ML20078J923

Public Version of Rev 3 to Emergency Plan Implementing Procedure LZP-1330-24, Determination of Reactor Coolant Hydrogen Offgas Concentrations at High Radiation Sampling Sys & Receipt Form

ML20078J923
Person / Time
Site:	LaSalle
Issue date:	09/16/1983
From:	Holyoak R COMMONWEALTH EDISON CO.
To:
Shared Package
ML20078J918	List: ML20078J923
References
LZP-1330-24, NUDOCS 8310170711
Download: ML20078J923 (38)

Text

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ATTACHMENT F Revision "O l (Page 1 of 2) .anuary it, tog 3

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.. 10C850.59 FORMAT FOR SAFiTf EfALUATION :o l-A$Mt.C $0UNTV f4170W UNIT

- STAT)CN sysity HRSS T~-siinnoCicuRE no. L2P-/330-26 $2Ll.4 TEST /PROCECURE T1T1.5lh%ndabien,o f Asache $oolon/ ""

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- SAFET/ 9/ALUATION: Answer the following questions with a "yes* or "no", and provice soecific reasons justifying the decision:

1. Is the prononility of an occurrence er the consequence of en accident, or malfunction of

{. , emiarnent irnoortant Yes t

to safe No, 3ecausa: /y as previously f% evaluated r hm in the Final h Safety Analy t.- increased?

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2. Is the possi*oility for en ceciaent or malfunction af a different tyoe therycny V previcusly No, 3ecause:

evolucted in the Final Safety Analysis Recort created? ---- Yes Gu2, M a. Cau.u d M by % M m ,4 t

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3. Is the margin of sag, as defined in the basis for any Technical Soecification, recuesa?

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I LZP INDEX GAGE ]

7/C5/83 DROC. NO. TITLE R Ev . AEV DATE CISAET l LZP 100-1 DELETED C3 11/8C Cl

.LP LCC-2 DELETED C+ 11/SC Cl LIP 1C0-3 DELETEC C3 10/60 Ci

.4P 200-1 DELETED C2 ll/SC 01 OELETED C2 ll/SC C1

' 4P

. 200-2

.ZD 2CO-3 DELETED C2 11/80 01

_ZP 200-4 DELETED C3 11/aC C1 LZP 210-1 DELETED C2 10/80 01 C4 d/30 C;

, .4P 300 DELETED LLP 300-2 DELETED C3 11/3C Ci C3 ll/8C Cl

_19- 310-1 GELETEC DELETED C2 10/8C 01 LIP 320-1 OELETED C1 10/6C 01 LLP 3J0-1 LIP 340-1 CELETED C1 10/80 C1 629 .5tC-1 CELETED C2 1C/80 C.

DELETED 02 LC/aC 01 LLP 3eL-1 DELETEQ Ci 10/dC 01 LIP 37L-1 C2 11/SC  ;;

LIP 400-1 OELETED CELETED C2 10/3C 01 LZ? 'CC-2 C; 11/3C C1 LZD *CC-3 OELETED OELETED Cl 11/8C 01

! LZ? 41C-1 L;D DELETEC C1 11/oC 01 420-1 C2 10/aC 21 LZ? 510-1 DELETED -

i CELETEC CZ 10/aC 01 i

L2P 520-1 l.

LLP 520-2 GELETED Ci .0/ec .i C1 10/50 21

LZ3 520-3 DELETED C1 10/8C 0; LZ? 530-1 'JELETED i

,, - - .m -: - ...- - _ . . . _ _ _ , . ,

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l IN0Ex PAGE 2 l 7/03/63- LZP PROC. NO. TITLE REv. AEv CATE GISAETT C2 10/30 01

_I? 23C-2 DELETED DELETED 01 1G/SC 01 IP 5*C-1 7CC-2 CELETED 01 11/60 01 L40 IP 71C-1 DELETED C2 10/80 01 31C-1 DELETED C1 10/6C 02 LZP IP 320-1 DELETED.- Cl 10/dC C2 01 1C/80 CZ

• I3 800-1 DELETED CELETED C1 10/6C 02 L4P 350-1 iP 360-1 DELETED C1 10/80 C2 DELETEC Cl ll/8C C2 LLP SSC-1

P 1110-1 STATION OIRECTOP ( ACTI 4G STATION C4 3/63 C2 CIRECTCR) IMPLEMENTING PRUCEDURE

• ? 1120-1 OPERATIONS CIRECTOR IMPLEMENTING C4. 2/ 8 3 C2

. PROCEC'JRE TECHNICAL DIRECTOR IMPLEMENTING PROC. C3 */dl 02

P 113C-1 9AINTENANCE DIRECTOR IAPLEMENTInG Cl 11/ SC 02 cIP 11-0-1 PROCECURE u'P 115C-1 STORES CIRECTCR IPPLEPENTI.4G PRCCECLRE C1 11/eG G2 ACMINISTRATIVE GIRECTGR IMPLEPENTI.4G C2 1/32 02 17 . loc-Cl PEOCECURE

• !P ll7C-1 SECURITY CIRECTOR IMPLEMENTING 04 7/83 CZ PROCECURE C3 7/81 02 LZP 113C-1 RAD / CHEM CIRECTCR IMPLEMENTING P RCC ECLR E 118C-2 RAC/ CHEM CIRECTCR INITIATED C1 11/dC 02 LIP ENVIRONMENTAL MCNITORING ACTIVITIES LLP 1190-1 ENVIRONS CIRECTCR I'NPLEFeNTING CC o/63 C3 PRCCEDURE CLASSIFICATIONS OF GSEP CG.wC IT IONS C3 d/S2 01

_lP 1200-1 HP 1200-2 CLASSIFICATION CF A NGoLE GAS RELEASE C1 5/d2 C2 LLP 12:C-3 CLASSIFICATION CF AN 10 CINE RELEASE Cl 2/32 C1

f LZP INDEX PAus 7/CS/d3 PROC. NO. TITLE RE/. AE4 OATE CISAETT CLASSIFICATION CF A LIOUIC RELdASE C1 3/82 01 LLP L20C-4 iP 121C-1 HAZARCOUS MATERIAL INCICENTS REPORTI'lG C2 3/o3 Cl ,

EMERGENCY TELEPHONE NU'4BER Cl 5/81 01 LZP 122C-1 DELETED Cl 7/81 01 19 122C-4 CCNTAINMENT ATMOSPHERE FOR RACICIDINES DETERMINATICN AND PARTICULATES ALTERNATE MEANS LIP 131C-1 NOTIFICATIONS Ott 7/83 C2 IP L320-1 AUGMENTATION CF PLANT STAFFING C5 9/83 c2 OELETED C2 7/82 02

' IP 133C-1 C2 7/d2 03

.49 1330-2 CELETED 133C-3 0ELETED C3 7/82 03

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OELETED C2 7/d2 03

'LZ? 1330-4 iP 1330-5 PCST-ACCIDENT NO3LE GAS AELEASE RATE CO ll/SC 03 DETERMINATION DELETED Cl 7/81 C3 IP 1330-o C2 7/ S2 C2 IP 1330-7 OELETED L43 133C-3 SAMoLING LICUIC PROCESS iCNITCRS Cjl 7[I3 C3 CU4ING LI4ulo MCHITOR nIGH RACIATION ALARM CCNCITICNS C1 1/82 03 Lo 133C-lO DELETED 133L-11 DILUTION AND TRANSFER OF GAS SAMPLES CC 11/d1 03 LLP 40 1330-2C PCST-ACCICENT ANALYSIS OF dARCN CO 3/o1 33 (SACAUP PRCCECURE)

ZP 1330-21 POST-ACCICENT ANALYSIS CF CMLCRIDE C3 o/82 03 L'ZP L330-22 CALIdRATICN OF THE"MODEL 1C CIONEX C2 */82 03 ICN CHRCMATCGRAPH 133C-23 CETERMINATICN CF REACTOR COOLANT PH, C2 S/d2 03 u!3 CCNDUCTIVITY AND OISSCLVE0 CXYGEN CCNCENTR ATICN AT THE HIGH RADIATICN SA'4PLE SYSTEM

• 47 13 30 -2 + OETERMINATICN OF REACTJR COOLANT 03 $[g1 Ja nYJRCGEN ANC CFF-GAS CJ,CENTRATIONS AT THE HIGH PADIATION SAMoLING SYSTEM

7/03/53 LZP INDEx PAGE 29JC. no. TITLE REV. REV DATE CISAETT ia 133C-25 SAMPLIr.G CF REACTOR CG0LANT AT THE 02 o/82 03 HIGH RACIATION SAMPLE SYSTEM iP 133C-2E SAMPLING OF CONTAINMENT AIR AT TnE 03 o/d2 03 HIGH RACIATICN S AMPLIf,0 SYST EM YP 133C-27 DELETED C2 10/e2 03 L2P 133C-29 SAMPLING CF RADI0 ACTIVE .vASTE LIQUICS C2 o/c2 03 RADI0 ACTIVITY AT TNE NIGd RAOIATICN

.19 1330-29 DELETED' ' C1 1C/82 03 IP L33C-3C TRANSFER OF dASTES FRCM THE HRSS WASTE CC 11/81 03 TANK ANC WASTE PUMP

' EP 1330-31 DELETED Cl 8/ 82 C3 uLo 1330-32 POST ACCICENT SAMPLING OF THE GE'4ERAL C2 3/83 C3 ATOMIC WICE RANGE GAS MONITOR LP 1330-33 ISOTOPIC ANALYSIS OF LIQUID SAMPLES CO 6/32 03 USING AAIS SOFTWARE =ITH PARAPS HARDWARE LIP 13 3C-34

• ISOTOPIC ANALYSIS OF NOSLE GAS SAMPLES CC o/o2 C3 USING AAIS SOFTaARE AND PARAPS MARDWARE 133C-35 ISCTOP IC ANALY SIS 1001.4 SAMPLES USING CO o/ci 03 LZP AAIS SCFTWARE ANO PARAPS MARDWARE L;P 1330-3o ISOTOPIC At4ALYSIS OF PARTICULATE CC o/62 C3 SAMPLES USING AAIS SOFT.iARE n1Th PARAPS NARDnARE RADIATION SURVEYS UNDER ACCIDENT CO 10/51 03 LLP 133C-5C CONDITICNS IMPLEMENTING PRCCECURE FOR FIRE: Cl 7/ dl 02 i L!P 134C-1 i FIRE MARSHALL i

ulP 1340-2 IMPLEMENTING PRCCEDURE FOR FIRE: C2 3/d3 Ci FIRE CHIEF (CESIGNATEC SnIFT FOREMAN) 13*C-3 IMPLEMENTING PRCCEDURE FOR FIRE: Cl 9/31 02 ZP FIRE OFFICER 31 (COGNIZANT MAINTENANCE FCREMAN) w2P 13*C-4 IMPL3MENTIdG PRCCEDURE FOR FIRE: Cl 9/51 Ci FIRE BRIGADE IMPLEMENTING PRCCEDURE F3R GIRE: Cl d/ol 02 I P L3*C-5 l FIRE CCMPANY NJ. 1 ( M A I 4T E'l A NC E '

PERSONNEL) l l

I/Co/S3 LZP Ih0EA da6E JR C. 40. TITLE REv. 4Ev 0 ATE GISAETT

.2? 1260-1 PROTECTIVE MEASURES FGR ON-SITE C3 7/dl 02 PERSONNEL (P 1360-2 USE OF POTASSIUM 10CICE (KI) AS A C1 1/S3 03 THYROID BLOCKING AGENT IP 136C-4 RADIATICN PROTECTION PRACTICES CURING CO 11/S1 33 ACCIDENT CONDITICNS iP 137C-1 RESCUE CO lO /oC C2 LZP L37C-2 PERSONNEL INJURIE'S CZ ll/c2 04 to 1370-3 SIRST AID, DECCNTAMINATION ANC CC 10/80 02 EVACUATION CF EXPOSED AN0/GR CONTAMINATED CASUALTIES

.LP 1330-1 CCNTROL OF CIL SPILLS Cl 12/32 02 LP 1620-1 ROLE ANC STAFFING OF THE 0*4-SITE T5C 01 11/8C 02 143U-L ROLE ANC STAFFING OF THE Cri-SITE CSC C2 */bl 02 LLo 16*C-1 ON-SITE GSEP COMMUNICATIONS SYSTEMS C3 12/d2 02 LP DELETED Cl 7/81 02 LZP l*s0-1 LP 145C-2 DELETED Cl 7/81 01 i EP 1510-1 GSEo CPERATIONAL READI::ESS CC 10/9C Cl

$20 L52C-L TRAI'4ING RECUIREMENTS CC 1]/oC 02 1530-1 dXhRCISES AND DRILLS Cl S/St 02 23 LL/ 155C-1 FIRST AID FACILITIES FONTHLY C2 12/82 OZ SunVEILLANCE LIP 15 5C -2 ENVIdONS SAMPLING SUPPLIES I 4VENTCRY C3 12/62 Cl DECL.4TAMINATICN FACILITIES MCATHLY 01 5/dl 02 LP 155C-3 SURVEILLANCE

'Z? 155C-4 ST. MARY'S HOSPITAL MEALin PHYSICS Cl 7/31 12 SUPPLIES LUARTERLY , SURVEILLANCE LIP 155C-5 TECHNICAL SUPPORT CENTER JUARTERLY C2 2/63 Cl SUAVEILLANCE LIP 155C-c CPERATICNAL SLDPCRT CEaTER CUARTERLY C2 2/33 01 3URVEILLANCE C3 -fo3 Q1 LLD If 5C-7 GELETEs

i LZP INDEt PAGd 7/Cd/33 2RCC. NO. TITLE REV. 46V OATE CISAETT P 155C-8 DELETED C3 3/83 02 (NARS) MONTHLY SURVEILLA4CE

!P 155C-9 SPECIAL TLD QUARTERLY SUAVEILLANCE O2 11/81 03 ,

1550-10 ENVIRCNNENTAL SURVEILLANCE STATIONS CO 7/dl C2 LZP IP 155C-11 POST-ACCICENT SAMPLING E;UIPMENT 01 7/g3 C3 INVENTORY

P lelC-1 RECOVERY ANO RE-ENTRY PLANS CJ IC/30 C1

_ZP 17CO-1 GSEP STATION GRCUP OIRECTLRY C5 1/63 01 iP 1700-2 STATION EMPLOYEE LIST c5 7/g3 al (P 1700-3 STATION PHONE LIST C, 7/83 C3 l

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LZP-1330-24 Revision 3 Septemoer lo, 1983 1

DETERMINATION CF REACTOR COOLANT HYOROGEN ANC 0FF-GAS CGNCENTR ATICNS AT THE HIGH R ACI ATION SAMPLING SYSTEM A. gugacS3 The ' purpose lof thi s procedure is to celineate a metnoc of obtaining a reactor coolant off gas sample at the Mign Raciation Sampling System (HRSS) during normal ano post-accicent conditions. This procacure incluces tne steps to route gas tc the Chamical Anal ysi s Panel (CAP) ano the Chemical Monitoring Panel (CMP) for hycrcgen analysis.

B. REFERENCES

1. Sentry Equipment Corpcration, Pcst-Accicent Sample System, Vclume 1.

2. LZP 1330-34, " Isotopic Analysis of Nocle Gas Sa.nples Using AAIS, Software witn PARAPS Harcaare."

C. gagggcurSrTeS

1. Estaolisn communications witn the Unit . Nuclear Station Operator (NS0) and i n f orni n im or all valves opened or closec from the HRSS Valve Cortrol Panal, OPLO9J.

2. Inform the Unit NSO :nat it may os necessary for nim to overrice i sol ati on signals, if prasent, to sample via the Reactor Recirc Loop 8. Install jumoers to overrica tne sample valve isclation signal s in accordance with the folicwinc:

l l

a. Install a jumoer oetaeen terminals AA-2o anc l

BS-7C in panel 1(2)H13-P623 to open valve 1(2)S33-F020, RX aTR SAMPLE VLV.

l I

o. Install a jumper cetween terminals AA-Zo ana 38-70 in panel 1(2)H13-P622 to oper. valve 1(2)e33-F019,, Rx ATR SAMPLE VLv.

[ 3. Verify that argen, anc nitrogen, app rcx imatel y 100 psig, is availaole at tne Liquia Samplir.g Panel (LSP), CPLG8J.

4. Verify that carrier and cal i o r at i on Jases are availaola to tne CAP, OPL51J, as folicws:

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• LZP-1330-26 Ravision 3 Septemcar 16, 19o3

a. Cnromatography grace argen carrier gas, approximatel y 40 PSIG.

o. Calioration gas ut, 10 percent nydrogen (oy volume) in argon carrier, apprcximately 20 PSIG.

c. Callbration gas 02, 2000 ppm (0.2 percent) hycrogen (by volume) i argen carrier, approx i matel y 20 PSIG.

d. Hycrogen, minimum 99.9 percent pure, ror Callorations onl y.

4. Equipment:

a. Gas tight syringe sizec as necessary, for caliorations onl y.

c. Hydro' gen concentratico vs. peak heigrt charts.

c. Reach rocs.

a. Griptong.

e. Reactor coolant orf-gas sample octtla nitn ,

septum.

f. Neeale flusn tool .

O. P3jcauTIch5

1. A Regulatory Guice 1.3 or 14 release of fission procucts implies estremely nign levels cr racioactivity. Oose rates may oe nigh encagn to prevent entry into mary areas of the plant tnat ara normally habitaole. Rac/ Chem Suoervisicn snoula te ccntacteo pricr to entry into any area anen sucn a release is suspectac.

2. near raciation dosimetry as recommended oy Rac/Cnem Supervision. ,

3. dear protective clotning anc respiratcry protection as recommenoec Oy lad / Chem Supervision.

4 Appropriata survey instrumsets snculd as availaole for monitoring curing tnis prccsaurs.

. Tv f

i LZP-1330-24 Ravision 3 Sep secer to, 1963 3

5. The chrcmatograph calioration should ce checxec daily or unen in use cy analyzing a calioration gas standara, CAL-1 or CAL-2.

6. CaliDration shoula De per formec upon i nstall ati on '

and ouarterly therea f te r . The s y ste.n sroulo ce recaliorated wnenever columns are changed. or syscem volume changeo, since ,sucn cnanges, oy affecting peak heights and retention times, can leac to ,

erroneous estimates of reactor cociant tycrogen ,

concentrations.

7. Retenticn time for hycrogen and otner gases .311 vary witn argon carrier gas pressure. Tne gas pressure snould remain constant at 40 PSIG for  ;

routine analytical use.

8. The systar is intencec to De operated usiqq on1y four (4) attentuation settings on tne cercmatcgrapn.

The settings are 5 x 1, 25 x 1, ICC x 1, 5x 1C0.

Under no circumstances snould tne system ce operatec alth attenuations different from these, except curing system warmup and stab il i zat i on.

9. Chromatograpn verification snows tnat tre enrematograpn performance has not cegrao+c. This is critically c9pencent on tne setting of the chrcmatcgrapn's cock oressure regulating val ve. Unaer oc circunstanc=s snoulo this valve ce aajusted without pricr ap;roval of Raa/ Chem Supervision.

10. Curing a post-accident conoition it will not ce possiole to change tne valve line-up in tre HRSS Cooler Room following sampling operations. Therfore, extrere care snould ce exercisac wnen performing-tne initial valvs line-up.

E. Lig!TATICNS ANC ACTICNS

1. Notify Rad / Chem Supervision if any proolers are encountered at the HRSS sanels.

2. This procecure, thougn intancea for use unaer sost-accidant conditions, con ce used for sanpling at the HRSS panel s curing rormal operaticos, during nhich the precautions li staa may nave limitsu apslications. However, normal routine sangling arecauticns shoula ce aoservec.

)

L2P-1330-24 -

Revision 3 Septsmoer 16, 1963 4

3. During sampling operations, the HRSS Waste Tanx pressure snoula oe coservea on the valve Control Panel, CPLO9J.- In tne event of the auste Tank pressure reaching 35 PSIS, all sampling operations shall oe secureo until tne waste gas in tre maste Gas Hola-up Tank i s trans f er red to a Supprassion Pool.

F. P10CE00RE qaurica

• Curing a post-accident condition it will not ce possible to change the valve line-up in tre HRSS Cooler Room following sampling operations. Therafore, extreme care shoula os exercisac wnen performing the initial valve line-up.

1. I f, dur ing post-acci dent sampling, tne valve line-up in the HRSS Cooler Room nas oesn verifiad curing previous sampling evolutions, it is nct requireo to veri fy the line-up onca acre. as tna raciation levels in the HRSS Ccoler Room would 00 entrsmely hign.

If the valve line-up nas not been verifisc, perform the line-up in accordance with tne folic ing:

a. For Unit 2 sampling procesa in acccrcance witn Step F.1.c; ror Unit 1 sampling, proceed in accordance witn tne folicwing:

1) LE12-F4133, RhR Laoc 13 adSS Saxpl a Aanual isolation, CPEN.

2) lE12-F913A, RNR Lcop 1A MRSS Saxple Aanual Isolation, CPEN.

3) 1233 8359, RR tcop 13 HRSS Saxole 3constream Manual I sol at i on , OPEN.

4) 1833-F3cC, RR Loop 13 HRSS Sample upstrear Manual Isclatione OPEN.

5) 1 B 3 3- 5 3 6'1, RR Loop 13 Al ternate Sampl ing Station Downstream Manual Isolation.

CLOSEC.

6) 1633-F362. RR Loop 13 Al te rnate Sa.npl ing Station Upstream Manual Isolaticn, CLOSEJ.

t -

L4P-1330-24 Ravision 3 Septemcer lo, 19o3 5

7) 1G33-F362, Unit 1 RT Cemin Inlat HRSS r Sample Manual Isolation, GPEN.

8) LG33-F360, Unit 1 RT Demin Cutlet nRSS Sample Manual Isol ation, GPEN.

9) 2G33-F3e0, Unit 2 RT Darin Cutlet MRSS

. Sample Manual Isol ation, CLCSED.

10) 2E33-F61, RR Loop 28 Alternate Sample Station Downstream Manual Isolation, UPEN.

11) 2833-F362. RR Loop 28 Al ternate Sampl e Station Upstream Manual Isolation, GPE 4.

12) 2S33-F359. RR Loop 23 HRSS Sarole Ocanstream Manual Isolation, CLOSE0.

13) 2833-F360, RR Loop 2d HH35 Sarple upstream Manual Isolation, CLOSEC

14) 2E12-F4138. RHR Loop 28 HRSS Sarbl e Manual Isolation, CLOSEO.

15) 2G33-F362, Unit 2 RT Oerin Inlet NRSS Sample Manual Isolation, CLOSED.

16) 2E12-F413A, RMA L0op 2 A HRSS S arpl e .danual Iso 11 tion, CLOSED.

17) Proceed to 5:40 F.2.

o. For Unit 2 sampling proceed in acccrcance witn the following:

1) LE12-F4136. RhR Loop la HRSS Sarple Manual Isolation, CLOSED.

2) lE12-F413A. RHR Loop 1A ndSS Sarple Manual Isolation CKOSED.

3) IB33-F359, RR Loop 18 HRSS Sarple Ocanstream Manual Tsolation, CLOSEC.

4) la33-F360, RR Loop 13 HRSS Sarple Upstream Manual Isolation, CLOSEC.

5) 1833-F361, RR Loop 13 Alternate Sampling Station.Dcwnstream Panual Isolation, GPEN.

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L2P-1333-2*

Revision 3 Saptamoer lo, 1983 e

6) IB33-F362, Rd Loop 13 Alternate Sampling Station Upstream Manual Isolaticn, CPE?l.

7) 1G33-F3o2, Unit 1 RT Demin Inlet NRSS Sample Manual Isolation, CLCSE0.

8) LG33-F360, Unic 1 RT Cerin Cutlat MRSS Sample Manual Isolation, CLCSED.

9) 2G33-F360, Unit 2 RT Damin Cutlet MRSS Sample Manual Isol aticn , OPEA.

10) 2833-F361, RR Loop 23 Alternate Sample Station Ocwnstream Manual Isolaticn, CLOSED.

11) 2833-F362, RR Loop 23 Alternata Sample Station Upstream Manual Isolatien, CLOSED.

12) 2833-F359, RA Loop 23 HRSS Sample downstream Manual Isclation, OPEN.

13) 2833-F360, RR Loop 23 HRSS Sarple upstreen Manual Isolati]n, OPEN.

14) 2E12-F4135, RPR Loop 23 HRSS Sample Manual I sol a t i o.n , CP E.1.

15) 2G33-F362. Unit 2 RT Camin Infat HRSS Sample Manual Isol aticn, CPEN.

lo) 2E12-F*13A. AMA Loop 2A ndSS Sample 1anual Isol ati on. CPE1.

2. If not already cne turn ne main power suiten an the CMP, CPLE4J, to tra JN positicn.

3. Verify tne prcper program is in tre microprocessor memory in acccrdance witn tne following:

a. Place all function swicchas in the OLT pcsi ti on.

o. By entering t'ne stea numcar, verify th a tia.a anc commano coca are entereo proparl f. E(AMPLE:

anter C1, tne oisplay sncalo reac Cl 0C Cl G3.

Ensure all steps rasc as follows:

E .

LZP-1330-24 Revision 3 Saptemoar lo, 1983 7

( '

IINE Ilts 50Gi 01 01 01 03 C2 00 C2 25 03 CC 25 01 04 01 CC 06 C5 01 15 00

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c. If all steps of tno program are not properly entereo in the memory, proceso in..accordanca with tne following:

1) Depress the ENTER anc CLEAR pusroustons.

2) Entar the (cllowing sequances or connancs, f rom lef t to rignt:

JIEE IDi 52Ss 01 CO 01 03 02 CO 02 25 03 CC 25 01 C4 C1 00 C4 05 C1 15 00

3) Repeat Steos F.3.a. ana F.3.0. to verify tha propar progra, mming.

.?.E15 c cr noun names associatec itn tne valves caerataa in tnis procacure, refer to Attachmgne G.

4. Perform the fc11owing valve lineup:

a. Verify valve V-1 is coen.

D. Open valve V-14 anc varif f tne 3rgen prassure gauge reacs 40 PSIG. Aajust pressure ragulating v al ve if necessary.

c. Open val ve V ,10 anc veri f f na air pressure gauge raads 100 PSIG. Adjust pressura regulating valve if necessary.

5. Startup tre gas enromatograph in accorcance with the following:

i

LZP-1330-24

' Revision 3 Septe noer los 1983 8

.a. Select an attenuation facter of 25C (25 x 10).

o. Despress MAN and CLEAR pushouttons.

c. Enter coce "00" cn neyooarc.

~

d. Allow tne enromatograph to stabilize for 30 minutes if pcwer was just restcred.

e. Cisplay platen setpoint temperature cy entering "01", tnen "35" anc recora for a minimum of 30 seconds. Tnen display actual platen temperature oy entering "45" and recera for a ririmum of 30 seconcs. Setpoint and actual temperatur2s snould oe witnin 1/2 gric mar <ing cf one anotner.

M3 0

The platen setpoint temperature is routinely 30 C.

f. As necessary, enter "4o" to reset the ci spl ay anc then repeat Steps F.5.e. and F.5.f. at a minitur cf five minute interval s urtil staoilization i s acnievec.

6. Perform the crrcmatograpn verification in acccrcance witn tne folicwing:

$3 This prccedure serves to serif / that tne enromatograon performance nas not chsngea fram previcus use anc calioration. The procecure shoulc ce run (1) unenever the instrument has ceen snutacan for extancea periocs and twice (2) dail) curing normal use.

a. Release AuTC anc ENTER pushcuttons.

o. Depress FAN anc CLEAR pusnouttens.

c. Enter coce "C0" cn Keyocarc.

d. Verify that SAMP pushoutton is releasec anc sarple Icop 01 i s selectea.

e. Enter "23" to initiata evacuation cf :ne enromatograon.

LZP-1330-24 Revision 3 Sep ta'noe r lo, 1963 9

f. Verify that the rac nign vacuum light is on ,

after a few minutes.

g. Enter "24" to termi nate evacuation.

n. Select SCO (5 x 100) attenuation if CAL 1 (1C percent hydrogen) will os used. Select 25 (25 x 1) attenuation if CAL 2 (2CCC ppn hycrogen) will oe ased.

i. Depending on the attenuation selectec, depress the CAL 1 or C AL 2 pusnoutton. wait 5 seconos and verify that tna amter low vacutm l ignt is ,

on.

j .. Release CAL 1 anc CAL 2 pusnoutton and wait 10 seconos.

k. Start tne L&N recorder ano depress AUTC pusnoutton.

1. Cepress CLEAR.

m. wait until the display clocx nas timed to tnrae (3) minutes, then release AUT0, capress CLEAR, anc enter "00". Stop the LsN recorder.

n. Laoel the L6N recorder trace with cate, tima, cal icration gas used, loco numoer, ano attanuaticn useu.

o. Calculate ene hycrogen peak neight "x" using:

x = (P x (A) / (ICC)

Where: P = Trace peax neicnt

( itn caseline suotractac),

L&N recorcer scale units.

A = Attsneation.

p. Verify that x i s .i tni n 2 5% of tne value snc.n on the ccncen'trati on ve rsus peax neignt cnar-for tne selectec attenuation and calioration gas. If x is greatar than 1 5t cf the value snown, ccatact Chamistry Supervisicn.

7. At une LSP. OPLD8J. aa r f o r.n the initial valve line-up in accorcance nitn tna following:

LLP-1330-24 Revision 3 Septemoer 16, 1983 10

a. RC-V-1.1 (closec), coordinate I-9.

o. RCV-1.2 (closec), coorcinate J-9.

c. RC-V-1 3 (closeo, coorainate K-9.

K-9.

d. RC ,V-1 4 (closec), ccorcinate

e. RCV-1.5 (closec), coordinate L-9.

f. RC-V-2 (Cicsed), coordinate I-7.

g. RC-V-3 (open), ccorcinate G-6.

n. Verify 9C-V-4. ccordinate J-lO, is closec.

Connect tne flush water hose tc RC-0-1 ano open tne flush water line salve.

i. RC-V-5.1 (closea), coorainate H-10.

j. RC-V-5.2 (closec), coordinate H-d.

^ '

4. RC-V-7 (closea), coordinate I-6.

1. RC-V-6 1 (closec), coorcinate M-9.

RC-V-8.2 (cpsn), ccorcinate .*-7.

m.

n. RC-V-9 (cpen). ccor Ji nate N-7.

c. RC-V-lO (ocen). c aoordi nate M-2.

p. FC-V-11 (closec), cacrainate C-3.

q. RC-V-12 (closed), coordinate L-1

r. RC-V-13 (closac), coordinate L-2.

s. RC-V-14 (closec, cooroinate L-2.

c. RC-V-15 (closec), cocrcinate K-2.

u. RC-V-16 (closao), coorcina+.e N-9.

v. RC-V-17 (closea), coordinate F-7.

, ,- g- ,-4 , - - - - -

r -s e e ,_,

LZP-1330-24 Revisicn 3 Septemoor to, 19da 11

d. RC-V-18 (6 o' clock), coorcinata C-7.

x. RC-V-19 (oypass). coorcinata P-8.

f. RC-V-22 (tc waste), cocrainate R-7.

z. RC-0V-1 (bypass), coorcinate Q-8.

aa. RC-DV-2 (9 o' clock), coordinate M-3.

Dry the expansion vessel RC-EV-1 in accercance itn S.

the following:

a. Turn RC-V-ll cloc4 wise tc tne 3 c'cicek position.

o. Pull open RC-VREL-2. wnen there is a snarp increase in pressure indicated on RC-G-3, rel ease RC-VREL-2.

c. Adjust RC-VREL-2 until RC-G-3 indicates approximately 20 PSIG. Dry RC-EV-1 witn argon for a minimum of one (1) minute.

c. Turn RC-V-11 ccunterclockwise to tr.e 9 o' clock position to permit RC-EV-1 te vent, unen close PC-V-9.

9. At tne HRSS Valve Control Panel, CPLO9J. procaac in accorcance witn the following:

a. Place tne U:4IT 1(2) POWER sai cn ir ne CPERATE positicn.

D. CPEN OWT-053, TBCCd IN VLv TC HRSS CCCLER RACA anc CWT-054, TSCCA RTN VLV FROM FRSS CCOLER RAC4, and verify the indication sncas CPEN.

c. CLCSE the normal sample valve for all systems l and verify all indication snow CLOSEC in accordance itn tne f ol l ow i ng:

1) 1(2)333 .F358, RR LOCP B TC NCRM SAMPLE VLV.

2) 1(23G33-F355. RT DEFIN IN TC AORM SAMPLE VLV.

3) 1(2)E12-F411A, A RHR LCCP TC ACRM SAMPLE VLV.

. _ . - _ .. i b

LZP-133C-24 Revision 3 Septemoer 16, 19e3 12

• ) 1(2)E12-F4113, S RHR LOCP TC AGRM SAMPLE VLV.

5) 1(2)G33-F357A, A RT JEAIN OUT TC NORM SAMPLE VLV.

1(2)G33-F3573, o RT DEMIN OUT TC NORM

6) ~ SAMPLE VLV.,

7) 1(2)G33-F357C, C RT 3EMIN OUT TC NORM SAMPLE VLV.

10. Request the Unit NSC per form tne initial valve line-up of the sample line containe.ent isolaticn valves on panel 1H13-0601 locateo in tne Centrel Room, for une sample to De ootainec, in accorcance witn tne follo ing:

33 In a post-accident condition, with containment isolation in effect the sample may De octainec from either Reactor Recird Loop 3, or RHR Heat Exchangers A or 8, of operating. However, if containment i sol at i on is not in effect, the sample way oe ootained from eitner Reactor Recirc Locp 3, RHR A, RHR d, R 'aC U inlet, RWCU A outle . RaCU 3 outlat. or RaCJ C outlet, aith no assistance frca the urit NSC.

a. To sample via Reactor Recirc Loop 2, aitn c0ntainment isciation in effect, request cne Unit NSO to open ene following:

1) 1(2)S33-F019, RX nTR SAMPLE VLV.

l 2) 1(2)d33-FC20, RX nTR SAMPLE VLV.

o. To sample via RHP Meat Exchanger A, witn containment isolation in effect, request ene Unit NSO to npen tne fcilowing:

85 The following valve ccatrol switenes rust ce held in the open pcsition.

l ~ - . _ _ .

I LZP-1330-24 Revision 3 -

Septernoer lo, 19o3 13

1) 1(2)E12-FC6CA, RHR A SAMPLE LA VLV.

2) 1(2)E12-F075A, RNR A SAMPLE LA VLV.

c. To sample via RHR Heat Excnanger d, witn containment isolation in affect, request the Unit r450 to open :ne follo.ing:

$IE The following valve control switcnes must ce helu in the cpen position.

1) 1(2)E12-FC603, RNR 8 SAMPLE LA VLV.

2) 1(2)E12-F0753, RHR 3 SAMPLE LN VLV.

11. OPEN the HRSS Sample valve for tne system to os sampled anc verify tne indication snows CPEN in accordance witn the following:

a. 1(2)B33-F357, RR LCOP B TO HRSS SAPPLE VL/.

o. 1(2)G33-F356, RT JEMIN IN TO NRSS SAFPLE VLt.

c. 1(2)S12-F412A, A RM4 LCCP TO HP SS SA*PLE VLV.

d. 1(2)E12-F4123, 3 RHR LCOP TO HRSS SAPPLE VLV.

a. 1(2)G33-F358A, A RT CEMIN CUT TO HRSS SAMPLE VLV.

f. L(2)G33-F3588, 3 AT DEMIN CUT TO HRSS SAMPLE VLV.

g. 1(2)G33-F358C, C iT CEMIN CUT TO HRSS SAMPLE VLV.

1.*,

12. At the LSP, OPLC8J. OPEN RC-V-1 1 (1 2, 13.

or 1 5) cepenoing on tne sample source.

13 At tne LSP, OFLC8J. OPEN RC-VREL-1 until RC-FI-L indicates 35-40 in'ches of nater. Purge fer a minimum f of 30 minutes.

14. Sl owl y cl ose RC-VREL-1 ant il RC-FI-l incicates 12-15 incnes of water. Continue the purgs for one (1) minute, than closs RC /-3.

L2P-133C-24 Revision 3 Septemoer 10, 19o3 14

15. Open RC-V-8.1.

16. Open RC-V-2.

17. Adjust RC-VREL-2 until RC-FI-2 incicates id-22 incnes

• of water. Purge for a minimum of three (3) ainutes.

18. Close RC'-V-8 2.

19. Closa RC-V-8.1.

2C. Close RC-V-1.1 (- 1. 2, - 1 3, - 1 4, -1.5). Recoro the time on LRC Form 1097A (Attacnment F) as tnis is tne sample time.

21. CLOSE the HRSS sample val ve opensa in Step F.11.

ana verify tne indication shows CLOSEC. For samoling during normal operaticns, OPEN tne normal sampl e valve closed in Step F.9.c. and verify tne incications snow OPEN.

22. Pl ace RE ACTCR CCOL ANT LIJUIC S AMPLE d ACxFLUSn switch to the sample line f or tne systera sampled.

23 Open RC-V-7 and then cpen RC-y-6

24. Adjust RC-vREL-2 until RC-FI-2 inoicates 1S-22 incnes of water. Flush ni tn demi neral i zed water for a minimum of three(3) minutes.

25. Close RC-V-7.

20. Open RC-V-3.

27. Adjust RC-vREL-1 until RC-FI-1 inoicates 35-40 incnes of .ater. Flush .ith ce.ni na ral i zed water for a minimum of one (1) minuta. Close RC-V-3.

Open RC-V-1.1 (-1.2, -1 3, -1.4, -1.5). Flusn nitn 26.

demin water for a mi ni mu.n of five (5) minutas.

29. Cl ose RC-V-1.1 (-1,.2, -1 3, -1 4 -1.5).

30. Close RC-V-4.

31. Inform tne Unit NSO that sampling operaticns are complete. and request tnat theasUnit 450 closa cne necessary.

valves openeo in-Step .10.,

__ ~ __ . . _ .

tZP"-1330-2*

Revision 3 Septemoer lo, 1963 15

32. Evacuate the_ expansion vessel and sample lines in accorcance with the following:

a. Install the oilutaa gas sample octtle on ene front panel needle.

D. Open RC-V-13 and then cpen RC-V-12 and ev6cuate unti l RC-G-2.1 and RC-G-2.2 incicate a minimum of 22 inches of mercury.

c. Turn RC-CV-2 to tne o o' clock positicn anc continue the evacuation until RC-G-2.2 indicates the same reading as RC-G-2.1, er a minimum of 22 inches of mercury.

d. Close in order, RC-V-13. RC-V-10, anc RC-V-12.

Record the vacuum on RC-G-2.1 cn LRC Form 1097A (Attachment dait for a minimur cf two (2) minutes and F). verity that the vacuum is hoicing.

e. Turn RC-V-ll glggigigg to tne CLCSE3 position. .

f. Turn RC-CV-2 to tne 9 c' clock positicn.

g. Open RC-V-14 and verify the pressure on RC-G-2 2 is approximataly 1 psig.

33. Prepare the gas chromatograpn for samcl a anal ysi s in accoraance nith tne following:

a. Open or cneck open valve V-1.

A i D. Release tne AUTO and ENTER Jusnouttons.

j

c. Depress NAN and CLEAR pusnouttons.

d. Enter coce "C0" on :ne keyocaro.

e. Cepress the SAMP sushoutton anc verify tne reo sarple light in cn.

f. Select Lcop 01.

t

g. Enter "23" to initiate evacuation cf the enromatograpn.

n. Verify tre red nigh vacuum light is en after a fea T.inutes.

LZP-1330-24 Revision 3

- Saptemoer lo, 1963 to

(

i. Cycle through locps le 2, 3, ana 4, pausing at eacn Icop for 5 seconcs. Repeat fcr a total of three cycles.

j. Select Lcop cl.

k. Ent,er "24" to terminate evacuation.

1. Select an attenuation cf 5 (5x1) fcr normal operation, or 500 (5 X 1C0) for. post-accident situations.

34. Open RC-V-9, wait approximately five (5) seconds, and close RC-V-9.

35. Open RC-V-16.

3o. Snap coen RC-V-9 and .ai- for one (1) minute.

37. Close RC-V-lo and then close RC-V-9.

38. Turn RC-V-11 gounterclocigigg to tne 9 c'cicck position. The pressure reacing on RC-G-2 1 is normally between 8 ano 10 psig. Recora tre reading on LRC Form IC97A (Attachnent F).

39. Verify with the C."P. CPLE4J. cperator trat tna gas chromatograpn is ready cc receive the sample.

40. Open RC-V-15.

• 1. Luad tne gas enromatograpn sample Icops and anal ge tne sample in accorcance witn ene fcilowing:

a. Cycle tnrougn locos 1, 2, 3. anc 4; pausing at each loop for 5 seconds. Rapeat fcr a total of three cycles.

b. Select icop 01, and release tne SA.VP pdshoutton.

c. Cicse RC-V-15.

d. Start the LC recorder and depress tra AUTO pushoutten.

e. Cepress CLEAR.

LZP-k330-24

' Revision 3 Septemoer lo. 1963 17

f. Wait until the oisplay clock nas timed to 3 minutes, thsn release AUTO, capress cue AR, ano enter "0C".

g. Label the L&N recorder trace with the date.

time, loop number, and attenuation setting.

h. Cep.encing on the traca just recoraec, select a different attenuation to ootain a cetter trace. If the traca is acceptacle, proceec to step F.41.k.

i. Select the next availaole loop and depress the AUTO pushoutton.

j. Repeat steps F.41.d. tnrougn F.*l.r..

K. Stop the LEN recorcer.

42. At tne LSP, OPLO8J, the pressure ino i c ateo on RC-G-2.1 is normally 5 ana 7 psig, record the reacing on LRC Form IC97A ( Attachme nt F).

43. Obtain tne diluted gas sample in accorcance aith the following:

a. Turn RC-CV-2 to tne 6 o' clock positicn. .i a i t until tne pressure on RC-G-2.2 returns tc 1 psig.

o. Turn PC-CV-2 to tne 9 o' clock position. Close RC-V-14.

c. Remove the griptong containing the cilutec gas sample and place cenind snielaing.

44. Flush the syster in accordance with the fc11owing:

a. Verify RC-V-15 is closac. Turn RC-V-11 counterclockwise to the 6 o'clocx positicn.

o. Open RC-V-9. , RC-V-7, anc RC-V-8.1 anc RC-V-4 l

c. Acjust RC-VREL-2 until RC-FI-2 ir.dicates 16-22 incnes of water. clusn witn cemineralized mater for a minimum of one (1) minute.

I , - _ , . , . - _ _ _ , . _ _ _. .. . .--- _ _ - _.

i

. l i

LZP-1330-24 Revision 3 Septe noer lo. 1963 18

d. Open RC-V-8.2.

e. Cl ose RC-V-9 and RC-V-7.

f. Adjust RC-VREL-2 until RC-FI-2 incicates 18-22 incnes of water. Flusn witn cemineralizea water for a minimum of tnree (3) minutes.

g. Cicse RC-V-d.l.

n. Turn RC-V-11 countercicckwise to tre 3 o'clocx position.

i. Cpen RC-V-9.

j. Pull open RC-VREL-2. wnen there is a snarp increase in pressure ir.cicatea on RC-G-3.

release RC-VREL-2. Adjust RC-VREL-2 until RC-G-3 indicates 2C psig. Flush with argon for a minimum of three (3) minutes.

K. Close RC-V-9

1. Cpen RC-V-lC.

m. Turn RC-V-ll counterclocknise to tre 9 3'clocx posi tion and allo RC-EV-1 te vent.

n. C1cse RC-V-lC.

o. Turn RC-V-11 clockwise tc CLCSED.

p. Open RC-V-8 1.

q. Adjust RC-VREL-2 until RC-FI-2 inaicates 18-22 incnes of water. Flush witn water fcr a minimum cf one (1) minute.

r. Terminate flushing oy cicsing tne f olicsing:

1) RC-V-8.2.

2) RC-V-8.l'.

3) RC-V-2.

LZP-1330-24 Revisicn 3 Septe.noer to, 19o3 l)

4) RC-V-4.

s. Close tne riush water valve ano disccnnect the flush water from RC-C-1. ,

t. At the CNP, OPLE4J. depress the SAPP pushoutton, enter coce *23" to evacuate tne enroratogracn until tne reo h! VACUUM light is on, then coce "I'3'" to purge tne l i n.as f rom RC-v-15.

u. Cycle through loops 1, 2, 3, and 4, pausing at each loop for 5 seconds. Repeat fcr a total cf three cycles.

v. Enter coca "14" to terminate tha purge, entor "24" to terminate evacuation.

w. Enter coce "C0".

x. Release tne SAMP oushoutton.

y. If nc further anal yses are requi rec, close valves V-1, V-la, anc V-10, en the CAP,' CPLElJ.

45. Place the REACTOR COOLANT LIOUIC SAMPLE SACKFLUSM s itch in the OFF position. If nc furtter sampling is to os perfcrmeil, closa O'nT-053, T3CCh IN VLv TC HRSS COCLER RACK anc CAT-054, TBCCd RTN VLv FROM PP.55 CCCLER RAC.<, anc verify tne inoications snc.

CLOSEC.

4o. If no furtner sampling is to ca performed place tne UNIT 1(2) PCwER switch in tne OFF position.

47. Following sampling operations during otter tnan a post-accicent conditicn, close or checx closea tne valves cpened in Step :.1.a. cr Step F.1.c.

48. Transport the off-gas sample to tre sample preparation area.

49. Prepare the off-gas sample for analysis in accorcance witn tne f olic ing:

a. wrap the vial in plastic wrap or seal it in a clastic bag.

-. - - + - . - - - , - - - - - -

y y

1

. - - - . - . . . - - l I

i LZP-L330-24 Revision 3 Saptemoer lo, 1963 2C

o. Lacel tne sample in accoraance ni n tne following;

1) System samplad and sample location.

2) Sample time.

3) , Sample cate.

4) Sample volure.

5) Initials.

6) Survey results.

50. Tha sample volume in tne vial is estimatec in accorcance witn the fol l ow i ng:

(V V ) (P + 1*.7)

V = 2 3 2 (V1) (P..

+ 16.7) wHERE: V = Sample volume in ml.

V 7

= System vclume (RC-EV-L anc lines te RC-V-15).

V =V luxa RC-DV-2.

2 V = Total glass vial sclume.

3 P = Pressure reacing from Step F.33.

P = Pressure reacing from Step F.42.

2

51. Analyze the sample in accorcance witn Reference *.

$.7,,g The results will ba in uCi/ml of cff gas not r4 actor water.

52. Determine the reactor cool ant nycrogen concentration of calculating the hycrogen peak height "X" in acccroance witn tne following f ormul a, anc recora the work on LRC FCR.* 13973 (Attachment E):

X = (P) x (A) / (10C)

L2P-1330-24 Revision 3 Septemoer 16, 1983 21

(

WHERE: P = Trace peak height (witn baseline suctractec),

LEN recorder scale units.

A = Attenuation setting.

53. From the plct of hycrogen concentration versus paak height for the attenuation setting usec, reac tne measuraa. hydrogen concentraticn at tne intersection of the curve for tne

• appropriate locp anc tne value of.X determinec in Steo F.52. Record the results on LRC Form IC97B (Attacnmen? E).

54. Report tne sample results to s. Rac/Cnem Director for evaluation.

55. Rcute all output data ano calculations to Rad / Chem Supervision for review.

56. To cispcse of the reactor ccolant off gas sa.nple, proceed in accorcance witn tne folicwing:

a. Verify the following valve lineup:

1) RC-V-1.1 (closed), coorcinata 1-9.

2) RC-V-1 2 (closed), coorcinate J-9.

3) RC-V-1 3 (c10sec), coorcinate A-9.

e) RC-V-1.4 (closec), coorcinata 5-9

5) RC-V-1.5 (closec), coorcinata L-9.

6) RC-V-lO (closed), ccordinate F-2.

7) RC-V-11 (closao), ccordinate C-3.

8) RC-V-12 (closec), coordinate L-1.

9) RC-V-13 (closac), coordinate L-2.

10) RC-V-14,(cicsed), ccorcinate L-2.

11) RC-V-15 (closad), ccordinate A-2.

12) RC-CV-2 (9 c'clocx), coercinate M-3.

c. Install tne cilutac gas sample octtle cn ena frcnt panel neeale.

... l LZP-1330-24 '

Ravision 3 September 16, 1933 22

c. Open RC-V-13.

c. Open RC-V-12 and avacuate until RC-G-2.2 indicates a minimum vacuum of 22 irches mercury.

e. Turn RC-CV-2 to tne 6 c' clock positicn and continue the evacuation until a mininum vacaum

.cf 22 inches of marcury is indicated on RC-G-2.2.

f. Close in orcer RC-V-13 and RC-V-12.

g. Open RC-V-14 and allow the octtle to pressurize to approximately 1 psig as indicatsa on RC-G-2.2.

h. Cicse RC-V-14.

i. Open RC-V-13 and R C -V- 12 a r.d evacuate until RC-G-2.2 indicates a mi nimum vacuun cf 22 incnes mercury.

j. Cicse in arcer RC-V-13 and RC-V-12.

k. Open RC-V-14 and allow the octtle to pressurize to approximately 1 asig as incicatsc on RC-G-2.2.

1. Cicse RC-V-14

m. Repeat Steps c.56.i. tnrcugh F.56 1. tnree tires to remove all racicactive gases.

n. Remove the sample cottle from rne panel.

o. Survey the sample cottle and cispose of as directed oy 2ad/Cnem Supervision.

57. Perform the calibration of the gas enronatograpn in acccrdance witn the fol l ow i ng:

3 15 This procedure serves to cal iorate tne enti re Li quia Sampling Panel (LSP). 0PLOSJ, Cnerical Analysis The Panel (CAP), CPLElJe anc cnromatograph system.

procedure snoulc be run wnenever system vclume nas changed or enromategracn hardware is replaced or moaifiec. This procecara procucas four crarts or

LLP-1330-24 Revision 3 Septemoer lo, 1983 23 nycrogen concentration versus enrcinatcgrapn peak neight, which are usec to estimate nycrcgen concentrations of the reactor coolant samples.

a. Perform tne enromatograph verificaticn procacure,

• Steps F.6.a. througn F.6.n. for CAL 2 gas.

D. Per-form the enromatograph ver i f icaticn procacure, Steps F.6.a. througn F.6.n for CAL 1 gas.

c. Depress the SAMP pusnoutton.

- d. At the LSP, OPLO8J, verify RC-EV-1 is tree at water in accordance with Steps F.d.a. tnrougn F.S.c.

e. In the Dack of the LSP, CPLO6Je renove tne plug from the tee at tne nottcm of RC-EV-1 anc replace it witn a saptum cap.

f. Verify RC-V-9 is closda then fill R C.- S F- 1. 2 with cemineralizac nater in accorcanca with the f olic.ing:

1) Open RC-V-3 1.

2) Open RC-V-8 2.

3) Open RC-V-2.

4) Open RC-V-3.

5) Open RC-V-4.

6) Adjust RC-VREL-2 until RC-FI-2 inoicatas 18-22 inches of .ater. Purge (cr a minimum of tnrse mirutas.

7) Close RC-V-8.1.

8) Close RC-V-8.2.

9) Close RC'-V-4

g. Evacuate RC-EV-1 anJ tne transfer lina to tna CAP in accordance .itn tra folloaing:

LZP'1330-24 Revision 3 Septemoer 16, 19e3 24

1) Open RC-V-15. .

2) Open RC-V-12 and RC-V-10.

3) Evacuate until RC-G-2.1 reacs a minimum of 22 inches Hg.

4) . Close RC-V-10 then close RC-V-12.

n. At the C.*P, OPLE4J, proceed in acccccance witn the folicwing:

1) Enter "23" to initiate evacuation of tne chromatograpn.

2) Verify tnat the red HI VACUUM light is on after a few minutes.

3) Cycle througn loops 1, 2, 3, anc 4 pausing l at each loop for 5 seconos or until the HI VACUUM light is on. Repeat for a total of tnrae cycles.

4) Select l oo p 11.

5) Enter "24" to terminate evacuation.

6) Select attenuation cf 5 (5 x 1).

i. At the LSP, OPLO8Je procaso in accercanca with the follcaing:

1) Verify the vacuum is a minimun cf 22 i r.cne s Hg en gauga RC-G-2.1.

2) Turn RC-V-11 clockwis6 to the 12 o' clock po s i ti on (CLJSED).

3) Inject tne nyarogen gas inte RC-EV-1 v i a the septum.

4) Open RC-V-9 enen wait approxitatel y fi ve (5) seconds.

5) Close RC-V-9.

l i

'^

LLP-1330-24 Revision 3

- Septemoer lo, 1983 25

( ,

6) Open RC-V-16.

7) Snap open RC-V-9 and wait one minute.

8) Cl ose RC-V-16 than close RC-V-9.

9) Turn RC-V-11 counterclocxwise tc tne 9

- o'clocx position.

10) Reccra sna ambient temperature en LRC FORM 1C978 (Attacnmert E).

J.

At the CMo, OPLE4J, prcceed in acccrcance witn the f olicding:

1) Cycle througn loops 1, 2, 3, anc 4, pausing at eacn loop for 5 seconds. Repeat for a tctal of tnree c ycl es.

2) Release the 3 AMP pusnoutton.

3) Start the L&N recorder.

6) Select loop ci anc capress Aui0 pusnoutton.

5) Depress CLEAR.

6) dait until tne di spl ay clocx ras tired -o 3 minutes, rel ease AUTO, cepress CLEAR, ano enter "GGa.

7) Repe3t Steps F.57.J.4) tnrougt 57.J.o) for loops 2, 3, and 4.

8) Stop tne L&h recorder.

9) Recora tne cate, time, cc of rycrogen used, attenuation setting and icop numoers on tne L&N racorder traca.

4. Repeat Steps F.57.c enrough F.57.j using tne allowed attenuation settings ano tre nyarogen volumes assignateJ oy Rad /Cnem Supervision.

1. Perform tne enromatograch verificaticn procecure, steps F.6.a. througn F.o.n. for CAL 2 gas.

Verify :ne results are equivalent to those cotained in step F.57.a.

LZP-133C-2*

' Revision 3 Septeiacer 13, 19o3 26 a

m. Perform tne chromJtograph verificaticn procecure, steps F.6.a tnrougn F.6.n for CAL 1 gas. Verify tne results are equi valent to tncse cotain o in Step F.57.o.

n. For each of the four attenuations (5, 25, 100, 500) cevelop a chart of hycrogen ccncentration (Y).versus. hydrogen peak heignt (X) in accorcance with the following:

1) Calculate X and Y in accordance with the following and recora :ne ork on LRC For.n 10973 (Attacnmert E):

Y = (H) x (273/(273 = T) / (0.030)

X = (P) X (A) / (10C) aHERE: H = Hydrogen volume injectec, cc.

I = Measured amcient temperature, U c.

P = Trace peak neignt (with caseline suotractea), LEN recorder scale units.

1 = Attenuation se tt i n g.

2) Jn each chart. pict uns nigr. anc low concentration data points and ccnnect sacn pair wi th a straignt line, refer to Attachments A, s, C, and C.

G. CHjCKLISTS

1. None.

H. T((HJ g j gC] ] Q ] Q J gER6NCE$

1. None.

- - = -

, - ., +-n -- r . , - - - - - , ,, c-- --

I I

I i

s .

.. _ _ _ _ _ . _ . _ . . ._- )

' ~ ' 1320-24 '

.C"'ACEMENT A lar sion 3 S

2.potamhar

/

1/ . 1o03 i f*m t r'i sticas Per Step F.5.a. .

. i

! LCOP di . ,

, f.

,r * - ,

POINT 1 POINT 2 Cg ,2, e Gas 40 : g ice 0.25 ee ,

_ i -

T 200 c 20*e .

' '^

53.3 scale units 17.7 sesla .m4ts

-  ? , e.

(^-

5 s

A 5 ,

\

- /

35 ' e

) )=7.76 l .

T (1) ('*73 'O*25)((273 27}+20) . , , ,

(273+20)_ 1.0 , ,

l

~

- 0.030 4

. c - -

a

, a.

i

.a - __

• • ~

Poi == 1 i -

a 50

~

- I (53.3)

/ .

o - -,5) s = 2.67 ((17.7) 100) s ,5) = 0.39 u - (LCO) . .

_w -

i  !*

• s

, . , i i

, , e , .

c

, l

, 4

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/

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'3 -

i /.

• 5 x 1 At:anuncien

= ,

f.

, ,o +

1: ,

.,a .,

g . f. .

g ,

. o .

• I

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u -

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. 0.5 1.0 b HTDRCGZ3 ?!aI E'Ji'l" (I) ,

1 '

', Scat 2' 2 AA..:.JJA *CN) -

100 _

l -e= e. .

L*? 1330-24 e

. AT"F*1NT 3 Invision 3 September 16, 1983

. 400 , 28 , ,

i I L i ,

380 .

m ,

e 4

360 .

i , , <

t I , I 4

, s 6

• l l l , , J

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320 , , / , , , ,

i 8

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300 ,

i  ? f I' / 4

) A e' I t i / / e /

• 4 I

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, . 6

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, p /i / / i a  !

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+

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', ,00 .

, a,,/,.

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e

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5 0', ,

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== s s

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i /, / .

y

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a

, ir i J 60 ' ' ' ' dTDRCCIN CCN(.",4:rI2ATICN ,

,,l#

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/ </. ' --i 25 x 1 Al"" TEA 1'ICN -

40 _ _ . ,

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a 75 / 4

~ ,=/

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e k as _U .+ o 4 6 s av. . 12._ .M s -

j

1

__ ..-._ - - -_ . _ _ . l e

, . L:.'? 1330-24 i

.**- - AT*1 N C Revision 3 September 16,1o83-l 1000 i 29

. .,e Loons 3 & 4 ,

1 l

1. i

. / 4

-. 7 Loco 2 < ,

1 1 s. . . s, . . 1 9 . -

m m4 -. _ toop i 6 g

,I ',l l, 4 900 ,

. 1 i . " . . .

i

• P1 l i ,

i

. If= 6

' II l- l

' Mfl F t , I f i

1. s e fe(6  ;

f i f f I .

. h W

. a , I. 4 t

si 800 II i

I' w ,

n i, , , i i If ' fl i ,. i

. 1 I. t

.,, a , 1

. N 'S 5 i I a ,r , s. .

4 , ,

, 1

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1 I

u .D

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2f. 700 .

2. r /s I'* 4

, ~

un . .

• ri r, I q 8e .1 .

e u1 .i. i o

u , , , , , ,

%# a j f.

600 ,

, *Pf I. i  !

4 ii 1- , .

F& A a i, .46 . 5

, 11- F e

. s ,

. , i i i . . , ,

. . . iii , '

// ~ .'

i h 500 . ,,, 1; it. #-

} (( A 0

(

g 1 i i

>> /

ow I

% \

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I w ,

z

.i if r N e 91 i e M . . t . . , i Q . I

, ,t (i

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- u1 8 '

,,, c , .

g 300 , 1. i. .

,

• i

. ..f I f' g --- , . , .

, e i

, s i6 f 6 6 i

g ,,, . . , ,

, s

. 3 ,

E // ! 6 I

. /P , .

,u,. ,

200 :1 , ,

i i F HC RCGIN CC L~".'.iT2A!!CN .

rs. PEAI EI!GHT I 100 100 x 1 ATTIMA !CN i~ '

i l

L .

l . .

-- .- .- ,- . . , ,n m 2n i .e.n - - -_ .

l l

L ? 1330-21 f Ravisics 3 l / ' * . A:*.*.u:: DIE:IT 0 Septemeer 16, to81

.i l

. 30 i

^ - - '

a is Loops 3,& 4 +

.s ,

'000

, / -Loop 2 .

(

1 Loco 1

f. 1 fa 6 e

{ , , , , r s

t I l' u as--

1300 ,

, 1 6

, I I' fQ f

, r , .i . .

,. 1 .,. . .

i '

, 4 i s N l' ,

4 / 4 4 ,

o ,

, s . <. ,

w w 1600' , ,. ,

3 I A i s 6 y I a /

e 6

. i 1.i.

g l e I-Q i 1 I r w 6 1400 ,.

0 ,* I i

(: ! !n

,.i i

,.o . . .

.m ,

, 1200 ,

I- i k

s 6

6

. ,, . j. .

f=

, ,i ,

, t ' '

. I' 't-1 t t

. 4 ,

i.

c 1000l

==. .

, i. , n  !

l a:

s, s.

ma. .

g i1 i. . .

s u ,. , . . . ,

= , . , . . , ,

1 0 , . u. . .

600 , ,,. , ,

g .,

1 i. ,

, i i

~ , , ,

8< ,.

5

, I i i i i

. e e

+

p . >

m

. i1 I'

i. '

100 ,

[

C.. . .

a. .

l  ;

HTDRCGT! CONC' ITRAT*CN ]1 ,

rs. 7EAK HZIG3: -

• 00 4 5 x 100 ATTT.:IUAr*CN 1 y '

t . i l

2 I

t 200 220 20 2:0 20 a0 50 30 --

100 L20. . 14.. 0 L0 :r e,- u 130 n . . . . . . .

6

- -------.---,.n_ -,- ---,. ...,.-,.,,.,.,,__,.me,__-_,., . , , . . , ee,-,.w,,,n--am-me--cw. w-.-

~

C7 1330-24

' ' levision 3 .

September 16, 1983 Ar ic rm,rT g 31 .

f mt Y ? COUNT! STATION

]

• ETDROGEf ANALYSIS AT THE ERSS Ambient Tamperature:

CALI3 RATION Loop #

E Hydrogen Volume Injected, cc T Measured Amblant Tamperature, C 7

Trace Peak Height, units A Attennation Serpoint a x 273/(273+T) / 0.030 Y

O P x A / 100 I

Fal uration Gas #

7erification Ccucentration, cc:

l i ANALYSIS Loop # .

'? Trace Peak Height, units __

A Attanuation Setpoinc ,

P, x A'/ 100,' -

e Z -

M M $

L2C 70RM 10973 es D

t.

_ _ _ - - _ _ - _ . , - ~

L2P l}30-24

+

- ~ -

Revis ithe 3 .

September 16, 1983

{'i *

~~

• 32 i

ATTACIIHEHT F .

1.aSalle County 8tation '

l (

IIRSS Analyses Date t.

Dissolved Omvuen.17P 1130-23 conduct 1'vity.LZP 1330-23 pH. LZP 1310-23 calibration Init/ Times _

Sample Init/ Times. _

Init/ Times Standardization 0 Recirc. Water Temperature, C:

g,,p g ,y,,,,,,g,,,, C:

• Calibration Check Init/ Times Rectre. Water 02Conc..mg/1:

Heasured Conductivity..umho/ca

• Heasured pitz (pil-7) _

Sample init/ Times ,

7.0 Cogrect the measured conductivity to -Sample D.O., og/1 l

Buf fer pil Values 25 C using the following formula Check SAT /UNSAT,10.1 pH unitst l

Init/ Time Sample Sample Temperature, "C:

Cg =C 2 - h.@Q.M x h Of f-fles LZP 1330 1 + 0.018 (Tg - 25 C)

' ' Heasured pil: Vacuum, RC-C-2.1., Step F.32.d o.liere Cg = Cogductivity corrected to Pressure, RC-C-2.1., Step F.38 IftijesamplepHtemperaturegxceeds 25 C Pressure, RC-C-2.1. . Step F. 42 20-30 C . correct the pH to 25 C in

! ccenidance with the following: C2 - Heasured Conductivity C Sample _ Init/ Times ping a pilg + 0.03 (Tg - 25) ,

T3 = Sample Temperature.

Wheres pilg s pit corrected to 25 C .

l Comments:

pHg. measured pH i

C Tg a Sample Temperature.

a i Neviewed:

i _ .

Conductivity at 2500, umho/cen:

ph at 2500: .. . ..

' -- -- t-

-L- --

t **.3 1330-24

~

I Revision 3

, September 16, 1983

~ ' * * -

• ATTACiM G T G 33

- - vat.:tE U STING ,

- AC-V-l.1 Reac.or Recies 1.cos 5 Smole Catsut Yalve 7 AC-V-1.2 AT Camin inlet Smole Cutour Va'Ive AC-V-1.3 AHR I.com A Sapia Catour. Valve AC-V-1.4 AttR 1. cap 5 Sample Catout Valve a

A M -1.5 Af Casin cut!.c famola Cateut 'talve O

I AC-V-1 Smole Source isolation Velve AC-V-3 famole Purge Cutout Valve

.-- AC-V4 Flushing.*Jacer Isolation Valve p AC-y-5.1 Pressartzed Samole irrier isolac!on-Valve

~~'

AC-V-i 2 Pressurl=ad fample Cuties isolatica Valve l *"*;

AC-V-7 01 lured fample Sypass Valve

• AC-V-8.1 AC-5F-l.2 Inlet isolation valve . _. .

AC-V-4.2 AC-5F-l.1 Cutlet IsolatIen Yalve y RC-V-9 AC-ft-1 Isolatica Valve J AC-V-l C AC ~V-1 bacuation Cutout Valve i 1 -~ AC-V-Il Off9as 4=wy Valve AC-V-11 Argcst to Ale Ejecter Out=ut Valve RC-V-13 Cff7as Vial hacuation Catout Valve AC-V-14 Argon fuoply to Cff9as Vial Cat =ut Valve f .

j AC-V-15 Cffwas Smole to Gas Chremotogrion isolatien Valve RC-V-16 AC-5F-l.1 Argon Purge Cateut Valve

- AC-V-17 Reacter Coolant Gesh Smole Cat =ut Valve l" AC-V-13 Asact=r Coolant Undil'uted Samole Backflush Cateut Valve.

RC-V-19 Asact=r Coolant Undllutad Samole injecticn Valve ,

1 AC-C-1 Fi l l Va lve .

! AC-V-10 AC-V -11 AC-I-I l'sof acien Valve

! AC-4-12 1.!cuid $mele :o CAP isolatten valve .

9 ,-

I -

.a c-y -----

- - - e a e.+ g -=w - - - , - - .---,aw ,,_.--.%.-. -my 7

v l

'. ~.? 1330 -2fr

" Revisien 3

. *. s

• September 16, 1983 ATTACmENT G (Cent'd) 34 (Final) i

~

r--

Reactor Coolanc Ollutsd Samole lajection Valve

~

] RC-0V-1

- AC-0V-1 Off gas tample injection Valve J AC-vREl.-t Reactor Coolant Purge Throttle Valve r' RC-VREL.-1 Reactor Coolant Samole Throttle Valve

" Off gas Sample to Gas Chromatograon Cutout Yaive V-1 V-10 instrument Air Cutout Valve a

V-14 Argon Supply Cutout Yalve m -

L,j AC-V-6,1 AC-5F-1.1 Inlet Isolactort Valve

.m AC-V-8.2 AC-5F-l.1 Outlet Isolation Valve

" AC-V-9 AC-EV-1 Isolation Valve p AC-V-10 AC-EV-1 ILvacuation Cutouc Valve

. .)

AC.-V-11 Off gas. Wy Valve t . AC-V-11 Argon to Air Ejector Cutout Valve u

, AC-V-f3 Off gas Vial Ivacuatica Cutout Valve 1  :

J AC-V-15 Cff gas Samole to Gas Chromatogrson isolatica Valve

-T AC-V-16 - AC-SF-1.1 Argon Purge Cut =ut Valve i

" Off-gas Sar:: ale injecclen Valve AC-CV-1 a'

1 t'~

lQ

^

g. -

I i

i L.

9 4..

- - - - , -r,- -,----w.,--. p-,--- , ,~,r-.- , , , - - - - - - ,