ML20093J082

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I-130 Removal Efficiency Determination of Adsorbent Samples
ML20093J082
Person / Time
Site: Byron  Constellation icon.png
Issue date: 10/10/1984
From:
NUCLEAR CONSULTING SERVICES, INC.
To:
Shared Package
ML20093J081 List:
References
NUDOCS 8410160489
Download: ML20093J082 (2)
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Text

.

PO DOX 29151 COLUMOUS OHIO 43229

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V h uc ear Q g! ting,y,,.

E~ Serv I . DETERMINATION b e OF ADSORBENT SAMPLES PERFORMED BY:

[.' NllCI. EAR CONSill. TING SERVICES, INC.

C OI.ti M Bil S , O H I O 432P.9 i

PERFORMF.D FOR:

COMMONWEAL.TH EDISON COMPANY, BYRON STATION POST OFFICE BOX 767 CHICAGO, ILLINDIS 60690 P 0. NO, 266364 DISTRIBilTION:

EXTERNAL v (2) DAN CHRISTIANA '

(1) BRUCE BYRNE INTERNAL (1) PROJECT MASTER FILE (1) I-LAB FILE (1) QA FII.E NilCON 13CE413/01 8410160489 841010 PDRADOCK05000g A

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C E IR T :1: la- ~l: C: A T I?E C) la' C: A 1... :l: B IR A T :l: C) N CLIENT: COMMONWEALTH EDISON COMPANY BYRON STATION POST OFFICE BOX 767 CHICAGO, II.LINDIS 60690

. Ph.No.: 266364 NUCON PROJECT No.I 13CE413 DATE: 11 APR 1984 TEST EP"TPMENT CALIBRATION STANDARDS LOG No. LAST CAL. DATE LOG No. NBS No. (IF APPLICABLE)

LO635 15 DEC 1983 LG350 522/223339 LO351 221482 LO299 08 MAR 1984 LQ414 NBS CIRCULAR 4 36 LO286 15 NOV 1983 LO416 213.12/216242 LO420 731/220788 LO421 731/220788 LO287 15 NOV 1983 LO416 213.12/P16242 Y LO420 731/2P.0788 LOA 21 731/220788

  • LO485 11 MAR 1584 LOS60 NBS SRM 4PA1-2 THIS IS TO CERTIFY THAT THE ABOVE LISTED EQUIPMENT HAS '

BEEN CALIBRATED TRACEABLE TO THE NATIONAL BUREAU OF STANDARDS, HAS BEEN DERIVED FROM ACCEPTED VALUES OF NATURAL PHYSICAL CONSTANTS, OR HAS BEEN DERIVED BY THE RATIO-TYPE OF SELF CALIBRATION TECHNIQtlE AND MFETS THE REQtlIREMENTS OF MIL STD 4566P.

BY __ j_ ff c./c__________ FOR QllALITY ASSURANCE DEPT.

MICHAEL J. TIEPPE NllCLEAR CONSULTING SERVICES, INC

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N NUCLEAR CONSULT!NG SERVICES, INC. (si4) 846-s7i0 l P. O. Box 29151 Columbus, Ohio 43229 TWX 810-337-2007 E

CERTIFICATION OF COMPLIANCE

{ )'] Client: Commonwealth Edison Company Date: 12 April 84 Byron Station Project: 13CE413 Address:P O Box 767 Chicago IL 60690

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.b Purchase Order: 2G6364 Dato: 10 Jan 1983 NUCON PRODUCT / SERVICE: Methyl Iodide Testing i

This is to certify that product /sorvice supplied conforms to specification (s) of CLIENT: of NUCON: y US NRC Reg Guide 1.52 Rev 2 NUCON QA Manual ,,

s. ,

And is so documented by NUCON QUALITY ASSURANCE with any exceptions noted.

Exceptions: Nono

/s/4 Quality Assuranco Nuclear Consulting Servicos, Inc. (NUCON)

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NllC0h* 13CE413/01 1 THESE REPORT SHEETS CONTAIN THE 70 DINE FISSION PRODllCT TEST DATA ORTAINFD FROM ADSORBFNT SAMPLES TF.STFD BY NllCON.

COUNTING WAS PERFORMED AT 0.364 MEV GAMMA l.F. VEL, TN A 4.0" THAL.LIllM ACTIVATED SODTllM IODIDE WF.I.l. CRYSTAL. CAI.IBRATION OF THE CulINTING CRYSTAL. HAS BEEN PERFORMED BY THE USE OF AN NBS TRACEABLE 131-7 STANDARD.

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NUCON 13CE413/01 COUNTING DATA FOR SAMPLF t8899 AIR COUNT DATA

  • PRE-LOADINC*

CPM = 546.2 ~STD DEV= 7.4 COUNTER EFFICIENCY = 1.000 . .

DPM= 546.2 STD DEV= 7.4

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  • POST-LOADING
  • CPM = 546.2 STD DEV= 7.4 COUNTER FFFICIENCY= 1.000 DPM= 546.2 STD DEV= 7.4 i

TB1 COUNT DATA MPRE-l.DADING*

CPM = 627.0 STD DEV= 7.9 COUNTER FFFICIENCY= .500 DPM= 1,081.0 STD DEV= 13.7 DPM-AIR = 534.0 STD DFV= 15.5

  • P OST-l.0 A DI NG
  • CPM = 1,023,769.3 STD DEV= 320.0 COUNTER EFFICIENCY = .580 DPM= 1,765,119.3 STD DEV= 551.7 DPM-AIR = 1,764,573.0 STD DEV= 551.7 v
  • NETx .

- NET DPM= 1,764,038.3 STD DEV= 551.9 GB1 COUNT DATA

  • PRE-LOADING
  • CPM = 600.7 STD DFV= 7. 8 COUNTER EFFICIENCY = .580 -

DPM= 1,035.7 STD DEV= 13.4 DPM-AIR = 489.5 STD DEV= 15.3 .

  • P OST-l. 0 AD ING* ,

CPM = G19.4 STD DEV= 9.1 .

COUNTER EFFICIENCY = .500 .

DPM= 1,412.0 STD DFV= 15.6 DPM-AIR = 866.6 STD DEV= 17.3

  • NET
  • NET DPM= 377.1 STD DEV= 23.1

NilCON 13CE413/01 3_

CollNTING DATA FOR SAMPLF $8899 GB2 CollNT DATA *PRF-LOADING

  • CPM = 600.7 STD DEV= 7.8 COUNTER FFFICIENCY= . 580 DPM= 1,035.7 STD DEV=

DPM-AIR = 13.4 489.5 STD DFV=- 15.3

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  • POST-iDADINGx CPM = 731.8 STD DEV= 8*6 COUNTER EFFICIENCY = . 580 DPM: 1, P.61. 7 STD DFU= 14,7

, DPM-AIR = 715.5 STD DFV=

, 16.5

  • NET
  • I NET DPM= 226.0 STD DFV= 22.5 WP e

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NUCON 13CE413/01 TEST REPORT: METHYL.70DIDE DATF PFRFORMED: 29 MAR 1984 CLIENT: COMMONWEALTH EDISON COMPANY, BYRON STATION POST OFFICE BOX 767 SAMPl.E 48899 P.O. NO.: 266364

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TEST CONDITIONS:

BED DEPTH = 5.08 CM. ( 2. 0 0 IN . )-

BED DIAMETER = 5.08 CM. ( 2.00 IN.)

TEMPERATllRES P R E-EO.lJIL7 BR ATION= 2.5.0 C ( 77.0 F)

LOADING = 25.0 C ( 77.0 F)

POST-l.0ADING= 25.0 C ( 77.0 F)

REl..ATIVE HllMIDITY= 95.0 %

FACE vel.0 CITY = 20.32 CM./SEC (40.0 FPM)

MEI LOADING = 1.75 nG./Cll.H.

TEST TIMES N' P R E-EQtJILIBR ATION= 16. HRS. .

. LOADING = '

2.0 HRS.

POST-SWEF.P= 2.0 HRS.

MEI-131 CONTENT = .80 MICROCtlRIES PRESSilRE= 1.0 ATM. -

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NUCON 13CE413/01 -

TEST REPORT: MF.THYl. TODTDE DATE PERFORMED: 29 MAR 1984 EFFICIENCY: 1ST BFD= 99.97% (STD. DEV.= .005%)

THE RESULTS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OllR BEST KNOWI.FDGE.

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PERIORMED BY b .

~~8ARii PI~K7U5~~~- UU5L FAE~F.5E5UI.T555~55RU5CF.S, INC.

APPROUFD BY ____ ___.__

W. PETFR FREFMAN

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NUCLEAR CONSitLTING SERVICES, INC.

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NUCON 13CE413/01 .

COUNTING DATA FOR SAMPl.E #9360 AIR CollNT DATA

  • PRE-l.DADING*

CPM = 555.0 STD DFV= 7.4 COUNTER EFFICIENCY = 1.000 DPMn 555.0 STD DEV= 7.4

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  • POST-l.0ADING*

CPM = 555.0 STD DEV= 7.4 CollNTER EFFICIF.NCY= 1.000 DPM= 555.0 STD DEV= 7.4 TB1 C0llNT DATA *PRF-LOADING * -

CPM = 598.4 STD DF.V= 7.7

, CollNTER EFFICIENCY = .500 DPM= 1,031.7 STD DEV= 13.3 DPM-AIR = 476.7 STD DEVn 15.3 xPOST-l.0ADING*

CPM = 2,191,702.5 STD DEV= 468.2 COUNTER FFFICIENCY= .580 DPM= 3,778,797.0 STD DEV= 807.2 DPM-AIR = 3,778,242.0 STD DEV= 807.2 s'

  • NF.T*

t NET DPM= 3,777,765.5 STD DEV= 807.3 '

CB1 COUNT DATA

  • PRE-l.0ADING*

CPM = 576.2 STD DF.V= 7.6

.580 CutlNTER EFFICIENCY = '

DPM= 993.4 STD DEV= 13.1 DPM-AIR = 438.4 STD DFV= 15.1 xPOST-LOADINGx CPM = 3,617.9 STD DEV= 19.0 C0llNTER EFFICIENCY =

.580 -

DP M. 6,237.8 STD DEV= 32,8 DPM-AIR = '

5,68P. 8 STD DFV= 33.6 xNET*

NET DPM= 5,244.3 STD DEV= 36.8

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NilCON 13CF413/01 _ 7_,

COUNTING DATA FOR SAMPLE #9360 CB2 C0llNT DATA *PRF-1.0ADINGx .

CPM = 576.2 STD DEV= 7.6 . -

COUNTER FFFICIFNCY= .580 "

DPM= 993.4 STD DEV= 13.1 DPM-AIR = 438.4 STD DEV= 15.1 '

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  • POST-l.0ADING* - a CPM = 781.6 STD DEV= 8.8 cot. INTER EFFICIENCY = .580 '

DPM= 1,347.6 STD DEV= '15.2 DPH-AIR = 792.6 STD DEV= '17.0

  • NFT* ,

NET DPM= 354.1 STD DEVn 22.7 e

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TEST REPORT: METHYL. IODIDE DATE PFRFORMED: 29 MAR 1984 CLIENT: COMMONWE6l.TH FDISON COMPANY, BYRON STATION POST OFFICE ROX 767 SAMPl.E 49360

... P.O. NO.t 266364 TEST CONDITIONS:

BED DEPTH = 5.08 CM. ( 2.00 IN.) ,

BED DIAMETER = 5.08 CM. ( 2.00 IN.)

TEMPER ATtlR ES PRE-EQtlII.IBR ATION= 25.0 C ( 77.0 F)

LOADING = 25.0 C ( 77.0 F)

POST-l.0ADING= 25.0 C ( 77.0 F)

REl..ATIVE HilMIDITY= 95.0 %

FACE vel.0 CITY = 20.3? CM./SEC (40.0 FPM)

MEI LOADING = 1.75 nG./Ctl.M.

TEST TIMES \'

P R E-EQtlII. I BR ATION= 16. HRS.

- LOADING = .

2.0 HRS.

POST-SWEEP =  ?.0 HRS. ,

MEI-131 CONTENT = 1.72 MICROCtlRIES PRESStJRE= 1.0 ATM. ,

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9-TEST RFPORT: METHYL. 70DIDE DATE PERFORMED: 29 MAR 1984 EFFICIENCY: IST BED = 99.85% (STD. DEV.= .004%)

THE REstlLTS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQtlES AND ACCORDING TO Ot!R BEST KNOWI. EDGE.

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PEhFORMED BY _ ___ _____i__L __ _______,'________________

MARK P. KING N Cl. EAR CONStil. TING SERVICES, INC.

MMM MM MM__MM____________M W. PFTER FREEMA R CONSULTING SERVICES, INC.

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l NilCON 13CE413/01 l COUNTINC DATA FOR SAMPLE t9620 t

AIR COUNT DATA

  • PRE-LOADING
  • CPM = 648.0 STD DEV= 8.0 COUNTER EFFICIENCY = .1.000 DPM= 648.0 STD DEV= 8.0 4
  • POST-LOADING
  • CPM = 648.0 STD DFV= 8.0 COUNTER EFFICIENCY = 1.000 DPM= 648.0 STD DEV= 0.0 TBt COUNT DATA
  • PRE-LOADING
  • CPMn 687.9 STD DEV= 8.3 COUNTER EFFICIENCY = .500 DPM= 1,186.0 STD DEV= 14.3 DPM-AIR = 538.0 STD DEV= 16.4 KPOST-l.0ADING*

CPM = 1,135,101.5 STD DEV= 336.9 COUNTER EFFICIENCY = .580 DPM= 1,957,071.5 STD DEVn 580.9 DPM-AIR = 1,956,4P.3.5 STD DEV= 500.9 s'

  • NET
  • t NET DPM= 1,955,885.5 STD DEV= 581.2 GB1 C0llNT DATA
  • PRE-l.0ADING*

CPM = 693.6 STD DEV= ^~

8.3 COUNTER EFFICIENCY = .580 .;

DPH= 1,195.9 STD DFV= 14.4  %

DPH-AIR = 547.9 STD DEV= 16.5 k P OST-l.0 ADING * ,.

CPM = 5,499.1 STD DEV= 23.5 COllNTER EFFICIENCY = .580 DPHn 9,401.2 STD DEV= 40.4 DPH-AIR = 0,833.2 STD DEV= 41.2 WNET*

HET DPHn 8,285.3 STD DEV= 44.4

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COUNTING DATA FOR SAMPLE 99620 GB2 COUNT DATA

  • PRE-LOADING
  • CPMn 693.6 STD DEV= B.3 COUNTER EFFICIENCY = .580 DPM= 1,195.9 STD DEV= 14.4 DPM-AIR = 547.9 STD DEV= 16.5

, , , . , .s *P OST-LO ADINGr:

CPM 78P. 2 STD DEV= 8.8 C0!!NTER FFFICIENCY= .580 DPM= 1,340.6 STD DEV= 15.2 DPM-AIR = 700.6 STD DEV= 1 *7 . 2 MNET*

NET DPM= 152.8 STD DEV= 23.8

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NtlCON 13CF413/01 TEST REPORT: METHYL TODTDE DATE PERFORMED: 03 APR 1984 CLIENT: COMMONWEALTH EDISON COMPANY, BYRON STATION POST OFFICE BOX 767 SAMPLE: 99620 .l'

,, P .._0 . NO. 266364 .a

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TEST CONDITIONS: '

BED DEPTH = 5.08 CM. ( 2.00 IN.)

BED DIAMETER = 5.08 CM. ( 2.00 IN.)

TEMPERATllRES PRE-EQtJILIBRATION= 25.O C ( 77.O F) t LOADING = 25.0 C ( 77.0 F)

POST-LOADING =  :'5.0 C ( 77.0 F)

RELATIVE HilMIDITY= 95.0 %

FACE VELOCITY = 20.32. CM./SEC (40.0 FPM)

NEI LOADING = 1.75 nG./CLI.M.

TEST TIMES *"-

PRE-EQlJILIBRATION= 16. HRS.

LOADINGn . 2.0 HRS.

POST-SWEEP = 2.0 HRS.

MEI-131 CONTENT = .89 MICR0 CURIES '

PRF.SSURF= .t 1.0 ATM. d'.' .

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TEST REPORT: METHYL IODIDE DATE PFRFORMED:

l 03 APR 1984 I

EFFICIENCY: 1ST BED = 99.57% (STD. DFV.= .005%)

THE REStil.TS ARE THE BEST ODTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OUR DEST KNOWl. EDGE.

PERFORMED BY ~~ -

NARK PI K U5(~~~~~ ~UCI55R 50U5UET5N5 55EUI55S, INC

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APPROVED BY __, _ _ g h _____________________

W. PETER FREEMAN NUCLEAR CONSULTING SERVICES, INC.

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NilCON 13CE413/01 .

COUNTING DATA FOR SAMPLE #8989 AIR COUNT DATA

  • PRE-LOADING
  • CPM = 569.2 STD DEV=

7.5 -

C0 TINTER EFFICIENCY = 1.000 DPM= 569.2 STD DEV= 7.5

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  • POST-LOADINGx CPM = 569.2 -

STD DEV= 7.5 COUNTER EFFICIENCY- 1.000 DPM= 569.2 STD DEV= 7.5 TB1 COUNT DATA

  • PRE-LOADINGx CPM = 592.4 STD DEV= 7.7 COUNTER EFFICIENCY = .500 DPM= 1,021.4 STD DEVn 13.3 DPM-AIRn 452.2 STD DEV= 15.3 WPOST-LOADING
  • CPM = 994,R10.0 STD DEV= 315.3 COUNTER EFFICIENCY = .500 DPM= 1,714,156.3 GTD DEV=

DPM-AIR =

543.6 1,713,587.0 STD DEV= 543.7 s.

  • NET *

- NET DPM= 1.,713,134.8 STD DEV= 543.9 CB1 COUNT DATA

  • PRE-LOADINCx CPM = 593.5 STD DEV= 7.7 a COUNTER EFFICIENCY = .580 '

DPM= 1,023.3 STD DEV=

DPM-AIR =

13.3 454.1 STD DEV= 15.3

  • POST-LOADING * .

CPM = 4,985.8 STD DEV= 2R.3 COUNTER EFFICIENCY = .580 ' ' J.

DPM= 8,596.2 STD DEV=

DPM-AIR =

8,027.0 38.5 STD DEV= 39.2 uNET*

NET DPM= 7,572.9 STD DEVA 42.1

NilCON 13CE413/01 COtJNTING DATA FOR SAMPl.E f8989 GB2 COUNT DATA

  • PRE-l.DADING*

CPM = 593.-5 STD DFV= 7.7 C0llNTER EFFICIENCY = .580 DPM= 1,023.3 STD DEV= 13.3 DPM-AIR =~ 454.1 STD'DEV= 15.3

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  • P OST-l.0 A DING-x CPM = 686.1 STD DEV= 8.3 CollNTFR EFFICIENCY = .580 DPM= 1,102.9 STD DEV= '14.3 DPM-nIR= 613.7 STD DEV= 16.2 WNET*

NET DPM= 159.7 STD DEV= 22.2

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NtlCON 13CE413/01 TEST REPORT: METHYL 70DIDE DATE PERFORMED: 04 APR 1984 Cl.7ENT : COMMONWEALTH EDISON COMPANY, BYRON STATION POST OFFICE BOX 767 SAMPl.E: 98989 P,0.

NO.: 266364

..t TEST CONDITIONS:

BED DEPTH = 5. 08 CM. ( 2.00 IN.)

BED DIAMETER = 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRE-EQUII.IBRATION= 25.0 C ( 77.0 F)

LOADING = 25.0 C ( 77.0 F)

POST-LOADING = 25.O C ( 77.0 F)

RELATIVE HLIMIDITY= 95.O %

FACE vel.0 CITY = 20.32 CM./SEC (40.0 FPM)

MEI LOADING = 1.75 r$G./CU.M.

TEST TIMES *'

PRE-EQUILIBRATION =

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16. HRS.

_ LOADING = .. 2.0 HRS.

POST-SWEEP = 2.0 HRS.

'1EI-131 CONTENT = .78 MICROCURIES PRESSURE = 1.0 ATM.

  • 9

NilCON 13CE413/01 TEST REPORT: HF.THYL IODIDE DATE PERFORMED: 04 APR 1984 EFFICIENCY: 1ST BED = 99.55% (STD. DEV.= .005%)

THE REstJI.TS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQt!ES AND ACCORDING TO OllR BEST KNOWI. EDGE.

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PERFORMED BY ..

ARK P. KING l! CLEAR CONSULTING SERVICES, INC.

APPROVED BY ___ _______ _

W. PETER FREEMAN N!!Cl. EAR CONSULTING SERVICES, INC.

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NUCON 13CE413/01 COUNTING DATA FOR SAMPLE #9275 AIR COUNT DATA xPRE-LOADING

  • CPM = 570.9 STD DEV= 7.6 COUNTER EFFICIFNCY= 1.000 DPM= 570.9 STD DEV= 7.6

.. m 6 xPOST-LOADING

  • CPM = 570.9 STD DEV= 7.6 COUNTER EFFICIENCY = 1.000 DPM= 570.9 STD DEV= 7.6 TB1 COUNT DATA xPRE-LOADING
  • CPM = 613.0 STD DEV= 7.8 COUNTER EFFICIENCY = .500 DPM= 1,056.9 STD DEV= 13.5 DPM-AIR = 486.0 STD DFV= 15.5
  • POST-LOADINGx CPM = 934,366.3 STD DEV= 305.7 COUNTER EFFICIFNCY= .580 DPM= 1,611,010.0 STD DEV= 527.0 DPM-AIR = 1,610,439.8 STD DEV= 527.1 v
  • NET
  • NET DPM= 1.,609,953.8 STD DEV= 527.3 GB1 COUNT DATA
  • PRE-LOADING
  • i CPM = 652.5 STD DEV= 8.1 COUNTER EFFICIENCY = .580 DPM= 1,125.0 STD DEV= 13.9 DPM-AIR = 554.1 STD DEV= 15.8 l ;w
  • POST-LOADINGx- - -

.1 l

i CPM = 17,926.1 STD DEV= . 42.3 l COUNTER EFFICIENCY = .500 ..;

l DPM= -30,907.1 STD DEV= 73.0

! DPM-AIR = 30,336.P- STD DEV= 73.4 s

  • NETS NET DPM= 'P9,782.1 STD DEV= 75.1

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NilCON 13CE413/01 .

COUNTING DATA FOR SAMPLE 49P.75 GB2 COUNT DATA

  • PRE-LOADING
  • CPM = 652.5 STD DEV= 8.1 COUNTER EFFICIENCY = .580 DPM= -

1,1 P.5. 0 STD DEV= 13.9 DPM-AIR = 554.1 STD DEV= 15.8 I

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MPOST-LOADINGn CPM = 9P.9.4 STD DEV= 9.6 COUNTER EFFICIENCY = .580 DPM= 1,60P.4 STD DEV= 16.6 DPM-AIR = 1,031.5 STD DEV= 18.3

  • NET
  • NET DPM= 477.4 STD DEV= 24.2 e

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NUCON 13CE413/01 TEST REPORT: METHYL IDDIDE DATE PERFORMED: 04 APR 1984 CLIENT: COMMONWEALTH EDISON COMPANY, BYRON STATION POST OFFICE BOX 767 SAMPLE: t9275

... P .41. NO.: 266364 TEST CONDITIONS:

BED DF.PTH= 5.08 CM. ( 2.00 IN.)

BED DIAMETER = -

5.08 CM. ( 2.00 IN.)

TEMPERATl!RES P R E-EQllII. IBR ATION= 25.0 C ( 77.0 F)

LOADING = 25.0 C ( 77.0 F)

POST-LOADING = 25.0 C ( 77.0 F)

RELATIVE HllMIDITY= 95.0 %

FACE VELOCITY = 20.32 CM./SEC (40.0 FPM)

MEI LOADING = 1.75 nG./CU.M.

TEST TIMES \'

PRE-EQllILIBRATION= 16. HRS.

LOADING = .. 2.0 HRS.

POST-SWEEP = 2.0 HRS.

MEI-131 CONTENT = .75 MICR0 CURIES

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PRESSURE = 1.0 ATM. ,.

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NtlCON 13CE413/01 TEST REPORT: METHYL IODIDE DATE PERFORMED: 04 APR 1984 EFFICIENCY: 1ST BED = 98.16% (STD. DEV.= .006%)

THE RESul.TS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OUR BEST KNOWLEDGE.

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O PdRFORMED BY _________L ___~_t______

NARK P. KING J Cl. EAR CONSULTING SERVICES, INC.

APPROVED BY ___ __2 ___ h _____________________

W. PETER FREEMAN NilCLEAR CONSULTING SERVICES, INC.

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1 NilCON 13CE413/01 C0tJNTING DATA FOR SAMPLE td364-9 AIR C0llNT DATA

  • PRE-LOADING
  • CPM = 600.0 STD DFV= 5.9 C0tJNTER EFFICIENCY = 1.000 DPM= 600.0 STD DEV= 5.9

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).

  • POST-LJADING*

CPM = 600.0 STD DEV= 5.9 C0tlNTER EFFICIENCY = 1.000 DPM= 600.0 STD DEV= 5.9 TB1 CollNT DATA

  • PRE-LOADING
  • CPM = 674.0 STD DEV= 6.7 COtJNTER EFFICIENCY = .580 DPM= 1,162.1 STD DEV= 11.6 DPM-AIR = 562.1 STD DEV= 13.0
  • P OST-L.0 A D ING
  • CPM = 344,828.0 STD DEV= 415.2 COtJNTER EFFICIENCY = .580 DPM= 594,531.0 STD DEV= 715.9 DPM-AIR = 593,931.0 STD DEV= 715.9 g-
  • NET
  • NET DPM= ___593,368.9 STD DEV= 716.1 GD1 C0llNT DATA
  • PRE-L.0ADING*

i , CPM = 672.0 STD DEV= 6.7 i COUNTER EFFICIENCY = .530 ' '

DPM= 1,158.6 STD DEV= 11.5 DPM-AIR- 558.6 STD DEV= 13.0

  • POST-l.DADING*

CPM = 1,488.0 STD DEV= 14.6 COLINTER EFFICIENCY = .580 -

DPM= 2,565.5 STD DEV= 25.1 l DPM-AIR = 1,965.5 STD DEV= 25.8

  • NET
  • l NET DPH= 1,406.9 STD DFV= 28.9

~

'NUCON 13CE413/01 CutlNTING DATA FOR SAMPl.E $2364-9 GB2 COLINT DATA

  • PRE-LOADING
  • CPH= 672.0 STD DEV= 6.7 COUNTER EFFICIENCY = .580 DPM= 1,158.6 STD DEV= 11.5 DPM-AIR = 558.6 STD DEV= 13.0

).'[.

  • POST-L.0ADING*

CPM = 719.0 STD DEV= 7.2 COUNTER EFFICIENCY = .580 DPM= 1,239.7 STD DEV= 12.4 DPM-AIR = 639.7 STD DEV= 13.7

  • NET
  • NET.DPM= 81.O STD DEV= 18.9
h. -

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NtlCON 13CE413/01 -P4-TEST REPORT: METHYL IDDIDE DATE PERFORMED:

CLIENT: -COMMONWEAL.TH EDISDN COMPANY, BYRON STATION POST OFFICE BOX 767 SAMPLE: # 2364-9

,, P..Q. NO.: 266364 TEST CONDITIONS:

BED DEPTH = 5.08 CM. ( 2.00 IN.)

BED DIAMETER = -

5.08 CM. ( 2.00 IN.)

TEMP ER ATLIR ES PRE-EQUILIBRATION = 25.0 C ( 77.0 F)

LOADING = -

25.0 C ( 77.0 F)

POST-LOADING = 25.0 C ( 77.0 F)

RELATIVE HtlMIDITY= 95.0 %

FACE VELOCITY = 20.32 CM./SEC (40.O FPM)

MEI' LOADING = 1.75 t1G /CU.H.

TEST TIMES \ '~

PRE-EQUILIERATION=

~

16. HRS.

LOADING = s. 2.0 HRS.

POST-SWEEP = 2.0 HRS.

MEI-131 CONTENT = .27 HICROCURIES PRESSURE = 1.0 ATM. .",

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3. .L F
  • 1*.

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  • . l NUCON 13CE413/G1 TEST REPORT: METHYL. IODIDE DATE PERFORMED:

EFFICIENCY: 1ST BED = 99.75% (STD. DEV.= . 083%)

THE RESULTS ARE THE BEST ORTAINABl.E UNDE.R CURRENT EXPER TECHNIQUES AND ACCORDING TO OUR BEST KNOWI. EDGE.

7. t- [ Q f PE'R' FORMED BY'____ _________ b MARK P. KJNG i_________________________

.J!UCLEAR CONSULTING SERVICES, INC.

APPROVFD BY __

___ M h ___________________

W. PETER FREEMAN NUCLEAR CONSULTING SERVICEfi, INC.

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PO BOX 29151 COLUMBUS OHIO 4S229 (614) 846 5710 TWX 810-337 2027 V h udear Consulting C Services', Inc.

IOpINF-131 REMOVAL-8 FFFICIFNCY DFTERMINATION OF ADSOREFNT SAMPLES

. . . r.

PFRFORMFD BY:

NUCl. EAR CONSilLTING SERVICES, INC.

C OI.tlM B U S , OHIO 432P9 DATE:

s -

30 MAY 1984 PFRFORMFD FOR:

COMMONWEALTH EDISON CnMPANY, BYRON STATION POST OFFICE BOX 7A7 CHICAGO, ILLINOIS 60690 P.O. NO. 266364 N'

DISTRIBllTION:

EXTERNAL (2) DAN CHRISTIANA (1) BRUCE BYRNE i INTFRNAL l

(1) PRO.TECT MASTER FILE (1) I-l.AB FILE f (1) QA FII.F (1) J. U. Jacox l

N!! CON' 13CE413/02 fFFETSTERED TRADEMMt 0F RK1 EAR CONSt!I.TINf'. SERU!!TS, INC.

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C I:' R T :l: 1 ' :l: C A T IE

(:) l ' C C M P l. :l: A N CIE Cl.IFNT : COMMONWFAl.TH EDISON COMPANY, BYRON STATION DATE: 28 MAY 1984 ADDRESS: POST OFFICE BOX 767 PROJECT: 13CE413/0?

CHICAGO, II.I.INDIS 60690

.. n. ..

PURCHASE ORDER: 266364 DATE: 10 JAN 1983 NUCON PRODUCT / SERVICE: METHYL. IODIDF TESTING PERFORMED ON 4641 BATCH 4 4784 BATCH 5 4053 BATCH 1 s -

SP05 BATCH 6 THIS IS TO CERTIFY THAT PRODUCT / SERVICE CONFORMS TO SPECIFICATION (S)

OF Cl.IENT: OF NUCON:

N' US NRC REG. GllIDE 1.52 REV. 2 NUCON QA MANUAL ,

~.

AND IS SO DOCUMENTED BY NUCON QUALITY ASSURANCE WITH ANY FXCEPTIONS NOTED.

EXCEPTIONS:-

NONE REVIEWFD IN ACCORDANCE WITH CHECKLIST OF NUCON PROCF.EDURE 95 (QA38 ATTACHED).

BY e FOR QUAL.ITY ASSURANCE DEPT.

MICll ARL'f M01'I'PW NUCLEAR CONSULTING SFRVICF.S, INC

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P.0, No.: 266364 NllCON PROJECT No.: 13CE413 ,DATE: MAY 30, 1984 TEST EqlJIPMENT CALIBRATION STANDARDS LOG No. C Al . . DUE LOG No. NBS No. (IF APPLICABLE)

. . . LD251 6 SEP 1984 L0350 522/223339 LO351 221482 LO263 11 JUN 1984 1.0561 NBS JOUR OF RES 81A 1.0563 NBS JOUR OF RES 81A 1.0565 NBS JOUR OF RFS 81A LO288 26 SEP 1984 LO414 NBS CIRCUI.AR t 36 LO485 11 JUN 1984 'LD560 NBS SRM 4241-2 THIS IS TO CERTIFY THAT THE ABOVE LISTED EQUIPMENT HAS BEEN cal.IBRATED TRACEABl.E TO THF NATIONAL BUREAU OF ..

STANDARDS, HAS BFEN DERIVED FROM ACCEPTED VALUES OF '

NATURAL PHYSICAL. CONSTANTS, OR HAS BEEN DERIVED BY THE -

i ~ RATIO-TYPE OF SEl.F-CALIBRATION TECHNIQUE AND MEETS THE REQllIREMENTS OF-MII. STD 45662.

BY Y .a ._ __ _

__ _ _ _ - _ _ _ ___ FOR QUALITY ASSURANCE DEPT.

MC iEL. J . D r.i-NUCLEAR CONSULTING SERVICES, INC.

e

. ~QA38 QA CHFCKLIST FOR RFVIEW OF INSPFCTION TEST DOCUMENTS

1. IS THE RF. PORT SIGNF.D BY PFRSON PERFORMING INSPFCTION OR TEST 7 ff) N
2. HAS THE REPORT BEEN REVIFWED AND SICNFD ( N BY AN AUTHORIZED PF.RSON?

3 93 IS ACCFPTANCE CRITERIA SPECIFIED? Y N s..

3a. IF SO, DOES IT MEET THE CUSTOMFRS Y N REQUIRFMENTS?

4. ARE INSPECTIONS OR TEST RF.SULTS SATISFACTORY?

)N 4a. IF NOT, WAS A NON-CONFORMANCF. REPORT Y N GENFRATED? s -

5. IF A NON-CONFORMANCE REPORT WA3 NOT GENERATED, EXPl.AIN BELOW.
6. COMMENTS: ///vf/#

t'

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SIGNATURE IN REVIEW SECTION OF DOCUMENT INDICATES SATTSFACTORY REVIEW.

~.

. NtICON 13CE413/02 THFSE RFPORT SHFF.TS CONTAIN THE IODINE FISSION PRODUCT TEST DATA OBTAINED FROM ADSORBENT SAMPl.F.S TFSTED BY NtiCON.

COUNTING WAS PERFORMED AT 0.364 MEV GAMMA 1.F. vfl., IN A 4.0" THAL.l.IUM ACTIVATFD SODIUM 70DIDE WElI. CRYSTAt., CALIBRATION OF THE CollNTING CRYSTAt HAS BEF.N PERFORMED BY THE USE OF AN NBS TRACEABl.F 131-7 STANDARD, g,

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-T- m *ty <-- e -

r NtlCON 13CE413/02 - P-TEST REPORT: MFTHYL 70DTDE DATF PERFORMED: 25 MAY 1984 SAMPLF: 4641 BATCH 4 *

SUMMARY

0F RESULTS

=======================

BED No. RFTENTION PENETRATTON STD. DEV.

1 99.370% .630% .0151%

THE* REST!LTS ARF THE BFST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUF.S AND ACCORDING TO OllR BEST- KNOWI.FDGE.

PERFORMFD BY DONAl.D P. WHITING DUCIEAR CONSULTIN SF.RVICES, INC.

APPROVED BY -

// / / M W. P. FRFFMAN '~NUCLFAR CONSULTING SERVTCES, INC.

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NUCON 13CF413/02

TEST REPORT: METHYL IODIDE DATE PERFORMED: P5 MAY 1984 CLIENT: COMMONUEAL.TH FDISON COMPANY, BYRON STATION POST OFFICF BOX 767 S AMP L.F : - 4641 BATCH 4 P.O. NO,t 266364

e. =. ** *%

TE'S'T CONDITIONS:

BED DFPTH 5.08 CM. ( 2.00 IN.)

BED DIAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATttRFS s

PRE-l.DADING 25.0 'C ( 77.0 'F) 1.0ADING 25.0 'C ~ ( 77.0 'F)

POST-1.0ADING R5.0 *C ( 77.0 'F)

REI.ATIVF HUMIDITY 95.0 %

FACE VFL.0 CITY 20.32 CM./SEC (40.O FPM)

CHAI.LENGE AGFNT CONCFNTRATION METHYL. TODIDF 1.75 nG./CU.M.

i TEST TIMF.S

~

PRE-LOADING 16. HRS.

LOADING 2. HRS.

, POST-l.0ADING 2. HRS. -

CAPTtlRED RADIDACTIVITY .33 MICR0 CURIES PRESSLtRF 1.00 ATM. ( 101.30 kP A) 5

r '

NUCON 13CF413/02 COUNTING DATA FOR SAMPl.F 4641 BATCH 4 AIR COUNT DATA

  • PRE-I_0ADING*

CPM = 1,353.0 STD DEV= 14.0 M P OST-l.0 ADING*

CPM = 1,353.0 STD DEV= 14.0 k*; _

TB1 COUNT DATA

  • PRE-l0ADING*

CPM = 1,381.0 STD DFV= 14.0 CPM-AIR = 28.0 STD DEV= 20.0 XPOST-l0ADING*

CPM = 342,470.0 ' - STD DEV= 480.0 CPM-AIR = 341,1P0.0 STD DEV= 480.0

  • NET
  • NET CPM = 341,090.0 STD DEV= 480.0 GB1 COUNT DATA
  • PRE-l.OADINGM CPM = 1,368.0 STD DEV= 14.0 CPM-AIR = 15.O STD DEV= 20.O y
  • POST-l.OADING* .

CPM = ~. 3,859.0 STD DFU= 36.0 CPM-AIR = P,206.0 STD DEV= 39.0

  • NET
  • NET CPM = P,191.0 STD DEV=

44.0 1

. ~

,. s.

iNUCON 13CF413/02 '

COUNTING DATA FOR SAMPLF 4641 BATCH 4 GB2 COUNT DATA

  • PRE-LOADING
  • CPM = 1,368.0 STD DF.V= 14.0 CPM-AIR = 15.0 STD DF.U= 20.0

' ' ' STD DFV= 13.0 <

I;';C P M - A I R = , -14.0 STD DF.V= 19.0

  • NET
  • NET CPM = -P.9.0 STD DF.V= 28.0 A +

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NllCON 13CF413'/02 -

TEST REPORT: METHYt. 70DIDE DATE PERFORMF.D: 26 MAY 1984 SAMPLE: 4784 DATCH 5

SUMMARY

0F RESULTS

:============================

BED No. RFTENTION PENETRATION STD. DEV.

p.v 1 99.59P% .408% .0079%

THE RFSUI.TS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUFS AND ACCORDING TO OUR BFST Kf! owl.FDGE.

/ ) /

PERFORMFD BY l A /

DONAl.D PY WHITING NUCI EAR CON 5ULTING SET JICES, INC.

APPROVED BY W. P.

FREEMAN

)///r/t414 NUCt. EAR CONSULTING SERVICFS, INC.

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NUCON 13CE413/0P ',

TEST RFPORT: METHYL IODIDE DATE PERFORMED: 26 MAY 1984 CLIENT: COMMONWFALTH EDISDN COMPANY, BYRON STATION POST OFFICE BOX 767 SAMPLE: 4784 BATCH 5 P.O. NO.: 266364

$.t, TEST CONDITIONS:

BED DEPTH 5.08 CM. ( 2.00 IN.)

BED DIAMETFR 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRF-LDADING PS.0 'C ( 77.0 'F) 1.0ADING P5.0 'C ( 77.0 'F)

POST-l.0ADING F5.0 'C ( 77.0 'F)

REl.ATIVE HUMIDITY 95.0 %

FACE vel 0 CITY 20.32 CM./SEC (40.0 FPM)

CHAL!.ENGE AGENT CONCENTRATION METHYi TODTDE .v 1.75 nG./CU.M.

TEST TIMFS ,,

PRE-LOADING 16. HRS.

LOADING 2. HRS.

POST-LOADING 2. HRS.

CAPTilRED RADIDACTIVITY .67 MICROCURIES PRESSURE 1.00 ATM. ( 101.30 kP A)

s l

1 NUCON 13CE413/02 - s-COUNTING DATA FOR SAMPIF 4784 BATCH 5 AIR COUNT DATA *PRF-l0ADING*

CPM = 1,P64.0 STD DEV= 13.0

  • POST-LOADING
  • CPM = 1,264.0 STD DEV= 13.0

$..s.

TBY COUNT DATA *PRF-l.0ADING*

CPM = 1,279.0 GTD DFV= 13.0 CPM-AIR = 15.0 STD DEV= 10.0 xPOST-LOADING * "

CPM = 694,440.0 s - STD DEV= 980.0 CPM-ATR= '693,180.0 STD DEV= 980.0

  • NET
  • NET CPM = 693,160.0 STD DEV= 980.0 GB1 COUNT DATA
  • PRE-l0ADING*

CPM = 1,360.0 STD DF.V= 14.0 CPM-ATR= 104.0 STD DFV= 19.0

  • P OST-l .D ADING
  • i CPM = s 4,P19.0 STD DEV= 4P.0
CPM-AIR = P,955.0 STD DEV= 44.0
  • NET
  • NET CPM = P.,831.0 STD DEV= 48.0 e

s u **e NUCON 13CF413/02 .

9- -

COUNTING DATA FOR SAMPLE 4784 TtATCH 5 GB2 COUNT DATA

  • PRE-l.0ADING*

CPM = 1,368.0 STD DEV= 14.0 CPM-A7R= 104.0 STD DEV= 19.0

  • POST-LOADING
  • CPM = 1,359.0 STD DEV= 14.0

-' CPM-AIR = 95.0

, STD DEV= 19.0

  • NET
  • NET CPM = -9.0 STD DFV= 27.0 6 e

. - s-j ., .. -

NUCON 13CE413/02 TEST RFPORT: MFTHYl. IOD7DE DATF PERFORMED: 27 MAY 1984 L-SAMPl. F : 4053'DATCH 1 l

SUMMARY

0F R E S-U L T S

==_==_-_===_======..================ _ .

BED No. RETENTION PENETRATION STD. DEV.

1 99.905% .095% .0061%

.THE RFSUI.TS ARE THE DEST ODTA7NABLE UNDER CURRFNT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OUR BEST KNOW1.F.DGE.

PERFORMF.D BY M DONAl.D P. WHIT)NG NUCl.FAR CONSUL ING SERVICES, INC.

APPROVED DY -

W. P. FREEMAN NUCl. EAR CONSULTING SERVICF.S, INC.

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. s NUCON 13CE413/0P TEST REPORT: METHYL. IODIDE DATE PERFORMED: 27 MAY 1984 CLIENT: COMMONWEAL.TH EDISON COMPANY, BYRON STATION POST OFFICE BOX 767 SAMPLE: 4053 BATCH 1 P.O. NO.: ?66364

.. +p, 6g TEST CONDITTONS:

BED' DEPTH 5.08 CM. ( 2.00 IN.)

DED DIAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATURES PRE-l.0ADING 25.0 'C ( 77.0 'F) 1.DADING 25.0 'C ( 77.0 'F)

POST-LOADING 25.0 'C ( 77.0 'F)

RELATIW HtlMIDITY 95.0 %

FACE vel.0 CITY 20.32 CM./SFC (40.0 FPM)

CHAl.LENGE AGENT CONCENTRATION

~,

METHYL IODIDE 1.75 nG./CU.M.

TEST TIMES PRE-LOADING 16. HRS.

LOADING 2. HRS.

POST-LOADING 2. HRS. '

CAPTllRED RADIOACTIVITY .50 MICR0 CURIES PRESSURE 1.00 ATM. ( 101.30 kPA)

2, = .

NUCON 13CE413/02 -1P-COUNTING DATA FOR SAMPl.E 4053 BATCH 1 AIR COUNT DATA'*PRF,-l_0ADINC*

CPM- 1,041.0 STD DFV= 10.0

  • POST-LOADING
  • CPM = 1,041.0 STD DEV= 10.0

.. e ff. l)

TBi COUNT DATA

  • PRE-lOADINGM CPM = 1,044.0 STD DEV= 10.0 CPM-AIR = 3.0 STD DEV= 14.0
  • POST-l.OADINGM CPM = 526,320.0 s - STD DFV= 740.0 CPM-AIR = SP5,280.0 STD DEV= 740.0
  • NET
  • NET CPM = 525,200.0 STD DEV= 740.0 GB1 COUNT DATA
  • PRE-l0ADING*

CPM = 1,068,0 STD DFV= 11.0 CPM-AIR = 27.0 STD DEV= 15.0

  • POST-LOADING
  • i CPM = 1,572.0 STD DEV=

16.0

. CPM-AIR = ,

531.0 STD DFV= 19.0

  • NET

504.0 STD DEV= 24.0 e

. s ev, -e =

NUCON 13CF413/02 COUNTING DATA FOR SAMPl.E 4053 BATCH 1 GB2 COUNT DATA

  • PRE-LOADING
  • CPM = 1,068.0 STD DEV= 11.0 CPM-AIR = 27.0 STD DEV= 15.0 MPOST-LOADING *

,,.. C P M r- 1,065.0 0; CPM-AIR = STD DEV= 11.0 24.0 STD DEV= 15.0

  • NET
  • NET CPM = -3.0 STD DEV= 21.0 N w e

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g_

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NUCON 13CF413/02 TEST REPORT: METHYL IDDIDE DATF PERFORMED: 28 MAY 1984 SAMPLE: 5?05 BATCH 6 '

S U M M'A R-Y- 0F RESULTS

~

=_==================::==

BED No.- RETFNTJON PFNETRATION STD. DEV.

cs 1 99.622% .378% .0084%

THE RFSULTS ARE THE BEST OBTAINABLE UNDER CURRENT EXPERIMENTAL TECHNIQUES AND ACCORDING TO OUR BEST- KNOWI.EDCF.

PERFORMED BY- /[_

~

DONAl.D P. WHITING NUCLE R CONSL TING SERVICES, INC.

APPROVED BY . g##A W. P. FREEMAN NtiCl. EAR CONSULTING SERVICES, INC.

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.,. . .' s i*~*,'* N,0 CON 13CF413/02- -

TEST ~ REPORT:. METHYL. TODIDF DATE PERFORMED: 19 riAY 1984 CLIENT: COMMONWFAl.TH EDISON COMPANY, BYRON STATION POST OFFICF BDX 767 SAMPl.E: 5705 BATCH 6 P.O. NO.: P66364

. v, TEST CONDITIONS:

BED DFPTH 5.08 CM. ( 2.00 IN )

BED DIAMETER 5.08 CM. ( 2.00 IN.)

TEMPERATURES 1 -

PRF-lDADING 25.0 'C ( 77.0 'F )

1.DADING 25.0 'C ( 77.0 'F )

POST-l.DADING 25.0 'C ( 77.0 'F )

RELATIVE HUMIDITY 95.0 %

FACE VELOCITY 20.32 CM./SEC (40.O FPM)

CHAI.LENGE AGFNT CONCFNTRATION METHYL. IODIDE 1.75 nG./CU.M.

TEST TIMES .

PRE-LOADING 16. HRS.

LOADING 2. HRS.

POST-l.0ADING 2. HRS.

CAPTURED RADIDACTIV7TY. .47 MICROCURIES PRESSURE 1.00 ATM. ( 101.30 kPA)

E.

r ~.  !

, . , ;~ . f.' \

  • NUCON 13CE413/02 COUNTING DATA FOR SAMPl.E SP05 BATCH 6 AIR COUNT DATA
  • PRE-l.0ADINGx CPM = 1,053.0 STD DEV= 11.0 MPOST-LOADING
  • CPM = 1,053.0 STD DFV= 11.0

.. 1..,

TBI'COUNTDATAMPRE-LOADING

  • CPM = 1,054.0 STD DEV= 11.0 CPM-AIR = 1.0 STD DEV= 16.0
  • POST-LOADING
  • CPM = 495,050.0 " - STD DEV= 700.0 CPM-AIR = 494,000.O STD DEV= 700.0
  • NET
  • NET CPM = 494,000.0 STD DEV= 700.0 GB1 COUNT DATA
  • PRE-l0ADING*

CPM = 1,060.0 STD DEV= 11.0 CPM-AIR = 15.0 STD DFV= 16.0 v

  • POST-LOADING *

~} _ CPM = '-

P.,890.0 STD DEV= 29.0 CPM-AIR = 1,837.0 STD DEV= 31.0

  • NET *

! NET CPM = 1,022.0 STD DEV= 35.0 e

[

c- .

3

, s .1

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. NUCON 13CE413/02 _j7, C0llNTING DATA FOR SAMPl.E SP05 BATCH 6 GB2 COUNT DATA

  • PRE-LOADING
  • CPM = 1,068.O STD DEV=

CPM-AIR =

11.O 15.0 STD DEV= 16.0 MPOST-1OADINGM CPM = 1,120.0

..* STD DEV= 11 0

,,f CPM-AIR = 67.0 STD DEV= 16.0

  • NF.T*

NET CPM = 5P. 0 STD DEV= P3.0 s -

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