ML18079A258
| ML18079A258 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 04/19/2016 |
| From: | Swanson M, Vania I Westinghouse |
| To: | Office of Nuclear Material Safety and Safeguards |
| References | |
| HEM-18-8 | |
| Download: ML18079A258 (23) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16616-2 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:
4/19/2016 3:43:16 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-16616-2 Page 2 of 23 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
7 Definitions/Glossary.......................................
8 Method Summary.........................................
9 Sample Summary.........................................
10 Client Sample Results......................................
11 QC Sample Results........................................
21 QC Association Summary...................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16616-2 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16616-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)
Report Number: 160-16616-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 3/22/2016 10:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 20.0º C and 20.0º C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L08-12-01-T-E-S-00 (160-16616-1), L08-12-02-T-E-S-00 (160-16616-2), L08-12-03-T-E-S-00 (160-16616-3),
L08-12-04-T-R-S-00 (160-16616-4), L08-12-05-T-E-S-00 (160-16616-5), L08-12-06-T-E-S-00 (160-16616-6), L08-12-07-T-R-S-00 (160-16616-7), L08-12-08-T-E-S-00 (160-16616-8), L08-12-09-T-R-S-00 (160-16616-9), L08-12-10-T-E-S-00 (160-16616-10),
L08-12-11-T-E-S-00 (160-16616-11), L08-12-12-T-R-S-00 (160-16616-12), L08-12-13-T-E-S-00 (160-16616-13), L08-12-14-T-R-S-00 (160-16616-14), L08-12-15-T-E-S-00 (160-16616-15), L08-12-15-T-E-Q-00 (160-16616-16), L08-12-16-T-R-S-00 (160-16616-17),
L08-12-17-T-E-S-00 (160-16616-18) and L08-12-18-T-E-B-00 (160-16616-19) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 03/22/2016, prepared on 03/25/2016 and analyzed on 04/15/2016.
Preparation Batch 160-242278:
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16616-2 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16616-2 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
The samples, analyzed by gamma spectroscopy, resulted in an RPD/RER (relative percent difference/replicate error ratio) outside of the acceptance criteria of 40%/1 for protactinium-231. Both the sample and sample duplicates activity are less than the MDC. The data have been qualified and reported. L08-12-01-T-E-S-00 (160-16616-1), L08-12-02-T-E-S-00 (160-16616-2), L08-12-03-T-E-S-00 (160-16616-3),
L08-12-04-T-R-S-00 (160-16616-4), L08-12-05-T-E-S-00 (160-16616-5), L08-12-06-T-E-S-00 (160-16616-6), L08-12-07-T-R-S-00 (160-16616-7), L08-12-08-T-E-S-00 (160-16616-8), L08-12-09-T-R-S-00 (160-16616-9), L08-12-10-T-E-S-00 (160-16616-10),
L08-12-11-T-E-S-00 (160-16616-11), L08-12-12-T-R-S-00 (160-16616-12), L08-12-13-T-E-S-00 (160-16616-13), L08-12-14-T-R-S-00 (160-16616-14), L08-12-15-T-E-S-00 (160-16616-15), L08-12-15-T-E-Q-00 (160-16616-16), L08-12-16-T-R-S-00 (160-16616-17),
L08-12-17-T-E-S-00 (160-16616-18), L08-12-18-T-E-B-00 (160-16616-19) and (160-16616-A-1-I DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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,Procedure l:IDP-PR-QA-006, Chain of Custody Page l of!
Hematite Decommissioning Project !Revision: 4 I
I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to l:IDP.
Chain of Cutodr ID No. I F-031816-01 Pae:e Project Name:
Westinghouse Electric Company Contact Person:
Clark Evers Phone Number:
314-810-3336 Sampler Name Kyle Weldon Sample ID Date Time L08-l2-01-T-E-S-00 3/18/2016 8:40 L08-12-02-T-E-S-OO 3/18/2016 8:42 L08-12-03-T-E-S-OO 3/18/2016 8:48 L08-12-04-T-R-S-OO 3/18/2016 9:00 L08-12-05-T-E-S-OO 3/18/2016 9:05 L08-12-06-T-E-S-OO 3/18/2016 9:14 L08-12-07-T-R-S-OO 3/18/2016 9:20 L08-12-08-T-E-S-OO 3/18/2016 9:22 L08-l 2-09-T-R-S-OO 3/18/2016 9:25 L08-l 2-1 O-T-E-S-00 3/18/2016 9:27 L08-12-l l-T-E-S-OO 3/18/2016 9:35 L08-12-12-T-R-S-00 3/18/2016 9:37 Reli.oouished by: ~ Date/rime CLvt ~,t--1
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Remarks 1 LSA08-12 1 LSA 08-12 1 LSA08-12 1 LSA08-1.2 rm 111 II 1II Ill II I Ill I 160-16616 Chain of Custody 1 LSA 08-12 1 LSA 08-12 1 LSA 08-12 LSA 08-12 Cooler Temperature:
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10 11 Procedure HDP-PR-QA-006, Chain of Custody Page 1 ofl Hematite Decommissioning Project jRevision: 4 I
I Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User mlist verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain ofCutody ID No. I F-031816-01 Page 2 of2 Project Name:
Westinghouse Electric Company Contact Person:
Clark Evers Phone Number:
314-8.10-3336 Sampler Name Kyle Weldon Sample ID L08-12-13-T-E-S-OO 108-12-14-T-R-S-OO L08-12-15-T-E-S-OO L08-12-15-T-E-Q-OO L08-12-l 6-T-R-S-OO L08-12-l 7-T-E-S-OO L08-12-l 8-T-E-B-OO Relinquished by:
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Date Time 3/18/2016 9:40 3/18/2016 9:46 3/18/2016 9:50 3/18/2016 9:50 3/18/2016 9:55 3/18/2016 9:57 3/18/2016 10:02 Date/Time 3/d'~/lv OC\\t,0 Date/Time Date/Tirp,e
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Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16616-2 Login Number: 16616 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time (excluding tests with immediate HTs)
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier F
Duplicate RPD exceeds the control limit Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 9 of 23 1
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Sample Summary TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-16616-1 L08-12-01-T-E-S-00 Solid 03/18/16 08:40 03/22/16 10:45 160-16616-2 L08-12-02-T-E-S-00 Solid 03/18/16 08:42 03/22/16 10:45 160-16616-3 L08-12-03-T-E-S-00 Solid 03/18/16 08:48 03/22/16 10:45 160-16616-4 L08-12-04-T-R-S-00 Solid 03/18/16 09:00 03/22/16 10:45 160-16616-5 L08-12-05-T-E-S-00 Solid 03/18/16 09:05 03/22/16 10:45 160-16616-6 L08-12-06-T-E-S-00 Solid 03/18/16 09:14 03/22/16 10:45 160-16616-7 L08-12-07-T-R-S-00 Solid 03/18/16 09:20 03/22/16 10:45 160-16616-8 L08-12-08-T-E-S-00 Solid 03/18/16 09:22 03/22/16 10:45 160-16616-9 L08-12-09-T-R-S-00 Solid 03/18/16 09:25 03/22/16 10:45 160-16616-10 L08-12-10-T-E-S-00 Solid 03/18/16 09:27 03/22/16 10:45 160-16616-11 L08-12-11-T-E-S-00 Solid 03/18/16 09:35 03/22/16 10:45 160-16616-12 L08-12-12-T-R-S-00 Solid 03/18/16 09:37 03/22/16 10:45 160-16616-13 L08-12-13-T-E-S-00 Solid 03/18/16 09:40 03/22/16 10:45 160-16616-14 L08-12-14-T-R-S-00 Solid 03/18/16 09:46 03/22/16 10:45 160-16616-15 L08-12-15-T-E-S-00 Solid 03/18/16 09:50 03/22/16 10:45 160-16616-16 L08-12-15-T-E-Q-00 Solid 03/18/16 09:50 03/22/16 10:45 160-16616-17 L08-12-16-T-R-S-00 Solid 03/18/16 09:55 03/22/16 10:45 160-16616-18 L08-12-17-T-E-S-00 Solid 03/18/16 09:57 03/22/16 10:45 160-16616-19 L08-12-18-T-E-B-00 Solid 03/18/16 10:02 03/22/16 10:45 TestAmerica St. Louis Page 10 of 23 1
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-1 Client Sample ID: L08-12-01-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:40 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.28 (2+/-)
0.196 (2+/-)
1 04/15/16 20:04 03/25/16 10:09 pCi/g 0.147 RL MDC 0.147 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.348 0.430 0.393 1.71 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.0772 0.183 0.120 1.35 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.0788 0.181 0.0906 1.21 Lead 212 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.0698 0.191 0.102 1.55 Lead 214 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.423 2.69 1.25 23.6 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 20:04 1
1.27 0.287 0.278 U
0.638 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.0772 1.00 0.183 0.120 1.35 Radium 226 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.147 0.196 0.147 1.28 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.893 0.601 0.572 1.75 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.220 0.192 0.184 0.532 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 20:04 1
0.112 0.0667 0.0667 U
0.0142 Americium 241 pCi/g 03/25/16 10:09 04/15/16 20:04 1
5.64 3.33 3.32 U
1.49 Protactinium 234m Tl-208 0.388 0.0500 0.0639 0.0402 pCi/g 03/25/16 10:09 04/15/16 20:04 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16616-2 Client Sample ID: L08-12-02-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:42 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.28 (2+/-)
0.175 (2+/-)
1 04/15/16 14:42 03/25/16 10:09 pCi/g 0.124 RL MDC 0.118 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.426 0.351 0.328 1.22 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.0672 0.166 0.103 1.26 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.0777 0.176 0.0892 1.17 Lead 212 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.0741 0.189 0.108 1.49 Lead 214 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.236 2.49 1.08 22.3 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 14:42 1
1.14 0.288 0.281 U
0.573 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.0672 1.00 0.166 0.103 1.26 Radium 226 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.124 0.175 0.118 1.28 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.825 0.697 0.655 2.27 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.219 0.191 0.179 0.658 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 14:42 1
0.0871 0.230 0.230 U
-0.00539 Americium 241 pCi/g 03/25/16 10:09 04/15/16 14:42 1
4.85 3.16 3.13 U
4.67 Protactinium 234m Tl-208 0.379 0.0486 0.0623 0.0384 pCi/g 03/25/16 10:09 04/15/16 14:42 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-3 Client Sample ID: L08-12-03-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 08:48 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.162 (2+/-)
1 04/15/16 14:44 03/25/16 10:09 pCi/g 0.0932 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.399 0.432 0.415 1.16 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.0519 0.155 0.0962 1.17 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.0584 0.156 0.0749 1.06 Lead 212 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.0691 0.168 0.0993 1.30 Lead 214 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.249 2.19 1.04 18.8 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 14:44 1
1.04 0.642 0.638 U
-0.640 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.0519 1.00 0.155 0.0962 1.17 Radium 226 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.0932 0.162 0.113 1.14 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.789 0.622 0.592 1.82 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.194 0.141 0.137 0.315 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 14:44 1
0.100 0.0595 0.0595 U
-0.00150 Americium 241 pCi/g 03/25/16 10:09 04/15/16 14:44 1
4.54 2.55 2.55 U
0.292 Protactinium 234m Tl-208 0.335 0.0386 0.0519 0.0272 pCi/g 03/25/16 10:09 04/15/16 14:44 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16616-4 Client Sample ID: L08-12-04-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:00 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.33 (2+/-)
0.222 (2+/-)
1 04/15/16 15:21 03/25/16 10:09 pCi/g 0.117 RL MDC 0.175 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.574 0.409 0.401 0.805 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0851 0.196 0.141 1.31 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0866 0.170 0.0981 1.08 Lead 212 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0883 0.192 0.114 1.49 Lead 214 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.408 2.25 1.36 17.5 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 15:21 1
1.46 0.279 0.277 U
0.273 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0851 1.00 0.196 0.141 1.31 Radium 226 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.117 0.222 0.175 1.33 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.889 0.351 0.322 1.34 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.227 0.157 0.154 0.303 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.123 0.0731 0.0731 U
-0.0116 Americium 241 pCi/g 03/25/16 10:09 04/15/16 15:21 1
7.27 2.29 2.28 U
2.85 Protactinium 234m Pb-210 2.23 0.842 0.882 0.993 pCi/g 03/25/16 10:09 04/15/16 15:21 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.385 0.0572 0.0698 0.0385 pCi/g 03/25/16 10:09 04/15/16 15:21 1
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-5 Client Sample ID: L08-12-05-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:05 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.176 (2+/-)
1 04/15/16 15:21 03/25/16 10:09 pCi/g 0.0942 RL MDC 0.140 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.412 0.318 0.303 0.911 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0626 0.151 0.0962 1.12 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0634 0.153 0.0768 1.02 Lead 212 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0628 0.156 0.0914 1.21 Lead 214 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.165 2.25 1.02 19.6 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 15:21 1
1.02 0.222 0.218 U
0.378 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0626 1.00 0.151 0.0962 1.12 Radium 226 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.0942 0.176 0.140 1.04 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.780 0.511 0.494 1.24 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.244 0.166 0.165 U
0.0916 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 15:21 1
0.100 0.0595 0.0595 U
-0.00117 Americium 241 pCi/g 03/25/16 10:09 04/15/16 15:21 1
4.48 2.49 2.49 U
0.0999 Protactinium 234m Tl-208 0.325 0.0418 0.0538 0.0325 pCi/g 03/25/16 10:09 04/15/16 15:21 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16616-6 Client Sample ID: L08-12-06-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:14 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.04 (2+/-)
0.162 (2+/-)
1 04/15/16 15:22 03/25/16 10:09 pCi/g 0.126 RL MDC 0.122 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.367 0.475 0.443 1.65 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.0634 0.169 0.112 1.21 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.157 0.0960 0.0953 U
0.0868 Lead 212 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.0726 0.162 0.0930 1.28 Lead 214 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.361 2.22 1.20 18.2 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 15:22 1
1.13 0.354 0.347 U
0.641 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.0634 1.00 0.169 0.112 1.21 Radium 226 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.126 0.162 0.122 1.04 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.799 0.521 0.507 1.16 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.196 0.136 0.134 0.225 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 15:22 1
0.0999 0.0601 0.0600 U
0.0290 Americium 241 pCi/g 03/25/16 10:09 04/15/16 15:22 1
5.75 3.61 3.59 U
3.80 Protactinium 234m Tl-208 0.381 0.0522 0.0655 0.0406 pCi/g 03/25/16 10:09 04/15/16 15:22 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-7 Client Sample ID: L08-12-07-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:20 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.37 (2+/-)
0.198 (2+/-)
1 04/15/16 15:23 03/25/16 10:09 pCi/g 0.115 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.404 0.486 0.461 1.52 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.0743 0.183 0.117 1.36 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.0703 0.166 0.0796 1.12 Lead 212 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.0718 0.184 0.106 1.44 Lead 214 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.338 2.54 1.15 22.5 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 15:23 1
1.19 0.255 0.247 U
0.551 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.0743 1.00 0.183 0.117 1.36 Radium 226 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.115 0.198 0.143 1.37 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.795 0.565 0.523 2.05 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.210 0.178 0.173 0.423 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 15:23 1
0.106 0.0629 0.0629 U
0.00544 Americium 241 pCi/g 03/25/16 10:09 04/15/16 15:23 1
5.06 2.57 2.50 6.11 Protactinium 234m Tl-208 0.442 0.0478 0.0659 0.0344 pCi/g 03/25/16 10:09 04/15/16 15:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16616-8 Client Sample ID: L08-12-08-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:22 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.17 (2+/-)
0.206 (2+/-)
1 04/15/16 16:02 03/25/16 10:09 pCi/g 0.150 RL MDC 0.167 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.613 0.697 0.673 1.74 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.0814 0.207 0.150 1.37 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.0995 0.179 0.111 1.08 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.118 0.229 0.159 1.60 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.492 2.50 1.55 19.2 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:02 1
1.36 0.451 0.449 U
0.407 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.0814 1.00 0.207 0.150 1.37 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.150 0.206 0.167 1.17 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:02 1
1.06 0.386 0.371 U
1.05 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.301 0.192 0.191 U
0.167 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:02 1
0.128 0.0758 0.0758 U
0.00788 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:02 1
7.74 4.41 4.41 U
1.14 Protactinium 234m Tl-208 0.420 0.0708 0.0832 0.0513 pCi/g 03/25/16 10:09 04/15/16 16:02 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-9 Client Sample ID: L08-12-09-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:25 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.11 (2+/-)
0.169 (2+/-)
1 04/15/16 16:03 03/25/16 10:09 pCi/g 0.0843 RL MDC 0.126 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.322 0.399 0.373 1.37 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0689 0.163 0.106 1.19 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0696 0.159 0.0805 1.06 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0681 0.162 0.0943 1.26 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.290 2.25 1.05 19.4 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:03 1
1.08 0.218 0.214 U
0.411 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0689 1.00 0.163 0.106 1.19 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0843 0.169 0.126 1.11 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.808 0.317 0.284 1.35 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.180 0.153 0.149 0.351 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.107 0.0638 0.0638 U
-0.00168 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:03 1
4.60 2.79 2.75 4.68 Protactinium 234m Pb-210 2.05 0.693 0.733 0.812 pCi/g 03/25/16 10:09 04/15/16 16:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.391 0.0446 0.0603 0.0309 pCi/g 03/25/16 10:09 04/15/16 16:03 1
Lab Sample ID: 160-16616-10 Client Sample ID: L08-12-10-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:27 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.179 (2+/-)
1 04/15/16 16:03 03/25/16 10:09 pCi/g 0.136 RL MDC 0.136 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.494 0.388 0.372 1.06 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0795 0.181 0.122 1.29 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0778 0.174 0.0893 1.15 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0792 0.189 0.110 1.48 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.478 2.43 1.33 19.9 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:03 1
1.11 0.348 0.335 U
0.877 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.0795 1.00 0.181 0.122 1.29 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.136 0.179 0.136 1.14 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.899 0.609 0.582 1.72 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.213 0.132 0.132 U
0.121 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:03 1
0.105 0.0622 0.0622 U
0.00106 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:03 1
6.63 2.11 2.06 U
4.15 Protactinium 234m Tl-208 0.403 0.0501 0.0652 0.0336 pCi/g 03/25/16 10:09 04/15/16 16:03 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-11 Client Sample ID: L08-12-11-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:35 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.38 (2+/-)
0.220 (2+/-)
1 04/15/16 16:04 03/25/16 10:09 pCi/g 0.0959 RL MDC 0.171 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.455 0.404 0.374 1.51 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.0743 0.199 0.125 1.51 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.0882 0.194 0.103 1.27 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.0971 0.206 0.120 1.61 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.383 2.71 1.26 23.8 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.921 0.557 0.555 U
0.384 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.0743 1.00 0.199 0.125 1.51 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.0959 0.220 0.171 1.38 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.963 0.821 0.798 1.83 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.268 0.163 0.162 U
0.108 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:04 1
0.112 0.0663 0.0663 U
0.00945 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:04 1
5.06 3.75 3.65 8.74 Protactinium 234m Tl-208 0.413 0.0511 0.0665 0.0400 pCi/g 03/25/16 10:09 04/15/16 16:04 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16616-12 Client Sample ID: L08-12-12-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:37 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.33 (2+/-)
0.208 (2+/-)
1 04/15/16 16:05 03/25/16 10:09 pCi/g 0.102 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.480 0.531 0.509 1.44 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.0789 0.180 0.122 1.27 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.0637 0.183 0.0850 1.26 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.0856 0.180 0.105 1.41 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.398 2.45 1.25 20.6 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:05 1
1.16 0.286 0.278 U
0.627 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.0789 1.00 0.180 0.122 1.27 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.102 0.208 0.158 1.33 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.864 0.561 0.545 1.28 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.252 0.137 0.137 U
0.0840 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:05 1
0.107 0.0643 0.0642 U
-0.0343 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:05 1
5.52 3.15 3.15 U
0.956 Protactinium 234m Tl-208 0.401 0.0507 0.0655 0.0347 pCi/g 03/25/16 10:09 04/15/16 16:05 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-13 Client Sample ID: L08-12-13-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:40 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.931 (2+/-)
0.183 (2+/-)
1 04/15/16 16:38 03/25/16 10:09 pCi/g 0.213 RL MDC 0.157 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.653 0.434 0.429 U
0.626 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.0653 0.191 0.136 1.28 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.0995 0.167 0.111 0.965 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.118 0.197 0.132 1.41 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.470 2.75 1.63 21.7 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:38 1
1.46 0.466 0.460 U
0.682 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.0653 1.00 0.191 0.136 1.28 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.213 0.183 0.157 0.931 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.987 0.656 0.634 1.62 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.303 0.180 0.179 U
0.220 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:38 1
0.130 0.0768 0.0768 U
0.00498 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:38 1
8.35 2.79 2.76 U
4.14 Protactinium 234m Tl-208 0.366 0.0568 0.0683 0.0364 pCi/g 03/25/16 10:09 04/15/16 16:38 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16616-14 Client Sample ID: L08-12-14-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:46 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.174 (2+/-)
1 04/15/16 16:39 03/25/16 10:09 pCi/g 0.114 RL MDC 0.131 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.404 0.452 0.434 1.19 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0685 0.168 0.107 1.24 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0703 0.156 0.0794 1.04 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0720 0.168 0.0942 1.34 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.347 2.36 1.11 20.4 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.908 0.296 0.292 U
0.444 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0685 1.00 0.168 0.107 1.24 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.114 0.174 0.131 1.13 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.862 0.597 0.561 1.96 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.166 0.123 0.116 0.424 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.106 0.0638 0.0638 U
0.0231 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:39 1
4.45 2.31 2.23 6.25 Protactinium 234m Tl-208 0.348 0.0421 0.0555 0.0336 pCi/g 03/25/16 10:09 04/15/16 16:39 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-15 Client Sample ID: L08-12-15-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:50 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.183 (2+/-)
1 04/15/16 16:39 03/25/16 10:09 pCi/g 0.120 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.354 0.407 0.384 1.29 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0805 0.196 0.129 1.42 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0712 0.158 0.0816 1.05 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0907 0.175 0.114 1.28 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.209 2.27 1.17 19.0 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:39 1
1.08 0.351 0.344 U
0.632 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0805 1.00 0.196 0.129 1.42 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.120 0.183 0.141 1.15 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.840 0.293 0.283 U
0.738 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.241 0.141 0.141 U
0.104 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:39 1
0.0966 0.0578 0.0577 U
-0.0176 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:39 1
5.37 3.02 3.02 U
0.268 Protactinium 234m Tl-208 0.348 0.0524 0.0636 0.0429 pCi/g 03/25/16 10:09 04/15/16 16:39 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16616-16 Client Sample ID: L08-12-15-T-E-Q-00 Matrix: Solid Date Collected: 03/18/16 09:50 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.23 (2+/-)
0.189 (2+/-)
1 04/15/16 16:40 03/25/16 10:09 pCi/g 0.104 RL MDC 0.143 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.353 0.435 0.406 1.51 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.0715 0.169 0.107 1.27 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.0744 0.168 0.0853 1.12 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.0696 0.175 0.100 1.37 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.250 2.39 1.09 21.1 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:40 1
1.19 0.725 0.722 U
-0.561 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.0715 1.00 0.169 0.107 1.27 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.104 0.189 0.143 1.23 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.835 0.668 0.656 1.24 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.253 0.160 0.160 U
0.0659 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:40 1
0.0975 42.5 42.5 U
-0.00903 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:40 1
5.25 3.03 3.03 U
0.699 Protactinium 234m Tl-208 0.373 0.0440 0.0584 0.0336 pCi/g 03/25/16 10:09 04/15/16 16:40 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-17 Client Sample ID: L08-12-16-T-R-S-00 Matrix: Solid Date Collected: 03/18/16 09:55 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.169 (2+/-)
1 04/15/16 16:41 03/25/16 10:09 pCi/g 0.103 RL MDC 0.123 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.381 0.462 0.436 1.48 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.0798 0.179 0.122 1.26 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.0570 0.179 0.0782 1.24 Lead 212 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.0688 0.164 0.0871 1.34 Lead 214 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.287 2.30 1.12 19.6 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 16:41 1
1.16 0.712 0.709 U
-0.652 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.0798 1.00 0.179 0.122 1.26 Radium 226 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.103 0.169 0.123 1.13 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.846 0.551 0.534 1.31 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.238 0.151 0.150 U
0.157 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 16:41 1
0.0988 0.0594 0.0593 U
-0.0277 Americium 241 pCi/g 03/25/16 10:09 04/15/16 16:41 1
5.39 3.06 3.06 U
0.519 Protactinium 234m Tl-208 0.376 0.0506 0.0639 0.0399 pCi/g 03/25/16 10:09 04/15/16 16:41 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16616-18 Client Sample ID: L08-12-17-T-E-S-00 Matrix: Solid Date Collected: 03/18/16 09:57 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.197 (2+/-)
1 04/15/16 18:12 03/25/16 10:09 pCi/g 0.160 RL MDC 0.159 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.417 0.446 0.426 1.26 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.0646 0.196 0.121 1.47 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.0689 0.177 0.0854 1.19 Lead 212 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.0854 0.183 0.100 1.48 Lead 214 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.333 2.48 1.29 20.7 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 18:12 1
1.12 0.325 0.316 U
0.715 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.0646 1.00 0.196 0.121 1.47 Radium 226 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.160 0.197 0.159 1.13 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.860 0.305 0.293 U
0.809 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.180 0.115 0.114 U
0.122 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.109 0.0644 0.0644 U
0.00310 Americium 241 pCi/g 03/25/16 10:09 04/15/16 18:12 1
5.78 3.19 3.14 5.83 Protactinium 234m Tl-208 0.344 0.0534 0.0642 0.0425 pCi/g 03/25/16 10:09 04/15/16 18:12 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16616-19 Client Sample ID: L08-12-18-T-E-B-00 Matrix: Solid Date Collected: 03/18/16 10:02 Date Received: 03/22/16 10:45 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.40 (2+/-)
0.220 (2+/-)
1 04/15/16 18:12 03/25/16 10:09 pCi/g 0.117 RL MDC 0.169 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.512 0.549 0.530 1.39 Bismuth 212 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.0864 0.193 0.130 1.38 Bismuth 214 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.0889 0.206 0.105 1.36 Lead 212 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.0888 0.213 0.128 1.63 Lead 214 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.347 2.75 1.36 23.7 Potassium 40 pCi/g 03/25/16 10:09 04/15/16 18:12 1
1.33 0.329 0.323 U
0.608 Protactinium 231 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.0864 1.00 0.193 0.130 1.38 Radium 226 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.117 0.220 0.169 1.40 Thorium 232 pCi/g 03/25/16 10:09 04/15/16 18:12 1
1.04 0.385 0.371 U
0.986 Thorium 234 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.283 0.180 0.180 U
0.120 Uranium 235 pCi/g 03/25/16 10:09 04/15/16 18:12 1
0.125 0.0744 0.0744 U
0.0180 Americium 241 pCi/g 03/25/16 10:09 04/15/16 18:12 1
6.23 3.51 3.51 U
0.163 Protactinium 234m Tl-208 0.419 0.0548 0.0697 0.0439 pCi/g 03/25/16 10:09 04/15/16 18:12 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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QC Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-242278/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246244 Prep Batch: 242278 Actinium 228 Analyte U
1 04/15/16 14:41 03/25/16 10:09 pCi/g 0.0870 MDC RL 0.0467 0.0467 (2+/-)
(2+/-)
MB
-0.01260 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.311 0.166 0.166 U
-0.02914 Bismuth 212 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.0181 0.0156 0.0156 U
0.0000 Bismuth 214 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.0274 0.0243 0.0242 U
-0.002973 Lead 212 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.0313 0.0139 0.0139 U
0.001726 Lead 214 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.237 2.33 2.33 U
-0.05829 Potassium 40 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.333 0.169 0.169 U
-0.008713 Protactinium 231 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.0181 1.00 0.0156 0.0156 U
0.0000 Radium 226 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.0870 0.0467 0.0467 U
-0.01260 Thorium 232 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.288 0.155 0.155 U
-0.01497 Thorium 234 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.0745 0.0346 0.0346 U
0.004824 Uranium 235 1
04/15/16 14:41 03/25/16 10:09 pCi/g 0.0225 0.0124 0.0124 U
-0.002749 Americium 241 1
04/15/16 14:41 03/25/16 10:09 pCi/g 3.73 0.600 0.600 U
0.0000 Protactinium 234m Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 03/25/16 10:09 04/15/16 14:41 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242278/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246245 Prep Batch: 242278 Americium 241 Analyte 116 87 98 98.78 101 10.3 0.503 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.0 32.70 3.42 0.145 pCi/g 96 87 - 120 Cobalt 60 31.6 29.63 2.99 0.119 pCi/g 94 87 - 115 Client Sample ID: L08-12-01-T-E-S-00 Lab Sample ID: 160-16616-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 246252 Prep Batch: 242278 Actinium 228 Analyte 1
0.55 1.086 1.28 0.165 0.110 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 1.71 1.219 0.334 0.243 pCi/g 0.64 1
Bismuth 214 1.35 1.187 0.162 0.0658 pCi/g 0.46 1
Lead 212 1.21 1.124 0.164 0.0599 pCi/g 0.24 1
Lead 214 1.55 1.389 0.174 0.0897 pCi/g 0.45 1
Potassium 40 23.6 20.70 2.43 0.363 pCi/g 0.57 1
Protactinium 231 0.638 U
-0.7669 U F 0.759 1.23 pCi/g 1.34 1
Radium 226 1.35 1.187 0.162 1.00 0.0658 pCi/g 0.46 1
Thorium 232 1.28 1.086 0.165 0.110 pCi/g 0.55 1
Thorium 234 1.75 1.356 0.344 0.860 pCi/g 0.42 1
Uranium 235 0.532 0.4079 0.157 0.197 pCi/g 0.36 1
Americium 241 0.0142 U 0.02613 U 0.0577 0.0961 pCi/g 0.1 1
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QC Sample Results TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: L08-12-01-T-E-S-00 Lab Sample ID: 160-16616-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 246252 Prep Batch: 242278 Protactinium 234m Analyte 1
0.01 U
1.429 1.49 U 2.91 4.99 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Tl-208 1
0.06 0.3800 0.388 0.0603 0.0334 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 22 of 23 1
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QC Association Summary TestAmerica Job ID: 160-16616-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Rad Leach Batch: 241584 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16616-1 L08-12-01-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-1 DU L08-12-01-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-2 L08-12-02-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-3 L08-12-03-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-4 L08-12-04-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-5 L08-12-05-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-6 L08-12-06-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-7 L08-12-07-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-8 L08-12-08-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-9 L08-12-09-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-10 L08-12-10-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-11 L08-12-11-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-12 L08-12-12-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-13 L08-12-13-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-14 L08-12-14-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-15 L08-12-15-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-16 L08-12-15-T-E-Q-00 Total/NA Solid Dry and Grind 160-16616-17 L08-12-16-T-R-S-00 Total/NA Solid Dry and Grind 160-16616-18 L08-12-17-T-E-S-00 Total/NA Solid Dry and Grind 160-16616-19 L08-12-18-T-E-B-00 Total/NA Prep Batch: 242278 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 241584 160-16616-1 L08-12-01-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-1 DU L08-12-01-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-2 L08-12-02-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-3 L08-12-03-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-4 L08-12-04-T-R-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-5 L08-12-05-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-6 L08-12-06-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-7 L08-12-07-T-R-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-8 L08-12-08-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-9 L08-12-09-T-R-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-10 L08-12-10-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-11 L08-12-11-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-12 L08-12-12-T-R-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-13 L08-12-13-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-14 L08-12-14-T-R-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-15 L08-12-15-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-16 L08-12-15-T-E-Q-00 Total/NA Solid Fill_Geo-21 241584 160-16616-17 L08-12-16-T-R-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-18 L08-12-17-T-E-S-00 Total/NA Solid Fill_Geo-21 241584 160-16616-19 L08-12-18-T-E-B-00 Total/NA Solid Fill_Geo-21 LCS 160-242278/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-242278/1-A Method Blank Total/NA TestAmerica St. Louis Page 23 of 23 1
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