ML18205A430
| ML18205A430 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 11/11/2015 |
| From: | Vania I Testamerica Labs, Westinghouse |
| To: | Barry Miller Office of Nuclear Material Safety and Safeguards, Perma-Fix Environmental Services |
| References | |
| HEM-17-35 | |
| Download: ML18205A430 (22) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-14225-2 Client Project/Site: HDP For:
Perma-Fix Environmental Services Inc.
2800 Solway Road Knoxville, Tennessee 37931 Attn: Brian Miller Authorized for release by:
11/11/2015 12:37:44 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP TestAmerica Job ID: 160-14225-2 Page 2 of 22 TestAmerica St. Louis 11/11/2015 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
4 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
20 QC Association Summary...................................
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Case Narrative Client: Perma-Fix Environmental Services Inc.
TestAmerica Job ID: 160-14225-2 Project/Site: HDP Job ID: 160-14225-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Perma-Fix Environmental Services Inc.
Project: HDP Report Number: 160-14225-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 10/12/2015 2:27 PM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 3 coolers at receipt time were 20.0º C, 20.0º C and 20.0º C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L03-01-01-P-S-S-00 (160-14225-1), L03-01-02-P-R-S-00 (160-14225-2), L03-01-04-P-S-S-00 (160-14225-3),
L03-01-05-P-R-S-00 (160-14225-4), L03-01-07-P-S-S-00 (160-14225-5), L03-01-08-P-R-S-00 (160-14225-6), L03-01-10-P-S-S-00 (160-14225-7), L03-01-11-P-R-S-00 (160-14225-8), L03-01-13-P-S-S-00 (160-14225-9), L03-01-14-P-R-S-00 (160-14225-10),
L03-01-16-P-S-S-00 (160-14225-11), L03-01-17-P-R-S-00 (160-14225-12), L03-01-19-P-S-S-00 (160-14225-13), L03-01-20-P-R-S-00 (160-14225-14), L03-01-22-P-S-S-00 (160-14225-15), L03-01-23-P-R-S-00 (160-14225-16), L03-01-01-P-S-Q-00 (160-14225-17),
L03-01-05-P-R-Q-00 (160-14225-18) and L03-01-25-P-S-B-00 (160-14225-19) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 10/13/2015, prepared on 10/15/2015 and analyzed on 11/06/2015.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 TestAmerica St. Louis 13715 Rider Trail North Chain of Custody Record TestAmerica l'HE LEADER IN ENVIRONMENTAL TESTING Earth City, MO 63045 phone 314.298.8566 fax Regulatory Program: O ow O NPDES 0 RCRA 0 Other:
TestAmerica Laboratories, Ine.
Client Contact Project Manager: Brian Miller Perma-Fix Environmental Services Tel/Fax: (314) 810-3333 2800 Solway Road Analysis Turnaround Time Knoxville, TN 37931 0 CALENDAR DAYS O WORKING DAYS Site
Contact:
Ellen Jakub Lab
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10 11 TestAmerica St. Louis 13715 RiderTrail North Earth City, MO 63045 phone 314.298.8566 fax Client Contact Perma-FtX Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Projec Site: Westinghouse Hematite, MO P 0#832953 sample ldentification L03-01-19-P-S-S-Q9 L03-01-20-P-R-S*OO L03-01-22-P-S-S-OO L03-01-23-P-R-S*OO L03-01-01-P-S-Q-OO L03-01-05-P-R-Q-OO L03-01-25-P-S-B-OO Chain of Custody Record Regulatory Program: D DW D NPDES 0RCRA EOther:
Project Manager: Brian Miller Site
Contact:
Eilen Jakub Date: 10/12/2015 Tel/Fax: (314) 810-3333 Lab
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A TestAmerica THE LEADER IN ENVIRONMENTAL TESTING TestAmerica Laboratories, Ine.
COC No: 101215-FSS1 2
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/".re any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the s~mple.
0 Non-Hazard O Flammable O s1n Initant O Poison B O Unknown 0 Retum to Client D Dlsposal by Lab 0 Archive foc Months Special l~truotioos/QC Req*i="'ts & Comr°" Pote.... Lfo, Radiologic,I co...-too Custody Seals lntact:
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Login Sample Receipt Checklist Client: Perma-Fix Environmental Services Inc.
Job Number: 160-14225-2 Login Number: 14225 Question Answer Comment Creator: Clarke, Jill C List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
N/A The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
N/A Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time.
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 22 11/11/2015 1
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Sample Summary TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID Client Sample ID Received Collected Matrix 160-14225-1 L03-01-01-P-S-S-00 Solid 10/08/15 15:15 10/12/15 14:27 160-14225-2 L03-01-02-P-R-S-00 Solid 10/08/15 15:30 10/12/15 14:27 160-14225-3 L03-01-04-P-S-S-00 Solid 10/08/15 14:30 10/12/15 14:27 160-14225-4 L03-01-05-P-R-S-00 Solid 10/08/15 14:45 10/12/15 14:27 160-14225-5 L03-01-07-P-S-S-00 Solid 10/08/15 16:05 10/12/15 14:27 160-14225-6 L03-01-08-P-R-S-00 Solid 10/08/15 16:15 10/12/15 14:27 160-14225-7 L03-01-10-P-S-S-00 Solid 10/08/15 13:40 10/12/15 14:27 160-14225-8 L03-01-11-P-R-S-00 Solid 10/08/15 14:05 10/12/15 14:27 160-14225-9 L03-01-13-P-S-S-00 Solid 10/08/15 11:15 10/12/15 14:27 160-14225-10 L03-01-14-P-R-S-00 Solid 10/08/15 11:30 10/12/15 14:27 160-14225-11 L03-01-16-P-S-S-00 Solid 10/08/15 10:30 10/12/15 14:27 160-14225-12 L03-01-17-P-R-S-00 Solid 10/08/15 11:05 10/12/15 14:27 160-14225-13 L03-01-19-P-S-S-00 Solid 10/08/15 10:00 10/12/15 14:27 160-14225-14 L03-01-20-P-R-S-00 Solid 10/08/15 10:15 10/12/15 14:27 160-14225-15 L03-01-22-P-S-S-00 Solid 10/08/15 09:25 10/12/15 14:27 160-14225-16 L03-01-23-P-R-S-00 Solid 10/08/15 09:40 10/12/15 14:27 160-14225-17 L03-01-01-P-S-Q-00 Solid 10/08/15 15:15 10/12/15 14:27 160-14225-18 L03-01-05-P-R-Q-00 Solid 10/08/15 14:45 10/12/15 14:27 160-14225-19 L03-01-25-P-S-B-00 Solid 10/09/15 10:10 10/12/15 14:27 TestAmerica St. Louis Page 9 of 22 11/11/2015 1
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-1 Client Sample ID: L03-01-01-P-S-S-00 Matrix: Solid Date Collected: 10/08/15 15:15 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.157 (2+/-)
1 11/06/15 11:13 10/15/15 14:20 pCi/g 0.115 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.279 0.309 0.291 0.995 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0725 0.165 0.111 1.18 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0649 0.145 0.0763 0.954 Lead 212 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0687 0.153 0.0848 1.23 Lead 214 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.275 2.13 1.05 18.1 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.882 10.5 10.5 U
0.136 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0725 1.00 0.165 0.111 1.18 Radium 226 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.115 0.157 0.113 1.07 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.751 0.527 0.495 1.71 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.262 0.120 0.120 U
0.0805 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0968 0.0585 0.0584 U
0.0342 Americium 241 pCi/g 10/15/15 14:20 11/06/15 11:13 1
4.36 2.64 2.63 U
1.95 Protactinium 234m Tl-208 0.382 0.0448 0.0598 0.0311 pCi/g 10/15/15 14:20 11/06/15 11:13 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14225-2 Client Sample ID: L03-01-02-P-R-S-00 Matrix: Solid Date Collected: 10/08/15 15:30 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.173 (2+/-)
1 11/06/15 09:40 10/15/15 14:20 pCi/g 0.103 RL MDC 0.131 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.288 0.353 0.329 1.24 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.0528 0.161 0.0975 1.23 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.0641 0.162 0.0781 1.10 Lead 212 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.0615 0.159 0.0877 1.28 Lead 214 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.400 1.76 0.952 14.5 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 09:40 1
1.00 0.203 0.199 U
0.359 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.0528 1.00 0.161 0.0975 1.23 Radium 226 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.103 0.173 0.131 1.11 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.682 0.448 0.433 1.11 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.209 0.105 0.105 U
0.0843 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 09:40 1
0.0906 0.0543 0.0543 U
-0.0191 Americium 241 pCi/g 10/15/15 14:20 11/06/15 09:40 1
4.00 2.35 2.35 U
1.51 Protactinium 234m Tl-208 0.323 0.0402 0.0523 0.0311 pCi/g 10/15/15 14:20 11/06/15 09:40 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-3 Client Sample ID: L03-01-04-P-S-S-00 Matrix: Solid Date Collected: 10/08/15 14:30 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.223 (2+/-)
1 11/06/15 09:43 10/15/15 14:20 pCi/g 0.124 RL MDC 0.188 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.600 0.435 0.425 0.890 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.0699 0.182 0.132 1.20 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.0866 0.173 0.102 1.08 Lead 212 pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.0872 0.193 0.121 1.44 Lead 214 pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.443 2.30 1.42 17.7 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 09:43 1
1.24 0.445 0.443 U
0.393 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.0699 1.00 0.182 0.132 1.20 Radium 226 pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.124 0.223 0.188 1.17 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 09:43 1
1.08 0.897 0.878 1.78 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.277 0.144 0.144 U
0.0721 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 09:43 1
0.114 0.0679 0.0679 U
-0.0249 Americium 241 pCi/g 10/15/15 14:20 11/06/15 09:43 1
7.31 2.51 2.48 U
3.94 Protactinium 234m Tl-208 0.289 0.0519 0.0599 0.0410 pCi/g 10/15/15 14:20 11/06/15 09:43 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14225-4 Client Sample ID: L03-01-05-P-R-S-00 Matrix: Solid Date Collected: 10/08/15 14:45 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.167 (2+/-)
1 11/06/15 10:25 10/15/15 14:20 pCi/g 0.0676 RL MDC 0.121 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.439 0.326 0.316 0.775 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.0686 0.150 0.102 1.06 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.0725 0.150 0.0827 0.968 Lead 212 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.0678 0.155 0.0963 1.17 Lead 214 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.230 2.02 1.08 16.7 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 10:25 1
1.05 0.257 0.252 U
0.423 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.0686 1.00 0.150 0.102 1.06 Radium 226 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.0676 0.167 0.121 1.13 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.809 0.289 0.275 0.852 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.223 0.135 0.135 U
0.0624 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 10:25 1
0.0943 0.0559 0.0559 U
-0.00256 Americium 241 pCi/g 10/15/15 14:20 11/06/15 10:25 1
5.32 2.31 2.30 U
1.74 Protactinium 234m Tl-208 0.345 0.0438 0.0566 0.0325 pCi/g 10/15/15 14:20 11/06/15 10:25 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-5 Client Sample ID: L03-01-07-P-S-S-00 Matrix: Solid Date Collected: 10/08/15 16:05 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.742 (2+/-)
0.130 (2+/-)
1 11/06/15 10:26 10/15/15 14:20 pCi/g 0.0846 RL MDC 0.105 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.286 0.254 0.239 0.813 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.0539 0.119 0.0830 0.819 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.0430 0.111 0.0562 0.743 Lead 212 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.0546 0.109 0.0650 0.844 Lead 214 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.178 1.65 0.850 13.9 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.870 0.147 0.146 U
0.188 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.0539 1.00 0.119 0.0830 0.819 Radium 226 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.0846 0.130 0.105 0.742 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.664 0.231 0.221 U
0.650 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.130 0.107 0.107 U
0.0743 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 10:26 1
0.0831 0.0495 0.0495 U
0.00888 Americium 241 pCi/g 10/15/15 14:20 11/06/15 10:26 1
4.42 17.8 17.8 U
-0.243 Protactinium 234m Tl-208 0.262 0.0376 0.0464 0.0294 pCi/g 10/15/15 14:20 11/06/15 10:26 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14225-6 Client Sample ID: L03-01-08-P-R-S-00 Matrix: Solid Date Collected: 10/08/15 16:15 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.05 (2+/-)
0.167 (2+/-)
1 11/06/15 11:13 10/15/15 14:20 pCi/g 0.0842 RL MDC 0.128 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.317 0.377 0.357 1.17 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0723 0.165 0.110 1.17 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0699 0.157 0.0817 1.03 Lead 212 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0839 0.169 0.105 1.28 Lead 214 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.244 1.89 1.06 15.3 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 11:13 1
1.03 0.327 0.323 U
0.487 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0723 1.00 0.165 0.110 1.17 Radium 226 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0842 0.167 0.128 1.05 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.677 0.270 0.257 0.784 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.236 0.155 0.155 U
0.125 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 11:13 1
0.0923 0.0552 0.0552 U
0.0196 Americium 241 pCi/g 10/15/15 14:20 11/06/15 11:13 1
3.97 4.24 4.18 6.88 Protactinium 234m Tl-208 0.319 0.0478 0.0581 0.0390 pCi/g 10/15/15 14:20 11/06/15 11:13 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-7 Client Sample ID: L03-01-10-P-S-S-00 Matrix: Solid Date Collected: 10/08/15 13:40 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.903 (2+/-)
0.131 (2+/-)
1 11/06/15 11:12 10/15/15 14:20 pCi/g 0.0964 RL MDC 0.0930 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.264 0.319 0.300 1.04 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.0721 0.149 0.102 1.05 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.0581 0.132 0.0684 0.873 Lead 212 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.0660 0.143 0.0799 1.14 Lead 214 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.342 1.85 0.982 15.3 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 11:12 1
1.04 0.198 0.193 U
0.381 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.0721 1.00 0.149 0.102 1.05 Radium 226 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.0964 0.131 0.0930 0.903 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.720 0.474 0.457 1.18 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.178 0.137 0.136 U
0.158 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 11:12 1
0.0830 0.0494 0.0494 U
0.0106 Americium 241 pCi/g 10/15/15 14:20 11/06/15 11:12 1
3.71 2.91 2.87 4.64 Protactinium 234m Pb-210 1.44 0.505 0.533 0.662 pCi/g 10/15/15 14:20 11/06/15 11:12 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.297 0.0498 0.0586 0.0398 pCi/g 10/15/15 14:20 11/06/15 11:12 1
Lab Sample ID: 160-14225-8 Client Sample ID: L03-01-11-P-R-S-00 Matrix: Solid Date Collected: 10/08/15 14:05 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.09 (2+/-)
0.191 (2+/-)
1 11/06/15 11:15 10/15/15 14:20 pCi/g 0.162 RL MDC 0.156 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.435 0.531 0.502 1.68 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.0766 0.180 0.129 1.22 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.0858 0.167 0.0975 1.05 Lead 212 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.0749 0.165 0.101 1.26 Lead 214 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.234 1.92 1.13 15.2 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.835 0.489 0.489 U
0.165 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.0766 1.00 0.180 0.129 1.22 Radium 226 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.162 0.191 0.156 1.09 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.849 0.562 0.542 1.40 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.243 0.161 0.161 U
0.0962 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 11:15 1
0.101 0.0599 0.0599 U
-0.00784 Americium 241 pCi/g 10/15/15 14:20 11/06/15 11:15 1
6.26 3.66 3.66 U
1.59 Protactinium 234m Tl-208 0.370 0.0576 0.0693 0.0444 pCi/g 10/15/15 14:20 11/06/15 11:15 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-9 Client Sample ID: L03-01-13-P-S-S-00 Matrix: Solid Date Collected: 10/08/15 11:15 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.897 (2+/-)
0.141 (2+/-)
1 11/06/15 11:49 10/15/15 14:20 pCi/g 0.109 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.323 0.387 0.367 1.20 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.0522 0.130 0.0849 0.945 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.0572 0.131 0.0676 0.867 Lead 212 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.0632 0.136 0.0786 1.07 Lead 214 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.353 1.95 0.995 16.4 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.944 0.579 0.576 U
-0.528 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.0522 1.00 0.130 0.0849 0.945 Radium 226 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.109 0.141 0.108 0.897 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.728 0.487 0.467 1.32 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.236 0.136 0.135 U
0.0680 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 11:49 1
0.0975 0.0584 0.0584 U
-0.0181 Americium 241 pCi/g 10/15/15 14:20 11/06/15 11:49 1
4.26 2.53 2.52 U
1.38 Protactinium 234m Pb-210 1.50 0.555 0.582 0.696 pCi/g 10/15/15 14:20 11/06/15 11:49 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.278 0.0413 0.0504 0.0316 pCi/g 10/15/15 14:20 11/06/15 11:49 1
Lab Sample ID: 160-14225-10 Client Sample ID: L03-01-14-P-R-S-00 Matrix: Solid Date Collected: 10/08/15 11:30 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.821 (2+/-)
0.135 (2+/-)
1 11/06/15 11:47 10/15/15 14:20 pCi/g 0.0855 RL MDC 0.106 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.375 0.426 0.404 1.29 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.0703 0.154 0.106 1.08 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.0662 0.142 0.0771 0.920 Lead 212 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.0634 0.139 0.0800 1.10 Lead 214 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.234 1.86 1.02 15.3 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.801 0.420 0.414 U
0.625 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.0703 1.00 0.154 0.106 1.08 Radium 226 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.0855 0.135 0.106 0.821 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.681 0.255 0.247 U
0.634 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.214 0.0957 0.0955 U
0.0628 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 11:47 1
0.0787 0.0468 0.0468 U
0.00972 Americium 241 pCi/g 10/15/15 14:20 11/06/15 11:47 1
4.46 2.63 2.59 4.61 Protactinium 234m Tl-208 0.297 0.0491 0.0580 0.0418 pCi/g 10/15/15 14:20 11/06/15 11:47 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-11 Client Sample ID: L03-01-16-P-S-S-00 Matrix: Solid Date Collected: 10/08/15 10:30 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.855 (2+/-)
0.129 (2+/-)
1 11/06/15 11:48 10/15/15 14:20 pCi/g 0.0864 RL MDC 0.0957 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.335 0.397 0.381 1.08 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.0523 0.149 0.0932 1.12 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.0598 0.127 0.0684 0.823 Lead 212 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.0572 0.147 0.0818 1.17 Lead 214 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.378 2.09 1.07 17.5 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 11:48 1
1.00 0.213 0.208 U
0.448 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.0523 1.00 0.149 0.0932 1.12 Radium 226 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.0864 0.129 0.0957 0.855 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.734 0.304 0.288 0.917 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.216 0.142 0.142 U
0.104 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 11:48 1
0.0914 0.0550 0.0549 U
-0.0252 Americium 241 pCi/g 10/15/15 14:20 11/06/15 11:48 1
4.20 2.65 2.61 4.54 Protactinium 234m Tl-208 0.299 0.0385 0.0494 0.0270 pCi/g 10/15/15 14:20 11/06/15 11:48 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14225-12 Client Sample ID: L03-01-17-P-R-S-00 Matrix: Solid Date Collected: 10/08/15 11:05 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.18 (2+/-)
0.176 (2+/-)
1 11/06/15 11:51 10/15/15 14:20 pCi/g 0.0860 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.378 0.463 0.437 1.49 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.0849 0.181 0.132 1.18 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.0830 0.166 0.0960 1.05 Lead 212 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.0733 0.174 0.114 1.26 Lead 214 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.392 2.09 1.27 16.2 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 11:51 1
1.37 0.291 0.286 U
0.489 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.0849 1.00 0.181 0.132 1.18 Radium 226 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.0860 0.176 0.129 1.18 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.905 0.321 0.304 0.966 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.201 0.157 0.155 U
0.199 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 11:51 1
0.0877 0.0521 0.0521 U
-0.0137 Americium 241 pCi/g 10/15/15 14:20 11/06/15 11:51 1
7.99 1.07 1.07 U
-0.223 Protactinium 234m Tl-208 0.353 0.0579 0.0685 0.0434 pCi/g 10/15/15 14:20 11/06/15 11:51 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-13 Client Sample ID: L03-01-19-P-S-S-00 Matrix: Solid Date Collected: 10/08/15 10:00 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.957 (2+/-)
0.148 (2+/-)
1 11/06/15 12:21 10/15/15 14:20 pCi/g 0.104 RL MDC 0.111 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.282 0.359 0.330 1.35 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0628 0.147 0.100 1.04 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0561 0.142 0.0669 0.964 Lead 212 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0712 0.144 0.0843 1.12 Lead 214 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.296 2.05 1.05 17.2 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.909 16.1 16.1 U
0.0635 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0628 1.00 0.147 0.100 1.04 Radium 226 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.104 0.148 0.111 0.957 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.782 0.609 0.593 1.34 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.232 0.121 0.120 U
0.118 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.106 0.0639 0.0638 U
-0.0407 Americium 241 pCi/g 10/15/15 14:20 11/06/15 12:21 1
4.06 2.38 2.38 U
1.20 Protactinium 234m Pb-210 1.71 0.654 0.684 0.789 pCi/g 10/15/15 14:20 11/06/15 12:21 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.330 0.0412 0.0536 0.0268 pCi/g 10/15/15 14:20 11/06/15 12:21 1
Lab Sample ID: 160-14225-14 Client Sample ID: L03-01-20-P-R-S-00 Matrix: Solid Date Collected: 10/08/15 10:15 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.06 (2+/-)
0.174 (2+/-)
1 11/06/15 12:19 10/15/15 14:20 pCi/g 0.136 RL MDC 0.136 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.409 0.402 0.388 1.01 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.0634 0.151 0.104 1.06 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.0674 0.151 0.0780 0.999 Lead 212 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.0701 0.152 0.0862 1.20 Lead 214 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.124 2.14 1.10 17.9 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 12:19 1
1.03 0.634 0.631 U
-0.585 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.0634 1.00 0.151 0.104 1.06 Radium 226 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.136 0.174 0.136 1.06 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.714 0.465 0.452 1.03 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.232 0.0989 0.0989 U
0.0328 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 12:19 1
0.0908 0.0538 0.0538 U
-0.00275 Americium 241 pCi/g 10/15/15 14:20 11/06/15 12:19 1
4.61 2.72 2.71 U
1.45 Protactinium 234m Tl-208 0.329 0.0485 0.0593 0.0396 pCi/g 10/15/15 14:20 11/06/15 12:19 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-15 Client Sample ID: L03-01-22-P-S-S-00 Matrix: Solid Date Collected: 10/08/15 09:25 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.802 (2+/-)
0.128 (2+/-)
1 11/06/15 12:21 10/15/15 14:20 pCi/g 0.113 RL MDC 0.0986 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.322 0.365 0.352 0.904 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0510 0.113 0.0818 0.747 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0613 0.117 0.0684 0.737 Lead 212 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0740 0.115 0.0766 0.823 Lead 214 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.338 1.83 1.01 14.9 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.923 0.559 0.557 U
-0.400 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0510 1.00 0.113 0.0818 0.747 Radium 226 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.113 0.128 0.0986 0.802 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.725 0.462 0.452 0.915 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.194 0.115 0.115 U
0.0850 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 12:21 1
0.0861 0.0509 0.0509 U
-0.00473 Americium 241 pCi/g 10/15/15 14:20 11/06/15 12:21 1
4.72 2.58 2.58 U
0.00331 Protactinium 234m Tl-208 0.214 0.0375 0.0435 0.0317 pCi/g 10/15/15 14:20 11/06/15 12:21 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14225-16 Client Sample ID: L03-01-23-P-R-S-00 Matrix: Solid Date Collected: 10/08/15 09:40 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.18 (2+/-)
0.203 (2+/-)
1 11/06/15 12:30 10/15/15 14:20 pCi/g 0.0848 RL MDC 0.163 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.354 0.439 0.413 1.44 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.0725 0.165 0.120 1.10 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.0798 0.155 0.0916 0.962 Lead 212 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.0711 0.173 0.113 1.27 Lead 214 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.362 2.07 1.23 16.3 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 12:30 1
1.29 0.313 0.308 U
0.479 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.0725 1.00 0.165 0.120 1.10 Radium 226 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.0848 0.203 0.163 1.18 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.871 0.316 0.302 U
0.869 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.182 0.143 0.142 U
0.154 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 12:30 1
0.109 0.0650 0.0649 U
0.00744 Americium 241 pCi/g 10/15/15 14:20 11/06/15 12:30 1
5.78 3.46 3.45 U
2.43 Protactinium 234m Tl-208 0.431 0.0581 0.0734 0.0399 pCi/g 10/15/15 14:20 11/06/15 12:30 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-17 Client Sample ID: L03-01-01-P-S-Q-00 Matrix: Solid Date Collected: 10/08/15 15:15 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.930 (2+/-)
0.168 (2+/-)
1 11/06/15 12:55 10/15/15 14:20 pCi/g 0.127 RL MDC 0.139 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.433 0.538 0.513 1.56 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.0677 0.145 0.102 1.00 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.0636 0.144 0.0746 0.953 Lead 212 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.0726 0.154 0.0976 1.15 Lead 214 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.397 2.13 1.12 17.7 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 12:55 1
1.14 0.171 0.168 U
0.263 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.0677 1.00 0.145 0.102 1.00 Radium 226 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.127 0.168 0.139 0.930 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.854 0.309 0.295 0.888 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.183 0.150 0.148 0.243 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 12:55 1
0.100 0.0594 0.0594 U
-0.00210 Americium 241 pCi/g 10/15/15 14:20 11/06/15 12:55 1
4.58 2.78 2.78 U
2.17 Protactinium 234m Tl-208 0.328 0.0512 0.0615 0.0390 pCi/g 10/15/15 14:20 11/06/15 12:55 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-14225-18 Client Sample ID: L03-01-05-P-R-Q-00 Matrix: Solid Date Collected: 10/08/15 14:45 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.176 (2+/-)
1 11/06/15 12:52 10/15/15 14:20 pCi/g 0.110 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.385 0.469 0.446 1.42 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.0710 0.168 0.114 1.19 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.0695 0.157 0.0825 1.03 Lead 212 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.0656 0.162 0.0890 1.30 Lead 214 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.130 2.01 1.08 16.5 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.735 0.295 0.290 U
0.469 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.0710 1.00 0.168 0.114 1.19 Radium 226 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.110 0.176 0.141 1.04 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.825 0.540 0.524 1.27 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.225 0.140 0.139 U
0.0637 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 12:52 1
0.0966 0.0577 0.0577 U
-0.0167 Americium 241 pCi/g 10/15/15 14:20 11/06/15 12:52 1
4.80 2.80 2.80 U
1.28 Protactinium 234m Tl-208 0.321 0.0464 0.0571 0.0380 pCi/g 10/15/15 14:20 11/06/15 12:52 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Lab Sample ID: 160-14225-19 Client Sample ID: L03-01-25-P-S-B-00 Matrix: Solid Date Collected: 10/09/15 10:10 Date Received: 10/12/15 14:27 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.829 (2+/-)
0.148 (2+/-)
1 11/06/15 12:53 10/15/15 14:20 pCi/g 0.131 RL MDC 0.121 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.402 0.421 0.408 1.00 Bismuth 212 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.0604 0.131 0.0883 0.926 Bismuth 214 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.0611 0.133 0.0730 0.861 Lead 212 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.0700 0.145 0.0966 1.04 Lead 214 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.364 1.99 1.08 16.4 Potassium 40 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.978 0.201 0.195 U
0.439 Protactinium 231 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.0604 1.00 0.131 0.0883 0.926 Radium 226 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.131 0.148 0.121 0.829 Thorium 232 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.782 0.501 0.489 1.03 Thorium 234 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.163 0.122 0.120 0.221 Uranium 235 pCi/g 10/15/15 14:20 11/06/15 12:53 1
0.0784 0.0464 0.0464 U
0.00774 Americium 241 pCi/g 10/15/15 14:20 11/06/15 12:53 1
5.54 2.12 2.08 U
4.03 Protactinium 234m Tl-208 0.283 0.0441 0.0529 0.0341 pCi/g 10/15/15 14:20 11/06/15 12:53 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 19 of 22 11/11/2015 1
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QC Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-216723/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 220516 Prep Batch: 216723 Actinium 228 Analyte U
1 11/06/15 10:27 10/15/15 14:20 pCi/g 0.0548 MDC RL 0.0104 0.0104 (2+/-)
(2+/-)
MB 0.002293 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.160 0.0289 0.0289 U
0.0000 Bismuth 212 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.0353 0.670 0.670 U
-0.01676 Bismuth 214 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.0233 0.0123 0.0122 U
0.004671 Lead 212 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.0341 0.615 0.615 U
-0.01537 Lead 214 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.247 0.116 0.116 U
0.01507 Potassium 40 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.251 0.124 0.124 U
0.08272 Protactinium 231 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.0353 1.00 0.670 0.670 U
-0.01676 Radium 226 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.0548 0.0104 0.0104 U
0.002293 Thorium 232 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.244 0.592 0.592 U
-0.1078 Thorium 234 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.0721 0.0695 0.0695 U
-0.009084 Uranium 235 1
11/06/15 10:27 10/15/15 14:20 pCi/g 0.0203 0.0120 0.0120 U
0.006644 Americium 241 1
11/06/15 10:27 10/15/15 14:20 pCi/g 1.51 0.0212 0.0212 U
-0.005770 Protactinium 234m Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 10/15/15 14:20 11/06/15 10:27 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-216723/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 220523 Prep Batch: 216723 Americium 241 Analyte 116 87 102 102.8 101 10.7 0.581 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.4 33.58 3.53 0.205 pCi/g 98 87 - 120 Cobalt 60 33.4 32.84 3.32 0.132 pCi/g 98 87 - 115 Client Sample ID: L03-01-01-P-S-S-00 Lab Sample ID: 160-14225-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 220517 Prep Batch: 216723 Actinium 228 Analyte 1
0.02 1.074 1.07 0.189 0.145 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 0.995 1.230 0.381 0.324 pCi/g 0.34 1
Bismuth 214 1.18 1.176 0.168 0.0752 pCi/g 0.01 1
Lead 212 0.954 1.049 0.163 0.0771 pCi/g 0.31 1
Lead 214 1.23 1.404 0.188 0.0771 pCi/g 0.52 1
Potassium 40 18.1 18.55 2.27 0.290 pCi/g 0.09 1
Protactinium 231 0.136 U 0.6988 U 0.368 0.891 pCi/g 0.05 1
Radium 226 1.18 1.176 0.168 1.00 0.0752 pCi/g 0.01 1
Thorium 232 1.07 1.074 0.189 0.145 pCi/g 0.02 1
Thorium 234 1.71 0.9037 0.303 0.826 pCi/g 0.98 1
Uranium 235 0.0805 U 0.1078 U 0.129 0.232 pCi/g 0.11 1
Americium 241 0.0342 U 0.02156 U 0.0586 0.0979 pCi/g 0.11 1
TestAmerica St. Louis Page 20 of 22 11/11/2015 1
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QC Sample Results TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: L03-01-01-P-S-S-00 Lab Sample ID: 160-14225-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 220517 Prep Batch: 216723 Protactinium 234m Analyte 1
0.39 U
-0.5390 1.95 U 3.66 6.43 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Tl-208 1
0.28 0.3478 0.382 0.0605 0.0381 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 21 of 22 11/11/2015 1
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QC Association Summary TestAmerica Job ID: 160-14225-2 Client: Perma-Fix Environmental Services Inc.
Project/Site: HDP Rad Leach Batch: 216044 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-14225-1 L03-01-01-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-1 DU L03-01-01-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-2 L03-01-02-P-R-S-00 Total/NA Solid Dry and Grind 160-14225-3 L03-01-04-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-4 L03-01-05-P-R-S-00 Total/NA Solid Dry and Grind 160-14225-5 L03-01-07-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-6 L03-01-08-P-R-S-00 Total/NA Solid Dry and Grind 160-14225-7 L03-01-10-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-8 L03-01-11-P-R-S-00 Total/NA Solid Dry and Grind 160-14225-9 L03-01-13-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-10 L03-01-14-P-R-S-00 Total/NA Solid Dry and Grind 160-14225-11 L03-01-16-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-12 L03-01-17-P-R-S-00 Total/NA Solid Dry and Grind 160-14225-13 L03-01-19-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-14 L03-01-20-P-R-S-00 Total/NA Solid Dry and Grind 160-14225-15 L03-01-22-P-S-S-00 Total/NA Solid Dry and Grind 160-14225-16 L03-01-23-P-R-S-00 Total/NA Solid Dry and Grind 160-14225-17 L03-01-01-P-S-Q-00 Total/NA Solid Dry and Grind 160-14225-18 L03-01-05-P-R-Q-00 Total/NA Solid Dry and Grind 160-14225-19 L03-01-25-P-S-B-00 Total/NA Prep Batch: 216723 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 216044 160-14225-1 L03-01-01-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-1 DU L03-01-01-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-2 L03-01-02-P-R-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-3 L03-01-04-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-4 L03-01-05-P-R-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-5 L03-01-07-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-6 L03-01-08-P-R-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-7 L03-01-10-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-8 L03-01-11-P-R-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-9 L03-01-13-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-10 L03-01-14-P-R-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-11 L03-01-16-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-12 L03-01-17-P-R-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-13 L03-01-19-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-14 L03-01-20-P-R-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-15 L03-01-22-P-S-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-16 L03-01-23-P-R-S-00 Total/NA Solid Fill_Geo-21 216044 160-14225-17 L03-01-01-P-S-Q-00 Total/NA Solid Fill_Geo-21 216044 160-14225-18 L03-01-05-P-R-Q-00 Total/NA Solid Fill_Geo-21 216044 160-14225-19 L03-01-25-P-S-B-00 Total/NA Solid Fill_Geo-21 LCS 160-216723/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-216723/1-A Method Blank Total/NA TestAmerica St. Louis Page 22 of 22 11/11/2015 1
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