ML20039A884

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Public Version of Revised Lzp Procedures Manual,Including Procedures LZP-1210-1 Re Hazardous Matl Incidents Reporting & LZP-1330-11 Re Dilution & Transfer of Gas Samples.Index & Tabs Encl
ML20039A884
Person / Time
Site: LaSalle  Constellation icon.png
Issue date: 11/13/1981
From:
COMMONWEALTH EDISON CO.
To:
Shared Package
ML20039A881 List:
References
PROC-811113-01, NUDOCS 8112210439
Download: ML20039A884 (55)


Text

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8/17/81 LZP INDEX PAGE 1 PROC. NO. TITLE REV. REV OATE DISKETT ZP 100-1 DELETED 03 11/80 01 LP 10J-2 DELETED 04 11/80 01 LZP 100-3 DELETED 03 10/80 01 ZP 200-1 DELETED 02 11/80 01 LZP 200-2 DELETED 02 11/80 01 ZP 200-3 DELETED 02 11/80 01 ZP 200-4 DELETED 03 11/80 01 LZP 210-1 DELETED 02 10/80 01 ZP 300-1 DELETEU 04 8/80 01 , LZP 300-2 DELETED 03 11/80 01  ; ZP 310-1 DELETED 03 11/80 01 LZP 320-1 DELETED 02 10/80 01 l ZP 330-1 OELETED 01 10/80 01 ZP 340-1 DELETED 01 10/80 01 ' LZP 350-1 DELETED 02 10/80 01 ZP 360-1 DELETE 0 02 10/80 01 LZP 370-1 DELETED 01 10/80 01 ZP 400-1 DELETED 02 11/80 01  ! ZP *00-2 DELETED 02 10/80 01 ZP 400-3 DELETED 01 11/80 01 LZP 410-1 DELETED 01 11/80 01 LZP 420-1 DELETED 01 11/oD 01 LLP 510-1 DELETED 02 10/80 01 LIP 520-1 DELETED C2 10/80 01 LZP 520-2 DELETED C1 10/80 01 LZP 52C-3 DELETED 01 10/80 01 LZP 530-1 DELETED 01 10/80 01

8/17/81 LZP INDEX PAGE 1 EPRUC. NO. TITLE REV. REV DATE CISKETT

      --------------_ ___    ------------ _=----           ------------------ --- --- ----------- I LZP            530-2  DELETED                                                    02           10/80    01 LZP            590-1  DELETED                                                    01           10/80    01 LZP            700-2  DELETED                                                     01          11/80    01 ZP          710-1  DELETED                                                    02           10/80    01 LZP            810-1  DELETED                                                    C1           10/80    02  )

uzP 820-1 DELETED OL 10/80 02 LZP 830-1 DELETED 01 10/80 02 l LZP 8>0-1 DELETED 01 10/80 02 860-1 DELETED 01 10/60 02 E_ZP LLP deo-1 DELETED 01 11/80 C2 1110-1 STATION DIRECTOR (ACTIN'G STATION 03 d/81 02 ELZP DIRECTOR) IMPLEMENTING PROCEDURE 1120-1 OPERATIONS DIRECTOR IMPLEMENTING 02 4/81 02 t' ZP DIRECTOR l LZP 1130-1 TECHNICAL DIRECTOR IMPLEMENTING PROC. 03 */81 02

       ._ Z P        1140-1 MAINTENANCE DIRECTOR IMPLEMENTING                          01           11/8C    02 PROCEDURE uZP           1L50-1 STORES DIRECTOR IMPLEPENTING PROCED'JRE                    01           11/80    02 LLP           1160-1 ADMINISTRATIVE DIRECTOR IMPLEMENTING                       01           11/80    02 PROCEDURE LLP           1170-1 SECURITY DIRECTOR IMPLEMENTING                              02           4/81    02 PROCEDURE LLP           1180-1 RAD / CHEM DIRECTOR IMPLEMEATING                           03            7/81    02 PROCEDURE LZP           1180-2 RAD / CHEM DIRECTOR INITIATED                               01          11/80    02 ENVIRONMENTAL MONITORING ACTIVITIES ZP         1200-1 CLASSIFICATIONS OF GSEP CONDITIONS                          01           7/81    01 1

1200-2 CLASSIFICATION OF A NOBLE GAS RELEASE 00 10/80 02 E'.ZP u2P 1200-3 CLASSIFICATION OF AN ICDINE RELEASE 00 10/80 01 l LLP 1200-4 CLASSIFICATION OF A LIJUID RELEASE 00 7/81 01 LLP 121C-1 HAZARDOUS MATERIAL INCIDENTS REPORTIilG 01 10/8/ 01 1

(. 8/17/81 LZP INDEX PAGE 3 ( "" " "":

                    ""                                                                                     ""- ""    ^   'S**"
 'ZP  1220-1        EMERGENCY TELEPHONE NUMBER                                                                01     5/81      01 ZP 1220-4       DELETED                                                                                    01     7/81      01

<ZP 1310-1 NOTIFICATIONS 00 10/80 02 LP 1320-1 AUGMENTATION OF PLANT STAFFING 02 o/81 02 ZP 1330-1 POST-ACCIDENT SAMPLING OF REACTOR 01 11/80 02 COOLANT p2P 1330-2 POST-ACCIDENT SAMPLING OF THE PRIMARY 01 3/81 03 L CONTAINMENT ATMOSPHERE FOR RADIGIDINES DETERMINATION AND PARTICULATES ALTERNATE MEANS ZP 1330-3 POST-ACCIDENT SAMPLING OF PRIMARY 02 3/81 03 CONTAINMENT ATMOSPHERE _ZP 1330-4 POST-ACCIDENT SAMPLING OF THE PLANT 01 11/80 03 VENT FOR RADIGIDINES AND PARTICULATES h2P 1330-5 POST-ACCIDENT NOSLE GAS RELEASE RATE DETERMINATION 00 11/80 03 ZP 1330-6 DELETED 01 7/81 03 1330-7 POST-ACCIDENT SAMPLING OF THE STANDBY 01 11/80 02 hlP GAS TREATHENTL (SBGT) SYSTEM EFFLUENT p2P 1330-8 SAMPLING LIQUID PROCESS MONITORS 00 d/81 03 L DURING LIQUID MONITOR HIGH RA01ATION ALARM CONDITIONS ZP 1330-10 DEPLOYMENT OF THE EBERLINE SAM-2 CO 11/80 03 STABILIZED ASSAY METER P 1330-11 DILUTION AND TRANSFER OF CAS SAMPLES 00 11/81 ZP 1330-20 POST-ACCIDENT ANALYSIS OF SARON 00 3/81 03 (BACKUP PROCEDURE) ZP 1330-21 DETEP'fINATION OF REACTOR COOLANT CHLORIDE CONCEN 01 10/81 03 TRATION AT THE HICH RADIATION SAMPLING SYSTDi ZP 1330-22 CALIBRATION OF THE MODEL 10 OIONEX 0l 10/81 03 ION CHROMATOGRAPH LP 1330-23 DETERMINATION OF REALTOR COOLANT PH, 00 10/83 03 CONDUCTIVITY AND DISSOLVED OXYGEN CONCENTRATION AT THE HIGH RA01ATION SAMPLE SYSTEM I

(8/17/81 LZP INDEX PAGE 4 PROC. No. TITLE REV. REV OATE DISKETT: ZP 1330-24 DETERMINATION OF REACTOR COOLANT 00 to/8l 03 HYOROGEN CONCENTRATION AT THE HIGH RADIATION SAMPLING SYSTEM ZP 1330-25 SAMPLING OF REACTOR C00IJLNT AT THE HIGH 00 go/Bl 03 RADIATION SAMPLE SYSTDI ZP 1330-26 SAMPLING OF CONTAINMENT AIR AT THE HIGH 00 to/Bl 03 RADIATION SAMPLING SYSTEM ZP 1330-27 5AMPLING JF REACTOR COOLANT OFF-GAS AT 00 10/8( 03 THE HIGH RAOIATION SAMPLE SYSTEM

  .ZP   133U-28                                                    SAMPLING OF PROCESS WATERS CONTATNINr. R.AnIn-                         00      a0/g j    03 ACTIVITY AT THE HIGH RADIATION SAMPLING SYSTDi ZP  1330-29                                                  SAMPLING AT THE HIGH RADIATION                                           CO       0/00     03 SAMPLING SYSTEM (VALVE OPERATION AT THE VALVE CONTROL PANEL)                                                                       l l

LLP 1330-30 TRANSFER OF WASTE FROM THE HRSS WASTE 00 0/00 03 ] TANK AND WASTE PUMP l

   ,ZP  1330-50                                                  RADIATION SURVEYS UNDER ACCIDENT CONDITIONS                               00     10/31
ZP 1390-1 IMPLEMENTING PROCEDURE FOR FIRE: 01 9/d/ 02 f j

FIRE MARSHALL j

  'ZP   1340-2                                                   IMPLEMENTING PROCE0'JRE FOR FIRE:                                        01        9/6/    02 FIRE CHIEF (OESIGNATED SHIFT FOREMAN)

LP 1390-3 IMPLEMENTING PROCEDURE FOR FIkE: 01 9/6/ 02 FIRE OFFICER OL (COGNIZANT MAINTENANCE FOREMAN) l ZP 1340-4 IMPLEMENTING PROCEDURE FOR FIRE: 0t 4/8/ 02 FIRE BRIGADE

  .ZP   1340-5                                                    IMPLEMENTING PROCEDURE FOR FIRE:                                        01       8/81     02 FIRE COMPANY NO. 1 (MAINTENANCE PERSONNEL)

ZP 1360-1 PRUTECTIVE MEASURES FOR ON-SITE C3 7/81 02 PERSONNEL ZP 1360-2 USE OF POTASSIUM IODIDE (KI) AS A 00 7/81 03 THYROID BLOCKING AGENT LZP 1360-4 SEE BELOW ZP 1370 ' RESCUE 00 10/80 02 LLP 1370-2 PERSONNEL INJURIES 01 11/80 02 LP 1370-3 FIRST AID, DECONTAMINATION ANC 00 10/80 02 EVACUATION CF EXPOSED AN0/OR CONTAMINATED CASUALTIES 'LZP 1380-1 CONTROL OF OIL SPILLS CO 10/80 02 LZP 1360-4 RADIATION PROTECTION PRACTICES DURING ACCIDENT CONDITIONS 00

8/17/81 LZP INDEX PAGE 6 PROC. NO. TITLE REV. REV DATE CISKETT ZP 1420-1 ROLE AND STAFFING OF THE ON-SITE TSC 01 11/80 02 ZP 1430-1 ROLE AND STAFFING OF TnE ON-SITE OSC 02 */81 02 LLP 1440-1 ON-SITE GSEP COMMUNICATIONS SYSTEMS 01 6/81 02 ZP 1950-1 DELETE 0 01 7/81 02 LLP 1950-2 DELETED OL 7/81 01 ZP 1510-1 GSEP OPERATIONAL READINESS CO 10/80 01 ZP 1520-L TRAINING REQUIREMENTS CO 10/60 02 29 1530-1 EXERCISES AND DRILLS 01 8/f f s 02 LP 1550-1 FIRST AID FACILITIES MONTHLY 01 7/81 02 j SURVEILLANCE ZP L550-2 ENVIRONS SAMPLING SUPPLIES INVENTORY 02 7/81 01 ZP 1550-3 DECONTAMINATION FACILITIES MONTHLY 01 5/81 02 SURVEILLANCE ZP L550-4 ST. MARY'S HOSPITAL HEALTH PHYSICS 01 7/81 02 SUPPLIES LUARTERLY SURVEILLANCE ZP 1550-5 TECHNICAL SUPPORT CENTER MONTHLY 01 7/81 C1 j SURVEILLANCE hlP 5 1550-6 OPERATIONAL SUPPORT CENTER MONTHLY SURVEILLANCE 01 7/81 01 L550-7 EMERGENCY OPERATIONS FACILITY OL 3/81 01 tZP MONTHLY SURVEILLANCE LLP 1550-8 NUCLEAR ACCIDENT REPORTING SYSTEM 02 7/81 02 (NARS) MONTHLY SURVEILLANCE LZP 1550-9 SPECIAL TLD QUARTERLY SURVEILLANCE 02 11/81 03 LZP L550-10 ENVIRONMENTAL SURVEILLANCE STATIONS CO 7/81 02 LLP 1610-1 RECOVERY AND RE-ENTRY PLANS CO 10/80 01 LZo 1700-1 GSEP STATION GROUP DIRECTORY 03 7/8L 01 l LLP 1700-2 STATION EMPLOYEE LIST 01 7/81 01 LLP L700-3 STATION PHUNE LIST 01 5/8L 03 l l _- -

l LZP-1210-1 Revision 1 Octooer 13, 198L f , 1 l HAZARDOUS MATERIAL INCIDENTS REPORTING A. PURPOSE The purpose of this procedure is to implement the reporting requirements of the State of Illinois Puolic Act 79-1442 (Reference 1). B. REFERENCES

1. State of Illinois Public Act 79-1442, " Hazardous Mater i al s -Regul at ion."
2. Generating Stations Emergency Plan (GSEP).
3. LZP 1220-1, " Emergency Telephone Numoer."
4. LZP 1310-1, " Notifications."
5. LZP 1370-2, " Personal Injuries."
6. General Company Order No. 19, Appendix A, " Chart  !

for Reporting Major Trouole."

7. T i tl e 10, Code of Feceral Regulations, Part 20.
8. Technical Specifications, Section 6.
9. Title 40, Code of Federal Regulations, Part 116.
10. Title 40, Code of Federal Regulations, Part 118.

C. PREREQUISITES

1. A reportable incident for hazardous materials (Reference 9 and 10) for tne purpose of con.piienov with Reference 1 is defined as one i nvol v i ng haz ar dous materials (poisons, explosives, compressed gases, or oxidizing, combustiole, flammable, irritating or corrosive materials) in which:
a. A person is killed or hospitalized, or
b. Property damage exceeas $50,000, or
c. A situation exists of sucn a nature that there is concern that C.I.a or C.l.a. may develop.

l l

LZP-1210-1 Revision 1 Octooer 13, 1981 2

2. A reportable incident for radioactive materials is one in which there is:
a. Any release exceeding technical specification limits, or
b. Any fire, breakage, spillage, or release from I materials which are in transit away from nuclear station sites, or C. Any exposure or contamination of a person at a level whicn exceeds 10CFR20 limits, or
d. A situation of such a nature that there is reasonable concern that C.2.a or C.2.0 or C.2.c may develop.

O. PRECAUTIONS

1. NONE.

E. LIMITATIOM_AND ACTIONS

1. In aGdition to requirements for reporting specified E in this procedure, reports shall also be made in accordance with References 2, 6, 7, and 8.

F. PROCFPURE

1. For reportable incidents for hazardous materials as defined in C.1:
a. The person discovering the hazardous material incident should call extension 211 anc report the incident.
o. Upon notification of a hazardnus material incident, the Shift Engineer or his cesignee will take tne actions specified in Appendix A l to General Company Order No. 19, " Chart for Reporting Major Trouble," (Attachment B).
c. Promptly notify Environmental Affairs of the incident. Environmental Affairs is responsible l for prompt notification by telephone to the i State of Illinois Emergency Services and Disaster Agency.

l 1 ._ _

E lg~ LZP-1210-1 l Revision 1 5 October 13, 1981 3

d. Notify the nearest emergency agency such as the Police or Fire Department. For incicents occurring at the LSCS site, notify the LaSalle l County Sheriff.
2. For reportaole incidents for radioactive materials  !

as defined in C.2, notifications shall ne made in E accordance with the GSEP (Reference 2) which results in notification of tne Emergency Service and Disaster Agency and the nearest Emergency Agency. For E incidents occuring at the LSCS site, notify the LaSalle County Sheriff.

3. Reports made in accordance with Step F.1 and Step F.2 above, shall incluae information on Attachment A. Followup reporting shall be done witnin 15 days to the Emergency Services and Disaster Agency in writing on forms provided oy that agency. ,
4. Forward the completed Hazardous Material incident Report (Attachment A) to the Administrative and Support Services Assistant Superintendent for review.

After the review, the form will De retained in the E Station Central File. G. CHECKLISTS

1. NONE.

H. TECHNICAL SPECIFICATION REFERENCES

1. Section 6.

E E I E E E

  • LZP-1210-1 ATTACHMENT A Revision 1 October 13, 1981 EMERGENCY INCIDENT DATA SEEET 4 g

DATE: .,- Time of Incident: Form Completed ty: Form Reviewed By: ACCDENT AND/OR INJURY FIRE

1. Nature of incident: 1. Location of Fire:
2. Number of injured: 2. Seriousness of Fire:

i 3. Probability of contamination: 3. Type of Fire (electrical, chemical, j 4. Location: etc.):

5. Can injured be moved? 4. Occupied areas in i=mediat.e jeopardy:
6. Damage to essential plant equipment:

NSO ACTION: NSO ACTION:

1. Not ify Shif t Engineer (X-202). 1. Notify Shift Engineer (X-202).
2. If Shif t Engineer or Shif t Foremen is not 2. Eclay infor=ation over public address immediat:17 available: system advising areas to be evacuated ,
a. Notify ambulance service (815-357-6442 ) 3. Intermittently sound the siren.
b. Notify Hospital (315-673-2311)
c. Notify Rad / Chem (X-241) .

l I CREMICAL /0iL SPILLS HIGH RADIATION OR CONTAMDIATION LEVELS

1. Type of Spill (acid, resin, oil, etc.)* 1. Location:
2. Radiation Level (if known):
2. Quantity of spill:
3. Location of spill and other affected 3. Number of personnel potencia11y tr-areas: radiated or contaminated:
,                 NSO ACTION:                                                                  NSO ACTICN:

15 1. Notify Shif t Engineer (X-202) . 1. Notify Shift Engineer (X-202).

2. Relay information over the public address 2. Relay information over public address 4 system advising areas to be evacuated. system advising areas to be evacuated j 3. Ascertain that Rad / Chem (X-241) has been 3. Accertain that Rad / Chem (X-241) has 3 notified if spill is potentially been notified of the nature of..the
 )

contaminated. incident. I FLOODING SECURITY INCIDCIT

1. Location: 1. Description of incident:
 '                2. Seriousness of flooding:

I E 2. Location:

3. Occupied areas in jeopardy:

NSO ACTION: l 4. Vital equipment in jeopardy:

1. Notify Security Shift Supervisor i (X-21S).
                                                                                                   *      *         *  "E       **#
  • NSO ACTION:
1. Notify Shift En;ineer (X-202).
2. Relay information over public address system advising areas to be evacuated.
              .,-.                                                 ..- - . = . . . . _ .                                                                          _ _ , ,                     ,.                                        , _

LZP-1210-1

               - ~ - -                                                                    _.
            ~

ATTACHMENT B gctober 13, 1981

                                                                                                                                                                                                                                                                                          ;           (Final)

CHART FOR REPORTING MAJOR TROUBLE

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Es \ LLP-1330-11 E Revision 0 ' Novemoer 3, 1981 1 OILUTION AND TRANSFER OF GAS SAMPLES A. PURPOSE The purpose of this procedure is to <1elineate a metnod E of diluting gas samples in preoaration for isotopic anal yses durino normal and post-accioent conditions. B. R E F E R t NC E _S_

1. Commonweal th Edison Company Radiation Protection Standards.
2. " Mixed Gamma Emitting Gas Standard", Analytics, Inc.
3. LCP 410-1, " Preparation of Samples for Gamma Ray Spectrometer Measurements."
4. Hewlett Packard Calculator Program.

C. PRFREQUISITES

1. equipment:
a. Gas tignt syringe, size as required.
o. 15 cc glass vial with septum.
c. Radiation stickers.
d. Labels.
e. Survey meter, C.P. or equivalent.

D. PRECAtiTIONS j 1. A Regulatory Guide 1.3 or 1.4 release of fission i products implies extremely nign levels of ! radioactivity. Dose rates may be nign enough to prevent edtry into many areas of ti , plant enat are normally habitaole. Rad /Cnem Supervision should oe contacted prior to entry into any area wnen such a release of fission products is suspected.

2. wear radiation dosimetry as recommended Dy Rad /Cnem Supervision.

L e { LZP-1330-11 Revision 0 Novemoer 3, 1981 ( 2

3. Wear protective clothing and respiratory protection as recommended oy Rad / Chem Supervision.
4. Appropriate survey instrumants should oe availaole

{ for monitoring during tnis procedure.

5. Gas transfers should be performed in an operating fume hood.

{

6. If the sample exceeds 2.5 mr/hr at contact, the samale snould oe kept in a cave or snielded area

( except anen it is necessary to handl e the semple directly.

7. If the sample exceeds 50 mr/hr at contact, it is

( recommended that the dilution De performed witn r.hielding present. Keep non-essential personnel away from sample. E. LIMITATIONS AND ACTIONS This procedure, thougn intended for use under post-( l. accident conditions, can be used for diluting gas samples during normal operations during wnicn the precautions listed may have limited applications. F. PROCEDURE l ( l. Llean the immediate work area.

2. Determine the volume of gas which must ce taken from the gas sample vial for dilution and radionuclide

( measurement. Unless directed otnerwise oy Cnemistry Supervision, add 2 mi to tnis volume to obtain tne volume of air to be removed from the transter vial. ( 2911 It is recommended that tnis procedure ce practiced (- several times on clean vials first to familiarize the anal yst with tne tecnniques. f 3. Remove the volume of air determined in Step F.2 trom the transfer vial, creating a slightly negative atmospnere in this vial.

4. Insert the syr inge needl e into tne noble gas sample vial towards tne cotto.n of tne vial.

( 1

                                                                                      )

1

   /

LZP-1330-11 Revision 0 Novemoer 3, 1981 3 $W CAUTICN 1 Refer to the precautions in Section D.

5. Pull the plunger baCK about nalf way, then disCnarge back into the vial. Tnis will remove the small quantity of air in tne needl e.
6. Pull the plunger bacx sl owl y to the mark at the volume of gas to De transferred for ailution and racionuclide measurement.
7. wait approx i matel y 30 seconds to allow the pressures to stabilize.
a. Carefully remove tne syringe needle from tne vial, taking care not to pull the septum off the vial.
9. Place the syringe neeole into the clean, partially '

evacuatea transfer vial towards the Dottom of tne vial.

10. Push tne plunger slowly to zero, then pull it oack about halfway and push it Dack again to zero to ensure all tne sample is flushed into the vial anc mixec.
11. Slowly withdraw the needle from the vial, taking care not to pull the septum off the vial.
12. Insert an open syringe neeole into tne sample transfer E vial for 2 to 3 seconas to briefly equalize pressure insiae the vial.
13. Calcul ate the actual volare of gas transferrea in accordance witn LRC Form 1101 (Attacnment A). Recora this volume on the ciluted sample viel label.

CL0. ,T,,g The syringe volume is not tne actual volume transferrea E because the volume in the original container expanos to a volume equal to tne container volume plus tne syringe volume. Refcr to the example calculations on Attachment d. 1*. Survey the ciluteo sampla vial at contact and recora the reading on the vial laoel.

LZP-1330-11 . Revision 0 Novemoer 3, 1981

15. Attach a radiation sticker to the diluted sample vial.
16. Prepare the sample for racionuclice measurement in accordance witn Reference 3.

G. CHECKLISTS

1. None.

H. TECHNICAL SPECIFICATION REFQ g Q S [ 1. None. [ [ [ [ [ [ [ r s r I s L

ATTACHMENT A LZP-1330-11

                .-                                             CALCULATION OF GAS SAMPLE                                      Revision 0 TRANSFERS AND DlLUTIONS                                        November 3, 1981 5

Sample Sample Time Sample Date Calculated By 4

                                        =

f 3 ky V 1

;                                     1                              i o

, 31+V o / l

                                        *(                   ml)            (         ml) i

( ml) + ( ml)

                                        =
                                                                                                                                            \

ml (record on sample label) _ _ _ . ~ _ . - _ _ - _. . . . . . ~ . . . . . . . . _ _ _ . - . II. Calculate the second volume of gas transferred from the same vial as above in accordance with the following:

                          .w _

V 2

                                        "              S 2                \(V-V) g j 32*      o           /

E = ( ml) ( ml- ml) ( )ml)+( ml)

                                         =
                                         =                            ml_(record on sample label) lil. Calculate the third volume of gas transferred from the same vial as above in accordance with the following:

V 3

                                        "       f        8 3       \(V o -V       I
                                                                                    -V)  2
                              ---                    3*         o)                               ~

ml- ml- ml)

                                               =               (              ml)              (

( ml)+( ml)

                                               =

l = ml (record on sample label) Reviewed

              -_LRC Form 1101                   _                       _ _

LZP-1330-11 7 - Revision 0 [- ATTACHMENT B November 3, 1981-6 EXAMPLE CALCULAT_ IONS OF GAS SAMPLE TRANSFERS AND DILUTIONS

     ~

[ 1. Calculate the first actual volume of gas transferred in accordance with the following: , _ _ V =( 8 1 1 3(V)o r ( S 1+v o

                       = Actual vo)lume of original vial.

[ Where V g V j

                       =   First volume of original gas actually transferred.

S = First syringe-measured volume. ( j Example: Analyst takes 14.9 mi vial and removes 2.0 ml as measured by syringe. Calculate the actual volume of original gas removed, Vj . V = 2.0 ml (14.9 ml) 2.0 mi + 14.9 ml

                       =   1.76 ml (record this Jample volume on label)
2. Csiculate the second actual volume of gas transferred from the same

( vial in accordance with the following: r V 2 S (vo ~ v ) 1 S2*vo Where V = Actual volume of original vial. V j = First volume of original gas transferred. V 2

                       =   Second volume of original gas transferred.

5 2

                       =   Second syringe-measured volume.

I

Example: Analyst takes the same 14.'9 mi vial and removes by a second 2. O mi volume as measured by a syring. Calculate the L actual volume of original gas removed in this second transfer, V
  • 2_ _

V = 2.0 ml .(14.9 al - 1.76 pl) 2 2.0 mi + 19 9 ml

                       =    1.56 ml (record this sample volume on label) s f

\ ____ ______ _____-__ ._ . - - _

LZP-1330-11 Revision 0 F November 3, 1981 < ATTACHMENT B (Cont'd) 7 (Final) EXAMPLE CALCULATIONS OF GAS SAMPLE ( TRANSFERS AND DILUTIONS

3. Calculate the third actcal volume of gas transferred from the same vial in accordance with the following:

V = 3 S 3 (Vg - V) -V) 2 5 3*V o Where V g = Actual volume of original vial. L V j

                                                       =         First volume of original gas transferred.

V 2

                                                       =

Second volume of original gas transferred. V 3

                                                       =

Third volume of original gas transferred. S = Third syringe- measured volume. 3 Example: Analyst takes the same 14.9 mi vial and removes a p third 2.0 mi volume as measured with the syringe. L Calculate the actual volume of original gas removed in this third transfer, V . 3 r L v = 2.0 ml (14.9 ml - 1.76 ml - 1.56 ml) 3 2.0 ml + 14.9 mi r L = 1 2/ ml (record this sample volume on label) NOTE When performing multiple transfers from the same vial, equal volumes of gas do not contain equal volumes of activity in the syringe. L L r i 9 I

LAP-620-6 . s . - Asvision 3

                                                                                                     -     -                                               .0ctober 23,'1979 5

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LZP-1330-23 ' Revision 0 October 19, 1981 1 DETERMINATION OF REACTOR COOLANT pH, CONOUCTIVITY AND DISSOLVED OXYGEN CONCENTRATION AT THE HIGH RADIATION SAMPLING SYSTEM A. PURPOSE Tne purpose of this procedure is to delineate the steps required to determine reactor coolant pH, conductivity, and dissolved oxygen concentration at the High Radiation Sampling System (HRSS) during normal and post-accident operating conditions. B. REFERENigS

1. Sentry Equipment Corporation, Post-Accident Sample System, Volume 1.
2. Standard Methods for tne Examination of water and wastewater, 14th Edition, 1975, pp. 446-447.
3. LZP 1330-29, " Sampling at the High Radiation Sampling System (valve Operation at the HRSS Valve Control Panel)."

C. PREREQUISITES

1. Verify that nitrogen, approximately 60 psig, is available at the Chemical Analysis Panel (CAP),

OPLELJ.

2. The operator should De familiar with the operation of the HRSS canels.
3. Establish communications with the Unit Nucl ea r Station Operator (NSO).
4. The sample must nave Deen obtained in accordance with Reference 3 prior to performing tnis procedure.
5. Ensure the buffer solution tanks are approximately nalf-full of i required Duffers.
6. Verify the oxygen calioration tank is filled witn demineralized water.

(

l. .

LZP-1330-23 l Revision 0 October 19, 1981 (. 2

7. Reagents:
a. Air Saturated demi neral i zed watur.
b. Buffer, pH 4.

{

c. Buffer, pH 7.

f D. PRECAUTIONS 1

1. A Regulatory Guide 1.3 or 1.4 release of fission '

products implies extremely high levels of ( radioactivity. Oose rates may be high enougn to prevent entry into many areas of the plant tnat are normall y habitable. Rad /Cnem Supervision should be [ contacted prior to entry into any area wnen such a release of fission products is suspected. ( 2. Wear radiation dosimetry as recommended oy Rad /Cnem Supervision.

3. wear protective clothing and respi ratory protection

[ as recommended by Rad /Cnem Supervision.

       *. Appropriate survey instruments snould oe availaole

( for monitoring during this procedure. E. LIMITATIONS AND ACTIONS

1. Notify Rad / Chem Supervision if any proolems are encountered at tne HRSS panels.

( 2. This procedure, though intended for use under post-accident conditions, can be used for sampling at the HRSS panels during normal operations, during which the precautions may nave limited applications. ( However, normal routine sampling precautions should oe observed. ( 3. Calibration operations must be performed prior to flowing reactor coolant to tne CAP, OPLElJ.

4. When operating at a nigh oxygen level, the Rexnord

( analyzer will achieve an equilibrium value in approx i matel y fifteen (15) minutes. After calioration r of the prone in a dissolved oxygen concentration of [ approximately 8 ppm, the probe will take approximately two hours to recover to oxygen levels in tne low r PP '8"9** i k

LZP-1330-23 Revision 0 Sk Octooer 19, 1981 3 p 5. when filling the aissolved oxygen recirculation b' [ tank, maintain a distance of three inches oetween the final water l evel and the recirculation spray n , nozzle.

6. A recirculation time of one hour is required to achieve complete air saturation of tne recirculation tank water.
7. pH readings are to be taken only after termination of flow and stabilization of the meter readout.
8. The oxygen analyzers should be calibrated weekly ..

when in use and when the analyzer is suspected to be out of calioration.

9. The pH instrument should De standardized at least once per day when in use, and when the instrument is suspected to De out of calloration.

(

10. The conductivity instrument should be calibrated at

[ least once per quarter and when the instrument is L suspected to be out of calioration.

11. If the Rexnord anal yzer nas been in a shutdown condition for a perioc longer than two (2) weeks, the probe should be conditioned oy flowing demineralized water througn the fl ow assemoly for a minimum of thirty (30) minutes prior to calioration.
12. The pH and conductivity monitors and dissolved oxygen analyzer must be energized for a period of 30 minutes prior to calibration or analyses being performed.

F. PROCEDURE

N,0,T_,E, For noun names associated with the valves operated in this procedure, refer to Attachment C.

1. At the Chemical Monitoring Panel (CMP), OPLE4J, verify the INJECT / LOAD switen for tne Ion Chromatograpn is in the LOAD position to permit final system flushing.

i l 2. At the Liquid Sampling Panel (LSP), OPLO8J, verify tne following valve lineup: 4

LZP-1330-23 Revision 0 E October 19, 1981 4 1

a. RC-V-1.1 (closed).
o. RC-V-1.2 (closed).
c. RC-V-1.3 (closed).
c. RC-V-1.4 (closed).
e. RC-V-1.5 (closed).
f. Verify RC-V-* is closed. Connect tne flush water nose to RC-O-1 and open tne fl ush water line valve.
g. RC-V-5.1 (closed).
h. RC-V-5.2 (closeo).
i. RC-V-2 (closed).
j. RC-VREL-1 (closed).
k. RC-V-16 (closed).
1. RC-V-S.1 (closeo).
m. RC-V-8.2 (closec).
n. RC-DV-1 (BYPASS).
o. RC-VREL-2 (closed).
p. RC-V-9 (CLOSED).
q. RC -V-20 (closed).
r. RC-V-21 (closed).
s. RC-V-ll (CLOSED).
t. RC-V-18 (6 o' clock). 1
u. RC-V-19 (BYPASS). l
v. RC-V-22 (TO CHEM PANEL).

II II

i LZP-1330-23 Revision 0 1

.E                                                      October 19, 1981 5

i

w. RC-V-17 (closed).

i x. RC-V-7 (open). I ! y. RC-V-3 (open). I j 3. At the CAP, OPLElJ, verify the following valve j lineup: i I a. V-10 (open). ill

o. V-ll (open).

l c. V-12 (open). { d. V-8 (open). ! i i e. V-2 (open). l

f. V-27 (vent).

] j j g. V-28 (vent). I 1 n. v-29 (vent). lII

i. V-16 (closea).

i

j. V-26 (closed).

1 i k. V-5 (CLOSED).

1. V-9 (closed).
m. V-17 (closed).

i i n. V-24 (closed). i l o. V-6 (0XYGEN CALIB SOLUTION). i i

p. V-30 (TO CAL-1, (pH-4 Duffer tank)).

l 4. For post-accident sampl i ng, align valve V-7 on tne

CAP, OPLElJ, to the YSI OXYGEN ANALYZER posi tion.

l .cor normal sampling, align valve V-7 to the RExNORD 0xYGEN ANALYZER posi tion. 1

5. Start-up tne pH meter at the Chemical Monitoring Panel (CMP), OPLE4J. in accordance with the following:

,Il

I h LZ'P-1330-23 Revision 0 October 19, 1981 6

a. Place the internal S-1 toggle switcn to tne ON position.

j o. Switch S-3 to tne OFF position.

c. Adjust R-3 standardize control for full downward and upward deflection and then reset to a reading of 7.0.

2

d. Switch S-3 to the ON position.
6. Start-up the concuctivity monitor at the CMP, OPLE4J, in accordance with tne following:

1

a. 00 serve that the meter reading is on zero wnen j the selector switch is on ZERO. If so, proceed to step F.6.c. If this is not the case,
disconnect the power Caole and rechecx the j mechanical zero witn power off. If necessary, j use a small screwdriver to adjust tne meter's 4 mechanical zero through the center hole in front of the panel .

D. Reconnect the power cable and ooserve the mechanical zero. Tne meter snould point to zero. If the pointer is not on zero, carefully ] adjust internal trimmer R36 to bring the pointer to zero.

c. Turn the selector switch to CHECK. The meter
;              indicator should move to CHECK on tne meter i

scale. If the meter does not CHECK properly, it is out of calibration, inform Rad / Chem i Supervision.

c. Switch the selector switcn to MEASURE. Tne monitor is now ready for operation.
7. For post-accident sampling, start-up the YSI dissolved oxygen analyzer in accordance with Step F.d. For sampling during normal operations, start-up the Rexnord dissolved oxygen analyzer at the CMP, OPLE4J, in accordance with the following:
a. Check that the power switch is in the OFF position.
                                                                  /

LZP-1330-23 Revision 0 Octooer 19, 1981 7 D. Use a small screwdriver to adjust the mechanical zero through the Olack screw on the meter face.

   '    c. Place the power switcn in the ON position.
d. Turn the function select switch to the ZERO position.
e. Use a small screwdriver to turn the ZERO ADJ for a zero reading on the instrument.
f. Turn the FUNCTION switch to the "20 mg/I" position.
8. For post-accident sampling, start-up tne YSI dissolvec oxygen analyzer at tne CMP, OPLE4J. in accordance with the following:
a. Turn the POWER switen to ON.
b. Turn the O FILTER switch to OFF.
c. Turn the 0 2

RANGE switch to 0-20 ppm.

d. Turn tne PEN INPUT to ZERO.
e. Turn the CHART SPEED to RAPID.
f. Adjust the PEN ZERO control until the pen traces a line on the 0-20 chart scale at O.

l

g. Turn the CHART SPEED to 10.
h. Turn the PEN INPUT to 0 .

E 9. If the calibration of the 0 2 analyzer to be used has been performed for tne week, proceed to Step F.10. If the calioration has not oeen performeo, E recirculate the dissolved 0 caliDration tank in 2 accordance with the following at tne CAP, OPLElJ:

a. Observe the level in the oxygen calibration tank CAL-4. If water must De added to the tank, open V-24 and fill the tank tnen close V-24.

i

1 [ I LZP-1330-23 Revision 0 ' Octooer 19, 1981

                                                  .                    8 D. Open fully V-17.

( c. Turn the recirculation pump ON. lignts for the pump snould light on corn the Incicator CAP, OPLElJ, and CMP, OPLE4J.

d. Recirculate the water for a period of one (1) hour.

( e. Continue to calibration recirculate until the actual is performed. When tne actual calibration is performed, read and record tne temperature of the water in CAL-4 on LRC Form { 1097A (Attachment A).

f. Determine tne dissolved oxygen concentration from Attachment 8 and record it on LRC Form 1097A (Attachment A).
10. If the pH instrument has been standardized for the day, proceed to Step F.ll., if the pH instrument has not Deen standardized for the day, proceea in accordance with the following at the CAP, OPLElJ, or as otnerwise directec:
d. Align V-30 to pH calioration tank CAL-1, pH 4 buffer tank.
b. Align V-6 to pH CALIB SOLUTION.
c. Align V-27 to the nitrogen supply line.
d. Adjust V-26 until sufficient flow is indicated by the red flow indicator l ignt. Allow to flush for a minimum of two (2) minutes.
e. Turn V-6 counterclockwise to OXYGEN CALIB SOLUTION to terminate flow and align V-27 to the vent position.
f. Adjust the pH meter reading to indicate a pH buffer value of 4.0 by turning standardize control R-3, on tne pH meter at the CMP, OPLE4J.
g. Observe the pH monitor' reading for two (2) minutes and adjust if arift exceeds + 0 1 pH units.

(

r l . L I I LZP-1330-23 Revision 0 October 19, 1981

h. Align V-6 to OEMIN WATER and flush for a minimum of two (2) minutes.
i. Close V-26.

J. Align V-30 to pH calioration tank CAL-2, pH 7 Duffer tank.

k. Align V-28 to the nitrogen supply line.

[ L

1. Align V-6 to pH CALIS SOLUTION and adjust V-lo until the rea flow indicator is lit. Allow to

( flush for a minimum of two (2) m>nutes.

m. Turn V-6 counterclockwiseto the OXYGEN CALIB SOLUTION to terminate flow and align V-28 to vent position.
n. Observe the pH reading and record on LRC Form 1097A (Attachment A). The pH reading should be within + 0.5 pH units of the buffer value of 7.0. If tne value is not + 0 5 pH units, repeat Steps F.10.a through F.10.m.
o. Al ign V-6 to DEMIN WATER and flush for a minimum of two (2) minutes.
p. Close V-16.
11. If the oxygen analyzer to be used has Deen calibrated for the week, proceed to Step F.12. If it has not been calibrated, proceed in accordance with the following at the CAP, OPLELJ, or as otherwise directed:
a. Open V-9.

D. Align V-6 to 0XYGEN CALIB SOLUTION.

c. ODserve tnat recirculation pump is ON.
d. Close V-17 until 200 ml/ min flow rate is indicated by the red fl ow indicator. Allow to

( flush for a minimum of five (5) minutes.

e. While flushing, adjust the 0, calibration knob on the YSI monitor or the CAC A0J on the Rexnord monitor, at the CMP, OPLE4Je to indicate the u

E LZP-1330-23 Revision 0 5 October 19, 1981 10 dissolved oxygen concentration in ppm previousiy determined in Step F.9.f.

f. Turn the recirculation pump 0FF.
g. Close V-9.
h. Align V-6 to LIQUID SAMPLE.
12. Purge the LSP, OPLD8J, and CAP, OPLElJ, in accordance with tne following:
a. At the CAP, OPLElJ, verify V-6 is aligned to LIQUID SAMPLE.

D. At the LSP, OPLD8J, open RC-V-1.1 (-1 2, -1.3,

               -1.4,  or -1.5) depending on tne sample source.
c. At the LSP, OPLD8J, open RC-VREL-1 until RC-FI-l indicates 35-40 inches of water. Purge for a minimum of five (5) minutes. Slowly close RC-VREL-1 until RC-FI-l indicates 12-15 inches of water. Continue the purge for a minimum of one (1) minute.
d. Close RC-V-3 on t.3 LSP, OPLudJ.
e. Open RC-V-2 on the LSP, OPLD8J.
f. At the LSP, OPLO8J, adjust RC-VREL-2 until RC-FI-2 indicates 18-22 inches of water.
g. Verify that the flow rate at the CAP, OPLElJ, i s 200 ml/mi n by ooserv ing the red flow indicator is lit. Adjust RC-VREL-R on the LSP, OPLD8J, E if necessary to ootain proper flow rate.
n. At CMP, OPLE4Je turn YSI CHART SPEED to RAPID and verify PEN INPUT is set to 0 f the YSI 2

monitor is to be used for tne analysis.

13. To per form tne sample anal yses, proceed in accordance E with the f ol l ow ing:
a. Purge the CAP, OPLElJ, for a minimum of fifteen l

(15) minutes. During purging, proceed to Step i F.13.o. l 5 'E

LZP-1330-23 Revision 0 OctoDer 19, 1981 11

b. Determine the dissolved oxygen concentration 1 at the CMP, OPLE4J, in accordance with the following as appropriate:
1) If the Rexnord dissolved oxygen meter is being used, observe the meter reading and turn to a lower scale position as tne meter reading decreases. Allow to purge for fifteen (l5) minutes, then record the dissolved oxygen reading on LRC Form 1097A (Attachment A).
2) If the YSI dissolved oxygen meter is being used, flush for five (5) minutes or until the YSI trace is linear.
c. Ouserve and record the conductivity meter reading and the temperature of the sample stream from the CMP, OPLE4J. Record on LRC Form 1097A (Attachment A).
d. At the CAP, OPLElJ, turn V-6 counterclockwise to OXYGEN CALIB SOLUTION to terminate flow.
e. After terminating flow, permit the pH reading to stabilize for a minimum of two (2) minutes.

Record the pH reading on LRC Form LO97A (Attachment A). 14 Flush the CAP, OPLElJ, and LSP, OPLD8J, in accordance with the following:

a. At the CAP, OPLElJ, align V-6 to LIQUID SAMPLE.

D. At the Valve Control Panel, OPLC9J, secure the sampling lineup in accordance witn Reference 3, Step F.1.c.9) through F.1.c.10). C. At the LSP, OPLD8J, close RC-V-1.1 (-1.2, -1.3,

                     -1,4, ~1.5).

i I

d. At the LSP, OPLD8J, open RC-V-4.
e. At the LSP, OPLD8J, adjust RC-VREL-2 until RC-FI-2 indicates 18-22 inches of water. Flush E with demineralized water for a minimum of tnree (3) minutes.

l l l l

L LZP-1330-23 Revision 0 Octooer 19, 1981 12

f. At the LSP, OPLD8J, close RC-V-7.
g. At the LSP, OPLD8J, open RC-V-3.
n. At the LSP, OPLD8J, adjust TC-VREL-1 until RC-FI-l inoicates 35-40 inches of water. Flusn with demineralized water for a minimum of one (1) minute.
i. At the LSP, OPLO8J. close RC-V-3.
j. At the LSP, OPLD8J, open RC-V-1.1 (-1.2, -1.3,
                                                                            -1.4,  -1.5) depending on the sample source sampled, and flush witn demineralized water for a minimum of five (5) minutes.
k. At the LSP, OPLD8J, close RC-V-1.1 (-1.2, -1.3,
                                                                            -1.4, -1.5).

[ 1. At the LSP, OPLO8J, open RC-V-8.1 and hL V-8.2.

m. At the LSP, OPLD8J, adfJst RC-VREL-2 until RC-FI-2 indicates 18-22 inches of water. Flusn with demineralized water for a minimum of tnree (3) minutes.
n. At the CAP, OPLE1J, turn V-6 to OXYGEN CALIB SOLUTION.
o. At the CAP, OPLElJ. turn V-5 to LIQUIO SAMPLE

[ and fl ush wi th demi neral i zed water for a minimum of three (3) minutes.

p. At the CAP, OPLElJ, turn V-5 to CLOSED.
q. At the CAP, OPLElJ. close the flush water valve

( and aisconnect the fl ush water nose from D-3.

r. Secure flusning by closing the following at the LSP, OPLD8J:
1) RC-V-8.2.
2) RC-V-8.1.
3) RC-V-2.
                                                                                                                                         ?          ,

O

l L [ L I L LZP-1330-23 Revision 0 - Octooer 19, 1981 13

4) RC-V-4.
5) RC-VREL-1.
6) RC-VREL-2.
s. At the LSP, OPLD8J, close the flush water valve and disconnect the fl us h water nose from RC-DV-1. .
15. Secure the sample system in accordance witn the following at the CMP, OPLE4J or as otherwise directed:
a. On the pH monitor, turn switches S-3 and S-1 to the OFF posi tion.

D. On the conductivity monitor, turn tne function select sw i rth to the ZERO position.

c. If the Rexnord monitor was useo, turn the  :

function select swi ten to the ZERO posi tion and place tne power switcn in the OFF position.

d. If the YSI monitor was used, checx that tne '

YSI power switcn is in the OFF position and remove the chart paper, mark the cnart paper with date, time, chart speed, 0 range, and 2 sample point.

e. Secure the system lineup in accordance with Reference 3, Steps F.L. coll) througn F.1.e.

F 16. If the sample pH exceeas 7 5, correct the pH to 25 C L in accordance with the following: , pH f

                             = pH 1
                                    + 0.03 (T 1 - 25) where:       pH g = pH correctea to 25 C.

pH g = pH from Step F.13.d. T = temperature ( C) from Step F.13.c. Record the results on LRC Form 1097A (Attachment A).

17. Correct the measurea conductivity to 25 C in accordance with the following f ormul a:

u

LZP-1330-23 4 g Revision 0 Octooer 19, 1981 E 14 Ci = C , - 0. O l d + ( 's . 8 E-5 x T,2) 1 + 0.018 (T1 -25 c) wnere: Cy = Conductivity corrected to 25 C. C = Conductivity from Step F.13.c. 2 Ty = Temperature C from Step F.13.c. Record the results on LRC Form 1097A (Attachment A).

18. Record the dissolved oxygen concentration off the YSI chart paper on LRC Form 1097A (Attachment A) as appropriate.

G. CHECKLISTS

1. None.

H. LE_C C M ICAL SPECIFICATION REFg g S

1. 3/4.4.4.

II

LZP-1330-23 Revision 0 October 19, 1981 ATTACllllEliT A 15 1,aSalle County Station llRSS Analyses g pit , LZp 1330-23 Conductivity.LZP 1330-23 _utssolved oxvnen.LZP 1130-23 Standardization Init/ Time: Sample Init/ Time: Calihration inIt/ Time: Init/ Time: Recirc. Water Temperature,"C: Calibration Check S de Tvrem "C: Measured pil: 11easured Conduct ivity,umho/cm: Recirc. Water 0 Conc.,mg/1: 2 Correct the measured conductivity to Sample Init/ Time: Buf fer pil Value: Check SAT /UNSAT,I O .1 pil units: 25" C using the following formula: Sample D.O., mg/1: Sample Init/ Time: Sample Temperature, ':: C =C2-[0.018&(5.8E-5xT1 )] y Measured pII: 14 0.018 (Tg - 25"C) Off-Gas LZP 1330-27 Vacuum, RC-G-2. l . , S t ep F.1.d . h . If the sample pil > 7.5, correct the pil to Where: Cg - Cogductivity corrected to Pressure, RC-G-7.1., Step F.2.r). g 25 C in accordance with the following 25 C formula: pressure, RC-G-2.1., Step F.2.v. C2 - Measured Conductivity Dilution factor, Step F.5 plir = pilg + 0.03 (Tg - 25) Sample init/ Time: Tg = Sample Temperature, "C Where: pilt s pil corrected to 25"C pil i= measured pil Comments: Tg Sampic Temperature, "C Reviewed: ph at 25"C: Conductivity at 25"C, umho/cm: ' I.RC FORM 1097A 'E-E- - - - - - - - - - - - - - -

                                              -~- E ~          ~E~E-E                       E                                                   E
g LZP-1330-23

'g Revision 0 October 19, 1981

      , .                                                                     16 l

l ATTACHMENT B SOLUBILITY OF OXYGEN IN WATER EXPOSED TO WATER-SATURATED AIR TEMPERATURE DISSOLVED OXYGEN TEMPERATURE DISSOLVED OXYGEN C mg/l C mg/l 0 14.6 1 14.2 26 8.2 2 13.8 27 8.1 3 13.5 28 7.9 4 13.1 29 7.8 5 12.8 30 7.6 l 6 12.5 31 7.5 7 12.2 32 7.4 8 11 9 33 7.3 E 9 10 11.6 11.3 14 35 7.2 7.1 11 11.1 36 7.0 12 10.8 37 6.9 13 10.6 38 6.8 14 10.4 39 6.7 E 15 10.2 40 6.6 16 10.0 41 6.5 17 9.7 42 6.4 18 9.5 43 6.3 19 9.4 44 6.2 20 9.2 45 6.1 21 90 46 6.0 22 8.8 47 59 23 8.7 48 5.8 24 8.5 49 57 25 8.4 50 5.6 l E ,E

               --                                                                    l l5 l

l= , L2e i330-23 Revisi on 0

   '  ~

October 19, 1981 ATTACHMENT C 17 (Final) VALVE LISTING l RC-V-1.1 Reactcr Recirc Loop B Sample Cutout Valve j RC-V-l.2 RT Demin Inlet Sample Cutout Valve RC-V-1.3 RHR Loop A Sample Cutout Valve i E RC-V-1.4 RHR Loop B Sample Cutout Valve RC-V-1.5 RT Demin Outlet Sample Cutout Valve RC-V-2 Sample Source Isolation Valve RC-V-3 Sample Purge Cutout Valve RC-V-4 Flushing Water Isolation Valve RC-V-5.1 Pressurized Sample Inlet Isolation Valve RC-V-5.2 Pressurized Sample Outlet i solati on Valve RC-V-7 Diluted Sample Bypass Valve RC-V-8.1 RC-SF-1.2 Inlet isolation Valve RC-V-8.2 RCSF-1.2 Outlet Isolation Valve RC-V-9 RC-EV-1 Isolati on Valve RC-V-10 RC-EV-1 Evacuation Cutout Valve RC-V-11 Of f-Gas 4-way Valve RC-V-12 Argon to Air Ejector Cutout Valve RC-V-13 Off gas Vial Evacuation Cutout Valve RC-V-14 Argon Supply to Off gas Vial Cutout Valve RC-V-15 Off gas Sample to Gas Chranatograph Isolation Valve RC-V-16 RC-SF-1.2 Argon Purge Cutout Valve RC-V-17 Reactor Coolant Grab Sample Cutout Valve RC-V-18 Reactor Coolant Undiluted Sample Backflush Cutout Valve RC-V-19 Reactor Coolant Undiluted Sample injecti on Valve RC-V-20 RC-C-1 Fill Valve RC-V-21 RC-C-1 Isolation Valve RC-V-22 Liquid Sample to CAP isolation Valve RC-DV-1 Reactor Coolant Diluted Sample Injection Valve RC-DV-2 Off gas Sample injecti on V-Ive RC-VREL-1 Reactor Coolant Purge Throt rie Valve RC-VREL-1 Reactor Coolant Sample Throttle Valve. V-1 Off gas Sample to Gas Chromatograph

   -4   V-2       lon Chromatograph to EAste'     _.4 lon Chromatograph Sample Source Selecti on 5      V-5 V-6       0, Analyzer Sample Source Selection V-7       0}AnalyzerSelection.

V-8 lon Chromatograph Discharge Valve V-9 02Calibration Soluti on Cu .out V-10 Instrument Air Cutout V-11 Demineralized Water Cutout Valve V-12 Nitrogen Supply Cutout Valve E V-14 Argon Supply Cutout Valve V-15 Cal-3 Isolation Valve V-16 Cal-2 Isolation Valve E V-17 V-18 0 Calibration Solution Tank Recirc Valve 0 calibration Solution Tank Drain valve V-19 C 1-3 Drain valve V-20 Cal-2 Drain Valve V-24 Demin Water Fill to 0 Cal. Soln. Tk. 2 V-25 Cal-1 Drain Valve V-26 Cal-1 Isolation Valve E V-27 V-28 Ni trogen Supply to Cal-1 Nitrogen Supply to Cal-2 l V-29 Nitrogen Supply to Cal-3 V-30 Cal-1 Cal-2 Selection Valve l

LZP-1360-4 f Revision 0 Novemoer 3, 1981 1 RADIATION PROTECTION PRACTICES E DURING ACCIDENT CONDITIONS A. PURPOSE The purpose of this procedure is to provide guidance for the performance of radiation protection acti'/ities during accident conditions. B. REFERENCES , 1. LZP L330-50, " Radiation Surveys Under Accident Conditions."

2. LZP 1360-1, " Protective Measures For On-Site Personnel."
3. LZP 1360-2, "Use of Potassium Iodide (KI) As A Thyroid Blocking Agent."
4. LRP 1250-2, " Exposure Control."
5. LRP 1470-1. " Personnel Monitoring For External Radioactive Contamination."
6. AIR l-81-330.

i

7. 10 CFR 20.

C. PREREQUISITES

1. Incividuals expected to perform radiation protection activities under emergency or accident conditions must be familiar with the types, locations, ano use of equipment dedicated for emergency use.
2. Potassium Iodide (KI) should be taKen Dy individuels prior to being suojected to or as soon as possiole after having been subjected to a dose equivalent of
10 rem or greater to the tnyroid tnat could oe or
was caused by radioiodine i nhal at i on (See Reference
3).

O. PRECAUTIONS I

                                                                                          \

L2P-1360-4 Revision 0 Novemoer 3, 1981 2

1. None.

E. LIMITATIONS AND ACTIONS

1. Every reasonable effort snall oe made to maintain radiation exposures witnin tne limitations of Reference 7. Emergency personnel radiation exposures shall oe limitea to the recommendations of tne U.S.

Environmental Protection Agency as follows: NOTE l E The emergency limits snall De voluntary and l i mi tea 1 to once in a l i f etime.

a. Emergency Workers - This applies to conaitions where it is desirable to enter an emergency area to protect facilities, eliminate serious unplanned release of effluents, or to control fires.
1) Planned whole oody dose equivalent snall ,

not exceed 25 rems.

2) Plannea cose equivalent of tne extremities shall not exceec 100 rems (inclucing tne whole Docy component).
3) Pl anned dose equivalent to tne thyroid shall not exceed 125 rems.

D. Life Saving Actions - This applies to searcn for ano removal of injured persons or entry to the emergency area to prevent conditions tnat would injure otner people.

1) Dose equivalent to the wnole Dody shall not exceed 75 rems.
2) Additional dose equivalent to the extremities shoulo not exceed 200 rems.
3) No limit for the tnyroid since total loss of thyroid function could be allowaole.

F. PROCEDURE

1. Priorities for Raciation Protection activities tnat are expected to De cerformed under accident conoiticns

LZP-1360-4 ( Revision 0 Novemoer 3, 1981 3 are provided in Attachment A. They are to be considered as guidelines anich may oe modified to , suit specific situations and varying conditions. L some of tne assumptions used for ene formulation of AttaCnment A are as follows:

a. Radiation /Cnemistry Department manoower levels are at normal oacksnift compliment consisting of two Rad /Cnem Tecnnicians under tne supervision of tne Shift Engineer.

{

o. The first 60 minutes are of primary concern.

After tne first 60 minutes augmentation of the plant staff is possiole so tnat many of tne necessary activities can proceed s i mul taneous l y.

c. Add i t i or.a l guidance for the performance of specific activities is provided in Steps F.2.

tnrougn F.6 Delow.

2. Instructions to notn station and contractor personnel regarding radiological conditions will be disseminated oy one or more of the following:

L a. Announcement over tne station public address system.

o. Briefing at tne station assemoly area.
c. Curing initial training (new employees).
c. Prior to receipt of security access control key card (personnel reentry).
3. External exposure control.
a. External exposure control snall be in accoraance witn Reference 4. Exposure updates snould ce performed on a cail y or snift1y casis as appropriate.

O. Surveys will be per formed as outlined in Reference 1.

c. Dosimetry requirements should oe cased upon:

LZP-1360-4 Revision 0 Novemoer 3, 1981 4

1) Survey results; or

[ 2) Guidance provided in Step F.3. of Reference L 1.

4. Contamination control.
a. Protective clotning requirements should De based upon:
1) Survey results; or
2) Guidance proviced in Steo F.2. of Reference 1.
c. Personnel monitoring requirements are provided in Reference 5.

su Background radiation levels during accicent concitions will likely necessitate the relocation of plant contamination control points. Every reasonaole effort should oe made to maintain the Service ana ( Auxiliary Buildings free of loose surface contamination.

5. Internal exposure control / respiratory protection.
a. The use of potassium iodide as a thyroic olocking

( agent is described in Reference 3.

o. Respiratory protective equipment requirements snoula De baseo upon:
1) Survey results; or
2) Guidance provided in Step F.2.d. of

[ Reference 1.

6. Following control and staoilization of tne emergency conoitions, recovery and reentry efforts are to oegin. Guidelines for general raciological control and assessment are provided as follows:
a. Recovery personnel will use station instrumentation ana appropriate Radiation I Protection proceoures to determine the extent L or radioactive contamination anc raciation

[

LZP-1360-4 Revision G Novemoer 3, 1981 exposure in the affected area. On-site Radiation Protection survey equipment is locatea primarily in the instrument calioration facility; other locations include Rad Protection Office, Control Room, OSC, TSC, and assemoly area.

o. Routine procedures nave oeen estaolished ror operating survey equipment necessary to cerine

( radiation and contamination areas and equ i pine nt. [ Radiation Protection personnel are qual i f i ec to interpret survey instrument responses to alpha, oeta, gamma, and neutron contamination levels and personnel aose rates. Whenever possiole, areas ano equipment snould oe postea or marked consistent with normal radiation protection procedures.

c. Resumption of routine operations and reentry shall occur onl y wnen raciation levels ano

( contamination levels are such tnat the criteria in 10 CFR 20 are met. G. CHECKLISTS

1. None.

H. TECHNICAL _ SPECIFICATION REFERg gs

1. None.

( ( (

LZP 1360-4

     ,                                                                                                     Revision 0 November 3, 1931 ATTACHMENT A                                              6    (Final)

RADIATION PROTECTION PRIORITIES UNDER ACCIDENT CONDITIONS Radiation Chemistry Technician on Shift assigned to Laboratory: ( L Obtain needed samples as expeditiously as possible in accordance with the following: ( Vent Stack / Release Potential Rx Coolant Drywell SBGT NONE 1 2 3 IMMINENT 2 1 3 occuppTNG 1 7 1 VERIFY STOPPED 3 2 1 Radiation Chemistry Technician on Shift assigned to Health Physics: Priority with Release Potential: NONE IMMINENT OCCURRING ACTIVITY [ Surveys in support of work aroups 1 1 1 r L Evacuation 3 2 2 Monitoring at assembly < area 2 3 3 l Surveys of normally Occuoied Areas 5 5 5 ( Setup Emergency Facilities 4 4 4 w _ _ _ __-- _

111. - 11 LZP 1550-9 g Revision 2 Novemoer 13, 1981 13 1 SPECIAL TLD QUARTERLY SURVEILLANCE A. PURPOSE l The purpose of this procedure is to specify the frequency ! and manner for performing inspections of special TLD's and to provide directions to the i r locati ons. B. REFERENCES

1. Environmental Program Noteoook in Health Physics Office.

I i C. PREREQUISITES j g' 1. Obtain a vehicle for transportation to the various jg TLD locations. j 2. Obtain Attachment C (LRC Form 066) from the LRC Form l File. D. PRECAUTIONS ] i 1. None. l E. LIMITATIONS AND ACTIONS j

1. None.

F. PROCEDURE

1. General.
a. This surveillance will oe performea on a quarterly casis.

O. This surveillance is used to verify the presence of Special TLD's around LaSalle County Station. i 2. Pt. 7rm an inspection of the Inner Ring and Outer Ring of Special TLD's as follows:

a. Verify, at each location, the presence of a TLD Receptacle.

, o. Complete Attachment C as the inspection is I made. i t

11

LZP 1550-9 Revision 2 Novemoer 13, 1981 2 UOLE If a TLD is missing or damaged, Healtn Pnysics supervision is to contact Hazleton Environmental Sciences anc have them correct tne deficiency.

3. Refer to LSCS Special TLD Inner Ring (Attacnment A) and LSCS Special TLD Outer Ring (AttaCnment B) for maps of TLD locations. The cirections to the f locations are as follows:
a. Beginning from tne intersection of N21 Roaa and E26 Road, wnich is the gate to LaSalle County Nuclear Power Station, go west on N2L Ra. to the 5tn ana 6tn poles west of the entrance f where 107-1 and 107-2 are located. (A-180 )
o. Continue west on N21 Rd. to the 12tn ano 13th

( poles west of entrange where 10d-1 and 108-2 are located. (A-295 ) I

c. Continue west on N21 Rd. to 17tn. anc 18tn f poles west of entrance. Find 109-1 and 109-1 (A-220 )
d. Continue west on N21 Rd. to 25tn and 26th poles

( Find 110-1 and 110-2. (A-wesg)of 230 entrance. f e. Continue west on N21 Rd. to intersection of N21 Rd. and E25 Rd., turn north (right) onto E25 Rd. to the 4tn and 5tn poles nortn of ( intersection. Find 111-1 and 111-2. (A-240 )

f. Continue nortn to tne 12tn and 13th poles north of N21 Rd. Find 113-1 and 112-d. (A-260 )

9 Continue north on E25 Ra. to 16th ana 17th poles. Find 113-1 and 113-1 (A-270 ')

n. Continue north on E25 Ro. to 21st and 22nd poles. Find 114-1 and 114-d. A-285 )

This completes the inner circle.

i. Continue nortn on E25 Rd. to intersection of f E25 Ra. and N23 Rd. Go east on N23 to 4th and 6th poles east of E25 Rd. Fino 216-1 ano 21o-1 (A-330 ).

II LLP 1550-9 Revision 2 E November 13, 1981 3

j. Continue east on N23 Rd. to the 22no and 23rd poles; find 201_1 and 2Q1-2 (A-0 )
k. Continue east on N23 Rd. to ist and 2nd poles E east of E2605. Find 202-1 and 202-2. (A-30 )
1. Continue east on N23 Rd to Route 170. Go north  ;

on 170 (1.1 miles) to the 3rd and 4th poles  ! south of N24; find 2QJ-2and 203-1. (A-50 )

m. Turn around and go south on 170 (2.2 miles);

I find 204-1 and 204-2. (A-75 ) , i 1

n. Continue south on 170 to 4rd and 4tn poles j south of N21; find 225-1 and 2QS-{. (A-110 ) 1
o. Continue south on 170 to 0 8 miles south of N20; fino 206-1 and 206-2. (A-140 )
p. Continue south on 170 to N18. Go nest to E28.

Go south to the 5th and 6th poles; find 207-1_ E and 192-3 (A-loo )

q. Continue south on E28 to N17 (wnich is also Route 170). Go west (left) on N17 to 13tn and 14th poles west of E27; find 19d-1 ana 191-1 (A-170 )
r. Continue west on N17 to E25. Go nortn (right) to N18. Go west (left) to 4tn and 5tn poles west ofo E25 where 209-1 and 209-2 are locateo.
s. Continue west on Nld to E24. Go north (right) to N19. Go west (lett) to 4th and 5th poles l I west of E24; find 219-1 and 310-2 (A-220U)
t. Continue west on N19 to 4th and 5th poles west of E22; find 211-1 and 211-2.
u. Turn around and go east on N19 to E22. Go north (left) on E22 to 3rd and 4tn poles soutn E of N21; tind 112-2 and 212-1 (A-260 )  !

l

v. Continue north on E22 to 8th and 9tn poles north of N22; find 113-1 and 112-1 (A-285 )
s. Turn around and go soutn on E22. Turn east (letti on N22. Turn nortn (left) on E24 and

l lE . E l l LZP 1550-9 Revision 2 E Novemoer 13, L981 4 go to 2na and 4th poles north of N22; find 214-2 and 214-1. (A-300 )

x. Continue north on E24 to N23. Go east ( ri gnt )

on N23 to the litn and 12th poles west of E25; find 215-2 and MS-1. (A-315 )

4. Return Attacnment C to Health Physicist for review, noting any deficiencies and corrective actions taken.

CHECALISTS l G.

1. None. 1 H. TECHf41C AL SPECIFICATION R gp_R,$g R S
1. u_.

E E E E E E E I l

LZP-1550-9 l - Revision 2 ATTACHMENT A November 13, 1981

                                        ~

LASALLE TLD's 5 Inner Ring - 16 Badges J.# , North 22nd Road - r  ;& L . r' 6. . . l4

                .c u                                                                                                >

s , a s M f a w - (  : l a.. . 114-1 - h

a. ,

114-1 ' f

                 \" M                                                                                                                       '

[ f

                        ,9 m                 '.,

l I l 4 -

                                                                                                                       .                            \                                              LA5ALLE                        C0UNTY l-                                                                                               's                                                     .                                                    ,

[ V. i L ,I N,  ; i NUCLEAR POVER 113-2

                                                                                                                                                                          ~
h. 5 TAT l C N AREA ig 113-1 ,.

n p \s . ( b I 'i' g .. I l5.__

                                                                                                                                                          !f'.vy,\

1 12.. .2..ou .- [ s. (1P 112-1

                                                                                                                                            ,/- l                                          .

i l

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                                                                                                           /                          -                                                                           \

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     ~                                                                                               -

l5 ' 111-2 . I 111-1

                                                                                              '8                                                                                                                              *
                                                                                           /

d [ ., / i \ L 3, / U s o {2

                             .:                                          ,            ,e m

r l3 - , - . o

                                                              -110-2              10-1                          M            109-2                      109-1                          108-2 108-1                                                        107-2 107-1

_)O

                              ;I e_ _ '.-..'. '-p@ @ i_',*._."'

_ 7__ Cg -

                                                                                                                                                                              ~
                                                                                                                                                               ' .,' . , ~" . - 4          c.h h '                  L_      5          I                   $         .

c.a u.e a.us..o - l L yl l.

                                                                ~
                                                                                                         , North 21st Road Scale:         1" = 400'
                                                                                                                                                                              ........c__                                                _ _ _ _ _ _ _ _                                      a

LZP-1550-9

    -             -                                        ATTACHMENT B                                        RavisIon 2 LASALLE TLD's
                                                                                                                             '9 6

Outer Ring 32 Sadges Ottavia E J E; l . g,z 0 f Marseilles 5 t on.

                                             ,s'
                                                   %.                      seeece e           215-1 216-1 201-1 202-1            ,203 -1                       -

215-2 216-2 201-2 202-2 a 203,-2 214-2 m O 213-2 .- 214-1 m I m204 -1 213-L = 3e c=204 2 - 6* ' o5 4 - 212-2 e205 -1

                                                                       '                    8 212-L
  • 205r2 o 13

( SITE PROPERTY

                                                                   .                        = 20 i-1 9o Grand Ridge ="211-1        2ii-2 ,,zio-i 204-2                     Verona 210-2 m207-1 as 209-1 2C9-2              m207-2        l
                                                                           ,,208-1 20s-2 Kinstnen Ilo Ransorn                 ,

i Kernan Streator _ 10 LA SALLE. ~ COUNTY > GRUNDY COUt

                                ~

OVINGSTON C0 LINTY e

                                       ;             L*~=                                                        '    ""

SCA_ . L

               "                                       ~

LZP-1550-9

     .                                                               ATTACHMENT C                                           Revision 2                   '

November 13, 1981 ( SPECIAL TLD PROGRAM LASALLE 7 (Final)

                              'Is T'LD Pre nt                        is TLC Present             is TLD Present Tt.01                (Yes or No)     TLD#         (Yes or No)     TLD#                             (Yes or No)
                                                                                                                                                .W 107-1                                       216-1                      208-1 107-2                                       216-2                      208-2                                                   .

t 108-1 209-1 201-1 _ l 108-2 201-2 209-2 r - [ 109-1 202-1 210-1 , i 202-2 210-2 ( 109-2 110-1 [ 110-1 203-1 211-1 L 203-2 211-2 [ 110-2 111-1 '204-1 212-2 g r 111-2 204-2 212-1 112 3 205-1 213-2 [ 112-2 205-2 213-1 e i j y_ t

                            ^

206-1 214-2 , 113-2 206-2 214-1 f [ . t 114-1 207-1 215-2 , f, r i L 114-2 207-2 215-1 , t L I k

              ,Conven t s :

p I 5 L Surveillance Perfor :ed By: - Date: l t L Reviewed by: Date: i Health Physicist  ! LRC Form ~3524 L ---------}}