ML20100R389
| ML20100R389 | |
| Person / Time | |
|---|---|
| Site: | Farley  |
| Issue date: | 02/20/1992 |
| From: | Cox C LIMITORQUE CORP. |
| To: | |
| References | |
| CIVP-A-071, CIVP-A-71, NUDOCS 9204080157 | |
| Download: ML20100R389 (67) | |
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!U 2 uun , t Rzv. 1- ! 11/10/82 T2 tiAR 13 Pd :47 [* ). GF!CE OF ^ECiu It.KV DUCKEhNG A SEesvici 5 RANCH-l 1 i QUALIFICATION TYPE TEST REPORT OF MULTI POINT TERMIfiAL STRIPS FOR USE IN LIMITORQUE VALVE ACTUATORS - l FOR PWR SERVICE i PRNECT #681041 4 i REPORT B0119 ) i i TEST PERFORMED 1 DECEMBER 1981 to 28 APRIL 1982 4 \O i
- PREPARED BY LIMITORQUE CORPORATION l TEST LABORATORY.
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- Cnarles H. Ccx f
Assistant Chief Test Engineer i i Data July 1,1982' . O'<h s W.-W Approved by _ Walteyr d. Denkowski Accepted by b Joseph 8,An.w uk' ~' 'i c. l !O - .i : .I C AOfOCK15705000348 920220 PDR.
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QUALIFICATION TYPE TEST REP C ' OF MULTI. POINT TERMitlAL STRIPS FOR USE IN LIMITORQUE VALVE ACTUATORS FOR PWR SERVICE PROJECT #681041 REPORT B0119 TEST PERFORMED 1 DECEMBER 1981 to 28 APRIL 1982 5 O PREPARED BY LIMITORQUE CORPORATION TEST LABORATORY Prepared by_ - - 01arles H. Ccx ' Assistant Chief Test Engineer Data July 1,1982 a Approved by & U: a ' ' ~~i'I"~ WaltePr J. Denkowskt Accepted by db Josepn B A w 3 ' O
O TA8LE OF CONTENT s, 1.0 Introduction . 2.0 !dentification of Test Samples 3.0 Type Test Procedure 3.1 Aging Test Procedure 3.1 1 Thermal Agin 3.1-2 Electrical A ing 3.1-3 Radiation Ag ng 3.2 Radiation Exposure 3.3 Seismic Testing 3.4 Loss of Coolant Accident Simulation 3.5 Post Test Inspection 3.6 Final Inspection . 4.0 Test Results 4.1 Acceleration Aging 4.1-1 Thermal Aging 4.1-2 Electrical Aging 4.13 Radiation Aging-- 4.2 Seismic Testing Results 4.3 Loss of Coolant Accident Test Results 4.4 Post Test Inspection 5.0 Conclusion . I O 4
LIST OF APPENDICES ,
- Appendix A Themal Aging Data Summary Appendix 8 Electrical Aging Data Sumary Appendix C Certificate of Irradiation Appendix D Seismic Test Report Appendix E L.O.C. A. Data Sunenary Figure 4 Actual vs. Specified Temperature / Pressure Profile Figure 5 Cycle Agenda Tables 1-7 Registance Data Appendix F Acceptance Criteria Appendix G Wiring Diagrams Figure 1 General Diagram Figure 2 Specific Diagram for Thermal. Electr' cal, and Seismic Aging Figure 3 Environmental Wiring (L.O.C.A.)
tppendix H Instrumentation List 1 Appendix I Chemical Spray Solution Appendix J Photographs Figure 6 Initial Set-Up Figure 7 Pre-L.O.C. A. Set-Up Figure 8 Post L.0.C. A. Inspection O
1.0 INTRODUCTION
Several types of miti point terminal strips (see Section 2.0-Ide'ntificatun of Test Sa@les) typically used in Limitorque valve actuator: N tevice in a Pressurized Water Reactor (PWR) containment chanber ir tthe Power $tition application, were submitted for qualificG, U the type test specified by lEEE 382 72.* As a vehicle for tett sequences, a Limitorque 5%0 valve actuator with . a nuclear motor was fixtured to accept all test samples simultaneously. The teminal strips were then subjected to tests as sequenced in the Limitorque Terminal Block Qualification Test Procedure (Revision 4), including Themal Aging and Hechanical Cycling, Irradiation. Seismic Testing, and Loss of Coolant Accident simulation, with acceptance criteria as specified in Appendix F.
*tiote : Although the general type test procedure references IEEE R2-72, portions of the test involving heat aging and seismic tests reference IEEE 344-75 and IEEE 382 % . .
2.0 *1DENTIFICATION OF TEST SAMPLES Marathon 300 -
- 8 pt. - .- 2 each 4^
Marathon 1600 6 pt. I each Buchanan 0222 6 pt. I rach Suchanan 0524 6 pt. 1 each N General Electric EB-5 1 each Cj Curtis Type "L" 6 pt. 6 pt. 1 each
*See photographs of test samples Appendix J.
3.0 TYPE TEST PROCEDURE The type tect plan consists of the folltwing basic sections and which were perfomed in the order shown. This is in accordance with IEEE 382-72 & 382-80.
- 1) Themal aTd Electrical Aging
- 2) Irradiatit.n 3 Seismic Testing 4 Loss of Coolant Accident Sinulation 5 Post Test Inspection 3.1 Aging Test Procedures 3.1.1 Themal Aoing
~ '
The teminal strips were heat aged at the Limitorque 4) - Research and Development Laboratory to an effective ' age of forty years (minimum). Appendix A contains ,' a data sunmary of the themal age test. 3.1.2 Electrics 1 Agino s
^ Electrical Aging was performed at the Limitorque I Research and Development Laboratory concurrent with
thermal aging. All test samples were wired in series . to a 15 lb-ft nuclear motor which was mounted to an 52-00 valve actuator located external to the heat age i chanber. (SeeFigure2). The SM-00-15 was then . operated through a full open-close-open cycle at rated torque (250lbft)andthrust(14,000lb.) values for a total of 2,000 operating cycles (minimum). Related data sumarization can be found in Appendix 8. 3.1.3 Radiation Aoino A total accumulative dose W 204 MegaRads was incurred by the terminal strip test 2amples. Exposure criteria is discussed in Section 3.2 of this report. 3.2 Radiation Exposure The test samples were subjected to gama radiation by placing them in a Cobalt 60 field of 0.40 MegaRads per hour (average) at an air equivalent dose. A total accumulative dose of 204 MegaRads (minimum) was applied after thennal and electrical aging sequences were completed. . The radiation exposure was conducted at Isomdix, Inc., Parsippany, O New Jersey, beginning on 24 December,1981, and terminating on 23 January,1982. A test certificate was supplied by Isomedix. Inc. and is presented in Appendix C. The test samples were retumed to Limitorque Corporation at completion of irradiation. 3.3 Seismic Testing The seismic tests were performd at Acton Environmental Testing Corporation. Acton, Massachusetts using a hydraulic, piston-actuated, single axis seismic simulator. The test samples (mounted in a Limitorque SM-0 housing) were subjected to a series of single frequency sine dwells performed at 1/3 octave intervals from 2.0 Hz. to 32 Hz and at an accelera-tion of 6.0 g. At the lower frequencies, the shake table was operated at its maximum capabilities. Each dwell lasted a total of fifteen (15) seconds duration. During each 15 second dwell, a Limitorque SMB 00-15 actuator (with the motor wired to the test samples--in series) was operated-(thrust seat-torque switch trip) a full open to close to open cycle. Testing was performed in each . of the three sutually orthogonal axes. A copy of Acton's Report #17346-82N appears as Appendix D. 3.4 Loss of Coolant Accident Sinulation The Loss of Coolant Accident (L.0.C.A.) simulation was perfomed at the Limitorque Research and Development Test Facility beginning
l 1 on 28 March,1982, and ending on 28 April,1982. All associated i test data can be found in Appendix E. . l
-3.4.1 Test Descriotion ;
The test samples were mounted in an $MB-0 actuator' arranged to breathe per standard containment actuator construction ; and wired according to Figure 3. The mounting position utilized is identical to that described in Limitorwe's < test report B-0058 as the worst case orientation. . This . assembly was then placed into a test chamber with all , electrical wiring exiting the chamber through flexible con-i duit connections. External wires were attached (per Figure 3) to a conjunction for megger purmses and electrical operation , of specified terminal strips. tressure and-temperature were monitored using a Fluke Detalogger. (Pressure-temperature profile is shown as Figure 4.) Cooling coils mounted inside the test chamber provided cooling capacity to reduce temperature at various plateaus during the test profile. A spray system was provided for delivery of.the specified chemical solution during the test profile. Flow meters mounted on the exterior of the test chamber provided control and monitoring of the fluid flow. Spray information can be found in Appendix 1. , 3.4.2 Test Procedure for L.0.C.A. Test The temperature / pressure profile illustrated in Figure 5 indicates the schedule for measuring insulation resistance of power and terminal strip leads, cycling of the SMB-00-15 actuator (external to the test chamber) and spray delivery. Temperature and pressure was maintained during the entire test period (30 days) using periodic controlled injections of steam into the test chamber, coupled with heating elements attached beneath the test chamber. This insured a saturated atmosphere in the test chan6er. 3.5 Post Test inspectkon A visual inspection of the test samples was made at~ the conclusion of the accident simulation. (See photographs Appendix J.)
..: . 3.6 Final Insoectien
[ - A complete physical inspection of the test samples was made at ..
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conclusi.on of 111, tests. Results are indicated in Section 4.4. 4.0 TEST RESULTS 4.1 Acceleration Acing t 4.1.1 Thermal Aging Thermal aging was concluded on'18 December,1981, having N .. $ . . - - . , .,,,,N..,,,,__:....,n, . . . , . , _,.n.,.n.m.,, -, e ,,, ,,.,,..__Lwm-.,.. ,, - h
subjected the test samples to a temperature of 1380C - O (dry air environnent) for a total of 300 hours. See Appendix A for data sumary of aging process. 4.1.2 Electrical Anino Electrical Aging was concluded on 18 December,1981 with a total of 2,002 cycles as described in Section 3.1.2. Related data sumary can be found in Appendix 8. 4.1.3 Radiation Asing The exposum to radiation (gansna ray) of the test samples was completed on 23 January,1982 at Isomedix, Inc. A total of 204 MegaRads (mininum) air equivalent dose was applied. A certificate of compliance can be found in Appendix C. 4.2 Seismic Testing Seismic tests were concluded at Acton Environnental Testing Corporation on 10 March,1982. The analyzed test data is presented in Acton Report #17346-82N (Appendix D). No evidence of phyysical damage or malfun~ction was observed as a result of seismic testing. 4.3 Loss of Coolant Accident Test Results The L.0.C. A. test was perfonned at the Limitorque Research and Development Laboratory, comencing on 28 March.1982 and tenninating on 28 April,1982. All test sanples perfonned in accordance with specified acceptance criteria (Appendix F). 4.4 Post Test Inspection
. An inspection of the test samples after the L.O.C.A. test revealed:
- 1) Marathon 300 - Phenolic was unaffected (except for appannt chemical deposits) and electrical characteristics approached baseline readings at room ambient. .
- 2) Marathon 1600 - Same as fl.
- 3) Buchanan 0222 - Same as #1.
- 4) Buchanan 0524 - Same as #1.
- 5) General Electric EB Same as #1.
- 6) Curtis Type *L" - Same as fl.
O
i O
5.0 CONCLUSION
- i It is concluded, based on the motor operator perfomance and the megger values measured during the test and attested to in this report, that the multi point teminal strips described herein are suitable for use in Limitorque valve actuators for use in a Pressurized Water Reactor containment chamber in a Nuclear Power Station application in a loss .
of coolant accident condition.
- Note: It is noted that the megger reading of the G.E. El-5 teminal block dropped in values slightly below those of the Marathon 300 teminal block. Prior experience with the G.E. EB-5 forces us to attribute this to an unexplained random situation that forced the stegger readings below their expected value. In a recent proprietary containment chamber test (that was more severe), a spare :entact of a G.E. EB-5 teminal block was meggered throughout the test with a minimum recorded value of 4 X ohms. ,
O 4 e N O _ _ _ _ _ _ _ _ - _ _ _ _ - _ _ _ _ _ _ _ _ _ _ _ _ _. \
i i- i mesq O . e APPENDIX A THEPFAl AGING DATA SUNRY O e e O
l 0 . 1.0 SPECIFICATIONS l 1.1 , spect=n Identification (See Section 2.0 of this report.) 1.2 711t . (Reference Procedures) 0 1.2-1 Temperature 138 C (280'F) max.141.55'C F1 min.136.610C (286.8,0 (277.9 F j 1.2-2 Duration 300 hours '.' ' 1.2-3 Environment Dry Air 2.0 REstATS 0 The test samples have been tested at a temperature of 138 C for 300 hours to yield an accelerated life of 40 years (minimum). Testing was begun on 4 December,1981, and completed on 18' December,1981. Pasistance data taken befort and after thermal al11ng (photographs in
\ Appendix J) can be found in Appendix E. Tables ', through 7.
x . e t 4
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O 4 t 6 4 APPENDIX 5 El.ECTRICAL AGING DATA
SUMMARY
4 e M O
1.0 SPECIFICATIONS 1.1* Specinen identification
' (See Section 2.0 of this report) 1.2 Test
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1.2 1 Total nun 6er of cycles during thennal aging 2,002 (a) Nun 6er of cycles per hour during cycling 97 sequences Note: Additional, unrecorded cycles were incurred during setup procedures.
- 2. 0 RESULTS The test specimens were electrically aged, having been subjected to sinulated operating current loads a total of 2,002 cycles.
Testing was conducted at the Limitorque Research and Development Laboratory beginning on 4 December,1981 and concluding once 2,000 cycles had been reached (before 18 Decen6er,1981). 4 0
,o ' e i
9 O
O t APPEN01X C CERTIFICATE OF 1RRADIATION O. . e 4 W O . 4
I O 9 v . di February 11, 1982 Mr. charles cox Limitorque corporation P.O. Box 11318 Lynchburg,-Virginia 24502
Dear Mr. Cox:
This will summarise parameters pertinent to the irradiation of one (1) SMB-0-15 Valve Actuator, as per your Purchase Order No. RD-416 dated December 9, 1981. . The actuator was exposed for a period of 529 hours at an average dose rate of 0.40 megarads. The calculated dose based on dosi-metry is 211 magarads. . Halfway through the exposure, the specimen-was rotated 180 degrees to give a more uniform dose-distribution. Dosimetry was performed.using Marvell Red 4034 Perspex dosimeter, utilizing a Bausch and 1,omb Model 710 spectrophotometer as'the readout instrument. This system is calibrated directly A with copy NBS, of the - with the last calibration being September 00, 1981. dosimetry correlation report is available upon request. Irradiation was conducted in air at ambient temperature and pres-sura. Radiant heat from the source heated the samples somewhat, but the temperature did not exceed 120 degrees F, as indicated by previous measurements on an oil solution in the same relative position. Irradiation was initiated on December 24, 1981 and was completed on January 23, 1982. , very truly yours, IsoMr. DIX, INC. pg7f. - David P. Constantine - Production-Manager DC/mjb Mr. George Diets cc loomedix Ins.
- ts Eastmane meas, Persippany. New Jersey 07054 * (201) ts7.tss4
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l \ i j APPENDIX D SEISMIC TEST REPORT G e
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AcT23 cowonAncm O No.of Pages 16 Test Report No. 1734-82N Fevision 1 - 7/21/82 Report of Test FOR SEISMIC TESTING 0F SEVEN (7) MULTIPOINT TERMINAL BLOCKS - FOR LIMITORQUE CORPORATION R&D PROJECT #681041 O Purchase Order No. RD-472 Prepared by:
^
Data 3 /EN#2. Timothy W. Fofphoff, Proje# EngTHer Acton Environnental Testing Corporation 533 Main Street, Acton, Massachusetts 01720 Ap( dM b Yl h $4 Dat. 4. ~L- 6 'Z William C. McGin(is_ ( Chief Dynamics Test Engineer v Acton Environmsntti Testing Corporation TWF/tjw
REVISION RECORD ' - CHANGES OR APPROVED REVISION PAGE PARAGRAPH ADDITIONS BY DATE NUMBER NUMBER NUMBER 0 ..-~ .-~ FI RS T I S S UE ~ ~---------~ ~ ~ ~ ~ 7/21/82 1 Cover - Report edited in its page 7 -
. entirety to reflect a .
change from the vehicle actuator to the terminal blocks as the test item e O . e 9 4 8
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Report No. ACTON casumonAttose .
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- ADMINISTRATIVE DATA
'0 PURPOSE OF TEST: Seismic testing of seven (7) multipoint terminal blocks for Limitorque Corporation
- R&D. Project No. 681041
2.0 MANUFACTURER
Limitorque Corporation P.O. Box 11318 Lynchburg. VA 24506 3.0 MANUFACTURER'S TYPE OR MODEL NO.: N/A 4.0 ORAWING, SPECIFICATION OR EIHIBIT: Limitorque Test Procedure Project No. 681041 5.0 _00ANTITY OF ITEMS TE UED: Seven(7) s .
. 6.0 SECURITY CLASSIFICATION OF ITEMS: Unclassified 7.0 DATE TEST COMPLETED: March 10, 1982 8.0 TEST CONDUCTED BY: M. Cormier 9.0 DISPOSITION OF SPECIMENS: Returned to Limitorque Corporation 10.0 ABSTRACT: Refer to Section 4.0 17346-82M Report No.
Rev. 1
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' [ ACTON compomAftops
l l v 1.0 . TEST ITEM 5even (7) selected suitipoint termina') b1'cks o were submitted by Limitorque Corporation for seismic testing at the Acton Eniironmental Testing Corporation. The terminal blocks were . tested in accordisce Mth the seismic test procedure for Limitorque RAD Project ,No. 681041. 17346 82N g,g g, Dev- 1
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O 2.0 TEST REQUIREMENTS . 1 The purpose of the test was to' subject the SMB 0 ktuator'to seismic aging f r an environmental qualification test of selected multipoint tersinal blocks. 9 17346-82N Rep at No. __ Rev. 1 s . MNO g.. _
O 3.0 TESTPROCEDURQ 3.1 Test Mounting . The s41tipoint terminal blocks were mounted inside the switch compartment of. an SMB-0 Actuator. The 3MB.0 ktuator , was bolted to an alumine fixture. The actuator / fixture plate assembly was rigidly clamped to the single axis hydraulic shaker for the seismic dwell testing. The 98-0 Actuator was wired in series through the terminal blocks to ariSMB-00 Actuator Motor mounted on a special fixture. The motor mounted en the special fixture was not included during the seismic testing. All mounti.g fixtures were supplied by Limitorque. 3.1 Test conditions The SM8-00 ktuator Motor was arranged to operate simulating thrust seat (torque switch trip) in one direction and position seat in the alternate (open) direc' tion. The stroke time was set for six (6) seconds. 3.3 Test Monitoring , The terminal' blocks housed within the SMB-0 ktuator were visually monitored for any evidence of mechanical damage or deterioration by Limitorque personnel. 17346 82N Report No. - esv. 1 ewwoeastrak 0 ACT9N I 4 componAttoM 9
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l1 d. 3.3 Test %nitoring (continued) . The SMB-0 ktuator was instrumented with thrdi (3) triaxial groups of accelerometers. The accelerometers were located as follows: . ACCELEROMETER SENSE 1.0 CAT!0N k 1 Y On fixture 2 Hi 3 H2 4 V On retor and cap 5 Hi 6 H2 7 Y On ktuator SMB-0 8 H1 9 H2 [ Hi - Parallel to the Ntor Axis H2 - Perpendicular to the Ntor Axis
. V - Vertical Outputs from all accelerometers, through appropriate signal conditioning, were r'ecorded on visicorder recording paper, which is included with this report.
The terminal blocks were monitored for functional integrity by the operation of the SMB-00 Actuator via wiring through the terminal blocks. 17346-82N R$ port No. Rev. 1
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o ' 3.4 $1ne M 11 Test The sine dwell test was pirformed in.three (3) mutually orthogonal axes of excitation, two (2) horizontal /and one (1) vertical- The test consisted of a sinusoidal waveform of 15 , seconds duration, with peak horizontal or vertical accelerations of 6g at each of the following frequencies; 2.0, 2.5, 3.15, 4.0, 5.0, 6.3, 8.0, 10, 12.5, 16.0, 20.0, 25.0, 32.0, and 35.0 Hz. Que to limitations of the shaker table, the maximum accelerations at 2.0 and 2.5 Hz were 49 59, respectively. , During each dwell, the SMB-00 ktuator was operated through a full close-stroke-open-stroke cycle via terminal blocks mounted in the SMB-0 ktuator.
. At the completion of the dwell testing in all three (3) axes of the SMB-0 ktuator, the SMB-00 ktuator was operated from open-to-close back to open. The terminal blocks mounted .
in the SMB-0 switch compartment were examined by Limitorque personnel. 17346-82N Report No. , Rev. 1 -
"" 6 name I'8'
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O' V A 4.0 TEST RESULTS . No anomalies in operation of the seven (7) sultipoint tenninal blocks were encountered during the sine dwell
- testing of the terminal blocks in any of the three (3) axes of excitation of the vehicle SMB-0 ktuator.
At the conclusion of the testing, the terstnal blocks within the $MB-0 switch compartment were visually inspected by Limitorque personnel. O I t 4 17346-8_2N
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O ~ 6.0 TEST EQUIPMENT LIST O 17346-82N Report No. O &
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Q O 'O TEST EQUIPMENT LIST ACCURACY INV.# CAL.FREQ. SER.NO._ RANGE MFGR. MODEL NAME 15% AC335 6 aanths 4442 1 Hz - 5 KHz
'PC8 302A 15% AC343 6 months Accelerometer 4437 1 Hz - 5 KHz PC8 302A 15% AC359 6 months Acceleroneter 2833 1 Hz - 5 KHz PCB 302A iS1 AC383 6 months Accelerometer. 2845 1 Hz - 5 KHz PCB 302A 15% AC385 6 months Accelerometer, 1 Hz.- 5 KHz 302A 695 6 months PCB 15% AC394 1
Accelerometer 2852 1 Hz - 5 KHz PC8 302A 15% AC410 6 months Accelerometer 2855 1 Hz - 5 KHz PC8 302A 15% AC435 6 months Accelerometer 1 Hz - 5 KHz 302A 1817 6 months PC8 151 AC436 Accelerometer 1 Hz - 5 KHz 302A 1820 0FS PC8 ilt Af002 Accelerometer 858 5 to 1 ptiz ild8 Output 500A W/8 Decade Amplifier ALI 20V/20k Ohm 13% 0$302 6 months T912 DC - 10 letz Dual Trace TEK T912 Scope. Storage 8011852 . 15% ampi PE367. 6 months 24 DA max. 908.34-01 DC-200 Hz, 22K force lbs Earthquake Simulator #3 204.635 Hydraulic Actuator ili PE367 DC to 2000 Hz . MTS 443.115 120 GPM Max. 3K-5K psi max NA Controller Dennison Mod. 63 Power Supply 250 HP 121 PE379 6 months 483A 299 12 Channel Gain: XI Power Supply- PC8 11 db RE347 6 months 1508 161715R 12 Channel - Metric HON 11 db RE349 6 months Visicorder 15-419 12 Channels. 8" Paper 1508 .SG321 6 months Visicorder HON 111 CO-100A 120 0.2 Hz to 5.0 KHz Sweep Oscillator Ling 0.1 to 9.9 octave / minute (7010) kC'
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5 4 0 . e 4 4 APPENDIX E ACCEPTANCE CRITERIA O J e
.rt O
l Os i Teminal Strip Environmental Test Acceptance Criteria _ The acceptance criteria is based on the motor operator's ability to function during the loca test. Power to the motor is connected to . the two Marathon 300 terminal blocks. Therefore, the lowest megger value measured on either of the two (2) Marathon 300 teminal blocks is considered the minimum megger value acceptable on the remainder of the test samples. 4 O t 9 O_
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s Ow ; w e APPENDIX G WIRING DI AGRAMS s 6 O - .
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4 ? i i s 9 APPENDIX H INSTRUMENTATION t.!ST_ l I 5 e l l l l 1
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J e ! 4 d I 4 4 I e APPENDIX ! CHEMICAL SPPAY $0Ll17!0N I l l l
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The test samples (mounted in a Limitorque SMS.O valve actuator) were sprayed uniformly for 24 hours at periods indic, 'ed on Figure 4. The chemical spray j solution was prepared using Table 1 of 16EE 382-1972. A sample of the solution was collected for analysis witn a copy of the analysis report appearing in this appendix. The desired concentration is 3000 ppm Boron with pH of 10.5. The flow rate was maintained at approximately .4 gpm. O. 4 6 4 0 0
l 3 ' M YTlC5 NO. 50063365
% 'P.O. Sox 26249 ACCOUNT NO. 6)2)1 i Richmond, VA 23260' SATE May 10, 1982 O Limitorque Corp.5114 voodall Road Lynchburg, VA 24506 Attention: Charles Cox SAMPLE OFs Liquid - 681041 DATE RECElvtD: April 15, 1982 REMARKS: mg/L = milligrams per liter RESULT pH 11.2 Boron 29t0 mg/L
- R. A. Wes t , Jr.
9 I i I e 4 e O
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O- e s O APPENDIX J
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