ML18079A232
| ML18079A232 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 04/19/2016 |
| From: | Swanson M, Vania I Testamerica Labs, Westinghouse |
| To: | Office of Nuclear Material Safety and Safeguards |
| References | |
| HEM-18-8 | |
| Download: ML18079A232 (17) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16635-2 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:
4/19/2016 5:01:24 PM Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-16635-2 Page 2 of 17 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
4 Receipt Checklists.........................................
5 Definitions/Glossary.......................................
6 Method Summary.........................................
7 Sample Summary.........................................
8 Client Sample Results......................................
9 QC Sample Results........................................
14 QC Association Summary...................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16635-2 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16635-2 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)
Report Number: 160-16635-2 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 3/23/2016 11:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 20.0º C.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples L08-09-01-T-R-S-00 (160-16635-1), L08-09-02-T-E-S-00 (160-16635-2), L08-09-03-T-E-S-00 (160-16635-3),
L08-09-04-T-E-S-00 (160-16635-4), L08-09-05-T-E-S-00 (160-16635-5), L08-09-06-T-E-S-00 (160-16635-6), L08-09-07-T-E-S-00 (160-16635-7), L08-09-08-T-E-S-00 (160-16635-8), L08-09-08-T-E-Q-00 (160-16635-9) and L08-09-09-T-E-S-00 (160-16635-10) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were leached on 03/23/2016, prepared on 03/25/2016 and analyzed on 04/15/2016.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 4 I
Page 1 ofll Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain ofCutod ID No.
F-032216-01 Pa e 1/1 Laborato Name:
Project Name:
TA-MO Westinghouse Electric Company C ta t P I 1
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IZ II
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.., IL b Add on c erson:
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a oratory ress:
Clai:kEvers
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13715 Rider Trail North
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Phone Number:
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.E Phone No.
314-810-3336 8 314-298-8566 Sampler Name f; ~ *.** ;
~ Laboratory Contact Person:
~(;'
0 Kyle Weldon
§ ~,:) ~ '.~
E-Ivan Vania Phone No.
708-870-8453 Turn Around Time Rush (7 days)
Sample ID Date Time Matrix Remarks L08-09-01-T-R-S-OO 3/22/2016 14:35 S
1 LSA 08-09 L08-09-02-T-E-S-OO 3/22/2016 14:40 S
G 1 LSA 08-09 L08-09-03-T-E-S-OO 3/22/2016 14:45 S
G 1 LSA 08-09 L08-09-04-T-E-S-OO 3/22/2016 14:50 S
1 LSA 08-09.
L08-09-05-T-E-S-OO 3/22/2016 14:55 S
1 LSA 08-09 L08-09-06-T-E-S-OO 3/22/2016 15:00 S
G 1 LSA 08-09 L08-09-07-T-E-S-OO 3/22/2016 15:05 S
G 1 LSA 08-09 L08-09-08-T-E-S-OO 3/22/2016 15:10 S
G 1 LSA 08-09 L08-09-08-T-E-Q-OO 3/22/2016 15:10 S
G 1 LSA08-09 160-16635 ChainofCustody L08-09-09-T-E-S-OO 3/22/2016 15:15 S
G 1 LSA 08-09 Relinquished by: G-criL'51L<.
~
Company Name:
w£c..-
Received by:
Company Name:
e:
o)""> ~
Date/Time 3/ J-?> I Iv l!J :,~
Date/Time Date/Time
'3*,'3- \\lo
,, '. o.:::>
.,, ' IC,-
Date/Time Company Name:
Date/Time Cooler Temperature:
Cooler ID: I Shipper and Number:
2-03 Comments: NIA Veri:fied By: Qc,-e.S'J'.'...l
~14-.._:
Ambient b5l ii, II II II I
- Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16635-2 Login Number: 16635 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time (excluding tests with immediate HTs)
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Qualifiers Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol DOE GA-01-R Radium-226 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 7 of 17 1
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Sample Summary TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-16635-1 L08-09-01-T-R-S-00 Solid 03/22/16 14:35 03/23/16 11:00 160-16635-2 L08-09-02-T-E-S-00 Solid 03/22/16 14:40 03/23/16 11:00 160-16635-3 L08-09-03-T-E-S-00 Solid 03/22/16 14:45 03/23/16 11:00 160-16635-4 L08-09-04-T-E-S-00 Solid 03/22/16 14:50 03/23/16 11:00 160-16635-5 L08-09-05-T-E-S-00 Solid 03/22/16 14:55 03/23/16 11:00 160-16635-6 L08-09-06-T-E-S-00 Solid 03/22/16 15:00 03/23/16 11:00 160-16635-7 L08-09-07-T-E-S-00 Solid 03/22/16 15:05 03/23/16 11:00 160-16635-8 L08-09-08-T-E-S-00 Solid 03/22/16 15:10 03/23/16 11:00 160-16635-9 L08-09-08-T-E-Q-00 Solid 03/22/16 15:10 03/23/16 11:00 160-16635-10 L08-09-09-T-E-S-00 Solid 03/22/16 15:15 03/23/16 11:00 TestAmerica St. Louis Page 8 of 17 1
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Client Sample Results TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-1 Client Sample ID: L08-09-01-T-R-S-00 Matrix: Solid Date Collected: 03/22/16 14:35 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.08 (2+/-)
0.177 (2+/-)
1 04/15/16 10:14 03/25/16 10:27 pCi/g 0.122 RL MDC 0.138 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.368 0.394 0.379 1.04 Bismuth 212 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.0700 0.149 0.105 1.01 Bismuth 214 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.0673 0.158 0.0805 1.05 Lead 212 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.0594 0.156 0.0890 1.23 Lead 214 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.261 1.96 0.988 16.5 Potassium 40 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.997 0.235 0.229 U
0.464 Protactinium 231 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.0700 1.00 0.149 0.105 1.01 Radium 226 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.122 0.177 0.138 1.08 Thorium 232 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.755 0.513 0.487 1.52 Thorium 234 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.213 0.136 0.136 U
0.132 Uranium 235 pCi/g 03/25/16 10:27 04/15/16 10:14 1
0.0869 0.0518 0.0517 U
0.00970 Americium 241 pCi/g 03/25/16 10:27 04/15/16 10:14 1
4.51 2.70 2.69 U
1.97 Protactinium 234m Pb-210 1.42 0.499 0.526 0.653 pCi/g 03/25/16 10:27 04/15/16 10:14 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.294 0.0417 0.0517 0.0343 pCi/g 03/25/16 10:27 04/15/16 10:14 1
Lab Sample ID: 160-16635-2 Client Sample ID: L08-09-02-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:40 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.12 (2+/-)
0.185 (2+/-)
1 04/15/16 10:20 03/25/16 10:27 pCi/g 0.148 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.380 0.500 0.468 1.68 Bismuth 212 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.0597 0.176 0.122 1.21 Bismuth 214 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.0943 0.172 0.106 1.05 Lead 212 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.0749 0.181 0.116 1.34 Lead 214 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.397 2.31 1.37 18.2 Potassium 40 pCi/g 03/25/16 10:27 04/15/16 10:20 1
1.44 0.214 0.209 U
0.381 Protactinium 231 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.0597 1.00 0.176 0.122 1.21 Radium 226 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.148 0.185 0.146 1.12 Thorium 232 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.886 0.328 0.313 0.930 Thorium 234 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.220 0.139 0.139 U
0.0991 Uranium 235 pCi/g 03/25/16 10:27 04/15/16 10:20 1
0.119 0.0716 0.0716 U
0.0282 Americium 241 pCi/g 03/25/16 10:27 04/15/16 10:20 1
7.30 2.86 2.80 U
6.17 Protactinium 234m Tl-208 0.358 0.0543 0.0658 0.0379 pCi/g 03/25/16 10:27 04/15/16 10:20 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-3 Client Sample ID: L08-09-03-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:45 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.998 (2+/-)
0.165 (2+/-)
1 04/15/16 11:16 03/25/16 10:27 pCi/g 0.0838 RL MDC 0.130 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.386 0.309 0.294 0.940 Bismuth 212 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0567 0.157 0.0978 1.19 Bismuth 214 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0625 0.147 0.0728 0.990 Lead 212 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0657 0.155 0.0838 1.25 Lead 214 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.237 2.12 1.01 18.2 Potassium 40 pCi/g 03/25/16 10:27 04/15/16 11:16 1
1.01 0.253 0.245 U
0.589 Protactinium 231 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0567 1.00 0.157 0.0978 1.19 Radium 226 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0838 0.165 0.130 0.998 Thorium 232 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.786 0.302 0.279 1.10 Thorium 234 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.148 0.103 0.102 0.187 Uranium 235 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0764 0.0454 0.0454 U
0.00971 Americium 241 pCi/g 03/25/16 10:27 04/15/16 11:16 1
4.31 6.58 6.58 U
-0.739 Protactinium 234m Tl-208 0.311 0.0409 0.0521 0.0318 pCi/g 03/25/16 10:27 04/15/16 11:16 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-4 Client Sample ID: L08-09-04-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:50 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.12 (2+/-)
0.178 (2+/-)
1 04/15/16 11:16 03/25/16 10:27 pCi/g 0.117 RL MDC 0.137 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.349 0.480 0.448 1.65 Bismuth 212 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0632 0.154 0.105 1.09 Bismuth 214 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0628 0.146 0.0747 0.965 Lead 212 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0780 0.138 0.0809 1.07 Lead 214 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.201 2.11 1.10 17.6 Potassium 40 pCi/g 03/25/16 10:27 04/15/16 11:16 1
1.03 0.174 0.172 U
0.228 Protactinium 231 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0632 1.00 0.154 0.105 1.09 Radium 226 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.117 0.178 0.137 1.12 Thorium 232 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.741 0.507 0.483 1.47 Thorium 234 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.247 0.140 0.139 U
0.188 Uranium 235 pCi/g 03/25/16 10:27 04/15/16 11:16 1
0.0944 0.0562 0.0562 U
0.00930 Americium 241 pCi/g 03/25/16 10:27 04/15/16 11:16 1
5.09 2.97 2.89 6.90 Protactinium 234m Tl-208 0.300 0.0461 0.0556 0.0348 pCi/g 03/25/16 10:27 04/15/16 11:16 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-5 Client Sample ID: L08-09-05-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:55 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.999 (2+/-)
0.155 (2+/-)
1 04/15/16 20:25 03/25/16 10:42 pCi/g 0.105 RL MDC 0.116 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.448 0.513 0.491 1.43 Bismuth 212 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.0801 0.160 0.116 1.06 Bismuth 214 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.0786 0.159 0.0862 1.03 Lead 212 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.0797 0.153 0.0944 1.15 Lead 214 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.322 2.09 1.16 17.0 Potassium 40 pCi/g 03/25/16 10:42 04/15/16 20:25 1
1.11 0.324 0.320 U
0.419 Protactinium 231 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.0801 1.00 0.160 0.116 1.06 Radium 226 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.105 0.155 0.116 0.999 Thorium 232 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.847 0.538 0.528 0.975 Thorium 234 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.236 0.136 0.136 U
0.0722 Uranium 235 pCi/g 03/25/16 10:42 04/15/16 20:25 1
0.0930 0.0551 0.0551 U
0.00762 Americium 241 pCi/g 03/25/16 10:42 04/15/16 20:25 1
5.11 3.23 3.21 U
3.39 Protactinium 234m Tl-208 0.384 0.0521 0.0656 0.0382 pCi/g 03/25/16 10:42 04/15/16 20:25 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-6 Client Sample ID: L08-09-06-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:00 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.13 (2+/-)
0.161 (2+/-)
1 04/15/16 06:58 03/25/16 10:42 pCi/g 0.127 RL MDC 0.113 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.243 0.334 0.304 1.35 Bismuth 212 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.0603 0.161 0.101 1.20 Bismuth 214 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.0574 0.161 0.0729 1.11 Lead 212 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.0745 0.169 0.101 1.31 Lead 214 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.264 2.00 0.997 16.9 Potassium 40 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.989 0.600 0.598 U
-0.449 Protactinium 231 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.0603 1.00 0.161 0.101 1.20 Radium 226 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.127 0.161 0.113 1.13 Thorium 232 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.713 0.487 0.462 1.48 Thorium 234 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.229 0.125 0.124 U
0.117 Uranium 235 pCi/g 03/25/16 10:42 04/15/16 06:58 1
0.0924 0.0552 0.0552 U
0.0158 Americium 241 pCi/g 03/25/16 10:42 04/15/16 06:58 1
4.21 2.49 2.49 U
1.63 Protactinium 234m Tl-208 0.360 0.0436 0.0575 0.0314 pCi/g 03/25/16 10:42 04/15/16 06:58 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-7 Client Sample ID: L08-09-07-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:05 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.02 (2+/-)
0.178 (2+/-)
1 04/15/16 07:00 03/25/16 10:42 pCi/g 0.144 RL MDC 0.145 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.419 0.476 0.454 1.38 Bismuth 212 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.0796 0.187 0.134 1.26 Bismuth 214 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.0808 0.168 0.0929 1.08 Lead 212 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.0788 0.173 0.113 1.26 Lead 214 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.246 2.34 1.35 18.6 Potassium 40 pCi/g 03/25/16 10:42 04/15/16 07:00 1
1.46 0.275 0.269 U
0.528 Protactinium 231 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.0796 1.00 0.187 0.134 1.26 Radium 226 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.144 0.178 0.145 1.02 Thorium 232 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.913 0.349 0.326 1.18 Thorium 234 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.272 0.142 0.142 U
0.0725 Uranium 235 pCi/g 03/25/16 10:42 04/15/16 07:00 1
0.122 0.0727 0.0727 U
-0.00795 Americium 241 pCi/g 03/25/16 10:42 04/15/16 07:00 1
7.02 3.92 3.92 U
-0.178 Protactinium 234m Tl-208 0.397 0.0594 0.0723 0.0398 pCi/g 03/25/16 10:42 04/15/16 07:00 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-8 Client Sample ID: L08-09-08-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:10 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.992 (2+/-)
0.148 (2+/-)
1 04/15/16 07:23 03/25/16 10:42 pCi/g 0.116 RL MDC 0.108 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.320 0.408 0.384 1.32 Bismuth 212 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0664 0.141 0.0961 0.994 Bismuth 214 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0597 0.142 0.0718 0.947 Lead 212 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0685 0.147 0.0891 1.13 Lead 214 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.255 2.05 1.01 17.5 Potassium 40 pCi/g 03/25/16 10:42 04/15/16 07:23 1
1.08 0.187 0.183 U
0.344 Protactinium 231 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0664 1.00 0.141 0.0961 0.994 Radium 226 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.116 0.148 0.108 0.992 Thorium 232 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.841 0.346 0.300 1.64 Thorium 234 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.187 0.151 0.137 0.629 Uranium 235 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0960 0.0570 0.0570 U
0.00360 Americium 241 pCi/g 03/25/16 10:42 04/15/16 07:23 1
4.41 2.33 2.29 4.42 Protactinium 234m Tl-208 0.312 0.0457 0.0560 0.0364 pCi/g 03/25/16 10:42 04/15/16 07:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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Client Sample Results TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-9 Client Sample ID: L08-09-08-T-E-Q-00 Matrix: Solid Date Collected: 03/22/16 15:10 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.990 (2+/-)
0.180 (2+/-)
1 04/15/16 07:23 03/25/16 10:42 pCi/g 0.0875 RL MDC 0.148 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.412 0.425 0.415 0.869 Bismuth 212 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0753 0.155 0.112 1.04 Bismuth 214 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0615 0.148 0.0751 0.987 Lead 212 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0784 0.142 0.0938 1.03 Lead 214 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.384 2.00 1.13 16.2 Potassium 40 pCi/g 03/25/16 10:42 04/15/16 07:23 1
1.05 0.257 0.253 U
0.401 Protactinium 231 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0753 1.00 0.155 0.112 1.04 Radium 226 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.0875 0.180 0.148 0.990 Thorium 232 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.767 0.334 0.297 1.45 Thorium 234 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.209 0.179 0.172 0.486 Uranium 235 pCi/g 03/25/16 10:42 04/15/16 07:23 1
0.102 0.0606 0.0606 U
0.00857 Americium 241 pCi/g 03/25/16 10:42 04/15/16 07:23 1
5.00 3.04 3.03 U
2.36 Protactinium 234m Tl-208 0.315 0.0478 0.0579 0.0378 pCi/g 03/25/16 10:42 04/15/16 07:23 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-10 Client Sample ID: L08-09-09-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:15 Date Received: 03/23/16 11:00 Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.33 (2+/-)
0.198 (2+/-)
1 04/15/16 07:32 03/25/16 10:42 pCi/g 0.0988 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.489 0.368 0.355 0.951 Bismuth 212 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.0599 0.182 0.114 1.38 Bismuth 214 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.0746 0.175 0.0811 1.20 Lead 212 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.0801 0.182 0.114 1.36 Lead 214 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.435 2.65 1.31 22.9 Potassium 40 pCi/g 03/25/16 10:42 04/15/16 07:32 1
1.28 0.784 0.780 U
-0.677 Protactinium 231 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.0599 1.00 0.182 0.114 1.38 Radium 226 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.0988 0.198 0.146 1.33 Thorium 232 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.880 0.577 0.558 1.41 Thorium 234 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.268 0.133 0.133 U
0.0595 Uranium 235 pCi/g 03/25/16 10:42 04/15/16 07:32 1
0.0925 0.0543 0.0543 U
0.00200 Americium 241 pCi/g 03/25/16 10:42 04/15/16 07:32 1
5.37 3.25 3.24 U
2.36 Protactinium 234m Tl-208 0.431 0.0526 0.0688 0.0365 pCi/g 03/25/16 10:42 04/15/16 07:32 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
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QC Sample Results TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-242280/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246244 Prep Batch: 242280 Actinium 228 Analyte U
1 04/15/16 07:36 03/25/16 10:27 pCi/g 0.0810 MDC RL 0.0100 0.00999 (2+/-)
(2+/-)
MB 0.008588 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.130 0.0862 0.0862 U
0.0000 Bismuth 212 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.0436 0.0282 0.0281 U
0.02906 Bismuth 214 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.0305 0.376 0.376 U
-0.009404 Lead 212 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.0374 0.0208 0.0208 U
-0.0004122 Lead 214 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.237 2.33 2.33 U
-0.05829 Potassium 40 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.340 0.179 0.179 U
-0.03237 Protactinium 231 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.0436 1.00 0.0282 0.0281 U
0.02906 Radium 226 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.0810 0.0100 0.00999 U
0.008588 Thorium 232 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.249 0.0192 0.0192 U
0.004998 Thorium 234 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.0816 0.0434 0.0434 U
0.009160 Uranium 235 1
04/15/16 07:36 03/25/16 10:27 pCi/g 0.0323 0.00864 0.00864 U
0.0000 Americium 241 1
04/15/16 07:36 03/25/16 10:27 pCi/g 3.73 0.424 0.424 U
0.0000 Protactinium 234m Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 03/25/16 10:27 04/15/16 07:36 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242280/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246245 Prep Batch: 242280 Americium 241 Analyte 116 87 100 100.9 101 10.5 0.497 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.0 33.32 3.49 0.148 pCi/g 98 87 - 120 Cobalt 60 31.6 30.16 3.04 0.120 pCi/g 96 87 - 115 Client Sample ID: Duplicate Lab Sample ID: 160-16620-A-4-G DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 246245 Prep Batch: 242280 Actinium 228 Analyte 1
0.08 0.5748 0.590 0.0917 0.0691 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 0.651 0.8581 0.305 0.247 pCi/g 0.34 1
Bismuth 214 0.641 0.6216 0.0888 0.0359 pCi/g 0.10 1
Lead 212 0.555 0.5135 0.0807 0.0403 pCi/g 0.25 1
Lead 214 0.650 0.6611 0.0882 0.0501 pCi/g 0.06 1
Potassium 40 12.3 13.20 1.56 0.238 pCi/g 0.29 1
Protactinium 231 0.278 U 0.3107 U 0.150 0.707 pCi/g 0.10 1
Radium 226 0.641 0.6216 0.0888 1.00 0.0359 pCi/g 0.10 1
Thorium 232 0.590 0.5748 0.0917 0.0691 pCi/g 0.08 1
Thorium 234 0.380 U 0.9516 0.369 0.475 pCi/g 1.03 1
Uranium 235 0.0779 U 0.04151 U 0.0944 0.158 pCi/g 0.19 1
Americium 241 0.00222 U 0.008093 U 0.0396 0.0665 pCi/g 0.07 1
TestAmerica St. Louis Page 14 of 17 1
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QC Sample Results TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Duplicate Lab Sample ID: 160-16620-A-4-G DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 246245 Prep Batch: 242280 Protactinium 234m Analyte 1
1.08 U
2.554 0.235 U 1.21 3.20 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Tl-208 1
0.08 0.1775 0.183 0.0357 0.0252 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides Client Sample ID: Method Blank Lab Sample ID: MB 160-242281/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246245 Prep Batch: 242281 Actinium 228 Analyte U
1 04/15/16 06:38 03/25/16 10:42 pCi/g 0.0537 MDC RL 0.0143 0.0143 (2+/-)
(2+/-)
MB 0.001595 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.114 0.0689 0.0688 U
0.04828 Bismuth 212 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.0348 0.00935 0.00934 U
0.005814 Bismuth 214 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.0253 0.0386 0.0386 U
-0.004668 Lead 212 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.0345 0.455 0.455 U
-0.01138 Lead 214 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.190 0.101 0.101 U
-0.009403 Potassium 40 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.331 0.0512 0.0512 U
-0.01259 Protactinium 231 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.0348 1.00 0.00935 0.00934 U
0.005814 Radium 226 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.0537 0.0143 0.0143 U
0.001595 Thorium 232 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.257 0.0777 0.0773 U
0.08018 Thorium 234 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.0604 2.80 2.80 U
-0.007672 Uranium 235 1
04/15/16 06:38 03/25/16 10:42 pCi/g 0.0239 0.0132 0.0132 U
-0.0002380 Americium 241 1
04/15/16 06:38 03/25/16 10:42 pCi/g 2.35 13.7 13.7 U
-0.3414 Protactinium 234m Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 03/25/16 10:42 04/15/16 06:38 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242281/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 246248 Prep Batch: 242281 Americium 241 Analyte 116 87 100 100.6 101 10.5 0.494 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.0 32.78 3.43 0.167 pCi/g 96 87 - 120 Cobalt 60 31.6 30.47 3.08 0.103 pCi/g 97 87 - 115 TestAmerica St. Louis Page 15 of 17 1
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QC Sample Results TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Radium-226 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: L08-09-05-T-E-S-00 Lab Sample ID: 160-16635-5 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 246252 Prep Batch: 242281 Actinium 228 Analyte 1
0.19 1.057 0.999 0.155 0.0999 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Bismuth 212 1.43 1.660 0.450 0.335 pCi/g 0.24 1
Bismuth 214 1.06 1.039 0.147 0.0654 pCi/g 0.07 1
Lead 212 1.03 1.016 0.151 0.0592 pCi/g 0.05 1
Lead 214 1.15 1.168 0.149 0.0603 pCi/g 0.05 1
Potassium 40 17.0 17.01 2.02 0.307 pCi/g 0
1 Protactinium 231 0.419 U 0.4599 U 0.225 1.00 pCi/g 0.07 1
Radium 226 1.06 1.039 0.147 1.00 0.0654 pCi/g 0.07 1
Thorium 232 0.999 1.057 0.155 0.0999 pCi/g 0.19 1
Thorium 234 0.975 1.404 0.504 0.750 pCi/g 0.41 1
Uranium 235 0.0722 U 0.1638 U 0.138 0.217 pCi/g 0.33 1
Americium 241 0.00762 U 0.008649 U 0.0568 0.0955 pCi/g 0.01 1
Protactinium 234m 3.39 U 0.5395 U 2.45 4.36 pCi/g 0.50 1
Tl-208 1
0.67 0.3048 0.384 0.0535 0.0332 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 16 of 17 1
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QC Association Summary TestAmerica Job ID: 160-16635-2 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Rad Leach Batch: 241585 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16620-A-4-G DU Duplicate Total/NA Leach Batch: 241804 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16635-1 L08-09-01-T-R-S-00 Total/NA Solid Dry and Grind 160-16635-2 L08-09-02-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-3 L08-09-03-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-4 L08-09-04-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-5 L08-09-05-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-5 DU L08-09-05-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-6 L08-09-06-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-7 L08-09-07-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-8 L08-09-08-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-9 L08-09-08-T-E-Q-00 Total/NA Solid Dry and Grind 160-16635-10 L08-09-09-T-E-S-00 Total/NA Prep Batch: 242280 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 241585 160-16620-A-4-G DU Duplicate Total/NA Solid Fill_Geo-21 241804 160-16635-1 L08-09-01-T-R-S-00 Total/NA Solid Fill_Geo-21 241804 160-16635-2 L08-09-02-T-E-S-00 Total/NA Solid Fill_Geo-21 241804 160-16635-3 L08-09-03-T-E-S-00 Total/NA Solid Fill_Geo-21 241804 160-16635-4 L08-09-04-T-E-S-00 Total/NA Solid Fill_Geo-21 LCS 160-242280/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-242280/1-A Method Blank Total/NA Prep Batch: 242281 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-21 241804 160-16635-5 L08-09-05-T-E-S-00 Total/NA Solid Fill_Geo-21 241804 160-16635-5 DU L08-09-05-T-E-S-00 Total/NA Solid Fill_Geo-21 241804 160-16635-6 L08-09-06-T-E-S-00 Total/NA Solid Fill_Geo-21 241804 160-16635-7 L08-09-07-T-E-S-00 Total/NA Solid Fill_Geo-21 241804 160-16635-8 L08-09-08-T-E-S-00 Total/NA Solid Fill_Geo-21 241804 160-16635-9 L08-09-08-T-E-Q-00 Total/NA Solid Fill_Geo-21 241804 160-16635-10 L08-09-09-T-E-S-00 Total/NA Solid Fill_Geo-21 LCS 160-242281/2-A Lab Control Sample Total/NA Solid Fill_Geo-21 MB 160-242281/1-A Method Blank Total/NA TestAmerica St. Louis Page 17 of 17 1
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