ML18003B038

Part 08 Enclosures (Rev. 1) - Part 8 - Enclosures - Geotechnical Exploration and Testing Data Report Appendix G.4 Carbonate Content Results Pages G.4-1 Thru G.4-37

ML18003B038
Person / Time
Site:	Clinch River
Issue date:	12/15/2017
From:	James Shea Tennessee Valley Authority
To:	Office of New Reactors
Fetter A
References
TVACLINCHRIVERESP, TVACLINCHRIVERESP.SUBMISSION.4, CRN.P.PART08, CRN.P.PART08.1
Download: ML18003B038 (37)

Text

APPENDIX G.4 -Carbonate Content Test Results-No Change for Rev. 4 Clinch River Data Report Rev. 4 CRP-1112.16 Page G.4-1 of 37

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Assignment Sheet Date: --::,;.9:..:/2;.:4.:..;/2;;.;0;..;;1==::3:::-:-------:---..--"'----------

Circle One: @ty Rela~

Non Safety Related Sample

Description:

Rock Core MP-101 L6-ll (90.9' to 91.5')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-101 L6-11 90.9-91.5 1.00 2.5 10 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Tested by:

M. Hamilton tA;'j~tjf Date:

12/27/2013 Reviewed by:

T. Landi/tcf Date:

1/2/2014 I "'1\\'A C02 Pressure (psi)

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i (nearest 1%)

27 Reading Time Calc. Equiv.

(min) I (nearest 1%) Chanqe (<0.3%)

2.5 20 27 0

Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

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Assignment Sheet Date:..:..9;.,:/2:,.4,.;/2;;.;0;..;;1..:..3.._=---------------

Circle One: ~ty Rela~Non Safety Related Tested by:

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Reviewed by:

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12/30/2013 Date:

1/6/2014 Sample

Description:

Rock Core MP-101, L6-12 (144.6' to 145.1')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading (g)

NA MP-101 L6-12 144.6-145.1 1.00 6.5 6.6 6.7 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Time (min) 10 20 30 C02 Pressure (psi)

Calc. Equiv.

(nearest 1%)

72 74 75 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)_

6.6 20 74 2.0 6.7 30 75 1.0 6.7 40 75 0.0 Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

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Project No. 6468-13-107?

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11 /6/2013 Project Name: Clinch River SMR Reviewed by:

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Assignment Sheet Date:

1 0/16/2013 Circle One: @ety Rei a~

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Description:

Rock Core MP-101, Ll-5 (148.7' to 149.7')

Weight of Tare 10 Boring ID Sample 10 Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-101 L 1-5 148.7 - 149.7 1.00 5.6 10 5.6 20 Equipment Used:

EquipmentiD CaL Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHL T-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 C02 Pressure (psi)

Calc. Equiv.

(nearest1%)

62 62 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)

5.6 20 62 0

5.6 30 62 0

Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of2

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Assignment Sheet Date:..:.9-:::/2;;,4;;..;/2;.;0:..:1;.;;.3_=------------

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111/2014 Date:

1/6/2014 Sample

Description:

Rock Core MP-101, L6-13 (184.6' to 185.2')

Weight of Tare ID BoringiD Sample ID Depth (ft) sample +/-0.01 Reading (g)

NA MP-101 L6-13 184.6-185.2 1.00 4.1 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Time (min) 10 C02 Pressure (psi)

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---

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Assignment Sheet Date:..:.9.;,:/2;::,4,..;/2;;..0;.;;1;.;;.3._=------------

Circle One: @ty Rei~ Non Safety Related

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Date:

12/31/2013 1/11/?.014 Date:------

Sample

Description:

Rock Core MP-101, L6-15 (378.9' to 379.6')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading (g)

NA MP-101 L6-15 378.9-379.6 1.00 4.2 4.3 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Time (min) 10 20 C02 Pressure (psi)

Calc. Equiv.

(nearest 1%)

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(min) (nearest 1%) Change (<0.3%)

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• Please see attatched Calibration Chart 1 of 2

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Assignment Sheet Date: ---:::::;l.;.;0/...;;.1.:..6/...;;.2~0.;.:13:::-----------

Circle One: @"ety Rel~Non Safety Related Sample

Description:

Rock Core l\\1P-101, Ll-13 (451.4' to 452.4')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-101 L 1-13 451.4-452.4 1.00 4.0 10 4.1 20 Equipment Used:

Equipment ID Cal. Due Date Scale CL T-0370 9/18/2014 Reaction Chamber CL T-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 C02 Pressure (psi)

Calc. Equiv.

(nearest 1 %)

44 45 Reading Time Calc. Equiv.

(min) (nearest 1%) Chanqe (<0.3%)

4.1 20 45 1

4.1 30 45 0

Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of2

amec!J 10 min. reading

_.......... =,...

20 and 30 min readings 2 of2

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ASTM D-4373 Rapid Determination of Carbonate Content of Soils ProjectNo. 6468-13-1072 Project Name: Clinch River SMR AMEC Lab Location: Charlotte, NC

--~~~-------------------------

Assignment Sheet Date:..::9.:..:/2;.4;;.;/2=.;0:...:1:..:3.._=----------------------

Circle One: ~ty Rela§g>'Non Safety Related Sample

Description:

Rock Core MP-202, L6-2 (78.5' to 79.1 ')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-202 L6-2 78.5-79.1 1.01 2.6 10 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Tested by:

Reviewed by:

1\\t::f'i-.

M. Hamilton 1It/l't Date:

12/30/2013 T. Landis Date:

1/6/2014 4,\\\\31\\k C02 Pressure (psi)

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(nearest 1%)

28 Reading Time Calc. Equiv.

(min) *(nearest 1%) Change (<0.3%)

2.6 20 28 0.0 Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

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Assignment Sheet Date:

9/24/2013 Circle One: -@-==a===~-ety R_e_l~""t'e::-:-N-on_S_a~-e-ty-R-el-at-e-:d----

Sample

Description:

Rock Core MP-202, L6-3 (113.1' to 113.7')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-202 L6-3 113.1 -113.7 1.00 3.7 10 Equipment Used:

Equipment 10 Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHL T-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Tested by:

e-ll Jf M. Hamilton 1111 ' Date:

12/27/2013 Reviewed by:

T. Landis ?("t/

Date:

1/2/2014

,, 131\\-\\

C02 Pressure (psi)

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(min) I I nearest 1%) Change (<0.3%)

3.7 20 40 0

Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

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Tested by:

G. Williams

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Date:

12/16/2013 Project Name: Clinch River SMR AMEC Lab Location:....:C:.._h_ar_l..::.o....:tt....:e,'-'N:...._C ___________ _

Assignment Sheet Date: ---::,;1,;.0/~1~6:.:

/2:.::0..;;,1::::3 __________ _

Circle One: @ty Rel~Non Safety Related Reviewed by:

T. Land4 Date:

12/18/2013 I *\\\\3\\~

Sample

Description:

Rock Core "MP-202, LI-22 (148.7' to 149.6')

Weight of Tare ID Boring ID Sample 10 Depth (ft) sample +/-0.01 Reading (g)

NA MP-202 L 1-22 148.7-149.6 1.00 2.6 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Time (min) 10 C02 Pressure (psi)

Calc. Equiv.

(nearest 1%)

28 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)

2.6 20 28 0

Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

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Assignment Sheet Date:...:.9.:..:/2;.4;.;.;/2~0::1:::.3"""""=-----------

Circle One: @ety Rei~ Non Safety Related Sample

Description:

Rock Core MP-202, L6-4 (195.8' to 197.9')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-202 L6-4 195.8-197.9 1.01 2.5 10 2.6 20 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Tested by:

<¢ M. Hamilton'"" *(11/i'f Date:

12/30/2013 Reviewed by:

T. Landis Date:

1/6/2014

~,,,3)1+

C02 Pressure (psi)

Calc. Equiv.

I (nearest 1%)

27 28 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)

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• Please see attatched Calibration Chart 1 of 2

ame&

"lJC')

I>>=

~ ~

ASTM D-4373 Rapid Determination of Carbonate Content of Soils G)

~~

Ntl) 0 c

~ ;.

% Calcite Equivalent per Mass(g) of CaC~

~

"'C

~

I 70 ~

~~******

4~~~:~::~:~uiva::~t (%CaC03)6'0 -----

80

-- 1~0 10

£ I

=.:119

~

60

~

t::=.. _._.~::::::...... _;

.. _... ::::::L.~:~:.::::::::.=====l

.::::::t:~::~ ::.:_

--:c --

• -*:r::::..: ::::::**:::::::~~::.:.::.. _ ___

• £-t"

• ====t 8 so

~

~

6

~

40

~

• -r----*-**............

--=====.

~

5

~30 - --= -~-=- - : - __ --: ~-

=L- _!* } __ **i=-~, ~

20

• • • • • +--

3 I****

~=*

-*=

_:= ~ ::._

~~-- * * ~:.~~~:-.. :=j~*

- =~=~:=-

.:~-~ _,,,:~~== =~~.:=! 2 10

.... ************************************.c.::.:************"-

L...

1 o *

• • <*******--******----***-*-*-*********-r--**-*---

--**-- --==t*******-****--**-***-**-****** _,.......

• • • **********---**-~*-* *************--** ********-*****..., ***********--* *****************--**-********

• • • • • • • • • • • • • • -*----***-r o 0

0.2 0.4 0.6 0.8 1

10 min. reading

---

20 and 30 min readings Mass CaC03 (g) 2 of2

"'C(")

Ill =

(Q ::I t1) n G'):::T

~~

Ntl)

N..,

0 c

-Ill w-

""-IDl

~

"'C 0

~

~

(")

o "P....

~

ASTM D-4373 Rapid Determination of Carbonate Content of Soils Project No. 6468-13-1072 Project Name: Clinch River SMR AMEC Lab Location: _C::....h....:.a"-rl'-'-o"-'tt-'-'e,c.::Ncc.C""-------------

Assignment Sheet Date:..::9..::;/2;.4~/2;:.0::.:1:..:3__,=--:-::----:---=--:---:---

Circle One: @Oety Rela§g:YNon Safety Related Sample

Description:

Rock Core MP-202, L6-5 (241.0' to 242.4')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-202 L6-5 241.0 - 242.4 1.00 4.5 10 4.6 20 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 II'C?i-i Tested by:

M. Hamilton l(ll/llf Date:

12/30/2013 Reviewed by:

T. Landis Date:

1/6/2014

/1!, )13)v\\

C02 Pressure (psi)

Calc. Equiv.

(nearest 1%)

49 51 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)

4.6 20 51 2.0 4.6 30 51 0.0 Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of2

"'C(")

Ill =

(Q ::I t1) n G'):::T

~~

Ntl) w..,

0 c

-Ill w-

""-I Ill

o t1)

"'C 0

I

~

o t1)

(")

o I

"P....

N....

ASTM D-4373 Rapid Determination of Carbonate Content of Soils

% Calcite Equivalent per Mass(g) of CaC03 Calcite Equivalent {%caC03) 0 20 40 60 80 100 70 k=.................

• • • • • +"......................................... t.. ___

.......................... )..,............................................ c......

....=:~.,_ ******-******

..... <j....

l 10 60 50 0....

==- 40

~

~ 30 ON u

20 10 0

I I

'it J

r i

• __ *::::::**==r

-r--

t::t:...

...................-.~~~*.t:................................

......... ___.... ::::).

........................................................ f.*********-**

~--***-****-::*::-*::::::::::::::.-::***-

-*--... +.....................

....... it

}--

).....

........... ::..1

--:=

...... :.:::::-::::-:::.. _::::::::.: *::::::.:*:::.:... t.....

0 0.2 0.4 Mass CaC03 (g) 10 min. reading

--=== 20 and 30 min readings 0.6

• I-

119

. **- +

2**r

..... ---.:::1 8 7

6 5

4 3

2 1

0 0.8 1

• u; E:

~

~

N 0 u 2 of2

"'C(")

Ill =

(Q ::I t1) n G'):::T

~~

Ntl) 0 c

-Ill w-

""-IDl

~

"'C 0

~

~

(")

o "P....

~

ASTM D-4373 Rapid Determination of Carbonate Content of Soils ProjectNo. 6468-13-1072 Project Name: Clinch River SMR AMEC Lab Location:....:C:..:h:..:a:=rl:..:o.:..:.tte.:2,-=N...:...C.::._ __________ _

Assignment Sheet Date: ---:::~9:.:12:...:4.:...:/2;;.;;0:.;;1=::3:-----------

Circle One: @ty Relarg!)i Non Safety Related Sample Desc1iption:

Rock Core MP-202, L6-6 (247.8' to 249.0')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-202 L6-6 247.8-249.0 1.00 4.9 10 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Tested by:

Reviewed by:

J'r'l e.t-f M. Ham1lton i)ll/11-1 Date:

T. Landis

.p Date:

\\\\,~\\'A.

12/27/2013 112/2014 C02 Pressure (psi)

Calc. Equiv.

(nearest 1%)

54 Reading Time Calc. Equiv.

(min) I (nearest 1%) Change (<0.3%)

4.9 20 54 0

Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

ame.

"'C(")

Ill =

ASTM D-4373 Rapid Determination of Carbonate Content of Soils (Q ::I t1) n G'):::T

~~

cn!!l

% Calcite Equivalent per Mass(g) of CaC03 0 c

-Ill w-

""-I Ill

o t1)

"'C 0

~

Calcite Equivalent (%CaC03) 0 I

o 70 t1) 40 60 20 80 100 10

(")

o I

60 "P....

9 N

8 50 7

'iU

n.

==- 40 6

• .e

QJ :;

QJ

.t 30 0

QJ :;

5

<I)

<I)

QJ

.t N

4 0

u u

20 3

2 10 1

0 0

0 0.2 0.4 0.6 0.8 1

Mass CaC03 (g) 10 and 20 min. readings 2 of2

"tl(")

Ill-IC -*

~ ~

G):::r

~;:c N ;::*

a>~

0 ;;

-Ill w-

....,.~:~~

~

"0 0

~

~

~

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tJ

~

~

a>

ASTM D-4373 Rapid Determination of Carbonate Content of Soils ProjectNo. 6468-13-1072 Project Name: Clinch !liver SMR AMEC Lab Location: -=C:...:.h.:..:ar.:..:l.::..ot:..:..te:..:i.,..::.N-'C=-------------

Assignment Sheet Date:..:..9-::::/2:::o4_12_0...;;1;.;.3-===------------

Circle One: @ty Rela~ Non Safety Related Sample

Description:

Rock Core MP-202, L6-9 (385.2' to 385.9')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-202 L6-9 385.2-385.9 1.00 3.5 10 L______

Equipment Used:

Equipment ID Cal. Due Date Scale CL T-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1 /2015 No. 40 Sieve CL T-0381 4/8/2014

~gil Tested by:

M. Hamilton 1/1*/14 Date:

1/2/2014 Reviewed by:

T. Landis Date:

1/6/2014 4*\\\\3\\v\\

C02 Pressure (psi)

Calc. Equiv.

I (nearest 1%)

39 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)

3.5 20 39 0.0 Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

"'C(")

~=

t1) ~

c;,:T

~;u N ;::*

.._.11)..,

S,c w!!l.

""-1111

~

"'C 0

~

u t1)

~

~

(")

u 7'

~

ASTM D-4373 Rapid Determination of Carbonate Content of Soils

% Calcite Equivalent per Mass{g) of CaC~

Calcite Equivalent {%CaC03) 0 20 40 60 80 70 60 50 0.. =- 40

~

J VI VI

~

0.. 30 0

u 10 0

• 0 0.2 0.4 0.6 0.8 Mass CaC03 (g)

• -----~-n.... *****-*--*-*---- ***

10 and 20 min. readings a me 100 10 9

8 7

6 "iii QJ 5

5 VI QJ

~

N 0 u 3

2 1

0 1

-~-~-n *---*-*******

2 of 2

"'C(")

~=

t1) ~

c;,:T

~;u N ;::*

cot!)

S,c w!!l.

-..jill

~

"'C 0

~

u t1)

~

~

(")

u 7'

~

amec!J ASTM D-4373 Rapid Determination of Carbonate Content of Soils ProjectNo. 6468-13-1072 Project Name: Clinch River SMR.

AMEC Lab Location: Charlotte, NC

---

~------------------------

Assignment Sheet Date:..:..9;.,:/2:.,4-.;/2~0;.;;1...;;.3.....,..=------------------

Circle One: @Oety Rela~ Non Safety Related Sample

Description:

Rock Core MP-401, L6-19 (79.0' to 79.6')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-401 L6-19 79.0-79.6 1.01 3.5 10 5.2 20 6.1 30 6.7 40 7.0 50 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Tested by:

Reviewed by:

M. Hamilton rrt1ft1"{ Date:

1/112014 T. Landis Date:

1/6/2014 4,\\\\:J}V\\:

C02 Pressure (psi)

Calc. Equiv.

(nearest 1%)

39 57 68 74 77 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)

5.2 20 57 18.0 6.1 30 68 11.0 6.7 40 74 6.0 7.0 50 77 3.0 7.0 60 77 0.0 Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

"tl(")

Ill:::

ASTM D-4373 Rapid Determination of Carbonate Content of Soils IC

1

~ n G):::r

~~

N~

<D..,

% Calcite Equivalent per Mass(g) of CaC03 0 c

-Ill w-

~:~~

a

~

"'0 0

~

Calcite Equivalent (%CaC03)

I 0

a 70

~

~

40 60 20 80 100 10

(")

a "tl 9

I 60 N

8 a>

50 7

ro-...

. 40 6

~

I

~

~

... 30 ON u

QJ 5

~

QJ d:

N 4

0 u 20 3

2 10 1

0 0

0 0.2 0.4 0.6 0.8 1

Mass CaC03 (g) 10 min. reading

-~~~~*~~~~-- 20 min. reading

---

30 min. reading

• • • • • • • • • • • • • • • 40 min. reading

• 50 and 60 min. readings 2 of 2

"lJC')

I>>=

(Q :::l n> n G):::T

~~

wn>

o..,

0 c

-I>>

w-

""-11>>

~

"'C 0

I.

~

C')

o "P

~

a me&

ASTM D-4373 Rapid Determination of Carbonate Content of Soils ProjectNo. 6468-13-1072 Project Name: Clinch River SMR AMEC Lab Location: -=C~h:.;;ar;;.:l-=:ot:..;.te:.z,..::N..:...C=------------

Assignment Sheet Date: 9/24/2013 Circle One:..:..<@:::;:a::;ife~ty;..;..::R.:.;.e:-la:gt>'""'te:::::-:-:-N:-o-n-=s=-a-::-fe-ty-=-R-=el:-at-e-:d----

Tested by:

M. Hamilton tt;f,1~y Date:

12/27/2013 Reviewed by:

T. LandisA Date:

1/2/2014 I 1\\'3\\\\~

Sample

Description:

Rock Core MP-401, L6-20 (216.4' to 216.9')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading (g)

NA MP-401 L6-20 216.4-216.9 1.00 6.3 8.1 Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Time (min) 10 20 C02 Pressure (psi)

Calc. Equiv.

I (nearest 1%)

70 90 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)

8.1 20 90 20 8.1 30 90 0

Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

"lJC')

I>>=

(Q :::l ASTM D-4373 Rapid Determination of Carbonate Content of Soils n> n G):::T

~~

wn>

0 c

-I>>

% Calcite Equivalent per Mass(g) of CaC03 w-

""-II>>

0 n>

"'C 0

I Calcite Equivalent (%CaC03)

I.

0 0

20 40 60 80 100 n>

70 C')

0

~----****-*--* ---

L.... ~-p __ :.:::.:--* - =i~----.-~~::.::.:~~--~~::~ -~---=-1:... __ :-

__... :::L*.. *:::: -

.:1::.... :.::.:. ____ -.:::::-*:-.:L

_::::::::::::::::~:::'r.:::::::-_____ ~ __ ::::L ~:: :-

.: *:.-:1::.::::::.::.:::::.::.*.~~:. ~.:.111 9 "P....

60 L

,;~;~.

c

.............. *

::::::.r.::::* ::.~:::::; -***- ***********-****.*

.. *l-*:::.::.:::::.::: t::

.::::** -,............................... *.:r :: ::**-***-***---1---*****. ***-*** 74""~=-~.::::.-::::-::..... ::;: 8 N....

50 7

--~-- -***-*-*-*-***--*---*-***

6

• v; D.

=- 40

~

~

J

J

-*--****" ***-*-¥.. -***--****-*- -

5

~*--**-

~*~*-

~

~

D.

D. 30 N

N 4

0 0 u u

3 2

10 1

o * ***--*-*******-*******-*-*-*-*<*-*- ****************************1*** ***-*-******* ** ***** * ******* * -~ * ********- ********** *- ** ****r******* ************************--j***

-*-*-**************--*-*****-*-~-----*-***-*-******-*** ****s*****-*- *****-***-**--*-*****l*

• • • • • • • • • • • • • • • • * * **************-*-~--*-********* ****** ************-f o 0

0.2 0.4 0.6 0.8 1

Mass CaC03 (g) 10 min. reading

---

~~~

20 and 30 min readings 2 of 2

"tl(")

Ill-IC -*

~ ~

G):::r

~;:c w :::*

N~

0 ;;

-Ill w-

....,.~:~~

~

"0 0

~

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~

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tJ

~

~

a>

ASTM D-4373 Rapid Determination of Carbonate Content of Soils ProjectNo. 6468-13-1072 Project Name: Clinch River S1\\.1R AMEC Lab Location: Charlotte, NC

---

~------------------------

Assignment Sheet Date:.;:.9-:/2;,4;;.;/2;;.;0;_;1;.,;.3._=----------------

Circle One: @ty Rela~ Non Safety Related Sample

Description:

Rock Core MP-415, L6-17 (25.1' to 25.7')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-415 L6-17 25.1-25.7 1.00 5.0 10 5.1 20 5.2 30

~

Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CLT-0734 9/13/2014 HCL CHLT-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Tested by:

M. Hamilton *\\7~1'1 Date:

12/3112013 T. Landis Date:

1/6/2014

/1'3,\\,3]\\-\\

Reviewed by:

C02 Pressure (psii Calc. Equiv.

(nearest 1%)

55 56 57 Reading Time Calc. Equiv.

(min) (nearest 1%) Change (<0.3%)

5.1 20 56 1.0 5.2 30 57 1.0 5.2 40 57 0.0 1-Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

"tl(")

Ill:::

IC :::1

~ n G):::r

~~

ASTM D-4373 Rapid Determination of Carbonate Content of Soils w~

w..,

0 c

-Ill w-

~:~~

% Calcite Equivalent per Mass(g) of CaC03

a

~

"'0 0

~

Calcite Equivalent (%CaC03)

I 0

a 70

~

~

40 60 20 80 100 10

(")

a "tl 9

I 60 N

8 a>

50 7

0..

. 40 6

"iii.e:

OJ :;

OJ 6: 30 6'

u OJ 5

~

OJ 6:

N 4

0 u 20 3

2 10 1

0 0

0 0.2 0.4 0.6 0.8 1

Mass CaC03 (g) 10 min. reading

-- 20 min. reading

---

30 and 40 min. readings 2 of2

"tl(")

Ill-IC -*

~ ~

G):::r

~;:c w :::*

""'~

0 ;;

-Ill w-

....,.~:~~

~

"0 0

~

~

~

(")

tJ

~

~

a>

ASTM D-4373 Rapid Determination of Carbonate Content of Soils ProjectNo. 6468-13-1072 Project Name: Clinch River SMR AMEC Lab Location:....:C:..::h:..::a:..:rl..:..ot:.:.te:.z'..::N....:C=------------

Assignment Sheet Date: -::-;i-9/

..::2....:4..::

/2....:0.c1:::3~---------

Circle One: @ty Rela~Non Safety Related Sample

Description:

Rock Core MP-415, L6-16 (28.5' to 28.9')

Weight of Tare ID Boring ID Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

(min)

NA MP-415 L6-16 28.5-28.9 1.00 7.9 10

_c____

Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CL T-0734 9/13/2014 HCL CHL T-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014

~

Tested by:

M. Hamilton

~/to/ILf Date:

12/27/2013 1/2/2014 Reviewed by:

T. Landis~

Date:

~Q-.,,~,~ ----

C02 Pressure (psi)

Calc. Equiv.

(nearest 1%)

88 Reading Time Calc. Equiv.

(min) '(nearest 1%) Change (<0.3%)

7.9 20 88 0

Note: If no reaction occurs increase amount of sample to next weight increment and rerun test

• Please see attatched Calibration Chart 1 of2

"tl(")

Ill-IC -*

~ ~

G):::r

~;:c w :::*

en~

0 ;;

-Ill w-

....,.~:~~

~

"0 0

~

~

~

(")

tJ

~

~

a>

ASTM D-4373 Rapid Determination of Carbonate Content of Soils

%Calcite Equivalent per Mass(g) of CaC03 Calcite Equivalent (%CaC03) 0 20 40 60 80 70 ~~~~~~~~~~~~~~~~~~

0..

60 50

. 40 Q) 5 Ul Ul Q)

Q: 30 s"

20 10 100 0 ~==t=====f"=-=-=:.o.:.o::.o.:r:::............. :.o:............. f:................... :-.:::....... f........... :.o.:.:... :............ ::F:.. __......... :.:.:.::::r:.....:::.::.... :.c:::~..... T.......... ___ ::.. ~:::.... :+/---......................... :... ::T 0

0.2 0.4 0.6 0.8 1

Mass CaC03 (g)

L_

10 and 20 min. readings 10 9

8 7

6 E;

Q) 5 5

Ul Ul

~

0..

N 4

0 u 3

2 1

0 2 of 2

"tl(")

Ill-IC -*

~ ~

G):::r

~;:c w :::*

a>~

0 ;;

-Ill w-

....,.~:~~

~

"0 0

~

~

~

(")

tJ

~

~

a>

ASTM D-4373 Rapid Determination of Carbonate Content of Soils ProjectNo. 6468-13-1072 Project Name: Clinch River S:rvrR AMEC Lab Location: _:C:.:h:=ar:..:lc:.ot::..:.te:..2,...;;N.;_C:;__ __________ _

Assig1m1ent Sheet Date:.;..9.:,:/2;,4;;.;/2;;..0;..;1;.;.;3-=------------

Circle One: @ty Rel~ Non Safety Related Sample

Description:

Rock Core MP-415, L6-18 (38.6' to 39.1')

Weight of Tare ID BoringiD Sample ID Depth (ft) sample +/-0.01 Reading Time (g)

_(min)

NA MP-415 L6-18 38.6-39.1 1.00 2.4 10 1--

Equipment Used:

Equipment ID Cal. Due Date Scale CLT-0370 9/18/2014 Reaction Chamber CL T-0734 9/13/2014 HCL CHL T-00667 3/1/2015 No. 40 Sieve CLT-0381 4/8/2014 Tested by:

~

M. Hamilton

• /11//f Date:

12/31/2013 Reviewed by:

T. Landis Date:

1/6/2014

-""'(i,\\\\11~

C02 Pressure (psi)

Calc. Equiv.

(nearest 1%)

26 Reading Time Calc. Equiv.

(min) I (nearest 1%) Change (<0.3%)

2.4 20 26 0.0 Note: If no reaction occurs increase amount of sample to next weight increment and rerun test.

• Please see attatched Calibration Chart 1 of 2

"tl(")

Ill:::

IC

1 ASTM D-4373 Rapid Determination of Carbonate Content of Soils

~ n G):::r

tJ

~ -*

~.,o<

..... ~

% Calcite Equivalent per Mass(g) of CaC03 0 c

-Ill w-

-..~:~~

tJ

~

"0 0

~

Calcite Equivalent (%CaC03)

I 0

tJ 70

~

~

~

40 60 2.0 80 100 10

(")

tJ 60

~

I 9

N :...

8 a>

so 7

0..

==.. 40 6

v; E:

~

ll:. 30 6'

5 ll:.

0 u

u 2.0 3

2.

10 1

0 0

0 0.2 0.4 0.6 0.8 1

Mass CaC03 (g)

--*----*-*-*-*-----__)

10 and 20 min. readings 2 of 2