ML18079A260
| ML18079A260 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 04/07/2016 |
| From: | Swanson M, Vania I Westinghouse |
| To: | Office of Nuclear Material Safety and Safeguards |
| References | |
| HEM-18-8 | |
| Download: ML18079A260 (24) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16732-1 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:
4/7/2016 12:37:30 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-16732-1 Page 2 of 24 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
19 QC Association Summary...................................
22 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16732-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16732-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)
Report Number: 160-16732-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 3/31/2016 11:10 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 1.5º C and 20.0º C.
TECHNETIUM-99 (ICPMS)
Samples L08-12-19-T-R-B-00 (160-16732-1), L08-12-20-T-R-B-00 (160-16732-2), L08-12-21-T-R-B-00 (160-16732-3),
L08-12-21-T-R-Q-00 (160-16732-4), L08-12-22-T-R-B-00 (160-16732-5), L08-12-23-T-R-B-00 (160-16732-6), L08-12-24-T-E-B-00 (160-16732-7), L08-12-25-T-E-B-00 (160-16732-8), L08-12-26-T-R-B-00 (160-16732-9) and L08-12-27-T-R-B-00 (160-16732-10) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 04/01/2016 and analyzed on 04/05/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDS Samples L08-12-19-T-R-B-00 (160-16732-1), L08-12-20-T-R-B-00 (160-16732-2), L08-12-21-T-R-B-00 (160-16732-3),
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16732-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16732-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
L08-12-21-T-R-Q-00 (160-16732-4), L08-12-22-T-R-B-00 (160-16732-5), L08-12-23-T-R-B-00 (160-16732-6), L08-12-24-T-E-B-00 (160-16732-7), L08-12-25-T-E-B-00 (160-16732-8), L08-12-26-T-R-B-00 (160-16732-9) and L08-12-27-T-R-B-00 (160-16732-10) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 04/01/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L08-12-19-T-R-B-00 (160-16732-1), L08-12-20-T-R-B-00 (160-16732-2), L08-12-21-T-R-B-00 (160-16732-3),
L08-12-21-T-R-Q-00 (160-16732-4), L08-12-22-T-R-B-00 (160-16732-5), L08-12-23-T-R-B-00 (160-16732-6), L08-12-24-T-E-B-00 (160-16732-7), L08-12-25-T-E-B-00 (160-16732-8), L08-12-26-T-R-B-00 (160-16732-9) and L08-12-27-T-R-B-00 (160-16732-10) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 03/31/2016, and prepared and analyzed on 04/01/2016.
Preparation Batch 160-243328:
Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214.
Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. L08-12-19-T-R-B-00 (160-16732-1), L08-12-20-T-R-B-00 (160-16732-2),
L08-12-21-T-R-B-00 (160-16732-3), L08-12-21-T-R-Q-00 (160-16732-4), L08-12-22-T-R-B-00 (160-16732-5), L08-12-23-T-R-B-00 (160-16732-6), L08-12-24-T-E-B-00 (160-16732-7), L08-12-25-T-E-B-00 (160-16732-8), L08-12-26-T-R-B-00 (160-16732-9),
L08-12-27-T-R-B-00 (160-16732-10), (LCS 160-243328/2-A), (MB 160-243328/1-A) and (160-16732-A-1-E DU)
The following samples, analyzed by gamma spectroscopy, did not meet the thorium-234 detection goal; L08-12-20-T-R-B-00 (160-16732-2), L08-12-23-T-R-B-00 (160-16732-6), L08-12-24-T-E-B-00 (160-16732-7), L08-12-25-T-E-B-00 (160-16732-8) and L08-12-27-T-R-B-00 (160-16732-10). The samples final activity was above the MDC. The samples are reported with the MDC achieved.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 12 Procedure HDP-PR-QAt006, Chain of Custody Hematite Decommissioning Project !Revision: 4 I
I Page 1 ofll Westinghouse Non-ProJlrietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a per4 n from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly.identified before the sample is released for use or analysis and send the completed CoC to,P.
Chain of Cutody ID No. I F-032916-02 Page 1/1 Project Name:
Westinghouse Electric Company Contact Person:
Clark Evers Phone Number:
314-810-3336 SampJer Name Donte Love Sample ID
- L08-12-19-T-R-B-OO L08-12-20-T-R-B-OO L08-12-21-T-R-B-OO L08-12-2 l-T-R-Q-OO L08-12-22-T-R-B-OO L08-I 2-23-T-R-B-OO L08-12-24-T-E-B-OO L08-12-25-T-E-B-OO L08-12-26-T-R-B-OO L08-12-27-T-R-B-OO Date 3/28/2016 3/28/2016 3/28/2016 3/28/2016 3/28/2016 3/28/2016 3/28/2016 3/28/2016 3/29/2016 3/29/2016 Relinquished by: G.,,.c.. "'IV-'\\.
Company Name:
~(..,
Received by:
Company Name:
- dby
- 3 ~ l 5
~:~t\\.'
Time 16:00 16:05 16:10 16:10 16:15 16:20 16:30 16:35 16:25 16:30 Date/Time 3/=>! / 11..,
o4to Dateffime Matrix s
s s
s s
s s
s s
s C,Cj r C Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North
~ "~-------------------,
j ~f :-~~r~566 e Laboratory Contact Person:
~ Ivan Vania Phone No.
708-870-8453 Turn Aroun..d.Time Rush (7 days)
Remarks l ILSA 08-12 Bias LSA 08-12 Bias l ILSA 08-12 Bias 1 ILSA 08-12 Bias 1 ILSA 08-12 Bias l ILSA 08-12 Bias l ILSA 08-12 Bias l ILSA 08-12 Bias 160-16732 Chain of Custody 1 ILSA 08-12 Bias l ILSA 08~12 Bias Cooler Temperature:
Ambient Shipper and Number:
0329-01~ 0330-01 Date/Time I Comments: NI A VerifiedBy: ~
~
3/3, h(.,
Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16732-1 Login Number: 16732 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
True Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time (excluding tests with immediate HTs)
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 24 1
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Sample Summary TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-16732-1 L08-12-19-T-R-B-00 Solid 03/28/16 16:00 03/31/16 11:10 160-16732-2 L08-12-20-T-R-B-00 Solid 03/28/16 16:05 03/31/16 11:10 160-16732-3 L08-12-21-T-R-B-00 Solid 03/28/16 16:10 03/31/16 11:10 160-16732-4 L08-12-21-T-R-Q-00 Solid 03/28/16 16:10 03/31/16 11:10 160-16732-5 L08-12-22-T-R-B-00 Solid 03/28/16 16:15 03/31/16 11:10 160-16732-6 L08-12-23-T-R-B-00 Solid 03/28/16 16:20 03/31/16 11:10 160-16732-7 L08-12-24-T-E-B-00 Solid 03/28/16 16:30 03/31/16 11:10 160-16732-8 L08-12-25-T-E-B-00 Solid 03/28/16 16:35 03/31/16 11:10 160-16732-9 L08-12-26-T-R-B-00 Solid 03/29/16 16:25 03/31/16 11:10 160-16732-10 L08-12-27-T-R-B-00 Solid 03/29/16 16:30 03/31/16 11:10 TestAmerica St. Louis Page 9 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-1 Client Sample ID: L08-12-19-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:00 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.25 (2+/-)
0.187 (2+/-)
1 04/01/16 16:16 04/01/16 14:08 pCi/g 0.112 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.108 0.0642 0.0642 U
-0.0178 Americium 241 pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.569 0.416 0.404 0.963 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.0748 0.131 0.104 0.779 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.0924 0.157 0.0861 1.01 Lead 212 pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.0812 0.127 0.0870 0.889 Lead 214 pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.268 2.21 1.23 17.9 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 16:16 1
1.29 0.282 0.272 U
0.694 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.0748 1.00 0.131 0.104 0.779 Radium 226 pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.907 1.00 0.360 0.341 1.08 Thorium 234 pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.239 0.231 0.211 0.927 Uranium 235 pCi/g 04/01/16 14:08 04/01/16 16:16 1
6.64 2.23 2.23 U
1.44 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 16:16 1
0.112 0.187 0.137 1.25 Thorium 232 Tl-208 0.340 0.0533 0.0639 0.0410 pCi/g 04/01/16 14:08 04/01/16 16:16 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-1 Client Sample ID: L08-12-19-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:00 Percent Solids: 82.8 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00012 0.000066 0.000020 mg/Kg
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Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.97 (2+/-)
0.212 (2+/-)
1 04/05/16 14:37 04/01/16 05:05 pCi/g 0.226 1.32 RL MDC 0.109 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 14:37 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Lab Sample ID: 160-16732-2 Client Sample ID: L08-12-20-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:05 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.12 (2+/-)
0.162 (2+/-)
1 04/01/16 16:18 04/01/16 14:08 pCi/g 0.0947 RL MDC 0.117 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:18 1
0.148 0.198 0.198 U
-0.0219 Americium 241 pCi/g 04/01/16 14:08 04/01/16 16:18 1
0.375 0.406 0.387 1.20 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 16:18 1
0.0750 0.124 0.0980 0.737 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 16:18 1
0.0669 0.152 0.0762 1.02 Lead 212 TestAmerica St. Louis Page 10 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-2 Client Sample ID: L08-12-20-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:05 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.801 (2+/-)
0.116 (2+/-)
1 04/01/16 16:18 04/01/16 14:08 pCi/g 0.0768 RL MDC 0.0812 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:18 1
0.247 2.51 1.11 22.4 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 16:18 1
1.15 0.706 0.702 U
-0.684 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 16:18 1
0.0750 1.00 0.124 0.0980 0.737 Radium 226 pCi/g 04/01/16 14:08 04/01/16 16:18 1
1.22 1.00 1.65 1.15 11.3 Thorium 234 pCi/g 04/01/16 14:08 04/01/16 16:18 1
0.303 0.546 0.253 4.75 Uranium 235 pCi/g 04/01/16 14:08 04/01/16 16:18 1
4.95 3.83 3.67 11.2 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 16:18 1
0.0947 0.162 0.117 1.12 Thorium 232 Tl-208 0.311 0.0471 0.0569 0.0388 pCi/g 04/01/16 14:08 04/01/16 16:18 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-2 Client Sample ID: L08-12-20-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:05 Percent Solids: 83.9 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0021 0.000061 0.000018 mg/Kg
04/01/16 05:05 04/05/16 14:41 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 35.2 (2+/-)
3.30 (2+/-)
1 04/05/16 14:41 04/01/16 05:05 pCi/g 0.210 1.23 RL MDC 0.627 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 14:41 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 97 Lab Sample ID: 160-16732-3 Client Sample ID: L08-12-21-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:10 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.422 (2+/-)
0.0819 (2+/-)
1 04/01/16 16:19 04/01/16 14:08 pCi/g 0.0637 RL MDC 0.0696 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.0617 0.0367 0.0367 U
-0.0106 Americium 241 pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.102 0.173 0.162 0.590 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.0467 0.0870 0.0670 0.534 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.0357 0.0626 0.0404 0.370 Lead 212 pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.0314 0.0871 0.0562 0.640 Lead 214 pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.214 0.920 0.589 6.90 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.580 0.191 0.187 U
0.346 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.0467 1.00 0.0870 0.0670 0.534 Radium 226 pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.581 1.00 0.528 0.430 2.93 Thorium 234 TestAmerica St. Louis Page 11 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-3 Client Sample ID: L08-12-21-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:10 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Uranium 235 0.868 (2+/-)
0.172 (2+/-)
1 04/01/16 16:19 04/01/16 14:08 pCi/g 0.153 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:19 1
1.74 2.46 2.34 7.38 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 16:19 1
0.0637 0.0819 0.0696 0.422 Thorium 232 Tl-208 0.135 0.0260 0.0295 0.0204 pCi/g 04/01/16 14:08 04/01/16 16:19 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-3 Client Sample ID: L08-12-21-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:10 Percent Solids: 86.9 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0014 0.000058 0.000018 mg/Kg
04/01/16 05:05 04/05/16 14:58 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 23.3 (2+/-)
2.22 (2+/-)
1 04/05/16 14:58 04/01/16 05:05 pCi/g 0.200 1.17 RL MDC 0.596 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 14:58 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 98 Lab Sample ID: 160-16732-4 Client Sample ID: L08-12-21-T-R-Q-00 Matrix: Solid Date Collected: 03/28/16 16:10 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.488 (2+/-)
0.102 (2+/-)
1 04/01/16 16:48 04/01/16 14:08 pCi/g 0.0680 RL MDC 0.0895 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.0959 0.0573 0.0573 U
0.0201 Americium 241 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.287 0.394 0.378 1.08 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.0614 0.105 0.0868 0.566 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.0533 0.0874 0.0598 0.492 Lead 212 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.0586 0.0995 0.0703 0.678 Lead 214 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.326 1.27 0.891 8.85 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.909 0.215 0.213 U
0.220 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.0614 1.00 0.105 0.0868 0.566 Radium 226 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.755 1.00 0.617 0.539 2.87 Thorium 234 pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.188 0.197 0.173 0.919 Uranium 235 pCi/g 04/01/16 14:08 04/01/16 16:48 1
4.01 13.3 13.3 U
-0.333 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 16:48 1
0.0680 0.102 0.0895 0.488 Thorium 232 TestAmerica St. Louis Page 12 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-4 Client Sample ID: L08-12-21-T-R-Q-00 Matrix: Solid Date Collected: 03/28/16 16:10 Date Received: 03/31/16 11:10 Tl-208 0.158 0.0332 0.0371 0.0265 pCi/g 04/01/16 14:08 04/01/16 16:48 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-4 Client Sample ID: L08-12-21-T-R-Q-00 Matrix: Solid Date Collected: 03/28/16 16:10 Percent Solids: 83.4 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0012 0.000063 0.000019 mg/Kg
04/01/16 05:05 04/05/16 15:02 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 20.8 (2+/-)
1.93 (2+/-)
1 04/05/16 15:02 04/01/16 05:05 pCi/g 0.216 1.26 RL MDC 0.249 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 15:02 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 Lab Sample ID: 160-16732-5 Client Sample ID: L08-12-22-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:15 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.913 (2+/-)
0.148 (2+/-)
1 04/01/16 16:49 04/01/16 14:08 pCi/g 0.0957 RL MDC 0.114 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.0904 0.0546 0.0545 U
0.0304 Americium 241 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.265 0.309 0.291 0.994 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.0457 0.0928 0.0687 0.601 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.0660 0.135 0.0754 0.870 Lead 212 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.0607 0.0926 0.0655 0.629 Lead 214 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.317 1.94 0.956 16.5 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.953 0.158 0.154 U
0.332 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.0457 1.00 0.0928 0.0687 0.601 Radium 226 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.765 1.00 0.676 0.553 3.72 Thorium 234 pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.236 0.221 0.192 1.08 Uranium 235 pCi/g 04/01/16 14:08 04/01/16 16:49 1
3.84 2.57 2.54 U
3.57 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 16:49 1
0.0957 0.148 0.114 0.913 Thorium 232 Tl-208 0.275 0.0379 0.0474 0.0279 pCi/g 04/01/16 14:08 04/01/16 16:49 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 13 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-5 Client Sample ID: L08-12-22-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:15 Percent Solids: 83.2 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00020 0.000066 0.000020 mg/Kg
04/01/16 05:05 04/05/16 15:07 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.39 (2+/-)
0.317 (2+/-)
1 04/05/16 15:07 04/01/16 05:05 pCi/g 0.225 1.32 RL MDC 0.0536 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 15:07 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 91 Lab Sample ID: 160-16732-6 Client Sample ID: L08-12-23-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:20 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.171 (2+/-)
1 04/01/16 16:50 04/01/16 14:08 pCi/g 0.115 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.133 0.0797 0.0797 U
-0.00370 Americium 241 pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.448 0.353 0.337 0.987 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.0757 0.120 0.0976 0.663 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.0720 0.187 0.0859 1.28 Lead 212 pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.0626 0.110 0.0801 0.722 Lead 214 pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.217 2.24 1.14 18.9 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.952 0.301 0.289 U
0.773 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.0757 1.00 0.120 0.0976 0.663 Radium 226 pCi/g 04/01/16 14:08 04/01/16 16:50 1
1.19 1.00 1.27 0.878 8.71 Thorium 234 pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.316 0.545 0.292 4.53 Uranium 235 pCi/g 04/01/16 14:08 04/01/16 16:50 1
3.63 4.46 4.24 13.7 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 16:50 1
0.115 0.171 0.123 1.17 Thorium 232 Tl-208 0.389 0.0513 0.0653 0.0384 pCi/g 04/01/16 14:08 04/01/16 16:50 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-6 Client Sample ID: L08-12-23-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:20 Percent Solids: 83.9 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00037 0.000062 0.000018 mg/Kg
04/01/16 05:05 04/05/16 15:11 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 6.26 (2+/-)
0.588 (2+/-)
1 04/05/16 15:11 04/01/16 05:05 pCi/g 0.211 1.23 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
TestAmerica St. Louis Page 14 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-6 Client Sample ID: L08-12-23-T-R-B-00 Matrix: Solid Date Collected: 03/28/16 16:20 Percent Solids: 83.9 Date Received: 03/31/16 11:10 Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 15:11 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 97 Lab Sample ID: 160-16732-7 Client Sample ID: L08-12-24-T-E-B-00 Matrix: Solid Date Collected: 03/28/16 16:30 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.954 (2+/-)
0.158 (2+/-)
1 04/01/16 16:52 04/01/16 14:08 pCi/g 0.0902 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.126 0.0752 0.0752 U
0.00456 Americium 241 pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.332 0.360 0.340 1.12 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.0735 0.122 0.0982 0.698 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.0640 0.145 0.0761 0.957 Lead 212 pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.0650 0.116 0.0852 0.757 Lead 214 pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.289 2.18 1.10 18.3 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 16:52 1
1.13 0.689 0.686 U
-0.536 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.0735 1.00 0.122 0.0982 0.698 Radium 226 pCi/g 04/01/16 14:08 04/01/16 16:52 1
1.09 1.00 0.839 0.734 3.90 Thorium 234 pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.331 0.905 0.335 8.26 Uranium 235 pCi/g 04/01/16 14:08 04/01/16 16:52 1
3.81 4.06 3.98 8.06 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 16:52 1
0.0902 0.158 0.124 0.954 Thorium 232 Tl-208 0.318 0.0482 0.0584 0.0356 pCi/g 04/01/16 14:08 04/01/16 16:52 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-7 Client Sample ID: L08-12-24-T-E-B-00 Matrix: Solid Date Collected: 03/28/16 16:30 Percent Solids: 81.1 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00018 0.000067 0.000020 mg/Kg
04/01/16 05:05 04/05/16 15:15 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.00 (2+/-)
0.309 (2+/-)
1 04/05/16 15:15 04/01/16 05:05 pCi/g 0.229 1.34 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 15:15 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 TestAmerica St. Louis Page 15 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-8 Client Sample ID: L08-12-25-T-E-B-00 Matrix: Solid Date Collected: 03/28/16 16:35 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.07 (2+/-)
0.175 (2+/-)
1 04/01/16 17:43 04/01/16 14:08 pCi/g 0.156 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.167 0.0995 0.0995 U
0.00144 Americium 241 pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.454 0.514 0.487 1.59 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.0846 0.156 0.126 0.889 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.0821 0.163 0.0954 1.02 Lead 212 pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.0734 0.132 0.0994 0.830 Lead 214 pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.267 2.51 1.45 20.0 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 17:43 1
1.51 0.220 0.219 U
0.207 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.0846 1.00 0.156 0.126 0.889 Radium 226 pCi/g 04/01/16 14:08 04/01/16 17:43 1
1.26 1.00 0.592 0.529 2.54 Thorium 234 pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.395 0.706 0.415 5.61 Uranium 235 pCi/g 04/01/16 14:08 04/01/16 17:43 1
6.41 4.38 4.36 U
4.32 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 17:43 1
0.156 0.175 0.137 1.07 Thorium 232 Tl-208 0.367 0.0561 0.0678 0.0389 pCi/g 04/01/16 14:08 04/01/16 17:43 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-8 Client Sample ID: L08-12-25-T-E-B-00 Matrix: Solid Date Collected: 03/28/16 16:35 Percent Solids: 84.1 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000056 J 0.000064 0.000019 mg/Kg
04/01/16 05:05 04/05/16 15:20 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.967 (2+/-)
0.159 (2+/-)
1 04/05/16 15:20 04/01/16 05:05 pCi/g 0.220 1.28 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 15:20 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 93 Lab Sample ID: 160-16732-9 Client Sample ID: L08-12-26-T-R-B-00 Matrix: Solid Date Collected: 03/29/16 16:25 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.937 (2+/-)
0.140 (2+/-)
1 04/01/16 17:44 04/01/16 14:08 pCi/g 0.0707 RL MDC 0.102 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0954 0.0571 0.0571 U
-0.0169 Americium 241 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.305 0.346 0.323 1.19 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0595 0.109 0.0822 0.696 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0579 0.134 0.0687 0.885 Lead 212 TestAmerica St. Louis Page 16 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-9 Client Sample ID: L08-12-26-T-R-B-00 Matrix: Solid Date Collected: 03/29/16 16:25 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.787 (2+/-)
0.111 (2+/-)
1 04/01/16 17:44 04/01/16 14:08 pCi/g 0.0633 RL MDC 0.0756 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.372 2.26 1.06 19.6 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.986 0.187 0.183 U
0.354 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0595 1.00 0.109 0.0822 0.696 Radium 226 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.721 1.00 0.488 0.466 1.40 Thorium 234 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.190 0.145 0.143 0.269 Uranium 235 pCi/g 04/01/16 14:08 04/01/16 17:44 1
4.51 2.58 2.58 U
0.683 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0707 0.140 0.102 0.937 Thorium 232 Tl-208 0.298 0.0359 0.0474 0.0240 pCi/g 04/01/16 14:08 04/01/16 17:44 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-9 Client Sample ID: L08-12-26-T-R-B-00 Matrix: Solid Date Collected: 03/29/16 16:25 Percent Solids: 85.0 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00092 0.000061 0.000018 mg/Kg
04/01/16 05:05 04/05/16 15:24 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 15.7 (2+/-)
1.51 (2+/-)
1 04/05/16 15:24 04/01/16 05:05 pCi/g 0.210 1.23 RL MDC 0.458 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 15:24 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 96 Lab Sample ID: 160-16732-10 Client Sample ID: L08-12-27-T-R-B-00 Matrix: Solid Date Collected: 03/29/16 16:30 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.172 (2+/-)
1 04/01/16 17:44 04/01/16 14:08 pCi/g 0.0963 RL MDC 0.129 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.114 0.0681 0.0681 U
-0.00548 Americium 241 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.431 0.536 0.516 1.42 Bismuth 212 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0715 0.128 0.0987 0.788 Bismuth 214 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0677 0.149 0.0797 0.972 Lead 212 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0796 0.117 0.0920 0.697 Lead 214 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.401 2.36 1.27 19.5 Potassium 40 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.596 0.432 0.419 0.975 Protactinium 231 pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0715 1.00 0.128 0.0987 0.788 Radium 226 pCi/g 04/01/16 14:08 04/01/16 17:44 1
1.04 1.00 0.909 0.742 5.03 Thorium 234 TestAmerica St. Louis Page 17 of 24 1
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Client Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16732-10 Client Sample ID: L08-12-27-T-R-B-00 Matrix: Solid Date Collected: 03/29/16 16:30 Date Received: 03/31/16 11:10 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Uranium 235 2.03 (2+/-)
0.313 (2+/-)
1 04/01/16 17:44 04/01/16 14:08 pCi/g 0.256 RL MDC 0.235 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/01/16 14:08 04/01/16 17:44 1
3.52 4.45 4.27 12.2 Protactinium 234m pCi/g 04/01/16 14:08 04/01/16 17:44 1
0.0963 0.172 0.129 1.11 Thorium 232 Tl-208 0.342 0.0529 0.0637 0.0392 pCi/g 04/01/16 14:08 04/01/16 17:44 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16732-10 Client Sample ID: L08-12-27-T-R-B-00 Matrix: Solid Date Collected: 03/29/16 16:30 Percent Solids: 86.4 Date Received: 03/31/16 11:10 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00031 0.000064 0.000019 mg/Kg
04/01/16 05:05 04/05/16 15:28 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 5.39 (2+/-)
0.569 (2+/-)
1 04/05/16 15:28 04/01/16 05:05 pCi/g 0.221 1.29 RL MDC 0.279 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/01/16 05:05 04/05/16 15:28 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 TestAmerica St. Louis Page 18 of 24 1
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QC Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-243094/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244372 Prep Batch: 243094 RL MDL Technetium 99 ND 0.000050 0.000015 mg/Kg 04/01/16 05:05 04/05/16 14:06 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-243094/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244372 Prep Batch: 243094 Technetium 99 0.00119 0.00113 mg/Kg 95 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: Matrix Spike Lab Sample ID: 160-16715-A-1-D MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 244372 Prep Batch: 243094 Technetium 99 0.000050 J 0.00132 0.00132 mg/Kg 97 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-16715-A-1-E MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 244372 Prep Batch: 243094 Technetium 99 0.000050 J 0.00132 0.00131 mg/Kg 96 75 - 125 1
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-243094/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244373 Prep Batch: 243094 Technetium 99 Analyte U
1 04/05/16 14:06 04/01/16 05:05 pCi/g 0.171 MDC 0.998 RL 0.0287 0.0285 (2+/-)
(2+/-)
MB 0.03930 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 04/01/16 05:05 04/05/16 14:06 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 100 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-243094/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244373 Prep Batch: 243094 Technetium 99 Analyte 120 80 95 19.33 20.3 1.80 0.993 0.170 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 101 LCS TestAmerica St. Louis Page 19 of 24 1
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QC Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: Matrix Spike Lab Sample ID: 160-16715-A-1-D MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 244373 Prep Batch: 243094 Technetium 99 Analyte 125 75 97 22.65 22.6 0.848 2.13 1.17 0.200 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 95 MS Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-16715-A-1-E MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 244373 Prep Batch: 243094 Technetium 99 Analyte 1
0.06 125 75 96 22.40 22.5 0.848 2.14 1.16 0.198 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 96 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-243328/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 243329 Prep Batch: 243328 Actinium 228 Analyte U
1 04/01/16 16:15 04/01/16 14:08 pCi/g 0.0556 MDC RL 0.0294 0.0294 (2+/-)
(2+/-)
MB 0.01161 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.0195 0.0102 0.0102 U
-0.0007794 Americium 241 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.278 0.145 0.145 U
-0.01854 Bismuth 212 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.0522 0.107 0.107 U
-0.01028 Bismuth 214 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.0282 0.0141 0.0141 U
0.002493 Lead 212 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.0364 0.0499 0.0499 U
-0.004754 Lead 214 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.254 0.0873 0.0873 U
-0.0006656 Potassium 40 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.265 0.105 0.105 U
0.0000 Protactinium 231 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.0522 1.00 0.107 0.107 U
-0.01028 Radium 226 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.281 1.00 0.137 0.137 U
0.03316 Thorium 234 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.0749 0.525 0.525 U
-0.01312 Uranium 235 1
04/01/16 16:15 04/01/16 14:08 pCi/g 5.24 15.2 15.2 U
-0.3801 Protactinium 234m 1
04/01/16 16:15 04/01/16 14:08 pCi/g 0.0556 0.0294 0.0294 U
0.01161 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 04/01/16 14:08 04/01/16 16:15 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 20 of 24 1
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QC Sample Results TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-243328/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 243330 Prep Batch: 243328 Americium 241 Analyte 116 87 95 95.81 101 9.97 0.498 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.1 32.43 3.39 0.200 0.151 pCi/g 95 87 - 120 Cobalt 60 31.7 29.61 2.99 0.120 pCi/g 93 87 - 115 Client Sample ID: L08-12-19-T-R-B-00 Lab Sample ID: 160-16732-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 243333 Prep Batch: 243328 Actinium 228 Analyte 1
0.28 1.359 1.25 0.221 0.111 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241
-0.0178 U
-0.00840 4
U 0.792 0.100 pCi/g 0.01 1
Bismuth 212 0.963 1.862 0.476 0.327 pCi/g 1.01 1
Bismuth 214 0.779 0.8501 0.129 0.0664 pCi/g 0.27 1
Lead 212 1.01 1.181 0.183 0.0851 pCi/g 0.49 1
Lead 214 0.889 0.9323 0.127 0.0720 pCi/g 0.17 1
Potassium 40 17.9 22.96 2.62 0.350 pCi/g 1.04 1
Protactinium 231 0.694 U 0.5724 U 0.234 1.25 pCi/g 0.24 1
Radium 226 0.779 0.8501 0.129 1.00 0.0664 pCi/g 0.27 1
Thorium 234 1.08 1.721 0.589 1.00 0.872 pCi/g 0.67 1
Uranium 235 0.927 1.007 0.245 0.248 pCi/g 0.17 1
Protactinium 234m 1.44 U 4.256 U 2.66 5.63 pCi/g 0.58 1
Thorium 232 1.25 1.359 0.221 0.111 pCi/g 0.28 1
Tl-208 1
0.55 0.4108 0.340 0.0653 0.0352 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 21 of 24 1
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QC Association Summary TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Metals Prep Batch: 243094 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16715-A-1-D MS Matrix Spike Total/NA Solid None 160-16715-A-1-E MSD Matrix Spike Duplicate Total/NA Solid None 160-16732-1 L08-12-19-T-R-B-00 Total/NA Solid None 160-16732-2 L08-12-20-T-R-B-00 Total/NA Solid None 160-16732-3 L08-12-21-T-R-B-00 Total/NA Solid None 160-16732-4 L08-12-21-T-R-Q-00 Total/NA Solid None 160-16732-5 L08-12-22-T-R-B-00 Total/NA Solid None 160-16732-6 L08-12-23-T-R-B-00 Total/NA Solid None 160-16732-7 L08-12-24-T-E-B-00 Total/NA Solid None 160-16732-8 L08-12-25-T-E-B-00 Total/NA Solid None 160-16732-9 L08-12-26-T-R-B-00 Total/NA Solid None 160-16732-10 L08-12-27-T-R-B-00 Total/NA Solid None LCS 160-243094/2-A Lab Control Sample Total/NA Solid None MB 160-243094/1-A Method Blank Total/NA Analysis Batch: 244372 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 243094 160-16715-A-1-D MS Matrix Spike Total/NA Solid 6020A 243094 160-16715-A-1-E MSD Matrix Spike Duplicate Total/NA Solid 6020A 243094 160-16732-1 L08-12-19-T-R-B-00 Total/NA Solid 6020A 243094 160-16732-2 L08-12-20-T-R-B-00 Total/NA Solid 6020A 243094 160-16732-3 L08-12-21-T-R-B-00 Total/NA Solid 6020A 243094 160-16732-4 L08-12-21-T-R-Q-00 Total/NA Solid 6020A 243094 160-16732-5 L08-12-22-T-R-B-00 Total/NA Solid 6020A 243094 160-16732-6 L08-12-23-T-R-B-00 Total/NA Solid 6020A 243094 160-16732-7 L08-12-24-T-E-B-00 Total/NA Solid 6020A 243094 160-16732-8 L08-12-25-T-E-B-00 Total/NA Solid 6020A 243094 160-16732-9 L08-12-26-T-R-B-00 Total/NA Solid 6020A 243094 160-16732-10 L08-12-27-T-R-B-00 Total/NA Solid 6020A 243094 LCS 160-243094/2-A Lab Control Sample Total/NA Solid 6020A 243094 MB 160-243094/1-A Method Blank Total/NA General Chemistry Analysis Batch: 243095 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-16732-1 L08-12-19-T-R-B-00 Total/NA Solid Moisture 160-16732-1 DU L08-12-19-T-R-B-00 Total/NA Solid Moisture 160-16732-2 L08-12-20-T-R-B-00 Total/NA Solid Moisture 160-16732-3 L08-12-21-T-R-B-00 Total/NA Solid Moisture 160-16732-4 L08-12-21-T-R-Q-00 Total/NA Solid Moisture 160-16732-5 L08-12-22-T-R-B-00 Total/NA Solid Moisture 160-16732-6 L08-12-23-T-R-B-00 Total/NA Solid Moisture 160-16732-7 L08-12-24-T-E-B-00 Total/NA Solid Moisture 160-16732-8 L08-12-25-T-E-B-00 Total/NA Solid Moisture 160-16732-9 L08-12-26-T-R-B-00 Total/NA Solid Moisture 160-16732-10 L08-12-27-T-R-B-00 Total/NA TestAmerica St. Louis Page 22 of 24 1
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QC Association Summary TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Rad Leach Batch: 243044 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16732-1 L08-12-19-T-R-B-00 Total/NA Solid Dry and Grind 160-16732-1 DU L08-12-19-T-R-B-00 Total/NA Solid Dry and Grind 160-16732-2 L08-12-20-T-R-B-00 Total/NA Solid Dry and Grind 160-16732-3 L08-12-21-T-R-B-00 Total/NA Solid Dry and Grind 160-16732-4 L08-12-21-T-R-Q-00 Total/NA Solid Dry and Grind 160-16732-5 L08-12-22-T-R-B-00 Total/NA Solid Dry and Grind 160-16732-6 L08-12-23-T-R-B-00 Total/NA Solid Dry and Grind 160-16732-7 L08-12-24-T-E-B-00 Total/NA Solid Dry and Grind 160-16732-8 L08-12-25-T-E-B-00 Total/NA Solid Dry and Grind 160-16732-9 L08-12-26-T-R-B-00 Total/NA Solid Dry and Grind 160-16732-10 L08-12-27-T-R-B-00 Total/NA Prep Batch: 243094 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16715-A-1-D MS Matrix Spike Total/NA Solid None 160-16715-A-1-E MSD Matrix Spike Duplicate Total/NA Solid None 160-16732-1 L08-12-19-T-R-B-00 Total/NA Solid None 160-16732-2 L08-12-20-T-R-B-00 Total/NA Solid None 160-16732-3 L08-12-21-T-R-B-00 Total/NA Solid None 160-16732-4 L08-12-21-T-R-Q-00 Total/NA Solid None 160-16732-5 L08-12-22-T-R-B-00 Total/NA Solid None 160-16732-6 L08-12-23-T-R-B-00 Total/NA Solid None 160-16732-7 L08-12-24-T-E-B-00 Total/NA Solid None 160-16732-8 L08-12-25-T-E-B-00 Total/NA Solid None 160-16732-9 L08-12-26-T-R-B-00 Total/NA Solid None 160-16732-10 L08-12-27-T-R-B-00 Total/NA Solid None LCS 160-243094/2-A Lab Control Sample Total/NA Solid None MB 160-243094/1-A Method Blank Total/NA Prep Batch: 243328 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 243044 160-16732-1 L08-12-19-T-R-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-1 DU L08-12-19-T-R-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-2 L08-12-20-T-R-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-3 L08-12-21-T-R-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-4 L08-12-21-T-R-Q-00 Total/NA Solid Fill_Geo-0 243044 160-16732-5 L08-12-22-T-R-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-6 L08-12-23-T-R-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-7 L08-12-24-T-E-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-8 L08-12-25-T-E-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-9 L08-12-26-T-R-B-00 Total/NA Solid Fill_Geo-0 243044 160-16732-10 L08-12-27-T-R-B-00 Total/NA Solid Fill_Geo-0 LCS 160-243328/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-243328/1-A Method Blank Total/NA TestAmerica St. Louis Page 23 of 24 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-16732-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 95 160-16715-A-1-D MS Percent Yield (Acceptance Limits)
Matrix Spike 96 160-16715-A-1-E MSD Matrix Spike Duplicate 92 160-16732-1 L08-12-19-T-R-B-00 97 160-16732-2 L08-12-20-T-R-B-00 98 160-16732-3 L08-12-21-T-R-B-00 95 160-16732-4 L08-12-21-T-R-Q-00 91 160-16732-5 L08-12-22-T-R-B-00 97 160-16732-6 L08-12-23-T-R-B-00 93 160-16732-7 L08-12-24-T-E-B-00 93 160-16732-8 L08-12-25-T-E-B-00 96 160-16732-9 L08-12-26-T-R-B-00 90 160-16732-10 L08-12-27-T-R-B-00 101 LCS 160-243094/2-A Lab Control Sample 100 MB 160-243094/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 24 of 24 1
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