 3,4-Benrefluoranthere < 10 ug/l 1908 Benzo (ghi) Perylene < 10 ug/l 0B09 Berzo(L)Fluorenthene < 10 og/1 1910. 31s(2-Chloroethory) Methene ( 10 ug/l 1 0011 Bis (2-Chloroethyl) Ether ( 10 mg/l 1812 lis(2-Chloroisopropyl) Ether ( 10 ug/l 0813 Bis (2-Ethylhexyl)Phtholete < 10 ug/l PAE NO: 3 h A Halliburton Company CLIENT ORIGINAL REtelT TO: Laborecory Services Division Park West Two NUS 5350 Campbons Run Road Cliff Mine Road Pittsburgh, PA 15205 Pittsburgh, PA 15275 412-788-1000 LAB ANALYSIS REPORT CLIENT llAE IllDIANA & NICHIGAN ELECTRIC CO. NUS CLIENT NO: 010904 ADDRESS: P. O. 30X 40 IRIS SAMPLE NO: 15021689 FORT WAYlE, IN 46801 YENDOR110: EPORT DATE: 03/26/85 WORK ORDER 110: 55830 ATTENTION: Ift. JONN HullEY DATE RECEIYED: 02/27/85 SAMPLE IENTIFICATION: LIIIT 1 SG 9 LOWDOWN 02/26 TEST DETERNIllATI0ll RESLLTS UNITS (3 14 4-37onophenyl Phenyl Ether < 10 ug/1 0015 Butyl Benzyl Phthelete < 10 ug/l 1916 2-Chloronophthalene ( 10 ug/l 0917 4-Chlorophenyl Phenyl Ether < 10 ug/l 1918 Chrysene < 10 ug/l 0819 0ibenzo( e,h)Anthiscene < 10 ug/1 1320 1,2-Bichlorobenzene < 10 ug/l DB21 1,3-Dichlorobenzene < 10 ug/1 1922 1,4-Bichlorobenzene < 10 ug/l 0823 3,3'-Dichlorobenzidine ( 10 ug/l 1924 Diethyl Phthelete < 10 ug/l 0825 linethyl Phtholote < 10 mg/l 1926 Di-N-Butyl Phthalate < 10 ug/l 0327 2,4-Dinittotoluene < 10 ug/l 1328 2,6-Dinitrotoluere ( 10 ug/l 0929 Di-N-Octyl Phtholote < 10 ug/l 1830 1,2-Diphengthydrorfre( Azobz) < 20 ug/1 0831 Fluoranthene < 10 ug/1 1832 Fluorene ( 10 ug/l 0933 Hexechlorbenzene < 10 ug/l 1934 Hexachlorobutodiene < 10 ug/l 0935 Hexochloro-cyclopentodiene < 10 ug/1 8336 Hexochloroethane < 10 og/1 0B37 Indeno(1,2,3 cd) Pyrene < 10 ug/l 9338 Isophotone < 10 cg/l 0839 14cphtbolene < 10 ug/l 1540 Mitrobenzene < 10 ug/l 0641 N-Nitrosodieethylonine < 10 vg/l lM2 N-Nitrosodi N-Prg ylonine ( 10 ug/l 0B43 N-Nittosodiphengleine < 10 ug/1 8544 Phenanthrere < 10 ug/l 0345 Pyrene < 10 ug/l PAE NO: 4 h A Halliburton Company CLIENT ORIGINAL REtefT TO: Latwatory Services DMelon Park West Two NUS $300 Campbells Run Road Cliff Mine Road Pittatwgh, PA 15206 Pittsburgh, PA 15275 mg 412-788-1000 LAB ANALYSIS REPORT (LIDif NAE: IISIAllA & MIDIIGAN ELECTRIC CO. NUS CLIENT 110: 010904 ABORESS: P. O. 30X 60 NUS SAlfLE NO: 15021689 FORT WAYlE, IN 46001 VEDOR MO: HEPORT BATE: 03/24/95 WORK ORE R NO: 55830 ATTENTION: IEt. J0lti HUSIEY DATE RECEIVED: 02/27/85 SAIFLE IDDITIFICATIOll: LBIIT 1 SG ILO W 0lti 02/26 TEST MTERMIllATI0ll RESULTS UNITS 3 46 1,2,4-Trichlorobenzene < 10 mg/l DE25 lose liestrel Extraction-Water 0141 PRIORITY POLLUTANT PCB'S DE11 PCI Extrection - Water IP19 PCI-1016 < 0.5 og/1 OP20 PCI-1221 ( 0.5 og/l IP21 PCI-1232 < 0.5 vg/l OP22 PCB-1242 ( 0.5 mg/l IP23 PCI-1248 < 0.5 ug/l DP24 PCI-1254 < 1.0 mg/l DP25 PCI-1260 ( 1.0 ug/l R450 RADIlm 226 AllD 228 2 04 Rodium-226 < 0.4 pCi/1 R005 Radium-228 <2 pCill R800 Gross Alphe (1 pCill R801 Gross Sete 2.8 t/-1.1 pCi/1 1032 Aesonie os N (distillation) < 0.1 ag/l WO50 900, 5-dog (02) <1 ag/l 1100 Carbon, organic (C) < 1.0 eg/l W120 C00 (02) <5 mg/l 1610 Solids, suspended at 103 C 2 ag/l COMM0lTS: Reviewed end Approved by: PM PAGE NO: 5 h A Halliburton Company CLIENT ORIGINAL Atast? TO: i Laboratory Services DMeion Park West Two NUS 5360 Campbells Run Road Cliff Mine Road Pittsburgh. PA 15206 Pittsburgh, PA 15275 412-786-1000 LAB ANALYSIS REPORT CLIDIT liAfE: INDIANA & NICHIGAN ELECTRIC CO. MUS CLIENT 110: 010904 AIORESS: P. O. BOX 60 NUS SAWLE NO: 15021690 FORT WAYlE, IN 46001 YENDOR NO: EPORT DATE: 03/26/95 WORK ORER 110: 55830 ATTENTI0Ils IWt. Jolti HUGIEY DATE RECEIYED: 02/27/85 SAIFLE IDDITIFICATION: UNIT 1SGILOWDOWN-GRAB 61 02/25 0720 TEST MTERMIllATION ESULTS UNITS 1A32 Fecal Caliform - IFil <3 col /100e1 W150 Chlorine, residual llPD (C12) < 0.1 og/l 1490 pH 7.8 U600 Oil, extraction gravinetric 2.3 ag/l 1 C019ENTS: Reviewed and Approved by: JNC h A Halliburton Company CLIENT ORIGINAL i RCMIT TO: 1.aboratory Services Division Park West Two NUS 5360 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-786-1000 LAB ANALYSIS REPORT CLIENT MAE IllDIANA & MICHIGAN ELECTRIC CO. IIUS CLIENT NO: 010904 ADDRESS: P. O. 30X 60 NUS SAlfLE NO: 15021691 FDRT llAYIE, Ill 46001 YENDOR NO: IIEPORT DATE: 03/26/85 110RK ORER NO: 55830 AllINTION: Itt. Jolti HUGET DATE RECEIYED: 02/27/85 SAlfLE 190lTIFICATION: UllIT 1 SG 3 LOUD 0litt - GRAB 42 02/25 1320 TEST DETERNIllATIOll RESULTS UllITS 1432 Fecal Califors - 1991 <3 col /100ml 9150 Chlorire, residuel DPD (C12) < 0.1 ag/l 1490 pH 7.9 9690 Oil, extractim grevisettic 2.2 ag/l i D M ENTS: Reviewed ord Approved by: JIC h A Halliburton Company CLIENT ORIGINAL REtelT TO: Laboratory Services DMeion Park West Two NUS 5350 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15205 Pittsburgh, PA 15275 412-786-1000 LAB ANALYSIS REPORT CLIDIT MAE INBIANA & MICH16All ELECTRIC CO. NUS CLIENT NO: 010904 ADDRESS: P. O. 30X 60 NUS SAMPLE NO: 15021692 FORT WAYE, Ill 46801 VDIDOR NO: REPORT DATE: 03/26/95 WORK ORER 110: 55830 ATTENTION: Ift. JOlti HUGHEY DATE E CEIVED: 02/27/85 SAIFLI IDDITIFICATIOII: LIIIT 1 SG 3 LOWDOWN - GRAI 93 02/25 1926 TEST KTERMINATI0ll RESULTS UllITS lA32 Fecel Califors - IfH <3 col /100e1 W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 8.2 W680 011, extraction growinetric 2.0 mg/l CDitENTS: Revi wed and Approved by: JIC h A Halliburton Company CLIENT ORIGINAL REasf7 TO: Laboratory Services DMaion Part West Two NUS 5360 Campbells Run Moed Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh. PA 15275 Mg 412-788-1000 s LAB ANALYSIS REPORT CLIENT IWE: ISIANA & NICHISAN ELECTRIC CO. NUS CLIDIT 110: 0109H ADDRESS: P. O. BOX 40 NUS SAWLE NO: 15021693 FORT WAYlE, IN 46001 YDIDOR 110: ItEPORT DATE: 03/26/95 UORK ORDut 110: 55830 ATTENTION: ISt. JM HUGIEY DATEItEMI'KB: 02/27/85 SAMLE IDENTIFICATION: UNIT 1 SG BLOWDOWN - GRAB H 02/26 0125 TEST DETERMINATION RESILTS UNITS IA32 Fecal Califore - In (3 col /100e1 W150 Chlorine, residual DPD (Cl2) < 0.1 ag/l I490 pH 8.1 U600 Oil, extraction gravinetric < 1.0 mg/l l l C H ENTS: Reviewed and Approved by:.plC h A Halliburton Company CLIENT ORIGINAL r I SECTION 11 PERMIT y ,gggg SEE INSTRUCTIONS NUMBER ON REVERSE SIDE asu ma io,ofA. TM joLLDwird REQdSTED INFOEATION N!!

F ADDRISSED EZ $.l S@ FACE HATER DISCHMGERS.

NEW USE DISchMGERS MI.l. PR041Lt urECTED VALES F# TM QUANTITATIVE 40 'CE. %EITATIVE IVCPtMTION REGULSTED BELW. A. 85 THis FACILITY A PRIMMY tmTRY? (REFER TO TABd IA PYE 91) III IO ( tr 'o, no 70 E) ( f F nt CO in P) PRIORITY B. ITICATE TYPE W PRIMRT INDUSTRY AS LISTED IN TABLE lA Pr{ 4J, POLLUTANTS Dit*8 F *f m d 1 I IL I lb I IPIwl 4, AND C. DCES THIS OUTFM OlSCHMGC CONTAIN ANY PROCEis WASTEWATER / Or w, m TO El (15 MS, o m c) S NO ADDITIONAL INFORMATION D.,1?CICATE *!CH GC/MS FRACTIONS HUST SE TESTO FOR. (PEFER TO TABLE IA PW4 d) VOLATILE FCR tcE! FCA EACH GC/MS FRACTICN OECKO,EACH S'ECIFIC CPGANIC T0XIC POLLUTANT WITHIN SURFACE EAO FRET 10N Nil BE MALY'ED FOR (SEE TABLE Ila PArg U2. IN AD0lf!CN, ALL PRlPWtY BASEhEUTRAL WATER IfCUSTRY APPLICA*.T3 mITH A PROCESS WASTEWATER DISCHMGE 23&I PROVIDE QUANT! TAT!ht WA EAm OlC WANT IN TABLE IIIA.M 4J. DISCHARGE ActD ONLY RECMD ALL DATA ON FCRtS PROVIDED (! TEM 7) IN THt$ B00KdT. l (CONT!P8JE wtTH EM BEL 0w) PESTICIX E. IF 4:;L S$ FACE HATER DISCHMGE APPLICANT (PRIMRY OR SECON!%RY IN3JSTRY), REGARDLESS OF InL DPE CF DISCHMGE, KNOWS OR HAS REASON TO BELIEVE THAT ANY POLLUTANT LISTED NOT APPLICABLE / BELIEVED A8SENT IN TABLE IIA AND [VA PAGES M 15 DISCHMGED FRQ1 ANY GlTFALL,TM QuM4TITATIVE i

ml BE PR0v!X3.

RECORD ALL DATA ON F0F?tS PROVIDED (ITEM 7) IN THis BOOKLET. gj g F. IF ANY $@ FACE WATER D[$CHMGE APPLICANT (PRIMMY OR SECONCARY IN3JSTRY), REGARDMSS OF TYPE OF D15. VIGE, h70rs OR HAS REASON TO BELIEVE ANY POLLUTANTS LISTED IN NOT APPLICABLE / BELIEVED ABSENT TASd VA PYE ARE DISCHARr,ED FRrN ANY CUTFALL TMI APPLICANT j$I DESCRIEE REASch5 FOR TK POLLUTANT BEltG PRESENT WO PROVIDE ANY AVAILABLE QUANTITATIVE DATA. RECDPD ALL DATA CN F0mS PROVIDED (ITEM 7) IN THIS BOOKLET. PRESENT/CATA IS ATTAO(D G. ALL SJFACE HATER DISCHMGE APPLICMTS (PRIMARY Ato SECOOMY INDUSTRIES) we: h NOT APPLICABLE / BELIEVED ABSENT i l & MNUFACTWES 2, 4, 5 - TRiOt.DRcP>coxY ACET! Act (2,4,5-T); 4, TRIO 4LomPt(NOyY PROP 4 IC ID ($1LVEX,, 4, ,TP) 4, texY ETHYL DIO1LCHOPROPIONATE ER9CP ; 0, Dt'TTHYL , 4, 'rTRICHLOR0PHENYL) PtOSPtOGOTH!CATE (R0ff4L); , 4, MTRIOt.OROPt(f0L (TCP); OR ME)(AC>t0POPHEtt (KP); (ALL DATA FOR TT AEO'E PtJST BE GENERATED UStrG STNCARD ANALYTICAL CALIBRATION PROCED$ES) OR ICO'S cwt NAS REASCW TO bel.fEVE THAT TCDD IS OR 79Y BE PRESENT IN THEIR DISCHARGE. PRESENT/CATA 15 ATTAGED tu'il PEPORT QUALITATIVE DATA, GENERATED WHIOJ,ULED A SCREEN!Pai PROCEDWE PCT 8, - TETRAOtCRCDIBENZPP-DIOx!N CAubRATED dlTH AMLYTICAL ST40ARDS, FOR 2, 2 /t (TCDO). RECORD ALL CATA ON FOPPtS PROV!DED (ITEM /) IN THIS 200KLET. l 81M41C% TCx! CITY TESTS WERE MADE IN THE LAST TWEE b(ASON TO EELIEVE THAT IF TbE $@ FACE HATER DISOAPGE APPLICMT krO#S Of HAS P f^ POT APPLICABLE J. ) YEARS ON MY OF THE j APPLICMT 5 DISCHMGES OR ON A RECElvirG WATER IN RELATION TO A DISCHMGE, PROVIDE THIS If(GRhATION AS M ATTAOfENT TO THIS APPLICATION. APPL.! CABLE /SEEATTACHED K. IF A CONTRACT LADJtATORY Of CONSULTI?G FIRM PERFCMED ## OF TFE #4.AYSES FEQUI'ED tcT APPLICABLE SY THIS AFPLICATICN, PROVIDE THE N#4 AND ADDPESS OF EA01 LABORATmY OR Fim #O THE MALY$is PERFORrTD AS M ATTAOftNT OF THIS APPLICATION. t L. DO YOU DISCHMG( ## OTKR 70x!C OR lt@l

1! CAL StBSTANCES NOT LISTED IN TAPdS IV PME D NO !!A TWOWH VA PARES 4 U. It VES, TVN IDENT!rY TE W M WBd O(MICAL SUBSTMCES NO ESTIMTF TM FIML EFFLUENT CorCENTRATIONS. 54RilT THIS IVCefiAfl0N AS M ATTAOfthi TO THIS AP8LICATl0N.

APPLICAJLE/SEE ATTACHO 9 I., 7 e I SECTION 11 gR 4 MI 000 58d.7 f 8R SEE INSTRUCTIONS iirr ON REVERSE SIDE r E-MM ,o,o,A, L ITEM i A. USE THl3 DATA SEET 70 RECORD INFUt%f!ON AS REQJIRQ IN: (DECK APPROPRIATE !OX FOR -lCH INF@MTION THIS DATA SHEET REPRESFft75.) E 7 e

1. SECTION II, ITEM 4-E. GR000MTER DISOWCE INFamAf TON (PAGE M CRITICAL

2. SECTim is, Ire,6. PRrORITY pouuTurr$ N $@ FACE HnTER Disow4 (PAGE 57)

E MATERIALS z-_. To"xic 3. B. BEtow: CRITICAL MATERIAL 5 (TABLE IV) IN SWFACE HATER DISONGE (PAGE 73) E-POLLUTANTS L HAZARDOUS == SUBSTANCES 3. tr$T usY CRITrCAL PATERIA4. (TABLE IV PAGE 6) NOT AD@ESSG IN SECTION !! ITEM 6 m!ORITY ICT m! CABLE PQLUT4dTS WICH VOU ic0w CA HAVE REASON in EELIEVE TO PE PPESENT IN TK DISCHMGE. SEE == IN REvtRSE $10E OF THIS PAGE FOR FURMR DIGECTIGiS. h ' APPLICABLE (SEE BELDs) DISCHARGE A. NMT OF CRITICAL MATDIAL m PR!ORITY FCLLt/ TANT [ , g g g 9 g,, B. AvtuGE COCENTRATION; S#fLE TM; I 0F AMLYSES

ft1 E #w vsEs y g,

9_g g g g 2

c. max!v COCENTUTim NO PASS

II N WI CCE "g

.J A. PJME OF CRITICAL MATER 1AL OR PRIORITY FUL1UT#dt _I 5 i f 1 I I i 1 1 SNfLE E I 0F hm a B. AVERAGE COCEN'RAtl0N; SAMPLE TYPEJ # OF ANALYSES l l l l,g g l g = C. ~~ memoT!. S$ , arco, w woT C. L_ ,,,...,,, u UNITS CODE g PW1E OF O!T! CAL PATUIAL OR PRI@!TY FCt.LifTANT A. l g l g g g g g l Q','

l' y '"g"' ", " " ", "

f

s. AvEuCE QCE= Tim; SmE TM, r Or mVSES i,,,,,,,,

=

gSg

, g,,,,.,,,, a-g C. -- me= Tim. S$ .J A. NAME OF CRITICAL MATERIAL OR PRIORITY POLLUTANT 4 l l l 9 [ ] [ l r S. AVEMGE CCrCDdTRATION; $#fLE TYPEJ # CF #@ LYSES g g g l,g g g j i , l =,,,,.,,,, g* C. -- Catenofim me.SS 2Un7 Couph ia j "u"' "i"IT B. ave 9x4 Cate<TRAT 0N: SuftE TveEJ 8 0r ANaLvSES i i i,i e = C. - - me mfim - -S , y,,,,.,,,, u-A. NArE OF CRITICAL MATERIAL OR Prim!TY PCLLUTANT E-g g g g g l [ g g

[' Cj" 5"u"' """*i'

B. AvEmE Caamtr0N; SmE TM; # Or mVSES i,,,,,,, i i <2 m C. "%XI'1MUCC4TPATl0N MO MASS ! 0% 9,, g s NAnE Or CRIT:Cel-Em m miOPm,cu.urun uE h~ B. A4MGE QCENTMTim; S#fLE TM: # OF kWLYSES i l l l,l [ [ [

" "' 'i

1. L C.

-tv COdNTUTION #O 455 ,,g g , y = A. att OF CRITICAL r%TERIAL OR F910RlfY 70LLf1T4dT l l l l l l [ { iE aor Cm s.me rwe n a w su 83 2. AVE 8AM CCPCD:TRATI';NJ S4ft E TYPEJ # & AMLYSES i I f l.I ! l l U U t t, 2 vo r aa un r cca C. Wlv CC' CENT 8ATION #0 MSS = L_ y,,, ,,g [_,j Acc!T! MAL PAGES CF THIS ITEM 7 AAE ATTAOC FOR TM REST 7 TM CRITICAL h YES PmTm!aLS #c/m PR!m Tv mu.U' ANTS REWED TO BE REPORTED. O NO = = l ? 11 g I ll SECTION ll gER N 00 SEE INSTRUCTIONS ON REVERSE SIDE l a:RL itMD idio,Bi ITEM A. - -Di - ,N,% ( iS iWit, m iciGi, rm ioiciSi, ma i i i9 iWi 1 mgRmEi-nAuE. - - -- - ,t, e,e, ,m a,c,a,r 4,4,u, C. YOU DISOt4E4 SEASOPeALif f 1F NO, CONTIM TO E) YES W DISCHARCE LOCATION D. IF YES, UST D150,44 PUt!ODS M PC. / MY PC. / My SCH DULE i e L_,,.L,,,j THRotos e e e r i i e FLOW I I I I ' I TmotDi I ' l I I RATE I i i 1 I I Wrai t i I I f I WASTEWATER gm/m. m.joAy in,/wg, TYPE CODE E. t# O MPUCATION RA n NA i i i. u i i i. u i i i. o Om hASTEHATER TYPE COCE i F. TYPE OF NASTDdTER DISCHMGE h U y 't J U L_.J l i 2 NONCONTACT G. DISowaGE SOtDutz (vtMLY AVERAGE) ,otp3/yy lhlNg my/ YEAR I 3I bl I COOuNo aw i e iItoi3i.i9i3.

M*

OtSOtMGE FLOW RATI gge. E#MD Fw hie 3 PROCESS H. 4 SANITARY 5 STORMWATER "I'T MINI " O *13IItbI tb CAlLY NAx1PtN 1 t t 1 t UNIT CODE Acomin i I I IO1

l$

1 MGY I, n( max!?tN DISCHARGE Flow RATE TO BE AllfHORIZED IN PEm17. I I l O*I b J. NAXI?tM DESIGd DISCHNtGE FLDt RATE

t t

1 CESIGN I I I i l i A. DO YOU USE WATIJt TREATMD(T GITIVES TO TREAT YOtR DISCHAK47 (IF NO, CONTINtE TO ITEN 3) YES 2 .. f@ME FthCTION, NO OCMICAL CDf0$lTION OF T'ESE G ITIVES. H 2 WATER TREATM ENT Ng A72iTIVES C. NME NO ADORESS OF PWAFACTtRERS OF M SE G !TIVES. UNITS CODE 1 Mgil 2 Ug/l gg MINIMtM UNITS AVERAGE thlTS max 1PtM LP*l TS D. EJGTCTED DISOiMGE COCENTRATION - A DITlVES. Nk COE

Com
CO2 l

GlT!vE PWT e, i e i t,,_; ; e e i e i L,,,,J ; e e t I i L._J ADDIT!W PWE i t iI i IJ J U ' ' 8 UJ 8 U GIII4 M i e i i y Jt i e i I L JJ 8 1 1 ' ' l-1 E. 00 YQJ TREAT DE DISCHARGE TO RD0W GlTIVES? NQ yES 70 F. W14T l$ THE RDOVAL EFFICIDeCY NO DISCHMGE FREQlINCY7 NQ MN#*EU %RE.UVAL WS*/ DAY Id d "'* AT.lflVE fWE i 1 1 I I I lI AIDITl4 P@tt I t i W l.-.3 ADDIT!W 'WT I i 8 I I I b-- I G. AS AN ATTAOtTNT TO Tht$ APPLICATI@ POvlX SPECIFIC vf'ALI AN @ '3 ATic T0x!COLnrilCAL CATA CR REFESDeCE wwlo1 APE AVAILA.%l AND IP.F05NATI3t Os DE RATE OF DECAATAfl0N OF DE FODLETS FOR EACH GlTIVE. 31 i i SECTION ll QRM M 000 %M BR SEE INSTRUCTIONS ON hEVERSE SIDE r1JTFAU. 4titR tOtOIO lTEM A. m Cr Pa0 Cess C mRrauTim to mE DiSo=E ,J., ,5,rini iCiEid., & L iD Wi i44i/i1i DeautH Tkts OUTFALL WO $lC CCTE 3. P50 CESS SOCOLE (YEMILY AVEMGd fIf mtpVmy t i i revs / yrs I a C. PioCEss Wu,E re urE ,,, ' M ' ' 4'4 ' *0if i ' ' m =. o u i '"!EA$S h 8A515: 1984 FLowl DATA ST , oi LisJ CONTRIBUTING a. TO DAILY Mu!PtN I I f I t t'I I I I D. PROCEs3 PROOuCTICN RATE M b g,,,,, I t i A. fwE CF P50 CESS C0tmt!BUT!PG TO DE DISOWIGE kg A D#cuCH This OUTFE WO $!C CCTY INii I I I I I I t g g 9 9 g g 9 g g g g g g 3. PROCESS $O0111 (YEARLY A'4MGE) KXRdDAY I I f DAYS / YEAR I I I I C. PROCESS WLott rLDW RATE ul.11 GEA g y y , g g g I t t t t i y un DAILY MIN! PEN I I I f f f f f f i LJ i l 1 POUNOS DA!LY MAxistM i t i f f I f f ' 8 Ld 2 GALLONS mlTS /TIPE D. PROCESS PROWCTION uTE I I I f f ' ' I I L 1/ LJ 3 Cusic A. tere OF Pa0 Cess CONTRisuTitC To DE DISOSRGE VARDS neue THis outru uO src crDE NA i,, i i i i i e i i i, i i,,,,, 4 7o"S l .. PROCESS soeutz (YTua A=Gd 5 ,GY ,x,gcA, , i i MYv o i, i i h 6 MGD mir m C. PROCESS wutt FLOW RATE 7 GPO TOTAL YMY l 1 I I I I I I I ' Id g i i i i i i e i i i t_r MILY MAxtPtN I f f I I I I ' ' I Ld ] D. PROCESS PRODUCTION RATE UN 7,u g 1 NOUR A. N#t OF P90CE53 CENTRIBUTifG TO DE DISO%RGE I neotre Tuts onrat.L MO SIC CrrE I I I I I P f I f f I I f f I I f I f i

3. PROCESS SOct11 (YEARLY AVEMGE) 3 WEEK muRs/ DAY l I I MYMYEM l l I I C.

PROCESS Wuft FLOW RATE 5 EAR TOTAL YEARLY I I I I I I I f I I e { [ DAILY MINIMLN I f f I f i 1 i f f L,J DAILY MMWN I ' I I I ' ' ' ' ' LJ WITS /TIPT D. P90 CESS PAODUCTION RATE t t i 1 t t t I t L 1/ L.J A. t*E OF P90 Cess CONTRIBuT!fG TO DE DISOSRGE g BfufN THIS OUTFu 40 $1C CCEE I f I f I ,,,,,,,,,,,, t, i S. PIOCESS SOG111 (YEMLY AVERAGd f ,OPVDAy t 1 j DAYS / YEAR 1 I f I l C. PROCESS wu,E re uTE mlT C 2 ,,L oLY ,, i i i i,, i i u l u. l-g M,g niui u e t i t t t i I f I L.J DAILY P%x!PtN I I I I ' ' I I f l-- I D. Pf0 CESS PRotAITICN RATE UNIT 3 / TlPE i e 1 1 1 1 1 L_.V LJ l SECTION 11 PERMIT C 000 % M NUMBER r SEEINSTRUCTIONS ON REVERSE SIDE < (LTFitt rUTER i o,0, S A. 15 DE DISCW4G FNM THIS OUTFALL DIREC TO THE CRouro OR GROUPOeATER$! IF 'O CONTINtE TO ITEM YES PC 8. NAS A MfCROCFOLOGICAL STtOY OR ITS EQUlVALENT BEEN PERFOAPED OR 15 THERE SWFICIENT CURRENT HYDIOGEOLpCPOUrONATER RtAI! CAL INFGNAT!Q4 AVAILABLE A$ REQUIRED (Y TLOATER RESOURCES '.13 NO CONIS$lCN FMT 4 0F AUGUST 141% R.Ja.Ely (PEE 4j) FOR GROUNOWATER THIS EXISTING CR PRCPOSED DISCHARGE IF YES ATTAOt A COPY OF THE REPORT. Ol$CHARCE C. ARE YOUfgSTl'C 41 EXC1PTIOd FR09 StfNITTING A HYDROGE0 LOGICAL REPORT UPOER INFORMATICN Rts.E R.)D.M/ (iQ (PAGE 16) CR FROt GR0(PObeATER 70NITORIrG PEQUjREMENTS YES to UPER wutt R.)2.5.2.d (5) (PEE 4D OF TFE PART R RtLES. IF "YES ATTACH DOC &OTS.rr;D EXP'./iATICN TO 000NSTRATE THAT YOUR DISOdRGE nCULD QUALIFY FOt NA A u oc m. A8E YOU REGtKSil*G A VARIArdCE FROM PgE 32.3.M (PEE (/ IF YES, ATTACH SUOt2) (NCPOEGRACATION) 0F D. THE ATER RESCURCES CatPIS$!ON PART U GR0l#OeATER RULES YES

T DCCFErits AS t.ECES$4tY TO A THE NE D FOR A VARI IN TE4*S OF M l

CAITERIA SPECIFIED 1:4 RtAI 10 PAGE OF THE PART RULES. E. LIST A:.L CMMICAL S4STA?dCES '.44(CH ARE TN *yCHlGAN'S CRIT [ CAL MA RIALS REGISTER TABLE IV (PAGE 6) N.3/OR U.S. EPA'S PRIORITY PQ.LUTANT LIST TABLE V (PAGE ) OR ANY OTHER SLESTANCES NOT APPLICABLE / bel.!EVED ABSENT W+1CH ARE CR MAY EECOPE INJURIOUS M T>E DES!GaATO USES OF TFE TDI CR TO THE PUBLIC >(ALTH T54T ARE DISch4RGED CR EXPECTED TO BE DISCHWAD TO T>E GROGOWATER BY THIS FACIL17Y. ESTIMATE THE FINAL EFFLUENT CC'JCENTRATIOr4 AiO RECORD ALL DATA IN ITEM 7 0F SECTION 11 IN THl3 BOCILET. THE APPLICANT MAY BE RE%'! RED TO DO A3)lTIOrdL MASTE AidLYSES. PRESENT, DATA PROVIDED IN ITEM 7 g A. DISCHARGE C%tACTE885 TICS CONCENTRATION LNITS CODE # ArdLYSES SAMPLE TYPE ITEM 5 'mo (oet! CAL 0xvcC4 CEMAND) I I I I*I I I I I I I I.I I I I l.IJ k,1_d l_.) b I ' ' U TOC AL AC m) WA$7E A ER CHARAC- .ml4 NtTw0ca (AS N) I ' I I1 I I I I ' I I.I I I I d 8 ' 8 L_J TERISTICS

TOTAL SUSPUCED SOLIDS I I f f

.t ' ' ' ' ' ' f.I I I I LJ W W UNITS CODE STAL PtOSPHORUS (AS P) l e f I .I i t f f I t i ei f f f L,jj (,,,_1,,,,,,J L,,j 1 Mg/l L Il I ' I tJ ' ' ' I.' ' ' ' ' ' ' ' ' ' ' I 2 Ug/l TCTAL PESIDUAL ot.ORINE e 3 COUNTS / U 100 ml D'530LVED O N MIN c S.U. .pg l l 1,U I L_J LJU ' ' ' W 5 'F 6 LBS/ DAY ' I I I I I I I I ' I I I W FECAL COLIFORN BACTUtlA rEmpATwE (SumR) ' ' '. L_! t f

f. L!

LEJ l i f U 'TEmRAnn (wtNTER) LLJ.LI I ' '. LJ LEJ tJ B. OTHDI WASTEWATER OdPACTERtSTICS e0,IgLst,fpR t E,A i SgE, g ,,,,i,, e i, ' '.' ' ' ' L_J l i I L_J SAMPQ t t i i f f i r i e t I t I t t.I i e i t i t i.t I t i y i I t L,,,J TYPE ' ' ' ' ' ' ' ' ' I ' ' ' ' ' ' I I I I ' '*I 1 GRAB 2 24 HOUR g cruPoSiTc t t t t t i i i i e i a e i .e t i e i t i i. La I L_ J l I i LJ e t i i e i e t i e i e t i,,,i i e i e i i i,i e i t L_j i t i L_,j i i i i t i, e i i e i e i e i. i i t i t t .I t i I L.,j t t t t., J i See attached sheets for data. Note: Results for triarylphosphate esters and hydrazine in Attachment I. i 7 l REAIIT 70. Labor % Services DMeion Park West Two NUS 5380 Campbelle Run Road Cilff Mine Road Pittsburgh, PA 15206 Pittsbuigh. PA 15275 my 412-7e61000 ) LAB ANALYSIS REPORT CLIENT IWE: IllBIANA & MICNIGAll ELECTRIC CO. NUS CLIENT NO: 010904 ABORESS: P. O. 30X H llVS SA M LE NO: 15021699 FORT IIAYlE, IN 46001 YDIDOR110: IEPORT DATE: 03/26/95 WORK ORE R NO: 55830 ATTEllTION: 10t. J0lti 14lOET DATE RECEIVED: 02/27/85 SAMLE IDDITIFICATION: UNIT 2 S6 BLOWD0lal 02/26 TEST KTERMIllATION RESLLTS UNITS 1361 WMS PAlti Y-B N010 Aluminus ( A1) < 0.1 ag/l 10 # krius (h) < 0.1 og/l M150 Cobelt (Co) < 0.01 og/l 1190 Iron, total (Fe) 0.02 og/l M230 Magnesive (Mg) < 0.001 ag/l 12 # Nangenese (Mn) < 0.01 ag/l M2H Molybdenue (Mo) <0.03 ag/l 13 # Tin (Sn) <1 ag/l M350 Titanius(Ti) < 0.5 ag/l 1055 Boron (3) 0.7 ag/l W060 troeide (Br) <2 og/l 1225 Color,True 20 Pt-Co W310 Fluoride, total (F) < 0.1 og/l 1390 Nitrate (M) < 0.1 og/l W410 Nitrite (N) < 0.01 ag/l 1435 Nitrogen, Kjeldahl (N) 1.1 ag/l W440 Nitrogen, Organic (N) 1.1 ag/l 15M Phosphorus, total (P) < 0.01 og/l W730 Sulfote, turbiditetric (SO4) <1 ag/l 17M Sulfide (S) < 0.1 og/l W7M Sulfite (S03) <2 og/l 1770 Surfectants (MBAS) < 0.1 ag/l M362 W M S PART V-C T0XIC METALS M020 Antimong (5b) < 0.1 ag/l 11030 Atsenic ( As) < 0.001 og/l 1050 Beryllisa (le) < 0.002 ag/l M090 Cadeive (Cd) < 0.005 mg/l 11M Chreatus (Crf ( 0.01 ag/l M1H Cr4per (Cu) < 0.01 og/l 1200 Leod (Pb) < 0.03 og/l M250 Mercury (Hg) < 0.0002 ag/l PA E NO: 1 h A Halliburton Company CLIENT ORIGINAL R EestT T O: Laboratory Services DMe6on Park West Two 5350 Comptoils Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgn, PA 15275 412-708-1000 mg LAB ANALYSIS REPORT CLIENT IIAIE: ISIAllA t MICNIGM ELECTRIC CD. NUS CLIENT 110 010904 ADDitESS: P. D. 30X 60 NUS SAMPLE NO: 15021699 FORT li4YE, IM 46001 VEMBOR 110 REPORT DATE: 03/26/95 Il0RK ORDER 110: 55830 ATTENTION: Ist. Jolti IRigEY DATE RECEIVED: 02/27/85 SAlfLE IDDITIFICATION: l pili 2 S6 BLOWD0lRI 02/26 TEST DETERMINATIOlt RESULTS UllITS lt270 Nickel (Ni) < 0.03 ogIl M290 Selenius (Se) <0.004 ag/l 1300 Silver ( Ag) < 0.01 ag/l M330 Thallius (T1) < 0.1 ag/l 1390 Zine (Zn) < 0.01 og/l U270 Cyanide, total (CN) < 0.005 mg/l 1500 Phenolics, ( 0.02 ag/l M220 Lithive(Li) < 0.01 og/l 1110 VOLATILES-PP IN WATER OV01 Acrolein ( 100 ug/l 1902 Acrylonitrile <100 ug/l DV03 Benzene <5 ug/l 1905 Brosofore <5 ug/l OV06 CarbonTetrochloride <5 ug/l 1V07 Chlorobenzene <5 ug/1 DV06 Chlorodibtonenethane <5 ug/1 IV09 Chloroethane < 10 ug/l DV10 2-Chloroethylvinyl Ether < 10 ug/l IV11 Chlorofore <5 ug/l OV12 Dichlorobronceethane <5 ug/l IV14 1,1-Dichloroethane <5 ug/l DV15 1,2-Dichloroethone <5 ug/l IV16 1,1-Dichloroethylene <5 ug/l DV17 1,2-Dichloropropone <5 ug/l IV18 1,3-Dichloropropylene <5 ug/l OV19 Ethylbenzene <5 ug/l IV20 Methyl Broeide < 10 ug/l OV21 Methyl Chloride < 10 ug/l IV22 Methylene chloride <5 mg/l DV23 1,1,2,2-Tettochloroethane <5 ug/1 IV24 TetrochloroethylenetPerchloro) <5 og/1 DV25 Toluene <5 ug/l PA(E NO: 2 h A Halliburton Company CLIENT ORIGINAL RE00fT 70: Latwatory Services DMolon Park West Two 5360 Campbells Run Road Cliff Mine Road Pittsburgh, PA 152o6 Pittsburgh, PA 15275 g 412-788-1000 LAB ANALYSIS R E P C) R T CLIENT NAE : INDIANA t MICHIGAN ELECTRIC CD. NUS CLIENT 110 010904 ADDRESS: P. O. 301 60 NUS SAMPLE NO: 15021699 FORT WAYlE, IN 46001 YOIDOR NO: REPORT DATE: 03/24/85 WORK ORDER NO: 55830 ATTENTION: IGt. JOHN HUGEY DATE RECEIVES: 02/27/85 SAltLE IDOITIFICATION: WIT 2 96 BLOWDOWN 02/26 TEST KTERMINATION RESULTS LIIITS OV26 1,2-Trans-Bichloroethylene <5 ug/l OY27 1,1,1-Trichloroethene <5 ug/l 1928 1,1,2-Trichloroethene (5 ug/l OV29 Trichloroethylene <5 ug/l IV31 Yinyl chloride <5 ug/l 0120 ACIDS - PP IN WATER 0401 2-Chlorophenol ( 10 mg/l 0A02 2,4-Bichlorophenol < 10 ug/l lA03 2,4-Dimethylpherel ( 10 ug/l 0A04 4,6-Dinitro-o-cresol ( 50 ug/l lA05 2,4-Dinitrophenol ( 50 mg/l 0406 2-Nitrophenol < 10 ug/l lA07 4-Nitrophenol ( 50 ug/l 0408 p-Chloro-n-cresol < 10 ug/l IA09 Pentechloropherel ( 50 ug/1 0A10 Phenol ( 10 ug/l IA11 2,4,6-Trichlorophenol < 10 ug/l DE30 Acid Extre.ction-Weter 0130 BASE NEUTRAL!,- PP IN WATER 0901 Acenophthine < 10 ug/l 1902 Acenophth lene < 10 ug/l g 0303 Anthrocen, ( 10 ug/l l 1904 Benzidine < 50 ug/l 0805 Benzo (o) Anthracene < 10 ug/l l906 BenzotoPyrene ( 10 ug/l 1 0907 3,4-lenzofluoranthene < 10 ug/l 9308 lenzo(ghi) Perylene < 10 ug/1 0909 Benzo (k)Fluorenthene < 10 mg/l 1910 91s(2-Chloroethoxy) Methane < 10 ug/l 0911 lis(2-Chloroethyl) Ether ( 10 ug/l 1912 lis(2-Chlotoisopropyl) Ether ( 10 ug/l 0813 Bis (2-Ethylhexyl)Phtholote ( 10 mg/l NE M: 3 $ A Ha!!! burton Company CLIENT ORIGINAL 0. r, REastT TO: t.aboratory Services DMsion Pstt West Two N 5360 Campbeits Run Road Cliff Mine Road Pittsburgh,PA 15206 Pittsburgh, PA 15275 412-7as toe 0 mg LAB ANALYSIS REPORT CLIENT llAIE: INBIANA & NICHIGAN ELECTRIC CO. NUS CLIENT NO: 010904 ABBRESS: P. O. BOX 60 NUS SAlFLE NO: 15021699 FORT WAYlE, Ill 46001 VENDOR 110: REPORT DATE: 03/26/85 WORK ORDER 110: 55830 ATTENTIOII: Itt. JOltl HUBIEY DATE RECEIVED: 02/27/95 SAltLE IDENTIFICATION: UNIT 2 SG BLOWDOWil 02/26 TEST BETERMINATIOlt RESULTS UllITS (3 14 4-Brosophenyl Phenyl Ether < 10 ug/l

0B15 htyl Benzyl Phtholote

< 10 ug/l 1816 2-Chloronophthelene < 10 og/l 0B17 4-Chlorophenyl Phenyl Ether < 10 ug/l 8818 Chrysene < 10 og/l 0B19 Dibenzo(a,h)Antheccene < 10 ug/1 1320 1,2-Dichlorobenzene ( 10 ug/l 0B21 1,3-Bichlorobenzene ( 10 ug/l 1822 1,4-lichtorobenzene < 10 ug/1 0923 3,3'-Dichlorobenzidine ( 10 vg/l 1824 Diethyl Phthelete < 10 ug/l 0825 Dimethyl Phtholete < 10 ug/l 1826 Di-N-htyl Phthalate < 10 ug/l OB27 2,4-Dinittotoluene < 10 ug/1 1928 2,6-Dinittotoluene < 10 ug/l 0329 Di-N-Octyl Phthalate < 10 ug/l ll30 1,2-Diphengthydrozine( Azobz) ( 20 ug/l 0931 Fluorsnthere < 10 ug/l 1832 Fluorene < 10 ug/l DB33 Hexechlorbenzene ( 10 ug/l IB34 Hexachlorobutodiene ( 10 ug/l 0835 Hexachloto-cyclopentodiene ( 10 ug/l ll36 Hexochloroethane ( 10 ug/l 0337 Indeno(1,2,3 cd) Pyrene < 10 ug/l 1938 Isophotone ( 10 ug/l 0B39 llophthelene < 10 ug/l 1940 Mitrobenzene < 10 ug/l 0541 N-Nitrosodieethylonine ( 10 og/l 1942 N-Nittosodi-N-Propylonine < 10 ug/1 0843 N-Nitrosodiphenyleine < 10 ug/l 1544 Phetenthrone < 10 ug/l 0845 Pyrene < 10 ug/l h A Halliburton Company CLIENT ORIGINAL REtelT TO: N 880'Y h M b Park West Two NUS 5300 Wie Run Road Cliff Mine Road Pettelmrgh, PA 15206 Pittsburgh. PA 15275 mg 412-786 1000 LAB ANALYSIS REPORT CLIENT llAE I SIANA 6 MICHIGAN ELECTRIC CO. NUSCLIENT110: 010904 AIORESS: P. O. 90X 40 NUS S N LE NO: 15021699 FORT N TIE, IN 46001 YEWOR NO: ) EPORT BATE: 03/26/95 WORK ORDER NO: 55830 ATTENTION: IGt. J0M HugEY DATE RECEIVED: 02/27/95 S M LE IKMTIFICATION: UNIT 2 SG ILOWD01Al 02/26 TEST ETERMIllATI0lt ESLA.TS UNITS (B46 1,2,4-Trichlorobenzene < 10 vg/1 E25 lose Neutrel Extraction-Water 0141 PRIORITY POLLUTANT Kl'S GE11 KB Extraction - Water IP19 PCI-1016 ( 0.5 mg/l DP20 KI-1221 ( 0.5 mg/l DP21 KB-1232 < 0.5 ug/1 OP22 PCI-1242 ( 0.5 ug/l IP23 Kl-1248 ' < 0.5 ug/l DP24 KI-1254 < 1.0 ug/l IP25 PCI-1260 < 1.0 ug/l R450 RADIUM 226 AND 228 RB04 Rodive-226 ( 0.4 pCi/1 R905 Rodium-228 <2 pC1/1 R800 Gross Alphe 2.5 f/-0.9 pCi/1 R901 GrossSete 3.7 f/-1.6 pCi/1 8032 Antonia es N (distillotion) < 0.1 ag/l WO50 900, 5-day (02) <1 ag/l 1100 Carbon, organic (C) < 1.0 mg/l W120 C09 (02) <5 mg/l 1110 Solids, suspended et 103 C <1 ag/l D ComDITS: lieviewed and Approved hs Pn PAGE NO: 5 h A Halliburton Company CLIENT ORIGINAL REtefT TO: W Servkas N Park West Two NUS 5380 Campbells Run Road Cilff Mine Road Pittsburgh.PA 15206 Pittsburgh, PA 15275 gg 412-708-1000 ] LAB ANALYSIS REPORT l CLIENT II M : 11191A114 6 NICH16All ELECTRIC CO. NUS CLIDif NO: 010904 ADDRGS: P. O. DOI 60 11U5 SMLE 110 15021700 l FORT WAYlE, IN 46001 YDSOR 110: KPORT MTE: 03/26/95 WORK ORER 110: 55830 AITINTION: MR. J0ml14161 0 94TE RECEIYD 02/27/85 SAltLE IDDITIFICATION: L311T 2 96 BLOWDOWN - GRAB ll 02/25 1040 1EST KTERNIllATION RESLA.TS UllITS 1432 Fecol Califors - In <3 col /100e1 W150 Chlorine, firsidual DPD (C12) < 0.1 ag/l 1490 pH 8.0 W680 Oil, extraction gravinetric 2.1 ag/l e ColtENTS: $ A Halliburton Company CLIEtlT ORIGINAL AttetT TO: Laboratory Services Division Park West Two 5360 Campbells Run Road Cliff Mine Road 1 Pittsburgh PA 15206 Pittsburgh, PA 1SDS g 4t2-7081000 ] LAB ANALYSIS R E P C1 R T CLIDif IIAllEs IllBIANA & NIQlIGAN ELECTRIC CO. IRIS CLIENT NO: 010904 ABBRESS: P. O. 30X 40 NUS SAlFLE 110: 15021701 FORT WAYE, IN 44001 VD80R 110: EPORT NTE: 03/26/95 WORK ORER 110: 55830 ATTENTION: 14t. Jolti HupKT N TE KCEIVE3: 02/27/85 SaltLE IDDITIFICATI0lls tpili 2 S6 DLOWD0Wil - GRAS 42 02/25 1340 1EST KTutNIllATI0lt RESULTS UNITS 1432 Fecel Colifors - IPN <3 col /100e1 W150 Chlorine, residuel IPD (Cl2) < 0.1 ag/l 1490 til 7.5 W600 Oil, exttsction grevinetric 2.4 ag/l o GlflENTS: h A Halliburton Company CLIENT ORIGINAL 1 REtstT TO: Laboratory Services N Park West Two S360 Campbells Run Road Cliff Mine Road Pittsburgh, PA 16206 Pittsburgh, PA 15275 412-700-1000 LAB ANALYSIS REPORT CLIDIT IWE INDI411A & NICMIGAN ELECTRIC CO. NUS CLIDIT 110: 010904 ADORESS: P. O. 90K 40 NUS SAlfLE 110: 15021702 FORT INmE, IN 46801 YD80R NO: REPORT DATE: 03/26/85 WORK ORER 110: 55830 ATTENTION: 18t. J0101 HUllHET DATE RECEIVED: 02/27/85 SAlFLE IKMTIFICATI0li IRIIT 2 SG DLOWDOWN - ORAB 93 02/25 1938 TEST KTERNIllATI0ld RESULTS UllITS lA32 Fetal Colifore - IPN <3 col /100e1 W150 Chlorine, residuel DPD (C12) < 0.1 ag/l 1490 pH 8.4 W680 011, extraction gravinetric 1.7 88 l/ 01)flENTS: Reviewed and Approved by: JIC h A Halliburton Company CLIENT ORIGINAL REASfT 70: % Servkles N Pete West Two NUS 5360 Campbene Run Road Cliff Mme Road PHtelmrgh,PA 15206 Pittsburgh, PA 15275 412-788-1000 gg LAB ANALYSIS REPORT CLIDif IIAlf ISIAll4 & MICHIGAll ELECTRIC CD. IluS CLIENT NO: 010904 ABIRESS: P. O. 30160 1106 SAIFLE 110: 15021703 FORT WATE, Ill 46001 YDOOR 110: IIEPORT DATE: 03/26/95 UORK ORDDt 110: 55830 ATTDITIDII: ltt. Jolti HUGIEY DATEItECEIYD: 02/27/95 SAMPLE IDDITIFICATIDII: LBilf 2 S6 R0WDOWII - liRAB 04 02/26 0135 TEST MTERMIllATIOli ItEStA.TS UllITS IA32 Fecal Califore - 1991 <3 col /100e1 W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 9.0 W600 011, extraction grevinetric 1.1 ag/l O e O COMENTS: 4 Reviewed and Approved by: JIC $ A Halliburton Company CLIENT ORIGINAL g-f SECTION 11 PERMIT MI 000 597 SEE INSTRUCTIONS NUMBER ON REVERSE SIDE ITFf4.L WR , 0, O i & ITEM ~IEm. f.Em U';E DISCwAr4RS g PpONKc. i.APECTED VALt15 FW TM QtAlsTITAT!vE Am2 -snD -T- -SSED s@F-E -nR dis-s. M G@LITATivE tr#CR%TIL.Ys REcutSTED RELCH. A. IS THl3 FACILITY A PRIMMY if0USTRY? (REFER TO TABLE lA PEE 4j,) 9( YE5 to ( tr "O, ro To E) i ta vg$, r4 Tr) p) PRIORITY B. IPCICATE TYPE CF PRIMARY lt00STRY AS LISTED IN TABLE IA PAfE 833 POLLUTANTS '"* 7",p w, m e, ) I f M 8d1 IkM M ANO C. [EES THIS CUTFh OlSchAKE Cor4TAIN ## PROCESS WASTCdTER! ( t r to, co TO E ) (rF vES, (;0 TO 0) YES 70 INCRMATION D. IZ!CATE WCM f6% FRACTIONS MT BE TESTED M. (FEFER TO TABLE lA PEE 481) h WLATILE PCTE! FCA EACH 6"/MS FRACTION OECKED,EACH SPECIFIC ORGANIC T0XfC POLLUTANT WITHIN i SURFACE E,ue F#KT!om M at AaLYZED FOR (SEE TA9LE !!A Par.E 92 IN ADOITICN, ALL PRtPWFY h SASE/ NEUTRAL WATER IfCUSTRY APPLla*.Ti WITH A PPOCES$ hASTCnATER DISChMGE d PROVIDE QtANTITAfivE ^ I"'

DISCHARGE

@ ActD ONLY RECCRD h CATA CN FORMS PROVIDED (ITEM 7) IN THl3 BOOKLET. (CONTINL( Wine E-K BELOW) PESTICIDE E. IF /,2. 5@ FACE HATER D15ChMGE APPLICANT (PRIMARY OR $ECOPCARY IN[1JSTRY), REGARDLESS OF I,( DPE CF DIS.hMGE, 4085 OR HAS REASON TO BELIEVE TNT #n POLLUTANT LISTED h0T APPLICABLE / BELIEVED ABSE,ff IN TABLE ilA AND !VA PAGES U IS DISCHARGED FROt ANY CUTFALL,DE QUANTITATIVE 351 BE PROV! ED. RECAD ALL DATA Ort FORMS F#0VIDED (ITEN 7) IN This 800df. PRESENT/CATA l$ ATTACHED F. IF ## $@ FACE >ATER DISCHARGE APPLICANT (PRIMARY OR SECONDARY INDUSTRY), REGARDLESS OF TYPE OF DISCp4, n.*CWS OR HAS REAS3d TO BELIEVE ANY POLLUTANTS LISTED IN NOT APPLICABLE /8ELIEVED ABSENT TABLE VA PF4 9 AJE DITHARrc FRrN ANY OUTFALL DE APPLICANT 831I DESCplEE REA50r65 FOR D( POLLUTANT BElfG PRESENT 40 PROVICE ## AVAILABLE QUANTITAT!vt DATA. RECCRD ALL DATA CN F0m5 Fil0VIDED (ITEM 7) IN THI5 50067. PRESENT/ DATA IS ATTAGED l

c. ALL s> FACE HAftR DISCHAPGE APPLICusis (PRIMARY no SECorreRY IrouSTRIEs) wo:

6 NOT APPLICABLE /8EL!EVED ASSENT ($t MNLFACT@ES 2 II,

TRICHLORCFv(PCXY ACETIC ACID (2, li, 5-T)J

, 4, 5-rR iCHtm0PHecxY PROPuoiC ACID (stLvEx, 2, 4, 5, TP) , 4, 5 T Enut 2, 2-OlOwCPROPIONATE (ERBON 0, Dit(D#L 0yrgCR0PoxYte. 4, 9-TRICacROPHENrL) P>osPum0THl0Afg (nore.EL)J

4. 'rTRICK.UIOPHEr0L (TCP); OR HEXAOt.OR0Pt(P( (FCPi! (ALL CATA FOR THE ADOW MUST BE GUeERATED USitG STAT 0ARD NdLYTICAL CALIBRATION PROCED@ES) OR WOv5 CR HAS REASON TO BELtEVE THAT TCIX) IS OR MAY BE PRESENT IN D(!R D!$CHARCE.

P.5t,8EPORT 'UALITATIVE DATA, GOERATED ***lOj ULED A SCREENIW PROCEDWE NOT PRESENT/ DATA !$ ATTACNED f @J6 FATED W!TH #AYTICAL ST4CAPDS, FOR 2, J /g)8, - TETRACHDIODIBENZD-P-dl0XIN iTCD01 FECORD ALL DATA Of4 F0pf95 PROVII,ED (ITEM / IN THl$ B00aLET. J. IF D( StMACE MATER CISCHARGE APPLtC#st udMS OR HA$ R(A50N TO BELIEVE THAT y ,gy gggggg Bl1 LOGIC 4 T0xlCITY TESTS wERE P%ff IN THE LAST TWEE (3) YEAAS ON W# CF TPE A APPt lC#dT,S D110tW45 OR ON A PECEIVI% WATER IN RELATICN TO A DISOtVIGE, PROVIDE THl$ iteFGTAf t;N AS #1 ATTAOf UT TO THl3 APPLtCATION. APPLICABLE /SEE ATTAOC K. 17 A C0rtT*8ACT LA&JRATORY CR C24SULT!'r. FIRM PERFCRED NN OF b( ANLAYSES REQUIRED tof APPLICABLE Bf f**ls AfPLICATl;N, PROVICE D( rdi'E NO ADOPESS OF EAOt t.A80RATORY OR Flfyt he D4 #AV5E3 PERF&f1ED AS AN ATTACsMNT OF THIS APPLICATION. APPLICA8tf/SEE ATTAOED IO YOU DI*,CHAfri( NA OTHER T0xiC CR ',WURICUS p(MICAL SLSST#eCES PCT LISTED IN WT APPLICA8L1 L. TAPLIS If FM4 h AD flA Der)r,e VA 5 8@@, 18 VE4, TTN ICENT!'Y DE OOICAL St&ST4dCES NO EST!%tTE THE L EFFLUENT CGCENTRAfl0NS. Sisilf THl1 It#WiAT10te AS Na ATTACiMNT TO Dils AePLICATION. APPLICABLE /SEE ATTAO(D I 9 f SECTION Il pERuir m N 000 D7 ' SEE INSTRUCTIONS WMBER v ON REVERSE SIDE UO lo,diBi ITEM A. USE THl$ DATA Sl(ET TO RECGW INFGNAft0N AS REQJ1 RED IN: (OECK AP.0PRIATE Box FOR mlCN INFOMATION THl3 DATA $6fET REPRESUNS.) 7

l. $ECTION !!, ITEM l-E.

GWX80 EATER DisodPGE tedFGNATION (PAGE $5) I CRITICAL yy

2. SECTION ll, ITEM 6. Pal @lTY MUTMTS IN SWFACE.TER DISCHAME (PAGE 37)

3. s. eEtoN: CRrfiCAL mATERtAt.s (TAeLE tv) IN suiFACE wArER DisodRGE (PAGE 5)

POLLUTANTS e g HOZARDOUS SUBSTANCES 3. List en CRITICAt..ite!AL (TAaLE IV PAGE 6) NOT ADWESSED IN SECTim !! ITEM 6 oggCR[n ,g7 App (g PQ L,JT4#$ wiCH v00 m.'Of Ot HAVE REASON fit BELIEVE TO DE PflESOR IN Tif DISCHARGE. SEE IN REVERSE 5tCE OF THIS PAGE FOR fumer DIRECT!ONS. DISCHARGE APPLICAaLE (SEE BELON) a A. PA*E OF CRITICAL NATDIAL Ot PRIORITY POLLUTANT ,,,,, g g g 5 CODE N DM #W#daMu

s. AVEMGE CmCENTw10N; SAMPLE TYPE; I & ANALYSES g g g

,,g g g 2 I WI M C. MAxtV COCENTRATION NO PASS A. Pi#T W CRITfCAA..TERIAL OR PRIORITY MUTANT g g g g g g g g B. AVEMGE CGCURRAT!ON; SMPLE TYPE; # OF ANALYSES l l g g,l l [ g c

i = = a a = = ~$$
i7 =,,,

.,,,, *i' P UNITS CODE -s A. PWT OF CRITICAL MAm!AL OR PRIORITY POLLin## g /g h y g usti CT4 SAPPL1 TYPE # OF WeA4.YSEs y B. AVEMCE C&CunRATION: SAMPLE TYPE; f CF AMLYSE$ l l, l,l l l l y a f, 4 3 LBS/ day 2 WIT CODE eli C444 C. MAxtu corCURRATION #O MAS $ g g, ,,g ,y g,,,,,,,, [_,j f 4 KG/ DAY A. PWT OF CRITICAL MATERIAL OR PRIORifY POL 11 RANT g l l l g g g g g y 8*"*'""

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ti*

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l l SECTION ll PERMIT M 000 M M NUMBER ' SEE INSTRUCTIONS ON REVERSE SIDE -n . =, wu two 1 tot 1C3 0 ITEM A. PM OF NESS CMIBumG 70 mE DISodAGE ,N,T, ,8,O,f;L,6lN, t8rL D W, i4i9i/i/i TWloutH Tk!S OUTFAL.L AtO SIC CCTE i 3 ,a,y, ,2,s, 8. PROCESS So<Du'E <<EMLY AvERAGd iss4 e,s/0A, E C. PROCESS WLthE FLOW RATE PROCESS TOTAL yEMLy I ' ' ' 'O'*' b STREAMS hA$l$'. \\984 Ft.oW DATA ,,y,,,,,,, ,,,,,,,,, o, @ CONTRIBUTING a. TO lO /'91 & DAILY MUIMM i I ' f ' l D. PROCESS PRODITION RATE DISC A E g, 9 g, ; g, g A. PWNE CP PROCESS CatiTRIBUTirG 70 ni DISCHMGE THOUGH THl5 O/TFALL NO SIC CTE NA i ' ' ' ' ' ' ' l 3. PROCESS SOEDA.E (YEMLY AVEMGE) ggy,, i gyy g ,,, a y, mir a C. PROCESS Wutt FLDs RATE g y , g, g g, g 3 g g y ee g DAILY MINIMtM ' ' ' ' ' ' ' ' ' ' U UNITS CODE gg DAILY P%XIttN ' ' ' f ' ' ' l ' ' lj 2 GALLONS D. PROCESS PRODITION RATE I I f ' ' ' ' f I lFU mt TS / TI4 A. hAet or Pn0 CESS CONTRisuf!PG TO DE DISodAGE VARDS Twiouret THIS ouTFALL #c SIC C00E N4 ' ' l 8 ' ' ' ' ' ' ' ' ' I ' ' ' ' ' ' 8. PROCESS Soeutz (YEMLY AVEMGd gggy g i i mVVvtM ' ' ' ' uhir a D C. PROCESS WList Flow RATE gg7g y g y I e i i t t I t t I LJ I I t t f I f f t f U DA!LY MINIMM DAILY M UIM N i i e i t t i t i i LJ D. PROCESS PROGET!ON RATE g a t t t t t t i TIME 1 HOUR A. N#( OF MCCESS apIm#pG m ME DISOME nerH THis ofr Att nO sie noE NA i ' ' ' ' ' ' ' ' ' ' ' ' - ' ' ' ' ' ' ' 3 WEEK I' tops / DAY L._L J mys/vtM i t I ' 4 MONTH m WT m g C. PR0tESS WL1PE Flow RATE TOTAL YtMLY ' ' ' ' ' ' ' ' ' ' L-I g* C DAILY MINIPtM l I l ' I ' ' ' ' ' U a PAfly MufM M I ' ' I I ' I ' ' I t w r5 f :4 D. PROCESS McDITim RATE t t t t t t t t i t.__v L_J A. PWE OF PROCESS CONTRIBUT!!G 70 DE DISOMAGE T40rH THis OUTFAu. At4D SIC CCTE h - I - I I I ' ' ' ' ' I ' ' l ' I ' ' l I l-5. PROCE15 SOED12 (YEMLY AVEMGd pOms/CAV I t t DAYS /YtM l l ' ' g elT CM g C. PROCESS M FLD# RATE 7ggg y g, e # # l t t t i i 1 y e f gaggy pgugsgp i f i I I I ' I l i U catty muttgp i f f ' I I I ' ' ' W D. McCESS MoouCTice RATE UN1f 5 / fl4 t i t t t t t ' t L__V L.J I l i i 1 3 I SECTION 11 PERMIT W00 MM NUMBER . SEEINSTRUCTIONS LN REVERSE SIDE 0,TFlu M M G , o, o, c, A. [5 M 01 FALN THIS OUTFALL DIREC TO THE GRouro OR GROLPOnATERS. IF PC, CmT!NUE T3 ITD' 3 YES NO 8 MAS A HYDROGE0 LOGICAL Sit 0V at iTS EQUIVALENT BEEN PERFOfttD OR l$ THRE StFFICIDT CURRENT HYDR 0GEC(QGICAL IWOINATION AVAILABLE A1 REguf 8ED Y teATER RESOURCES SES NO CCPNi$$!ON PAAT H GROLFOdTER RULE CF ALLUST 14, d@ R. (PEE id) FOR 1 .g GROUNOWATER THl3 utst!NG CR PROPOSED DISCHARGE [F YES ATTAot A CCPY OF THE REPORT. Ol5 CHARGE C. ARE You R I AN DCffim FRO 9 StaMITTl?G A HY30 GEOLOGICAL REPCRT LFCER INFORMATION RIAE R (PEE %) OR FRm GROLJOsATLR MONITORING REQUjREMENTS VES 90 LPCER HULE R. (3) (PEE 142) 0F M PART H RULES. IF YE5 ATTACH DOCLtENT$ #O DPLNdTION TO C&Os5TRATE THAT Y0 Lit 0150t4 AGE *OLD QUALIFY FOR .w o u m n. NA ME YOU REOLE$il!G A VARIANCE FRCH REE 323.M (PEE y IF YES, ATTACH SUCH (NCFCEGRADATICN) CF D. ygg IO ikE WATER RESOURCES C3NIS5tCN PART U GRotsoeATER RULE 3. DOC: penis As hECE55AAY TO TE M NE FOR A VARI A, IN TE7NS OF M CRITERIA SPECIFID IN RIAE (PME OF M PART RULE $. E. (IST AL.L CHEMICAL $la5fM(.E5 *tO4 ARE TN MICHIGAN $ CRITICAL MA RIAL 5 REGISTER TABLE IV (PEE h) AND/OR U.S. EPA'5 PRI3 TTY Pot 1UTANT LIST TABLE V (PAGE OR ANY CMR SLAST4CES NOT MICABLE/ BELIEVED ABSENT

!CH ARE CR MAY BECOPT IPUURious TO M CESIGNATED USES OF T>E TER Of TO TNE PUBLIC HEALTH THAT ARE DISCH4AGC OR EXPECTO TO EE DISCH4 AGED TO M GROLfOe4TER SY THl3 FAC[LITY. EST! MATE THE FIVL EFFLUENT C0ftENTRATICH NO RECCRD ALL DATA IN ITD9 7 0F SECTION ll !N THIS 9004.ET.

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UNITS CODE. TOTAL PPOSPHCRUS (AS P) l I I I.I I I I I f I I *l I l i L.I.J B f f L_j 1 Cg/l LIl ' ' ' LJ 2 Ug/l tota. RESIDUAL o(ORINE 3 COUNTS / I I I I I I ' ' ' ' ' .I ' ' I b' U 100 ml OtS$0LVED CM Mtg o S. U. og I I I. L_1 w.u t.qj L_L_J L_J $ 'F 6 LBS/ DAY W U FECAL COLIFORM BACTERIA 'ToetufuRE (stiTv) L L_l L J L J_J. d LEJ L-3 'TerEuftn (wlNTER) L L A. L_J LL!.LI L.E.1 L L_J L_J f. B. OTH0t h4STEhATTR CHARACTERfSTfCS toi leL # 4 A p pt trA t S t E t i e i e ,i e i 1 e e t ,e I e # y W y gg i i e i i e i t i i i e i t i.I i e i a e i j.I e t i L,J L,, J._l L,) ,q, l., ,.1 u t_u a 2 24 HOUR i e t i e i i i e i i t i e i i.e i e i i i e i.i i e i LJ L_J COMPOSITE e t t i i t i i e i i i e e t

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t i i e i i i e i i i.t i t i e f i e.I i e i LJ L_L_J L_.I 7 REtelT TO: W atory W M e Park West Two NUS S300 CampbeHe Run Road Cliff MM Road Ptttsburgh,PA 15206 pittsburgh. PA 15275 412-706-1000 mg LAB ANALYSIS R E P C3 R T CLIDIT llANE: INBIANA & MICHIGAN ELECTRIC CO. NUS CLIENT NO: 010904 ABORESS: P. O. 30X 60 MVS SAfrLE NO: 15021727 FORT MYNE, IN 46801 YENDOR NO: EPORT MTE: 03/26/95 WORK ORER NO: 55630 hiTENTION: NR. J0WI IREMEY DATE E CEIVED: 02/27/85 SAlfLE IENTIFICATION: AUX. EATING 90!LER BLOWD0lal 02/24 TEST KTERMINATION ESLA.TS UNITS a_ 1341 NPMS PART V-l M010 Aluminus ( All (0.1 ag/l 8040 Borius (k) < 0.1 og/l M150 Cobolt (Co) 40.01 og/l 1190 Iton, total (Fe) 33 ag/l M230 Magnesius (Mg) 0.44 ag/l 1240 Mor,genese (Mn) 0.31 og/l M260 Molybdenue(Mo) < 0.03 ag/l 1340 Tin (Sn) (1 og/1 M350 Titanius (ii) <0.5 mg/l 1055 Boron (3) <0.2 og/l 9060 Broeide(9r) <2 og/l 1225 Color,True 240 Pt-Co W310 Fluoride, total (F) < 0.5 mg/l 1410 Nittite (M) <0.01 og/l W435 Nitrogen, Kjeldehl (N) 0.8 og/l 1440 Nitrogen, Organic (M) 0.1 og/l W540 Phosphorus, total (P) 4.3 ag/l 1730 Sulfate, terbiditetric (SO4) 7 og/l W740 Sulfide (S) < 0.1 og/l 1760 Sulfite (S03) (2 og/l W770 Surfactants (MBAS) < 0.1 og/l H362 MPMS PART V-C T0XIC METALS M020 Anttoony (Sb) ( 0.1 ag/l 8030 Arsenic ( As) 0.005 mg/l M050 Beryllius (le) <0.002 og/l 1090 Codelue (Cd) < 0.005 eg/l M140 Chrontus (Cr) 0.01 og/1 1160 Copper (Cu) 7.9 og/l M200 lead (Pb) <0.03 ag/l 1250 Mercury (Hg) < 0.0002 og/l M270 Nickel (Nil ( 0.03 og/l PAT NO: 1 h A Halliburton Company CLIENT ORIGINAL REbefT TO: 1.atsoretory Servkies DMeken Park West Two 5300 ComptieNs Run Road Cim Mine Road Pmetturgh, PA 15206 Pittsburgh. PA 15275 412 7as toso mg LAB ANALYSIS R E P C3 R T 1 CLIDIT liblE IISIAllA & MICHIGAll ELECTRIC CO. IlUS CLIENT 110: 010904 ABIRESS: P. O. DOX 40 1105 SAlfLE 110: 15021727 FORTllAYIIE, Ill 46801 VDOOR 110: EPORT BATE: 03/26/95 WORK ORKR 110: 55830 ATTENT!0ll Itt. 30Hil HUGEY DATE KCEIVED: 02/27/85 SAlfLE IDDITIFICATI0ll: AUX. EATING DOILER BLOWDOWil 02/26 TEST KTERMIllATIOlt ESILTS UlllTS 1990 Selenius (Se) <0.004 og/1 N300 Silver ( Ag) < 0.01 og/l 1330 Thellius(T1) <0.1 ogIl R390 Zinc (In) 0.04 ogIl 1270 Cyanide, total (Cll) < 0.01 og/l 11500 Phenolics <0.02 og/l M220 Lithius (L1) < 0.01 ag/l 0110 VOLATILES-PP IN WATER 0101 Acrolein (100 ug/l OY02 Acrylonitrile ( 100 ug/l 1903 Senzere (5 ag/l OV05 Itonofore <5 ug/l 1906 Cathon Tetrochloride <5 ag/l OYO7 Chlorobenzere <5 ugIl 1908 Chlorodibtonomethene <5 og/1 DV09 Chlorcethane < 10 og/1 IV10 2-ChloroethylvinylEther < 10 ug/l DV11 Chlorofore <5 ug/l IV12 Dichlorobtotonethane <5 ug/l DV14 1,1-Dichloroethane <5 ug/l IV15 1,2-Dichloroethane <5 ug/l DV16 1,1-Dichlorcethylere <5 ug/1 IV17 1,2-Dichloropropare <5 ug/l DV18 1,3-Dichloroptopylere <5 ug/1 IV1T Ethylbenzene <5 ug/l OY20 Methyl Itontde < 10 ug/l IV21 Methyl Chloride < 10 ug/l ov22 MethyleneChloride <5 ug/l 1923 1,1,2,2-Tetrochloroethone <5 ug/1 OY24 Tettathloroethylene(Perchloro) <5 ug/l IV25 foluere (5 ug/l DV26 1,2-Trans-Dichloroethylene <5 ug/l Pn(E NO: 2 h A Halliburton Company CLIENT ORIGINAL REstri 70: h4 W Neon Park West Two 5360 Campbells Run Road Cliff Mine Road Plttehurgh, PA 15206 Pittsburgh, PA 15275 mg 412-788-1000 LAB ANALYSIS R E P C3 R T CLIENT llAE INDIAIIA & MICHIGAN ELECTRIC CO. NUS CLIENT NO: 010904 AIORESS: P. O. 30X 60 NUS SAlfLE 110: 15021727 F014 WAYE, IN 46001 WNDOR NO: KPORT SATE: 03/26/05 WCRK ORDut NO: 55830 ATTENTION: IWt. J0001 HUGEY DATE K CEIVED: 02/27/95 SAIFLE IKMTIFICATION: AUX. E* TING BOILER BLOWD0181 02/26 TEST KTERMillATION ESULTS UNITS 9/27 1,1,1-Trichloroethene <5 ug/l DV28 1,1,2-Trichloroethane <5 ug/l IV29 Trichloroethylene <5 ug/l OY31 Vinyl chloride <5 ug/l 0120 ACIDS - PP IN WATER 0A01 2-Chlorophenol ( 10 ug/l lA02 2,4-lichlorophenol < 10 ug/l 0403 2,4-Dimethylphenot < 10 ug/l lA04 4,6-Dinitro-o-cresol ( 50 ug/l 0A05 2,4-Dinitrophenol ( 50 ug/l lA06 2-Mittophenol ( 10 ug/l 0407 4-Nitrophenol ( 50 ug/l lA08 p-Chloro-e-cresol < 10 ug/l 0A3 Pentochlorophenot < 50 ug/1 lA10 Phenol < 10 ug/l 0A11 2,4,6-Trichlorophenol ( 10 ug/l lE30 AcidExtraction-Water 0130 BASE EUTRALS - PP IN WATER 301 Acenophthene < 10 ug/l 0902 Acenophthylene ( 10 ug/l l903 Anthracene < 10 ug/l 0904 lenzidine <50 ug/l 1905 Senzo(a)Anthrocene < 10 ug/l 0006 Berso(e) Pyrene < 10 ug/1 1907 3,4-Deraofluotanthene ( 10 ug/l 0000 lenzo(ght)Perglene < 10 ug/1 1809 lenzo(k)Fluotanthene ( 10 ug/l Wie lis(2-Chloroethoxy) Methene ( 10 ug/l Illi lis(2-Chloroathyl) Ether < 10 ug/l 0812 list 2-Chloroisoptopyl) Ether < 10 ugIl till lis(2-Ethylhexyl)Phtholote < 10 ug/l 0914 4-trotophenylPhenylEther ( 10 ug/l l PA E MO: 3 1 h A Halliburton Company CUENT ORlG!NAt. REsotT TO: Lettoratory Services Divleion Park West Two 5360 Comptiotie Run Road Cliff Mine Road 1 Pettet,urgh, PA 15206 Pittsburgh, PA 15275 g 412-786 1000 l i LAB A P4 A L Y S I S REPORT CLIENTIIAIE: IMIAllA 6 NICH10All ELECTRIC CO. NUS CLIENT NO: 010904 ABIRESS: P. O. BOX 40 WUS SAlfLE NO: 15 P 727 FORT HATIE, IN 46001 VENDOR 110: ID ORT DATE: 03/26/95 W0ltK ORKR 110: 55130 ATTENTI0ll IEt. JOlel illOIET DATE K CEIYED: 02/27.'85 SAlftE IKNTIFICATIOll: AUX. lEATING 10!LER BL0llD01A1 02/26 TEST KTERNIllATI0ll KSULTS Ull1TS 3 15 Butyl Benzyl Phthelete < 10 ug/l 0816 2-Chloronephthelone ( 10 ug/l l 1817 4-Chlorophenyl Phergl Ether ( 10 ug/l ( 10 ug/l 0010 Chrysene < 10 ug/l 8817 Dibenzo(e h) Anthracene 0920 1,2-Dichlorobenzene < 10 ug/l 6321 1,3-Dichlorobenzene ( 10 ug/l 0822 1,4-Dichlorobenzene < 10 mg/l ll23 3,3'-Dichlorobenzidine ( 10 mg/l 0024 Diethyl Phthelete < 10 ug/l 1925 Dimethyl Phthelete < 10 og/l 0826 li-N-Dutyl Phtholete < 10 ug/l 1827 2,441nitrotoluene ( 10 ug/l 0828 2,6-Dinitrotoluene < 10 ug/l IB29 Di-II-Octyl Phthelete < 10 ug/l 0830 1,2-Diphengthydrezine(Azobz) < 20 ug/1 1831 Fluorenthene < 10 vg/l 0832 Fluotene < 10 ug/l 1933 Hexechlorbenzere ( 10 ug/l 0934 Hexechlorobutediene < 10 ug/l 1835 Hexechloro-cyclopentediene ( 10 vg/l 0836 Hexechloroethene < 10 ug/l 1837 Indeno(1,2,3 cd) Pyrene ( 10 ug/l 0830 !sophotone < 10 ug/l 1839 Ilophthetene < 10 ug/l OMO Nitrobenzene < 10 ug/l IM1 N-Nittosodieethyleelne ( 10 ug/l 0842 M itrosodi-N-Propyleetne < 10 ug/l 1943 Il-littrosodiphenyleine ( 10 ug/l OM4 Phenenthrone < 10 ug/l IM5 Pyrene ( 10 ug/l OM6 1,2,4-Trichlorobenzene < 10 ug/l j Pn 2 NO: 4 h A Halliburton Company CLIENT ORIGINAL REI8f7 TO: Laboratory Services DMeion Port West Two NUS 5360 Campbelle Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-786-1000 l_ A B ANA1YSIS REPORT CLIENT MAE INDIANA t NICHIGAN ELECTRIC CO. NUS CLIENT 1101 010904 ABORESS: P. O. 30X 60 MUS SAIFLE N0: 15021727 FORT WAYE, Ill 46001 VDIDOR 110: REPORT MTE: 03/26/95 WORK ORER 110: 55830 ATTENTION: NR. Jolti HUGET DATE RECEIVED: 02/27/85 SAIFLE IDDITIFICATION: AUX. EATING 90!LER BLONDOWN 02/26 TEST DETERMINATI0ll RESULTS UNITS E25 h se Neuttel Extraction-Water 0141 PRIORITY POLLUTANT Kl'S E11 K3 Extraction - hter OPit KB-1016 (0.5 mg/l IP20 KS-1221 ( 0.5 mg/l OP21 KB-1232 ( 0.5 ug/l $P22 KI-1242 < 0.5 ug/l OP23 Kl-1248 ( 0.5 ug/l lP24 K3-1254 ( 1.0 ug/l OP25 KB-1260 ( 1.0 mg/l R450 RADIUM 226 AND 226 RM4 Redive-226 ( 0.4 pC1/1 1905 Radiue-228 <3 pCi/1 R900 Gross Alphe <1 pCi/1 1901 Gross hte 2.4 l/-1.1 pC1/1 9032 Aeoonie es N (distillation) 0.7 og/l 1050 300, 5-day (02) <1 og/l W100 Carbon, organic (C) <1 ag/l 1120 000 (02) 11 og/l W390 Hittote (N) 1610 Solids, suspended at 103 C 99 og/l Com0lTS: Reviewed and Approved hi JIC P E NO: 5 h A Halliburton Company CLI,ENT ORIGINAL --..~ REANT TO: Laboratory Services Division Part West Two NUS 6300 Campbelle Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 CCH3CF% TON 412-786 1000 LAB ANALYSIS R E P C3 R T CLIENT MAE ISIAL L MICHIGAN ELECTRIC CO. NUS CLIENT NO: 010904 ADtRESS: P. O. 30X 40 NUS SAfrLE NO: 15021728 FORT WAYE, IN 44001 VENDOR NO: EPORT DATE: 03/24/85 UORK ORKR NO: 55830 ATTryttoN: pet. JOHN HUGEY DATE RECEIYEB 02/27/85 SAIFLE INNTIFICATIDM AUX. EATING 90!LER 3 LOWDOWN-GRAB 01 02/24 1230 1EST KTERMINATION RESLR.TS UNITS lA32 Fecol Califore - IPN <3 col /100ml W150 Chlorine, residuel DPD (C12) < 0.1 og/l 1490 pH f.2 W680 Oil, extraction grevisetric 1.3 ag/l Gt9 TENTS: Revtwed ard Approved by: JNC $ A Halliburton Company CLIENT ORIGINAL Reas 7 To: Laboratofy Services Ovision Park West Two NUS 5360 Campbelle Run Mood Cittf Mine Road P*ttsburgh, PA 15206 Pittsburgh, PA 15275 CCFPCFMM 412-786-1000 I i LAB ANALYSIS R E P C3 R T CLIENT NAE 1 9 1ANA & MICHIGAN ELECTRIC CO. NUS CLIENT 110: 010904 ADMESS: P, O. 30X 40 NUS SAIFLE NO: 15021729 FORT WYE, IN 44001 VD80R 110: EPORT MTE: 03/2&/85 WORK ORKR NO: 55830 ATTENTION: IWt. J0M HUGEY MTE ECEIYD 02/27/95 SAltLE IKMTIFICATION: AUX. EATING SOILER K000lal 02/26 1530 1EST MTERMillATION ESULTS UNITS IA32 Fecel Califore - IPN <3 col /100e1 V150 Chlorine, residuel DPD (C12) < 0.1 og/l 8490 pH 8.6 W680 011,extractiongravinetric 3.0 eg/l .l m m Ewisi i l l l Reviewed end Approved hi Jnc h A Halliburton Company CLIENT ORIG:NAL 9 L. m REINT TO: Laboratory Services DMeion Park West Two NUS 5350 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-786-1000 LAB ANALYSIS REPORT CLIDIT llAIE: INDIAM L MICNISAM ELECTRIC CO. IIUS CLIENT 110: 010904 ABORESS: P. O. BOX 60 IluS SAMPLE NO: 15021730 FORTWAYlE, Ill 44001 VDIBOR 110: IIEPORT DATE: 03/24/95 WORK ORKR NO: 55830 ATTENTION: Idl. J0101 HUBIEY DATE K CEIVED: 02/27/95 SAIFLE IDDITIFICATION: AUX.EATIll0 DOILER BLOWDOWN-GRAB 63 02/26 1830 TEST KTERMIIIATI0ll RESLA.TS LRilTS 1432 Fecel Califors - 1991 <3 col /100e1 W150 Chlotine, resideel DPD (Cl2) < 0.1 og/l 1490 pH 8.3 W680 Oil, extraction grevisettic 2.1 ag/l l DMIENTS: Reviewed and Approved 1 : .DC @ A Halliburton Company 1 CLIENT ORIGINAL ) REtelT TO: s 1 aboratory Serviose DMelon Park West Two NUS 5300 Campbelle Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 Mg 412-786 1000 s _ LAB ANALYSIS REPORT i CLIDifIWE IllBIANA 4 NICHIGAll ELECTRIC CO. IIUS CLIENT NO: 010904 AIOMSS: P. O. BOX 40 IlUS SAWLE NO: 15021731 FORT WAYlE, IN 46001 YEN 90R 110: EPORT Wil 03/26/95 il0RK ORER 110 '555'O ATTENTION: IWt. JOlti HUIEY DATE ECEIVEDs 02/R/85 SAMLE IDDITIFICATI0ll ' AUX. EATING 90!LER BLOWDOWN-GRAB 44 02/26 2130 TEST KTE3111ATI0ll MSULTS UllITS lA32 Fecal Collfots - fril (3 ccl/100el U150 Chlorine, residual DPD (Cl2) < 0.1 ag/l 1990 pH 7.9 9600 Oil, extrtction grevisetric < 1.0 mg/l s 4 \\ e k A s e

D Gl9IENTS:

i s h A Halliburton Company CLIENT Oi!!G!NAL - - - - ~ ~ --- SECTION 11 PERMIT . MIoco SD7 SEE INSTRUCTIONS NUM!ER ON REVERSE SIDE (1,VltL 1*ER ,d,oiG, TkE FOLLDv!PG REQWSTED l'#0Pr% TION M ! 'I ADWESSED BL.M. SWFACE WATER CISCHARGER$. lGE! NDe USE DISCHVGERS %E. PACvia urECTED VALES M THE QLANTITATIVE NO GLAITATIVE thFCRPSTION REOUL$ RED BELLw. A. !$ THIS FActLITY A PRIPWIY If0USTRY? (REFER TO TABLE IA PE4 43 @ YES hr v), M TO E! (tr VES. @ TO B) r0 PRIORITY B. INclCATE TYPE OF PRIMARY IPOUSTRY AS LISTED IN TABLE lA PEE 41 POLLUTANTS 'm3WEwtm d IbIIIMI d I b f t t C. I tMi(AA kg AND C. D:ES THIS CUTFE DISCHMGE CONTAIN ## PROCESS hASTEWATER! v hr 'O. m UFYM,m 0 A U NO ADDITIONAL INFIRhlATION D. ItOICATE welch GC/MS FRACTICNS MUST BE TESTED FOR. (PEFER TO TABLE !A PEE UD VOLATILE FOR NO.E! FOR EAOf GC/MS FRACTION O(CKED,EAO4 SPECIFIC ORGANIC T0XIC POLLUTANT WITHIN SURFACE EAo* FRACTION LM.T BE ANALYZED FOR (SEE TA8JLE IIA PME U2. IN AC9til0N, N.L PRIMARY BASE /t(UTRAL WATER ltOUSTRY APPLtC/nfi ulTH A PPOCE$$ WASTEhATER DISCHARGE 53I PROVICE QuMT[ TAT [VE WA M W MC M1mTABaIttA M @. DISCHARGE ACID l ONLY RECDPD ALL DATA ON FGNS PRQVIDED ([TT/t 7) IN THl3 B006. j (CONTINUE wtTH E1 BELOW) PESTICIDE t. IF 4*J. SWFACE HATER CISCHMGE APPLIC#st (PRIMARY OR SECGCARY INDUSTRY), REGAR3.ESS OF T4 nPE u c:sadRGE, uns c2 HAS REASON TO BELIEVE THAT ## Pou.UTANT L15 FED PCT APPLICAaLE/ BELIEVED ABSENT IN TABa llA A'e0 IVA PE,E$ d ($ DISCHMGED Fret ## QJTFAL1,DC QtANTITATIVE asI BE PlW[MD. RECORD ALL CATA Ota FJRMS PROVIDED (lTEM 7) IN THIS 800MLET. PRUMA !$ AN F. IF ANY $@ FACE WATER O!SChMGE APPLICANT (PRIMMY CR SECofGRY (NDUSTRY), RCGMDLESS OF TYPE OF DISonoGE, NovS CR HAS REA304 TO BELIEVE ## POLLUTANTS LISTED IN M NOT APPLICA8LE/ BELIEVED ABSENT TA8LE VA PEE 4} APE OlsCHApre Fern ANY OfrFALL Th( APPLICANT 5$I CESCRIBE REA$chs FCR DE POLLUTANT BEttG PoESENT NO PROVIEC ANY AVAILABLE QUANTITATIVE DATA. RECCRD ALL DATA Cid F0FNS PROVICED (ITEM 7) IN TH15 B00xLET. PPESENT/CATA IS ATTAO(D G. ALL 1@ FACE MATER DISOARGE APPLIC#eTS (PRIMMY Ato SECCtOARY IPOUSTRIES) MO: >) NOT APPLICABLd8ELIEVED AB$ENT OR,wuAcr@n 2, 4. - TRiC40Rm(roxv ACEfipciD (2, 4, 5-rb , 4, )7P(CHLCROP4*CXY PROP 4Qlc ACID (SILVtX, 4, 4, 5, TP)f , 4,

TRICHLDROPMNOXY ETHYL 4 2-c!CHt0ROPROPl0NATE (EPs0Nn 0, OltTTHYL U-(2, 4, 5-TRICM OROPNFJ#L) PtOSPFLwOTH!OATJ (R0rt.EL);

4, b-TRIOt0RmEPOL (TCP)! OR HEXAOt0ROPHEt( bCPJJ (ALL DATA FOR THE ABOVE MU5T BE GEt(RATED US!?6 STNOMD NdLYTICAL CALIBRATION PROCED@ES) CR K?mt Gt NAS PEASON T3 BELIEVE THAT TCDD !$ CR MAY BE PPESENT IN DitR DISOdRGE. PEPCRT %ALITATIVE DATA, GE'(RATED WitOJ UitD A SCREENING PROCEDlFE NOT PRESENT/ DATA !$ ATTACHED 16 RATED WIDi #dLYTICAL STNOMDS, FOR 2, J, /()8,

TETRAOLOROCIBEN&P-DIQXIN TCLD). RECCRD ALL LATA Cr# F0fMS PROVIOED (ITEM / IN THl$ B00NLET.

J. IF Ted SURFACE MATER CISOdAE APPLICANT Wod$ OR HAS PgASON TO BELIEVE THAT T BIOLOGICAL T0XICITY TESTS =E8E MADE l's D( LAST D*EE (3) YEMS ON ## CF D( h1 POT APPLICABLE APPLICANT,$ D!$OtARGES Ot ON A PECEIVI?G FATER IN RELAfl0N TO A DISOSRGE, PROVICE THIS ITORf ATICH A3 #4 ATTACTOIT TO THl3 APPLICATICN. APPLICABLM5EE ATTAO(D R. IF A Cor# TRACT LANRATJRY JI CCf6tA fl?0 Fl AM PEDFCRPtD ## OF DE #4.AYSES REWIRED POT APPLICABLE l BY Troll Af PLICATI;N, PROVIDE Di r#E 40 ADI. FESS OF EAO4 LABORAT(*Y OR Filf1 NO THE #ptVSES PERFRED AS ## ATTAOf TNT OF THIS APPLICATION. APPLICABLE /SEE ATTAO(D L. DO YOU DISOtMGE ## OD(4 70xtc (A l'ut#1015 ICAL Sta$f# aces POT LISTED IN TAPLES tv P44 0 40 llA T40n4 VA PEFl Q-4 It VES, TVN ICENil8Y THr M APPLICABLE 04pfCAL SUBSTAt4E1 #4D E5fivrE Tr( FIML tFFLuLNT CO(ENTRATIJ45. $tEPtlT THi$ it#0ifuflore A$ Na ATTAOft.hT TO TH!) APPLICATION. APPLICA8LE/SEE ATTAO(D 9 l' SECTION 11 . PERMIT w MIcoo5%7 ~ NUMBER r

SEE INSTRUCTIONS
ON REVERSE SIDE NN io,0, C, ITEM A.

USE THis DATA SKET To RtJORD INFmMATIOt AS PE2J1 RED IN: (O(CK APm0PRIATE 80x FOR 48tCH INFm, TION THis DATA SHEET REME55STS.)

1. sECTION !!, ITEM 4-E.

GRottedTER CISCHARM twomAf t0N (PAGE SS) I CRITICAL

2. SECTION !!, ITEM 6. PRIORITY POU.UTANTS IN SLPFACE MTD DISOMiE (PAGE F; Q

MATERIALS 6

3. s. sEtat: CRITICAL MATotAts (TAstr tv) N SURFACE NATD DISOdRGE (f' AGE 39)

POLLUTANTS e HAZARDOUS SUBSTANCES B. Lt$T ANY CRITICAL MTDIAL (TABLE tv PicE 6) NOT AD&ESSED IN SECT!CN !! ITEM 6 DRIORITY PCT APPLICABLE i Rx.LUT465 441CH VOU CLV OR HAVE REASON fn EELIEVE TO BE PRESENT IN TM DISOdRGE. SEE IN RENERSE $1DE OF THis PAGE FCR FWVR CIRECTICNS. DISCHARCE ( ' APPLICABLE (SEE BELOW) A. NAME OF CRITICAL MATDIAL CR PR!Gt!TY POLLUTANT , g y, 9 9 g y 3. AVERAGE CDCENTRATION; $#fLE TYm; # OF ANALYSES g g g g g g g g 2 WI CCCE, WI CCE C. MAxtv COCENTRATION #0 PASS A. MME OF CRIT! CAL MATERIAL OR PR!GilTY POLLUTANT g g y, g g g, N 8. AVERAGE CONCDURATION; S49LE TYPE; # OF ANALYSES l l l g,g l l g 2 C. max!M COCENT2ATION #O MAS $ (#41T CCE ifalf COCE a t t t I t t t t_j t i e s,e e ! J (_) UNITS CODE -J A. 4tt OF CRITICAL MATERIAL m PRIORITY PCELUTANT l l l l l l l l 1 Mg/g h WIT CCCE !AM.A DPE 5 OF ANALYSss y 5. AvtRAGE CDCENmATION; SAMPLE TYPEI f CF ANALYSES l l l l,l l l l y y ,, i 4 3 LBS/ DAY 2 Wii M Lteli c a C. Pnxie COGURATION #O PESS ,,,,,,,, y,,, ,,e ,, i g,_j 4 KG/ DAY A. N#'E OF CRITICAL MATERIAL OR PRIGtlTY POLLUTANT l l l g g g g g h

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max!M COCURRATICN NO MASS M,

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ig=,,,,,,,,, =il CP C.

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g,,,,,,,, *g C.

=v mecuf! #0,ss Acc Tram paces & THrs ITEM 7 ARE ATTACan Fm T>c eEst OF T>< CR TICx. 5 YEs MAratALs uC/m PR!stTY PCx.LUTuns PE2;IRc to at REPORTo. -] 30 l 11 SECTION ll gER

YiI 000 bD 7 SEE INSTRUCTIONS

--i ON REVERSE SIDE j ORHU. tina o,o D, e ITEM ,n, w, t, s,c. -,o,5,. m, o,c,s.. ma a, w, A. <0 CAT-1 uE. -= - Sem A,8,s,o,4,p,r,,,o,u, ,P,o.u,D, 5 .. YTo!I REai - M = t i i C. YOU DISOd%E SEASmA&Af/ E I' "' '"I *

I Di$ CHARGE LOCATION D.

IF YES, LIST DISCMEE Pat!@S NA m / Dav m / Sr SCHEDULE W t t THaouaH I t e e i e o i pg,0w I t t t t t T).ftalm i i i i 1 I i EtATE I ? t t I THrjifN f f, t t i WASTEWATER gN,/,vt. >#t./ DAY IN,/wg. TYPE CODE E. thc Am ! CAT-RATE NA i i i. t__ i i i. o i i i.t m 1 CONTACT "ASDATE8 "_,,N F. TYPE OF MSTEHATER DISOtMGE [_ ) L) t ) L,J L_ J 2 NONCONTACT G. DISCHMGE SOCULE (YEMLY AVEi@GE) , Cuts / DAY i i i Mv/YEM 13i(A isi E CoOuNG x

ieWe6, mbCDE DISOtMGE FLos STATE gg ggpECTm Fw MTE 3

PRGCESS M. mw i,, i t 4 SANITARY O b 5 STORMWATER DAILY MINie f i f I I I I f f '}'*' DAILY M4*I M I UNR CM g g g,,, g j g, g fg 1 MGY I. M max!M.M DISCHMGE FLOW RATE TO BE AUTHORIZED IN PEFNIT. 2 MGD MS tGN I t I t ! t ! Ib r

I St J.

MAXtPLM DESIGt DISCHMGE Flof RATE. 3 GFD A. 00 YOU USE MTER TREATMDIT GITIVES TC TREAT Yout DISCHMCE7 (!F NO, CONT!M TO ITEM 3) YES NO ~ ITEM -T=.~o - C-Sna = n CF TitSE GITIVEs. $0t FORic ACID [ uTia.s TY W A 57GW Aftt 2 s o o.u ~ a x oe.e>u oE) oisc Aace ,a NELSTRAf.J f Al B 6 kJ ] WATER TREATMENT ADDITIVES C. m no GRESS OF MAN #ACTWERS Sopaurw >4V Dila A DE OF MSE GITIVES. Sutroeic. AcsD PB j 5 CHEM 8 CAL 9; TNC.

g. r. De N e,%,,,3, y,,c,

110 0 N. ADAM 5 sT. 3 UNITS CooE 1 Mg/l SonTE 3SS' NNDECSCN, KY tlay 30 m 2 Ug/l 4:e0 Rocc5tDE Woo 0S GLvD 'CN DEpirNDENCR OHlO 441413i j D. EXPECTED DISCHMGE CONCENTRATION - GIT!WS. 3 AVERME th 5, MAXIMLM UN $ = 1,o, tj,,,,, g,o, o, w,,1,o,o,o,

t_i_,

g e nin - Soosom Sot. rats GlTIVE M g_ _j ;,,,,, u;,,,,,

g__,

ki i I t t t (_.j ; i i, t 1 L__I J ' ' ' ' ' L_.1 E. DO YGJ TitEAT M DISCHARGE To ROCVE O!TIVES? YES pc 4 WtAT IS THE RDCVAL EFFICIENCY AND DISCHMGE FREGLOCY? NA = = ' " - F. %RDOVAL MtS./ DAY DAYS /w(. GITIVE - g i ; g i g (,_j g. -d G!TIVE NaME ,, i y f( GlTIVE PWT t,, t_ L J LJ

:

G. AS Me ATTAOftNT TO TWIS AP5'llCATICh PQ0VIT SPECIFIC Mat 9dALI AN Gt AQtATIC 70xlCOLfir.! CAL DATA Of REFERENCE WHIO4 ARE AVAIL.ABL.E AND d 'EIL INFGMATI3t CN M RATE OF EEGRA^ATION OF TK P5100UCTS FGt EACH GITIVE. App 2 eve m 4TELN INSTANTANEOUS NELIT2Ali TAT 104 0904 MIXf N G r a T- => 31 ni 7' I

0 SECTION ll QR I MOOO S837 I .SEE INSTRUCTIONS ON REVERSE S10E nnu mot io o Di lTEM r n A. m CP mxEu CmTRisVTiNG TO M DiSoWa neozM ne:S Ourve uc sic ccm , o, 7,,, t.,, w, A, s, r,E, ,w, r,R i i4,9, /, /, B. m3 CESS SOGLLE (YEA %Y AVEMCd gyy I}Ik1 13Ibf yyg/yrj f a

c. Pa0 CESS wuse ro. Mn PROCESS i/,si4,.i6,7.7,*t.ff mA,Euity STREAMS lC SQ F(,CuJ DATA ce t

CONTRIBUTING A d* cA Ly n Nt e i e t t t 'O' Lsj TO stLY wie i I I f ' f IN f

o$'[,*,$,

b I l_! D. muu man:On MrE NA

O/O i i, ' ' ' ' ' i A.

hatt CF P40 CESS (DNTRIBUT!NG TO M DISQWIGE T40use This OUTFu 40 SIC CGT M i f f f f f I I f f f I f f I t t I ii B. PROCESS N (MY AW) ,ctB,sjMy g,, cAysjytMt O 8a TOTA YEA %Y I I I I I I I I I ' E UNITS CODE cAILy mgN!mpt ! ' ' I I I I ' ' I U 1 POUNOS "I'Y *I" ' ' ' ' ' ' ' ' ' ' U 2 GALLONS D. PROCESS PRODJCTION MTE b 3 CutlC 1 I I t t f f f I A. YAftOS NMT OF PROCESS CDNTRIBUTING TO M DISOt4 IGE TwoJM THIS Cu178u. wo SIC CCDE Na a i i i i i e i i i i e i i i i i i i ii 4 TONS S M GY 6 MGD sotas/cAv i I 8 DAYS /vfAR 8 ' ' ' l 7 GPD W M A YEARLY ' ' ' ' ' ' ' ' ' ' ll f Darty n Nime i f I 8 I ' ' ' ' LJ g!Ly wtMsg i f f I f f I f I I-U D. Pn0 CESS P90m;CT10N MTE-TIME ] ~ 1-HOUR A. N#E CF PROCESS CNTRIBUTING TO DE DISOWIGE ~ [,,,,',,,,,,,,,,,,,,~, muru mis curru no sit cerE g 3 WEEK 8' "33 ' ~ 4 MONTH, gxsrs/ cay I f I Days / vest i f f 1 m S TEAR 0 tmIT CCCE TOTA YEARLY I I ' ' ' ' ' ' ' ' LJ g, DAILY MINIMf9 I f I 8 I I I f I I LJ ggty ggygg,, I f f f f I f f I I U D. PYCCESS PRODUCT!ON RA'E LMITS fit 4 1 1 I t I t f I I lVL! A. hatt CF P90 CESS CDNTRIBUTitC 70 DE DIS 0WICE T40rpt This CUTFu #d) SIC CCEE g I I I f I f ' ' I,,,,,,,,,,, S. PROCKSS SOctLE (fEARLY AVOIAGd May l t i Days / YEAR I f f f ,g C. PROCESS wLLPT Ft.N MTE wtT C;ii. go TOTA MY I ' I I I ' ' f f f U a DAILY MINIMlft I I ! I f f f ' f f L' J l CA!LY %xtPtN I t t,,,,,,, g D. P50 CESS F5000CTICN MTE g g i t i I i f t t 1 y

g SECTION 11 PERMIT N MO W 7 NUMBER 7 SEEINSTRUCTIONS ON REVERSE SIDE NN iO,ciDt ITEM -===-C 'o - - m r, " ~ o'sytIF NO, CONTINLE 70 ITDs 'y) R-GI0t.PeeATEAS. Q yts L_,J eo 8. MAS A HYDR 0 GEOLOGICAL STlDr OR ITS EQUIVALENT BEEN PelFoeED OR IS THRE SLEFICIENT CJRRENT HY310CE0 LOGICAL IWGPATION AVAILABLE A}4, RE RED LY TM_uiATER RESOURCES 43 NO cot 915110N PART U G10GOe4TER RIAE OF ALGUST 1 R.w.LW (PEE f) FOR GitOum0 WATER THIS DISTIE OR PROPD5ED DISOWLE IF YES ATTA04 A CUPY OF THE REPGtT. DISCHARGE C. ARE V W R TM 4a NTfm N StaritTTI5 A NEOLOGtCAL REN M INFORMATION RUL1 R. Q),(PEE M) Gt FROM GRouOeATLR fos!TORIPC gEQU[RD'ENT5 YES to JGR WLE R. 44J6 (51 (PEE 'd) OF M PART H RtLES. IF YES ATTACH DOCJtl4TS AfD OtPvJdTION TO CCDe5TRATE THAT Y0tJt DISOWIGE icAD QUALIFY FOt Me ryt'9noN. AAE YOU REOLEST!'G A VARIANCE FRGi RtAE 323.M (PEE y F YES, ATTAOe SUCH (*OCEGRADATION) 0F D. YES PC M MATER RESOURCES C3ftl5510N PART R GIOLAOe4TER RfA.ES. I DOC #'ENTS AS MCESSARY TO TRATE M NEED FGt A VARIANCE IN TER15 & M OtlTERIA SPECIFIED IN RL11 . 0 (PAGE 9]) 0F THE PART U RAIS. I E. Ll5T AL,L OctCAL StBSTAN[IS 'MiOc APE IN MJCHIGAN $ CRITICAL MAT { RIALS REGISTER TABLE IV (PEE 0) AND/0R U.S. EPA'S Pel!ORITY fu1UTANT LIST TABLE V (PAGE /) OR ANY OTMR StaSTANCES teelCH ARE OR MY BECCPE IPUURICUS TO M DESIGNATED USES OF T4 C40tJOenTUt OR TO T4 NOT APPLICAR.E/E!EVED ABSEE PUBLIC HEALTH THAT ARE DISOWIGED OR DPECTED TO BE DISOWIGED TO Tit GR0pounTDtJtY THIS FACILITY. ESTIMATE THE FthAL EFFLLENT CONCENTRATIG4 AfC RECDID ALL DATA IN liet / & SECT!31 II IN THIS BOCit ET. T4 APPLICANT MAY BE RE3JtRED TO 00 AICIT!ChAL HASTE ANALYSES. PRESEM, DATA NIDED IN ID 7 A. DISOWIGE OtARACTERISTICS CDNCENTRATIGd tAf!TS CODE # ANALYSES SMft1 T1 ITEM 5

C D (OtNICA CrYGEN DDwe)

I i f Ie I f f I I I I I.I f, I WI I I U j t. ' ' ' ' U TOC (TOTAL ORGANIC CARBON) T ATE C Ac- ,4 N,,40G,,, (A,N) ,, l. I,,,,,,..,,,, aI,, o TERISTICS l ' 8 I.I I I I ' ' ' I.I I ' TOTA SI)5PEtEED SCL.!DS di I I (_.] ~ ~ UNITS CODE TOTAL PtOSPHCRUS (AS P) _i l *i tm I i i l I f f I. I I f I L},,) [,_j,,,,_j U 1 Mg/l I ' d P.' 8.I '.' I l ' i. LI ,2 Ug/I' . TOTAL RESIDJAL O4 ORINE 3 COUNTS / b8 ! I I I

I

! I I I I I I I I I (J m mi DISSOLVED OXYCEN Mgg 4 S.U. .pg i l i, [,_J ,,, y g w y 5 'F FEcA COLtFO@t MRIA L)3 I U 6 LBS/OAY I I I I I I I I I I I I 'TDPERAftPE (50tTR) I ' I U I. U L.5; i t i U a 'TE.*fE;tATURE (nlNTER) '.U I ' '. L. J LI 8. OTHet ndSTENATER OWtACTIRISTICS j 1 0, !, L,1, 6, R, E, A, S, E, e t,e e # l' 1 e,i t t t y l , g y $ A Mpg I I t t t I I t t t t t i I t t I f f f i f I t.I I t i U f f f U. TYPE I f f f I f f f f f l l 1 I t I.l I f I f I l I.1 I l ! U l l i U 2 24 HOUR y, t, y COMPOSITt i I t i t i f I t t I t I t I t I 1 f f I f i f.I t t I U t I t U i t t I t t i 1 I t I i t I t t. I t t t I t t i.I t U i f f Q l t t t i 1 t I f f I i 1 e I e.I f f I f f f I.I l i 1 Q l f f U See attached sheets for data. Note: Results for triarylphosphate esters and hydrazine in Attachment I. I 7

REMfT TO: Laboratory Services OMsion Park West Two 5350 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15205 Pittsburgh, PA 15275 412-788-1080 1AB A N A1._ Y S I S REPQRT CLIENT NAME: IC IANA & MICHIGAN ELECTRIC CO. NUS CLIENT NO: 010904 ADDRESS: P. O. BOX 60 NUS SAMPLE NO: 15021694 FORT WAYNE, IN 46801 VED OR NO: REPORT DATE: 03/26/85 WORK ORK R NO: 55830 ATTENTION: MR. JOHN HUGHEY DATE RECEIVED: 02/27/85 SAMPLE IDENTIFICATION: TURBINE ROOM SUMP 02/26 TEST DETERMINATION RESULTS UNITS 1361 NPDES PART V-B M010 Aluminus ( All 0.4 og/l 1040 Borium (Bo) < 0.1 ag/l M150 Cobalt (Co) < 0.01 ag/l 1190 Iton, total (Fe) 0.21 ag/l M230 Magnesium (Mg) 17 og/1 1240 Manganese (Mn) 0.01 og/l M260 Molybdenum (Mo) < 0.03 ag/l 1340 Tin (Sn) <1 og/l M350 Titanium (Ti) < 0.5 og/l 1055 Baron (B) < 0.2 og/l WO60 Broeide (Br) <2 ag/l 1225 Color,True 70 Pt-Co W310

Fluoride, total (F) 34F-d0 5 mg/l 1390 Nitrate (N) 0.7 og/l W410 Hittite (N)

< 0.01 ag/l 1435 Nitrogen, Kjeldahl (N) 0.1 ag/l W440 ~ Nitrogen, Organic (N) 0.1 ag/l 1540 Phosphorus, total (P) < 0.01 ag/l W730 Sulfate, turbidinetric (SO4) 450 mg/l 1740 Sulfide (S) < 0.1 ag/l W760 Sulfite (503) <2 og/l 1770 Surfactants (PPAS) < 0.1 og/l M362 NPDES PART V-C T0XIC METALS 11020 Antimony (Sb) 0.2 og/l M030 Arsenic ( As) 0.001 og/l 1050 Betyllius (Pe) < 0.002 og/1 M090 Codnium (Cd) < 0.005 mg/l 1140 Chrentum (Cr) < 0.01 ng/1 M160 Copper (Cu) < 0.01 ag/l 1200 lead (Pb) < 0.03 ag/l M250 Mercury (Hg) < 0.0002 ag/l j 1

A recheck of the same sample was made by NUS.

PAE NO: 1 ) The first reported result was in. error, h A Halliburton Company CLIIT;T CRlG:N.;L

REtalT TO: Laboratory Services N Park West Two 5360 CampbeNs Run Road Cliff Mine Road PittstMargh, PA 15205 Pittsburgh, PA 15275 mg 412-708 1000 6 l AB AN AL YSIS REPORT CLIDif ME: IllBIANA L MICHI6All ELECTRIC CO. NUSCLIENTNO: 010904 ADDRESS: P. O. BOX 40 NUS SAlfLE NO: 15021694 FORT liAYE, Ill 44001 VENDOR NO: REPORT MTE: 03/24/85 il0RK ORDER NO: 55830 ATTENTION: 10t. Jolti HUliEY MTE ECEIVED: 02/27/85 SAltLE IDDITIFICATION: TURBIE ROOM Sulf 02/26 TEST KTERMIllATI0li RESLA.TS UNITS 100 llicitel (111) < 0.03 ag/l M290 Selenius (Se) < 0.004 ag/l 1300 Silver ( Ag) < 0.01 ogIl M330 Thalline (T1) < 0.1 ag/l 1390 Zinc (Zn) < 0.01 og/l li270 Cyanide, total (Cll) < 0.005 mg/l 1500 Phenolics < 0.02 og/l M220 Lithius (Li) < 0.01 6g/1 8110 VOLATILES-PP Ill llATER OV01 Acrolein ( 100 ug/l 1V02 Acrylonitrile <100 ug/l DV03 Benzene <5 mg/l IV05 Brosofors <5 ug/l DV06 Carbon Tetrachloride <5 ug/l 1907 Chlorobenzene (5 ug/l DV06 Chlorodibronomethane (5 ug/l 1909 Chloroethane < 10 ug/l OV10 2-Chloroethylvinyl Ether < 10 ug/l IV11 Chlorofots (5 ug/l DV12 Dichlorobronomethane <5 ug/l IV14 1,1-Dichloroethane <5 ug/l DV15 1,2-Dichloroethene (5 ug/l IV16 1,1-Dichlottethylene <5 ug/l OV17 1,2-Dichloropropone <5 ug/l IV18 1,3-Dichloropropylene <5 ug/l DV19 Ethylbenzene (5 ug/l IV20 Methyl Broeide < 10 og/l OV21 Methyl Chloride < 10 mg/l IV22 Methylene chloride <5 ug/l OV23 1,1,2,2-Tetrechloroethane <5 og/l IV24 Tettechloroethylene(Perchloro) (5 mg/l DV25 Toluene <5 mg/l PAE MO: 2 h A Halliburton Company CLIENT ORIGINAL

REeetT TO: Laboratory Services Division Park West Two NUS 5360 Campbells Run Road Cliff MmeQoed Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-785-1000 l LAB ANALYSIS R El* O R T CLIDIT IINE: IllDIAllA & NICHIGNI ELECTRIC CD. NUS CLIENT'NO: 010904 AleRESS: P. O. BOX 60 NUS SNFLE 110: 15021694 FORT WAYlE, IN 46801 YDIDOR 110: REPORT DATE: 03/26/85 UORK ORKR 110: 55830 ATTENTION: IWt. JOlti HUGIEY DATE RECEIVED: 02/27/85 SAIFLE IDOITIFICATION: TURBINE ROOM Sulf 02/26 TEST KTDtNIllATI0lt RES(LTS UNITS OG 1,2-Trans-Dichloroethylene <5 vg/l OY27 1,1,1-Trichloroethane <5 ug/l IV28 1,1,2-Trichloroathene <5 og/l OY29 Trichloroathylene ug/1 IV31 Vinyl chloride <5 ug/l 0120 ACIDS - PP IN WATER (M01 2-Chloropher( < 10 vg/l 0402 2,4-Dichlorop h ol < 10 ug/l IA03 2,4-Dimethylphenol ( 10 ug/l 0A04 4,6-Dinitro-o-cresol ( 50 ug/l IA05 2,4-Binitrophenol ( 50 ug/l 0406 2-Nitrophenol ( 10 ug/l IA07 4-Nitrophenol ( 50 ug/l 0408 p-Chloro-e-cresol ( 10 ug/l lA09 Pentechlorophenol < 50 ug/l 0410 Phenol < 10 ug/l lAll 2,4,6-Trichlorophenol ( 10 ug/l DE30 Acid Extraction-Water 0130 BASE NEUTRALS - PP IN WATER 0901 Acenophthene < 10 ug/l l 1902 Acenophthylene ( 10 ug/l i 0903 Anthrocene < 10 ug/l 1904 Benzidine < 50 ug/l 0905 Benzo (a)Aathrecene ( 10 ug/l l 1906 Benzo (oPyrene < 10 ug/l 0D07 3,4-Benzofluoronthene ( 10 ug/l 1908 Benzo (ghi)Perglene < 10 ug/l 0909 Benzo (k)Fluoronthene < 10 ug/l 9310 list 2-ChloroethoxyINethane < 10 ug/1 OB11 lis(2-Chloroethyl) Ether ( 10 eg/l 1912 91s(2-Chloroisopropyl) Ether ( 10 ug/l 0813 Dis (2-Ethylhexyl)Phtholate ( 10 ug/l PAE NO: 3 h A Ha!!iburton Company CLIENT ORIGINAL

REtetT TO: hWN Park West Two NUS 5360 Campboite Run Road Cliff Mine f.oed Pittstwrgh, PA 15206 Pittsburgh, PA 15275 412 788-1000 mg LAB ANALYSIS REPORT CLIENT llAfE IllDIANA & NICH16All ELECTRIC CO. NUS CLIENT NO: 010904 ADDRESS: P. O. 30X H llUS SAlftE NO: 15021694 FORTllAYlE, IN 46001 VD190R 110: IEPORT DATE: 03/26/85 110Rit ORDER 110: 55830 ATTENTION: Ift. Jolti HUGIET DATE RECEIVED: 02/27/85 SAltLE IDENTIFICATION: TURIINE ROON SL N 02/26 TEST DETERMINATI0ll RESiA.TS UllITS 3 14 4-Brosophenyl Phenyl Ether <10 og/l 0815 Butyl Benzyl Phtholote < 10 ug/l 1816 2-Chloronophtholene ( 10 ug/l 0017 4-Chlorophenyl Phenyl Ether < 10 ug/l 1318 Chrysene < 10 ug/l 0B19 Dibenzo(o,h)Anthrocene ( 10 ug/l IB20 1,2-Dichlorobenzene < 10 og/l 0921 1,3-Dichlorobenzene < 10 ug/l 9322 1,4-Dichlorobenzene < 10 ug/l 0B23 3,3'-Dichlorobenzidine < 10 ug/l 1324 Diethyl Phtholote < 10 ug/l 0825 Dimethyl Phtholote < 10 ug/l 1926 Di-N-Butyl Phtholote < 10 ug/l 0327 2,4-Dinitrotoluene < 10 ug/l IB2B 2,6-Dinitrotoluene ( 10 ug/l 0829 Di-N-Octyl Phtholote < 10 ug/l IB30 1,2-Diphengthydrozire( Azobz) ( 20 ug/l 0331 Fluoronthene ( 10 ug/l 1932 Fluorene ( 10 ug/l 0933 Hexachlorbenzere < 10 ug/l j 1934 Hexothlorobutodiene ( 10 ug/l OB35 Hexothloro-cyclopentodiene < 10 ug/l IB36 Hexothloroethane < 10 og/l 0837 Indeno(1,2,3 cd) Pyrene < 10 ug/l 1938 Isophotone ( 10 ug/l 0039 Nephthalene < 10 ug/l l540 Nitrobenzene < 10 ug/l 0941 N-Nitrosodieethylonine ( 10 ug/l IB42 N-Nitrosodi-N-Propylonine ( 10 ug/l 0843 N-Nitrosodiphenyleine < 10 ug/l 1844 Phenonthrone ( 10 ug/l 0345 Pyrene < 10 og/l \\ ME E: 4 h A Halliburton Company CLIENT ORIGINAL

REtsf7 TO: Laboratory Services DMeion Park West Two NUS 5360 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh. PA 15275 412 708-1000 LAB ANALYSIS R E P C3 R T CLIENT NAlf INDIANA & NIQlI6AN ELEC1 TIC CO. IlUS CLIENT NO: 010904 ADDRESS: P. O. 30X 60 NUS SAIFLE NO: 15021694 1 FORT HAYlE, IN 46801 YENDOR 110: EPORT DATE: 03/26/95 UORK ORDER NO: 55830 ATTENTION: Ift. JOHN HUGIET DATE RECEIVED: 02/27/85 SAMPLE IKNTIFICATION: TURBINE R00lt SUlr 02/26 TEST KTERNIllATI0ll RESULTS UNITS 3 46 1,2,4-Trichlorobenzene ( 10 ug/l OE25 lose Neutral Extraction-Water 0141 PRIORITY POLLUTANT PCB'S DE11 PCI Extraction - Water IP19 KB-1016 ( 0.5 ug/l GP20 Kl-1221 ( 0.5 ug/l IP21 Kl-1232 < 0.5 ug/1 OP22 PCI-1242 < 0.5 ug/l IP23 KB-1248 (0.5 ug/l DP24 KB-1254 ( 1.0 ug/l IP25 PCI-1260 < 1.0 ug/l R450 RADIUM 226 AND 228 19 04 Rodium-226 < 0.4 9 1/1 C R805 Rodium-228 <2 pCi/1 IB00 Gross Alpha 7.4 +/-2.8 pCi/1 RB01 Gross leto 5.8 +/-1.3 pCi/l 1032 Antonio os N (distillation) < 0.1 ag/l WO50 300, 5-dog (02) <1 og/l 1100 Carbon, organic (C) 19.5 mg/l U120 C0D (02) 9 ag/l 1610 Solids, suspended at 103 C 7 og/l ComENTS: Reviewed end Approved by: PM PAGE NO: 5 h A Halliburton Company CLIENT ORIGINAL

\\ RE4HT TO: Laboratory Seevices DMeion Park West Two 5350 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-788-1000 l_ A Et ANAL _YSIS R E P C3 R T CLIENTIUE: IRIANA & NICHIGAN ELECTRIC CD. MUS CLIENT NO: 010904 ADDRESS: P. O. 90% 40 WS SAFLE NO: 150216M FORT WYE, IN 44001 YENDOR MO: REPORT FATE: 03/26/95 WORK OR ER 110: 55830 ATTENTION: 10t. Jolti HUGHEY DATE RECEIYD: 02/27/95 SAlfLE IDENTIFICATION: TURRIE R00R SLN - GRAB 41 02/25 0635 ) TEST DETERMINATION RESLLTS UNITS ' lA32 Fecal Califors - W M 21 col /100e1 V150 Chlorine, residual DPD (C12) < 0.1 ag/l l 1490 pH 7.8 W680 Oil, extrettion gravinetric 3.3 ag/l 1 Gl9 TENTS: Reviewed and Approved ha AC h A Halilburton Company CLIENT OR!GINAL

REtsfT TO: Laboratory Services N Park West Two NUS 5380 Campbells Run Road Cliff Mine Road PittetMargh, PA 15206 Pittsburgh, PA 15275 412-7es toso mg LAB ANALYSIS REPORT CLIDif IINE: IFliANA & NICHISAll ELECTRIC CO. NUS CLIENT 110: 010904 ADBRESS: ?. c. 30X 60 NUS SAMLE NO: 15021696 FORT WATIE, IN 46801 YDIDOR 110: REPORT DATE: 03/26/85 WORK ORER NO: 55830 ATTENTION: IWt. JOlti HU8EY DATE RECEIVED: 02/27/85 SAltLE IDDITIFICATION: TURRINE ROOM Sur - GRAB 02 02/25 1440 TEST KTERMIllATIOll RESLA.TS UllITS 8432 Fecol Culifors - Irli 9 col /100ml W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 8.1 W680 011, extraction gravinetric 2.1 ag/l D M OITS: Reviewed end Approved by: JC h A Halliburton Company CLIENT ORIGINAL

REmfT 70: Laboratory Services DMelon Park West Lg NUS 5360 Campbells Run Road Chtf Mine Rosa Pittsburgh, PA 15206 Pittsburgh.PA 16275 412-788-1C40 LAB ANALYSIS R E P C3 R T CLIDIT NAE IllBIANA 6 MICHIGAll ELECTRIC CD. NUS CLIENT NO: 010904 ABORESS: P. O. 30X 40 IIUS SAMLE NO: 15021697 FORT WAYlE, Ill 46001 VENDOR NO: REPORT MTE: 03/26/95 WORK ORER MO: 55830 ATTENTION: lWt. JOHN HUGEY MTE E CEI ED: 02/27/95 SAWLE IKMTIFICATION: TURBIE ROOM Sulf - GRAS 43 02/25 2030 TEST KTERMIllATI0ll ESULTS UNITS lA32 Fecol Colifort - 1991 <3 co1/100e1 W150 Chlorine, residual DPD (C12) < 0.1 mg/l 1490 pH 7.9 9680 Oil, extraction gravinetric 2.7 ag/l l i 00tmENTS: Reviewed and Approved by: E h A Halliburton Company CLIENT ORIG lNAL

REletT TO: Laboratory Services DMeion Park West Two G350 Campbells Run Road Cittf Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-738-1000 g LAB ANALYSIS R E P C3 R T CLIDif IIAIE: INDIANA & MIQi! Gall ELECTRIC CO. IluS CLID(T 110 010904 ADDRESS: P. O. DOX 60 NUS SAIFLE 110: 15021699 FDRT llAYIE, Ill 46001 YEKDOR 110: IIEPORT DATE: 03/26/85 llORK ORDER 110: 55830 ATTENTION: IEt. J0001 HUGIEY DATE ECEIVED: 02/27/95 SAIFLE IDD(TIFICATI0ll TURBIIE ROOK Sulf - GRAB H 02/26 0235 TEST DETERMIllATI0li ItESULTS 1911TS IA32 Fecol Califors - IFil _9 col / local 9150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 7.0 1i680 011, extraction gravinetric 3.0 mg/l l i 1 GitqENTS: Reviewed and Approved by: JIC $ A Halliburton Company CLIENT ORIGINAL

SECTION 11 PERMIT IM 000 S89'? $EE INSTRUCTIONS NUMBER ON REVERSE SIDE rou..ma ,o,o,D, D4 FOLLOWING REQUESTQ IWOmATION C AD3ESSCD Elia. StFFACE.e4TER DISCWGERS. EE! MW trE DISOWGERS 2184 P610VI:n 6.APECTED VALtLS Fr.dt M 7JINTITATIVE AgG QuailTATIVE IMOit%T!WN REOLASTED BELO8 A. 15 THl1 FACILITY A PRt?WlY IfouSTRY? (REFUt TO TABLE (A PW4 S1) (tr 'c, to Yo E) t f F VEL f 0 YO 9) 'E3 PC PRIORITY B. IM)fCATE TYPE OF PR!PwtY IfCUSTRY AS LISTED IN TABLE IA PME d, POLLUTANTS 'W I *M d f N d I' I I I I I PlId RI l APs0 C. m m!$ cWFu MSCwGE COP 4AIN ANY PHOCESS mASTEMTW ADOITIONAl. INFOEMATION D. IrOICATE WCH GChtS FRACTIONS MUST BE TESTED FOt. (REFER TO TA8tf IA PM4 8]d) X NOLATILE tcE! Fat EA04 G"./MS FRACTION OECKED.EAOg SPECIFIC ORGAntC TCXIC POLLUT&ff wtTHIN f SURFACE EAOe FRACTION fld.T BE AMLY2ED FOR (SEE TABLE IIA PME 'J2. IN A[y)lfl0N, ALL PRIPAftY 8ASE/ NEUTRAL WATE14 ItcuSTRY APPL 1LAt.fi MtTM A P80 CESS WASTEHATER DISCMRGE g PROVIDE CunNTITATIVE DISCHARGE IN TAK E H!A M @. i f ACtD ONLY RECORD E DATA ON Fams PROVIDED (ITEM 7) (N THt$ 80CNLET. (Confiru wiTH E-< aEus) PESTICIDE E. IF 47. SLAFACE HATER DISOWGE APPLICANT (PRIMARY OR SEC3CARY INDUSTRY), REGARDLESS OF M. TrPE OF DISOWGE, 4085 OR MS REASON TO BELIEVE THAT ## POU,UTANT USTED iOT APPLICABLE /BEUEVED ABSENT IN TABLE IIA A'iD [VA PAGES M 15 DISOWGED FROt ANf OUTFAt.1,M QuRNTITATIVE nn sE PR0vrxD. RECDRD A&.L DATA ON F0m5 PROVIDED (ITEM 7) IN THIS BOOKLET. 7 F. IF ## SJtFACE nATER DISCheRGE APPLICANT (PRIMARY CR SEcorOARY IPOUSTRY), REGARDLESS OF TYPE OF DISOA%E, CO*S OR HAS REA30t TO BELIEW ANY POLLUTANTS LISTC IN b NOT APPLICABLE /8ELIEVO A8SENT TABLE VA PACE 4 ADE DISCHAEED FRr?4 ANY OUTFALL T4 APPLICANT %iT DESCRIEE REASchs FCR D( POLLUTANT BElrG PRESENT WO PROVIDE ANY AVAILABt.1 QuahTITATIVE DATA. RECORD ALL DATA ON FONS PROVIDED (! TEM 7) IN THIS BOOKLET. PRESENT/ DATA l$ ATTAOED ~ C. ALL SLAFACE MTER DISOWGE APPLIC#sTS (PRIMARY WO SECONDARY treJSTRIES) Mc: ~ K POT APPLICAKE/aELIENEDf8SENT OR P%tafACTtRES 2, li, - TRIOEOROPEPOXY ACETIC ACI (2, 31, 5-T); i i - , 4, 5-rRtOR.oPOPHEtcXY PROPAN0!C ACID ($1LVEx 2, 4. . TP)- , 4, 5-pigt ROPw cxY EmYL 2, 2-DIDOOPROPIOMTE ERBCN): 0, D!rETHYL g-(z, 4, 5-TRIO 4Ap0PHENYL) PPCSP>0ROTH10 ATE (R0r#EL); 34, $-TRIOLOROPF(*OL (TCP); OR HEXAOt0ROPHILE (tCP); (ALL DATA FOR TE ABOVE PtJST BE GEt4AATED USitG STAPCARD ANALYTICAL CALIBRATICri PROCERRES) OR Cots OR HAS REASON TO BELIEVE TMT TCED is OR MAY BE PRESENT IN MIR DISOWCE, tim PEPORT '1]ALITATIVE DATA, GENERATED welOj t. QED A SCREEN!NG PRocEDLRE !OT PRESENT/ DATA IS ATTAO(D CAL 18 RATED plTH #enLYTICAL ST# CARDS, FOR 2, 2. / 8. - TETRAOWODIBEN2D-P-DIQXIN t (TCDD). RECORD All DATA ON F0mS PROVIDED (ITD1/) IN THIS 800utIT. J. IF T;E SLRFACE sdTER DISOWGE APPLICANT EPOWS Ot HAS REASON TO BELIEVE THAT BIOLOGICAI,$ DISOWGES OR ON A RECEIVIPG MATER IN RELATION TO A DISOWGETCx! CITY TESTS WEPE MADE POT APPLICABLE APPLICAr# , PROV!CE THl3 ITGth4TI:;;4 AS #4 ATTAOfbT TO THIS APPLICATION. APPLICA8LE/SEE ATTAOED IF A CONTRACT LABGtATORY OR CD6tLTim FIRM PERFOMD ANY OF T4 AM.AYSES REQUIRED R. St NIS AFPLICATICN, P6t0 VIDE TM hAME WO ADOPESS OF EACH LABORATORY OR Fim NO NOT APh! CABLE THE ATiALYSES PERF3dED AS AN ATTAOtENT OF THIS APPLICAT[ cpg. APPLICABLE /SEE ATTACHED DO YOU DISOWGE ## CDER TCxic OR iPLARI O ICAL StBSTANCES NOT LISTED IN L. [F YES, TtEN IDENTgev TE K NOT APPLICABLE TAPLES IV PEE D A:D IIA TWor** VA PARES -, O(MICAL SLASTANCES #4D ESTIMATE THE FIML EFFuKhi COCENTRAT!3ts. SLD9ff THl3 IVC #% TION AS #4 ATTActf1ENT TO THIS APPLICATIori. APPLICA8LE/SEE ATTAOED O

= i SECTION 11 PERMIT /M OOo$S37 SEE INSTRUCTIONS NUMBER ON REVERSE SIDE I t t t ITEM A. USE TN!S DATA 9(ET TO RECOW IWGMTION AS REGJ1 RED IN: (OECK APPYt0PRIATE BOX 80t wetCN INF0lMATIOe TH1$ DATA 9(ET ilEPR

1. SECTIGI II, ITEM '4-E.

GlotAOefs OfSO4ARGE teTION (PAGE 55) CRITICAL X

2. SECTION !!, ITEM 6. PRIORITY POLLUTETS IN SUNACE 2T5 O!$ CME (PAGE 37)

X 3. B. BELDW: G!TICAL mTUIALS (TAILE TV) IN SURFAQ *TER DISOtARGE (PAGE 33) POLLUTANTS e NAZAR00US SU857ANCES 8. LIST ANY CRITICAL MATERIAL (TABLE IV PAGE 6) NOT ADORESSED IN SECTION !! ITN $ 8RIORITY NOT m! CABLE PQ.LUT4(TS WelCM W CD8 CR HAVE REASON fn BELIEVE TO BE PRESENT IN T)( DISOdRGE. SE IP4 REVERSE $1DE OF THIS PAGE FOR FUPMR DIRECTIO6. Ot$ CHARGE X mtCAaLE (SEE BELDd) s A. N4( OF CRITICAL mTERIAL Ot Mt!ORITY POLLUTANT g, ;, 9 g g g y 5"a2 " ' " ~ * " ~

yc=5 AvEmE CocEmAfi= S=E Tm; a CF mVSES u

i i 2 C. MAxte COCENTRATION #0 MASS ,m CDE A., N#C OF CRITICAL MATERIAL Gt Pft!ORITY P0QUTANT g g g g g g g g

'f$ 8 es B.

AVERAGE COCENTRATION: $4fLE TYPE; # OF ANALYSES l l l l,l l l g 3 C. mx!PtM CDC(MATIOI Arc MS$ L881T CODE mti CCE a r i I.I t t t y I t t t,e t t t (_j A. NMC OF O!TICAL ' MATERIAL OR PR!3!N POLWTANT ~ UNITS CODE g l l t l l l l l g ugf 3 m!T CcmE Sn M 1 TYPE # M ANALYSES gg, y S. AVERAGE CONCENTRATlW SMPLE TYPE; l' 0F ANALYSES l l l l,l l l l LJ t_.J -S L8S/ DAY 2 W T CODE mlT CGDE

c. mxtric CacENTRATION AfC MSS g,,,,g,

,, y y. p g,e g I e y ,4 KG/OAY ~ ~ NAPE & CRITICAL MATERIAL,0R PRIORITY POLLUTANT l l l' l l l I l a A. 5. AVERAGE CDPC(TRATION; $49LE TYPE; # OF AMLYSES mli CIDE SMFL1 TYPE A & NtALYSES g l l l,3 g ) l Lj t _j r,, L7t!T CCEE LPelf COE 2 C. MAXM.M C3@tTRATION APO MSS ,,,,,g ,,, y 3, g g,3 g I e (,,J SAMPLE TYPE g A. NMC CF CRITICAL MTDIAL OR PRIORITY POLWTANT 1 GRAS l l g g g g g l I # SES 2 24 HR. COMP 8. AVERVE CONCENTRATIOM; $49LE TYPE; # OF ANALYSES g g l [,g l l l g t t f f,f f i f U t f f 1,I f f f A. N#C & CRITICAL MTERIAL CR PRIC3t!TY PRLUTANT j g g g g g l l g B. AVERAGE COCUlTRATION; S#fLE TYPE; I & ANALYSES g g g g,l l l l 2 CODE, , el CODE C. WtitM CorCC(RATION A?O MASS

s. NA,C, o TicAL -oiAL OR P io.iu,muTANr E

Valf Cf4E S#fLE TYPE 8 0F AMLYSES f* 8. AVERAGE CONCEFRAT!?s; $#*LE TYPE; # OF ANALYSES l l l [,[ l l l U y i 3 WII E mlT COM, C. WMN COCENMtATION NO 453 t,_y (_j A. NArt OF CRITICAL f'ATERIAL OR MICRITY Pott'lTANT l l g g l [ g,

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4 MI0005827 Section2, Item 2(g) MATERIAL SAFETY DATA SHEET Material: Sodium Hydroxide, 50% solution

== Description:== Viscous water white liquid Formula: Na0H Physical Data Mol. Wt.: 40.01 d: 1.52 mp: 53*F (approx.) vap.-press: 1.5 mmHg at 20*C bp: 293 F (approx.) Toxic Rating a. Acute Local Irritant: Severe toxicity Ingestion: Severe toxicity Inhalation: Moderate toxicity b. Chronic Local Irritant: Moderate toxicity Severe toxicity means that a single exposure lasting seconds or minutes causes injury to skin or mucous membranes of sufficient severity to threaten life or to cause permanent physical impairment or disfigurement. Moderate toxicity means that a single exposure lasting seconds or minutes or hours can cause moderate effects on the skin or mucous membranes. D. C. Cook Plant use: to neutralize sulfuric acid, demineralizer resin regenerant solution, prior to discharge. Chemical reaction upon mixing produces a pH neutral, dilute solution of sodium sulfate, which is discharged to the absorption pond. 1 Ref: Sax, N. Irving. 1968. Dangerous Properties of Industrial Materials. Van Nostrand Reinhold Company.

MI0005827 Section 2, Item 2(g) MATERIAL SAFETY DATA SHEET Material: Sulfuric Acid, 92-96% solution

== Description:== Colorless, oily liquid Formula: H 50g 2 Physical Data Mol. Wt.: 98.08 d: 1.834 mp: 10.49'C vap. press: 1 mm at 145.8'C bp: 330 C Toxic Rating a. Acute Local Irritant: Severe toxicity Ingestion: Severe toxicity -Inhalation: Severe toxicity Severe toxicity means that a single exposure lasting seconds or minutes causes injury to skin or mucous membranes of sufficient severity to threaten life or to cause permanent physical impairment or disfigurement. b. Chronic Local Irritant: Moderate toxicity Inhalation: Moderate toxicity Moderate toxicity means that a single exposure lasting seconds or minutes or hours can cause moderate effects on the skin or mucous membranes. D. C. Cook Plant use: to neutralize sodium hydroxide, demineralizer resin regenerant solution', prior to discharge. Chemical reaction upon mixing produces a pH neutral, dilute solution of sodium sulfate, which is discharged to the absorption pond. Ref: Sax, N. Irving. 1968. Dangerous Properties of Industrial Materials. Van Nostrand Reinhold Company.

SECTION 11 PERMIT NOOO ND NUMBER 7 8h"afvVn"sE!8E8 ORFALL MMER ,o,0,6, ITEM A. ED mfi - Di - .N,W, ( 5,6 g,sa m ioi6i, m io i s iS i, wct t.1,9 i W i i i 1 - ue - -a'- - ,s,a ",,, r,4,2,v, .4.s.s.o.a.. e.o,", o, wr C. CD YOU DisonWIGE SEA 50MLLYl (IF ML CDNTIME TO E) YES 8 ggggggg LOCATION D. IF YES, List DISCHUlGE PERIODE NA re. / oaY Po. / mv SCHEDIAE W W TH40ume a t i i e a e FLQW l t I W THODI I I i f i ! CATE I I f f 1 l THIOLDt t I I I f I WASTEWATER g g,j,,, g,f yy gg,g* TYPE COOf E. l.A @ APPLICATION RATE NA i i i. U i i i. t; e i i.ia Om 1 CONTACT tl M5MAM TYPE M F. TYPE OF MSTDt4TER DISOWIGE Q U U LJ U U 2 NONCONTACT G. DISOWIGE SOEDULE (YTMLY AVEMGE) epsjyy g $,4 i Day /vEMt 13 4 ICI COOLING DISOtIRGE FLDi RATE ggg. EXfMD EM MI IeI ei3gI i 5" 3 PROCESS H. gg a 4 SANITARY 'O#'8'3' a mi'Y atate s SToRuwnrER I I UNIT CODE ,gne,, g ,, g ,Og,,o,3glg 1 MGY

3. M Pux!M DischnaGE FLOW RATE TO BE Aun(RIZED IN PEm!T.

J. pax!M DESIGt D!$CHWIGE FLDi RATE. d 5I f f I PO DE5!GN i t I i I*I A. DD YOU USE MATER TREATPENT GIT!vES TO TREAT EtJt DISOWir47 (IF PC, CONTIME TO ITEM N YES W ITEM IESE ElT!WS. = - - -iT-0F T 2 WATER THEATMENT NA ADDITIVES C. PWE APC A[11RESS OF P9NEACTLRERS OF MSE @lTIVES. UNITS CODE 1 Mg/l 2 Ug/l g MINIM tmlis AVERAGE LNIT5 MAxle WITS D. EXPECTED D! Sot 4EE CDCDiDIATION & 61TIVES. NQ m-m- m e t t i L_I AIO!T!YE P64PE e i e t y ;e e i e r y; e ADDITIVE PtAPE I f f I i LJJ' ' ' ' ' L J;e i e ' I L._J t_j j i MIT!YE - , e r i y g__j ;,,,, g E. 00 YOU TREAT M DISOWIGE TO RDO4 GlTivt37 NA vt3 ao F. tesi 13 THE ROTNAL EFFICIENCY APC DISDWICE FREGOCY7 NA gRDovat Pes./mv navs/w. WITINE Pearf I I I l _J J U GlTIVE P6ert i r i W U GtTIVE Peart I ' 8 W U G. A$ AN ATTAOfENT TO THIS APPLICATICN F830 VIDE SPECIFIC Mart %LIAN Gt A2ATIC T0xtCCUr.lCAL CATA Ot REFERENCE WHICH ARE AVAlt.ABLI INTIOe De M RATE OF DEGRADATIOe CF T)E PR00LETS FOR EA04 AiolTIVE. NA 31

o SECTION 11 PERMIT MICOOS D7 SEE INSTRUCTIONS NUMBER ON REVERSE SIDE r W /41.flM G OrD 6: i i ITEM a- - - ~ = = 'un= = =EDi - D40tAH NIS OUTTALL 40 SIC CCe( , s,a, n,,, r,4, e, v,, w,a,r, e, a,,9,9, i, i, B. PROCESS SOEDIAI (YEN'LY AVEMGE) g3, t) tnt Ib I biIt gyg g C. Pa0 CESS wust roow urE ,S,,2,7,9,* T PROCESS TOTA YEuit, STREAMS @bb b g \\9 314 FLOld DAIA CAfLY Mt w i ' ' ' 'O0'O'3f L4d CONTRIBUTING TO cArLy max Mat i 1 ' f ,O r e tOhib ' b o,$#( D. n oCE u mooutncN a rE NA

"VO t

A. PesPE OF P40 CESS CDNTRIBUT!PC 70 DE DISQWGE Twee Tw S OuTTaLL 4e SIC Cart I ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' ' PfCCESS SOE3A.E (YE#tLY Am) ggy,,, gyg g my N +n a TOTA YENILY ' I ' I I I I I I ' U [8" UNITS C00f DA!LY MINIMft ' ' ' I I I I ' ' ' Po DS 0"I'* '"*I"#' ' ' ' ' ' ' ' ' ' ' U 2 CALLONS D. PROCESS PICCUCTION RATE WITS /TIPE I I l ' ' ' ' I I L. V U YARDS NAPE OF P40 CESS CDNTRIBUT!PC TO DE DISOWGE A. Twee THIS OUTFALL NO $!C CODE NA i ' ' ' ' ' ' ' ' ' ' ' ' ' '- ' ' ' ' ' 3. Pfl0 CESS SOEDIAI (YEARLY AVERAGE) ggy g g, ggyg/yggg g i t h GD C. Pm0 CESS wttrE Flow RATE 4H m 7 GPD TOTA YmY l ' ' ' ' ' ' ' ' ' L! DAILY MINIMft I I I I I I I ' ' ' Dally MA.XtPtst I ' l ' ' ' ' I I 'U D. PROCESS PROQJCT!CN RATE _ TIM E b~ g,,, ~g e e t t . 1 HOUR. A. PdPE & PROCESS CDNTR18UTIPG TO THE DINGE TWCthf N!S OUfTALL #0 Sic CODE NA i i e i ' ' -1 3 WEEK

8. PIOCESS SOEDAE (NY AM) -

,cupdDAY I f ' MYS/ YEAR I I ' ' 4 MONTH my C. PROCESS VXJPE FLO# RATE

U N TOTA YEARtf

' ' ' ' ' ' ' ' ' ' b-I 8' ga DAILY MIN!Ptst I ' I f ' ' ' ' ' ' U ggty gygp, i t' f ' ', ' ' ' l U D. P50 CESS PSDDLETION RATE Lpe!TS TIPE I f f f i ' f f ' U A. Pe4PE OF Pf0 CESS CDP (TRIBUT!PC TO T)E DISOtARGE D@0U[H Twi$ OUTFALL #O SIC CCIE g I ' ' ' I ' I I I,,,,,,,,,, B. PROCESS 504D11 (YEARLY ASAGE) mdpY f f f D4YVYEMt I ' ' ' gg C. PIOCESS WLtJE FLDw RATE m!T C2 vo TOTA YMY ' ' ' ' ' ' ' ' ' ' U DA!LY MINIMLPt f I E I I I ' ' ' ' CAlLY 7%XI'tN ' I f ' ' ' ' ' ' ' U D. P50 CESS PRCCLCT!ON RATE WITS / Tl?E ,, i t i f f I t L_ V L J 5

SECTION 11 PERuir MI 000 Sb7 SEEINSTRUCTIONS NUMBER ON REVERSE SIDE ORLMG i d, c,E, ITEM

== ~ ~> ~ '" a-GIOLFOeATwEA$.tIF 'O. CONTINUE TO ITEM *S= ro - - ) ygg .g 8. NAS A HYDROGEDLOGICAL SitcY OR ITS EQUtv4 LENT SEEN PEW 0fMD Gt IS MRE SLFFICIENT CARENT HY:FIOGELY,1 CAL IPF0fMATION AVAILABLE A4 REQu RED (Y EndTER RESOLplCES YES Pc 1 C09ti$$!0N PMT d GROUPOdTER Elta.E OF ALGusT 114, l.iau N.ui.lm/ (PEE d) 700 GR0uh0 WATER THis DIST!PG OR PROPOSG DISCHMGE IF YES ATTAO4 A COPY OF THE REPUtT. OlSCHARGE C. ARE YOU 8 TUC #4 E)tENTION FR0t $dritTT!*G A HYOP0 GEOLOGICAL REMRT tJOER INFORMATM RULE R. ( ) (PEE f) OR FMPt ca0LionA 4 PostTCRIPC D [RE**ENT5 YES ?O Lti ER WLA.E R. (5) (PEE I47) y M PART rites. IF ATTACw 00CPOTS ND EXPLRdTION TO D60s5TRATE THAT Vout DISOtWIGE icta.D QUALIFY FGt A3 r> E'FY f 0fi. D. ME YOU REQLESTI'G A VARIANCE FRCM Q D.M (PAGE ) ("OCEGRADATIGI) 0F b M =ATER RE501 ACES C394155!ON PART l.2 GROL70 EATER Rt1ES. IF YES, ATTAO4 SUCH YES m DOCP'ENTS AS NECESSARY TO TRA M NEgD FOR A VARfANg IN TEY5 0F M l CRITERIA $PECIFIED IN RLA.E 'O PEE g) OF ikE PART U %A13. k E. IST L OelCAL SLBSTAKES WHIOf APE TN PeJCHIGAN'S CRITICAL PW RfALS REGISTER TAR.E IV EE ) AND/OR U.S. EPA'S PR!Gt!TY PGLUTANT LIST TABLE V (PEE ) OR ANY CTM1t SLBSTAfCE5 @ por m! CARE /EIEVG AEENT nellCH ARE Gt MAY BECOPE !PUURICUS TO M ESIONATED USES OF TM GI0tf0dTElt Gt TO M PUBLIC *(ALTH THAT ME DISCHMGED OR EXPECTD TO PE DISCHMGED TO Tif GIOLDOdTEltJY THt$ FACILITY. EST!*TE THE Flp.4L EFFLUENT CONCENTRATIO4 AfC RECDID ALI. DATA IN 17179 / W SECTIOs il IN Thl$ BOCl4.ET. M APPLICANT MAY BE REQJIRED TD 00 A3)lTIONAL *STE AMLYSES. PRESDT, DATA PROVIDED IN ITEM 7 . A. DISOWIGE CHARACTERISTICS CONCENTRATION LNITS CODE # AMLYSES SArft.1 TYP ITEM ~ 5 '2'

cc0 (o(MICAL 0xYGEN tewc)

I f ' If f I I I I i I.I I I I d.J (_LJ (_)

TOC (TUTAL ORGANIC CARBON) kb3 b- !

TE En C ARAC- ._, A N,,ROG, (A,,) , f, I., ,, I,, l..,,, I ef,, o TCISTICS

TcTA SUSFE'oc s6tTDs I ' I I l ' ' ' ' ' ' I 8

LJ f f I L_J I e UNf7S CODE TOTAL P>c5PICRU5 (AS P) I f 'l i =1 1 -t i I f f f.I I f f f f y 1 M /1 ~ , df 9 ' ' ' ' - ' ' ' ' ' ' e' . dI ' ' L-J 2 Ug / l. TcTAL REstD;AL otDRINE_ 3 COUNTS / I ' ' ' ' ' ' ' ' ' '=8 l I.3 Diss0LVG CMEN MIN t- ! 4 S U-

g I I i. U s e f.y af f

f y S F 6 L8S/ DAY FECAL COL! FORM 8ACTERIA ' ' I I ' ' l bI ' ' ' U

TDfERAftPE (SLMR)

' ' d*Ld ' ' '- L-J L.!J U

TEVE;tATLFE (w!NTER)

' ' '* U I ' '. L-J L. J 8. OTHER MSTEWATER OdRACTERISTICS ,0,I: L,1,6,R,E,A,S,E, g,y g 9, g _j $'.UP(( l f f f f f f f I f f f I f f 9.I f f I I f f n.I f f I Q l i f W TYPE i f I f f i f f f I f 1 i i f I.I l l l l I I I.I f f I C l l ! U 2 23 HOUR y,,, y COMPOSITC 1 I f I f f f f f I i 1 i f f f.I f f f i f I f,f f f f L.J l f i U f f f I t f f f f f f f I f f f.t i l f f f I f.t f f 1 U f f I W l f f f f f f f f i I I I f f f.I f f 1 I l f f.I f I I [_,,) I f f U See attached sheets for data. I 7

4/+/rs REeeff TO: 1 Laboratory Services Division Porti West Two I 5380 Campbells Run Road Cliff Mine Road ) Pittsburgh, PA 15205 Pittsburgh, PA 15275 412-7es-10e0 j LAB ANALYSIS REPORT CLIDIT llAIE: IIIBIAlls & MICHIGAll ELECTRIC CD. IlUS CL1DIT 110: 010904 AIORUS: P. D. BOX 60 l FORTli4YlE, Ill 46001 VDIDOR110: j REPORT MTE: 03/13/85 WORK OR E R 110: 55830 ATTDITI0ll IIt.10101 HulilEY MTE RECEIVED: 03/07/85 SAIFLE IDDITIFICATI0ll NUSSAIFLE110 RESULTS tillITS EUME PLAllT 03/06 040846ft 15030305 W030 Aneonie (II) 74 ag/l W050 300, 5-day (02) 36 ag/l 5100 Carbon orgenic (C) 107 ag/l W120 COB (02) 160 mg/l 1610 Solids, suspended at 103 C 11 ag/l SDiME PLAlli - liRAB 03/05 01-1100 15030306 M32 Fuel Califors - 1991 1100 col /100e1 SDiAE PLAlli - GRAS 03/05 02-1700 15030307 M32 Fecel Colifors - IFil > /= 2400 col /100el SEWAE PLAlli - GRAS 03/05 43-2300 15030308 M32 Fecal Califors - IFII > /= 2400 col /100e1 SDiAGE PLAlli - GRAB 03/06 44-0500 15030309

32 Fecel Colifors - 1991

> /= 2400 col /100ml COMRDITS: Reviewed and Approved hs JIC h A Hallibu ton Company CLIENT ORIGINAL . -... - ~. -... 1

l. SECTION 11 PERMIT M O W M-SEE INSTRUCTIONS NUMBER ON REVERSE SIDE 1TF41 218 ,O,og, ITEM

m. POf USE O!SotARGERS 28M. PRGNGL brECTED VAL 2S FGt fM QUANTITATIVE 40=== i-= A M

QUALITATIVE IWGMATION REQUEsfED SC.Jr. A. ($ THIS FACILITY A Mt?tARY trCUSTlY? OICFOt T3 TAM 1. TA PVE @ tit 'O, f4 TO E) IfF vt3, P4 TO 94 YES PC PRIORITY B. IslCATE TYPE OP P,e: MARY treuSTRY AS LISta IN wtE IA Put d. W'8 E "f

r.

i Tr i i ci iPie,4. POLLUTAN TS ANO C. DcES THl3 CUTFM DISOWGE CONTAIR ANY P8IESS MSTDeATER? fit e, G3 70 E) (f F TES, GO To 0) YES C INF;RMATION D. !@lCATE **lCH GdMS FRACTIONS MUST BE TESU FOR. (REFER TO TABLE IA Pv4 31) VOLATILE tcIE! FGt EAot GdMS FRACTION OECKED,EACH SPECIFIC ORGANIC TCXIC POLLUTANT WIThlN SUMACE EAQ4 FRACTION rMI SE ANALY2ED FGt (SEE TA9LE IIA PF4 'Q. IN A001T!ON. ALL 8 RIP'AdtY BASE / NEUTRAL WhTER trouSTRY APPLICANTS WITM A P90 CESS WASTEHATER DISOWGE ML* PROVIDE QuANTITAT!vt DeSCHARGE " I* ACID Opply RECGt0 h DATA ON FGM5 PROVIDED (ITDI 7) IN THl$ 800aLET. (CONT!mE WITH E-E BELDr) PESTICIDE E. [F M $$ FACE HATER DISCHARGE APPLIC#dT (PRIMARY OR SECOCARY IPOJSTRY), REGAAD.ESS NOT APPLICABLE /8ELIEVE!J ABSENT OF 14 TrPE CF DISOMGE, MOWS OR HAS REASON TO BELIEVE THAT ANY PC*1UTANT LISTED IN TABLE IIA AFC JVA PAGES Bl t$ DISOtARGED FROt ANY GJTFAL1,TM GMTITATIVE 215I SE PROVIDED. RECDRD ALL DATA ON FOMS PROVIDED (ITD1 D IN THis 800ktET. g F. IF ANY $@ FACE HATER DisotARGE APPLICANT (PRIMARY CR SECONDARY INDUSTRY), REGARDt.ESS OF TrPE OF DISOAvi, Cots CR HAS REA3ON TO 8CLIEVE ANY POLLUTANTS LISTED IN NOT APPLICABLE /8ELIEVED ABSENT TABLE VA Pr.E M ARE DISCHAEED FRrPt ANY OUT8ALL THE APPLICANT "'W DESCRIEE REASONS FON T)( PQLLUTANT BEIPG PRESENT NO PROVICE ANY AVAILA8LE QUANTITATIVE DATA. RECORD ALL CATA CN FGNS PROVIDED (ITD1 N IN THIS 80067. PRESENT/ DATA ($ ATTAOED -G. ALL $$ FACE nATER DISOWGE APPL! CANTS (PRIMARY #0 SECONDARY IPOUSTRIES) Dee: ~ b PCT APPLICABLE /8ELIEWD ABSENT ~ OR M4AFACTtRES 2, 31, - TRIOLOR$ TEN 0xY" ACETIC ACID ( ,4 TA!OLOROPMDCXY PROPANQtC ACID ($!LVEx, 2, 4, 5,2, 31, 5-T); , 4, ) TRIQt.CR0r+ aoxY .rP)- 7 ETHYL z, 2-DIO(OROPROP 0NATE (ER80N1; 0,- DiaETHYL @(4, 44, 9-(TRIOLDROPHENYL) PtCSPFOPOTHICAT{;(R0re.EL)T 4, b-TRIOtCR&4NDL (TCP)J OR HEXAOt.OROPHDE (> cpi (ALL DATA FOR T)( ABOW PtJST BE GU4.AATED USING STWOARD ANALYTICAL CALIBRATION PROCCLRES) OR CCWS OR HAS PFASON TO BELIEW THAT TCDD !$ OR MAY BE PRESENT IN T)(IR DISOtARGE. M,,5I REPCRT r1]ALITAfivE DATA, GDERATED te4tOJ UE SCIEENING PROCGtRE NOT PRESDiT/ DATA IS ATTAOED CAuBRATED mlTH AMLYTICAL STNCARDS, FOR 2, ), /, - TETRAO(CR00!8EN2D-P-DIOXIN (TCO). RECORD ALL DATA CN F0fMS PROVIDED (ITDt ) IN THIS B004.ET. J. IF T)E SL.stFACE MATER DISOMGE APPLICANT xmWS Ot HAS REASON 70 BELIEW THAT 8!0LOGICA($ DISCHAPGES OR CN A RECEIVIPG MATER IN RELATION TO A DISONGE, PROVICE T0x! CITY TESTS WEPE MADE IN THE LAST T)#EE (3) YEARS ON ANY OF T>E WT MIN APPLICANT + THIS INFGRMT!34 AS #8 ATTAOf E..T TO THIS APPLICATICN. APPLICA8(E/SEE ATTAO(D IF A C3dTRACT LABORATORY OR CONStLT!?G FIRM PERFGNED ANY OF T){ 40YSES REQUIRED (. BY THis AFPLICATJCm, PROVICE Tid NAPE #C ADCPESS OF EACH LABORATORY OR FifM 40 g NOT APPLICABLE / THE #6ALYSES PERF0PitD AS AN ATTAOffMT OF THIS APPLICATION. APPLICA8LE/SEE ATTAOCD L. ID YOU DISONGE ## OT)(A TCx!C CR IlotFI ICAL St2 STANCES NOT LISTD IN TABLES IV PM.E 6 WD IIA T590744 VA PVES '4 IF YES, TV N IDENT!'Y TW W M IC88LI OetCAL SLSST#dCES Ne3 EST! MATE THE FINAL EFFu1NT Ca(ENTRATIONS. StJNif THIS IVCrhATIOff AS #4 ATTACetOT TO THl1 APPLICATICn. APPLICABLE /SEE ATTAOED i 9

_= .I. SECTION 11 PERMIT l 'SEE INSTRUCTIONS NUMBER /hI00O S8M ON REVERSE SIDE EU E ,O, O r bt ITEM A. us TMis DATA SEET TO RECO2 twGDuf!aN As REastRG IN: (OECK Arm 0PRIATE Box POR welch INPODWTION THIS DATA 9(ET 7 NA L sECr:0 ii. i= *== =4 r-'oa (Far S CRITICAL

2. SECT!Gs II. Im 6. PRfCRITY pouufmTS IN SUFACE MTER DISCMrit (MGE 57)

MATERIALS 3.

8. BELDs: CRITICAL MTDfALS (TARE IV) IN SWIFACE HATER Dt50#RGE (PAGE E)

POLLUTANTS e NAZAROOUS SUBSTANCES 3. LIST ANY CRITICAL MATERfAL (TARI IV PAGE 6) NOT ADFESSED IN SECTION !! [TD9 6 84!0RITYQ ,gy appgggggy PEUT ##5 delCH vou cos OR HAVE #EASON fn BELIEVE TO BE PRESDfT IN DE DISOARGE. SEE M REW.RSE $!DE OF THIS PAGE FGt FWR DIRECTICMS. DISCHARGE APPLICARE (stE m) g NAPE OF CRITICAL MATG!AL Ot PRIGilTY POLLIKANT A. g,, g y g g g j.-

y" 5'** "'"

8 * ** '5"

s. AvuAGE CmCENrRArim; smE nPE; # OF =YsEs g

3 C. Mxte CONCENTRATION AfC MSS

I M,

,., mi CODE A. Mare OF CRIT! CAL MTERIAL OR PR!m!TY POLLUTApff g g,, g,,, C E TYPE I OF AMLYSES ce B. AVERAGE CmCENTRATIDs; SAME TYPE; # OF APWLYSES l l l l,l l l g 2 C. Mx!PtM CGCENTRATION APO MAS $ , UNIT COE, mIT COT i i i ,,t gy ,,,,,, e e g_j UNITS CODE .a A. feart OF CRITICAL MATUlAL OR 'PRlGtlTY POLDRANT t l l l l l l l 1 Mg/l m!T CM SAP'Pli DPE # M #sALYSES y

5. AVERAGE CONCENTRATION: SAMPLE TYPE; f 0F AMLYSES l l g l,l l l l g g

3 L8S/ DAY 2 Wir CM unti CCDE C. mx!ttM COCENTRAt!ON APO MS$ 4 KG/ DAY .g ,,g -g ,g Lg, g,, q t t y .J A. NAME & CRITICA MATER!AL OR PRIORITY, POL 1UTANT l l l g g g g g 5 5. AVERAGE CDCDURAfl0N; SAffLE TYPE; # & AMLYSES g g g g,g g g g 2 C. MAxistM CofCCITRATION APO MS$ SAMPLE TYPE g A. NAPE & CRITICAL MTERIAL OR PRIORITY POLURANT 1 GRAS g ; y 9 g g g, 2 24 HR. COMP B. AVERAriE CONCENTRAT! Ort; SAtftf TYPE; # 0F AMLYSES CM SAMPLE TYPE OF AMLYSE5 [ g g l,g l l l

c. = t= =C=-im = -15

' Lcf',,,,.,,,, =,' =,

g A. NAME W CRITICAL MATERIAL OR PRIGt!TY POLLUTANT g g g g g g g g 5. AVERAGE CGCENTRATION; SAffLE TYPE; I 0F ANALYSES PE OF YSES g g g g g g g g 2 g, gg.tM CarCDURATICN APO MS$ ,m! CODE, , mi Com j t. NAfE OF OITICAL MATERIAL OR PRIORITY Pat.LUTANT i f f I I f f l g thit C M S#eu TYPE 7 8. AvERKE CorvCDnRAT!0N; $ AMPLE UPE; # OF MALYSES l l g I.! l I f U g,,_j s OF A,ML,fSES t 4 C. MARLU C0rCENTRATION AtO MASS Lhli COM J*lT U.M i,,,,,,, t L,,,j [,,,,,,,, g .J A. NINE OF ClttTICAL faATERIAL OR PRIGilTY Phi #mT l-1 I f f I f f1 II

# ^**

8. A4*El CDCD:TRATION; SArPLE UPE; # OF AMLYSES I f l_ ]. I f f I [_.J t_j i,, 2

l T C;'CE J.i T a C.

MAXLv CC'CE.NTRATION Arc Mss t t t ,.I f , i L_I t r r i.I e, # L.] 6 ACCITIOML PAGES & THIS ITEM I AAE ATTAcc FGt X REST OF M CRITICA4. O vEs MTm!ALs Arc /OR Prim:TY nsAurs *E2nRc To as av0RTc. Ji1iO a 1 'f I 11

SECTION ll gl,T E 000 ESD R ' 2A'NUv,TR SN S gS QITFM.L M iS oifi i A. LOCATION OF DISO4WIGE , N, N, ( i hi% ( EGS i O, $ 1, M i, b, h, ME / t 9,% O S. NME lECEIVIPC WTUt LtE. GROUOem W M & NG ,L,A,t,E, iu, r i c, H, f,G, A,4 ,,,,,i wAT9t C. Q0 vou D150eNIGE SEA 50Peatty/ LIF 90, CDMTIME TO E) US W DMAM LEA D. IF YES, LIST DISCHWtif PDt!ODS NA ao / day Po. / D=Y W f I I Dft0 UGH I, I e,, e FLOW L,,,,j,_j t , 8 n#ouas W W CATE WASTEWATER i 7u e'"'l7 u [] m TYPE CODE E. L#C MICAN RATE NA u '" *' u e i oh u u u u u f CONTACT F. TYPE OF MSTDeTER DISOMRGE COOuNa '2 NONCONTACT G, ogsOWIGE SOEDULE (YENLY AVEAME) w3Y iNiAi of. ,, N A, COOLING IJi CDIE 3 PROCESS H. DISCHNIGE FIDf RATE 4 SANITARY SASIS t AVERAUc ANNUAL. RAIN NLL FCE l'.NEAnLY DAILY MINIM M i i i f f I I .0i 5 STORMWATER 'OO'#'A' LS8 UNIT CODE I 8" IO NE 14 HE STtE" fee DA'W 6*M D"I'Y *N , 0,,, 9,,, 2, g= , Mov i. ,E,.x Oi,C - E,t RG 1 m - i iNFemiT. 2 MOD J. max!MM DEstos DisChmRGE FLDi RATE. bg CEstGN I I I I I I f , I 3 CPO A. DO YOU U5E MATER TREATPENT WIT [WS 10 TREAT 100t DISOARrd? (!F ND, CfWTINLE TO ITEP4 3) YES PO = ITEM rag --i-2 WATER TREATMENT NA ADDITIVES C. NME APO ADDRESS OF P9MFACTUIDts CF DESE ADDITIVES. UNITS CODE 1 Mg/l 2 Ug/l NA D. DMCTED DISCHARGE COCENTRATION & A[DIT!YES. NA E ^~

E E

~~ C i t I n L., ] WIT!VE NME i t i,, t,,,,,j ; e a e n (_,,) ; e AIDITIVE fePE t e e t 1 U J' ' ' ' ' L JJ 8 ' ' ' i LI 6171W M gj;,,,,, g,,j ;,,,,, (,_,,y E. DO YOLI TREAT DE DISOMRGE 10 flEMNE 6tTIW57 NA 0 Us Fi WST IS THE RDc/AL EFFICIDCY #c DISO9A2 FREFAOCY? N A ! Retyvg tes.fDAY DAYS /*. O!TIVE Pe4E I I I I I I U GITIVE NME I I I LL) 1I I t i i f I lJ ADDIT!vE NNE G. A1 AN ATTAOfENT TO THt$ APPLICATIO4 PED /t:E $PECIFIC MIAN CR A3ATIC YOXICOLrrilCAL DATA OR REFDtENCE idHIO4 ARE AVAILABLE NO INFONATIOf Os DE RATE & CEGRAD4TIOt & DE PR0[1ETS FOt EAOi ArolTIW. 31

SECTION 11 PERMIT IDf00038A7 NUMBER 7 SE INSTRUCTIONS 5 ON REVERSE S!DE muus iS io i li ITEM A. m or mxx$$ C0mRisurim to M Dr$0wCE ,N,, e t At 7, e i th iS 1 A 15 i i iMi Mi4tii/i i THtuuG4 THIS OUTTALL APO Sic CODE 3 ,N,A, ,N,A, .. PROCESS SoetE (YuRY AmAGE)

ogy,

,,yy, h ' 7 ' * ' {8 ' C. Pfl0 CESS Vouff Fl.0W RATE TOTA YDAY I f ' ' ' STREAMS MILY Mm!M i ' I I I ' ' 1 IOt 1 CONTRI8UTING A TO DAILY W I M l I 1 I I I*I II1 1 PROCESS Pf00UCTION MTE iNiAi

&O DISC RGE ti i t i t A.

NME OF P50 CESS (DN11t!BUTim 10 M DISOWtGE THOLDI THl$ OUTFALL APO SIC CCDE I f f f I l I I I i f I I f I I I I I f 8. PROCESS SCKDLLE (YEARLY AVERAGE) PCUts/ DAY l t I DAYS /vtAR I I f I C. 6 M % RAM OTA YEAAY I I I I ' ' I I I ' I t t I t t I f f I U ogity pimists, teNiTS CODE DAILY w t p I t t f 1 1 I I I I U 1 POUNOS 2 GALLONS D. Pfl0 CESS PROCUCTION RATE I 1 I i t t I t ! A. NME OF PROCESS CONTRIBUTIPG TO M DISOWIGE YARDS THIOUGH Df!S OUTFALL #O SIC COE I I I I I I I f 1 I f 1 I I I I I I ' I 8. Pfl0 CESS SOEDULE (YEARLY AVERAGE) g, gyg g g,,, m WII A d C. P90 CESS M FLOW RATE TOTAL YEA A Y I ' I I I I ' I I I U r I I ' ' ' I ' ' ' ' DA!LY MIN!Ptti DAILY PEX!Put I l I I I I I I I I L.- I b D. PROCESS PRODUCTION RATE 1 HOUR A. MME OF PROCESS CONTRIBUTING TO M DISCMAGE T410EH NIS 01TTAL.L WO SIC EOE 8. PROCESS SOOLE (YENILY AGAGE) 3 WEEK POURdDAY I i 1 DAYMYDR I I I i 4 MONTH e m!T COM TOTAL YEARLY I I ' I I ' I I ' I U 5 YEAR 8' C DAILY MIN!Ptit 1 I I I I I f f I I L] I ' I I I ' ' ' I I lI DAILY pmXI M tJet TS TIPE D. P90 CESS PICOLETION RATE

I t i t i t I t tJ A.

NME OF Pf0GS$ CONTRIBUT!?G TO M DISO%RCE T40LD4 THIS OUTTALL AND SIC CTE t t I t i i i f 1 I I ' ' ' I ' I I ' ' 8. P50 CESS SOEDLA.E (YEARLY AGAGE) mVDAY I I I DAYYYDR I I I I e WIT G g C. PROCESS M FLDW RATE TOTA YEAAY l l I I I I ' ' ' ' lJ Wt l I I I I I I I l l U gA[Ly MjNjpg), DA!LY P%XIPt.Pt i f I I ' l I ' ' I C LMITS / TIPE D. W S$ W ION RATE ,,,, g g,,, L,,,,,,y L.,,j j l 33

SECTION 11 PERMIT MIOOO SD7 NUMBER SEEINSTRUCTIONS ON REVERSE SIDE amt ma ,S,o,t, ITEM pIF ro, CONTIME To tTmse - - -= o'Re A-is - => YES Pc GRotht>ATERS 8. NAS A HYDROGE0 LOGICAL STUDY OR ITS EQUIVALENT BEEN PGFORPED OR IS MRE StFFICIENT QJRRENT HYDROGECLQGICAL IPFOINATION AVAILABLE AS REQUIRED Y T1w,ATER RESOURCES TES to CONISSION PART H GROOOdTG RULEg OF AIEUST 14,1% R. .uw (PME %) FOR GROUNOWATER THIS EXISTING OR PROPOSED DISOWGE. IF YES ATTAOI A COPY OF THE REPORT. g DISCHARGE C. ARE YOU # ! AN EXENPTIO4 FRm SLEMITTING A HYDR 0 GEOLOGICAL REPORT UPOER INFORMATION Ri1E R. (PAGE I6) OR FRG1 GROOOMTM PONITORIPG MREMENTS YES PC LFCER RULE R. (S) (PME 4 ) 0F TM PART H Rt1ES. IF YES ATTACH 00CutNTS #O EXPLNATION TO DE? TRATE THAT Yout DISCHARGE WAA.D QUALIFY FCR a.a AN EXEPPTf 0N. IN N ARE YOU REQtESTING A VARIANCE FROt RI&E 323.m (PAGE p)IF YES, ATTACH SUCH (toeceGRADAft0N) Or D. YES pc TM HATER RESOI.RCES CONIS$10N PART U GRottOdTER RULES. 00CLNENTS AS NECESSARY TO TE TM FOR A VARIANg IN TUNS OF TM CRITERIA SPECIFIED IN RLAI 0 (PAuE ) 0F THE PART H RULES. IST Ay, OEMICAL StBSTANCES *!CH ARE TN MICHIGAN'S CRITICAL MATER 1ALS REGISTER TABLE !Y E. '(PAGE Q) #C/OR U.S. EPA'S Mt!Ot!TY POLLUTANT LIST TABLE V (PAGE /).OR ANV OTER StBSTANCES NOT APPLICABLE / BELIEVED ABSENT

!CH ARE OR MAY BECOE IPULRIOUS TO TM DESIGNATED USES OF TM GiiOOOdTG OR TO TM PUBLIC HEALTH THAT ARE Ot$ CHARGED OR EXPECTED TO BE DISOWGED TO TM GROLFOdTER.BY THIS FACILITY. EST!MATF THE FINAL EFFLLENT CONCENTRATIO8 Ato RECORD E DATA IN ITEN / OF SECTION [I IN THIS B00PLET.

PRESENT, DATA PROVIDED IN ITm 7 TM APPLICANT MAY BE RE2JtRED TO DO A3)lTIChAL MASTE AMYSES. A. DISOMGE OWACTERISTICS CONCENTRATION Ot!TS CEE # AhALYSES 549tE TYPE ITEM 5 % (O ,m ome, _.) i.I ww a bJ ' ' TOC (TOTAL ORGANIC CARBON) WASTE AT R - #t0NIA NITROGEN (AS N) l I I Ie I I I I I I I I*I ! ! I b I I I U CHARAC-TERISTICS

TOTAL SUSPETED SOLICS I I I i I ' I i ' I I I.I

' I I lIJ ' ' I C I i 1, f I f I.I I f I di UNITS CODE TUTAL Pg:SPHORUS (AS P) i I I i 1 i L! 1 Mg/l b' L-I 2 Ug/l TOTAL RESIDUAL Oct!NE e 3 COUNTS, b' I I I I .I I I I I I I I I I ! I W 100 ml otSSQ.WD OMEN Mig 4,S. U. .g 1 I I,U ,,, y 3,, i y 5 F 6 LBS/ DAY I I I ' ' I I ' ' ' ' ' L.d FER R! FORM BACTG!A I ' I I-I I I I. L.I U

rePERATURE (Sitter) e
TEPPERATUR4i (dlNTER) 8 LJ I ' '. L!

L.- ! 8. OTHG WASTDdTER CHAPACTERISTICS

0, I, L, 1, ft, R # E,A,S,E, y gy y

SAMPLE I I I t I f f I I I t i i I t t.I t I 1 i f f I I I t i LI t t i U TYPE 1 GRA8 2 24 HOUR y,,, y COMPOSITE i t i t t t t t t t t i e i e t,i t I i e t i I.I i i 1 LJ t t i L] t t i i e i i i i e i i i i i s. i e i e i e i.: i i i LJ t i i L _J i e i e i t i .I I t 1 U I e i L_! t i i t i i e i e i i i i i e i. See attached sheets for data. 35

r i REMIT 70: RECEIVED

- - ~'*""*a NUS 5360 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 8

u CDFv3 ORAM APR 8 E.'5 .E .ENVIR OIG."EI!TAL ~ AFFAIRS 1-B LAB ANALYSIS REPORT CLIENTllAfE IllDIANA & MICHI6AN ELECTRIC CO. NUS CLIENT 110: 010904 I ABDitESS: P. O. 30X 60 FORT li4YlE, IN 46001 YDIDOR 110: 05411000 REPORT DATE: 04/03/85 WORK ORDER 110: 55830 AT1ENTIDII: Igt. Jolti HUGIC DATE RECEIVED: 03/13/95 SAMPLE IDOITIFICATIOli lluS SAlfLE 110 RESULTS IMITS o-STORillATER RU110FF 03/11 15030712 M140 Chrceive (Cr) < 0.01 ag/l M160 Copper (Cu) 0.01 ag/l 1190 Iron, total (Fe) 2.4 og/l M390 line (In) 0.27 ag/l 1032 Antonie as N (distillation) 9.9 og/l 9050 30D, 5-day (02) < 1.0 mg/l 1100 Corbon, o genic (C) 26.5 ogIl 11120 C00 (02) 21 og/1 1610 Solids, suspended at 103 C 39 og/l i l I B 8 RDITS: 't* Reviewed and Approved by: JIC $ A Hallitiurton Company CLIENT ORIGINAL { l

f SECTION 11 PERMIT g7 o oo gg 7 l SEE INSTRUCTIONS NUMBER l ON REVERSE SIDE (UIM.L fi1HR i$ioili / M OLLOWIM REQL4STED IWOft% TION A IRESSED EEL $@ FACE NATER DISCMAGERS. 2CIE IEW USE DISCMAGERS 23L PROVICL CTED VALES FOR TM QuMTITATIVE AND QUALITATIVE INF0ft% TION REQUESTED BELOW. A. ($ THl3 FACILITY A PRINRY l@uSTRY? (REFER TO TABLE !A PY4 $) YES PC (tF No, GO 70 E) (f F YES, GO TO B) PMIORITY B. INDICATE TYPE OF PRIPWty (POUSTRY AS LISTQ IN TABd IA PY4 $. POLLUTANTS kONTN Wi* CJ l Ib Ib b I Mib Ag C. DOES TH15 OUTFALL DISCMAGE CONTAIN ANY PROCESS WASTEWATER? fj ADOITIONAL INFORMATION D..l@lCATE W11CH GC/MS FRACTIONS ftJST BC TESTED Fm. (REFER TO TABLE IA PY4 (Q) VOLAT!d FCIE! FOR EAO4 GC/MS FRACTION OECKED,EACH SPEC 3FIC ORGANIC TOMC POLLUTANT WITHIN SURFACE EAO4 FRACTION [Sdf BE #4ALYZED FGt (SEE TABLE I!A PAGE L.2. IN AD0! TION, ALL PR!ldARY BASE / NEUTRAL WATER INDUSTRY APPLICANTS WITH A PROCESS WASTEWATER DISO9RGE tigI PROVIDE QUANTITATIVE g i N IN TAad IIIA N4 @. OISCHARGE ACID I ONLY RECDR3 ALL DATA ON F0Fets PROVIDED (ITEM 7) IN THIS B00417. (CONTIPAJE WITH E1 BElaw) PESTICIDE E. IF Ag S@ FACE WATER DISO9 AGE APPL! CANT (PRIMRY OR SECDOARY IPCUSTRY), RE'NSS h NOT APPLICABLE / BELIEVED ABSENT OF M TYPE OF DISodAGE, KNOWS OR MS REASON TO BELIEVE THAT ANY POLLUTANT LtSTED IN TABLE LIA APO IVA PAGES $$1 is DISOdRGED FROM ANV CUTFAu,TW QJANTITATIVE 2141 BE PROVIDED. RECORD ALL DATA ON F0ftts PROVIDED (ITEM 7) IN TH15 BC0KLET. ENT/MM !$ MM F. IF ANY $@ FACE WATER DISO9RGE APPLICANT (PRIP%RY OR SECDPCARY IPOUSTRY), REGARDLESS OF TYPE & dis E, MFCMS OR HAS REASON TO BELtEVE ANY POLLUTANTS LISTED IN NOT APPLICABLE / BELIEVED ABSENT I TA8d VA PV4 ARE DISCHAEED FRrN ANY OUTFALL TT AP8LICANT '$gI DESCRIBE i REASONS FOR T)E POLLUTANT BElm PRESENT #C PROVIDE ANY AVAILABLE QUANTITATIVE DATA. RECORD ALL DATA ON FGP15 PROVIDED (ITEM 7) IN THIS B00NLET. l G. ALL SWFACE NATER DISotARGE WPLICMTS (PRIMARY AND SECQOARY IPOUSTRIES) Mc: h NOT APPLICABLE / BELIEVED ABSENT OR MAtafACTWES 2, 4, - TRIOtm0 PHEN 0XY ACET! ACID (2, 4, 5-T); l, , 4, TRIO 1LOROPHENOXY PRTANOIC ACID ($1LVEX,, 4, $, TP) ETHYL 2, 2-DioiLOROPROPiCNATE (ERSON$'; 0, , 4, IRI NOxY DITTWitIP(,4, TRIOtDROPHENVL) PH20ROTHICATE (RothEL)J 4, kTRIOt.GIOP4 tot (TCP); Gt HEAAOLOROPM?E (HCP); (ALL DATA FOR THE ABOVE MUST BE GENERATED US!$ STNEARD AMLYTICAL CALIBRATION PROCEDLFES) OR CCWS OR HAS REASON TO BELtEVE THAT TCID 15 OR MAY BE PRESENT IN THEIR OtSOdRGE. NJ, REPORT r11ALITATIVE DATA, GENERATED M4tOJ A SCREENING PROCEDLPE PCT PRESENT/ DATA 15 ATTACHED ABRATED WITH ANALYTICAL ST40ARDS, FOR 2, 2, 8, - TETRAOt0RODIBEN20-P-010XIN TCDD). RECCRD ALL DATA m FmMS PROVIDED (ITEM ) IN THIS B00xLET. J. IF M SURFACE WATER DISCMPGE APPLICMT c(>S OR HAS REASON TO BELIEVE THAT @ PCT APPLICABLE 810 LOGICAL ToxlCITY TESTS WERE MADE IN THE LAST TWEE (3) YEARS ON #ff 0F THE f APPLICANT S DISOdRGES Gt CH A RECE! VIM HATER IN RELATION TO A DISOMRGE, PROVICE THIS INFORNATION AS AN ATTAOfENT TO THIS APPLICATION. APPLICABLE /SEEATTACHED K. IF A Cat. TRACT LABORATORY OR CONStLTI% FIEH PERFGP1ED ANY OF T4 #43YSES REQUIRED g roi APPLICABLE BY This APPLICATION, PROVIDE M NAME AND ADmESS OF EAOf L.ABORATmV OR FIRM NO M #dLYSES PERFORtfD AS AN ATTAOftNT OF THIS APPLICATION. APPLICABLE /SEE ATTACHED 00 Vou DISCHAPGE ANY OTHER T0x!C OR 14JURiop.h. Is vES, TVN IDENT!'Y T)f L. TAPLES [V PAGE Q No ilA T) Pour 4e VA Par 45 S. qEMICAL SLESTANCES NOT LISTED IN PCT APPLICA3d O(MICAL SLASTANCES NO ESTIMATE THE FINAL EFFLUENT CGdCENTRAfl0NS. SIBilf THl3 IWGt% TION AS AN ATTAOf1ENT TO THIS APPLICATION. APPLICABLE /SEE ATTAGED l 37

I = SECTION 11 PERMIT + NUMBER MI O00 SD7 SEE INSTRUCTIONS ON REVERSE SIDE = i wwma ,5,o,l, L ITEM ~ = A. USE THIS CATA SKET TO RECORD INFORMATION AS REQUIRED IN: (OECK APPROPRIATE BOX 80R peitCH INFORMATION THIS CATA SHEET REPRESENTS.) [ 7 r h

1. SECTION li, ITEM 4E. GR0ttodTER OtSo#GE INFOR'ATION (PAGE $5)

[ C"'IICA'

2. SECTim !I, ITDt 6. PRIORITY POU.UTANTS IN SGWACE MTS DisctwE (PAGE 37)

MATERIALS 3.

8. BELOW: CRITICAL MATERIALS (TABLE IV) IN SURFACE NATO DISCHARGE (PAGE 39) f TOXIC COLLUTANTS HAZARDOUS SUBSTANCES 8.

LIST ANY CRITICAL MATGIAL (TABLE IV PEE 6) NOT A:XRESSED IN SECTION !! ITEM fs eqgoggTy -m g P0l1UTANTS be4!CH YOU COs OR HAVE REASON TO BEi.lEVE TO BE PRESENT IN TE DISOWGE. SEE E IN REVERSE SIDE OF THIS PEE FOR FURMR DIRECT!CNS. e DISCHARGE APPLICABLE (SEE BO.0H) E .J A. MPT OF CRITICAL MATERIAL m PRIORITY POLLUTANT 5 ,, g, g g g g 8. AVERAGE CONCENTRATION; S#fLE TYPE; I 0F AMLYSES g g g g_g g 9 g I [ C. MAXI *U9 CONCENTRAT!CN NO MASS b A. N#T OF CRITICAL MATERIAL OR PR!m!TY POLLUTANT g g g g g g y g g 7 N 8. AVERAGE CmCENTRATION; SAMPLE TYPE; # W AMLYSES l l l l,l g g g = a t t i I f i e I t t j,t 1 1 l UNITS CODE -a A. N#'E OF CRITICAL MATERIAL OR PRIORITY POLWTANT 5 g g g g g g g g 3. AVERAGE CCPCENTRATION; SAMPLE TYPE; f 0F AMLYSES l g g g,g g g g j

==

= ,, t'r : C. - - - 55 E .a A. NAME & CRITICAL MATERIAL OR PRIORITY POLLUTANT l l l g l g g l s S. AVERAGE CotCINTRATION; $4fLE TYPE; # OF ANALYSES b g g g l,g 9 [ g C. MAX 1PU1 COPCENTRATION NO MASS SAMPLE TYPE g A. N#E U CRITICAL MATERIAL OR PRIORITY POLLUTANT g g [ g g g g g 2H COMP B. AVERAGE CONCD0RAtl0N; $#fLE TYPE; # OF ANALYSES l l [ l,l [ l g e C. MAXI *U* COPCENTRATION MO MASS IT CODE, mt CODE g A. PME OF CRITICAL MATERIAL OR PR!m!TY POLLUTANT g g g g g 3 l l g g g l ,l l l g

, N*

B.

AVERAGE COPCENTRATION: SANF1.E TYPE; # OF AMLYSES I C. MAXI'U1-CorCENTRATION APO MASS UNIT CODE th!T COCE i t I .I f f I y a f f f,t t I i [.__j K s y A. N#T OF CRITICAL MATERIAL OR PR!OPITY POLLUTANT l l t 1 I l. L_L g g WIT C44 SAPPLE TrPE # OF AtiALYSOJ 7 B. AVERME CmCENTRATION; SAMPLE TYE: # OF AMLYSES g g l I.I l l I LJ t.J e ii n ' C. MAXI *t.79 CCPCENTRATION NO MASS WIT CODE Wil 04E I I I I .I 1 f f (_.J t t i 1.t t t i U g j a A. MNE & CRITICAL MATERIAL OR PRg0p!TY POWJTANT t i l ! 1 1 W _ g WH T SES ge B. AvEPAGE CmCENTRATION; $#fLE TYM; # OF AMLYSES l i I I I f f f (__.] t_j i i e 2 WuCe mtT Cc0E l C. MAXl'U9 C0rCENmAT10N ArO MASS 1 i i t.i i i i l_J i e i i. i e i y AColTIOML PEES OF THIS ITD17 ARE ATTAOED FOR T>E REST OF DE CRITICAL C YES MAro !ALS A o 0R Prim TY m UTA TS RE R T o E E L l 30 } u m

SECTION 11 PERMIT MI 000 SU7 NUMBER F 82"#&"sE8E8 anwuw , s, o, o., ITEM A. <o== - Di- ,u, wi t. s wl t sa m. M >. =.o,c,3. o r a,9,w, 8. NME OF RECEIVING MTER (IE. GRotmdTG W NAPE OF $@ FACE , L, A, K, E I iMi i iC iH i i iG i A i Ali wats) i i i e i i C. YQu DISCMAGE SEAS 0esLLf f I No, Niu M E) OtSCHARGE a LOCATION D. IF YES, LIST OtsotsJird PERIODS NO./ DAY PC. / CAY e SCHEDULE e t ie i i TWlotDi L_.L_J t t s I FL OW ' ' t i f I~ fl@0 UGH I I I I I I l t t t t t f T'acine I f I t i I WASTEWATER gN,/te. ee,/ cay IN,/wg, TYPE CODE E. Lee MICAN RATE M Om; 1 1 I. U l i I. t__.) i i

1. L_J 1 CONTACT MSTBdTER TYPE CCCE F.

TYPE OF MSTDdTER DIS 0WIGE I (_,,,j l_J L_J L_1 L_.J l . DI EN MYAM) ocURS/ DAY l I4f day /ygjp i iM iA i 3 PROCESS H. DISOtARGE FU)# RATE mg7 mag t Ni e t l t I i W TOTAL YtApt,Y l I t I 4 SANITARY GAS 5: AvC3 A N NuAL g Ao6 alt. Fo R.

7. NEAE4.y 5 STORMWATER DAILY MINIS e e e i t e i eon i

i o,.,t/ i3,9, tp,; UNIT CODE IIN 10 Nf 14 HR STORM foe DAity M, CArLY t%xt e i, 1 MGY 1. M max!MLPt DISCHARGE FLI)f RATE TO BE AUDOtiZED IN PER9tT. AUNDRIZED I l i 10 I' IN' b l$ I 2 MG3 3 CPD J. 7%xte MSIGi DISCHWtGE FLOf RATE. NA oES:GN i i i i e i., i t; l A. DO YOU USE MATER TREAT *ENT A;X)lT!YES TO TREAT Y0lR DISOdRrE7 (IF NO, COPITINtf To fTEM 3) YES Po ITEM kSE GtT!WS. = 0F T 2 WATER TREAT;;ENT g A00lTIVES C. NAPE Are ADCRESS OF MM4EACTWERS OF THESE 6tTIVES. UNITS CODE 1 Mg/l 2 Ug/l MINIPtst m!TS AVERAGE WITS t%x!Ptst Lrtt TS D. DPECTED DISCHARCE CDCENTRAf t0N OF GtTIVES. M CDCE ' CODE ' CCDE GIT!YE MPE i e, e i t_,,j ; a e e i i L,,,,J e i i i y; i WIT!vE NAPE t I e i I L.,,,J ; I e f i t t _l j f f I 1 i U O tT M M i 1 i I i LJJI ' I f I l__l i ' ' ' ' ' L--- ! l E. to YCU TREAT M DISOdRr4 TO RDOVE EITIVES? YES Po tedT IS THE RDcVAL EFFICIDCY 40 f.l, HARGE FREGINCr? Q Q k F. n f twf Fem'm l 3 RDcVAL t@S./ DAY DAYS /WE. WITIVE NME w w y A;I)!Tivt N4E i t i t, 1, ) l__l ADDIT!vE Pe PE I f I l l.- I l3 n G. AS #e ATTAOfENT TO THIS APPLICATION PROVIDE SPECIFIC M#t.ALIAN 0t AQUATIC T0XICOLriri! CAL DATA CR REFERDCE WHICH ARE AVAILASLE #iD INFONATION ON M RATE OF IfGRADAf t0N OF M PDCQJCTS FOR EACH ATOITIVE. NA 31

SECTION ll gR MIoOOSD 7 I R E INSTRUCTIONS REVERS 6 SIDE (L'TFML fUTER 16 iO t A ITEM A. NAff 0F PECESS (DNTR!R/ TING TO THE DISOWIGE ,$,, C, A,7,c, M, , Q, A,3,9 iQ,,,,,,i TW10UtN TH15 CUTFE Ape SIC CODE B. Pf0 CESS SOEDAI (YEMILY AVERAGE) KXRS/ DAY INf4I DAYS /YfE I INI4I e MIT QXe e C. Pfl0 CESS WLIM Fl.DW RATE i Nt

I I t l 1

(,,l,,,) POCESS W TOTA YEAPLy I t I t t ( STREAMS m!LY MINIM i f I I f f f f I O' I b I CONT.ll8UTING TO O *I4t3lIf [_2.) mrty twtgets, I I t t t f [ D. PROCESS PRODI.CTION RATE g Di R A. NAE CF PROQSS (DNTRIButts TO TE DISO4RGE THOUIN THIS OUTFALL Are SIC C00E l I f I I I I I I I I I I ' l I ' l I I 8. Pf0 CESS SotDAI (YEMILY AM) KXRS/ DAY I I I DAYS /vEAR I m elI GEA C. Pfl0 CESS WLIM Fl.DW RATE , 0( Y f f I I I I I I f i L! N I ' ' I ' ' ' ' ' ' E DA!LY MINIMLM UNITS CODE 1 POUNOS 'L I 2 GALLONS Lh!TS / TIE D. PROCESS PRODUCTION RATE I I I I I t f f I L_.V L.J A. NM OF PROCESS (DNTRIBUTING TO TE DISOWIGE YARDS T)fl0 UGH THIS OUTFE APO $1C (EE I I I f f I I I ' 1 I I I ' I I I ' 'I 4 TONS 5 L'GY 'Ol8dDAY DAMEd8 ' ' ' ' 6 CGD C. PROGS $ WUM Ft.0W RATE 7 TOTAL YE#tLY I e I I I I I ' I I LJ W [ ongty nigge i f I I I f I i i I LJ DAILY MAxte i I f f f I f ' ' ' lJ b D. Pf0 CESS PROCLETION RATE ,,,,, i e e i l TIME 1 HOUR A. Napf 0F PROCESS CDNTRIBUTING TO TE DISCHARGE TMOUGH TWfS CtfTFALL Ato SIC CODE ,,,,,,,,,,,,,, g,,,, g I* 3 WEEK scuRS/ DAY l t I DAYS / YEAR I I I i 4 MONTH m m1T m E, TOTAL MY l I ' ' ' ' ' ' ' ' U 5 YEAR l DA!LY MINIPt7t I f I I I I I I I I l-.J e. g,(y ggy I f I f I f I I I I lJ tmlTS /TIPt. D. P50 CESS P90DLET!0N RATE I i 1 t t t i i i L _ V L_.J A. NAff 0F PRDCESS CONTRIBUTim 70 TE DISOWIGE TM10UtN THIS OUTFALL Ato SIC C3E I I l I f f f I I I I I I ' I I,,,, B. PROCESS SOCLA.E (YE#tLY AVERAGE) KX.RS/ LAY t 1 I DAYS / YEAR t I I I e WIT m y C. PROCESS WLIM FLDN RATE yg7AL ymy ,,,, ;, e i t t (,_j um DAILY MIN!Pt.M I ! ! ! ! I I ' ' ' On[(y pwttegpg I t i t t I f I f I L_ UNITS / TIPE D. P50 CESS Plot 1CTION RATE g ,, g g,,,, (_y L J l 1 33 l

SECTION ll PERuiT MIo00 5'7M r NUMBER SliEINSTRUCTIONS ON REVERSE SIDE wn.uum ,5,o I:3., ITEM !$ TM FEM THl3 OUTFALL DIRECTED TO TM GROUte OR g GA0uro,DI. IF to, CONTIME TO LTm Sr Yt3 to A. ATEps. 8. NAS A HYLROGEOLOGICAL SitEY OR ITS E2JIVALENT BEEN PERF0fM3 OR l$ THRE StFFICIENT YES to CURRENT HYDROGEOLQGICAL IPFolNATION AVAILABLE AS REQUIDQ LY TQATER RESOURCES CGttisit0N PART d GROLMMATER RULE OF At&UST 1419fo R.w.zeue (PsE 6) FOR GROUNOWATER THl3 DISTING OR PR0fCSED DISCHAPGE tF YES ATTA04 A COPY OF THE REPORT. g DISCHARCE C. AAE YOU DjQUES I AN EXEMPTION FROt SLEMITTIPG A HYIP(X;EOLOGICAL REPORT IJOER INFORMAtl0N YES to Rt1.E R.3o.220 ) (PAGE M) OR FRO 9 GRotMMATER PONITORIPG KQJjRENENTS UNDER HULE R.5 (5) (PME 4[) 0F T4 PMT H RtA.ES. IF YES ATTACH C0CtrENTS Ato EXPLANATION TO COONSTRATE THAT YOUR DISCHARGE MXA.D QUALIFY FOR a AN EXDff!ON. M AAE You REQLKSTIPG A VARIANCE FRGt RM 32.3.M (PAGE f. IF YES, ATTACH SUCHOct0EGRADATIGd) 0F D. Y'I PO T4 HATER RESOURCES CCPt915510N PART d GROLMMATER RLLES 00CtrENTS AS NECESSARY TO TE NE FOR A VARI IN TEfMS OF TE PAGE ) (F THE PART RULES. ) CRITEAIA SPECIFIED IN RtA.E E. t.!ST AL,L CHEMICAL StBSTAr_ES HHtCH ARE IN MICHIGAN'S CRITICAL MAT { RIALS REGISTER TABLE tv (PME t)) Arc /OR U.S. EPA'S PRI3t!TY PCLLUTANT LIST TABLE V (PAGE /) OR ANY OTER StBSTANCEC NOT APPLICABLE / BELIEVED ABSENT Wi!CH ARE OR MAY BECOE tPuist10US TO TW CESIGNATO USES OF TE G40LPOGATER OR TO THE PUBLIC HEALTH THAT APW DISCHMGED OR EXPECTED TO BE DISCHMGED TO TE GRotMMATER.BY THIS FACILIT/ ESTIMATE THE FINAL EFFLUENT CONCENTRATION Ato RECORD ALL DATA IN ITEM / OF SECTICN !! IN Dt!S B00NLET. PRESENT, CATA PROVIDED IN ITEM 7 T4 APPLICANT MAY BE REQJ1 RED TO DO AG)lTICNAL HASTE ANALYSES. g A. DISCHARGE OtARACTERISTICS CONCENTRATION IJt!TS C:X)E T ANALYSES SAffLE TYPE ITEM ' ' ' I I I I I ' I*I I I I kbd L..d d L3 - *B005 (FIVE DAY BIOLOGICAL OXYGEN DEMAND)

C00 (CgntCAL oxvGgN pmnto) i 1 I i.I t i I t i I t.I I t t l,,,}j it i L,,,,)

EXPECTED I *I I I I I I.' ' I I I ' I U WASTEWATER - MC (CTAL MC CARBON) CHARAC- _eAttUi!A N1TROGEN (AS N) l I I I.I l I I I I I I.I I I I L}J l 1 J d TERISTICS I I l 1 .I I f I i 1 I II I I I l !.] t I f LJ

TOTAL SUSPEPOED SOLIDS UNITS CODE TOTAL PHOSPHORUS (AS P) i I I I

.I f I l I I t 1

I I t I d8 f I L_J 1 Mg/l dI f f U

I I I '.' ' ' ' ' ' ' J.' I 2 Ug/l TCTAL RESIOUAL Ot.ORINE 3 COUNTS / L}J e t I (,,,,,,3 I t i I.i f 1 I t i e f .I 1 : ! MSSOLVED OXYGEN ggg 100 mi i I I, [__J t t .y g_qj L,,_y L.,j 4 S.U. .pg 5 'F I I I ' ' ' L3 6 LBS/ DAY FECAL COLIFCm BACTERIA i I I.U l I. L3 I f I U

TDfERAftFE (Sitt1ER)

I ' I. L._J L -.J 8 U

TE.'fERATIFE (dlNTER)

B. OTMR HASTEWATER CHMACTERISTICS O gRlE,A,S i E, g t i e t i i t I t t 1

i. i I i 1.__I L _L !

L! 3 0 t !,Ll2 9 SAMPL( I I f f i f f f I t I i t t I i.e i i t t I i t.I I t 1 L,,) I I f y TYPE ,,,,,,,,,,, ;,,i,, i L_j i i I U 1 GRAS ,,,,, I t t t I t i e e i I.i I f f I I i t.' ' ' f LJ ' ' ' U 2 24 HOUR COMPOSITE t i I t i t I i t i e i i t t i.I t t t t t i 1.t I I i U f ' i L._J s t i f t i e e t I i t i e t i .t I t e i i i t.i i 1 f U t I 1 L-.J e i I f i e i i i e i i i I e.i t i t i t t i.e t t I L] I I I L_J k SToD4 wATse oisc.wAccao THQouca corra Se a is SimeAc. p STo Rot w A TTP. DiscHAECE D Dt EoucH o u rrA L(. So 1. THEEEFo26, ) IN Dt AN A d MIC.4sC AAJ E WCTasc C om fA*f EE4we5T5 petmesseoAs 7n OM TH6 SccET AJ N C pare F2cu ourrAs.t Sol TD CdAEACTEf.#M 7Mt3 D8 fCH4 2C E. 35 l

~l SECTION 11 PERMlT y ggq SEE INSTRUCTIONS NUM _,ER ON REVERSE SIDE anmuum , S, o,9, THE OLLDv!NG REQLESTED IT0mATION '

AIXPESSED 31.AL SWFACE NEATER DISCHMIGERS.

!CIE Piw USE DISCHMGERS 2$.L PROV ECTED VALIES FOR THE QUANTITATIVE APO QuALITAT!vE IWOR%TICH REQUES!ED BELOW. A. 15 THIS FACILITY A PRIMty trCLETRY7 (REFER TO TABLE IA PM4 41) (!F.c, ro TO E1 (!F VES, GO TO B) YES to PRIORITY 8. IretCATE TYPE OF e:'MNtY IPCUSTRY AS L!$TED IN TABLE lA PM4 91 POLLUTANTS (cmT!'*E WITH C.) i g II MI IElbl6f01 1 Piuh Ri ANO C. OcES THIS OUTFALL DISCHMCE CONTAIN MY PROCESS WASTEHATER? (18 4. Go M d (!F YES, GO M D) YES to ADolTIONAL INFORMATION D.. INDICATE *ICH GC/MS FRACTIONS MUST BE TESTED Fm. (REFER TO TABLE IA PW4 91) WLATILE FOR !CIE! FOR EACH GC/MS FRACTION OECKED,EACH SPECIFIC ORGANlc T0XIC POLLUTANT WITHIN SURFACE EAOe FRACTION tigJ BE AMLYZED FOR (SEE TABLE IIA PAGE 42. IN ADCITION. E PRIMARY BASE / NEUTRAL WATER ItOJSTRY APPLICANTS WITH A PROCESS WASTDeATER DISOeGE SgI PROVIDE QUANTITATIVE DISCHARGE

I"

III" ## b *

^ ACID ONLY RECORD h DATA ON F0mS PROVIDED (ITEM 7) IN THIS B00u1ET. (CDNTINUE WITH E-K BELOW) PESTICtrE E. !F M. SLAtFACE MATER DISCHARGE APPLICANT (PRIMARY OR SECONDARY INIUSTRY), REGARDLESS OF TH[ TYPE m DISotARGE, KtOWS OR HA! REASON TD BELIEVE THAT ANY POLLUTANT LISTED NOT APPLICABLE /8ELIEVED A8SENT IN TABLE IIA APO IVA PAGES Dil IS DISCHARGQ FAQ1 ANY QJTFALL,TW QUANTITATIVE 5&I 8E PROv!Eu. RECDRD E DATA ON F0mS PROVIDED (ITEM 7) IN TH15 BOONLET. PRESENT/W !$ ATTAOED F. IF ANY SLJtFACE WATER DISCHARGE APPLICANT (PRIMARY OR SECOPCARY IPOJSTRY), REGARDLESS OF TYPE OF DISOfRGE, MNOWS OR HAS REASON TO BELIEVE ANY POLLUTANTS LISTED IN NOT APPLICABLE /8ELLEVED ASSENT TABLE VA PK4 92 ARE DISCHARGED FRrM ANY OLITFALL M APPLICANT Sg! DESCRIBE REASONS FOR T4 PCELUTANT BE!PG PRESENT #0 PROVIDE ANY AVAILABLE QUANTITATIVE DATA. RECORD E DATA ON FO@tS PROVIDQ (ITEM 7) IN THis BOONLET. G. ALL S$ FACE WATER DISCHARGE APPLICANTS (PRIMARY AND SECONDARY INDUSTRIES)

c:

PCT APPLICABLE / BELIEVED ABSENT OR t%NUFACTtFES 2, 4, 5 - TRIOGROPKFOXY ACET!q ACI (2, 4, 5-T); , 4, 5-TRIQt0ROPHEtCXY) PROP IC ACID ($1LVEX, 4, 4, , 4, > PCXYJ ETHYL 2-DiCHtm0PROPIONATE, TP)IJ 0, DIMETHYL TRICHLOROPENYL) PWSPt0ROTH10AT (RoteEL)J 4, S-TRIOLOROPE*0L (TCP); OR HEXAOLOROPHETE (W.P{i; (ALL DATA FOR THE A80VE MUST BE GENERATED USING STWCARD ANALYTICAL CALIBRATION PROCEDLRES) OR xtCWS OR HAS REASON TO BEL! EVE THAT TCDD IS m MAY BE PRESENT IN TMIR DISOMRGE. $$1 REPmi fb4LITATIVE DATA, GEFERATED *IOj UqED A SCREENING PROCED@E NOT PRESENT/ DATA IS ATTAOED CAtlBRATED WITH ANALYTICAL ST# CARDS, FOR 2, 2, f )8, - TETRAOLORODIBEN2PP*DIQXIN (TCDD). RE(DRD ALL DATA ON FORMS PROVIDED (ITEM / IN THIS booklet. J. 1F TM SijRFACE MATER DISO#GE APPLICANT KtOWS OR HAS REASON TO BELIEVE THAT BIOLOGICAi T0XICITY TESTS wERE MADE IN THE LAST TWEE (3) YEARS ON ANY OF TW por 4ppgg;jgtg APPLICANT,S O!SOWGES OR ON A RECE!VING HATER IN RELATION TO A DISOtARGE, PROVIDE THl3 ITORMTICN AS AN ATTAOfENT TO THis APPLICATION. APPLICABLE /SEEATTACHED K. IF A C0hTRACT LABORATORY OR CONSLA. TING FilV1 PERFORMED ANY OF TM AM.AYSES REQUIRED fj NOT APPLICABLE BY THis APPLICATION, PROVIDE THE P=8ME A?C ADDRESS OF EAOf LABORATORY OR FIRM 40 TM ANALYSES PERF0FMD AS AN ATTAOf1ENT OF THis APPLICATION. APPLICABLE /SEE ATTACHED TfJtLES tv PAGE ) #D IIA TW0the VA PF.ES 4M. D0 YOU DISCHARG ANY OTHER T0XIC OR Ifo@!OUS ICAL StESTANCES POT L1STED IN L. g IF YES, TMN IENTICY TW PCT APPL! CABLE OdNICAL SUBSTANCES 40 ESTIMATE T4 FINAL EFFLLENT CONCENTRATIONS. SLEMIT THis IWomAfl0N AS AN ATTAOfiNT TO THIS APPLICATION. APPLICABLE /SEE ATTAGED l 37

l l SECTION 11 PERMIT MIo006837 NUMBER 'SEE INSTRUCTIONS ON REVERSE SIDE m me i Sio ia ITEM A. USE THIS DATA SPEET TO RECCAD INFORPSTION AS REQJIRED IN: (OECK APPROPRIATE BOX POR WICH INFONATION N!$ DATA SHEET REPRESENTS.) 7

1. SECTION II, ITEM l-E.

GROLPOSTER DISCHAPGE INFOR*ATION (PAGE 35) l

2. SECTim II, ITEM 6. PRIORITY PauuTANTS IN $$ FACE WATER DISCHAME (PAGE 37)

MATERIALS

3. a. aELON: CRritCAL MATERIAt$ (TAatE tv) IN SLRFACE MATER DISOSRGE (PAGE 39)

TOXIC POLLUTANTS 4 e 1 HAZARDOUS SLCSTANCES 8. LIST ANY CRITICAL PETERIAL (TABLE IV PAGE 6) NOT AD@ESSED IN SECTION ll ITEM 6 DRIORITY WT MICABLE PQ.LLTANTS WICN VOU 1008 OR HAVE REASON Til BELIEVE TO BE PRESENT IN TE DISCHARGE. SEE IN REVER3E $1DE OF THIS PAGE POR FUPMR DIRECTims. DISCHARGE APPLICABLE (SEE BELOW) A. NAPt OF CRITICAL MATERIAL OR PRIORITY ICLLUTANT g, g, ;,,, W M W ES 8. AVERAGE CONCENTRATION; SMPLE TYPE; I 0F ANALYSES g ;, g g g g g

'L ",,,..,,,, *!'f =

C- = i M = ='= Ti= = = SS A. N#E OF CRITICAL MATERIAL OR PRIORITY POLLUTANT g g g g g g

I

# " '3E8 be*

8. AVERAGE CONCENTRATION; S#RE TYPEJ # OF AMLYSES l l l l.[ l l I L_J t_) i i i y I t f f.I f f

i. WIT CODE LNIT CODE 3

C. PmXIPtM COdCENTRATION WO P%S$ L _.) t t t t,i t I l U UNITS CODE J A. PM OF CRITICAL MATERIAL @ PRIORITY POLLUTW g g l l l l l l h WIT CODE SMPLE TYPE 8 0F h vSES t g fg g y 5. AVEMGE CONCENTRATION; SMPLE TYPE; f 0F ANALYSES l l l l,l l l l g d W!T CODE W!I CODE 3 LBS/ DAY 2 C. P%XIM COPCENTRATION MO P%$$ g,,,,,,,, g,,, g,; i,, g 4 KG/ DAY A. N#E CF CR!TICAL P%TER!AL OR PR10RITY POLLUTANT g g g g g g g g W M SMRE PE YSES B. AVERACE COPCENTRATION; $#RE TYPE; # OF #AYSES g g g g,g g g g I C00E WI CODE 2 C. MAXIM COPCENTRATION #O P%55 SAMPLE TYPE g A. m 0F CRgigCAL PuTERIAL OR PR!@ TTY P0dMTMT l g g g g g g g 1 GRAS g W 00E S#1PLE TYPE # OF #AYSES B. AVEPEE COPCENTRAfl0NJ SAPRE TYPE; # OF AMLYSES [ g l l,g l l l ,[ 2 24 HR.COMR WIT CODE treti COCE C. PnXIM COPCENMATION NO MASS i f f f .I f 1 1 y I l 1 l,t t t l U g A. PWE OF CRITICAL MATERIAL OR PRI@lTY POLLUTANT g g 9 g g g g g CCE S#R TYPE W YSES e B. AVERAGE COCENTRATION; SMPLE TYPE; I 0F ANALYSES l g g g,l g l g X UNIT CODE th!T CCM C. MAXIM COPCENTUTION NO P%$$ f f f f .I i t i U t t t f.I 1 l i U A. N#E OF CRITICAL MATERIAL OR PRIORITY prntfrAgy I i f f I I e g g LPell CODE SAMPLE rYPE # W #eALYSES 7 B. AVERKE CDNCENTRATION; SAMPtf TYE: # W APAYSES l g g l.I I I I L_1 o i i i WIT COM WH W I PnXIM C0rCENTRATION NO PS$$ C. t t t .I t I t U i i + 1.I I i i g_j .J A. NAPE OF CRITICAL MATERIAL OR PRIORITY POLUJTANT f f I I I I i l j th!T C00E SMRf TYPE # OF # M SES e 8. AVEPME CDCENTRATION; SANPLE TYPE; # OF #AYSES l f f I.I I I I L._J t_ J t t i UPI!T CODE WIT CODE 2 C. P%X1M COPCENTRATION NO MA$$ I I f f.I f f I L_J l 1 i f.I i 1 1 U ADDITIChAL PAGES OF THl3 ITm 7 APE ATTAOC FOR DE REST OF DE CRITICAL O YES mTERrALS #c/m PR @lTY P0twrANTS REQ;tRC TO BE REPORTC. 30

Re vd 4 -1 MS ATTAC1DiENT I ( REMIT TO: Laboratory Services Division Park West Two e'r-5350 Campbells Run Road Cliff Mine Road u Pittsburgh, PA 15205 Pittsburgh, PA 15275 ( 412-788-1080 ( ( l_. A D A N A L. Y S I S R E P (3 R T CLIENTNAME: INDIANA 5 MICHIGAN ELECTRIC CD. NUS CLIENT NO: 010904 ADDRESS: P. C. BOX 60

- - ~

FORT 'JAYNE, IN 46801 VENDCR NO: 05411000 r REPORT DATE: 04/12/85 WORX ORDER NO: 55830 MTENT101: MR. JOHN HUGHEY DATE RECEIVED: 03/20/85 1 SAMDLE IDENTIFICATION NUS SAMPLE NO RESULTS UNITS ( LANE MICHIGAN INTAKE 02/26 15031141 ~ CD26 Triorylphosphate' esters < 50 ug/l W340 Hgdtczine < 0.04 ag/l ( LEIT 1 DISCHARGE 02/26 15031142 III' OD26 Triary1 phosphate esters < 50 ug/l ( 1320 Hydrozine < 0.04 ag/l UNITE 1 SG BLOWDOWN 02/26 15031143 ( 0026 Tristylphosphote esters < 50 ug/l W340 Hgdtczine 0.20 mg/l ( TURBINE R00P. S2 P 02/26 15031144 0026 Triory1 phosphate esters < 50 ug/l 1340 Hydrozine < 0.04 og/l ( A' X. FEATIN3 POILER ! LOWDOWN 02/26 15031145 8I' J 0026 Triory1 phosphate esters < 50 ug/l i kIA0 Hydrazine < 0.04 ag/l LMIT 2 S3 BLOWLOWN 02/26 15031547 ( 0026 Trtorylphosphate esters < 50 ug/l 13 0 Hydrazire 0.40 mg/l ( UNIT 2 IISCHARGE 02/26 15031548 CD26 Triory1 phosphate esters < 50 ug/l l'30 Hydrazine ( 0.04 ag/l 3 L L F?ENTS: ( Reviewed and Approved by: JP.0 (, h A Halliburton Company CLIENT ORIGINAL. i

4/3/es RElefT 70: Laborecory Services DMelon Park West Two NUS 5360 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 g 412-700-1000 LAB ANALYSIS REPORT CLIENT NME: INDIANA & MICHISAN ELECTRIC CO. MUS CLIENT NO: 010904 ADDRESS: P. O. 30X 60 NUS SAMPLE NO: 15021679 FORT WAYE, IN 46801 VENDOR MO: REPORT DATE: 03/26/95 WORK OR ER NO: 55830 ATTENTION: Ift. J0lti HUGEY DATE RECEIVED: 02/27/95 SAlfLE IKMTIFICATION: LAKE MICHI6All INTAKE 02/26 TEST KTERMINATION REStA.TS UNITS i 5361 NP M S PART V-3 M010 Aluminus ( A1) < 0.1 ag/l 1040 krive (Be) < 0.1 ag/l M150 Cobolt (Co) < 0.01 ag/l l190 Iron, total (Fe) 0.06 og/l M230 Mognesius (Mg) 12 ag/l 12M Mongenese (Mn) < 0.01 ag/l M260 Molybdenue (Mo) < 0.03 ag/l 13M Tin (Sn) <1 ag/l M350 Titanine (Ti) < 0.5 mg/l 1055 Boron (3) < 0.2 og/l W060 Broeide(tr) <2 ag/l 1225 Color, Trtie 120 Pt-Co W310 Fluoride, total (F) 0.6 ag/l 1390 Mitrete (N) 0.4 og/l W410 Nitrite (N) < 0.01 ag/l 1435 Nitrogen, Kjeldehl (N) 0.3 og/l W4M Nitrogen, Organic (N) 0.3 ag/l 15 # Phosphorus, total (P) 0.47 ag/l V730 Sulfate, turbidinetric (SO4) 26 ag/l 17M Sulfide (S) < 0.1 ag/l W760 Sulfite (SO3) <2 og/l 1770 Surfactants (MBAS) < 0.1 og/l M362 NP M S PART V-C T0XIC METALS M020 Antimony (Sb) < 0.1 og/l M030 Arsenic ( As) < 0.001 og/1 5050 Beryllius (Be) < 0.002 og/l M090 Codnius (Cd) < 0.005 mg/l 1140 Chronius (Cr) 0.01 ogIl M160 Copper (Cu) < 0.01 ag/l 1200 Lead (Pb) < 0.03 ag/l M250 Mercury (Hg) < 0.0002 ag/l PAE NO: 1 h A Halliburton Company CLIENT ORIGINAL

REMIT TO: Laborecovy Serv 6ces DMelon Park West Two NUS 5350 Campbells Run Road Cliff Mne Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-7as-10eo LAB ANALYSIS REPORT CLIENT llAfE: INDIANA & KICHI6All ELECTRIC CD. MUS CLIENT NO: 010904 ADDRESS: P. O. 30X 60 NUS SAMPLE NO: 15021679 FORT WAYlE, Ill 46001 VEMBOR 110: IIEPORT DATE: 03/26/05 WORK ORER 110: 55830 ATTENTI0ll MR. 30HN HUGIEY DATE RECEIVED: 02/27/85 SAftLE IDENTIFICATION: LAKE MICHIGAN INTAIE 02/26 ) 1EST DETERMIIIAT10ll RESULTS LMITS M270 Nickel (Mil < 0.03 ag/l M290 Selentue (Se) < 0.004 og/l 1300 Silver ( Ag) 0.01 ag/l M330 Thallius (TI) < 0.1 ag/l 1390 Zinc (Zn) 0.01 ag/l W270 Cyanide, total (CN) < 0.005 mg/l 1500 Phenolics ( 0.02 og/l M220 Lithius (Li) < 0.01 ag/l $110 VOLATILES-PP IN UATER OV01 Acrolein <100 ug/l 1902 Acrylonitrile ( 100 ug/l DV03 Benzene (5 ug/l 1905 Brosofors <5 ug/l DV06 Carbon Tetrochloride <5 ug/l IV07 Chlorobenzene <5 og/l DV08 Chlorodibtonceethane <5 ug/1 IV09 Chloroethane < 10 ug/l DV10 2-Chloroethylvinyl Ether < 10 ug/l IV11 Chlorofore (5 ug/l DV12 Dichlorobronomethane <5 ug/l IV14 1,1-Dichloroethene <5 ug/l DV15 1,2-Dichloroethene <5 ug/l I IV16 1,1-Dichloroethylene (5 ug/l OV17 1,2-Dichloropropone <5 ug/l l IV18 1,3-Dichloropropylene <5 ug/l OY19 Ethylbenzene (5 ug/l IV2C Methyl Droeide < 10 ug/l DV21 MethylChloride < 10 ug/l IV22 MethyleneChloride <5 og/l OY23 1,1,2,2-Tetrachloroethane <5 mg/l IV24 Tetrochloroathylene(Perchloro) <5 og/1 OV25 Toluene <5 ug/l PA T NO: 2 h A Halliburton Cornpany CLIENT ORIGINA1.

REterT TO: Laborsecry W h Park West Two NUS 5350 CampboHs Run Road Chtf Mins 71oed Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-788-1000 g LAB ANALYSIS REPORT CLIENT HAE INDIAllA & NICHIGAll ELECTRIC CO. NUS CLIENT NO: 010904 ABORESS: P. O. 30X 40 NUS S W LE NO: 15021679 FORT WAYIE, IN 44001 VENDOR NO: EPORT DATE: 03/26/85 WORK ORDER NO: 55830 AllINTION: IWt. J0lti WJEEY DATE K CEIVEls 02/27/85 SWLE IDENTIFICATION: LAKE MICHIGAN INTAKE 02/26 TEST MTERMIllATIOlt RES(R.TS UNITS IN26 1,2-Trens-Dichloroethylene <5 ug/l OY27 1,1,1-Trichloroethene <5 mg/l W28 1,1,2-Trichloroethene (5 ug/l OY29 Trichloroethylene <5 ug/l IY31 Vinyl chloride <5 ug/l 0120 ACIDS - PP IN WATER 0A01 2-Chlorophenol ( 10 ug/l 0A02 2,4-Dichlorophenol < 10 ug/l lA03 2,4-Bioethylphenol ( 10 ug/l 0404 4,6-Binitro-o-cresol ( 50 ug/l lA05 2,4-Dinitrophenol ( 50 ug/l 0406 2-Nitrophenol < 10 ug/l 4407 4-Nitrophenol ( 50 ug/l 0A00 p-Chloro-e-cresol < 10 ug/1 lA09 Pentochlorophenol ( 50 ug/l 0410 Phenol < 10 ug/l lAll 2,4,6-Trichlorophenol ( 10 ug/l OC30 Acid Extraction-Water 0130 BASE NEUTRALS - PP IN WATER 0801 Acenophthene < 10 ug/l 1302 Acenophthylene ( 10 ug/l 0903 Anthracene < 10 ug/l 1904 Benzidine < 50 ug/l 0905 Benzo (o)Anthrecene < 10 ug/1 IM6 Benzo (aPyrene < 10 ug/l OM7 3,4-lenzofluorenthene < 10 ug/l 9308 Berco(ghiPerylene < 10 ug/1 0009 Benzo (kFluorenthene ( 10 mg/l 1910 lis(2-Chloroethoxy)Methone ( 10 ug/l 0B11 lis(2-Chloroethy1 Ether < 10 mg/l IB12 Bis (2-ChlorcisopropylEther < 10 ug/1 0813 Bis (2-EthylhexylPhtholote ( 10 ug/l PA(E NO: 3 l 1 j h A Halliburton Company CLIENT ORIGINAL

REteff TO: Laborecory Services Division Park West Two 5350 Campbelle Run Road Cliff Mme Road n'ittsburgh, PA 15206 P,ttsburgh, PA 15275 412-788-1000 l_. A B A N A L. Y S I S REPQRT CLIENTIWlE IllDIANA 6 MICHIGAN ELECTRIC CO. NUS CLIENT NO: 010904 ABORESS: P. O. 90X 60 NUS SAWLE 110: 15021679 FORT liAYE, IN 46001 VENDOR 110: KPORT DATE: 03/26/85 liORK ORDER 110: 55830 ATTENTION: IEt. J0lti HUGEY DATE RECEIVED: 02/27/85 SAMLE IDDITIFICATION: LAKE MICHIGAll INTAKE 02/26 1EST NTERMINATI0ll ESIA.TS UNITS (3 14 4-Stonophenyl Phenyl Ether < 10 ug/l 0815 Putyl Benzyl Phtholote < 10 ug/l 9316 2-Ch19tonophtholene ( 10 ug/l 0017 4-Chlorophenyl Phenyl Ether < 10 ug/l 1918 Chrysene ( 10 ug/l 0919 Dibenzo(o,h)Anthrocone < 10 ug/1 9820 1,2-Dichlorobenzene ( 10 eg/l 0521 1,3-Dichlorobenzene ( 10 mg/l 1922 1,4-Dichlorobenzene < 10 ug/l 0823 3,3'-Dichlorobenzidine < 10 ug/l 1824 Diethyl Phtholote < 10 ug/l 0B25 Dioethyl Phtholote < 10 ug/l IB26 Di-N-Dutyl Phtholote < 10 ug/l 0927 2,4-Dinitrotoluene < 10 ug/l 1928 2,6-Dinitrotoluene < 10 ug/l 0329 Di-N-Octyl Phtholote < 10 ug/l 1830 1,2-Diphengthydrozine( Azobz) ( 20 ug/l 0B31 Fluoronthene < 10 ug/l ll32 Fluorene < 10 ug/l 0933 Hexothlorbenzene ( 10 ug/l IB34 Hexachlorobutodiene ( 10 ug/l 0335 Hexachloro-cyclopentodiene ( 10 ug/l 1836 Hexachloroethane < 10 og/l 0837 Indeno(1,2,3 cd) Pyrene < 10 ug/l 1938 Isopherone < 10 ug/1 0339 Nephtholene < 10 ug/l ll40 Mittobenzene < 10 ug/l 0841 N-Nittosodinethylonine < 10 ug/1 1842 N-Nittosodi-N-Propylonine < 10 ug/1 0543 N-Nitrosodiphenyleine < 10 ug/l ll44 Phenanthrone < 10 ug/l 0345 Pyrene ( 10 ug/l PAE NO: 4 h A Halliburton Company CLIENT ORIGINAL

REtffT TO: Laboratory Services N Park West Two 5360 CampboHs Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 mg 41 M as-toso LAB ANALYSIS REPORT CLIENT NAME: INDIANA & NICHI6AN ELECTRIC CD. NUS CLIENT NO: 010904 ADDRESS: P. D. BOX 60 NUS SAWLE NO: 15021679 FORT WAYE, IN 46801 YDSOR NO: REPORT DATE: 03/26/95 WORK ORDut NO: 55830 ATTENTION: IEt. Jolti IWG E Y DATE RECEIVES: 02/27/85 SAMLE IDENTIFICATION: LAKE NICHIGAN INTAKE 02/26 TEST DETERNINATION REStA.TS UNITS (346 1,2,4-Trichlorobenzere < 10 eg/l OE25 Bose Neutral Extraction-Water 0141 PRIORITY POLLUTANT PCB'S DE11 PCB Extraction - Water IP19 PCB-1016 ( 0.5 ug/l OP20 PCB-1221 < 0.5 ug/l IP21 PCI-1232 <0.5 og/l DP22 PCI-1242 ( 0.5 ug/l IP23 PCI-1248 ( 0.5 ug/l OP24 PCI-1254 < 1.0 ug/l IP25 PCI-1260 ( 1.0 mg/l R450 RADIUM 226 AND 228 RB04 Rodive-226 < 0.4 pC1/1 R805 Rodive-228 <2 pCi/1 F500 Oross Alphe <2 pti/1 R801 Gross Dete <2 pCi/1 1032 Ansonia os N (distillation) < 0.1 og/l 9050 300, 5-dev (02) <1 og/l 1100 Carbon, organic (C) 19.5 mg/l W120 C0D (02) <5 mg/l j .I610 Solids, suspended at 10} C <1 ag/l COMMDITS: Reviewed and Approved hi PN PAGE NO: 5 h A Halliburton Company CLIENT ORIGINAL.

RElefT TO: Laboratory Services DMeion Park West Two 5300 Campbella Run Road Chff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 412-700-1000 g l l LAB ANALYSIS REPORT CLIDT NAME: IllDIMA & MICHIGAN ELECTRIC CO. W S CLI S T NO: 010904 ABORESS: P. O. 00X 60 WS SAMLE NO: 15021600 FORT WAYE, Ill 46001 ENDOR NO: l EPORT DATE: 03/26/95 WORK OR KR NO: 55830 AiTENTION: Itt. J0lti HUBET DATE RECEIED: 02/27/85 SA MLE I M NTIFICATION: LAKE MICHIGAll INTAKE - GRAB 01 02/25 0855 1EST KTERMINATI0ll RESLA.TS UNITS lA32 Fecel Califore - F N 4 col /100e1 W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 8.1 W600 011, extraction grevisetric 2.1 kg/l COMENTS: Reviewed and Approved by: JIC h A Halliburton Company CLIENT ORIGINAL

s REteff TO: Laborecory Services DMeion Park West Two 5380 Campbells Run Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 g 412-733 1030 LAB ANALYSIS REPORT CLIDif IIAIE: IllDIANA & MICHIGAll ELECTRIC CO. IlUS CLIDIT 110 010904 ANItESS: P. O. 30X 60 IluS SAIFLE 110: 15021682 FORT MAYlE, Ill 46801 VD00lt 110: IEP0lti MTE: 03/26/85 90ltK OltDDt NO: 55830 ATTDITIOli lWt.' J0lti HUOlEY MTE ItECEIVED: 02/27/85 SAIFLE IDDITIFICATI0lls LAKE MICHI6All INTAKE - GRAS 43 02/25 2110 1EST KTDtMIllATIDIl RESULTS UllITS IA32 Fecel Colifors - IPN <3 col /100s1 W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 8.C W680 011, extraction-gravinetric 1.1 ag/l l 1 COMENTS: Reviwed and Approved by: JIC h A Ha!!iburton Company CLIENT ORIGINAL

REast? TO: W Laboratory Services DMeion Park West Two 5360 Campbells Run Road Citff Mine Road Mttsburgh, PA 15206 Pittsburgh, PA 15275 412-788-1000 g LAB ANALYSIS REPORT CLIENT llAE 1 814114 & NICNIGAll ELECTRIC CO. IIUS CLIENT 110: 010904 ADDRESS: P. O. 30X 60 IluS S W NO: 15021683 FORT WAYIE, IN 46801 VD80R 110: EPORTllATE: 03/26/85 WORK ORDER 110: 55830 ATTENTION:' IIt. JoltiillOEY BATE ECEIED: 02/27/85 SAltLE IDOITIFICATION: LAKE MICHIGAll INTAKE - GRAB 04 02/26 0310 TEST ETERNIllATI0li ItESULTS UNITS 3432 Fecel Califors - IPN 9 col /100n1 W150 Chlorine, residual IPD (C12) < 0.1 ag/l 1990 pH 8.1 W600 Oil, extraction grevinetric 1.5 mg/l l l C0ltENTS: Reviewed and Approved by:.DIC h A Halliburton Company CLIENT ORIGINAL

REMIT TO: Laboratory Services DMolon Park West Two 5360 Campbells Qun Road Cliff Mine Road Pittsburgh, PA 15206 Pittsburgh, PA 15275 g 412-786 1000 LAB ANALYSIS REPORT Q.!DIT llAE IllDIANA & NICHI6AN ELECTRIC CO. NUS CLIENT NO: 010904 AIORESS: P. O. 30X 60 NUS SAIFLE NO: 15021681 FORT WAYE, Ill 46801 YENDOR NO: EPORT DATE: 03/24/85 WORK ORDER 110: 55830 ATTENTION: lWt. J0ml HUBEY DATE RECEIYEli 02/27/85 SAlFLE IDDITIFICATION: LAKE MICHIGAN INTAKE - GRAB 02 02/25 1510 TEST DETERMIllATI0lt RESULTS Ull1TS IA32 Fecel Califots - IPN 7 col /100a1 W150 Chlorine, residual DPD (C12) < 0.1 ag/l 1490 pH 8.0 W680 Oil, extraction gravinetric 1.5 mg/l 00t9ENTS: Reviwed end Approved ist JIC h A Halliburton Company CLIENT ORIGINAL .}}

ML20128F662

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ML20128F662

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