ML19312E643

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Forwards Matl on QA Program for Shipping Container for 1 Ci Am-241 Sealed Source to Be Used for Analysis of Mineral Samples.Requests Notification of Addl Required Info
ML19312E643
Person / Time
Site: 07100389
Issue date: 05/12/1980
From: Muse L
GEORGIA, UNIV. OF, ATHENS, GA
To: Macdonald C
NRC OFFICE OF NUCLEAR MATERIAL SAFETY & SAFEGUARDS (NMSS)
References
NUDOCS 8006050454
Download: ML19312E643 (21)
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Text

{{#Wiki_filter:. _ _. 9 ~7 / .-) e, o < 3 b // .s v 4 PUBLIC SAFETY DIVISION THE UNIVERSITY CF GEORGIA Athens. Georgia 30to2 . ~. m..C. a y' k, D....,.-m m a S A ts ^ _= n _, IM@..?w., !rs! s% Notta.: ne. r, i y%.unt N,,\\..r.ien D ;mmat th. sum: h%. cA::n ~, ' 4&$G%i N-92. ! 12.' M-5Cfa'3 ,.;*' /.'J? 0; t r., %,. .ine. g -/ 4 -..-/ ~ s. f v g May 12, 1980 f j,*,d 2 1 "" 5" 'k f'M, i - THIS DOCUMENT CONTAINS a .a ( \\ 'y N'c g g W' P0OR QUALITY PAGES !!:Donalu. = / b Mr. C. E. Y ~ [~ liO g Chief, Transportation Branch l-Division of Fuel Cycle & Material Safety U.S. Nuclear Regulator / Cornission "+ Washington, DC 20555 ,t, D Daar Mr. Mcdonald: @,2 cc o Dr. John Ucakes, Director of the Center for Applied Isotope Studiosi,) Univer-sity of Ccorgia, has applied for a license to use a 1.0 curie Americium-241 scaled source for analysis of mineral samples in Alaskan Coastal Waters. Appropriate steps are being taken by the University Radiation Safety Con-mittee and this office to establich safety procedures and cbtain a license amendment from the Coorgia Department of Human Resources. Mr. Glenn Murphy, Research Coordinator for Dr. Moakes, has prepared the enclosed material on the quality assurance program for the shipping container. Since this is our first experience in meeting the requirements of a quality assurance program of this kind, we are requesting that you let us know what ,( further information you will require. Questions or information should be addressed to me at this office. Yours very truly, v .u.t (f G. Ill d Lowell A. Muse Radiation Safety Officer Environmental Safety Services LAM:swc Enclosure Booooso154- ~~ -~ ~ =- -=- C _.. _ ~

CEt TER FOR APPLIED ISOTOPE STUDIES ' - ~... -... . ~. _.. THf. tlMlVEf4'JITY of Ct.OR"lA 4 )10 pt ERistr4D RD. ATH Et4 5. C. A. 3.,002 I 84C4l 542-5379 e 1- .i - .,e Ispril. 18, 1930 ../. r 4 Lowell A. !'use ) Radiation Safety Officar Environnental Safaty Services r 'L'niv,ersity of Geor'gidI i. Athens", GA 30602. r.

Dear Lowell:

--/ Attached.id, the'l:iformatiori 'ycu'Uquested for the lic'ense candmant for the -1 curie aracricium-241 sealed cource. .. _ e. . _ ~. . e Please forward the raquest.to the, stata-as scen as possible, and keep me advised of any'. developments or need for-further information. ..,. ;. ~~~:.+m,~.p....#..-..- ~ s. Sincoroly, n.s 1 .... -~~. /,. lj

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i., / / f .a .4.. Glenn'L. M uphy - , Research Coordinator II ~ '. '...,' i 4 o gg,, a. l Enc.: Radiation Safety Procedures Security / Protection /, Instrumentation Source Dose Rat.e Location of Usel Public Rolatic.hs Materials.,. .. q .k? # ~ l 7 q. 5 ,; *. *e - 4= ~.,, ,.,.as j { t .c.. ,.~ :;. - ^ g. ~ I ] s 3-e o. j-u :qat emparemr<.unmvr,:

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I Radiation Safety.Procadures I. Transpo'rta tion s. The Am source will bd t'ransported in"a DOT 6M, Type B, shipping container'. ,;n / ':"nc shipping, contain 3,r 0111 be t.:ar%cd as follows: 1) " DOT 6M - TYPE D", "IODIOT.CTIVE MATERIALS" 2) Nama and address of centaiper registra..t ~ ~ Wh e'n the sealed source is used in' ar.y location other than the labor-atory ' (University o( Coorgia), the source will be stored in the shipping container. During trar nort, the cource will he accompanied by Health ~" Physicist. ~- II. S.y ; tem Set Up c "[Thesourcawillbestoredin he sl$ipping contain r in the secondary fluorescance code only, wit. h.t.h. e. 51umif.6,m.'.co.ver/ shield in place. ~?- . -....,.... -. ~. -.... The source will be. removed-from ths shipping container, seated on the Si(Li) detector and tightened down with thumb screws. The source will re:a'ain aitaEhed to the Si(Li) detector unless the following conditions occur: 1) removal for stor$tge in shipping ~centainer 2) change from secondary,to direct, fluorescence mode (or vice versa). Prior to storage in,the shipping' container, the ' exciter system will 4 be converted to the secondary fluorescence mode; III. Direct f Secondary Fluorescence Mode Conversion O ......z.>. c.;,. Direct -+ - Secondary m:.o.m-+ '~ - w 1). RcI.ove the exciter system from the Si(Li) detector.

2). Unscrew tha aluminum retaining ring.,

3). Turn upside down on table and slide housing' upward. I 4). Place hous'in'g f,ijht.s.ide'.up' on table.

5). Using Tones:

a.) remove primary shiel'd f' rom stack and place in housing. b.) recove ring shield and store. c.) place target (Sn, Mo, Dy) on primary shield. d.) remcve spacer shield and place on target. e.) remove annular cource (active side g down) and place on l spacer shield (active side stays down). l 4 ' en i n.

I / f.) replace alumin :n retaining ring and cover. g.) place exciter aysten on S1(Li) detector and tighten thunb Scr6WS. h.) syntas t'. ..c. e n 9. Cn.- oporstien, secondary + Direct

  • l). P.cnovo tha e::citor cyntem from the Si(Li) detector.

2). Us.cc .- tF.0 retainin; ring and re. ova

3).

Turn up.Md.: c'. -in en tabic c.r.d.' slide hca 1::g of f. 4) Placa housing ri;M '.+ up on' table.

5). Using Tonas:

a.) remove' prinary shield and place. p,.';St in housing. b '.* ) r.: sv5 and : stoS3',taE50' ca'iffi'al). ',,, b.) placa, ring. shield,on pri::.ary shiold. d.) remova spacar shield and set aside. e.) ' remove annular sealed cource (active sida in up) and place in Ecusing (active side is up). f.) replace cpacer shiald. - ,e

6).

F.eplace retaining' ring with hovar.. Excitar systda can nc#'he toYe'd"o{' [> laced en Si(Li). detector. IV. Change Target iaterial. ~ ~

1). Follow steps 1-5b of Secondary + Direct convercion, then folicw steps Sc-Sh of Direct 1 3econdary conversion.

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e e. .ewcarity Duringtranspoet$tionorstorage, thu ?.m coaled ccurca '. rill be kept ur.dcr lock tind key in a Type B chippinJ ccntaincr. When tha cource is placed in operath n en the Si(Li) detecter, the tchle top uill b3 clocri and locked. Accaas of percennel in the vicinity of the c.ourca.. vill ha lin'ted b.r tha health.chvalcist on duty. Prc t a ct !.c n/In : trui.d.ta tion During transpcrt and usa, a calibrated,Zbt.rline nad 0,il (na:: 500 R/hr) loa chr; Mr and an Eberlin-s E530 GM curvey noter (nax 0.2 n./hr) will be. availcble. Th:23 individualc.rcrking dir ac:ly with the source, Dr. J. !:oakes, J. Srr 1 ding, and G..'u rp y, vill La monitored using film badges supplied h by The C:avoisity o' Caergia. The film badcas will be worn on tha shirt collar. Also,' finger 4 D balge uill be worn when loading, changing mode 3. of c,m2h*: ion er u.scarine; the courcs. 1 i e ..e o ~.- ~, * 's, a...,. * .N }p..'"a. s.1 M..=./J. ' r e.+:. V. e. se a*

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Source Do.;o PY.e Iq.u riciuT.- 2 41 1.C Currie ,P.33E CF OPE.%TIO3 7 CI.0 SED Tcp curfaco 3.0 p.R/hr Top 6" O.7 c.h/hr Side surfa::e 250 .T.R/h r $1.30 3" 0.7 ;-n/hr -.s y -) ..a......... .a 4 i:. s -.. r......... 4 ,,c r. ........:~..,...e.-... n DIRECT. FLUCPESCE; ICE- ...... ~.. _., .s,,. :.., Top surf ach (window)

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,R/hr Top 3 . ' -* - *: ' # 4.2 R/hr. .. ~ Top 6" ' . 1.65 R/hr Top 9" 0.85 R/hr Top 12" 0.5 R/hr 0.4 mR/hr Side Surface. O.1 mR/hr S.ido 3" y- .I ,,..c s l l \\ .,m, ( ( . 2 1 Infccation Supplied b/ :lew Ongland ::ttelaar b \\ g M4

. v. retordurg, A.l waha i ~ Ship: Stevic Dato: 1 Iwguct - 15 October.1730.. Cetalla of Use:

1. st.rvey will be con '.uet.:d c,C tl c Duncan Canal sadi.bnts 'using Chrte. alloy's res2 arch ship, "3 evie," within the peried of Septz-ber 6-22, 1080.. fadi. cont sa.pl,c,and XPT analytical equip.wnt will be used in the survey. The.procc)ure to be folicwed will be to sucP. the surficial sedi-ra:ent's from tha c3 abed floor aboard the Stieve where an autstated samplo preparatica cyatcm vill rap'.dly prepare the s rples for XT7 analysis.

Chrerallc.y luss b-een pining barius ors for many years,in this arca and tha purpose of tha survey will bo to try and evaluate the extent to which :-ine tailings may hxn diffused into the canal araa. ..s 3 r-( Skidaway Island, Georgia-

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Chip Tit Jones Dates: June 1980, with ocher datos to be added wit h concurrence of Radiatica Safety Officer (RSO).

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?..... CENTEP. FOR APPLIED ISOTOPE STUDIES RIVT PBCfiO ft8ESE AH0H L 44 Cit ATQpY V L C '., ' " J. : _, 7*/ (; / d r,v H.il4 10 0 HIVC 'f Ct* N o AD. ATHCfd,C4 DOCO2 (404l 5 42 *,r.7) ,_ April 18, 1980 Lovell A. Muse Radiation Safoty officer Environ:-antai-Safety Sc-vices Univ 2rs(ty of Georgia Athens, GA 30602-i ~ s a Daar Lowell 6 Attached is information which ic necessary for submitting to: i Mr. C. E. "cDonald Chief, Transportation Branch Division of Fuel Cycle G Material Safety USNRC Washington, D.C. 20555 Tho. University must apply for and obtain approval for a Quality Assuranco (QA) Program pursuant to 10CFR Part 71, so that we can transport the sealed source (241Am) to Alaska for testing of the sea floor sampling and XRF analyses system. 5 The "10 CRT Part 71 QA Program, University of Georgia" let'ter must be forwarded to the NRC as soon as possible. Please note, an organizational chart will hoed to be daveloped showing the relationship of: 1) President 2) Radiation Safety Committee 3) Radiation Safety Officer (RS0)

4) Vice President for Research l

5: Center for Applied Isotope Studies (CAIS) The organizational chart should be attached to the letter as appendix A. .:._.. u. w The QA Program and the written procedures should be acted on by the f Radiation Safety Committ'e and ir.plemented. e e l b i 4 L AN C O U 41,. C**09'WPelT*1F#tF war s g. -

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Ljaell.. *:asc 1,pril 19, 193') P.qc 2 .i.e inferrutien generated above is f ren cor.municatien with :'P.C, 13 cya aeries nr.d DOC r.ar."c.l. If you hcw ar.y que:,tictu un this plea >o give mc a call. Dealing with ti;? !;RC ma'/ ta%2 ti: c, and we need to have approval by 1 August 1980 (our scheduled'date of dup 2rture). Sincerely, d# fl/ f gdQ. /uj G,T:4:s v/ -,Glenn L !urpuy' ( Research Coordinator II GU4: cm Enc.: 10CFR Part 71 QA Progream, QA Program Training Procedures Inspectien/ Tost / Operating Procedures 4 .D N =*%$

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OhPRocLJ4 10 CFR PART 71 Ur'"aesity of Ccorgia 1. ORGANICATION Tho final responaihility for the' Quality Assurance (CA) Program for Part 71 rpquiroments, rests with the University of Geo'rgia. Design and Fabricat, ion shall not bd conducted under this C? program. The CA Progras is implem4nted using the organizational chart attached as Appendi:t A. The Radiation Safety officer (RS0) is responsible for overalf administration of the program, training and certification, document control and auditing.. The Direhtor, Center for Applied Isotope Studies (CAIS) is respon-s,ible for handling, storing, shtpping, inspectien, test and cperation status and record keeping. 2. ' QUALITY ASSURM1CE r.".OCRtai 1 Tha Radiation Safety Cor.mittaa (RS0) of the U,niversity of Georgia establishes and implements this QA program. Training, prior to engage-me.it, for'all ga functions is required according to written' procedures. QA prcgran rev,isions will be ma'de according to written procedures with RSC approval. The QA program will emph(112e control of the character-istics of the package which aro critical to safety. The RSO shall assure that alp radioactive material shipping packages are designed and manufactured under a QA-Program approved by NRC, for all packages dos,igned or fabricated after the effective date of the CA Program. Certification from the manufacturer will be kept on file by nGO. t 3. DOCU:'EN,T Cdl. TROL ~ i- .~..+....~...e All documents for the shipping container will be controlled by the RSO. All document changes will be approved by the RSC. The RSO shall insure that all CA functions are conducted in accordance with the latest applicable guidelines issued by the RSC. 4. HANDLING, S':ORAGE t. SHIPPING *

  • Written safety procadures concerning the handling, storage and transportation of the shipping containei will be,follcwed.

Transper-tation will not be made unless all tests, certificatiens, acceptances, and trial inspections have been completed. Work instructions will be provided for handling, storage and shipping operations. The CAIS health physicist shall perform the critical nandling, storage and shipping operations. e .e- + O-- e ' 9P

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.t;;nic:1, U.sT A::D GPlW 'I !:'O GTA':U3 Ir.specticn, test chd cI0 rating tatus o'f the Type C shipping c;n*.cinar rill be controlled by uritten proccourcs. Ctatuc will ba ir.1! cited by lo3 cntry. Status of r.on-confer. ming contain:er will be peritively.M',ntained by writton procedures.

CAIS livalth Phy0icist shall perform the regulatory required in;..:tions an: Losts in accordance with uritten procedures. The g3 chall it. on e that th3sc fenecions.are perforred. 6. QUAL rt ASCC:C CE RECCaDS R2 cords o! package approvals (including references and drawings), procurement, inspe:tions, tests,'cperating logs, audit results, pers:nnel trainind and qualificatiens and records of shipr.ents will be raintained. Dc;;riptions of equip =cnt and s.'ritten procc-lures will also La naintained. These records *. rill be t$intained in accordance with written ' pec edures. The rc:erds will be identifiable and retricvable. A list of thru records, with their storage locations, will be main-tained by t': e R50. 7. ,;UD:IS Established' schedules'of audits of the QA Progran will be performed us;ng written checkli;ts. Results of audits will be ' maintained and reported to RSC. Audit reports will be evaluated and deficient areas corre ed. An audit will be conducted at least once per year. Audit reports will be raintained as cart'of,tha,QA records. Members of the audit team will be drawn freq the RSC. a p ;.7. - o .e 4 0 a G o a e 9 + m% ,,e 6 e s. em...-e-. .e..>.=** = * * * " * "

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1. SCOPE The nSO regularly accesaca the Geope, status and irplementation of the QA Pr<rjer.m. This QA Profra.n will c.mply with ICCFR Part 71, Arpendix E, "Guality Assurance Criteria for Shipp'ing Packagcs for P.cdicactive

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2. Pim.' A't CHA':GE3 .Pevision: to tha CA program will b2 approved by the RSC. The RSC vill be responsible for ensurir.; that tha QA Program is implerented and enforc;d. 3. FU:;0 TIC:1 The Ca Program vill colely govern ene 037 Et, Type a shippir.g centaincr. The ESC is the final authorit/ in rc:alving di:putes involving quality, aris t:*g from the difference of o? nion hatween Ci/CC personnel cnd other i depfrteent personnal.i 4. TPAI!!I::3 A training program sill be entablished such that:

1). Personnal respons'ible 'for performing quality-related activities are instructed as ta the rarpose, scope, and irplenentation of the CA procedures.

2). Personnel parforting quality-af fecting activities are trained in the techniques of the activity being performed. 3). Tho' secpe, objective and method of imp (crenting the training progr,am is docunertad. l 4). Proficienc;; of personnel performing quality-affecting activitics is maintained by retraining, re-examination and/or recertifying. 5). Quality related activities are perfo'rmed with specified equiprent !I under suitabla conditions. o l l 6). Prerequisites hav'e been satisfied. prior to inspection and test. 5. RECORDS l Records will be maintained by the RSO to provide docementary l evidence of the quality and safety of items and the activities affecting quality and cafety. l l l I l

C;. Records will inclu S: 1). Op rating Iv;Js - as necessary. 2). Results of revic 0, irmpu:tions,. :.es ts, audits and material analyses - as ncceccacy. 3). Qualification of personnel, p' ocedures and equirment. r 4). Drc.uing's and spa ifications - as necessary. 5). Procure.mont dee'rento. 6). Calibration'preenduras,and reports - as nacessary. 7). 1:an-conforman:a reports. 8). Corrective action reporta. 1%cordri vill be' raaintained identifiable and ' retrievable. A list will ba ::faintained cf the records and their, storage locations. Design related r'bcords will be maintained for the life of the shipping container. All othe,r records will be maintained for two years. Inspection and test records will cntain at least the following information: 1). A description of the observation. 2). Evidence of ccmpleting and verifying an inspection or test operation. ~ i s i, 3). Date and resultis of the. test. 4). Conditions whi.ch reduce qual'ity. O i 5). Identificatien of the'incpector. e l l l ( l 1 g-e e m. $% $ 4#Mesq4>664

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M!.iING P.S.CCI:DU; MS 1. The drum r.ust raet nbecification C:!. 2. T,ha drum. eu:t be either 30 gal, or 55 gal. capacity. 3. The dre..must contain at least fcur 1/2" vents (pressure-relief) near tho ten of the drur.. 4. Inner cantainmant vessel must be made of stainless steel or equivalent material. Max I.D. - 5.25" ein I.D. - 4"; min length - 6". .~ 5. Inn.tr contain.T.ent vesuel cust be fixed in place using nachined discs and rings.%dJ 'of fiberboard' having a density of at least 0.24 g/cc, fitten r,uch.that the clearance between the ch.ll, fitaboard and inner vcasal do not exc. red 1/*". 6. The cuter drut closure cuat he at least 12-gauge bolted ring with drop forge.1 lu;c, one of '4hich is threaded, and a 5/8" steel bolt with loc.k -4 nut. 7. Th cicuure device must havo r eans for the attachment of a tarper-proof lock and coa.l.* ~ 8. Th. drum nuct be narked " DOT-6M Type B" "PJ,DICACTIVE MATI.tI ALS" (gauge / rated capa' city /yr'of nanufacture) 1.e. (18-30-80) or (18/16 80) - la gaugo body - 16 gauge head. t.... w 1

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~ 1::SPncT!u:!, 'IC. T />.::D 0: tix;; :: i noci.tc;i -J 1. Ger. ural Tnquirenata no chippir.g ntainer shall r aet the criteris spe:ified in Titio 40 Tra.d.sportation par::s - 173.104-1 through l'1c.104-5 (general requirer.cnts, ra?.ed capacity, canstruction, closuro, narkings). s 2. Status Conditreat The applicaticn or rc Ova' of inspection and welding st;mps and staCus,injicators cuch c.s tags, narkings, labels and sta ps will be approved by RSC caly. Ecpired inspections; tests and othar operations will be controlled by the F.50. 1:or.-confornir.g parts, inoperative parts cr r.alfunctioning packages wfl'. be flaggad by the R20. The container will be tagged ":;ct for use." / a .~ 1 .s .a,... ....:..~.... o

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APPE:IDIX A b o PRESIDE!;T FADIATIC: S/JETY VICE PTISIDE!!T CC::MITTZF I'OR FISEARCl! DIRECTOR CF PUBLIC SAFETY D".RZCTOR CF CZ:;TER FOR APFLIED ISOTCP1: STUDIE3 FADIATIO!! SAFE'I't CFFICER 4 a

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~ 401-512 2200 49 4 -P.12-5T 01 401-312 1122 404 542,5073 IHrre ar May 5, 1950 101 $ l2 22 n t'r. Glenn Murphy Research Coordinator II Centor for Applied Isoto e Studies Riverbend Research Lab Carpus

Dear Glenn:

In order to fscilitate the licensing of a 1.0 curie 1 Am source to be used in Alaskan Unters, the folitaing additional information is requ0sted. F 1. Please furnish a diagram of the shipping container. a. Shos radiatien levels b. Show locks, seals, and other security devices, Specify construction materials in the inner and outer containers. c. 2. Furnish documents from the builder of the shipping container, cortifying that the container meets all requiremerts of the U.S. Ocpart=cnt of Trans-portation and the Nuclear Rcgulator'f Co:micsion. Show results of inspec-tions, tests, and material analysis. 3. Furnish the name and phone nu-her of a person representing the builder of the shipping container who can be contacted for further information. ~r 4. Furnish a drawing of the source capsulo with model and serial number. 5. Furnish a diagram of the proposed analyzer syster. as it will be used en the ship. Show safeguards to prevent excessive exposure to crc'.- members or other a. personnel, b. Show security measures to ensure that the source cannot be lost over-board in case of severe weather or accident. Show expected radiatien levels around the source while the system is c. in operation. 6.' List any training or special instructicns which will be given to the ship's crew. 7. Furnish a copy of a checklist to be ured by the audit team checking the quality assurance progra:. Ccpies of at least one cer.cleted audit to be furnished before the source leaves ca. pus. O. List make, model, tag nu-ter, and. ncrship of the vehicle which will be used t transport the conrce frce C' te tha <! cat C :st of the Un:.ted Statec. AN ::e u. ce? nTut.iTY M T: ' F '.1 4 :~:CN M~.* UTI O N ... -.. -. ~. .... ~. -.. -. -..... -...

O O .:t. Glen;.INtphy P rj e 2 ' :y 5, 1983 9. Furnich doceentation to chew that the vehi:le has boon inspected and in in condition to m:ct upplicable ragul<.tions for vehicles hauling hazardcas caterials. Tirts, steering, braking, lights, and crergsacy equipment should specifically he licted. 10. Furnish credentials of tha driver whc will drive the lehicle, indicating that he has had the training and any special license required for this typ: of vehicle. 11. D2aignate the parcon who will be responsible for ensuring that tha quality assurance program and other applicable safety regulations are strictly followed while the radistica source is off ccrpus. 12. Furnich calibration roc;rds for the instrurcnts to ba used to survey the cource and container while off campus. 13. Furnish information on the vessel to ba used in the sedinent survey. !!cadquarte s addresa and the name and phenc nurber of a responsible a. official of the Chroma 11oy Ccrpany who can be contacted for further information. b. Tonnage, type of vessel & type of research routinely carried out by this chip and crew. 14. Furnish' map with proposed route across the United States to the West Ccart. I realice that all of the abcvc informatica cannot be furniched immediately. However, it thould all be in before departure from the Carr>us with the source. Since the University is responsibic for the source while off, as-well-as-en, further information may be required by the Radiation Safety Cctaittee campuo; l. or the Re.diation Safety Officer. Everv effort must be made to ensure that the shipping container, equipment, and l oper$ ting procedures meet the most exacting safety standards, 1 l Sincerely, o$ y.a g k 0 Y t W. 2 Lowell A. !!use l l Radiation Safety Officer Environmental Safety Services i I t Lv.:swc l [ cc: Edward T. Kassinger J. R. Rawacn John Noakes i %}}

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