ML18079A233
| ML18079A233 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 04/11/2016 |
| From: | Swanson M, Vania I Testamerica Labs, Westinghouse |
| To: | Office of Nuclear Material Safety and Safeguards |
| References | |
| HEM-18-8 | |
| Download: ML18079A233 (21) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16768-1 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:
4/11/2016 4:53:20 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-16768-1 Page 2 of 21 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
16 QC Association Summary...................................
19 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16768-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16768-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)
Report Number: 160-16768-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 4/1/2016 3:30 PM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 2.1º C.
TECHNETIUM-99 (ICPMS)
Samples L08-09-10-T-E-B-00 (160-16768-1), L08-09-11-T-E-B-00 (160-16768-2), L08-09-12-T-E-B-00 (160-16768-3),
L08-09-13-T-E-B-00 (160-16768-4), L08-09-14-T-E-B-00 (160-16768-5) and L08-09-15-T-E-B-00 (160-16768-6) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 04/04/2016 and analyzed on 04/05/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDS Samples L08-09-10-T-E-B-00 (160-16768-1), L08-09-11-T-E-B-00 (160-16768-2), L08-09-12-T-E-B-00 (160-16768-3),
L08-09-13-T-E-B-00 (160-16768-4), L08-09-14-T-E-B-00 (160-16768-5) and L08-09-15-T-E-B-00 (160-16768-6) were analyzed for percent TestAmerica St. Louis Page 3 of 21 1
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16768-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16768-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued) solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 04/05/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L08-09-10-T-E-B-00 (160-16768-1), L08-09-11-T-E-B-00 (160-16768-2), L08-09-12-T-E-B-00 (160-16768-3),
L08-09-13-T-E-B-00 (160-16768-4), L08-09-14-T-E-B-00 (160-16768-5) and L08-09-15-T-E-B-00 (160-16768-6) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 04/04/2016, and prepared and analyzed on 04/05/2016.
Preparation Batch 160-244356:
Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214.
Because the samples have not had a 21-day ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. L08-09-10-T-E-B-00 (160-16768-1), L08-09-11-T-E-B-00 (160-16768-2), L08-09-12-T-E-B-00 (160-16768-3),
L08-09-13-T-E-B-00 (160-16768-4), L08-09-14-T-E-B-00 (160-16768-5), L08-09-15-T-E-B-00 (160-16768-6), (LCS 160-244356/2-A), (MB 160-244356/1-A) and (160-16768-A-1-E DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 12 Procedure.HDP-PR-QA-006, Chain ofCustody Hematite Decommissioning Project !Revision: 4 I
Page 1 ofll Westinghouse Non-Proprietary Class 3 FORt\\1 HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain of Cutodv ID No. I F-033116-01 Piu?e Project Name:
Westinghouse Electric Company Contact Person:
Clark Evers Phone Number:
314-810-3336 Sampler Name J. Willams Sample ID L08-09-l O-T-E-B-00 L08-09-l l-T-E-B-OO L08-09-12-T-E-B-OO L08-09-13-T-E-B-OO L08-09-l 4-T-E-B-OO L08-09-15-T-E-B-OO Date Time 3/31/2016 9:20 3/31/2016 9:40 3/31/2016 9:30 3/31/2016 9:25 3/31/2016 9:15 3/31/2016 9:35 e,......t" Company Name:
c._J J: c R~:/<4<-.
Com7 )]N_FfL Relinquished bv:
Company Name:
Date/Time oqol lf.p
/S:S'O Date/Time 1/1 Matrix s
s s
s s
s
- ~
,0"""'
Laboratory Name:
TA-MO Laboratory Address:
13715 Rider Trail North
~ "1---------------------i
- E PhoneNo-8 314-298-8566
~ Laboratory Contact Person:
~ Ivan Vania Phone No_
708-870-8453 Turn Aro_!ID.d Time Rush LSA-08-09 Bias 1 ILSA-08-09 Bias 1 ILSA-08-09 Bias 1 ILSA-08-09 Bias 1 ILSA-08-09 Bias LSA-08-09 Bias Cooler Temperature:
Shipper and Number:
(7 days)
Remarks 160-16768 Chain of Custody Ambient Ve,ifi,dBy, 'fh 0 -
' ;::,cf /if,-- 4.-
J-.j-/-/l
Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16768-1 Login Number: 16768 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
True Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time (excluding tests with immediate HTs)
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 21 1
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Sample Summary TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-16768-1 L08-09-10-T-E-B-00 Solid 03/31/16 09:20 04/01/16 15:30 160-16768-2 L08-09-11-T-E-B-00 Solid 03/31/16 09:40 04/01/16 15:30 160-16768-3 L08-09-12-T-E-B-00 Solid 03/31/16 09:30 04/01/16 15:30 160-16768-4 L08-09-13-T-E-B-00 Solid 03/31/16 09:25 04/01/16 15:30 160-16768-5 L08-09-14-T-E-B-00 Solid 03/31/16 09:15 04/01/16 15:30 160-16768-6 L08-09-15-T-E-B-00 Solid 03/31/16 09:35 04/01/16 15:30 TestAmerica St. Louis Page 9 of 21 1
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Client Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16768-1 Client Sample ID: L08-09-10-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:20 Date Received: 04/01/16 15:30 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.08 (2+/-)
0.155 (2+/-)
1 04/05/16 17:20 04/05/16 14:12 pCi/g 0.0922 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.0971 0.0574 0.0574 U
-0.000174 Americium 241 pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.371 0.387 0.371 1.05 Bismuth 212 pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.0609 0.118 0.0892 0.745 Bismuth 214 pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.0636 0.157 0.0789 1.05 Lead 212 pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.0512 0.115 0.0803 0.788 Lead 214 pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.238 2.27 1.19 18.9 Potassium 40 pCi/g 04/05/16 14:12 04/05/16 17:20 1
1.05 0.626 0.625 U
-0.292 Protactinium 231 pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.0609 1.00 0.118 0.0892 0.745 Radium 226 pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.805 1.00 0.296 0.286 U
0.755 Thorium 234 pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.219 0.131 0.131 U
0.0743 Uranium 235 pCi/g 04/05/16 14:12 04/05/16 17:20 1
5.21 1.99 1.98 U
1.71 Protactinium 234m pCi/g 04/05/16 14:12 04/05/16 17:20 1
0.0922 0.155 0.108 1.08 Thorium 232 Tl-208 0.333 0.0455 0.0571 0.0308 pCi/g 04/05/16 14:12 04/05/16 17:20 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16768-1 Client Sample ID: L08-09-10-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:20 Percent Solids: 80.6 Date Received: 04/01/16 15:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00062 0.000064 0.000019 mg/Kg
04/04/16 10:02 04/05/16 13:28 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 10.7 (2+/-)
0.986 (2+/-)
1 04/05/16 13:28 04/04/16 10:02 pCi/g 0.219 1.28 RL MDC 0.0854 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/04/16 10:02 04/05/16 13:28 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 97 Lab Sample ID: 160-16768-2 Client Sample ID: L08-09-11-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:40 Date Received: 04/01/16 15:30 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.14 (2+/-)
0.170 (2+/-)
1 04/05/16 17:21 04/05/16 14:12 pCi/g 0.0833 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.0917 0.0547 0.0547 U
0.0127 Americium 241 pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.315 0.416 0.388 1.45 Bismuth 212 pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.0632 0.110 0.0840 0.686 Bismuth 214 pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.0538 0.147 0.0700 0.999 Lead 212 TestAmerica St. Louis Page 10 of 21 1
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Client Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16768-2 Client Sample ID: L08-09-11-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:40 Date Received: 04/01/16 15:30 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.755 (2+/-)
0.109 (2+/-)
1 04/05/16 17:21 04/05/16 14:12 pCi/g 0.0663 RL MDC 0.0756 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.388 2.07 1.07 17.3 Potassium 40 pCi/g 04/05/16 14:12 04/05/16 17:21 1
1.01 0.205 0.200 U
0.416 Protactinium 231 pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.0632 1.00 0.110 0.0840 0.686 Radium 226 pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.748 1.00 0.266 0.250 0.869 Thorium 234 pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.164 0.0849 0.0840 U
0.119 Uranium 235 pCi/g 04/05/16 14:12 04/05/16 17:21 1
4.62 2.95 2.95 U
0.000 Protactinium 234m pCi/g 04/05/16 14:12 04/05/16 17:21 1
0.0833 0.170 0.124 1.14 Thorium 232 Tl-208 0.307 0.0488 0.0582 0.0372 pCi/g 04/05/16 14:12 04/05/16 17:21 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16768-2 Client Sample ID: L08-09-11-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:40 Percent Solids: 81.2 Date Received: 04/01/16 15:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00017 0.000065 0.000019 mg/Kg
04/04/16 10:02 04/05/16 13:32 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 2.90 (2+/-)
0.342 (2+/-)
1 04/05/16 13:32 04/04/16 10:02 pCi/g 0.221 1.29 RL MDC 0.214 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/04/16 10:02 04/05/16 13:32 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 94 Lab Sample ID: 160-16768-3 Client Sample ID: L08-09-12-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:30 Date Received: 04/01/16 15:30 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.31 (2+/-)
0.196 (2+/-)
1 04/05/16 17:58 04/05/16 14:12 pCi/g 0.139 RL MDC 0.144 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.110 0.0656 0.0656 U
0.0149 Americium 241 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.400 0.395 0.360 1.56 Bismuth 212 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0728 0.131 0.101 0.795 Bismuth 214 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0590 0.191 0.0800 1.34 Lead 212 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0772 0.135 0.0888 0.981 Lead 214 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.319 2.19 1.14 18.3 Potassium 40 pCi/g 04/05/16 14:12 04/05/16 17:58 1
1.04 0.281 0.272 U
0.637 Protactinium 231 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0728 1.00 0.131 0.101 0.795 Radium 226 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.788 1.00 0.585 0.575 1.04 Thorium 234 TestAmerica St. Louis Page 11 of 21 1
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Client Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16768-3 Client Sample ID: L08-09-12-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:30 Date Received: 04/01/16 15:30 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Uranium 235 0.285 (2+/-)
0.160 (2+/-)
1 04/05/16 17:58 04/05/16 14:12 pCi/g 0.187 RL MDC 0.157 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/05/16 14:12 04/05/16 17:58 1
5.50 3.19 3.19 U
1.44 Protactinium 234m pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.139 0.196 0.144 1.31 Thorium 232 Pb-210 2.10 0.767 0.805 0.900 pCi/g 04/05/16 14:12 04/05/16 17:58 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.443 0.0524 0.0697 0.0362 pCi/g 04/05/16 14:12 04/05/16 17:58 1
Lab Sample ID: 160-16768-3 Client Sample ID: L08-09-12-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:30 Percent Solids: 64.6 Date Received: 04/01/16 15:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 ND 0.000086 0.000026 mg/Kg
04/04/16 10:02 04/05/16 13:36 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.194 U (2+/-)
0.159 (2+/-)
1 04/05/16 13:36 04/04/16 10:02 pCi/g 0.294 1.72 RL MDC 0.158 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/04/16 10:02 04/05/16 13:36 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 92 Lab Sample ID: 160-16768-4 Client Sample ID: L08-09-13-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:25 Date Received: 04/01/16 15:30 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.929 (2+/-)
0.162 (2+/-)
1 04/05/16 17:59 04/05/16 14:12 pCi/g 0.118 RL MDC 0.132 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.0754 0.0443 0.0443 U
0.00551 Americium 241 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.466 0.523 0.508 1.20 Bismuth 212 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.0758 0.131 0.104 0.764 Bismuth 214 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.0704 0.160 0.0852 1.05 Lead 212 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.0669 0.123 0.0831 0.868 Lead 214 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.359 2.18 1.24 17.5 Potassium 40 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.944 0.285 0.270 U
0.824 Protactinium 231 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.0758 1.00 0.131 0.104 0.764 Radium 226 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.875 1.00 0.303 0.293 U
0.720 Thorium 234 pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.229 0.140 0.140 U
0.102 Uranium 235 pCi/g 04/05/16 14:12 04/05/16 17:59 1
5.44 2.60 2.57 U
3.86 Protactinium 234m pCi/g 04/05/16 14:12 04/05/16 17:59 1
0.118 0.162 0.132 0.929 Thorium 232 TestAmerica St. Louis Page 12 of 21 1
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Client Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16768-4 Client Sample ID: L08-09-13-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:25 Date Received: 04/01/16 15:30 Tl-208 0.322 0.0543 0.0637 0.0405 pCi/g 04/05/16 14:12 04/05/16 17:59 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16768-4 Client Sample ID: L08-09-13-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:25 Percent Solids: 76.1 Date Received: 04/01/16 15:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000055 J 0.000069 0.000021 mg/Kg
04/04/16 10:02 04/05/16 13:41 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.947 (2+/-)
0.0941 (2+/-)
1 04/05/16 13:41 04/04/16 10:02 pCi/g 0.236 1.38 RL MDC 0.0354 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/04/16 10:02 04/05/16 13:41 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 96 Lab Sample ID: 160-16768-5 Client Sample ID: L08-09-14-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:15 Date Received: 04/01/16 15:30 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.950 (2+/-)
0.177 (2+/-)
1 04/05/16 18:00 04/05/16 14:12 pCi/g 0.106 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.0975 0.0574 0.0574 U
0.00142 Americium 241 pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.303 0.358 0.337 1.18 Bismuth 212 pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.0594 0.119 0.0877 0.777 Bismuth 214 pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.0705 0.145 0.0799 0.932 Lead 212 pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.0741 0.126 0.0881 0.864 Lead 214 pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.286 2.34 1.14 20.3 Potassium 40 pCi/g 04/05/16 14:12 04/05/16 18:00 1
1.12 0.292 0.285 U
0.593 Protactinium 231 pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.0594 1.00 0.119 0.0877 0.777 Radium 226 pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.705 1.00 0.480 0.458 1.39 Thorium 234 pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.239 0.124 0.124 U
0.0941 Uranium 235 pCi/g 04/05/16 14:12 04/05/16 18:00 1
4.05 2.58 2.57 U
1.10 Protactinium 234m pCi/g 04/05/16 14:12 04/05/16 18:00 1
0.106 0.177 0.149 0.950 Thorium 232 Tl-208 0.331 0.0438 0.0554 0.0295 pCi/g 04/05/16 14:12 04/05/16 18:00 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 13 of 21 1
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Client Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16768-5 Client Sample ID: L08-09-14-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:15 Percent Solids: 79.2 Date Received: 04/01/16 15:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00020 0.000067 0.000020 mg/Kg
04/04/16 10:02 04/05/16 13:45 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.41 (2+/-)
0.399 (2+/-)
1 04/05/16 13:45 04/04/16 10:02 pCi/g 0.228 1.33 RL MDC 0.247 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 04/04/16 10:02 04/05/16 13:45 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 Lab Sample ID: 160-16768-6 Client Sample ID: L08-09-15-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:35 Date Received: 04/01/16 15:30 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.986 (2+/-)
0.180 (2+/-)
1 04/05/16 17:58 04/05/16 14:12 pCi/g 0.175 RL MDC 0.149 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0936 0.0575 0.0572 U
0.0550 Americium 241 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.438 0.601 0.571 1.82 Bismuth 212 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0781 0.143 0.115 0.820 Bismuth 214 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0878 0.164 0.0998 1.01 Lead 212 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0777 0.136 0.101 0.881 Lead 214 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.275 2.42 1.43 19.1 Potassium 40 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.986 0.591 0.589 U
0.366 Protactinium 231 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.0781 1.00 0.143 0.115 0.820 Radium 226 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.951 1.00 0.613 0.599 1.24 Thorium 234 pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.226 0.00819 0.00819 U
0.00280 Uranium 235 pCi/g 04/05/16 14:12 04/05/16 17:58 1
7.39 4.11 4.11 U
0.565 Protactinium 234m pCi/g 04/05/16 14:12 04/05/16 17:58 1
0.175 0.180 0.149 0.986 Thorium 232 Tl-208 0.374 0.0517 0.0646 0.0271 pCi/g 04/05/16 14:12 04/05/16 17:58 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16768-6 Client Sample ID: L08-09-15-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:35 Percent Solids: 78.2 Date Received: 04/01/16 15:30 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00058 0.000069 0.000021 mg/Kg
04/04/16 10:02 04/05/16 14:02 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 10.0 (2+/-)
0.981 (2+/-)
1 04/05/16 14:02 04/04/16 10:02 pCi/g 0.237 1.39 RL MDC 0.336 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
TestAmerica St. Louis Page 14 of 21 1
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Client Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16768-6 Client Sample ID: L08-09-15-T-E-B-00 Matrix: Solid Date Collected: 03/31/16 09:35 Percent Solids: 78.2 Date Received: 04/01/16 15:30 Re 30 - 110 Carrier 04/04/16 10:02 04/05/16 14:02 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 95 TestAmerica St. Louis Page 15 of 21 1
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QC Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-243510/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244372 Prep Batch: 243510 RL MDL Technetium 99 ND 0.000050 0.000015 mg/Kg 04/04/16 10:02 04/05/16 12:32 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-243510/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244372 Prep Batch: 243510 Technetium 99 0.00119 0.00117 mg/Kg 98 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: Matrix Spike Lab Sample ID: 160-16595-A-1-K MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 244372 Prep Batch: 243510 Technetium 99 0.000036 J 0.00149 0.00148 mg/Kg 97 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-16595-A-1-L MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 244372 Prep Batch: 243510 Technetium 99 0.000036 J 0.00149 0.00149 mg/Kg 98 75 - 125 1
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-243510/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244373 Prep Batch: 243510 Technetium 99 Analyte U
1 04/05/16 12:32 04/04/16 10:02 pCi/g 0.171 MDC 0.998 RL 0.0612 0.0612 (2+/-)
(2+/-)
MB 0.01708 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 04/04/16 10:02 04/05/16 12:32 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 99 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-243510/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244373 Prep Batch: 243510 Technetium 99 Analyte 120 80 98 19.99 20.3 1.94 1.03 0.176 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 97 LCS TestAmerica St. Louis Page 16 of 21 1
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QC Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: Matrix Spike Lab Sample ID: 160-16595-A-1-K MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 244373 Prep Batch: 243510 Technetium 99 Analyte 125 75 97 25.28 25.5 0.611 2.36 1.33 0.227 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 94 MS Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-16595-A-1-L MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 244373 Prep Batch: 243510 Technetium 99 Analyte 1
0.05 125 75 98 25.53 25.5 0.611 2.41 1.36 0.232 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 92 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-244356/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244348 Prep Batch: 244356 Actinium 228 Analyte U
1 04/05/16 17:18 04/05/16 14:12 pCi/g 0.0649 MDC RL 0.0177 0.0176 (2+/-)
(2+/-)
MB 0.009182 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.0200 0.0110 0.0110 U
-0.0009736 Americium 241 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.223 0.125 0.125 U
-0.04009 Bismuth 212 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.0326 0.0588 0.0588 U
-0.007987 Bismuth 214 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.0235 0.0443 0.0443 U
-0.005986 Lead 212 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.0299 0.0661 0.0661 U
-0.007121 Lead 214 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.239 0.282 0.282 U
-0.03113 Potassium 40 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.262 0.146 0.146 U
0.04953 Protactinium 231 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.0326 1.00 0.0588 0.0588 U
-0.007987 Radium 226 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.258 1.00 1.19 1.19 U
-0.1737 Thorium 234 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.0811 0.0222 0.0222 U
-0.002583 Uranium 235 1
04/05/16 17:18 04/05/16 14:12 pCi/g 1.26 13.3 13.3 U
-0.3313 Protactinium 234m 1
04/05/16 17:18 04/05/16 14:12 pCi/g 0.0649 0.0177 0.0176 U
0.009182 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 04/05/16 14:12 04/05/16 17:18 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 17 of 21 1
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QC Sample Results TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-244356/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 244351 Prep Batch: 244356 Americium 241 Analyte 116 87 103 103.3 101 10.8 0.543 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.1 36.36 3.76 0.200 0.146 pCi/g 107 87 - 120 Cobalt 60 31.7 32.83 3.26 0.0859 pCi/g 104 87 - 115 Client Sample ID: L08-09-10-T-E-B-00 Lab Sample ID: 160-16768-1 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 244352 Prep Batch: 244356 Actinium 228 Analyte 1
0.83 0.8289 1.08 0.149 0.106 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241
-0.00017 4
U 0.001406 U 0.0375 0.0639 pCi/g 0.02 1
Bismuth 212 1.05 1.675 0.404 0.261 pCi/g 0.79 1
Bismuth 214 0.745 0.6520 0.106 0.0574 pCi/g 0.42 1
Lead 212 1.05 0.9677 0.144 0.0591 pCi/g 0.26 1
Lead 214 0.788 0.7946 0.112 0.0641 pCi/g 0.03 1
Potassium 40 18.9 18.07 2.13 0.326 pCi/g 0.19 1
Protactinium 231
-0.292 U 0.3225 U 0.165 0.984 pCi/g 0.78 1
Radium 226 0.745 0.6520 0.106 1.00 0.0574 pCi/g 0.42 1
Thorium 234 0.755 U 1.362 0.509 1.00 0.670 pCi/g 0.75 1
Uranium 235 0.0743 U 0.1121 U 0.123 0.193 pCi/g 0.15 1
Protactinium 234m 1.71 U 1.753 U 2.62 4.36 pCi/g 0.01 1
Thorium 232 1.08 0.8289 0.149 0.106 pCi/g 0.83 1
Tl-208 1
0.13 0.3486 0.333 0.0552 0.0304 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 18 of 21 1
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QC Association Summary TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Metals Prep Batch: 243510 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16595-A-1-K MS Matrix Spike Total/NA Solid None 160-16595-A-1-L MSD Matrix Spike Duplicate Total/NA Solid None 160-16768-1 L08-09-10-T-E-B-00 Total/NA Solid None 160-16768-2 L08-09-11-T-E-B-00 Total/NA Solid None 160-16768-3 L08-09-12-T-E-B-00 Total/NA Solid None 160-16768-4 L08-09-13-T-E-B-00 Total/NA Solid None 160-16768-5 L08-09-14-T-E-B-00 Total/NA Solid None 160-16768-6 L08-09-15-T-E-B-00 Total/NA Solid None LCS 160-243510/2-A Lab Control Sample Total/NA Solid None MB 160-243510/1-A Method Blank Total/NA Analysis Batch: 244372 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 243510 160-16595-A-1-K MS Matrix Spike Total/NA Solid 6020A 243510 160-16595-A-1-L MSD Matrix Spike Duplicate Total/NA Solid 6020A 243510 160-16768-1 L08-09-10-T-E-B-00 Total/NA Solid 6020A 243510 160-16768-2 L08-09-11-T-E-B-00 Total/NA Solid 6020A 243510 160-16768-3 L08-09-12-T-E-B-00 Total/NA Solid 6020A 243510 160-16768-4 L08-09-13-T-E-B-00 Total/NA Solid 6020A 243510 160-16768-5 L08-09-14-T-E-B-00 Total/NA Solid 6020A 243510 160-16768-6 L08-09-15-T-E-B-00 Total/NA Solid 6020A 243510 LCS 160-243510/2-A Lab Control Sample Total/NA Solid 6020A 243510 MB 160-243510/1-A Method Blank Total/NA General Chemistry Analysis Batch: 244119 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-16768-1 L08-09-10-T-E-B-00 Total/NA Solid Moisture 160-16768-1 DU L08-09-10-T-E-B-00 Total/NA Solid Moisture 160-16768-2 L08-09-11-T-E-B-00 Total/NA Solid Moisture 160-16768-3 L08-09-12-T-E-B-00 Total/NA Solid Moisture 160-16768-4 L08-09-13-T-E-B-00 Total/NA Solid Moisture 160-16768-5 L08-09-14-T-E-B-00 Total/NA Solid Moisture 160-16768-6 L08-09-15-T-E-B-00 Total/NA Rad Leach Batch: 243455 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16768-1 L08-09-10-T-E-B-00 Total/NA Solid Dry and Grind 160-16768-1 DU L08-09-10-T-E-B-00 Total/NA Solid Dry and Grind 160-16768-2 L08-09-11-T-E-B-00 Total/NA Solid Dry and Grind 160-16768-3 L08-09-12-T-E-B-00 Total/NA Solid Dry and Grind 160-16768-4 L08-09-13-T-E-B-00 Total/NA Solid Dry and Grind 160-16768-5 L08-09-14-T-E-B-00 Total/NA Solid Dry and Grind 160-16768-6 L08-09-15-T-E-B-00 Total/NA TestAmerica St. Louis Page 19 of 21 1
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QC Association Summary TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Prep Batch: 243510 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16595-A-1-K MS Matrix Spike Total/NA Solid None 160-16595-A-1-L MSD Matrix Spike Duplicate Total/NA Solid None 160-16768-1 L08-09-10-T-E-B-00 Total/NA Solid None 160-16768-2 L08-09-11-T-E-B-00 Total/NA Solid None 160-16768-3 L08-09-12-T-E-B-00 Total/NA Solid None 160-16768-4 L08-09-13-T-E-B-00 Total/NA Solid None 160-16768-5 L08-09-14-T-E-B-00 Total/NA Solid None 160-16768-6 L08-09-15-T-E-B-00 Total/NA Solid None LCS 160-243510/2-A Lab Control Sample Total/NA Solid None MB 160-243510/1-A Method Blank Total/NA Prep Batch: 244356 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 243455 160-16768-1 L08-09-10-T-E-B-00 Total/NA Solid Fill_Geo-0 243455 160-16768-1 DU L08-09-10-T-E-B-00 Total/NA Solid Fill_Geo-0 243455 160-16768-2 L08-09-11-T-E-B-00 Total/NA Solid Fill_Geo-0 243455 160-16768-3 L08-09-12-T-E-B-00 Total/NA Solid Fill_Geo-0 243455 160-16768-4 L08-09-13-T-E-B-00 Total/NA Solid Fill_Geo-0 243455 160-16768-5 L08-09-14-T-E-B-00 Total/NA Solid Fill_Geo-0 243455 160-16768-6 L08-09-15-T-E-B-00 Total/NA Solid Fill_Geo-0 LCS 160-244356/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-244356/1-A Method Blank Total/NA TestAmerica St. Louis Page 20 of 21 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-16768-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 94 160-16595-A-1-K MS Percent Yield (Acceptance Limits)
Matrix Spike 92 160-16595-A-1-L MSD Matrix Spike Duplicate 97 160-16768-1 L08-09-10-T-E-B-00 94 160-16768-2 L08-09-11-T-E-B-00 92 160-16768-3 L08-09-12-T-E-B-00 96 160-16768-4 L08-09-13-T-E-B-00 95 160-16768-5 L08-09-14-T-E-B-00 95 160-16768-6 L08-09-15-T-E-B-00 97 LCS 160-243510/2-A Lab Control Sample 99 MB 160-243510/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 21 of 21 1
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