Text

Plant Chemistry Procedure 1800.4:chemistry Inventory
	ML19224B427
Person / Time
Site:	Crane
Issue date:	09/17/1975
From:	; Metropolitan Edison Co
To:	Mullinix W; NRC/IE
References
	1800.4, TM-0182, TM-182, NUDOCS 7906150088
	Download: ML19224B427 (19)
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DOCUMENT NO:__

0F DOCUMENT l'ROVIDED BY COPY MADE ON f

h liETROPOLITAN EDISON COMPANY.

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Wilda R. Mullinix, NRC 6

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204 048 O

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09/17/75 THREE MILE ISLAND NUCLE AR STATION C0i\\ l 0'__EJ C03Y PLANT CHEMISTRY PROCEDURE 1800.4 STATION VMT8 m3Y

.,f CHEMISTRY INVENTORY 4

Table of Ef fective Pages DO NOT REMOV Page Date Revision Pm Date Revision Pg Date Rev n

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', Unit 1 Staff Recommends Approval Unit 2 Staff Recommends Approval Datc9/ /75 Dateq!k#,/75Approval t

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PLANT CHEMISTRY PROCEDURE CHEMISTRY INVENTORY 1.0 PU RPOSE The intention of this inventory system is to insure that ne ce ssa ry chemical supplies are maintained in the Chemistry Laboratory to support the sampling and analysis schedule as set forth in Plant Chemistry Procedure 1990.2.

2.0 DISCUSSION 2.1 Each week (preferably on Monday) a Rad Chem Tech /Jr. will -

refer to the inventory schedule (Figure 1800.4-1) and from this schedule determine which inventory categories are - _ _ _. _.. - _

required that week. This inventory schedule is also incor-porated in the master chemistry scheduling program. The program will print out the appropriate inventory when it is due in accordance with the inventory schedule. -

j' 2.2 At least one inventory category (condensed inventory) is q

d required weekly. Other quarterly inventories may also be due.

2.3 Refer to the appropriate section for specific directions on required inventories.

. _. J. _

I 2.4 Log inventory completion in the Chemistry Log Book.

2.5 Forward the completed inventory and purchase requisitions to a Chemistry Foreman / Supervisor.

S 3.0 REYERENCES 4lI 3.1 Plant Chemistry Procedures

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204 050 1.o

09/17/75 1800.4 Revision 0 4

4 4.0 EQUIPMENT 4.1 None 5.0 PROCEDURE 5.1 Condensed Inventory 5.1.1 Each Monday a Rad. Chem. Tech /Jr. shall perform an inventory using the " Condensed Inventory Order Form (Form 1800.4-1).

5.1.2 The Condensed Inventory is comprised primarily of essential reagents and solvents needed for analysis of Reactor Coolant, Feedwater and Steam Generator Samp1_es._

5.1.3 The Rad. Chem. Tech /Jr. performing the inventory 1,

should do the following:

5.1.3.1 Log the quantity of each chemical on hand and compare this with the " Minimum Quantity" for that chemical.

5.1.3.2 If the quantity on hand does not exceed the

" Minimum Quantity" the Item and the Quantity under "GPU Systems Laboratory Supply" column

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should be circled.

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5.1.3.3 Forward the completed inventory to a chemistry Foreman / Supervisor for approval and transmittal to GPU System La,boratory, 4h~

t 5.1.3.4 Make note of the completed inventory in the i

204 051 2.0

09/17/75 1800.4 Revision 0 4.

Chemistry Record Book.

5.1.3.5 other items not listed on the form can be ordered 4

by writing them on the reverse side of the f o rm.

5.1.3.6 More than one form may be completed during a week.

5.2 General Chemistry Inventory will be completed quarterly (i.e.

during September, December, March cnd June) in the following marner:

5.2.1 Using Form 1800.4-2, log the quantity of each chemical on hand in the primary and secondary laboratory.

5.2.2 Record these quantities in the column marked " Comments".

5.2.3 Add the name of any chemical presently stocked in the laboratory that is not mentioned in the inventory.

L 5.2.4 Compare the quantity of each chemical on hand with the I

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corresponding minimum quantity.

v 5.2.5 If necessary, order. new supply of the chemical by preparing a Purchase Requisition Form (See 5.6 for instructions on Purchase Requisitions) or a GPU Standard Order Blank.

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5.2.6 Use a current Vendor Catalog to find catalog numbers (Form 1800.4-2).

5.2.7 Forward General Chemical Inventory form along with applicable g

purchase requisitions to Chemistry Foreman / Supervisor.

j 5.3 Chemical Standard Solutions 1

J.3.1 Figure 1800.4-2 is a partia,1 listing of chemical standard solutions to be maintained in the Chemistry Laboratory.

204 052 _

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09/17/75 1800.4 Revision 0 4.,

5. 3'. 2 An inventory will be conducted quarterly (January, April, 6

July, October) to insure that the minimum quantity of each standard listed in Figure 1800.4-2 is in stock.

i.3.3 If the p antity on hand of a particular standard does not exceed the minimum quantity, a new supply must be ordered.

5.3.4 Prepare a purchase requisition for items in lov supply by orderin; the amount listed under the guantity to order column in Figure 1800.4-2. Refer to section 5.6 for specfic not_s on cumpletion of purchase requisitions.

.5.4 On Line Analyzer Reagent Invent o ry

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In order to avoid interruptions in on line analyzer service, an inventory dill be performed quarterly to maintain reagents and t

i standards used in the analyzers.

5.4.1 This inventory will be performed quarterly (November, February, i

May and August).

5.4.2 Determine the amount of each tengent listed in Figure 1800.4-3 that is currently stocked in the secondary sample room.

(0 pen reagent bottles are not considered) 5.4.3 Compare the nuantity on hand with the minimum quantity listed

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for each chemical.

5.4.4 If the guantity on hand does not exceed the minimum quantity, more reagent must be ordered.

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5.4.5 Prepare a purchase requisition to order more reagent if

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required.

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09/17/75 1800.4 Revision 0 4

4 5.4.6 Order the amount of chenical listed under the quantity to order column in figure 1800.4-3 (The addresses of the vendors are included).

NOTE:

For the completion of purchase requisitions, see section 5.6.

5.4.7 Forward any completed purchase requisitions to a Chemistry Foreman /Superviser for approval.

5.5 Cases Several Different gases, used in conjunction with laboratory instruments, are needed to support the sampling and analysis _ _ _

schedule.

5.5.1 Twice a week (Preferably Monday and Wednesday) a Rad. Chem. Tech /Jr. will perform the Gas bottle inventory.

5.5.2 This inventory includes pressure gauge readings on in-use bottles and the quantity of bottles presently "in service", " full spares" and/or " empty".

5.5.3 If a gas bottle is below the minimum pressure (indicated on Form 1800.4-3) it should be changed by the Rad. Chem.

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'fech/Jr. and then noted on the form.

5.5.4 At least two (2) full spare bottles must be on hand at all times. If not, notify a Radiation Protection /

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Chemistry Foreman to, order more.

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g 5.0 204 054- _

09/17/75 1800.4 Revision 0 4

I 4

5.5.5 The Gas bottle inventory Form 1800.4-3 should be forwarded to a Radiation Protection Foreman upon completion.

5.6 Preparation of Purcht.se Requisitions 5.6.1 If chemicals or other items are needed that are not supplied by the GPU System Laboratory, a purchase requisition must be submitted.

5.6.2 Prepare a purchase requisition in accordance with Figure 1800.4-4 and forward to Chemistry Foreman /

Supervisor for approval.

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09/17/75 1800.4

~ FI'GU RE' 1800. 4-2 Revision 0 STANDARD SOLUTION INDEX QUANTITY MINIMUM TO STANDARD SOLUTION QUANTITY ORDER VENDOR CAT. NO.

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Iron Standard 1000 ppm Fe 500 ml 500 ml Harleco

7634, For A.A. Spectroscopy w

Silica Standard 1 ML = 1 MG S10 500 ml 16 oz.

Harleco 1973 2

(1000 ppm)

Lead Standard 1000 ppm Pb 500 n1 500 ml Harleco 7635 Copper Standard 1000 ppm Cu 500 ml 500 ml Harleco 7635 Lithium Standard 1000 ppm 500 ml 500 ml Harleco 7709 Sodium Standard 1000 ppm 500 ml 500 ml Harleco 7642 Boron Standard

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1000 ppm 500 ml 500 ml Harleco 7699

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L Chloride Standard f.

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1000 ppm c1 16 oz.

2 x 16 oz.

Harleco 1713

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Fluoride Standard

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100 ppm F 16 oz.

16 oz.

Harleco 18105 7ra(P.O Box 779) rifiTadelTilii~a Menna.191b'5 NOTE:

3rder above Standards from: A rthur H. Thoma ' comnanv. V "r

,e Hydrogen Standard (1 container)

(1 container)

MG Scientific g

Pure H2 12 Liter @

12 Liter @

Gases NONE f 200 psig 200 psig Nitrogen Standard 12 Liter @

12 Liter @

1 4 05' Pure N2 200 PSIG 200 PSIG MG Scient.

.c (1 container)

(1 container)

Cases NONE 12 Liter 12 Liter Oxygen Standard

@ 200 PSIG

@ 200 PSIG MG Scientific (1 container) (1 container)

GASES NONE Pure 02 Order above f_ rom :__MG Sc ient ij _ic Gases _,_ MG 'l achnical_Froduc ts..lnc..._1100_ tarrison_ Aman i, NOTE:

09/17/75

, l'800.4 Revision 0 FIGUPI l800.4-3 On Line Analyzer Reagent Data REAGENT MINIMUM QUANTITY VEND 0rl C T. NO.

QUANTITY TO ORDER Sodium Buffer Calgon Corp.

6938-2068-5 Solution (160ZBottle )

12 16 Eox_1346

.Pltt.shurgh EL_

Sodium Standard 15230 Solution (lgt.)

12 l

24 Calgon Corp.

6938-2069-3 100 ppb Amir._a Acid II leagent -

3 Case 6 Cases HACH chemical Co.

2309-17 4 Bottles / Case p n

% ony Eglybdate Ames, Iowa 50010 Reagent 3 Cases _

6_ Cases HACH

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1995 ~

4 Bottles / case

_Dxalic Acid Reajent 3 Cases 6 Cases HACH 975-17 4 Bottles _Lcase Electro Dose 1 Unit 2 Unit Hays Corp. -

C-731-99 Chips Michistan city.

s Indiana, 46360 Glacial Acetic

_ltid 2 Carton 4 Carton Fischer & Porter C o.

141B097U01 4 Bottles / Carton h}rg g nst ha if 97/[

Rd I

Potassium Iodide (2000) 1 1

Fischer & Porter 141B075U01 Phenyl Arsene p

0xid_e Solution

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2 16 oz.

216 oz.

Fischer &

- 141_B080U01

.N psedinchlorine)

Bottles Bottles Porter

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pH 7 Buffer 20 4 oz.

20 4 oz.

Fischer &

141E079UO3 1

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Titrator)

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09/17/75 1800.4 Revision 0 FIGURE 1800.4 __(cont'd)._ __

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REAGEf1T MIf4IMUM QUAf4TITY VEr100R CAT. f40.

QUAT 4TITY TO ORDER JH 4 Buffer 20 4 oz.

20 4 oz.

Fischer &

1418079UO2 (used in chlorine Bottles Bottles Porter Titrator)

Potassium Iodide 20 4 oz.

20 4 oz.

Fischer &

1418079U01 Solution 5%

Bottles Bottles Porter

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[...".'..'.'.I '. Y52"2 TERMS-F.O.D.-

REQ.No.

DATE ISSUE TO roo ~of use Tsis srAct SHIP TO OR DER No.

4-DO NOT WRITE IN THIS_SfACF D0_50I3PITE TN _THIS SPACE DELIVERY REQUEST ED D ELIV ERY VI A.

QU A NTITY ACCOUNT D ESC RIPTIO N ustorasr CHARGEABLE 04 M AND D

to C ATS (MANDATORY ENTRIES ON ALL REQUISITIONS FOR EACH LINE ITEM Oh THE REQUISITION.)

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NOUN NAME OF THE ITE_M:

MANUFACTURER'S PART NUMBER OR MFC. CATALOG ITEM NUMBER &

APPROXIMATE COST:

USE CURRENT VENDOR'S MANUALS AVAILABLE IN CHEMISTRY OFFICE

-[i APPLICATION:

BRIEF DESCRIPTION t

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l ACCOUNT Nt M23 VENDOR'S NAME AND ADDRESS 7gg ggg vvu_

couritto ey_ YOUR NAFE curexro my Aprooveo my DATr DATE DATF

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. F.0RM, '1800.4-1 CONDENSED IRfliIORLDHDER F0PM_.

1800.4 F.c a rd Revision 0

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DATE RAD CHEM TECH I GPU SYSTEMS j

ITEM QUANITY ON HAND MINIflUM QUAf4TITY LABORATORY

+

SUPPLY THIS

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CONC HNO 2_Ga.

4 Gal.

b 3

J_ _

METHANOL 1 Gal.

4 Gal.

BUFFER 7.

10 Packets 50 Packets

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BUFFER 4 10 Packets 50 Packets BUFFER 10 10 Packets 50 Packets GIYCER0L 1 Gal.

4 Gal.

CONC HCI 1 Gal.

4 Gal.

1 Gal.

4 Gal.

CONC H 50 2

4 METHYL IS0BUTYLKETCf4E 1 Gal.

2 Gal.

ACETONE 1 Gal.

4 Gal.

nil 0L 5lbs.

10 lbs.

SODIt" HYDR 0XIDE 1 KG 1 KG POTASSIUM HYDR 0XIDE 1 KG 1 KG POTASSIUM ACID PHALATE 7

1 lb.

2 lbs.

' HILIPORE FILTERS 45N 100 Filters 500 Filters INDIGO CARMINE 10 Grams 25 Grams DEXTROSE 1 lb.

2 lb.

NES$LER'S REAGENT 1 Liter 1 liter APDC 10 Grams 20 Grams AMIN 0NAPTHOL SULFONIC SOL.

32 oz. Bottl1._ _

_ _[2) 32 oz. Boj;tps__

4 OXALIC ACID SOL. 105

- 32_oz,__Bottl e

.(2) 32 oz. Bot les i

g AMMONIUM MOLYBENATE SOL.

32 oz.' Bottle (2) 32 07. Bo_itle_s_

204 061

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4 c,,.

NH 0H 4

HYDRAZINE INDICATOR 32 oz. Bottle (2) 32 oz. Bottles APPROVED BY:

GPU SYSTEMS LABORATORY:

Consider this an order for items and quantities circled above.

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l CHEMICAL 11 APE FORMULA MINIMUM QUANTITY-GRAND OF CHEMICA1.

S11PPLY CALALOG CGit'D:TS QUANTITY TO ORDER RCAGENT Pa0C. NO.

SOURCE NUMBER

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ACS 1917, 1955 Fisher A38 Acetic Acid (glac)'

CH C00H 2 pt 1 pt 3

8

. Ammonium Acetate CH COONH 2 lbs 1 lb ACS 1917, 1955 Fisher A637 3

4 Ammonium Chloride Nil Cl 1 lb 1 lb ACS 1904 Fisher A661 4

(NH )6 o7 244H C 1/4 lb 1/4 lb ACS 1906 Fisher A674 M 0 Ammonium Molybdate 4

3 (NH ) 224 H O 1 lb 1 lb ACS 1955 Fisher A679 4 C0 2

Ammonium Oxalate 1902,1907 Fisher M274 Ammonium Purpurate (Murex 1de) 5G SG 1920 1/4 lb 1/4 lb 1937 Fisher A714 NH V03 Ammonium Vandadate 4

Barium Nitrate-Ba(NO )2 1 lb 1 lb ACE 1955 7isher B53 7

3 3

Bromophenol Blue 5G 5G 1907 Fisher B392

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P Calcium Chloride CaCl2

+

f Carbon Tetrachloride CCl 1 qt 1 qt ACS 1952 Fisher C187 4

Carminic Acid 5G 5G 1913 Fisher C585 Chloroform CHCl 2 gal 1 gal ACS 1911 Fisher C299 3

Chrome Black T c3 2 x 100 G 100.G 1902,1905 Fisher E512 4

g D86 5G 5G 1907 Fisher Diphenyl Carbozone CB Disodium Ethylenediamine N

xc Tetracetate 1/4 lb 1/4 lb

.ACS 1902 Fisher S311

@E

c C H 0H 2 gal 1 gal 1955 Fisher A407 oR Ethanol (denatured) 25 ow (C H )20!

2.lb-6 x'1 lb ACS 1955 Fisher E138 Ethyl Ether; 25 FeCl.6H O 3 lbs 1 lb

'ACS 1954 Fisher 188 Ferric Chloride 3

2

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Fe(NO )3 9H O 1 lb 1 lb ACS 1955 Fisher 1110 Ferric Nitrate 3

2 3

Ferrous Ammonium S61 fat (Fe(NH4)2 (SO4)2 1 lb 1 lb ACS Fisher I77

1800.4 J

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xevision u CHErfICAL NAME FORMULA MINIMUM QUANTITY GRAND OF CHEMICAL l SUPPL.Y CALALOG CU@9hh -

QUANTITY TO ORDER REAGENT PROC. NO.I SOURCE NUMBER l

T. _ _

=

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__7 1,10 Phenanthraline 5C 5G 1917 Fisher P-70 h

Ortho Toluidene

.1% Sol'n 1 pt 1 pt 1927 Fisher S0-0-14 t-Oxalic Acid HC0 1 lb 1 lb ACS 1906 Fisher A 219 4 24 Phenolphthalein Indicator 1 pt 1 pt ACS 1930 Fisher S0-P-62 Phosphoric Acid H PO4 1 qt 1 qt ACS 1911 Fisher A 242 3

Potassium Chloride kcl 1 lb 1 lb ACS 1901 Fisher P 217 Potassium Dichromate K2CR207 1 lb !

l lb ACS 1934 Fisher P 188 Potassium Dihydrogen Phosphate KH2PO4 1/4 lb 1/4 lb ACS 1937 Fisher P285

'% Potassium Iodate K103 1/4 lb 1/4 lb ACS 1932 Fisher P 253 o

Potassium Iodide KI 1 lb 5 lb ACS 1911,1934 Fisher P 410 i

1952 Potassium Thiocyanate KSCN 1/4 lb 1/4 lb ACS 1932 Fisher P 317 Salicylic Acid 1 lb 1 lb ACS 1932 Fisher A 277 Sodium Bicarbonate NaHCO3 1 lb 1 lb ACS 1934 Fisher S 233 Sodium Bisulfite NaHS03 2 lb 1 lb ACS 1906,1952 Fisher S 645 r0 Sodium Carbonate cp Na2CO3 1 lb 1 lb ACS 1902 Fisher S 263 Sodium Chloride Nacl i

1 lb 1 lb ACS 1902 Fisher S 271 z-y Stannous Chloride SnCl 2H O 1/4 lb 1/4 lb ACS 1931 Fisher T 163 2 2 r

' Sodium Chromate' Na2 r0.10H O 5 lb 5 lb ACS 1955 Fisher S 272 C 4 2

Sodium Flouri A. ~4.-

NaF 1/4 lb 1/4 lb ACS 1902 Fisher (5-

,t

+

Sodium Hypochlorite Na0Cl (sot) 4-P 1 qt 1 qt.

1952 Fisher So-S-290 (5% C12 min' u.

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CllDfICAL DAME FORMULA MINIMUM QUANTITY GRMD OF CHEMICAL SUPPLY CALALOG C0' tit :TO QUANTITY TO ORDER REAGENT PROC. NO.

SOURCE NUMBER Sodium Phosphate Fisher S 369 Na H PO.H O 1 lb 1 lb ACS (Monobasic) 2 4 2 1T certified 1906 Fisher S 408 SiO.9H O 1 lb Sodium Silicate.

Na2 3

2 Na2 9H O 1 lb 1/4 lb

'ACS 1902 Fisher S 425 5

2 Sodium Sulfide 1 lb 1 lb ACS 1906 Fisher S 430 Sodium Sulfite Na2SO3 Na2 4 7 10H O 1 lb 1 lb ACS 1902 Fisher S 248 B0 2

Sodium Tetraborate Thenoyl Trifluoro-(TTA) 6 x 25 G 2 (6 x.25G)

!ACS 1954 Fisher T 402 acetone Sodium Phosphate (Dibasic)

Na2HPO 1 lb 1 lb ACS Fisher S 374 4

SrCl.6H O 1 lb '

1 lb ACS Fisher S 541 Strontium Chloride 2

2 Fisher B 35 1 lb 1 lb Barium Chloride BaCl2 Fisher B 385

. Bromine i

Br2 1/4 lb CeCl.7H O 1/4 lb 1/4 lb Fisher C 252 Cerium (ous) Chloride 3

2 N

C 24 Cesium Chloride c3 Csci 25 G 25 G 4

Copper (metal)

Cu 1 lb 1 lb

.ACS Fisher C 430 Cobalt Chloride CoCl.6H O 1 lb 1 lb ACS 1972 Fisher C 371 2

2 Fisher H 319 Hydrazine Hydrochlorid2 NH NH. hcl 500 G 500 G 2 2 Manganous Chloride MnCl.4H O 1 lb 1 lb '

ACS 1972 Fisher M 87 2

2 i

1 lb 1 lb

,ACS 1934 Fisher S 445 i

Na2 2 3 5H O S0 2

Sodium Thiosulfate Soluble Starch (For Iodometry) 1 lb 1 lb

ACS.

1934 Fisher S 516 f

1972 Fisher Zirconyl Chlor Zr0Cl.8H O 1 lb 1 lb 2

2 Carbon Disulfide CS2 2 pc.

1 pt

!ACS Fisher C 184 I

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09/17/75 1800.4 FORf1 Revision 0 1800.4-3 m

4 CAS BOTTLE INVENTORY e

DATE FULL GAS BOTTLE GAGE IN SPARE EMPTY READING SERVICE BOTTLES BOTTLES COFDIENTS

100% Methanc

10% Methane-90% Argon

Acethylene

Propane t

Nitrous Oxide r

Liquid Nitrogen

100% Argon L,

the case,

At least two (2) full spare bottles must be on hand at all times. If this is not

}

notify the HP/ Chem Supervisor to order more. Check the bottle that is in use. Record gage reading - if empty, change it.

- Indicate if the bottle is k, h or 3/4 or full (Also write in the serial number of the bottle).

)

fl COMPLETED BY APPROVED BY nn,

ZU4 U6/

18.0

ML19224B427

Text

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