ML20003G554

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Forwards Data Developed for Measuring U-235 Content in Floor Tiles & Concrete Generated as Result of Decommissioning Effort.Matl Will Be Measured Using Nondestructive Assay
ML20003G554
Person / Time
Site: Wood River Junction
Issue date: 02/27/1981
From: Lheureux J
UNC RECOVERY SYSTEMS, UNITED NUCLEAR CORP. (SUBS. OF UNC, INC.)
To: Partlow J
NRC OFFICE OF NUCLEAR MATERIAL SAFETY & SAFEGUARDS (NMSS)
References
18679, MQA:81-11, NUDOCS 8104300055
Download: ML20003G554 (11)


Text

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'l UnC RECOVERY SYSTCmS

, Y4s70-720 Dnns'on of Unced Nucfear Corporation One Narragansett Trail WJephone 401' ~,,.

U C A une assounces comrame wooorwerauncion.nnoegde N

3 h

^L MOA:

81-11 REGIVED a?:t f<

il-f-

MAR 11198'E h Y g'# h February 27, 1981

$%g

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ss u,'f*L s.s'

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U.

S.

Nuclear Regulatory Commission s @,,3 im c

James G.

Partlow, Chief G

Material Control and Accountability t

M Licensing Branch DOCKETED Division of Safeguards USNRC MAR 111981 > C Washington, D.C.

20555 k.

Reference:

Decommissioning FNMC Plan NM5S C

9 Mall SECTION l-Gentlemen:

DOMT CLERK

'u s -...

/

Enclosed please find data developed for the purp s,q;,~ i ! L of measuring U-235 content in floor tiles and concrete which will be generated as a result of our ongoing decommissioning effort.

It is our intent to measure this material using non destructive assay (drum counter).

.If levels exceed the range of calibration, the drums will be broken down into two or more components and recounted.

Isotopic determi-nations will be made by dissolving a minimum of five randomly selected samples representing different loca-tions within the process area and submitting the samples to a qualified lab for mass spec analysis.

l As this submittal does not decrease the effectiveness of the nuclear material control program, no license fee is being submitted consistent with your letter of March 20, 1979.

If you have any questions regarding this submittal, please give me a call.

Yours truly, kNAb t ;

/.

H.

L'Heureux Manager, Quality Assurance r

JHL:ddm

(..

-('

Enclosure

~

b S.' u 2 S') L 8104300055

.7.8679

(:

Subject:

Cement Calibration for U-235 1,

Purpose:

To develop a standard curve in order to establish measurements of U-235 in concrete material being_ discarded as a result of the decommissioning program.

Procedure:

Clean cement blocks'were broken up and placed in a 55 gallon drum.

Known quantities of U-235 (in strip form) were then added to the drum in a random fashion.

A series of'20 counts was then taken with the positioning of the strips being changed every 5 or 6 counts.

The statistical average was then calculated and plotted.

Data:

Recorded data pn attached sheets.

n.A y;sv..~

  • sk 4

4 TAA:ddm 2/27/81 i

i l

i l-I

-. - - - - - - - - < - -- - - r - - -

]

~

Cement Std 1 gm U-235 2 gm

~~

U 605 601 529 587

.554 512 555 554 555 608 546 499-594 567 506-631 603 497 560 570 518-591

-556 493 569 565 549 611 533

+

519 568 622 D

537 632 534 591 574 613 548 571 583

'634

~

518 566 r;5V' g.. P. ip 6

530 610 s v

,: =

563 579 580 598

"~

573.65 589' Bkg 517.65 583.52 Not 55.95 Bkg 517.65 Net 65.87 l

l I

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I

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~

3 gm 5 gm

'8 gm 10 gn _

674 763 921 974 596 706 868 967 651 699 883 1006

'650 721 876 944 660 740 785 930 617 709 843 1008 648 712 872 1001 663 719 821 1016 631 728 860 1025 682 700 884 963 642 739 902

.947 675 723 906 914 621 764 882 1023 638 764 933

989 611 761 919 1069 640 718 891 952 676 770 900 988 614 f;

... dt712 926 976 i

610 "' N !J'" 1717 898 980 620 759 948 984 641.2 731.2 885.9 982.8-517.65 517.65 517.65 517.65 Net 123.55 213.55 368.25 465.2 9

{

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20 gm U-235 30 gm U-235-1660 1931 1592 3054 1624

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Subject:

Floor Tile Calibration for U-235

Purpose:

A standard curve was developed in order to_ establish U-235 values for floor tile being discarded from the process area.

Procedure:

New tiles were bro, ken up and placed in a 55 gallon drum.

Known quantities'of U-235 (in strip form) were then added

/d random fashion.

Three (3) serie.s,of to th(6)y,urp:.iripc ten (1 counts' were recorded for each point, with the-position l,;o~f the strips being changed for each series.

The statistical average was calculated ~and plotted.

Data:

Recorded data on attached sheett.

Note:

Background subtraction not reflected in the -table, but reflected on the graph.

T. A. Ashley February 18, 1981 8

.o

===.

Background===

546 532 537 571 531 543.4 1 gra_m U-235 Pos. 1

.Pos. 2 Pos. 3 578 589 595 555 591 572 573 580 600 591 575 581 599 550 600 577 55v 643 597 563 618 591 592 578 593 627 589

-603 607

_rg.~...2.sp573 575

" NIF 666

^

598.3.,

577 598 2 gram U '>35 578 671 705 618 674 688 581 642 709 602 622 707 606 653 680 659.8_-

630 655 682 630 691 696 656 671 713 636 657 717 636 692 696 617.3 662.8 699.3 3 gram U-235 640 735 726 674 720 667 680.2 654 696 680 668 658 656 674 660' 740' 654 671 709 669 689 691 683 697

,694 660 631 659 664 684 704 664 684.1 692.6

~

^

4 gram U-235 Pos. 1 Pos. 2 Pos. 3 742 785 834 722 719 858 790 742 824

  • S9 757 816 785.l i

739 775 861 743 730 846 810 763 838 782 763 834 737 730 852 794 763 846 761.8 752.7 840.9 5 gram U-235 i

852 866 882 1

901 841 924 884 857 888 857 879

.913 879.9 886 865 898

^

886

' M !d*5~p850.

896 s-826 R

'"904 866 885 854 881 882 954 870 858 901 879.1 872.8 887.9 8 gram U-235 1109 1096 1188 1083 1037 1102 1070.7 1083 1023 1103 1074 1036 1041

.1020 1055 1115 1054 1047 997 1050 1076 1061 1128 1075 1078 1048 1075 1060 l

1083 1057 1069 l

1073 1057.7 1081.4 10 gram U-235 1242 1191 1248 1234 1181 1294 1239 1206 1278 1281 1212 1196 1212 1170 1270 1185.3-1330 1165 1184 1209 1208 1217 1199 1172 1190 1163 1156 1246 i

1262 1167 1239 i

1237.1 1182.8 1136.2

/

. ~ _

20 gram U-235

.Pos. 1 Pos'. 2

.Pos.'3 2131 1587 1996-2106 1672 2021 2178 1680 1997 2094 1643 2072 2075 1634 2020 1931.7 2088 1692 2145 2157 1660 1965 2084 1686 1829 2175 1686 1960 2155 1619 2149 2125 1655.9 2015.4 30 gram U-235 2707 2745 2761 2803 2850 2783 2947 2852 2699 2863 2874 2793 2760

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