ML20100R393
| ML20100R393 | |
| Person / Time | |
|---|---|
| Site: | Farley  |
| Issue date: | 02/20/1992 |
| From: | ALABAMA POWER CO. |
| To: | |
| References | |
| CIVP-A-076, CIVP-A-76, NUDOCS 9204080298 | |
| Download: ML20100R393 (230) | |
Text
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. Test Report f(
'? REPORT NO. 401961 40196
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s 1.0 CUSTOMER Alabama Power Comoany ADDRESS 600 N.18th Street. Birrr.inchasn. Alabama 35291-0430 1 10 TEST SPECIMEN 4 Grease Samples and 5 Oil Samples (See Paragraph 6 0) 3.0 MANUFACTURER Texaco 4.0
SUMMARY
Four Grease Samples and five Oil Samples, described in Paragraph 6.0 and hereinaf ter called the specimens, were subjected to a Radiation Exposure and Accident Simulation Test Program as specified in Wyle Laboratories' Test Procedure 40196 00, Revision C. The test program was performed to satisfy the intent of 10 CFR 50.49 and IEEE 3231974, 'IEEE Standard for Qualifying Class IE Equipment for Nuclear Power Generating Stations.'
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g LABORATORIES SCIENTIFIC SERVICES & SYSTEMS GROUP HUNT,$VILLE, ALAa AMA
Page No. 2 Test Report No. 40196 1 _
1 4.0
SUMMARY
(Continued)
The test sequence for the test program was as follows:
o Baseline Functional Test (ASTM tests by Texaco) o Radiation Exposure o Post Radiation Functional Test (ASTM tests by Texaco) o Accident Simulation Test o Post Accident Functional Test (ASTM tests by Texaco)
Paragraphs 9.0,10.0, and 11.0 contain descriptions of the test requirements, procedures, and results.
it was concluded by Texaco after performing the Baseline, Post Radiation, and Post Accident ASTM Tests that the i; tease acd oil samples retained sufficient lubricating properties anu performance characteristics to adequately perform their normal functions (reference Texaco Test Report T.! contained in Appendix I of this report).
Based on Texaco's evaluation of the ASTM test results and the Texaco timilarity evaluation for the greases and oils that were not tested but were judged to be encompassed by the greases and oils that were tested, the greases and oils listed in Paragraph 6.0 are qualified for the normal and design basis accident conditions specified in Paragraph 2.1 of Wyle Laboratories' Test Procedure 40196 00. The qualified life of the greases and oils is 10 years '
based on radiation exposure. It should be noted that justification for the exemption of thermal aging is the responsibility of Alabama Power Cornpany.
The following are brief summaries of the ASTM test results for each grease and oil sample from Texaco Test Report T-1:
Premium RB Greate (new)
The data for the ASTM tests performed af ter Radiation and Design Basis Accident Testing indicate no significant changes in the grease thickener system as evidenced by dropping point results. Although the consistency of the grease changed during the testing proced the grease maintained an acceptable consistency required to provide good h._rication.
Premium RB Grease (4 vears old)
The data for the ASTM tests performed after Radiation and Design Basis Accident Testing showed no significant degradation to the thickener system as indicated by the dropping point results. The consistency of the grease did change (softened) during the testing cycle but the grease maintained an acceptable consistency requi ed to provide good lubrication.
Mr*fak AP (Multif ak EP 2) Greast The data for the ASTM tests performed after Radiation and Design Basis Accident Testing showed no significant degradation to the grease thickener system as indicated by the dropping point results. The consistency of the grease changed very little during the te. ting cycle and showed no evidence of )
excessive hardening or softening.
. WYLE t.ABORATORIES MuntSWM PACIHfy I
Pege No. 3 Te.t Report No. 40196 1 4.0
SUMMARY
(Continued)
Starolex 2 Greate The data for the ASTM tests performed after Radiation and Design Basis Accident Testing showed no significant degradation to the grease thickener system as indicated by the dropping point results. The consistency of the grease changed very little during the testing cycle and showed no evidence of excessive hardening or softening.
Reent R & O 68 011 The data for the ASTM Tests performed after Radiation and Design Basis Accident Testing indicats a change in the product as evidenced by the viscosity results. Although the viscosity of the product changed during the testing procedure, the product maintained an acceptable viscosity required to provide good lubrication.
Rees1 R & O 220 011 The data for the ASTM Tests performed after P.adiation and Design Basis Accident Testing indicate a change in the product as evidenced by the viscosity. Although the viscosity of the product changed during the testing procidure, the product maintained an acceptable viscosity required to provide good lubrication.
Mereen 320 Oil The data for the A$TM Tests perfor;ned after Radiation and Design Basis Accident Testing indicate a change in the product as evidenced by the viscosity. Although the viscosity of the product changed during the testing ,
procedure, the product maintalried an acceptable viscosity required to provide good lubrication.
Meroes 680 Oil The data for the ASTM Tests performed after Radiation and Design Basis Accident Testing indicate a change in the product as evidenced by the viscosity. Although the viscosity of the product changed during the testing procedure, the product maintained an acceptable viscosity required to provide good lubrication.
Rando Oil HD 68 Th. data for the ASTM Tests performed after Radiatien a'nd Design Basis Accident Testing indicate a change in the product as evidenced by the viscosity. Although the viscosity of the product changed during the testing procedure, the product maintained an acceptable viscosity required to provide good lubrication.
WYl.E LABORATORIES Hueterme Facmty
Pcge Nr. 4 Test Report No. 40196 1
5.0 REFERENCES
5.1 Alabama Power Company Purchase Order No. QP 3004.
5.2 Wyle Laboratories' Test Procedure 40196-00 dated August 25,1988, Revision C, dated November 17,1988.
5.3 IEEE Standard 3231974 ' Standard for Qualifying Class IE Equipment for Nuclear Power Genersting Stations'.
5.4 Wyle Laboratories' (Eastern Operations) ' Quality Assurance Program
- manual dated June 1988.
5.5 ASTM D566
- Standard Test Method for Dropping Point of Lubricating Grease',
December 1987.
5.6 ASTM D217 ' Standard Test Method for Cone Penetration of Lubricating Grease". November 1986.
5.7 ASTM D2266 " Standard Test Method for Wear Preventive Characteristics of Lubricating Orcase (Four Ball Method)', December 1986.
5.8 ASTM D2272
- Standard Test Method for Oxidation Stability of Steam Turbine Oils by Rotating Bomb', December 1985.
5.9 ASTM D92 ' Standard Test Method for Flash and Fire Points By Cleveland Open Cup *, December 1985.
5.10 ASTM D665 ' Standard Test Method for Rust Preventing Characteristics of Inhibited Mineral Oil in the Presence of Water', November 1983.
5.11 ASTM D1401
- Standard Test Method for Water Separability of Petroleum Oils and Synthetic Fluids', January 1985.
5.12 ASTM D942 " Standard Test Method for Oxidation Stability of Lubricating Greases by the Oxygen Bomb Method *, October 1978.
5.13 ASTM D2596 " Standard Test Method for Measurement of Extreme Pressure Peoperties of Lubricating Grease (Four Ball Method)*, December 1987.
5.14 /.STM D1743
- Standard Test Method for Corrosion Preventive Properties of Lubricating Greases', July 1987.
5.15 ASTM D4048
- Standard Test Method for Detection of Copper Corrosion from Lubricating Grease by the Copper Strip Tarnish Test', December 1986.
5.16 ASTM D445 " Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)".
December 1986.
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WYLE LABORATOfties Hun tr tt6e Fwitty
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l Pcse No. 5 Test Report No. 401961
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5.0 REFERENCES
(Continued) 5.17 ASTM D1500 ' Standard Test Method for ASTM Color of Petroleum Products (ASTM Color Scale)', January 1988.
5.18 ASTM D130 " Standard Test Method for Detection of Copper Corrosion from Petroleum Pr.; ducts by the Copper Strip Tarnish Test". January 1984.
5.19 ASTM D892
- Standard Test Method for Foaming Characteristics of Lubricating Oils". October 1974.
5.20 ASTM D664 ' Standard Test Method for Neutralization Number by Potentiometric Titration", December 1987.
6.0 TEST SPECIMEN DESCRIPTION The Texaco lubricant products encompassed by this test program are listed below.
Grease Oil Premium RB (new)' Regal R & O 32 Premium RB (4 years old)* Regal R & O 46 Multifak EP 0 Regal R & O 68*
Multifak EP 1 Regi R & O 150
( Marfak AP (Multifak EP 2)' kegal R & O 220' Starplex 2* Meropa 68 Meropa 150 Meropa 220 Meropa 320' Meropa 680' Rando Oil HD 32 Rando Oil HD 46 Rando Oil HD 68'
'These nine greases and oils were selected by Texaco to be the test specimens. The lubricating properties and performance characteristics were judged by Texaco to encompass all of the other greases and oils listed. The Texaco report contained in Appendix I of this report contains a similarity evaluation.
7.0 TEST EQUIPMENT AND INSTRUMENTATION DESCRIPTION The measuring and test equipment used by Wyle Laboratories in recording data are shnwn on the Instrumentation Equipment Sheet located in Appendix VI of this report. The equipment was calibrated in accordance with Wyle Laboratories' Quality Assurpnce Program. Which complies with the requirements of Military Specification MIL STD 45662A. Standards used in performing all calibrations are traceable to the National Bureau of Standards by report number and date. Where no national standards exist, the standards are traceabic to international standards or the basis for calibration is otherwise
( documented.
WYL.E LABORATORIES Humsvine Facuity I,
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Page No. 6 Test Report No. 40196-1
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8.0 QUALITY ASSURANCE _
All work performed on this test program was done in accordance with Wyle Laboratories' Quality Assurance Program, which comp 9es with the applicable requirements of 10 CFR 50, Appendix B; ANSI No.2 and the " daughter" standards.
9.0 TEST REQUIREMENTS 9.1 Basellne Functional Test 9.1.1 Test Snecimen Prenaration Texaco shall prepare three samples of each of the nine lubricants selected to be test specimens. One sample of each lubricant shall be subjected to the
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functional tests described in Paragraph 9.1.2. The second sample of each lubricant shall be subjected to the radiation exposure described in Paragraph 9.2 followed by the functional tests described in Paragraph 9.1.2. The third sample of each lubricant shall be subjected to the radiation exposure described in Paragraph 9.2, the accident simulation test described in Paragraph 9.4, and then the functional tests described in Paragraph 9.1.2.
9.1.2 Funettonal Tests The following functional tests shall be performed on the nine lubricant samples by Texaco. The tests shall be witnessed by the Wyle Test Engineer and a Wyle Quality Assurance Representative. The data oot:ined from the Baseline Functional Tests shall be used for comparison with the data obtained from the Post Radiation and Post Accident Functional Tests.
Greases In1 ASTM Standard Dropping point (melting) D 566 Cone Penetration D 217' Four Ball Wear D 2266 Oxidation Stability D 942 Oxtreme Pressure Properties D 2596**
Copper Corrosion D 4048 Corrosion Preventive Properties D-1743 Infrared Analysis
' Premium RB samples worked 60 strokes and worked 100,000 strokes /Marfak AP (Multifak EP 2) and Starplex 2 worked 60 strokes and worked 10,000 strokes.
- Test is not required for Premium RB samples since this type of gresse contains no extreme pressure additives.
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WYLE LABORATORita Huntsythe Pacikty
I Page No. 7 Test Report No. 40196 1 9.1.2 Funettonni Tests (Continued) ma y ASTM Standard Flash Point COC D 92 Oxidation Test D 2272 Rust Test D 665 Water Separability Test D 1401 Viscosity Test D-445 Color Test D 1500*
Copper Corrosion D 130 Foam Test D 892 Neutralization D 664" Extreme Pressure Properties D 2596" Four Ball Wear D 2266
' Color test (D 1500) is not required for Meropa oils since they are opaque.
- Neutralization test (D 664) is not required for Meropa oils since this type of test is not conducted for such oils. Neutralization (D 664),
Extreme Pressure Properties (D 2596), and Foar Ball Wear (D 2266) l 8 9.1.3 tests are not required for Regal R & O type oils since these are not inhibited to have antiwear proper;ies.
Acceetance Criteria The dropping point and cone penetration tests on the grease samples and the viscosity tests on the oll samples shall be used to determine acceptability of the lubricants. The acceptance criteria for each lubricant shall be determined by Texaco and documented in the Texaco report to be provided to Wyle Laboratories after completion of all testing. The test data for all other teste listed in Paragraph 9.1.2 shall be included in the Texaco report for information only.
9.2 Radiation Exposure The second and third samples of each lubricant shall be exposed to a radiation dose of 2.12E8 rads gamma, air-equivalent. The dose is the sum of the 10 year normal dose of 2.88E6 rads and the accident dose of 1.9E8 with a 10% margin added.
9.3 Post-Radiation Functional Test The functional tests described in Paragraph 9.1.2 shall be performed on the second sample of each lubricant by Texaco. The functional tests shall be witnessed by a Wyle Quality Assurance Representative.
(0 WYLE 1.A80RATORitS Heritsvwe Fac6taty
Page NO 8 Test Report No. 40196 I 9.4 Accident Simulation Test 9.4.1 Secelmen Prenaratio_n The cans containing the third samples of the lubricants shall be mounted on Wyle supplied test fixtures. The lids of the cans shall be suspended approximately one-eighth hch above the cans to allow exposure of the samples to the test chamber environment but to p; event the dripping of water into the cans. The specimens shall then be installe.1 in an accident simulation test chamber.
i 9.4.2 Chamber Instrumentatlog Three thermocouples shall be installed in the test chamber and mounted within '
, two inches of selected test specimens to monitor chamber temperature. The thertnocouple indicating the highest temperature prior to the accident test shall be used for control purposes during t'ae initial ramp. The average of the three thermocouples shall be used for control purposes for the remainder of the test.
A pressure transducer shall be provided to monitor chamber pressure. The three temperature indications, the average of the three temperature indications, and the chamber pressure shall be recorded at the maximum rate of the Data Acquisition System for the first 15 minutes of the test, at 15 minute intervals from the 15 minute point to the 24 hour2.777778e-4 days <br />0.00667 hours <br />3.968254e-5 weeks <br />9.132e-6 months <br /> point, and then hourly for the remainder of the test.
9..i.3 Aceldent Test The specimens shall be subjected to the environmental conditions specified on the test profile shown in Figure 1 in Appendix III of this section. The profile includes the appropriate temperature, pressure, and time margins required by IEEE 323. Prior 'o the initial ramp, the test chamber shall be stabilized at 120*F and held for a minimum of 30 minutes. The initial ramp shall be performed on a P tst effort basis.
1 9.5 Post Accidaat Functional Test The functional tests described in Paragraph 9.1.2 shall be performed on the third sample of each lubricaut by Texaco. The functional tests shall be witnessed by a Wyle Quality Assurance Representative.
10.0 PROCEDURES I The specimens werc subjected to the Radiation Exposure and Accident l Simulation Test Program described in Paragraph 9.0. The radiation exposure was performed by Itemedix, Inc. in Whippany, New Jersey. The functiond tests were performed at the Texaco Research Laboratory in Port Arthur, hxa: The i Baseline Functional Tests were witnessed by the Wyle Test Engineer and a Wyle Quality Assurance Representative. The Post Radiation and Post Accident Functional Tests were witnessed by a Wyle Quality Assurance Representative.
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Huntsvm Facmty
t Pcte N:. 9 Test Rep:rt Ns. 40195 1
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k 11.0 RESULTS
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The test report for the functional tests provided by Texaco is contained in Appendix L The certification for the radiation exposure is contained in AppenCir U.
Figures showing the required and actual temperature and pressure profiles for the Accident Simulation Test are contained in Appendix IIL Photographs showing the Accident Simulation Test Setup and the grease samples after compledon of the Accident Simulation Test are contained in Appendix IV.
A typical cornuter printot A tue data recorded during the Accident Simulation Test n 4.sta%d in Appendix V.
The instrumentation used forI the Accident Simulation Test is listed on the Instrumentation Equipment Sheet contained in '.ppendix VL Wyle Laboratories' Test Procedure 40196 00, Revision C, is contained in Appendix Vll.
Raw test data consisting of temperature charts, chamber surveillance records, and computer printouts from the Accident Simulation Test shall be provided to Alabama Power with this test report.
9 WYLE LABORATORIES Huntsen. F wmy
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APPENDIX 1 TEXACO TEST REPORT k
WYLE LABORATORIES tauntsviue Facmty
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s Test Report No. 40196 1
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FUNCTIONAL TESTS REPORT FOR TEXACO LUSRICANTS TEXACO REPORT NO. T-1
<8 Prepared B - -[4 Date: Y
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Checked By: C MA.A cate: s'/k/se Approved By.
Date: // fo I
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l Page No.14 Test Report No. 40195 1 REVISIONS Report No. T-;
Revision __ 0 Date: //,/.Td f f P Page or Paragraph Rev. No. Date Affected A Descrietion of Change S
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Pege No 15 Test Rep:rt No. 40196 1 Report No. T-1
(-(~g TABLI 0F CONTENTS Pace No.
1.0 objective 1 2.0 References 1 3.0 Lubricants Generic Group Identification, 3 Description and Test Sample Selection Rationale 4.0 Functional-Test Acceptance Criteria 7 5.0 Functional Tests 9 Appendix I - Lubricant Sample Identification I-1 Appendix II - Functional Tests Results II-1 Tab A Lubricant Summary Sheet - Premium RB II-2 Grease (New)
Tab A-1 Baseline Data Sheets II-7 Tab A-2 Post-Radiation Data Sheets II-18 Tab A-3 Post-DBA Data Sheets II Tab A-4 Instrumentation Equipment Shests II-35 Tab B Lubricant Summary Sheet - Premium RB II-38 Grease (4 Year old)
Tab B-1 Baseline. Data Sheets II-43 Tab B-2 Post-Radiation Data Sheets II-54 Tab B-3 Post-DBA-Data Sheets II-63 -
Tab B-4 Instrumentation Equipment Sheets II-72 Tab C Lubricant Summary Sheet - Marfak AP II-75 (Multifak EP2) Grease Tab C-1 Baseline Data Sheets II-80 Tab C-2 Post-Radiation Data Sheets II-91 Tab C-3 Post-DBA Data Sheets II-100 Tab C-4 Instrumentation Equipment Sheets II-109 Tab D Lubricant Summary Sheet - II-112 Starplex 2 Grease Tab D-1 Baseline Data Sheets II-121 Tab D-2 Post-Radiation Data Sheets II-129 Tab D-3 Post-DBA Data Sheets II-138 Tab D-4 Instrumentation Equipment Sheets II-147 11 (0
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Page No.16 Test Report No. 40196 1 TABLE OF CONTEtMS I
4 Pace No.
Tab E Lubricant Summary Sheet - II-150 Regal R&O 68 Oil Tab E-1 Baseline Data Sheets II-155 Tab E-2 Post-Radiation Data Sheets II-167 Tab E-3 Post-DBA Data Sheets II-177 Tab E-4 Instrumentation Equipment Sheets II-186 Tab F Lubricant Summary Sheet - II-189 .
Regal R&O 220 011 Tab F-1 Baseline Data Sheets II-194 Tab F-2 Post-Radiation Data Sheets II-205 ,
Tab F-3 Post-DBA Data Sheets II-214 Tab F-4 Instrumentation Equipment Sheets II-223 Tab G Lubricant Summary Sheet - II-226 Meropa 320 Oil Tab G-1 Baseline Data Sheets II-231 Tab G-2 Post-Radiation Data Sheets II-244 Tab G-3 Post-DBA Data Sheets II-254 Tab G-4 Instrumentation Equipment Sheets II-264 Tab H Lubricant Summary Sheet - II-267 Meropa 680 011 Tab H-1 Baseline Data Sheets II-272 Tab H-2 Post-Radiation Data Sheets II-285 Tab H-3 Post-DBA Data Sheets II-295 Tab H-4 Instrumentation Equipment Sheets II-305 Tab I Lubricant Summary Sheet - II-308 Rando Oil HD 68 Tab I-1 Baseline Data Sheets II-313 Tab I-2 Post-Radiation Data Sheets II-329 Tab I-3 Post-DBA Data Sheets II-341 Tab I-4 Instrumestation Equipment Sheets II-353 iii t'
Page No.17 Test Report No. 40196 1 Report No. T-1 OBJECTIVE
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1.0 1.1 The lubricants in this program vill be exposed to high radiation and Design Basis Accident (DBA) tests to verify that lubricants can perform their intended functions despite these harsh environmental conditions. Prior to the environmental tests, after the radiation exposure and after the DBA testing, ASTM functional tests will be conducted. This report describes the baseline functional tests, the functional tests after the radiation exposure and after the design basis accident. The purpose of these functional tests in the qualification test program is to demonstrate that the performance characteristics and the lubricating properties of Texaco lubricants remain within Texaco's acceptable (required) values after being subjected to 1.he entire test program.
1.2 The functional tests which shall be performed on the lubricants for acceptance criteria purposes are identified in Section 4.0 of this test report. Other ASTM tests performed on the lubricants and identified in this report are for information only.
2.0 REFERENCES
2.1 Wyle Test Procedure No. 40196-00, Rev. C IEEE 323-1974 " Standard for Qualifying Class 1E Equipment (8
2.2 for Nuclear Power Generating Stations" 2.3 ASTM-D566 " Standard Test Method for Dropping Point of Lubricating Grease", December 1987 2.4 ASTM-D217 " Standard Test Method for Cone Penetration of Lubricating Grease", November 1986 2.5 ASTM-D2266 " Standard Test Method for Wear Preventive Characteristics of Lubricating Grease (Four-Ball Method)",
December 1986 2.6 ASTM-D2272 " Standard Test Method for Oxidation Stability of Steam Turbine Oils by Rotating Bomb", December 1985 2.7 ASTM-D92 " Standard Test Method for Flash and Fire Points by cleveland Open Cup", December 1985 2.8 ASTM-D665 " Standard Test Method for Rust-Preventing Characteristics of Inhibited Mineral' Oil In the Presence of Water", November 1983 2.9 ASTM-D1401 " Standard Test Method for Water Separability of Petroleum Oils and Synthetic Fluids", January 1985 1
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Pate No.18 Test Report No. 40196 1 Report No. T-1 2.10 ASTM-0942 " Standard Test Method for Oxidation Stability of Lubricating Greases by the Oxygen Bomb Method", October 1978 2.11 ASTM-D2596 " Standard Test Method for Measurement of Extreme-Pressure Properties of Lubricating Grease (Four Ball Method)", December 1987 2.12 ASTM-D1743 " Standard Test Method for Corrosion Preventive 4
Properties of Lubricating Greases", July 1987 2.13 ASTM-D4048 " Standard Test Method for Detection of copper Corrosion from Lubricating Grease by the Copper Strip Tarnish Test", December 1986 2.14 ASTM-D445 " Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)", December 1986 2.15 ASTM-D1500 " Standard Test Method for ASTM Color of Petroleum Products ( ASTM Color Scale)", Canuary 1988 2.16 ASTM-D130 " Standard Test Method for Detection of Copper corrosion from Petroleum Products by the Copper Strip Tarnish Testa, January 1984 I
2.17 ASTM-D892 " Standard Test Method for Foaming Characteristics of Lubricating Oils", October 1974 2.18 ASTM-D664 " Standard Test Method for Neutralization Number by Potentiometric Titration", December 1987 2.19 Wyle Laboratories Quality Assurance Program Manual, April, 1987 .
2.20 Texaco Lubricating Oil, Grease and Antifreeze Coolant Digest, 1988 2.21 Texaco Product Data Book, U.S. Manufacture, Research, Environment & Safety Department, Beacon Research Laboratories, 1982 Edition 2.22 Texaco Manufacturing Specifications Book 2.23 Texaco Research Report No. 4450-415, May 31, 1984 4 2.24 Texaco Research Report No. 4450-416, May 31, 1984 2.25 Texaco Research Report No. 4450-417, July 30, 1984 2.26 Texaco Research Report No. 4850-62, July 18, 1985 2
Page No.19 Test Report No. 40196-1 Report No. T-1
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3.0 LUBRICANTS GENERIC GROUP IDENTIFICATION, DESCRIPTION AND TEST SAMPLE SELECTION RATIONALE 3.1 Representative samples of lubricants shall be tested in this program. This section provides the description and engineering rationale for the selection of lubricants which are to be type tested in the qualification program. Typical test data are provided for each of the lubricants included in the test program.
These typical test data represent an average of a number of tests obtained on batches of each of the products and represent average typical characterjstics. These data are subject to normal batch-to-batch variations. The lubricants selected for type teating and engineering rationale for their selection are provided in Section 3.3 of the test report, their description and the typical test data are provided below:
3.2 DESCRIPTION
OF LUBRICANTS 3.2.1 Premiun RB (Nevi Premium RB Grease is a No. 2 grade brown, buttery lithium soap, oxidation and rust resistant grease made with a highly refined mineral oil. It is very shear stable and water resictant, and
] gives quiet bearing operation.
Dropping Point, 'F: 395 Penetration
( Worked (60 strokes): 280 Worked (100,000 strokes): 297 Points Change: +17 3.2.2 Premium RB (4 Year Old)
Premium RB Grease is a No. 2 grade brown, buttery lithium soap, oxidation and rust resistant grease made with a. highly refined mineral oil. It is very shear stable and water resistant, and gives quiet bearing operation.
Dropping Point, 'F: 395 Penetration Worked (60 strokes): 280 Worked (100,000 strokes): 297 Points Change: +17 3
Page No. 20 Test Report No. 40196 1 Report No. T-1 ,
3.2.3 Marfak AP (Multifak EP 2)
Marfak All Purpose (Multifak EP 2) is a brown, oxidation resistant lithium soap grease which contains a non-lead extreme pressure additive package. It is very shear stable and provides ,
high-load-carrying capacity, excellent rust protection, corrosion resistance, resistance to water washout, and has good pumping capabilities at low temperatures and in centralized lubrication systems.
Dropping Point, *F: 382 Penetration Worked (60 strokes): 278 Worked (10,000 strokes): 279
% Change: <1 3.2.4 Staroler 2 Starplex 2 is a lithium complex soap grease which contains a specially formulated extreme pressure additive package. It provides excellent rust protection and resistance to water washout. Starplex 2 is suited for industrial bearing applications involving heavy loads, elevated temperatures and wet conditions.
Dropping Point, 'F: 450 minimum Penetration Worked (60 strokes): 282 Worked (10,000 strokes): 289
% Change +2 3.2.5 Recal R&O 68 Regal Oil R&O 68 is a premium grade oil formulated to meet the stringent rust and oxidation requirements of steam and gas turbines,* hydraulic systems and air compressors. Regal Oil R&O 68 is formulated with highly refined -paraffin distillate stocks. ,
it contains a carefully balanced rust and oxidation inhibitor package and an effective anti-foamant.
Viscosity cst at 40*C: 64.7 cst at 100*C: 8.3 3.2.6 E12a1 REO 220 Regal Oil R&O 220 is a heavy bodied lubricating oil manufactured from a combination of paraffin distillate and residual base stocks. The additive package includes rust and oxidation inhibitors and an anti-foamant.
Viscosity cst at 40*C: 201 cst at 100'C: 16.9 4
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l-Page No. 21 Test Report No. 40196 1 Report No. T-1 (O 3.2.7 Merona 320 Meropa 320 is a industrial gear oil blended from a high' quality paraffin distillate stock and a residual base stock. This product contains a sulfur-phosphorus EP antivaar additive and a pour point depressant.
Viscosity cst at 40*C: 337 cst at 100'C: 24.9 3.2.8 Merona 680 Meropa 680 is a industrial gear oil blended primarily with a residual base stock. A small amount of a high quality paraffin base stock is also present. Meropa 680 contains a sulfur-phosphorus EP/antivaar. additive and a pour point depressant.
Viscosity cst at-40*C: . .
672 cst at 100*C: 38.8 3.2.9 Rando Oil HD 69 Rando 011 HD 68 is a light-colored, premium, anti-wear hydraulic oil blended from high quality paraffin distillate stocks with excellent stability. It is rust and oxidation inhibited and contains a specially selected anti-foamant.
( Viscosity cst at 40'C: 61.5 cst at 100'C: 8.2 3.3 ENGINEERING RATIONALE FOR LUBRICANT SELECTION An engineering rationale for the basis of the lubricants selection which are needed to be type tested is provided in Sections 3.3.1 through 3.3.9.
3.3.1 himium RB (New)
The new sample of Premium RB grease is a single grade product not representative of any other product of this type. Therefore no additional rationale is required.
3.3.2 Premium RB f4 Year Old)
The naturally aged sample of Premium RB grease is included for comparison to the unaged sanple. It also is not representative of any other product of this type so additional rationale is not required.
5 rS 9
Page Ns. 22 Test Repsrt Ns. 40196 1 Report No. T-1 3.3.3 Marfak AP (Multifak EP2)
Marfak AP (Multifak EP2) grease is representative of the Multifak EP series, which also includes Multifak EPO and Multifak EPl.
The rationale for this representation is as follows:
Multifak EP 2 was selected to be tested because it is the most widely used member of the Multifak EP Series. Its composition is representative of Multifak EP 1 and Multifak EP 0, except for thickener content. Multifak EP 2 typically contains 7.5 wt.%
thickener, as compared to 6.0 wt.% thickener for Multifak EP 1 and 4.0 wt.% thickener for Multifak EP 0. Since Multifak EP 2 contains the highest amount of thickener, the results of the tests on Multifak EP 2 would be more pronounced than for the 1 and 0 grade products. Any property changes (including penetration and dropping point tests used for functional test acceptance) for Multifak EP 2 would envelope the same property changes for Multifak EP 1 and Multifax EP 0.
3.3.4 Starnier 2 starplex 2 grease is a single grade product which is not representative of any other product of this type so additional rationale is not required.
3.3.5 Recal RLO 68 Regal R&O 68 oil is representative of Regal R&O 32 and Regal R&O )
- 46. The rationale for this representation is as follows:
Regal Oils R&O 32, 46 and 68 contain the same type of base stocks. As viscosity of base stocks increase, the harder they are to inhibit against oxidation. Therefore, the 68 grade product was selected for testing since this product contains the highest percentage of the high viscosity base stock used in these three products.
3.3.6 Recal R&O 220 Regal R&O 220 oil is representative of Regal R&O 150. The rationale for this representation is as follows:
Regal Oil R&O 150 contains two refined paraffin distillate stocks, whereas Regal Oil R&O 220 contains a combination of paraffin distillate and residual base stocks. Since residual base stocks are harder to inhibit against oxidation, Regal R&O 220 was selected for testing.
6 8'
l Page .No. 23 Test Report No. 40196 1 3.3.7 Maroca 320 Meropa 320 oil is representative of Meropa 68, Meropa 150 and Meropa 220. The rationale for this representation is as follows:
Meropa Oils 68, 150, 220 and 320 contain the same type of base stocks. As viscosity of base stocks increase, the harder they are to inhibit against oxidation. Therefore, the 320 grade product was selected for testing since this product contefr.s the highest percentage of the high viscosity base stock used An these four products.
3.3.8 Merona 6B0 Meropa 680 oil is not representative of any other oil, so additional rationale is not required.
3.3.9 Rando Oil MD 68 ,
Rando Oil HD 68 is representative of Rando Oil HD 32 and Rando Oil HD 46. The. rationale for this representation is as follows:
Rando Oils HD 32, 46 and 68 contain the same type of base stocks.
As viscosity of base stocks increase, the harder they are to inhibit against oxidation. Therefore, the 68 grade product was selected for testing since this product contains the highest g percentage of the high viscosity base stock used in these three products.
4.0 FUNCTIONAL TEST ACCEPTANCE .CBIIEET&
4.1 The penetration and dropping point for the grease and viscosity for the oil shall remain within the manufacturer's specified range when the test sample is subjected to ASTM tests ,
as noted below or justification shall be provided for their suitability in the given application. Other functional tests per ASTM standards as identified in Appendix II are for information only. The manufacturer's specified range for each tested lubricant for acceptance criteria purposes is noted in '
Sections 4.1.1 through 4.1.9.
4.1.1 Premium RB (New)
ASTM-D566, Dropping Point, 'F: 385 minimum ASTM-D217, Penetration Worked (60 strokes): 265-295 Worked (100,000 strokes): 245-315 .
Points Change: 120 maximum
(
Page No. 24 Test Report No. 40196 1 4.1.2 Premium RB (4 Year Old)
ASTM-D566, Dropping Point, *F: 385 minimum ASTM-D217, Penetration Worked (60 strokes): 265-295 Worked (100,000 strokes): 245-315
' Points Change: 120 maximum 4.1.3 Marfak AP (Multifak EP2)
ASTM-D566, Dropping Point, 'F: 350 minimum ASTM-D217, Penetration Worked (60 strokes): 265-295 Worked (10,000. strokes): 238-325
% Change 110 maximum 4.1.4 Starelex 2 ;i ASTM-D566, Dropping Point, 'F: 450 minimum ASTM-D217, Penetration Worked (60 strokes): 265-295 .
Worked (10,000 strokes): 278-310 g % Change +5 maximum 4.1.5 Recal R&O 68 k
ASTM-D445, Viscosity cst at 40*C:
4.1.6 cst at 100*C:
Recal R&O 220 61.3-67.8 7.6 minimum 9
ASTM-D445, Viscosity cst at 40*C: 200-211 cst at 100*C: 16.84 minimum 4.1.7 Mereen 320 ASTM-D445, Viscosity cst at 40*C: 290-340 cst at 100'C: 21.67 minimum 4.1.8 Mercea 680 ASTM-D445, Viscosity cst at 40'C: 610-720 cst at 100*C: 35.19 minimum 4.1.9 Egndo Oil HD 68 ASTM-D445, Viscosity cst at 40*C: 61.3-67.8 cst at 100*C: 7.97 minimum 8
Page No. 25 -
Test Report'No. 40196 1-l
/- Report No. T-1 5.o IMLCT10NAL 'IESTS 5.1 REQUIREMENTS 5.1.1 visuai Ynanaction A visual inspection of all lubricants shall be performed by Texaco to determine any visual signs of degradation-(appearance, color, and odor) . Any noticeable differences in color, or other physical attributes between items of same type shall be noted.
All observations shall'be recorded.- Test lubricants identificat.an shall be checked and recorded. Test samples shall '
be ucrked to maintain their identity throughout the test program.
5.1.2 Functional Tests The functional tests shall be performed to determine the lubricating properties and the performance characteristics of each lubricant prior to.and after the radiation exposure test and the design basis-accident-test. The baseline functional test shall provide a basis for comparison with'the data obtained from the post-radiation and the post-DBA functional tests. Each functional test shall be performed in accordance with the applicable ASTM standard-test method as identified on each lubricant summary sheet included in Appendix II. : The functional 8
tests shall be witnessed'and inspected by Wyle Laboratories-technical and Quality Assurance personnel.
Any deviation from the ASTM standard test-method during the functional test shall also be identified and, documented. Any.
anomaly noted during the-test shall also be-noted and analyzed.
All observations and test data shall be recorded.
5.2 PROCEDURES _ _
5.2.1 visual Insnaction A visual inspection of each lubricant shall be conducted before the start of the baseline,- post-radiation ar.d. post-DBA functional
~
test. A vistal inspection of each lubricant shall be performed._
by Texaco personnel when the lubricants are received at Texaco's '
Port Arthur Research Laboratories located at Port Arthur, Texas initially from Texaco lubricants manufacturing locations as identified in Appendix I, from Isomedix,:Inc. in Parsippany, New -
Jersey for post-radiation functional testing and from Wyle Laboratories in'Huntsville, Alabama for post-DBA functional-testing. .The' inspection shall ensure that the lubricants have no visual evidence of damage- to the color and torture. - The 9
9 l
l Pageflo.26 Test Report No. 40l961 Report No. T-1 lubricants identity shall be checked and recorded on the inspection form. The test sample shall be tagged with Quality Assurance " Test Sample" tags to ensure their identification 6)'
throughout the test program. The test samples shall be prepared by Texaco from the lubricants whose identification (batch number, code number, etc.) is provided in Appendix I. A test sample from each of the nine (9) lubricants needed to be functionally tested is identified in Appendix I.
5.2.2 runctional Tests 5.2.2.1 Each lubricant test sample shall be subjected to the functional testing in accordance with the precedure and the requirements of the applicable ASTM standard test methods.
5.2.2.2 The functional tests shall be witnessed and inspected by Wyle Laboratories technical and Quality Assurance personnel.
5.2.2.3 Functional test data shall be measured and recorded per ASTM standard test method requirements.
5.3 RISULTS 5.3.1 Visual inspection and functional test results for each lubricant tested are included in a lubricant summary sheet included in Appendix II. The summary sheet shows the visual inspection and functional test results for baseline, post-radiation, post-DBA and the acceptable (required) manufacturer's specified range.
Data mi.asts showing the data recorded during the functional tests are contained in Appendix II.
Equipment used in recording data is shown on Instrumentation Equiprent Sheets contained in Appendix II.
10 0'
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ . _ _ _ _ _ _ _ _ _ _ _ _ il
Page No. 27 Test Report No. 40196 1 Report No. T-1 3
)
)
APPENDIX I LUBRICAl'T SAMPLE IDENTIFICATION 8 ,
W I-1
(
Page No. 28 Test Report No. 40196-1 Report No. T-1 Test samples subjected to functional testing were prepared from the lubricants as identified below. A group of three test samples from each of the nine lubricants noted below was prepared by Texaro. The first group of test samples (total of nine lubricants) remained at Texaco's Port Arthur Research i
Laboratories (PARL) in Port Arthur, Texas for baseline functional testing. The second and third group were shipped to the -
radiation facility (Isomedix) for radiation exposure. After the radiation exposure, the second group was sent back to Texaco 3 Laboratories for post-radiation functional testing whereas the third group was shipped to Wyle Laboratories for DBA testing.
. After the DBA test, the third group of test samples was also sent back to Texaco Laboratories for post-DBA functional testing.
Each test sample before the start of the baseline, post-radiation and the post-DBA functional testing was identified by a test i sample identification number assigned by Texaco as identified below:
- 1. Premium RB Grease (New)
Baseline Test Sample No.: 468-88-1248-001 Post-Radiation Test Sample No.: 468-88-1248-200 Post-DBA T2st Sample No. : 468-88-1248-300 Quantity: 5 lbs.
Product Code: 1939 Manufacturing Location: Southwest Petro Chem.,
Bakerstown, Pennsylvania Batch No.: QG805232 Fill Date: 062388 Sot,aence No.: 0004 Storage Loc.: C-9-B (PARL)
- 2. Premium RB Grease (4 Year Old)
. B:seline Test Sample No.: 468-88-1259-001 Post-Radiation Test Sample No.: 468-88-1259-200 Post-DBA Test Sample No.: 468-88-1259-300 Quantity: 5 lbs.
Product Code: 1939 Manufacturing Location: Scuthwest Petro Chem.,
- Olathe, Kansas Batch No.
- QD251 Fill Date: 030784 Sequence No.: N/A Storage Loc.: R-3SHED (PARL)
- 3. Marfak AP (Multifak EP21 Crease
- Baseline Test Sample No.: 468-88-1257-001 Post-Radiation Test Sample No.: 468-88-1257-200 Post-DBA Test Sample No.: 468-88-1257-300 Quantity: 5 lbs.
I-2 Ill)
Page No. 29 Test Report No. 40196 1 4
Product Code: 0995 Manufacturing Location: Southwest Petro Chem.,
Bakerstown, Pennsylvania Batch No.: QG807153 Fill Date: 072088 Sequence No.: 0073
) Storage Loc.: C-9-E (PARL)
- 4. Starolex 2 Grease Baseline Test Sample No.: 467-88-8173-001 Post-Radiation Test Sample No.: 467-88-8173-200 ,
Post-DBA Test Sample No.: 467-88-8173-300 Qvntity: 5 lbs.
Product Code: 1935 Manufacturing Location: Texaco Research Labs.,
Port Arthur, Texas Batch No.: 467-88-8173-000 Fill Date: 082588 Sequence No. : N/A Storage Loc.: 151-12-5-0 (PARL)
- 5. Recal R&O 68 011 Baseline Test Sample No.: 446-88-0101-000 Post-Radiation Test Sample No.: 446-88-0109-000 0 Post-DBA Test Sample No.:
Quantity:
Product Code:
Manufacturing Location:
446-88-0118-000 1 gal.
0702 Texaco charleston Terminals, Charleston, South Carolina Batch No.: TC2150 Fill Date: 081788 Sequence No.: 0332 Storage Loc.: 131-5-3-0 (PARL)
- 6. Recal R&O 220 Oil Baseline Test Sample No.: 446-88-0092-000 Post-Radiation Test Sample No. : 446-88-0108-000 Post-DBA Test Sample No.: 446-88-0119-000 Quantity: 1 gal.
Product Code: 1531 Manufacturing Location: Texaco Charleston Terminals, Charleston, South Carolina Batch No.: TC1744 Fill Date: 070688 Sequence No.: 0006 Storage Loc.: 131-6-6-3 (PARL)
l Page Ns,30 Test Repset Nt. 40196 1
- 7. Maroca 320 011 Baseline Test Sample No.: 450-88-0058-000 Post-Radiation Test Sample No.: 450-88-0063-000 Post-DBA Test Sample No.: 450-88-0067-000 Quantity: 1 gal.
Product Code: 2324 Manufacturing Location: Texaco Charleston Terminals, Charleston, South Carolina Batch No.: TC1132 Fill Date: 050488 Sequence No.: 0032 Storage Loc.: 131-6-5-2 (PARL)
- 8. Merona 680 Oil Baseline Test Sample No.: 450-88-0056-000 Post-Radiation Test Sample No.: 450-88-0064-000 Post-DBA Test Sample No.: 450-88-0068-000 Quantity: 1 gal.
Product Code: 2342 Manufacturing Location: Texaco Charleston Terminals, Charleston, South Carolina Batch No.: TC088 Fill Date: 041288 Sequence No. 0166 Storage Loc.: 131-6-5-1 (PARL)
- 9. Rando 011 MD 68 011 Baseline Test Sample No.: 444-88-0107-000 Post-Radiation Test Sample No.:
444-88-0143-000 Post-DBA Test Sample No.: 444-88-0161-000 Quantity: 1 gal.
Product Code: 1659 Manufacturing Location: Texaco Charleston Terminals, Charleston, South Carolina Batch No.: TC1902 Fill Date: 072688 Sequence ho.: 0332 Storage Loc.: 131-6-5-1 (PARL)
I-4 i
Page No. 31 Test Report No. 801961 Report No. T-1
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APPENDIX II FUNCTIONAL TESTS RESULTS 9
II-1 f
I
Page No. 32 Test Report No.' 40194 1 Report No. T-1 p
TAB A LUBRICANT
SUMMARY
SHEET PREMIUM RB (NEW) cPJASE II-2 8'
mm
~
6 i
+
- e t eepost so. f-t l
itMCil0NAL ffSit RESULf 5 tuseltant asewtf safti - Vl9)At le5PEC110m seseline Sample Idetif tentlan so.t 468-88-1268-001 if 51 SmPLE t Praefue as (new) Post-Redietten Sample Identificetters No.: 468 88-1248-200 Post pt4 Sayle ldmttfleetlan so.: 668-88-1268 393 pe<estrett Reuerks Post-Redf et f ert Post-ce4 Vleuel frosectlert MilfM .
Smooth, Samoth, Sesoth, Samoth, tuttery W ence Suttery M tery Suttery Note 1 p
Dark Red $rteet Sremet Dark Brown flie O Color to steck WoteI 2 an Surface; ~ g Bulk color Brown file en 4 *tf Surface; E$
Bulk Color
- 21 u se Silsht Slight Adfitive $llsht Slight O Otor AdfltIvs Addltive Adit tive $.
" i mens none unne bene Sollds (Particles) foaminetters
!D.J.Ut Surface esidotters cet ~
- 1. Dark trous surface film truficative of ontdetfart et surface interf ace with alr.
reneidered to adversely degrade performance el the testk greese.
- 2. Dark red color ret coreldered tenseuel edwes emine entioxiderste of the type arsed in this libricant are esposed to elevated temperatures. the tAack surf ace film lauficettve of further ontdetten et surface Surf ace esidation set coresidered to adversely degrade perforsme of tese bulk greese.
interf ace with air.
Il-3 2
1
- - - - - - - - - - i
Report me. I-l ftarClious Tests RESULf 8 tteeltAst sueuRT SMEEI
- A$fM ffff$
itt! $ApePtEs Premium as (sou) Basetine sample Identificat'en No.: 466-08-1248 001
- Post sadletten Sampie IdentIficatfan me.: 468-88 1248 200
- est-004 Sample Identification me.s 468 88-1248-300 I l
I Se<ailredts) Seestt e functional 1331 EttillfW f25t-R adiatim Post 984 H
en 391 398 391 385 min.
orgpieg Point, *f (ASIN 0 566) 53 to Penetratten 2S (ASIM D-217) See setice of Anmenty *z *g 363 305 265-20 Worted (68 strokes) 284 ??
342 30T 245-315 mos.1 aruf 2.
wrted (100,000 strates) 288 8I
-21 e2 +20 sea. See setice of Anmmely Points Charge 0 :;;
- e. 3
?
w far Ball war, sun 0.69 0.48 0.69 0.T(b)
(A$iN 0 2266)
Osidation Stabilley (ASTM D-942) pel d ep 8 100 hr. 5 5 to 10 man.
IT 20 (c) 18 ans.(d) See notice of Anasty 8 500 br.
No. 4 Corrosien Preventive Preperties Pese Pass Pese Pass (ASIM t-1T41)
Cegper Carrosim la la le ib man.(e)
(Astm 0-4048) snte ered Analysis no change no change si Change st andudt f)
Ie 4
^ - .
m
~
- O Seport No. T-1 N0ff1:
(a) tkitees otherstee noted, dets from fesoco Manuf acturleg Speciffcatione seek (inetteled teufer feb A-1).
(b) nealam llelt ceneldered by fenece for non-tP type gresse such as thfe prodzt that de not emteln entlueer arkfttisee.
(c) Estended tesub esidstlen (500 bre) test was not rtes en post-dea enspie airce 100 hre result was etitt within rewired lletto and ett prevleus 500 hre results were well betens typical welus.
416. (Deport en tenece*e file at PARL)
(d) Seele refererte deve reported in Tenece Research separt me. 4450 Ne ptb(Ished date avaitsbte.
(e) typlest volus canaldered by tesace booed en esperlerre with this prairt.
(f) Standard SE seen for thle intricant inctisied neuser isb A 1.
q motite of Anaestr =
~
~~
The canelaterry wee ulthin
- 1. The poet-redletlen osupte had softened outelds the me. 2 grade range (265-295). M the me. 8 grade range (355-385) editch le within the acceptable ceneisterry range for the esplicotten of 3 Prashee SS grosse. The other primertlee of the prodzt (carroelen eruf osidation reelsterrel were rust 2S affected by the redletten espesure. TZ
- 2. The omrted (46 streses) penetretten ef ter the poet-dea test woe elightly eutelde but very near the me. 2 Asa grade tarse (265-295). It le reted that the oef ten!ng ef fect of the redleticre mes comter-belenced ty the o herdoning ef fect of the 304 ervrirersant test such that the everett consletency of the sospie efterged only -
frces the Inittet (beeetire) 288 pmetretten to the finst 305 penetretten. This slight thenge In consletency le not ceneidered detrienntet to the setlefectory perforeerre of the predzt.
- 3. Altheugh the canaletency of the post-redletlen eespie esse sof ter then the Be. 2 grade range (see N.O.A.
me.1) the prodzt eahlbited no further settening evers prolonged sheering, and actustly hardmed sceneet, edsich Indicates that the fiber structure of the thickerer ese not degraded by the redletten espesure. Even thcugh the 23 pointe change in penettetles le cutelde the respaired 20 points change es, sines. thle change Indiretes to degradetion of the sheer etability of the grease end therefore le not canel& red detrimmtet to the setlefectory performance of the predzt.
- 4. Post redletters result slightly esceeds rerpsired value but entdetion etability carmidered within acceptable limit for graviding acceptable libricetleri, the result of 20 le else within the test repeatsbility to the re w ired welue of 18.
It 5 r , --
L_
Page No. 36 Test Report No. 40196 1 9
W I 2 s l IIll la r= '
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1,5 :.ui 1 1111 11 u $
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i Page No. 37 Test Peport No. 40196 1 l
Report !!o. T-1 1
(
h i
4 e
l TAB A-1
! BASELINE DATA SHEETS O
l 1
i II-7 l
1
'S
. . - - . . . - . _ .-...--..---.--..-_._.-....-..._u.,_.---,-_...,-...,.-.--.-.. .. . . . . . - . - . . - . -
F unc t a can [ ]
g bt HL t t4 31 - - - - - - - - - - - - - -
-- Page No. II-3
_ _ - - - - - ------------- GLNER AL REStL T S REIR I EVAL -
Report No. T-1 Ss.nple Id: 460-110-1243-008 Pr oaer t No. : 4450 its e t s als DAT g Pr uduc. t Naane:18HEMIUM RD GREASE Pr odoc t Code 1939 Tests Pending O Not es.:
g Login:OG/24 /B0 10:36 Ver 4 F icat ion 09/03/D0 12:21 Cosept et s on 09/20/CD 10:30 Additional Notes? N RESILTS I Sf'ECIFICATIONS g REStLT I ESTIMATE TYPE MAX It1UM MINIMUM TEST CODE SHORT NAME LAB 00181 DROP PT F PAP 391 i ST, 350 00243 OK.S.100H PAP 5 8 g 17 I 01017 OK-STABLOO PAP
. . 40136 PEN, UNWK PARL 279 8 40138 PEN. WK FARL 208 1 40340 PEN 100000 PARL 283 I
. 40101 DROP P T, F PARL 393F i ST. 350 44299 CSC24/100C PARL 1A I 45151 4-DALL WEA PARL .69 8
,-4 45169 RUST PR.R PARL 1 I =
a SLREUJ 31 Faeric t ic.c. t )
h o m
_ = - - - - - _ _ _ . - - - - - -
GENERAL RESILTS REIRIEVAL -
Sam.ple Ius 460-011-1240-001 Pr ce.st c t No. : 4450 l es i t s a l s.:!V.i Pr odue t Code: 1V39 Pr oduct Ni.nne: PREMIUM RC GREAE hh 1 es. t t. Pesett i rey O Notes.: G Logie. OD/?4 /D's 18:36 Ver e r sc at ion 09/03/UU 12:Pt Coing.let ic.ri OV/20/DU 10:30 Additiunal Notes? N RESta is TEST CODE SHORT NAME L At: Stt SLE_T I ESTIMAIE TYPE XI I gnain 45570 RtST PR.A PAf(L (ni :
65835 IR GR FILM PARL Suet 1I T I I .
I I
- Test codes 40136 and 40181 not appitcable I to functional tests - included for Texaco e ir.fonnation only I I
I O .
O O -
i, .
rage no. .a.y Page Ns.39 Report No. T.1 Test Report No. 401961
(
TEXAC6 Mf,N7F/CM,11N3 SPECIFICATIONS 300K FACE NO. G.072C3 FACE BIV. DATE 06/01/88 F10 DUCT CODE 01939 FRIMIUM 13 ca. East MANUFACTUPID AT 3AKTVN MINIMVM MAXIMLM IFECITICATIONS...
FIN VK D 0217 265 193 FEH VK 100.000 STRKS, CRANCE. FOINTS +/.20 CROFFING 70!NT. T D 0366 305 RVET TEST. RATING D 1743 1 CXID STAB CPIASE D 0942 SOMB METHOD. FFJ55 DROF 100 ERS. F5I 10 0 .
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TEX ACO INC.,2000 Westcheeler A.e., White Pleine, N. Y.10650 '. I,.. '**
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CODE No.1939 PREMIUM RB GREASE g Typical Characteristics
^
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Lithium Soap, % 15.3 L, '
Penetration, ASTM at 77'r , ,
Unworked
- 237
]l.
1 Worked 280 j Dropping Pt., or 395 <
011 Viscosity, cst at 40'C 129 '
s
, cst at 100'C 12.9 '0._
SUS at 100'r 676 . ,
SUS at 210'r 71.0 :s p Guide te Usable Temp.
Max., 'T 350 .
Hin., 'T -30 'd '
Max. for Prolonged Period, 'r 325 1 5i -
Premium RB Grease is a No. 2 grade brown, buttery lithium , 4hq,'s .,
soap, oxidation and rust resistant grease made with a highly - -
refined mineral oil. It is very shear stable and water l l resistant, and gives quiet bearing operation. ,
In extensive simulated service and field tests by major 8 bearing manufacturers and other users, Premium RB Grease has consistently demonstrated its ability to provide lubrication for extended periods at high temperatures. It is recommend-ed for all ball and roller bearings in electrical, indus-l, trial and automotive service where temperatures up to 325'r ;I are expected. It will allow starting and running of bear-y' .
ings down to about -30'r. l a
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_ _ _ _ _ _ _ _ _ _ . . - - - - - ----- GENER AL REStJLT S RET R IEVAL ------- --- --
Sample Id 460-09-1240-200 Pr o iec t No. : 4450 Initials:DAT Pr oduc t Code 1939 Product Name: PREMIUM RC GREASE Tests Pending: O Notes:
Login:10/03/08 14:43 Ver i f itct ion: 10/17/00 14: 51 Comp 1ttson:11/29/f:0 13:40 Additional Notes? tl RESULTS I SPECIF ICAT IDt!S RESULT I ESTIMATE TYPE MAXIMUM MItttMt>M TEST CODE SHORT NAME LAB 00101 DROP PT F PAP 390 ! ST. 350
, 00343 OX.S.100H PAP 5 1 01017 OX-STA0500 PAP 20 1
40140 PEN 100000 PARL 342 I
45151 4-DALL WEA PARL .40 I ~
45169 RUST PR.R PARL 1 1 SCREEN 31'
~ ~~~~
GENERAL RESULTS RETR IEVAL - _ _ _ _ _ -- oo,,
Ah Sample Id: 460-09-1240-200 Praject No.: 4450 f re i t i al s:DAT 3*
Product Code 1939 Product Name:PREMItiM RB GREASE Tes ts Peridirigt O Notes: $
Login 10/03/DD 14:43 Ver ification 10/17/DD 14:51 Com.pl et irm: 11/29/DD 13:40 Additional Notes? N l
RESULTS I SI'EC t r1CATIOfin TEST CODE SHORT NAME LAB RESULT I ESTIMATE TYPE NAXIMUM MINIMUM 45170 RUST PR.A PARL DK I 65115 IR GR FILM PARL SUBMIT I I
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Pace No.57 Test Report No. 40196 1 Report No. T-1
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O TAB A-3 POST-DBA DATA SHEETS 8
4 II-26
<g 1 I
SCRIEN 31 F unc t t on [ ]
- - - -- - - -- GENER AL R ESt iL T S R E T R I EVAL ------- - -- - -
^ Sample Ida 468-00-1240-300 Pr o ier t No. : 4450 Initials:DAT Product Code:1939 Product Nname: PREMIUM RB GREASE Tests Pending: 1 Notes:
Login:11/OD/DD 00:29 Verification 11/13/DD 13:21 Cosapletion: 00:00 Additional Notes? N RESULTS I SPECIFICATIONS TEST CODE S140RT NAME LAD RESULT I ESTIMATE TYPE MAXIMUM MINIMim l 00101 DROP PT F PAP 393 i ST. 350 00243 OX.S.100H PAP 10 1 01017 DX-STADSOO PAP --
t
- 40101 DROP PT, F PARL 397 1 3T. 350 -
44299 CSC24/100C PARL 1A I 45151 4-DALL WEA PARL .69 i e 45169 RUST PR.R PARL 1 i
.a y SCREEN 31 Function [ ] 2 GENERAL RESULTS RETRIEVAL ------------ - - - - - - - - - - - E 33 Sample Id: 460-08-1240-300 Pro. ject No.: 4450 Initials:DAT ,;
Product Code:1939 Product Name: PREMIUM RD GREASE o **
Tests Pending: 1 Notes: %
Login 11/OD/DD 00:29 Verification:11/13/DD 13:21 Complettosi: 00:00 .:. l Additional Notes 7 N :
RESULT S I SPECIFICATIONS l TESY CODE SHORT NAff. LAB RESULT I ESTIMATE TYPE MAXIMUM MINIMUN 45170 RUST PR.A PARL OK I 65115 IR GR FILM PARL StK:MIT I I
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- Test codes 40136 and 40181 not i applicable to functional tests - e included for Texaco information only :
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i i WYLE LABORATORIES Muntswne Facauty
4
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tepart so.1-1 INSTAleENIAFloit EGURP9ENT $NEET
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- M -DSA functlenol
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stperler ties ----- 0 1001 ---- -- --- 0$M 1 rouerstet Elect. Co. H
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IIet tler FP90 ll67956 0-$72F *, 0.1f --- -~
N/A 12 Central Procesoor, 13 Dreppice seettler IP83 e67973 0-$T2f + 0.1f -- -~ N/A Point Cett '
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N/A N/A -~ -- Infrared phete.eeer Eleeurr AnaIysis bettenal ---- ---~ N/A N/A -- --- D 1743 15 oven Agpliance Co.
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I Page No. 71 Test Report No. 40196 1
- Report No. T-1 TAB B LUBRICANT
SUMMARY
SKEET PREMIUM RB (4 YEAR OLD)
GREASE l
II-38 1
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tueelCAef SL9NtRT $Nffl - A11M ffsts seestire sagte Identitleetteri so.: 468-88-1259-001 ifst $#rttz Preolue de (4 Year Old) Post-Badletten Sample identifiestien No.: 448-88-1259-200 Poet dea Sospie Identificellen us.: 448-88-1259-300 f_ag!Lr g e) pomerte Poet-Redtetfen Pog t-(MIA.
ftretieneI fest feettlM 384 385 min. See setice of Annosty prepping Point. *f 386 380 .t
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366 375 tearted (199,988 strd ee) 290 m20 een.
'n 'a Polette therge -f to O 8*
0.7tb) 0.62 9.45 0.56 '
feia-sett ifeer, sus EAST # 9-2266)
Omidetton Stablilty tasin 0-942) 16 ass.
8 9 19 pel & g a fee hre. see motice of Armaety 20 30 (c) 18 ass.td3 e 500 lire.
see. 5 and 6.
Psee Pese See getice of Anemely felt Corroelen Preventive Presertles Paes so. 7 (light etelne)
(Asin 0-1743) to to le Ib ese.(e) terper terroelen tAstn 0-40 2 3 infrered Analyeis no thenge me thenge , no Charge 5tanderd(f) 88 40
-)
I sepre es.1 1 El&
(s) taitene otherwise noted, dote free leance seenufactur6re Specificatione Seek (Incitated under Isb 8 l).
(b) samateus tielt considered by tenece for renEP type grease enzt es thle predat that de not cerrteln entiinaer utst elves.
(c) fotended beob eeldation (500 bre) teet wee not rest en post-tea sospie altre 100 bra reeutt was atitt inithin regstred llette and ett prowlete 500 bre reeutto aere mott below typical vette.
(d) teste reference dets reported in leesce Seeeerch esprt se. 4450-416. temport in tenece*e files et Poet)
(e) typical wesus caneldered by leance based en espes lance with this preert. ee pnellehed date swellebte.
(f) Standarit la seen fee thle tierleent incitaded asider lab t 1.
metice of Ancealv
- 1. The ah wire point of the post-redletlep esopfm te elightly betens the regstred vetus of 385 etnisam, tmat le within the saaptable rarge of settfrg pelate 4 s tithfies soap thickensre, eelch le appresteetely
[
E 3FS-395*f. The watue obtelnad is si:Ala the repeatability Itelt (2*f) of the 305 regstred vetus. 2:
- 2. The rirtyplag point of the poet-dea eQs le slightly below the roupstred welus of 325 min. by enty one f2
- 8' degree eAlch le ceneidered within the r=pestability of the test.
2z
??~
- 3. f%e post-redletten semple had eef tened outside the so. 2 grade rese (265-295). The centlatency was within the so. e grade rarge (355-385) eAlch to within the acceptable ceneistency renes for the esplicatlen of 8f G
Praette et grocee.
T
- 4. The post-dea sample oef tened sharing the 904 test eithstoph the carelatency wee within the so. O erede range (355-385) eAlch le within the acceptable canelatency rege for the erytication of Praeltse as preese. the pointe charge ef ter eartirg 100,008 str%ee showed no further esiten6tg Indicatire that the yeese was sheer stable.
l
- 5. ontdetion result en post-cos semple escoede regstrers tielt but still la within en acceptable rence for the prachict to provide libricetteet.
- 6. Enterused esidetien result (500 bre) en the post-redietfan eespie escoeds the required limit tmst still la within en acceptable rence for the preist to provide tiericetlen. The stichtly higher welue of 70 reted for the besetire sospie is ceneidered within the repeatebility llelt for the test as campered with the reg 48 ted 18 watue.
Il 41 9-O O
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sepori No. t-t F.
The felt fif t he stelru) retlege eri the poet redletten asuple to ret cmsidered elelficant to the everett test altee the later poet td4 semple gave a pose ree A t. The it eteles noted esauld not result in the gresee ret providtrg edigsste Stericettaen.
l Test seevite tusserv and cenetaleri the date for the redf atten end deelgre %eole accidmt teettre of the 4 year old Freeltesthe Deesemelstancy grosee chained of ' re elplf tcent degradstlen to time thicioner eyttes es frtficated by the droppftg pefnt results, the greese did therge sof tened dJring the teettne cycle tant the presse insintelred eri acceptable carelaterury regsfred to provide good tierfcetters. Thus, the 4 yeer old semple, es did the prevleus reis semple, of Premites at scease issutd be esquected to survive e turnet to year radiation environment and reseln fwetfernt darfew a
~4 sidme,ssnt 38 eleye deelen boele accident.
2 U
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Page No. 76 Test Report No. 40196 1 9
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Page No. 77 Test Report No. 40196-1 Report He. T-1
(
TAB B-1 8 BASELINE DATA SHEETS i
II-43 1
9
Function i 1
-~~~~-~~
O 6j,(Eti
___ b----------------- GENER AL 'RESULTS RETR IEVAL -- -
Page No. 11-44 Sample Id 460-09-1259-001 Project No.: 4450 Initials DAT Report No. T-1 O proooce Code:1939 Pr oduct Name: PREMIUM RD GREASE lests Pending: O Notes t ginica/24/so 10:37 ver iricationsov/oa/os 12:21 Completion 09/20/ea 10:30 0 Additional Hotes? N l
I SPECIFICAT IOt4S
) RESULTS MINIMUM O RFSULT I ESTIMATE TYPE MAXIMUM TEST CODE SHORT NAME LAB i ST. 350 00101 DROP PT F PAP 365 4 X.S.1 H PAP D I 0 010t7 OX-STAC500 PAP 20 1
~
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=
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-=--------------- GENERAL RESULTS RETRIEVAL - - ------------- --
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,e Sample Ida 460-08-1259-001 Project No.: 4450 Initials DAT 8$
Product Code:1939 Product Name:PREMlUM RB GREASE G lests Pending O Notes:
Login:OD/24/00 10:37 Verification 09/03/DD 12:21 Completion 09/20/DD 10:30 $
Additional Notes? N RESULTS I SPECIFICATIONS
- RESULT I ESTIMATE TWE MAXINUM MINIHtN1 TEST CODE SHORT NAME LAB 45170 RUST PR.A PARL DK I 65115 1R GR FILM PARL SUCHIT I i
1 I
8
- Test codes 40136 and 40181 not applicable to functional tests - ',
- Included for Texaco information only ,
I e
S-O @
Page No. 79 Test Report No. 40196 1 Report No. T.1 9
TEXACO MANUFACTURING SPECIFICATIONS BOOK FACE 30. C 072CB FACE REY. DATE 06/01/88 F10 DUCT CODE 01939 F3.EMIUM 15 CE.EA!!
MANUTACTURID AT SAKTUN SPECIFICATIONS... MINIMUM MAXIMUN FIN vt D 0217 265 295 PEN UK 100,000 STRES, CHANCE. FOINTS +/.20 DROFFING FOIFT F D 0566 385 RUST TEST, RATING D 1743 1 CIID STAB CREASE D 0942 BOMB METECD, FRESS DROP 100 ERS. FSI 10 t
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Typical Characteristics Lithium Soap, % 15.3 >
Penetration, ASTM at 77'T _f p' .'
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Guide te Usable Temp. 1, .
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--- Pcge No. 11-55 Report No. T-1 g Sample Ida 460-08-1259-200 Pr oject No. 4450 Initlats:DAT Product Code:1939 Pr oduct Name: PREMIUM RD GREASE Tests Pending O Notest g Login:10/03/09 14:42 Verification: 10/14/00 13:31 Completlon 11/17/00 17:48 Addltional Notes? N g RESULTS I SPECIFICATIONS TEST CODE SilORT NAME LAD RESULT I ESTIMATE TYPE MAXIMUM MINIMUM 00101 DRDP PT F PAP 380 i ST. 350 g 00243 GX.S.100H PAP 9 1 01017 DX-STABSOO PAP 30 1
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- GENERAL RESULTS RETRIEVAL -- - - - ---------------- Repo r t No . T- 1 Sample Ida 460-09-1259-300 Pr ojec t No. : 4450 Initials:DAT Product Code:1939 Product Name:PRENIUM RD GREASE Tests Pending: 1 Notes:
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' Report No. T-1 TAB C LUBRICANT
SUMMARY
SHEET MARFAK AP (MULTIFAX EP2)
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Seport No. T 1 ftJWCliole4L IE815 RESAl$
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Casper Cartestern le mamely me. 4 2, tasta e-4468) 53
- .e t
Infrared Analyele met *arge se Charge ao Charge Steraterdtc) o*
OS z2 oo i WT[1r e.
to) Imlese otherwise noted, dets free Tenace ennustacturleg speelficettene seek tierlassed is tats C-1). 35
^
tb) seele refereere ekste reported in Deeeerch Separt me. 44";G-417. (tgynrt en tenacs's file et past) E*
(c) Steward 58 Scan for tble tiericant lerlisend arder Tel* C-1.
uotice of Armaety
+
- 1. The poet *redletten semple sof terund greater then the SE emelenas rogstred laat the censleterry meo Ay
' olightly autelds the us.1 grade range (319-348) and le within the acceptehde carsisterry rev for the eggd 6 cat ten of storf sk AP (Insttif att EP 23.
j 2. The post-Den sougde oef temd greeter than the 19E maalem togstred tua the canelstersey was within the me.1 grade targe (330-344) eruf le enthin the acceptab4e canalsterry rence for the essdication of samrfst ar (shaltifet EP2). l
- 3. the higher estentlen seeutt noted samstd te espected for a gresee eyesed to grotenced heet6ng. the am6dation level unutd not adversely of fect the satisf actory perforamrue of the gresse to provide edegante I.er 6c at ion.
18 18 O_
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Depart De. f-1
- 4. The cesper corroelare roeult noted for the poet-Den semple eaccede the tv psleed llelt M mastd be eepected for t%Ie grease 36ese esposed to ble temperettsree for e proleryd perled. The terresee actielty temord cegyer le ese to the effect of high temperetwee are ero of the compenent of the outdttlee pactose. The cigger corroelen level eastd set effect the lieeltetleg preperties of the yeeee. I I e
! fest seemite Summary and terrlemlen i i t'c
. date for the redlettee end deelgre beels accident testig of the searfsk aNahelttfd EP2) yeese sempte i
shemmed ne slamificant depredstlen to the Feese thleterer eyotes se ladicated by the droppleg point reeutte, '
! the ceruleterry of the grosse charigod very llttle earleg the testleg cycle ord shemed to evidsete of eerseelee l herdenleg er esf tentes. Temas, snartak ANthsilfsk EP2) reese W be euyseted to suretee e suunnel te year i redlettere grevironment ord reseln feartieret earleg e : _^ 4 30 alsye streiys boole accident.
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I Page No.119 Test neport No. 40196 1 Report No. T-1 TAB C-1 BASELINE DATA SHEETS II-80 f8
SCR]}[_f - ----- GENERAL RESULTS RET 3 t EVAL 468-88-1257-001 Pr o.iec t No. : 4450 Initials:DAT pg, g .j y^
Sample Id g g.g, Pr oduct Code:995 Product Name:MULTIFAK EP 2 Tests Pending: O Notes:
LogineOU/24/08 10:38 Verificatloa 0?/03/00 12:21 Cosapletion 09/06/D0 14:21 ,
Additional Hotes? H I SPECIFICATIDNS DESULTS TYPE MAXIMUM MINIMUM RESULT I ESTIMA1E TEST C00E SHORT NAME LAB 390 l ST. 350 00181~ DROP PT F PAP PAP 4 i 00243 OK.S.100H
40375 HP, MG GRS PARL 250 8 I j 44299 CEC 24/lOOC PARL IA t 45151 4-BALL WEA PARL .30 =
_ _ :n 4o "'8 SCREEN 31 Function t 3
- - - - --- GENER At. RESULTS RETR IEVAL - -- -- -
Sample Id 460-09-1257-001 Pr o.iec t No. : 4450 Initials:DAT (;
Product Code:995 Product NaenenMULTIFAK EP 2 og Tests Pending: 0 Notes: g Login 00/24/BB 10:38 Ver-I F icat ion 09/03/B0 12:21 Coenpletion 09/06/UU 14:21 /.
Additional Hotes? N REGUI.TS I SPECIFICATIONS TEST CODE SHORT HAME LAB RF.SULT I ESTIMATE TYPE MAX Il1UM MINIMIR1 45169 RUST PR.R PARL 1 1 45170 RUST PR.A PARL OK I 65115 IR GR FILM PARL SUOMIT I i
I I
I I
- Test codes 40136 and 40181 not applicable to functional tests -
included for Texaco information only l
Pase Ns.121 Test keport No. 40196 1 Page No. 11 82 Report No. T-1 TI.KACO MANUYACTUILING SPECIFICATIONS SOCK FACE Wo. G.082C FACE RIV. DATE 05/26/88 F10 DUCT CCDE 00995 MULTITAK EP 2 REIRAND CODE 01917 MARFAK ALL PU170$E MANUTACTURED AT RAKTVN SPECIFICATIONS... MINIMUM MAXIMUM PEN VK D 0217 til 295 FIN VK 10,000 STtxs,
% CMANCE 10 DROFFING FCINT. F D 0566 350 CORRN CV STF D 4048 24 IIR AT 212F(100C) 1 OIID STAS CREASE D 0942 50MB X1180D. FRISS DROF 100 HRS. FS1 10
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Page No. !!.84 Report No.,T.1
( TEXACO INC.,2000 Westchester A.... White Plains, N. Y.10650 CODE HO. 1917 MARTAK ALL PURPOSE 'g Typical Characteristics Appearanen Brown '
Lithium Sosp, t 7.5 :
Penetration, ASTM at 77'T 9' -
Unverked 286 Ll Worked 278 Dropping Pt., 'T 382 011 Viscosity, cst at 40*C 168 cst at 100'C -
15.4
- SUS at 100'T 886 SUS at 210'T 82.2 !
Tinken OK Lead, 1bs. 40 j
Guide to Usable Tamp. -
- Min., 'T -30
- Continuous Service, Max., 'T 250 .
Short Exposure, Max., 'T 350
,'l .
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Marfak All Purpose is a brown, oxidation resistant lithium 8 soap grease which contains a non-lead extreme pressure l additive package. It is the most versatiin member of the . .
Marfak series. It is very sheer stable and provides high load-carrying capacity, excellunt rust protection, cor- ,
resion resistance, resistance to water washout, and has i good pumping capabilities at low temperatures and in ,
I centralized lubrication systems. It is recommended for most automotive, truck, bus, trailer and tractor applica- {i tions which include wheel bearings, ball joints, universal r ;-*
i joints, splines, and linkages. It should not be used for lubricating the constant velocity joints used on front- .M. *
.t, drive cars. Marf ak All Purpose is approved for Hack MG-C ,
applications. Harfak All Purpose has been assigned PET 1 Classification A with respect to its use in food, feed and fj drink plants. l'{
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lb l Page Noe 151 Test Report No. 40196 1 (- Report No. T-1 1 I l TAB C-4 ( INSTRUMENTAITON EQUIPMENT SREETS II-109 f(
esport so. T-1 lastmMuf Af fCII EmitfWat SMEEt Date l Type feet Osseline. Post Badiation and
# Post-Den fiertint test Ecgineer . ! feet semple norfak AP t hittfat EP 21 Cell.,.t. ..t. A.,.
stadet seriel Test uo. teo- Emma_ Accwary h Due me. so. Instnament narnsfactwer s.perler ties ~~- 0-1001 - - - -- - 9-564 j 1 rouerstet E Elect. Co. W Proclelen - - - I-4 0-640 ~~ 16/38 -~ D-21T 2 Penetre-seter sclantific t/10 aus 2 3 Grosse
- T3501 L-10 N/A N/A N/A N/A 9-21T 2
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- Il-AG-3 * * *
- D-21T ??
4 3 . . . ii Ac.3 - - - - e-2iT g g . e p0m.2330 ----- * * *
- D-21T G" T *
- T3501 P-3 * *
- 8' D-21T ?
g . . . 3-3 . . . . p.337
* = = = s-21T 9
- Lebtins 4120 133 10 Owen stue N 147-490A-2 Ji-5304 100-
- 27 11/98 -~ D-4048 Elect. Co- 500f 11 Temp. Gage eachester 5/A N/A 0-600f
- 27 11/88 5/A D-4048 12 Centret stettler FP80 D67956 0-5727 + 0.1f -~ --- m/4 Processer 13 Dreppiry stettler IPS3 D6F9F3 0-572f +-0.1f --- --
m/4 Point Cell 1420 5/A N/A -- -~ gnfrared 14 it 54ectro- Perkin- ----- giunameter Elemer Anotysto estional --- ---- N/A m/A -~ -- p-1743 15 oven Agptlance Co. 11-110 O O
-m. p.
'7 s T
t Report No. t-1 IW51mstutAtION falflPMENT SNEf f Date type feet Beset tne. Post-Redletters and !
# Post-004 Fwwtlanet r
test Ergineer , - feet Semple Nor fet AP f ehrit t f ak EP 2)
/
Cetlisret ten Date astut stedet Serlot feet Ite. Instrument IIsresfactwer to. So. terme Acewecy EWs Due me. 14 feet Prectalen 75015 s/A e/A s/A --- - - - - D-2596 geschine Scientific M. 1F *
- 73403 J4 h/A N/A --- --- 9-2266
* * --- 9-2246 E
18 73603 E-2 N/A N/A --- i 19 ' Pressure llelse G196878 m/A 0-150 pelg N/A 3/28/00 --- D-M2 so.e :" x -i
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l Page No.154 Test Report No. 40196 1
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Page No.155 Test Report No. 40196 1 Report No. T-2
,' i TAB D LUBRICANT
SUMMARY
SHEET !(O l STARPLEX 2 GREASE l II-112 l
___ _ . _ _ _ _ _ . . . . _ _m . i 1 1 l i toport me. 1-1 functecent Tests REsAls LugalCAuf 9.seuRT SNEll - VISJAL INSPECllON list SAMPLE: Storplee 2 seseline temp 4e fdsntifleetless es.: 463-88-81T3-Ott Peet medletten sesyte Identificellen me. 463-88-81T3-200
- Post-DSA semple Identificetten he.t 463 88-31T3-3e0 Post-Redletion P9et DM Reasired Sepstte Vleust inocection Betellrw Aggserence geseth, Sesoth, ftrirgy Smeeth, Smeeth, sete 1 strirwy striryr strerey j
=
trem arous mete 2 ; cater steun asefish sresi odor Astitive siisht totidiend strars Aetitive mete 3 E('8 { A&sitive 7
??
setida iPertIctesi Esemiretien mane mane see sans gg T' 4 NQlf$r
- 1. sesyte es received af ter SGA test une grossly conteelneted with water such that the saapte centeleer mes filled ulth free aseter with sense greees fleeting in the water, ibis inspectlen cemeent le retened to the grease reonining in the contaltwr.
- 2. Coter charge free brown te e reefish trews le cmeldered typical for grease cmteinine emire type entissidente eben esposed to verleus types of resentieri (as for easeple oltrevistet s eJsetten from swilight). The fennetten of small assets of color bodies & not effect performance of the grease.
- 3. strong ed$ltive embr is espected seen outje grease is engesed to high tesgeratire.
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tugalCANT RespAY SIEET - ASTN tests r Test saa tt Sterplom 2 Seeellne Suple Identificetlen me.t 447-08 81T5-081.. i-Post-Redlettui Sample Identificetten me.: 447-88-01T3-200 Post-tea sample Identlfleetien so.: 467-88-8173-300 Segelffs Poet papffetist P9et-904 99effredte) ' Deserte Fwctlenet feet i 496 522 458 min. H erospi g Point *r 529 * (Astn 9-564) 5tf 4 *W Penettetten S En (Asin B-21T) 255 290 2T4 265-295 see estice of Anasty 'Z *Z Worted tes ettdes) oo
- h. t a
106 29e 340 278-319 a taarned (10,080 strekee) 3D 1 Eliege +12 0 +24 +5 sum. See metIce of Anumely mee. 2 and 3. E* four-sett taper, me 8.36 0.29 0.41 9.4(b) See maalce of Anesely i me. 4 .! (A5fM 9 2266) Ontdatten Stability , (ASIN 3-942) 2 22 17 19 uma. See metice of Arumely pet alrep 8100 hre. Noe. 5 aruf 6 Estraes Prosauro Properties i (Astn 3-2596) * ' Lead Weer inden, as 46 -. 39 39 3P sin.(c)
, Weld Point, as 258 200 200 200 min.(c) i l
j Corrosion Preventive Properties (A$1M 0 1743) Pass Pass felt Pess (b) See notice of Anomaly (Dark Steln) me. T 11-114
Segert so. 51 FlasCitanAt IElfS RESUL18 LLBA!CNtf SLDetAtt SEET - f. Sill TEtis ifEI SAM LEs Storptes 2 (Cent.) Sesettre semple identificetlan me.: 447-88-81 0-801 Post-Redletion Sample identificetten so.: e47-se-81 0-290 Post-DAA Sample Identificellen me.: 467 88-81 D-300 Fwrtlenet feet Seseline Post-Redletten Post 904 SElbilf211(a) Seearte Cgper Carresten 3e le als eso. tb ees. See motice of g a Answty me. 8 (Attle D-4048) infrared Anotyeis se thence he Charge me cierge Etendard(d) ( 8* a* EIU 2Z oo (e) thtees otherulee noted, date from tamara storesf acturfre speelficettene Seek (included trader Tab S-1). , o na (b) teele reference date reported la teseco seeeerdi esport so. 4450-415. leeport en fesace's file et Past) (c) Typical welue considered by Teence bened en esperlass:e with thle preekset. to padstlehed data eveliable. g 4, (d) standard It Scan for thle tidsricant inciteind under 1stm 91. petist of Annastr
- 1. Roseline semple slightly outelde ragstred esorted (60 strekee) penetretten targe Sadicating greese slightly harder then deelred. the etishtly harder penettetten assutd not degrade the performance of the grease for its appalcetten.
- 2. Werked (10,000 strokee) penettetlan t chence en baseline esepte escoede e5 eso. ekse to esorted (60 strekee) penetretten tielag slightly outside regaired range (sw N.O.A. the.1). If inittet baseline semple cenelatency ese oef ter tappreslemtely 279 to 2M) thers wetted (18.000 strateel penetration I caerve assutd hows tseen lese, thouewer, thle dowletten assutd not degrade the perfereence of the grease for its espiIcetlen.
II-115 0V 0 0
^ ,a Report so. 7 1
- 3. Worted (10.000 stretee) perettetten 1 ciege enceeds +5 ass. fcr poet-984 semple &o to eecessive unter centeelvetten of eemple. Neuever, cenetetency of greeee sfeer wortleg is within so. I grade rense (198-340) dich le within the accepteMe canelstency rarge for the esplicotten of Sterplee 2.
4, Slightly higher woue (9.4') not caselderd slyttfleantly different free roupstred tielt (0.4) bened en the repeatebility of the test. es effect en the perforumree of the gresee le espotted.
- 5. The eeldeelen statellity noted for the post redletten sempte enceeds the regelred vetue test le etitI caroldered Indicative of edthlting reslotence to further eeldetten.
- 4. The soldation etabitIty noted for the post-904 semple enceeds the regsfred vetus but le stitt Indicettwo of enhibilleg reelsterre to further eeldation.
I F. Fett reeutt (durt stein) noted for post-sea semple ehema e typicet effect of preterged heetire et eleveted p I temperatisree en the addittwo pochese tened in thle preshact. thle corresten towel umuld not degrade the .g Idriceting properttee of the grosos. pg i
*M
, S. Capper cerroeless result (4b) poted for the post-334 esople le caneldered typicel for thle grease den Res eW to high temperatures for e preferged perled. Cogger correeien levet usuto not effect the t driceting proporties of the gresee. corresten reeutt (3e) noted for the basellew semple le htWier ttien oo
- espected and reflects the variability of the teet. The 13el reeutt ese not canaldered to adversely of fact A o ta the upsetificotten of the semple. . w w
'T feet Results tieserv and tenclenten the date for the redletten and deelys heele accident testing of the Storytes 2 grosse shamed no elpilficest degradetion to the grosos thlehener system ao indiceted by the dropping point reautte. The cereistency of the gresee changed very little ehrleg the testing cycle and ehesed me owldunce of esceoolve heedenleg er esitening.
Thus, Storplee 2 grosse asestd be espected to survive e mornet 18 veer redletteen entfrersment eruf remain fasettenet & ring a *=r-nt 30 days duely, boule accident. I i ll 1M a i
Page No.160 Test Report No. 40196 1 Page No. !!-117 Report No. T-1 TEIACO MAN 7TACTURING SPECITICATIONS BOOK FACE No. 0 090C FACE RIV. DATE , 08/12/88 , PRODUCT CODE 01935 STARFLEI 2 MANUTACTURID AT *AT SPECIFICATIONS... MINIMUM MAIIMUM DROFFING FCINT. 7 D 0566 450 PEN VK D 0217 265 295 FIN VK 10.000 STRIS, l % CRANGE +5 CORFJi CU STF D 4048 24 MR AT 212F(100C) 13 RUS7 TEST. RATING D 1743 1 CIID 37A3 CLEASE D 0942 809 METHOD PRISS DROF 100 HRS. PSI 10 l l
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Page No.162 EEEBeBib8BBB. TEXACO REFINING AND MARKETING INC. P.O. BOX 52332 HOUSION. TX 77052 Page No !!-119 Report No. T-1 INDUSTRIAL PRODUCTS - . CODE 1935 STARPLEX 2 CODE 1936 STARPLEX HD 2 CODE 1937 STARPLEX PRIMIUM 1 Typical Characteristics Starplex 2 HD 2 Premium 1 Appearance Tan, Smooth Brown, Buttery Dk Brown, Tacky Lithium Soap, % 15.0 . 13.2 9.0 Penetration, ASTM at 77 T Unworked 253 265 302 Worked 282 284 311 . Dropping Point, T 450+ 450+ 450+ Mineral Oil Viscosity cst at 40 C 210 680 472 cst at 100 C 17 34.5 30.0 SUS at 100 T 11CO 3600 2537 SUS at 21; F 90 175 147 , Ti::Aen OK, 12 40 40 40 Guide to Usable Temp. Max, T 450 450 450 Min, :T -15 0 0 continuous Temp. :T 250 250 250 Starplex 2 is a lithium ec= plex soap grease which contains a specially formulated extreme pressure additive package. It provides excellent rust protection and resistance to water wash-cut. Starplex 2 is specifically designed as an automotive wheel bearing and chassis grease where its high drepping point makes it suitable for today's disc brake equipped cars, especially these operating under severe conditions. It can be recom= ended for
=est automotive, truck, bus, trailer and tractor applications which include wheel bearings, ball joints and other chassis lubrication points. It is also well suited for industrial bear-ing applications involving heavy leads, elevated temperatures and wet conditions.
Starplex HD 2 is an NLGI Ho.=2 lithium complex soap thickened grease, cade with a high viscosity base oil and cor.taining addi-tives to provide rust preventive properties, oxidation resis-(Issued 4-88) CcHTAcT THE NEAREST TEXACO MARKPTINo DIV151cN FoM ADDIT 1cNAL INFoRMATIcN: CEN3AL (9J 3) $60 6000 B MIDWEST (312) 505-9339 e NcRTHEAST (6C9) 7781400 ScUTHEAST (404) 321s411 e SOUTHWEST (214) 238 7909 e WE:IrTERN (818) 605-2400 J h n . .
Page N.o.163 ' Test Report No. 401961 Page No. Il-120 Report No. T-1 (( - tance, and extrema pressure properties. It is particularly intended for autonctive and indusu la1. service where a high viscosity base oil is desired. It is recommended for heavy duty autonotive service including whos! baaring and chassis lubrica- . tion for -busses, trucks and att-rsad vehicles operating under severe conditions. Starplex Premium 1 is an NLGI No. 1 grade of theItversatile is recom-Starplex series of lithium complex 'sosp grosses. mended for use as a multi-purpose grensa in heavy duty industrial equipment operating under adverse conditions such as high and low temperatures, heavy continuous or-.i.ntarmittent shock loads and water contamination. Starplex Premium 1 is particularly suited for use in grease lubricated paper nachines where its outstanding water resistance characteristics, excellent oxidation stability and high dropping point eliminates the need for separate greases in the machine's wet and dry ends and felt roll bearings. It will also lubricate high Icaded prass sections of the paper machine. t
'l Page N s.164 Test Report No. 40196-1
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Page No.165 Test Report No. 40196 1 Report No. T-1 1 9 9 O e TAB D-1 BASELINE DATA SHEETS II-121 0
SCREEN 31 Functson ( 3 O ----------- --= =-- GENERAL RESULTS RETRIEVAL - - - - - - - - - -
---Pc.ge No. 11- 122 Report No. T-1 g Sample te 467-08-0173-001 Project No.: 4450 Initials DAT Produc t LJe: 1935 Product Name:STARPLEX 2 lests Pending: O Notes:
g Login:08/29/00 08:02 Ver i f i c a t i cen 09/03/00 12: 21 Completion 11/17/88 16:26 Additional Notes? N g resin.TS I SPECIFICATIONS TEST CODE SHORT NAME LAB RESULT I ESTIMATE TYPE MAXIMUM MINIMUM 00101 DRDP PT F PAP 529 i ST. 350 g 00243 OX.S.100H PAP PARL 222 2 I
- 40136 PEN, UNWK 1
'40138 PEN, WK PARL 255 i g 40139- PEN 10000 PARL 206 1
- 40181 DROP PT, F PARL 543F l ST. 350 40374 LWI,KG GRS PARL 46 i g 40375 WP, KG GRS PARL 250 I 44299 CSC24/100C PARL 3A I 45151 4-BALL WEA PARL O.36 i y E
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------- ---- -= -- GENERAL RESULTS RETRIEVAL -= -
zz Sample Id 467-08-8173-001 Project No.: 4450 Initials:DAT PP Product Code 1935 Product NamesSTARPLEX 2 g-Tests Pending: O Notes: -m Login:OO/29/80 00:02 Verification 09/03/00 12:21 Completion: 11/17/00 16:26 ? Addltlonal Notes? N RESULTS I SPECIFICATIONS TEST CODE SHORT NAME LAB RESULT I ESTIMATE TYPE MAXIMUM MINIMUM 45169 RUST PR.R PARL 1 1 45170 RUST PR.A PARL DK I 45300 SRT100H/PB PARL CANCEL i 65115 IR GR FILM PARL SUCHIT I
. 1 I
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- Test codes 40136 and 40181 not applicable I to functional tests - included for Texaco I informa.tfon only I e e e
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