ML18079A231
| ML18079A231 | |
| Person / Time | |
|---|---|
| Site: | 07000036 |
| Issue date: | 03/30/2016 |
| From: | Ridenhower R, Swanson M, Vania I Testamerica Labs, Westinghouse |
| To: | Office of Nuclear Material Safety and Safeguards |
| References | |
| HEM-18-8 | |
| Download: ML18079A231 (26) | |
Text
ANALYTICAL REPORT TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North Earth City, MO 63045 Tel: (314)298-8566 TestAmerica Job ID: 160-16635-1 Client Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
For:
Westinghouse Electric Company LLC 3300 State Road P Festus, Missouri 63028 Attn: Mr. Martin Swanson Authorized for release by:
3/30/2016 9:59:57 AM Rhonda Ridenhower, Manager of Project Management rhonda.ridenhower@testamericainc.com Designee for Ivan Vania, Project Manager II (314)298-8566 ivan.vania@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
TestAmerica Job ID: 160-16635-1 Page 2 of 26 TestAmerica St. Louis 3/30/2016 Cover Page..............................................
1 Table of Contents.........................................
2 Case Narrative...........................................
3 Chain of Custody..........................................
5 Receipt Checklists.........................................
6 Definitions/Glossary.......................................
7 Method Summary.........................................
8 Sample Summary.........................................
9 Client Sample Results......................................
10 QC Sample Results........................................
19 QC Association Summary...................................
23 Tracer Carrier Summary....................................
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16635-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16635-1 Laboratory: TestAmerica St. Louis Narrative CASE NARRATIVE Client: Westinghouse Electric Company LLC Project: HDP RFP-CBA-022 (7 DAY TAT)
Report Number: 160-16635-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmericas operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT The samples were received on 03/23/2016; the samples arrived in good condition, properly preserved. The temperature of the coolers at receipt was 20.0 C.
TECHNETIUM-99 (ICPMS)
Samples L08-09-01-T-R-S-00 (160-16635-1), L08-09-02-T-E-S-00 (160-16635-2), L08-09-03-T-E-S-00 (160-16635-3),
L08-09-04-T-E-S-00 (160-16635-4), L08-09-05-T-E-S-00 (160-16635-5), L08-09-06-T-E-S-00 (160-16635-6), L08-09-07-T-E-S-00 (160-16635-7), L08-09-08-T-E-S-00 (160-16635-8), L08-09-08-T-E-Q-00 (160-16635-9) and L08-09-09-T-E-S-00 (160-16635-10) were analyzed for Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared on 03/24/2016 and analyzed on 03/28/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
PERCENT SOLIDS Samples L08-09-01-T-R-S-00 (160-16635-1), L08-09-02-T-E-S-00 (160-16635-2), L08-09-03-T-E-S-00 (160-16635-3),
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Case Narrative Client: Westinghouse Electric Company LLC TestAmerica Job ID: 160-16635-1 Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Job ID: 160-16635-1 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
L08-09-04-T-E-S-00 (160-16635-4), L08-09-05-T-E-S-00 (160-16635-5), L08-09-06-T-E-S-00 (160-16635-6), L08-09-07-T-E-S-00 (160-16635-7), L08-09-08-T-E-S-00 (160-16635-8), L08-09-08-T-E-Q-00 (160-16635-9) and L08-09-09-T-E-S-00 (160-16635-10) were analyzed for percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 03/24/2016.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CESIUM-137 & OTHER GAMMA EMITTERS (GS)
Samples L08-09-01-T-R-S-00 (160-16635-1), L08-09-02-T-E-S-00 (160-16635-2), L08-09-03-T-E-S-00 (160-16635-3),
L08-09-04-T-E-S-00 (160-16635-4), L08-09-05-T-E-S-00 (160-16635-5), L08-09-06-T-E-S-00 (160-16635-6), L08-09-07-T-E-S-00 (160-16635-7), L08-09-08-T-E-S-00 (160-16635-8), L08-09-08-T-E-Q-00 (160-16635-9) and L08-09-09-T-E-S-00 (160-16635-10) were analyzed for Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were dried on 03/23/2016, prepared on 03/25/2016 and analyzed on 03/27/2016.
Prep Batch 242189 Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214.
Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved.L08-09-01-T-R-S-00 (160-16635-1), L08-09-02-T-E-S-00 (160-16635-2),
L08-09-03-T-E-S-00 (160-16635-3), L08-09-04-T-E-S-00 (160-16635-4), (LCS 160-242189/2-A), (MB 160-242189/1-A), (160-16620-A-4-D) and (160-16620-A-4-E DU)
Prep Batch 242193 Radium-226 is reported in these samples at the client's request. Radium-226 is reported from the 609.31 keV line of bismuth-214.
Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved.L08-09-05-T-E-S-00 (160-16635-5), L08-09-06-T-E-S-00 (160-16635-6),
L08-09-07-T-E-S-00 (160-16635-7), L08-09-08-T-E-S-00 (160-16635-8), L08-09-08-T-E-Q-00 (160-16635-9), L08-09-09-T-E-S-00 (160-16635-10), (LCS 160-242193/2-A), (MB 160-242193/1-A) and (160-16635-A-5-E DU)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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10 11 12 Procedure HDP-PR-QA-006, Chain of Custody Hematite Decommissioning Project !Revision: 4 I
Page 1 ofll Westinghouse Non-Proprietary Class 3 FORM HDP-PR-QA-006-1 CHAIN OF CUSTODY Instructions: Each time the container is transferred to another organization, a person from each organization should sign the CoC. The Laboratory/End User must verify that the sample is correctly identified before the sample is released for use or analysis and send the completed CoC to HDP.
Chain ofCutod ID No.
F-032216-01 Pa e 1/1 Laborato Name:
Project Name:
TA-MO Westinghouse Electric Company C ta t P I 1
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IZ II
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.., IL b Add on c erson:
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a oratory ress:
Clai:kEvers
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13715 Rider Trail North
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Phone Number:
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.E Phone No.
314-810-3336 8 314-298-8566 Sampler Name f; ~ *.** ;
~ Laboratory Contact Person:
~(;'
0 Kyle Weldon
§ ~,:) ~ '.~
E-Ivan Vania Phone No.
708-870-8453 Turn Around Time Rush (7 days)
Sample ID Date Time Matrix Remarks L08-09-01-T-R-S-OO 3/22/2016 14:35 S
1 LSA 08-09 L08-09-02-T-E-S-OO 3/22/2016 14:40 S
G 1 LSA 08-09 L08-09-03-T-E-S-OO 3/22/2016 14:45 S
G 1 LSA 08-09 L08-09-04-T-E-S-OO 3/22/2016 14:50 S
1 LSA 08-09.
L08-09-05-T-E-S-OO 3/22/2016 14:55 S
1 LSA 08-09 L08-09-06-T-E-S-OO 3/22/2016 15:00 S
G 1 LSA 08-09 L08-09-07-T-E-S-OO 3/22/2016 15:05 S
G 1 LSA 08-09 L08-09-08-T-E-S-OO 3/22/2016 15:10 S
G 1 LSA 08-09 L08-09-08-T-E-Q-OO 3/22/2016 15:10 S
G 1 LSA08-09 160-16635 ChainofCustody L08-09-09-T-E-S-OO 3/22/2016 15:15 S
G 1 LSA 08-09 Relinquished by: G-criL'51L<.
~
Company Name:
w£c..-
Received by:
Company Name:
e:
o)""> ~
Date/Time 3/ J-?> I Iv l!J :,~
Date/Time Date/Time
'3*,'3- \\lo
,, '. o.:::>
.,, ' IC,-
Date/Time Company Name:
Date/Time Cooler Temperature:
Cooler ID: I Shipper and Number:
2-03 Comments: NIA Veri:fied By: Qc,-e.S'J'.'...l
~14-.._:
Ambient b5l ii, II II II I
- Login Sample Receipt Checklist Client: Westinghouse Electric Company LLC Job Number: 160-16635-1 Login Number: 16635 Question Answer Comment Creator: Dedner, Connie L List Source: TestAmerica St. Louis List Number: 1 True Radioactivity wasn't checked or is </= background as measured by a survey meter.
True The cooler's custody seal, if present, is intact.
N/A Sample custody seals, if present, are intact.
True The cooler or samples do not appear to have been compromised or tampered with.
N/A Samples were received on ice.
True Cooler Temperature is acceptable.
True Cooler Temperature is recorded.
True COC is present.
True COC is filled out in ink and legible.
True COC is filled out with all pertinent information.
True Is the Field Sampler's name present on COC?
True There are no discrepancies between the containers received and the COC.
True Samples are received within Holding Time (excluding tests with immediate HTs)
True Sample containers have legible labels.
True Containers are not broken or leaking.
True Sample collection date/times are provided.
True Appropriate sample containers are used.
True Sample bottles are completely filled.
True Sample Preservation Verified.
True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs N/A Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True Multiphasic samples are not present.
True Samples do not require splitting or compositing.
N/A Residual Chlorine Checked.
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Definitions/Glossary TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Qualifiers Metals Qualifier Description J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier Rad Qualifier Description U
Result is less than the sample detection limit.
Qualifier Glossary These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation
%R Percent Recovery CFL Contains Free Liquid CNF Contains no Free Liquid DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision level concentration MDA Minimum detectable activity EDL Estimated Detection Limit MDC Minimum detectable concentration MDL Method Detection Limit ML Minimum Level (Dioxin)
NC Not Calculated ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit QC Quality Control RER Relative error ratio RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method Summary TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method Method Description Laboratory Protocol SW846 6020A Metals (ICP/MS), Tc-99 TAL SL EPA Moisture Percent Moisture TAL SL SW846 6020A Metals (ICP/MS), Tc-99 in Activity TAL SL DOE GA-01-R Cesium-137 & Other Gamma Emitters (GS)
TAL SL Protocol
References:
DOE = U.S. Department of Energy EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory
References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566 TestAmerica St. Louis Page 8 of 26 3/30/2016 1
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Sample Summary TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID Client Sample ID Received Collected Matrix 160-16635-1 L08-09-01-T-R-S-00 Solid 03/22/16 14:35 03/23/16 11:00 160-16635-2 L08-09-02-T-E-S-00 Solid 03/22/16 14:40 03/23/16 11:00 160-16635-3 L08-09-03-T-E-S-00 Solid 03/22/16 14:45 03/23/16 11:00 160-16635-4 L08-09-04-T-E-S-00 Solid 03/22/16 14:50 03/23/16 11:00 160-16635-5 L08-09-05-T-E-S-00 Solid 03/22/16 14:55 03/23/16 11:00 160-16635-6 L08-09-06-T-E-S-00 Solid 03/22/16 15:00 03/23/16 11:00 160-16635-7 L08-09-07-T-E-S-00 Solid 03/22/16 15:05 03/23/16 11:00 160-16635-8 L08-09-08-T-E-S-00 Solid 03/22/16 15:10 03/23/16 11:00 160-16635-9 L08-09-08-T-E-Q-00 Solid 03/22/16 15:10 03/23/16 11:00 160-16635-10 L08-09-09-T-E-S-00 Solid 03/22/16 15:15 03/23/16 11:00 TestAmerica St. Louis Page 9 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-1 Client Sample ID: L08-09-01-T-R-S-00 Matrix: Solid Date Collected: 03/22/16 14:35 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.15 (2+/-)
0.177 (2+/-)
1 03/27/16 18:25 03/25/16 10:27 pCi/g 0.104 RL MDC 0.133 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.102 0.0612 0.0612 U
-0.0140 Americium 241 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.387 0.407 0.394 0.992 Bismuth 212 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.0591 0.123 0.0865 0.845 Bismuth 214 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.0597 0.150 0.0722 1.02 Lead 212 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.0558 0.125 0.0756 0.955 Lead 214 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.245 1.99 0.968 17.0 Potassium 40 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.980 0.205 0.200 U
0.426 Protactinium 231 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.0591 1.00 0.123 0.0865 0.845 Radium 226 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.724 1.00 0.484 0.465 1.30 Thorium 234 pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.221 0.132 0.131 U
0.111 Uranium 235 pCi/g 03/25/16 10:27 03/27/16 18:25 1
4.34 2.66 2.65 U
2.56 Protactinium 234m pCi/g 03/25/16 10:27 03/27/16 18:25 1
0.104 0.177 0.133 1.15 Thorium 232 Tl-208 0.360 0.0456 0.0590 0.0320 pCi/g 03/25/16 10:27 03/27/16 18:25 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-1 Client Sample ID: L08-09-01-T-R-S-00 Matrix: Solid Date Collected: 03/22/16 14:35 Percent Solids: 83.3 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000096 0.000065 0.000019 mg/Kg
03/24/16 08:53 03/28/16 14:32 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.64 (2+/-)
0.172 (2+/-)
1 03/28/16 14:32 03/24/16 08:53 pCi/g 0.221 1.29 RL MDC 0.0821 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 14:32 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 89 Lab Sample ID: 160-16635-2 Client Sample ID: L08-09-02-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:40 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.10 (2+/-)
0.195 (2+/-)
1 03/27/16 18:26 03/25/16 10:27 pCi/g 0.146 RL MDC 0.160 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.0984 0.0585 0.0585 U
-0.0107 Americium 241 pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.405 0.474 0.450 1.45 Bismuth 212 pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.0623 0.134 0.0968 0.894 Bismuth 214 pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.0588 0.158 0.0774 1.07 Lead 212 TestAmerica St. Louis Page 10 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-2 Client Sample ID: L08-09-02-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:40 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.927 (2+/-)
0.138 (2+/-)
1 03/27/16 18:26 03/25/16 10:27 pCi/g 0.0760 RL MDC 0.0986 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.409 2.21 1.22 18.0 Potassium 40 pCi/g 03/25/16 10:27 03/27/16 18:26 1
1.02 0.317 0.309 U
0.650 Protactinium 231 pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.0623 1.00 0.134 0.0968 0.894 Radium 226 pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.847 1.00 0.529 0.522 U
0.816 Thorium 234 pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.231 0.128 0.127 U
0.0894 Uranium 235 pCi/g 03/25/16 10:27 03/27/16 18:26 1
5.43 3.15 3.12 U
4.27 Protactinium 234m pCi/g 03/25/16 10:27 03/27/16 18:26 1
0.146 0.195 0.160 1.10 Thorium 232 Pb-210 1.68 0.600 0.632 0.758 pCi/g 03/25/16 10:27 03/27/16 18:26 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.354 0.0431 0.0566 0.0253 pCi/g 03/25/16 10:27 03/27/16 18:26 1
Lab Sample ID: 160-16635-2 Client Sample ID: L08-09-02-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:40 Percent Solids: 81.5 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00039 0.000070 0.000021 mg/Kg
03/24/16 08:53 03/28/16 14:36 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 6.63 (2+/-)
0.626 (2+/-)
1 03/28/16 14:36 03/24/16 08:53 pCi/g 0.240 1.40 RL MDC 0.141 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 14:36 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Lab Sample ID: 160-16635-3 Client Sample ID: L08-09-03-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:45 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.31 (2+/-)
0.186 (2+/-)
1 03/27/16 18:27 03/25/16 10:27 pCi/g 0.135 RL MDC 0.131 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.101 21.8 21.8 U
-0.00852 Americium 241 pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.388 0.429 0.410 1.23 Bismuth 212 pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.0685 0.137 0.0965 0.944 Bismuth 214 pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.0628 0.161 0.0749 1.10 Lead 212 pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.0626 0.145 0.0882 1.10 Lead 214 pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.253 2.46 1.11 21.8 Potassium 40 pCi/g 03/25/16 10:27 03/27/16 18:27 1
1.15 0.280 0.273 U
0.580 Protactinium 231 pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.0685 1.00 0.137 0.0965 0.944 Radium 226 TestAmerica St. Louis Page 11 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-3 Client Sample ID: L08-09-03-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:45 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Thorium 234 1.15 (2+/-)
0.304 (2+/-)
1 03/27/16 18:27 03/25/16 10:27 pCi/g 0.811 1.00 RL MDC 0.279 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.240 0.149 0.148 U
0.145 Uranium 235 pCi/g 03/25/16 10:27 03/27/16 18:27 1
6.25 2.12 2.12 U
0.173 Protactinium 234m pCi/g 03/25/16 10:27 03/27/16 18:27 1
0.135 0.186 0.131 1.31 Thorium 232 Tl-208 0.344 0.0495 0.0608 0.0397 pCi/g 03/25/16 10:27 03/27/16 18:27 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-3 Client Sample ID: L08-09-03-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:45 Percent Solids: 84.5 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00022 0.000068 0.000020 mg/Kg
03/24/16 08:53 03/28/16 14:51 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.82 (2+/-)
0.355 (2+/-)
1 03/28/16 14:51 03/24/16 08:53 pCi/g 0.232 1.35 RL MDC 0.0496 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 14:51 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 88 Lab Sample ID: 160-16635-4 Client Sample ID: L08-09-04-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:50 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.934 (2+/-)
0.143 (2+/-)
1 03/27/16 21:18 03/25/16 10:27 pCi/g 0.0944 RL MDC 0.107 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.0878 0.0524 0.0523 U
0.0115 Americium 241 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.343 0.378 0.362 1.04 Bismuth 212 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.0593 0.118 0.0847 0.797 Bismuth 214 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.0516 0.142 0.0663 0.975 Lead 212 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.0536 0.116 0.0699 0.885 Lead 214 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.241 1.98 0.966 16.9 Potassium 40 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.837 0.241 0.233 U
0.539 Protactinium 231 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.0593 1.00 0.118 0.0847 0.797 Radium 226 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.619 1.00 0.456 0.419 1.72 Thorium 234 pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.169 0.137 0.132 0.367 Uranium 235 pCi/g 03/25/16 10:27 03/27/16 21:18 1
4.53 2.07 2.03 U
4.18 Protactinium 234m pCi/g 03/25/16 10:27 03/27/16 21:18 1
0.0944 0.143 0.107 0.934 Thorium 232 TestAmerica St. Louis Page 12 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-4 Client Sample ID: L08-09-04-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:50 Date Received: 03/23/16 11:00 Pb-210 1.26 0.413 0.439 0.578 pCi/g 03/25/16 10:27 03/27/16 21:18 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.298 0.0371 0.0483 0.0282 pCi/g 03/25/16 10:27 03/27/16 21:18 1
Lab Sample ID: 160-16635-4 Client Sample ID: L08-09-04-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:50 Percent Solids: 85.6 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00050 0.000066 0.000020 mg/Kg
03/24/16 08:53 03/28/16 14:55 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 8.52 (2+/-)
0.945 (2+/-)
1 03/28/16 14:55 03/24/16 08:53 pCi/g 0.225 1.32 RL MDC 0.529 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 14:55 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Lab Sample ID: 160-16635-5 Client Sample ID: L08-09-05-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:55 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.06 (2+/-)
0.181 (2+/-)
1 03/27/16 21:17 03/25/16 10:42 pCi/g 0.0970 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.0996 0.0593 0.0593 U
-0.00711 Americium 241 pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.364 0.420 0.400 1.24 Bismuth 212 pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.0617 0.126 0.0901 0.846 Bismuth 214 pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.0552 0.156 0.0672 1.08 Lead 212 pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.0625 0.135 0.0860 0.996 Lead 214 pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.329 2.12 1.05 18.0 Potassium 40 pCi/g 03/25/16 10:42 03/27/16 21:17 1
1.08 0.182 0.178 U
0.330 Protactinium 231 pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.0617 1.00 0.126 0.0901 0.846 Radium 226 pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.747 1.00 0.501 0.481 1.35 Thorium 234 pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.232 0.0709 0.0708 U
0.0500 Uranium 235 pCi/g 03/25/16 10:42 03/27/16 21:17 1
4.32 4.14 4.13 U
-1.35 Protactinium 234m pCi/g 03/25/16 10:42 03/27/16 21:17 1
0.0970 0.181 0.146 1.06 Thorium 232 Tl-208 0.331 0.0414 0.0538 0.0303 pCi/g 03/25/16 10:42 03/27/16 21:17 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
TestAmerica St. Louis Page 13 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-5 Client Sample ID: L08-09-05-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 14:55 Percent Solids: 83.4 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000072 0.000066 0.000020 mg/Kg
03/24/16 08:53 03/28/16 14:59 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 1.23 (2+/-)
0.197 (2+/-)
1 03/28/16 14:59 03/24/16 08:53 pCi/g 0.225 1.31 RL MDC 0.162 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 14:59 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 90 Lab Sample ID: 160-16635-6 Client Sample ID: L08-09-06-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:00 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.03 (2+/-)
0.177 (2+/-)
1 03/27/16 21:19 03/25/16 10:42 pCi/g 0.150 RL MDC 0.142 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.0783 0.0463 0.0463 U
-0.00516 Americium 241 pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.511 0.581 0.556 1.62 Bismuth 212 pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.0583 0.138 0.0950 0.961 Bismuth 214 pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.0838 0.160 0.0803 1.07 Lead 212 pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.0829 0.143 0.0909 1.06 Lead 214 pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.304 2.16 1.15 17.8 Potassium 40 pCi/g 03/25/16 10:42 03/27/16 21:19 1
1.18 0.195 0.190 U
0.402 Protactinium 231 pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.0583 1.00 0.138 0.0950 0.961 Radium 226 pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.847 1.00 0.302 0.293 U
0.700 Thorium 234 pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.236 0.141 0.141 U
0.0586 Uranium 235 pCi/g 03/25/16 10:42 03/27/16 21:19 1
5.08 3.12 3.07 5.62 Protactinium 234m pCi/g 03/25/16 10:42 03/27/16 21:19 1
0.150 0.177 0.142 1.03 Thorium 232 Pb-210 1.75 0.616 0.649 0.743 pCi/g 03/25/16 10:42 03/27/16 21:19 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.249 0.0506 0.0568 0.0664 pCi/g 03/25/16 10:42 03/27/16 21:19 1
Lab Sample ID: 160-16635-6 Client Sample ID: L08-09-06-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:00 Percent Solids: 70.1 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.000049 J 0.000083 0.000025 mg/Kg
03/24/16 08:53 03/28/16 15:03 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier TestAmerica St. Louis Page 14 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-6 Client Sample ID: L08-09-06-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:00 Percent Solids: 70.1 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 0.839 (2+/-)
0.105 (2+/-)
1 03/28/16 15:03 03/24/16 08:53 pCi/g 0.285 1.66 RL MDC 0.0718 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 15:03 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Lab Sample ID: 160-16635-7 Client Sample ID: L08-09-07-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:05 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.28 (2+/-)
0.172 (2+/-)
1 03/27/16 21:20 03/25/16 10:42 pCi/g 0.0924 RL MDC 0.115 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.0845 0.397 0.397 U
-0.0112 Americium 241 pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.439 0.553 0.527 1.62 Bismuth 212 pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.0740 0.146 0.105 0.987 Bismuth 214 pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.0723 0.160 0.0811 1.06 Lead 212 pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.0717 0.136 0.0872 1.00 Lead 214 pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.259 2.40 1.11 21.2 Potassium 40 pCi/g 03/25/16 10:42 03/27/16 21:20 1
1.19 0.291 0.285 U
0.517 Protactinium 231 pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.0740 1.00 0.146 0.105 0.987 Radium 226 pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.819 1.00 0.681 0.663 1.47 Thorium 234 pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.247 0.138 0.137 U
0.0906 Uranium 235 pCi/g 03/25/16 10:42 03/27/16 21:20 1
4.97 2.92 2.86 5.81 Protactinium 234m pCi/g 03/25/16 10:42 03/27/16 21:20 1
0.0924 0.172 0.115 1.28 Thorium 232 Pb-210 1.59 0.605 0.633 0.735 pCi/g 03/25/16 10:42 03/27/16 21:20 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Tl-208 0.384 0.0443 0.0593 0.0321 pCi/g 03/25/16 10:42 03/27/16 21:20 1
Lab Sample ID: 160-16635-7 Client Sample ID: L08-09-07-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:05 Percent Solids: 85.2 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00021 0.000068 0.000020 mg/Kg
03/24/16 08:53 03/28/16 15:07 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 3.68 (2+/-)
0.362 (2+/-)
1 03/28/16 15:07 03/24/16 08:53 pCi/g 0.232 1.35 RL MDC 0.130 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 15:07 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 TestAmerica St. Louis Page 15 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-8 Client Sample ID: L08-09-08-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:10 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.898 (2+/-)
0.154 (2+/-)
1 03/27/16 21:51 03/25/16 10:42 pCi/g 0.0915 RL MDC 0.124 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.0995 0.0593 0.0593 U
-0.0104 Americium 241 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.316 0.421 0.391 1.49 Bismuth 212 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.0731 0.127 0.0971 0.787 Bismuth 214 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.0589 0.149 0.0731 1.00 Lead 212 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.0753 0.131 0.0817 0.991 Lead 214 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.273 2.02 1.02 17.0 Potassium 40 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.992 0.200 0.194 U
0.472 Protactinium 231 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.0731 1.00 0.127 0.0971 0.787 Radium 226 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.786 1.00 0.333 0.299 1.40 Thorium 234 pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.214 0.197 0.184 0.694 Uranium 235 pCi/g 03/25/16 10:42 03/27/16 21:51 1
4.27 1.92 1.90 U
2.60 Protactinium 234m pCi/g 03/25/16 10:42 03/27/16 21:51 1
0.0915 0.154 0.124 0.898 Thorium 232 Tl-208 0.317 0.0413 0.0528 0.0321 pCi/g 03/25/16 10:42 03/27/16 21:51 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-8 Client Sample ID: L08-09-08-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:10 Percent Solids: 88.4 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0011 0.000064 0.000019 mg/Kg
03/24/16 08:53 03/28/16 15:10 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 19.6 (2+/-)
1.84 (2+/-)
1 03/28/16 15:10 03/24/16 08:53 pCi/g 0.218 1.28 RL MDC 0.394 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 15:10 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Lab Sample ID: 160-16635-9 Client Sample ID: L08-09-08-T-E-Q-00 Matrix: Solid Date Collected: 03/22/16 15:10 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 0.932 (2+/-)
0.147 (2+/-)
1 03/27/16 21:49 03/25/16 10:42 pCi/g 0.0821 RL MDC 0.112 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.104 0.0623 0.0623 U
-0.0130 Americium 241 pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.316 0.387 0.367 1.18 Bismuth 212 pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.0554 0.116 0.0807 0.805 Bismuth 214 pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.0571 0.143 0.0697 0.963 Lead 212 TestAmerica St. Louis Page 16 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-9 Client Sample ID: L08-09-08-T-E-Q-00 Matrix: Solid Date Collected: 03/22/16 15:10 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Lead 214 0.996 (2+/-)
0.129 (2+/-)
1 03/27/16 21:49 03/25/16 10:42 pCi/g 0.0594 RL MDC 0.0773 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.290 2.01 0.981 17.1 Potassium 40 pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.945 0.179 0.175 U
0.350 Protactinium 231 pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.0554 1.00 0.116 0.0807 0.805 Radium 226 pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.774 1.00 0.547 0.510 1.89 Thorium 234 pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.172 0.151 0.138 0.595 Uranium 235 pCi/g 03/25/16 10:42 03/27/16 21:49 1
4.29 2.46 2.45 U
0.818 Protactinium 234m pCi/g 03/25/16 10:42 03/27/16 21:49 1
0.0821 0.147 0.112 0.932 Thorium 232 Tl-208 0.282 0.0397 0.0493 0.0317 pCi/g 03/25/16 10:42 03/27/16 21:49 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-9 Client Sample ID: L08-09-08-T-E-Q-00 Matrix: Solid Date Collected: 03/22/16 15:10 Percent Solids: 85.0 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.0013 0.000067 0.000020 mg/Kg
03/24/16 08:53 03/28/16 15:14 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 21.8 (2+/-)
2.05 (2+/-)
1 03/28/16 15:14 03/24/16 08:53 pCi/g 0.231 1.35 RL MDC 0.423 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 15:14 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 Lab Sample ID: 160-16635-10 Client Sample ID: L08-09-09-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:15 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Analyte Actinium 228 1.31 (2+/-)
0.207 (2+/-)
1 03/27/16 21:52 03/25/16 10:42 pCi/g 0.0977 RL MDC 0.159 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.0806 0.648 0.648 U
-0.00908 Americium 241 pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.385 0.492 0.461 1.67 Bismuth 212 pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.0791 0.153 0.113 0.996 Bismuth 214 pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.0683 0.169 0.0829 1.14 Lead 212 pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.0766 0.155 0.0990 1.15 Lead 214 pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.389 2.46 1.24 21.1 Potassium 40 pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.901 0.531 0.531 U
0.197 Protactinium 231 pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.0791 1.00 0.153 0.113 0.996 Radium 226 pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.906 1.00 0.325 0.310 0.930 Thorium 234 TestAmerica St. Louis Page 17 of 26 3/30/2016 1
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Client Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Lab Sample ID: 160-16635-10 Client Sample ID: L08-09-09-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:15 Date Received: 03/23/16 11:00 Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Analyte Uranium 235 0.0908 U (2+/-)
0.147 (2+/-)
1 03/27/16 21:52 03/25/16 10:42 pCi/g 0.245 RL MDC 0.146 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
pCi/g 03/25/16 10:42 03/27/16 21:52 1
4.25 3.21 3.14 6.38 Protactinium 234m pCi/g 03/25/16 10:42 03/27/16 21:52 1
0.0977 0.207 0.159 1.31 Thorium 232 Tl-208 0.375 0.0469 0.0607 0.0337 pCi/g 03/25/16 10:42 03/27/16 21:52 1
(2+/-)
(2+/-)
MDC RL Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Other Detected Radionuclides Uncert.
Uncert.
Lab Sample ID: 160-16635-10 Client Sample ID: L08-09-09-T-E-S-00 Matrix: Solid Date Collected: 03/22/16 15:15 Percent Solids: 80.4 Date Received: 03/23/16 11:00 Method: 6020A - Metals (ICP/MS), Tc-99 RL MDL Technetium 99 0.00045 0.000072 0.000022 mg/Kg
03/24/16 08:53 03/28/16 15:18 1
Analyte Dil Fac Analyzed Prepared Unit D
Result Qualifier Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Analyte Technetium 99 7.78 (2+/-)
0.823 (2+/-)
1 03/28/16 15:18 03/24/16 08:53 pCi/g 0.248 1.45 RL MDC 0.406 Dil Fac Analyzed Prepared Unit Result Qualifier Count Total Uncert.
Uncert.
Re 30 - 110 Carrier 03/24/16 08:53 03/28/16 15:18 1
Dil Fac Analyzed Prepared Qualifier Limits
%Yield 87 TestAmerica St. Louis Page 18 of 26 3/30/2016 1
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QC Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 Client Sample ID: Method Blank Lab Sample ID: MB 160-241900/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242490 Prep Batch: 241900 RL MDL Technetium 99 ND 0.000053 0.000016 mg/Kg 03/24/16 08:53 03/28/16 13:34 1
MB MB Analyte Dil Fac Analyzed Prepared D
Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-241900/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242490 Prep Batch: 241900 Technetium 99 0.00119 0.00122 mg/Kg 103 80 - 120 Analyte LCS LCS D
Unit Result Qualifier
%Rec Spike Added
%Rec.
Limits Client Sample ID: Matrix Spike Lab Sample ID: 160-16634-A-1-D MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242490 Prep Batch: 241900 Technetium 99 ND 0.00166 0.00172 mg/Kg 103 75 - 125
Analyte MS MS D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-16634-A-1-E MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242490 Prep Batch: 241900 Technetium 99 ND 0.00158 0.00166 mg/Kg 105 75 - 125 3
30
Analyte MSD MSD D
Unit Result Qualifier
%Rec Spike Added Sample Result Sample Qualifier
%Rec.
Limits Limit RPD RPD Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Client Sample ID: Method Blank Lab Sample ID: MB 160-241900/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242491 Prep Batch: 241900 Technetium 99 Analyte U
1 03/28/16 13:34 03/24/16 08:53 pCi/g 0.182 MDC 1.06 RL 0.0423 0.0423 (2+/-)
(2+/-)
MB 0.001640 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Carrier Re 30 - 110 03/24/16 08:53 03/28/16 13:34 1
Dil Fac Prepared Analyzed Qualifier Limits
%Yield 94 MB MB Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-241900/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242491 Prep Batch: 241900 Technetium 99 Analyte 120 80 103 20.95 20.4 2.03 1.06 0.181 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 LCS Qualifier Limits
%Yield 94 LCS TestAmerica St. Louis Page 19 of 26 3/30/2016 1
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QC Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)
Client Sample ID: Matrix Spike Lab Sample ID: 160-16634-A-1-D MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 242491 Prep Batch: 241900 Technetium 99 Analyte 125 75 102 29.37 28.4 0.381 2.90 1.63 0.279 RL MDC (2+/-)
MS MS pCi/g Unit Result Qual
%Rec Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total Re Carrier 30 - 110 MS Qualifier Limits
%Yield 86 MS Client Sample ID: Matrix Spike Duplicate Lab Sample ID: 160-16634-A-1-E MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 242491 Prep Batch: 241900 Technetium 99 Analyte 1
0.17 125 75 103 28.45 27.1 0.381 2.65 1.56 0.267 RL MDC (2+/-)
MSD MSD pCi/g Unit Result Qual
%Rec Limit Added Spike Result Sample Sample Qual Limits
%Rec.
Uncert.
Total RER RER Re Carrier 30 - 110 MSD Qualifier Limits
%Yield 85 MSD Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)
Client Sample ID: Method Blank Lab Sample ID: MB 160-242189/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242403 Prep Batch: 242189 Actinium 228 Analyte U
1 03/27/16 15:14 03/25/16 10:27 pCi/g 0.0952 MDC RL 0.0115 0.0115 (2+/-)
(2+/-)
MB 0.001988 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.0233 0.0125 0.0125 U
-0.0006256 Americium 241 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.276 0.0352 0.0352 U
0.0000 Bismuth 212 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.0443 0.0207 0.0207 U
0.001855 Bismuth 214 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.0278 0.0140 0.0140 U
0.003391 Lead 212 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.0393 0.160 0.160 U
-0.007417 Lead 214 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.243 2.48 2.48 U
-0.06207 Potassium 40 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.424 0.120 0.120 U
0.02519 Protactinium 231 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.0443 1.00 0.0207 0.0207 U
0.001855 Radium 226 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.280 1.00 0.137 0.137 U
0.03156 Thorium 234 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.0698 0.0125 0.0125 U
0.01167 Uranium 235 1
03/27/16 15:14 03/25/16 10:27 pCi/g 1.90 15.2 15.2 U
-0.3801 Protactinium 234m 1
03/27/16 15:14 03/25/16 10:27 pCi/g 0.0952 0.0115 0.0115 U
0.001988 Thorium 232 Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 03/25/16 10:27 03/27/16 15:14 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected TestAmerica St. Louis Page 20 of 26 3/30/2016 1
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QC Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242189/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242396 Prep Batch: 242189 Americium 241 Analyte 116 87 103 104.1 101 10.9 0.511 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.1 37.59 3.89 0.200 0.155 pCi/g 110 87 - 120 Cobalt 60 31.8 34.45 3.41 0.101 pCi/g 108 87 - 115 Client Sample ID: Duplicate Lab Sample ID: 160-16620-A-4-E DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 242394 Prep Batch: 242189 Actinium 228 Analyte 1
0.01 0.6326 0.629 0.115 0.0854 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241 0.0140 U 0.01144 U 0.0373 0.0627 pCi/g 0.03 1
Bismuth 212 0.683 0.6091 0.248 0.230 pCi/g 0.15 1
Bismuth 214 0.461 0.5373 0.0895 0.0501 pCi/g 0.45 1
Lead 212 0.480 0.4979 0.0827 0.0479 pCi/g 0.11 1
Lead 214 0.592 0.6521 0.0914 0.0517 pCi/g 0.34 1
Potassium 40 13.3 12.67 1.55 0.183 pCi/g 0.19 1
Protactinium 231 0.218 U 0.2292 U 0.170 0.746 pCi/g 0.04 1
Radium 226 0.461 0.5373 0.0895 1.00 0.0501 pCi/g 0.45 1
Thorium 234 0.687 0.5604 0.343 1.00 0.547 pCi/g 0.20 1
Uranium 235 0.0654 U 0.1222 U 0.114 0.148 pCi/g 0.28 1
Protactinium 234m
-0.488 U 2.994 U 1.50 4.33 pCi/g 0.45 1
Thorium 232 0.629 0.6326 0.115 0.0854 pCi/g 0.01 1
Pb-210 1
0.68 0.6953 1.29 0.427 0.552 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides Tl-208 0.182 0.1964 0.0408 0.0280 pCi/g 0.20 1
Client Sample ID: Method Blank Lab Sample ID: MB 160-242193/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242403 Prep Batch: 242193 Actinium 228 Analyte U
1 03/27/16 18:43 03/25/16 10:42 pCi/g 0.0727 MDC RL 0.0350 0.0350 (2+/-)
(2+/-)
MB 0.01189 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.0239 0.0131 0.0131 U
-0.002021 Americium 241 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.298 0.168 0.168 U
0.07196 Bismuth 212 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.0577 0.0139 0.0138 U
0.008331 Bismuth 214 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.0251 0.0124 0.0124 U
0.004119 Lead 212 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.0359 0.132 0.132 U
-0.01165 Lead 214 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.281 0.120 0.120 U
-0.004057 Potassium 40 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.312 0.156 0.156 U
0.007493 Protactinium 231 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.0577 1.00 0.0139 0.0138 U
0.008331 Radium 226 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.247 1.00 0.116 0.116 U
-0.007078 Thorium 234 1
03/27/16 18:43 03/25/16 10:42 pCi/g 0.0628 0.0561 0.0561 U
-0.004101 Uranium 235 1
03/27/16 18:43 03/25/16 10:42 pCi/g 3.05 1.86 1.86 U
-0.05790 Protactinium 234m TestAmerica St. Louis Page 21 of 26 3/30/2016 1
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QC Sample Results TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)
Client Sample ID: Method Blank Lab Sample ID: MB 160-242193/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242403 Prep Batch: 242193 Thorium 232 Analyte U
1 03/27/16 18:43 03/25/16 10:42 pCi/g 0.0727 MDC RL 0.0350 0.0350 (2+/-)
(2+/-)
MB 0.01189 MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Other Detected Radionuclide None MB (2+/-)
(2+/-)
MDC RL pCi/g 03/25/16 10:42 03/27/16 18:43 1
MB Dil Fac Prepared Analyzed Unit Result Qualifier Uncert.
Count Uncert.
Total Radionuclides Other Detected Client Sample ID: Lab Control Sample Lab Sample ID: LCS 160-242193/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 242403 Prep Batch: 242193 Americium 241 Analyte 116 87 105 105.9 101 11.0 0.606 RL MDC (2+/-)
LCS LCS pCi/g Unit Result Qual
%Rec Added Spike Limits
%Rec.
Uncert.
Total Cesium 137 34.1 35.04 3.68 0.200 0.223 pCi/g 103 87 - 120 Cobalt 60 31.8 32.30 3.27 0.138 pCi/g 102 87 - 115 Client Sample ID: L08-09-05-T-E-S-00 Lab Sample ID: 160-16635-5 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 242394 Prep Batch: 242193 Actinium 228 Analyte 1
0.13 1.014 1.06 0.158 0.0916 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
Total RER RER Americium 241
-0.00711 U 0.002243 U 0.0557 0.0943 pCi/g 0.08 1
Bismuth 212 1.24 1.376 0.413 0.338 pCi/g 0.16 1
Bismuth 214 0.846 0.7624 0.124 0.0678 pCi/g 0.33 1
Lead 212 1.08 1.079 0.160 0.0605 pCi/g 0.02 1
Lead 214 0.996 0.9098 0.132 0.0718 pCi/g 0.32 1
Potassium 40 18.0 18.15 2.21 0.342 pCi/g 0.04 1
Protactinium 231 0.330 U 0.5307 U 0.276 1.08 pCi/g 0.44 1
Radium 226 0.846 0.7624 0.124 1.00 0.0678 pCi/g 0.33 1
Thorium 234 1.35 0.8122 U 0.309 1.00 0.849 pCi/g 0.67 1
Uranium 235 0.0500 U 0.04279 U 0.144 0.238 pCi/g 0.03 1
Protactinium 234m
-1.35 U 1.344 U 2.94 5.30 pCi/g 0.38 1
Thorium 232 1.06 1.014 0.158 0.0916 pCi/g 0.13 1
Tl-208 1
0.14 0.3463 0.331 0.0563 0.0245 RL MDC (2+/-)
DU DU pCi/g Unit Result Qual Limit Result Sample Sample Qual Uncert.
RER RER Total Other Detected Radionuclides TestAmerica St. Louis Page 22 of 26 3/30/2016 1
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QC Association Summary TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Metals Prep Batch: 241900 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16634-A-1-D MS Matrix Spike Total/NA Solid None 160-16634-A-1-E MSD Matrix Spike Duplicate Total/NA Solid None 160-16635-1 L08-09-01-T-R-S-00 Total/NA Solid None 160-16635-2 L08-09-02-T-E-S-00 Total/NA Solid None 160-16635-3 L08-09-03-T-E-S-00 Total/NA Solid None 160-16635-4 L08-09-04-T-E-S-00 Total/NA Solid None 160-16635-5 L08-09-05-T-E-S-00 Total/NA Solid None 160-16635-6 L08-09-06-T-E-S-00 Total/NA Solid None 160-16635-7 L08-09-07-T-E-S-00 Total/NA Solid None 160-16635-8 L08-09-08-T-E-S-00 Total/NA Solid None 160-16635-9 L08-09-08-T-E-Q-00 Total/NA Solid None 160-16635-10 L08-09-09-T-E-S-00 Total/NA Solid None LCS 160-241900/2-A Lab Control Sample Total/NA Solid None MB 160-241900/1-A Method Blank Total/NA Analysis Batch: 242490 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6020A 241900 160-16634-A-1-D MS Matrix Spike Total/NA Solid 6020A 241900 160-16634-A-1-E MSD Matrix Spike Duplicate Total/NA Solid 6020A 241900 160-16635-1 L08-09-01-T-R-S-00 Total/NA Solid 6020A 241900 160-16635-2 L08-09-02-T-E-S-00 Total/NA Solid 6020A 241900 160-16635-3 L08-09-03-T-E-S-00 Total/NA Solid 6020A 241900 160-16635-4 L08-09-04-T-E-S-00 Total/NA Solid 6020A 241900 160-16635-5 L08-09-05-T-E-S-00 Total/NA Solid 6020A 241900 160-16635-6 L08-09-06-T-E-S-00 Total/NA Solid 6020A 241900 160-16635-7 L08-09-07-T-E-S-00 Total/NA Solid 6020A 241900 160-16635-8 L08-09-08-T-E-S-00 Total/NA Solid 6020A 241900 160-16635-9 L08-09-08-T-E-Q-00 Total/NA Solid 6020A 241900 160-16635-10 L08-09-09-T-E-S-00 Total/NA Solid 6020A 241900 LCS 160-241900/2-A Lab Control Sample Total/NA Solid 6020A 241900 MB 160-241900/1-A Method Blank Total/NA General Chemistry Analysis Batch: 241878 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture 160-16634-A-1 DU Duplicate Total/NA Solid Moisture 160-16635-1 L08-09-01-T-R-S-00 Total/NA Solid Moisture 160-16635-2 L08-09-02-T-E-S-00 Total/NA Solid Moisture 160-16635-3 L08-09-03-T-E-S-00 Total/NA Solid Moisture 160-16635-4 L08-09-04-T-E-S-00 Total/NA Solid Moisture 160-16635-5 L08-09-05-T-E-S-00 Total/NA Solid Moisture 160-16635-6 L08-09-06-T-E-S-00 Total/NA Solid Moisture 160-16635-7 L08-09-07-T-E-S-00 Total/NA Solid Moisture 160-16635-8 L08-09-08-T-E-S-00 Total/NA Solid Moisture 160-16635-9 L08-09-08-T-E-Q-00 Total/NA Solid Moisture 160-16635-10 L08-09-09-T-E-S-00 Total/NA TestAmerica St. Louis Page 23 of 26 3/30/2016 1
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QC Association Summary TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Rad Leach Batch: 241585 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16620-A-4-E DU Duplicate Total/NA Leach Batch: 241804 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Dry and Grind 160-16635-1 L08-09-01-T-R-S-00 Total/NA Solid Dry and Grind 160-16635-2 L08-09-02-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-3 L08-09-03-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-4 L08-09-04-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-5 L08-09-05-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-5 DU L08-09-05-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-6 L08-09-06-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-7 L08-09-07-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-8 L08-09-08-T-E-S-00 Total/NA Solid Dry and Grind 160-16635-9 L08-09-08-T-E-Q-00 Total/NA Solid Dry and Grind 160-16635-10 L08-09-09-T-E-S-00 Total/NA Prep Batch: 241900 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid None 160-16634-A-1-D MS Matrix Spike Total/NA Solid None 160-16634-A-1-E MSD Matrix Spike Duplicate Total/NA Solid None 160-16635-1 L08-09-01-T-R-S-00 Total/NA Solid None 160-16635-2 L08-09-02-T-E-S-00 Total/NA Solid None 160-16635-3 L08-09-03-T-E-S-00 Total/NA Solid None 160-16635-4 L08-09-04-T-E-S-00 Total/NA Solid None 160-16635-5 L08-09-05-T-E-S-00 Total/NA Solid None 160-16635-6 L08-09-06-T-E-S-00 Total/NA Solid None 160-16635-7 L08-09-07-T-E-S-00 Total/NA Solid None 160-16635-8 L08-09-08-T-E-S-00 Total/NA Solid None 160-16635-9 L08-09-08-T-E-Q-00 Total/NA Solid None 160-16635-10 L08-09-09-T-E-S-00 Total/NA Solid None LCS 160-241900/2-A Lab Control Sample Total/NA Solid None MB 160-241900/1-A Method Blank Total/NA Prep Batch: 242189 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 241585 160-16620-A-4-E DU Duplicate Total/NA Solid Fill_Geo-0 241804 160-16635-1 L08-09-01-T-R-S-00 Total/NA Solid Fill_Geo-0 241804 160-16635-2 L08-09-02-T-E-S-00 Total/NA Solid Fill_Geo-0 241804 160-16635-3 L08-09-03-T-E-S-00 Total/NA Solid Fill_Geo-0 241804 160-16635-4 L08-09-04-T-E-S-00 Total/NA Solid Fill_Geo-0 LCS 160-242189/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-242189/1-A Method Blank Total/NA Prep Batch: 242193 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 241804 160-16635-5 L08-09-05-T-E-S-00 Total/NA Solid Fill_Geo-0 241804 160-16635-5 DU L08-09-05-T-E-S-00 Total/NA Solid Fill_Geo-0 241804 160-16635-6 L08-09-06-T-E-S-00 Total/NA Solid Fill_Geo-0 241804 160-16635-7 L08-09-07-T-E-S-00 Total/NA Solid Fill_Geo-0 241804 160-16635-8 L08-09-08-T-E-S-00 Total/NA Solid Fill_Geo-0 241804 160-16635-9 L08-09-08-T-E-Q-00 Total/NA TestAmerica St. Louis Page 24 of 26 3/30/2016 1
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QC Association Summary TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Rad (Continued)
Prep Batch: 242193 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Fill_Geo-0 241804 160-16635-10 L08-09-09-T-E-S-00 Total/NA Solid Fill_Geo-0 LCS 160-242193/2-A Lab Control Sample Total/NA Solid Fill_Geo-0 MB 160-242193/1-A Method Blank Total/NA TestAmerica St. Louis Page 25 of 26 3/30/2016 1
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Tracer/Carrier Summary TestAmerica Job ID: 160-16635-1 Client: Westinghouse Electric Company LLC Project/Site: HDP RFP-CBA-022 (7 DAY TAT)
Method: 6020A - Metals (ICP/MS), Tc-99 in Activity Prep Type: Total/NA Matrix: Solid Lab Sample ID Client Sample ID (30-110)
Re 86 160-16634-A-1-D MS Percent Yield (Acceptance Limits)
Matrix Spike 85 160-16634-A-1-E MSD Matrix Spike Duplicate 89 160-16635-1 L08-09-01-T-R-S-00 88 160-16635-2 L08-09-02-T-E-S-00 88 160-16635-3 L08-09-03-T-E-S-00 87 160-16635-4 L08-09-04-T-E-S-00 90 160-16635-5 L08-09-05-T-E-S-00 87 160-16635-6 L08-09-06-T-E-S-00 87 160-16635-7 L08-09-07-T-E-S-00 87 160-16635-8 L08-09-08-T-E-S-00 87 160-16635-9 L08-09-08-T-E-Q-00 87 160-16635-10 L08-09-09-T-E-S-00 94 LCS 160-241900/2-A Lab Control Sample 94 MB 160-241900/1-A Method Blank Tracer/Carrier Legend Re = Re TestAmerica St. Louis Page 26 of 26 3/30/2016 1
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