ML19263A729

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10CFR71 QA Program Implementation Procedures
ML19263A729
Person / Time
Site: 07100215
Issue date: 11/29/1978
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SPACE SCIENCE SERVICES, INC.
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References
NUDOCS 7901020190
Download: ML19263A729 (34)


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4 10CFR71 Quality Assurance Program Implementation Procedures November 29, 1978 7901020190~

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SPACE SCIENCE SERVICES g C

6.

November 29, 1978 10CFR71 Quality Assurance Program Imolementatior. Procedures Index Paragraphs 1.

Records to be maintained.

2.

Manufacturer's Certification.

3.

Handling Storage and Shipping Records.

4.

Inspection Test and Operating Status.

5.

Quality Assurance Records.

6.

Audits.

7.

Receiving, Handling, Storage, and Shipping Instructions.

Attachments 1.

Form 10CFR71-A - Reference paragraph 3.

2.

Form 10CFR71-B - Reference paragraph 4.

3.

Form 10CFR71-C - Reference paragraph 6.

4.

Operating and Emergency Procedures - Reference paragraph 7a.

5.

49 CFR 173.414 - Reference paragraph 7b.

6.

10 CFR, Part 34 - Reference paragraph 7c.

7.

Shipper's Certificate for Radioactive Materials - Reference paragraph 7h.

8.

Internal Inspection System - Reference Attachment 6G.

9.

Overall Organizational Structure - Reference Attachment 6H.

10.

Corporate Officers - Reference Attachment 10.

SPACE SCIENCE SERVICES M

s.

Novembe r 29, 1978 Space Science Services, Inc.'s 10CFR71 Quality Assurance Program Implementation Procedures 1.

Records to be maintained:

Manufacturer's certification for each shipping container.

a.

b.

Handling Storage and Shipping records.

c.

Inspection, Test and Operating Status.

d.

Quality Assurance records.

e.

Audit records.

2.

Manufacturer's Certification:

This section is in the Radioactive Materials License Log Book, for the NRC, State of Florida, and State of Alabama.

3.

Handling Storage and Shipping Records:

The receipts and transfers section of the Space Science Services, Inc.'s Radioactive Materials Record Book will contain these records.

The attached form 10CFR71-A, along with other pertinent shipping and receiving documents will be filed there.

4.

Inspection Test and Operating Status:

The Equipment Maintenance Section of the Space Science Services, Inc. 's Radioactive Materials Record Book will contain these records.

The attached form 10CFR71-B will be filed in this section.

5.

Quality Assurance Records:

In addition to the foregoing records, other records such as operating logs, personnel training and qualifications along with other records stated in Space Science Services, Inc.'s Operating and Emergency Procedures nre maintained in the Radiation Safety File pertaining to personnel training, cer**fication, and radiation history.

SPACE SCIENCE SERVICES

10CFR71 QA Program Implementation Procedures Page 2 November 29, 1978 6.

Audits:

Records of audits of the Quality Assurance program required by 10CFR71 will be maintained and filed in the Radiation Safety File. Form 10CFR71-C will be used.

7.

Receiving, Handling, Storage, and Shipping Instructions:

Upon receipt of a new source, the shipping container is to a.

be surveyed in accordance with Section II, Para. VII E and H of Space Science Services, Inc.'s Operating and Emergency Procedures and inspected for damage.

b.

Verify the container seal is intact and container labeled properly as per 49CFR,Part 173, Para.173.402(8) and 173.414.

c.

Upon removing the source changer from the shipping container, survey it for compliance with 10 CFR, Part 34, Para.'s 34.21, 34.22, and 34.28 attached.

d.

Transfer from source changer to projector and vice versa shall be done in accordance with the manufacturer's instructions as contained in Space Science Services, Inc.'s Operating and Emergency Procedures.

Prior to shipping, survey the source changer for compliance e.

as per Para. C above.

f.

Af ter placing source changer in the shipping container, seal and label as per Para. b above and as per attachment I.

g.

Af ter the shipping container is sealed, labeled, and surveyed, inspect again for damage.

h.

Prepare the shipping documents and particularly the Shipper's Certificate for Radioactive Materials, a copy of which is attached.

1.

Turn in completed form 10CFR71-A or B to Radiation Safety Officer for filing.

SPACE SCIENCE SERVICES M SPACE SCIENCE SERVICES, INC.

Form No. 10CFR71-A Receipt of Radioactive Material Acc.

Rej.

Shipping Container 1.

Seal Affixed...............................

e 2.

Properly Labeled...........................

t 3.

Damaged....................................

3.

Radiation Survey

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i.

Date:

Time:

Surface mr/hr........

One Meter mr/hr........

Source Changer f.-

1.

Locked and functioning.....................

2.

P r op e rly Lab e led...........................

3.

Radiation Survey Surface mr/hr........

Six inches mr/hr........

One Meter mr/hr........

Performed by (Radiographer's Signature)

(

SPACE SCIEh E SERVICES, INC.

Form No. 10CFR71-B Shipping of Radioactive Material Source Changer Acc.

Rej.

1.

Locked and functioning properly............

2.

Properly Laboled...........................

3.

Radiation Survey Surface mr/hr.....

Six Inches mr/hr.....

One Meter mr/hr.....

Shipping Container 1.

Inspect for damage.........................

2.

Properly Labeled...........................

3.

Radiation Survey Surface mr/hr.....

One Meter mr/hr.....

4.

Scaled.....................................

Shipping Documents 1.

Decay Chart 2.

Leak Test..................................

3.

Shipper's Certification....................

4.

Co rre c t Bill of Lading.....................

SPACE SCIENCE SERVICES, INC.

Herndon Airport, Building 180, P.O. Box 20126 Orlando, Florida 32814 QUALITY CONTROL AND RADIATION SAFETY AUDIT CHECK LIST...... FORM NO. 10CFR71-C ACCEPT UNACCEPT I.

Radioactive Sources A.

Records 1.

Receipts and Transfers.....................

2.

Inventory..................................

3.

Decay Charts...............................

4.

Usage Logs.................................

5.

Shipping Container Records.................

B.

Storage 1.

Location...................................

2.

Signs.......................................

3.

Shic1 ding..................................

4.

Keys.......................................

C.

Usage 1.

Signs......................................

2.

Ropes......................................

3.

S'. i c 1 d i n g..................................

4.

Daily Maintenance Check....................

II.

Personnel Monitoring A.

Equipment 1.

Survey Meters - Calibration Date...........

2.

Dos ime te r Ch a rge...........................

3.

Dosimeters.................................

4.

Film Badges and Records....................

B.

Safety Procedures..............................

C.

Required Postings 1.

AEC........................................

2.

S tate Board o f Health......................

3.

0SHA.......................................

Form No. 10CFR71-C Page 2 ACCEPT UNACCEPT III. Quality of Work A.

Radiographic 1.

Film Storage and Handling..................

2.

Record of Chemical Changes / Fila Processed..

3.

Cleanliness of Film Processing Equipment...

4.

Storage of Completed Film..................

5.

Packaging and Reporting....................

6.

Records ard Reports........................

7.

Densitometer Operation and Calibration.....

8.

Penetrameters - Condition of and Quantity..

9.

Lead Numbers - Condition of and Quantity...

10.

Film Holders and Screens...................

11.

Pe rsonnel Certifications...................

12.

Procedure Certifica tions...................

B.

Magnetic Particle 1.

Condition of Equipment *.....................

2.

Calibration of Gages.......................

3.

S to rage o f Ma te rial........................

4.

Magnatometers - available..................

5.

Records and Reports........................

6.

Personnel Certifications...................

7.

Procedure Ce rtifications...................

C.

Penetrant 1.

Material Storage...........................

2.

Material Certification.....................

3.

Personnel Ce rtification....................

4.

Procedure Certification....................

D.

Ultrasonic 1.

Condition of Equipment.....................

2.

Calibration of Blocks......................

3.

Couplant Certifications....................

4.

Pe rsonnel Certifica tions...................

5.

Pro cedure Ce rtifications...................

E.

Eddy Current 1.

Condition of Equipment.....................

2.

Personnel Certifications...................

3.

Procedure Certifications...................

Form No. 10CFR71-C Page 3 ACCEPT UNACCEPT IV.

Specifications A.

Pe r tinen t to p roj e c t...........................

B.

Current including addendums....................

C.

Reference Radiographs if required..............

V.

Evaluation and Remarks.............................

d;[ SPACE SCIENCE SERVICES

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POST OFFICE BOX 20126 e ORLANDO, FLORIDA 32814 e PHONE (305) 8941751 n' !3 O 'a.b!

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Attacliment 4 OPERATING PROCEDURES SECTION II NON. DESTRUCTIVE, METALLURGICAL, PHYSICAL AND CHEMICAL TESTING AND INSPECTION PROGR AMS

/

SPACE SCIENCE SERVICES, INC.

Operating Procedures SECTION II CONTENTS PAGE PART IV.

INSTRUMENT CALIBRATION PROCEDURES 1

V.

SPECIFIC SURVEY INSTRUhENTS TO BE USED 1

VI.

REQUIREFENTS FOR CALIBRATED AND OPERABLE SURVEY INSTRUMENTS 1

VII.

CONDUCTING SURVEYS 1

VIII.

CONTROLS AT EXPOSURE SITES 4

6 IX.

SECURITY X.

PERSONNEL MONITORING - RADIATION MONITORING 6

8 XI.

TRANSPORTATION XII.

EMERGENCIES - KEEP COOL - FOLLOW INSTRUCTIONS - THINK 9

11 XIII.

RECORDS XIV.

CllECK LIST FOR RADIOGRAPilIC OPERATION 12

SPACE SCIENCE SERVICES, INC.

Operating Procedures IV.

INSTRUMENT CALIBRATION PROCEDURES.

Survey meters are to be sent to the following approved sources for calibration:

1.

Southeastern Atomic Laboratories 3520 N. W. 7th Avenue Gainesville, Florida 32601 2.

Meter Manufacturer Meters must be recalibrated within 3 months of the last calibra-tion date in order to be used for surveys required under Federal and State regulations.

V.

SPECIFIC SURVEY INSTRUMENTS TO BE USED.

The following instruments will be used for monitoring and survey-ing gamma radiation:

Eberline Model E120G 0-1000 mr/hr Eberline Model E510G' 0-1000 mr/hr Victorcen Model 492 0-1000 mr/hr Victorcen Model 592B 0-1000 mr/hr V1.

_ REQUIREMENTS FOR CALIBRATED AND OPERABLE SURVEY INSTRUMENTS:

At least one properly calibrated and usable instrument of at least 0 to 1,000 mr/hr capability will be available at each ex-posure site if an exposure is to be made in the field.

No ex-posures shall be made at any time unless this instrument is at the site and is in workable condition. After each radiographic exposure the survay instrument shall be used to positively de-termine that scaled sources have been returned to their shicided positions.

VII.

CONDUCTING SURVEYS.

A.

Levels at perimeter of restricted areas.

1

9 SPACE SCIENCE SERVICES, INC.

f Operating Procedures VII.

CONDUCTING SURVEYC (CONT.)

Post "High Radiation Areas" with signs reading " Caution High Radiation Area."

If time factors are not considered, such posting vill apply to the area bounded by the 100 mr/hr iso-l dose line.

The following is an example of the ef fect of time factors:

If the total exposure time in any one hour is 6 min-utes (1/10th of that hour) the high radiation area may be post-ed at the 1,000 mr/hr isodose line since 0.1 hr X 1,000 mr/hr equals 100 mr.

" Radiation Areas" post with signs reading " Caution Radiation Area."

Since the limits for a radiation area are 5 mr in 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> and 100 mr in 1 week, posting at the 5 mr/hr isodose line will result in compliance with Part 20 if not more than 20 hours2.314815e-4 days <br />0.00556 hours <br />3.306878e-5 weeks <br />7.61e-6 months <br /> of exposure are made in 1 weel at one location (5 mr/hr X 20 hr/wk equals 100 mr/wk).

Radiation levels #. unrestricted areas are to be lisited such that a person '- 2n unrestricted area may not receive a dose of more than 2 in 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> or 100 mrem in seven consecutive days.

Restriction

-6ns, barricades, surveillance) of a radiography area at the 2 mr/hr isodose line will assure compliance with the 100 mrem per week limit if the exposure time in 1 week is less than 50 hours5.787037e-4 days <br />0.0139 hours <br />8.267196e-5 weeks <br />1.9025e-5 months <br />.

If the restricted area will be such that the radiation level anywhere at its perimeter will exceed 2 mr/hr, it will be necessary to limit exposure time in each hour such that a dose of 2 mrem may not be exceeded in one hour.

The 50-hour limit on total exposure time in 1 week at a singic lo-cation, will, of course, still apply.

It may be seen from the preceding that posting at three differ-ent, successive perimeters may be appropriate.

The innermost perimeter being the perimeter of the "High Radiation Area," the next perimeter being the perimeter of the " Radiation Area," and the third perimeter beir.g the perimeter of the radiographic area separating the restrictad area from the unrestricted area.

Post-ing of the first two pt imeters is required.

Posting of the third perimeter, although not required, is highly desirable as an aid to controlling access to the restricted radiographic area and instructions for doing so should be included in your operat-ing procedures.

2

SPACE SCIENCE SERVICES, INC.

Operating Procedures VII.

CONDUCTING SURVEYS (CONT.)

The use of " Caution Radiation Area" signs at the perimeter of the restricted radiographic area is acceptable.

Such signs then accomplish the double purpose of warning individuals of the ex-istence of a " Radiation Area" and helping the radiographer and his assistant in controlling access to the restricted radio-graphic area.

The use of " Caution High Radiation Area" signs at the perimeter of the restricted radiographic area is not ac-ceptable_.

Therefore, as a minimum, two perimeters should be posted, that is, the perimeter of the "High Radiation Area" and the perimeter of the restricted radiography area.

B.

Levels Outside of Permanent Facilities.

At the present time Space Science Services has no permanent radiographic facilities (exposure rooms) for gamma radio-graphy.

C.

Survey After Each Exposure.

After each exposure and source has been returned to the stor-age position, the exposure device must be surveyed to insure that the source is in fact completely withdrawn into the stor-age position. Particularly, survey the source guide tube.

CAUTION:

Survey both front and rear ends of the exposure device.

If the source is not in the full storage position, this condi-tion may not be detected if only the rear part of the expos-ure device is surveyed.

D.

Survey Before Securing De.vice.

Before securing the exposure device, survey to make sure the source is locked in the full storage position.

E.

Survey Surface Levels on Devices and Containers.

After the source has secured in the exposure device or ship-ping container, survey to see if there is radiation in excess of 200 mr/hr on the surface, or radiation in excess of 10 mr/hr at a distance of 3 feet from the external surface.

3 - Revision I

SPACE SCIENCE SERVICES, INC.

Operating

'ncedures VII.

CONDUCTING SURVEYS (CONT.)

F.

Survey Surface Levels on Vehicles.

\\

After an exposure device or shipping container has been placed inside a vehicle for trarsportation, the exterior, and the passenger compartment of the vehicle must be surveyed to insure that there is no radiation in excess of 2 mr/hr.

G.

Survey at Scene of Emergar.ey.

In case of emergency, immediately survey, establish a 2 mr/hr perimeter, and post signs, Patrol the area.

H.

Upon receipt of a new source, within 3 hours3.472222e-5 days <br />8.333333e-4 hours <br />4.960317e-6 weeks <br />1.1415e-6 months <br /> during nor-mal working hours, or within 18 hours2.083333e-4 days <br />0.005 hours <br />2.97619e-5 weeks <br />6.849e-6 months <br /> after normal working hours, a survey of the device or container must be made in accordance with paragraph E above.

The readings will be recorded on the shipping ticket ac-companying the source.

VIII.

CONTROLS AT EXPOSURE SITES.

Post "High Radiation Areas" with signs reading " Caution High Radiation Area."

If time facters are not considered, such post-ing will apply to the area bounded by the 100 mr/hr isoiose line.

The following is an example of the effect of time factors:

If the total exposure time in any one hour is 6 minutes (1/10th of that hour) the high radiation area may be posted at the 1,000 mr/hr isodose line since 0.1 hr X 1,000 mr/hr equals 100 mr.

Radiation Areas post with signs reading " Caution Radiation Area".

Since the limits for a radiation area are 5 mr in 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> and 100 mr in 1 week, position at the 5 mr/hr isodose line will result in compliance with Part 20 if.not more than 20 hours2.314815e-4 days <br />0.00556 hours <br />3.306878e-5 weeks <br />7.61e-6 months <br /> of exposure are made in 1 week at one location (5 mr/

hr X 20 hr/wk equals 100 mr/wk).

Radiation levels in unrestricted areas are to be limited such O

4

St..CE SCIENCE SERVICES, INC.

Operating Procedures VIII.

CONTROLS AT EXPOSURE SITES.

(CONT.)

. hat a person in an unrestricted area may not receive a dose of more than 2 mrem in 1 hour1.157407e-5 days <br />2.777778e-4 hours <br />1.653439e-6 weeks <br />3.805e-7 months <br /> or 100 mrem in seven consecutive days.

Restriction (signs, barricades, surveillance) of a radiography area at the 2 mr/hr isodose line will assure compliance with the 100 mrem per week limit if the exposure time in 1 week is less than 50 hours5.787037e-4 days <br />0.0139 hours <br />8.267196e-5 weeks <br />1.9025e-5 months <br />.

If the restricted area will be such that the radiation level anywhere at its perimeter will exceed 2 mr/

hr, it will be necessary to limit exposure time in each hour such tnat a dose of 2 mrem may not be exceeded in one hour.

The 50-hour limit on total exposure time in 1 week at a single lo-cation, will, of course, still apply.

It may be seen from the preceding that posting at three diffetant, successive perimeters ma r be appropriate.

The innermost peri-meter being the perir.t r of the "High Radiation Area," the next perimeter being the te imeter of the " Radiation Aren," and the third perimeter bein< the perimeter of the radiographic area sep-arating the restrict d area from the unrestricted area.

Posting of the first two pc-imeters is required.

Posting of the third perimeter, although not required, is highly desirable as an aid to controlling access to the restricted radiographic area and in-structions for doing so should be included in your opercting pro-cedures.

The use of " Caution Radiation Area" signs at the crimeter of the restricted radiographic area is acceptable.

Such signs then ac-complish the double purpose of warning individuals of the exist-ence of a " Radiation Area" and helping the radiographer and his assistant'in controlling access to the restricted radiographic area. The use of " Caution High Radiation Area" signs at the per-imeter of the restricte6.;diographic area is not acceptable.

Therefore, as a minimum, two perimeters should be posted, that is, the perimeter of the "High Radiation Area" and the perimeter of the restricted radiogrrphy area.

Rope or other suitab1r. barricades shall be used to define the per-imeters of the "Radf'. tion Areas."

Under no circumstances is a " Radiation Area" to be left unattended.

5

SPACE SCIENCE SERVICES, INC.

Operating Procedures IX.

SECURITY.

At all times, except during radiographic, storage containers and exposure devices are to be locked.

Storage rocms and vehicles must be locked when left unattended and plainly posted with " Caution Radioac tive Material" signs.

Under special circumstances, when an expcsure device mus: be left for a short period of time on a tower or similar sr.cel structure, it must be chained and locked to a structurtl mem-ber and properly posted with " Caution Radioactive Material" signs.

X.

PERSONNEL FONITs R"!O - RADIATION MONITORING.

A.

Personnel Monitoring 1.

Dosimeters and film badges must be worn at all times by radiographic personnel during radiographic operations.

Dosimeters must cover a range of 0 to 200 mr/hr.

2.

Dosimeters and film badges should be worn by the person where he is likely to receive the most radiation.

For example:

If a radiographer were to receive most of the radiation on his legs then he would wear the dosimeter and film badge low on a pocket.

3.

Operating instructions for dosimeters and dosimeter charg-ers are outlined in Paragraph 12 of these procedures.

4.

Film badge schedule provides a change of film on a monthly basis.

During this period, badges are not to be inter-changed with other employees.

5.

Since most radiographers work away from the home office, each radiographer is held responsibic for his own charg-ing and reading of his dosimeter, and. recording of the daily dose on the weekly report.

6.

Dosimeters are to be read as o(ten as necessary to deter-mine if an abnorms dose of radiation has been received.

If a dosimeter is found to be off-scale, an emergency sit-uation shall be considered to exist and the corresponding 6

SPACE SCIENCE SERVICES, INC.

Operating Procedures i

X.

PERSONNEL MONITORING - RADIATION MONITORING. (CONT.)

film badge must be immediately returned to the supplier h

for processing, i

j 7.

Radiographic personnel shall be removed from exposure to radiation when necessary to keep their individual dosages from exceeding the maximum amounts prescribed by Federal and State laws.

B.

Operating Instructions for Pocket Dosimeters and Chargers.

1.

Dosimeters a.

All radiographers and radiographer's assistants shall wear a pocket dosimeter at all times during working hours.

b.

Pocket dosimeters measure the amount of gamma and x-ray radiation received, c.

Dosimeters are delicate instruments and should be treated as such. Jarring or dropping the instru-ment may cause a high reading.

If damage to your dosimeter is suspected,. notify your supervisor im-mediately, d.

If a dosimeter should go off-scale (over 200 mr),

stop work and notify your supervisor or the Radia-tion P atection Officer immediately.

i e.

Section 34.33 (b) of CFR Part 34, requires that if a dosimeter becomes fully discharged, the film badge shall be processed immediately to determine if any over-exposure has taken place. Such a film badge must be sent to the home office and from there it w'll be sent to the film badge supplier for immediate processing. Having followed this procedure, immediately recharge the dosimeter and leave in an area which is free of any type of radiation for a period of approximately one hour. After this time lapse, recheck the dosimeter.

If it is again dis-charged, tot &lly or partially, in all probability 7 (Rev. 9/76) e

SPACE SCIENCE SERVICES, INC.

Operating Procedures X.

PERSONNEL MONITORING - RADIATION MONITORING (CONT.)

you have not been exposed to an overdose of radia-tion.

This would indicate that the dosimeter is probably faulty. Having determined this, inform your supervisor. Only the Radiation Protection Offi-cer may decide whether or not you may return to ra-diation work after he has carefully evaluated the situation.

f.

The radiographer shall read the dosimeter at the end of each day ano shall record these daily readings on the weekly report.

2.

Dosimeter Chargers Insert dosimeter into charging socket.

a.

b.

Held dosimeter in contact (pressure required against spring).

c.

Turn large knob to adjust dosimeter to zero, d.

Remove dosimeter from charger and check hairline pos-ition by looking through dosimetr it the source of light.

Batteries should be checked occasionally and spares e.

available.

XI.

TRANSPORTATION.

A.

Unless spe tal permission is given, by the Radiation Protection

Officer, aly company owned or leased vehicles are permitted to carry radioactive materials.

B.

Storage containers and projectors carried in vehicles should be placed as far away from passengers as possible, making sure no overexposure results.

All vehicles carrying Radioactive Yellow III labeledmaterials in C.

storage containers or projectors will be clearly posted with " Caution-Radioactive Material" signs, as well as all 4 sides of the vehicle placarded with DOT approved " Radioactive" signs.

It is not re-quired to placard vehicles carrying Radioactive Yellow II and White I labeled materials as long as the containers or projectors are labeled in accordance with existing regulations.

8 (Rev. 9/76)

SPACE SCIENCE SERVICES, INC.

Operating Procedures XI.

TRANSPORTATION. (CONT.)

D.

Vehicles containing radioactive materials will be locked when left unattended.

E.

When it is necessary to remain overnight, the storage con-tainer or projector should be lef t locked in the vehicle only as the last resort.

Place the container in a lock-ed room or chain and lock it at the job site if possible.

" Caution - Radioactive Material" signs and radiation area signs will be posted as appropriate.

XII.

EMERGENCIES - KEEP COOL - FOLLOW INSTRUCTIONS - THINK.

A.

An emergency is any situation in which there is physical An danger to human life from overexposure to radiation.

emergency condition may exist because of damage to a radioactive material container, disconnected and/or lost radiation " pigtail," or impending danger because of fire or some natural disturbance.

B.

The radiographer in charge shall admit only duly author-ized representatives of government or industry inside the radiation area at the scene of an emergency, sud then only if they have personnel monitoring equipment.

C.

A 2 mr limit boundary shall be established using ropes, tape, lumber, etc. as a barricade.

D.

The radiographer will nonitor and maintain direct surveil-lance of the emergency area until relieved by duly author-ized personnel, either governmental or company.

E.

In the case of damage to the container or loose source, the radiation area should be reduced to as small an area as pos-sible using shielding materials such as lead, steel, concrete blocks, or sand bags.

In case of fire or severe weather, during radiography, re-turn the source to the storage position and lock. Call the 9

SPACE SCIENCE SERVICES, INC.

Operating Procedures XII.

EMERGENCIES - KEEP COOL - FOLLOW INSTRUCTIONS - THINK (CCNT) proper authorities and report the fire or severe weather.

If possible thke the storage container with you when making the phone call, otherwise return and remove the material from the danger area, if it is still possible.

F.

Aft'er the basic steps as outlined above have been taken no-tify the following in this order:-

Donald A Geiger 2926 Parkland Court Orlando, Florida 32814 Telephone:

305 645-0850 home 305 894-1751 office David A. Geiger 1606 Squire Court i

Dothan, Alabama 36301 Telephone:

205 792-4704 home 205 983-4531 office i

G.

If additional help is required, call the local sheriff's office or state highway patrol.

H.

In the event of a vdhicular accident while transport-ing radioactive material.

Check the material ontainer simultaneously visually and with a survey meter zor dam-age or-leakage.

If the meter -is damaged substitute a dosimeter.

If the container-is damaged, and your survey meter and __

dosimeter have been damaged so -that -there is no. way to ascertain of the capsule has been damaged, calculate and -

rope off the 2 fur level and wait for a proper survey me-ter to arrive before. moving the conatiner.

10 (Rev. 9/76)

SPACE SCIENCE SERVICES, INC.

Operating Procedures XIII.

RECORDS.

A.

The original or a copy of all instrument calibrations will be maintained in a loose leaf record book at the Orlando, Florida home office.

B.

The original or a copy of all leak test results will be maintained in the loose Icaf " Radioactive Materials" book at the Orlando, Florida home office.

C.

The requirements for maintenance of a " Utilization Log" are met by two forms t aquired to be filled out each day and/or each time a radiographer uses a sealed source. The forms are the " Daily Time Sheet" and the " Daily Mainte-nancc Check and ' Area Survey" form.

The " Daily Time Sheet" has a space for the Make and Model of the exposure device, the identity of the radiographer, and the location and date of use.

The " Daily Maintenance Check and Area Survey" form provides the same information.

All forms are to be sent in each week for filing at the home office at Orlando, Florida.

D.

An inventory will be made quarterly of all radioactive material.

This inventory will include for each sealed source used for radiography the following information:

1.

Isotope 2.

Strength in curies.

3.

Serial number of exposure device containing it.

4.

Physical locatien by City and State.

5.

Surface reading and reading at one meter.

6.

Date of the inventory.

E.

Records of the following surveys will be kept:

1.

The area survey of radiation levels in unrestrict-ed areas is to be recorded on the " Daily Mainte-nance Check and Area Survey" form.

Thi; #crm is 11

SPACE SCIENCE SERVICES, INC.

Operating Procedures XIII.

RECORDS (CONT.)

to be sent in weekly to the Orlando, Florida home office for filing.

2.

The survey made when securing each exposure device and storage container is to be recorded on the

" Daily Time Sheet" and sent in weekly to the Orlando, Florida home office for filing.

3.

Surveys made when receiving and shipping radioactive materials in accordance with para. VII H, are to be sent to the Orlando, Florida home office and filed in the loose leaf " Radioactive Materials" book.

F.

Personnel monitoring records include the daily dosimeter report and the monthly film badge report.

1.

The " Daily Time Sheet" includes the information required for the daily dosimeter report.

The time sheet is to be sent in weekly to the Orlando, Florida home office and filed.

2.

The monthly film badge record is to be received at the Orlando, Florida home offic;,and filed.

G.

All training records of personnel shall be maintained in a separate file at Orlando, Florida. All copies of training records and certifications will be sent here.

XIV.

CHECKLIST FOR RADIOGRAPHIC OPERATION A.

Set-Up of Area Prior to Radiography 1.

Wear film badge and pocket dosimeters.

2.

Determine that survey meter is operable.

3.

Survey device to determine that the source is in the shielded position before removing from the vehicle.

Remove equipment from the vehicle, perform the " daily maintenance" check, and complete the form.

4.

Place RADIATION AREA signs to outline restricted area at the 2 mr/hr level, and HIGH RADIATION AREA signs to outline the 100 mr/hr level.

12

SPACE SCIENCE SERVICES, INC.

Operating Procedures XIV.

CHECKLIST FOR RADIOGRAPHIC OPERATION (CONT.)

5.

Place device within restricted area and check with survey meter.

6.

Place film'.

7.

Unlock device, locate control cable and source guide cable to take advantage of shielding and distance.

8.

Check source Position indicator.

9.

Notify workers that radiography is to be performed.

B.

Conduct of Radiography 1.

Keep area under constant surveillance.

2.

Manipulate device to expose source.

3.

Verify source position with survey meter.

4.

Survey restricted area boundaries and adjust signs if higher than 2 mr/hr.

5.

Return source to shicided position and verify with survey meter and position indicator.

P.articularly, survey the source guide tube.

6.

Remove or replace film.

C.

Actions Upon Completion of Radiographic Job 1.

Remove cables, and lock device.

2.

Place device in vehicle, and check with survey meter to make sure source is in shielded position.

3.

Record security survey if source is to be kept in vehicle, if not, when put in storage.

4.

Remove signs and place in vehicle.

5.

Lock vehicle.

6.

Notify workers that radiography is completed.

7.

Record pocket dosimeter readings at end of day, and record job location survey.

13 - Revision I

Attachrnent 5 The proper selection of a label depends on the Transportation Index '

and the radiation level at the surface of the package. In the case of fissile Class ll material, the T.I. is set forth in the regulations. For non fissile shipments, the T.I. is a measure of the penetrating radiation (X-rays,y rays and neutrons) emanating from the packages. The T.I.

number is the highest radiation dose rate in millirem per hour at 3 feet from any accessible external surface of the package. Values shall be expressed to the nearest higher tenth (i.e.1.01 would become 1.1 on the label).

Which labels should you use?

' Labels and their use are discussed in Paragraph 173.414. See Chart 7.

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PART 34-LICENSES FOR RADIOGRAPilY AND RADIATION SAFETY. ETC.

months. In the absence of a certJficate (b) The Jdentity of the radiographer Subport B-Rudiation Safely from a transferor that a test has been to whom assigned; and p IU;* *"I' made within the 6 months prior to the (c) The plant or site where used and transfer, the scaled source shall not be dates of use, Equirr4 EHr CONT Ro!,

put lnto use until tested.

6 34.21 I.fmita on iciels of railiatton for (c) The leak test shall be capable of, 6 34.28 Inspection and mainicnance of radiogr.pfile, ex pomre <fencee mod railiographic exposure elewicce and detecting the presence of 0.005 micro-aiorage soutaincra.

curle of removable contamination on the a

storage containers..

Radiographic exposure dev!ces meas

  • sealed source. An acceptable Icak test - The licensee shall cenduct a program using less than four (4) Inches from the for scaled sources In the possess!on of a f for inspection and meintenance of radio-sealed source storage position to any ex-radlography !!censee would be to test. graphic exposure devices and storage conta!ners to assure proper functioning testor surf ace of the device shall have no at the nearest accessible point to the a

radiation 1cvel in excess of 50 rnllit*

scaled source storage posttion, or other {gf components impoitant to safety

  • s ocntgens per hour at s!x (8) inches frotn appropriate measuring point, by a pro-any exterior surface of the device. -

cedure to be approved pursuant to j 34.11 PrnsoNAt. RAmte Dren Rhma t-Radiographic exposure dev!ces measur-(f). Records of leak test results sha!!

Ing a mtn! mum of four (4) Inches from be kept in units of microcuries and main.

aAs ntas,oa RAD 10cRAPHERs AND mNrs r AssisrANrS the sealed cource storage positton to any tained for inspection by the Commission. =8 exterior surface of the device, and all '

(d) Any test conducted pursuant to 5 34.31 r.rmiimiton -

storage contatners for scaled sources or paragraphs (b) and (c) of this section g (a) e I!censee shall not penn!t any which reveals the presence of 0.005 act as a rad! grapher untQ for rad!ographic exposure dev!ces, shall have no radiation level in excess of 200 mtcrocurie or more of removable radio a Pers n t mt!!! roentgens per hour at any exterior active material shall be considered ev! n such person.flas been Instructed in the sutv (1) surface, and teh (10) milltroentgens per dence that the scaled source is leaking.

jects out!!ryed in Appendix A of this part hour at one meter fmm any exterior sur-The licensee shall immed!ately w Ithdraw and shall have demonstrated under-face.

  • he rad!atton levels spec! fled are the equipment involved from use and

. standing thereof; with th(e scaled source in the shieldest shall cause it to be decontam!nated and (i.e., "off") position.

repaired or to be disposed of,In accord-f (2) IIas received copfes of and instruc-23nce with Commission regulations. A 2 tion in the regulations contained in this g3L22 focfdng of radiograpnic c r.

posure desices and storage contain, report shall be filed, wit 1dn 5 days of the a part and in the applicable sections of test, with the. Director of Licensing,*

N Part.s 19 and 20 of th!s chapter AEC US. At m!c Energy e !! cense (s), and the licensee's operating crs.

Each radiographic exposure destce Commission, Washington, D.C.,

20545 and emerger.cy procedures, and shall shall be provided with a locit or outer describ!ng the (quipment involved, the "l have demonstrated understanding there-locked container des!gned to prevent un-test results, and the corrective action authortred or acc' dental removal or ex-taken. A copy of such report shall be t,of; and posure of a scaled cource and shall be sent to the Director of the appropriate (3) Itas demon'strated competence to kept locked at au ttmes except when

^t *%

"**# h"*I^00 use the radiographic exposure devices, under the direct Eurveillance of a rad!-

Regulatory Opnatmns Reg.mnal Office

  • scaled sources related handling tools e ographer or radiographer's asstatant. or listed in Appendix D and survey instruments which will be

" as may be otherwise authorized pursuant g employed in his ass!gnment.

" to 13 411. Each storage conta!ner Itke-g of Part 20 of this chapter

  • Standards for Protection Agalnst Radiation."

(b) The licensee shall not permit any I wise shall be provided with a lock and o kept locked when containing scaled a fe) A sealed source which is not fas-person to act as a radiographer's assist-g

" sources except when the container is y tened to or contained in a radio-ant until such personi graph!c exposure device shall have per-(1) Itas received coples of and Instruc-under the direct surveillance of a radi.

manently attached to it a durable tag at tions in the !!censee's operating and

~

ographer or indipgrapher's assistant, least one (1) Inch square bearing the pre-ernergency procedurm. and shall have scribed radtation cautton symbolin con-demonstrated understanding thereof;

$ 34.23 Storage precaut.io n Ircked radlographic exposure devices ventional colors, magenta or purple ort and and storage containers shat! be phyalcally a yellow background, and at least the $

(2) Itas demonstrated competence to secured to prevent tampering or remova]

Instructions: " Danger-Itadioactive Ma-E use under the personal supervis!on of the' terial-Do Not IIandle-Notify Civil Au* c radlographer the radlograph!c expmure' by unauthortzed personnel.

thorit!csif Found."

devices, scaled sources, related handlingi

$ 31.24 itadiation sursey in iruments, n tools and rad!ation survey instrumentat

$ 31.26 QusHerly insentory.

which will be employed in his assign $

ne !!censee shan maintain sufficient Each !!censee shah conduct a quarterly ment.

callbrated and operable radiation sur-physical Inventory to account for au vey Instruments to make physical radia-tlon surveys as required by this part and scaled sources received and possessed

$ 34.32 Operating and emergency pro 4

Part 20 of this chapter. Each radiation under his !! cense. De records of the ced ures.

inventories shall be maintained for in.

J survey Instrument shah be calibrated at spection'by the Commission. and shall se y pr es si an inc ude nstr c 1 fntervals not to exceed three (3) months include the quantitles and kinds of by-at least the following*

tions in,Ite handling and use'of licensel and after each instrument serv!cIng and a record maintained of the latest date of product material, location of s.ealed g,)

I calibratfort Instrumen'ation required apprces, and the date of the inventory.

sealed sources and radiographic expod sure devices to be employed such that nt by this section sha!! ! ave a range such 27 IJtilization logs.

person is Ukcly to be exposed to radla '

that two rnlH! roentgens per hour through Each Ilcensee shan rnalntain current tion doses in excess of the 11mits estab-one roentgen per bour can be measured.

gs, which shan be kept avanable for

]!shed in Part 20 of this chapter "Str nd-

$ 34.25 Isak te tin re a'

f Prom!on Against Radladon7 ope nin g, modification en I rey ce add spec fled in I!ce e, sho -

ment of cated sources.

Ing for each scaled source the following fa) The replacement of any sealed Information:

source f astened to or contained in a radt-(a) A description (or make and model number) of the radiographic exposure ographic exposure device and Icak test-device or storage container in which the Ing, repair, tagging. opening or any other modification of any scaled source scaled source is located; shall be performed only by persons spe-cifically authorized by the Commission to do so.

(b) Each scaled source shall be tested

. Amended by 38 FR 12h1.

for leakage at intervals not to exceed 6 124 August 31,1973

PART 9 - SHIPPING DOCUMENTS (Continued) for Radioactive Materials 3.

Special Form of Shipper's Certificate SHIPPER'S CERTIFICATION FOR RADIOACTIVE MATERIALS (to be completed in duplicate) the contents of this consignment are properly described by This is to certify that name and are packed, marked and labelled and are in proper' condition for carriage applicable carrier and governmental regulations.

(For by air according to al' international shipmen'cs add "and to the IATA Restricted Articles Regulations".)

(cross This consignment is within the limitations prescribed for passenger / cargo out one) carrying aircraft.

Name and address of Shipper or his authorized agent.................................

Date.............................

(Signature) following information may be included here for each package of the consignment:

The if not, it must be given in other shipping documents.

PACKAGE NATURE AND QUANTITY OF CONTENT RADIONUCLIDE GROUP FORM ACTIVITY CATEGORY PPANSPORT TYPE INDEX NAME OF PRINCIPAL GROUP EITHER CHEMICAL NUMBER OF I WHITE FOR INDUSTRIAL RADIOACTIVE NUMBERS OF FORM PLUS GAS /

CURIES OR OR FELLOW OR CONTENT GROUPS LIQUID / SOLID MILLI-II YELLOW LABEL TYPE A I TO VII OR SPECIAL FOR.

CURIES OR CATEGORY OR OR SPECIAL AS III YELLOW ONLY TYPE B ENCAPSULATION SPECIFIED LABEL I ridi um - 192 II I Special Forin Yellow Type B ADDITIONAL INFORMATION REQUIRED FOR FISSILE MATERIALS ONLY NOT EXEMPTED EXEMPTED FROM THE ADDITIONAL REQUIREMENTS FOR FISSILE MATERI ALS FISSILE CLASS I E7 FISSILE CLASS II D

FISSILE CLASS III Q NAMES, PLUS QUANTITY IN GRAMS, OR CONCENTRATION OR ENRICHMENT IN U235 Additional certificates obtaEned by the shipper when necessary:

Special Form Encapsulation Certificate (s)

[]

[3 Type "B" Packaging Certificate (s)

[3 Certi ficate ( s) for Fissile Material Certificate (s) for Large Radioactive Source

[3

[3 Government Approvals / Permits For explanation of abbreviations and ref erence marks used but unexplained herein, EFFECTIVE May 30, 196{

see Pages 9 and 10 ISSUED April 30, 1969

POST OFFICE BOX 20126 e ORLANDO, FLORIDA 32814 e PHONE (305) 894-1751 "1110 m

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UJu.S.I.

a INTERNAL INSPECTION SYSTEM ATTACHMENT 6G OVERALL ORGANIZATIONAL STRUCTURE ATTACHMENT 6H CORPORATE OFFICERS ATTACHMENT 10 T AMP A - Post Of f ne Box 1386, Gibsonton F L 33534 /(813) 677-1555 P.O. Som 40031, 2753 Rosselle St.,' Jacksonville F L 32203/(904) 388 0488 NON-DESTRUCTIVE, METALLURGICAL, PHYSIC AL AND CHEMICAL TESTING AND INSPECTION PROGR AMS

f I

SPACE SCIENCE SERVICES, INC.

ATTACllMENT 6G INTERNAL INSPECTION SYSTEM.

A.

Scope.

The following items will be of primary interest:

1.

Proper posting of notices.

2.

Records.

3.

Personnel exposure.

4.

Exposure devices and monitoring equipaent.

5.

Caution signs and barricade materials.

6.

Storage of radioactive material and security of same.

7.

Radiographers - possession of operating and emergency pro-cedures.

B.

Frequency.

All sites where radiography is being performed on a permanent or semi-permanent basis will be inspected at Icast once every two months.

C.

Personnel Conducting Inspections.

1.

All inspections will be conducted by the Radiation Protection Officer or his assistants.

2.

Qualifications.

For the qualifications of the Radiation Protection Officer and his assist' ants see organizational structure.

2.

Management inspection of operations.

Since the president and vice president of Space Science Services,'Inc. are the Radiation Protection Officer and Ass-6 istant Radiation Protection Officers for Alabama respectfully, management review and inspection will be done apart from the regular inspection and at least once a year.

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MAO J

JAMES H. GEIGER Level of Certification - SNT II Eddy Current, Magnetic Particle, Penetrant, Radiographic, Ultrasonic Educational Background and Experience

- Space Science Services, Inc.

1967 to present

- Safe-Handling of Radioactive Isotopes, Southeastern Atomic Laboratories

- Or.!ando Junior College 1 year

- Palm Beach Junior College 1/2 year

- George C. Wallace Junior College (Associate in Arts Degree, A. A.)

1 year

- Troy State University (Major - Business Administration, Management Emphasis) 2 years

SPACE SCIENCE SERVICES, INC.

DUTIES OF RADIATION PROTECTION OFFICER 1.

Serve as the, licensee's liaison officer with the Atomic Energy Commission on license matters.

2.

Maintain control,of procurcment and disposal of licensed byproduct material.

3.

Develop and maintain up-to-date operating and emergency procedures.

4.

Establish and maintain a personnel monitoring pror, ram.

5.

Procure and maintain radiation survey instruments.

6.

Establish and conduct the training program for radiographers' assistants.

7.

Examine and determine competency of radiographic personnel.

8.

Establish and maintain storage facilities.

9.

Maintain exposure devices, radiography facilities, and associated equipment.

10.

Establish and maintain the leak testing program.

11.

Establish and maintain the internal inspection system.

12.

Perform source replacement and source tagging operations.

13.

Conduct quarterly inventories and maintain utilization logs.

14.

Establish and conduct a survey instrument calibration program.

15.

Establish and maintain the licensee's record keeping system.

16.

Review aEd insure maintenance of those records not kept by himself.

17.

Assume control and institute corrective action in emergency situations.

18.

Investigate cause of incidents and determine necessary pre-ventive action.

19.

Act in advisory capacity to licensee's management and radio-graphy personnel.

4

f SPACE SCIENCE SERVICES, INC.

i DUTIES OF ASSISTANT RADIATION PROTECTION OFFICERS 1.

To assist the Radiation Protection Officer in the performance of his duties as listed above, particularly in their geogra-phic areas.

2.

Maintain a constant watch to insure that Space Science Services, Inc. operating procedures are followed in the areas under their

/

jurisdiction.

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SPACE SCIENCE SERVICES, INC.

ATTACHMENT 10 a.

Donald A. Geiger 2926 Parkl'.nd Court Orlando, Florida 100% of stock b.

PRESIDENT Donald A. Geiger 2926 Parkland Court Orlando, Florida VICE PRESIDENT David A. Geiger 1606 Squire Court Dothan, Alabama SECRETARY-TREASURER James H. Geiger 1410 W. Duval Street Lantana, Florida