ML17009A184

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{{Adams | number = ML17009A184 | issue date = 12/14/2016 | title = Radiological Survey and Dose Assessment Report for the Western New York Nuclear Service Center and Off-Site Areas in Follow Up to Aerial Gamma Radiation Survey, Rev. 1, Appendix G: Certificates of Analysis (Coa 405235, 406240 and 405245), P | author name = | author affiliation = State of NY, Energy Research & Development Authority | addressee name = | addressee affiliation = NRC/NMSS, NRC/NRR | docket = 05000201, P00M-032 | license number = | contact person = | package number = ML17006A156 | document type = Environmental Monitoring Report | page count = 3118 }}

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{{#Wiki_filter:GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 29-SEP-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1598620 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE EML HASL-300,1-01 Modified Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

DER Report No.: 1562566 Revision No.: Type: Process Client Code: MJWC Sample received out of holding: Samples were analyzed in a timely manner upon receipt. Reporting results. 405235 021,022,023,024,025,026,027,028,029, 030,031,032,033,034,035,036,037,038, 039,040 QC 1203627438DUP,1203627 439MS Originator's Name: Data Validator/Group Leader: Spencer Collins 29-SEP-16 Bryan Williams 29-SEP-16 Page 1 Page 2690 of 5809 I-129 Queue Sheet 09/14/.2016 Batch #:1598620 Analyst: MJHl First Client Due Date:I0/0412016 Internal Due Date:09/30/2016 Spike Isotope: [-129 Spike Code: /U.1.b-" LCS Isotope: I-129 LCS Code: it.ii D-K Prep Date: '1-1-h-i b lnitials:...-\AA<j 4-Expiration Date:<. l Vol: O. lv..'-l Nomin:il ___ _ Expiraiion Date: 3->o-l bl] Vol: o. .Nominal Concentration: 1\ik Pipette lD: /L/ 2c1303 'Vitness:_N_1..P..._, ___ _ j "6'":' \);2!.i w<--r G Aliquot Hazard Type Code RDL "05235021-1 405235022-l -105235023* 1 405235024-1 405235025-1 405235026-1 40523502i-1 405235028-l 405235029-1 405!35030-1 405235031-1 405235032-1 405235033-1 405235034-1 4()5235035-1 405235036-1 405235037-1 405235038-1 405235039-1 405235040-1 120362743i-l 1203627438-l 1203627439-J 12036274-10-1 4.!8.R.2.3 4.28.R.l.3 4.28.R.1 l.2 4.28.R.2.2 4.28.R.1.2 4.2C.R.l.3 4.2C.R.JA 4.3J\Rl.3 4.3.B.R. l.3 4.3A.R.2.3 4.3.BR19.2 4.3B.R.:;.3 4.3B.R.3.4 4.3.B.R.IA 4.3B.R.2.3 4.3B.R.2.4 4.4C.R.2A 4.4C.R.1.3 4..IC.R.lA 4.40.R.l.3 .\IB for batch 1598620 4.'.?B.R.2.3(4052350:?.JOUP) 4.28.R.2.3( lil 1$) LCS for batch 159$620 GEL Laboratories LLC, Radiochemistry Division S . .\MPLE SA.'\lPLE S . .\;'\lPLE SAMPLE SAMPLE SAMPLE SA.,"\JPLE SA;llPLE SAMPLE SA;llPLE SAMPLE SAMPLE SAMPLE SA,'\IPLE SAMPLE SAMPLE SAl\tPLE SAMPLE SAMPLE SAMPLE MB DUP .'.>IS LCS l pCi/g I pCl!g 1 pCi/g

  • l pCi/g l pCilg I pCllg I pCilg I pCi/g l pCi/g 1 pCiig I pCl/g l pCi/g l pCi/g I pCi/g 1 pCi/g 1 pCi/g I pCUg l pCi/g I pCilg 1 pCi!g l pCifg l pCi/g l pCi/g I pCi/g MJWCOOl MJWCOOJ MJWCOOJ MJWCOOl MJWCOOI MJWCOOl MJWCOOl MJWCOOl i\lJWCOOl MJWCOO! i\-1JWC001 MJWCOOl MJWCOOt SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL 3, .<\'-\ .12 1,.co -:; .C-5 :i.k3 ;! '.!." .... -'i:Z. ?.'S"\ '-! .tlJ l\lJWCOOI SOIL *3* "1 c:. MJWCOOl SOIL -; ."/ ']... MJWCOOl SOIL MJWCOOl SOIL
  • C°3 M.JWC0.01 SOIL 3. MJWCOOl SOIL 3 .'11 MJWCOOJ SOJL i1 .1 5 QC ,\CCOUNT SOIL QCACCOUNT SOIL '-;.ci QC i\CCOUi'\T .SOIL '?.5 I. QC ACCOUNT SOIL 08-DEC-15 l-l:17 Gi j x l ! rwf 08-DEC-15 13:43 l:l1! ::.u 0 X-2.. I rtJl 02-0£c-1: 10:-10 o>/ 3. :l'-1 )( t.f ./ flcV OS-DEC-b 14:13 . .,,o A.5!i 08 C r----** /'> 11. . -DE -15 13:38 Srl z. 5 i: i\ b I OS-DEC-15 10:1:5 ___ 08-0EC-1510:19 ;nl 2.'17 Xl :z.1.-, l A!:{ lfl..t 23-:\0V-15 ll:lOS<'l,! 2. 'CC '1.,5 23-NOV-15 14:4-1r.,iq2.bO :?6-NOV-15 j 2 .1 b *XI ia.J 23-NOV-1511:48Qzj J.8b J'2, Mf:: rcr 2:>-xov-15 11:2om'il 2 .% Xs. 23-NOV-15 ;2. £\le §bl j! (?4 23-NOV-15 11:12t'3;i,.J z. b 7 f>.. _ 31h'\OV-t5 11: 19;)11 !,..., -ij 42.F 30-NOV-15 2. e2. 'l<.{ i\lJ 30-NOV-1510:43&<;! 3.11 S(3 jv.f 30-NOV-15 13:23(3l.oj 3. ?l.j }U: l il"f Cf-l&,** iJ.:; 3 Si y: I j !*.1% OS-DEC-15 '/(',_ jJA.) :Z.'i'i 'i.4 IVIS' '1-2b-lb 3z4 35"1 'I-SI Vl6 Pagel of I Weight/Loss Aliquot Correction Report http://prodsvrOI.gel.com :7778/pls/lims/weight_ loss _rpts.show _report Weight/Loss Aliquot Correction Report Select What to Correct Aliquot to ( Ash Dry *weight 0 Dry Weight ,,;i Wet Weight Submit i . '* ,,,., .* .... .. ;;.-,.! Batch ID: 1598620 Aliquot Correction to Dry Weight for Batch 1598620 rsample Id [Aliquot (G) [Sample Type !Parent Sample IdJLoss (Dcc):lcorrected Aliquot (G) 1405235021 r 3.94 lsAMPLE INA J.1654 :13.28si792682897o6 1405235022 r 3.23 lsAMPLE [NA 1.1937 12.604187628721362( lsAMPLE INA 1.2255 j3.237336i:a1sai77i [405235024 li22 . -JsAMPLE \NA 1.1939 j2.s9s32-ii16s27562! .[405235025 ,I 3.00 *1 SAMPLE INA f .2138 12.3SB3584l073:i486: J405235026 f 3.05 lsAMPLE INA 1.1664 j2.542323751273092 \ 40523 5021 13.63 \SAMPLE \NA \ .1816 I 2. 97o78o65ss972ss£ \NA \.2267 12:6135s89oo3i8237--14o5235029 13.47 lsAMPLE INA 1.1932 r 2.79956391512922 --[40523503o-j3.42 [SA"MrLE-[NA \.2389 I 2.60288s76827o461 * -. [405235031 J3.57 I SAMPLE 1.2258 I [405235032.l 3.sg -** *** -*.lsAMPLE INA 1.2036 :\ £85874ii37928386: 1405235033 .j4.oo rSAMPLE [NA 'j.1762 :( i294B8881B763so6-Fo5235034 f3.7o JsAMPLE INA J.1956 _'\2.9761179"2.9o65soo( :1405235035 r 3.42 lsAMPLE INA 1.1626 *12.863609378360937! 1405235036 j3.24 --lsAMPLE JNA 1.1769 J 2:666ss7io86ooso*1: . 1405235037 13.03 \sAMPLE \NA 1.0623 \ 2.s4121618026i'5s2 1405235038 [ 3.37 1.1634 I 2.8190l047368s432' -* f4o5235039J 3.47 jsAMPLE 1.0869 [ 14o5235040-14.15 lsAMPLE INA 1.1478 13.S3532so7s496o36 , .ji2o36274371 ___ jNIB !NA -!NA I *f120362743si 4:01 -* *IDuP 1405235021 1.16s4 I i34-6s9136969i4i42* ! 120362743913.s2
  • 1Ms 1405235021 :j.1654 \2.93766269G543os7( * --**---*--. GEL Laboratories LLC I of l 9/27/2016 11:25 AM Page 2692 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:56.34 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235021.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 8-DEC-2015 14:17:00. Acquisition date : 28-SEP-2016 08:45:02 Sample ID I405235021 Sample quantity 3.29000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:38:04.89 Elapsed real time: 0 00:38:05.06 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 59.10 BACKGROUND*CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 0 0.54 297.14 294 6 3.06E-03 37.8 Flag: "*" = Peak area was modified by background subtraction Page 2693 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:57.11 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235021.CNF;l *
  • Acquisition date 28-SEP-2016 08:45:02 Sensitivity 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:04.89 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:05.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Analyst initials: MJHl *
  • Sample ID I405235021 Sample Quantity 3.2900E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 1.235E+OO 4.824E+OO I-129 5.697E-02 2.039E-01 Page 2694 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 9.388E+OO 4.564E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:55.55 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2695 of 5809 Energy 59.10 Area 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.54 297.14 294 6 3.06E-03 37.8 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:56.68 Nuclide Line Activity Report Flag: "*" = Keyline Page 2696 of 5809 Summary of Nuclide Activity Sample ID : 1405235021 Acquisition date Page : 2 28-SEP-2016 08:45:02 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2697 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted . Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235021 Page : 3 Acquisition date : 28-SEP-2016 08:45:02 It 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 59.10 7 0 0.54 297.14 294 6 3.06E-03 75.6 l.63E+Ol Flags: "T" = Tentatively associated Page 2698 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:58.57 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235021.CNF;l * *Acquisition date 28-SEP-2016 08:45:02 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:04.89 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:05.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
  • Sample ID I405235021 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 3.2900E+00 GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : Il29 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2699 of 5809 Le (pCi/GRAM 4.057E+OO NOT IDENT. l.892E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:23:59.61 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235021.CNF;l *
  • Acquisition date 28-SEP-2016 08:45:02 Sensitivity 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:04.89 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:05.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
  • Sample ID I405235021 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 3.2900E+OO GRAM *
  • Quantity Err(%) 3.0395E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 l.235E+00 4.828E+OO I-129 5.697E-02 2.040E-01 Page 2700 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.860E+OO 2.056E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2701of5809 MDA COUNTS 11. 038 9 5.9373 6.0593 6. 2894 5.5290 0. 9690 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:19.03 ********************************************************************************
  • GEL. Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235022.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 8-DEC-2015 13:43:00. Acquisition date : 28-SEP-2016 08:45:25 Sample ID I405235022 Sample quantity 2.60000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:37:43.11 Elapsed real time: 0 00:37:43.26 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK *REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 6.24 27 50 0.49 30.14 28 6 1.20E-02 47.6 2 0 72 .18 6 2 0.48 360.25 356 7 2.76E-03 53.2 3 0 82.04 8 2 0.53 409.63 406 8 3.71E-03 44.5 4 0 92.46* 9 4 0.71 461.84 455 14 3.99E-03 68.1 5 0 132.97 9 0 0.33 664.67 658 12 3.98E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Page 2702 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:19.83 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235022.CNF;l * *Acquisition date 28-SEP-2016 08:45:25 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:37:43.11 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:37:43.26 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:43:00 Analyst initials: MJHl *
  • Sample ID I405235022 Sample Quantity 2.6000E+00 GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 8.869E+OO 9.085E+OO I-129 1.625E-01 3 .115E-01 Page 2703 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.302E+Ol 7.337E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:18.36 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 6.24 27 50 0.49 30.14 28 6 l.20E-02 47.6 2 0 72 .18 6 2 0.48 360.25 356 7 2. 7.6E-03 53.2 3 0 82.04 8 2 0.53 409.63 406 8 3. 71E-03 44.5 4 0 92.46 19 4 0.71 461. 84 455 14 8.61E-03 30.5 5 0 132.97 9 0 0.33 664.67 658 12 3.98E-03 33.3 Page 2704 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:19.38 Nuclide Line Activity Report Flag: "*" = Keyline Page 2705 of 5809 Summary of Nuclide Activity Sample ID : I405235022 Total number of lines in spectrum Number of unidentified lines Acquisition date 5 5 Page : 2 28-SEP-2016 08:45:25 Number of lines tentatively identified by **** There are no nuclides meeting summary NID 0 criteria 0.00% **** Flags: "K" "E" Page 2706 of 5809 Keyline not found Manually edited "M" Manually accepted "A" Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235022 Acquisition date : 28-SEP-2016 08:45:25 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 6.24 27 50 0.49 30.14 28 6 l.20E-02 95.3 2.66E-30 0 72.18 6 2 0.48 360.25 356 7 2.76E-03 **** 4.60E-04 0 82.04 8 2 0.53 409.63 406 8 3.71E-03 89.l 5.78E-06 0 92.46 9 . 4 o. 71 461.84 455 14 3.99E-03 **** 4.36E-08 0 132. 97 9 0 0.33 664.67 658 12 3.98E-03 66.7 6.43E-17 Flags: "T" = Tentatively associated Page 2707 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:21.69 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235022.CNF;l *
  • Acquisition date 28-SEP-2016 08:45:25 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:37:43.11 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:37:43.26 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:43:00 Nuclide Library : IODINE *
  • Sample ID I405235022 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.6000E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2708 of 5809 Le (pCi/GRAM 9.582E+00 NOT IDENT. 2.984E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:22.73 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235022.CNF;l *
  • Acquisition date 28-SEP-2016 08:45:25 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:37:43.11 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:37:43.26 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:43:00 Nuclide Library : IODINE *
  • Sample ID I405235022 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.6000E+00 GRAM *
  • Quantity Err(%) 3.8462E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 8.869E+OO 9.217E+OO I-129 1.625E-01 3.120E-01 Page 2709 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 1.005E+Ol 3.205E-01 NOT IDENT. NOT IDENT.
                                                                                                                                                              • * * *
  • GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29. 62 35.49 39.58 Page 2710 of 5809 MDA COUNTS 2.1038 3.2110 3.2426 2.2015 2.2293 2.2868 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:42.35 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235023.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 2-DEC-2015 10:40:00. Acquisition date : 28-SEP-2016 08:45:52 Sample ID I405235023 Sample quantity 3.24000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:37:20.59 Elapsed real time: 0 00:37:20.71 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2711 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:43.56 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235023.CNF;l *
  • Acquisition date 28-SEP-2016 08:45:52 Sensitivity 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:37:20.59 Abundance limit : 75.000 * *Elapsed real time: 0 00:37:20.71 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:40:00 Analyst initials: MJHl *
  • Sample ID I405235023 Sample Quantity 3.2400E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-s igma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -6.749E+00 5.000E+OO I-129 5.620E-02 2 .196E-01 Page 2712 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.406E+OO 5.229E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:41.52 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2713of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:24:43.03 Nuclide Line Activity Report Flag: "*" = Keyline Page 2714 of 5809 Summary of Nuclide Activity Sample ID : 1405235023 Acquisition date Page : 2 28-SEP-2016 08:45:52 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2715of5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235023 None Flags: "T" Tentatively associated Page 2716of5809 Acquisition date Page : 3 28-SEP-2016 08:45:52 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:06.50 ********************************************************************************

  • GgL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235024.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 75-SEP-2016 12:23:15 Sample date 8-DEC-2015 14:13:00. Acquisition date : 28-SEP-2016 08:46:16 Sample ID I405235024 Sample quantity 2.60000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:36:58.84 Elapsed real time: 0 00:36:58.88 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2717 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:07.39 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235024.CNF;l *
  • Acquisition date 28-SEP-2016 08:46:16 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:36:58.84 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:36:58.88 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:13:00 Analyst initials: MJHl *
  • Sample ID I405235024 Sample Quantity 2.6000E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.080E-01 4.166E+OO I-129 -2.406E-01 2. 722E-01 Page 2718 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.214E+Ol 2.542E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:05.65 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2719of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:06.88 Nuclide Line Activity Report Flag: "*" = Keyline Page 2720 of 5809 Summary of Nuclide Activity Sample ID : I405235024 Acquisition date Page : 2 28-SEP-2016 08:46:16 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2721of5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235024 None Flags: "T" Tentatively associated Page 2722 of 5809 Acquisition date Page : 3 28-SEP-2016 08:46:16 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:09.59 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235024.CNF;l *
  • Acquisition date 28-SEP-2016 08:46:16 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:36:58.84 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:36:58.88 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:13:00 Nuclide Library : IODINE *
  • Sample ID I405235024 Analyst initials: MJHl * *Batch Number 1598620 Sample Quantity : 2.6000E+00 GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2723 of 5809 Le (pCi/GRAM 3.836E+OO NOT IDENT. O.OOOE+OO NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:11.02 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235024.CNF;l *
  • Acquisition date 28-SEP-2016 08:46:16 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:36:58.84 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:36:58.88 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:13:00 Nuclide Library : IODINE *
  • Sample ID I405235024 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.6000E+OO GRAM *
  • Quantity Err(%) 3.8462E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Geometry : Il29 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 3.080E-01 4.167E+OO I-129 -2.406E-01 2.733E-01 Page 2724 of 5809 TPU (1.96-sigma) TPU ( 1. 96-sigma) 4.169E+OO 2.940E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2725 of 5809 MDA COUNTS 0. 8133 2.5641 1. 7568 0.9231 0.0000 2.0378 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:34.51 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235025.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 8-DEC-2015 13:38:00. Acquisition date : 28-SEP-2016 08:46:38 Sample ID I405235025 Sample quantity 2.36000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:36:39.40 Elapsed real time: 0 00:36:39.44 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2726 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:36.40 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235025.CNF;l * *Acquisition date 28-SEP-2016 08:46:38 Sensitivity : 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:36:39.40 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:36:39.44 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:38:00 Analyst initials: MJHl *'
  • Sample ID I405235025 Sample Quantity 2.3600E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6'I129.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.082E+OO 4.463E+OO I-129 2.049E-01 2. 772E-01 Page 2727 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.515E+Ol 9.224E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:32.99 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2728 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:35.36 Nuclide Line Activity Report Flag: "*" = Keyline Page 2729 of 5809 Summary of Nuclide Activity Sample ID : 1405235025 Acquisition date Page : 2 28-SEP-2016 08:46:38 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2730 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235025 None Flags: "T" Tentatively associated Page 2731 of 5809 Page : 3 Acquisition date 28-SEP-2016 08:46:38 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:39.58 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235025.CNF;l * *Acquisition date 28-SEP-2016 08:46:38 Sensitivity 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:36:39.40 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:36:39.44 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:38:00 Nuclide Library : IODINE *
  • Sample ID I405235025 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.3600E+OO GRAM *
  • Recovery 1.00000 Carrier Weight :
  • 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2732 of 5809 Le (pCi/GRAM 5.298E+OO NOT IDENT. 3.291E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 09:25:41.99 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235025.CNF;l *
  • Acquisition date 28-SEP-2016 08:46:38 Sensitivity : 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:36:39.40 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:36:39.44 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:38:00 Nuclide Library : IODINE *
  • Sample ID I405235025 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.3600E+OO GRAM *
  • Quantity Err(%) 4.2373E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.082E+OO 4.472E+OO I-129 2.049E-01 2.780E-01 Page 2733 of 5809 TPU ( 1. 96-sigma) TPU (1. 96-sigma) 4.683E+OO 2.929E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2734 of 5809 MDA COUNTS 0.0000 0.0000 0.0000 2.3167 0.0000 0.8284 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:42.48 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235026.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 8-DEC-2015 10:15:00. Acquisition date : 28-SEP-2016 09:28:33 Sample ID I405235026 Sample quantity : 2.54000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:46:46.72 Elapsed real time: 0 00:46:46.92 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 95.02 120.45 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 6 3 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.39 10 0.30 478.17 606.33 474 8 2.14E-03 40.8 598 10 1.07E-03205.5 Flag: "*" = Peak area was modified by background subtraction Page 2735 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:43.29 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235026.CNF;l * *Acquisition date 28-SEP-2016 09:28:33 Sensitivity 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 * *Elapsed live time: 0 00:46:46.72 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:46.92 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:15:00 Analyst initials: MJHl *
  • Sample ID I405235026 Sample Quantity 2.5400E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 7.436E-01 3.805E+00 I-129 2.314E-02 1.752E-01 Page2736of5809 MDA (pCi/GRAM MDA (pCi/GRAM 7.756E+OO 3.996E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:40.82 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2737 of 5809 Energy 95.02 120.45 Area 6 3 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.39 478.17 10 0.30 .606.33 474 8 2.14E-03 40.8 598 10 l.07E-03205.5 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:42.85 Nuclide Line Activity Report Flag: "*" = Keyline Page 2738 of 5809 Surrunary of Nuclide Activity Sample ID : 1405235026 Acquisition date Page : 2 28-SEP-2016 09:28:33 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting surrunary Flags: "K" "E" Page 2739 of 5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria **** 0.00% Manually accepted . Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235026 Page : 3 Acquisition date : 28-SEP-2016 09:28:33 It 0 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 95.02 120.45 6 3 0 0.39 10 0.30 Flags: "T" = Tentatively associated Page 2740 of 5809 478.17 474 8 2.14E-03 81.6 5.50E+OO 606.33 598 10 1.07E-03 **** 2.27E+OO VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:44.92 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235026.CNF;l *
  • Acquisition date 28-SEP-2016 09:28:33 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 * *Elapsed live time: 0 00:46:46.72 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:46.92 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:15:00 Nuclide Library : IODINE *
  • Sample ID I405235026 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.5400E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2741of5809 Le (pCi/GRAM 3.204E+OO NOT IDENT. l.586E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:15:46.24 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235026.CNF;l *
  • Acquisition date 28-SEP-2016 09:28:33 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 * *Elapsed live time: 0 00:46:46.72 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:46.92 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:15:00 Nuclide Library : IODINE *
  • Sample ID I405235026 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.5400E+OO GRAM *
  • Quantity Err(%) 3.9370E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0.00000 * * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-s igma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.436E-01 3.807E+OO I-129 2.314E-02 1. 752E-01 Page 2742 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.822E+OO 1. 755E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2743 of 5809 MDA COUNTS 6.1327 4.2409 6.0593 4.4924 4.6075 4.8449 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:06.11 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235027.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : Z5-SEP-2016 12:22:59 Sample date 8-DEC-2015 10:19:00. Acquisition date : 28-SEP-2016 09:28:55 Sample ID I405235027 Sample quantity 2.97000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:46:24.90 Elapsed real time: 0 00:46:25.06 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 54.20 6 7 0.71 270.24 263 9 2.31E-03 82.7 2 0 87.03 9 3 0.99 434.61 430 10 3.28E-03 46.8 3 0 92.83* 9 3 0.82 463.68 458 11 3.41E-03 63.7 4 0 126.22 9 0 0.40 630.89 625 12 3.23E-03 33.3 5 0 129.38 9 3 0.35 646.72 639 13 3.19E-03 53.5 6 0 144.07 11 0 0.56 720. 27 716 10 3.95E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 2744 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:06.88 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235027.CNF;l * *Acquisition date 28-SEP-2016 09:28:55 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:46:24.90 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:25.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:19:00 Analyst initials: MJHl *
  • Sample ID I405235027 Sample Quantity 2.9700E+00 GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15 '* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -5.286E-02 7.746E+00 I-129 4.226E-02 2.471E-01 Page 2745 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.557E+Ol 5.254E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:05.43 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 13.90 5 27 0.31 68.47 61 10 1.78E-03202.6 2 0 54.20 6 7 0.71 270.24 263 9 2.31E:--03 82.7 3 0 87.03 9 3 0.99 434.61 430 10 3.28E-03 46.8 4 0 92.83 22 3 0.82 463.68 458 11 8.02E-03 25.5 5 0 126.22 9 0 0.40 630.89 625 12 3.23E-03 33.3 6 0 129.38 9 3 0.35 646.72 639 13 3.19E-03 53.5 7 0 144.07 11 0 0.56 720.27 716 10 3.95E-03 30.2 Page 2746 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:06.44 Nuclide Line Activity Report Flag: "*" = Keyline Page 2747 of 5809 Summary of Nuclide Activity Sample ID : 1405235027 Acquisition date Page : 2 28-SEP-2016 09:28:55 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2748 of 5809 Keyline not found Manually edited "M" "A" 6 6 NID 0 criteria **** .o. 00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235027 Acquisition date : 28-SEP-2016 09:28:55 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 54.20 6 7 0.71 270.24 263 9 2. 31E-03 **** 4.79E-01 0 87.03 9 3 0.99 434.61 430 10 3.28E-03 93.6 5.73E-07 0 92.83 9 3 0.82 463.68 458 11 3.41E-03 **** 3.66E-08 0 126.22 9 0. 0.40 630.89 625 12 3.23E-03 66.7 2.lOE-15 0 129.38 9 3 0.35 646.72 639 13 3.19E-03 **** 4. llE-16 0 144.07 11 0 0.56 720.27 716 10 3.95E-03 60.3 1. 97E-19 Flags: "T" = Tentatively associated Page 2749 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:08.39 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235027.CNF;l * *Acquisition date 28-SEP-2016 09:28:55 Sensitivity 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:46:24.90 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:25.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:19:00 Nuclide Library : IODINE *
  • Sample ID I405235027 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.9700E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2750 of 5809 Le (pCi/GRAM 6.407E+OO NOT IDENT. 2.140E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:09.44 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235027.CNF;l * *Acquisition date 28-SEP-2016 09:28:55 Sensitivity 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:46:24.90 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:25.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:19:00 Nuclide Library : IODINE *
  • Sample ID I405235027 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.9700E+OO GRAM *
  • Quantity Err(%) 3.3670E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -5.286E-02 7.746E+OO I-129 4.226E-02 2. 471E-01 Page 2751of5809 TPU ( 1. 96-sigma) TPU ( 1 . 96-sigma ) 7.746E+OO 2.478E-01 NOT IDENT. NOT IDENT.
                                                                                                                                                              • * * *
  • GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2752 of 5809 MDA COUNTS 7.3633 5.3517 2.1618 3.3023 2.2293 3.4302 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:29.09 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235028.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 23-NOV-2015 14:50:00 Acquisition date : 28-SEP-2016 09:29:20 Sample ID I405235028 Sample quantity 2.61000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:46:04.82 Elapsed real time: 0 00:46:04.97 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 35.56 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 7 4 0.60 177.46 173 7 2. 35E-03 61. 8 Flag: "*" = Peak area was modified by background subtraction Page 2753 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:29.91 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235028.CNF;l * *Acquisition date 28-SEP-2016 09:29:20 Sensitivity : 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:46:04.82 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:04.97 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:50:00 Analyst initials: MJHl *
  • Sample ID I405235028 Sample Quantity 2.6100E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.708E+OO 4.341E+OO I-129 -2. llOE-01 2.433E-01 Page 2754 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.169E+Ol 3.417E-01 FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:28.17 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 35.56 7 4 0.60 177.46 173 7 2.35E-03 61. 8 2 0 92.73 5 7 0.22 463.91 460 6 1.73E-03100.6 Page 2755 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:29.41 Nuclide Line Activity Report Flag: "*" = Keyline Page 2756 of 5809 Summary of Nuclide Activity Sample ID : 1405235028 Acquisition date Page : 2 28-SEP-2016 09:29:20 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2757 of 5809 Keyline not found Manually edited "M" "A" 1 0 NID 1 criteria 100.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235028 Page : 3 Acquisition date : 28-SEP-2016 09:29:20 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 35.56 7 4 0.60 177.46 173 7 2.35E-03 **** 1.66E+Ol T Flags: "T" Tentatively associated Page 2758 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:31.48 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235028.CNF;l *
  • Acquisition date 28-SEP-2016 09:29:20 Sensitivity 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:46:04.82 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:04.97 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:50:00 Nuclide Library : IODINE *
  • Sample ID I405235028 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.6100E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : Il29 *
  • Eff.' File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2759 of 5809 Le (pCi/GRAM 4.504E+OO FAIL ABUN 1.080E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:32.55 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235028.CNF;l *
  • Acquisition date 28-SEP-2016 09:29:20 Sensitivity 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:46:04.82 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:46:04.97 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:50:00 Nuclide Library : IODINE *
  • Sample ID I405235028 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.6100E+OO GRAM *
  • Quantity Err(%) 3.8314E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1 . 96-s i grna) Non-Identified Nuclides Nuclide I-125 I-129 Page 2760 of 5809 Key-Line Activity (pCi/GRAM 2.708E+00 -2. llOE-01 K.L Act error ( 1. 96-sigma) 4.366E+OO 2.442E-01 TPU (1.96-sigma) TPU (1. 96-sigma) 4.534E+00 FAIL ABUN 2.621E-01 NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2761 of 5809 MDA COUNTS 1.0858 5.5444 4.4884 1.1470 1.1645 3.6015 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:52.26 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235029.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 23-NOV-2015 11:10:00 Acquisition date : 28-SEP-2016 09:29:56 Sample ID I405235029 Sample quantity 2.80000E+OO GRAM Detector name : XRAY5 Detector geometry: Il29 Elapsed live time: 0 00:45:30.43 Elapsed real time: 0 00:45:30.47 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It l 0 Energy 63.59* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err l 4 0.56 316.31 310 8 2.83E-04569.7 Flag: "*" = Peak area was modified by background subtraction Page 2762 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:53.03 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235029.CNF;l *
  • Acquisition date 28-SEP-2016 09:29:56 Sensitivity : 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: O 00:45:30.43 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:45:30.47 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:10:00 Analyst initials: MJHl *
  • Sample ID I405235029 Sample Quantity 2.8000E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -4.832E+OO 4.735E+OO I-129 -5.022E-02 2.177E-01 Page 2763 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.025E+OO 5.210E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:51.60 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2764 of 5809 Energy 63.59 Area 6 Bkgnd FWHM Channel 4 0.56 316.31 Left 310 Pw Cts/Sec %Err 8 2.12E-03 73.1 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:52.59 Nuclide Line Activity Report Flag: "*" = Keyline Page 2765 of 5809 Summary of Nuclide Activity Sample ID : I405235029 Acquisition date Page : 2 28-SEP-2016 09:29:56 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2766 of 5809 Keyline not found Manually edited "M" "A" l 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235029 Page : 3 Acquisition date : 28-SEP-2016 09:29:56 It 0 Energy 63.59 Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 1 4 0.56 316.31 310 8 2.83E-04 **** 3.14E+OO Flags: "T" Tentatively associated Page 2767 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:54.58 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235029.CNF;l *
  • Acquisition date 28-SEP-2016 09:29:56 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:45:30.43 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:45:30.47 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:10:00 Nuclide Library : IODINE *
  • Sample ID I405235029 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.BOOOE+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO:'[CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2768 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. l.647E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:16:55.66 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235029.CNF;l *
  • Acquisition date 28-SEP-2016 09:29:56 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:45:30.43 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:45:30.47 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:10:00 Nuclide Library : IODINE *
  • Sample ID I405235029 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.8000E+00 GRAM *
  • Quantity Err(%) 3.5714E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : Il29 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.832E+OO 4.810E+OO I-129 -5.022E-02 2.177E-01 Page 2769 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5.280E+OO 2.189E-01 NOT IDENT. NOT IDENT.
                                                                                                                                                              • * * *
  • GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2770 of 5809 MDA COUNTS 3.2531 1. 7094 0.8784 4.6154 0.9543 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:15.32 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235030.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Configuration Background file Background date : 75-SEP-2016 12:23:20 Sample date 23-NOV-2015 14:44:00 Acquisition date : 28-SEP-2016 09:30:21 Sample ID I405235030 Sample quantity : 2.60000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:45:07.66 Elapsed real time: 0 00:45:07.72 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 7.43* 10.27 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 4 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 2 0.56 1 0.36 36.37 50.62 34 49 5 1.66E-03 81.4 4 2.68E-03 41.4 Flag: "*" = Peak area was modified by background subtraction Page 2771 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:16.26 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235030.CNF;l *
  • Acquisition date 28-SEP-2016 09:30:21 Sensitivity : 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 * *Elapsed live time: 0 00:45:07.66 Abundance limit : 75.000 * *Elapsed real time: 0 00:45:07.72 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:44:00 Analyst initials: MJHl *
  • Sample ID I405235030 Sample Quantity 2.6000E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -2.092E+OO 4.lOlE+OO I-129 -6.592E-02 2.316E-01 Page 2772 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 4.005E+OO 4.432E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:14.59 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2773 of 5809 Energy 7.43 10.27 Area 7 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 2 0.56 1 0.36 36.37 50.62 34 49 5 2.59E-03 49.7 4 2.68E-03 41.4 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:15.71 Nuclide Line Activity Report Flag: "*" = Keyline Page 2774 of 5809 Summary of Nuclide Activity Sample ID : 1405235030 Acquisition date Page : 2 28-SEP-2016 09:30:21 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2775 of 5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria 0.00% **** Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235030 Page : 3 Acquisition date : 28-SEP-2016 09:30:21 It 0 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 7.43 10.27 4 7 2 0.56 1 0.36 Flags: "T" = Tentatively associated Page 2776 of 5809 36.37 50.62 34 5 1.66E-03 **** 3.52E-03 49 4 2.68E-03 82.8 7.lOE-02 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:17.92 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235030.CNF;l *
  • Acquisition date 28-SEP-2016 09:30:21 Sensitivity : 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 * *Elapsed live time: 0 00:45:07.66 Abundance limit : 75.000 * *Elapsed real time: 0 00:45:07.72 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:44:00 Nuclide Library : IODINE *
  • Sample ID I405235030 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.6000E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2777 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT.
  • l.241E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:17:19.07 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235030.CNF;l * *Acquisition date 28-SEP-2016 09:30:21 Sensitivity 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:45:07.66 Abundance limit : 75.000 * *Elapsed real time: 0 00:45:07.72 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:44:00 Nuclide Library : IODINE *
  • Sample ID I405235030 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.6000E+OO GRAM *
  • Quantity Err(%) 3.8462E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016' 10: 07: 09 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( l. 96-sigma) Non-Identified Nuclides Key-Line-Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.092E+OO 4.105E+OO I-129 -6.592E-02 2.317E-01 Page 2778 of 5809 TPU (1. 96-sigma) TPU (1.96-sigma) 4.212E+00 2.336E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2779 of 5809 MDA COUNTS 1. 4157 1.4643 0.0000 0.7722 0.7906 1. 6568 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:30.25 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235031.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : Z5-SEP-2016 12:22:54 Sample date 26-NOV-2015 14:25:00 Acquisition date : 28-SEP-2016 10:17:59 Sample ID I405235031 Sample quantity 2.76000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.14 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 23.69 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 20 20 0.56 118.72 113 11 l.09E-02 53.0 Flag: "*" = Peak area was modified by background subtraction Page 2780 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:31.04 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration. DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235031.CNF;l *
  • Acquisition date 28-SEP-2016 10:17:59 Sensitivity 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
  • Sample date 26-NOV-2015 14:25:00 Analyst initials: MJHl * *Sample ID I405235031 Sample Quantity 2.7600E+00 GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1 . 96-sigma ) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1.96-sigma) I-125 -9. 311E-01 5. 701E+OO I-129 O.OOOE+OO 2.630E-01 Page 2781of5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.077E+Ol 5.775E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:29.46 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2782 of 5809 Energy 23.69 Area 20 Bkgnd FWHM Channel 20 0.56 118.72 Left 113 Pw Cts/Sec %Err 11 l.09E-02 53.0 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:30.59 Nuclide Line Activity Report Flag: "*" == Keyline Page 2783 of 5809 Summary of Nuclide Activity Sample ID : 1405235031 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 10:17:59 Number of lines tentatively identified by **** There are no nuclides meeting summary 1 1 NID 0 criteria 0.00% **** Flags: "K" "E" Page 2784 of 5809 Keyline not found Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235031 Page : 3 Acquisition date : 28-SEP-2016 10:17:59 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 23.69 20 20 0.56 118.72 113 11 l.09E-02 **** l.80E+Ol Flags: "T" = Tentatively Page 2785 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:32.83 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235031.CNF;l *
  • Acquisition date 28-SEP-2016 10:17:59 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
  • Sample date 26-NOV-2015 14:25:00 Nuclide Library : IODINE *
  • Sample ID I405235031 Analyst initials: MJHl * *Batch Number 1598620 Sample Quantity : 2.7600E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-1'25 I-129 Page 2786 of 5809 Le (pCi/GRAM 4.276E+OO NOT IDENT. 2.296E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:48:33.95 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235031.CNF;l * *Acquisition date 28-SEP-2016 10:17:59 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.14 Half life ratio : ***** *
  • Sample date 26-NOV-2015 14:25:00 Nuclide Library : IODINE *
  • Sample ID I405235031 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.7600E+00 GRAM *
  • Quantity Err ( % ) 3. 6232E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 * *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM . ( 1. 96-sigma) I-125 -9. 311E-01 5.703E+OO I-129 O.OOOE+OO 2.630E-01 Page 2787 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 5. 719E+OO O.OOOE+OO NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2788 of 5809 MDA COUNTS 6.1327 5.0891 4.3281 6.2894 8.2934 6.7829 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:03.08 ******************************************************************************** GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235032.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 75-SEP-2016 12:22:59 Sample date 23-NOV-2015 11:48:00 Acquisition date : 28-SEP-2016 10:18:25 Sample ID I405235032 Sample quantity 2.86000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.13 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike Ib : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 185.52* *BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 13 0 1.80 927.89 920 15 7.44E-03 32.7 Flag: "*" = Peak area was modified by background subtraction Page 2789 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:03.88 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* ** * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235032.CNF;l *
  • Acquisition date 28-SEP-2016 10:18:25 Sensitivity 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:48:00 Analyst initials: MJHl *
  • Sample ID I405235032 Sample Quantity 2.8600E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -7.655E-01 1. 096E+Ol I-129 9.754E-02 3.274E-01 Page 2790 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.298E+Ol 7.522E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:02.41 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2791 of 5809 Energy 185.52 Area 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 1.80 927.89 920 15 1.00E-02 23.6 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:03.42 Nuclide Line Activity Report Flag: "*" = Keyline Page 2792 of 5809 Summary of Nuclide Activity Sample ID : 1405235032 Acquisition date Page : 2 28-SEP-2016 10:18:25 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K". = Keyline not found "E" = Manually edited Page 2793 of 5809 "M" "A" 1 1 NID 0 criteria 0.00% **** Manually.accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235032 Page : 3 Acquisition date : 28-SEP-2016 10:18:25 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 185.52 13 0 1. 80 927.89 920 15 7.44E-03 65.3 5.39E-29 Flags: "T" = Tentatively associated Page 2794 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:05.33 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235032.CNF;l * *Acquisition date 28-SEP-2016 10:18:25 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:48:00 Nuclide Library : IODINE *
  • Sample ID I405235032 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.8600E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;15
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2795 of 5809 Le (pCi/GRAM 8.854E+OO NOT IDENT. 2.979E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:06.55 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* ** * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235032.CNF;l *
  • Acquisition date 28-SEP-2016 10:18:25 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.13 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:48:00 Nuclide Library : IODINE *
  • Sample ID I405235032 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.8600E+OO GRAM *
  • Quantity Err(%) 3.4965E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -7.655E-01 1.096E+Ol I-129 9.754E-02 3.275E-01 Page 2796 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 1.097E+Ol 3.305E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2797 of 5809 MDA COUNTS 4.2076 3.2110 5.4044 5.5038 2.2293 2.2868 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:26.12 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235033.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 23-NOV-2015 11:53:00 Acquisition date : 28-SEP-2016 10:18:47 Sample ID I405235033 Sample quantity 3.29000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.09 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2798 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:26.94 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235033.CNF;l *
  • Acquisition date 28-SEP-2016 10:18:47 Sensitivity : 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:53:00 Analyst initials: MJHl *
  • Sample ID I405235033 Sample Quantity 3.2900E+00 GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4 * .Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert (1.96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 5.241E-01 1.560E+OO I-129 7.937E-02 1.313E-01 Page 2799 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 6.979E+OO 4.649E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:25.37 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2800 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:26.47 Nuclide Line Activity Report Flag: "*" = Keyline Page 2801of5809 Summary of Nuclide Activity Sample ID : I405235033 Acquisition date Page : 2 28-SEP-2016 10:18:47 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2802 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235033 None Flags: "T" Tentatively associated Page 2803 of 5809 Acquisition date Page : 3 28-SEP-2016 10:18:47 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:29.21 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235033.CNF;l *
  • Acquisition date 28-SEP-2016 10:18:47 Sensitivity 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:53:00 Nuclide Library : IODINE *
  • Sample ID I405235033 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 3.2900E+OO GRAM *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2804 of 5809 Le (pCi/GRAM 1.852E+OO NOT IDENT. 1.559E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:30.33 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235033.CNF;l *
  • Acquisition date 28-SEP-2016 10:18:47 Sensitivity 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.09 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:53:00 Nuclide Library : IODINE *
  • Sample ID I405235033 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 3.2900E+OO GRAM *
  • Quantity Err(%) 3.0395E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 '*
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 5.241E-01 1.563E+OO I-129 7.937E-02 1.316E-01 Page 2805 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 1.581E+OO l.364E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2806 of 5809 MDA COUNTS 0.0000 0.0000 1.1221 4.5881 2.3289 1.2005 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:51.59 ******************************************************************************** GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235034.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 75-SEP-2016 12:23:15 Sample date 23-NOV-2015 11:20:00 Acquisition date : 28-SEP-2016 10:19:14 Sample ID I405235034 Sample quantity 2.98000E+00 GRAM Detector name : XRAY5 Detector geometry: Il29 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.02 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.33* *BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0 0.33 315.00 311 7 3.16E-03 54.5 Flag: "*" = Peak area was modified by background subtraction Page 2807 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:52.44 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235034.CNF;l *
  • Acquisition date 28-SEP-2016 10:19:14 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:20:00 Analyst initials: MJHl *
  • Sample ID I405235034 Sample Quantity 2.9800E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;'5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1 . 96-sigma ) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -5.212E+OO 7.694E+OO I-129 O.OOOE+OO 1.978E-01 Page 2808 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.450E+Ol 2.734E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:50.97 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2809 of 5809 Energy 63.33 Area 9 Bkgnd FWHM Channel 0 0.33 315.00 Left 311 Pw Cts/Sec %Err 7 5.00E-03 33.3 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:51.95 Nuclide Line Activity Report Flag: "*" = Keyline Page 2810of5809 Summary of Nuclide Activity Sample ID : 1405235034 Acquisition date Page : 2 28-SEP-2016 10:19:14 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K".= Keyline not found "E" = Manually edited Page 2811of5809 "M" "A" 1 1 NID 0 criteria **** 0.00% Manually.accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235034 Page : 3 Acquisition date : 28-SEP-2016 10:19:14 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 63.33 6 0 0.33 315.00 311 7 3.16E-03 **** 3.19E+OO Flags: "T" Tentatively associated Page 2812of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:54.28 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235034.CNF;l *
  • Acquisition date 28-SEP-2016 10:19:14 Sensitivity : 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:20:00 Nuclide Library : IODINE *
  • Sample ID I405235034 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.9800E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File' : DKAlOO:[CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2813of5809 Le (pCi/GRAM 4.383E+OO NOT IDENT. O.OOOE+OO NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:49:55.54 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235034.CNF;l *
  • Acquisition date 28-SEP-2016 10:19:14 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.02 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:20:00 Nuclide Library : IODINE *
  • Sample ID I405235034 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.9800E+OO GRAM *
  • Quantity Err(%) 3.3557E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry * : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 -5.212E+OO 7.748E+OO I-129 O.OOOE+OO O.OOOE+OO Page 2814 of 5809 TPU ( 1. 96-sigma) TPU (1.96-sigma) 8.097E+OO O.OOOE+OO NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2815of5809 MDA COUNTS 3.2531 0.0000 0.0000 0.9231 0.9543 0.0000 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:15.90 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235035.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 25-SEP-2016 12:23:20 Sample date 23-NOV-2015 11:06:00 Acquisition date : 28-SEP-2016 10:19:45 Sample ID I405235035 Sample quantity 2.86000E+OO GRAM Detector name : XRAY6 Detector geometry: I129 Elapsed live time: 0 00:30:00.00 Elapsed real time: 0 00:30:00.04 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.28* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 9 0 0.35 315.83 312 7 5.17E-03 37.8 Flag: "*" = Peak area was modified by background subtractiori Page 2816of5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:16.74 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235035.CNF;l *
  • Acquisition date 28-SEP-2016 10:19:45 Sensitivity 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:06:00 Analyst initials: MJHl *
  • Sample ID I405235035 Sample Quantity 2.8600E+00 GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 O.OOOE+OO 3. 969E+OO I-129 5.275E-02 3.929E-01 Page 2817 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 5.488E+OO 9.144E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:15.20 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 Page 2818 of 5809 Energy 63.28 Area 12 Bkgnd FWHM Channel 0 0.35 315.83 Left 312 Pw Cts/Sec %Err 7 6.67E-03 28.9 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:16.26 Nuclide Line Activity Report Flag: "*" = Keyline Page 2819of5809 Summary of Nuclide Activity Sample ID : 1405235035 Acquisition date Page : 2 28-SEP-2016 10:19:45 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2820 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : I405235035 Page : 3 Acquisition date : 28-SEP-2016 10:19:45 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 63.28 9 0 0.35 315.83 312 7 5.17E-03 75.6 3.09E+OO Flags: "T" = Tentatively associated Page 2821of5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:18.32 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235035.CNF;l *
  • Acquisition date 28-SEP-2016 10:19:45 Sensitivity 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:06:00 Nuclide Library : IODINE *
  • Sample ID I405235035 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.8600E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBE'RRA.GAMMA]EFF XRAY6 Il29.CNF;5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2822 of 5809 Le (pCi/GRAM O.OOOE+OO NOT IDENT. 3.240E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 10:50:19.52 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235035.CNF;l * *Acquisition date 28-SEP-2016 10:19:45 Sensitivity 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:30:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:30:00.04 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:06:00 Nuclide Library : IODINE *
  • Sample ID I405235035 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.8600E+OO GRAM *
  • Quantity Err(%) 3.4965E-03 % *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 O.OOOE+OO 0.000E+OO I-129 5.275E-02 3.929E-01 Page 2823 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) O.OOOE+OO 3.936E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2824 of 5809 MDA COUNTS 0.0000 1.4643 0.0000 0.0000 0.7906 0.8284 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:06.75 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235036.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY1.CNF;415 Background date : 25-SEP-2016 12:22:54 Sample date 23-NOV-2015 11:12:00 Acquisition date : 28-SEP-2016 11:17:38 Sample ID I405235036 Sample quantity 2.67000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.22 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 32.52 108.45 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 15 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 6 0.53 9 0.21 163.19 545.85 157 533 12 4.22E-03 41.1 16 2.35E-03 82.6 Flag: "*" = Peak area was modified by background subtraction Page 2825 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:07.53 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235036.CNF;l *
  • Acquisition date 28-SEP-2016 11:17:38 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.22 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:12:00 Analyst initials: MJHl *
  • Sample ID I405235036 *Sample Quantity 2.6700E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 * *' Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6 * ***********************************************F*****F************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.077E+OO 4.349E+OO I-129 3.934E-05 l.665E-01 Page 2826 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 7.270E+OO 3.518E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:06.05 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 32.52 15 6 0.53 163.19 157 12 4.22E-03 41.1 2 0 108.45 8 9 0.21 545.85 533 16 2.35E-03 82.6 Page 2827 of 5809 - VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:07.11 Nuclide Line Activity Report Flag: "*" Key line Page 2828 of 5809 Summary of Nuclide Activity Sample ID : 1405235036 Total number of lines in spectrum Number of unidentified lines Acquisition date 2 Page : 2 28-SEP-2016 11:17:38 Number of lines tentatively identified by **** There are no nuclides meeting summary 2 NID 0 criteria 0.00% **** Flags: "K" "E" Page 2829 of 5809 Keyline not found Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235036 Page : 3 Acquisition date : 28-SEP-2016 11:17:38 It 0 0 Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 32.52 108.45 15 8 6 0.53 9 0.21 Flags: "T" = Tentatively associated Page 2830 of 5809 163.19 157 12 4.22E-03 82.2 2.28E+Ol 545.85 533 16 2.35E-03 **** 3.47E+OO VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:09.17 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235036.CNF;l *
  • Acquisition date 28-SEP-2016 11:17:38 Sensitivity 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: O 01:00:00.22 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:12:00 Nuclide Library : IODINE *
  • Sample ID I405235036 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.6700E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl I129.CNF;6
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2831 of 5809 Le (pCi/GRAM 3.040E+OO NOT IDENT. 1.454E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:10.23 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235036.CNF;l * *Acquisition date 28-SEP-2016 11:17:38 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.22 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:12:00 Nuclide Library : IODINE *
  • Sample ID I405235036 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.6700E+OO GRAM *
  • Quantity Err(%) 3.7453E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -2.077E+OO 4.365E+OO I-129 3.934E-05 1.665E-01 Page 2832 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 4.464E+OO 1.665E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29. 62 27.34 29. 62 35.49 39.58 Page 2833 of 5809 MDA COUNTS 13.4920 7.6336 7.7906 6.7387 3.6860 4.8449 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:32.74 ********************************************************************************
  • GEL Laboratories *LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235037.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 25-SEP-2016 12:22:59 Sample date 30-NOV-2015 11:19:00 Acquisition date : 28-SEP-2016 11:18:01 Sample ID I405235037 Sample quantity 2.84000E+OO GRAM Detector name : XRAY2 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.20 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 24.46 10 5 0.50 121.32 114 10 2.65E-03 55.0 2 4 91. 42 12 3 0.79 456.60 454 14 3.41E-03 27.3 3.05E+OO 3 4 92.50* 19 2 0.86 462.00 454 14 5.23E-03 33.7 4 0 147.24 9 11 1. 41 736.13 723 15 2.45E-03 89.4 5 0 153.65 13 0 0.33 768.23 763 10 3.61E-03 27.7 6 0 185.93* 20 0 1.14 929.93 920 18 5.49E-03 29.2 Flag: "*" = Peak area was modified by background subtraction Page 2834 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:33.51 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235037.CNF;l * *Acquisition date 28-SEP-2016 11:18:01 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
  • Sample date 30-NOV-2015 11:19:00 Analyst initials: MJHl *
  • Sample ID I405235037 Sample Quantity 2.8400E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • E'ff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.085E-01 5.704E+OO I-129 -l.442E-02 2.213E-01 Page 2835 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 1.168E+Ol 4.373E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:32.06 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 24.46 10 5 0.50 121. 32 114 10 2.65E-03 55.0 2 4 91. 42 12 .3 0.79 456.60 454 14 3. 41E-03 27.3 3.05E+OO 3 4 92.50 35 2 0.86 462.00 454 14 9.84E-03 16.4 4 0 147.24 9 11 1. 41 736.13 723 15 2.45E-03 89.4 5 0 153.65 13 0 0.33 768.23 763 10 3. 61E-03 27.7 6 0 185.93 29 0 1.14 929.93 920 18 8.06E-03 18.6 Page 2836 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:33.06 Nuclide Line Activity Report Flag: "*" = Keyline Page 2837 of 5809 Summary of Nuclide Activity Sample ID : 1405235037 Acquisition date Page : 2 28-SEP-2016 11:18:01 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2838 of 5809 Keyline not found Manually edited "M" "A" 6 6 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235037 Acquisition date : 28-SEP-2016 11:18:01 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 24.46 10 5 0.50 121.32 114 10 2.65E-03 **** 2.50E+OO 4 91. 42 12 3 0.79 456.60 454 14 3.41E-03 54.7 7.19E-08 4 92.50 19 2 0.86 462.00 454 14 5.23E-03 67.5 4.30E-08 o. 147.24 9 11 1. 41 736.13 723 15 2.45E-03 **** 3.74E-20 0 153.65 13 0 0.33 768.23 763 10 3.61E-03 55.5 1.28E-21 0 185.93 20 0 1.14 929.93 920 18 5.49E-03 58.5 4.33E-29 Flags: "T" = Tentatively associated Page 2839 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:35.14 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235037.CNF;l *
  • Acquisition date 28-SEP-2016 11:18:01 Sensitivity 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
  • Sample date 30-NOV-2015 11:19:00 Nuclide Library : IODINE *
  • Sample ID I405235037 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.8400E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : Il29 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129'.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2840 of 5809 Le (pCi/GRAM 4.616E+OO NOT IDENT. l.793E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:18:36.22 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235037.CNF;l * *Acquisition date 28-SEP-2016 11:18:01 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.20 Half life ratio : ***** *
  • Sample date 30-NOV-2015 11:19:00 Nuclide Library : IODINE *
  • Sample ID I405235037 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.8400E+OO GRAM *
  • Quantity Err(%) 3.5211E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 , * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 -4.085E-01 5.704E+00 I-129 -l.442E-02 2.213E-01 Page 2841 of 5809 TPU ( 1 . 96-sigma ) TPU ( 1. 96-sigma) 5.707E+OO 2.214E-01 NOT IDENT. NOT IDENT.
                                                                                                                                                              • * * *
  • GEL Laboratories LLC 2040 Savage Road Charleston, SC 29407 GAMMA SPECTROSCOPY BACKGROUND REPORT * * * * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2842 of 5809 MDA COUNTS 5.2595 7.4924 5.4044 5.5038 5.5733 4.5736 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:14.89 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235038.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : Z5-SEP-2016 12:23:10 Sample date 30-NOV-2015 10:40:00 Acquisition date : 28-SEP-2016 11:18:47 Sample ID I405235038 Sample quantity 2.82000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.18 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 4 15.84* 8 8 0.55 78.64 75 17 2. llE-03 83.5 2.83E+OO 2 4 16.51* 1 7 0.38 82.00 75 17 1.55E-04***** 3 4 17.89 8 5 0.57 88.91 75 17 2.20E-03 51. 7 4 0 31. 71 7 2 0.36 158.14 155 6 1.82E-03 56.0 5 0 92.53* 8 0 0.78 462.94 458 9 2.25E-03 55.6 6 0 132.35 8 3 1. 50 662.49 656 10 2. 31E-03 49.9 Flag: "*" = Peak area was modified by background subtraction Page 2843 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:15.71 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235038.CNF;l * *Acquisition date 28-SEP-2016 11:18:47 Sensitivity 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Analyst initials: MJHl *
  • Sample ID I405235038 Sample Quantity 2.8200E+00 GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Nuclide I-125 I-129 Page 2844 of 5809 Key-Line Activity (pCi/GRAM 7.595E-01 5.630E-02 K.L. Cnt Uncert ( 1. 96-sigma) 2.363E+OO l.910E-01 MDA (pCi/GRAM MDA (pCi/GRAM 6.306E+00 4.337E-01 FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:13.98 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 4 15.84 15 8 0.55 78.64 75 17 4.lOE-03 39.6 2.83E+00 2 4 16.51 8 7. 0.38 82.00 75 17 2.15E-03 75.6 3 4 17.89 8 5 0.57 88.91 75 17 2.20E-03 51. 7 4 0 31.71 7 2 0.36 158.14 155 6 l.82E-03 56. 0 5 0 92.53 16 0 0.78 462.94 458 9 4.44E-03 25.0 6 0 132.35 8 3 1. 50 662.49 656 10 2. 31E-03 49.9 Page 2845 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:15.25 Nuclide Line Activity Report Flag: "*" = Keyline Page 2846 of 5809 Summary of Nuclide Activity Sample ID : 1405235038 Acquisition date Page : 2 28-SEP-2016 11:18:47 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 284 7 of 5809 Keyline not found Manually edited "M" "A" 6 5 NID 1 criteria **** 16.67% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : I405235038 Acquisition date : 28-SEP-2016 11:18:47 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 15.84 8 8 0.55 78.64 75 17 2. llE-03 **** 1.12E+OO 4 16.51 1 7 0.38 82.00 75 17 1.55E-04 **** 1.48E+OO 4 17.89 8 5 0.57 88.91 75 17 2.20E-03 **** 2.41E+OO 0 31.71 .7 2 0.36 158.14 155 6 l.82E-03 *.*** 1. 55E+Ol T 0 92.53 8 0 0.78 462.94 458 9 2.25E-03 **** 5.17E-01 0 132.35 8 3 1. 50 662.49 656 10 2.31E-03 99.9 l.40E-02 Flags: "T" = Tentatively associated Page 2848 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:17.28 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235038.CNF;l *
  • Acquisition date 28-SEP-2016 11:18:47 Sensitivity : 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Nuclide Library : IODINE *
  • Sample ID I405235038 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.8200E+00 GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2849 of 5809 Le (pCi/GRAM 2.273E+00 FAIL ABUN 1.722E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:18.35 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235038.CNF;l *
  • Acquisition date 28-SEP-2016 11:18:47 Sensitivity 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Nuclide Library : IODINE *
  • Sample ID I405235038 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.8200E+OO GRAM *
  • Quantity Err(%) 3.5461E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Nuclide I-125 I-129 Page 2850 of 5809 Key-Line Activity (pCi/GRAM 7.595E-01 5.630E-02 K.L Act error ( 1. 96-sigma) 2.367E+OO 1. 911E-01 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 2.391E+00 FAIL ABUN 1.928E-01 NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2851 of 5809 MDA COUNTS 1.0858 3.3266 1.4961 2.2941 4.6579 4.8019 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:44.16 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235039.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 30-NOV-2015 10:43:00 Acquisition date : 28-SEP-2016 11:19:10 Sample ID I405235039 Sample quantity 3.17000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.05 0.0% Energy tolerance 1.00000 keV Analyst Initials : MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE *PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.90* 2 4 0.26 233.18 228 7 4.22E-04268.3 2 0 63.52* 9 3 0.60 315.92 312 9 2.46E-03 57.1 3 0 92.75* 3 2 1. 01 461.54 456 10 8.74E-04176.9 Flag: "*" = Peak area was modified by background subtraction Page 2852 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:44.99 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235039.CNF;l * *Acquisition date 28-SEP-2016 11:19:10 Sensitivity : 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.05 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:43:00 Analyst initials: MJHl *
  • Sample ID I405235039 Sample Quantity 3.1700E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.840E-01 3.302E+OO I-129 l.378E-02 1. 729E-01 Page 2853 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 8.592E+OO 4.404E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:43.46 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.90 6 4 0. 26 233.18 228 7 1.53E-03 70.7 2 0 63.52 15 3 0.60 315.92 312 .9 4.30E-03 31. 0 3 0 92.75 18 2 1. 01 461.54 456 10 4.92E-03 28.9 Page 2854 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:44.52 Nuclide Line Activity Report Flag: "*" = Keyline Page 2855 of 5809 Summary of Nuclide Activity Sample ID : 1405235039 Acquisition date Page : 2 28-SEP-2016 11:19:10 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2856 of 5809 Keyline not found Manually edited . "M" "A" 3 3 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Page : 3 Sample ID : 1405235039 Acquisition date : 28-SEP-2016 11:19:10 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 46.90 2 4 0.26 233.18 228 7 4.22E-04 **** 7.78E+OO 0 63.52 9 3 0.60 315.92 312 9 2.46E-03 **** 3.16E+OO 0 92.75 3 2 1. 01 4 61. 54 456 10 8.74E-04 **** 3.55E-01 Flags: "T" = Tentatively associated Page 2857 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:46.90 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235039.CNF;l * *Acquisition date 28-SEP-2016 11:19:10 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.05 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:43:00 Nuclide Library : IODINE *
  • Sample ID I405235039 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 3.1700E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2858 of 5809 Le (pCi/GRAM 3.054E+OO NOT IDENT. 1.560E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:19:47.99 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235039.CNF;l * *Acquisition date 28-SEP-2016 11:19:10 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.05 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:43:00 Nuclide Library : IODINE *
  • Sample ID I405235039 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 3.1700E+00 GRAM *
  • Quantity Err ( % ) 3. 154 6E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129' *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 I129.CNF;5 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1.96-sigma) I-125 3.840E-01 3.303E+OO I-129 1 .. 378E-02 1.729E-01 Page 2859 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 3.307E+OO 1. 731E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2860 of 5809 MDA COUNTS 1.6265 1. 7094 0.0000 1.8461 3.8174 1.0189 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:21.94 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235040.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY6.CNF;215 Background date : 75-SEP-2016 12:23:20 Sample date 30-NOV-2015 13:23:00 Acquisition date : 28-SEP-2016 11:19:53 Sample ID I405235040 Sample quantity 3.54000E+OO GRAM Detector name : XRAY6 Detector geometry: Il29 Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.07 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 Energy 63.27* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err 3 2 0.54 315.77 312 7 8.07E-04131.4 Flag: "*" = Peak area was modified by background subtraction Page 2861 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:22.76 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235040.CNF;l * *Acquisition date 28-SEP-2016 11:19:53 Sensitivity : 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:23:00 Analyst initials: MJHl *
  • Sample ID I405235040 Sample Quantity 3.5400E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1 . 96-sigma ) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.535E-01 l.477E+OO I-129 -7.671E-02 1. 793E-01 Page 2862 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM 5.546E+OO 2.928E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:21.14 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 63.27 8 2 0.54 315.77 312 7 2.31E-03 43.5 2 0 92.65 6 3 0.19 462.75 458 7 .1. 70E-03 63.6 Page 2863 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:22.32 Nuclide Line Activity Report Flag: "*" = Keyline Page 2864 of 5809 Summary of Nuclide Activity Sample ID : 1405235040 Acquisition date Page : 2 28-SEP-2016 11:19:53 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2865 of 5809 Keyline not found Manually edited "M" "A" 1 1 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 1405235040 Page : 3 Acquisition date : 28-SEP-2016 11:19:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 63.27 3 2 0.54 315.77 312 7 8.07E-04 **** 3.09E+OO Flags: "T" = Tentatively associated Page 2866 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:24.89 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235040.CNF;l *
  • Acquisition date 28-SEP-2016 11:19:53 Sensitivity : 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:23:00 Nuclide Library : IODINE *
  • Sample ID I405235040 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 3.5400E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : Il29 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2867 of 5809 Le (pCi/GRAM 1.753E+00 NOT IDENT. 9.254E-02 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 12:20:26.03 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I405235040.CNF;l *
  • Acquisition date 28-SEP-2016 11:19:53 Sensitivity : 3.000 *
  • Detector ID XRAY6 Energy tolerance: 1.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.07 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:23:00 Nuclide Library : IODINE *
  • Sample ID I405235040 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 3.5400E+OO GRAM *
  • Quantity Err(%) 2.8249E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 10:07:09 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY6 I129.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificaie of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 7.535E-01 1.478E+OO I-129 -7. 671E-02 l.795E-01 Page 2868 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 1. 517E+OO 1.828E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29. 62 35.49 39.58 Page 2869 of 5809 MDA COUNTS 0.0000 2.9286 1. 4921 0.0000 1.5811 3.3136 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:24.89 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627437.CNF;l DKA100: [CANBERRA. GAMMA.ARCHIVE. GAMMA] BKG XRAYl. CNF; 415 Background date : 75-SEP-2016 12:22:54 Sample date 26-SEP-2016 00:00:00 Acquisition date : 28-SEP-2016 12:50:58 Sample ID I1203627437 Sample quantity 3.54000E+OO GRAM Detector name : XRAYl Detector geometry: I129 Elapsed live time: 0 00:40:07.21 Elapsed real time: 0 00:40:07.36 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT No peaks were found Page 2870 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:25.77 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627437.CNF;l *
  • Acquisition date 28-SEP-2016 12:50:58 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:40:07.21 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:40:07.36 Half life ratio : ***** *
  • Sample date 26-SEP-2016 00:00:00 Analyst initials: MJHl *
  • Sample ID I1203627437 Sample Quantity 3.5400E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 2.094E-02 l.050E-01 I-129 4.719E-02 1. 896E-01 Page 2871of5809 MDA (pCi/GRAM MDA (pCi/GRAM 2.142E-01 4.177E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:24.23 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION No peaks were found Page 2872 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:25.31 Nuclide Line Activity Report Flag: "*" = Keyline Page 2873 of 5809 Summary of Nuclide Activity Sample ID : 11203627437 Acquisition date Page : 2 28-SEP-2016 12:50:58 **** There are no nuclides meeting summary criteria **** Flags: "K" "E" Page 2874 of 5809 Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : 11203627437 None Flags: "T" Tentatively associated Page 2875 of 5809 Acquisition date Page : 3 28-SEP-2016 12:50:58 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:27.29 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627437.CNF;l *
  • Acquisition date 28-SEP-2016 12:50:58 Sensitivity 3.000, *
  • Detector ID XRAYl Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:40:07.21 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:40:07.36 Half life ratio : ***** *
  • Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
  • Sample ID I1203627437 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 3.5400E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 * * . Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2876 of 5809 Le (pCi/GRAM 8.853E-02 NOT IDENT. 1.744E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:28.31 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627437.CNF;l *
  • Acquisition date 28-SEP-2016 12:50:58 Sensitivity : 3.000 *
  • Detector ID XRAYl Energy tolerance: 1.000 * *Elapsed live time: 0 00:40:07.21 Abundance limit : 75.000 * *Elapsed real time: 0 00:40:07.36 Half life ratio : ***** *
  • Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
  • Sample ID I1203627437 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 3.5400E+OO GRAM *
  • Quantity Err(%) 2.8249E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 9-JUN-2016 11:39:23 Eff: Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAYl Il29.CNF;6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM (1. 96-sigma) I-125 2.094E-02 1. 051E-01 I-129 4.719E-02 1. 897E-01 Page 2877 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) l.055E-01 1.909E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2878 of 5809 MDA COUNTS 6.1327 6.7854 4.3281 1. 7 970 1.8430 10.6588 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:00.80 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627438.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY2.CNF;379 Background date : 75-SEP-2016 12:22:59 Sample date 8-DEC-2015 14:17:00. Acquisition date : 28-SEP-2016 12:51:32 Sample ID Il203627438 Sample quantity 3.35000E+OO GRAM Detector name : XRAY2 Detector geometry: Il29 Elapsed live time: 0 00:39:28.38 Elapsed real time: 0 00:39:28.53 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** Pk It 1 0 2 0 Energy 92.71* 96. 42 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 10 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.94 463.05 3 0.37 481.65 457 11 4.25E-03 48.5 474 12 3.40E-03 55.6 Flag: "*" = Peak area was modified by background subtraction Page 2879 of 5809 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:01.59 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627438.CNF;l *
  • Acquisition date 28-SEP-2016 12:51:32 Sensitivity 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:39:28.38 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:39:28.53 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Analyst initials: MJHl *
  • Sample ID I1203627438 Sample Quantity 3.3500E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : 1129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Non-Identified Nuclides ----Nuclide Key-Line Activity (pCi/GRAM K.L. Cnt uncert ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert Nuclide (pCi/GRAM (1. 96-sigma) I-125 3.393E+OO 7.155E+OO I-129 2.433E-01 2.666E-01 Page 2880 of 5809 MDA (pCi/GRAM MDA (pCi/GRAM l.631E+Ol 6.452E-01 NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:00.10 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It 1 0 2 0 Page 2881of5809 Energy 92.71 96. 42 Area 21 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 0 0.94 463.05 3 0 . 3 7. 4 81. 6 5 457 11 8.87E-03 21.8 474 12 3.40E-03 55.6 Fit VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:01.13 Nuclide Line Activity Report Flag: "*" = Keyline Page 2882 of 5809 Summary of Nuclide Activity Sample ID : 11203627438 Acquisition date Page : 2 28-SEP-2016 12:51:32 Total number of lines in spectrum Number of unidentified lines Number of lines tentatively identified by **** There are no nuclides meeting summary Flags: "K" "E" Page 2883 of 5809 Keyline not found Manually edited "M" "A" 2 2 NID 0 criteria **** 0.00% Manually accepted Nuclide specific abn. limit Unidentified Energy Lines Sample ID : Il203627438 Page : 3 Acquisition date : 28-SEP-2016 12:51:32 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 0 92.71 96. 42 10 8 0 0.94 3 0.37 Flags: "T" = Tentatively associated Page 2884 of 5809 463.05 457 11 4.25E-03 97.0 3.89E-08 481.65 474 12 3.40E-03 **** 6.49E-09 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:03.06 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627438.CNF;l *
  • Acquisition date 28-SEP-2016 12:51:32 Sensitivity : 3.000 *
  • Detector ID XRAY2 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:39:28.38 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:39:28.53 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
  • Sample ID I1203627438 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 3.3500E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 Il29.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide Le (pCi/GRAM ----Non-Identified Nuclides Nuclide I-125 I-129 Page 2885 of 5809 Le (pCi/GRAM 6.719E+OO NOT IDENT. 2.719E-01 NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:32:04.39 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627438.CNF;l * *Acquisition date 28-SEP-2016 12:51:32 Sensitivity 3.000 *
  • Detector ID XRAY2 . Energy tolerance: 1. 000 *
  • Elapsed live time: 0 00:39:28.38 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:39:28.53 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
  • Sample ID I1203627438 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 3.3500E+OO GRAM *
  • Quantity Err(%) 2.9851E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 27-JUL-2016 12:15:07 Eff. Geometry : 1129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY2 I129.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM Act Error ( 1. 96-sigma) Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1. 96-sigma) I-125 3.393E+OO 7.180E+OO I-129 2. 4)3E-01 2.677E-01 Page 2886 of 5809 TPU ( 1. 96-sigma) TPU ( 1. 96-sigma) 7. 341E+OO 2.893E-01 NOT IDENT. NOT IDENT.
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 27.34 29.62 35.49 39.58 Page 2887 of 5809 MDA COUNTS 4.2076 3.2110 5.4044 7.7053 7.8027 4.5736 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:36.22 ********************************************************************************
  • GEL.Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627439.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY4.CNF;433 Background date : 25-SEP-2016 12:23:10 Sample date 8-DEC-2015 14:17:00. Acquisition date : 28-SEP-2016 12:52:05 Sample ID I1203627439 Sample quantity 2.94000E+OO GRAM Detector name : XRAY4 Detector geometry: I129 Elapsed live time: 0 00:38:50.89 Elapsed real time: 0 00:38:51.04 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT . Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 4 27.00 10 22 0.63 134.54 127 32 4.35E-03 77.9 1. 74E+OO 2 4 27.78 19 18 0.53 138.46 127 32 7.98E-03 45.3 3 4 28.69 11 14 0.44 143.00 127 32 4.92E-03 81.1 4 4 29.70 247 13 0.65 148.09 127 32 1. 06E-01 7 .1 5 0 33.60 23 27 0.36 167.62 164 8 l.OOE-02 43.2 6 0 39.65 29 9 0.75 197.94 193 9 1.25E-02 26.2 Flag: "*" = Peak area was modified by background subtraction Page 2888 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:37.06 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627439.CNF;l *
  • Acquisition date 28-SEP-2016 12:52:05 Sensitivity : 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:50.89 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:51.04 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Analyst initials: MJHl *
  • Sample ID I1203627439 Sample Quantity 2.9400E+00 GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File. : DKAlOO: [CANBERRA.GAMMA]EFF XRAY4 Il29.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Activity (pCi/GRAM 9.138E+OO 1.203E+Ol Cnt uncert ( 1. 96-sigma) 1.395E+Ol 1.679E+OO Non-Identified Nuclides Nuclide Page 2889 of 5809 Key-Line Activity (pCi/GRAM K.L. Cnt Uncert ( 1. 96-sigma) MDA (pCi/GRAM l.362E+Ol 7.659E-01 MDA (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:35.49 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 4 27.00 10 22 0.63 134.54 127 32 4.35E-03 77.9 1. 74E+OO 2 4 27.78 19 18 0.53 138.46 127 32 7.98E-03 45.3 3 4 28.69 11 14 0.44 143.00 127 32 4.92E-03 81.1 4 4 29.70 247 13 0.65 148.09 127 32 1.06E-01 7.1 5 0 33.60 23 27 0.36 167. 62 164 8 l.OOE-02 43.2 6 0 39.65 29 9 0.75 197.94 193 9 1. 25E-02 26.2 Page 2890 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:36.58 Nuclide Line Activity Report .Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-125 27.34 10 114 .10* 1.198E+Ol 2.925E-01 9 .138E+OO 155.83 30.97 ------20.30 1.514E+Ol ------Line Not Found ------35.49 ------6.68 1.660E+Ol ------Line Not Found ------Nuclide Type: FISSION Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-129 29.62 247 56.60* 1.431E+Ol 1.203E+Ol 1.203E+Ol 14.24 33.59 23 10.04 1.626E+Ol 5.644E+OO 5.644E+00 86.43 39.58 29 7.51 1.617E+Ol 9.467E+OO 9.467E+OO 52.35 Flag: "*" Key line Page 2891 of 5809 Summary of Nuclide Activity Sample ID : I1203627439 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 12:52:05 Number of lines tentatively identified by NID 6 2 4 66.67% Nuclide Type : Nuclide I-125 Hlife 59.40D Decay 31. 2 Total Activity Nuclide Type : FISSION Nuclide Hlife I-129 1.57E+07Y Decay 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 2.925E-01 ---------2.925E-01 Uncorrected pCi/GRAM l.203E+Ol ---------1.203E+Ol 1. 232E+Ol Flags: "K" "E" Keyline not found Manually edited Page 2892 of 5809 Decay Corr Decay Corr 2-Sigma pCi/GRAM 2-Sigma Error %Error 9.138E+OO 14.24E+OO 155.83 ---------9 .138E+OO Decay Corr Decay Corr 2-Sigma pCi/GRAM 2-Sigma Error %Error 1.203E+Ol 0.171E+Ol 14.24 ---------1.203E+Ol 2. ll 7E+Ol Manually accepted' "M" "A" Nuclide specific abn. limit Flags Flags Unidentified Energy Lines Page : 3 Sample ID : 11203627439 Acquisition date : 28-SEP-2016 12:52:05 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 27.78 19 18 0.53 138.46 127 32 7.98E-03 90.6 l.27E+Ol 4 28.69 11 14 0.44 143.00 127 32 4.92E-03 **** l.35E+Ol Flags: "T" = Tentatively associated Page 2893 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:38.97 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627439.CNF;l *
  • Acquisition date 28-SEP-2016 12:52:05 Sensitivity 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:50.89 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:51.04 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
  • Sample ID I1203627439 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 2.9400E+OO GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Le (pCi/GRAM 5.626E+OO 3.169E-01 ----Non-Identified Nuclides Nuclide Page 2894 of 5809 Le (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:40.16 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627439.CNF;l *
  • Acquisition date 28-SEP-2016 12:52:05 Sensitivity : 3.000 *
  • Detector ID XRAY4 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:50.89 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:51.04 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Nuclide Library : IODINE *
  • Sample ID I1203627439 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 2.9400E+00 GRAM *
  • Quantity Err(%) 3.4014E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 08:18:14 Eff. Geometry : I129 *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF XRAY4 I129.CNF;14
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 I-129 9.138E+OO 1.203E+Ol Act Error (1.96-sigma) 1.407E+Ol 2.057E+OO Non-Identified Nuclides Nuclide Page 2895 of 5809 Key-Line Activity (pCi/GRAM K.L Act error ( 1. 96-sigma) TPU ( 1. 96-sigma) 1.407E+01 2.057E+OO TPU ( 1. 96-sigma)
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 30.97 33.59 35.49 39.58 Page 2896 of 5809 MDA COUNTS 7.6004 7.7622 7.8547 17.2054 12.8092 7.2029 ENERGY MDA COUNTS ENERGY MDA COUNTS VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:10.80 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627440.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG XRAY5.CNF;58 Background date : 25-SEP-2016 12:23:15 Sample date 26-SEP-2016 00:00:00 Acquisition date : 28-SEP-2016 12:52:43 Sample ID I1203627440 Sample quantity 3.54000E+OO GRAM Detector name : XRAY5 Detector geometry: I129 Elapsed live time: 0 00:38:05.93 Elapsed real time: 0 00:38:05.98 0.0% Energy tolerance 1.00000 keV Analyst Initials MJHl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1598620 Detector SN# Matrix Spike ID : 1470-K LCS ID : 1470-K ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 6 27.21 14 0 0.57 135.07 129 25 6.34E-03 35.9 2.22E+OO 2 6 29.70 198 0 0.61 147.48 129 25 8.66E-02 7.4 3 0 32.46 8 3 0.55 161. 23 157 7 3.34E-03 54.2 4 0 33.67 27 16 0.53 167.29 164 8 1.18E-02 31. 3 5 0 39.64 38 5 0.58 196.99 192 10 1.68E-02 19.4 6 0 76.98* 4 0 0.58 383.00 380 6 l.87E-03 59.8 Flag: "*" = Peak area was modified by background subtraction Page 2897 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:11.78 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627440.CNF;l *
  • Acquisition date 28-SEP-2016 12:52:43 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:05.93 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:05.98 Half life ratio : ***** *
  • Sample date 26-SEP-2016 00:00:00 Analyst initials: MJHl *
  • Sample ID Il203627440 Sample Quantity 3.5400E+OO GRAM *
  • Batch Number 1598620 Carrier Weight 0.00000 *
  • Recovery 1.00000 Standard Weight 0.00000 *
  • Nuclide Library : IODINE.NLB;l * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File . : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Activity (pCi/GRAM 5.681E-01 1.320E+Ol Cnt uncert ( 1. 96-sigma) 3.992E-01 1.907E+OO Non-Identified Nuclides Nuclide Page 2898 of 5809 Key-Line Activity (pCi/GRAM K.L. Cnt Uncert ( 1 . 96-sigma) MDA (pCi/GRAM 2.681E-01 4.688E-01 MDA (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:09.99 PEAK REPORT WITHOUT BACKGROUND SUBTRACTION Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 6 27.21 14 0 0.57 135.07 129 25 6.34E-03 35.9 2.22E+OO 2. 6 29.70 198 0 0.61 147.48 129 25 8. 66E.,-02 7.4 3 0 32.46 8 3 0.55 161. 23 157 7 3.34E-03 54.2 4 0 33.67 27 16 0.53 167.29 164 8 1.18E-02 31. 3 5 0 39.64 38 5 0.58 196. 99 192 10 1. 68E-02 19.4 6 0 76.98 6 0 0.58 383.00 380 6 2.62E-03 40.8 Page 2899 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:11.25 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-125 27.34 14 114 .10* 7.693E+OO 5.514E-01 5. 681E-01 71. 71 30.97 ------20.30 9.289E+OO ------Line Not Found ------35.49 ------6.68 9.988E+OO ------Line Not Found ------Nuclide Type: FISSION Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error I-129 29.62 198 56.60* 8. 851E+OO 1. 320E+Ol 1.320E+Ol 14.75 33.59 27 10.04 9.860E+OO 9.070E+OO 9.070E+OO 62.69 39.58 38 7.51 9.649E+OO 1. 769E+Ol 1.769E+Ol 38.83 Flag: "*" Key line Page 2900 of 5809 Summary of Nuclide Activity Sample ID : Il203627440 Total number of lines in spectrum Number of unidentified lines Acquisition date Page : 2 28-SEP-2016 12:52:43 Number of lines tentatively identified by NID 6 2 4 66. 67% Nuclide Type : Nuclide I-125 Hlife 59.40D Decay 1. 03 Total Activity Nuclide Type : FISSION Nuclide Hlife I-129 l.57E+07Y Decay 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 5.514E-01 ---------5.514E-01 Uncorrected pCi/GRAM 1.320E+Ol ---------1.320E+Ol 1. 37 5E+Ol Flags: "K" "E" Keyline not found Manually edited Page 2901 of 5809 Decay Corr Decay Corr 2-Sigma pCi/GRAM 2-Sigma Error %Error 5.681E-01 4.073E-01 71. 71 ---------5.681E-01 Decay Corr Decay Corr 2-Sigma pCi/GRAM 2-Sigma Error %Error 1.320E+Ol 0.195E+Ol 14.75 ---------1.320E+Ol 1.376E+Ol Manually accepted "M" "A" Nuclide specific abn. limit Flags Flags Unidentified Energy Lines Page : 3 Sample ID : 11203627440 Acquisition date : 28-SEP-2016 12:52:43 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 32.46 8 3 0.55 161. 23 157 7 3.34E-03 **** 9.66E+OO 0 76.98 4 0 0.58 383.00 380 6 1. 87E-03 **** 1.22E+OO Flags: "T" = Tentatively associated Page 2902 of 5809 VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:14.03 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Il203627440.CNF;l *
  • Acquisition date 28-SEP-2016 12:52:43 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:05.93 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:05.98 Half life ratio : ***** *
  • Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
  • Sample ID I1203627440 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity : 3.5400E+00 GRAM *
  • Recovery 1.00000 Carrier Weight : 0.00000 *
  • Standard Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide I-125 I-129 Le (pCi/GRAM 8.148E-02 l.438E-01 ----Non-Identified Nuclides Nuclide Page2903of5809 Le (pCi/GRAM VAX/VMS Nuclide Identification Report Generated 28-SEP-2016 13:31:15.78 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA *
  • *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]I1203627440.CNF;l *
  • Acquisition date 28-SEP-2016 12:52:43 Sensitivity 3.000 *
  • Detector ID XRAY5 Energy tolerance: 1.000 *
  • Elapsed live time: 0 00:38:05.93 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:38:05.98 Half life ratio : ***** *
  • Sample date 26-SEP-2016 00:00:00 Nuclide Library : IODINE *
  • Sample ID I1203627440 Analyst initials: MJHl *
  • Batch Number 1598620 Sample Quantity 3.5400E+OO GRAM *
  • Quantity Err(%) 2.8249E-03 % *
  • Recovery 1.00000 Carrier Weight 0.00000 *
  • Standard Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 30-AUG-2016 11:41:11 Eff. Geometry : I129 *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF XRAY5 Il29.CNF;5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM I-125 I-129 5.681E-01 1.320E+Ol Act Error ( 1. 96-sigma) 4.125E-01 2. 311E+OO Non-Identified Nuclides Nuclide Page 2904 of 5809 Key-Line Activity (pCi/GRAM K.L Act error ( 1. 96-sigma) TPU ( 1 . 96-sigma) 4.125E-01 2. 311E+OO TPU (1. 96-sigma)
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY 27.34 29.62 30.97 33.59 35.49 39.58 Page 2905 of 5809 MDA COUNTS 0.8133 0.8547 0.0000 7.3846 6.6804 1.0189 ENERGY t-'[DA COUNTS ENERGY MDA COUNTS Effective 3/25/2010 Radiochemistry Batch Checklist Revision 1 Effective March 2010 10/03/16 1596247 Batch#. _________ _ Gamma Solid MJWC Product: _______ _ Criteria: Yes Sample Solids are less than or equal to 100 m11 for GAB. Samples have been blank corrected (tf required). Blank correction renorted included fif renulred\. If activity less than 10x MDA/MDC, error Is less Date: 10/03/16 No Comments n/a n/a than or equal to 150% of sample activity. ./ If greater than 10* MDA/ MDC, error Is 40% or less. I( !2!.l!QW 1!!!.l MQAl !lrr2r 21!i!l11 Instrument source check Is within limits. Instrument bkn check h: within limits. ./ Method RDL/ LLD has been met. ./ If duplicate activities are: Less than S* MDA/ MDC, then RPO Is 100% or less, see narrative If greater S* MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO Is 0%, ./ Or meets the client's reauired RER acceotance criteria. Tracer yield is 15-125%
  • Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). ,., /;i Method blank is less than the RDL/ LLD. ./ (I! rail !iillDRl!llio S :2°lQ !!f ;:u;tll!itv\ Samole was run within hold time. ./ DER 1563869 Samole was correctlv oreserved if reauired. ./ Smears Taken for Radioactive batches. n/a Method Spike ;ind LCS are within 75-1250/o ./ lror meets the client's contract acceotance criteria\, No blank sp;ices on data forms. ./ All line outs initialed and dated. N2.J.ranscrjotfon errors an:: aooarcnt Aux data is correct. ./ Client Special reouirements oaae has been checked. ./ Raw Data and/ or spectrum are included and orooerlv statused. ../ MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and ./ v .. rifl"d ILH* .. {If mm1**--v\ / llitkh...ellten:d.JntQ..C.---./ Batch Data Exception (DER) comnleted If annllcable. /' DER 1563869 Batch Data Exception Reports (DER) second reviewed. ./ Dlsnos!tlon verified to be com11leted. Cgrre!;!!Qn completed If reoulred n/a Review sample historical results If available ./ (If REMP, results above MDC have been verified bv historical results recount or re-analvsls.) Primary Review Performed By:. ____ 3_.;_.( l_h ___ _ Page 2906 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 03-0CT-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1596247 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE HASL 300, 4.5.2.3/Ga-01-R Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received of holding Specification and Requirements DER Disposition: Exception

Description:

DER Report No.: 1563869 Revision No.: 1 Type: Process Client Code: MJWC Samples 405235 001, 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, Samples were analyzed in a timely manner upon receipt. Reporting 012, 013, 014, 015, 016, 017, 018, 019, 020, and 1203621351 (duplicate) results. were received outside of the holding period. Originator's Name: Data Validator/Group Leader: Spencer Collins 03-0CT-16 Michael Hilton 03-0CT-16 Page 1 Page 2907 of 5809 Gamma Spec Queue Sheet I j -6. -Io/ b r I(., 09/16/2016 Batch #:1596247 Analyst: MXRl First Client DueDate:l0/04/2016 Internal Due Date: 09/30/2016 Gamma LCS Isotope: Mixed Gamma LCS Code: IS" S1o Expiration Date: 411 l '3, 1 Vol: \,0 ........ L-__ Prep Date: CJ) 12-/ l(O Library: h Balance ID:_N___...\ ___ _ Hazard 1:fa Sealing Dateffime Sample JD Client Description I 405235001-1 4.1.B.R.l.2 405235002-1 4.1.B.R.l.3 405235003-1 4.1.B.R.1.4 405235004-1 4.1.B.R.7.2 405235005-1 4.1.C.R.l.3 405235006-1 4.1.C.R.l.4 405235007-1 4.1.C. R.2.3 405235008-1 4.1.C.R.2.4 405235009-1 4.1.D.R.l.3 405235010-1 4.1.D.R.l.4 405235011-l 4.1.D.R.3.2 405235012-t 4.1.D.R.2.4 405235013-1 4.2A.R.2.3 405235014-1 4.2A.R.l.3 405235015-1 4.2A.R.1.4 405235016-1 4.2A.R.2.4 405235017-1 4.2A.R.3.2 405235018-1 4.2A.R.4.2 405235019-1 4.2B.R.2.4 405235020-1 4.28.R.l.4 1203621350-1 MB 1203621351-1 DUP 4.l.B.R.1.2(405235001) 1203621352-1 LCS er ID GEL Laboratories LLC, Radiochemistry Division Type Code SA.MP LE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP LCS Client Matru MJWCOOl SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOI SOIL i\IJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOl SOIL MJWCOOI SOIL MJWCOOI SOIL MJWCOOI SOIL QC ACCOUNT SOIL QC ACCOUNT SOIL QC ACCOUNT SOIL Collect Date Geometry ( I ) Detector (if Applicable) 10-DEC-15 14:20:00 tl\(J... CAN I 141.921 g I z. li'I 1rz.,.l1c,, l 10-DEC-15 14:30;00\Z.f 123.837 g I .3C' ! 10-DEC-15 14:35:00 \W 140.486 g ! '8" . 09-DEC-15 14:00:00 fl f 148.94 g I 't I I 10-DEC-15 157.331 g i l9 IO-DEC-15 13:25:00 \ ,. 156.342 g I Zal 10-DEC-15 13:55:00 l'Zf I 152.523 g i '3L.I 147.889 g f IO-DEC-1510:30:0t\-'IA2:: 134.381 g I "2..S 10-DEC-1510:35:00rl..f I 141.695 g I u; 09-DEC-15 10:13:00 tlf 146.502 g I "$)! 10-DEC-15 11:25:00<l1t j 154.64 g I 36'1 08-DECA; 11,23,oor 144.574 g l L\l j 08-DEC-15 10:49:00 , . 153.732 g I 08-DEC-15 10:56:00 7 145.075 g I 4Lli 08-DEC-15 11:29:00 fl¥' 163.118 g I n ' 02-DEC-15 10:02:00Qf 148.561 g I le I 02-DEC-15 10:19:00 155.815 g I 1.71 14,30,00 175.975 g l \\ 110.163 g I l ' 11b'.'17('1 '3\ 1* 10-DEC-15 14:20:oolt c; i u Jn-I ' *-I . ----..... Data Reviewed By: to-"3*/b Page 1 of 1 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:57:39.80 ********************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM02.CNF;493 Background date : Sample date 10-DEC-2015 14:20:00 Acquisition date : Z-OCT-2016 11:00:01. 3-0CT-2016 07:56:53. 1. 41921E+02 GRAM CAN Sample ID G405235001 Sample quantity Detector name : GAM02 Detector geometry: Elapsed live time: 0 01:00:00.00 Elapsed real time: Energy tolerance 1.50000 keV Analyst Initials 0 01:00:00.40 0.0% MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 0 0 0 0 0 6 6 0 0 0 0 0 0 0 1 1 0 0 4 4 0 0 0 0 0 0 0 0 1 1 0 Energy 62.77* 74.90* 77.10 92.82* 112.23* 143.48* 186.02* 208.83 238.54* 241.94 270.65 295.25 338.34* 351. 68* 382.01 464.18 510.86* 546.32 548.66 583.19* 609.14* 658.58 661.37 717.42 726. 67 755.24 769.00 795.57 808.56 812.22 911. 29* 964. 76* 969.00* 1023.46 Page 2909 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 30 134 214 107 12 10 77 67 414 115 84 153 102 258 14 18 54 22 18 145 183 16 174 13 33 14 24 28 14 6 79 26 49 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 156 219 173 266 140 140 141 162 71 81 95 83 48 72 39 44 54 18 28 28 49 20 30 19 15 25 40 17 20 12 11 1 5 15 0.99 1.19 1.25 1. 47 1. 42 1. 27 1.10 2. 65 1. 26 2.10 3. 65 1.10 1. 41 1. 53 2.94 0.60 2.48 1. 84 1. 67 1. 34 1. 35 1. 94 1. 79 3.43 1. 28 1. 36 0.88 1. 37 1.21 1. 07 1. 64 2.17 2.17 4.60 125.05 149.28 153.69 185.10 223.88 286.32 371.32 416.92 476.29 483.07 540.43 589.60 675. 71 702.37 762.98 927.18 1020.46 1091.33 1096.00 1165. 01 1216.87 1315.69 1321.26 1433.28 1451. 75 1508.86 1536.36 1589.45 1615.42 1622.73 1820.74 1927.61 1936.08 2044.92 122 146 146 180 223 283 366 411 471 471 533 585 671 696 756 918 1015 1088 1088 1159 1210 1312 1312 1429 1448 1502 1527 1582 1608 1618 1815 1922 1922 2036 8 8.25E-03 79.1 16 3.72E-02 19.9 16 5.95E-02 13.0 12 2.97E-02 34.1 8 3.36E-03174.4 8 2.92E-03203.7 11 2.13E-02 34.6 13 l.86E-02 41.0 18 l.15E-01 6 .1 18 3.20E-02 19.7 14 2.34E-02 26.8 10 4.26E-02 13.7 10 2.83E-02 16.4 12 7.17E-02 9.2 9 3.79E-03 79.9 13 5.13E-03 78.4 15 1.51E-02 37.4 18 6.19E-03 35.8 18 5.09E-03 58.2 13 4. 04E-02 11. 5 15 5. 08E-02 11. 4 17 4.55E-03 56.0 17 4.82E-02 9.5 12 3.65E-03 70.7 8 9.04E-03 27.5 10 3.91E-03 71.6 12 6.74E-03 55.5 15 7. 65E-03 41. 3 11 3.75E-03 71.6 9 1. 80E-03101. 7 11 2.20E-02 14.4 21 7.22E-03 27.6 21 l.36E-02 18.2 15 3.33E-03 76.0 Fit 2.23E+OO l.54E+OO 2.69E+OO 6.25E+00 6.57E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235001 Acquisition date 3-0CT-2016 07:56:53 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1099.87 16 18 0.80 2197.65 2188 14 4.35E-03 66.3 36 0 1120.14* 42 12 1. 94 2238.17 2233 15 1.17E-02 24.3 37 0 1130 .15 18 . 6 3.23 2258.17 2252 12 5.00E-03 36.0 38 0 1154. 59 26 10 2.10 2307.01 2300 14 7.16E-03 33.1 39 2 1186.65 15 8 2.55 2371. 09 2361 26 4.09E-03 62.7 1.04E+OO 40 2 1191. 84 14 17 2.55 2381.47 2361 26 4.0lE-03 52.9 41 0 1195. 72 9 7 1. 37 2389.22 2386 7 2.50E-03 59.1 42 0 1222.52 15 8 1. 55 2442.79 2438 10 4.24E-03 42.3 43 0 1228.78 14 5 2.06 2455.30 2451 9 3.96E-03 37.8 44 0 1252.82 23 3 3.01 2503.34 2498 12 6.31E-03 26.0 45 0 1282. 31 24 4 5.42 2562.30 2555 16 6.59E-03 28.0 46 0 1325.72 13 0 2.73 2649.08 2644 12 3.61E-03 27.7 47 0 1378.42* 14 7 1.11 2754.41 2750 10 3.91E-03 47.3 48 0 1460.66* 375 8 1. 79 2918.80 2910 15 1.04E-01 5.5 49 0 1729.65* 7 2 0.69 3456.50 3450 11 l.90E-03 63.9 50 0 1764.48* 33 0 2.63 3526.12 3520 13 9.15E-03 19.8 Flag: "*" = Peak area was modified by background subtraction Page 2910 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 08:57:42 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 14:20:00 G405235001 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:56:53 141. 92 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA2 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 2911 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 AM-243 TH-228 PB-212 BI-211 Line 240.99 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.40 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235001 Acquisition date 3-0CT-2016 07:56:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66*. l.059E+OO l.685E+Ol l.685E+Ol 10.98 OK C0-58 810.76 99.45* l.711E+OO 2.038E-02 3.751E-01 203.37 OK BA-137M 661.66 89.90* 2.016E+OO 5.224E-01 5.323E-01 18.94 OK CS-137 661. 66 85.10* 2.016E+OO 5.519E-01 5.624E-01 18.94 OK TL-208 277.37 6.60 4.173E+OO Line Not Found Absent 583.19 85.00* 2.233E+OO 4.222E-01 4.222E-01 23.00 OK 860.56 12.50 l.634E+OO Line Not Found Absent PB-212 74.82 10.28 3.783E+OO 1.545E+OO 1.545E+OO 59.01 OK 77 .11 17.10 4.000E+OO 2.030E+OO 2.030E+OO 25.96 OK 238.63 43.60* 4.702E+OO l.200E+OO 1.200E+OO 12.25 OK 300.09 3.30 3.910E+OO Line Not Found Absent BI-214 609.32 45.49* 2.155E+OO l.025E+OO 1. 026E+OO 22.80 OK 1120.29 14.92 l.323E+OO l .112E+OO 1.112E+00 48.51 OK 1764.49 15.30 8.931E-01 l.201E+OO 1.202E+OO 39.68 OK PB-214 74.82 5.80 3.775E+OO Line Not Found <<INT Reject 77 .11 9.70 4.000E+OO 3.579E+OO 3.580E+OO 25.96 OK 87.09 3.41 4.837E+OO Line Not Found Absent 242.00 7.25 4. 651E+OO Line Not Found <<INT Reject 295.22 18.42 3.963E+OO l.226E+OO 1. 226E+OO 27.45 OK 351.93 35.60* 3.418E+OO 1. 221E+OO 1.221E+OO 18.38 OK RN-222 609.32 45.49* 2.155E+OO 1.025E+OO 1.026E+OO 22.80 OK 1120. 29 14.92 1.323E+OO l.112E+OO 1.112E+OO 48.51 OK 1764.49 15.30 8.931E-01 1. 201E+OO 1.202E+OO 39.68 OK RA-224 240.99 4.10* 4.652E+OO 1.414E+OO 1.414E+OO 108.39 OK RA-226 609.32 45.49* 2.155E+OO 1.025E+OO 1. 026E+OO 22.80 OK 1120. 29 14.92 1.323E+OO l .112E+OO 1.112E+OO 48.51 OK 1764.49 15.30 8.931E-01 l.201E+00 1.202E+OO 39.68 OK AC-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.533E+OO 1.479E+OO 1. 47.9E+OO 32.75 OK 794.95 4.25 1.739E+OO l.999E+00 1.999E+OO 82.62 OK 835.71 1. 61 1.672E+OO Line Not Found Absent 911.20 25.80* 1. 561E+OO 1.041E+OO l.041E+00 28.80 OK 968. 97 15.80 *1. 487E+00 l.lOOE+OO 1.lOOE+OO 36. 32 OK RA-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.533E+OO 1.479E+OO 1.479E+OO 32.75 OK 794.95 4.25 1.739E+OO 1.999E+OO l.999E+00 82.62 OK 835. 71 1. 61 1.672E+OO Line Not Found Absent 911. 20 25.80* 1.561E+OO 1. 041E+OO 1.041E+OO 28.80 OK 968.97 15.80 l.487E+OO l.lOOE+OO 1.lOOE+OO 36.32 OK TH-228 74.82 10.28 3.783E+OO l.545E+00 1.545E+OO 59.01 OK 77 .11 17.10 4.000E+OO 2.030E+OO 2.030E+OO 25.96 OK 238.63 43.60* 4.702E+OO l.200E+OO 1.200E+OO 12.25 OK 300.09 3.30 3.910E+OO Line Not Found Absent TH-230 609.32 45.49* 2.155E+OO 1.025E+OO 1.025E+OO 22.80 OK 1120.29 14.92 1.323E+OO l.112E+OO 1.112E+OO 48.51 OK 1764.49 15.30 8.931E-01 1. 201E+OO 1.201E+OO 39.68 OK TH-232 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11.27 3.533E+OO 1.479E+OO 1.479E+OO 32.75 OK 835.71 1. 61 1.672E+OO Line Not Found Absent Page 2912 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235001 Acquisition date 3-0CT-2016 07:56:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 911.20 25.80* 1.561E+OO l.041E+OO l.041E+OO 28.80 .OK 968. 97 15.80 l.487E+OO l.lOOE+OO 1.lOOE+OO 36.32 OK TH-234 63.29 3.70* 2.417E+OO 2.186E+OO 2.186E+OO 158.12 OK 92.59 4.23 5.211E+OO 3.099E+OO 3.099E+OO 68.16 OK U-234 609.32 45.49* 2.155E+OO l.025E+OO l.025E+00 22.80 OK 1120. 29 14.92 1.323E+OO l .112E+OO 1.112E+OO 48.51 OK 1764.49 15.30 8.931E-01 1.201E+OO 1.201E+OO 39.68 OK U-235 89. 96 3.47 5.033E+OO Line Not Found Absent 93.35 5.60 5.211E+OO 2.341E+OO 2.341E+OO 68.16 OK 143.76 10. 96* 6.129E+OO 9.669E-02 9.669E-02 407.43 OK 163.33 5.08 5.908E+OO Line Not Found Absent 185.72 57.20 5.553E+OO 1.464E-01 l.464E-01 69.13 OK 205.31 5.01 5.230E+OO Line Not Found Absent U-238 63.29 3.70* 2.417E+00 2.186E+00 2.186E+OO 158.12 OK 92.59 4.23 5.211E+OO 3.099E+OO 3.099E+OO 68.16 OK AM-243 43.53 5.90 2.878E-01 Line Not Found Absent 74.66 67.20* 3.783E+OO 2.363E-01 2.364E-01 59.01 OK ANH-511 511. 00 100.00* 2. 491E+OO 1. 218E-01 1.218E-01 74.84 OK Flag: "*" = Keyline Page 2913 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:57:43.46 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l * *Acquisition date 3-0CT-2016 07:56:53 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:20:00 Analyst initials: MXRl *
  • Sample ID G405235001 Sample Quantity 1.4192E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.685E+Ol 1.814E+OO 5.916E-01 C0-58 3. 751E-01 7.476E-01 l.576E-01 BA-137M 5.323E-01 9. 881E-02 8.448E-02 CS-137 5.624E-01 1.044E-01 8.924E-02 TL-208 4.222E-01 9.518E-02 7.254E-02 PB-212 1.200E+OO 1. 441E-01 1. 072E-01 BI-214 1. 026E+OO 2.292E-01 1.350E-01 PB-214 1. 221E+OO 2.199E-01 l.460E-01 RN-222 1. 026E+OO 2.292E-01 1.350E-01 RA-224 1. 414E+OO 1.502E+OO 1.149E+OO RA-22 6 1.026E+OO 2.292E-01 1.350E-01 AC-228 1.041E+OO 2.939E-01 2.560E-01 RA-228 1. 041E+OO 2.939E-01 2.560E-01 TH-228 1. 200E+OO l.441E-01 1.072E-01 TH-230 1.025E+OO 2.291E-01 1.350E-01 TH-232 1. 041E+OO 2.939E-01 2.560E-01 TH-234 2.186E+OO 3.388E+OO 2.955E+OO U-234 1.025E+OO 2.291E-01 l.350E-01 U-235 9.669E-02 3.860E-01 3.806E-01 U-238 2.186E+OO 3.388E+OO 2.955E+OO AM-243 2.364E-01 1.367E-01 l.249E-01 ANH-511 l.218E-01 8.937E-02 6.502E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM. ( 1. 96-sigma) (pCi/GRAM BE-7 -l.033E+Ol 1.586E+Ol 2.726E+Ol NOT IDENT. NA-22 1.975E-02 5.169E-02 1.055E-01 NOT IDENT. NA-24 O.OOOE+OO l.349E+41 O.OOOE+OO SHORT HLIF AL-26 -l .136E-02 2. 8'55E-02 5.642E-02 FAIL ABUN SC-46 -2.504E-01 4.309E-01 7.340E-01 FAIL ABUN V-48 O.OOOE+OO l.594E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.612E+02 O.OOOE+OO SHORT HLIF MN-54 l.886E-02 7.391E-02 l.496E-01 NOT IDENT. Page 2914 of 5809 C0-56 -3.947E-01 5.563E-01 9.794E-01 NOT IDENT. MN-56 0.000E+OO l.410E+41 O.OOOE+OO SHORT HLIF C0-57 4.240E-02 5.649E-02 l.081E-01 NOT IDENT. FE-59 l. lllE+Ol l.443E+Ol l.734E+Ol FAIL ABUN C0-60 -3.648E-02 5.042E-02 7.292E-02 NOT IDENT. ZN-65 -4. 372E-03 2.487E-01 4.150E-01 NOT IDENT. GE-68 -5.512E-01 2.709E+OO 5.102E+OO NOT IDENT. AS-73 8.307E+OO l.268E+Ol 2.537E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.478E+03 O.OOOE+OO SHORT HLIF SE-75 -l.764E-01 2.576E-01 4. 087E-0.l NOT IDENT. BR-77 O.OOOE+OO l.407E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.141E+02 0.000E+OO SHORT HLIF RB-83 2.717E-01 7.858E-01 1. 531E+OO NOT IDENT. KR-85 l.558E+OO 9.643E+OO l.629E+Ol NOT IDENT. SR-85 l.601E-01 9. 966E-01 l.683E+OO NOT IDENT. RB-86 O.OOOE+OO 3.140E+04 O.OOOE+OO SHORT HLIF Y-88 4.653E-02 2.202E-01 5.156E-01 NOT IDENT. Y-91 -l.329E+02 6.400E+02 l.180E+03 NOT IDENT. NB-94 -l.070E-02 3.508E-02 6.669E-02 NOT IDENT. NB-95 -2.388E-01 l.250E+OO 2.107E+00 NOT IDENT. NB-95M -4. 962E-01 2.845E+OO 4.826E+OO NOT IDENT. ZR-95 l.934E+OO 2.712E+OO 3. 715E+OO FAIL ABUN NB-97 O.OOOE+OO l.097E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF M0-99 0.000E+OO l.179E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.572E+41 O.OOOE+OO SHORT HLIF RH-101 -l.953E-02 4. 321E-02 7.469E-02 NOT IDENT. RH-102 1. 531E-02 7.310E-02 l.392E-01 NOT IDENT. RU-103 5.366E+OO 5. 231E+OO l .151E+Ol FAIL ABUN RH-106 -2.953E-01 6.393E-01 l.102E+OO NOT IDENT. RU-106 -2.953E-01 6.393E-01 l.102E+OO NOT IDENT. AG-108M 3.360E-02 3.703E-02 7.512E-02 NOT IDENT. CD-109 2.982E+OO l.609E+00 3.067E+OO NOT IDENT. AG-llOM 5.130E-02 l.239E-01 2.550E-01 FAIL ABUN SN-113 l.139E-01 2.743E-01 5.386E-01 NOT IDENT. CD-115 O.OOOE+OO 2.020E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.017E+05 O.OOOE+OO SHORT HLIF TE-123M 5.067E-02 l.533E-01 3.055E-01 NOT IDENT. SB-124 -6. 571E-01 l.707E+OO 3.429E+OO NOT IDENT. SB-125 -4.868E-02 1. 220E-01 2.192E-01 FAIL ABUN TE-125M 8.935E+Ol 3.109E+02 5.793E+02 NOT IDENT. I-126 O.OOOE+OO 9.782E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.382E+06 O.OOOE+OO SHORT HLIF SN-126 l.453E-01 l.028E-01 2.016E-01 NOT IDENT. SB-127 O.OOOE+OO l.820E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.953E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3 .181E+26 O.OOOE+OO SHORT HLIF BA-133 2.367E-02 4. 8 69E-02 8.874E-02 NOT IDENT. I-133 0.000E+OO 7.179E+40 O.OOOE+OO SHORT HLIF CS-134 1. 306E-01 l.058E-01 l.338E-01 FAIL ABUN CS-135 2.299E-02 l.592E-01 3.083E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.992E+05 O.OOOE+OO SHORT HLIF CE-139 -2.036E-03 l.259E-01 2.457E-01 NOT IDENT. BA-140 O.OOOE+OO l.537E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.300E+05 O.OOOE+OO SHORT HLIF CE-141 -5.740E+00 3.088E+Ol 4.955E+Ol NOT IDENT. CE-143 O.OOOE+OO l.042E+41 O.OOOE+OO SHORT HLIF CE-144 -4.306E-02 3.893E-01 6.950E-01 NOT IDENT. PM-144 3.248E-02 6.778E-02 l.395E-01 NOT IDENT. PR-144 2.802E+00 5.879E+OO l.210E+Ol NOT IDENT. PM-146 l.939E-02 5.429E-02 l.056E-01 NOT IDENT. ND-147 O.OOOE+OO 3.661E+07 0.000E+OO SHORT HLIF PM-147 l.318E+02 9.980E+02 l.821E+03 NOT IDENT. PM-149 O.OOOE+OO 2.721E+40 O.OOOE+OO SHORT HLIF EU-150 -4.283E-03 3.377E-02 5.634E-02 FAIL ABUN EU-152 5.747E-03 l.128E-01 2.144E-01 FAIL ABUN GD-153 -9.845E-02 2.504E-01 4.109E-01 NOT IDENT. EU-154 4.574E-02 l.263E-01 2.570E-01 NOT IDENT. EU-155 7. 2 65E-02 l.258E-01 2.402E-01 NOT IDENT. TB-160 -l.448E+OO l.972E+OO 3.443E+OO FAIL ABUN H0-166M 2.139E-02 6.676E-02 1. 331E-01 NOT IDENT. TM-171 -2. 711E+OO 3. 23 6°E+Ol 6.126E+Ol NOT IDENT. HF-172 -l.167E-02 2.786E-01 4.995E-Ol FAIL ABUN LU-172 -3.326E-02 l.334E-01 2.099E-01 FAIL ABUN LU-176 -9.986E-03 2. 611E-02 4.822E-02 NOT IDENT. HF-181 2.255E-01 5.453E+OO l.019E+Ol NOT IDENT. Page 2915 of 5809 TA-182 1.438E+OO 1.193E+OO 2.312E+OO FAIL ABUN RE-183 -2.638E+OO 4.377E+OO 7.887E+OO NOT IDENT. RE-184 2.943E+Ol 3.645E+Ol 7.818E+Ol NOT IDENT. W-188 -3.587E+Ol l.423E+02 2.362E+02 FAIL ABUN IR-192 -4.362E-01 5.188E-01 9.087E-01 FAIL ABUN HG-203 4.209E-01 2.751E+OO 5.309E+OO NOT IDENT. BI-207 -2.553E-02 5.978E-02 l.077E-01 FAIL ABUN PB-210 -1.184E+OO 5.916E+OO 1.104E+Ol NOT IDENT. BI-211 0.000E+OO 6.058E-01 9.921E-01 FAIL ABUN PB-211 -3.378E-02 8.026E-01 1.503E+OO NOT IDENT. BI-212 1.412E+OO 7.607E-01 1.461E+OO FAIL ABUN RN-219 -l.153E-01 4.514E-01 8. 272E-01 FAIL ABUN RA-223 -2.656E-01 6.892E-01 1. 2 62E+OO FAIL ABUN AC-227 l.042E-02 2.582E-01 4.975E-01 NOT IDENT. TH-227 l.042E-02 2.582E-01 4.975E-01 NOT IDENT. TH-229 l.264E-01 5.363E-01 1.054E+OO NOT IDENT. PA-231 5.744E-02 5.328E-01 1.019E+OO NOT IDENT. TH-231 -2.656E-01 6.892E-01 1.262E+OO FAIL ABUN PA-233 -8.485E-03 6.648E-02 1.255E-01 NOT IDENT. PA-234 -1.485E-01 3.838E-01 6.989E-01 FAIL ABUN PA-234M -1. 313E+OO 5.149E+OO 1. 012E+Ol NOT IDENT. NP-237 -8.485E-03 6.648E-02 l.255E-01 NOT IDENT. NP-238 O.OOOE+OO l.204E+41 O.OOOE+OO SHORT HLIF NP-239 3.933E-01 3.00lE-01 5.656E-01 NOT IDENT. PU-239 2.344E+Ol 3.894E+02 7. 001E+02 NOT IDENT. 2.139E-01 2.158E-01 4.059E-01 NOT IDENT. CM-243 -1. OSlE-02 l.259E-01 2.275E-01 NOT IDENT. BK-247 -6.994E-02 8.734E-02 l.363E-01 NOT IDENT. CM-247 -3.403E-02 4.0SOE-02 6.917E-02 NOT IDENT. CF-249 3.059E-03 4.283E-02 8.169E-02 NOT IDENT. CF-251 -1.555E-02 l.229E-01 2.383E-01 NOT IDENT. Page 2916of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:51:40.93 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 360 10.66* 1.059E+OO l.685E+Ol 1.685E+Ol 10.98 C0-58 810.76 7 99.45* 1. 711E+OO 2.038E-02 3.751E-01 203.37 BA-137M 661.66 179 89.90* 2.016E+OO 5.224E-01 5.323E-01 18.94 CS-137 661.66 179 85.10* 2.016E+OO 5.519E-01 5.624E-01 18.94 TL-208 277.37 ------6.60 4.173E+OO ------Line Not Found ------583.19 151 85.00* 2.233E+OO 4.222E-01 4.222E-01 23.00 860.56 ------12.50 1. 634E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 3.574E+OO ------Line Not Found ------351.06 281 12.92* 3.418E+OO 3.364E+OO 3.364E+OO 18.38 PB-212 74.82 164 10.28 3.783E+OO 2.237E+OO 2.237E+OO 39.87 77 .11 262 17 .10 4.000E+OO 2.030E+OO 2.030E+OO 25. 96 238.63 465 43.60* 4.702E+00 1.200E+OO 1.200E+00 12.25 300.09 ------3.30 3.910E+OO ------Line Not Found ------BI-214 609.32 190 45.49* 2.155E+OO 1.025E+OO 1. 02 6E+OO 22.80 1120. 29 41 14.92 1. 323E+OO 1.112E+OO 1.112E+OO 48.51 17'64. 49 31 15.30 8. 931E-01 1.201E+OO 1.202E+OO 39.68 PB-214 74.82 164 5.80 3.783E+OO 3.964E+00 3. 966E+00 39.87 77 .11 262 9.70 4.000E+OO 3.579E+OO 3.580E+OO 25. 96 87.09 ------3.41 4.837E+00 ------Line Not Found ------242.00 129 7.25 4.652E+OO 2.026E+OO 2.027E+OO 39.44 295.22 169 18.42 3. 963E+OO 1.226E+OO 1.226E+OO 27.45 351. 93 281 35.60* 3.418E+OO 1.221E+OO l.221E+00 18.38 RN-222 609.32 190 45.49* 2.155E+OO 1.025E+OO 1.026E+OO 22.80 1120.29 41 14.92 1.323E+OO 1.112E+OO l .112E+OO 48.51 1764.49 31 15.30 8.931E-01 1.201E+OO 1.202E+OO 39.68 RA-224 240.99 129 4.10* 4.652E+OO 3.582E+OO 3.582E+00 39.44 RA-226 609.32 190 45.49* 2.155E+OO 1.025E+OO 1. 026E+OO 22.80 1120.29 41 14.92 1.323E+OO 1.112E+OO 1.112E+OO 48.51 1764.49 31 15.30 8.931E-01 1.201E+OO 1.202E+OO 39.68 AC-228 105.21 ------1.10 5.776E+00 ------Line Not Found ------338.32 111 11. 27 3.533E+OO 1.479E+OO 1.479E+OO 32.75 794.95 28 4.25 1. 739E+OO 1.999E+00 1.999E+OO 82. 62 835. 71 ------1. 61 l.672E+00 ------Line Not Found ------911.20 79 25.80* 1.561E+OO l.041E+OO 1. 041E+OO 28.80 968. 97 49 15.80 1.487E+OO 1.lOOE+OO 1.lOOE+OO 36.32 RA-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 111 11. 27 3.533E+00 1. 479E+OO 1.479E+OO 32.75 794.95 28 4.25 1. 739E+OO l.999E+00 1.999E+OO 82.62 835.71 ------1. 61 1. 672E+00 ------Line Not Found ------911.20 79 25.80* 1.561E+OO 1. 041E+OO 1.041E+OO 28.80 968. 97 49 15.80 1.487E+OO 1.lOOE+OO 1.lOOE+OO 36.32 TH-228 74.82 164 10.28 3.783E+OO 2.237E+00 2.237E+OO 39.87 77 .11 262 17.10 4.000E+OO 2.030E+OO 2.030E+OO 25.96 238.63 465 43.60* 4.702E+OO 1.200E+OO 1.200E+00 12.25 300.09 ------3.30 3.910E+OO ------Line Not Found ------TH-230 609.32 190 45.49* 2.155E+OO 1.025E+OO 1.025E+OO 22.80 1120.29 41 14.92 1.323E+OO 1.112E+OO 1.112E+OO 48.51 Page 2917 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235001 Acquisition date Page : 2 3-0CT-2016 07:56:53 Nuclide Type: Nuclide TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Flag: "*" Page 2918of5809 Energy 1764.49 105.21 338.32 835. 71 911. 20 968.97 63.29 92.59 609.32 1120.29 1764.49 89. 96 93.35 143.76 163.33 185.72 205.31 63.29 92.59 43.53 74.66 511. 00 Key line Area 31 111 79 49 37 129 190 41 31 129 12 88 37 129 164 57 %Abn 15.30 1.10 11. 27 1. 61 25.80* 15.80 3.70* 4.23 45.49* 14.92 15.30 3.47 5.60 10.96* 5.08 57.20 5.01 3.70* 4.23 5.90 67.20* 100.00* %Eff 8.931E-01 5.776E+OO 3.533E+OO 1. 672E+OO l.561E+00 1.487E+OO 2.417E+OO 5. 211E+OO 2.155E+OO 1. 323E+OO 8.931E-01 5.033E+00 5. 211E+OO 6.129E+OO 5.908E+OO 5.553E+OO 5.230E+OO 2.417E+OO 5. 211E+OO 2.878E-01 3.783E+OO 2.491E+OO Uncorrected Decay Corr pCi/GRAM pCi/GRAM 1.201E+OO 1.201E+OO ------Line Not Found 1.479E+OO 1.479E+OO ------Line Not Found 1.041E+OO 1.041E+OO 1.lOOE+OO 1.lOOE+OO 2.186E+OO 2.186E+OO 3.099E+OO 3.099E+OO 1.025E+OO 1.025E+OO 1.112E+OO l.112E+00 1.201E+OO 1.201E+OO ------Line Not Found 2.341E+OO 2.341E+OO 9.669E-02 9.669E-02 ------Line Not Found 1.464E-01 1.464E-01 Line Not Found 2.186E+OO 2.186E+OO 3.099E+OO 3.099E+OO ------Line Not Found 3.421E-01 3.422E-01 l.218E-01 l.218E-01 2-Sigma %Error 3.9. 68 32.75 28.80 36.32 158.12 68.16 22.80 48.51 39.68 68.16 407.43 69.13 158.12 68.16 39.87 74.84 Summary of Nuclide Activity Sample ID : G405235001 Acquisition date Page : 3 3-0CT-2016 07:56:53 Total number of lines in spectrum 50 Number of unidentified lines 16 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 C0-58 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 70.86D 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600.00Y 1600.00Y 1.41E+10Y 1600.00Y 1. 41E+10Y 1. 41E+10Y 1.41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 18.4 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 685E+Ol 2.038E-02 5.224E-01 5.519E-01 4.222E-01 3.364E+OO 1. 200E+OO l.025E+OO 1. 221E+OO l.025E+OO 3.582E+OO 1.025E+OO 1. 041E+OO 1. 041E+OO l.200E+OO 1. 025E+OO 1. 041E+OO 2.186E+00 1.025E+OO 9.669E-02 2.186E+OO 3. 421E-01 l.218E-01 4.212E+Ol 4.212E+Ol Decay Corr pCi/GRAM 1.685E+Ol 3.751E-01 5.323E-01 5.624E-01 4.222E-01 3.364E+OO 1.200E+OO 1. 026E+OO 1. 221E+OO 1.026E+OO 3.582E+OO 1.026E+OO 1.041E+OO 1.041E+OO 1.200E+OO '1. 025E+OO l.041E+OO 2.186E+OO 1.025E+OO 9.669E-02 2.186E+OO 3.422E-01 1.218E-01 4.250E+Ol 4.250E+Ol 68.00% Decay Corr 2-Sigma Error 0.185E+Ol 7.629E-01 l.008E-01 1.065E-01 0. 971E-01 0.618E+OO 0.147E+OO 0.234E+OO 0.224E+OO 0.234E+OO 1.413E+OO 0.234E+OO 0.300E+OO 0.300E+OO 0.147E+OO 0.234E+00 0.300E+OO 3.457E+OO 0.234E+00 39.39E-02 3.457E+OO 1. 364E-01 0.912E-01 "M" Manually accepted 2-Sigma %Error 10.98 203.37 18.94 18.94 23.00 18.38 12.25 22.80 18.38 22.80 39.44 22.80 28.80 28.80 12.25 22.80 28.80 158.12 22.80 407.43 158.12 39.87 74.84 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 2919of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235001 Acquisition date : 3-0CT-2016 07:56:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 112. 23 14 167 1. 42 223.88 223 8 3.36E-03 **** 5.97E+OO T 0 208.83 76 184 2.65 416.92 411 13 1. 8 6E-02 82.0 5.17E+OO 0 270.65 94 105 3.65 540.43 533 14 2.34E-02 53.6 4.26E+OO T 0. 382.01 15 43 2.94 762.98 756 9 3.79E-03 **** 3.19E+OO 0 464.18 20 46 0.60 927.18 918 13 5.13E-03 **** 2.70E+OO T 1 546.32 23 19 1. 84 1091.33 1088 18 6.19E-03 71. 6 2.36E+00 T 1 548.66 19 29 1. 67 1096.00 1088 18 5.09E-03 **** 2.35E+OO 4 658.58 17 21 1. 94 1315.69 1312 17 4.55E-03 **** 2.02E+OO T 0 717.42 13 19 3.43 1433.28 1429 12 3.65E-03 **** l.89E+OO 0 726. 67 33 16 1. 28 1451. 7 5 1448 8 9.04E-03 55.0 l.87E+OO T 0 755.24 14 25 1. 36 1508.86 1502 10 3.91E-03 **** l.81E+OO T 0 769.00 25 40 0.88 1536.36 1527 12 6.74E-03 **** 1. 7 9E+00 0 808.56 14 20 1. 21 1615.42 1608 11 3.75E-03 **** 1. 72E+00 T 1 964. 76 26 1 2.17 1927.61 1922 21 7.22E-03 55.2 l.49E+OO T 0 1023.46 12 15 4.60 2044.92 2036 15 3.33E-03 **** 1. 42E+OO 0 1099.87 15 18 0.80 2197.65 2188 14 4.35E-03 **** 1. 34E+OO T 0 1130 .15 18 6 3.23 2258.17 2252 12 5.00E-03 72. 0 1. 31E+OO T 0 1154.59 25 10 2.10 2307.01 2300 14 7.16E-03 66.1 l.29E+OO 2 1186.65 14 8 2.55 2371. 09 2361 26 4.09E-03 **** l.26E+OO 2 1191. 84 14 17 2.55 2381. 4 7 2361 26 4. OlE-03 **** l.26E+OO 0 1195. 72 9 7 1. 37 2389.22 2386 7 2.50E-03 **** 1. 25E+OO 0 1222.52 15 8 1. 55 2442.79 2438 10 4.24E-03 84.7' l.23E+OO T 0 1228.78 14 5 2.06 2455.30 2451 9 3.96E-03 75.7 l.23E+OO 0 1252.82 22 3 3.01 2503.34 2498 12 6.31E-03 52.1 1. 21E+OO 0 1282.31 23 4 5.42 2562.30 2555 16 6.59E-03 55.9 l.18E+OO 0 1325. 72 13 0 2.73 2649.08 2644 12 3. 61E-03 55.5 l.15E+OO 0 1378.42 14 7 1.11 2754.41 2750 10 3.91E-03 94.7 l. llE+OO 0 1729.65 6 2 0.69 3456.50 3450 11 l.90E-03 **** 9.lOE-01 Flags: "T" = Tentatively associated Page 2920 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:58:05.87 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l *
  • Acquisition date 3-0CT-2016 07:56:53 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:20:00 Nuclide Library : SOLID *
  • Sample ID G405235001 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.4192E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-58 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.322E-01 O.OOOE+OO 3.814E-02 4.029E-02 3.242E-02 4.997E-02 6.005E-02 6.692E-02 6.005E-02 5.359E-01 6.005E-02 1.lOOE-01 1.lOOE-01 4.997E-02 6.003E-02 1.lOOE-01 1.395E+OO 6.003E-02 1.791E-01 1.395E+OO 5.947E-02 2.957E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 2921of5809 Le (pCi/GRAM 1.234E+Ol 4.521E-02 O.OOOE+OO 1.999E-02 3.135E-01 O.OOOE+OO O.OOOE+OO 6.639E-02 4.262E-01 NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 . RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU...:.150 EU-152 GD-153 EU:--154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 2922 of 5809 O.OOOE+OO 5.099E-02 7.686E+OO 2.947E-02 l.825E-01 2.199E+OO 1.192E+Ol O.OOOE+OO 1.881E-01 O.OOOE+OO 0.000E+OO 6.927E-01 7.428E+OO 7.675E-01 0.000E+OO l.997E-01 5.143E+02 2.955E-02 9.515E-01 2.254E+OO 1.672E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.522E-02 6.238E-02 5.151E+OO 4.904E-01 4.904E-01 3. 472E-02 l.469E+OO 1.133E-01 2.474E-01 O.OOOE+OO O.OOOE+OO 1.443E-01 1.215E+OO 9.914E-02 2.724E+02 O.OOOE+OO O.OOOE+OO 9.664E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.066E-02 0.000E+OO 6.047E-02 1.433E-01 O.OOOE+OO O.OOOE+OO 1.157E-01 O.OOOE+OO O.OOOE+OO 2.333E+Ol 0.000E+OO 3.248E-01 6.308E-02 5.470E+OO 4.823E-02 0.000E+OO 8.571E+02 O.OOOE+OO 2.599E-02 9.888E-02 1.942E-01 1.lOOE-01 l.131E-01 1. 461E+OO 5.947E-02 2.873E+Ol 2.351E-01 9.346E-02 2.205E-02 4.643E+OO 1.025E+OO SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 2923 of 5809 3. 711E+OO 3.498E+Ol l.093E+02 4.152E-01 2.471E+OO 4.672E-02 5.173E+OO 4.796E-01 6.871E-01 6.722E-01 3. 771E-01 5.807E-01 2.312E-01 2.312E-01 4. 961E-01 4.740E-01 5.807E-01 5.767E-02 3.097E-01 4.465E+OO 5.767E-02 O.OOOE+OO 2. 671E-01 3.308E+02 l.924E-01 1.073E-01 6.243E-02 3.123E-02 3.729E-02 1.115E-01 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:58:11.72 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235001.CNF;l *
  • Acquisition date 3-0CT-2016 07:56:53 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:20:00 Nuclide Library : SOLID *
  • Sample ID G405235001 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity 1.4192E+02 GRAM *
  • Quantity Err(%) 1.4092E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.685E+Ol 2.017E+OO 2.017E+OO C0-58 3. 751E-01 7.478E-01 7.478E-01 BA-137M 5.323E-01 l.014E-01 1.014E-01 CS-137 5.624E-01 1.071E-01 1.071E-01 TL-208 4.222E-01 9.686E-02 9.686E-02 PB-212 1.200E+OO l.576E-01 1. 57 6E-01 BI-214 1.026E+OO 2.334E-01 2.334E-01 PB-214 1.221E+OO 2.258E-01 2.258E-01 RN-222 1.026E+OO 2.334E-01 2.334E-01 RA-224 l.414E+OO 1. 511E+OO 1. 511E+OO RA-226 1.026E+OO 2.334E-01 2.334E-01 AC-228 1.041E+OO 2.987E-01 2.987E-01 RA-228 1.041E+OO 2.987E-01 2.987E-01 TH-228 1.200E+OO l.576E-01 1.576E-01 TH-230 1.025E+OO 2.333E-01 2.333E-01 TH-232 1. 041E+OO 2.987E-01 2.987E-01 TH-234 2.186E+OO 3.422E+OO 3.422E+OO U-234 1. 025E+OO 2.333E-01 2.333E-01 U-235 9.669E-02 3.861E-01 3.861E-01 U-238 2.186E+OO 3.422E+OO 3.422E+OO AM-243 2.364E-01 1.381E-01 l.381E-01 ANH-511 1.218E-01 8. 951E-02 8.951E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM * ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.033E+Ol 1.586E+Ol 1.653E+Ol NOT IDENT. NA-22 1. 97 5E-02 5.170E-02 5.246E-02 NOT IDENT. NA-24 -l.OOOE+41 l.417E+41 O.OOOE+OO SHORT HLIF AL-26 -l.136E-02 2.856E-02 2.901E-02 FAIL ABUN SC-46 -2.504E-01 4.310E-01 4.456E-01 FAIL ABUN V-48 1.277E+04 l.595E+04 1. 696E+04 SHORT HLIF CR-51 2.842E+02 4.614E+02 4.789E+02 SHORT HLIF MN-54 1. 886E-02 7.391E-02 7.440E-02 NOT IDENT. Page 2924 of 5809 C0-56 -3.947E-01 5.565E-01 5.843E-01 NOT IDENT. MN-56 -l.OOOE+41 l.410E+41 O.OOOE+OO SHORT HLIF C0-57 4.240E-02 5.653E-02 5.967E-02 NOT IDENT. FE-59 1. lllE+Ol l.445E+Ol 1.529E+Ol FAIL ABUN C0-60 -3.648E-02 5.044E-02 5.306E-02 NOT IDENT. ZN-65 -4. 372E-03 2.487E-01 2.487E-01 NOT IDENT. GE-68 -5.512E-01 2.709E+OO 2.720E+OO NOT IDENT. AS-73 8.307E+OO 1.279E+Ol 1.333E+Ol NOT IDENT. AS-74 5.670E+03 7.493E+03 7.917E+03 SHORT HLIF SE-75 -1. 7.64E-01 2.577E-01 2.697E-01 NOT. I DENT. BR-77 1. l 72E+38 1.007E+39 O.OOOE+OO SHORT HLIF SR-82 1.438E+02 7 .141E+02 7.170E+02 SHORT HLIF RB-83 2.717E-01 7.867E-01 7. 962E-01 NOT IDENT. KR-85 1.558E+OO 9.643E+OO 9.668E+OO NOT IDENT. SR-85 1. 601E-01 9. 966E-01 9.992E-01 NOT IDENT. RB-86 -1.205E+04 3 .141E+04 3 .187E+04 SHORT HLIF Y-88 4.653E-02 .2. 202E-01 2.212E-01 NOT IDENT. Y-91 -l.329E+02 6.400E+02 6.428E+02 NOT IDENT. NB-94 -1. 070E-02 3.508E-02 3. 541E-02 NOT IDENT. NB-95 -2.388E-01 l.250E+OO l.255E+OO NOT IDENT. NB-95M -4.962E-01 2.845E+OO 2.854E+OO NOT IDENT. ZR-95 1.934E+OO 2. 714E+OO 2.850E+00 FAIL ABUN NB-97 l.OOOE+41 1.098E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 4.411E+41 O.OOOE+OO SHORT HLIF M0-99 1. 831E+31 1.179E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.576E+41 O.OOOE+OO SHORT HLIF RH-101 -1.953E-02 4.335E-02 4.424E-02 NOT IDENT. RH-102 1.531E-02 7. 311E-02 7.344E-02 NOT IDENT. RU-103 5.366E+OO 5.237E+OO 5.769E+OO FAIL ABUN RH-106 -2.953E-01 6.396E-01 6.533E-01 NOT IDENT. RU-106 -2.953E-01 6.396E-01 6.533E-01 NOT IDENT. AG-108M 3.360E-02 3.705E-02 4.003E-02 NOT IDENT. CD-109 2.982E+OO l.628E+00 2. lllE+OO NOT IDENT. AG-llOM 5 .130E-02 1.239E-01 1. 2 60E-01 FAIL ABUN SN-113 l.139E-01 2.743E-01 2.791E-01 NOT IDENT. CD-115 6.777E+38 2.023E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 2.239E+03 l.017E+05 1. 017E+05 SHORT HLIF TE-123M 5.067E-02 l.533E-01 l.550E-01 NOT IDENT. SB-124 -6. 571E-01 1.707E+OO 1.733E+OO NOT IDENT. SB-125 -4.868E-02 l.220E-01 l.239E-01 FAIL ABUN TE-125M 8.935E+Ol 3.109E+02 3.135E+02 NOT IDENT. I-126 1.189E+05 9.783E+05 9.798E+05 SHORT HLIF SB-126 -4.278E+05 1. 384E+06 l.398E+06 SHORT HLIF SN-126 l.453E-01 l.032E-01 l.222E-01 NOT IDENT. SB-127 -1.412E+22 2.651E+22 O.OOOE+OO SHORT HLIF I-131 1.886E+09 4.954E+09 5.026E+09 SHORT HLIF I-132 -l.OOOE+41 1. 847E+42 O.OOOE+OO SHORT HLIF TE-132 -1.375E+26 3.229E+26 O.OOOE+OO SHORT HLIF BA-133 2.367E-02 4.870E-02 4.985E-02 NOT IDENT. I-133 -1.000E+41 1. 935E+41 O.OOOE+OO SHORT HLIF CS-134 1.306E-01 1. 059E-01 1.212E-01 FAIL ABUN CS-135 2.299E-02 1.592E-01 1. 596E-01 NOT IDENT. I-135 1.000E+41 7. 696E+41 O.OOOE+OO SHORT HLIF CS-136 2.616E+05 3.005E+05 3.229E+05 SHORT HLIF CE-139 -2.036E-03 l.259E-01 l.259E-01 NOT IDENT. BA-140 1.090E+06 l.538E+06 l.615E+06 SHORT HLIF LA-140 1. 213E+05 5.300E+05 5.328E+05 SHORT HLIF CE-141 -5.740E+OO 3.089E+Ol 3.099E+Ol NOT IDENT. CE-143 1.000E+41 1.047E+41 O.OOOE+OO SHORT HLIF CE-144 -4.306E-02 3.893E-01 3.898E-01 NOT IDENT. PM-144 3.248E-02 6.781E-02 6.937E-02 NOT IDENT. PR-144 2.802E+00 5.880E+OO 6.014E+OO NOT IDENT. PM-146 1.939E-02 5.431E-02 5.500E-02 NOT IDENT. ND-147 -2.717E+07 3.664E+07 3.863E+07 SHORT HLIF PM-147 1.318E+02 9.980E+02 9.998E+02 NOT IDENT. PM-149 -9.014E+39 2*. 728E+40 O.OOOE+OO SHORT HLIF EU-150 -4.283E-03 3.377E-02 3.382E-02 FAIL ABUN EU-152 5.747E-03 1.128E-01 1.128E-01 FAIL ABUN GD-153 -9.845E-02 2.505E-01 2.544E-01 NOT IDENT. EU-154 4.574E-02 1.263E-01 l.280E-01 NOT IDENT. EU-155 7.265E-02 l.259E-01 l.301E-01 NOT IDENT. TB-160 -1.448E+OO 1.974E+OO 2.079E+OO FAIL ABUN H0-166M 2.139E-02 6.677E-02 6.746E-02 NOT IDENT. TM-171 -2. 711E+OO 3.236E+Ol 3.239E+Ol NOT IDENT. HF-172 -1.167E-02 2.786E-01 2.787E-01 FAIL ABUN LU-172 -3.326E-02 l.334E-01 l.342E-01 FAIL ABUN LU-176 -9.986E-03 2.612E-02 2.650E-02 NOT IDENT. HF-181 2.255E-01 5.453E+OO 5.454E+OO NOT IDENT. Page 2925 of 5809 TA-182 l.438E+OO 1.195E+OO l.359E+OO FAIL ABUN RE-183 -2.638E+OO 4. 396E+OO 4.554E+OO NOT IDENT. RE-184 2.943E+Ol 3.712E+Ol 3.942E+Ol NOT IDENT. W-188 -3.587E+Ol l.424E+02 l.433E+02 FAIL ABUN IR-192 -4.362E-01 5.191E-01 5.551E-01 FAIL ABUN HG-203 4.209E-01 2.751E+OO 2.757E+OO NOT IDENT. BI-207 -2.553E-02 5.979E-02 6.088E-02 FAIL ABUN PB-210 -l.184E+OO 5.917E+OO 5.941E+OO NOT IDENT. BI-211 3.364E+OO 6.243E-01 1.640E+OO FAIL ABUN PB-211 -3.378E-02 8.026E-01 8.027E-01 NOT IDENT. BI-212 l.412E+OO 7.641E-01 9.945E-01 FAIL ABUN RN-219 -l.153E-01 4.517E-01 4.547E-01 FAIL ABUN RA-223 -2.656E-01 6.894E-01 6.997E-01 FAIL ABUN AC-227 l.042E-02 2.582E-01 2.583E-01 NOT IDENT. TH-227 l.042E-02 2.582E-01 2.583E-01 NOT IDENT. TH-229 1.264E-01 5.363E-01 5.393E-01 NOT IDENT. PA-231 5.744E-02 5.329E-01 5.336E-01 NOT IDENT. TH-231 -2.656E-01 6.894E-01 6.997E-01 FAIL ABUN PA-233 -8.485E-03 6.648E-02 6.659E-02 NOT IDENT. PA-234 -1.485E-01 4.197E-01 4.250E-01 FAIL ABUN PA-234M -1.313E+OO 5.149E+OO 5.183E+OO NOT IDENT. NP-237 -8.485E-03 6.648E-02 6.659E-02 NOT IDENT. NP-238 1.000E+41 1.205E+41 O.OOOE+OO SHORT HLIF NP-239 3.933E-01 3.019E-01 3.501E-01 NOT IDENT. PU-239 2.344E+Ol 3.894E+02 3.896E+02 NOT IDENT. AM-241 2.139E-01 2.164E-01 2.369E-01 NOT IDENT. CM-243 -1.051E-02 l.259E-01 l.260E-01 NOT IDENT. BK-247 -6.994E-02 8.847E-02 9.392E-02 NOT' IDENT. CM-247 -3.403E-02 4.090E-02 4.368E-02 NOT IDENT. CF-249 3.059E-03 4.283E-02 4.286E-02 NOT IDENT. CF-251 -1.555E-02 1.229E-01 1.231E-01 NOT IDENT. Page 2926 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 78.2704 87.09 134.7812 136.47 85.0401 45.60 71. 5784 87.57 127.0328 140.51 0.0000 46.54 72.7927 88.03 103.5126 143.76 85.8807 49. 72 0.0000 88.34 141. 0985 144.24 85.9352 51. 35 77.8999 88.47 136.6277 145.44 91.8101 51. 87 86.3264 89. 96 143.0228 152.43 89.3353 52.39 78 .1111 1093.63 137.1702 153.25 0.0000 52.97 63.6255 91.11 0.0000 323.87 90.7811 53.44 65.7908 92.59 114. 5844 156.02 0.0000 54.07 78.4481 93.35 114.7400 158.56 0.0000 57.36 0.0000 94.56 114. 9858 159.00 89.2407 57.53 88.6213 94.65 115. 0043 162.33 96. 3059 57.98 101.3919 94.67 115. 0082 162.66 0.0000 59.27 69.2175 94.87 115. 0482 163.33 90.5537 59.32 69.2258 97.43 100.6885 165.86 88.3075 59.54 81. 9838 98.43 85.9617 176.31 78.3306 60. 96 93.6061 98.44 85. 9634 176.60 0.0000 ,61.17 86.5572 99.53 97.6068 177.52 75.0288 62.93 94.0358 100 .11 100.0017 181. 07 0.0000 63.29 94 .1133 102.03 93.4072 181.52 80.9379 63.58 94.1761 103.18 94.7418 184.41 77.3337 64.28 102.9014 103.37 94. 7718 143.76 77.4463 66.73 100.5944 105.21 73.0336 193.51 78.9761 67.24 103.5850 105.31 73.0456 197.03 85. 3722 125.81 111. 2457 106.12 85.9137 198.01 77.6124 67.75 111.2622 106.47 98.7410 201. 83 78.8013 69.67 100.8815 109.28 75.8505 203.43 72. 3545 70.83 144.6296 111. 00 84.2492 205.31 56.6783 72.81 141.2314 111.76 0.0000 210.85 70.2564 72. 87 141.2491 114.06 99.9395 215.65 63.0488 74.66 130.4477 116. 30 0.0000 222 .11 78.6445 74.82 130.4904 116.74 61.3925 227.09 80.8209 74.97 130.5312 119.76 83.0230 227.38 80.8429 77 .11 131.1005 121.12 82.0038 228.16 0.0000 78.74 131.5290 121.22 82.0159 228.18 86.2988 79.69 131. 77 69 121. 78 83.2740 116.74 86.2988 80 .12 ' 104.9197 122.06 72.5976 235.69 71. 97 57 80.19 0.0000 122.92 95.3308 235. 96 71. 9943 80.57 121.2817 123.07 95.3522 238.63 63.5486 81. 00 113.9828 265.00 90.6657 238.98 0.0000 81. 07 113.9984 125.81 87.3586 240.99 63.6874 81. 75 121. 5611 127.23 104.3257 242.00 63.7465 83.79 109.3894 127.91 80.4223 244.70 64.3611 84.00 101.6162 129.30 96.2170 252.40 0.0000 85.43 164.5944 131. 20 86.8293 252.80 53.3366 86. 55 138.0118 133. 02 91.8886 254.15 0.0000 8 6. 7 9 131.3385 133. 52 71. 3841 256.23 57.1884 86.94 134.7437 136.00 69.2017 260.90 0.0000 Page 2927 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 59.9320 355.39 0.0000 584.27 23.8292 264.80 57.1520 356.01 31. 3994 595.83 0.0000 265.00 57.1620 364.49 0.0000 427.87 29.7303 268.22 55.9216 366.42 0.0000 602.52 0.0000 269.46 55.9802 372.51 40.3223 604. 72 32.6505 270.03 56.0071 375.05 35.3418 607.14 . 25.8060 271.23 56.0645 377.52 40. 9622 609.32 21. 8134 273.65 0.0000 356.01 36.5625 610.33 21. 8234 276.40 65.3180 388.16 35.6473 614.28 24.1642 277.37 56.3538 388.63 0.0000 618.01 28.8157 277.60 56.3647 391.69 35.7285 620.36 19.6154 278.00 48.8653 264.66 36. 9602 621.93 28.8676 279.20 57.3799 401.81 40.0696 630.19 0.0000 279.54 60.2188 402.40 43.1672 631. 29 22.0314 279.70 61.1676 404.85 39 .1164 633.25 27.8535 280.46 61.2060 410.95 37.1990 634.78 0.0000 283.69 45.3184 413.71 35.1925 635.95 25.5628 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 48.2182 423.72 0.0000 645.85 20.1313 285.90 0.0000 427.09 39.6552 657.76 29.5620 287.50 55.8767 427.87 36.5424 657.90 0.0000 290.67 56. 9690 433.94 33.5313 661. 66 29.0835 293.27 0.0000 439.40 35.7425 664.57 0.0000 '351.93 48.6000 453.88 31.8048 666.33 0.0000 295.96 48.6291 463.37 27.7144 666.50 0.0000 879.38 51.5962 468.07 38.4756 667.71 0.0000 299.98 61. 6970 473.00 0.0000 677.62 24.8452 300.09 61. 7023 475.06 37.5535 685.70 0.0000 300.13 61. 7036 476.78 35.4412 695.00 0.0000 301.36 57.4548 477.60 41.9041 696.49 23.2531 302.85 54.6447 482.18 34.4701 696. 51 23.2531 256.23 47.0361 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 19.6824 306.78 45.1956 497.08 11. 9453 697.49 23.2626 308.46 31.7740 505.52 27.8164 702.65 24.2084 311. 90 41. 5119 507.63 0.0000 706.68 22.4525 316.51 53.2835 511. 00 33.9141 711. 68 19.5414 319.41 0.0000 514.00 32. 8720 720.70 0.0000 320.08 0.0000 514.00 32.8720 721. 93 0.0000 321. 04 47.6322 520.40 25.2854 722.78 14.4634 323.87 51.6284 520.69 0.0000 722. 91 14.4644 325.23 59.4822 522.65 0.0000 723.31 14.4668 328.76 0.0000 527.90 0.0000 724.19 16.8836 333.37 58.8562 528.26 19.8691 '727.33 11.5918 333.97 50.0496 529.59 34.2430 733.00 18.1537 334.37 50.0641 529.87 0.0000 735.93 18.1744 338.28 40.3619 531. 02 0.0000 333.97 16.3669 338.32 40.3627 537.26 0.0000 739.50 0.0000 311. 90 50.2851 546.56 0.0000 747.24 19.1684 340.48 50.2851 552.55 26.8184 748.06 21.9133 340.55 0.0000 563.25 34.8233 752.31 24.8766 344.28 46.4664 569.33 38.3067 753.82 0.0000 345.93 50.4802 946.00 38.3095 756.73 16.1240 351.06 40.7289 569.70 39.4405 756.80 14.6587 351. 93 40.7531 583.19 23.8173 884.68 23.5188 Page 2928 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 27.9489 1274.44 20.9000 1620.50 1.8637 766.42 24.8288 1001.03 14.9506 1621. 92 3.7285 766.84 24.8321 1002.74 17.9506 1678.03 0.0000 772.60 0.0000 1004.73 21. 9530 1690.97 3.7814 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 . 1025.87 0.0000 1764.49 4.7957 778.90 17.5551 1028.54 0.0000 1063.66 13.4429 783.70 0.0000 1037.84 13.1031 1771.35 7.6832 785.37 19.4504 1038.76 0.0000 1791.20 0.0000 792.07 19.3134 631. 29 14.1487 1808.65 3.8691 794.95 9.2953 1048.07 0.0000 1810.72 0.0000 795. 8 6 9.2984 1049.04 7.0795 1836.06 2.9169 810.06 0.0000 1050.41 14.1649 810.29 0.0000 1063.66 19.2992 344.28 0.0000 1077.00 0.0000 810.76 0.0000 1077.34 15.2975 815.77 0.0000 1085.87 12.2681 1048.07 0.0000 1093.63 26.2313 832.01 20. 7284 1099.45 16.4219 834.85 17.9203 1112. 07 15.4504 835.71 12.2649 1112.84 8.2422 836.80 0.0000 1115.54 18.1468 846.75 0.0000 1120.29 11. 3572 846.77 23.6794 1120. 55 11.3578 856.80 0.0000 1221.41 11. 3599 860.56 16.1803 1129. 67 11.3867 871. 09 15.2842 1131.51 0.0000 873.19 17.2073 1147.95 0.0000 875.33 0.0000 1173.23 12. 5720 879.38 18.2021 1177.95 9.7908 880.51 12.4589 1189.05 10.1010 883.24 19.1852 1204.77 17.9629 884.68 16.3157 1221.41 8.4902 889.28 16.3411 1231. 02 11. 9164 894.76 15.4087 1235.36 0.0000 898.04 23.1387 1238.28 11. 7258 900. 72 18.3344 1260.41 0.0000 903.28 14.4873 1271.87 10.7520 911.20 12.5890 1274.44 8.6074 912.08 9.2991 1274.54 8.6074 923.98 0.0000 1291.59 4.3223 926.50 15.5728 1298.22 0.0000 929 .11 23.3789 1312 .11 0.0000 937.49 25.3970 1332.49 13.0994 944 .13 0.0000 1362.66 0.0000 946.00 25.4676 1365.19 8.8022 949.00 19.6094 1368.63 0.0000 667. 71 0.0000 1384.29 7.3686 962. 31 17.3298 1408.01 6.6691 964.08 11. 822 8 1457.56 0.0000 966 .17 11. 8304 1460.82 4.5005 911. 20 11. 8411 1489.16 2. 7176 968.97 11. 8411 1505.03 12.7265 983.53 0.0000 1584.12 13.8713 984.45 0.0000 1596.21 0.0000 Page 2929 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:58:47.82 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM30.CNF;300 Background date : Z-OCT-2016 11:01:47. Sample date 10-DEC-2015 14:30:00 Acquisition date : 3-0CT-2016 07:57:26. Sample ID G405235002 Sample quantity : 1.23837E+02 GRAM Detector name : GAM30 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.45 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ********************************************************************************* Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 3 2 2 2 0 0 0 2 2 0 3 3 0 2 2 0 0 5 5 2 2 0 0 3 3 0 0 0 0 0 0 Page 2930 of 5809 Energy 63.20* 72. 96 74.81 77.12* 87.18 89.84 92.75* 105.57 186.31* 209.30 238.71* 241.88 270.44 295.25* 300.21 331.76* 338.35* 341. 35 352.21* 387.36 430.57 433.18 463.17 466.96 511.12* 524.39 583.26* 587.03 609.64* 639.66 660.26 666.48 727. 68 737.36 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 16 37 170 277 96 66 93 39 88 49 530 122 43 185 28 83 112 22 259 19 15 24 38 14 35 15 97 15 18 6 25 44 31 58 15 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 128 158 155 129 181 141 140 134 173 89 59 62 116 38 59 97 38 51 74 50 7 9 20 18 58 26 18 12 31 28 33 12 12 16 1.12 1. 31 1. 31 1.10 1.19 0.97 1. 23 1.15 1.18 1. 00 1. 20 1. 44 1. 50 1.25 1. 65 7.88 1. 45 1. 54 1. 34 1. 86 1. 54 1. 64 1. 65 1. 50 1. 97 1. 69 1. 39 1. 92 1. 39 3.74 7.52 0.67 2.21 0.78 126.12 145.65 149.35 153.97 174.09 179.40 185.22 210.87 372.35 418.34 477.15 483.50 540.64 590.25 600.18 663.28 676.47 682.46 704.19 774.49 860.93 866.14 926.14 933.73 1022.06 1048.59 1166.36 1173.92 1219.15 1279.20 1320.41 1332.84 1455.27 1474.65 123 142 142 142 169 169 169 207 365 415 471 471 536 585 585 652 672 672 699 767 859 859 919 919 1015 1041 1162 1162 1213 1271 1309 1328 1448 1471 7 17 17 17 25 25 25 10 14 8 18 18 13 27 27 20 21 21 13 10 11 11 31 31 17 10 15 15 14 14 20 12 16 7 4.52E-03122.3 l.03E-02 65.1 4.72E-02 15.1 7.68E-02 9.3 2.66E-02 23.7 1.82E-02 30.4 2.59E-02 25.9 1. 09E-02 57. 3 2.43E-02 34.5 1. 37E-02 35. 8 1.47E-01 5.0 3.40E-02 16.6 l.20E-02 53.1 5.13E-02 9.6 7.74E-03 54.9 2.32E-02 31.4 3.12E-02 14.4 6.02E-03 60.7 7.19E-02 9.4 5.29E-03 73.1 4.04E-03 32.2 6.72E-03 32.8 l.05E-02 29.8 3.98E-03 62.2 9.64E-03 60.7 4.07E-03 73.5 2.70E-02 13.8 4.llE-03 42.9 5.17E-02 9.9 7.02E-03 48.6 1.22E-02 36.2 8.61E-03 28.7 1.60E-02 18.8 4.27E-03 49.7 Fit 1.24E+OO 2.94E+OO 2.23E+OO 1.17E+OO 3.34E+OO 7.52E-01 1. 95E+OO 2.37E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235002 Acquisition date 3-0CT-2016 07:57:26 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 3.5 0 794.89 31 10 1. 34 1589.74 1585 10 8.61E-03 26.2 36 0 851. 32 14 2 0.66 1702.64 1699 8 3.98E-03 31. 2 37 0 860.49 37 14 1. 26 1720.98 1715 12 l.03E-02 26.4 38 0 911. 52 111 27 1. 55 1823.07 1817 14 3.09E-02 13.5 39 0 935.80 26 3 2. 68 1871. 64 1867 10 7.31E-03 22.6 40 5 964. 58* 22 32 2. 64 1929.22 1921 27 6.24E-03 63.9 8.74E-01 41 5 969.20* 50 22 1. 87 1938.48 1921 27 1.39E-02 23.9 42 0 1065.20 8 13 0.77 2130.55 2124 11 2.lOE-03101.3 43 0 1115. 32 11 14 1. 38 2230.82 2223 14 3.06E-03 78.2 44 0 1121.17* 57 7 2.07 2242.53 2236 14 1. 59E-02 16.8 45 0 1167. 01 19 20 5. 96 2334.25 2325 16 5.34E-03 56.7 46 0 1212.44 9 14 0.66 2425.14 2420 7 2.59E-03 73.9 47 0 1238.24 21 12 1. 35 2476. 76 2469 12 5.83E-03 39.6 48 0 1328.10 6 5 1. 03 2656.58 2652 7 1.64E-03 76.0 49 0 1378.05 16 2 1. 36 2756.53 2751 10 4. 37E-03 31. 3 50 0 1393.55* 4 4 1. 41 2787.55 2781 8 1.16E-03101.2 51 0 1430.88 6 5 1. 40 2862.25 2855 10 1.67E-03 80.8 52 0 1461. 22* 432 10 1. 91 2922.95 2916 14 l.20E-01 5.1 53 0 1547.80 9 0 0.88 3096. 22 3091 10 2.50E-03 33.3 54 0 1731.15 7 5 0.77 3463.13 3455 10 1.92E-03 71.6 55 0 1765.18* 23 '6 3.09 3531.24 3526 11 6.51E-03 30.0 Flag: "*" = Peak area was modified by background subtraction Page 2931 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:58:50 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 14:30:00 G405235002 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:57:26 123.84 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA30 0 01:00:00.00 1.50 keV No Empirical 75.00 Interference Report Interfering Nuclide Page 2932 of 5809 PB-214 PB-214 PB-214 PB-214 PB_..:214 PB-214 PB-214 PB-214 PB-214 Line 87.09 87.09 87.09 87.09 242.00 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide EU-155 SN-126 SN-126 CD-109 RA-224 AM-243 TH-228 PB-212 BI-211 Line 86.55 86.94 87.57 88.03 240.99 74.66 74.82 74.82 351. 06 CAN 0 01:00:01.45 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235002 Acquisition date 3-0CT-2016 07:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.307E+OO l. 784E+Ol 1. 784E+Ol 10.20 OK ZN-65 1115. 54 50.60* 1.652E+OO 7.695E-02 1. 792E-01 156.41 OK CD-109 88.03 3.70* 6.548E+OO 1.395E+OO 2.183E+OO 92.25 OK SN-126 64.28 9.60 3.867E+OO 3.007E-01 3.007E-01 244.55 OK 86.94 8.90 6.548E+OO 5.801E-01 5.801E-01 92.25 OK 87.57 37.00* 6.548E+OO l.395E-01 1.395E-01 92.25 OK BA-137M 661. 66 89.90* 2.546E+OO 1.156E-01 1.178E-01 72. 35 OK CS-137 661.66 85.10* 2.546E+OO l.222E-01 1.245E-01 72. 35 OK EU-155 86.55 30:70 6.548E+OO 1.682E-01 1.894E-01 92.25 OK 105.31 21.10* 7.284E+OO l.703E-01 1.918E-01 114. 53 OK TL-208 277.37 6.60 4.820E+OO Line Not Found Absent 583.19 85.00* 2.799E+OO 2.485E-01 2.485E-01 27.65 OK 860.56 12.50 2.059E+OO 8.550E-01 8.550E-01 52.88 OK PB-212 74.82 10.28 5.441E+OO 1.291E+OO 1.291E+OO 49.80 OK 77 .11 17.10 5.693E+OO 1.928E+OO l.928E+OO 18.63 OK 238.63 43.60* 5.356E+OO 1. 449E+OO 1. 449E+OO 10.08 OK 300.09 3.30 4.554E+OO 1.169E+OO 1.169E+OO 109.89 OK BI-214 609.32 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 OK 1120.'29 14.92 1.644E+OO 1.366E+OO 1. 366E+'OO 33.69 OK 1764.49 15.30 l.121E+00 7.769E-01 7.771E-01 59.97 OK PB-214 74.82 5.80 5.442E+OO Line Not Found <<INT Reject 77 .11 9.70 5.693E+OO 3.400E+OO 3. 401E+OO 18.63 OK 87.09 3. 41 6.542E+00 Line Not Found <<INT Reject 242.00 7.25 5.305E+OO Line Not Found <<INT Reject 295.22 18.42 4.609E+OO 1.374E+OO 1. 37 5E+00 19.23 OK 351.93 35.60* 4.058E+OO 1.119E+OO 1.120E+OO 18.84 OK RN-222 609.32 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 OK 1120.29 14.92 1.644E+OO 1.366E+00 l.366E+00 33.69 OK 1764.49 15.30 1.121E+OO 7.769E-01 7.771E-01 59.97 OK RA-224 240.99 4.10* 5.307E+OO l.160E+OO 1.160E+OO 110.62 OK RA-226 609.32 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 OK 1120.29 14.92 1.644E+OO 1.366E+OO 1.366E+OO 33.69 OK 1764.49 15.30 1.121E+OO 7.769E-01 7. 771E-01 59.97 OK AC-228 105.21 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114. 53 OK 338.32 11. 27 4.178E+00 1.494E+OO 1.494E+OO 28.78 OK 794.95 4.25 2.197E+OO l.980E+00 1. 980E+00 52.41 OK 835.71 1. 61 2.109E+00 Line Not Found Absent 911.20 25.80* 1. 962E+00 1.298E+OO 1.298E+OO 26.93 OK 968. 97 15.80 1.863E+OO 9.990E-01 9.990E-01 47.84 OK RA-228 105.21 1.10 7.284E+OO 3.267E+OO 3.267E+00 114. 53 OK 338.32 11. 27 4.178E+OO 1. 494E+00 1.494E+OO 28.78 OK 794.95 4.25 2.197E+OO 1.980E+OO 1.980E+OO 52.41 OK 835. 71 1. 61 2.109E+OO Line Not Found Absent 911. 20 25.80* 1. 962E+OO l.298E+OO l.298E+OO 26.93 OK 968.97 15.80 l.863E+00 9.990E-01 9.990E-01 47.84 OK TH-228 74.82 10.28 5.441E+OO 1.291E+OO 1.291E+OO 49.80 OK 77.11 17.10 5.693E+00 1.928E+00 1.928E+OO 18.63 OK 238.63 43.60* 5.356E+OO 1.449E+OO 1.449E+OO 10.08 OK 300.09 3.30 4.554E+OO 1.169E+OO 1.169E+OO 109.89 OK Page 2933 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235002 Acquisition date 3-0CT-2016 07:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 2.707E+OO 9.149E-01 9.149E-01 19 .. 80 OK 1120.29 14.92 1.644E+OO l.366E+OO 1.366E+OO 33.69 OK 1764.49 15.30 1.121E+OO 7.769E-01 7.769E-01 59.97 OK PA-231 283.69 1. 70 4.743E+OO Line Not Found Absent 301.36 5.35* 4.554E+OO 7. 211E-01 7. 211E-01 109.89 OK TH-232 105.21 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114. 53 OK 338.32 11. 27 4.178E+OO l.494E+OO l.494E+OO 28.78 OK 835. 71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1. 962E+OO 1.298E+OO 1.298E+OO 26.93 OK 968.97 15.80 1.863E+OO 9.990E-01 9.990E-01 47.84 OK TH-234 63.29 3.70* 3.867E+OO 7.801E-01 7.801E-01 244.55 OK 92.59 4.23 6.868E+OO 2.155E+OO 2.155E+OO 51. 86 OK U-234 609.32 45.49* 2.707E+OO 9.149E-01 9.149E-01 19.80 OK 1120.29 14.92 1.644E+OO 1.366E+00 1.366E+OO 33.69 OK 1764.49 15.30 1.121E+OO 7.769E-01 7.769E-01 59.97 OK U-235 89. 96 3.47 6.713E+OO 1.893E+OO 1.893E+OO 60.80 OK 93.35 5.60 6.868E+OO 1.628E+OO 1.628E+OO 51. 86 OK 143.76 10. 96* 7 .121E+OO Line Not Found Absent 163.33 5.08 6.750E+OO Line Not Found Absent 185. 72 57.20 6.287E+OO l.577E-01 1.577E-01 69.06 OK 205.31 5.01 5.922E+OO Line Not Found Absent U-238 63.29 3.70* 3.867E+OO 7. 801E-01 7. 801E-01 244.55 OK 92.59 4.23 6.868E+OO 2.155E+OO 2.155E+OO 51. 86 OK AM-243 43.53 5.90 8.765E-01 Line Not Found Absent 74.66 67.20* 5. 441E+OO 1. 975E-01 1.975E-01 49.80 OK CF-249 252.80 2.50 5.147E+OO Line Not Found Absent 333.37 14.60 4.223E+OO Line Not Found Absent 388.16 66.00* 3.787E+OO 4.741E-02 4.748E-02 146.17 OK ANH-511 511. 00 100.00* 3.091E+OO 6.875E-02 6.875E-02 121. 32 OK Flag: "*" = Keyline Page 2934 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:58:51.71 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l *
  • Acquisition date 3-0CT-2016 07:57:26 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:30:00 Analyst initials: MXRl *
  • Sample ID G405235002 Sample Quantity 1.2384E+02 GRAM * **Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 784E+Ol 1. 782E+OO ZN-65 1. 7 92E-01 2.747E-01 CD-109 2.183E+OO 1.973E+OO SN-126 l.395E-01 1.262E-01 BA-137M 1.178E-01 8.354E-02 CS-137 1. 245E-01 8.825E-02 EU-155 1.918E-01 2.153E-01 TL-208 2.485E-01 6.732E-02 PB-212 1.449E+OO 1. 431E-01 BI-214 9.152E-01 1. 775E-01 PB-214 1.120E+OO 2.068E-01 RN-222 9.152E-01 1.775E-01 RA-224 1.160E+OO 1.258E+OO RA-226 9.152E-01 1.775E-01 AC-228 1.298E+OO 3.426E-01 RA-228 1.298E+OO 3.426E-01 TH-228 1.449E+OO 1. 431E-01 TH-230 9.149E-01 1.775E-01 PA-231 7. 211E-01 7.766E-01 TH-232 1. 2 98E+00 3.426E-01 TH-234 7.801E-01 1.870E+OO U-234 9.149E-01 1.775E-01 U-235 5.447E-02 1. 765E-01 U-238 7.801E-01 1.870E+OO AM-243 1. 975E-01 9.638E-02 CF-249 4.748E-02 6.802E-02 ANH-511 6.875E-02 8.174E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 2935 of 5809 Key-Line Activity (pCi/GRAM -5.252E+OO 2.002E-02 O.OOOE+OO K.L. Cnt Uncert (1.96-sigma) 1.101E+Ol 4.927E-02 1.960E+41 MDA (pCi/GRAM 6.674E-01 2.520E-01 1. 831E+OO l.176E-01 5.633E-02 5. 951E-02 1.766E-01 6.449E-02 9.642E-02 8.187E-02 1.155E-01 8.187E-02 1.033E+OO 8.187E-02 2.069E-01 2.069E-01 9.642E-02 8.184E-02 8.034E-01 2.069E-01 l.939E+OO 8.184E-02 3.287E-01 1.939E+OO 7.383E-02 6.705E-02 4.622E-02 MDA (pCi/GRAM 1.916E+Ol 1.049E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 1.369E-03 2.682E-02 6. 071E-02 NOT IDENT. SC-46 1.978E-01 3.668E-01 7. 672E-01 FAIL ABUN V-48 O.OOOE+OO l.554E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.903E+02 O.OOOE+OO SHORT HLIF MN-54 5.343E-02 6.886E-02 l.437E-01 NOT IDENT. C0-56 2.914E-01 4.921E-01 9.506E-01 FAIL ABUN MN-56 O.OOOE+OO 1.689E+41 O.OOOE+OO SHORT HLIF C0-57 -5.272E-02 4. 967E-02 8.267E-02 NOT IDENT. C0-58 -2.314E-01 4.909E-01 8.752E-01 NOT IDENT. FE-:-59 4.032E+OO 6.865E+OO 1.428E+Ol NOT IDENT. C0-60 -1.437E-02 4.976E-02 9.113E-02 NOT IDENT. GE-68 -2.439E+OO 2.787E+OO 4.454E+OO NOT IDENT. AS-73 3.034E+OO 7.472E+OO 1.464E+Ol NOT IDENT. AS-74 O.OOOE+OO 5. 971E+03 O.OOOE+OO SHORT HLIF SE-75 5.062E-02 2.085E-01 3.827E-01 NOT IDENT. BR-77 O.OOOE+OO 1.395E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6. 441E+02 O.OOOE+OO SHORT HLIF RB-83 -1.0lOE-01 7.256E-01 1.230E+OO NOT IDENT. KR-85 1.877E+OO 6.059E+OO 1.224E+Ol NOT IDENT. SR-85 1.922E-01 6.260E-01 1. 2 65E+OO NOT IDENT. RB-86 O.OOOE+OO 3.177E+04 O.OOOE+OO SHORT HLIF Y-88 -7.362E-02 1.373E-01 2.849E-01 NOT IDENT. Y-91 2.211E+Ol 5.808E+02 l.084E+03 NOT IDENT. NB-94 -3.826E-03 3. 251E-02 6.065E-02 NOT IDENT. NB-95 -1.197E+OO 9.999E-01 1. 569E+OO NOT IDENT. NB-95M 1. 723E+OO 2.489E+00 4.477E+OO NOT IDENT. ZR-95 9.690E-01 1.418E+OO 2.980E+OO NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT'HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.281E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 -1.948E-02 3.571E-02 6.210E-02 NOT IDENT. RH-102 4.200E-02 5.459E-02 l.172E-01 NOT IDENT. RU-103 3.008E+OO 5.206E+OO 1.083E+Ol FAIL ABUN RH-106 3.384E-01 4.781E-01 1. OllE+OO NOT IDENT. RU-106 3.384E-01 4.781E-01 1. OllE+OO NOT IDENT. AG-108M 4.739E-02 3.046E-02 4.786E-02 FAIL ABUN AG-llOM -8.785E-02 9.486E-02 1.497E-01 NOT IDENT. SN-113 4.570E-02 2.014E-01 4.059E-01 NOT IDENT. CD-115 O.OOOE+OO 1.549E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 8.813E+04 0.000E+OO SHORT HLIF TE-123M 8.256E-02 1.258E-01 2.419E-01 NOT IDENT. SB-124 -7.328E-01 2.022E+OO 3.914E+OO NOT IDENT. SB-125 4.379E-02 l.152E-01 2 .117E-01 FAIL ABUN TE-125M 8.068E-01 2.778E+02 4.673E+02 NOT IDENT. I-126 O.OOOE+OO 1.080E+06 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO 1.004E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.524E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.394E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 5.620E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.627E+26 O.OOOE+OO SHORT HLIF BA-133 -3.670E-03 4. 171E-02 7.281E-02 NOT IDENT. I-133 O.OOOE+OO 1.130E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 6.647E-02 1.205E-01 FAIL ABUN CS-135 4.649E-02 1.530E-01 2.611E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.317E+05 O.OOOE+OO SHORT HLIF CE-139 1.710E-03 1.169E-01 2.107E-01 NOT IDENT. BA-140 O.OOOE+OO 1.067E+06 0.000E+OO SHORT HLIF LA-140 0.000E+OO 4.015E+05 O.OOOE+OO SHORT HLIF CE-141 -5.014E+OO 2.309E+Ol 4. lllE+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 665E+41 0.000E+OO SHORT HLIF CE-144 9.386E-03 3.450E-01 6.333E-01 NOT IDENT. PM-144 2.222E-03 5.523E-02 1. 084E-01 NOT IDENT. PR-144 1. 775E-01 4.789E+OO 9.394E+OO NOT IDENT. PM-146 4.628E-02 4.510E-02 9.611E-02 FAIL ABUN ND-147 O.OOOE+OO 2.628E+07 O.OOOE+OO SHORT HLIF PM-147 l.446E+03 7.769E+02 l.641E+03 NOT IDENT. PM-149 O.OOOE+OO 2.674E+40 O.OOOE+OO SHORT HLIF EU-150 1.870E-02 3.044E-02 5.659E-02 FAIL ABUN EU-152 -1. 7 98E-03 9.207E-02 l.629E-01 FAIL ABUN GD-153 -6.544E-02 l.732E-01 2.840E-01 NOT IDENT. EU-154 4.660E-02 l.204E-01 2.560E-01 NOT IDENT. TB-160 -3.604E-02 2.009E+OO 3.794E+OO FAIL ABUN H0-166M 8.084E-03 5.809E-02 1.129E-01 NOT IDENT. TM-171 -2.052E-01 1. 746E+Ol 3.327E+Ol NOT IDENT. HF-172 1. 331E-01 2.256E-01 4.322E-01 FAIL ABUN LU-172 3.109E-02 7.343E-02 1.518E-01 FAIL ABUN Page 2936 of 5809 LU-176 -3.930E-03 2.940E-02 4.668E-02 FAIL ABUN HF-181 1.039E+OO 3.943E+OO 7.927E+OO NOT IDENT. TA-182 2.800E-02 9.320E-01 1.866E+00 FAIL ABUN RE-183 -9.476E-02 2.642E+OO 4.972E+OO NOT IDENT. RE-184 -2.167E+OO 2.852E+Ol 5. 396E+Ol NOT IDENT. W-188 5.014E+Ol 1. 2 68E+02 2.174E+02 FAIL ABUN IR-192 -l.458E-02 4.490E-01 8.747E-01 FAIL ABUN HG-203 -1.183E+OO 2.437E+OO 4.072E+OO FAIL ABUN BI-207 1.742E-02 4.722E-02 9.617E-02 FAIL ABUN PB-210 3.524E_:Ol 2.359E+OO 4.605E+OO NOT IDENT. BI-211 O.OOOE+OO 5.695E-01 8.315E-01 FAIL ABUN PB-211 4.493E-01 6.822E-01 l.403E+OO NOT IDENT. BI-212 O.OOOE+OO 8 .115E-01 1.330E+OO FAIL ABUN RN-219 -6.924E-02 3.679E-01 7.015E-01 FAIL ABUN RA-223 4.601E-02 6.537E-01 1.159E+OO FAIL ABUN AC-227 l.881E-02 2.380E-01 4.276E-01 FAIL ABUN TH-227 1. 881E-02 2.380E-01 4.276E-01 FAIL ABUN TH-229 2.042E-01 4.583E-01 8.605E-01 FAIL ABUN TH-231 4.601E-02 6.537E-01 1.159E+OO FAIL ABUN PA-233 -1.265E-02 5.819E-02 l .116E-01 FAIL ABUN PA-234 9. 521E-03 2.502E-01 4.885E-01 NOT IDENT. PA-234M -2.099E+OO 4.725E+OO 8.194E+OO NOT IDENT. NP-237 -1.265E-02 5.819E-02 1.116E-01 FAIL ABUN NP-238 O.OOOE+OO 1.097E+41 O.OOOE+OO SHORT HLIF NP-239 5.193E-03 2.345E-01 4.312E-01 FAIL ABUN PU-239 3.268E+02 3.267E+02 6.386E+02 NOT IDENT. AM-241 5.439E-02 1.330E-01 2.406E-01 NOT IDENT. CM-243 -1.163E-02' 9. 611E-02 1.625E-01 NOT IDENT. BK-247 -1.203E-02 7.576E-02 l.324E-01 FAIL ABUN CM-247 -5.026E-03 3.442E-02 6.584E-02 NOT IDENT. CF-251 -1.778E-01 l.232E-01 1.907E-01 NOT IDENT. Page 2937 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:58:48.94 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Ef f pCi/GRAM pCi/GRAM %Error K-40 1460.82 410 10.66* 1.307E+OO 1. 784E+01 1. 784E+Ol 10.20 ZN-65 1115. 54 11 50.60* 1.652E+OO 7.695E-02 1. 792E-01 156.41 CD-109 88.03 106 3.70* 6.548E+OO 2.662E+OO 4.163E+OO 47.48 SN-126 64.28 18 9.60 3.867E+OO 3.007E-01 3.007E-01 244.55 86.94 106 8.90 6.548E+OO 1.107E+OO 1.107E+OO 47.48 87.57 106 37.00* 6.548E+OO 2.662E-01 2.662E-01 47.48 BA-137M 661. 66 44 89.90* 2.546E+OO 1.156E-01 1.178E-01 72. 35 CS-137 661. 66 44 85.10* 2.546E+OO 1.222E-01 1.245E-01 72.35 EU-155 86.55 106 30.70 6.548E+OO 3.208E-01 3. 613E-01 47.48 105.31 43 21.10* 7.284E+OO 1.703E-01 1.918E-01 114. 53 TL-208 277.37 ------6.60 4.820E+OO ------Line Not Found ------583.19 98 85.00* 2.799E+OO 2.485E-01 2.485E-01 27.65 860.56 36 12.50 2.059E+00 8.550E-01 8.550E-01 52.88 BI-211 72.87 41 1. 23 5.224E+OO 3.913E+OO 3.913E+OO 130.26 351.06 267 12.92* 4.058E+OO 3.084E+OO 3.084E+00 18.84 PB-212 74.82 191 10.28 5. 441E+OO 2.066E+OO 2.066E+OO 30.27 77 .11 310 17.10 5.693E+OO 1.928E+OO 1.928E+OO 18.63 238.63 558 43.60* 5.356E+OO 1.449E+OO l.449E+OO 10.08 300.09 29 3.30 4.554E+OO 1.169E+OO 1.169E+OO 109.89 BI-214 609.32 186 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 1120.29 55 14.92 1.644E+OO 1. 366E+OO 1.366E+00 33.69 1764.49 22 15.30 1.121E+OO 7.769E-01 7.771E-01 59.97 PB-214 74.82 191 5. 80 5.441E+OO 3.662E+OO 3.663E+OO 30.27 77 .11 310 9.70 5.693E+OO 3.400E+OO 3.401E+OO 18.63 87.09 106 3.41 6.548E+OO 2.888E+OO 2.889E+OO 47.48 242.00 129 7.25 5.307E+OO 2.030E+00 2.031E+OO 33.30 295.22 192 18.42 4.609E+OO 1.374E+OO 1. 375E+00 19.23 351. 93 267 35.60* 4.058E+OO 1.119E+OO l.120E+00 18.84 RN-222 609.32 186 45.49* 2.707E+00 9.149E-01 9.152E-01 19.80 1120.29 55 14.92 l.644E+OO 1.366E+OO 1.366E+OO 33.69 1764.49 22 15.30 1.121E+OO 7.769E-01 7. 771E-01 59.97 RA-224 240.99 129 4.10* 5.307E+OO 3.590E+OO 3.590E+OO 33.30 RA-226 609.32 186 45.49* 2.707E+OO 9.149E-01 9.152E-01 19.80 1120.29 55 14.92 l.644E+OO 1.366E+OO 1.366E+OO 33.69 1764.49 22 15.30 1.121E+OO 7.769E-01 7.771E-01 59.97 AC-228 105.21 43 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114.53 338.32 116 11.27 4.178E+OO 1.494E+OO 1.494E+OO 28.78 794.95 31 4.25 2.197E+OO 1.980E+OO 1.980E+OO 52.41 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911.20 108 25.80* 1. 962E+OO 1.298E+OO l.298E+00 26. 93 968.97 49 15.80 l.863E+OO 9.990E-01 9.990E-01 47.84 RA-228 105.21 43 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114.53 338.32 116 11.27 4.178E+OO 1.494E+00 1.494E+OO 28.78 794.95 31 4.25 2.197E+OO l.980E+OO 1.980E+OO 52.41 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911. 20 108 25,.80* 1. 962E+OO 1.298E+OO 1.298E+OO 26.93 968.97 49 15.80 1.863E+OO 9.990E-01 9.990E-01 47.84 Page 2938of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235002 Acquisition date 3-0CT-2016 07:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 191 10 .. 28 5.441E+OO 2.066E+OO 2.066E+OO 30 .. 27 77 .11 310 17.10 5.693E+OO 1.928E+OO 1.928E+OO 18.63 238.63 558 43.60* 5.356E+OO 1.449E+OO 1.449E+OO 10.08 300.09 29 3.30 4.554E+OO 1.169E+OO l.169E+OO 109.89 TH-230 609.32 186 45.49* 2.707E+OO 9.149E-01 9.149E-01 19.80 1120.29 55 14.92 1.644E+OO 1.366E+OO 1.366E+OO 33.69 1764.49 22 15.30 1.121E+OO 7.769E-01 7.769E-01 59.97 PA-231 283.69 ------1. 70 4.743E+OO ------Line Not Found ------301.36 29 5.35* 4.554E+00 7. 211E-01 7.211E-01 109.89 TH-232 105.21 43 1.10 7.284E+OO 3.267E+OO 3.267E+OO 114. 53 338.32 116 11.27 4.178E+OO 1.494E+OO 1.494E+OO 28.78 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911. 20 108 25.80* 1. 962E+OO 1.298E+OO 1.298E+OO 26.93 968. 97 49 15.80 1. 863E+OO 9.990E-01 9.990E-01 47.84 TH-234 63.29 18 3.70* 3.867E+OO 7. 801E-01 7.801E-01 244.55 92.59 103 4.23 6.868E+OO 2.155E+OO 2.155E+OO 51. 86 U-234 *609.32 186 45.49* 2.707E+OO 9.149E-01 9.149E-01 19.80 1120.29 55 14.92 1.644E+OO 1.366E+OO 1.366E+OO 33.69 1764.49 22 15.30 l.121E+OO 7.769E-01 7.769E-01 59.97 U-235 89. 96 73 3.47 6.713E+OO 1.893E+OO 1.893E+OO 60.80 93.35 103 5.60 6.868E+OO 1. 628E+OO 1.628E+OO 51. 86 143.76 ------10.96* 7 .121E+OO ------Line Not Found ------163.33 ------5.08 6.750E+OO ------Line Not Found ------185. 72 94 57.20 6.287E+00 1.577E-01 1.577E-01 69.06 205.31 ------5.01 5.922E+OO ------Line Not Found ------U-238 63.29 18 3.70* 3.867E+OO 7.801E-01 7. 801E-01 244.55 92.59 103 4.23 6.868E+OO 2.155E+OO 2.155E+OO 51. 86 AM-243 43.53 ------5.90 8.765E-01 ------Line Not Found ------74.66 191 67.20* 5.441E+OO 3.161E-01 3.161E-01 30.27 CF-249 252.80 ------2.50 5.147E+OO ------Line Not Found ------333.37 ------14.60 4.223E+OO ------Line Not Found ------388.16 20 66.00* 3.787E+OO 4.741E-02 4.748E-02 146.17 ANH-511 511. 00 35 100.00* 3.091E+OO 6.875E-02 6.875E-02 121. 32 Flag: "*" Key line Page 2939 of 5809 Summary of Nuclide Activity Sample ID : G405235002 Acquisition date Page : 3 3-0CT-2016 07:57:26 Total number of lines in spectrum 55 Number of unidentified lines 17 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CF-249 ANH-511 Hlife l.25E+09Y 244.06D 461. 40D 2.30E+05Y 30.08Y 30.08Y 4.75Y l.41E+10Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+l0Y 1600.00Y 1. 41E+l0Y 1. 41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 351.00Y l.00E+09Y Decay 1. 00 2.33 1. 56 1. 00 1. 02 1. 02 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 784E+Ol 7.695E-02 2.662E+OO 2.662E-01 l.156E-01 l.222E-01 l.703E-01 2.485E-01 3.084E+OO 1. 449E+OO 9.149E-01 l .119E+OO 9.149E-01 3.590E+OO 9.149E-01 1. 298E+OO 1.298E+OO 1.449E+OO 9.149E-01 7.211E-01 l.298E+00 7. 801E-01 9.149E-01 1.577E-01 7.801E-01 3.161E-01 4.741E-02 6.875E-02 4.353E+Ol 4.353E+Ol Decay Corr pCi7GRAM 1.784E+Ol 1. 792E-01 4.163E+OO 2.662E-01 1.178E-01 l.245E-01 l.918E-01 2.485E-01 3.084E+OO 1. 449E+OO 9.152E-01 l.120E+00 9.152E-01 3.590E+OO 9.152E-01 1.298E+OO 1.298E+OO l.449E+OO 9.149E-01 7. 211E-01 1.298E+OO 7.801E-01 9.149E-01 l.577E-01 7. 801E-01 3 .161E-01 4.748E-02 6.875E-02 4.516E+Ol 4.516E+Ol 69.09% Decay Corr 2-Sigma Error 0.182E+Ol 2.803E-01 l.977E+OO l.264E-01 0.852E-01 0. 901E-01 2.197E-01 0.687E-01 0.581E+OO 0.146E+00 l.812E-01 0. 211E+OO 1.812E-01 1.195E+00 1.812E-01 0.350E+OO 0.350E+OO 0.146E+OO 1. 811E-01 7.924E-01 0.350E+OO 19.08E-01 1.811E-01 l.089E-01 19.08E-01 0.957E-01 6.941E-02 8. 341E-02 "M" Manually accepted 2-Sigma %Error 10.20 156.41 47.48 47.48 72. 35 72.35 114. 53 27.65 18.84 10.08 19.80 18.84 19.80 33.30 19.80 26.93 26. 93 10.08 19.80 109.89 26.93 244.55 19.80 69.06 244.55 30.27 146.17 121.32 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 2940 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235002 Acquisition date : 3-0CT-2016 07:57:26 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.30 53 94 1. 00 418.34 415 8 l.37E-02 71. 6 5.85E+OO 0 270.44 45 121 1. 50 540.64 536 13 l.20E-02 **** 4.91E+OO T 0 331. 76 86 100 7.88 663.28 652 20 2.32E-02 62.8 4.24E+OO 2 341.35 22 53 1. 54 682.46 672 21 6.02E-03 **** 4.15E+OO T 5 430.57 15 8 1. 54 860.93 859 11 4.04E-03 64.4 3. 51E+OO 5 433.18 25 9 1. 64 866.14 859 11 6. 72E-03 65.6 3.49E+00 T 2 463.17 38 20 1. 65 926.14 919 31 1. 05E-02 59.6 3.32E+OO T 2 466.96 15 18 1. 50 933.73 919 31 3.98E-03 **** 3.30E+OO T 0 524.39 15 27 1. 69 1048.59 1041 10 4.07E-03 **** 3.03E+OO 3 587.03 15 12 1. 92 1173.92 1162 15 4. llE-03 85.8 2.79E+OO 0 639.66 25 28 3.74 1279.20 1271 14 7.02E-03 97.2 2. 61E+OO 0 666.48 31 12 0.67 1332.84 1328 12 8.61E-03 57.3 2.53E+OO T 0 727. 68 57 12 2.21 1455.27 1448 16 l.60E-02 37.7 2.36E+OO T 0 737.36 15 15 0.78 1474.65 1471 7 4.27E-03 99.5 2.33E+OO T 0 851. 32 14 2 0.66 1702.64 1699 8 3.98E-03 62.5 2.08E+OO 0 935.80 26 3 2.68 1871. 64 1867 10 7. 31E-03 45.1 l.92E+OO 5 964. 58 22 31 2.64 1929.22 1921 27 6.24E-03 **** l.87E+00 T 0 1065.20 7 13 0.77 2130.55 2124 11 2.lOE-03 **** 1. 72E+OO 0 1167. 01 18 19 5. 96 2334.25 2325 16 5.34E-03 **** 1. 59E+OO 0 1212.44 9 13 0.66 2425.14 2420 7 2.59E-03 **** l.54E+OO 0 1238.24 20 11 1. 35 2476.76 2469 12 5.83E-03 79.1 l.51E+OO T 0 1328.10 6 5 1. 03 '2656.58 2652 7 1. 64E-03 **** l.42E+OO 0 1378.05 15 2 1. 36 2756.53 2751 10 4.37E-03 62. 6 l.37E+OO 0 1393.55 4 4 1. 41 2787.55 2781 8 l.16E-03 **** l.36E+OO 0 1430.88 6 5 1. 40 2862.25 2855 10 1. 67E-03 **** 1. 33E+OO 0 1547.80 9 0 0.88 3096. 22 3091 10 2.50E-03 66.7 l.25E+OO 0 1731.15 6 5 0.77 3463.13 3455 10 1. 92E-03 **** 1.14E+OO Flags: "T" = Tentatively associated Page 2941of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:59:09.04 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l *
  • Acquisition date 3-0CT-2016 07:57:26 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:30:00 Nuclide Library : SOLID *
  • Sample ID G405235002 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.2384E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 11-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.'CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CF-249 ANH-511 Le (pCi/GRAM 2.750E-01 1. 031E-01 8.616E-01 5.532E-02 2.448E-02 2.586E-02 8.214E-02 2.877E-02 4.464E-02 3.421E-02 5.198E-02 3.421E-02 4.783E-01 3. 421E-02 8.719E-02 8.719E-02 4.464E-02 3.420E-02 3.674E-01 8.719E-02 9.105E-01 3.420E-02 1.536E-01 9.105E-01 3.459E-02 3.019E-02 2.043E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 2942 of 5809 Le (pCi/GRAM 8. 396E+OO 4.554E-02 O.OOOE+OO 2.292E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 co-56 MN-56 C0-57 C0-58 FE-59 C0-60 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 2943 of 5809 3.354E-01 O.OOOE+OO O.OOOE+OO 6.429E-02 4.182E-01 O.OOOE+OO 3.849E-02 3.670E-01 6.244E+OO 3.912E-02 1.906E+OO 6.849E+OO O.OOOE+OO 1. 754E-01 O.OOOE+OO 0.000E+OO 5.487E-01 5.468E+OO 5.647E-01 O.OOOE+OO 9.004E-02 4.726E+02 2.692E-02 6. 931E-01 2.082E+OO 1.323E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.905E-02 5.209E-02 4.862E+OO 4.509E-01 4.509E-01 2.129E-02 6.200E-02 1.825E-01 O.OOOE+OO O.OOOE+OO 1.127E-01 1.500E+OO 9.613E-02 2.182E+02 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.289E-02 O.OOOE+OO 5.451E-02 1.200E-01 O.OOOE+OO O.OOOE+OO 9.837E-02 O.OOOE+OO O.OOOE+OO 1.916E+01 O.OOOE+OO 2.951E-01 4.818E-02 4.177E+OO 4.387E-02 O.OOOE+OO 7.709E+02 O.OOOE+OO 2.621E-02 7.356E-02 1.323E-01 1. llOE-01 1.662E+00 5. OllE-02 1.549E+01 2.024E-01 6.539E-02 2 .136E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-251 Page 2944 of 5809 3.548E+OO 8.122E-01 2. 331E+OO 2.326E+Ol l.002E+02 3.998E-01 1.857E+OO 4.158E-02 2.139E+OO 4.00lE-01 6.414E-01 6.129E-01 3.167E-01 5.309E-01 1. 966E-01 1. 966E-01 3.994E-01 5.309E-01 5.091E-02 2.082E-01 3.558E+OO 5.091E-02 O.OOOE+OO 2.012E-01 3.012E+02 l.131E-01 7.556E-02 6.059E-02 2.979E-02 8.784E-02 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:59:18.87 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235002.CNF;l *
  • Acquisition date 3-0CT-2016 07:57:26 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:30:00 Nuclide Library : SOLID *
  • Sample ID G405235002 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.2384E+02 GRAM *
  • Quantity Err(%) : 1.6150E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) K-40 1. 784E+Ol 2.389E+OO 2.389E+OO ZN-65 l.792E-01 2.770E-01 2.770E-01 CD-109 2.183E+OO 2.007E+OO 2.007E+OO SN-126 l.395E-01 1.281E-01 1. 281E-01 BA-137M l.178E-01 8.405E-02 8.405E-02 CS-137 1.245E-01 8.879E-02 8.879E-02 EU-155 1.918E-01 2.159E-01 2.159E-01 TL-208 2.485E-01 7.033E-02 7.033E-02 PB-212 1.449E+OO 1.858E-01 1.858E-01 BI-214 9.152E-01 1.924E-01 1.924E-01 PB-214 1.120E+OO 2.265E-01 2.265E-01 RN-222 9.152E-01 1.924E-01 l.924E-01 RA-224 1.160E+OO 1. 292E+OO l.292E+OO RA-226 9.152E-01 1.924E-01 l.924E-01 AC-228 1.298E+OO 3.876E-01 3.876E-01 RA-228 1.298E+OO 3.876E-01 3.876E-01 TH-228 1.449E+OO 1.858E-01 1.858E-01 TH-230 9.149E-01 1.923E-01 1.923E-01 PA-231 7.211E-01 7.933E-01 7.933E-01 TH-232 1.298E+OO 3.876E-01 3.876E-01 TH-234 7.801E-01 1. 878E+OO l.878E+00 U-234 9.149E-01 1.923E-01 l.923E-01 U-235 5.447E-02 1. 765E-01 l.765E-01 U-238 7. 801E-01 1. 878E+OO 1.878E+OO AM-243 1. 975E-01 9. 910E-02' 9.910E-02 CF-249 4.748E-02 6.821E-02 6.821E-02 ANH-511 6.875E-02 8.194E-02 8.194E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -5.252E+00 1.102E+Ol l.127E+Ol NOT IDENT. NA-22 2.002E-02 4.930E-02 5.012E-02 NOT IDENT. NA-24 1.000E+41 1. 285E+42 O.OOOE+OO SHORT HLIF Page 2945 of 5809 AL-26 1.369E-03 2.682E-02 2.683E-02 NOT IDENT. SC-46 l.978E-01 3.677E-01 3.784E-01 FAIL ABUN V-48 1. 221E+04 1. 565E+04 l.659E+04 SHORT HLIF CR-51 -2.639E+02 3.909E+02 4.086E+02 SHORT HLIF MN-54 5.343E-02 6.914E-02 7.322E-02 NOT IDENT. C0-56 2.914E-01 4.934E-01 5.106E-01 FAIL ABUN MN-56 l.000E+41 l.693E+41 O.OOOE+OO SHORT HLIF C0-57 -5. 272E-02 4. 981E-02 5.519E-02 NOT IDENT. C0-58 -2.314E-01 4.916E-01 5.025E-01 NOT IDENT. FE-59 4.032E+OO 6.914E+OO 7 .148E+OO NOT IDENT. C0-60 -l.437E-02 4.977E-02 5.019E-02 NOT IDENT. GE-68 -2.439E+OO 2.823E+OO 3.030E+OO NOT IDENT. AS-73 3.034E+OO 7.498E+OO 7.622E+OO NOT IDENT. AS-74 -2.159E+02 5. 971E+03 5.972E+03 SHORT HLIF SE-75 5.062E-02 2.085E-01 2.098E-01 NOT IDENT. BR-77 l.412E+38 l.214E+39 O.OOOE+OO SHORT HLIF SR-82 l.989E+02 6.444E+02 6.506E+02 SHORT HLIF RB-83 -l.OlOE-01 7.257E-01 7.272E-01 NOT IDENT. KR-85 l.877E+OO 6.061E+OO 6.120E+OO NOT IDENT. SR-85 l.922E-01 6.262E-01 6.321E-01 NOT IDENT. RB-86 -2.369E+04 3.208E+04 3.381E+04 SHORT HLIF Y-88 -7.362E-02 1. 374E-01 l.414E-01 NOT IDENT. Y-91 2. 211E+Ol 5.808E+02 5.809E+02 NOT IDENT. NB-94 -3.826E-03 3.251E-02 3.256E-02 NOT IDENT. NB-95 -1.197E+OO 1.007E+OO 1.143E+OO NOT IDENT. NB-95M 1.723E+OO 2.495E+OO 2. 613E+OO NOT IDENT. ZR-95 9.690E-01 1. 421E+OO 1.487E+OO NOT IDENT. NB-97 1.000E+41 6.207E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 l.229E+42 0.000E+OO SHORT HLIF M0-99 -4.789E+31 l.282E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.414E+42 O.OOOE+OO SHORT HLIF RH-101 -1.948E-02 3.590E-02 3. 696E-02 NOT IDENT. RH-102 4.200E-02 5.477E-02 5.795E-02 NOT IDENT. RU-103 3.008E+OO 5.212E+OO 5.386E+OO FAIL ABUN RH-106 3.384E-01 4. 791E-01 5.028E-01 NOT IDENT. RU-106 3.384E-01 4.791E-01 5.028E-01 NOT IDENT. AG-108M 4.739E-02 3.071E-02 3.741E-02 FAIL ABUN AG-llOM -8.785E-02 9.557E-02 1.035E-01 NOT IDENT. SN-113 4.570E-02 2.014E-01 2.025E-01 NOT IDENT. CD-115 l.004E+39 l.561E+39 O.OOOE+OO SHORT HLIF SN-117M 6.973E+03 8.814E+04 8.819E+04 SHORT HLIF TE-123M 8.256E-02 1. 259E-01 1.313E-01 NOT IDENT. SB-124 -7.328E-01 2.023E+OO 2.049E+OO NOT IDENT. SB-125 4.379E-02 l.153E-01 1.170E-01 FAIL ABUN TE-125M 8.068E-01 2.778E+02 2.778E+02 NOT IDENT. I-126 1. 922E+06 l.118E+06 l.414E+06 SHORT HLIF SB-126 8.688E+04 1. 004E+06 1.005E+06 SHORT HLIF SB-127 -3. 331E+21 1.591E+22 O.OOOE+OO SHORT HLIF I-131 3.100E+09 4.402E+09 4.618E+09 SHORT HLIF I-132 1. OOOE+41 l.836E+42 O.OOOE+OO SHORT HLIF TE-132 1. 363E+26 2.685E+26 O.OOOE+OO SHORT HLIF BA-133 -3.670E-03 4.171E-02 4.174E-02 NOT IDENT. I-133 -1.000E+41 2.124E+41 O.OOOE+OO SHORT HLIF CS-134 1. 294E-01 6.790E-02 8. 951E-02 FAIL ABUN CS-135 4.649E-02 1.530E-01 1.545E-01 NOT IDENT. I-135 -1.000E+41 2.665E+42 O.OOOE+OO SHORT HLIF CS-136 1.536E+04 3.317E+05 3.317E+05 SHORT HLIF CE-139 l.710E-03 l.169E-01 1.169E-01 NOT IDENT. BA-140 -7.668E+05 1.069E+06 1.124E+06 SHORT HLIF LA-140 -1. 875E+05 4.018E+05 4.106E+05 SHORT HLIF CE-141 -5.014E+OO 2.309E+Ol 2.320E+Ol NOT IDENT. CE-143 1.000E+41 1.669E+41 O.OOOE+OO SHORT HLIF CE-144 9.386E-03 3.450E-01 3.450E-01 NOT IDENT. PM-144 2.222E-03 5.523E-02 5.524E-02 NOT IDENT. PR-144 1.775E-01 4.790E+OO 4.790E+OO NOT IDENT. PM-146 4.534E-02 4.991E-02 FAIL ABUN ND-147 -9.633E+06 2.629E+07 2.665E+07 SHORT HLIF PM-147 l.446E+03 7.833E+02 l.019E+03 NOT IDENT. PM-149 -3.778E+39 2.675E+40 O.OOOE+OO SHORT HLIF EU-150 l.870E-02 3.048E-02 3.163E-02 FAIL ABUN EU-152 -1.798E-03 9.207E-02 9.208E-02 FAIL ABUN GD-153 -6.544E-02 1.733E-01 1. 758E-01 NOT IDENT. EU-154 4.660E-02 l.205E-01 l.223E-01 NOT IDENT. TB-160 -3.604E-02 2.009E+OO 2.009E+OO FAIL ABUN H0-166M 8.084E-03 5.809E-02 5.821E-02 NOT IDENT. TM-171 -2.052E-01 1.746E+Ol 1. 746E+Ol NOT IDENT. HF-172 l.331E-01 2.268E-01 2.346E-01 FAIL ABUN LU-172 3.109E-02 7. 372E-02 7.504E-02 FAIL ABUN Page 2946 of 5809 LU-176 -3.930E-03 2.940E-02 2.945E-02 FAIL ABUN HF-181 1. 039E+OO 3.944E+OO 3. 972E+OO NOT IDENT. TA-182 2.800E-02 9.320E-01 9.321E-01 FAIL ABUN RE-183 -9.476E-02 2.642E+OO 2.642E+OO NOT IDENT. RE-184 -2.167E+OO 2.852E+Ol 2.854E+Ol NOT IDENT. W-188 5.014E+Ol l.270E+02 1.290E+02 FAIL ABUN IR-192 -1.458E-02 4.490E-01 4.491E-01 FAIL ABUN HG-203 -1.183E+OO 2.439E+OO 2. 496E+OO FAIL ABUN BI-207 1. 742E-02 4.733E-02 4.797E-02 FAIL ABUN PB-210 3.524E-01 2.359E+OO 2.364E+OO NOT IDENT. BI-211 3.084E+OO 6.258E-01 1.525E+OO FAIL ABUN PB-211 4.493E-01 6.833E-01 7.127E-01 NOT IDENT. BI-212 2.197E+OO 8.384E-01 1.298E+OO FAIL ABUN RN-219 -6.924E-02 3.680E-01 3.693E-01 FAIL ABUN RA-223 4. 601E-02 6.537E-01 6.540E-01 FAIL ABUN AC-227 1. 881E-02 2.380E-01 2.382E-01 FAIL ABUN TH-227 1. 881E-02 2.380E-01 2.382E-01 FAIL ABUN TH-229 2.042E-01 4.585E-01 4.677E-01 FAIL ABUN TH-231 4.601E-02 6.537E-01 6.540E-01 FAIL ABUN PA-233 -1.265E-02 5.820E-02 5.848E-02 FAIL ABUN PA-234 9.521E-03 2.505E-01 2.505E-01 NOT IDENT. PA-234M -2.099E+OO 4.737E+OO 4.831E+OO NOT IDENT. NP-237 -1.265E-02 5.820E-02 5.848E-02 FAIL ABUN NP-238 1.000E+41 l.108E+41 O.OOOE+OO SHORT HLIF NP-239 5.193E-03 2.345E-01 2.345E-01 FAIL ABUN PU-239 3.268E+02 3.275E+02 3.591E+02 NOT IDENT. AM-241 5.439E-02 1.330E-01 1.353E-01 NOT IDENT. CM-243 -1.163E-02 9.612E-02 9.626E-02 NOT IDENT. BK-247 -1.203E-02 7.580E-02 7.600E-02 FAIL ABUN CM-247 -5.026E-03 3.444E-02 3. 451E-02 NOT IDENT. CF-251 -1.778E-01 l.252E-01 1.486E-01 NOT IDENT. Page 294 7 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 37.0694 87.09 84.5633 136.47 56.9975 45.60 58.6698 87.57 84.6261 140.51 0.0000 46.54 47.5979 88.03 84.6864 143.76 55.3058 49.72 0.0000 88.34 84.7267 144.24 47.7410 51. 35 64.1478 88.47 84.7440 145.44 67.3612 51. 87 66.1086 89. 96 84.9376 152.43 78.8291 52.39 61.4550 1093.63 85.0254 153.25 0.0000 52.97 57.7443 91.11 0.0000 323.87 63.6234 53.44 61.5921 92.59 85.2760 156.02 0.0000 54.07 59.7763 93.35 85.3727 158.56 0.0000 57.36 0.0000 94.56 85.5259 159.00 48.5124 57.53 71.6703 94.65 85.5374 162.33 73.0214 57.98 75.5609 94. 67 85.5400 162 .. 66 0.0000 59.27 77.6734 94.87 85.5650 163.33 62.0216 59.32 77.6811 97.43 66.8003 165.86 65.5143 59.54 71. 6383 98.43 70.9922 176.31 54.9829 60. 96 82.1009 98.44 70.9932 176.60 0.0000 61.17 82.1344 99.53 59.4815 177.52 78.6400 62.93 79.1938 100 .11 66. 7154 181.07 0.0000 63.29 79.2483 102.03 63.1232 181.52 85.7122 63.58 79.2917 103.18 61.8507 184.41 55.4151 64.28 76.1693 103.37 61. 8672 143.76 55.4839 66.73 86.8927 105.21 58.9239 193.51 46.7650 67.24 69.1252 105.31 58.9322 197.03 49.2043 125.81 71.1292 106.12 58.9978 198.01 60.7014 67.75 71.1381 106.47 59.0261 201.83 47.1197 69.67 88.6620 109.28 63.7561 203.43 71.3554 70.83 69.2471 111. 00 76.0587 205.31 43.0385 72.81 73.7497 111. 76 0.0000 210.85 50. 9710 72.87 73.7572 114.06 67.9973 215.65 46.5295 74.66 73.9861 116. 30 0.0000 222 .11 65.4994 74.82 74.0061 116.74 65.0855 227.09 51. 6773 74.97 74.0250 119.76 62.1757 227.38 49.3405 77 .11 74.2945 121.12 40 .1141 228.16 0.0000 78.74 76.8147 121. 22 40 .1193 228.18 45.8465 79.69 83.5674 121. 78 59.1646 116.74 45.8465 80.12 87.6086 122.06 86.6646 235.69 39.4251 80.19 0.0000 122.92 66.6554 235.96 39.4338 80.57 77.0466 123.07 60.3185 238.63 52.1641 81. 00 82.4175 265.00 70.9544 238.98 0.0000 81. 07 82. 4270 125.81 59.4611 240.99 52.2621 81. 75 80.8548 127.23 84.0285 242.00 52.3037 83.79 98.8127 127.91 72. 3885 244.70 31. 7668 84.00 96.1743 129.30 62.9135 252.40 0.0000 85.43 84.3435 131.20 73.7442 252.80 37.1616 86.55 84.4922 133.02 69.6199 254.15 0.0000 86.79 84.5236 133. 52 58.9444 256.23 42.0667 86.94 84.5435 136.00 69.8639 260.90 0.0000 Page 2948 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 36.2869 355.39 0.0000 584.27 23.0508 264.80 42.3390 356.01 30.8540 595.83 0.0000 265.00 42.3454 364.49 0.0000 427.87 23.2080 268.22 37.1906 366.42 0.0000 602.52 0.0000 269.46 48.5535 372. 51 30.2917 604.72 23.2471 270.03 48.5742 375. 05. 23.4025 607.14 21.8161 271.23 48.6169 377.52 30.3800 609.32 8.7341 273.65 0.0000 356.01 24.8285 610.33 8.7378 276.40 40.6667 388.16 27.5093 614.28 14.5862 277.37 37.8456 388.63 0.0000 618.01 21.4253 277.60 34.1891 391. 69 23.6261 620.36 19.4954 278.00 34.1993 264.66 29.9008 621.93 14.6313 279.20 45.2304 401.81 31. 6802 630.19 0.0000 279.54 45.2417 402.40 32.5707 631.29 12.7276 279.70 41. 577 6 404.85 28.2070 633.25 13.2275 280.46 31. 8121 410.95 31.8391 634.78 0.0000 283.69 42.9222 413. 71 30 .1152 635.95 8.8275 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 33.1518 423. 72 0.0000 645.85 16.7392 285.90 0.0000 427.09 21.4106 657.76 14.8383 287.50 38 .1190 427.87 26.7743 657.90 0.0000 290.67 37.7933 433.94 20.1448 661.66 14.8602 293.27 0.0000 439.40 22.4467 664.57 0.0000 351. 93 38.3243 453.88 21. 7095 666.33 0.0000 295. 96 38.3441 463.37 17.2686 666.50 0.0000 879.38 38.4123 468.07 17.3088 667.71 0.0000 299.98 38.4492 473.00 0.0000 677.62 16.9440 300.09 38.4520 475.06 16.4542 685.70 0.0000 300.13 38.4529 476.78 16.4681 695.00 0.0000 301.36 38.4851 477.60 23.0646 696.49 17.0636 302.85 38.5239 482.18 21.0978 696. 51 17. 0636 256.23 38.5674 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18. 0725 306.78 41. 5334 497.08 18.4774 697.49 18.0740 308.46 43.6592 505.52 20.8699 702.65 21.1256 311. 90 40.0088 507.63 0.0000 706.68 22.1647 316.51 38.4578 511. 00 19.5284 711. 68 19.1770 319.41 0.0000 514.00 19.5551 720.70 0.0000 320.08 0.0000 514.00 19.5551 721. 93 0.0000 321.04 35.2179 520.40 25.2169 722. 78 16.7202 323.87 39.0622 520.69 0.0000 722. 91 18.2410 325.23 37.8360 522.65 0.0000 723. 31 18.2439 328.76 0.0000 527.90 0.0000 724 .19 13. 6873 333.37 40.5684 528.26 15.9340 727.33 14.2096 333.97 40.5830 529.59 25.3224 733.00 12.2046 334.37 40.5938 529.87 0.0000 735.93 15.2716 338.28 29.2484 531.02 0.0000 333.97 16.8075 338.32 29.2491 537.26 0.0000 739.50 0.0000 311. 90 29.2884 546.56 0.0000 747.24 12.2656 340.48 29.2884 552.55 14.2120 748.06 15.3363 340.55 0.0000 563.25 25.7014 752.31 13. 3110 344.28 29.3578 569.33 14.3158 753.82 0.0000 345.93 37.0536 946.00 16.2260 756.73 13. 3317 351.06 27.3438 569.70 16.2273 756.80 12.3066 351. 93 27.3581 583.19 23.0400 884.68 15. 4211 Page 2949 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 37.0342 1274.44 16.5686 1620.50 1.9110 766.42 33.9547 1001.03 19.9087 1621. 92 3. 8232 766.84 23.6691 1002.74 9.9591 1678.03 0.0000 772.60 O.OObO 1004.73 13.2861 1690.97 5.8092 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.9057 778.90 18.5999 1028.54 0.0000 1063.66 8.8391 783.70 0.0000 1037.84 13. 4072 1771.35 4.4905 785.37 5.1778 1038.76 0.0000 1791.20 0.0000 792.07 20.2387 631.29 16.7993 1808.65 -2.9663 794.95 11.4279 1048.07 0.0000 1810.72 0.0000 795.86 15.5884 1049.04 16.8103 1836.06 1. 9869 810.06 17.7498 1050.41 8. 968 8 810.29 16.7070 1063.66 10.1257 344.28 12.5308 1077.00 0.0000 810.76 13.5761 1077.34 20.3247 815.77 0.0000 1085.87 11.3167 1048.07 0.0000 1093.63 9. 0716 832.01 18.9280 1099.45 10.2209 834.85 14.7354 1112. 07 1. 7090 835.71 12.6338 1112. 84 3.4187 836.80 0.0000 1115. 54 6.8423 846.75 0.0000 1120.29 15.4138 846. 77 11. 0934 1120.55' 15.4149 856.80 0.0000 1221.41 15.4171 860.56 13.7945 1129.67 6.8667 871.09 12.7754 1131. 51 0.0000 873.19 17.0449 1147.95 0.0000 875.33 0.0000 1173.23 15.2722 879.38 17.0775 1177.95 13.9004 880.51 18.1510 1189.05 13.9375 883.24 9.6174 1204.77 15.1571 884.68 17.1055 1221.41 14.9248 889.28 10.7060 1231.02 14.0791 894.76 10.7239 1235.36 0.0000 898.04 20.3955 1238.28 10.5776 900.72 11.8173 1260.41 0.0000 903.28 13.9770 1271. 87 14.2139 911.20 9.6995 1274.44 10.6670 912.08 9.7020 1274.54 10.6670 923.98 0.0000 1291. 59 8.0316 926.50 15.1570 1298.22 0.0000 929 .11 6.5007 1312.11 0.0000 937.49 9.7753 1332.49 15.4395 944.13 0.0000 1362.66 0.0000 946.00 10.8883 1365.19 6.3502 949.00 15.2572 1368.63 0.0000 667.71 0.0000 1384.29 7.2876 962. 31 15.3159 1408.01 10.9871 964.08 15.3239 1457.56 0.0000 966 .17 15.3330 1460.82 7.4063 911.20 15. 3450. 1489.16 7.4492 968. 97 15.3450 1505.03 0.9341 983.53 0.0000 1584.12 7.5908 .>'/ 984.45 0.0000 1596.21 0.0000 Page 2950 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:01:35.64 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM08.CNF;320 Background date : Z-OCT-2016 11:00:23. Sample date 10-DEC-2015 14:35:00 Acquisition date : 3-0CT-2016 08:01:06. Sample ID G405235003 Sample quantity 1.40486E+02 GRAM Detector name : GAM08 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.68 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 0 0 0 0 0 0 3 3 0 0 0 7 7 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 2951 of 5809 Energy 41. 47 63.66* 74.52* 77.01* 86.98* 92.58* 104.66 129.00 185.88* 209.35 238.59* 241.51 270.63 278.02* 294. 96* 338.25* 342.50 352.04* 367.54 401. 74 416. 72 463.41 511. 20* 517.47 583.39* 596. 95 609.38* 679.31 706.97 727.97* 781.12 785.41 860.11* 876.69 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 14 67 116 157 51 14 31 18 56 64 371 90 29 15 116 70 33 189 22 16 12 12 42 18 121 14 116 25 9 24 21 25 25 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 99 146 145 119 178 204 88 116 108 112 56 76 77 60 48 52 61 76 30 51 27 30 31 17 33 7 42 17 19 29 2 0 10 7 1. 38 1. 58 1. 30 1.10 1. 03 1. 43 1. 66 0.83 1. 54 3.58 1.15 1. 79 1.12 1. 02 1. 30 1. 72 2.84 1. 25 2.73 4.42 1. 30 1. 33 1. 97 3.86 1. 36 1. 66 1. 56 3.78 0.98 1. 06 0.90 0.87 0.82 3.30 83.16 127.57 149.30 154.28 174.23 185.43 209.61 258.30 372 .11 419.08 477.57 483.42 541.69 556.48 590.38 676.98 685.48 704.59 735.59 804.01 834.00 927.40 1023.03 1035.57 1167.46 1194.59 1219.46 1359.36 1414.71 1456.73 1563.07 1571. 64 1721.09 1754.26 80 122 143 143 171 182 207 253 367 413 473 473 535 550 585 672 672 698 731 795 830 923 1015 1030 1161 1191 1213 1350 1411 1448 1558 1568 1714 1748 7 3. 94E-03118. 8 11 1.87E-02 37.6 16 3.22E-02 20.8 16 4.35E-02 14.7 8 1.41E-02 47.8 9 3.85E-03198.0 7 8.75E-03 52.7 9 4. 96E-03111. 6 9 1.55E-02 38.5 14 l.78E-02 37.2 18 1.03E-01 6.3 18 2.51E-02 27.7 10 8.0lE-03 60.0 9 4.25E-03100.0 10 3.21E-02 14.8 20 1.93E-02 23.1 20 9.06E-03 53.0 14 5.24E-02 12.4 9 6.12E-03 49.3 15 4.37E-03103.2 8 3.34E-03 81.1 8 3.45E-03 81.3 16 l.17E-02 40.9 11 4.86E-03 50.9 12 3.36E-02 13.3 7 3.75E-03 42.1 12 3.23E-02 14.8 17 7.05E-03 42.1 7 2. 61E-03 91. 4 13 6.75E-03 51.9 10 5.72E-03 26.2 8 6.94E-03 20.0 13 6.86E-03 34.3 10 2.16E-03 74.8 Fit 3.53E+OO 1. OlE+OO 2.33E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235003 Acquisition date 3-0CT-2016 08:01:06 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911. 50* 67 13 1. 62 1823.91 1818 14 l.87E-02 17.3 36 0 934.52 9 9 0.92 1869.96 1863 9 2.45E-03 70.0 37 0 963. 07* 27 6 0.63 1927.07 1920 13 7.49E-03 28.3 38 0 968. 96* 44 11 2.45 1938.86 1934 10 1.22E-02 21. 7 39 0 1042.94 18 4 1. 35 2086.86 2082 11 4.90E-03 34.5 40 0 1097.55 11 6 1. 29 2196.11 2192 8 3.14E-03 47.7 41 0 1121.15* 34 10 3.88 2243.33 2236 18 9.40E-03 30.9 42 0 1145 .18 9 7 1.18 2291. 40 2287 8 2.40E-03 69.3 43 0 1155. 67 21 7 2.04 2312.38 2304 14 5.79E-03 34.7 44 0 1239.66 11 12 3.50 2480.41 2473 13 3.12E-03 71. 9 45 0 1243.50 10 0 1. 53 2488.10 2485 7 2.78E-03 31. 6 46 0 1310.84 12 5 1.11 2622.80 2617 12 3.38E-03 48.6 47 0 1408.11 9 2 1. 57 2817.40 2813 9 2. 41E-03 46.2 48 0 1430.72 8 6 0.66 2862.62 2853 13 2.14E-03 76.8 49 0 1460.85 291 3 1. 90 2922.90 2916 13 8.08E-02 6.0 50 0 1764.80* 17 3 1. 03 3530.91 3525 11 4.68E-03 34.6 Flag: "*" = Peak area was modified by background subtraction Page 2952 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:01:37 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 14:35:00 G405235003 Acquisition date : Sample quantity Sample. geometry Detector geometry: 3-0CT-2016 08:01:06 140.49 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMAS 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 TL-208 277.37 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 2953 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 8 6. 94 SN-126 87.57 CD-109 88.03 RA-224 240.99 CM-247 278.00 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.68 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235003 Acquisition date 3-0CT-2016 08:01:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 9.671E-01 1. 446E+Ol 1.446E+Ol 12.00 .OK CD-109 88.03 3.70* 4.281E+OO l .101E+OO 1.722E+OO 181.21 OK SN-126 64.28 9.60 2.181E+OO 2.125E+OO 2.125E+OO 75.23 OK 86.94 8.90 4.281E+OO 4.577E-01 4.577E-01 181.21 OK 87.57 37.00* 4.281E+OO l. lOlE-01 l.lOlE-01 181.21 OK EU-155 86.55 30.70 4.281E+OO l.327E-01 l.495E-01 181.21 OK 105.31 21.10* 5.121E+OO l.853E-01 2.088E-01 105.38 OK TL-208 277.37 6.60 3.703E+OO 3.695E-01 3.695E-01 199.99 OK 583.19 85.00* 2.006E+OO 3.940E-01 3.940E-01 26.63 OK 860.56 12.50 1.479E+00 7.179E-01 7.179E-01 68.57 OK BI-212 727. 33 6.67* l.684E+00 1.178E+OO 1.178E+OO 103.81 OK 785.37 1.10 1.587E+OO 7.754E+OO 7.754E+OO 40.00 OK 1620.50 1. 47 8.836E-01 Line Not Found Absent PB-212 74.82 10.28 3.291E+OO 1.644E+OO 1.644E+OO 57.64 OK 77 .11 17.10 3.516E+OO 1.694E+OO 1.694E+OO 29.38 OK 238.63 43.60* 4.175E+OO 1.218E+OO 1.218E+OO 12. 63 OK 300.09 3.30 3.479E+OO Line Not Found Absent BI-214 609.32 45.49* 1.938E+00 7.300E-01 7.303E-01 29.55 OK 1120.29 14.92 1. 202E+OO 9.905E-01 9.908E-01 61. 72 OK 1764.49 15.30 8.179E-01 6.774E-01 6.777E-01 69.13 OK PB-214 74.82 5.80 3.318E+OO Line Not Found <<INT Reject 77 .11 9.70 3.516E+OO 2.986E+OO 2.987E+OO 29.38 OK 87.09 3.41 4.288E+OO Line Not Found <<INT Reject 242.00 7.25 4.130E+OO Line Not Found <<INT Reject 295.22 18.42 3.529E+OO 1.045E+OO 1.045E+OO 29.69 OK 351.93 35.60* 3.045E+OO 1.007E+OO 1.008E+OO 24.88 OK RN-219 271.23 10.80 3.784E+OO 4.176E-01 4.176E-01 120.01 OK 401.81 6.60* 2.725E+OO 5.016E-01 5.016E-01 206.32 OK RN-222 609.32 45.49* l.938E+OO 7.300E-01 7.303E-01 29.55 OK 1120. 29 14.92 1.202E+OO 9.905E-01 9.908E-01 61. 72 OK 1764.49 15.30 8.179E-01 6.774E-01 6.777E-01 69 .13 OK RA-224 240.99 4.10* 4.136E+OO 1.333E+OO 1.333E+OO 138.31 OK RA-226 609.32 45.49* 1.938E+OO 7.300E-01 7.303E-01 29.55 OK 1120.29 14.92 1. 202E+OO 9.905E-01 9.908E-01 61. 72 OK 1764.49 15.30 8.179E-01 6.774E-01 6.777E-01 69 .13 OK AC-228 105.21 1.10 5 .121E+OO 3.555E+OO 3.555E+OO 105.38 OK 338.32 11. 27 3.149E+OO 1.138E+OO 1.138E+OO 46.11 OK 794.95 4.25 1.572E+OO Line Not Found Absent 835.71 1. 61 1.512E+OO Line Not Found Absent 911. 20 25.80* 1.413E+OO 9.868E-01 9.868E-01 34.65 OK 968. 97 15.80 1.348E+OO 1.097E+OO 1.097E+OO 43.42 OK RA-228 105.21 1.10 5 .121E+OO 3.555E+OO 3.555E+OO 105.38 OK 338.32 11. 27 3.149E+OO 1.138E+OO 1.138E+OO 46 .11 OK 794.95 4.25 l.572E+OO Line Not Found Absent 835. 71 1. 61 1.512E+OO Line Not Found Absent 911.20 25.80* 1.413E+OO 9.868E-01 9.868E-01 34.65 OK 968. 97 15.80 l.348E+00 1.097E+OO l.097E+OO 43.42 OK TH-228 74.82 10.28 3. 291E+OO 1.644E+OO 1.644E+OO 57.64 OK 77 .11 17.10 3.516E+OO 1.694E+OO 1.694E+OO 29.38 OK Page 2954 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235003 Acquisition date 3-0CT-2016 08:01:06 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCilGRAM %Error Status 238.63 43.60* 4.175E+OO 1.218E+OO 1.218E+OO 12.63 OK 300.09 3.30 3.479E+OO Line Not Found Absent TH-230 609.32 45.49* 1.938E+OO 7.301E-01 7.301E-01 29.55 OK 1120.29 14.92 1.202E+OO 9.905E-01 9.905E-01 61. 72 OK 1764.49 15.30 8.179E-01 6.774E-01 6.774E-01 69.13 OK TH-232 105.21 1.10 5.121E+OO 3.555E+OO 3.555E+OO 105.38 OK 338.32 11. 27 3.149E+OO 1.138E+OO 1.138E+OO 46.11 OK 835.71 1. 61 1.512E+00 Line Not Found Absent 911.20 25.80* 1.413E+00 9.868E-01 9.868E-01 34.65 OK 968. 97 15.80 1.348E+OO 1.097E+OO 1.097E+00 43.42 OK TH-234 63.29 3.70* 2.181E+OO 5.514E+OO 5.514E+OO 75.23 OK-92.59 4.23 4.614E+OO 4.562E-01 4.562E-01 395.92 OK U-234 609.32 45.49* 1. 938E+OO 7.300E-01 7. 301E-01 29.55 OK 1120.29 14.92 1. 202E+OO 9.905E-01 9.905E-01 61.72 OK 1764.49 15.30 8.179E-01 6.774E-01 6.774E-01 69.13 OK U-238 63.29 3.70* 2 .181E+OO 5.514E+OO 5.514E+OO 75.23 OK 92.59 4.23 4.614E+OO 4.562E-01 4.562E-01 395.92 OK AM-243 43.53 5.90 2.327E-01 Line Not Found Absent 74.66 67.20* 3.291E+OO 2.515E-01 2.515E-01 57.64 OK CM-247 278.00 3.40 3.703E+OO Line Not Found <<INT Reject 287.50 2.00 3.604E+OO Line Not Found Absent 402.40 72.00* 2.725E+00 4.598E-02 4.598E-02 206.32 OK ANH-511 511. 00 100.00* 2.232E+OO 1. 061E-01 1.061E-01 81. 81 OK Flag: "*" = Keyline Page 2955 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:01:38.98 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l *
  • Acquisition date 3-0CT-2016 08:01:06 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:35:00 Analyst initials: MXRl *
  • Sample ID G405235003 Sample Quantity l.4049E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;14
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.446E+Ol 1. 700E+OO CD-109 1. 722E+OO 3.058E+OO SN-126 1.lOlE-01 1.955E-01 EU-155 2.088E-01 2.156E-01 TL-208 3.940E-01 l.028E-01 BI-212 1.178E+OO 1.199E+OO PB-212 1.218E+OO 1.508E-01 BI-214 7.303E-01 2 .115E-01 PB-214 l.008E+OO 2.457E-01 RN-219 5.016E-01 1.014E+OO RN-222 7.303E-01 2.115E-01 RA-224 1.333E+OO 1.807E+OO RA-226 7.303E-01 2 .115E-01 AC-228 9.868E-01 3. 351E-01 RA-228 9.868E-01 3. 351E-01 TH-228 1.218E+OO 1.508E-01 TH-230 7. 301E-01 2 .114E-01 TH-232 9.868E-01 3. 351E-01 TH-234 5.514E+OO 4.065E+OO U-234 7.301E-01 2 .114E-01 U-238 5.514E+OO 4.065E+OO AM-243 2.515E-01 1. 421E-01 CM-247 4.598E-02 9.297E-02 ANH-511 1.061E-01 8.509E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 2956 of 5809 Key-Line Activity (pCi/GRAM 3.769E-01 -3.017E-02 O.OOOE+OO 2.807E-04 -4 .138E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) l.220E+Ol 6. llOE-02 1. 960E+41 l.819E-02 3.385E-01 1.452E+04 MDA (pCi/GRAM 8.167E-01 3.055E+OO 1.900E-01 2.455E-01 6.557E-02 1.0lOE+OO 1.099E-01 1. 733E-01 l.604E-01 8.686E-01 l.733E-01 l.178E+OO 1.733E-01 3.106E-01 3.106E-01 1.099E-01 1.733E-01 3.106E-01 2.879E+OO l.733E-01 2.879E+OO 1.162E-01 7.973E-02 5.025E-02 MDA (pCi/GRAM 2.376E+Ol l.074E-01 O.OOOE+OO 4.928E-02 6.862E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 4.984E+02 O.OOOE+OO SHORT HLIF MN-54 l.168E-02 6. 721E-02 1.390E-01 NOT IDENT. C0-56 -3.603E-01 5.812E-01 1.044E+OO FAIL ABUN MN-56 O.OOOE+OO 1.603E+41 O.OOOE+OO SHORT HLIF C0-57 3.215E-02 5.676E-02 1. 088E-01 NOT IDENT. C0-58 -7.275E-01 6.999E-01 1.167E+OO NOT IDENT. FE-59 2.551E+OO 9.019E+OO 1.654E+Ol NOT IDENT. C0-60 4. 8 61E-03 5.650E-02 1.113E-01 NOT IDENT. ZN-65 9.557E-02 2.044E-01 3.990E-01 NOT IDENT. GE-68 9.350E-01 2.840E+OO 5.888E+OO NOT IDENT. AS-73 4.679E+OO 1. 492E+Ol 2. 911E+Ol NOT IDENT. AS-74 0.000E+OO 5.875E+03 O.OOOE+OO SHORT HLIF SE-75 2.433E-01 2.254E-01 4.693E-01 FAIL ABUN BR-77 0.000E+OO 1. 469E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.886E+02 O.OOOE+OO SHORT HLIF RB-83 -4.842E-01 8.995E-01 l.357E+OO NOT IDENT. KR-85 9.885E+OO 9. 717E+OO 1.687E+Ol NOT IDENT. SR-85 1.019E+OO 1.004E+OO 1. 743E+OO NOT IDENT. RB-86 O.OOOE+OO 3.377E+04 O.OOOE+OO SHORT HLIF Y-88 -8.771E-02 2.218E-01 4.392E-01 NOT IDENT. Y-91 -2.454E+02 4.722E+02 8.419E+02 NOT IDENT. NB-94 9.471E-03 4.610E-02 8.292E-02 NOT IDENT. NB-95 -6.313E-01 1.019E+00 l.846E+00 NOT IDENT. NB-95M -2.326E-01 2.792E+OO 4.837E+OO NOT IDENT. ZR-95 -9.418E-02 1. 968E+OO 3.838E+OO NOT IDENT. NB-97 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 517E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.217E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 1.169E-02 4.169E-02 7.220E-02 NOT IDENT. RH-102 3.701E-03 6. 831E-02 l.306E-01 NOT IDENT. RU-103 1.458E+OO 6.553E+OO l.286E+Ol FAIL ABUN RH-106 -2.142E-01 6.246E-01 1.109E+OO NOT IDENT. RU-106 -2.142E-01 6.246E-01 1.109E+OO NOT IDENT. AG-108M -9.918E-03 3.475E-02 6.372E-02 NOT IDENT. AG-llOM -2.885E-02 9. lOlE-02 l.769E-01 FAIL ABUN SN-113 7.813E-02 2.482E-01 4.970E-01 NOT IDENT. CD-115 O.OOOE+OO 2.060E+39 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.123E+05 O.OOOE+OO SHORT HLIF TE-123M 1. 883E-01 1. 573E-01 3.123E-01 NOT IDENT. SB-124 -7.623E-01 1.056E+OO 1.104E+OO NOT IDENT. SB-125 -5.468E-02 1.179E-01 2.122E-01 FAIL ABUN TE-125M 1.069E+02 3.419E+02 6. 351E+02 NOT IDENT. I-126 O.OOOE+OO l. ll 7E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.198E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.667E+22 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 5.195E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.039E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.815E+26 O.OOOE+OO SHORT HLIF BA-133 1.325E-02 5.067E-02 9.088E-02 NOT IDENT. I-133 O.OOOE+OO 1.167E+41 O.OOOE+OO SHORT HLIF CS-134 8.258E-02 5.926E-02 l.380E-01 NOT IDENT. CS-135 9.185E-02 l.707E-01 3.171E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.500E+05 O.OOOE+OO SHORT HLIF BA-137M 6.763E-03 4.608E-02 8.695E-02 NOT IDENT. CS-137 7.144E-03 4.868E-02 9.186E-02 NOT IDENT. CE-139 -4.362E-02 1. 406E-01 2.432E-01 NOT IDENT. BA-140 O.OOOE+OO l.724E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.627E+05 O.OOOE+OO SHORT HLIF CE-141 3.308E+OO 3.052E+Ol 5.510E+Ol NOT IDENT. CE-143 O.OOOE+OO 8.286E+40 O.OOOE+OO SHORT HLIF CE-144 9.356E-02 4.746E-01 8.603E-01 NOT IDENT. PM-144 -l.355E-02 6.227E-02 1.212E-01 NOT IDENT. PR-144 -1.232E+OO 5.393E+OO l.048E+Ol NOT IDENT. PM-146 4.955E-03 5.043E-02 9.762E-02 NOT IDENT. ND-147 0.000E+OO 4.064E+07 O.OOOE+OO SHORT HLIF PM-147 -9 .139E+02 1.045E+03 1. 7 53E+03 NOT IDENT. PM-149 O.OOOE+OO 2. 372E+40 O.OOOE+OO SHORT HLIF EU-150 -6.881E-03 3.208E-02 5.364E-02 FAIL ABUN EU-152 7.929E-04 1.151E-01 l.992E-01 FAIL ABUN GD-153 -8.738E-02 2. 201E-01 3.926E-01 FAIL ABUN EU-154 -7.705E-02 1.494E_..:01 2.614E-01 NOT IDENT. TB-160 -7.311E-01 1.832E+OO 2. 961E+OO FAIL ABUN H0-166M 6.388E-02 7.824E-02 l.640E-01 FAIL ABUN TM-171 -1.557E+Ol 3.878E+Ol 7.150E+Ol NOT IDENT. HF-172 -9.778E-02 2.939E-01 4.742E-01 FAIL ABUN LU-172 4.333E-02 1.119E-01 2 .119E-01 FAIL ABUN Page 2957 of 5809 LU-176 2.191E-02 2.782E-02 5.780E-02 FAIL ABUN HF-181 2.207E+OO 4.754E+OO 9.671E+OO NOT IDENT. TA-182 -8.885E-01 1.158E+OO 1.927E+OO FAIL ABUN RE-183 1.486E-01 4.431E+OO 8.474E+00 NOT IDENT. RE-184 9.336E+OO 3.418E+Ol 7.087E+Ol NOT IDENT. W-188 9.807E+OO 1. 24 7E+02 2.208E+02 FAIL ABUN IR-192 -l.562E-01 5.335E-01 9. 972E-01 FAIL ABUN HG-203 2.509E+OO 4.918E+OO 4.798E+OO FAIL ABUN BI-207 -2.470E-02 6.450E-02 1.176E-01 FAIL ABUN PB-210 4.378E+OO 6.861E+.OO 1.389E+Ol NOT IDENT. BI-211 O.OOOE+OO 6. 7 67E-01 9.852E-01 FAIL ABUN PB-211 -6.341E-02 7.940E-01 1.350E+OO NOT IDENT. RA-223 -3.459E-01 6.499E-01 1.14 7E+OO FAIL ABUN AC-227 6.193E-02 2.609E-01 5.171E-01 NOT IDENT. TH-227 6.193E-02 2.609E-01 5.171E-01 NOT IDENT. TH-229 3 .118E-01 5.182E-01 1.061E+OO FAIL ABUN PA-231 8.794E-01 5.953E-01 1.261E+OO NOT IDENT. TH-231 -3.459E-01 6.499E-01 1.147E+OO FAIL ABUN PA-233 -1.557E-02 6.863E-02 1.294E-01 NOT IDENT. PA-234 6. OllE-02 3.615E-01 7.255E-01 NOT IDENT. PA-234M 1.138E+OO 6.167E+OO 1. 246E+Ol NOT IDENT. U-235 l.168E-01 2.250E-01 4.286E-01 FAIL ABUN NP-237 -l.557E-02 6.863E-02 l.294E-01 NOT IDENT. NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 4.035E-02 3.200E-01 5.880E-01 FAIL ABUN PU-239 3.234E+02 7. 071E+02 7.300E+02 FAIL ABUN AM-241 1.208E-02 2.140E-01 3.793E-01 NOT IDENT. CM-243 1.908E-01 1.970E-01 2. 313E-01 FAIL ABUN BK-247 3.487E-02 8.713E-02 l.603E-01 NOT IDENT. CF-249 -2.600E-02 4.139E-02 7.336E-02 NOT IDENT. CF-251 5.720E-02 l.289E-01 2.619E-01 NOT IDENT. Page 2958 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:01:36.41 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 279 10.66* 9.671E-01 1.446E+Ol l.446E+Ol 12.00 CD-109 88.03 61 3.70* 4.281E+OO 2.064E+OO 3.228E+OO 95.67 SN-126 64.28 83 9.60 2.181E+OO 2.125E+OO 2.125E+OO 75.23 86.94 61 8.90 4.281E+OO 8.580E-01 8.580E-01 95.67 87.57 61 37.00* 4.281E+OO 2.064E-01 2.064E-01 95.67 EU-155 86.55 61 30.70 4.281E+OO 2.487E-01 2.802E-01 95.67 105.31 37 21.10* 5.121E+OO l.853E-01 2.088E-01 105.38 HG-203 70.83 ------3.69 2.935E+OO ------Line Not Found ------72. 87 ------6.19 3 .135E+00 ------Line Not Found ------279.20 17 81.56* 3.703E+00 2.990E-02 2.509E+OO 199.99 TL-208 277.37 17 6.60 3.703E+OO 3.695E-01 3.695E-01 199.99 583.19 126 85.00* 2.006E+OO 3.940E-01 3.940E-01 26.63 860.56 25 12.50 1.479E+OO 7.179E-01 7.179E-01 68.57 BI-211 72.87 ------1. 23 3.135E+OO ------Line Not Found ------351.06 204 12.92* 3.045E+OO 2.776E+OO 2.776E+OO 24.88 BI-212 727: 33 25 6.67* 1.684E+OO l.178E+OO 1.178E+OO 103.81 785.37 25 1.10 1.587E+OO 7.754E+00 7.754E+00 40.00 1620.50 ------1. 47 8.836E-01 ------Line Not Found ------PB-212 74.82 141 10.28 3.291E+OO 2.233E+00 2.233E+OO 41. 69 77 .11 191 17.10 3.516E+OO 1.694E+OO 1.694E+OO 29.38 238.63 415 43.60* 4.175E+OO l.218E+00 l.218E+00 12.63 300.09 ------3.30 3.479E+OO ------Line Not Found ------BI-214 609.32 120 45.49* 1.938E+00 7.300E-01 7.303E-01 29.55 1120.29 33 14.92 1. 202E+OO 9.905E-01 9.908E-01 61. 72 1764.49 16 15.30 8.179E-01 6.774E-01 6.777E-01 69 .13 PB-214 74.82 141 5.80 3.291E+OO 3.959E+OO 3.960E+OO 41. 69 77 .11 191 9.70 3.516E+OO 2.986E+00 2.987E+OO 2 9 .'3 8 87.09 61 3.41 4.281E+OO 2.239E+00 2.240E+OO 95.67 242.00 101 7.25 4.136E+OO 1.799E+OO 1.799E+OO 55.34 295.22 127 18.42 3.529E+OO 1.045E+OO 1.045E+OO 29.69 351. 93 204 35.60* 3.045E+OO 1.007E+OO 1.008E+OO 24.88 RN-219 271.23 32 10.80 3.784E+OO 4.176E-01 4.176E-01 120.01 401. 81 17 6.60* 2.725E+OO 5.016E-01 5.016E-01 206.32 RN-222 609.32 120 45.49* 1.938E+OO 7.300E-01 7.303E-01 29.55 1120.29 33 14.92 1.202E+OO 9.905E-01 9.908E-01 61. 72 1764.49 16 15.30 8.179E-01 6.774E-01 6.777E-01 69.13 RA-224 240.99 101 4.10* 4.136E+OO 3.181E+OO 3 .181E+OO 55.34 RA-226 609.32 120 45.49* 1.938E+OO 7.300E-01 7.303E-01 29.55 1120.29 33 14.92 1.202E+OO 9.905E-01 9.908E-01 61. 72 1764.49 16 15.30 8.179E-01 6.774E-01 6.777E-01 69.13 AC-228 105.21 37 1.10 5.121E+OO 3.555E+OO 3.555E+OO 105.38 338.32 76 11. 27 3.149E+OO l.138E+OO 1.138E+OO 46.11 794.95 ------4.25 1. 572E+OO ------Line Not Found ------835.71 ------1. 61 1.512E+OO ------Line Not Found ------911.20 67 25.80* 1. 413E+OO 9.868E-01 9.868E-01 34.65 968. 97 44 15.80 1.348E+OO 1.097E+OO 1.097E+OO 43.42 RA-228 105.21 37 1.10 5.121E+OO 3.555E+00 3.555E+00 105.38 Page 2959 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235003 Acquisition date 3-0CT-2016 08:01:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 338.32 76 11. 27 3.149E+OO 1.138E+OO 1.138E+OO 46 .11 794.95 ------4.25 1. 572E+OO ------Line Not Found ------835. 71 ------1. 61 1.512E+OO ------Line Not Found ------911.20 67 25.80* 1.413E+OO 9.868E-01 9.868E-01 34.65 968.97 44 15.80 l.348E+OO l.097E+OO 1.097E+OO 43.42 TH-228 74.82 141 10.28 3.291E+OO 2.233E+OO 2.233E+OO 41. 69 77 .11 191 17.10 3.516E+OO 1.694E+OO l.694E+OO 29.38 238.63 415 43.60* 4.175E+OO 1.218E+OO 1.218E+OO 12.63 300.09 ------3.30 3.479E+OO ------Line Not Found ------TH-230 609.32 120 45.49* 1.938E+OO 7. 301E-01 7.301E-01 29.55 1120.29 33 14.92 l.202E+OO 9.905E-01 9.905E-01 61. 72 1764.49 16 15.30 8.179E-Ol 6.774E-01 6.774E-01 69.13 TH-232 105.21 37 1.10 5.121E+OO 3.555E+00 3.555E+OO 105.38 338.32 76 11.27 3.149E+OO 1.138E+OO 1.138E+OO 46.11 835. 71 ------1. 61 l.512E+OO ------Line Not Found ------911.20 67 25.80* 1.413E+OO 9.868E-01 9.868E-01 34.65 968. 97 44 15.80 1. 348E+OO 1.097E+OO 1.097E+OO 43.42 TH-234 63.29 83 3.70* 2.181E+OO 5.514E+OO 5.514E+OO 75.23 92.59 17 4.23 4.614E+OO 4.562E-01 4.562E-01 395.92 U-234 609.32 120 45.49* l.938E+OO 7.300E-01 7. 301E-01 29.55 1120.29 33 14.92 1.202E+OO 9.905E-01 9.905E-01 61. 72 1764.49 16 15.30 8.179E-01 6.774E-01 6.774E-01 69.13 U-238 63.29 83 3.70* 2.181E+OO 5.514E+OO 5.514E+OO 75.23 92.59 17 4.23 4.614E+OO 4.562E-01 4.562E-01 395.92 AM-243 43.53 ------5.90 2.327E-01 ------Line Not Found ------74.66 141 67.20* 3.291E+OO 3.417E-01 3.417E-01 41. 69 CM-247 278.00 17 3.40 3.703E+OO 7.173E-01 7.173E-01 199.99 287.50 ------2.00 3.604E+OO ------Line Not Found ------402.40 17 72.00* 2. 725E+OO 4.598E-02 4.598E-02 206.32 ANH-511 511.00 44 100.00* 2.232E+OO 1. 061E-01 1.061E-01 81. 81 Flag: "*" Key line Page 2960 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235003 Acquisition date 3-0CT-2016 08:01:06 Total number of lines in spectrum 50 Number of unidentified lines 13 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 SN-126 EU-155 HG-203 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 . AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 CM-247 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 4.75Y 46.59D 1.41E+10Y 7.04E+08Y 1.41E+l0Y l.41E+l0Y 1600. OOY 1600. OOY 7.04E+08Y 1600. OOY l.41E+l0Y 1600.00Y l.41E+l0Y 1.41E+10Y 1. 41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.56E+07Y 1.00E+09Y Decay 1. 00 1. 56 1. 00 1.13 83.9 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.446E+Ol 2.064E+OO 2.064E-01 l.853E-01 2.990E-02 3.940E-01 2.776E+OO l. l 78E+OO 1.218E+OO 7.300E-01 l.007E+00 5.016E-01 7.300E-01 3.181E+00 7.300E-01 9.868E-01 9.868E-01 1.218E+OO 7.301E-01 9.868E-01 5.514E+OO 7.300E-01 5.514E+OO 3.417E-01 4.598E-02 1.061E-01 4.655E+Ol 4.655E+Ol Decay Corr pCi7GRAM l.446E+Ol 3.228E+OO 2.064E-01 2.088E-01 2.509E+OO 3.940E-01 2.776E+OO 1.178E+OO 1.218E+OO 7.303E-01 1.008E+OO 5.016E-01 7.303E-01 3.181E+OO 7.303E-01 9.868E-01 9.868E-01 1.218E+OO 7. 301E-01 9.868E-01 5.514E+OO 7. 301E-01 5.514E+OO 3.417E-01 4.598E-02 l.061E-01 5.022E+Ol 5.022E+Ol 74.00%. Decay Corr 2-Sigma Error 0.173E+Ol 3.088E+OO 1.974E-01 2.200E-01 5.018E+OO 1.049E-01 0.690E+OO 1.223E+OO 0.154E+00 2.158E-01 0.251E+OO 10.35E-01 2.158E-01 1. 760E+OO 2.158E-01 3.419E-01 3.419E-01 0.154E+OO 2.157E-01 3.419E-01 4.148E+OO 2.157E-01 4.148E+OO 1.425E-01 9.486E-02 0.868E-01 "M" Manually accepted 2-Sigma %Error 12.00 95. 67 95. 67 105.38 199.99 26.63 24.88 103.81 12.63 29.55 24.88 206.32 29.55 55.34 29.55 34.65 34.65 12.63 29.55 34.65 75.23 29.55 75.23 41. 69 206.32 81. 81 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 2961of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235003 Acquisition date : 3-0CT-2016 08:01:06 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 41. 47 18 126 1. 38 83.16 80 7 3.94E-03 **** l.33E-01 0 129.00 21 136 0.83 258.30 253 9 4. 96E-03 **** 5.48E+OO T 0 185.88 64 123 1. 54 372 .11 367 9 l.55E-02 76.9 4.93E+OO T 0 .209. 35 72 126 3.58 419.08 413 14 1.78E-02 74.5 4.58E+OO T 7 342.50 35 66 2.84 685.48 672 20 9.06E-03 **** 3.12E+OO 0 367.54 24 32 2.73 735.59 731 9 6.12E-03 98.5 2.94E+OO T 0 416.72 13 29 1. 30 834.00 830 8 3.34E-03 **** 2.64E+OO 0 463.41 13 31 1. 33 927.40 923 8 3.45E-03 **** 2.42E+OO T 0 517.47 18 17 3. 86 1035.57 1030 11 4.86E-03 **** 2.21E+OO 0 596. 95 14 7 1. 66 1194.59 1191 7 3.75E-03 84.1 l.97E+OO T 0 679.31 26 17 3.78 1359.36 1350 17 7.05E-03 84.2 1. 78E+OO 0 706.97 10 19 0.98 1414.71 1411 7 2.61E-03 **** 1. 72E+OO T 0 781.12 21 2 0.90 1563.07 1558 10 5. 72E-03 52.5 l.59E+OO 0 876.69 8 7 3.30 1754.26 1748 10 2.16E-03 **** 1.46E+OO T 0 934.52 9 9 0.92 1869.96 1863 9 2.45E-03 **** 1.39E+OO 0 963.07 27 6 0.63 1927.07 1920 13 7.49E-03 56.7 1.35E+OO T 0 1042.94 17 4 1. 35 2086.86 2082 11 4.90E-03 69.1 1.27E+OO 0 1097.55 11 6 1. 29 2196 .11 2192 8 3.14E-03 95.4 1.22E+OO 0 1145 .18 8 7 1.18 2291. 40 2287 8 2.40E-03 **** 1.18E+OO 0 1155. 67 20 7 2.04 2312.38 2304 14 5.79E-03 69.5 1.17E+OO 0 1239.66 11 11 3.50 2480.41 2473 13 3.12E-03 **** 1. llE+OO T 0 1243.50 10 0 1. 53 2488.10 2485 7 2.78E-03 63.2 I. llE+OO 0 1310. 84 12 5 1.11 2622.80 2617 12 3.38E-03 97.2 1. 06E+OO T 0 1408 .11 8 2 1. 57 2817.40 2813 9 2. 41E-03 92.3 9.98E-01 T 0 1430. 72 7 6 0.66 2862.62 2853 13 2.14E-03 **** 9.84E-01 Flags: "T" = Tentatively associated Page 2962 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:01:56.09 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l *
  • Acquisition date 3-0CT-2016 08:01:06 Sensitivity 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:35:00 Nuclide Library : SOLID *
  • Sample ID G405235003 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4049E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 EU-155 TL-208 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-22 6 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 3.380E-01 1.453E+OO 9.024E-02 1.148E-01 2.846E-02 4.395E-01 5.081E-02 7.832E-02 7. 331E-02 3.930E-01 7.832E-02 5.448E-01 7.832E-02 l.353E-01 1.353E-01 5.081E-02 7.829E-02 1.353E-01 1.343E+00 7.829E-02 1.343E+OO 5.467E-02 3.607E-02 2 .181E-;-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 2963 of 5809 Le (pCi/GRAM 1.043E+Ol 4.538E-02 O.OOOE+OO 1.558E-02 2.834E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M' RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 2964 of 5809 6.013E-02 4.509E-01 O.OOOE+OO 5.090E-02 4. 960E-01 7.178E+OO 4.792E-02 1. 717E-01 2.553E+OO 1.364E+Ol O.OOOE+OO 2.162E-01 0.000E+OO O.OOOE+OO 5. 964E-01 7.628E+OO 7.877E-01 O.OOOE+OO 1.556E-01 3.369E+02 3. 721E-02 8.089E-01 2.238E+OO 1.712E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 3.369E-02 5.716E-02 5.748E+OO 4.864E-01 4.864E-01 2.865E-02 7. 251E-02 2.238E-01 O.OOOE+OO O.OOOE+OO 1.466E-01 O.OOOE+OO 9.428E-02 2.980E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.124E-02 O.OOOE+OO 6.184E-02 1. 4 63E-01 O.OOOE+OO O.OOOE+OO 3.888E-02 4.108E-02 1.135E-01 O.OOOE+OO 0.000E+OO 2.591E+Ol O.OOOE+OO 4.045E-01 5.312E-02 4.593E+OO 4.368E-02 0.000E+OO 8.158E+02 O.OOOE+OO 2.434E-02 9.019E-02 l.835E-01 1.102E-01 1.190E+OO 7.409E-02 3.345E+Ol 2.205E-01 9.319E-02 2.657E-02 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 2965 of 5809 4.324E+OO 8.178E-01 3. 962E+OO 3.085E+Ol l.004E+02 4.542E-01 2.190E+OO 5.088E-02 6.513E+OO 4.739E-Ol 6.025E-01 5.165E-01 2.386E-01 2.386E-01 4.951E-01 5.901E-01 5.165E-01 5.895E-02 3.184E-01 5.567E+OO 2.016E-01 5.895E-02 O.OOOE+OO 2.763E-01 3. 431E+02 1.772E-01 1.084E-01 7.365E-02 3.265E-02 1.223E-01 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:02:07.13 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235003.CNF;l * *Acquisition date 3-0CT-2016 08:01:06 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:35:00 Nuclide Library : SOLID *
  • Sample ID G405235003 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4049E+02 GRAM *
  • Quantity Err(%) : 1. 4236E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 21-JUL-2016 '06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.446E+Ol 1.860E+00 1. 860E+OO CD-109 l.722E+00 3.067E+00 3.067E+OO SN-126 1.lOlE-01 1. 960E-01 1. 960E-01 EU-155 2.088E-01 2.161E-01 2 .161E-01 TL-208 3.940E-01 1.042E-01 l.042E-01 BI-212 1.178E+OO l.200E+00 1.200E+OO PB-212 1.218E+OO l.640E-01 1.640E-01 BI-214 7.303E-01 2.138E-01 2 .138E-01 PB-214 1.008E+OO 2.492E-01 2.492E-01 RN-219 5.016E-01 1. 016E+OO 1.016E+OO RN-222 7.303E-01 2.138E-01 2.138E-01 RA-224 1.333E+OO 1. 812E+OO 1.812E+OO RA-226 7.303E-01 2.138E-01 2.138E-01 9.868E-01 3.389E-01 3.389E-01 RA-228 9.868E-01 3.389E-01 3.389E-01 TH-228 1.218E+OO 1.640E-01 l.640E-01 TH-230 7.301E-01 2.137E-01 2.137E-01 TH-232 9.868E-01 3.389E-01 3.389E-01 TH-234 5.514E+OO 4.245E+OO 4.245E+OO U-234 7.301E-01 2 .137E-01 2.137E-01 U-238 5.514E+OO 4.245E+OO 4.245E+OO AM-243 2.515E-01 1.434E-01 1.434E-01 CM-247 4.598E-02 9.329E-02 9.329E-02 ANH-511 1.061E-01 8.520E-02 8.520E-02 Non-Identified Nuclides ----Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 3.769E-01 1.220E+Ol 1.220E+Ol NOT IDENT. NA-22 -3.017E-02 6. lllE-02 6.261E-02 NOT IDENT. NA-24 -1.000E+41 8.361E+41 O.OOOE+OO SHORT HLIF AL-26 2.807E-04 l.819E-02 1. 819E-02 NOT IDENT. SC-46 -4.138E-02 3.385E-01 3.390E-01 FAIL ABUN V-48 -8.087E+03 l.452E+04 1.497E+04 SHORT HLIF Page 2966 of 5809 CR-51 2. 431E+02 4.985E+o2 5.104E+02 SHORT HLIF MN-54 1.168E-02 6. 721E-02 6.742E-02 NOT IDENT. C0-56 -3.603E-01 5.814E-01 6.037E-01 FAIL ABUN MN-56 -1.000E+41 1. 604E+41 0.000E+OO SHORT HLIF C0-57 3.215E-02 5.678E-02 5.860E-02 NOT IDENT. C0-58 -7.275E-01 7.006E-01 7.736E-01 NOT IDENT. FE-59 2.551E+OO 9.021E+OO 9.094E+OO NOT IDENT. C0-60 4.861E-03 5.650E-02 5.654E-02 NOT IDENT. ZN-65 9.557E-02 2.045E-01 2.090E-01 NOT IDENT. GE-68 9.350E-01 2.840E+OO 2. 871E+OO NOT IDENT. AS-73 4.679E+OO l.495E+Ol l.510E+Ol NOT IDENT. AS-74 7.125E+03 5.904E+03 6.722E+03 SHORT HLIF SE-75 2.433E-01 2.257E-01 2.509E-01 FAIL ABUN BR-77 1.187E+38 1. 020E+39 O.OOOE+OO SHORT HLIF SR-82 -5.075E+Ol 7.886E+02 7.890E+02 SHORT HLIF RB-83 -4.842E-Dl 9.019E-01 9.280E-01 NOT IDENT. KR-85 9.885E+OO 9.725E+OO 1.070E+Ol NOT IDENT. SR-85 1.019E+OO 1.005E+OO l.105E+OO NOT IDENT. RB-86 l.534E+03 3.377E+04 3.378E+04 SHORT HLIF Y-88 -8. 771E-02 2.218E-01 2.253E-01 NOT IDENT. Y-91 -2.454E+02 4. 723E+02 4. 851E+02 NOT IDENT. NB-94 9.471E-03 4.610E-02 4.630E-02 NOT IDENT. NB-95 -6.313E-01 1.019E+OO l.058E+OO NOT IDENT. NB-95M -2.326E-01 2.792E+OO 2.794E+OO NOT IDENT. ZR-95 -9.418E-02 l.968E+00 1. 968E+OO NOT IDENT. NB-97 -l.000E+41 3.976E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 1.517E+41 O.OOOE+OO SHORT HLIF M0-99 5.623E+30 1.217E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 3.882E+41 O.OOOE+OO SHORT HLIF RH-101 l.169E-02 4.175E-02 4.208E-02 NOT IDENT. RH-102 3. 701E-03 6. 831E-02 6.833E-02 NOT IDENT. RU-103 1.458E+OO 6.554E+OO 6.586E+OO FAIL ABUN RH-106 -2.142E-01 6.247E-01 6.321E-01 NOT IDENT. RU-106 -2.142E-01 6.247E-01 6.321E-01 NOT IDENT. AG-108M -9.918E-03 3.475E-02 3.504E-02 NOT IDENT. AG-110M -2.885E-02 9.102E-02 9.195E-02 FAIL ABUN SN-113 7.813E-02 2.482E-01 2.507E-01 NOT IDENT. CD-115 -1.298E+39 2.074E+39 O.OOOE+OO SHORT HLIF SN-117M 1. 370E+04 1.123E+05 l.125E+05 SHORT HLIF TE-123M 1. 883E-01 l.576E-01 l.790E-01 NOT IDENT. SB-124 -7.623E-01 1.057E+OO l .112E+OO NOT IDENT. SB-125 -5.468E-02 l.179E-01 1.205E-01 FAIL ABUN TE-125M 1.069E+02 3.420E+02 3.453E+02 NOT IDENT. I-126 -3.319E+04 1.117E+06 l.117E+06 SHORT HLIF SB-126 5.939E+05 1.203E+06 l.233E+06 SHORT HLIF SB-127 2.057E+21 l.690E+22 O.OOOE+OO SHORT HLIF I-131 -3.372E+09 5.197E+09 5.415E+09 SHORT HLIF I-132 l.OOOE+41 1.838E+42 0.000E+OO SHORT HLIF TE-132 -1. 489E+26 2.879E+26 O.OOOE+OO SHORT HLIF BA-133 l.325E-02 5.067E-02 5.102E-02 NOT IDENT. I-133 1.000E+41 2.142E+41 O.OOOE+OO SHORT HLIF CS-134 8.258E-02 5.936E-02 7.007E-02 NOT IDENT. CS-135 9.185E-02 1.708E-01 1.757E-01 NOT IDENT. I-135 1.000E+41 2.658E+42 O.OOOE+OO SHORT HLIF CS-136 2.261E+05 3.508E+05 3.653E+05 SHORT HLIF BA-137M 6.763E-03 4.608E-02 4.619E-02 NOT IDENT. CS-137 7.144E-03 4.868E-02 4.879E-02 NOT IDENT. CE-139 -4.362E-02 l.409E-01 1.422E-01 NOT IDENT. BA-140 -4.541E+05 1.724E+06 1. 737E+06 SHORT HLIF LA-140 -7.891E+04 3.627E+05 3.644E+05 SHORT HLIF CE-141 3.308E+OO 3.052E+Ol 3.055E+Ol NOT IDENT. CE-143 l.OOOE+41 8.347E+40 O.OOOE+OO SHORT HLIF CE-144 9.356E-02 4.746E-01 4.765E-01 NOT IDENT. PM-144 -l.355E-02 6.227E-02 6.257E-02 NOT IDENT. PR-144 -l.232E+00 5.394E+OO 5.422E+00 NOT IDENT. PM-146 4.955E-03 5.043E-02 5.048E-02 NOT IDENT. ND-147 -5. 972E+06 4.064E+07 4.073E+07 SHORT HLIF PM-147 -9.139E+02 l.046E+03 l.124E+03 NOT IDENT. PM-149 -6.305E+39 2.376E+40 O.OOOE+OO SHORT HLIF EU-150 -6. 881E-03 3.208E-02 3.223E-02 FAIL ABUN EU-152 7.929E-04 1.151E-01 l.151E-01 FAIL ABUN GD-153 -8.738E-02 2.202E-01 2.237E-01 FAIL ABUN EU-154 -7.705E-02 l.494E-01 1.534E-01 NOT IDENT. TB-160 -7. 311E-01 1.832E+OO 1.862E+OO FAIL ABUN H0-166M 6.388E-02 7. 831E-02 8.344E-02 FAIL ABUN TM-171 -l.557E+01 3.880E+Ol 3.943E+Ol NOT IDENT. HF-172 -9.778E-02 2.943E-01 2.976E-01 FAIL ABUN LU-172 4.333E-02 l.119E-01 l.136E-01 FAIL ABUN Page 2967 of 5809 LU-176 2 .191E-02 2.783E-02 2.953E-02 FAIL ABUN HF-181 2.207E+00 4.755E+OO 4.858E+OO NOT IDENT. TA-182 -8.885E-01 1.159E+OO 1.226E+OO FAIL ABUN RE-183 1. 486E-01 4.431E+OO 4. 431E+OO NOT IDENT. RE-184 9.336E+OO 3.425E+Ol 3. 451E+Ol NOT IDENT. W-188 9.807E+00 1. 24 7E+02 l.248E+02 FAIL ABUN IR-192 -l.562E-01 5.335E-01 5.382E-01 FAIL ABUN HG-203 2.509E+OO 4.919E+OO 5.048E+OO FAIL ABUN BI-207 -2.470E-02 6.451E-02 6.546E-02 FAIL ABUN PB-210 4.378E+OO 6.874E+OO 7.151E+OO NOT IDENT. BI-211 2.776E+OO 6.879E-01 1.428E+OO FAIL ABUN PB-211 -6.341E-02 7.940E-01 7.945E-01 NOT IDENT. RA-223 -3.459E-01 6.502E-01 6.687E-Ol FAIL ABUN AC-227 6.193E-02 2.610E-01 2.625E-01 NOT IDENT. TH-227 6.193E-02 2.610E-01 2.625E-01 NOT IDENT. TH-229 3 .118E-01 5.184E-01 5. 372E-01 FAIL ABUN PA-231 8.794E-01 6.242E-01 7.395E-01 NOT IDENT. TH-231 -3.459E-01 6.502E-01 6.687E-01 FAIL ABUN PA-233 -1.557E-02 6.864E-02 6.900E-02 NOT IDENT. PA-234 6. OllE-02 3.680E-01 3.690E-01 NOT IDENT. PA-234M 1.138E+OO 6.167E+OO 6.189E+OO NOT IDENT. U-235 1.168E-01 2. 251E-01 2. 311E-01 FAIL ABUN NP-237 -l.557E-02 6.864E-02 6.900E-02 NOT IDENT. NP-238 -9.871E+40 2.386E+41 O.OOOE+OO SHORT HLIF NP-239 4.035E-02 3.200E-01 3.206E-01 FAIL ABUN PU-239 3.234E+02 7.073E+02 7.222E+02 FAIL ABUN AM-241 1.208E-02 2.140E-01 2 .141E-01 NOT IDENT. CM-243 l.908E-01 1.978E-01 2.157E-01 FAIL ABUN BK-247 3.487E-02 8.741E-02 8. 881E-02 NOT IDENT. CF-249 -2.600E-02 4.145E-02 4.307E-02 NOT IDENT. CF-251 5.720E-02 1. 291E-01 1. 317E-01 NOT IDENT. Page 2968 of 5809
  • GEL Laboratories LLC *
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  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 59.6892 87.09 118. 9514 136.47 81.1235 45.60 68.0586 87.57 119. 0594 140.51 0.0000 46.54 61.2173 88.03 127.9901 143.76 60.2501 49. 72 0.0000 88.34 128.0645 144.24 72.3468 51. 35 64.0687 88.47 128.0954 145.44 79.7094 51. 87 70. 2 67 9 89. 96 126.2374 152.43 62.1633 52.39 75.4637 1093.63 104.2217 153.25 0.0000 52.97 68.4295 91.11 0.0000 323.87 76.9658 53.44 61.3554 92.59 107.9328 156.02 0.0000 54.07 67.6015 93.35 108.0823 158.56 0.0000 57.36 0.0000 94.56 84.8680 159.00 50.3948 57.53 66 .1311 94.65 84.8813 162.33 59.2449 57.98 68.2737 94.67 84.8848 162.66 0.0000 59.27 66.4148 94.87 84.9149 163.33 58.0823 59.32 66.4231 97.43 78.5674 165.86 73.1387 59.54 66.4585 98.43 68.5859 176.31 68.6178 60. 96 63.9081 98.44 68.5873 176.60 0.0000 61.17 63.9402 99.53 63.0850 177.52 57.8208 62.93 63.8584 100 .11 75.5524 181. 07 0.0000 63.29 63.9123 102.03 63.3568 181.52 64.4029 63.58 63.9555 103.18 64.9917 184.41 64.1930 64.28 64.0596 103.37 66.5246 143.76 64.2881 66.73 70.4041 105.21 70.5224 193.51 52.9009 67.24 76.1237 105.31 70.5343 197.03 70.2344 125.81 87.4877 106.12 71. 3888 198.01 53.1602 67.75 86.0897 106.47 68.3908 201. 83 68.0136 69.67 72.2842 109.28 62.9815 203.43 53.8135 70.83 89.5185 111. 00 75.7883 205.31 55.7348 72. 81 83.4790 111. 7 6 0.0000 210.85 47.7999 72.87 83.4897 114.06 70.3898 215.65 69.1703 74.66 83.8069 116. 30 0.0000 222 .11 52.7423 74.82 83.8349 116.74 77.6390 227.09 48.5843 74.97 83.8611 119. 76 68.6882 227.38 50.3655 77 .11 84.2342 121.12 81.6633 228.16 0.0000 78.74 88.1268 121. 22 81.6761 228.18 58.3630 79.69 94.0862 121. 78 65. 3960 116.74 58.3630 80.12 76.7822 122.06 58.4141 235.69 53.4418 80.19 0.0000 122.92 58.4900 235. 96 52 .1194 80.57 58.0013 123.07 59.6730 238.63 50. 9112 81. 00 74.0150 265.00 62.0702 238.98 0.0000 81. 07 95.7975 125.81 67.3581 240.99 51.0242 81. 75 101. 37 68 127.23 58.0801 242.00 51. 0724 83.79 74.4222 127.91 60.1026 244.70 41.7688 84.00 74.4528 129.30 60.2240 252.40 0.0000 85.43 112.7193 131.20 77.3620 252.80 40.7217 86.55 118.8295 133.02 68.8573 254.15 0.0000 86.79 118.8831 133.52 74.8471 256.23 43.5703 86.94 118.9177 136.00 77.4940 260.90 0.0000 Page 2969 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 27.4353 355.39 0.0000 584.27 10.0789 264.80 26.0664 356.01 27.9886 595.83 0.0000 265.00 35.6762 364.49 0.0000 427.87 8.4644 268.22 37.1522 366.42 0.0000 602.52 0.0000 269.46 42.2425 372. 51 20.8590 604. 72 27 .1387 270.03 42.2640 375.05 27.8604 607.14 35.6592 271. 23 46.9056 377.52 20.9299 609.32 29.4626 273.65 0.0000 356.01 29.0254 610.33 25.5093 276.40 40.6466 388.16 31.1154 614.28 28.9625 277.37 40.6798 388.63 0.0000 618.01 14.7906 277.60 40.6878 391.69 23.1390 620.36 28.4749 278.00 40.2387 2 64. 66 30.3571 621.93 21.6564 279.20 30.5568 401. 81 30.3796 630.19 0.0000 279.54 30.5656 402.40 30.3906 631.29 16.0251 279.70 30. 5696 404.85 24.3506 633.25 10. 3110 280.46 27.8082 410.95 26.4819 634.78 0.0000 283.69 38.1072 413.71 33.6700 635.95 13.7646 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 35.3691 423. 72 0.0000 645.85 10.3693 285.90 0.0000 427.09 29.8349 657.76 23.1641 287.50 27.0388 427.87 27.7905 657.90 0.0000 290.67 32.2504 433.94 30.9924 661.66 22.0437 293.27 0.0000 439.40 37.3125 664.57 0.0000 351. 93 36.5919 453.88 22.9981 666.33 0.0000 295. 96 40.8379 463.37 25. 2271 666.50 0.0000 879.38 57.8577 468.07 30.5647 667.71 0.0000 299.98 52.7427 473.00 0.0000 677.62 11.3897 300.09 52.7472 475.06 27. 5118 685.70 0.0000 300.13 38.6193 476.78 19.0649 695.00 0.0000 301.36 41.4863 477.60 16.9544 696. 49 19.4293 302.85 55.6942 482.18 18.0601 696.51 19.4299 256.23 56.7126 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.0863 306.78 30.3008 497.08 19.2799 697.49 22.0879 308.46 36.9775 505.52 11. 2981 702.65 22.6672 311. 90 38.9780 507.63 0.0000 706.68 31. 0416 316.51 40.0706 511. 00 14.5688 711.68 18.2825 319.41 0.0000 514.00 12.9707 720.70 0.0000 320.08 0.0000 514.00 12.9707 721. 93 0.0000 321. 04 31.5928 520.40 26.0293 722.78 19.9979 323.87 33.5794 520.69 0.0000 722. 91 19.9992 325.23 43.2175 522.65 0.0000 723. 31 22.8602 328.76 0.0000 527.90 0.0000 724 .19 17.1510 333.37 33.3345 528.26 25.0468 727.33 15.2050 333.97 36.2488 529.59 17.4362 733.00 14.3433 334.37 43. 5114 529.87 0.0000 735.93 17.0529 338.28 29.0912 531.02 0.0000 333.97 12.5730 338.32 29.0918 537.26 0.0000 739.50 0.0000 311. 90 29.1376 546.56 0.0000 747.24 16.2285 340.48 29.1376 552.55 23.1542 748.06 14.4297 340.55 0.0000 563.25 17.7357 752.31 20.7778 344.28 30.6784 569.33 22.2355 753.82 0.0000 345.93 46.8037 946.00 22.2380 756.73 23.5284 351.06 38.1669 569.70 21.1276 756.80 23.5292 351. 93 38.1907 583.19 14.5509 884.68 19.9650 Page 2970 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 24.5198 1274.44 22.6315 1620.50 2.7681 766.42 21. 8005 1001.03 16.7525 1621.92 5.5377 766.84 19.0787 1002.74 19. 7192 1678.03 0.0000 772. 60 0.0000 1004.73 17.7583 1690.97 1.8724 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 .3.8000 778.90 10.2228 1028.54 0.0000 1063.66 4.7551 783.70 0.0000 1037.84 6.3785 1771. 35 2.8538 785.37 8.7838 1038.76 0.0000 1791.20 0.0000 792.07 22.9332 631.29 4.7968 1808.65 0.9581 794.95 12.8563 1048.07 0.0000 1810.72 0.0000 795.86 9.1864 1049.04 14.6676 1836.06 3.8525 810.06 20.3175 1050.41 13.0063 810.29 23.0896 1063.66 18.0802 344.28 23. 0911 1077.00 0.0000 810.76 22.1697 1077.34 11.0933 815.77 0.0000 1085.87 8.0884 1048.07 0.0000 1093.63 11. 3490 832.01 7.4478 1099.45 11. 3682 834.85 12 .1153 1112. 07 13.2436 835.71 17. 7122 1112.84 15.2847 836.80 0.0000 1115. 54 8.1582 846.75 0.0000 1120.29 12.2534 846. 77 20.5908 1120.55 12.2542 856.80 0.0000 1221.41 12.2571 860.56 15.9894 1129. 67 10.9212 871.09 10.5731 1131. 51 0.0000 873.19 9.0694 1147.95 0.0000 875.33 0.0000 1173.23 10.3638 879.38 9.0888 1177.95 19.7167 880.51 4.5461 1189.05 15.6125 883.24 6.6362 1204.77 9.4076 884.68 9.4849 1221.41 18.8987 889.28 8.5501 1231. 02 16.8418 894.76 10.4696 1235.36 0.0000 898.04 10.4814 1238.28 13.4992 900. 72 15.2598 1260.41 0.0000 903.28 12.4093 1271. 87 9.5746 911.20 15.3140 1274.44 14.9041 912.08 15.3184 1274.54 14.9041 923.98 0.0000 1291.59 13.8998 926.50 9.6204 1298.22 0.0000 929 .11 7.7029 1312 .11 0.0000 937.49 10.8141 1332.49 10.8026 944.13 0.0000 1362.66 0.0000 946.00 15.4922 1365.19 7.6225 949.00 11. 6305 1368. 63 0.0000 667. 71 0.0000 1384.29 10.9393 962.31 15.5742 1408.01 4.4004 964. 08 19.4788 1457.56 0.0000 966 .17 15.5938 1460.82 7.7960 911. 20 12.4863 1489.16 6.7255 968. 97 12.4863 1505.03 11. 2488 983.53 0.0000 1584.12 10.0719 984.45 0.0000 1596.21 0.0000 Page 2971of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:02:43.73 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM09.CNF;335 Background date : Z-OCT-2016 11:00:29. Sample date 9-DEC-2015 14:00:00. Acquisition date : 3-0CT-2016 08:01:44. Sample ID G405235004 Sample quantity l.48940E+02 GRAM Detector name : GAM09 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 0 2 0 3 4 4 4 5 0 6 0 7 0 8 . 0 9 0 10 4 11 4 12 0 13 . 1 14 1 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 2972 of 5809 Energy 58.87 63.49* 74.93 77.15 83.38* 87.17 185.97* 190.86 209.28 238.68* 241.57 295.43* 299.56 301.06 327.62 338.35* 352.00* 438.80 462. 68 510.90* 582.98* 592.66 609.23* 661. 71 701.42 727.52 752. 96 768.41 795.16 808.19 820.39 861.30 872.46 910.79* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 42 24 86 149 16 116 74 16 36 428 116 146 33 25 32 89 264 16 40 32 147 35 173 72 18 53 20 24 28 17 7 11 17 90 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 77 163 189 129 126 153 148 79 89 69 96 58 44 34 54 77 91 24 30 64 24 16 52 17 24 28 33 13 7 3 10 14 19 6 1. 95 0.93 1. 03 0.78 0.99 1.14 0.94 1. 00 0.82 0.93 1. 61 1.10 1.16 1.16 2.41 1. 52 1.29 0.52 1. 07 2.16 1. 38 3.82 1.10 1. 64 1. 39 1. 63 3.45 0.82 1.15 0.73 0.62 2.20 0.94 1. 73 117.40 126.66 149.54 153.99 166.45 174.03 371. 72 381.50 418.36 477.18 482. 96 590.73 599.00 602.00 655.13 676.60 703.92 877.59 925.37 1021.86 1166. 08 1185.46 1218.60 1323. 62 1403.06 1455.29 1506.21 1537.12 1590.64 1616.71 1641.13 1722. 98 1745.32 1822.02 114 124 146 146 165 170 367 378 415 473 473 585 596 596 651 671 699 874 919 1013 1159 1179 1212 1319 1396 1447 1497 1532 1586 1613 1636 1717 1736 1816 7 l.17E-02 37.9 9 6.78E-03 97.6 16 2.39E-02 25.8 16 4.15E-02 14.l 6 4.36E-03117.2 8 3.23E-02 20.7 11 2.06E-02 35.4 7 4.57E-03 92.7 7 9.88E-03 47.2 15 l.19E-01 5.8 15 3.21E-02 21.7 10 4.07E-02 12.9 12 9.24E-03 38.1 12 7.00E-03 50.4 10 8.75E-03 46.8 11 2.48E-02 22.0 12 7.34E-02 9.5 9 4.36E-03 62.4 12 l.12E-02 31.3 17 8.82E-03 67.1 14 4.09E-02 11.1 13 9.70E-03 29.2 14 4.82E-02 11.9 11 l.99E-02 16.2 14 4.99E-03 62.9 16 l.47E-02 26.3 17 5.66E-03 69.0 10 6.56E-03 36.5 10 7.71E-03 26.4 8 4.63E-03 31.8 8 l.95E-03 86.5 11 3.02E-03 73.0 16 4.75E-03 67.3 12 2. 51E-02 12. 2 Fit 4.15E+OO 1.17E+OO 2.17E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 964.44 21 10 1. 25 1929.37 1926 7 5.86E-03 33.3 36 0 968. 67 40 21 1. 22 1937.82 1933 10 1. llE-02 26. 3 37 0 112.0. 29 50 11 1. 03 2241.21 2233 .15 l.39E-02 20.3 38 0 1183 .15 12 5 1. 27 2367.01 2363 9 3.35E-03 43.2 39 0 1216.65 23 9 2.98 2434.04 2428 12 6.46E-03 33.0 40 0 1220. 72 12 4 1.10 2442.17 2439 7 3.19E-03 40.0 41 1 1224.31 17 3 1. 98 2449.36 2446 19 4.80E-03 24.7 1.13E+OO 42 1 1226.95 18 3 1. 98 2454.64 2446 19 4.99E-03 39.4 43 1 1230.12 23 0 1. 80 2461.00 2446 19 6.30E-03 21. 6 44 0 1239.21 10 20 0.56 2479.18 2473 9 2.78E-03 89.8 45 0 1460.26* 352 14 1. 63 2921. 51 2914 14 9.77E-02 5.9 46 0 1542.51 6 2 1. 20 3086.11 3082 7 1. 79E-03 51. 7 47 0 1763.43* 29 0 1. 85 3528.19 3522 11 7.94E-03 20.2 Flag: "*" = Peak area was modified by background subtraction Page 2973 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:02:46 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 9-DEC-2015 14:00:00 G405235004 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:01:44 148.94 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA9 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 ps:....214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 2974 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.146E+00 .1.398E+Ol 1.398E+Ol 11. 70 OK NB-94 702.65 99.81* 2.061E+OO 4.576E-02 4.576E-02 125.83 OK 871.09 99.89 1. 740E+OO 5.040E-02 5.040E-02 134.51 OK CD-109 88.03 3.70* 4.855E+OO 3.083E+OO 4.830E+OO 55.48 OK SN-126 64.28 9.60 2.292E+OO 7.198E-01 7.198E-01 195.25 OK 86.94 8.90 4.855E+OO 1.282E+OO 1.282E+OO 55.48 OK 87.57 37.00* 4.855E+00 3.083E-01 3.083E-01 55.48 OK BA-137M 661.66 89.90* 2.157E+OO l.943E-01 l.980E-01 32.30 OK CS-137 661.66 85.10* 2.157E+OO 2.053E-01 2.092E-01 32.30 OK TL-208 277.37 6.60 4.352E+OO Line Not Found Absent 583.19 85.00* 2.382E+OO 3.877E-01 3.877E-01 22.10 OK 860.56 12.50 1. 757E+OO 2.538E-01 2.538E-01 145. 96 OK BI-211 72. 87 1. 23 3.448E+OO Line Not Found Absent 351. 06 12.92* 3.588E+OO 1.803E-01 1.803E-01 546.38 OK PB-212 74.82 10.28 3.682E+OO 8.364E-01 8.364E-01 91. 68 OK 77.11 17.10 3.923E+OO 1.421E+OO 1. 421E+OO 28.16 OK 238.63 43.60* 4.882E+OO 1.167E+OO l.167E+OO 11. 52 OK 300.09 3.30 4.092E+00 1.399E+OO l.399E+OO 76.19 OK BI-214 609'. 32 45.49* 2.301E+OO 8.801E-01 8.804E.'...Ol 23.73 OK 1120.29 14.92 1.429E+OO 1.171E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 OK PB-214 74.82 5.80 3.669E+OO Line Not Found <<INT Reject 77 .11 9.70 3.923E+OO 2.506E+OO 2.507E+OO 28.16 OK 87.09 3.41 4.849E+OO Line Not Found <<INT Reject 242.00 7 .. 25 4.832E+OO Line Not Found <<INT Reject 295.22 18.42 4.139E+00 1.093E+OO 1.093E+OO 25.74 OK 351. 93 35.60* 3.588E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.301E+OO 8.801E-01 8.804E-01 23.73 OK 1120.29 14.92 1. 429E+OO 1.171E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 OK RA-224 240.99 4.10* 4.839E+OO 1.444E+OO 1.444E+OO 106. 96 OK RA-226 609.32 45.49* 2.301E+OO 8.801E-01 8.804E-01 23.73 OK 1120. 29 14.92 l.429E+OO 1.171E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 OK AC-228 105.21 1.10 5.896E+OO Line Not Found Absent 338.32 11. 27 3.706E+OO l.201E+00 1.201E+OO 44.00 OK 794.95 4.25 1. 869E+OO 1.809E+OO 1.809E+OO 52.80 OK 835. 71 1. 61 1. 799E+OO Line Not Found Absent 911. 20 25.80* 1.682E+OO 1.062E+OO 1.062E+OO 24.49 OK 968.97 15.80 1.603E+OO 8.012E-01 8.012E-01 52.66 OK RA-228 105.21 1.10 5.896E+OO Line Not Found Absent 338.32 11. 27 3.706E+OO 1.201E+OO 1.201E+OO 44.00 OK 794.95 4.25 1.869E+OO 1.809E+OO 1.809E+OO 52.80 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO l.062E+00 1.062E+OO 24.49 OK 968.97 15.80 1.603E+OO 8.012E-01 8.012E-01 52.66 OK TH-228 74.82 10.28 3.682E+OO 8.364E-01 8.364E-01 91. 68 OK 77 .11 17.10 3.923E+OO 1.421E+OO 1. 421E+OO 28.16 OK 238.63 43.60* 4.882E+OO 1.167E+OO 1.167E+OO 11. 52 OK Page 2975 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 . 3. 30 4.092E+OO 1.399E+OO 1.399E+OO 76.19 OK TH-230 609.32 45.49* 2.301E+OO 8.801E-01 8. 801E-01 23.73 OK 1120.29 14.92 1. 429E+OO l.171E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9. 661E-01 9.205E-01 9.205E-01 40.37 OK PA-231 283.69 1. 70 4.275E+OO Line Not Found Absent 301.36 5.35* 4.076E+OO 6.560E-01 6.560E-01 100.87 OK TH-232 105.21 1.10 5.896E+OO Line Not Found Absent 338.32 11. 27 3.706E+OO 1. 201E+OO 1.201E+OO 44.00 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 1.062E+OO 1.062E+OO 24.49 OK 968. 97 15.80 1.603E+OO 8.012E-01 8.012E-01 52.66 OK U-234 609.32 45.49* 2. 301E+OO 8.801E-01 8.801E-01 23.73 OK 1120.29 14.92 1.429E+OO 1.171E+OO 1.171E+OO 40.66 OK 1764.49 15.30 9.661E-01 9.205E-01 9.205E-01 40.37 OK AM-241 59.54 35.90* 1. 701E+OO 4.489E-01 4.495E-01 75.85 OK AM-243 43.53 5.90 1. 969E-01 Line Not Found Absent 74.66 67.20* 3.682E+OO l.279E-01 l.280E-01 91. 68 OK ANH-511 511. 00 100.00* 2.647E+OO 6.485E-02 6.485E-02 134.22 OK Flag: "*" Key line Page 2976 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:02:49.39 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l *
  • Acquisition date 3-0CT-2016 08:01:44 Sensitivity : 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 9-DEC-2015 14:00:00 Analyst initials: MXRl *
  • Sample ID G405235004 Sample Quantity 1.4894E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1. 398E+Ol 1.603E+OO 5.756E-01 NB-94 4.576E-02 5.643E-02 5.494E-02 CD-109 4.830E+OO 2.626E+OO 2.236E+00 SN-126 3.083E-01 1. 67 6E-01 1.268E-01 BA-137M l.980E-01 6.270E-02 6.185E-02 CS-137 2.092E-01 6.623E-02 6.534E-02 TL-208 3.877E-01 8.398E-02 5.989E-02 BI-211 1.803E-01 9.657E-01 3. 372E-01 PB-212 1.167E+OO 1.317E-01 9.158E-02 BI-214 8.804E-01 2.048E-01 1. 088E-01 PB-214 1.159E+OO 2.166E-01 3.510E-01 RN-222 8.804E-01 2.048E-01 1.088E-01 RA-224 1.444E+OO 1.514E+OO 9.818E-01 RA-226 8.804E-01 2.048E-01 1.088E-01 AC-228 1.062E+OO 2.549E-01 2.386E-01 RA-228 1.062E+OO 2.549E-01 2.386E-01 TH-228 1.167E+OO 1.317E-01 9.158E-02 TH-230 8.801E-01 2.047E-01 1.088E-01 PA-231 6.560E-01 6.485E-01 7.231E-01 TH-232 1.062E+OO 2.549E-01 2.386E-01 U-234 8.801E-01 2.047E-01 1.088E-01 AM-241 4.495E-01 3.342E-01 3.277E-01 AM-243 1. 28 OE-01 1.150E-01 1.048E-01 ANH-511 6.485E-02 8.530E-02 4.609E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM BE-7 -1.312E+OO 1.196E+Ol 2.345E+Ol NOT IDENT. NA-22 2.943E-02 3.671E-02 8.789E-02 NOT IDENT. NA-24 O.OOOE+OO l.883E+41 O.OOOE+OO SHORT HLIF AL-26 -5.207E-03 2.342E-02 4.981E-02 NOT IDENT. SC-46 -7.557E-02 3.229E-01 6.092E-01 FAIL ABUN V-48 O.OOOE+OO 1.251E+04 O.OOOE+OO SHORT HLIF Page 2977 of 5809 CR-51 O.OOOE+OO 4.078E+02 O.OOOE+OO SHORT HLIF MN-54 7.091E-03 6.386E-02 l.250E-01 NOT IDENT. C0-56 -4.387E-02 4.399E-01 8.425E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.608E-02 3.948E-02 7.496E-02 NOT IDENT. C0-58 l.278E-01 4.763E-01 9.224E-01 NOT IDENT. FE-59 -7.773E+OO 8.275E+OO l.291E+Ol NOT IDENT. C0-60 -2.285E-02 2.699E-02 4.509E-02 NOT IDENT. ZN-65 -8. 201E-03 1.538E-01 2.637E-01 NOT IDENT. GE-68 -3.959E-01 2.345E+OO .4. 453E+OO NOT IDENT. AS-73 7.034E+OO 1.179E+Ol 2.556E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.264E+03 O.OOOE+OO SHORT HLIF SE-75 1.159E-01 l.817E-01 3.649E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 731E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.308E+02 O.OOOE+OO SHORT HLIF RB-83 5.138E-01 6.149E-01 l.340E+OO NOT IDENT. KR-85 4. 621E+OO 6.934E+OO 1.360E+Ol NOT IDENT. SR-85 4.825E-01 7.244E-01 1.420E+OO NOT IDENT. RB-86 O.OOOE+OO 2. 671E+04 O.OOOE+OO SHORT HLIF Y-88 8.201E-02 1.545E-01 4.203E-01 NOT IDENT. Y-91 3.388E+02 5.518E+o2 l.185E+03 NOT IDENT. NB-95 -2.377E-01 8.955E-01 l.468E+OO NOT IDENT. NB-95M 3.039E-01 2.355E+OO 4.109E+OO NOT IDENT. ZR-95 2.840E-01 1.845E+OO 3.234E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.326E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.655E-02 2.779E-02 4.988E-02 NOT IDENT. RH-102 7.622E-03 5.477E-02 1.104E-01 NOT IDENT. RU-103 4.191E+OO 5.418E+OO 1.168E+Ol FAIL ABUN RH-106 4.606E-02 3.733E-01 7. 7 51E-01 NOT IDENT. RU-106 4.606E-02 3.733E-01 7.751E-01 NOT IDENT. AG-108M 2.466E-02 2.478E-02 5.507E-02 NOT IDENT. AG-110M -6.962E-02 8.794E-02 l.452E-01 NOT IDENT. SN-113 -2.848E-02 2.040E-01 4.059E-01 NOT IDENT. CD-115 O.OOOE+OO 2.022E+39 O.OOOE+OO SHORT HLIF SN-117M 0.000E+OO 7.413E+04 O.OOOE+OO SHORT HLIF TE-123M 3.041E-02 l.078E-01 2.135E-01 NOT IDENT. SB-124 7.987E-01 1.642E+OO 4.128E+OO NOT IDENT. SB-125 -2.940E-02 9.972E-02 l.932E-01 FAIL ABUN TE-125M 2.234E+02 2.220E+02 4. 761E+02 NOT IDENT. I-126 0.000E+OO 7.250E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.274E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1. 679E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.399E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.933E+26 O.OOOE+OO SHORT HLIF BA-133 l.473E-03 3.922E-02 6.709E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 6.121E-02 l.158E-01 FAIL ABUN CS-135 -1.026E-01 l.337E-01 2.271E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.525E+05 O.OOOE+OO SHORT HLIF CE-139 -3.435E-04 1.007E-01 l.924E-01 NOT IDENT. BA-140 0.000E+OO 1.062E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.202E+05 O.OOOE+OO SHORT HLIF CE-141 6.175E-01 2.076E+Ol 4.018E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.514E+41 O.OOOE+OO SHORT HLIF CE-144 -1. 473E-01 3. 011E-01 5.628E-01 NOT IDENT. PM-144 5.270E-03 4.419E-02 8.239E-02 NOT IDENT. PR-144 4.725E-01 3.840E+OO 7.163E+OO NOT IDENT. PM-146 1.615E-02 3.930E-02 8.246E-02 NOT IDENT. ND-147 O.OOOE+OO 2.882E+07 O.OOOE+OO SHORT HLIF PM-147 -2.104E+02 6.816E+02 l.307E+03 NOT IDENT. PM-149 0. 'OOOE+OO 3.252E+40 O.OOOE+OO SHORT HLIF EU-150 -l.637E-02 2.736E-02 4.185E-02 FAIL ABUN EU-152 -7.932E-03 8.013E-02 1.466E-01 FAIL ABUN GD-153 5.437E-03 1.603E-01 3.174E-01 'NOT IDENT. EU-154 6.543E-02 9.358E-02 2.185E-01 FAIL ABUN EU-155 1.214E-01 9.804E-02 2 .110E-01 FAIL ABUN TB-160 l.399E-01 1.814E+OO 3.562E+OO FAIL ABUN H0-166M l.280E-02 5.584E-02 l.121E-01 FAIL ABUN TM-171 6.161E+OO 3.042E+Ol 6.404E+Ol NOT IDENT. HF-172 -6.209E-02 1. 7 63E-01 3.368E-01 FAIL ABUN LU-172 2.174E-03 8.933E-02 1.675E-01 FAIL ABUN LU-176 2.479E-03 2.245E-02 4.216E-02 FAIL ABUN HF-181 -5.894E-01 3.197E+OO 6.381E+OO FAIL ABUN Page 2978 of 5809 TA-182 9.666E-01 7. 572E-01 1.821E+OO FAIL ABUN RE-183 O.OOOE+OO 6.730E+OO 7.122E+OO FAIL ABUN RE-184 -8.777E-02 3.088E+Ol 5.919E+Ol NOT IDENT. W-188 8.756E+Ol 8.965E+Ol 1.804E+02 FAIL ABUN IR-192 -5.684E-02 4. 725E-01 8.544E-01 FAIL ABUN HG-203 -l.680E+OO 2.336E+OO 3.975E+OO NOT IDENT. BI-207 -8.270E-04 3.599E-02 7.363E-02 FAIL ABUN PB-210 6.344E-01 6.095E+OO 1. 271E+Ol NOT IDENT. PB-211 -1. 7 63E-01 5.784E-01 1.130E+OO NOT IDENT. BI-212 O.OOOE+OO 1.064E+OO 1..38 6E+OO FAIL ABUN RN-219 6.745E-02 3.160E-01 6.557E-01 NOT IDENT. RA-223 -4.703E-02 5.776E-01 9.710E-01 FAIL ABUN AC-227 -8.334E-02 2.338E-01 4.178E-01 FAIL ABUN TH-227 -8.334E-02 2.338E-01 4.178E-01 FAIL ABUN TH-229 2.894E-01 4.550E-01 8.509E-01 FAIL ABUN TH-231 -4.703E-02 5.776E-01 9.710E-01 FAIL ABUN PA-233 -1.322E-02 5.324E-02 9. 572E-02 FAIL ABUN PA-234 3.338E-02 2.817E-01 5. 511E-01 NOT IDENT. PA-234M -3.346E-01 4.292E+OO 8.503E+OO NOT IDENT. TH-234 1. 868E+OO 3.573E+OO 3.066E+OO FAIL ABUN U-235 -2.460E-02 1.600E-01 3.047E-01 FAIL ABUN NP-237 -1.322E-02 5.324E-02 9. 572E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 898E+41 O.OOOE+OO SHORT HLIF U-238 1. 868E+OO 3.573E+OO 3.066E+OO FAIL ABUN NP-239 -4.922E-02 2.028E-01 3.920E-01 NOT IDENT. PU-239 2.068E+02 2.724E+02 5.608E+02 NOT IDENT. CM-243 -5. 301E-02 8.741E-02 1.649E-01 NOT IDENT. BK-247 2.268E-03 6.609E-02 1.239E-01 FAIL ABUN CM-247 1.361E-02 2.862E-02 6.109E-02 NOT IDENT. CF-249 -1.180E-02 3.731E-02 6.494E-02 NOT IDENT. CF-251 5.653E-02 1. 029E-01 2.054E-01 NOT IDENT. Page 2979 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:02:45.10 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 339 10.66* 1.146E+OO 1.398E+Ol 1.398E+Ol 11. 70 NB-94 702.65 19 99.81* 2.061E+OO 4.576E-02 4.576E-02 125.83 871.09 17 99.89 1. 740E+OO 5.040E-02 5.040E-02 134.51 CD-109 88.03 146 3.70* 4.855E+OO 4.090E+OO 6.408E+OO 41. 34 SN-126 64.28 31 9.60 2.292E+OO 7.198E-01 7.198E-01 195.25 86.94 146 8.90 4.855E+OO 1.701E+OO 1. 701E+OO 41. 34 87.57 146 37.00* 4.855E+OO 4.090E-01 4.090E-01 41. 34 BA-137M 661. 66 75 89.90* 2.157E+OO 1.943E-01 1. 980E-01 32.30 CS-137 661.66 75 85.10* 2.157E+OO 2.053E-01 2.092E-01 32.30 TL-208 277.37 ------6.60 4.352E+OO ------Line Not Found ------583.19 156 85.00* 2.382E+OO 3.877E-01 3.877E-01 22.10 860.56 11 12.50 1. 757E+OO 2.538E-01 2.538E-01 145. 96 BI-211 72.87 ------1.23 3.448E+OO ------Line Not Found ------351. 06 293 12.92* 3.588E+OO 3 .191E+OO 3 .191E+OO 19.07 PB-212 74.82 109 10.28 3.682E+OO 1.453E+OO 1.453E+OO 51. 64 77 .11 189 17.10 3.923E+OO 1.421E+OO 1.421E+OO 28.16 238.63 493 43.60* 4.882E+OO 1.167E+OO 1.167E+OO 11. 52 300.09 37 3.30 4.092E+OO 1.399E+OO 1.399E+OO 76.19 BI-214 609.32 183 45.49* 2. 301E+OO 8. 801E-01 8.804E-01 23.73 1120.29 50 14.92 1.429E+OO 1.171E+OO 1. l 71E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 PB-214 74.82 109 5.80 3.682E+OO 2.575E+OO 2.576E+OO 51. 64 77 .11 189 9.70 3.923E+OO 2.506E+OO 2.507E+00 28.16 87.09 146 3.41 4.855E+OO 4.438E+00 4.440E+OO 41. 34 242.00 133 7.25 4.839E+OO 1.909E+OO 1.910E+OO 43.31 295.22 165 18.42 4 .139E+OO 1.093E+OO 1.093E+OO 25.74 351. 93 293 35.60* 3.588E+00 l.158E+00 1.159E+OO 19.07 RN-222 609.32 183 45.49* 2. 301E+OO 8.801E-01 8.804E-01 23.73 1120.29 50 14.92 l.429E+00 l.171E+OO 1.171E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 RA-224 240.99 133 4.10* 4.839E+OO 3.376E+OO 3.376E+OO 43.31 RA-226 609.32 183 45.49* 2.301E+OO 8.801E-01 8.804E-01 23.73 1120.29 50 14.92 l.429E+OO l .171E+OO 1.171E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.208E-01 40.37 AC-228 105.21 ------1.10 5.896E+OO ------Line Not Found ------338.32 100 11. 27 3.706E+OO 1.201E+OO l.201E+OO 44.00 794.95 29 4.25 1.869E+OO 1. 809E+OO 1.809E+OO 52.80 835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911.20 91 25.80* 1.682E+OO 1. 062E+00 1.062E+OO 24.49 968. 97 40 15.80 l.603E+00 8.012E-01 8.012E-01 52.66 RA-228 105.21 ------1.10 5.896E+OO ------Line Not Found ------338.32 100 11. 27 3.706E+OO 1.201E+OO 1.201E+OO 44.00 794.95 29 4.25 1. 869E+OO 1.809E+OO 1.809E+OO 52.80 835. 71 ------1. 61 1. 799E+OO ------Line Not Found ------911.20 91 25.80* 1.682E+OO 1.062E+OO 1.062E+OO 24.49 968. 97 40 15.80 1.603E+OO 8.012E-01 8.012E-01 52.66 TH-228 74.82 109 10.28 3.682E+OO 1.453E+OO 1.453E+OO 51. 64 Page 2980 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235004 Acquisition date 3-0CT-2016 08:01:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 77 .11 189 17.10 3.923E+OO 1.421E+OO l.421E+OO 28.16 238.63 493 43.60* 4.882E+OO l.167E+OO 1.167E+OO 11.52 300.09 37 3.30 4.092E+OO 1.399E+OO 1.399E+OO 76.19 TH-230 609.32 183 45.49* 2.301E+OO 8.801E-01 8.801E-01 23.73 1120. 29 50 14.92 l.429E+OO l.171E+OO 1.171E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.205E-01 40.37 PA-231 283.69 ------1. 70 4.275E+OO ------Line Not Found ------301.36 28 5.35* 4.076E+OO 6.560E-01 6.560E-01 100.87 TH-232 105.21 ------1.10 5.896E+OO ------Line Not Found ------338.32 100 11. 27 3.706E+OO l.201E+OO 1.201E+OO 44.00 835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 91 25.80* 1.682E+OO l.062E+OO l.062E+OO 24.49 968.97 40 15.80 1.603E+OO 8.012E-01 8.012E-01 52.66 U-234 609.32 183 45.49* 2. 301E+OO 8.801E-01 8. 801E-01 23.73 1120.29 50 14.92 1.429E+OO l .171E+OO 1.171E+OO 40.66 1764.49 27 15.30 9.661E-01 9.205E-01 9.205E-01 40.37 AM-241 59.54 54 35.90* 1. 701E+OO 4.489E-01 4.495E-01 75.85 AM-243 43.53 ------5.90 1. 969E-01 ------Line Not Found ------74.66 109 67.20* 3.682E+OO 2.223E-01 2.223E-01 51. 64 ANH-511 511. 00 34 100.00* 2.647E+OO 6.485E-02 6.485E-02 134.22 Flag: "*" Key line Page 2981of5809 Summary of Nuclide Activity Sample ID : G405235004 Acquisition date Page : 3 3-0CT-2016 08:01:44 Total number of lines in spectrum 47 Number of unidentified lines 11 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 NB-94 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-241 AM-243 ANH-511 Hlife 1.25E+09Y 20300.00Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 432.60Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 00 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.398E+Ol 4.576E-02 4.090E+OO 4.090E-01 l.943E-01 2.053E-01 3.877E-01 3.191E+OO 1.167E+OO 8.801E-01 1.158E+OO 8.801E-01 3.376E+OO 8. 801E-01 1. 062E+OO 1.062E+OO 1.167E+OO 8.801E-01 6.560E-01 1.062E+OO 8. 801E-01 4.489E-01 2.223E-01 6.485E-02 3.835E+Ol 3.835E+Ol Decay Corr pCi/GRAM 1.398E+Ol 4.576E-02 6.408E+OO 4.090E-01 l.980E-01 2.092E-01 3.877E-01 3 .191E+OO 1.167E+OO 8.804E-01 1.159E+OO 8.804E-01 3.376E+OO 8.804E-01 1.062E+OO 1. 062E+OO 1.167E+OO 8.801E-01 6.560E-01 1.062E+OO 8.801E-01 4.495E-01 2.223E-01 6.485E-02 4.068E+Ol 4.068E+Ol 76.60% Decay Corr 2-Sigma Error 0.164E+Ol 5.759E-02 2.649E+OO l.691E-01 0.640E-01 0.676E-01 0.857E-01 0.609E+OO 0 .134E+OO 2.089E-01 0.221E+OO 2.089E-01 1.462E+OO 2.089E-01 0.260E+OO 0.260E+OO 0 .134E+OO 2.089E-01 6.617E-01 0.260E+OO 2.089E-01 3.410E-01 1.148E-01 8.704E-02 "M" Manually accepted 2-Sigma %Error 11. 70 125.83 41. 34 41. 34 32.30 32.30 22.10 19.07 11. 52 23.73 19.07 23.73 43.31 23.73 24.49 24.49 11. 52 23.73 100.87 24.49 23.73 75.85 51. 64 134.22 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 2982 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235004 Acquisition date : 3-0CT-2016 08:01:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.38 20 158 0.99 166.45 165 6 4.36E-03 **** 4.53E+OO T 0 185.97 87 174 0.94 371. 72 367 11 2.06E-02 70.8 5.74E+OO T 0 190.86 19 92 1. 00 381.50 378 7 4.57E-03 **** 5.66E+OO 0 209.28 41 104 0.82 418.36 415 7 9.88E-03 94.3 5.35E+OO 0 327.62 35 61 2.41 655.13 651 10 8.75E-03 93.5 3.81E+OO T 0 438.80 17 26 0.52 877.59 874 9 4.36E-03 **** 2.99E+OO T 0 462.68 44 32 1. 07 925.37 919 12 1.12E-02 62.7 2.87E+OO T 0 592.66 37 17 3.82 1185.46 1179 13 9.70E-03 58.4 2.35E+OO 0 727. 52 55 29 1. 63 1455.29 1447 16 l.47E-02 52.6 2.00E+OO T 0 752. 96 21 34 3.45 1506.21 1497 17 5.66E-03 **** 1.95E+OO T 0 768.41 24 14 0.82 1537.12 1532 10 6.56E-03 73.l 1.92E+OO 0 808.19 17 3 0.73 1616.71 1613 8 4.63E-03 63.6 1. 85E+OO 0 820.39 7 10 0.62 1641.13 1636 8 1.95E-03 **** 1.82E+OO 0 964. 44 21 10 1. 25 1929.37 1926 7 5.86E-03 66.6 1. 61E+OO T 0 1183 .15 12 5 1.27 2367.01 2363 9 3.35E-03 86.4 1.37E+OO 0 1216.65 23 9 2.98 2434.04 2428 12 6.46E-03 66.1 1.34E+OO 0 1220.72 11 3 1.10 2442.17 2439 7 3.19E-03 79.9 l.33E+OO T 1 1224.31 17 3 1. 98 2449.36 2446 19 4.80E-03 49.5 1.33E+OO 1 1226.95 18 3 1. 98 2454.64 2446 19 4.99E-03 78.7 1.33E+OO 1 1230.12 22 0 1. 80 2461.00 2446 19 6.30E-03 43.2 1.32E+OO T 0 1239.21 10 20 0.56 2479.18 2473 9 2.78E-03 **** 1.32E+OO T 0 1542.51 6 1 1.20' 3086.11 3082 7 l.79E-03 **** 1.09E+OO Flags: "T" = Tentatively associated Page 2983 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:03:14.91 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l * *Acquisition date 3-0CT-2016 08:01:44 Sensitivity 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 9-DEC-2015 14:00:00 Nuclide Library : SOLID *
  • Sample ID G405235004 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4894E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 NB-94 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-241 AM-243 ANH-511 Le (pCi/GRAM 2.316E-01 2.408E-02 1.056E+OO 5.937E-02 2.726E-02 2.879E-02 2.649E-02 1.534E-01 4.244E-02 4. 772E-02 1.700E-01 4.772E-02 4.550E-01 4. 772E-02 1.033E-01 1.033E-01 4.244E-02 4.770E-02 3.289E-01 1.033E-01 4.770E-02 l.524E-01 4.944E-02 2.039E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 2984 of 5809 Le (pCi/GRAM l.054E+Ol 3.729E-02 0.000E+OO l.765E-02 2.566E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 2985 of 5809 5.502E-02 3.642E-01 O.OOOE+OO 3.460E-02 3.906E-01 5.570E+OO 1.637E-02 1. 096E-01 1.914E+OO 1.188E+Ol O.OOOE+OO 1. 674E-01 O.OOOE+OO O.OOOE+OO 6.039E-01 6.150E+OO 6.424E-01 O.OOOE+OO l.586E-01 5.249E+02 6.418E-01 1.906E+OO 1.450E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.294E-02 4.873E-02 5.282E+OO 3.332E-01 3.332E-01 2.496E-02 5.990E-02 l.829E-01 O.OOOE+OO O.OOOE+OO 9.882E-02 1.618E+OO 8. 710E-02 2.216E+02 0.000E+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 3.016E-02 O.OOOE+OO 5.216E-02 1.036E-01 O.OOOE+OO O.OOOE+OO 8.953E-02 O.OOOE+OO O.OOOE+OO 1.871E+Ol O.OOOE+OO 2.602E-01 3.521E-02 3.062E+OO 3. 711E-02 O.OOOE+OO 6.033E+02 0.000E+OO 1.892E-02 6.572E-02 1. 480E-01 9. 296E-02 9.894E-02 l.547E+00 4.973E-02 2.975E+Ol l.547E-01 7.359E-02 l.919E-02 2.773E+OO 7.936E-01 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 CM-243 BK-247 CM-247 CF-249 CF-251 Page 2986 of 5809 3. 301E+OO 2.587E+Ol 8.199E+Ol 3.910E-01 l.816E+OO 3.049E-02 5.892E+OO 5.064E-01 6.410E-01 2.946E-01 4.392E-01 1.927E-01 1.927E-01 3. 965E-01 4.392E-01 4.320E-02 2.402E-01 3.725E+OO 1.446E+OO 1.419E-01 4.320E-02 O.OOOE+OO 1.446E+OO 1. 813E-01 2.624E+02 7.638E-02 5.670E-02 2.749E-02 2.923E-02 9.565E-02 FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:03:28.23 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235004.CNF;l *
  • Acquisition date 3-0CT-2016 08:01:44 Sensitivity : 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 9-DEC-2015 14:00:00 Nuclide Library : SOLID *
  • Sample ID G405235004 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity 1.4894E+02 GRAM *
  • Quantity Err(%) 1.3428E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-s igma) K-40 1.398E+Ol 1. 761E+OO 1. 761E+OO NB-94 4.576E-02 5.647E-02 5.647E-02 CD-109 4.830E+OO 2.663E+OO 2.663E+OO SN-126 3.083E-01 l.692E-01 l.692E-01 BA-137M l.980E-01 6.327E-02 6.327E-02 CS-137 2.092E-01 6.684E-02 6.684E-02 TL-208 3.877E-01 8.558E-02 8.558E-02 BI-211 1.803E-01 9.829E-01 9.829E-01 PB-212 l.167E+00 1.454E-01 1.454E-01 BI-214 8.804E-01 2.082E-01 2.082E-01 PB-214 1.159E+OO 2.218E-01 2.218E-01 RN-222 8.804E-01 2.082E-01 2.082E-01 RA-224 1.444E+OO 1. 521E+OO 1.521E+OO RA-226 8.804E-01 2.082E-01 2.082E-01 AC-228 1.062E+OO 2.606E-01 2.606E-01 RA-228 1.062E+OO 2.606E-01 2.606E-01 TH-228 l.167E+OO 1.454E-01 1.454E-01 TH-230 8.801E-01 2.081E-01 2.081E-01 PA-231 6.560E-01 6.634E-01 6.634E-01 TH-232 1.062E+OO 2.606E-01 2.606E-01 U-234 8.801E-01 2.081E-01 2. 081E-01 AM-241 4.495E-01 3.359E-01 3.359E-01 AM-243 1. 280E-01 l.159E-01 l.159E-01 ANH-511 6.485E-02 8.534E-02 8.534E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma ) BE-7 -1.312E+OO 1.196E+Ol l.198E+Ol NOT IDENT. NA-22 2.943E-02 3.673E-02 3.905E-02 NOT IDENT. NA-24 1.000E+41 1.933E+41 O.OOOE+OO SHORT HLIF AL-26 -5.207E-03 2.343E-02 2.354E-02 NOT IDENT. SC-46 -7.557E-02 3.229E-01 3.247E-01 FAIL ABUN V-48 l.075E+03 l.251E+04 l.252E+04 SHORT HLIF Page 2987 of 5809 CR-51 -2.238E+02 4.079E+02 4.202E+02 SHORT HLIF MN-54 7.091E-03 6.386E-02 6.394E-02 NOT IDENT. C0-56 -4.387E-02 4.399E-01 4.404E-01 FAIL ABUN MN-56 -l.000E+41 8.989E+41 O.OOOE+OO SHORT HLIF C0-57 -1.608E-02 3.948E-02 4.014E-02 NOT IDENT. C0-58 l.278E-01 4.763E-01 4.798E-01 NOT IDENT. FE-59 -7.773E+OO 8.294E+OO 9.004E+OO NOT IDENT. C0-60 -2.285E-02 2.700E-02 2.890E-02 NOT IDENT. ZN-65 -8.201E-03 1.538E-01 l.539E-01 NOT IDENT. GE-68 . -3.959E-01 2.345E+OO 2.352E+OO NOT IDENT. AS-73 7.034E+OO l.188E+Ol l.230E+Ol NOT IDENT. AS-74 l.324E+03 5.265E+03 5.299E+03 SHORT HLIF SE-75 l.159E-01 1.818E-01 1. 8 91E-01 NOT IDENT. BR-77 l.533E+38 l.322E+39 O.OOOE+OO SHORT HLIF SR-82 l.195E+02 6.308E+02 6.331E+02 SHORT HLIF RB-83 5.138E-01 6.189E-01 6.608E-01 NOT IDENT. KR-85 4.621E+OO 6.937E+OO 7.243E+OO NOT IDENT. SR-85 4.825E-01 7.246E-01 7.566E-01 NOT IDENT. RB-86 -6.350E+02 2.671E+04 2. 671E+04 SHORT HLIF Y-88 8. 201E-02 l.546E-01 1.590E-01 NOT IDENT. Y-91 3.388E+02 5.519E+02 5.726E+02 NOT IDENT. NB-95 -2.377E-01 8.956E-01 9.020E-01 NOT IDENT. NB-95M 3.039E-01 2.355E+OO 2.359E+OO NOT IDENT. ZR-95 2.840E-01 1.845E+OO l.849E+OO NOT IDENT. NB-97 -1.000E+41 2.193E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 3.295E+41 O.OOOE+OO SHORT HLIF M0-99 -4.049E+31 1.327E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 5.879E+41 O.OOOE+OO SHORT HLIF' RH-101 -2.655E-02 2.820E-02 3.063E-02 NOT IDENT. RH-102 7.622E-03 5.477E-02 5.488E-02 NOT IDENT. RU-103 4.191E+OO 5.421E+00 5.741E+OO FAIL ABUN RH-106 4.606E-02 3.733E-01 3.739E-01 NOT IDENT. RU-106 4.606E-02 3.733E-01 3.739E-01 NOT IDENT. AG-108M 2.466E-02 2.480E-02 2.718E-02 NOT IDENT. AG-110M -6.962E-02 8.801E-02 9.344E-02 NOT IDENT. SN-113 -2.848E-02 2.040E-01 2.044E-01 NOT IDENT. CD-115 l.572E+39 2.042E+39 O.OOOE+OO SHORT HLIF SN-117M 1.471E+04 7.415E+04 7.445E+04 SHORT HLIF TE-123M 3. 041E-02 l.078E-01 1. 086E-01 NOT IDENT. SB-124 7.987E-01 l.643E+OO 1.682E+OO NOT IDENT. SB-125 -2.940E-02 9. 972E-02 1.006E-01 FAIL ABUN TE-125M 2.234E+02 2.224E+02 2. 441E+02 NOT IDENT. I-126 7.169E+05 7.315E+05 7.997E+05 SHORT HLIF SB-126 8.367E+05 9.405E+05 1. 013E+06 SHORT HLIF SB-127 -3.384E+21 l.742E+22 O.OOOE+OO SHORT HLIF I-131 2.533E+09 4.401E+09 4.547E+09 SHORT HLIF I-132 -1.000E+41 1.857E+42 O.OOOE+OO SHORT HLIF TE-132 -1.554E+26 3.000E+26 O.OOOE+OO SHORT HLIF BA-133 1.473E-03 3.922E-02 3.922E-02 NOT IDENT. I-133 -l.000E+41 2.884E+41 O.OOOE+OO SHORT HLIF CS-134 1.183E-01 6.141E-02 8.133E-02 FAIL ABUN CS-135 -1. 026E-01 l.338E-01 l.416E-01 NOT IDENT. I-135 1.000E+41 1.184E+42 O.OOOE+OO SHORT HLIF CS-136 -1.122E+05 2.528E+05 2.578E+05 SHORT HLIF CE-139 -3.435E-04 l.007E-01 1.007E-01 NOT IDENT. BA-140 -5.276E+05 1.062E+06 1. 088E+06 SHORT HLIF LA-140 1.248E+03 2.202E+05 2.202E+05 SHORT HLIF CE-141 6.175E-01 2.076E+Ol 2.076E+Ol NOT IDENT. CE-143 -1.000E+41 l.517E+41 O.OOOE+OO SHORT HLIF CE-144 -1.473E-01 3.012E-01 3.085E-01 NOT IDENT. PM-144 5.270E-03 4.420E-02 4.426E-02 NOT IDENT. PR-144 4. 725E-01 3.840E+OO *3. 846E+OO NOT IDENT. PM-146 1.615E-02 3.932E-02 3.999E-02 NOT IDENT. ND-147 -2.097E+07 2.884E+07 3.035E+07 SHORT HLIF PM-147 -2.104E+02 6.816E+02 6.882E+02 NOT IDENT. PM-149 -1. 076E'+40 3.261E+40 O.OOOE+OO SHORT HLIF EU-150 -1.637E-02 2.737E-02 2.835E-02 FAIL ABUN EU-152 -7.932E-03 8.013E-02 8. 021E-02 FAIL ABUN GD-153 5.437E-03 1.603E-01 1.603E-01 NOT IDENT. EU-154 6.543E-02 9.362E-02 9.815E-02 FAIL ABUN EU-155 l.214E-01 9.842E-02 l.126E-01 FAIL ABUN TB-160 1.399E-01 1.814E+OO l.815E+OO FAIL ABUN H0-166M l.280E-02 5.585E-02 5.615E-02 FAIL ABUN TM-171 6.161E+OO 3.042E+Ol 3.055E+Ol NOT IDENT. HF-172 -6.209E-02 1. 766E-01 1. 788E-01 FAIL ABUN LU-172 2.174E-03 8.933E-02 8.933E-02 FAIL ABUN LU-176 2.479E-03 2.245E-02 2.248E-02 FAIL ABUN HF-181 -5.894E-01 3.197E+OO 3.208E+OO FAIL ABUN Page 2988 of 5809 TA-182 9.666E-01 7. 581E-01 8.744E-01 FAIL ABUN RE-183 9.053E+OO 6.876E+OO 7.996E+00 FAIL ABUN RE-184 -8.777E-02 3.088E+Ol 3.088E+Ol NOT IDENT. W-188 8.756E+Ol 9.018E+Ol 9.844E+Ol FAIL ABUN IR-192 -5.684E-02 4.725E-01 4.732E-01 FAIL ABUN HG-203 -1. 68 OE+OO 2.337E+OO 2.457E+OO NOT IDENT. BI-207 -8.270E-04 3.599E-02 3.599E-02 FAIL ABUN PB-210 6.344E-01 6.095E+OO 6.102E+OO NOT IDENT. PB-211 -1. 7 63E-01 5.785E-01 5.839E-01 NOT IDENT. BI-212 2.064E+OO l.069E+OO 1. 417.E+OO FAIL ABUN RN-219 6.745E-02 3.162E-01 3.176E-01 NOT IDENT. RA-223 -4.703E-02 5.776E-01 5.780E-01 FAIL ABUN AC-227 -8.334E-02 2.341E-01 2. 371E-01 FAIL ABUN TH-227 -8.334E-02 2.341E-01 2.371E-01 FAIL ABUN TH-229 2.894E-01 4.552E-01 4.736E-01 FAIL ABUN TH-231 -4.703E-02 5.776E-01 5.780E-01 FAIL ABUN PA-233 -l.322E-02 5.324E-02 5.358E-02 FAIL ABUN PA-234 3.338E-02 2.843E-01 2.847E-01 NOT IDENT. PA-234M -3.346E-01 4.292E+OO 4.295E+OO NOT IDENT. TH-234 l.868E+OO 3.597E+OO 3.695E+OO FAIL ABUN U-235 -2.460E-02 l.600E-01 l.604E-01 FAIL ABUN NP-237 -l.322E-02 5.324E-02 5.358E-02 FAIL ABUN NP-238 l.OOOE+41 l.898E+41 O.OOOE+OO SHORT HLIF U-238 l.868E+OO 3.597E+OO 3.695E+OO FAIL ABUN NP-239 -4.922E-02 2.029E-01 2. 041E-01 NOT IDENT. PU-239 2.068E+02 2.725E+02 2.880E+02 NOT IDENT. CM-243 -5.301E-02 8.755E-02 9.075E-02 NOT IDENT. BK-247 2.268E-03 6.610E-02 6.610E-02 FAIL ABUN CM-247 1. 361E-02 2.871E-02 2.936E-02 NOT IDENT. CF-249 -l.180E-02 3.732E-02 3.770E-02 NOT IDENT. CF-251 5.653E-02 1. 031E-01 l.062E-01 NOT IDENT. Page 2989 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 44.2373 87.09 72.3018 136.47 63.3131 45.60 48.4640 87.57 72.3787 140.51 0.0000 46.54 43.1295 88.03 94.6541 143.76 59.1933 49.72 0.0000 88.34 94.7184 144.24 57.2949 51. 35 50.9800 88.47 94.7455 145.44 60.3198 51. 87 47.8720 89. 96 77.4505 152.43 73.7423 52.39 53.5440 1093.63 135 .1493 153.25 0.0000 52.97 51. 2388 91.11 0.0000 323.87 58.1628 53.44 46.5024 92.59 75.2317 156.02 0.0000 54.07 57.8386 93.35 107.2662 158.56 0.0000 57.36 0.0000 94.56 120.8698 159.00 46.6572 57.53 51.9465 94.65 120.8915 162.33 52.8641 57.98 58.5162 94.67 120. 8967 162.66 0.0000 59.27 58.7348 94.87 104.0505 163.33 55.9359 59.32 58.7433 97.43 58 .1113 165.86 60.1447 59.54 58.7802 98.43 68.9799 176.31 56.9408 60. 96 44.2631 98.44 68.9811 176.60 0.0000 61.17 44.2893 99.53 61.0528 177.52 49.9039 62.93 69.2328 100 .11 67.4160 181.07 0.0000 63.29 69.3013 102.03 59.5532 181. 52 54.6037 63.58 69.3563 103.18 65 .1143 184.41 57.5492 64.28 69.4888 103.37 65.1385 143.76 57.6466 66.73 75.4984 105.21 56.2930 193.51 48.5145 67.24 82.2706 105.31 49.0388 197.03 54.2947 125.81 74.5749 106.12 47.2964 198.01 48.0882 67.75 75.7010 106.47 53.6992 201.83 52.5131 69.67 74.6816 109.28 41.1764 203.43 69.4513 70.83 90.8935 111. 00 74.3567 205.31 52.0297 72. 81 94.7316 111.76 0.0000 210.85 49.5399 72. 87 94.7461 114. 06 60.9299 215.65 45.9021 74.66 91. 7677 116. 30 0.0000 222 .11 48.3913 74.82 91. 8040 116. 74 55.6604 227.09 42.1724 74.97 91.8377 119.76 45.7012 227.38 47.5946 77 .11 92.3148 121.12 54.2250 228.16 0.0000 78.74 92.6741 121.22 54.2343 228.18 56.2982 79.69 92.8817 121. 78 56.1594 116.74 56.2982 80.12 68.8708 122.06 56.1868 235.69 52.3938 80.19 0.0000 122.92 41.2653 235. 96 50.9534 80.57 67.2193 123.07 45.0282 238.63 53.6536 81. 00 67.2865 265.00 47.8930 238.98 0.0000 81. 07 75.9258 125.81 49.0107 240.99 53.7881 81. 75 67.4038 127.23 63.3007 242.00 53.8457 83.79 72. 9277 127.91 54.8609 244.70 41.1415 84.00 72. 9623 129.30 54.0402 252.40 0.0000 85.43 73.1975 131.20 64.6735 252.80 41.1169 86.55 72.2154 133.02 59.1439 254.15 0.0000 86.79 72.2539 133. 52 60.1469 256.23 54.6420 86.94 72.2778 136.00 57.5139 260.90 0.0000 Page 2990 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 30.3626 355.39 0.0000 584.27 19.7302 264.80 35.9902 356.01 25.9889 595.83 0.0000 265.00 38.2469 364.49 0.0000 427.87 19.8994 268.22 50.7816 366.42 0.0000 602.52 0.0000 269.46 36.1553 372. 51 28.3773 604. 72 14.2444 270.03 47.4794 375.05 27.1959 607.14 17.1145 271.23 48.6663 377.52 23.5308 609.32 17.1335 273.65 0.0000 356.01 31.1073 610.33 17.1423 276.40 35.2600 388.16 32.4548 614.28 20. 0396 277.37 42.1230 388.63 0.0000 618.01 9.5610 277.60 40.9933 391.69 30.0359 620.36 18.1867 278.00 34.1739 264.66 28.5512 621. 93 11. 4956 279.20 51. 3199 401.81 23.5316 630.19 0.0000 279.54 36.5059 402.40 21.0195 631.29 17.3240 279.70 39.9336 404.85 29.4786 633.25 15.4141 280.46 38.8207 410.95 43.1392 634.78 0.0000 283.69 30.9221 413.71 23.7298 635.95 14.4702 284.31 0.0000 414.70 0.0000 636.99 o.o*ooo 285.41 37.8541 423. 72 0.0000 645.85 18.4178 285.90 0.0000 427.09 33.3585 657.76 19.0120 287.50 26.4344 427.87 32.5202 657.90 0.0000 290.67 18.4429 433.94 18.0456 661. 66 18.5593 293.27 0.0000 439.40 26.7359 664.57 0.0000 351. 93 38.5824 453.88 21.7667 666.33 0.0000 295. 96 38.6078 463.37 14. 0160 666.50 0.0000 879.38 25.5416 468.07 14.0576 667.71 0.0000 299.98 34.0984 473.00 0.0000 677.62 13.7790 300.09 34 .1011 475.06 25.5921 685.70 0.0000 300 .13 34.1029 476.78 33.5701 695.00 0.0000 301.36 34.1405 477.60 26.5161 696.49 10.4252 302.85 29.5236 482.18 16.8415 696. 51 10.4252 256.23 32.6792 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 11. 9189 306.78 32.7450 497.08 19.6783 697.49 11. 9199 308.46 43.3345 505.52 22.9247 702.65 16.9260 311. 90 32.8920 507.63 0.0000 706.68 16.4584 316.51 41. 27 94 511. 00 19.8422 711. 68 17.9956 319.41 0.0000 514.00 20.3293 720. 70 0.0000 320.08 0.0000 514.00 20.3293 7 21. 93 0.0000 321. 04 27.2311 520.40 17.2311 722. 78 12.0566 323.87 31. 6479 520.69 0.0000 722.91 12.0571 325.23 23.7634 522.65 0.0000 723.31 13.5670 328.76 0.0000 527.90 0.0000 724 .19 15.0800 333.37 22.3302 528.26 13.6652 727. 33 16.1081 333.97 41. 4904 529.59 22.7926 733.00 0.0000 334.37 39.9078 529.87 0.0000 735.93 15.1587 338.28 33.6302 531.02 0.0000 333.97 9 .1011 338.32 33. 6311 537.26 0.0000 739.50 0.0000 311. 90 32.0858 546.56 0.0000 747.24 13.7098 340.48 32.0858 552.55 24.9368 748.06 13.7148 340.55 0.0000 563.25 17.6509 752.31 20.3556 344.28 26.5527 569.33 24.2343 753.82 0.0000 345.93 22. 9620 946.00 24.2364 756.73 22.9431 351.06 33. 9772 569.70 19.5773 756.80 22.9440 351. 93 34. 0011 583.19 19.7191 884.68 15.3430 Page 2991of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 19. 9610 1274.44 14.5224 1620.50 4.9722 766.42 19. 9666 1001.03 12.3083 1621. 92 4.9738 766.84 16.8975 1002.74 14.5546 1678.03 0.0000 772. 60 0.0000 1004.73 13.4438 1690.97 2.0200 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0 .. 0000 1025.87 0.0000 17 6.4. 49 1.6415 778.90 11. 3227 1028.54 0.0000 1063.66 5.1361 783.70 0.0000 1037.84 9.0625 1771.35 3.0822 785.37 10.3210 1038.76 0.0000 1791.20 0.0000 792.07 13.9719 631.29 7.9525 1808.65 1.0354 794.95 10.3617 1048.07 0.0000 1810.72 0.0000 795.86 10.3658 1049.04 9.0957 1836.06 1. 0411 810.06 4.6917 1050.41 20.4741 810.29 4.6921 1063.66 5. 7117 344.28 4.6924 1077.00 0.0000 810.76 7.8217 1077.34 12. 6212 815.77 0.0000 1085.87 14.9561 1048.07 0.0000 1093.63 17.2998 832.01 18.9324 1099.45 25. 4196 834.85 16.8477 1112. 07 8.1200 835.71 13.6935 1112.84 6. 9614 836.80 0.0000 1115. 54 8.7091 846.75 0.0000 1120.29 13.9551 846.77 14.8106 1120.55 13.9561 856.80 0.0000 1221.41 13.9590 860.56 12.7632 1129. 67 12.8289 871.09 13.8823 1131. 51 0.0000 873.19 13.8934 1147.95 0.0000 875.33 0.0000 1173.23 15.0670 879.38 13.9262 1177.95 5.9167 880.51 7.5019 1189.05 11.1941 883.24 9.6552 1204.77 13.4180 884.68 15.0277 1221.41 3.5952 889.28 11.8276 1231.02 12.9788 894.76 10.7743 1235.36 0.0000 898.04 14.0241 1238.28 19.8690 900.72 12.9580 1260.41 0.0000 903.28 16.2128 1271.87 10.0285 911.20 14.0923 1274.44 5.4741 912.08 14.6393 1274.54 4.5618 923.98 0.0000 1291. 59 8.2502 926.50 9.8108 1298.22 0.0000 929.11 10. 9111 1312.11 0.0000 937.49 15.3216 1332.49 7.4146 944.13 0.0000 1362.66 0.0000 946.00 14.2706 1365 .19 12.1534 949.00 17.5827 1368.63 0.0000 667.71 0.0000 1384.29 6.5766 962. 31 19.8735 1408.01 4.'7260 964. 08 11.6002 1457.56 0.0000 966 .17 6.6335 1460.82 5.7466 911.20 13.2798 1489.16 1. 9288 968.97 13.2798 1505.03 5.8088 983.53 0.0000 1584.12 5.9176 984.45 0.0000 1596.21 0.0000 Page 2992 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:04:17.52 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM19.CNF;561 Background date : Z-OCT-2016 11:01:07. Sample date 10-DEC-2015 13:15:00 Acquisition date : 3-0CT-2016 08:02:09. Sample ID G405235005 Sample quantity 1.57331E+02 GRAM Detector name : GAM19 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.81 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 6 6 5 5 5 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 8 Page 2993 of 5809 Energy 53.91 63.56* 74.83* 77.19* 87.35 90.10 92.75* 185.62* 208.99 238.58* 241. 88 270.49 295.09* 300.17 326.32 338.70 351.79* 463.18 471.99 489.26* 510.87* 561. 21 569.64* 583.12* 609.18*

614.42* 661.60 665.45 727.26 757.10 763.15* 829.83 911. 02* 948.19 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 3 51 157 221 75 32 100 135 26 364 93 60 166 36 74 125 246 66 13 23 45 18 16 127 186 14 55 25 38 22 17 21 97 16 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 179 190 150 118 256 170 195 164 120 91 111 73 85 70 98 56 84 55 45 17 72 34 24 33 32 30 18 19 35 22 8 7 23 4 1. 51 0.74 1.16 1. 06 1. 56 1. 21 1. 73 1. 38 1. 26 1.14 1. 70 1. 20 1.18 1. 09 5.86 1. 70 1. 35 2.43 0.86 4.22 2.01 1. 39 1.19 1. 57 1. 59 0.83 1. 50 2.40 1. 59 2.86 1. 09 1. 22 2.05 3.21 108.59 127.90 150.45 155.17 175.52 181.00 186.31 372.14 418.88 478.09 484.71 541.94 591.15 601. 33 653.64 678.41 704.61 927.47 945.12 979.67 1022.91 1123.63 1140.49 1167.46 1219.62 1230.09 1324.50 1332.20 1455.87 1515.57 1527.69 1661.10 1823.55 1897.92 102 123 145 145 170 170 170 365 416 472 472 538 584 598 643 672 698 918 940 974 1014 1118 1136 1161 1213 1226 1320 1329 1448 1509 1523 1656 1817 1894 10 7.37E-04956.6 10 1. 43E-02 53. 2 17 4.35E-02 15.5 1.19E+OO 17 6.15E-02 10.6 23 2.08E-02 37.1 3.61E+OO 23 9.0lE-03 68.7 23 2.77E-02 31.3 14 3.74E-02 22.4 8 7.22E-03 75.6 18 1.0lE-01 6.9 1.84E+OO 18 2.58E-02 25.2 9 1. 68E-02 28. 7 13 4.60E-02 14.1 9 9.93E-03 44.9 18 2.07E-02 33.4 15 3.48E-02 15.8 12 6.83E-02 9.9 18 1.83E-02 29.7 10 3.61E-03100.4 11 6.41E-03 42.2 18 1.26E-02 51.6 11 5.12E-03 64.8 11 4.35E-03 98.9 12 3.52E-02 12.9 13 5.17E-02 9.9 9 3.94E-03 76.8 9 1.54E-02 19.2 9 6.99E-03 36.5 13 l.06E-02 37.0 14 6.24E-03 48.3 8 4.78E-03 38.6 10 5.75E-03 33.0 15 2.68E-02 15.1 15 4.33E-03 32.2 1.63E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235005 Acquisition date 3-0CT-2016 08:02:09 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 8 951. 23 17 9 1. 93 1904.00 1894 15 4.66E-03 38.1 36 2 962. 21 16 2 1. 73 1925.97 1923 12 4.46E-03 33.6 7.21E-01 .37 2 964. 22 26 12 1. 94 1930.00 1923 12 7.24E-03 32.8 38 0 969. 02 58 20 2.28 1939.60 1934 13 1. 60E-02 20. 6 39 0 1024.33 4 10 0.47 2050.27 2044 8 1.0lE-03160.1 40 0 1120.64 48 12 1.23 2242.97 2236 12 1.33E-02 20.5 41 0 1130.03 22 10 4.80 2261.75 2253 16 6.00E-03 41. 4 42 0 1197. 83 28 41 8.79 2397.43 2382 28 7.64E-03 69.3 43 5 1212.75 10 3 1. 49 2427.27 2426 11 2.65E-03 32.6 2.29E+OO 44 5 1215.68 17 5 1. 82 2433.14 2426 11 4.61E-03 30.9 45 0 1376.89 17 6 4.26 2755.69 2749 13 4.79E-03 38.5 46 0 1460.49 391 4 1. 98 2922.98 2916 15 1. 09E-01 5.2 47 0 1694.43 7 3 1. 47 3391.07 3384 10 2.00E-03 56.0 48 0 1764. 28* 43 0 2.21 3530.83 3523 15 1.19E-02 16.1 Flag: "*" = Peak area was modified by background subtraction Page 2994 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:04:21 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 10-DEC-2015 13:15:00 G405235005 Acquisition date : Sample quantity Sample geometLy : 3-0CT-2016 08:02:09 157.33 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA19 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 2995 of 5809 Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.81 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235005 Acquisition date 3-0CT-2016 08:02:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.161E+OO 1.461E+Ol 1.461E+Ol 10.35 OK AS-73 53.44 10.30* 2.017E+OO 8.281E-02 l.083E+001913.23 OK CD-109 88.03 3.70* 5.494E+OO 1.200E+OO 1.876E+OO 143.99 OK SN-126 64.28 9.60 3.338E+OO 1.024E+OO l.024E+OO 106.41 OK 86.94 8.90 5.494E+OO 4.987E-01 4.987E-01 143.99 OK 87.5';! 37.00* 5.494E+OO 1.200E-01 1.200E-01 143.99 OK BA-137M 661.66 89.90* 2.164E+OO 1.444E-01 1.471E-01 38.46 OK CS-137 661. 66 85.10* 2.164E+OO 1.526E-01 1.554E-01 38.46 OK TL-208 277.37 6.60 4.415E+OO Line Not Found Absent 583.19 85.00* 2.392E+OO 3.206E-01 3.206E-01 25.76 OK 860.56 12.50 1. 763E+OO Line Not Found Absent PB-212 74.82 10.28 4.545E+OO 1.445E+OO 1.445E+OO 47.20 OK 77 .11 17.10 4.754E+OO 1.710E+OO 1. 710E+OO 21.10 OK 238.63 43.60* 4. 960E+OO 9.499E-01 9.499E-01 13.81 OK 300.09 3.30 4 .141E+OO 1.443E+OO 1.443E+OO 89.83 OK BI-214 609.32 45.49* 2.310E+00 9.063E-01 9.066E-01 19.71 OK 1120.29 14.92 1.437E+OO 1.064E+OO 1.065E+00 41. 00 OK 1764.49 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 OK PB-214 74.82 5.80 4. 544E+OO . Line Not Found <<INT Reject 77 .11 9.70 4.754E+OO 3.015E+OO 3.016E+OO 21.10 OK 87.09 3.41 5.478E+OO Line Not Found <<INT Reject 242.00 7.25 4.908E+OO Line Not Found <<INT Reject 295.22 18.42 4.199E+OO 1.183E+00 1.183E+OO 28.12 OK 351. 93 35.60* 3.630E+00 1.032E+OO 1.033E+OO 19.83 OK RN-222 609.32 45.49* 2.310E+OO 9.063E-01 9.066E-01 19. 71 OK 1120.29 14.92 1.437E+OO 1.064E+OO 1.065E+OO 41. 00 OK 1764.49 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 OK RA-224 240.99 4.10* 4.910E+OO 5.045E-01 5.045E-01 284.33 OK RA-226 609.32 45.49* 2.310E+OO 9.063E-01 9.066E-01 19. 71 OK 1120.29 14.92 1.437E+OO 1.064E+OO 1.065E+OO 41. 00 OK 1764.49 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 OK AC-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.747E+OO 1.616E+OO l.616E+00 31. 60 OK 794.95 4.25 1. 875E+OO Line Not Found Absent 835.71 1. 61 1. 803E+OO Line Not Found Absent 911.20 25.80* 1.687E+OO 1.084E+00 1.084E+OO 30.29 OK 968. 97 15.80 1. 609E+OO 1.098E+OO 1.098E+OO 41. 21 OK RA-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.747E+OO 1.616E+OO 1.616E+OO 31.60 OK 794.95 4.25 1. 875E+OO Line Not Found Absent 835.71 1. 61 1.803E+OO Line Not Found Absent 911.20 25.80* 1.687E+OO 1.084E+OO 1.084E+OO 30.29 OK 968. 97 15.80 1.609E+OO 1.098E+OO 1.098E+OO 41. 21 OK TH-228 74.82 10.28 4.545E+OO 1.445E+OO 1.445E+OO 47.20 OK 77.11 17.10 4.754E+OO 1.710E+OO 1. 710E+OO 21.10 OK 238.63 43.60* 4. 960E+OO 9.499E-01 9.499E-01 13.81 OK 300.09 3.30 4 .141E+OO 1.443E+OO 1.443E+OO 89.83 OK TH-230 609.32 45.49* 2.310E+00 9.063E-01 9.063E-01 19.71 OK 1120.29 14.92 l.437E+OO 1.064E+OO 1.064E+OO 41. 00 OK Page 2996 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235005 Acquisition date 3-0CT-2016 08:02:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1764.49 15.30 9.862E-01 1.282E+OO l.282E+OO 32.20 OK PA-231 283.69 1. 70 4.336E+OO Line Not Found Absent 301.36 5.35* 4.141E+OO 8.901E-01 8.901E-01 89.83 OK TH-232 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.747E+00 1.616E+OO l.616E+OO 31. 60 OK 835.71 1. 61 l.803E+OO Line Not Found --r--Absent 911.20 25.80* 1.687E+00 1.084E+OO l.084E+OO 30.29 OK 968. 97 15.80 l.609E+OO 1.098E+OO 1.098E+OO 41.21 OK TH-234 63.29 3.70* 3.338E+OO 2.657E+OO 2.657E+OO 106.41 OK 92.59 4.23 5. 791E+OO 2.516E+OO 2.516E+OO 62.65 OK U-234 609.32 45.49* 2.310E+OO 9.063E-01 9.063E-01 19.71 OK 1120.29 14.92 1.437E+OO 1.064E+OO 1.064E+OO 41. 00 OK 1764.49 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 OK U-235 89. 96 3.47 5.653E+OO 1.024E+OO 1. 024E+OO 137.50 OK 93.35 5.60 5.791E+OO 1.900E+OO 1.900E+OO 62. 65 OK 143.76 10.96* 6.462E+OO Line Not Found Absent 163.33 5.08 6.216E+OO Line Not Found Absent 185.72 57.20 5.848E+OO 2.332E-01 2.332E-01 44.76 OK 205.31 5.01 5.506E+OO Line Not Found -----Absent U-238 63.29 3.70* 3.338E+OO 2.657E+OO 2.657E+OO 106.41 OK 92.59 4.23 5.791E+OO 2.516E+OO 2.516E+OO 62. 65 OK AM-243 43.53 5.90 5.190E-01 Line Not Found Absent 74.66 67.20* 4.545E+OO 2. 211E-01 2. 211E-01 47.20 OK ANH-511 511. 00 100.00* 2.662E+OO 8.853E-02 8.853E-02 103.14 OK Flag: "*" Key line Page 2997 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:04:23.25 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l *
  • Acquisition date 3-0CT-2016 08:02:09 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.81 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:15:00 Analyst initials: MXRl *
  • Sample ID G405235005 Sample Quantity 1.5733E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.461E+Ol l.481E+OO AS-73 1.083E+OO 2.030E+Ol CD-109 1.876E+OO 2.648E+00 SN-126 1.200E-01 1.693E-01 BA-137M 1.471E-01 5.546E-02 CS-137 l.554E-01 5.858E-02 TL-208 3.206E-01 8.095E-02 PB-212 9.499E-01 1. 285E-01 BI-214 9.066E-01 1. 751E-01 PB-214 1.033E+OO 2.006E-01 RN-222 9.066E-01 1. 751E-01 RA-224 5.045E-01 1.406E+OO RA-226 9.066E-01 1. 751E-01 AC-228 l.084E+OO 3.219E-01 RA-228 1.084E+OO 3.219E-01 TH-228 9.499E-01 1.285E-01 TH-230 9.063E-01 l.751E-01 PA-231 8. 901E-01 7.835E-01 TH-232 1.084E+OO 3.219E-01 TH-234 2.657E+OO 2.771E+00 U-234 9.063E-01 1. 751E-01 U-235 -4.374E-02 1. 754E-01 U-238 2.657E+OO 2. 771E+OO AM-243 2. 211E-01 1.023E-01 ANH-511 8 .. 853E-02 8.948E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 2998 of 5809 Key-Line Activity (pCi/GRAM 1.076E+Ol 4.948E-03 O.OOOE+OO -3.904E-03 1.237E-01 K.L. Cnt Uncert ( 1. 96-sigma) 1.249E+Ol 4.450E-02 1. 960E+41 2.083E-02 3.257E-01 MDA (pCi/GRAM 6. 721E-01 1.538E+Ol 2.107E+OO 1.354E-01 5.420E-02 5.726E-02 5.774E-02 9.481E-02 1. 201E-01 1.353E-01 1.201E-01 l.016E+OO 1.201E-01 2.582E-01 2.582E-01 9. 481E-02 1.201E-01 8.240E-01 2.582E-01 2.013E+OO 1.201E-01 3.346E-01 2. 013E+OO 9.013E-02 5.654E-02 MDA (pCi/GRAM 2.588E+Ol 8.902E-02 O.OOOE+OO 4.619E-02 6.951E-01 NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN V-48 O.OOOE+OO 1.287E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.153E+02 O.OOOE+OO SHORT HLIF MN-54 -8.393E-03 7. 391E-02 l.255E-01 NOT IDENT. C0-56 -l.813E-01 4.386E-01 8.220E-01 NOT IDENT. MN-56 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 2.889E-02 4.520E-02 9.408E-02 NOT IDENT. C0-58 -3.563E-01 5.850E-01 1.064E+OO NOT IDENT. FE-59 -4.730E-02 5.995E+OO 1.186E+Ol NOT IDENT. C0-60 l.429E-03 3.289E-02 6.726E-02 NOT IDENT. ZN-65 2.099E-02 l.873E-01 3.293E-01 NOT IDENT. GE-68 -7.859E-01 1.695E+OO 3.141E+OO NOT IDENT. AS-74 O.OOOE+OO 5.432E+03 O.OOOE+OO SHORT HLI.F SE-75 -2.272E-02 2.061E-01 3.943E-01 NOT IDENT. BR-77 O.OOOE+OO 1.273E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.671E+02 O.OOOE+OO SHORT HLIF RB-83 -3.352E-01 7.244E-01 1.278E+OO NOT IDENT. KR-85 -2.354E+OO 8.780E+OO l.394E+Ol NOT IDENT. SR-85 -2.437E-01 9.080E-01 l.441E+OO NOT IDENT. RB-86 O.OOOE+OO 1. 979E+04 O.OOOE+OO SHORT HLIF Y-88 1. 075E-01 l.516E-01 4.219E-01 NOT IDENT. Y-91 1.331E+02 5.863E+02 1.042E+03 NOT IDENT. NB-94 4.733E-03 3.297E-02 6.606E-02 NOT IDENT. NB-95 l.607E-01 9.452E-01 1. 689E+OO NOT IDENT. NB-95M -9.658E-01 2.638E+OO 4.397E+OO NOT IDENT. ZR-95 2.661E+OO 2.518E+OO 3.235E+OO FAIL ABUN NB-97 O.OOOE+OO 8.289E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 7.667E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.064E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.643E+41 O.OOOE+OO SHORT HLIF RH-101 2.392E-02 3.357E-02 6.960E-02 FAIL ABUN RH-102 -1.925E-02 6. 311E-02 1.125E-01 NOT IDENT. RU-103 -2.171E+OO 5.207E+OO 9.347E+OO FAIL ABUN RH-106 -7.927E-02 5.362E-01 9.786E-01 NOT IDENT. RU-106 -7.927E-02 5.362E-01 9.786E-01 NOT IDENT. AG-108M -7.699E-04 3.053E-02 5.740E-02 FAIL ABUN AG-llOM 2.930E-02 9.489E-02 1.976E-01 FAIL ABUN SN-113 -9.900E-02 2.233E-01 4.050E-01 NOT IDENT. CD-115 0.000E+OO 1. 782E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.822E+04 O.OOOE+OO SHORT HLIF TE-123M -4.327E-02 l.294E-01 2.495E-01 NOT IDENT. SB-124 l.082E-01 1.674E+OO 3.422E+OO NOT IDENT. SB-125 -1.718E-02 1. 041E-01 1.941E-01 FAIL ABUN TE-125M -2.351E+02 2.895E+02 4.908E+02 NOT IDENT. I-126 O.OOOE+OO l.105E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 263E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.380E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.066E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.699E+26 O.OOOE+OO SHORT HLIF BA-133 3.556E-02 4.089E-02 7.893E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 4.287E-02 5.612E-02 l.184E-01 FAIL ABUN CS-135 7.152E-02 l.535E-01 2.784E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.387E+05 O.OOOE+OO SHORT HLIF CE-139 -7.430E-02 l.067E-01 2.002E-01 NOT IDENT. BA-140 O.OOOE+OO l.271E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.458E+05 O.OOOE+OO SHORT HLIF CE-141 4. 671E+OO 2.202E+Ol 4.422E+Ol NOT IDENT. CE-143 O.OOOE+OO 6.428E+40 O.OOOE+OO SHORT HLIF CE-144 -2.000E-01 3.390E-01 6.502E-01 NOT IDENT. PM-144 -5.629E-02 5.442E-02 9.538E-02 NOT IDENT. PR-144 -4.870E+OO 4.724E+OO 8.285E+OO NOT IDENT. PM-146 -4.808E-02 4.381E-02 7.142E-02 NOT IDENT. ND-147 0.000E+OO 3.376E+07 0.000E+OO SHORT HLIF PM-147 -l.015E+o2 7.754E+02. l.543E+03 NOT IDENT. PM-149 O.OOOE+OO 2.610E+40 0.000E+OO SHORT HLIF EU-150 -8.023E-03 2.560E-02 4.216E-02 FAIL ABUN EU-152 2.626E-03 8. 48 6E-02' 1.484E-01 FAIL ABUN GD-153 -4.lOlE-02 1. 947E-01 3.238E-01 NOT IDENT. EU-154 9. 896E-03 1.088E-01 2.170E-01 FAIL ABUN EU-155 -1.051E-02 l.152E-01 2.083E-01 FAIL ABUN TB-160 5.362E-01 1.681E+OO 3.524E+OO FAIL ABUN H0-166M -5.176E-02 5.397E-02 9.423E-02 FAIL ABUN TM-171 1.322E+Ol 2.074E+Ol 4.122E+Ol NOT IDENT. HF-172 -1.790E-01 2.219E-01 4. 211E-01 FAIL ABUN LU-172 -l.386E-02 7.778E-02 1. 478E-01 FAIL ABUN LU-176 l.804E-02 2.493E-02 5.073E-02 FAIL ABUN Page 2999 of 5809 HF-181 -l.929E+OO 4.398E+OO 7.850E+OO NOT IDENT. TA-182 -5.309E-01 1. 051E+OO 1. 775E+00 FAIL ABUN RE-183 9.693E-01 2.792E+OO 5.408E+00 NOT IDENT. RE-184 -9.237E+OO 2.423E+Ol 4.590E+Ol NOT IDENT. W-188 -7.491E+Ol l.312E+02 2.094E+02 FAIL ABUN IR-192 2.868E-01 4.517E-01 9.166E-01 FAIL ABUN HG-203 -5.437E-01 2.322E+OO 4.376E+OO NOT IDENT. BI-207 -7.770E-02 9.420E-02 2.223E-01 FAIL ABUN PB-210 -9.949E-02 3.206E+OO 6.122E+OO NOT IDENT. BI-211 O.OOOE+OO 5.526E-01 8.424E-01 FAIL ABUN PB-211 5.173E-01 6.659E-01 l.367E+OO NOT IDENT. BI-212 O.OOOE+OO l.037E+OO l.307E+OO FAIL ABUN RN-219 2.706E-02 3.912E-01 7.474E-01 FAIL ABUN RA-223 2.309E-01 6.365E-01 l.249E+OO FAIL ABUN AC-227 -5.213E-04 2.273E-01 4.389E-01 FAIL ABUN TH-227 -5.213E-04 2.273E-01 4.389E-01 FAIL ABUN TH-229 4.061E-02 4.873E-01 9.525E-01 FAIL ABUN TH-231 2.309E-01 6.365E-01 l.249E+OO FAIL ABUN PA-233 4.542E-02 6.106E-02 l.244E-01 FAIL ABUN PA-234 -2.884E-02 2.437E-01 4.246E-01 FAIL ABUN PA-234M 6.096E-01 4.818E+OO 9.595E+00 NOT IDENT. NP-237 4.542E-02 6.106E-02 l.244E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 -2.650E-02 2.318E-01 4.623E-01 NOT IDENT. PU-239 2.374E+02 3.222E+02 6.651E+02 NOT IDENT. AM-241 9.053E-02 l.381E-01 2.545E-01 NOT IDENT. CM-243 -8.033E-02 1. 089E-01 1. 866E-01 NOT IDENT. BK_.:247 -3.373E-02 7.300E-02 l.354E-01 NOT IDENT. CM-247 2.414E-04 3.662E-02 6.939E-02 NOT IDENT. CF-249 -l.809E-02 3.760E-02 6.786E-02 NOT IDENT. CF-251 -4. 791E-03 l .119E-01 2.190E-01 NOT IDENT. Page 3000 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:04:19.07 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 379 10.66* 1.161E+OO 1. 4 61E+Ol l.461E+Ol 10.35 AS-73 53.44 4 10.30* 2.017E+OO 8.281E-02 1.083E+OO 1913.23 CD-109 88.03 98 3.70* 5.494E+OO 2.290E+OO 3.582E+OO 74.24 SN-126 64.28 69 9.60 3.338E+OO 1.024E+OO 1.024E+OO 106.41 86.94 98 8.90 5.494E+OO 9.519E-01 9.519E-01 74.24 87.57 98 37.00* 5.494E+OO 2.290E-01 2.290E-01 74.24 BA-137M 661.66 59 89.90* 2.164E+OO l.444E-01 1.471E-01 38.46 CS-137 661. 66 59 85.10* 2.164E+OO 1.526E-01 l.554E-01 38.46 TL-208 277.37 ------6.60 4.415E+OO ------Line Not Found ------583.19 137 85.00* 2.392E+OO 3.206E-01 3.206E-01 25.76 860.56 ------12.50 1. 763E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 4.361E+OO ------Line Not Found ------351.06 280 12.92* 3.630E+OO 2.844E+OO 2.844E+00 19.83 PB-212 74.82 207 10.28 4.545E+OO 2 .113E+OO 2 .113E+OO 31. 05 77 .11 291 17.10 4.754E+OO 1. 710E+OO 1.710E+OO 21.10 238.63 431 '43.60* 4. 960E+OO 9.499E-01 9.499E-01 13.81 300.09 41 3.30 4 .141E+OO l.443E+00 l.443E+00 89.83 BI-214 609.32 200 45.49* 2.310E+OO 9.063E-01 9.066E-01 19. 71 1120.29 48 14.92 1.437E+OO 1. 064E+OO 1.065E+OO 41. 00 1764.49 41 15.30 9.862E-01 1.282E+OO 1.282E+OO 32.20 PB-214 74.82 207 5.80 4.545E+OO 3.745E+OO 3.746E+OO 31. 05 77 .11 291 9.70 4.754E+OO 3.015E+OO 3.016E+OO 21.10 87.09 98 3.41 5.494E+OO 2.485E+OO 2.485E+OO 74.24 242.00 110 7.25 4.910E+OO l.468E+OO l.469E+00 50.39 295.22 192 18.42 4.199E+OO 1.183E+OO l.183E+OO 28.12 351. 93 280 35.60* 3.630E+OO 1.032E+OO 1.033E+OO 19.83 RN-222 609.32 200 45.49* 2.310E+00 9.063E-01 9.066E-01 19. 71 1120.29 48 14.92 1.437E+OO 1.064E+OO 1.065E+OO 41.00 1764.49 41 15.30 9.862E-01 l.282E+OO 1.282E+OO 32.20 RA-224 240.99 110 4.10* 4.910E+OO 2. 596E+OO 2. 596E+OO 50.39 RA-226 609.32 200 45.49* 2.310E+OO 9.063E-01 9.066E-01 19.71 1120.29 48 14.92 1.437E+OO 1.064E+OO 1.065E+OO 41. 00 1764.49 41 15.30 9.862E-01 l.282E+OO 1.282E+OO 32.20 AC-228 105.21 ------1.10 6.259E+00 ------Line Not Found ------338.32 143 11. 27 3.747E+OO 1.616E+OO 1. 616E+OO 31. 60 794.95 ------4.25 1.875E+OO ------Line Not Found ------835.71 ------1. 61 1.803E+OO ------Line Not Found ------911.20 99 25.80* 1.687E+OO 1.084E+OO 1.084E+OO 30.29 968.97 59 15.80 1.609E+OO 1.098E+OO 1.098E+OO 41. 21 RA-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 143 11. 27 3.747E+OO 1.616E+OO 1.616E+OO 31. 60 794.95 ------4.25 1.875E+OO ------Line Not Found ------835.71 ------1. 61 1.803E+OO ------Line Not Found ------911.20 99 25.80* 1.687E+OO 1.084E+OO 1.084E+OO 30.29 968.97 59 15.80 1.609E+OO 1.098E+OO 1.098E+OO 41. 21 TH-228 74.82 207 10.28 4.545E+OO 2 .113E+OO 2 .113E+OO 31. 05 77 .11 291 17.10 4.754E+OO 1. 710E+OO 1.710E+OO 21.10 Page 3001 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235005 Acquisition date 3-0CT-2016 08:02:09 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 431 43.60* 4.960E+OO 9 .. 499E-01 9.499E-01 13.81 300.09 41 3.30 4.141E+OO 1.443E+OO l.443E+OO 89.83 TH-230 609.32 200 45.49* 2.310E+OO 9.063E-01 9.063E-01 19.71 1120.29 48 14.92 1.437E+OO 1.064E+OO 1.064E+OO 41. 00 1764.49 41 15.30 9.862E-01 1.282E+OO l.282E+OO 32.20 PA-231 283.69 ------1. 70 4.336E+OO ------Line Not Found ------301.36 41 5.35* 4.141E+OO 8.901E-01 8. 901E-01 89.83 TH-232 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 143 11. 27 3.747E+00 1.616E+OO 1.616E+OO 31. 60 835.71 ------1. 61 1.803E+OO ------Line Not Found ------911.20 99 25.80* 1.687E+OO 1. 084E+OO l.084E+OO 30.29 968. 97 59 15.80 1.609E+OO 1.098E+OO 1.098E+OO 41.21 TH-234 63.29 69 3.70* 3.338E+OO 2.657E+OO 2.657E+OO 106.41 92.59 129 4.23 5.791E+OO 2.516E+OO 2.516E+OO 62. 65 U-234 609.32 200 45.49* 2.310E+OO 9.063E-01 9.063E-01 19. 71 1120.29 48 14.92 l.437E+OO 1.064E+00 l.064E+00 41. 00 1764.49 41 15.30 9.862E-01 1. 282E+OO 1.282E+OO 32.20 U-235 89. 96 42 3.47 5.653E+OO 1.024E+OO 1.024E+OO 137.50 93.35 129 5.60 5.791E+OO 1.900E+OO 1.900E+OO 62. 65 143.76 ------10.96* 6.462E+OO ------Line Not Found ------163.33 ------5.08 6.216E+OO ------Line Not Found ------185.72 163 57.20 5.848E+00 2.332E-01 2.332E-01 44.76 205.31 ------5.01 5.506E+OO ------Line Not Found ------U-238 63.29 69 3.70* 3.338E+OO 2.657E+00 2.657E+OO 106.41 92.59 129 4.23 5.791E+OO 2.516E+OO 2.516E+OO 62. 65 AM-243 43.53 ------5.90 5.190E-01 ------Line Not Found ------74.66 207 67.20* 4.545E+OO 3.232E-01 3.232E-01 31. 05 ANH-511 511.00 49 100.00* 2.662E+OO 8.853E-02 8.853E-02 103.14 Flag: "*" Key line Page 3002 of 5809 Summary of Nuclide Activity Sample ID : G405235005 Acquisition date Page : 3 3-0CT-2016 08:02:09 Total number of lines in spectrum 48 Number of unidentified lines 11 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228' TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 80.30D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 7.04E+08Y l.41E+10Y 1600.00Y 1600. OOY 1600.00Y 1.41E+10Y 1600.00Y 1. 41E+l0Y 1. 41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 13.1 1. 56 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 461E+Ol 8.281E-02 2.290E+OO 2.290E-01 1.444E-01 1. 526E-01 3.206E-01 2.844E+OO 9.499E-01 9.063E-01 1.032E+OO 9.063E-01 2.596E+00 9.063E-01 1.084E+OO 1.084E+OO 9.499E-01 9.063E-01 8.901E-01 l.084E+00 2.657E+OO 9.063E-01 2.332E-01 2.657E+OO 3.232E-01 8.853E-02 4.083E+Ol 4.083E+Ol Decay Corr pCi/GRAM 1.461E+Ol 1.083E+OO 3.582E+OO 2.290E-01 l.471E-01 1.554E-01 3.206E-01 2.844E+OO 9.499E-01 9.066E-01 1.033E+OO 9.066E-01 2. 596E+OO 9.066E-01 1.084E+OO 1. 084E+OO' 9.499E-01 9.063E-01 8. 901E-01 1.084E+OO 2.657E+OO 9.063E-01 2.332E-01 2.657E+OO 3.232E-01 8.853E-02 4.313E+Ol 4. 313E+Ol 77.08% Decay Corr 2-Sigma Error 0.151E+Ol 20. 71E+OO 2.659E+OO 1.700E-01 0.566E-01 0.598E-01 0.826E-01 0.564E+OO 1. 311E-01 1.787E-01 0.205E+OO l.787E-01 1.308E+OO l.787E-01 0.328E+OO 0.328E+OO 1. 311E-01 l.787E-01 7.995E-01 0.328E+OO 2.827E+OO l.787E-01 l.044E-01 2.827E+OO 1.004E-01 9 .131E-02 "M" Manually accepted 2-Sigma %Error 10.35 1913.23 74.24 74.24 38.46 38.46 25.76 19.83 13. 81 19. 71 19.83 19. 71 50.39 19. 71 30.29 30.29 13.81 19. 71 89.83 30.29 106.41 19. 71 44.76 106.41 31. 05 103.14 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3003 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235005 Acquisition date : 3-0CT-2016 08:02:09 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 208.99 31 144 1.26 418.88 416 8 7.22E-03 **** 5.44E+OO 0 270.49 71 85 1. 20 541.94 538 9 1.68E-02 57.3 4.50E+OO T 0 326.32 85 112 5.86 653.64 643 18 2.07E-02 66.8 3.87E+OO T 0 463.18 73 61 2.43 927.47 918 18 1. 83E-02 59.4 2.89E+OO .T 0 471. 99 14 50 0.86 945.12 940 10 3. 61E-03 **** 2.84E+OO T 0 489.26 25 18 4.22 97 9. 67 974 11 6.41E-03 84.3 2.76E+OO 0 561.21 20 36 1. 39 1123. 63 1118 11 5.12E-03 **** 2.47E+OO 0 569.64 17 26 1.19 1140.49 1136 11 4.35E-03 **** 2.44E+OO T 0 614.42 15 32 0.83 1230.09 1226 9 3.94E-03 **** 2.29E+OO T 0 665.45 27 20 2.40 1332.20 1329 9 6.99E-03 73.1 2.15E+OO T 0 727. 26 40 37 1. 59 1455.87 1448 13 l.06E-02 74.0 2.0lE+OO T 0 757.10 23 23 2.86 1515.57 1509 14 6.24E-03 96. 5 1.95E+OO T 0 763.15 18 8 1. 09 1527.69 1523 8 4.78E-03 77.2 1.93E+OO T 0 829.83 21 8 1.22 1661.10 1656 10 5.75E-03 66.1 1.81E+OO 8 948.19 16 4 3.21 1897.92 1894 15 4.33E-03 64.4 l.64E+OO T 8 951.23 17 9 1. 93 1904.00 1894 15 4.66E-03 76.1 1. 63E+OO 2 962. 21 16 2 1. 73 1925.97 1923 12 4.46E-03 67.1 l.62E+00 T 2 964. 22 27 12 1. 94 1930.00 1923 12 7.24E-03 65.6 1. 61E+OO T 0 1024.33 4 10 0.47 2050.27 2044 8 1.0lE-03 **** 1.54E+OO 0 1130. 03 22 10 4.80 2261. 75 2253 16 6.00E-03 82.8 1.43E+OO T 0 1197.83 27 41 8.79 2397.43 2382 28 7.64E-03 **** 1.36E+OO 5 1212'. 75 9 3 1. 49 2427.27 2426 11 2.65E-03 65.1 1. 35E+OO 5 1215.68 16 4 1. 82 2433.14 2426 11 4.61E-03 61. 7 1.35E+OO 0 1376.89 17 6 4.26 2755.69 2749 13 4.79E-03 77.0 l.22E+00 0 1694.43 7 3 1. 47 3391.07 3384 10 2.00E-03 **** 1.02E+OO Flags: "T" = Tentatively associated Page 3004 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:04:50.15 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l *
  • Acquisition date 3-0CT-2016 08:02:09 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.81 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:15:00 Nuclide Library : SOLID *
  • Sample ID G405235005 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.5733E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.835E-01 7.232E+OO 1. OOlE+OO 6.427E-02 2.362E-02 2.495E-02 2.559E-02 5. 372E-02 6.241E-02 5. 372E-02 4.744E-01 5.372E-02 1.140E-01 l.140E-01 4.426E-02 5.371E-02 3.814E-01 l.140E-01 9.491E-01 5. 371E-02 1. 576E-01 9.491E-01 4.277E-02 2.576E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3005 of 5809 Le (pCi/GRAM 1.184E+Ol 3.825E-02 O.OOOE+OO 1. 636E-02 3.025E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3006 of 5809 0.000E+OO 5.568E-02 3.574E-01 O.OOOE+OO 4.439E-02 4.658E-Ol 5.106E+OO 2.783E-02 1.437E-01 1..276E+OO O.OOOE+OO 1. 831E-01 O.OOOE+OO O.OOOE+OO 5.770E-01 6.356E+OO 6.573E-01 O.OOOE+OO 1.634E-01 4.578E+02 2.982E-02 7.580E-01 2.061E+OO 1.461E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.296E-02 5.012E-02 4.155E+00 4.380E-01 4.380E-01 2.626E-02 8.678E-02 l.837E-01 O.OOOE+OO O.OOOE+OO 1.174E-01 1. 301E+OO 8.806E-02 2.306E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.628E-02 O.OOOE+OO 5.380E-02 1.299E-01 O.OOOE+OO O.OOOE+OO 9.388E-02 O.OOOE+OO O.OOOE+OO 2.085E+Ol O.OOOE+OO 3.055E-01 4.203E-02 3. 651E+OO 3.181E-02 O.OOOE+OO 7.255E+02 O.OOOE+OO l.919E-02 6.704E-02 1.525E-01 9.313E-02 9.822E-02 l.542E+OO 4 .111E-02 1. 948E+Ol 1.979E-01 6.430E-02 2.359E-02 3.537E+OO SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT, SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3007 of 5809 7.780E-01 2.554E+OO 1.948E+Ol 9.706E+Ol 4.245E-Ol 2.029E+OO 1. 052E-01 2.874E+OO 4.070E-01 6.286E-01 6.042E-01 3.424E-01 5.808E-01 2.043E-01 2.043E-01 4.491E-01 5.808E-01 5.784E-02 1. 788E-01 4.299E+OO 5.784E-02 O.OOOE+OO 2.177E-01 3.158E+02 l.203E-01 8.786E-02 6.275E-02 3'.181E-02 3.087E-02 1.029E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:04:58.76 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235005.CNF;l *
  • Acquisition date 3-0CT-2016 08:02:09 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.81 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:15:00 Nuclide Library : SOLID *
  • Sample ID G405235005 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity l.5733E+02 GRAM *
  • Quantity Err(%) 1.2712E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date . 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.461E+Ol 1.667E+OO 1.667E+OO AS-73 l.083E+00 2.030E+Ol 2.030E+Ol CD-109 1. 876E+OO 2. 661E+OO 2.661E+OO SN-126 1.200E-01 1. 700E-01 1.700E-01 BA-137M 1.471E-01 5.582E-02 5.582E-02 CS-137 l.554E-01 5.897E-02 5.897E-02 TL-208 3.206E-01 8. 211E-02 8. 211E-02 PB-212 9.499E-01 l.381E-01 l.381E-01 BI-214 9.066E-01 1. 795E-01 1. 795E-01 PB-214 1.033E+OO 2.052E-01 2.052E-01 RN-222 9.066E-01 1. 795E-01 1. 795E-01 RA-224 5.045E-01 l.413E+OO l.413E+OO RA-226 9.066E-01 1. 795E-01 1. 795E-01 AC-228 1.084E+OO 3.267E-01 3.267E-01 RA-228 1.084E+OO 3.267E-01 3.267E-01 TH-228 9.499E-01 1.381E-01 1. 381E-01 TH-230 9.063E-01 1.794E-01 1.794E-01 PA-231 8.901E-01 8.062E-01 8.062E-01 TH-232 1.084E+OO 3.267E-01 3.267E-01 TH-234 2.657E+OO 2.833E+OO 2.833E+OO U-234 9.063E-01 1. 794E-01 1.794E-01 U-235 -4.374E-02 1. 754E-01 1. 754E-01 U-238 2.657E+OO 2.833E+OO 2.833E+OO AM-243 2.211E-01 1.040E-01 1.040E-01 ANH-511 8.853E-02 8.955E-02 8.955E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) BE-7 1. 076E+01 1.250E+Ol 1.341E+Ol NOT IDENT. NA-22 4.948E-03 4.450E-02 4.456E-02 NOT IDENT. NA-24 -1.000E+41 3.245E+41 O.OOOE+OO SHORT HLIF AL-26 -3.904E-03 2.083E-02 2.090E-02 FAIL ABUN SC-46 1.237E-01 3.258E-01 3.305E-01 FAIL ABUN Page 300S of 5809 V-48 6.546E+03 1.287E+04 1. 321E+04 SHORT HLIF CR-51 -1.643E+02 4.154E+02 4.219E+02 SHORT HLIF MN-54 -8.393E-03 7.391E-02 7.401E-02 NOT IDENT. C0-56 -1. 813E-01 4.387E-01 4.462E-01 NOT IDENT. MN-56 -1. OOOE+41 2.420E+41 O.OOOE+OO SHORT HLIF C0-57 2.889E-02 4.522E-02 4.705E-02 NOT IDENT. C0-58 -3.563E-01 5.852E-01 6.069E-01 NOT IDENT. FE-59 -4.730E-02 5.995E+00 5.995E+OO NOT IDENT. C0-60 1.429E-03 3.289E-02 3.289E-02 NOT IDENT. ZN-65 2. 099E-02. 1.873E-01 1. 875E-01 NOT IDENT. GE-68 -7.859E-01 1.695E+OO 1.732E+OO NOT IDENT. AS-74 -4.299E+02 5.432E+03 5.436E+03 SHORT HLIF SE-75 -2.272E-02 2.062E-01 2.064E-01 NOT IDENT. BR-77 9.409E+37 8.088E+38 O.OOOE+OO SHORT HLIF SR-82 -7.664E+02 6. 681E+02 7. 521E+02 SHORT HLIF RB-83 -3.352E-01 7.258E-01 7.414E-01 NOT IDENT. KR-85 -2.354E+OO 8.781E+OO 8.845E+OO NOT IDENT. SR-85 -2.437E-01 9.080E-01 9.147E-01 NOT IDENT. RB-86 -5.544E+03 1.979E+04 l.995E+04 SHORT HLIF Y-88 1. 07 5E-01 1.518E-01 l.593E-01 NOT IDENT. Y-91 1. 331E+02 5. 8 63E+02 5.894E+02 NOT IDENT. NB-94 4.733E-03 3.297E-02 3.304E-02 NOT IDENT. NB-95 l.607E-01 9.452E-01 9.480E-01 NOT IDENT. NB-95M -9.658E-01 2.639E+OO 2.675E+00 NOT IDENT. ZR-95 2.661E+OO 2.520E+OO 2.791E+OO FAIL ABUN NB-97 -1.000E+41 8.300E+40 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 7.678E+40 O.OOOE+OO SHORT HLIF M0-99 -1.402E+31 1.064E+32 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 l.646E+41 O.OOOE+OO SHORT HLIF RH-101 2.392E-02 3.385E-02 3.552E-02 FAIL ABUN RH-102 -1.925E-02 6.313E-02 6.373E-02 NOT IDENT. RU-103 -2 .171E+OO 5.208E+OO 5.299E+OO FAIL ABUN RH-106 -7.927E-02 5.362E-01 5.374E-01 NOT IDENT. RU-106 -7.927E-02 5.362E-01 5.374E-01 NOT IDENT. AG-108M -7.699E-04 3.053E-02 3.053E-02 FAIL ABUN AG-llOM 2.930E-02 9.490E-02 9.581E-02 FAIL ABUN SN-113 -9.900E-02 2.233E-01 2.277E-01 NOT IDENT. CD-115 6.419E+38 1. 785E+39 O.OOOE+OO SHORT HLIF SN-117M -l.092E+04 8.823E+04 8.836E+04 SHORT HLIF TE-123M -4.327E-02 l.294E-01 l.309E-01 NOT IDENT. SB-124 l.082E-01 1.674E+OO 1. 67 5E+OO NOT IDENT. SB-125 -1.718E-02 1. 041E-01 1.044E-01 FAIL ABUN TE-125M -2.351E+02 2.898E+02 3.086E+02 NOT IDENT. I-126 1.543E+06 1.124E+06 1.322E+06 SHORT HLIF SB-126 -7.978E+04 1. 2 63E+06 l.264E+06 SHORT HLIF SB-127 -4.045E+21 1.487E+22 O.OOOE+OO SHORT HLIF I-131 l.159E+09 4.067E+09 4.100E+09 SHORT HLIF I-132 -1.000E+41 1.901E+42 O.OOOE+OO SHORT HLIF TE-132 -3.288E+25 2.703E+26 0 .. OOOE+OO SHORT HLIF BA-133 3.556E-02 4.092E-02 4.394E-02 NOT IDENT. I-133 -1.000E+41 4.526E+41 O.OOOE+OO SHORT HLIF CS-134 4.287E-02 5.615E-02 5.938E-02 FAIL ABUN CS-135 7.152E-02 1.535E-01 1.569E-01 NOT IDENT. I-135 -1.000E+41 l.298E+42 O.OOOE+OO SHORT HLIF CS-136 -7.556E+04 2.389E+05 2.413E+05 SHORT HLIF CE-139 -7.430E-02 1.077E-01 l.128E-01 NOT IDENT. BA-140 -3.243E+05 1.271E+06 1. 280E+06 SHORT HLIF LA-140 -2.754E+04 4.458E+05 4.459E+05 SHORT HLIF CE-141 4.671E+OO 2.202E+Ol 2.212E+Ol NOT IDENT. CE-143 l.000E+41 6.508E+40 O.OOOE+OO SHORT HLIF CE-144 -2.000E-01 3. 391E-01 3.509E-01 NOT IDENT. PM-144 -5.629E-02 5.453E-02 6.014E-02 NOT IDENT. PR-144 -4.870E+00 4.729E+OO 5.214E+OO NOT IDENT. PM-146 -4.808E-02 4.395E-02 4.900E-02 NOT IDENT. ND-147 7.985E+06 3.376E+07 3.395E+07 SHORT HLIF PM-147 -l.015E+02 7.754E+02 7.768E+02 NOT IDENT. PM-149 -3.334E+39 2.611E+40 O.OOOE+OO SHORT HLIF EU-150 -8.023E-03 2.560E-02 2.586E-02 FAIL ABUN EU-152 2.626E-03 8.486E-02 8.487E-02 FAIL ABUN GD-153 -4. lOlE-02 l.948E-01 1.956E-01 NOT IDENT. EU-154 9. 896E-03 l.088E-01 l.089E-01 FAIL ABUN EU-155 -1.051E-02 1.152E-01 l.153E-01 FAIL ABUN TB-160 5.362E-01 1. 681E+OO 1.698E+OO FAIL ABUN H0-166M -5.176E-02 5.404E-02 5.886E-02 FAIL ABUN TM-171 1. 322E+Ol 2.077E+Ol 2.161E+Ol NOT IDENT. HF-172 -1.790E-01 2.238E-01 2.379E-01 FAIL ABUN LU-172 -1. 386E-02 7.779E-02 7.804E-02 FAIL ABUN LU-176 l.804E-02 2.494E-02 2.623E-02 FAIL ABUN Page 3009 of 5809 HF-181 -1.929E+OO 4.398E+OO 4.484E+OO NOT IDENT. TA-182 -5.309E-01 1. 051E+OO l.078E+00 FAIL ABUN RE-183 9.693E-01 2.796E+OO 2.830E+OO NOT IDENT. RE-184 -9.237E+OO 2.433E+Ol 2.469E+Ol NOT IDENT. W-188 -7.491E+Ol 1.314E+02 1.357E+02 FAIL ABUN IR-192 2.868E-01 4.519E-01 4.700E-01 FAIL ABUN HG-203 -5.437E-01 2.322E+OO 2.335E+OO NOT IDENT. BI-207 -7.770E-02 9.425E-02 1.005E-01 FAIL ABUN PB-210 -9.949E-02 3.206E+OO 3.206E+OO NOT IDENT. BI-211 2.844E+OO 5. 671E-01 1.402E+OO FAIL ABUN PB-211 5.173E-01 6.664E-01 7.060E-01 NOT IDENT. BI-212 1.431E+OO 1.040E+OO l.223E+OO FAIL ABUN RN-219 2.706E-02 3.912E-01 3.914E-01 FAIL ABUN RA-223 2.309E-01 6.366E-01 6. 451E-01 FAIL ABUN AC-227 -5.213E-04 2.273E-01 2.273E-01 FAIL ABUN TH-227 -5. 213E-04 2.273E-01 2.273E-01 FAIL ABUN TH-229 4. 061E-02 4.873E-01 4.876E-01 FAIL ABUN TH-231 2.309E-01 6.366E-01 6.451E-01 FAIL ABUN PA-233 4.542E-02 6.llOE-02 6.444E-02 FAIL ABUN PA-234 -2.884E-02 2.459E-01 2.463E-01 FAIL ABUN PA-234M 6. 096E-01 4.818E+OO 4.826E+OO NOT IDENT. NP-237 4.542E-02 6. llOE-02 6.444E-02 FAIL ABUN NP-238 8.874E+40 2.429E+41 O.OOOE+OO SHORT HLIF NP-239 -2.650E-02 2.318E-01 2.321E-01 NOT IDENT. PU-239 2.374E+02 3.224E+02 3.397E+02 NOT IDENT. AM-241 9.053E-02 l.382E-01 1. 441E-01 NOT IDENT. CM-243 -8.033E-02 l.092E-01 l.150E-01 NOT IDENT. BK-247 -3.373E-02 7.332E-02 7.488E-02 NOT IDENT. CM-247 2.414E-04 3.662E-02 3.662E-02 NOT IDENT. CF-249 -1.809E-02 3.763E-02 3.850E-02 NOT IDENT. CF-251 -4.791E-03 1.119E-01 l.120E-01 NOT IDENT. Page 3010 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 83.8463 87.09 117.3344 136.47 87.6127 45.60 77.4971 87.57 117.4180 140.51 0.0000 46.54 73.1555 88.03 117.4979 143.76 90.0468 49.72 0.0000 88.34 117.5512 144.24 80.5642 51. 35 69.7358 88.47 117.5742 145.44 85.0043 51. 87 81.9514 89.96 117.8302 152.43 92.6217 52.39 82.0382 1093.63 117.9472 153.25 0.0000 52.97 82 .1346 91.11 0.0000 323.87 90.1659 53.44 82.2123 92.59 118.2780 156.02 0.0000 54.07 82.3162 93.35 118.4060 158.56 0.0000 57.36 0.0000 94.56 118.6095 159.00 93.2460 57.53 90.9330 94.65 89.6816 162.33 75.0226 57.98 86.4029 94.67 89.6844 162.66 0.0000 59.27 87.7696 94.87 89.7096 163.33 82.1649 59.32 87.7779 97.43 86.7563 165.86 92.9976 59.54 80.1111 98.43 82.3683 176.31 87.6730 60.96 105.0388 98.44 82.3698 176.60 0.0000 61.17 95.8082 99.53 94.8048 177.52 81.5033 62.93 90.6917 100 .11 104.7377 181.07 0.0000 63.29 90.7511 102.03 87. 7143 181.52 74.1656 63.58 90.7987 103.18 107.6462 184.41 82.9258 64.28 90.9129 103.37 107.6734 143.76 83.0250 66.73 120.1840 105.21 94.2891 193.51 89.0587 67.24 131. 2269 105.31 94.3013 197.03 76.5728 125.81 125.0741 106.12 90.6758 198.01 73.9015 67.75 98.5074 106.47 90.7170 201.83 83.2991 69.67 118.8364 109.28 104.7680 203.43 84.3305 70.83 139.8981 111. 00 99.9988 205.31 89.5148 72.81 127.7457 111. 76 0.0000 210.85 78.8647 72. 87 127.7589 114. 06 99.5492 215.65 63.8993 74.66 115. 0854 116. 30 0.0000 222 .11 75.4069 74.82 115 .1150 116. 74 89.8089 227.09 75.7076 74.97 115.1431 119.76 79.1891 227.38 85.0746 77 .11 115.5427 121.12 85.2259 228.16 0.0000 78.74 115.8424 121.22 85.2362 228.18 83.2573 79.69 119. 6045 121.78 77.6933 116.74 83.2573 80.12 119. 6854 122.06 77. 7195 235.69 84.6890 80.19 0.0000 122.92 65 .1148 235. 96 80.4711 80.57 99.0093 123.07 76.9673 238.63 66.0181 81. 00 81.4976 265.00 94.7979 238.98 0.0000 81. 07 81. 5064 125.81 101.8250 240.99 66.1377 81. 75 135.9875 127.23 87.5446 242.00 66.1883 83.79 154.0664 127.91 91. 8 677 244.70 52 . .5851 84.00 154 .1162 129.30 97.9788 252.40 0.0000 85.43 133.5342 131.20 100.7545 252.80 66. 7259 86.55 117.2404 133.02 105.2414 254.15 0.0000 86.79 117.2818 133.52 95.0282 256.23 60.2045 86.94 1*17.3085 136.00 72. 9725 260.90 0.0000 Page 3011 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 58.6495 355.39 0.0000 584.27 22.1938 264.80 59.6172 356.01 27.'5284 595.83 0.0000 265.00 63.4716 364.49 0.0000 427.87 27.4951 268.22 53.4969 366.42 0.0000 602.52 0.0000 269.46 53.5432 372. 51 36.0233 604. 72 24.0975 270.03 63.6985 375.05 42.2587 607.14 20.6748 271.23 63.7522 377.52 37.1565 609.32 24.1411 273.65 0.0000 356.01 30.0372 610.33 24.1505 276.40 68.8304 388.16 42.5665 614.28 24.1881 277.37 57.2355 388.63 0.0000 618.01 20.7634 277.60 57.2451 391.69 39.5277 620.36 28.8635 278.00 46.5850 264.66 43.9004 621. 93 26.5713 279.20 54.3936 401. 81 38.6975 630.19 0.0000 279.54 70.9222 402.40 40.8027 631.29 26.6667 279.70 70.9311 404.85 30.3800 633.25 17.4048 280.46 68.0518 410.95 38.8849 634.78 0.0000 283.69 51. 6381 413.71 35.7840 635.95 19.7455 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 65.3547 423.72 0.0000 645.85 31. 4791 285.90 0.0000 427.09 37.0921 657.76 21.0798 287.50 61. 5401 427.87 34.9860 657.90 0.0000 290.67 61.6721 433.94 39.3479 661.66 15.4811 293.27 0.0000 439.40 34.1237 664.57 0.0000 351.93 48.6037 453.88 39.7393 666.33 0.0000 295. 96 48.6269 463.37 35.6063 666.50 0.0000 879.38 17.7133 468.07 19.4656 667.71 0.0000 299.98 47.2783 473.00 0.0000 677.62 17.6953 300.09 47.2822 475.06 35.8057 685.70 0.0000 300.13 47.2832 476.78 35.8346 695.00 0.0000 301.36 51. 7577 477.60 24.9855 696.49 29.3967 302.85 66.6101 482.18 34.8372 696. 51 29.3967 256.23 53.3452 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.0584 306.78 44.5203 497.08 27.4043 697.49 21.3867 308.46 63.3854 505.52 29.7109 702.65 26.7828 311. 90 43.6742 507.63 0.0000 706.68 27. 7144 316.51 40.8148 511. 00 35.2995 711. 68 27.7636 319.41 0.0000 514.00 41. 4215 720.70 0.0000 320.08 0.0000 514.00 41. 4215 721. 93 0.0000 321. 04 38.9349 520.40 36.5557 722.78 33.0861 323.87 52.0042 520.69 0.0000 722.91 27.3329 325.23 52.0487 522.65 0.0000 723.31 27.3366 328.76 0.0000 527.90 0.0000 724.19 37.4194 333.37 40.7406 528.26 22.2314 727.33 29.7159 333.97 40.7554 529.59 31.1423 733.00 19.5918 334.37 49.8243 529.87 0.0000 735.93 18. 9665 338.28 40.3573 531.02 0.0000 333.97 23.4943 338.32 40.3589 537.26 0.0000 739.50 0.0000 311. 90 40. 4110 546.56 0.0000 747.24 20.8529 340.48 40. 4110 552.55 30.3278 748.06 19.9516 340.55 0.0000 563.25 30.4640 752.31 26.1554 344.28 28.8583 569.33 16.9678 753.82 0.0000 345.93 42.5699 946.00 16. 9690 756.73 14.5527 351. 06 47.7822 569.70 16.9702 756.80 14.5527 351.93 47.8061 583.19 20.4771 884.68 37.9285 Page 3012 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS .765.81 23.3547 1274.44 16.6176 1620.50 6.7394 766.42 16. 0596 1001.03 18.5970 1621.92 5. 6177 766.84 14.6016 1002.74 23.5012 1678.03 0.0000 772.60 o.ooob 1004.73 15. 67 63 1690.97 3.0340 776.52 0.0000 507:63 0.0000 1750.46 0.0000. 739.50 0.0000 1025.87 0. 00*00 1764.49 2.7662. 778.90 21. 0733 1028.54 0.0000 1063.66 11. 9990 783.70 0.0000 1037.84 20.7578 1771.35 3.6926 785.37 24.7909 1038.76 0.0000 1791.20 0;0000 792.07 36.8079 631. 2 9 14.8608 1808.65 2.7872 794.95 21.1842 1048.07 0.0000 1810.72 0.0000 795.86 .22 .1111 1049.04 13.8787 1836.06 0.9333 810.06 28.6907 1050.41 13.8838 810.29 26.8415 1063.66 9.9512 344.28 26.8.432 1077.00 0.0000 810.76 24.0687 1077.34 9.9860 815.77 0.0000 1085.87 14. 0111 1048.07 0.0000 1093.63 17.0467 832.01 19.3845 1099.45 13. 0555 834.85 22.3865 1112.07 16 .1191 835.71 25.5912 1112.84 13.0992 836.80 0.0000 1115. 54 14.5195 846.75 0.0000 1120.29 13.1230 846.77 19.6599 1120.55 13 .1238 856.80 0.0000 1221.41 14.5406 860.56 23.5039 1129. 67 17.2013 871. 09 15.0903 1131.51 0.0000 873.19 15.1001 1147.95 0.0000 875.33 0.0000 1173.23 22.4968 879.38 13.2369 1177.95 17.4036 880.51 15.1333 1189.05 13 .1383 883.24 17.0387 1204.77 14.8359 884.68 14.2049 1221.41 23.6398 889.28 . 11. 3796 1231.02 13.4753 894.76 18.0468 1235.36 0.0000 898.04 10.4582 1238.28 20.7654 900.72 17.1271 1260.41 0.0000 903.28 14.2831 1271. 87 8.3701 911.20 19 . .0881 1274.44 11. 5156 912.08 19.0930 1274.54 11.5156 923.98 0.0000 1291. 59 15.7626 . 926.50 14.3797 1298.22 0.0000 929 .11 24.9439 1312 .11 0.0000 937.49 17.3101 1332.49 7.4221 944.13 0.0000 1362.66 0.0000 946.00 10.7967 1365.19 4. 2712 949.00 10.6129 1368.63 0.0000 667.71 0.0000 1384.29 9.6487 962. 31 3.'0989 1408.01 3.2324 964.08 7.7512 1457.56 0.0000 966 .17 7.7556 1460.82 9.8020 911.20 13.9711 1489.16 6. 5717 968. 97 13.9711 1505.03 7. 6913 983.53 0.0000 1584.12 14.5028 984.45 0.0000 1596.21 0.0000 }'. Page 3013 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:05:32.50 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date : Z-OCT-2016 11:01:13. Sample date : 10-DEC-2015 13:25:00 Acquisition date : 3-0CT-2016 08:02:32. Sample ID : G405235006 Sample quantity : 1.56342E+02 GRAM Detector name : GAM20 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:14.99 0.4% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 7 7 0 1 1 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3014 of 5809 Energy 26.75* 28.24* 63.57* 73.54 76.84 84.32* 87.19 89.95* 92.82* 105.40 121.39 128.75 186.06* 210.28 238.45* 241.57 270.34 295.06* 300.35 338.55* 351.77* 446.92 462.90 511. 01
  • 543.83 583.49* 609.34* 654.51 727.18 786.46 794.94 835.82 911. 38* 957.75 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 15 38 0 51 316 33 83 36 94 42 32 38 63 35 473 80 66 201 53 96 288 39 46 15 64 164 179 26 32 17 29 18 142 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 7 68 243 190 172 119 181 107 201 147 99 82 164 146 122 84 106 72 61 78 60 30 50 79 30 42 49 14 14 29 7 15 19 11 1.19 2.00 0.50 1. 23 1. 24 0.77 1. 03 0.96 1. 51 1.17 1. 33 1. 75 0.93 2.42 1.22 1.22 1. 48 0.98 1. 02 1.14 1. 24 2.59 1. 74 1. 85 5.63 1. 32 1. 52 1. 06 2.01 0.64 2.70 4.43 1. 54 3.21 53.71 56.68 127.29 147.22 153.82 168.76 174.51 180.02 185.76 210.90 242.85 257.57 372.12 420.54 476.85 483.08 540.60 590.03 600.60 676.98 703.41 893.68 925.64 1021.84 1087.48 1166.82 1218.53 1308.89 1454.27 1572.89 1589.85 1671.64 1822.85 1915.67 51 51 123 144 144 166 172 178 178 207 239 255 367 411 471 481 535 584 596 671 698 885 919 1016 1074 1159 1211 1304 1448 1568 1585 1664 1817 1910 16 4.30E-03 69.1 2.88E+OO 16 1. 05E-02 59. 6 9 1.0lE-04***** 16 1.42E-02 50.3 2.27E+Ol 16 8.78E-02 9.5 6 9.21E-03 56.2 7 2.29E-02 29.0 13 1.00E-02 42.8 3.0lE+OO 13 2.60E-02 30.6 10 1.17E-02 55.6 7 8.84E-03 55.2 6 1.05E-02 41.4 11 1.76E-02 42.8 12 9.85E-03 70.3 10 1. 31E-01 6. 5 7 2.21E-02 22.5 13 1.84E-02 34.5 11 5.59E-02 10.8 11 1.46E-02 31.8 13 2.68E-02 21.6 12 8.0lE-02 8.0 15 1. 09E-02 34. 4 15 1.29E-02 36.1 15 4.17E-03143.3 30 1.76E-02 28.1 16 4.55E-02 12.0 13 4. 97E-02 11. 1 10 7.08E-03 34.5 11 8.96E-03 28.4 14 4.75E-03 70.2 9 8.14E-03 24.4 12 4.99E-03 49.2 15 3.95E-02 10.8 9 3.83E-03 51.5 Peak Search Report (continued) Page : 2 Sample ID : G405235006 Acquisition date 3-0CT-2016 08:02:32 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 1 964. 57 41 10 1. 94 1929.32 1922 22 1. 15E-02 22.3 2.97E+OO 36 1 969. 00 73 17 1. 87 1938.18 1922 22 2.03E-02 14.7 37 0 1088.96 11 12 1.19 2178.31 2174 9 2.92E-03 65.5 38 0 1095.52 29 11 4.82 2191. 43 2183 17 8.07E-03 33.4 39 0 1104. 64 12 6 3.10 2209.70 2204 11 3.19E-03 49.3 40 0 1108.77 11 4 1.17 2217.95 2214 7 2.92E-03 42:7 41 0 1120. 71 33 22 1.18 2241. 8 6 2239 8 9.18E-03 30.1 42 1 1203.69 17 9 1. 87 2408.00 2400 20 4.59E-03 40.0 6.67E-01 43 1 1206.69 14 7 1. 87 2414.00 2400 20 3.77E-03 54.5 44 0 1238.48 27 7 2.23 2477.66 2472 10 7.42E-03 27.2 45 0 1258.60 11 11 1. 01 2517.96 2512 9 3.12E-03 61. 3 46 0 1288.43 15 7 2.88 2577.68 2572 13 4.17E-03 43.8 47 0 1334.20 17 6 1.19 2669.34 2664 12 4.73E-03 37.6 48 0 1360.53 6 5 0.55 2722.08 2718 6 1.53E-03 74.4 49 0 1377.89 22 5 1. 34 2756.85 2751 11 6.08E-03 29.7 50 0 1416.25 6 9 0.55 2833.68 2823 12 1.74E-03103.4 51 0 1460.92* 480 0 2.16 2923.15 2916 14 l.33E-01 4.6 52 0 1588.20 11 6 4.32 3178.14 3171 12 3.06E-03 53.8 53 0 1630.78 11 0 0.83 3263.45 3257 11 3.06E-03 30.2 54 0 1729.10 13 3 0. 72 3460.47 3453 13 3.67E-03 39.0 55 0 1764.39 43 0 2.54 3531.19 3525 12 1.19E-02 15.2 Flag: "*" = Peak area was modified by background subtraction Page 3015of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:05:34 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 13:25:00 G405235006 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:02:32 156.34 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report S.OLID GAMMA20 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3016of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 RA-224 240.99 BI-211 72.87 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:14.99 10.00 0.00 % Peak Energy 0.4%

Nuclide Line Activity Report Page : 2 Sample ID : G405235006 Acquisition date 3-0CT-2016 08:02:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-:-40 1460.82 10.66* 1.312E+OO 1.597E+.Ol 1.597E+Ol 9.18 OK MN-54 834.85 99.98* 2.057E+OO 4.332E-02 8.395E-02 98.38 OK C0-57 122.06 85.60* 7.574E+OO 2. 963E-02 6.333E-02 110.46 OK 136.47 10.68 7.468E+OO Line Not Found Absent Y-91 1204.77 0. 26* 1.543E+OO 1. 960E+Ol 6.675E+02 79.96 OK CD-109 88.03 3.70* 6.842E+OO 8.453E-01 1.322E+OO 142.57 OK SN-126 64.28 9.60 4.822E+OO 5.031E-03 5.031E-03******* OK 86.94 8.90 6.842E+OO 3.514E-01 3.514E-01 142.57 OK 87.57 37.00* 6.842E+OO 8.453E-02 8.453E-02 142.57 OK PM-147 121. 22 0.00* 7.574E+OO 8.899E+02 1.104E+03 110.46 OK EU-155 86.55 30.70 6.842E+OO 1.019E-01 1.147E-01 142.57 OK 105.31 21.10* 7.457E+OO 1.643E-01 1.850E-01 111.18 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.718E+OO 3.661E-01 3.661E-01 24.08 OK 860.56 12.50 2. OllE+OO Line Not Found Absent BI-212 727. 33 6.67* 2.290E+OO 1.064E+OO 1. 064E+OO 56.79 OK 785.37 1.10 2.156E+OO 3.600E+OO 3.600E+OO 140.46 OK 1620. 50 1. 47 1.197E+OO Line Not Found Absent PB-212 74.82 10.28 5.996E+OO Line Not Found <<INT Reject 77 .11 17.10 6.163E+OO 1.887E+OO 1.887E+00 19.08 OK 238.63 43.60* 5.555E+OO 1.105E+OO 1.105E+OO 12.91 OK 300.09 3.30 4.643E+OO 1.896E+OO 1.896E+OO 63.67 OK BI-214 609.32 45.49* 2.627E+OO 7.694E-01 7.696E-01 22.24 OK 1120.29 14.92 1.635E+OO 6.500E-01 6.502E-01 60.22 OK 1764.49 15.30 1.106E+OO 1.155E+OO 1.155E+OO 30.50 OK PB-214 74.82 5.80 5.884E+OO 9.459E-01 9.463E-01 100.67 OK 77 .11 9.70 6.163E+OO 3.326E+OO 3.328E+OO 19.08 OK 87.09 3.41 6.836E+OO Line Not Found <<INT Reject 242.00 7.25 5.502E+OO 1.127E+OO 1.128E+OO 45.00 OK 295.22 18.42 4.710E+OO 1.287E+OO 1.287E+OO 21. 68 OK 351. 93 35.60* 4.085E+OO 1.079E+OO 1.080E+OO 16.10 OK RN-222 609.32 45.49* 2.627E+OO 7.694E-01 7. 696E-01 22.24 OK 1120.29 14.92 1. 635E+OO 6.500E-01 6.502E-01 60.22 OK 1764.49 15.30 l.106E+OO 1.155E+OO 1.155E+00 30.50 OK RA-226 609.32 45.49* 2.627E+OO 7.694E-01 7.696E-01 22.24 OK 1120.29 14.92 1.635E+OO 6.500E-01 6.502E-01 60.22 OK 1764.49 15.30 1.106E+OO 1.155E+OO 1.155E+00 30.50 OK AC-228 105.21 1.10 7.457E+OO 3 .151E+OO 3.151E+00 111.18 OK 338.32 11. 27 4.214E+OO 1. llOE+OO 1.llOE+OO 43.25 OK 794.95 4.25 2 .138E+OO 1.609E+OO 1.609E+OO 48.85 OK 835.71 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 OK* 911.20 25.80* 1.923E+OO 1.408E+OO 1.408E+OO 21. 64 OK 968. 97 15.80 1.834E+OO 1. 229E+OO 1. 229E+OO 29.49 OK RA-228 105.21 1.10 7.457E+OO 3 .151E+OO 3 .151E+OO 111.18 OK 338.32 11. 27 4.214E+OO 1. llOE+OO 1. llOE+OO 43.25 OK 794.95 4.25 2 .138E+OO 1.609E+OO 1.609E+OO 48.85 OK 835.71 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 OK 911. 20 25.80* 1.923E+OO 1. 408E+OO 1.408E+OO 21. 64 OK 968. 97 15.80 1.834E+OO 1.229E+OO 1.229E+OO 29.49 OK Page 3017 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235006 Acquisition date 3-0CT-2016 08:02:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 5. 996E+OO Line Not Found <<INT Reject 77 .11 17.10 6.163E+OO 1.887E+OO 1.887E+OO 19.08 OK 238.63 43.60* 5.555E+OO l.105E+OO 1.105E+OO 12.91 OK 300.09 3.30 4.643E+OO 1. 896E+OO 1.896E+OO 63. 67 OK TH-229 85.43 14.70 6.681E+OO 2.108E-01 2.108E-01 112. 36 OK 88.47 24.00 6.842E+OO 1.303E-01 1.303E-01 142.57 OK 193.51 4.41* 6.409E+OO Line Not Found Absent 210.85 2.80 6.074E+00 l .196E+00 1.196E+OO 140.62 OK TH-230 609.32 45.49* 2.627E+OO 7.694E-01 7.694E-01 22.24 OK 1120.29 14.92 1.635E+OO 6.500E-01 6.500E-01 60.22 OK 1764.49 15.30 1.106E+OO 1.155E+OO 1.155E+00 30.50 OK PA-231 283.69 1. 70 4.860E+OO Line Not Found Absent 301.36 5.35* 4.643E+OO 1.169E+OO 1.169E+OO 63.67 OK TH-232 105.21 1.10 7.457E+OO 3.151E+OO 3 .151E+OO 111.18 OK 338.32 11. 27 4.214E+OO 1. llOE+OO 1. llOE+OO 43.25 OK 835.71 1. 61 2.057E+00 2.690E+OO 2.690E+OO 98.38 OK 911. 20 25.80* 1.923E+OO 1.408E+OO 1.408E+OO 21. 64 OK 968. 97 15.80 l.834E+OO 1.229E+OO 1.229E+OO 29.49 OK TH-234 63.29 3.70* 4.822E+OO 1.305E-02 l.305E-02******* OK 92. 59 4.23 7 .101E+OO 1.932E+OO 1.932E+OO 61. 25 OK U-234 609.32 45.49* 2.627E+OO 7.694E-01 7.694E-01 22.24 OK 1120.29 14.92 1.635E+OO 6.500E-01 6.500E-01 60.22 OK 1764.49 15.30 1.106E+OO 1.155E+OO 1.155E+OO 30.50 OK U-235 89. 96 3.47 6.978E+OO 9.241E-01 9.241E-01 85.65 OK 93.35 5.60 7. lOlE+OO 1.459E+OO l.459E+OO 61.25 OK 143.76 10.96* 7.370E+OO Line Not Found Absent 163.33 5.08 7.024E+OO Line Not Found Absent 185.72 57.20 6.562E+OO 9.797E-02 9.797E-02 85. 62 OK 205.31 5.01 6.171E+00 Line Not Found Absent U-238 63.29 3.70* 4.822E+OO 1.305E-02 l.305E-02******* OK 92.59 4.23 7.101E+OO 1.932E+OO 1.932E+OO 61. 25 OK ANH-511 511. 00 100.00* 3.019E+00 2.603E-02 2.603E-02 286.68 OK Flag: "*" = Keyline Page 3018of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:05:35.82 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l *
  • Acquisition date 3-0CT-2016 08:02:32 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.99 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:25:00 Analyst initials: MXRl *
  • Sample ID G405235006 Sample Quantity 1.5634E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 597E+Ol l.437E+00 MN-54 8.395E-02 8.094E-02 C0-57 6.333E-02 6.855E-02 Y-91 6.675E+02 5.231E+02 CD-109 l.322E+OO 1.847E+00 SN-126 8.453E-02 l.181E-01 PM-147 1.104E+03 l.195E+03 EU-155 1.850E-01 2.016E-01 TL-208 3.661E-01 8.638E-02 BI-212 1.064E+OO -5.920E-01 PB-212 1.105E+OO 1.398E-01 BI-214 7. 696E-01 l.678E-01 1.080E+OO 1.703E-01 RN-222 7.696E-01 l.678E-01 RA-226 7. 696E-01 1.678E-01 AC-228 l.408E+OO 2.987E-01 RA-228 1.408E+OO 2.987E-01 TH-228 1.105E+OO 1.398E-01 TH-229 7.367E-02 4.123E-01 TH-230 7.694E-01 l.677E-01 PA-231 l.169E+OO 7.297E-01 TH-232 1.408E+OO 2.987E-01 TH-234 l.305E-02 2.015E+OO U-234 7.694E-01 1.677E-01 U-235 -2.283E-02 1.683E-01 U-238 1.305E-02 2.015E+OO ANH-511 2.603E-02 7.312E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3019of5809 Key-Line Activity (pCi/GRAM 1.023E+OO -2.495E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 8.808E+OO 3.358E-02 1. 960E+41 MDA (pCi/GRAM 3.706E-01 1.126E-01 7.947E-02 6.999E+02 1.773E+OO 1.137E-01 1.179E+03 l.643E-01 5.374E-02 6.980E-01 8.502E-02 1.143E-01 l.083E-01 1.143E-01 l.143E-01 l.578E-01 1.578E-01 8.502E-02 8.250E-01 1.143E-01 6 .113E-01 l.578E-01 l.560E+OO l.143E-01 3.042E-01 1.560E+OO 4.614E-02 MDA (pCi/GRAM 1.761E+Ol 5.855E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 O.OOOE+OO 8.732E-03 1.210E-02 NOT IDENT. SC-46 l.332E-01 2.927E-01 6.099E-01 FAIL ABUN V-48 O.OOOE+OO 1.052E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.021E+02 O.OOOE+OO SHORT HLIF C0-56 1.650E-01 2.952E-01 6.507E-01 FAIL ABUN MN-56 O.OOOE+OO 1.789E+41 O.OOOE+OO SHORT HLIF C0-58 -3.271E-01 4.576E-01 7.628E-01 NOT IDENT. FE-59 4.920E+OO 3.163E+OO 9.091E+OO NOT IDENT. C0-60 4.019E-02 2.818E-02 7.222E-02 NOT IDENT. ZN-65 -3.067E-02 . 1. 335E-01 2.514E-01 NOT IDENT. GE-68 -2.497E-01 1.905E+OO 3.777E+OO NOT IDENT. AS-73 4.709E-02 5.122E+OO 9.820E+OO NOT IDENT. AS-74 O.OOOE+OO 4.730E+03 O.OOOE+OO SHORT HLIF SE-75 -6.351E-02 1. 68 OE-01 3.059E-01 FAIL ABUN BR-77 O.OOOE+OO 1.382E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.250E+02 O.OOOE+OO SHORT HLIF RB-83 3.126E-02 5.566E-01 l.083E+OO NOT IDENT. KR-85 l.789E+OO 6.540E+OO l.171E+Ol NOT IDENT. SR-85 l.852E-01 6.763E-01 1. 211E+OO NOT IDENT. RB-86 O.OOOE+OO 2.298E+04 O.OOOE+OO SHORT HLIF Y-88 4.852E-02 7.663E-02 2.677E-01 NOT IDENT. NB-94 2.643E-02 2.816E-02 5.967E-02 NOT IDENT. NB-95 -4.482E-01 7.824E-01 1.348E+OO NOT IDENT. NB-95M -7.774E-02 2.027E+OO 3.588E+OO NOT IDENT. ZR-95 -1.106E-01 1. 356E+OO 2.525E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 9.017E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF RH-101 1. 017E-02 3.106E-02 5.424E-02 NOT IDENT. RH-102 -1.268E-02 4.314E-02 8. 041E-02 NOT IDENT. RU-103 -8.177E-01 4.273E+OO 8.146E+OO FAIL ABUN RH-106 2.870E-01 4.005E-01 8.522E-01 NOT IDENT. RU-106 2.870E-01 4.005E-01 8.522E-01 NOT IDENT. AG-108M -2.404E-02 2.189E-02 3.677E-02 NOT IDENT. AG-llOM -2.067E-02 7.810E-02 1. 429E-01 NOT IDENT. SN-113 -1. 728E-01 2.027E-01 3.583E-01 NOT IDENT. CD-115 O.OOOE+OO l.463E+39 0.000E+OO SHORT HLIF SN-117M O.OOOE+OO 8.675E+04 O.OOOE+OO SHORT HLIF TE-123M 7.504E-02 l.194E-01 2.273E-01 NOT IDENT. SB-124 1.068E+OO 1.509E+OO 3.831E+OO NOT IDENT. SB-125 5.590E-02 8.202E-02 1. 728E-01 FAIL ABUN TE-125M 3.300E+Ol 2. 511E+02 4.330E+02 NOT IDENT. I-126 O.OOOE+OO 6.554E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.492E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1. 2 93E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.417E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.209E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 2.209E+26 O.OOOE+OO SHORT HLIF BA-133 -1.606E-03 3.919E-02 7.061E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 5.032E-02 l.OOlE-01 FAIL ABUN CS-135 6.807E-02 1.326E-01 2.466E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.078E+05 O.OOOE+OO SHORT HLIF BA-137M 3.260E-02 3.657E-02 7.489E-02 NOT IDENT. CS-137 3.443E-02 3.863E-02 7. 911E-02 NOT IDENT. CE-139 3.492E-02 9. 631E-02 1. 800E-01 NOT IDENT. BA-140 O.OOOE+OO 8.021E+05 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 2.277E+05 O.OOOE+OO SHORT HLIF CE-141 -2.549E+OO 2.069E+Ol 3.738E+Ol NOT IDENT. CE-143 O.OOOE+OO 4.447E+40 O.OOOE+OO SHORT HLIF CE-144 8.658E-02 3.246E-01 6.052E-01 NOT IDENT. PM-144 9.297E-03 3.994E-02 8.052E-02 NOT IDENT. PR-144 7.690E-01 3.459E+OO 6. 964E+OO NOT IDENT. i?M-146 -4.613E-03 3.653E-02 6.994E-02 NOT IDENT. ND-147 O.OOOE+OO 2.538E+07 O.OOOE+OO SHORT HLIF PM-149 O.OOOE+OO l.938E+40 O.OOOE+OO SHORT HLIF EU-150 -1.374E-02 2.402E-02 3.900E-02 FAIL ABUN EU-152 2.263E-02 8.124E-02 l.563E-01 FAIL ABUN GD-153 3. 451E-02 l.485E-01 2. 811E-01 NOT IDENT. EU-154 -5.181E-02 8.030E-02 l.437E-01 NOT IDENT. TB-160 -1.190E+OO 1.530E+OO 2.487E+OO FAIL ABUN H0-166M 2.688E-02 4.531E-02 9.477E-02 NOT IDENT. TM-171 -1. 661E+OO 1.166E+Ol 2.218E+Ol NOT IDENT. HF-172 2.763E-02 2.097E-01 3.599E-01 FAIL ABUN LU-172 8.659E-02 6.847E-02 1.520E-01 FAIL ABUN LU-176 3.988E-03 2.147E-02 4.260E-02 FAIL ABUN Page 3020 of 5809 HF-181 1.079E+OO 3.284E+OO 6.687E+OO NOT IDENT. TA-182 7.436E-01 8.528E-01 1.849E+OO FAIL ABUN RE-183 -2.026E-01 1.829E+OO 3.463E+OO NOT IDENT. RE-184 -2.740E+00 2.614E+Ol 4.846E+Ol NOT IDENT. W-188 -4.717E+Ol 1.004E+02 1.672E+02 FAIL ABUN IR-192 -1.267E-01 3.466E-01 6.595E-01 FAIL ABUN HG-203 -7.852E-02 2.006E+OO 3.918E+OO FAIL ABUN BI-207 -l.900E-02 3. 968E-02 7.421E-02 FAIL ABUN PB-210 -1.283E+OO 1.617E+OO 2.972E+OO NOT IDENT. BI-211 0.000E+OO 4.691E-01 7.832E-01 FAIL ABUN PB-211 3.265E-02 5.032E-01 9.959E-01 NOT IDENT. RN-219 8.218E-02 3.087E-01 6 .196E-01 FAIL ABUN RA-223 2.836E-01 4.879E-01 1.005E+OO FAIL ABUN RA-224 O.OOOE+OO 8.792E-01 1.309E+OO FAIL ABUN AC-227 l.949E-02 1.984E-01 3.929E-01 FAIL ABUN TH-227 1.949E-02 1.984E-01 3.929E-01 FAIL ABUN TH-231 2.836E-01 4.879E-01 1.005E+OO FAIL ABUN PA-233 -2.120E-02 5.083E-02 9.575E-02 FAIL ABUN PA-234 l.098E-01 2.475E-01 5.245E-01 NOT IDENT. PA-234M 2.820E+OO 3.809E+OO 8.419E+OO NOT IDENT. NP-237 -2.120E-02 5.083E-02 9.575E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -1.976E-01 2.067E-01 3.502E-01 FAIL ABUN PU-239 4.764E+02 3.862E+02 5.310E+02 FAIL ABUN AM-241 2.954E-02 9.556E-02 l.724E-01 NOT IDENT. AM-243 8.165E-02 8.055E-02 1.lOOE-01 FAIL ABUN CM-243 1.654E-02 7. 731E-02 1.368E-01 NOT IDENT. BK-247 -1.296E-02 '6.102E-02 1. 061E-01 FAIL ABUN CM-247 -l.052E-02 2. 8 67,E-02 5.364E-02 NOT IDENT. CF-249 1.569E-02 3.256E-02 6. 621E-02 NOT IDENT. CF-251 6.862E-02 l.006E-01 2.083E-01 NOT IDENT. Page 3021 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:05:33.27 Nuclide Line Activity Report Nuclide Type:. Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 465 10.66* 1.312E+OO 1.597E+Ol 1.597E+Ol 9.18 MN-54 834.85 19 99.98* 2.057E+OO 4.332E-02 8.395E-02 98.38 C0-57 122.06 40 85.60* 7.574E+OO 2. 963E-02 6.333E-02 110. 46 136.47 ------10.68 7.468E+OO ------Line Not Found ------Y-91 1204.77 16 0.26* 1.543E+OO 1. 960E+Ol 6.675E+02 79. 96 CD-109 88.03 107 3.70* 6.842E+OO 2. 031E+OO 3.177E+OO 57.97 SN-126 64.28 0 9.60 4.822E+00 5. 031E-03 5.031E-03 15752.45 86.94 107 8.90 6.842E+OO 8.444E-01 8.444E-01 57.97 87.57 107 37.00* 6.842E+OO 2.031E-01 2.031E-01 57.97 PM-147 121. 22 40 0.00* 7.574E+OO 8.899E+02 1.104E+03 110.46 EU-155 86.55 107 30.70 6.842E+OO 2.448E-01 2.757E-01 57.97 105.31 54 21.10* 7.457E+00 1.643E-01 1.850E-01 111.18 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 176 85.00* 2.718E+OO 3.661E-01 3.661E-01 24.08 860.56 ------12.50 2. OllE+OO ------Line Not Found ------BI-211 72. 87 67 1. 23 5.884E+OO 4.460E+OO 4.460E+OO 100:67 351.06 327 12.92* 4.085E+OO 2.974E+OO 2.974E+OO 16.10 BI-212 727.33 34 6.67* 2.290E+OO 1.064E+OO 1.064E+OO 56.79 785.37 18 1.10 2.156E+OO 3.600E+OO 3.600E+OO 140.46 1620.50 ------1. 47 1.197E+OO ------Line Not Found ------PB-212 74.82 67 10.28 5.884E+OO 5.337E-01 5.337E-01 100.67 77 .11 414 17.10 6.163E+OO 1. 887E+OO 1.887E+OO 19.08 238.63 557 43.60* 5.555E+OO l.105E+OO 1.105E+OO 12.91 300.09 60 3.30 4.643E+OO l.896E+OO 1. 896E+OO 63. 67 BI-214 609.32 191 45.49* 2.627E+00 7.694E-01 7. 696E-01 22.24 1120.29 33 14.92 1.635E+OO 6.500E-01 6.502E-01 60.22 1764.49 41 15.30 1.106E+OO l.155E+OO 1.155E+OO 30.50 PB-214 74.82 67 5.80 5.884E+00 9.459E-01 9.463E-01 100.67 77 .11 414 9.70 6.163E+OO 3.326E+00 3.328E+OO 19.08 87.09 107 3.41 6.842E+OO 2.204E+00 2.205E+OO 57.97 242.00 94 7.25 5.502E+OO l.127E+OO 1.128E+OO 45.00 295.22 232 18.42 4.710E+OO l.287E+OO 1.287E+OO 21. 68 351.93 327 35.60* 4.085E+OO 1. 079E+OO 1.080E+OO 16.10 RN-222 609.32 191 45.49* 2.627E+OO 7.694E-01 7. 696E-01 22.24 1120.29 33 14.92 1.635E+OO 6.500E-01 6.502E-01 60.22 1764.49 41 15.30 1.106E+OO l.155E+OO 1.155E+OO 30.50 RA-224 240.99 94 4.10* 5.502E+00 1.994E+OO 1.994E+OO 45.00 RA-226 609.32 191 45.49* 2.627E+OO 7.694E-01 7.696E-01 22.24 1120.29 33 14.92 l.635E+00 6.500E-01 6.502E-01 60.22 1764.49 41 15.30 1.106E+OO l.155E+OO l.155E+00 30.50 AC-228 105.21 54 1.10 7.457E+OO 3 .151E+OO 3 .151E+OO 111.18 338.32 110 11. 27 4.214E+OO 1. llOE+OO 1. llOE+OO 43.25 794.95 30 4.25 2.138E+OO 1.609E+OO l.609E+OO 48.85 835.71 19 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 911. 20 146 25.80* 1. 923E+OO 1.408E+OO 1.408E+OO 21. 64 968. 97 74 15.80 1.834E+OO 1.229E+OO 1.229E+OO 29.49 RA-228 105.21 54 1.10 7.457E+OO 3.151E+OO 3 .151E+OO 111.18 Page 3022 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235006 Acquisition date 3-0CT-2016 08:02:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 338.32 110 11.27 4.214E+OO 1. llOE+OO l. llOE+OO 43.25 794.95 30 4.25 2 .138E+OO 1.609E+OO l.609E+OO 48.85 835.71 19 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 911. 20 146 25.80* l.923E+OO l.408E+OO l.408E+OO 21. 64 968.97 74 15.80 1.834E+OO 1.229E+OO 1.229E+OO 29.49 TH-228 74.82 67 10.28 5.884E+OO 5.337E-01 5.337E-01 100.67 77 .11 414 17.10 6.163E+OO 1.887E+OO 1.887E+OO 19.08 238.63 557 43.60* 5.555E+OO 1.105E+OO 1.105E+OO 12.91 300.09 60 3.30 4.643E+OO 1. 896E+OO 1.896E+OO 63.67 TH-229 85.43 43 14.70 6.681E+OO 2.108E-01 2.108E-01 112. 36 88.47 107 24.00 6.842E+OO 3 .131E-01 3 .131E-01 57.97 193.51 ------4.41* 6.409E+OO ------Line Not Found ------210.85 42 2.80 6.074E+OO 1.196E+OO 1.196E+OO 140.62 TH-230 609.32 191 45.49* 2.627E+OO 7.694E-01 7.694E-01 22.24 1120.29 33 14.92 1.635E+OO 6.500E-01 6.500E-01 60.22 1764.49 41 15.30 1.106E+OO 1.155E+OO 1.155E+OO 30.50 PA-231 283.69 ------1. 70 4.860E+OO ------Line Not Found ------301.36 60 5.35* 4.643E+OO 1.169E+OO 1.169E+OO 63.67 TH-232 10'5. 21 54 1.10 7.457E+OO 3 .151E+OO' 3 .151E+OO 111.18 338.32 110 11. 27 4.214E+OO 1. llOE+OO 1. llOE+OO 43.25 835.71 19 1. 61 2.057E+OO 2.690E+OO 2.690E+OO 98.38 911.20 146 25.80* 1.923E+OO 1.408E+OO l.408E+OO 21. 64 968.97 74 15.80 1.834E+OO 1.229E+OO l.229E+OO 29.49 TH-234 63. 29 0 3.70* 4.822E+OO 1.305E-02 1.305E-02 15752.45 92.59 121 4.23 7.101E+OO 1.932E+OO 1.932E+OO 61. 25 U-234 609.32 191 45.49* 2.627E+OO 7.694E-01 7.694E-01 22.24 1120.29 33 14.92 1.635E+OO 6.500E-01 6.500E-Ol* 60.22 1764.49 41 15.30 1.106E+OO l.155E+00 l.155E+OO 30.50 U-235 89. 96 47 3.47 6.978E+OO 9.241E-01 9.241E-01 85.65 93.35 121 5.60 7.101E+OO l.459E+00 1.459E+OO 61. 25 143.76 ------10.96* 7.370E+OO ------Line Not Found ------163.33 ------5.08 7.024E+OO ------Line Not Found ------185.72 77 57.20 6.562E+OO 9.797E-02 9.797E-02 85. 62 205.31 ------5.01 6.171E+OO ------Line Not Found ------U-238 63.29 0 3.70* 4.822E+OO l.305E-02 l.305E-02 15752.45 92.59 121 4.23 7.101E+OO 1.932E+OO 1.932E+00 61. 25 AM-243 43.53 ------5.90 1.315E+OO ------Line Not Found ------74.66 67 67.20* 5.884E+OO 8.164E-02 8.165E-02 100.67 ANH-511 511. 00 16 100.00* 3.019E+OO 2.603E-02 2.603E-02 286.68 Flag: "*" Key line Page 3023 of 5809 Summary of Nuclide Activity Sample ID : G405235006 Page : 3 Acquisition date 3-0CT-2016 08:02:32 Total number of lines in spectrum 55 Number of unidentified lines 20 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 MN-54 C0-57 Y-91 CD-109 SN-126 PM-147 EU-155 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 312.05D 271.74D 58. 510 461. 40D 2.30E+05Y 2.62Y 4.75Y l.41E+10Y 7.04E+08Y 1. 41E+10Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+10Y 1. 41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y. 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 94 2.14 34.1 1. 56 1. 00 1. 24 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.597E+Ol 4.332E-02 2.963E-02 1. 960E+Ol 2.031E+OO 2.031E-01 8.899E+02 1.643E-01 3.661E-01 2.974E+OO 1.064E+OO 1.105E+OO 7.694E-01 1.079E+OO 7.694E-01 1.994E+OO 7.694E-01 1.408E+OO l.408E+00 1.105E+OO 3.131E-01 7.694E-01 l.169E+OO 1.408E+OO l.305E-02 7.694E-01 9.797E-02 l.305E-02 8.164E-02 2.603E-02 9.474E+02 9.474E+02 Decay Corr pCi/GRAM 1.597E+Ol 8.395E-02 6.333E-02 6.675E+02 3.177E+OO 2. 031E-01 l.104E+03 l.850E-01 3.661E-01 2.974E+OO 1.064E+OO 1.105E+OO 7. 696E-01 1.080E+OO 7. 696E-01 1.994E+OO 7. 696E-01 1.408E+OO 1.408E+OO l.105E+OO 3.131E-01 7.694E-01 1.169E+OO 1.408E+OO l.305E-02 7.694E-01 9.797E-02 l.305E-02 8.165E-02 2.603E-02 1. 811E+03 1. 811E+03 63.64% Decay Corr 2-Sigma %Error 9.18 98.38 110.46 79. 96 57.97 57.97 110.46 111.18 24.08 16.10 56.79 12.91 22.24 16.10 22.24 45.00 22.24 21. 64 21. 64 12.91 57.97 22.24 63. 67 21. 64 2-Sigma Error 0.147E+Ol 8.259E-02 6.995E-02 5.337E+02 1.842E+OO 1.177E-01 l.219E+03 2.057E-01 0.881E-01 0.479E+OO 0.604E+00 0.143E+OO 1. 712E-01 0.174E+OO l.712E-01 0.897E+OO 1.712E-01 0.305E+OO 0.305E+OO 0.143E+OO l.815E-01 l.711E-01 0.745E+OO 0.305E+OO 205.6E-02 1. 711E-01 8.388E-02 205.6E-02 8.220E-02 7.461E-02 15752.45 22.24 85.62 15752.45 100.67 286.68 Flags: "K" Keyline not found "E" = Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Page 3024 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235006 Acquisition date : 3-0CT-2016 08:02:32 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 7 26. 75 22 11 1.19 53.71 51 16 4.30E-03 **** 1. 71E-07 7 28.24 54 98 2.00 56.68 51 16 1. 05E-02 **** 1.29E-05 0 128.75 47 103 1. 75 257.57 255 6 l.05E-02 82.7 7.54E+OO T 0 270.34 77 123 1. 48 540.60 535 13 1. 84E-02 69.1 . 5. 05E+OO T 0 446.92 43 33 2.59 893.68 885 15 1. 09E-02 68.8 3.36E+OO 0 462.90 51 55 1. 74 925. 64 919 15 1.29E-02 72.2 3.27E+OO T 0 543.83 69 33 5.63 1087.48 1074 30 1. 7 6E-02 56.2 2.87E+OO 0 654.51 27 15 1. 06 1308.89 1304 10 7.08E-03 69.0 2.48E+OO 0 957.75 14 11 3.21 1915.67 1910 9 3.83E-03 **** 1. 85E+OO 1 964. 57 42 10 1. 94 1929.32 1922 22 1. 15E-02 44.6 1. 84E+OO T 0 1088.96 11 12 1.19 2178.31 2174 9 2.92E-03 **** 1. 67E+OO 0 1095.52 29 11 4.82 2191.43 2183 17 8.07E-03 66.8 l.66E+00 0 1104. 64 12 6 3.10 2209.70 2204 11 3.19E-03 98.6 1.65E+OO 0 1108. 77 11 4 1.17 2217.95 2214 7 2.92E-03 85.4 1. 65E+OO 1 1206.69 13 7 1. 87 2414.00 2400 20 3.77E-03 **** 1.54E+OO 0 1238.48 26 7 2.23 2477.66 2472 10 7.42E-03 54.4 1.51E+OO T 0 1258.60 11 11 1. 01 2517.96 2512 9 3.12E-03 **** 1.49E+OO 0 1288.43 15 7 2.88 2577.68 2572 13 4.17E-03 87.6 1.46E+OO 0 1334.20 17 6 1.19 2669.34 2664 12 4.73E-03 75.1 1. 42E+OO 0 1360.53 5 4 0.55 2722.08 2718 6 l.53E-03 **** 1.39E+OO 0 1377. 89 21 5 1. 34 2756.85 2751 11 6.08E-03 59.3 1.38E+OO 0 1416.25 6 8 0.55 2833.68 2823 12 1. 74E-03 **** 1.35E+OO 0 1588.20 11 6 4.32 3178.14 3171 12 3.06E-03 **** 1.22E+OO 0 1630.78 11 0 0.83 3263.45 3257 11 3.06E-03 60.3 1.19E+00 0 1729.10 13 3 0.72 3460.47 3453 13 3.67E-03 78.0 l.13E+OO Flags: "T" = Tentatively associated Page 3025 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:05:47.73 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l *
  • Acquisition date 3-0CT-2016 08:02:32 Sensitivity 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.99 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:25:00 Nuclide Library : SOLID *
  • Sample ID G405235006 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.5634E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 C0-57 Y-91 CD-109 SN-126 PM-147 EU-155 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 ANH-511 Le (pCi/GRAM l.384E-01 5.004E-02 3.745E-02 2. 941E+02 8.436E-01 5. 411E-02 5. 496E+02 7.715E-02 2.397E-02 3.053E-01 3. 968E-02 5.156E-02 4.948E-02 5.156E-02 5.156E-02 6.554E-02 6.554E-02 3. 968E-02 3.882E-01 5.154E-02 2.781E-01 6.554E-02 7.400E-01 5.154E-02 l.435E-01 7.400E-01 2.085E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3026 of 5809 Le (pCi/GRAM 7.828E+00 2.373E-02 0.000E+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 C0-56 MN-56 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3027 of 5809 2.652E-01 O.OOOE+OO O.OOOE+OO 2.781E-01 O.OOOE+OO 3.229E-01 3.818E+OO 3.097E-02 1. 072E-01 1.628E+OO 4.638E+OO O.OOOE+OO 1.403E-01 O.OOOE+OO O.OOOE+OO 4.866E-01 5. 311E+OO 5.493E-01 O.OOOE+OO 9 .115E-02 2.700E-02 5.977E-01 1.670E+OO 1.124E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0. OOOE+OO' 2.551E-02 3.477E-02 3.613E+OO 3.807E-01 3.807E-01 1. 621E-02 6.085E-02 1.624E-01 O.OOOE+OO O.OOOE+OO 1.071E-01 1.548E+OO 7.840E-02 2.040E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.246E-02 O.OOOE+OO 4.526E-02 1.149E-01 O.OOOE+OO O.OOOE+OO 3.438E-02 3.632E-02 8.445E-02 O.OOOE+OO O.OOOE+OO 1. 757E+Ol O.OOOE+OO 2.854E-01 3.526E-02 3.048E+OO 3 .151E-02 O.OOOE+OO O.OOOE+OO 1. 781E-02 7.175E-02 l.327E-01 5.823E-02 1.050E+OO 4.209E-02 1.044E+Ol 1. 689E-01 6.752E-02 l.971E-02 2.999E+OO FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. TA-182 RE-183 RE-184 W-188 IR-:j.92 HG-203 BI-207 PB-210 BI-211 PB-211. RN-219 RA-223 RA-224 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3028 of 5809 8.279E-01 1.634E+OO 2 .117E+Ol 7.674E+Ol 2.995E-01 1. 817E+OO 3.182E-02 1.398E+OO 3.789E-01 4.488E-01 2.818E-01 4.637E-01 6.245E-01 1.828E-01 1. 828E-01 4.637E-01 4.395E-02 2.327E-01 3.770E+OO 4.395E-02 O.OOOE+OO 1.635E-01 2.509E+02 8.159E-02 5.328E-02 6.378E-02 4.862E-02 2.425E-02 3.038E-02 9.823E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:05:53.20 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235006.CNF;l *
  • Acquisition date 3-0CT-2016 08:02:32 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.99 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:25:00 Nuclide Library : SOLID *
  • Sample ID G405235006 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.5634E+02 GRAM *
  • Quantity Err(%) : l.2792E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. 'Cal. date 30-JUN-2016 06: 52: 39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 1.597E+Ol l.661E+OO MN-54 8.395E-02 8.lOlE-02 C0-57 6.333E-02 6.862E-02 Y-91 6.675E+02 5.236E+02 CD-109 1.322E+OO 1.865E+OO SN-126 8.453E-02 1.191E-01 PM-147 l.104E+03 1. 196E+03 EU-155 1.850E-01 2.020E-01 TL-208 3.661E-01 8.776E-02 BI-212 1.064E+OO 5.944E-01 PB-212 1.105E+OO l.515E-01 BI-214 7. 696E-01 l.710E-01 PB-214 1.080E+OO 1.761E-01 RN-222 7. 696E-01 l.710E-01 RA-22 6 7.696E-01 1.710E-01 AC-228 1.408E+OO 3. 072E-01 RA-228 l.408E+OO 3.072E-01 TH-228 1.105E+OO l.515E-01 TH-229 7.367E-02 4.123E-01 TH-230 7.694E-01 1. 709E-01 PA-231 1.169E+OO 7.712E-01 TH-232 l.408E+OO 3. 072E-01 TH-234 l.305E-02 2.015E+OO U-234 7.694E-01 1.709E-01 U-235 -2.283E-02 l.684E-01 U-238 l.305E-02 2.015E+OO ANH-511 2.603E-02 7.313E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3029 of 5809 Key-Line Activity (pCi/GRAM 1.023E+OO -2.495E-02 l.OOOE+41 K.L Act error ( 1. 96-sigma) 8.808E+OO 3.359E-02 3.151E+41 TPU ( 1. 96-sigma) 1. 661E+OO 8. lOlE-02 6.862E-02 5.236E+02 1.865E+OO 1.191E-01 1.196E+03 2.020E-01 8.776E-02 5.944E-01 1.515E-01 1.710E-01 1. 761E-01 1.710E-01 1.710E-01 3.072E-01 3.072E-01 1.515E-01 4.123E-01 l.709E-01 7. 712E-01 3.072E-01 2.015E+OO l.709E-01 'l.684E-01 2.015E+OO 7.313E-02 TPU ( 1. 96-sigma) 8.820E+OO 3.542E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 O.OOOE+OO O.OOOE+OO O.OOOE+OO NOT IDENT. SC-46 l.332E-01 2.928E-01 2.989E-01 FAIL ABUN V-48 -7.895E+02 l.052E+04 l.053E+04 SHORT HLIF CR-51 -l.589E+02 3.022E+02 3.105E+02 SHORT HLIF C0-56 l.650E-01 2.953E-01 3.045E-01 FAIL ABUN MN-56 l.OOOE+41 1. 790E+41 O.OOOE+OO SHORT HLIF C0-58 -3.271E-01 4.578E-01 4.809E-01 NOT IDENT. FE-59 4.920E+OO 3.183E+OO 3.880E+OO NOT IDENT. C0-60 4.019E-02 2.821E-02 3.353E-02 NOT IDENT. ZN-65 -3.067E-02 l.335E-01 l.342E-01 NOT IDENT. GE-68 -2.497E-01 1.905E+OO l.909E+OO NOT IDENT. AS-73 4.709E-02 5.122E+OO 5.122E+OO NOT IDENT. AS-74 5. 8 66E+02 4.730E+03 4.738E+03 SHORT HLIF SE-75 -6. 351E-02 l.681E-01 l.705E-01 FAIL ABUN BR-77 l.092E+38 9.390E+38 O.OOOE+OO SHORT HLIF SR-82 -3.489E+02 6.252E+02 6.447E+02 SHORT HLIF RB-83 3.126E-02 5.566E-01 5.568E-01 NOT IDENT. KR-85 1. 789E+OO 6.540E+00 6.590E+OO NOT IDENT. SR-85 l.852E-01 6.763E-01 6.815E-01 NOT IDENT. RB-86 -8.693E+03 2.298E+04 2.331E+04 SHORT HLIF Y-88 4.852E-02 .7. 669E-02 7.975E-02 NOT IDENT. NB-94 2.643E-02 2.818E-02 3.059E-02 NOT IDENT. NB-95 -4.482E-01 7.827E-01 8.083E-01 NOT IDENT. NB-95M -7.774E-02 2.027E+00 2.028E+OO NOT IDENT. ZR-95 -l.106E-01 1. 356E+OO 1. 356E+00 NOT IDENT. NB-97 -1.000E+41 l.063E+42 0.000E+OO SHORT HLIF ZR-97 1.000E+41 1. 758E+42 O.OOOE+OO SHORT HLIF M0-99 -2.556E+31 9.018E+31 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 4.493E+41 O.OOOE+OO SHORT HLIF RH-101 1.017E-02 3. lllE-02 3.145E-02 NOT IDENT. RH-102 -l.268E-02 4.315E-02 4.353E-02 NOT IDENT. RU-103 -8.177E-01 4.273E+OO 4.289E+OO FAIL ABUN RH-106 2.870E-01 4.009E-01 4.212E-01 NOT IDENT. RU-106 2.870E-01 4.009E-01 4.212E-01 NOT IDENT. AG-108M -2.404E-02 2 .191E-02 2.444E-02 NOT IDENT. AG-llOM -2.067E-02 7.810E-02 7.866E-02 NOT IDENT. SN-113 -l.728E-01 2.029E-01 2.173E-01 NOT IDENT. CD-115 -2.604E+38 l.464E+39 O.OOOE+OO SHORT HLIF SN-117M -6.846E+03 8.675E+04 8. 681E+04 SHORT HLIF TE-123M 7.504E-02 l.195E-01 l.242E-01 NOT IDENT. SB-124 l.068E+00 1.510E+OO 1.585E+OO NOT IDENT. SB-125 5.590E-02 8.205E-02 8.583E-02 FAIL ABUN TE-125M 3.300E+Ol 2. 511E+02 2.516E+02 NOT IDENT. I-126 2.407E+04 6.554E+05 6.555E+05 SHORT HLIF SB-126 -2. 921E+05 9.508E+05 9.598E+05 SHORT HLIF SB-127 -l.057E+21 1. 301E+22 O.OOOE+OO SHORT HLIF I-131 2.058E+09 3.419E+09 3.542E+09 SHORT HLIF I-132 -1.000E+41 l.839E+42 O.OOOE+OO SHORT HLIF TE-132 l.221E+26 2.263E+26 O.OOOE+OO SHORT HLIF BA-133 -l.606E-03 3.919E-02 3.919E-02 NOT IDENT. I-133 -l.000E+41 l.045E+43 O.OOOE+OO SHORT HLIF CS-134 1.051E-01 5.052E-02 6.926E-02 FAIL ABUN CS-135 6.807E-02 1.327E-01 1.362E-01 NOT IDENT. I-135 -1.000E+41 2.090E+42 O.OOOE+OO SHORT HLIF CS-136 -4.409E+03 2.078E+05 2.078E+05 SHORT HLIF BA-137M 3.260E-02 3.659E-02 3.943E-02 NOT IDENT. CS-137 3.443E-02 3.866E-02 4.166E-02 NOT IDENT. CE-139 3.492E-02 9.656E-02 9.784E-02 NOT IDENT. BA-140 2.207E+04 8. 021E+05 8.022E+05 SHORT HLIF LA-140 -5.841E+04 2.277E+05 2.292E+05 SHORT HLIF CE-141 -2.549E+OO 2.069E+Ol 2. 072E+Ol NOT IDENT. CE-143 l.000E+41 4.561E+40 O.OOOE+OO SHORT HLIF CE-144 8.658E-02 3.247E-01 3.270E-01 NOT IDENT. PM-144 9.297E-03 3.995E-02 4.017E-02 NOT IDENT. PR-144 7.690E-01 3.460E+OO 3.477E+OO NOT IDENT. PM-146 -4.613E-03 3.653E-02 3:659E-02 NOT IDENT. ND-147 -1.414E+07 2.539E+07 2.618E+07 SHORT HLIF PM-149 -1.459E+40 1. 964E+40 O.OOOE+OO SHORT HLIF EU-150 -l.374E-02 2.403E-02 2. 481E-02 FAIL ABUN EU-152 2.263E-02 8.125E-02 8.189E-02 FAIL ABUN GD-153 3. 451E-02 l.485E-01 l.493E-01 NOT IDENT. EU-154 -5.181E-02 8.033E-02 8.365E-02 NOT IDENT. TB-160 -1.190E+OO 1. 532E+OO 1.623E+OO FAIL ABUN H0-166M 2.688E-02 4.533E-02 4.692E-02 NOT IDENT. TM-171 -1.661E+OO 1.166E+Ol 1.168E+Ol NOT IDENT. HF-172 2.763E-02 2.097E-01 2.lOlE-01 FAIL ABUN LU-172 8.659E-02 6.902E-02 7.930E-02 FAIL ABUN LU-176 3.988E-03 2.147E-02 2.154E-02 FAIL ABUN Page 3030 of 5809 HF-181 1.079E+OO 3.284E+OO 3.320E+OO NOT IDENT. TA-182 7.436E-01 8.532E-01 9.167E-01 FAIL ABUN RE-183 -2.026E-01 1. 829E+OO 1.832E+OO NOT IDENT. RE-184 -2.740E+OO 2.614E+Ol 2.617E+Ol NOT IDENT. W-188 -4.717E+Ol 1. 005E+02 l.027E+02 FAIL ABUN IR-192 -1. 267E-01 3.466E-01 3. 513E-01 FAIL ABUN HG-203 -7.852E-02 2.006E+OO 2.007E+OO FAIL ABUN BI-207 -1.900E-02 3. 968E-02 4.060E-02 FAIL ABUN PB-210 -1.283E+OO 1.621E+OO 1.721E+OO NOT IDENT. BI-211 2.974E+OO 4.874E-01 1. 42 6E+OO EAIL ABUN PB-211 3.265E-02 5.032E-01 5.034E-01 NOT IDENT. RN-219 8.218E-02 3.089E-01 3. lllE-01 FAIL ABUN RA-223 2.836E-01 4.882E-01 5.047E-01 FAIL ABUN RA-224 1.994E+OO 8.856E-01 l.262E+OO FAIL ABUN AC-227 l.949E-02 1.984E-01 1. 98 6E-01 FAIL ABUN TH-227 1.949E-02 1.984E-01 1. 98 6E-Ol FAIL ABUN TH-231 2.836E-01 4.882E-01 5.047E-01 FAIL ABUN PA-233 -2.120E-02 5.084E-02 5.173E-02 FAIL ABUN PA-234 l.098E-01 2.776E-01 2.820E-01 NOT IDENT. PA-234M 2.820E+OO 3. 811E+OO 4.0lBE+OO NOT IDENT. NP-237 -2.120E-02 5.084E-02 5.173E-02 FAIL ABUN NP-238 -2.635E+40 2.010E+41 O.OOOE+OO SHORT HLIF NP-239 -1. 976E-01 2.073E-01 2.257E-01 FAIL ABUN PU-239 4.764E+02 3.868E+02 4.424E+02 FAIL ABUN AM-241 2.954E-02 9.558E-02 9. 651E-02 NOT IDENT. AM-243 8.165E-02 8. 071E-02 8.870E-02 FAIL ABUN CM-243 1.654E-02 7.733E-02 7.769E-02 NOT IDENT. BK-247 -1. 296E-02 6.107E-02 6.135E-02 FAIL ABUN CM-247 -1.052E-02 2.873E-02 2. 911E-02 NOT IDENT. CF-249 1.569E-02 3.259E-02 3.335E-02 NOT IDENT. CF-251 6.862E-02 1.009E-01 l.055E-01 NOT IDENT. Page 3031 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 95.6707 87.09 127.8269 136.47 90.6452 45.60 88.5982 87.57 127.9089 140.51 0.0000 46.54 95.1794 88.03 127.9884 143.76 91.3067 49.72 0.0000 88.34 114.3227 144.24 88.9131 51. 35 100.3728 88.47 114. 3421 145.44 81. 7012 51. 87 99.3889 89. 96 97.7650 152.43 84.7055 52.39 89.7516 1093.63 97.8522 153.25 0.0000 52.97 87.6816 91.11 0.0000 323.87 92.2256 53.44 96. 4237 92.59 98.1009 156.02 0.0000 54.07 90.0252 93.35 98.1973 158.56 0.0000 57. 36 0.0000 94.56 87.5926 159.00 69.1694 57.53 90.5761 94.65 87.6031 162.33 68.1407 57.98 97.1988 94.67 87.6054 162.66 0.0000 59.27 94.8598 94.87 87.6274 163.33 70.6829 59.32 94.8677 97.43 84.4413 165.86 68.3581 59.54 94.9031 98.43 85.7053 176.31 75.2582 60. 96 98.0573 98.44' 85.7065 176.60 0.0000 61.17 98.0917 99.53 86.9820 177.52 75.3369 62.93 114.5288 100 .11 70.7961 181.07 0.0000 63.29 114.5964 102.03 69.7998 181.52 69.2938 63.58 114.6506 103.18 68.3440 184.41 75.7764 64.28 114. 7809 103.37 59.0379 143.76 74.1739 66.73 115.2322 105.21 79.4105 193.51 80.5873 67.24 143.4160 105.31 79.4198 197.03 73.1591 125.81 134.6384 106.12 79.4966 198.01 61.2971 67.75 134.6532 106.47 79.5298 201.83 64.0450 69.67 129.1194 109.28 84.4868 203.43 67.9726 70.83 141.2427 111. 00 94.0619 205.31 71.9260 72. 81 118.5529 111.76 0.0000 210.85 77.3932 72. 87 118.5634 114.06 96.7519 215.65 69.0454 74.66 118.8796 116.30 0.0000 222 .11 74.5816 74.82 118.9079 116.74 91.1279 227.09 76.5954 74.97 118.9338 119.76 71.2473 227.38 76.6115 77 .11 119.3066 121.12 63.0289 228.16 0.0000 78.74 102.2885 121. 22 63.0358 228.18 63.5898 79.69 100.9205 121. 78 77.7523 116.74 63.5898 80.12 85.9099 122.06 88.8866 235.69 61.7442 80.19 0.0000 122.92 73.0823 235.96 61. 7 556 80.57 83.7022 123.07 77.8615 238.63 65.8218 81. 00 90.5438 265.00 79.5029 238.98 0.0000 81. 07 104.1359 125.81 74.9039 240.99 79.1171 81. 75 83.8411 127.23 75.0167 242.00 62.0188 83.79 93.9259 127.91 76.6682 244.70 37.0166 84.00 84.8608 129.30 78.3799 252.40 0.0000 85.43 93.3780 131.20 88.1520 252.80 46.0850 86.55 93.5194 133.02 83.0999 254.15 0.0000 86. 79 93.5494 133. 52 84.3480 256.23 57.7399 86.94 127.8013 136.00 88.1857 260.90 0.0000 Page 3032 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 48.2377 355.39 0.0000 584.27 22.9722 264.80 48.2421 356.01 35.3600 595.83 0.0000 265.00 44.2279 364.49 0.0000 427.87 23 .1127 2 68. 22 51.0358 366.42 0.0000 602.52 0.0000 269.46 49.2854 372.51 35.1934 604.72 23.6737 270.03 49.3033 375.05 36.1925 607.14 28.4337 271.23 49.3413 377.52 26.7023 609.32 28.4568 273.65 0.0000 356.01 26.7889 610.33 22.1416 276.40 47.5256 388.16 33.5595 614.28 31.6760 277.37 51.3373 388.63 0.0000 618.01 16.9167 277.60 49.5439 391. 69 46.1064 620.36 29.6304 278.00 45. 0511 264.66 34.7344 621.93 14.8232 279.20 55.0045 401.81 29.9272 630.19 0.0000 279.54 52.3100 402.40 35.7301 631.29 16.9980 279.70 55.9239 404.85 27.0715 633.25 12.7573 280.46 60.4625 410.95 35.8799 634.78 0.0000 283.69 43.4043 413.71 33.0150 635.95 22.3467 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 53.4087 423. 72 0.0000 645.85 20.2896 285.90 0.0000 427.09 26.3859 657.76 22.5193 287.50 41.6950 427.87 22.4848 657.90 0.0000 290.67 51.7676 433.94 34.3143 661. 66 24. 6967 293.27 0.0000 439.40 24.7688 664.57 0.0000 351. 93 28.6879 453.88 29.6832 666'. 33 0.0000 295.96 30.0681 463.37 24.8418 666.50 0.0000 879.38 27.3779 468.07 23.8979 667. 71 0.0000 299.98 34.2514 473.00 0.0000 677.62 16.1951 300.09 34.2537 475.06 16.9799 685.70 0.0000 300.13 34.2545 476.78 20.9910 695.00 0.0000 301.36 34.2796 477.60 19.9984 696.49 14.1251 302.85 39.7998 482.18 21.0402 696. 51 14.1251 256.23 42. 5872 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 19.5630 306.78 47.6889 497.08 23.1919 697.49 20.6514 308.46 54.1626 505.52 21.2508 702.65 17.4199 311. 90 49.6736 507.63 0.0000 706.68 19.6238 316.51 38.7393 511. 00 29.4136 711.68 14.1960 319.41 0.0000 514.00 27.4197 720. 70 0.0000 320.08 0.0000 514.00 27.4197 721. 93 0.0000 321.04 44.3896 520.40 25.4557 722. 78 27.9467 323.87 37.0516 520.69 0.0000 722.91 27.9477 325.23 56.5471 522.65 0.0000 723. 31 23.0192 328.76 0.0000 527.90 0.0000 724 .19 11.5130 333.37 51.6857 528.26 26.5586 727.33 16.4636 333.97 48.9090 529.59 20.4411 733.00 19.7922 334.37 53.1128 529.87 0.0000 735.93 13.2075 338.28 40.1550 531.02 0.0000 333.97 17.6185 338.32 40.1559 537.26 0.0000 739.50 0.0000 311. 90 51.8912 546.56 0.0000 747.24 19.8823 340.48 51.8912 552.55 10.8303 748.06 15.4680 340.55 0.0000 563.25 18.6445 752.31 25.4454 344.28 37.1024 569.33 24.9180 753.82 0.0000 345.93 43.8883 946.00 30 .1104 756.73 23.2653 351.06 37.6164 569.70 30.1128 756.80 23.2661 351.93 37.6343 583.19 22. 9623 884.68 16.6559 Page 3033 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 28.8861 1274.44 12.4457 1620.50 6.0806 766.42 27.7812 1001.03 12.4606 1621. 92 4.0547 766.84 18.8933 1002.74 13.3566 1678.03 0.0000 772. 60 0.0000 1004.73 24.0535 1690.97 2.0516 776.52 0.0000 507.63 0.0000 1750.46 0.0000 . 739. 50 0.0000 1025.87 0.0000 1764.49 0.0000 778.90 11.1552 1028.54 0.0000 1063.66 3 .1183 783.70 0.0000 1037.84 10.7798 1771.35 3 .1190 785.37 15.0892 1038.76 0.0000 1791.20 0.0000 792.07 10.0800 631.29 14.4043 1808.65 0.0000 794.95 13.4517 1048.07 0.0000 1810. 72 0.0000 795.86 18.5014 1049.04 11.7098 1836.06 0.0000 810.06 19.1430 1050.41 12.6149 810.29 22.5228 1063.66 17.1758 344.28 20.2712 1077.00 0.0000 810.76 18.0208 1077.34 14.5117 815.77 0.0000 1085.87 8. 7252 1048.07 0.0000 1093.63 7.2842 832.01 13.6006 1099.45 0.0000 834.85 21. 5520 1112. 07 8.7791 835.71 21.5575 1112.84 14.6348 836.80 0.0000 1115. 54 13.5985 846.75 0.0000 1120.29 11. 7281 846.77 6. 82 9'3 1120. 55 16.1272 856.80 0.0000 1221.41 19.2466 860.56 7.9992 1129. 67 13.7741 871.09 12.6077 1131. 51 0.0000 873.19 11. 4685 1147.95 0.0000 875.33 0.0000 1173.23 20.4048 879.38 18.3815 1177.95 18.5693 880.51 14.9397 1189.05 17.6849 883.24 6.9004 1204.77 9.3402 884.68 13.8066 1221.41 14.0616 889.28 10.3682 1231. 02 . 15. 9697 894.76 17.3065 1235.36 0.0000 898.04 16.1676 1238.28 15.0537 900. 72 13.8682 1260.41 0.0000 903.28 17.3474 1271.87 7.5815 911.20 8. 112 8 1274.44 11.3782 912.08 8 .1148 1274.54 12.3264 923.98 0.0000 1291.59 7.6128 926.50 12.8020 1298.22 0.0000 929 .11 12.8110 1312 .11 0.0000 937.49 20.1348 1332.49 1.5355 944.13 0.0000 1362.66 0.0000 946.00 15.7934 1365.19 11.5928 949.00 17.5623 1368.63 0.0000 667.71 0.0000 1384.29 8.7275 962. 31 7. 0496 1408.01 6.2355 964.08 15 .1130 1457.56 0.0000 966 .17 15.1214 1460.82 2.9528 911. 20 15.1324 1489.16 3.9583 968. 97 15.1324 1505.03 12.9024 983.53 0.0000 1584.12 6.4441 984.45 0.0000 1596.21 0.0000 Page 3034 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:06:26.57 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM32.CNF;277 Background date : 2-0CT-2016 11:01:57. Sample date 10-DEC-2015 13:55:00 Acquisition date : 3-0CT-2016 08:02:54. Sample ID G405235007 Sample quantity 1.52523E+02 GRAM Detector name : GAM32 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.63 Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 0 5 5 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 7 7 0 0 0 0 0 0 0 0 0 0 Page 3035 of 5809 Energy 62.99* 75.19 77.47 87.49 93.12* 94.77 129.53 186.37* 209.43 239.11* 242 .11 270.47 295.71* 300.59 338.59 352.25* 464.99 511. 31* 534.57 583.92* 609.94* 662.17 707.28 710.32 720.76 728.15* 797.49 803.54* 812.25 816.56 861.47* 911.71* 969.39 996.21 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 45 109 181 38 46 32 31 139 71 381 93 46 168 24 114 255 14 46 24 139 165 91 11 27 14 35 23 19 13 9 20 103 56 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 145 157 135 136 153 84 117 169 76 91 90 61 74 52 63 67 51 53 36 38 38 55 9 15 7 27 26 11 11 15 18 8 44 13 1. 34 1. 29 1.14 1. 68 1. 93 1. 26 1. 78 1. 23 1. 25 1.23 1. 62 1. 08 1. 34 1. 45 1. 03 1.13 0.67 1. 96 3.98 1.19 1. 42 1. 77 1. 96 2.00 3.40 0.95 1. 86 0.66 3.67 1. 70 1. 45 1. 62 1. 73 1.17 127.20 151.59 156.14 176.20 187.46 190.76 260.27 373. 96 420.08 479.43 485.43 542.17 592.64 602.40 678.40 705.72 931.20 1023.86 1070.37 1169. 08 1221.11 1325.59 1415.81 1421.88 1442.77 1457.55 1596. 23 1608. 33 1625.76 1634.38 1724.20 1824.69 1940.04 1993.69 123 147 147 174 184 184 256 368 416 474 474 537 588 599 673 699 925 1017 1064 1162 1215 1319 1413 1413 1438 1450 1586 1604 1617 1630 1719 1819 1933 1989 9 1. 25E-02 51. 6 13 3.02E-02 23.0 13 5.02E-02 13.1 6 1. 05E..:02 51. 5 10 1.28E-02 51.7 10 8.77E-03 57.2 8 8.50E-03 64.0 13 3.85E-02 21.6 8 1.97E-02 24.4 17 1.06E-01 6.6 17 2.57E-02 25.5 10 l.27E-02 35.6 11 4.66E-02 12.7 8 6.67E-03 55.9 11 3.15E-02 16.5 12 7.08E-02 9.0 11 3.97E-03101.l 14 l.28E-02 41.6 13 6.57E-03 56.1 14 3.85E-02 12.8 14 4.59E-02 11.3 13 2.52E-02 19.9 25 3.12E-03 48.2 25 7.41E-03 35.6 10 3.86E-03 45.4 12 9.78E-03 34.8 14 6.26E-03 53.8 11 5.25E-03 44.7 13 3.52E-03 64.3 8 2.62E-03 76.6 10 5.62E-03 45.5 11 2. 87E-02 11. 5 17 1.56E-02 30.9 12 3.43E-03 63.2 Fit 9.54E-01 4.56E+00 l.54E+OO 1.37E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235007 Acquisition date 3-0CT-2016 08:02:54 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1049.83 19 6 3.87 2100.93 2093 14 5.20E-03 37.6 36 0 1121.18* 38 14 1. 72 2243.64 2238 10 1. 05E-02 25.4 37 0 1190.02 9 7 0.61 2381. 31 2378 6 2.57E-03 56.4 38 0 1227.61 16 12 3.52 2456.49 2449 15 4.58E-03 50.8 39 0 1234.03 27 5 2.60 2469.34 2464 10 7.53E-03 24.6 40 0 1239.00 23 6 1. 24 2479.29 2475 11 6.25E-03 29.2 41 0 1245.45 17 3 3.62 2492.19 2486 11 4.79E-03 30.4 42 0 1250.95 17 15 3.83 2503.18 2497 14 4.77E-03 52.4 43 0 1333.81 15 3 4.00 2668.91 2663 11 4.25E-03 33.0 44 0 1337.86 6 0 1. 50 2677.00 2674 6 1.67E-03 40.8 45 0 1461.22* 389 3 1. 96 2923.73 2917 14 1.08E-01 5.2 46 0 1544.74 9 2 0.52 3090.77 3086 8 2.58E-03 41. 8 47 0 1765.38* 23 0 1. 50 3532.08 3527 10 6.40E-03 22.4 Flag: "*" = Peak area was modified by background subtraction Page 3036 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:06:28 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 13:55:00 G405235007 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:02:54 152.52 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA32 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3037 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.63 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235007 Acquisition date 3-0CT-2016 08:02:54 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l .119E+00 1.552E+Ol 1.552E+Ol 10.42 OK C0-58 810.76 99.45* 1.793E+OO 3.603E-02 6.633E-01 128.52 OK CD-109 88.03 3.70* 4.577E+OO 2.402E-01 3.758E-01 612.50 OK SN-126 64.28 9.60 2.075E+OO 1.451E+OO 1.451E+OO 103.12 OK 86.94 8.90 4.577E+OO 9.988E-02 9.988E-02 612.50 OK 87.57 37.00* 4.577E+OO 2.402E-02 2.402E-02 612.50 OK BA-137M 661. 66 89.90* 2.104E+OO 2.484E-01 2.531E-01 39.80 OK CS-137 661. 66 85.10* 2.104E+OO 2.624E-01 2.674E-01 39.80 OK TL-208 277.37 6.60 4.277E+OO Line Not Found Absent 583.19 85.00* 2.325E+OO 3.684E-01 3.684E-01 25.69 OK 860.56 12.50 1.712E+OO 4.765E-01 4.765E-01 90. 96 OK PB-212 74.82 10.28 3.461E+00 l.229E+OO 1.229E+OO 73.91 OK 77 .11 17.10 3.693E+OO 1.813E+OO 1. 813E+OO 26.24 OK 238.63 43.60* 4.786E+OO 1.046E+OO l.046E+00 13 .16 OK 300.09 3.30 4. OllE+OO 1.017E+OO 1. 017E+00 111.80 OK BI-214 609.32 45.49* 2.246E+00 8.454E-01 8.457E-01 22.62 OK 1120.29 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 OK 1764.49 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 OK PB-214 74.82 5.80 3.423E+OO Line Not Found <<INT Reject 77 .11 9.70 3.693E+OO 3 .196E+OO 3.197E+OO 26.24 OK 87.09 3.41 4.545E+OO Line Not Found <<INT Reject 242.00 7.25 4.745E+OO Line Not Found <<INT Reject 295.22 18.42 4.064E+00 l.258E+OO l.258E+00 25.48 OK 351. 93 35.60* 3. 521E+OO l.122E+00 1.122E+OO 18.06 OK RN-222 609.32 45.49* 2.246E+OO 8.454E-01 8.457E-01 22.62 OK 1120.29 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 OK 1764.49 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 OK RA-224 240.99 4.10* 4.743E+OO 4.991E-01 4.991E-01 300.41 OK RA-226 609.32 45.49* 2.246E+OO 8.454E-01 8.457E-01 22.62 OK 1120.29 14.92 l.392E+OO 8.904E-01 8.907E-01 50.87 OK 1764.49 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 OK AC-228 105.21 1.10 5.586E+00 Line Not Found Absent 338.32 11.27 3.639E+00 1.535E+OO l.535E+00 32.99 OK 794.95 4.25 1.823E+OO Line Not Found Absent 835.71 1. 61 1. 753E+OO Line Not Found Absent 911.20 25.80* 1.638E+OO 1. 226E+00 l.226E+00 22.98 OK 968. 97 15.80 l.561E+00 l.130E+OO 1.130E+OO 61. 71 OK RA-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.639E+OO 1.535E+OO 1.535E+OO 32.99 OK 794*_95 4.25 1.823E+OO Line Not Found Absent 835.71 1. 61 1. 753E+00 Line Not Found Absent 911.20 25.80* 1.638E+OO l.226E+00 1.226E+OO 22.98 OK 968. 97 15.80 1. 561E+OO l.130E+OO 1.130E+OO 61.71 OK TH-228 74.82 10.28 3.461E+OO l.229E+OO 1.229E+OO 73.91 OK 77 .11 17.10 3.693E+OO 1. 813E+OO l.813E+00 26.24 OK 238.63 43.60* 4.786E+OO 1.046E+OO 1.046E+OO 13.16 OK 300.09 3.30 4. OllE+OO 1.017E+OO 1.017E+OO 111. 80 OK TH-230 609.32 45.49* 2.246E+00 8.454E-01 8.455E-01 22.62 OK 1120. 29 14.92 1.392E+OO 8.904E-01 8.904E-01 50.87 OK Page 3038 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235007 Acquisition date Page : 3 3-0CT-2016 08:02:54 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1764.49 15.30 9. 459E-01. 7.405E-01 7.405E-01 44.75 OK PA-231 283.69 1. 70 4.201E+OO Line Not Found Absent 301.36 5.35* 4. OllE+OO 6.271E-01 6. 271E-01 111.80 OK TH-232 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11.27 3.639E+OO l.535E+OO 1.535E+OO 32.99 OK 835. 71 1. 61 1. 753E+OO Line Not Found Absent 911.20 25.80* 1.638E+OO 1. 22 6E+OO 1.226E+OO 22.98 OK 968.97 15.80 1.561E+OO 1.130E+OO 1.130E+OO 61. 71 OK TH-234 63.29 3.70* 2.075E+OO 3.764E+OO 3.764E+OO 103.12 OK 92.59 4.23 4.971E+OO 1.370E+OO 1.370E+OO 103.36 OK U-234 609.32 45.49* 2.246E+OO 8.454E-01 8.454E-01 22.62 OK 1120.29 14.92 1.392E+OO 8.904E-01 8.904E-01 50.87 OK 1764.49 15.30 9.459E-01 7.405E-01 7.405E-01 44.75 OK U-238 63.29 3.70* 2.075E+OO 3.764E+OO 3.764E+OO 103.12 OK 92.59 4.23 4. 971E+OO 1.370E+OO 1.370E+OO 103.36 OK AM-243 43.53 5.90 1. 701E-01 Line Not Found Absent 74.66 67.20* 3.461E+OO l.880E-01 1.880E-01 73.91 OK ANH-511 511. 00 100.00* 2.588E+OO 9.466E-02 9.466E-02 83.19 OK Flag: "*" = Keyline Page 3039 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:06:29.83 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l * *Acquisition date 3-0CT-2016 08:02:54 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:55:00 Analyst initials: MXRl *
  • Sample ID G405235007 Sample Quantity 1.5252E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff. File . : DKA100: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1.96-sigma) K-40 1.552E+Ol 1.585E+OO C0-58 6.633E-01 8.354E-01 CD-109 3.758E-01 2.256E+OO SN-126 2.402E-02 1.442E-01 BA-137M 2. 531E-01 9. 871E-02 CS-137 2.674E-01 1.043E-01 TL-208 3.684E-01 9.275E-02 PB-212 1.046E+OO 1.349E-01 BI-214 8.457E-01 1. 875E-01 PB-214 1.122E+OO 1. 98 6E-01 RN-222 8.457E-01 1.875E-01 RA-224 4.991E-01 1.470E+OO RA-226 8.457E-01 l.875E-01 AC-228 1.226E+OO 2.762E-01 RA-228 1.226E+00 2.762E-01 TH-228 1. 046E+OO 1. 349E-01 TH-230 8.455E-01 1.874E-01 PA-231 6.271E-01 6. 871E-01 TH-232 1.226E+OO 2.762E-01 TH-234 3.764E+OO 3.804E+00 U-234 8.454E-01 l.874E-01 U-238 3.764E+OO 3.804E+OO AM-243 1. 880E-01 l.362E-01 ANH-511 9.466E-02 7. 717E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3040 of 5809 Key-Line Activity (pCi/GRAM 2.468E+OO -l.801E-02 O.OOOE+OO 2.599E-02 -7.774E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) l.180E+Ol 4.318E-02 1.523E+41 3.510E-02 4.446E-01 l.266E+04 MDA (pCi/GRAM 5.415E-01 8.694E-01 2.825E+OO l.669E-01 7.217E-02 7.624E-02 5.456E-02 l.025E-01 l.254E-01 l.280E-01 1.254E-01 1.098E+OO 1.254E-01 2.634E-01 2.634E-01 1.025E-01 1.254E-01 8.744E-01 2.634E-01 3.193E+OO 1.254E-01 3.193E+OO 1.165E-01 4.992E-02 MDA (pCi/GRAM 2.337E+Ol 8.088E-02 O.OOOE+OO 8.479E-02 8.057E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 4.162E+02 0.000E+OO SHORT HLIF MN-54 8.976E-03 6.462E-02 1. 236E-01 NOT IDENT. C0-56 -1.060E-02 4.543E-01 8.620E-01 FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 3.147E-02 5.427E-02 l.030E-01 NOT IDENT. FE-59 -3.185E+OO 5.999E+OO 1. llOE+Ol NOT IDENT. C0-60 6.774E-02 4.386E-02 8.395E-02 FAIL ABUN ZN-65 -3.150E-02 2.052E-01 3.480E-01 NOT IDENT. GE-68 1.743E+OO 2.387E+OO 5.269E+OO NOT IDENT. AS-73 -3.993E-01 1.505E+Ol 2.858E+Ol NO'C IDENT. AS-74 0.000E+OO 5.810E+03 O.OOOE+OO SHORT HLIF SE-75 -3.559E-02 2.054E-01 3.949E-01 NOT IDENT. BR-77 0.000E+OO 1.326E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.736E+02 O.OOOE+OO SHORT HLIF RB-83 -5.887E-01 6.134E-01 l.020E+OO NOT IDENT. KR-85 5. 211E+00 8.053E+OO l.500E+Ol NOT IDENT. SR-85 5.350E-01 8.321E-01 1.550E+OO NOT IDENT. RB-86 O.OOOE+OO 2.647E+04 O.OOOE+OO SHORT HLIF Y-88 1.131E-01 1.280E-01 4.065E-01 NOT IDENT. Y-91 -l.149E+Ol 5.321E+02 1.050E+03 NOT IDENT. NB-94 8.328E-03 3.326E-02 6.198E-02 NOT IDENT. NB-95 4.546E-01 9.760E-01 l.920E+OO NOT IDENT. NB-95M 8.656E-01 2.662E+OO 4.785E+OO NOT IDENT. ZR-95 8. 962E-02 1. 322E+OO 2. 572E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.305E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO l.158E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 5.080E-03 3.847E-02 6.507E-02 NOT IDENT. RH-102 3.756E-02 5.752E-02 1.208E-01 NOT IDENT. RU-103 -3.909E+OO 5.lOOE+OO 8.823E+OO FAIL ABUN RH-106 -7.579E-02 4.995E-01 9.362E-01 FAIL ABUN RU-106 -7.579E-02 4.995E-01 9.362E-01 FAIL ABUN AG-108M 1. 727E-02 2.729E-02 5.656E-02 NOT IDENT. AG-llOM -8.523E-02 l.004E-01 1.593E-01 FAIL ABUN SN-113 -2.925E-02 2.040E-01 3.917E-01 NOT IDENT. CD-115 O.OOOE+OO 1.825E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.374E+04 0.000E+OO SHORT HLIF TE-123M 4.718E-03 1.414E-01 2.795E-01 NOT IDENT. SB-124 -1.878E+OO 1.637E+OO 1.776E+OO NOT IDENT. SB-125 -l.082E-02 9.934E-02 1. 901E-01 NOT IDENT. TE-125M 6.273E+Ol 3.059E+02 5.674E+02 NOT IDENT. I-126 O.OOOE+OO 9.549E+05 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO l.086E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.598E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.096E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.430E+26 O.OOOE+OO SHORT HLIF BA-133 2.323E-02 4.307E-02 8.057E-02 NOT IDENT. I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 5.025E-02 6.329E-02 1.281E-01 NOT IDENT. CS-135 -6.215E-02 1.478E-01 2.463E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.422E+05 O.OOOE+OO SHORT HLIF CE-139 2.333E-02 l.015E-01 2.050E-01 NOT IDENT. BA-140 O.OOOE+OO 1.297E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.761E+05 O.OOOE+OO SHORT HLIF CE-141 1.00lE+Ol 2.238E+Ol 4.585E+Ol NOT IDENT. CE-143 0.000E+OO 1. 576E+41 O.OOOE+OO SHORT HLIF CE-144 6.062E-02 4.104E-01 7.478E-01 NOT IDENT. PM-144 -2.192E-02 5.275E-02 9.415E-02 NOT IDENT. PR-144 -1.887E+OO 4.579E+OO 8.179E+OO NOT IDENT. PM-146 1. 579E-03 4 .119E-02 8.030E-02 NOT IDENT. ND-147 O.OOOE+OO 3.634E+07 O.OOOE+OO SHORT HLIF PM-147 2.177E+02 9.659E+02 1. 781E+03 NOT IDENT. PM-149 0.000E+OO 2.3.48E+40 O.OOOE+OO SHORT HLIF EU-150 2.461E-02 2.784E-02 5.355E-02 FAIL ABUN EU-152 -1.533E-02 9.628E-02 1.832E-01 NOT IDENT. GD-153 5.333E-02 2.075E-01 3.610E-01 NOT IDENT. EU-154 -7.429E-03 9.930E-02 2.006E-01 FAIL ABUN EU-155 9.166E-02 1. 201E-01 2.338E-01 FAIL ABUN TB-160 -9.629E-01 2.004E+OO 3.461E+OO FAIL ABUN H0-166M O.OOOE+OO 8.884E-02 1.223E-01 FAIL ABUN TM-171 -1. 4 73E+Ol 4.019E+Ol 7. 396E+Ol NOT IDENT. HF-172 3.379E-03 2.709E-01 4.519E-01 FAIL ABUN LU-172 7.175E-02 7.846E-02 1. 765E-01 FAIL ABUN LU-176 -l.076E-02 2.381E-02 4.436E-02 FAIL ABUN HF-181 1. 271E+OO 3.789E+OO 7. 711E+OO NOT IDENT. Page 3041of5809 TA-182 3.677E-01 9.252E-01 1. 780E+OO FAIL ABUN RE-183 -l.069E-02 4.879E+OO 9.182E+OO NOT IDENT. RE-184 l.417E+Ol 2.767E+Ol 5.768E+Ol NOT IDENT. W-188 -4.823E+Ol l.084E+02 1. 923E+02 FAIL ABUN IR-192 3. 096E-01 4.344E-01 9.031E-01 FAIL ABUN HG-203 2.435E+OO 2.341E+OO 4.928E+OO NOT IDENT. BI-207 -4.060E-02 4.397E-02 7.559E-02 FAIL ABUN PB-210 -6. 291E-01 8.393E+OO l.595E+Ol NOT IDENT. BI-211 O.OOOE+OO 5.470E-01 7.906E-01 FAIL ABUN PB-211 -2. 468E-:-02 6.710E-01 1.289E+00 NOT IDENT. BI-212 O.OOOE+OO 9.448E-Ol l.374E+OO FAIL ABUN RN-219 -3.656E-02 3.732E-01 7.139E-01 FAIL ABUN RA-223 -3.302E-01 5.544E-01 1.015E+OO FAIL ABUN AC-227 -7.881E-02 2.487E-01 4.705E-01 FAIL ABUN TH-227 -7.881E-02 2.487E-01 4.705E-01 FAIL ABUN TH-229 4.338E-02 4.603E-01 9.108E-01 FAIL ABUN TH-231 -3.302E-01 5.544E-01 l.015E+OO FAIL ABUN PA-233 -6.032E-03 5. 711E-02 l.102E-01 FAIL ABUN PA-234 -9.698E-02 2.745E-01 5.269E-01 FAIL ABUN PA-234M 1.616E+OO 3.597E+OO 7.521E+OO NOT IDENT. U-235 -2.144E-02 1. 797E-01 3.545E-01 FAIL ABUN NP-237 -6.032E-03 5. 711E-02 1.102E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 l.792E-02 2.553E-01 4.693E-01 NOT IDENT. PU-239 4.826E+02 6.058E+02 6.983E+02 FAIL ABUN AM-241 -l.091E-01 2.368E-01 3.916E-01 NOT IDENT. CM-243 -1.018E-01 l.076E-01 1. 803E-01 NOT IDENT. BK-247 l.296E-02 7.448E-02' 1.413E-01 NOT IDENT. CM-247 -2.391E-03 3.386E-02 6.502E-02 NOT IDENT. CF-249 l.156E-02 3.690E-02 7.375E-02 NOT IDENT. CF-251 -3.520E-02 1. 088E-01 2.104E-01 NOT IDENT. Page 3042 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:06:27.42 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 376 10.66* l .119E+OO 1.552E+Ol l.552E+Ol 10.42 C0-58 810.76 13 99.45* 1. 793E+OO 3.603E-02 6.633E-01 128.52 CD-109 88.03 48 3.70* 4.577E+OO 1.399E+OO 2.189E+OO 103.01 SN-126 64.28 59 9.60 2.075E+OO 1. 451E+OO l.451E+OO 103.12 86. 94 48 8.90 4.577E+OO 5.818E-01 5.818E-01 103.01 87.57 48 37.00* 4.577E+OO 1.399E-01 1.400E-01 103.01 BA-137M 661.66 95 89.90* 2.104E+OO 2.484E-01 2. 531E-01 39.80 CS-137 661.66 95 85.10* 2.104E+OO 2.624E-01 2.674E-01 39.80 TL-208 277.37 ------6.60 4.277E+OO ------Line Not Found ------583.19 148 85.00* 2.325E+OO 3.684E-01 3.684E-01 25.69 860.56 21 12.50 1.712E+OO 4.765E-01 4.765E-01 90. 96 BI-211 72.87 ------1. 23 3.214E+00 ------Line Not Found ------351. 06 286 12.92* 3. 521E+OO 3.091E+OO 3.091E+00 18.06 PB-212 74.82 140 10.28 3.461E+OO 1.938E+OO 1.938E+OO 45.91 77 .11 233 17.10 3.693E+OO 1. 813E+OO 1.813E+OO 26.24 238.63 443 43.60* 4.786E+OO l.046E+OO 1. 046E+OO 13.16 300.09 27 3.30 4.0llE+OO 1. 017E+OO 1. 017E+00 111. 80 BI-214 609.32 175 45.49* 2.246E+OO 8.454E-01 8.457E-01 22. 62 1120.29 38 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 PB-214 74.82 140 5.80 3.461E+OO 3.436E+OO 3.437E+OO 45.91 77 .11 233 9.70 3.693E+OO 3 .196E+OO 3.197E+OO 26. 24 87.09 48 3.41 4.577E+OO l.519E+OO 1.519E+OO 103.01 242.00 108 7.25 4.743E+OO 1.540E+OO l.541E+00 50.98 295.22 191 18.42 4.064E+OO l.258E+OO 1.258E+OO 25.48 351. 93 286 35.60* 3. 521E+OO l.122E+OO 1.122E+OO 18.06 RN-222 609.32 175 45.49* 2.246E+OO 8.454E-01 8.457E-01 22. 62 1120.29 38 14.92 l.392E+OO 8.904E-01 8.907E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 RA-224 240.99 108 4.10* 4.743E+OO 2.723E+OO 2.723E+OO 50.98 RA-226 609.32 175 45.49* 2.246E+OO 8.454E-01 8.457E-01 22. 62 1120.29 38 14.92 1.392E+OO 8.904E-01 8.907E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.408E-01 44.75 AC-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 128 11. 27 3.639E+OO l.535E+OO 1.535E+OO 32.99 794.95 ------4.25 1.823E+OO ------Line Not Found ------835. 71 ------1. 61 1. 753E+OO ------Line Not Found ------911. 20 105 25.80* 1.638E+OO 1. 22 6E+OO 1.226E+00 22.98 968.97 57 15.80 1.561E+OO l .130E+OO 1.130E+00 61. 71 RA-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 128 11. 27 3.639E+OO l.535E+OO 1.535E+OO 32.99 794.95 ------4.25 1.823E+OO ------Line Not Found ------835.71 ------1. 61 1.753E+OO ------Line Not Found ------911. 20 105 25.80* 1.638E+OO 1. 22 6E+OO 1. 22 6E+00 22.98 968.97 57 15.80 1.561E+OO l.130E+OO 1.130E+OO 61. 71 TH-228 74.82 140 10.28 3.461E+OO 1.938E+OO 1.938E+OO 45.91 77 .11 233 17.10 3.693E+OO l.813E+OO 1.813E+OO 26. 24 Page 3043 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235007 Acquisition date 3-0CT-2016 08:02:54 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 443 43.60* 4.786E+OO 1.046E+OO 1.046E+OO 13.16 300.09 27 3.30 4. OllE+OO 1.017E+OO 1.017E+OO 111.80 TH-230 609.32 175 45.49* 2.246E+OO 8.454E-01 8.455E-01 22.62 1120.29 38 14.92 1. 392E+OO 8.904E-01 8.904E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.405E-01 44.75 PA-231 283.69 ------1. 70 4. 201E+OO ------Line Not Found ------301.36 27 5.35* 4. OllE+OO 6.271E-01 6. 271E-01 111.80 TH-232 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 128 11. 27 3.639E+OO 1. 535E+OO l.535E+OO 32.99 835.71 ------1. 61 1. 753E+OO ------Line Not Found ------911. 20 105 25.80* 1.638E+OO 1.226E+OO 1.226E+OO 22.98 968. 97 57 15.80 1.561E+OO 1.130E+OO l .130E+OO 61. 71 TH-234 63.29 59 3.70* 2.075E+OO 3.764E+OO 3.764E+OO 103.12 92.59 59 4.23 4.971E+OO 1.370E+OO 1.370E+OO 103.36 U-234 609.32 175 45.49* 2.246E+OO 8.454E-01 8.454E-01 22.62 1120.29 38 14.92 1.392E+OO 8.904E-01 8.904E-01 50.87 1764.49 22 15.30 9.459E-01 7.405E-01 7.405E-01 44.75 U-238 63.29 59 3.70* 2.075E+OO 3.764E+OO 3.764E+OO 103.12 92.59 *59 4.23 . 4.971E+OO 1.370E+OO 1. 37 OE+'OO 103.36 AM-243 43.53 ------5.90 1. 701E-01 ------Line Not Found ------74.66 140 67.20* 3.461E+OO 2. 965E-01 2. 965E-01 45.91 ANH-511 511. 00 50 100.00* 2.588E+OO 9.466E-02 9.466E-02 83.19 Flag: "*" Key line Page 3044 of 5809 Summary of Nuclide Activity Sample ID : G405235007 Acquisition date Page : 3 3-0CT-2016 08:02:54 Total number of lines in spectrum 47 Number of unidentified lines 9 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 70.86D 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y l.41E+10Y 1600.00Y 1600.00Y 1600. OOY l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 18.4 1. 56 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.552E+Ol 3.603E-02 1.399E+OO l.399E-01 2.484E-01 2.624E-01 3.684E-01 3.091E+OO 1.046E+OO 8.454E-01 1.122E+OO 8.454E-01 2.723E+OO 8.454E-01 1.226E+OO 1.226E+OO 1.046E+OO 8.454E-01 6.271E-01 1.226E+OO 3.764E+OO 8.454E-01 3.764E+OO 2. 965E-01 9.466E-02 4.345E+Ol 4.345E+Ol Decay Corr pCi/GRAM 1.552E+Ol 6.633E-01 2.189E+OO l.400E-01 2. 531E-01 2.674E-01 3.684E-01 3.091E+OO 1.046E+OO 8.457E-01 1.122E+OO 8.457E-01 2. 723E+OO 8.457E-01 l.226E+OO 1.226E+OO 1.046E+OO 8.455E-01 6. 271E-01 1.226E+OO 3.764E+OO 8.454E-01 3.764E+OO 2. 965E-01 9.466E-02 4.488E+Ol 4.488E+Ol 80.85% Decay Corr 2-Sigma Error 0.162E+Ol 8.525E-01 2.255E+OO l.442E-01 1.007E-01 l.064E-01 0.946E-01 0.558E+OO 0.138E+OO l.913E-01 0.203E+OO 1. 913E-01 1.388E+OO 1.913E-01 0.282E+OO 0.282E+OO 0.138E+OO 1.912E-01 7. OllE-01 0.282E+OO 3.882E+OO 1.912E-01 3.882E+OO l.362E-01 7.874E-02 "M" Manually accepted 2-Sigma %Error 10.42 128.52 103.01 103.01 39.80 39.80 25.69 18.06 13.16 22.62 18.06 22.62 50.98 22.62 22.98 22.98 13.16 22.62 111.80 22.98 103.12 22.62 103.12 45.91 83.19 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3045 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235007 Acquisition date : 3-0CT-2016 08:02:54 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 94.77 40 106 1. 26 190.76 184 10 8.77E-03 **** 5.07E+OO T 0 129.53 38 145 1. 78 260.27 256 8 8.50E-03 **** 6.09E+OO T 0 186.37 165 201 1.23 373. 96 368 13 3.85E-02 43.l 5.60E+OO T 0 209.43 84 90 1.25 420.08 416 8 1. 97E-02 48.7 5.24E+OO T 0 270.47 52 71 1. 08 542.17 537 10 l.27E-02 71. 2 4.36E+OO T 0 464.99 16 55 0. 67 931. 20 925 11 3.97E-03 **** 2.80E+OO 0 534.57 25 39 3.98 1070.37 1064 13 6.57E-03 **** 2.50E+OO 7 707.28 12 9 1. 96 1415.81 1413 25 3.12E-03 96.3 2.00E+OO T 7 710. 32 28 16 2.00 1421. 88 1413 25 7.41E-03 71.1 1.99E+OO T 0 720.76 14 7 3.40 1442.77 1438 10 3.86E-03 90.8 1. 97E+OO T 0 728 .15 37 29 0.95 1457.55 1450 12 9.78E-03 69.5 1.95E+OO T 0 797.49 23 27 1. 86 1596.23 1586 14 6.26E-03 **** 1. 82E+OO 0 803.54 19 12 0.66 1608. 33 1604 11 5.25E-03 89.5 1. 81E+OO 0 816.56 10 15 1. 70 1634.38 1630 8 2.62E-03 **** 1. 79E+OO T 0 996.21 12 13 1.17 1993.69 1989 12 3.43E-03 **** 1. 53E+OO T 0 1049.83 19 6 3.87 2100.93 2093 14 5.20E-03 75.2 1. 4 7E+OO T 0 1190. 02 9 7 0.61 2381. 31 2378 6 2.57E-03 **** 1.33E+OO T 0 1227.61 16 11 3.52 2456.49 2449 15 4.58E-03 **** l.29E+00 0 1234.03 27 5 2.60 2469.34 2464 10 7.53E-03 49.2 1.29E+OO T 0 1239.00 22 5 1. 24 2479.29 2475 11 6.25E-03 58.4 1.28E+OO T 0 1245.45 17 3 3.62 2492.19 2486 11 4.79E-03 60.9 1.28E+OO 0 1250.95 17 15 3.83 2503.18 2497 14 '4.77E-03 **** 1.27E+OO 0 1333.81 15 3 4.00 2668.91 2663 11 4. 25E-03 66.1 1.21E+OO T 0 1337.86 6 0 1. 50 2677.00 2 674 6 l.67E-03 81. 6 l.21E+OO 0 1544.74 .9 2 0.52 3090.77 3086 8 2.58E-03 83.5 1.07E+OO Flags: "T" = Tentatively associated Page 3046 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:06:43.93 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l * *Acquisition date 3-0CT-2016 08:02:54 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:55:00 Nuclide Library : SOLID *
  • Sample ID G405235007 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.5252E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.145E-01 3.645E-01 1.347E+OO 7.925E-02 3.241E-02 3.424E-02 2.382E-02 4.791E-02 5.602E-02 5.848E:-02 5.602E-02 5.134E-01 5.602E-02 1.157E-01 l.157E-01 4.791E-02 5.600E-02 4.048E-01 1.157E-01 1.504E+OO 5.600E-02 1.504E+OO 5. 511E-02 2.231E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3047 of 5809 Le (pCi/GRAM 1.052E+Ol 3.377E-02 O.OOOE+OO 3.517E-02 3.552E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 .TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 3048 of 5809 5.427E-02 3.743E-01 O.OOOE+OO 4.857E-02 4.676E+OO 3.579E-02 1.518E-01 2.322E+OO 1.334E+Ol O.OOOE+OO 1.825E-01 O.OOOE+OO O.OOOE+OO 4.445E-Ol 6.854E+OO 7.079E-01 O.OOOE+OO 1.522E-01 4.580E+02 2.759E-02 8.686E-01 2.246E+OO 1.120E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.050E-02 5.390E-02 3.863E+OO 4 .138E-01 4 .138E-01 2. 571E-02 6.691E-02 1.760E-01 O.OOOE+OO 0.000E+OO 1.318E-01 4.471E-01 8.557E-02 2.670E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.691E-02 O.OOOE+OO 5.834E-02 l.132E-01 O.OOOE+OO O.OOOE+OO 9.582E-02 O.OOOE+OO O.OOOE+OO 2.155E+Ol O.OOOE+OO 3.523E-01 4.108E-02 3.569E+OO 3.604E-02 O.OOOE+OO 8.393E+02 O.OOOE+OO 2.478E-02 8.402E-02 1.694E-01 8.393E-02 1.lOlE-01 1.498E+OO 5.479E-02 3.458E+Ol 2.120E-01 7.807E-02 2.030E-02 3.445E+OO 7.733E-01 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3049 of 5809 4.320E+OO 2.517E+Ol 8.804E+Ol 4.158E-01 2.296E+OO 3.144E-02 7.468E+OO 3.802E-01 5.862E-01 6.347E-01 3.238E-01 4.613E-01 2.191E-01 2.191E-01 4.264E-01 4.613E-01 5.045E-02 2.280E-01 3.232E+OO l.667E-01 5.045E-02 O.OOOE+OO 2.195E-01 3.307E+02 l.837E-01 8.386E-02 6.539E-02 2.947E-02 3.364E-02 9.812E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IbENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:06:49.63 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235007.CNF;l *
  • Acquisition date 3-0CT-2016 08:02:54 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
  • Sample date 10-DEC-2015 13:55:00 Nuclide Library : SOLID *
  • Sample ID G405235007 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.5252E+02 GRAM *
  • Quantity Err(%) : 1.3113E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date* 23-AUG-2016 07: 56: 33 Eff. Geometry : *cAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1. 96-sigma) (1.96-sigma) K-40 1.552E+Ol 1. 780E+OO 1. 780E+OO C0-58 6.633E-01 8.359E-01 8.359E-01 CD-109 3.758E-01 2.267E+OO 2.267E+OO SN-126 2.402E-02 1.449E-01 1. 449E-01 BA-137M 2.531E-01 9. 931E-02 9. 931E-02 CS-137 2.674E-01 1.049E-01 1. 049E-01 TL-208 3.684E-01 9.407E-02 9.407E-02 PB-212 l.046E+00 l.459E-01 l.459E-01 BI-214 8.457E-01 1.909E-01 l.909E-01 PB-214 1.122E+OO 2. 041E-01 2. 041E-01 RN-222 8.457E-01 1.909E-01 1.909E-01 RA-224 4.991E-01 l.477E+00 1.477E+OO RA-226 8.457E-01 1.909E-01 l.909E-01 AC-228 1.226E+OO 2.832E-01 2.832E-01 RA-228 1.226E+OO 2.832E-01 .2.832E-01 TH-228 1.046E+OO 1.459E-01 l.459E-01 TH-230 8.455E-01 l.909E-01 1.909E-01 PA-231 6.271E-01 7.000E-01 7.000E-01 TH-232 1.226E+OO 2.832E-01 2.832E-01 TH-234 3.764E+00 3.895E+00 3.895E+OO U-234 8.454E-01 1.909E-01 l.909E-01 U-238 3.764E+OO 3.895E+00 3.895E+OO AM-243 1. 880E-01 1.373E-01 l.373E-01 ANH-511 9.466E-02 7. 726E-02 7.726E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ') ( 1. 96-sigma) ( 1. 96-sigma) BE-7 2.468E+OO 1.180E+Ol l.185E+Ol NOT IDENT. NA-22 -1. 801E-02 4.319E-02 4.395E-02 NOT IDENT. NA-24 l.000E+41 1.583E+41 O.OOOE+OO SHORT HLIF AL-26 2.599E-02 3.513E-02 3.704E-02 NOT IDENT. SC-46 -7.774E-02 4.446E-01 4.460E-01 FAIL ABUN V-48 7.600E+03 l.266E+04 1.312E+04 SHORT HLIF Page 3050 of 5809 CR-51 6.530E+Ol 4.162E+02 4.173E+02 SHORT HLIF MN-54 8.976E-03 6.462E-02 6.475E-02 NOT IDENT. C0-56 -1.060E-02 4.543E-01 4.543E-01 FAIL ABUN MN-56 -l.000E+41 4.285E+42 O.OOOE+OO SHORT HLIF C0-57 3.147E-02 5.429E-02 5.612E-02 NOT IDENT. FE-59 -3.185E+OO 6.003E+00 6.173E+OO NOT IDENT. C0-60 6.774E-02 4.393E-02 5.350E-02 FAIL ABUN ZN-65 -3.150E-02 2.052E-01 2.057E-01 NOT IDENT. GE-68 1. 743E+OO 2.388E+OO 2.514E+OO NOT IDENT. AS-73 -3.993E-01 l.505E+Ol 1.505E+Ol NOT IDENT. AS-74 2.245E+03 5.813E+03 5.901E+03 SHORT HLIF SE-75 -3.559E-02 2.054E-01 2.060E-01 NOT IDENT. BR-77 1.028E+38 8.832E+38 O.OOOE+OO SHORT HLIF SR-82 -2.144E+02 6.737E+02 6.806E+02 SHORT HLIF RB-83 -5.887E-01 6.187E-01 6.732E-01 NOT IDENT. KR-85 5. 211E+OO 8.056E+OO 8. 391E+OO NOT IDENT. SR-85 5.350E-01 8.324E-01 8.667E-01 NOT IDENT. RB-86 l.804E+04 2.648E+04 2.770E+04 SHORT HLIF Y-88 1.131E-01 l.282E-01 1.380E-01 NOT IDENT. Y-91 -l.149E+Ol 5.321E+02 5.322E+02 NOT IDENT. NB-94 8.328E-03 3.326E-02 3.347E-02 NOT IDENT. NB-95 4.546E-01 9.762E-01 9.975E-01 NOT IDENT. NB-95M 8.656E-01 2.663E+OO 2.691E+OO NOT IDENT. ZR-95 8. 962E-02 1.322E+OO 1.323E+OO NOT IDENT. NB-97 -l.000E+41 2.015E+41 0.000E+OO SHORT HLIF ZR-97 -1.000E+41 l.306E+41 O.OOOE+OO SHORT HLIF M0-99 -6. 792E+31 1.159E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.054E+42 O.OOOE+OO SHORT HLIF RH-101 5.080E-03 3.848E-02 3.854E-02 NOT IDENT. RH-102 3.756E-02 5.760E-02 6.004E-02 NOT IDENT. RU-103 -3.909E+OO 5.104E+OO 5.399E+OO FAIL ABUN RH-106 -7.579E-02 4.995E-01 5.007E-01 FAIL ABUN RU-106 -7.579E-02 4.995E-01 5.007E-01 FAIL ABUN AG-108M 1.727E-02 2.730E-02 2.839E-02 NOT IDENT. AG-llOM -8.523E-02 1.005E-01 1.076E-01 FAIL ABUN SN-113 -2.925E-02 2.040E-01 2.044E-;-01 NOT IDENT. CD-115 7.006E+38 1.830E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 4.147E+04 9.386E+04-9. 571E+04 SHORT HLIF TE-123M 4.718E-03 l.414E-01 l.414E-01 NOT IDENT. SB-124 -1.878E+OO l.640E+OO 1.846E+OO NOT IDENT. SB-125 -1.082E-02 9.934E-02 9.946E-02 NOT IDENT. TE-125M 6.273E+Ol 3.059E+02 3.072E+02 NOT IDENT. I-126 4.551E+05 9.569E+05 9.787E+05 SHORT HLIF SB-126 1.220E+06 1.110E+06 l.239E+06 SHORT HLIF SB-127 4.058E+21 1.691E+22 O.OOOE+OO SHORT HLIF I-131 -3.554E+09 4.099E+09 4.401E+09 SHORT HLIF I-132 -l.000E+41 1.865E+42 O.OOOE+OO SHORT HLIF TE-132 -3.447E+24 2.430E+26 O.OOOE+OO SHORT HLIF BA-133 2.323E-02 4.308E-02 4.434E-02 NOT IDENT. I-133 1.000E+41 7.821E+41 O.OOOE+OO SHORT HLIF CS-134 5.025E-02 6.332E-02 6.725E-02 NOT IDENT. CS-135 -6.215E-02 1. 478E-01 l.505E-01 NOT IDENT. I-135 l.000E+41 8.076E+41 O.OOOE+OO SHORT HLIF CS-136 -9. 321E+04 2.425E+05 2.461E+05 SHORT HLIF CE-139 2.333E-02 l.016E-01 l.022E-01 NOT IDENT. BA-140 1.476E+05 1.297E+06 1.299E+06 SHORT HLIF LA-140 4.078E+04 3.761E+05 3.766E+05 SHORT HLIF CE-141 1.00lE+Ol 2.238E+Ol 2.283E+Ol NOT IDENT. CE-143 1.000E+41 l.579E+41 O.OOOE+OO SHORT HLIF CE-144 6.062E-02 4.105E-01 4 .114E-01 NOT IDENT. PM-144 -2.192E-02 5.277E-02 5.368E-02 NOT IDENT. PR-144 -1. 887E+OO 4.580E+OO 4.658E+OO NOT IDENT. PM-146 1. 579E-03 4 .119E-02 4.120E-02 NOT IDENT. ND-147 -7.968E+06 3.635E+07 3.652E+07 SHORT HLIF PM-147 2.177E+02 9.659E+02 9.709E+02 NOT IDENT. PM-149 l.655E+40 2. 375E+"40 O.OOOE+OO SHORT HLIF EU-150 2.461E-02 2.786E-02 2.999E-02 FAIL ABUN EU-152 -l.533E-02 9.629E-02 9.653E-02 NOT IDENT. GD-153 5.333E-02 2.075E_.:_01 2.089E-01 NOT IDENT. EU-154 -7.429E-03 9.930E-02 9.936E-02 FAIL ABUN EU-155 9.166E-02 l.203E-01 1.272E-01 FAIL ABUN TB-160 -9.629E-01 2.005E+OO 2.052E+OO FAIL ABUN H0-166M 1.275E-01 8. 911E-02 1.060E-01 FAIL ABUN TM-171 -l.473E+Ol 4. 021E+Ol 4.076E+Ol NOT IDENT. HF-172 3.379E-03 2.709E-01 2.709E-01 FAIL ABUN LU-172 7.175E-02 7.880E-02 8.518E-02 FAIL ABUN LU-176 -1.076E-02 2.382E-02 2. 431E-02 FAIL ABUN HF-181 1. 271E+OO 3.789E+OO 3.832E+OO NOT IDENT. Page 3051 of 5809 TA-182 3.677E-01 9.253E-01 9.400E-01 FAIL ABUN RE-183 -l.069E-02 4.879E+OO 4.879E+OO NOT IDENT. RE-184 1.417E+Ol 2.788E+Ol 2.860E+Ol NOT IDENT. W-188 -4.823E+Ol l.085Et02 1.106E+02 FAIL ABUN IR-192 3.096E-01 4.346E-01 4.564E-01 FAIL ABUN HG-203 2.435E+OO 2.344E+OO 2.588E+OO NOT IDENT. BI-207 -4.060E-02 4.399E-02 4.765E-02 FAIL ABUN PB-210 -6. 291E-01 8.393E+OO 8.398E+OO NOT IDENT. BI-211 3.091E+OO 5.643E-01 1.503E+OO FAIL ABUN PB-211 -2.468E-02 6.710E-01 6. 711E-01 NOT IDENT. BI-212 1.387E+OO 9.474E-01 1.135E+OO FAIL ABUN RN-219 -3.656E-02 3.732E-01 3.736E-01 FAIL ABUN RA-223 -3.302E-01 5.548E-01 5.744E-01 FAIL ABUN AC-227 -7.881E-02 2.489E-01 2.514E-01 FAIL ABUN TH-227 -7.881E-02 2.489E-01 2.514E-01 FAIL ABUN TH-229 4.338E-02 4.603E-01 4.607E-01 FAIL ABUN TH-231 -3.302E-01 5.548E-01 5.744E-01 FAIL ABUN PA-233 -6.032E-03 5. 711E-02 5.718E-02 FAIL ABUN PA-234 -9.698E-02 2. 961E-01 2.993E-01 FAIL ABUN PA-234M l.616E+OO 3.598E+OO 3. 671E+OO NOT IDENT. U-235 -2.144E-02 1. 797E-01 1.799E-01 FAIL ABUN NP-237 -6.032E-03 5. 711E-02 5.718E-02 FAIL ABUN NP-238 -1.000E+41 1. 995E+41 O.OOOE+OO SHORT HLIF NP-239 l.792E-02 2.553E-01 2.554E-01 NOT IDENT. PU-239 4.826E+02 6. 061E+02 6.440E+02 FAIL ABUN AM-241 -1.091E-01 2.370E-01 2.420E-01 NOT IDENT. CM-243 -1.018E-01 1. 080E-01 1.173E-01 NOT IDENT. BK-247 l.296E-02 7.453E-02 7.476E-02 NOT IDENT. CM-247 -2.391E-03 3.386E-02 3.388E-02 NOT IDENT. CF-249 1.156E-02 3.691E-02 3.728E-02 NOT IDENT. CF-251 -3.520E-02 1. 089E-01 1.lOlE-01 NOT IDENT. Page 3052 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 60.1854 87.09 115.6747 136.47 95.9819 45.60 71. 5991 87.57 117.7241 140.51 0.0000 46.54 68.3569 88.03 141.1892 143.76 85.6973 49. 72 0.0000 88.34 141. 2417 144.24 82.3725 51. 35 66.6640 88.47 146.0260 145.44 71.5216 51. 87 72.3762 89. 96 135.9516 152.43 83.8122 52.39 78.0977 1093.63 109.8045 153.25 0.0000 52.97 71. 3746 91.11 0.0000 323.87 84.7890 53.44 66.8942 92.59 105.2728 156.02 0.0000 54.07 82.8521 93.35 105.3661 158.56 0.0000 57.36 0.0000 94.56 105.5151 159.00 91.0932 57.53 73.0383 94.65 105.5259 162.33 83.6625 57.98 84.5096 94.67 105.5286 162.66 0.0000 59.27 76.2866 94.87 105.5527 163.33 79.4602 59.32 99.1800 97.43 70.5753 165.86 63.3574 59.54 90.0554 98.43 75.8743 176.31 60.4368 60. 96 68.8346 98.44 75.8752 176.60 0.0000 61.17 68.8564 99.53 73.5568 177.52 70.8641 62.93 88.5981 100 .11 74.8113 181.07 0.0000 63.29 88.6451 102.03 83.4357 181.52 66.3173 63.58 88.6830 103.18 85. 9630 184.41 82.1030 64.28 102.9933 103.37 82.3479 143.76 69.5744 66.73 87.9318 105.21 67.9522 193.51 69.9821 67.24 83.3648 105.31 67.9599 197.03 72.7947 125.81 99.6370 106.12 72.8778 198.01 55.2935 67.75 99.6468 106.47 88.7014 201.83 75.6892 69.67 97.5925 109.28 79.2183 203.43 49.3429 70.83 85.3366 111. 00 90.3512 205.31 55.5851 72.81 99.5703 111. 76 0.0000 210.85 65.1035 72.87 101.1340 114. 06 77.1663 215.65 79.9850 74.66 102.9377 116. 30 0.0000 222 .11 62.4862 74.82 102.9598 116.74 68.7806 227.09 55.5303 74.97 102.9807 119. 76 85.0066 227.38 52.8536 77 .11 103.2727 121.12 82.6551 228.16 0.0000 78.74 106.6284 121.22 82.6633 228.18 60.0522 79.69 108.3291 121. 78 69.1301 116.74 60.0522 80.12 111.5305 122.06 75.3234 235.69 70.2582 80.19 0.0000 122.92 74.1513 235.96 70.2701 80.57 73.8726 123.07 74.1623 238.63 68.5874 81. 00 86.4936 265.00 89.0480 238.98 0.0000 81. 07 86.5015 125.81 76.0139 240.99 68.6918 81.75 97.9888 127.23 71.1540 242.00 68.7358 83.79 106.5255 127.91 81.1361 244.70 62.5130 84.00 113.6565 129.30 83.3165 252.40 0.0000 85.43 104.3704 131.20 94.6799 252.80 58.2786 86.55 131.4335 133.02 93.1784 254.15 0.0000 86. 79 131. 4724 133. 52 84.8983 256.23 68.4406 86.94 115. 6539 136. 00 90.9342 260.90 0.0000 Page 3053 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 53.2009 355.39 0.0000 584.27 15.8948 264.80 48.4355 356.01 30.3689 595.83 0.0000 265.00 48.4408 364.49 0.0000 427.87 24.5105 268.22 52.3950 366.42 0.0000 602.52 0.0000 269.46 43.2354 372.51 28.1846 604. 72 24. 0115 270.03 43.2497 375.05 32 .1111 607.14 30.4401 271.23 43.2803 377.52 37.9939 609.32 23.5155 273.65 0.0000 356.01 32.2454 610.33 23.5236 276.40 46.1843 388.16 31.3314 614.28 22.4843 277.37 55.4529 388.63 0.0000 618.01 13.9363 277.60 54.5359 391.69 28.4407 62 0. 3 6 26.8219 278.00 49.0006 264. fr6 24.6195 621. 93 21. 4689 279.20 41.6336 401. 81 33.4999 630.19 0.0000 279.54 58.2986 402.40 32.5233 631.29 15.0755 279.70 58.3037 404.85 34.5329 633.25 16.1627 280.46 50.9224 410.95 31.6602 634.78 0.0000 283.69 38.0321 413.71 31. 6992 635.95 20.4913 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 42. 7123 423.72 0.0000 645.85 16.2299 285.90 0.0000 427.09 30.8909 657.76 19.5520 287.50 53.9183 427.87 28.9080 657.90 0.0000 290.67 48.0559 433.94 23.9868 661.66 26.1016 293.27 0.0000 439.40 31.0561 664.57 0.0000 351.93 44.8184 453.88 25.1994 666.33 0.0000 295.96 44.8369 463.37 26.3110 666.50 0.0000 879.38 36.4832 468.07 34.9808 667.71 0.0000 299.98 36.5117 473.00 0.0000 677.62 18.5834 300.09 44.9404 475.06 23.3870 685.70 0.0000 300.13 44.9414 476.78 27.4735 695.00 0.0000 301.36 51.9985 477.60 24.4292 696.49 20.8926 302.85 36.5696 482.18 19.3753 696. 51 20.8926 256.23 36.6030 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18.6982 306.78 46.9859 497.08 26. 6713 697.49 20.8995 308.46 31.9795 505.52 32.4203 702.65 17.1869 311. 90 41.4631 507.63 0.0000 706.68 21. 5098 316.51 33.0639 511.00 23. 7225 711. 68 9.9430 319.41 0.0000 514.00 26.3311 720.70 0.0000 320.08 0.0000 514.00 26.3311 721. 93 0.0000 321.04 36.9315 520.40 27.9492 722.78 13.3022 323.87 43.6257 520.69 0.0000 722.91 13.3027 325.23 48.4019 522.65 0.0000 723.31 13.3042 328.76 0.0000 527.90 0.0000 724.19 13.3076 333.37 35.7414 528.26 19.9344 727. 33 10.6563 333.97 34.3220 529.59 21.8135 733.00 12.0085 334.37 35.7597 529.87 0.0000 735.93 13.3545 338.28 39.1757 531. 02 0.0000 333.97 15.5876 338.32 39.1766 537.26 0.0000 739.50 0.0000 311. 90 31. 5673 546.56 0.0000 747.24 18.9825 340.48 31.5673 552.55 31.4294 748.06 13.4028 340.55 0.0000 563.25 18. 9309 . 752.31 22.3657 344.28 44.0880 569.33 20.0267 753.82 0.0000 345.93 39.1374 946.00 20.0275 756. 73 14.5568 351.06 37.5067 569.70 20.0290 756.80 14.5573 351. 93 37.5234 583.19 15.8887 884.68 28.0528 Page 3054 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 23.5771 1274.44 8.9459 1620.50 1. 012 0 ) 766.42 31. 4419 1001.03 5.7320 1621.92 1.0123 766.84 35.9375 1002.74 16.7253 1678.03 0.0000 772. 60 0.0000 1004.73 12.5499 1690.97 6.1425 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025 .. 87 0.0000 1764.49 4. 9714. 778.90 9.0156 1028.54 0.0000 1063.66 7.2563 783.70 0.0000 1037.84 7.2271 1771.35 5.1840 785.37 11. 2903 1038.76 0.0000 1791.20 0.0000 792.07 11.8774 631.29 i0.1384 1808.65 3.1282 794.95 22.6424 1048.07 0.0000 1810.72 0.0000 795.86 22.6481 1049.04 12.6807 1836.06 0.0000 810.06 9.0954 1050.41 12.6849 810.29 9. 0960 1063.66 13.6322 344.28 9*. 0964 1077.00 0.0000 810.76 9.0970 1077.34 10.9395 815.77 0.0000 1085.87 6.3937 1048.07 0.0000 1093.63 10.0648 832.01 16.0132 1099.45 14.6582 834.85 14.8810 1112. 07 13.7805 835.71 18.3197 1112.84 11. 9455 836.80 0.0000 1115. 54 17.6531 846.75 0.0000 1120.29 14.7256 846.77 14.9292 1120.55 14.7266 856.80 0.0000 1221.41 13.2565 860.56 10.3740 1129.67 15.6781 871.09 11. 5588 1131. 51 0.0000 873.19 10.4088 1147.95 0.0000 875.33 0.0000 1173.23 15.8254 879.38 19.6929 1177.95 12 .1145 880.51 15.0635 1189.05 12.1423 883.24 13.9150 1204.77 15.9313 884.68 18.5599 1221. 41 10.5314 889.28 20.9055 1231.02 7.5376 894.76 15 .1196 1235.36 0.0000 898.04 17.4609 1238.28 0.0000 900.72 17.4725 1260.41 0.0000 903.28 10.4905 1271.87 12.3502 911.20 17.5195 1274.44 9.5050 912.08 17.5238 1274.54 12.3565 923.98 0.0000 1291.59 9.5374 926.50 7.9146 1298.22 929 .11 15.8395 1312 .11 0.0000 937.49 25.5732 1332.49 12.3055 944 .13 0.0000 1"362. 66 0.0000 946.00 17.6740 1365.19 5.8041 949.00 9.7281 1368.63 0.0000 667.71 0.0000 1384.29 6.7958 962. 31 21. 2944 1408.01 7.8008 964. 08 14.2026 1457.56 0.0000 966. 17 17.0520 1460.82 4.9228 911.20 15.1085 1489.16 3.9583 .968.97 15.1085 1505.03 3. 9692 983.53 0.0000 1584.12 4.0237 ,,., ' 984.45 0.0000 1596.21 0.0000 Page 3055 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:07:22.76 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM39.CNF;l34 Background date : Z-OCT-2016 11:02:13. Sample date 10-DEC-2015 14:05:00 Acquisition date : 3-0CT-2016 08:03:23. Sample ID G405235008 Sample quantity 1.47889E+02 GRAM Detector name GAM39 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:07.23 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 2 0 0 0 0 0 0 0 3 3 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3056 of 5809 Energy 46.75* 63.19* 72. 81 74.90* 77.17* 87.21 92.82* 129.55 153.90* 185.18* 209.61 217.41 238.66* 241. 62 270.81* 295.22* 299.64* 338.10* 352.09* 375. 96 411. 7 6 454.53 464. 96 511.52* 534.00 552.45 562. 62 583.26* 595.97 609.56* 663.04 669.35 693.49 808.79 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 50 1 32 222 272 56 74 49 21 91 31 35 392 77 25 111 24 78 210 9 61 39 74 12 14 21 13 72 9 130 52 14 33 37 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 157 252 141 172 159 169 176 107 107 175 101 79 74 95 64 60 62 89 62 32 34 16 57 82 13 21 34 51 28 49 24 6 24 4 1. 60 1.10 1. 27 1.17 1. 08 1.17 1. 48 0.95 0.61 1. 55 0.98 0.74 1.20 1. 83 1. 90 1. 56 1. 57 1.12 1. 44 1. 27 6.89 6.16 9.36 1. 73 1. 46 1. 27 1. 79 1. 59 1. 27 1. 22 2 .17 1. 24 6.10 4.03 93.34 126.23 145.47 149.65 154.17 174.26 185.47 258.94 307.64 370.20 419.06 434.67 477.17 483.09 541.47 590.28 599.12 676.04 704.03 751. 77 823.38 908.93 929. 79 1022.92 1067.88 1104.78 1125 .13 1166.40 1191. 82 1219.01 1325.97 1338.59 1386.88 1617.50 89 123 143 143 143 171 183 256 305 364 413 430 472 472 536 586 586 669 698 748 816 902 917 1016 1065 1099 1118 1160 1185 1214 1319 1335 1378 1610 8 1.39E-02 47.5 8 3.42E-04***** 16 8.84E-03 64.2 8.87E-01 16 6.17E-02 12.1 16 7.56E-02 9.8 7 1. 55E-02 40. 8 8 2.05E-02 35.8 8 1.36E-02 39.1 8 5.81E-03 89.8 15 2.53E-02 34.0 10 8.56E-03 64.0 9 9.66E-03 49.5 17 1.09E-01 6.4 l.84E+OO 17 2.15E-02 33.2 9 6.87E-03 62.7 21 3.09E-02 16.1 7.31E-01 21 6.57E-03 65.0 14 2.15E-02 28.4 12 5.84E-02 10.5 8 2.42E-03115.6 17 1.69E-02 25.4 15 1.09E-02 26.8 28 2.06E-02 30.9 17 3.24E-03201.7 6 3.80E-03 50.2 11 5.72E-03 49.2 10 3.61E-03 89.4 12 2.00E-02 23.8 10 2.54E-03112.4 10 3.61E-02 13.3 17 1.45E-02 25.9 8 3.97E-03 39.6 20 9.lOE-03 41.2 16 1. 03E-02 20. 5 Peak Search Report (continued) Page : 2 Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 860.71 30 14 2.16 1721.35 1715 11 8.40E-03 29.9 36 0 870. 96 14 12 1.14 1741. 86 173"6 10 3. 96E-03 53.1 37 0 881.92 27 23 8.82 1763.78 1749 23 7.50E-03 50.0 38 0 911. 61
  • 55 26 1.16 1823.17 1816 13 l.52E-02 24.4 39 1 964. 7 0 22 17 2.03 1929.37 1919 26 6.05E-03 42.6 9.26E-01 40 1 969.17* 51 14 2.03 1938.30 1919 26 1. 42E-02 22.5 41 0 1033.58 14 2 1.12 2067.13 2063 8 3.91E-03 31. 7 42 0 1120.49 23 25 1. 73 2241. 00 2236 8 6.31E-03 39.4 43 0 1160.33 18 3 1. 58 2320.67 2315 10 5.lOE-03 28.4 44 0 1175.83 28 9 0.75 2351.69 2343 17 7.64E-03 30.9 45 0 1228.04 9 7 0.90 2456.12 2453 8 2.39E-03 61. 6 46 0 1384.20 7 5 1. 35 2768.50 2763 10 1.94E-03 70.7 47 0 1460.83* 284 4 1. 75 2921.78 2914 16 7.89E-02 6.3 48 0 1509.87 9 2 0.93 3019.90 3014 10 2.39E-03 48.3 49 0 1587.75 13 0 1. 53 3175.69 3170 11 3. 61E-03 27.7 50 /0 1764.45 18 0 2.02 3529.17 3524 10 5.00E-03 23.6 51 0 1887.13 4 3 1. 36 3774.60 3767 10 l.23E-03 82.2 Flag: "*" = Peak area was modified by background subtraction Page 3057 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:07:26 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 10-DEC-2015 14:05:00 G405235008 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:03:23 147.89 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA39 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3058 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351. 06 CAN 0 01:00:07.23 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 8.984E-01 1.449E.+Ol 1.449E+Ol 12.51 OK CD-109 88.03 3.70* 6.754E+OO 5.138E-01 8.037E-01 232.54 OK SN-126 64.28 9.60 6.932E+00 l.205E-02 1.205E-024690.27 OK 86.94 8.90 6.754E+00 2.136E-01 2.136E-01 232.54 OK 87.57 37.00* 6.754E+OO 5.138E-02 5.138E-02 232.54 OK BA-137M 661.66 89.90* 1.755E+OO 1. 757E-01 1.790E-01 51. 88 OK CS-137 661.66 85.10* 1. 755E+OO 1.856E-01 l.891E-01 51. 88 OK TL-208 277.37 6.60 3.709E+OO Line Not Found Absent 583.19 85.00* 1.953E+00 2.325E-01 2.325E-01 47.52 OK 860.56 12.50 1. 416E+OO 8.818E-01 8.818E-01 59.82 OK PB-210 46.54 4.25* 6.842E+OO 1.145E+OO 1.174E+OO 94.92 OK BI-211 72. 87 1. 23 6.824E+OO 2.436E+OO 2.436E+OO 128.32 OK 351. 06 12.92* 3.013E+OO 3.292E-01 3.292E-01 327.48 OK PB-212 74.82 10.28 6. 811E+OO l.481E+OO 1. 481E+OO 35.42 OK 77 .11 17.10 6.799E+00 1.497E+OO 1.497E+OO 19.65 OK 238.63 43.60* 4.211E+OO 1.242E+OO l.242E+OO 12.83 OK 300.09 3.30 3.469E+OO 1.178E+OO l.178E+OO 130.01 OK BI-214 609.32 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26. 57 OK 1120.29 14.92 1.136E+00 6.735E-01 6.737E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 OK PB-214 74.82 5.80 6.812E+OO Line Not Found <<INT Reject 77 .11 9.70 6.799E+00 2.640E+OO 2.641E+OO 19.65 OK 87.09 3.41 6.755E+OO Line Not Found <<INT Reject 242.00 7.25 4.163E+OO Line Not Found <<INT Reject 295.22 18.42 3.514E+OO 9.817E-01 9.821E-01 32.23 OK 351. 93 35.60* 3.014E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26.57 OK 1120.29 14.92 1.136E+OO 6.735E-01 6.737E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 OK RA-224 240.99 4.10* 4.168E+OO 8. 981E-01 8.981E-01 204.49 OK RA-226 609.32 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26.57 OK 1120.29 14.92 1.136E+OO 6.735E-01 6.737E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 OK AC-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11.27 3.122E+OO 1.243E+OO 1.243E+OO 56.75 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835. 71 1. 61 1. 451E+OO Line Not Found Absent 911. 20 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 OK 968.97 15.80 l.284E+OO 1.288E+OO 1.288E+OO 44.91 OK RA-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3.122E+OO 1.243E+OO 1.243E+OO 56.75 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835. 71 1. 61 1. 451E+OO Line Not Found Absent 911. 20 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 OK 968. 97 15.80 1.284E+OO 1.288E+OO 1.288E+OO 44.91 OK TH-228 74.82 10.28 6. 811E+OO l.481E+OO 1. 481E+OO 35.42 OK 77 .11 17.10 6.799E+OO 1.497E+OO 1.497E+OO 19.65 OK 238.63 43.60* 4.211E+OO 1.242E+OO 1.242E+OO 12.83 OK 300.09 3.30 3.469E+OO 1.178E+OO 1.178E+OO 130.01 OK Page 3059 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH--:230 609.32 45.49* 1.882E+OO 8. lOOE-0.1 8.lOOE-01 26.57 OK 1120.29 14. 92 1.136E+OO 6.735E-01 6.735E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.533E-01 47.14 OK TH-232 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3.122E+OO l.243E+OO 1.243E+OO 56.75 OK 835.71 1. 61 1.451E+OO Line Not Found Absent 911.20 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 OK 968. 97 15.80 l.284E+OO l.288E+OO 1.288E+OO 44.91 OK TH-234 63.29 3.70* 6.932E+OO 3.126E-02 3.126E-024690.27 OK 92.59 4.23 6.722E+00 1.635E+OO l.635E+00 71.63 OK U-234 609.32 45.49* 1.882E+OO 8.lOOE-01 8.lOOE-01 26. 57 OK 1120. 29 14.92 l.136E+OO 6.735E-01 6.735E-01 78.75 OK 1764.49 15.30 7.485E-01 7.533E-01 7.533E-01 47.14 OK U-238 63.29 3.70* 6.932E+OO 3.126E-02 3.126E-024690.27 OK 92.59 4.23 6. 722E+00 1.635E+OO 1.635E+OO 71. 63 OK PU-239 129.30 0.01* 6.237E+OO 7.647E+02 7.647E+02 78.19 OK 375.05 0.00 2.845E+OO l.099E+03 1.099E+03 231.16 OK 413.71 0.00 2.617E+OO Line Not Found Absent AM-243 43.53 5:90 6.236E+OO Line Not Found -----Absent 74.66 67.20* 6. 811E+OO 2.266E-01 2.266E-01 35.42 OK ANH-511 511. 00 100.00* 2 .181E+OO 2.903E-02 2.903E-02 403.36 OK Flag: "*" = Keyline Page 3060 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:07:28.43 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l *
  • Acquisition date 3-0CT-2016 08:03:23 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:07.23 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:05:00 Analyst initials: MXRl *
  • Sample ID G405235008 Sample Quantity 1.4789E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.449E+Ol 1.777E+OO CD-109 8.037E-01 1.832E+OO SN-126 5.138E-02 1.171E-01 BA-137M 1.790E-01 9.lOlE-02 CS-137 1.891E-01 9.614E-02 TL-208 2.325E-01 l.083E-01 PB-210 1.174E+OO 1.092E+OO BI-211 3.292E-01 l.057E+OO PB-212 1.242E+OO 1.561E-01 BI-214 8.103E-01 2. llOE-01 PB-214 1.102E+OO 2.257E-01 RN-222 8.103E-01 2. llOE-01 RA-224 8.981E-01 1. 800E+OO RA-226 8.103E-01 2.llOE-01 AC-228 8.054E-01 3.855E-01 RA-228 8.054E-01 3.855E-01 TH-228 1. 242E+OO 1.561E-01 TH-230 8.lOOE-01 2.109E-01 TH-232 8.054E-01 3.855E-01 TH-234 3.126E-02 1.437E+OO U-234 8.lOOE-01 2.109E-01 U-238 3.126E-02 1.437E+OO PU-239 7.647E+02 5.860E+02 AM-243 2.266E-01 7.864E-02 ANH-511 2.903E-02 1.147E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3061 of 5809 Key-Line Activity (pCi/GRAM 3.700E+OO 1.582E-03 O.OOOE+OO 8.283E-03 1.544E-01 K.L. Cnt Uncert ( 1. 96-sigma) l.362E+Ol 5.716E-02 1. 960E+41 3.889E-02 4.379E-01 MDA (pCi/GRAM 8 .112E-01 2.195E+OO 1.308E-01 7.925E-02 8.372E-02 8.491E-02 9.860E-01 4.359E-01 1. lllE-01 1.622E-01 3.711E-01 1.622E-01 1.192E+OO 1.622E-01 3.191E-01 3.191E-01 1. lllE-01 1. 621E-01 3.191E-01 1.238E+OO l.621E-01 1.238E+OO 6.159E+02 6.463E-02 6.277E-02 MDA (pCi/GRAM 2.698E+Ol 1.145E-01 O.OOOE+OO 8.760E-02 9. lllE-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 0.000E+OO 1.467E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 5. 071E+02 O.OOOE+OO SHORT HLIF MN-54 -2.318E-02 7.886E-02 l.514E-01 NOT IDENT. C0-56 -2.644E-01 5.683E-01 1.066E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.366E-02 4.783E-02 8.895E-02 NOT IDENT. C0-58 6.019E-01 6.532E-01 1.490E+OO NOT IDENT. FE-59 2.132E-01 6.512E+OO l.349E+Ol NOT IDENT. C0-60 -3.340E-03 4.175E-02 8.481E-02 NOT IDENT. ZN-65 -7.592E-02 2.510E-01 4.065E-01 NOT IDENT. GE-68 1. 875E-01 3.101E+OO 6.185E+OO NOT IDENT. AS-73 1.305E-01 2.674E+00 5.00lE+OO NOT IDENT. AS-74 O.OOOE+OO 1.055E+04 0.000E+OO SHORT HLIF SE-75 2.219E-01 2.432E-01 5.059E-01 NOT IDENT. BR-77 O.OOOE+OO 1.531E+37 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 8.059E+02 O.OOOE+OO SHORT HLIF RB-83 4.312E-02 7.892E-01 l.517E+OO FAIL ABUN KR-85 4.428E+OO 8.639E+OO 1. 731E+Ol NOT IDENT. SR-85 4.578E-01 8. 931E-01 1.789E+OO NOT IDENT. RB-86 O.OOOE+OO 3.395E+04 O.OOOE+OO SHORT HLIF Y-88 -1. 521E-02 2.493E-01 5. 313E-01 NOT IDENT. Y-91 6.165E+Ol 6.898E+o2 l.360E+03 NOT IDENT. NB-94 7.994E-03 4.165E-02 7.975E-02 FAIL ABUN NB-95 -6.481E-01 1.134E+OO 1.916E+OO NOT IDENT. NB-95M 2.790E+OO 2.797E+OO 5.364E+OO NOT IDENT. ZR-95 1.184E+OO 1. 798E+OO 3.723E+OO NOT IDENT. NB-97 O.OOOE+OO l.657E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 439E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.315E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.661E-03 4.124E-02 6.760E-02 NOT IDENT. RH-102 3.605E-02 6.848E-02 1.413E-01 NOT IDENT. RU-103 2.292E+OO 6.649E+OO 1.327E+Ol FAIL ABUN RH-106 -7.648E-02 6.488E-01 l.203E+00 NOT IDENT. RU-106 -7.648E-02 6.488E-01 1.203E+OO NOT IDENT. AG-108M -1.319E-02 2.899E-02 5.281E-02 NOT IDENT. AG-llOM 3.183E-02 1.457E-01 2.676E-01 FAIL ABUN SN-113 -2.081E-02 2.744E-01 5.218E-01 NOT IDENT. CD-115 O.OOOE+OO 2.009E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.913E+04 O.OOOE+OO SHORT HLIF TE-123M 5.890E-03 1.393E-01 2.645E-01 NOT IDENT. SB-124 1.653E+OO 2.049E+OO 5.536E+00 NOT IDENT. SB-125 -5.299E-02 l.243E-01 2.259E-01 NOT IDENT. TE-125M -7.003E+Ol 2.762E+02 4.901E+02 NOT IDENT. I-126 O.OOOE+OO 6.358E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.277E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.434E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.927E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 4.267E+40 0.000E+OO SHORT HLIF TE-132 O.OOOE+OO 3.028E+26 O.OOOE+OO SHORT HLIF BA-133 -9.803E-03 5.528E-02 9.266E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3.874E-02 7.077E-02 1.476E-01 FAIL ABUN CS-135 -8.423E-02 1. 764E-01 2.891E-01 NOT IDENT. I-135 O.OOOE+OO 1. 552E+41 O.OOOE+OO SHORT HLIF CS-136 0.000E+OO 3.474E+05 O.OOOE+OO SHORT HLIF CE-139 -8.275E-02 1.131E-01 2 .114E-01 NOT IDENT. BA-140 O.OOOE+OO 1.509E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.638E+05 O.OOOE+OO SHORT HLIF CE-141 -1. 571E+Ol 2.454E+Ol 4.663E+Ol NOT IDENT. CE-143 O.OOOE+OO 9.757E+40 O.OOOE+OO SHORT HLIF CE-144 2.523E-01 4.242E-01 7.943E-01 NOT IDENT. PM-144 3.898E-03 6.171E-02-1.187E-01 NOT IDENT. PR-144 3.382E-01 5.354E+OO 1.030E+Ol NOT IDENT. PM-146 O.OOOE+OO 8.015E-02 l.067E-01 FAIL ABUN ND-147 O.OOOE+OO 3.842E+07 O.OOOE+OO SHORT HLIF PM-147 -4.548E+02 8. 518E+o2 l.466E+03 NOT IDENT. PM-149 O.OOOE+OO 2.847E+40 O.OOOE+OO SHORT HLIF . EU-150 -4.633E-03 2.973E-02 5.055E-02 FAIL ABUN EU-152 4.066E-03 l.131E-01 2.089E-01 FAIL ABUN GD-153 -2.382E-01 2.075E-01 3.089E-01 NOT IDENT. EU-154 6.934E-03 1.409E-01 2.832E-01 NOT IDENT. EU-155 3.278E-02 l.168E-01 2.159E-01 FAIL ABUN TB-160 4.738E-01 2.158E+OO 4.395E+OO FAIL ABUN H0-166M 4.661E-03 6.804E-02 1.301E-01 FAIL ABUN TM-171 -2.266E-01 5.845E+OO 1. 089E+Ol NOT IDENT. HF-172 1.805E-01 2.778E-01 4.889E-01 FAIL ABUN LU-172 -5.872E-02 8.580E-02 1.515E-01 FAIL ABUN Page 3062 of 5809 LU-176 -2.576E-02 2.683E-02 4. 501E-02 FAIL ABUN HF-181 1.594E+OO 4.821E+OO 9.668E+OO NOT IDENT. TA-182 1. 301E+OO l.153E+OO 2.620E+OO FAIL ABUN RE-183 -5.289E-01 1. 231E+OO 2.220E+OO NOT IDENT. RE-184 8.884E+OO 3.801E+Ol 7.801E+Ol NOT IDENT. W-188 -1.235E+02 l.460E+02 2.257E+02 , FAIL ABUN IR-192 -1. 293E-01 5.466E-01 1.029E+OO FAIL ABUN HG-203 7.372E-01 2.945E+OO 5.769E+OO FAIL ABUN BI-207 4.104E-02 6.548E-02 l.399E-01 FAIL ABUN PB-211 4.073E-01 7.909E-Ol l.548E+OO NOT IDENT. BI-212 -4.087E-02 6.376E-01 1.190E+OO NOT IDENT. RN-219 l.161E-01 4.444E-01 8.780E-01 FAIL ABUN RA-223 -l.003E-01 7. 311E-01 1.384E+OO FAIL ABUN AC-227 -l.829E-02 2.469E-01 4.781E-01 FAIL ABUN TH-227 -1.829E-02 2.469E-01 4.781E-01 FAIL ABUN TH-229 2.750E-02 4.927E-01 9.700E-01 FAIL ABUN PA-231 2.686E-01 5.359E-01 1. 072E+OO NOT IDENT. TH-231 -l.003E-01 7.311E-01 l.384E+OO FAIL ABUN PA-233 5.629E-04 6.771E-02 1. 311E-01 FAIL ABUN PA-234 -7.937E-02 3.624E-01 6.983E-01 FAIL ABUN PA-234M -l.304E+OO 5.456E+OO l.058E+Ol NOT IDENT. U-235 l.313E-02 l.897E-01 3.775E-01 FAIL ABUN NP-237 5.629E-04 6.771E-02 1. 311E-01 FAIL ABUN NP-238 O.OOOE+OO l.900E+41 O.OOOE+OO SHORT HLIF NP-239 -8.397E-02 2.566E-01 4.509E-01 NOT IDENT. AM-241 4.371E-02 7.067E-02 l.263E-01 NOT IDENT. CM-243 -4.231E-02 1. 013E-01 1. 776E-01 NOT IDENT. BK-247 9. 072E-02 8.940E-02 l.808E-01 NOT IDENT. CM-247 -3.040E-02 4.226E-02 7.421E-02 NOT IDENT. CF-249 7.471E-03 4.250E-02 8.354E-02 NOT IDENT. CF-251 1. 046E-02 l.315E-01 2.587E-01 NOT IDENT. Page 3063 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:07:24.23 Nuclide Line Activity Report Nuclide Type:. Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 273 10.66* 8.984E-01 l.449E+Ol 1.449E+Ol 12.51 CD-109 88.03 70 3.70* 6.754E+OO l.419E+OO 2.219E+OO 81. 68 SN-126 64.28 2 9.60 6.932E+OO l.205E-02 1.205E-02 4690.27 86. 94 70 8.90 6.754E+OO 5.898E-01 5.898E-01 81. 68 87.57 70 37.00* 6.754E+OO 1.419E-01 1.419E-01 81.68 BA-137M 661. 66 55 89.90* l.755E+OO 1. 757E-01 l.790E-01 51. 88 CS-137 661.66 55 85.10* 1. 755E+OO 1.856E-01 1.891E-01 51. 88 TL-208 277.37 ------6.60 3.709E+OO ------Line Not Found ------583.19 76 85.00* 1.953E+OO 2.325E-01 2.325E-01 47.52 860.56 31 12.50 1.416E+OO 8.818E-01 8.818E-01 59.82 PB-210 46.54 66 4.25* 6.842E+OO 1.145E+OO 1.174E+OO 94.92 BI-211 72.87 40 1. 23 6.824E+OO 2.436E+OO 2.436E+OO 128.32 351.06 233 12.92* 3.013E+OO 3.034E+OO 3.034E+OO 20.91 PB-212 74.82 281 10.28 6.811E+OO 2.035E+OO 2.035E+00 24.24 77 .11 343 17.10 6.799E+OO 1.497E+OO l.497E+OO 19.65 238.63 449 43."60* 4.211E+00 1.242E+OO 1.242E+OO 12.83 300.09 27 3.30 3.469E+OO 1.178E+OO l.178E+OO 130.01 BI-214 609.32 137 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26.57 1120.29 22 14.92 1.136E+OO 6.735E-01 6.737E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 PB-214 74.82 281 5.80 6.811E+OO 3.607E+00 3.608E+OO 24.24 77 .11 343 9.70 6.799E+OO 2.640E+OO 2.641E+00 19.65 87.09 70 3.41 6.754E+OO 1.539E+OO 1.540E+OO 81. 68 242.00 89 7.25 4.168E+00 l.490E+OO 1.490E+OO 66.41 295.22 125 18.42 3.514E+OO 9.817E-01 9.821E-01 32.23 351. 93 233 35.60* 3.013E+OO 1.lOlE+OO l.102E+OO 20.91 RN-222 609.32 137 45.49* l.882E+OO 8.lOOE-01 8.103E-01 26.57 1120.29 22 14.92 1.136E+OO 6.735E-01 6.737E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 RA-224 240.99 89 4.10* 4.168E+OO 2.634E+OO 2.634E+OO 66.41 RA-226 609.32 137 45.49* 1.882E+OO 8.lOOE-01 8.103E-01 26.57 1120.29 22 14.92 1.136E+OO 6.735E-01 6.737E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.536E-01 47.14 AC-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 86 11. 27 3.122E+OO 1.243E+OO l.243E+OO 56.75 794.95 ------4.25 1.512E+OO ------Line Not Found ------835.71 ------1. 61 1.451E+OO ------Line Not Found ------911.20 55 25.80* 1.350E+OO 8.054E-01 8.054E-01 48.84 968. 97 51 15.80 1.284E+OO 1. 28 8E+OO l.288E+00 44.91 RA-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 86 11. 27 3.122E+OO l.243E+OO l.243E+OO 56.75 794.95 ------4.25 l.512E+OO ------Line Not Found ------835.71 ------1. 61 1. 451E+OO ------Line Not Found ------911. 20 55 25.80* l.350E+OO 8.054E-01 8.054E-01 48.84 968. 97 51 15.80 l.284E+OO 1. 28 8E+OO 1.288E+OO 44.91 TH-228 74.82 281 10.28 6. 811E+OO 2.035E+OO 2.035E+OO 24.24 77 .11 343 17.10 6.799E+OO 1. 497E+OO l.497E+OO 19.65 Page 3064 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCilGRAM %Error 238.63 449 .43.60* 4. 211E+OO 1.242E+OO l.242E+OO 12.83 300.09 27 3.30 3.469E+OO 1.178E+OO 1.178E+OO 130.01 TH-230 609.32 137 45.49* l.882E+OO 8.lOOE-01 8.lOOE-01 26.57 1120.29 22 14.92 l.136E+OO 6.735E-01 6.735E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.533E-01 47.14 TH-232 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 86 11. 27 3.122E+OO l.243E+OO 1.243E+OO 56.75 835. 71 ------1. 61 1.451E+OO ------Line Not Found ------911.20 55 25.80* l.350E+OO 8.054E-01 8.054E-01 48.84 968. 97 51 15.80 1. 284E+OO 1.288E+OO 1.288E+OO 44.91 TH-234 63.29 2 3.70* 6.932E+OO 3.126E-02 3.126E-02 4690.27 92.59 92 4.23 6.722E+OO 1.635E+OO 1. 635E+OO 71. 63 U-234 609.32 137 45.49* l.882E+OO 8.lOOE-01 8.lOOE-01 26.57 1120.29 22 14.92 1.136E+OO 6.735E-01 6.735E-01 78.75 1764.49 17 15.30 7.485E-01 7.533E-01 7.533E-01 47.14 U-238 63.29 2 3.70* 6.932E+00 3.126E-02 3.126E-02 4690.27 92.59 92 4.23 6. 722E+OO 1.635E+OO 1.635E+OO 71.63 PU-239 129.30 59 0.01* 6.237E+OO 7.647E+02 7.647E+02 78.19 375.05 10 0.00 2.845E+OO 1.099E+03 1.099E+03 231.16 413. 71 ------0.00 2.617E+OO ------Line Not Found ------AM-243 43.53 ------5.90 6.236E+OO ------Line Not Found ------74.66 281 67.20* 6.811E+OO 3 .113E-01 3 .113E-01 24.24 ANH-511 511. 00 12 100.00* 2.181E+OO 2.903E-02 2.903E-02 403.36 Flag: "*" Key line Page 3065 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235008 Acquisition date 3-0CT-2016 08:03:23 Total number of lines in spectrum 51 Number of unidentified lines 12 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 PU-239 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY l.41E+10Y 1600.00Y l.41E+l0Y 1. 41E+10Y 1. 41E+l0Y 7.54E+04Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 24110. OOY 7370.00Y 1.00E+09Y Decay 1. 00 1. 56 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.449E+Ol 1.419E+OO l.419E-01 l.757E-01 1. 856E-01 2.325E-01 l.145E+00 3.034E+OO 1.242E+OO 8.lOOE-01 1.101E+OO 8.lOOE-01 2.634E+OO 8.lOOE-01 8.054E-01 8.054E-01 1.242E+OO 8.lOOE-01 8.054E-01 3.126E-02 8.lOOE-01 3.126E-02 7.647E+02 3.113E-01 2.903E-02 7.986E+02 7.986E+02 Decay Corr pCi/GRAM 1.449E+Ol 2.219E+OO 1.419E-01 1. 790E-01 1.891E-01 2.325E-01 1.174E+OO 3.034E+OO l.242E+00 8.103E-01 1.102E+OO 8.103E-01 2.634E+OO 8.103E-01 8.054E-01 8.054E-01 1.242E+OO 8.lOOE-01 8.054E-01 3.126E-02 8.lOOE-01 3.126E-02 7.647E+02 3 .113E-01 2.903E-02 7.995E+02 7.995E+02 76.47% Decay Corr 2-Sigma Error 0.181E+Ol 1.812E+OO l.159E-01 0.929E-01 0.981E-01 l.105E-01 l.114E+OO 0.634E+OO 0.159E+OO 2.153E-01 0.230E+OO 2.153E-01 1. 749E+00 2.153E-01 3.933E-01 3.933E-01 0.159E+00 2.153E-01 3.933E-01 146.6E-02 2.152E-01 146.6E-02 5.980E+02 0.755E-01 11. 71E-02 "M" Manually accepted 2-Sigma %Error 12.51 81. 68 81. 68 51. 88 51. 88 47.52 94.92 20.91 12.83 26.57 20.91 26.57 66.41 26.57 48.84 48.84 12.83 26.57 48.84 4690.27 26. 57 4690.27 78.19 24.24 403.36 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3066 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235008 Acquisition date : 3-0CT-2016 08:03:23 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 153.90 25 128 0.61 307.64 305 8 5.81E-03 **** 5.75E+OO T 0 185.18 107 205 1. 55 370.20 364 15 2.53E-02 67.9 5.12E+00 T 0 209.61 36 117 0.98 419.06 413 10 8.56E-03 **** 4.67E+OO T 0 217.41 40 92 0.74 434.67 430 9 9.66E-03 98.9. 4.54E+OO 0 270.81 28 73 1. 90 541. 47 536 9 6.87E-03 **** 3.79E+OO T 0 411. 7 6 67 37 6.89 823.38 816 17 1. 69E-02 50.7 2.63E+OO T 0 454.53 43 17 6.16 908.93 902 15 1. 09E-02 53.6 2.41E+OO T 0 464. 96 80 61 9.36 929.79 917 28 2.06E-02 61. 8 2.37E+OO 0 534.00 15 14 1. 46 1067.88 1065 6 3.80E-03 **** 2.lOE+OO 0 552.45 22 23 1. 27 1104.78 1099 11 5. 72E-03 98.3 2.04E+OO T 0 562.62 14 36 1. 79 1125 .13 1118 10 3.61E-03 **** 2.0lE+OO T 0 595.97 10 29 1. 27 1191. 82 1185 10 2.54E-03 **** 1.92E+OO T 0 669.35 15 6 1. 24 1338.59 1335 8 3.97E-03 79.1 1.74E+OO 0 693.49 34 25 6.16 1386.88 1378 20 9.lOE-03 82.3 1. 69E+OO 0 808.79 38 4 4.03 1617.50 1610 16 1. 03E-02 40.9 1.49E+OO T 0 870. 96 14 12 1.14 1741.86 1736 10 3. 96E-03 **** 1.40E+OO T 0 881. 92 27 23 8.82 1763.78 1749 23 7.50E-03 **** 1.39E+OO T 1 964.70 22 17 2.03 1929.37 1919 26 6.05E-03 85.2 1.29E+OO T 0 1033.58 14 2 1.12 2067.13 2063 8 3. 91E-03 63.5 1.22E+OO 0 1160.33 18 3 1. 58 2320.67 2315 10 5.lOE-03 56.9 1.lOE+OO 0 1175.83 27 8 0.75 2351.69 2343 17 7.64E-03 61. 8 1. 09E+OO 0 1228.04 8 7 0.90 2456.12 2453 8 2.39E-03 **** 1. 05E+OO 0 1384.20 7 5 1. 35 2768.50 2763 10 1.94E-03 **** 9.44E-01 T 0 1509.87 8 2 0.93 3019.90 3014 10 2.39E-03 96. 7 8. 71E-01 0 1587.75 12 0 1. 53 3175.69 3170 11 3.61E-03 55.5 8. 31E-01 0 1887.13 4 2 1. 36 3774.60 3767 10 1.23E-03 **** 6.98E-01 Flags: "T" = Tentatively associated Page 3067 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:07:55.80 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l * *Acquisition date 3-0CT-2016 08:03:23 Sensitivity 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:07.23 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:05:00 Nuclide Library : SOLID *
  • Sample ID G405235008 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4789E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 PU-239 AM-243 ANH-511 Le (pCi/GRAM 3.335E-01 1.052E+OO 6.250E-02 3.510E-02 3.708E-02 3.822E-02 4.668E-01 1.997E-01 5.165E-02 7.288E-02 1. 790E-01 7.288E-02 5.541E-01 7.288E-02 1. 396E-01 1. 396E-01 5.165E-02 7.286E-02 1.396E-01 5.902E-01 7.286E-02 5.902E-01 2.895E+02 3. 072E-02 2.815E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3068 of 5809 Le (pCi/GRAM 1.207E+Ol 4.879E-02 O.OOOE+OO 3.437E-02 3. 961E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3069 of 5809 O.OOOE+OO 6.639E-02 4.626E-01 O.OOOE+OO 4.162E-02 6.582E-01 5.643E+00 3.452E-02 1. 7 52E-01 2.699E+OO 2.368E+OO O.OOOE+OO 2.353E-01 0.000E+OO O.OOOE+OO 6.784E-01 7.863E+OO 8.129E-01 O.OOOE+OO l.989E-01 5.950E+02 3.568E-02 8.452E-01 2. 511E+OO 1.656E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.178E-02 6.266E-02 5. 969E+OO 5.350E-01 5.350E-01 2.328E-02 l.180E-01 2.370E-01 O.OOOE+OO 0.000E+OO 1.236E-01 2.197E+OO 1.015E-01 2.301E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.227E-02 0.000E+OO 6.667E-02 1.328E-01 O.OOOE+OO O.OOOE+OO 9.834E-02 O.OOOE+OO O.OOOE+OO 2.187E+Ol O.OOOE+OO 3.753E-01 5 .196E-02 4.509E+OO 4.837E-02 O.OOOE+OO 6.835E+02 O.OOOE+OO 2.289E-02 9.539E-02 l.456E-01 1. 208E-01 l.021E-01 1.908E+OO 5.722E-02 5.146E+00 2.307E-01 6.289E-02 2.026E-02 SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF .FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3070 of 5809 4.335E+OO 1.162E+OO 1.052E+OO 3.443E+Ol 1.032E+02 4. 718E-01 2.685E+OO 6 .196E-02 7.036E-01 5.302E-01 3.989E-01 6.370E-01 2.200E-01 2.200E-01 4.520E-01 4.976E-01 6.370E-01 6.002E-02 3.048E-01 4.627E+OO 1.777E-01 6.002E-02 O.OOOE+OO 2 .113E-01 6.022E-02 8.343E-02 3.343E-02 3.787E-02 l.214E-01 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. 'NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:08:01.36 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235008.CNF;l * *Acquisition date 3-0CT-2016 08:03:23 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:07.23 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:05:00 Nuclide Library : SOLID *
  • Sample ID G405235008 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.4789E+02 GRAM *
  • Quantity Err(%) : l.3524E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff.' Cal. date 27-JUL-2016 13: 04: 01 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.449E+Ol 1. 931E+OO 1. 931E+OO CD-109 8.037E-01 1. 841E+OO 1. 841E+OO SN-126 5.138E-02 1.177E-01 1.177E-01 BA-137M 1.790E-01 9.134E-02 9.134E-02 CS-137 1.891E-01 9.649E-02 9.649E-02 TL-208 2.325E-01 1.087E-01 1.087E-01 PB-210 1.174E+OO 1. 096E+OO 1. 096E+OO BI-211 3.292E-01 1.070E+OO 1.070E+OO PB-212 1. 242E+OO l.694E-01 l.694E-01 BI-214 8.103E-01 2.139E-01 2.139E-01 PB-214 1.102E+OO 2.303E-01 2.303E-01 RN-222 8.103E-01 2 .139E-01 2.139E-01 RA-224 8.981E-01 1.804E+OO 1.804E+OO RA-226 8.103E-01 2 .139E-01 2.139E-01 AC-228 8.054E-01 3.877E-01 3.877E-01 RA-228 8.054E-01 3.877E-01 3.877E-01 TH-228 1.242E+OO l.694E-01 l.694E-01 TH-230 8.lOOE-01 2.138E-01 2.138E-01 TH-232 8.054E-01 3.877E-01 3.877E-01 TH-234 3.126E-02 1.437E+OO l.437E+OO U-234 8.lOOE-01 2 .138E-01 2 .138E-01 U-238 3.126E-02 l.437E+OO l.437E+OO PU-239 7.647E+02 5.870E+02 5.870E+02 AM-243 2.266E-01 8.058E-02 8.058E-02 ANH-511 2.903E-02 l.148E-01 l.148E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1 . 96-sigma) ( 1. 96-sigma) BE-7 3.700E+OO 1.362E+Ol 1. 372E+Ol NOT IDENT. NA-22 1.582E-03 5.716E-02 5.717E-02 NOT IDENT. NA-24 l.OOOE+41 2.556E+43 O.OOOE+OO SHORT HLIF AL-26 8.283E-03 3.889E-02 3.907E-02 NOT IDENT. SC-46 1.544E-01 4.379E-01 4.434E-01 FAIL ABUN Page 3071 of 5809 V-48 1.063E+04 1.468E+04 1.544E+04 SHORT HLIF CR-51 -5.832E+Ol 5. 071E+02 5.078E+02 SHORT HLIF MN-54 -2.318E-02 7.886E-02 7.955E-02 NOT IDENT. C0-56 -2.644E-01 5.684E-01 5.808E-01 NOT IDENT. MN-56 -l.000E+41 2.187E+41 O.OOOE+OO SHORT HLIF C0-57 l.366E-02 4.783E-02 4.822E-02 NOT IDENT. C0-58 6.019E-01 6.537E-01 7.078E-01 NOT IDENT. FE-59 2.132E-01 6.512E+OO 6.513E+OO NOT IDENT. C0-60 -3.340E-03 4.175E-02 4.177E-02 NOT IDENT. ZN-65 -7.592E-02 2.SlOE-01 2.533E-01 NOT IDENT. GE-68 1. 875E-01 3.101E+OO 3.102E+OO NOT IDENT. AS-73 1.305E-01 2.674E+OO 2.675E+OO NOT IDENT. AS-74 4.791E+03 l.056E+04 1.078E+04 SHORT HLIF SE-75 2.219E-01 2.434E-01 2.631E-01 NOT IDENT. BR-77 l.218E+38 1.047E+39 O.OOOE+OO SHORT HLIF SR-82 1.689E+02 8.059E+02 8.095E+02 SHORT HLIF RB-83 4.312E-02 7.892E-01 7.894E-01 FAIL ABUN KR-85 4.428E+OO 8.641E+OO 8.869E+OO NOT IDENT. SR-85 4.578E-01 8.933E-01 9.168E-01 NOT IDENT. RB-86 1.566E+04 3.396E+04 3.468E+04 SHORT HLIF Y-88 -1. 521E-02 2.493E-01 2.494E-01 NOT IDENT. Y-91 6.165E+Ol 6.898E+02 6.903E+02 NOT IDENT. NB-94 7.994E-03 4.165E-02 4.180E-02 FAIL ABUN NB-95 -6. 481E-01 l .134E+00 1.171E+OO NOT IDENT. NB-95M 2.790E+OO 2.806E+OO 3.075E+OO NOT IDENT. ZR-95 1.184E+OO 1. 799E+OO 1.877E+OO NOT IDENT. NB-97 1.000E+41 1. 658E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1. 439E+41 O.OOOE+OO SHORT HLIF M0-99 -5.484E+31 1.315E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 4.182E+41 O.OOOE+OO SHORT HLIF RH-101 -2.661E-03 4.125E-02 4.126E-02 NOT IDENT. RH-102 3.605E-02 6.854E-02 7.044E-02 NOT IDENT. RU-103 2.292E+OO 6.650E+OO 6.730E+OO FAIL ABUN RH-106 -7.648E-02 6.489E-01 6.498E-01 NOT IDENT. RU-106 -7.648E-02 6.489E-01 6.498E-01 NOT IDENT. AG-108M -l.319E-02 2.900E-02 2. 960E-02 NOT IDENT. AG-110M 3.183E-02 l.457E-01 1.464E-01 FAIL ABUN SN-113 -2. 081E-02 2.744E-01 2.746E-01 NOT IDENT. CD-115 2.413E+38 2.010E+39 O.OOOE+OO SHORT HLIF SN-117M 2.909E+03 9.913E+04 9. 913E+04 SHORT HLIF TE-123M 5.890E-03 1.393E-01 1.394E-01 NOT IDENT. SB-124 1.653E+OO 2.051E+OO 2.182E+OO NOT IDENT. SB-125 -5.299E-02 1.243E-01 1. 2 66E-01 NOT IDENT. TE-125M -7.003E+Ol 2.762E+02 2.780E+02 NOT IDENT. I-126 1.392E+06 6.630E+05 9.130E+05 SHORT HLIF SB-126 -7.973E+05 l.286E+06 l.335E+06 SHORT HLIF SB-127 -3.168E+20 2.434E+22 O.OOOE+OO SHORT HLIF I-131 -2.939E+08 4.927E+09 4.929E+09 SHORT HLIF I-132 l.OOOE+41 1.836E+42 O.OOOE+OO SHORT HLIF TE-132 2.547E+25 3.029E+26 O.OOOE+OO SHORT HLIF BA-133 -9.803E-03 5.528E-02 5.546E-02 NOT IDENT. I-133 -l.OOOE+41 2.749E+41 O.OOOE+OO SHORT HLIF CS-134 3.874E-02 7.079E-02 7.292E-02 FAIL ABUN CS-135 -8.423E-02 l.764E-01 1.805E-01 NOT IDENT. I-135 -1.000E+41 6.905E+41 O.OOOE+OO SHORT HLIF CS-136 -1.289E+05 3.477E+05 3.525E+05 SHORT HLIF CE-139 -8.275E-02 l.143E-01 1.203E-01 NOT IDENT. BA-140 2.024E+05 1.509E+06 1.512E+06 SHORT HLIF LA-140 2.085E+05 4.639E+05 4.733E+05 SHORT HLIF CE-141 -1.571E+Ol 2.455E+Ol 2.555E+Ol NOT IDENT. CE-143 1.000E+41 9.810E+40 O.OOOE+OO SHORT HLIF CE-144 2.523E-01 4.245E-01 4.394E-01 NOT IDENT. PM-144 3.898E-03 6 .171E-02 6.173E-02 NOT IDENT. PR-144 3.382E-01 5.354E+OO 5.356E+OO NOT IDENT. PM-146 l.527E-01 8. 091E-02 l.062E-01 FAIL ABUN ND-i47 -l.039E+06 3.842E+07 :5.843E+07 SHORT HLIF PM-147 -4.548E+02 8. 521E+o2 8.764E+02 NOT IDENT. PM-149 -8.392E+39 2.853E+40 O.OOOE+OO SHORT HLIF EU-150 -4.633E-03 2.973E-02 2.981E-02 FAIL ABUN EU-152 4.066E-03 1.131E-01 l.132E-01 FAIL ABUN GD-153 -2.382E-01 2.080E-01 2.340E-01 NOT IDENT. EU-154 6.934E-03 l.409E-01 l.410E-01 NOT IDENT. EU-155 3.278E-02 l.169E-01 1.178E-01 FAIL ABUN TB-160 4.738E-01 2.159E+OO 2.169E+OO FAIL ABUN H0-166M 4.661E-03 6.804E-02 6.808E-02 FAIL ABUN TM-171 -2.266E-01 5.845E+OO 5.846E+OO NOT IDENT. HF-172 1.805E-01 2.793E-01 2.909E-01 FAIL ABUN LU-172 -5. 872E-02 8.601E-02 8.999E-02 FAIL ABUN Page 3072 of 5809 LU-176 -2.576E-02 2.686E-02 2.926E-02 FAIL ABUN HF-181 1. 594E+OO 4.822E+OO 4.875E+OO NOT IDENT. TA-182 1.301E+OO l.154E+OO 1. 294E+OO FAIL ABUN RE-183 -5.289E-01 l.234E+00 l.257E+OO NOT IDENT. RE-184 8.884E+OO 3.807E+01 3.828E+Ol NOT IDENT. W-188 -1.235E+02 l.467E+02 l.569E+02 FAIL ABUN IR-192 -1.293E-01 5.466E-01 5.497E-01 FAIL ABUN HG-203 7.372E-01 2.946E+OO 2. 964E+OO FAIL ABUN BI-207 4.104E-02 6.550E-02 6.806E-02 FAIL ABUN PB-211 .4. 073E-01 7.912E-01 8.122E-01 NOT IDENT. BI-212 -4.087E-02 6.376E-01 6.379E-01 NOT IDENT. RN-219 1.161E-01 4.446E-01 4.477E-01 FAIL ABUN RA-223 -1.003E-01 7. 311E-01 7.325E-01 FAIL ABUN AC-227 -1.829E-02 2.470E-01 2.471E-01 FAIL ABUN TH-227 -l.829E-02 2.470E-01 2.471E-Ol* FAIL ABUN TH-229 2.750E-02 4.927E-01 4.929E-01 FAIL ABUN PA-231 2.686E-01 5.389E-01 5.524E-01 NOT IDENT. TH-231 -l.003E-01 7. 311E-01 7.325E-01 FAIL ABUN PA-233 5.629E-04 6. 771E-02 6. 771E-02 FAIL ABUN PA-234 -7.937E-02 3.736E-01 3.753E-01 FAIL ABUN PA-234M -l.304E+OO 5.456E+OO 5.487E+OO NOT IDENT. U-235 1. 313E-02 1.897E-01 l.898E-01 FAIL ABUN NP-237 5.629E-04 6. 771E-02 6.771E-02 FAIL ABUN NP-238 1.000E+41 l.900E+41 0.000E+OO SHORT HLIF NP-239 -8.397E-02 2.567E-01 2.594E-01 NOT IDENT. AM-241 4.371E-02 7.074E-02 7.343E-02 NOT IDENT. CM-243 -4.231E-02 1.013E-01 1. 031E-01 NOT IDENT. BK-247 9.072E-02 9.125E-02 1.000E-01 NOT IDENT. CM-247 -3.040E-02 4.257E-02 4.472E-02 NOT IDENT. CF-249 7. 471E-03 4.250E-02 4.264E-02 NOT IDENT. CF-251 1. 046E-02 1.315E-01 1.316E-01 NOT IDENT. Page 3073of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 84.9955 87.09 151.3662 136.47 76.0925 45.60 104.8623 87.57 151.4658 140.51 0.0000 46.54 105.0630 88.03 175.2441 143.76 71. 6081 49.72 0.0000 88.34 153.2064 144.24 66.5855 51. 35 101.5943 88.47 153.2330 145.44 79.3240 51. 87 94.9898 89. 96 87.8530 152.43 86.6695 52.39 89.4901 1093.63 123.5825 153.25 0.0000 52.97 89.5877 91.11 0.0000 323.87 69.7948 53.44 94.1498 92.59 123.9063 156.02 0.0000 54.07 99.8704 93.35 124.0308 158.56 0.0000 57.36 0.0000 94.56 101.9316 159.00 67.7201 57.53 123.0845 9,4. 65 100.3505 162.33 73.7645 57.98 120.9224 94.67 100.3537 162.66 0.0000 59.27 110.2482 94.87 100.3800 163.33 55.8038 59.32 110.2578 97.43 127.8914 165.86 75.7271 59.54 117.8549 98.43 82.8361 176.31 70.3617 60. 96 151.4684 98.44 82.8372 176.60 0.0000 61.17 145.4619 99.53 81. 7502 177.52 76.5238 62.93 140.1993 100 .11 78.2011 181.07 0.0000 63.29 140.2847 102.03 104.9228 181.52 70.6822 63.58 140.3530 103.18 91. 7883 184.41 62.9854 64.28 138.6134 103.37 91. 8103 143.76 63.0557 66.73 131.5265 105.21 92.0191 193.51 61.7072 67.24 134.6972 1'05. 31 92.0307 197.03 62.7707 125.81 130.9636 106.12 88.4853 198.01 53.0884 67.75 134.4252 106.47 88.5232 201.83 57.6909 69.67 110.6375 109.28 85.1747 203.43 63.9866 70.83 121. 6157 111. 00 87.7879 205.31 57.4073 72.81 121. 6057 111.76 0.0000 210.85 64.3638 72.87 121.6169 114. 06 67.3025 215.65 69.9885 74.66 121.9510 116.30 0.0000 222 .11 61.6786 74.82 121. 9806 116.74 82.2421 227.09 69.6935 74.97 122.0079 119.76 77.5988 227.38 69.7084 77 .11 122.4012 121.12 76.4844 228.16 0.0000 78.74 143.3419 121. 22 76.4929 228.18 67.0328 79.69 127.9390 121.78 64.1958 116.74 67.0328 80.12 128.0191 122.06 64.2161 235.69 49.1869 80.19 0.0000 122.92 72.9303 235. 96 43.7300 80.57 106.2320 123.07 76.6514 238.63 58.4199 81. 00 120.3673 265.00 82.8892 238.98 0.0000 81. 07 132.8860 125.81 74.4035 240.99 58.5189 81. 75 129.1043 127.23 84.4547 242.00 58.5612 83.79 116 .1403 127.91 82.8603 244.70 38.5047 84.00 116.1745 129.30 82.1548 252.40 0.0000 85.43 125.8472 131.20 86.4805 252.80 54.3984 86.55 151.2529 133.02 76.6508 254.15 0.0000 86.79 151.3027 133.52 81. 27 58 256.23 46.2097 86.94 151.3350 136.00 80.2344 260.90 0.0000 Page 3074 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.8277 355.39 0.0000 584.27 27.8035 264.80 41.8323 356.01 39.7881 595.83 0.0000 265.00 41. 27 99 364.49 0.0000 427.87 18.6519 268.22 53.1082 366.42 0.0000 602.52 0.0000 269.46 43.8273 372.51 20.8154 604. 72 26.3730 270.03 43.8435 375.05 .17.8660 607.14 26.3965 271.23 46.2129 377.52 32.7966 609.32 26.4180 273.65 0.0000 356.01 28.9174 610.33 31. 3841 276.40 52.4590 388.16 28.9817 614.28 24.8135 277.37 52.4920 388.63 0.0000 618.01 19.8779 277.60 53.4375 391.69 34.0408 620. 36 19.8955 278.00 53.4514 264.66 19.1098 621. 93 23.2251 279.20 55.3701 401. 81 29.1847 630.19 0.0000 279.54 55.3821 402.40 39.2603 631.29 14.4266 279.70 55.3881 404.85 25.3994 633.25 15.5478 280.46 53. 5372 410.95 31.3406 634.78 0.0000 283.69 57.4134 413.71 31. 3835 635.95 22.2323 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 42.4008 423. 72 0.0000 645.85 23.4276 285.90 0.0000 427.09 36.6841 657.76 15.1249 287.50 30.1921 427.87 32.6204 657.90 0.0000 290.67 56.7236 433.94 24.5366 661. 66 20.1943 293.27 0.0000 439.40 28.7007 664.57 0.0000 351. 93 45.5088 453.88 15.4797 666.33 0.0000 295. 96 45.5303 463.37 17.1022 666.50 0.0000 879.38 45.6045 468.07 17.1388 667.71 0.0000 299.98 45.6436 473.00 0.0000 677. 62 21. 4353 300.09 45.6465 475.06 28.7590 685.70 0.0000 300 .13 45.6475 476.78 18.7701 695.00 0.0000 301.36 45.6826 477.60 18.7771 696.49 15.8970 302.85 41. 437 9 482.18 20.9062 696. 51 15.8970 256.23 24.3156 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.6299 306.78 42.0145 497.08 22.0950 697.49 13.6304 308.46 27. 7197 505.52 30.0957 702.65 21. 6193 311. 90 39. 2716 507.63 0.0000 706.68 13. 6729 316.51 45.1430 511. 00 25.4028 711. 68 17.1198 319.41 0.0000 514.00 25.4355 720.70 0.0000 320.08 0.0000 514.00 25.4355 721. 93 0.0000 321.04 49.1168 520.40 23.3786 722.78 18.3288 323.87 47 .2694 520.69 0.0000 722. 91 18.3294 325.23 52.1334 522.65 0.0000 723. 31 16.0405 328.76 0.0000 527.90 0.0000 724.19 19.4833 333.37 30.5554 528.26 25.5879 727.33 18.3561 333.97 33.4766 529.59 25.6025 733.00 14.9419 334.37 34.9402 529.87 0.0000 735.93 23.0103 338.28 27.2367 531. 02 0.0000 333.97 17.2662 338.32 27. 2372 537.26 0.0000 739.50 0.0000 311. 90 37.9836 546.56 0.0000 747.24 18.4753 340.48 37.9836 552.55 16.1517 748.06 10.3953 340.55 0.0000 563.25 27.5762 752.31 17.3492 344.28 36.3084 569.33 28.1847 753.82 0.0000 345.93 37.5148 946.00 28.1857 756.73 13.8989 351.06 40.1692 569.70 28.1878 756.80 13.8994 351. 93 40.1884 583.19 27.2471 884.68 13. 9307 Page 3075 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 26.7163 1274.44 8.3752 1620.50 4.2529 766.42 27.8838 1001.03 14.9072 1621. 92 2.1270 766.84 20.9158 1002.74 15.8462 1678.03 0.0000 772. 60 0.0000 1004.73 14.9219 1690.97 1.0764 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1. 7438 778.90 22.1613 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 12.0383 1771. 35 2.1824 785.37 24.5436 1038.76 0.0000 1791.20 0.0000 792.07 30.7425 631. 29 12.2534 1808.65 3.2937 794.95 28.1328 1048.07 0.0000 1810.72 0.0000 795.86 21.9849 1049.04 17.9203 1836.06 3.3083 810.06 9. 7153 1050.41 15.0957 810.29 9.7160 1063.66 13.2523 344.28 9.7166 1077.00 0.0000 810.76 9.7177 1077.34 15 .1963 815.77 0.0000 1085.87 14.2767 1048.07 0.0000 1093.63 14.3033 832.01 15 .1142 1099.45 8.5941 834.85 20.4661 1112. 07 14.3665 835. 71 17.8009 1112. 84 17.2430 836.80 0.0000 1115. 54 16.8706 846.75 0.0000 1120. 29 29.1735 846.77 19.6448 1120.55 19. 9621 856.80 0.0000 1221.41 15.3584 860.56 16.1378 1129. 67 15.3887 871.09 9.5924 1131.51 0.0000 873.19 7.1987 1147.95 0.0000 875.33 0.0000 1173.23 14.5743 879.38 12.3624 1177.95 12.4500 880.51 12.3662 1189.05 11. 7012 883.24 12.3758 1204.77 14.6786 884.68 15.8893 1221. 41 8.8401 889.28 11. 3641 1231.02 17.3239 894.76 14.4858 1235.36 0.0000 898.04 19.0300 1238.28 16.7603 900.72 13.6034 1260.41 0.0000 903.28 16.3356 1271.87 5.9590 911. 20 16.3718 1274.44 10.9308 912.08 16.3757 1274.54 10.9308 923.98 0.0000 1291.59 9.9731 926.50 12.7875 1298.22 0.0000 929 .11 8.2263 1312 .11 0.0000 937.49 14.6582 1332.49 7.0419 944 .13 0.0000 1362.66 0.0000 946.00 18.3649 1365 .19 8.1021 949.00 12.8661 1368.63 0.0000 667.71 0.0000 1384.29 8.1333 962. 31 14.7563 1408.01 5.1077 964. 08 14.7637 1457.56 0.0000 966 .17 14.7720 1460.82 7.2252 911. 20 14.7827 1489.16 2.0756 968. 97 14.7827 1505.03 4. 9966 983.53 0.0000 1584.12 3.3801 984.45 0.0000 1596.21 0.0000 Page 3076 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:08:34.60 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM25.CNF;357 Background date : Z-OCT-2016 11:01:25. Sample date 10-DEC-2015 10:30:00 Acquisition date : 3-0CT-2016 08:06:24. Sample ID G405235009 Sample quantity 1.34381E+02 GRAM Detector name : GAM25 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.62 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 0 0 3 3 6 6 0 6 6 0 1 1 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3077 of 5809 Energy 46.38* 63.59* 74.85* 77.11* 84.01* 87.39 90.02 92.97* 186.07* 188.01 209.48 238.76* 241.66 269.95 295.28* 297.40 300.15 304.40 328.57 338.73* 352.20* 359.52 365.92 463.66 481.50 511. 58* 583.51* 609.59* 628.56 661.82 728.64 794.87 861.31 911. 58* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 76 35 252 432 51 137 55 144 118 27 41 481 147 31 218 28 57 28 42 69 269 12 22 56 13 53 138 214 16 477 54 14 30 98 207 307 186 147 199 180 171 168 138 51 94 61 116 95 43 31 32 28 46 94 76 45 53 80 28 51 59 41 20 23 23 21 19 18 1. 01 1. 04 0.99 0.85 1. 42 1. 52 1. 01 1.15 1. 32 0.74 0.60 1. 00 2.04 0.60 1. 36 1.18 1.36 1. 37 1. 66 1. 29 1.26 0.89 3.16 2.90 0.66 1. 89 1. 65 1. 36 1. 65 1. 45 2.05 1. 64 1. 07 1. 50 92.26 126.67 149.20 153. 72 167.51 174.27 179.53 185.42 371. 60 375.48 418.42 476.98 482.78 539.36 590.02 594.25 599.75 608.25 656.61 676.91 703.86 718. 50 731.31 926.81 962. 48 1022.65 1166.55 1218. 72 1256.67 1323.20 1456.89 1589.39 1722.34 1822.92 88 121 145 145 164 171 177 177 367 367 415 471 471 535 583 583 583 583 653 672 698 714 725 917 958 1016 1162 1213 1250 1317 1449 1584 1715 1816 9 2.12E-02 10 9.62E-03 14 6.99E-02 14 1.20E-01 7 1. 41E-02 7 3.80E-02 12 1.52E-02 12 4. OlE-02 11 3.27E-02 11 7.42E-03 7 l.15E-02 18 1.34E-01 18 4.09E-02 9 8.59E-03 34 6.07E-02 34 7.78E-03 34 1.60E-02 34 7.66E-03 9 l.18E-02 11 1.91E-02 12 7.48E-02 6 3.43E-03 10 6. OlE-03 18 1.55E-02 7 3.67E-03 16 1.48E-02 14 3.82E-02 14 5.95E-02 10 4.44E-03 12 1.32E-01 17 1. 49E-02 9 3.78E-03 15 8.32E-03 15 2.73E-02 36.9 99.l 10.8 9.42E-01 6.6 48.8 18.5 37.8 2.80E+OO 18.6 20.3 2.78E+OO 49.9 41. 9 5.3 2.lOE+OO 21. 4 59.5 8.5 3.16E+OO 48.8 22.6 45.6 32.5 30.5 9.0 90.3 69.4 40.0 71. 8 38.1 15.2 9.5 58.1 5.0 26.6 68.0 36.5 14.1 Peak Search Report (continued) Page : 2 Sample ID : G405235009 Acquisition date 3-0CT-2016 08:06:24 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 5 931. 00 10 3 2.15 18 61. 77 1859 12 2.79E-03 34.6 3.lOE-01 36 5 934.05 14 3 1. 37 1867.88 1859 12 3.87E-03 33.3 37 0 968.97* 46 18 2.45 1937.76 1934 11 1. 27E-02 23.8. 38 0 1087.13 12 2 1. 60 2174.21 2168 10 3.33E-03 37.5 39 0 1120.99* 25 24 1. 41 2241.97 2235 12 6.92E-03 46.1 40 0 1198. 08 10 20 3.41 2396.26 2385 14 2.87E-03 98.5 41 0 1277.97 15 34 7.78 2556.16 2542 23 4.07E-03107.3 42 0 1294.72 10 2 0.68 2589.68 2585 9 2. 72E-03 42.2 43 0 1377. 63 11 7 5.07 2755.63 2745 14 2.95E-03 61. 4 44 0 1444.68 7 0 0.99 2889.86 2883 12 1.94E-03 37.8 45 0 1460.82* 355 7 1. 99 2922.17 2915 15 9.86E-02 5.6 46 0 1848.28 9 3 1. 79 3697.89 3692 10 2.63E-03 45.2 Flag: "*" = Peak area was modified by background subtraction Page 3078 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:08:37 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 10-DEC-2015 10:30:00 G405235009 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:06:24 134.38 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA25 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3079 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09' 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 74.66 74.82 74.82 351.06 CAN 0 01:00:00.62 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235009 Acquisition date 3-0CT-2016 08:06:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.131E+OO 1. 571E+Ol 1. 57.lE+Ol 11. 22 OK CD-109 88.03 3.70* 9.275E+OO 1.166E+OO 1.824E+OO 85.38 OK SN-126 64.28 9.60 9.538E+00 2.527E-01 2.527E-01 198.23 OK 86.94 8.90 9.275E+OO 4.846E-01 4.846E-01 85.38 OK 87.57 37.00* 9.275E+OO 1.166E-01 l.166E-01 85.38 OK BA-137M 661.66 89.90* 2.257E+OO 1.333E+OO 1.359E+OO 10.04 OK CS-137 661.66 85.10* 2.257E+00 l.409E+OO 1.435E+OO 10.04 OK TL-208 277.37 6.60 4.809E+OO Line Not Found Absent 583.19 85.00* 2.509E+OO 3*. 698E-01 3.698E-01 30.35 OK 860.56 12.50 1.809E+OO 7.369E-01 7.369E-01 72.92 OK PB-210 46.54 4.25* 9.109E+OO 1.347E+OO 1.381E+OO 73.81 OK PB-212 74.82 10.28 9.404E+OO 8.358E-01 8.358E-01 47.84 OK 77 .11 17.10 9.383E+OO 1. 775E+OO 1. 775E+OO 13 .12 OK 238.63 43.60* 5.476E+OO 1.232E+OO 1.232E+OO 10.64 OK 300.09 3.30 4.485E+OO 2.336E+OO 2.336E+OO 45.10 OK BI-214 609.32 45.49* 2.418E+OO l.112E+OO 1.112E+OO 18.92 OK 1120.29 14.92 l.443E+OO 6.310E-01 6.312E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Found Absent PB-214 74.82 5.80 9.405E+00 Line Not Found <<INT.Reject 77 .11 9.70 9.383E+OO 3.130E+00 3.131E+00 13.12 OK 87.09 3.41 9.279E+OO Line Not Found <<INT Reject 242.00 7.25 5.413E+OO Line Not Found <<INT Reject 295.22 18.42 4.551E+OO 1.570E+OO 1.570E+OO 17.08 OK 351. 93 35.60* 3.891E+OO l.155E+00 1.156E+OO 18.02 OK RN-222 609.32 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 OK 1120.29 14.92 1.443E+OO 6.310E-01 6.312E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Found Absent RA-224 240.99 4.10* 5.420E+OO l.275E+OO 1.275E+OO 141.00 OK RA-226 609.32 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 OK 1120. 29 14.92 l.443E+00 6.310E-01 6.312E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Found Absent AC-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.029E+OO 9.021E-01 9. 021E-01 61. 06 OK 794.95 4.25 1.935E+OO 9.264E-01 9.264E-01 135.94 OK 835.71 1. 61 1.856E+00 Line Not Found Absent 911.20 25.80* 1. 724E+OO 1.225E+OO 1.225E+OO 28.29 OK 968. 97 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 OK RA-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.029E+OO 9.021E-01 9. 021E-01 61. 06 OK 794.95 4.25 1.935E+OO 9.264E-01 9.264E-01 135. 94 OK 835.71 1. 61 1.856E+OO Line Not Found Absent 911.20 25.80* 1.724E+OO 1.225E+OO l.225E+00 28.29 OK 968. 97 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 OK TH-228 74.82 10.28 9.404E+OO 8.358E-01 8.358E-01 47.84 OK 77 .11 17.10 9.383E+OO 1. 775E+OO 1. 775E+OO 13.12 OK 238.63 43.60* 5.476E+OO 1.232E+OO 1.232E+OO 10.64 OK 300.09 3.30 4.485E+OO 2.336E+00 2.336E+OO 45.10 OK TH-229 85.43 14.70 9.314E+OO 2.437E-01 2.437E-01 97.55 OK 88.47 24.00 9.275E+OO 1. 797E-01 1.797E-01 85.38 OK Page 3080 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235009 Acquisition date 3-0CT-2016 08:06:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 193.51 4.41* 6. 496E+00 Line Not Found Absent 210.85 2.80 6.103E+OO 1.494E+OO 1.494E+OO 83.76 OK TH-230 609.32 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 OK 1120.29 14.92 1.443E+OO 6.310E-01 6.310E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Found Absent PA-231 283.69 1. 70 4. 715E+OO Line Not Found Absent 301.36 5.35* 4.485E+OO 1. 441E+OO 1.441E+OO 45.10 OK TH-232 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.029E+OO 9.021E-01 9.021E-01 61. 06 OK 835.71 1. 61 1.856E+OO Line Not Found Absent 911. 20 25.80* 1. 724E+OO 1.225E+OO 1.225E+OO 28.29 OK 968. 97 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 OK TH-234 63.29 3.70* 9.538E+OO 6.556E-01 6.556E-01 198.23 OK 92.59 4.23 9.199E+OO 2.418E+OO 2.418E+OO 37.13 OK U-234 609.32 45.49* 2.418E+00 1.112E+OO 1.112E+OO 18.92 OK 1120.29 14.92 1.443E+OO 6.310E-01 6.310E-01 92.16 OK 1764.49 15.30 9.336E-01 Line Not Found Absent U-235 89. 96 3.47 9.241E+OO 1.118E+OO 1.118E+OO 75. 64' OK '93. 35 5.60 9.199E+OO 1.827E+OO 1.827E+OO 37.13 OK 143.76 10. 96* 7.922E+00 Line Not Found Absent 163.33 5.08 7.333E+OO Line Not Found Absent 185.72 57.20 6.691E+OO 1. 913E-01 1.913E-01 40.58 OK 205.31 5.01 6.202E+OO Line Not Found Absent U-238 63.29 3.70* 9.538E+OO 6.556E-01 6.556E-01 198.23 OK 92.59 4.23 9.199E+OO 2.418E+OO 2.418E+OO 37 .13 OK AM-243 43.53 5.90 8.344E+OO Line Not Found Absent 74.66 67.20* 9.404E+OO 1.279E-01 1. 27 9E-01 47.84 OK ANH-511 511. 00 100.00* 2.807E+OO l.099E-01 1.099E-01 76.13 OK Flag: "*" = Keyline Page 3081 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:08:38.16 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l * *Acquisition date 3-0CT-2016 08:06:24 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
  • Sample date 10-DEC-2015 10:30:00 Analyst initials: MXRl *
  • Sample ID G405235009 Sample Quantity 1.3438E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File. : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.571E+Ol 1. 727E+00 CD-109 1.824E+OO 1.526E+00 SN-126 l.166E-01 9.753E-02 BA-137M 1.359E+OO l.336E-01 CS-137. l.435E+OO 1.412E-01 TL-208 3.698E-01 1.lOOE-01 PB-210 1.381E+OO 9.991E-01 PB-212 1.232E+OO 1.284E-01 BI-214 1.112E+OO 2.062E-01 PB-214 1.156E+OO 2.041E-01 RN-222 1.112E+OO 2.062E-01 RA-224 1. 27 5E+OO 1. 761E+OO RA-226 1.112E+OO 2.062E-01 AC-228 1.225E+OO 3.396E-01 RA-228 1.225E+OO 3. 396E-01 TH-228 l.232E+00 1.284E-01 TH-229 -3. 296E-01 4.288E-01 TH-230 l .112E+00 2.061E-01 PA-231 1.441E+OO 6.369E-01 TH-232 l.225E+00 3. 396E-01 TH-234 6.556E-01 1.274E+OO U-234 1.112E+OO 2.061E-01 U-235 4.637E-02 1.639E-01 U-238 6.556E-01 1. 274E+OO AM-243 1. 27 9E-01 5.995E-02 ANH-511 l.099E-01 8.199E-02 Noh-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3082 of 5809 Key-Line Activity (pCi/GRAM 2.661E+OO 3.162E-02 O.OOOE+OO 6.255E-03 K.L. Cnt Uncert ( 1. 96-sigma) 1. 4 7 6E+Ol 5.806E-02 1.960E+41 2.080E-02 MDA (pCi/GRAM 5.843E-01 l.295E+00 8.267E-02 7. 723E-02 8.159E-02 7.677E-02 6.610E-01 8.755E-02 l.304E-01 l.252E-01 l.304E-01 9.401E-01 1.304E-01 2.891E-01 2.891E-01 8.755E-02 7.339E-01 1.303E-01 6.375E-01 2.891E-01 8.056E-01 l.303E-01 3.117E-01 8.056E-01 4.413E-02 5.541E-02 MDA (pCi/GRAM 2.592E+Ol l.205E-01 O.OOOE+OO 5.709E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 1.855E-01 4.335E-01 8.997E-01 FAIL ABUN V-48 O.OOOE+OO 1. 611E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 4.361E+02 O.OOOE+OO SHORT HLIF MN-54 l.633E-02 7.268E-02 l.465E-01 NOT IDENT. C0-56 -5.956E-02 4.434E-Ol 8.743E-01 NOT IDENT. MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.905E-02 3.876E-02 6. 981E-02 NOT IDENT. C0-58 3. 051E-02 4.858E-01 l.009E+OO NOT IDENT. FE-59 1. 751E+OO 6.862E+OO 1.432E+Ol NOT IDENT. C0-60 1. 35.0E-02 4.504E-02 9.302E-02 NOT IDENT. ZN-65 -l.109E-01 2.428E-Ol 3.679E-01 NOT IDENT. GE-68 8.788E-01 2.899E+OO 5.824E+OO NOT IDENT. AS-73 l.073E+00 1.691E+OO 3.508E+OO NOT IDENT. AS-74 O.OOOE+OO 6.245E+03 O.OOOE+OO SHORT HLIF SE-75 -3.233E-02 1. 893E-01 3.366E-01 NOT IDENT. BR-77 O.OOOE+OO l.317E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.213E+02 O.OOOE+OO SHORT HLIF RB-83 3. 231E-01 6.745E-01 1.366E+OO NOT IDENT. KR-85 4.405E+00 7.677E+OO 1.539E+Ol NOT IDENT. SR-85 4.537E-01 7.946E-01 1. 592E+OO NOT IDENT. RB-86 O.OOOE+OO 2.881E+04 O.OOOE+OO SHORT HLIF Y-88 -l.335E-01 2.806E-01 5.170E-01 NOT IDENT. Y-91 1.692E+02 5.887E+02 1.181E+03 NOT IDENT. NB-94 7.792E-03 3.280E-02 6.358E-02 NOT IDENT. NB-95 1.508E-01 1. 069E+OO 1. 980E+00 NOT IDENT. NB-95M 7.155E-01 2.422E+OO 4 .. 167E+OO NOT IDENT. ZR-95 -6.851E-03 1. 372E+OO 2.599E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 852E-f41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.355E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.969E-02 2.744E-02 4.788E-02 NOT IDENT. RH-102 l.982E-02 5.620E-02 1.052E-01 NOT IDENT. RU-103 -7.399E-01 6.537E+OO 1.202E+Ol FAIL ABUN RH-106 4.417E-01 5.306E-01 1.087E+OO NOT IDENT. RU-106 4.417E-01 5.306E-01 1.087E+OO NOT IDENT. AG-108M -1.515E-02 2.932E-02 5.325E-02 NOT IDENT. AG-110M -4.508E-02 1.170E-01 2.178E-01 NOT IDENT. SN-113 1.091E-01 2.420E-01 4. 872E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 862E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 7.590E+04 O.OOOE+OO SHORT HLIF TE-123M 2.173E-02 1.111E-01 2 .113E-01 NOT IDENT. SB-124 5.418E-01 1.661E+OO 4.176E+OO NOT IDENT. SB-125 3.870E-02 1.256E-01 2.457E-01 FAIL ABUN TE-125M 2. 2 69E+02 2.014E+02 4.163E+02 NOT IDENT. I-126 O.OOOE+OO 9.701E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.109E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.618E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 8.383E+09 0.000E+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.480E+26 0.000E+OO SHORT HLIF BA-133 -1. 782E-02 5.633E-02 7.376E-02 NOT IDENT. I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 6.054E-02 8.065E-02 l.199E-01 FAIL ABUN CS-135 3. 691E-02 1.595E-01 2.701E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.272E+05 O.OOOE+OO SHORT HLIF CE-139 -4.642E-02 9. 727E-02 1.740E-01 NOT IDENT. BA-140 O.OOOE+OO l.451E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.369E+05 O.OOOE+OO SHORT HLIF CE-141 -5.909E+OO 2.174E+Ol 3.970E+Ol NOT IDENT. CE-143 O.OOOE+OO $.509E+40 O.OOOE+OO SHORT HLIF CE-144 -4.959E-02 2.739E-01 5.136E-01 NOT IDENT. PM-144 -4.640E-03 5.639E-02 1.046E-01 NOT IDENT. PR-144 -4.345E-01 4.889E+OO 9.061E+OO NOT IDENT. PM-146 -6.640E-02 4.803E-02 7. 713E-02 NOT IDENT. ND-147 O.OOOE+OO 3.458E+07 O.OOOE+OO SHORT HLIF PM-147 2.122E+02 6.514E+02 1. 274E+03 NOT IDENT. PM-149 O.OOOE+OO 2.676E+40 O.OOOE+OO SHORT HLIF EU-150 2.936E-03 2.949E-02 5.224E-02 FAIL ABUN EU-152 -1.635E-02 1.027E-01 1.880E-01 FAIL ABUN GD-153 -l.370E-02 1.225E-01 2.330E-01 NOT IDENT. EU-154 7.697E-02 l.424E-01 2.954E-01 NOT IDENT. EU-155 6 .138E-02 7.207E-02 l.484E-01 FAIL ABUN TB-160 -9.744E-01 1.701E+OO 3.108E+OO FAIL ABUN H0-166M -2.264E-02 6.623E-02 1.166E-01 NOT IDENT. TM-171 1.070E+OO 3.740E+00 7.617E+OO NOT IDENT. HF-172 -6.646E-02 l.776E-01 3.291E-01 FAIL ABUN Page 3083 of 5809 LU-172 1.140E-01 9.308E-02 2.091E-01 FAIL ABUN LU-176 l.849E-02 2.267E-02 4.486E-02 FAIL ABUN HF-181 4.208E+OO 5.925E+OO 9.140E+OO FAIL ABUN TA-182 7.320E-02 9.871E-01 1.925E+OO FAIL ABUN RE-183 8.592E-02 7.612E-01 1.540E+OO NOT IDENT. RE-184 -2.544E+00 3.071E+Ol 6.019E+Ol NOT IDENT. W-188 -8.215E+OO 1.243E+02 2.019E+02 FAIL ABUN IR-192 -4.103E-01 4. 411E-01 7.933E-01 FAIL ABUN HG-203 -1.422E+OO 2.615E+OO 4.400E+OO NOT IDENT. BI-207 -6.303E-03 4. 881E-02 9.438E-02 FAIL. ABUN BI-211 O.OOOE+OO 5.623E-01 8.326E-01 FAIL ABUN PB-211 1. 501E-01 7.320E-01 1.433E+OO NOT IDENT. BI-212 0.000E+OO 1.134E+OO 1.475E+OO FAIL ABUN RN-219 -3.899E-01 4.248E-01 7.423E-01 FAIL ABUN RA-223 -5.684E-01 6.527E-01 1.117E+OO FAIL ABUN AC-227 -1.566E-01 2.106E-01 3.488E-01 FAIL ABUN TH-227 -1.566E-01 2.106E-01 3.488E-01 FAIL ABUN TH-231 -5.684E-01 6.527E-01 l .117E+OO FAIL ABUN PA-233 1.157E-02 6 .159E-.02 1.222E-01 FAIL ABUN PA-234 5 .117E-02 2. 771E-01 5.682E-01 NOT IDENT. PA-234M -1.149E+OO 4.204E+OO 8.188E+OO NOT IDENT. NP-237 1.157E-02 6.159E-02 1.222E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -3.652E-02 l.884E-01 3.558E-01 NOT IDENT. PU-239 2.896E+Ol 2.737E+02 5.202E+02 NOT IDENT. AM-241 1.940E-02 4.328E-02 8.364E-02 NOT IDENT. CM-243 -1.326E-02 6.780E-02 1.296E-01 NOT IDENT. BK-247 -1.995E-02 6.859E-02 1.199E-01 FAIL ABUN CM-247 -2.568E-02 3.748E-02 6.723E-02 NOT IDENT. CF-249 -3.489E-04 4. 091E-02 7.876E-02 NOT IDENT. CF-251 -8.440E-03 1.038E-01 1.910E-01 NOT IDENT. Page 3084 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:08:35.47 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 339 10.66* l.131E+OO 1. 571E+Ol 1.571E+Ol 11. 22 CD-109 88.03 160 3.70* 9.275E+OO 2.612E+OO 4.087E+OO 36.90 SN-126 64.28 41 9.60 9.538E+OO 2.527E-01 2.527E-01 198.23 86.94 160 8.90 9.275E+OO 1.086E+OO l.086E+OO 36.90 87.57 160 37.00* 9.275E+OO 2.612E-01 2.612E-01 36.90 BA-137M 661. 66 484 89.90* 2.257E+00 1.333E+OO 1.359E+OO 10.04 CS-137 661. 66 484 85.10* 2.257E+OO 1.409E+OO l.435E+00 10.04 TL-208 277.37 ------6.60 4.809E+OO ------Line Not Found ------583.19 141 85.00* 2.509E+OO 3.698E-01 3.698E-01 30.35 8 60. 56 30 12.50 l.809E+OO 7.369E-01 7.369E-01 72.92 PB-210 46.54 93 4.25* 9.109E+OO 1.347E+OO l.381E+OO 73.81 BI-211 72. 87 ------1.23 9.424E+OO ------Line Not Found ------351.06 286 12.92* 3. 891E+OO 3.183E+OO 3.183E+OO 18. 02 PB-212 74.82 298 10.28 9.404E+OO 1. 722E+OO 1. 722E+OO 21. 50 77 .11 510 17.10 9.383E+OO 1. 775E+OO 1. 77 5E+OO 13.12 238.63 527 43.60* 5.476E+OO 1.232E+OO 1.232E+OO 10.64 300.09 62 3.30 4.485E+OO 2.336E+OO 2.336E+OO 45.10 BI-214 609.32 219 45.49* 2.418E+OO l .112E+00 1.112E+OO 18.92 1120. 29 24 14.92 l.443E+00 6.310E-01 6.312E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------PB-214 74.82 298 5.80 9.404E+OO 3.051E+OO 3.052E+OO 21. 50 77 .11 510 9.70 9.383E+OO 3 .130E+OO 3 .131E+OO 13.12 87.09 160 3.41 9.275E+OO 2.835E+OO 2.836E+OO 36.90 242.00 161 7.25 5.420E+OO 2. 291E+OO 2.291E+00 42.80 295.22 236 18.42 4.551E+OO 1.570E+OO l.570E+OO 17.08 351. 93 286 35.60* 3. 891E+OO 1.155E+OO 1.156E+OO 18.02 RN-222 609.32 219 45.49* 2.418E+OO l .112E+OO l .112E+OO 18.92 1120.29 24 14.92 1.443E+OO 6.310E-01 6.312E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------RA-224 240.99 161 4.10* 5.420E+OO 4.050E+OO 4.050E+OO 42.80 RA-226 609.32 219 45.49* 2.418E+OO 1.112E+OO 1.112E+OO 18.92 1120.29 24 14.92 1.443E+OO 6.310E-01 6.312E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------AC-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 73 11. 27 4.029E+OO 9. 021E-01 9.021E-01 61. 06 794.95 14 4.25 1.935E+OO 9.264E-01 9.264E-01 135.94 835. 71 ------1. 61 l.856E+00 ------Line Not Found ------911. 20 98 25.80* 1.724E+OO l.225E+00 1.225E+OO 28.29 968. 97 45 15.80 l.637E+00 9.749E-01 9.749E-01 47.53 RA-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 73 11. 27 4.029E+OO 9. 021E-01 9.021E-01 61. 06 794.95 14 4.25 1.935E+00 9.264E-01 9.264E-01 135. 94 835.71 ------1. 61 1.856E+OO ------Line Not Found ------911.20 98 25.80* 1.724E+OO 1.225E+OO 1.225E+OO 28.29 968.97 45 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 TH-228 74.82 298 10.28 9.404E+OO l.722E+00 1. 722E+OO 21. 50 77 .11 510 17.10 9.383E+OO 1. 775E+OO 1.775E+OO 13.12 Page 3085 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235009 Acquisition date 3-0CT-2016 08:06:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 527 43.60* 5.476E+OO .1. 232E+OO 1.232E+OO 10.64 300.09 62 3.30 4.485E+OO 2.336E+OO 2.336E+OO 45.10 TH-229 85.43 60 14.70 9.314E+OO 2.437E-01 2.437E-01 97.55 88.47 160 24.00 9.275E+OO 4.027E-01 4.028E-01 36.90 193.51 ------4.41* 6.496E+OO ------Line Not Found ------210.85 46 2.80 6.103E+OO 1.494E+OO 1. 494E+OO 83.76 TH-230 609.32 219 45.49* 2.418E+OO 1.112E+OO l .112E+OO 18.92 1120.29 24 14.92 1.443E+OO 6.310E-01 6.310E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------PA-231 283.69 ------1. 70 4.715E+OO ------Line Not Found ------301.36 62 5.35* 4.485E+OO 1.441E+OO 1.441E+OO 45.10 TH-232 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 73 11. 27 4.029E+OO 9.021E-01 9.021E-01 61. 06 835. 71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 98 25.80* l.724E+OO 1.225E+OO l.225E+OO 28.29 968. 97 45 15.80 1.637E+OO 9.749E-01 9.749E-01 47.53 TH-234 63.29 41 3.70* 9.538E+OO 6.556E-01 6.556E-01 198.23 92.59 168 4.23 9.199E+OO 2.418E+OO 2.418E+OO 37.13 U-234 609.32 219 45.49* 2.418E+OO l .112E+OO 1.112E+OO 18.92 1120.29 24 14.92 1.443E+OO 6.310E-01 6.310E-01 92.16 1764.49 ------15.30 9.336E-01 ------Line Not Found ------U-235 89. 96 64 3.47 9.241E+OO 1.118E+OO 1.118E+OO 75.64 93.35 168 5.60 9.199E+OO 1.827E+OO 1.827E+OO 37.13 143.76 ------10. 96* 7.922E+OO ------Line Not Found ------163.33 ------5.08 7.333E+OO ------Line Not Found ------185. 72 131 57.20 6.691E+OO 1.913E-01 1.913E-01 40.58 205.31 ------5.01 6.202E+00 ------Line Not Found ------U-238 63.29 41 3.70* 9.538E+OO 6.556E-01 6.556E-01 198.23 92.59 168 4.23 9.199E+OO 2.418E+OO 2.418E+OO 37 .13 AM-243 43.53 ------5.90 8.344E+OO ------Line Not Found ------74.66 298 67.20* 9.404E+OO 2.634E-01 2.634E-01 21. 50 ANH-511 511. 00 55 100.00* 2.807E+OO l.099E-01 1.099E-01 76.13 Flag: "*" Key line Page 3086 of 5809 Summary of Nuclide Activity Sample ID : G405235009 Acquisition date Page : 3 3-0CT-2016 08:06:24 Total number of lines in spectrum 46 Number of unidentified lines 11 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+10Y 22.20Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600.00Y 1600.00Y l.41E+10Y 1600.00Y 1. 41E+l0Y 1. 41E+10Y 1.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 56 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.571E+Ol 2.612E+00 2.612E-01 1.333E+OO l.409E+OO 3.698E-01 1. 347E+00 3.183E+OO 1.232E+OO 1.112E+OO 1.155E+OO 1.112E+OO 4.050E+OO 1.112E+OO 1.225E+OO 1. 225E+OO l.232E+OO 4.027E-01 1.112E+OO 1. 441E+OO 1.225E+OO 6.556E-01 1.112E+OO l.913E-01 6.556E-01 2.634E-01 l.099E-01 4.685E+Ol 4.685E+Ol Decay Corr pCi/GRAM 1.571E+Ol 4.087E+OO 2.612E-01 l.359E+OO l.435E+OO 3.698E-01 1.381E+OO 3.183E+OO 1.232E+OO 1.112E+OO 1.156E+OO 1.112E+OO 4.050E+OO 1.112E+OO 1.225E+OO 1.225E+OO l.232E+OO 4.028E-01 1.112E+OO 1.441E+OO l.225E+OO 6.556E-01 1.112E+OO 1.913E-01 6.556E-01 2.634E-01 l.099E-01 4.841E+Ol 4. 841E+Ol 76.09% Decay Corr 2-Sigma Error 0.176E+Ol 1.508E+OO 0. 964E-01 0.136E+OO 0.144E+OO l.122E-01 1.019E+OO 0.574E+OO 0.131E+OO 0.210E+OO 0.208E+OO 0.210E+OO l.733E+00 0.210E+OO 0.347E+OO 0.347E+OO 0 .131E+OO l.486E-01 0.210E+OO 0.650E+OO 0.347E+OO 13.00E-01 0.210E+OO 0.776E-01 13.00E-01 0.566E-01 0.837E-01 "M" Manually accepted 2-Sigma %Error 11.22 36.90 36. 90 10.04 10.04 30.35 73.81 18.02 10.64 18.92 18.02 18.92 42.80 18.92 28.29 28.29 10.64 36.90 18.92 45.10 28.29 198.23 18.92 40.58 198.23 21. 50 76.13 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3087 of 5809 Flags K K Unidentified Energy Page : 4 Sample ID : G405235009 Acquisition date : 3-0CT-2016 08:06:24 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 6 188.01 30 56 0.74 375.48 367 11 7.42E-03 99.8 6.64E+OO 0 269.95 34 103 0.60 539.36 535 9 8.59E-03 **** 4.92E+OO T 1 297.40 30 34 1.18 594.25 583 34 7.78E-03 97.6 4.52E+OO T 1 304.40 30 30 1.37 608.25 583 34 7.66E-03 91.2 4.43E+OO. T 0 328.57 45 49 1. 66 656.61 653 9 1.18E-02 65.0 4.14E+OO T 0 359.52 13 47 0.89 718. 50 714 6 3.43E-03 **** 3.82E+OO 0 365.92 23 57 3.16 731.31 725 10 6.0lE-03 **** 3.76E+OO T 0 463.66 58 84 2.90 926. 81 917 18 1.55E-02 80.1 3.06E+OO T 0 481.50 14 29 0.66 962.48 958 7 3.67E-03 **** 2. 96E+OO T 0 628.56 16 20 1. 65 1256.67 1250 10 4.44E-03 **** 2.36E+OO 0 728. 64 54 24 2.05 1456.89 1449 17 1. 49E-02 53.2 2.08E+OO T 5 931. 00 10 2 2.15 1861. 77 1859 12 2.79E-03 69.3 1. 69E+OO 5 934.05 14 3 1. 37 1867.88 1859 12 3.87E-03 66.6 1.69E+OO 0 1087 .13 12 2 1. 60 2174.21 2168 10 3.33E-03 75.0 1.48E+OO T 0 1198.08 10 19 3.41 2396.26 2385 14 2.87E-03 **** 1.36E+OO 0 1277.97 14 33 7.78 2556.16 2542 23 4.07E-03 **** 1.28E+OO 0 1294.72 9 2 0.68 2589.68 2585 9 2. 72E-03 84.4 1.27E+OO 0 1377.63 10 7 5.07 2755.63 2745 14 2.95E-03 **** 1. 20E+OO 0 1444.68 7 0 0.99 2889.86 2883 12 l.94E-03 75.6 1.14E+OO 0 1848.28 9 2 1. 79 3697.89 3692 10 2.63E-03 90.3 8.88E-01 Flags: '"T" = Tentatively associated Page 3088 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:08:53.03 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l *
  • Acquisition date 3-0CT-2016 08:06:24 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
  • Sample date 10-DEC-2015 10:30:00 Nuclide Library : SOLID *
  • Sample ID G405235009 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.3438E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.294E-01 6 .115E-01 3.904E-02 3.477E-02 3.673E-02 3.479E-02 3.094E-01 4.052E-02 5.822E-02 5.700E-02 5.822E-02 4.351E-01 5.822E-02 1. 274E-01 1. 274E-01 4.052E-02 3.397E-01 5.820E-02 2.863E-01 1. 274E-01 3.803E-01 5.820E-02 1. 468E-01 3.803E-01 2. 081E-02 2.497E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3089 of 5809 Le (pCi/GRAM 1.176E+Ol 5.294E-02 0.000E+OO 2.023E-02 3.990E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3090 of 5809 O.OOOE+OO 0.000E+OO 6.531E-02 3.768E-01 O.OOOE+OO 3.261E-02 4.299E-01 6.209E+OO 3. 967E-02 . 1. 598E-01 2.574E+OO 1.649E+OO O.OOOE+OO 1.535E-01 O.OOOE+OO O.OOOE+OO 6.153E-01 7.026E+OO 7.271E-01 0.000E+OO 1. 996E-01 5.172E+02 2.822E-02 8.934E-01 1. 941E+00 1.124E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 231E-02 4.582E-02 5.446E+00 4.870E-01 4.870E-01 2.399E-02 9.534E-02 2.234E-01 O.OOOE+OO O.OOOE+OO 9.859E-02 1. 58 6E+OO 1.132E-01 1. 962E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.347E-02 O.OOOE+OO 5.386E-02 1.252E-01 O.OOOE+OO O.OOOE+OO 8. 096E-02 O.OOOE+OO O.OOOE+OO 1.867E+Ol O.OOOE+OO 2.390E-01 4.603E-02 3.985E+OO 3.434E-02 O.OOOE+OO 5. 971E+02 O.OOOE+OO 2.412E-02 8.634E-02 l.095E-01 l.297E-01 6.949E-02 1.306E+OO 5.164E-02 3.572E+OO l.534E-01 9.348E-02 SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT . NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHO.RT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3091of5809 2.055E-02 4.148E+OO 8.349E-01 7.237E-01 2.616E+Ol 9.289E+Ol 3.607E-01 2.033E+OO 4.033E-02 4. OllE-01 6. 572E-01 6.826E-01 3.373E-01 5.120E-01 1.585E-01 l.585E-01 5.120E-01 5.648E-02 2.461E-01 3.525E+OO 5.648E-02 O.OOOE+OO 1.665E-01 2.452E+02 3.951E-02 6.052E-02 5.478E-02 '3. OSlE-02 3.610E-02 8.898E-02 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:09:00.45 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235009.CNF;l *
  • Acquisition date 3-0CT-2016 08:06:24 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
  • Sample date 10-DEC-2015 10:30:00 Nuclide Library : SOLID *
  • Sample ID G405235009 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.3438E+02 GRAM *
  • Quantity Err(%) : 1.4883E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. 1-AUG-2016 08:41:33 Eff. Geometry :*CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.571E+Ol l.912E+OO CD-109 1.824E+OO 1. 559E+OO SN-126 l.166E-01 9.943E-02 BA-137M 1.359E+OO l.458E-01 CS-137 1.435E+OO l.540E-01 TL-208 3.698E-01 1. lllE-01 PB-210 1. 381E+OO 1.006E+OO PB-212 1.232E+OO 1.440E-01 BI-214 l .112E+00 2. ll 7E-01 PB-214 1.156E+OO 2.097E-01 RN-222 1.112E+OO 2. ll 7E-01 RA-224 1.275E+OO 1.772E+OO RA-226 l .112E+00 2. ll 7E-01 AC-228 1.225E+OO 3.453E-01 RA-228 1.225E+OO 3.453E-01 TH-228 1.232E+OO 1.440E-01 TH-229 -3. 296E-01 4.291E-01 TH-230 1.112E+OO 2 .116E-01 PA-231 L 441E+OO 7.072E-01 TH-232 1.225E+OO 3.453E-01 TH-234 6.556E-01 1.282E+OO U-234 1.112E+OO 2 .116E-01 U-235 4.637E-02 l.639E-01 U-238 6.556E-01 1.282E+OO AM-243 1. 27 9E-01 6.285E-02 ANH-511 l.099E-01 8. 211E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3092 of 5809 Key-Line Activity (pCi/GRAM 2.661E+00 3.162E-02 -l.OOOE+41 6.255E-03 K.L Act error (1.96-sigma) 1.476E+Ol 5.807E-02 5.479E+41 2. 081E-02 TPU ( 1 . 96-s i grrla ) 1. 912E+OO 1.559E+OO 9.943E-02 1.458E-01 1.540E-01 l. lllE-01 1.006E+OO 1.440E-01 2. ll 7E-01 2.097E-01 2. ll 7E-01 1. 772E+OO 2. ll 7E-01 3.453E-01 3.453E-01 1.440E-01 4.291E-01 2 .116E-01 7. 072E-01 3.453E-01 1.282E+OO 2 .116E-01 1.639E-01 1.282E+OO 6.285E-02 8.211E-02 TPU ( 1. 96-sigma) 1.481E+Ol 5.980E-02 O.OOOE+OO 2.lOOE-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 1.855E-01 4.335E-01 4.415E-01 FAIL ABUN V-48 -9.990E+02 1.611E+04 1.612E+04 SHORT HLIF CR-51 3.589E+02 4.363E+02 4.654E+02 SHORT HLIF MN-54 l.633E-02 7.269E-02 7.306E-02 NOT IDENT. C0-56 -5.956E-02 4.434E-01 4.442E-01 NOT IDENT. MN-56 -1.000E+41 8.191E+41 O.OOOE+OO SHORT HLIF C0-57 -2.905E-02 3.878E-02 4.093E-02 NOT IDENT. C0-58 3.051E-02 4.858E-01 4.860E-01 NOT IDENT. FE-59 1. 751E+OO 6.864E+OO 6.909E+OO NOT IDENT. C0-60 1. 350E-0.2 4.504E-02 4.545E-02 NOT IDENT. ZN-65 -1.109E-01 2.429E-01 2.480E-01 NOT IDENT. GE-68 8.788E-01 2.899E+OO 2.926E+OO NOT IDENT. AS-73 l.073E+OO 1.706E+OO 1. 773E+OO NOT IDENT. AS-74 4.227E+03 6.254E+03 6.538E+03 SHORT HLIF SE-75 -3.233E-02 1. 893E-01 1.899E-01 NOT IDENT. BR-77 l.263E+38 1. 086E+39 O.OOOE+OO SHORT HLIF SR-82 -3. 719E+02 8.215E+02 8.384E+02 SHORT HLIF RB-83 3.231E-01 6.759E-01 6.915E-01 NOT IDENT. KR-85 4.405E+OO 7.679E+OO 7.932E+OO NOT IDENT. SR-85 4.537E-01 7.948E-01 8.207E-01 NOT IDENT. RB-86 2.143E+04 2.883E+04 3.040E+04 SHORT HLIF Y-88 -1.335E-01 2.808E-01 2. 871E-01 NOT IDENT. Y-91 1.692E+02 5.887E+02 5.936E+02 NOT IDENT. NB-94 7.792E-03 3.280E-02 3.298E-02 NOT IDENT. NB-95 l.508E-01 1.069E+OO 1. 071E+00 NOT IDENT. NB-95M 7.155E-01 2.423E+OO 2.444E+OO NOT IDENT. ZR-95 -6. 851E-03 1. 372E+OO 1.372E+OO NOT IDENT. NB-97 -l.OOOE+41 l.852E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 l.019E+43 O.OOOE+OO SHORT HLIF M0-99 -4.374E+31 1.356E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 l.210E+42 O.OOOE+OO SHORT HLIF RH-101 -2. 969E-02 2.796E-02 3.lOOE-02 NOT IDENT. RH-102 l.982E-02 5.623E-02 5.693E-02 NOT IDENT. RU-103 -7.399E-01 6.537E+OO 6.546E+OO FAIL ABUN RH-106 4.417E-01 5.313E-01 5.674E-01 NOT IDENT. RU-106 4.417E-01 5. 313E-01 5.674E-01 NOT IDENT. AG-108M -1.515E-02 2.932E-02 3. 011E-02 NOT IDENT. AG-110M -4.508E-02 1.171E-01 l.188E-01 NOT IDENT. SN-113 1. 091E-01 2.420E-01 2.470E-01 NOT IDENT. CD-115 3.038E+38 l.862E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 2.652E+04 7.597E+04 7.690E+04 SHORT HLIF TE-123M 2.173E-02 1.111E-01 l .115E-01 NOT IDENT. SB-124 5.418E-01 1.662E+OO l.679E+OO NOT IDENT. SB-125 3.870E-02 1.256E-01 l.268E-01 FAIL ABUN TE-125M 2.269E+02 2. 018E+02 2.263E+02 NOT IDENT. I-126 8.903E+05 9.775E+05 l.057E+06 SHORT HLIF SB-126 4.828E+05 l .112E+06 l.134E+06 SHORT HLIF SB-127 8.216E+21 1. 969E+22 O.OOOE+OO SHORT HLIF I-131 6.167E+09 8.388E+09 8.837E+09 SHORT HLIF I-132 -1.000E+41 l.858E+42 O.OOOE+OO SHORT HLIF TE-132 2.070E+26 2.617E+26 O.OOOE+OO SHORT HLIF BA-133 -1.782E-02 5.634E-02 5.691E-02 NOT IDENT. I-133 -l.000E+41 9.416E+41 O.OOOE+OO SHORT HLIF CS-134 6.054E-02 8.069E-02 8.518E-02 FAIL ABUN CS-135 3.691E-02 1.595E-01 l.604E-01 NOT IDENT. I-135 -l.OOOE+41 1. 271E+43 O.OOOE+OO SHORT HLIF CS-136 3.652E+03 3.272E+05 3.272E+05 SHORT HLIF CE-139 -4.642E-02 9.772E-02 9.994E-02 NOT IDENT. BA-140 8.721E+05 l.452E+06 l.504E+06 SHORT HLIF LA-140 -l.823E+05 4.370E+05 4.446E+05 SHORT HLIF CE-141 -5.909E+OO 2.174E+Ol 2.190E+Ol NOT IDENT. CE-143 1.000E+41 5.601E+40 O.OOOE+OO SHORT HLIF CE-144 -4.959E-02 2.739E-01 2.748E-01 NOT IDENT. PM-144 -4.640E-03 5.639E-02 5.643E-02 NOT IDENT. PR-144 -4.345E-01 4.889E+OO 4.893E+OO NOT IDENT. PM-146 -6.640E-02 4.827E.:_02 5.680E-02 NOT IDENT. ND-147 -l.046E+07 3.458E+07 3.490E+07 SHORT HLIF PM-147 2.122E+02 6.515E+02 6.585E+02 NOT IDENT. PM-149 1.439E+40 2.694E+40 O.OOOE+OO SHORT HLIF EU-150 2.936E-03 2.949E-02 2.952E-02 FAIL ABUN EU-152 -1.635E-02 1.028E-01 l.030E-01 FAIL ABUN GD-153 -l.370E-02 l.225E-01 1.227E-01 NOT IDENT. EU-154 7.697E-02 1.424E-01 1. 466E-01 NOT IDENT. EU-155 6.138E-02 7.220E-02 7.732E-02 FAIL ABUN TB-160 -9.744E-01 l.702E+OO 1. 758E+OO FAIL ABUN H0-166M -2.264E-02 6.624E-02 6.702E-02 NOT IDENT. TM-171 l.070E+OO 3.741E+OO 3. 772E+OO NOT IDENT. HF-172 -6.646E-02 1.779E-01 1.804E-01 FAIL ABUN Page 3093 of 5809 LU-172 1.140E-01 9.379E-02 1. 069E-01 FAIL ABUN LU-176 l.849E-02 2.268E-02 2.416E-02 FAIL ABUN HF-181 4.208E+OO 5.928E+OO 6.224E+OO FAIL ABUN TA-182 7.320E-02 9. 871E-01 9.877E-01 FAIL ABUN RE-183 8.592E-02 7.614E-01 7.623E-01 NOT IDENT. RE-184 -2.544E+OO 3. 071E+Ol 3.073E+Ol NOT IDENT. W-188 -8.215E+00 1. 243E+02 l.244E+02 FAIL ABUN IR-192 -4.103E-01 4.415E-01 4.787E-01 FAIL ABUN HG-203 -l.422E+OO 2.616E+OO 2.693E+OO NOT IDENT. BI-207 -6.303E-03 4.881E-02 4.889E-02 FAIL ABUN . BI-211 3.183E+OO 5.799E-01 1.548E+OO FAIL ABUN PB-211 1.501E-01 7.320E-01 7.352E-01 NOT IDENT. BI-212 2.176E+OO 1.140E+OO l.504E+OO FAIL ABUN RN-219 -3.899E-01 4.276E-01 4.623E-01 FAIL ABUN RA-223 -5.684E-01 6.536E-01 7.021E-01 FAIL ABUN AC-227 -1.566E-01 2 .116E-01 2.231E-01 FAIL ABUN TH-227 -1.566E-01 2 .116E-01 2.231E-01 FAIL ABUN TH-231 -5.684E-01 6.536E-01 7.021E-01 FAIL ABUN PA-233 l.157E-02 6.159E-02 6.181E-02 FAIL ABUN PA-234 5 .117E-02 2.832E-01 2.842E-01 NOT IDENT. PA-234M -1.149E+OO 4.204E+OO 4.236E+OO NOT IDENT. NP-237 1.157E-02 6.159E-02 6.181E-02 FAIL ABUN NP-238 -1.000E+41 2.176E+41 O.OOOE+OO SHORT HLIF NP-239 -3.652E-02 l.884E-01 1.892E-01 NOT IDENT. PU-239 2. 896E+Ol 2.737E+02 2.740E+02 NOT IDENT. AM-241 1.940E-02 4. 331E-02 4.418E-02 NOT IDENT. CM-243 -1.326E-02 6.781E-02 6.808E-02 NOT IDENT. 'BK-247 -l.995E-02 6.871E-02 6.930E-02 FAIL ABUN CM-247 -2.568E-02 3.773E-02 3.947E-02 NOT IDENT. CF-249 -3.489E-04 4.091E-02 4. 091E-02 NOT IDENT. CF-251 -8.440E-03 l.038E-01 1.039E-01 NOT IDENT. Page 3094 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 73.4783 87.09 95.5220 136.47 69.6050 45.60 71.3332 87.57 95.6613 140.51 0.0000 46.54 71. 6618 88.03 95.7946 143.76 70.6794 49.72 0.0000 88.34 68.4888 144.24 72. 7150 51. 35 79.2780 88.47 68.5156 145.44 79.7888 51. 87 76.4654 89. 96 100.9381 152.43 78.9144 52.39 66.8749 1093.63 101.1413 153.25 0.0000 52.97 68.5541 91.11 0.0000 323.87 69.1664 53.44 64.9216 92.59 101.7205 156.02 0.0000 54.07 71.1566 93.35 101.9443 158.56 0.0000 57.36 0.0000 94.56 66.2623 159.00 60.7004 57.53 80.6626 94.65 69.7675 162.33 64 .1372 57.98 74.6553 94.67 69.7717 162.66 0.0000 59.27 99.0366 94.87 69.8114 163.33 56.0969 59.32 80.4835 97.43 79.1071 165.86 70.7056 59.54 80.5557 98.43 79.3275 176.31 61.6009 60. 96 99. 7124 98.44 79.3295 176.60 0.0000 61.17 99.7959 99.53 71. 6116 177.52 63.8231 62. 93 94.9933 100 .11 80.5803 181.07 0.0000 63.29 95.1262 102.03 63.1992 181.52 71.6389 63.58 95.2328 103.18 71.4301 184.41 88.9302 64.28 95.4895 103.37 71. 4667 143.76 74.2714 66.73 88.1461 105.21 54.7595 193.51 68.7832 67.24 91.5053 105.31 54.7740 197.03 60. 5271 125.81 89.5226 106.12 72. 8871 198.01 62.7861 67.75 87.9466 106.47 74.7552 201.83 72. 9674 69.67 115.9398 109.28 62.5981 203.43 76.4258 70.83 87.3166 111. 00 91.1186 205.31 81. 0290 72.81 115.0662 111.76 0.0000 210.85 63.3120 72.87 114.0042 114. 06 91.8175 215.65 55.6122 74.66 91.7690 116. 30 0.0000 222 .11 48.2818 74.82 91. 8186 116. 74 75.7864 227.09 66.7216 74.97 91.8656 119. 76 64.2358 227.38 64.4868 77 .11 92.5321 121.12 67.2446 228.16 0.0000 78.74 76.4198 121. 22 67.2605 228.18 45.3052 79.69 102.2104 121.78 83.2508 116.74 45.3052 80.12 102.3536 122.06 85.1778 235.69 54.9397 80.19 0.0000 122.92 64.7154 235. 96 54. 9602 80.57 90.2466 123.07 62.8616 238.63 51.7140 81. 00 92.0454 265.00 65.7692 238.98 0.0000 81. 07 92.0664 125.81 71.7579 240.99 51.8802 81.75 86.1159 127.23 88.0922 242.00 51.9509 83.79 102.4324 127.91 87.2800 244.70 49.4362 84.00 102.5000 129.30 87.5527 252.40 0.0000 85.43 101.8259 131.20 80.2791 252.80 38.6467 86.55 95.3647 133.02 89.2366 254.15 0.0000 86.79 95.4340 133.52 64.3593 256.23 47.0526 86.94 95.4784 136.00 62.7744 260.90 0.0000 Page 3095 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 39.2358 355.39 0.0000 584.27 31. 4380 2 64. 80 35.6754 356.01 39.4482 595.83 0.0000 265.00 42.8214 364.49 0.0000 427.87 24.3523 268.22 49. 3621 366.42 0.0000 602.52 0.0000 269.46 52.6273 372. 51 29.3900 604. 72 19.1067 270.03. 52.6649 375.05 38.3870 607.14 35.0813 271.23 62.3324 377.52 38.4753 609.32 23.4198 273.65 0.0000 356.01 38.7010 610.33 23.4341 276.40 50.6633 388.16 40.6604 614.28 14.4146 277.37 42.2685 388.63 0.0000 618.01 23.5442 277.60 42.2803 391.69 33.5388 620.36 24.6490 278.00 45.9263 264.66 43.8584 621. 93 14.1598 279.20 58.0957 401.81 49.3912 630.19 0.0000 279.54 61.7516 402.40 43.9258 631.29 11. 3271 279.70 61. 7640 404.85 37.6009 633.25 18.3606 280.46 55.7593 410.95 40.5670 634.78 0.0000 283.69 55.9741 413.71 35.1186 635.95 12.9810 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 47.5527 423. 72 0.0000 645.85 19.5850 285.90 0.0000 427.09 48.6051 657.76 23.0081 287.50 63.5591 427.87 40.2189 657.90 0.0000 290.67 45.8008 433.94 35. 7216 661.66 27.4516 293.27 0.0000 439.40 31.1604 664.57 0.0000 351. 93 25.8982 453.88 43.9448 666.33 *o.oooo 295. 96 25.9200 463.37 35. 6119 666.50 0.0000 879.38 25.9975 468.07 30.4291 667.71 0.0000 299.98 26.0385 473.00 0.0000 677.62 19.9446 300.09 26.0417 475.06 27.1939 685.70 0.0000 300.13 26.0430 476.78 32.0916 695.00 0.0000 301.36 26.0789 477.60 29.1925 696.49 19.0337 302.85 26.1225 482.18 33.6879 696.51 19.0344 256.23 26.1705 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 15.6822 306.78 26.2372 497.08 31.5951 697.49 15.6833 308.46 37.5513 505.52 28.3127 702.65 17.9746 311.90 46.0694 507.63 0.0000 706.68 21.3912 316.51 49.6672 511. 00 27.9259 711. 68 24.8359 319.41 0.0000 514.00 27.9852 720.70 0.0000 320.08 0.0000 514.00 27.9863 721. 93 0.0000 321.04 42. 2963 520.40 21.0846 722.78 23.8472 323.87 54.9809 520.69 0.0000 722.91 23.8489 325.23 42.0597 522.65 0.0000 723.31 18.7424 328.76 0.0000 527.90 0.0000 724.19 25.5698 333.37 50.1306 528.26 28.2689 727. 33 13.6597 333.97 46.3030 529.59 27.2834 733.00 13.7007 334.37 43.7482 529.87 0.0000 735.93 13.7212 338.28 44.7859 531. 02 0.0000 333.97 19.4543 338.32 44.7869 537.26 0.0000 739.50 0.0000 311. 90 42.7274 546.56 0.0000 747.24 23.0029 340.48 42.7274 552.55 22.5819 748.06 20.7114 340.55 0.0000 563.25 22.7430 752.31 19.6037 344.28 45.7521 569.33 29.0618 753.82 0.0000 345.93 45.1329 946.00 21.7981 756.73 13.8691 351.06 34.8950 569.70 23.8778 756.80 13.8696 351.93 34.9251 583.19 31.4172 884.68 24.3599 Page 3096 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 26.7042 1274.44 10.6156 1620.50 2.8216 766.42 25.5512 1001.03 12.5695 1621. 92 3.7635 766.84 29.0415 1002.74 9.6753 1678.03 0.0000 772.60 0.0000 1004.73 14.5244 1690.97 1.9146 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025 .. 87 0.0000 1764.49 1.9488 778.90 22.7889 1028.54 0.0000 1063.66 16.5883 783.70 0.0000 1037.84 11.7700 1771. 35 6.8322 785.37 14.0688 1038.76 0.0000 1791.20 0.0000 792.07 12.7037 631.29 14.7620 1808.65 0.9846 794.95 16.9617 1048.07 0.0000 1810.72 0.0000 795.86 14.1411 1049.04 13.7906 1836.06 6.9354 810.06 14.2383 1050.41 14.7830 810.29 12.4598 1063.66 12.8762 344.28 12. 4611 1077.00 0.0000 810.76 10.6824 1077.34 15.9287 815.77 0.0000 1085.87 4.9936 1048.07 0.0000 1093.63 10.0153 832.01 l8.8826 1099.45 9.0330 834.85 19.8079 1112. 07 10.0830 835.71 19.8160 1112.84 16.1367 836.80 0.0000 1115. 54 20.9980 846.75 0.0000 1120.29 17.1909 846.77' 14.4854 1120. 55 17.1930 856.80 0.0000 1221.41 17.8041 860.56 15.4882 112 9. 67 16.2344 871. 09 13. 7311 1131. 51 0.0000 873.19 11. 9114 1147.95 0.0000 875.33 0.0000 1173.23 11.3323 879.38 14.7007 1177.95 16.5098 880.51 10 .1118 1189.05 17.9533 883.24 15.6465 1204.77 13.5364 884.68 21.1821 1221.41 13 .. 6118 889.28 15.6880 1231. 02 24.1595 894.76 13.8757 1235.36 0.0000 898.04 10.1903 1238.28 20.0054 900.72 15.7668 1260.41 0.0000 903.28 15.7845 1271.87 8.5151 911.20 18.6334 1274.44 11. 7177 912.08 18.6407 1274.54 11. 7184 923.98 0.0000 1291.59 10.2820 926.50 15.0049 1298.22 0.0000 929 .11 10.5150 1312 .11 0.0000 937.49 9.0448 1332.49 8.6777 944 .13 0.0000 1362.66 0.0000 946.00 12.2918 1365.19 6.5731 949.00 16.0937 1368.63 0.0000 667.71 0.0000 1384.29 8.8140 962.31 23.7976 1408.01 4.4377 964.08 15.2417 1457.56 0.0000 966.17 9.1529 1460.82 4.5054 911.20 18.1355 1489.16 1.8164 968. 97 18.1355 1505.03 7.2977 983.53 0.0000 1584.12 15.8387 984.45 0.0000 1596.21 0.0000 Page 3097 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:09:40.98 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : Z-OCT-2016 11:01:35. Sample date 10-DEC-2015 10:35:00 Acquisition date : 3-0CT-2016 08:06:48. Sample ID G405235010 Sample quantity l.41695E+02 GRAM Detector name : GAM28 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.44 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 1 1 0 7 7 0 0 3 3 0 0 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 7 Page 3098 of 5809 Energy 74.87* 77.34 88.10 90.12 92.81* 186.51* 209.46 238.84* 241. 88 270.52 281.98 295.46 328.59 338.71 352.30* 381.75 415.85 418.05 498.95 511. 08* 537.63* 583.55* 609.92* 662.07* 690.92 728. 43 777.17 862.69 880.77 889.35 911. 66* 925.88 957.60 965. 52 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 115 233 29 71 86 91 55 415 91 68 26 172 25 102 263 10 24 23 10 39 33 167 157 109 10 39 22 35 17 7 98 12 8 23 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 142 145 281 89 163 164 98 101 87 98 149 108 46 61 80 34 11 25 12 53 67 20 47 35 32 58 18 26 9 15 12 15 29 16 1. 22 1.23 1. 27 1.17 1. 45 1. 65 2.05 1. 41 1. 80 1. 57 3.65 1. 52 1.14 1. 70 1. 49 0.78 1. 67 1. 67 1. 39 1. 24 7.89 1. 75 1. 67 1. 71 0.91 1. 37 1. 40 1. 64 0.82 0.72 2.04 5.21 4.25 2.53 149.82 154.78 176.31 180.35 185.73 373.28 419.22 478.01 484 .11 541.41 564.35 591.33 657.65 677.90 705.10 7 64. 04 832.30 836.70 998.62 1022.90 1076.05 1167. 95 1220. 72 1325.10 1382.84 1457.91 1555.47 1726.64 1762.82 1780.00 1824.66 1853.11 1916.61 1932.45 145 145 169 178 178 368 415 473 473 534 552 584 654 672 698 759 829 829 994 1016 1063 1160 1215 1318 1371 1450 1549 1718 1756 1771 1819 1843 1903 1928 15 3.21E-02 20.5 2.90E+00 15 6. 47E-02 11.1 10 7.99E-03111.2 12 1.98E-02 22.9 1.05E+OO 12 2. 39E-02 31. 4 12 2. 51E-02 31. 2 9 1. 53E-02 35. 2 16 1.15E-01 6.5 2.08E+OO 16 2.52E-02 23.8 14 1. 88E-02 33. 4 17 7.25E-03110.1 14 4.77E-02 15.0 7 6.97E-03 48.9 11 2.82E-02 17.9 14 7.32E-02 9.6 7 2.68E-03106.2 13 6.54E-03 31.0 l.76E+OO 13 6.48E-03 46.0 7 2.86E-03 64.0 14 1.08E-02 50.2 23 9.llE-03 68.2 16 4.65E-02 9.9 12 4.36E-02 12.0 13 3.04E-02 15.1 13 2.82E-03119.5 16 1. 09E-02 45. 6 14 6.12E-03 45.6 18 9.81E-03 38.3 12 4.72E-03 42.8 10 1. 94E-03110. 2 12 2.73E-02 12.5 16 3.23E-03 82.0 15 2.29E-03148.6 18 6.35E-03 39.3 2.09E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235010 Acquisition date 3-0CT-2016 08:06:48 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 7 969.75 30 25 2.06 1940.92 1928 18 8.40E-03 36.3 36 0 1120.99* 47 6 2.03 2243.64 2237 11 1.30E-02 18.1 37 0 1227.79 6 16 3.42 2457.39 2446 13 1.67E-03143.6 38 0 1331.39 15 0 1. 06 2664.73 2659 12 4.17E-03 25.8 39 0 1362.03 9 7 2.99 2726.06 2721 11 2.57E-03 60.3 40 0 1461.82* 402 15 2.22 2925.80 2918 15 1. 12E-01 5.4 Flag: "*" = Peak area was modified by background subtraction Page 3099 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:09:43 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 10-DEC-2015 10:35:00 G405235010 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:06:48 141.70 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit .SOLID GAMMA28 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3100 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.44 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235010 Acquisition date 3-0CT-2016 08:06:48 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.237E+OO 1.548E+Ol 1.548E+Ol 10.88 OK SC-46 889.28 99.98* 1. 841E+OO 2.023E-02 2.379E-01 220.39 OK 1120.55 99.99 1. 539E+OO 1.584E-01 1.862E+OO 36. 29 OK BA-137M 661.66 89.90* 2.305E+OO 2.882E-01 2.937E-01 30.20 OK CS-137 661. 66 85.10* 2.305E+OO 3.045E-01 3.103E-01 30.20 OK TL-208 277.37 6.60 4.566E+OO Line Not Found Absent 583.19 85.00* 2.540E+OO 4.280E-01 4.280E-01 19.83 OK 860.56 12.50 1.888E+OO Line Not Found Absent PB-212 74.82 10.28 4.348E+OO 9.762E-01 9.762E-01 73.52 OK 77 .11 17.10 4.595E+OO l.922E+OO 1.922E+OO 22.12 OK 238.63 43.60* 5.102E+OO 1. llOE+OO 1.llOE+OO 13.00 OK 300.09 3.30 4.295E+00 Line Not Found Absent BI-214 609.32 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 OK 1120. 29 14.92 1.539E+OO 1. 061E+OO 1.062E+OO 36. 29 OK 1764.49 15.30 1.045E+OO Line Not Found Absent PB-214 74.82 5.80 4.343E+OO Line Not Found <<INT Reject 77 .11 9.70 4.595E+OO 3.388E+OO 3.389E+OO 22.12 OK 87.09 3.41 5.480E+OO 9.889E-01 9.893E-01 222.31 OK 242.00 7.25 5.054E+OO Line Not Found -----<<INT Reject 295.22 18.42 4.348E+OO 1.253E+OO 1.253E+OO 29.93 OK 351.93 35.60* 3.782E+OO 1.127E+OO l.128E+OO 19.25 OK RN-222 609.32 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 OK 1120.29 14.92 1.539E+00 1.061E+OO 1. 062E+OO 36.29 OK 1764.49 15.30 1.045E+OO Line Not Found Absent RA-224 240.99 4.10* 5.056E+OO 3.884E-01 3.884E-01 361.47 OK RA-226 609.32 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 OK 1120.29 14.92 1.539E+OO 1. 061E+OO 1.062E+OO 36.29 OK 1764.49 15.30 1.045E+OO Line Not Found Absent AC-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.903E+OO l.334E+OO 1.334E+OO 35.71 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835.71 1. 61 l.930E+00 Line Not Found Absent 911.20 25.80* 1.806E+OO 1.118E+OO 1.118E+OO 25.05 OK 968. 97 15.80 1. 723E+OO 5.862E-01 5.862E-01 72. 56 OK RA-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.903E+OO 1.334E+OO 1.334E+OO 35. 71 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835. 71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 1.118E+OO 1.118E+OO 25.05 OK 968.97 15.80 1.723E+OO 5.862E-01 5.862E-01 72. 56 OK TH-228 74.82 10.28 4.348E+OO 9.762E-01 9.762E-01 73.52 OK 77 .11 17.10 4.595E+OO 1.922E+OO 1.922E+OO 22.12 OK 238.63 43.60* 5.102E+OO 1.llOE+OO 1. llOE+OO 13.00 OK 300.09 3.30 4.295E+OO Line Not Found Absent TH-230 609.32 45.49* 2.455E+OO 7.735E-01 7.735E-01 24.04 OK 1120.29 14.92 1.539E+OO 1. 061E+OO 1.061E+OO 36.29 OK 1764.49 15.30 1.045E+OO Line Not Found Absent TH-232 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.903E+OO 1.334E+OO 1.334E+OO 35.71 OK Page 3101of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235010 Acquisition date 3-0CT-2016 08:06:48 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 835.71 1. 61 1. 930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 1.118E+OO 1.118E+OO 25.05 OK 968. 97 15.80 1. 723E+OO 5.862E-01 5.862E-01 72.56 OK U-234 609.32 45.49* 2.455E+OO 7.735E-01 7.735E-01 24.04 OK 1120.29 14.92 1. 539E+OO 1.061E+OO 1.061E+OO 36.29 OK 1764.49 15.30 1.045E+OO Line Not Found Absent U-235 89. 96 3.47 5.613E+OO 2.346E+OO 2.346E+OO 45.73 OK 93.35 5.60 5.774E+OO 1.699E+OO 1.699E+OO 62.79 OK 143.76 10. 96* 6.593E+OO Line Not Found Absent 163.33 5.08 6.352E+00 Line Not Found Absent 185.72 57.20 5.972E+OO 1.607E-01 1.607E-01 62.42 OK 205.31 5.01 5.647E+OO Line Not Found Absent AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.348E+OO 1.493E-01 1.493E-01 73.52 OK ANH-511 511. 00 100.00* 2.815E+OO 7.735E-02 7.735E-02 100.37 OK Flag: "*" = Keyline Page 3102 of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:09:45.53 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l *
  • Acquisition date 3-0CT-2016 08:06:48 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.44 Half life ratio : ***** *
  • Sample date 10-DEC-2015 10:35:00 Analyst initials: MXRl *
  • Sample ID G405235010 Sample Quantity 1.4170E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN * *'Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 548E+Ol 1.651E+OO SC-46 2.379E-01 5.138E-01 BA-137M 2.937E-01 8.693E-02 CS-137 3.103E-01 9.183E-02 TL-208 4.280E-01 8.316E-02 PB-212 1. llOE+OO 1.414E-01 BI-214 7.738E-01 l.823E-01 PB-214 1.128E+OO 2.127E-01 RN-222 7.738E-01 1.823E-01 RA-224 3.884E-01 1. 376E+OO RA-226 7.738E-01 1.823E-01 AC-228 1.118E+OO 2.745E-01 RA-228 1.118E+OO 2.745E-01 TH-228 1. llOE+OO 1.414E-01 TH-230 7.735E-01 l.822E-01 TH-232 l .118E+OO 2.745E-01 U-234 7.735E-01 1.822E-01 U-235 5.665E-02 2.136E-01 AM-243 l.493E-01 1.076E-01 ANH-511 7.735E-02 7.608E-02 Non-Identified Nuqlides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3103 of 5809 Key-Line Activity (pCi/GRAM 1.688E+OO 2.246E-02 O.OOOE+OO -2.222E-02 O.OOOE+OO 0.000E+OO 5.688E-03 8.791E-02 O.OOOE+OO l.294E-02 K.L. Cnt Uncert (1.96-sigma) 1.184E+Ol 4.683E-02 1. 960E+41 2.865E-02 l.431E+04 4.367E+02 6.780E-02 4.665E-01 1. 960E+41 5.206E-02 MDA (pCi/GRAM 7.790E-01 5.677E-01 6.608E-02 6.981E-02 5.872E-02 9. 957E-0'2 1.343E-01 1.199E-01 1.343E-01 1.067E+OO l.343E-01 l.944E-01 1.944E-01 9.957E-02 1.343E-01 l.944E-01 1.343E-01 3.889E-01 1.007E-01 5.153E-02 MDA (pCi/GRAM 2.292E+Ol 9.887E-02 O.OOOE+OO 4. 911E-02 O.OOOE+OO O.OOOE+ciO 1.345E-01 9. 481E-01 O.OOOE+OO 9.583E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 -2.229E-01 6.006E-01 1.133E+OO NOT IDENT. FE-59 -4 .196E+OO 7.282E+OO 1.292E+Ol NOT IDENT. C0-60 6.396E-02 3.237E-02 8.164E-02 FAIL ABUN ZN-65 5.230E-02 2.045E-01 3.667E-01 NOT IDENT. GE-68 -4.752E-01 2.518E+OO 4.891E+OO NOT IDENT. AS-73 2.390E+OO 9.590E+OO 1.832E+Ol NOT IDENT. AS-74 0.000E+OO 6.002E+03 0.000E+OO SHORT HLIF SE-75 -8.366E-02 2.154E-01 3.575E-01 NOT IDENT. BR-77 0.000E+OO 1.448E+37 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 1.191E+03 0.000E+OO SHORT HLIF RB-83 -3.177E-02 6.447E-01 1.215E+OO NOT IDENT. KR-85 8.201E+OO 8.453E+OO l.599E+Ol NOT IDENT. SR-85 8.474E-01 8.751E-01 l.655E+OO NOT IDENT. RB-86 0.000E+OO 2.899E+04 O.OOOE+OO SHORT HLIF Y-88 4.586E-02 2.072E-01 4.784E-01 NOT IDENT. Y-91 -3.295E+Ol 5.892E+02 1.118E+03 NOT IDENT. NB-94 2.235E-02 3.464E-02 6.927E-02 NOT IDENT. NB-95 -2.932E-01 8.910E-01 1.686E+OO NOT IDENT. NB-95M 2.382E+OO 2.519E+OO 4.765E+OO NOT IDENT. ZR-95 l.093E+OO 1. 411E+OO 3. 071E+OO NOT IDENT. NB-97 O.OOOE+OO l.511E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 8.353E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.083E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.385E-02 3.724E-02 6.332E-02 NOT IDENT. RH-102 -4.469E-02 6 .196E-02 1.034E-01 NOT IDENT. RU-103 3.193E+OO 4.627E+OO 9.254E+OO FAIL ABUN RH-106 -4.160E-01 5.095E-01 8:365E-01 NOT IDENT. RU-106 -4.160E-01 5.095E-01 8.365E-01 NOT IDENT. AG-108M 6.887E-03 2.765E-02 5.420E-02 NOT IDENT. CD-109 1.426E+OO 3.106E+OO 2.659E+00 FAIL ABUN AG-110M 7.324E-03 l.277E-01 1. 711E-01 NOT IDENT. SN-113 -1. 797E-01 2.263E-01 3.929E-01 NOT IDENT. CD-115 O.OOOE+OO l.853E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.019E+05 O.OOOE+OO SHORT HLIF TE-123M 3.932E-02 1.466E-01 2.659E-01 NOT IDENT. SB-124 2.091E-01 1. 723E+OO 3.804E+OO NOT IDENT. SB-125 7.877E-02 1. 031E-01 2.129E-01 NOT IDENT. TE-125M 4 .114E+Ol 2.824E+02 5.199E+02 NOT IDENT. I-126 O.OOOE+OO 8.109E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8.774E+05 O.OOOE+OO SHORT HLIF SN-126 9 .114E-02 1.986E-01 1.810E-01 FAIL ABUN SB-127 O.OOOE+OO 1. 7 93E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.261E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.678E+26 O.OOOE+OO SHORT HLIF BA-133 -2.253E-02 4.414E-02 7.019E-02 NOT IDENT. I-133 0.000E+OO 1.188E+41 O.OOOE+OO SHORT HLIF CS-134 3.080E-02 5.427E-02 l.132E-01 NOT IDENT. CS-135 6.612E-02 l.343E-01 2.702E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.768E+05 O.OOOE+OO SHORT HLIF CE-139 -1.225E-01 1.030E-01 l.856E-01 NOT IDENT. BA-140 O.OOOE+OO 3.992E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4. 611E+05 0.000E+OO SHORT HLIF CE-141 -2.890E+Ol 2.759E+Ol 4.480E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.293E-01 4.016E-01 6.848E-01 NOT IDENT. PM-144 1. 911E-02 5.353E-02 1.055E-01 NOT IDENT. PR-144 1.643E+OO 4.643E+OO 9 .151E+OO NOT IDENT. PM-146 7.738E-04 4.315E-02 8.231E-02 NOT IDENT. ND-147 O.OOOE+OO 3.238E+07 O.OOOE+OO SHORT HLIF PM-147 1.114E+02 8.989E+02 l.640E+03 NOT IDENT. PM-149 O.OOOE+OO 2.644E+40 O.OOOE+OO SHORT HLIF EU-150 1.735E-02 2.584E-02 4.861E-02 FAIL ABUN EU-152 -l.553E-02 8.440E-02 1.597E-01 FAIL ABUN GD-153 -l.236E-01 1.838E-01 3.185E-01 NOT IDENT. EU-154 4.809E-02 1.135E-01 2.383E-01 NOT IDENT. EU-155 9.599E-02 l.155E-01 2.241E-01 NOT IDENT. TB-160 2. 821E+OO 2.367E+OO 3.319E+OO FAIL ABUN H0-166M -l.197E-02 6.195E-02 1.114E-01 NOT IDENT. TM-171 -1.198E+OO 2.291E+Ol 4.280E+Ol NOT IDENT. HF-172 -1.589E-01 2.482E-01 4.226E-01 NOT IDENT. LU-172 -4.140E-02 7.390E-02 1.322E-01 FAIL ABUN LU-176 -2.567E-03 2.640E-02 4.999E-02 FAIL ABUN HF-181 6.322E-01 4.423E+OO 8.501E+OO NOT IDENT. TA-182 -3.562E-01 1.000E+OO 1.565E+OO FAIL ABUN RE-183 -6.587E-01 3 .101E+OO 5.754E+OO NOT IDENT. Page 3104of5809 RE-184 1.787E+Ol 3.187E+Ol 6.685E+Ol NOT IDENT. W-188 4.322E+Ol 1.161E+o2 2 .112E+02 NOT IDENT. IR-192 -2.023E-01 4.750E-01 8.734E-01 FAIL ABUN HG-203 2.180E+OO 2.401E+OO 4.943E+OO NOT IDENT. BI-207 3.199E-02 4.675E-02 l.016E-01 FAIL ABUN PB-210 3.202E-01 3. 896E+OO 7.399E+OO NOT IDENT. BI-211 O.OOOE+OO 5.860E-01 8.039E-01 FAIL ABUN PB-211 3.286E-01 6.805E-01 1.358E+OO NOT IDENT. BI-212 l.489E+OO 1.330E+OO 1.516E+OO FAIL ABUN RN-219 5.262E-02 3. 531E-01 6.889E-01 FAIL ABUN RA-223 5.300E-01 6.662E-01 l.304E+OO FAIL ABUN AC-227 -8.847E-02 2.256E-01 4.217E-01 NOT IDENT. TH-227 -8.847E-02 2.256E-01 4.217E-01 NOT IDENT. TH-229 -2.527E-01 4.570E-01 8.562E-01 FAIL ABUN PA-231 l.510E-02 5.457E-01 9.892E-01 NOT IDENT. TH-231 5.300E-01 6.662E-01 l.304E+OO FAIL ABUN PA-233 -2.707E-02 5.936E-02 1.091E-01 NOT IDENT. PA-234 2.153E-02 3.000E-01 5.934E-01 FAIL ABUN PA-234M -1.253E+OO 4.256E+OO 8.510E+OO NOT IDENT. TH-234 -2.636E-01 1.457E+OO 2.692E+OO FAIL ABUN NP-237 -2.707E-02 5.936E-02 1. 091E-01 NOT IDENT. NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF U-238 -2.636E-01 l.457E+OO 2.692E+OO FAIL ABUN NP-239 -1. 749E-01 2. 651E-01 4.527E-01 NOT IDENT. PU-239 2.404E+02 3.353E+02 6.365E+02 NOT IDENT. AM-241 -9.236E-02 1.471E-01 2.629E-01 NOT IDENT. CM-243 -l.132E-01 1.092E-01 1.817E-01 NOT IDENT. BK-247 8. 431E-03 7.088E-02 1.261E-01 NOT IDENT. CM-247 -2. 331E-02 3.432E-02 6.035E-02 NOT IDENT. CF-249 l.601E-02 3.725E-02 7.428E-02 NOT IDENT. CF-251 5.780E-02 1.161E-01 2.343E-01 NOT IDENT. Page 3105of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:09:42.03 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 385 10.66* l.237E+OO 1.548E+Ol l.548E+Ol 10.88 SC-46 889.28 7 99.98* 1.841E+OO 2.023E-02 2.379E-01 220.39 1120.55 46 99.99 1.539E+OO 1.584E-01 1.862E+OO 36.29 CD-109 88.03 35 3.70* 5.480E+OO 9 .114E-01 1.426E+OO 222.31 SN-126 64.28 ------9.60 3.124E+OO ------Line Not Found ------86.94 35 8.90 5.480E+OO 3.789E-01 3.789E-01 222.31 87.57 35 37.00* 5.480E+OO 9 .114E-02 9 .114E-02 222.31 BA-137M 661.66 113 89.90* 2.305E+OO 2.882E-01 2.937E-01 30.20 CS-137 661. 66 113 85.10* 2.305E+00 3.045E-01 3.103E-01 30.20 TL-208 277.37 ------6.60 4.566E+OO ------Line Not Found ------583.19 174 85.00* 2.540E+00 4.280E-01 4.280E-01 19.83 860.56 ------12.50 1.888E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 4.138E+OO ------Line Not Found ------351. 06 287 12.92* 3.782E+00 3.107E+00 3.107E+OO 19.25 PB-212 74.82 142 10.28 4.348E+OO 1. 679E+OO 1.679E+OO 40.90 77 .11 285 17'.10 4.595E+OO 1.922E+OO 1.922E+OO 22.12 238.63 466 43.60* 5.102E+00 1. llOE+OO 1. llOE+OO 13. 00 300.09 ------3.30 4.295E+OO ------Line Not Found ------BI-214 609.32 163 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 1120.29 46 14.92 l.539E+OO 1.061E+OO l.062E+OO 36.29 1764.49 ------15.30 1.045E+OO ------Line Not Found ------PB-214 74.82 142 5.80 4.348E+OO 2.976E+OO 2.977E+OO 40.90 77 .11 285 9.70 4.595E+OO 3.388E+OO 3.389E+00 22.12 87.09 35 3.41 5.480E+OO 9.889E-01 9.893E-01 222.31 242.00 102 7.25 5.056E+OO 1.472E+OO 1.473E+OO 47.53 295.22 189 18.42 4.348E+OO l.253E+00 1.253E+OO 29.93 351.93 287 35.60* 3.782E+OO l.127E+OO l.128E+OO 19.25 RN-222 609.32 163 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 1120.29 46 14.92 1.539E+OO l.061E+OO 1.062E+OO 36.29 1764.49 ------15.30 l.045E+OO ------Line Not Found ------RA-224 240.99 102 4.10* 5.056E+OO 2.604E+OO 2.604E+OO 47.53 RA-226 609.32 163 45.49* 2.455E+OO 7.735E-01 7.738E-01 24.04 1120.29 46 14.92 l.539E+OO 1. 061E+OO 1.062E+OO 36.29 1764.49 ------15.30 l.045E+OO ------Line Not Found ------AC-228 105.21 ------1.10 6.315E+00 ------Line Not Found ------338.32 111 11. 27 3.903E+OO 1.334E+OO 1.334E+OO 35.71 794.95 ------4.25 2.005E+OO ------Line Not Found ------835. 71 ------1. 61 l.930E+OO ------Line Not Found ------911. 20 98 25.80* 1.806E+OO l .118E+OO 1.118E+OO 25.05 968. 97 30 15.80 1. 723E+OO 5.862E-01 5.862E-01 72. 56 RA-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 111 11.27 3.903E+OO l.334E+OO 1.334E+OO 35.71 794.95 ------4.25 2.005E+OO ------Line Not Found ------835. 71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 98 25.80* 1.806E+OO l .118E+00 1.118E+OO 25.05 968. 97 30 15.80 1. 723E+OO 5.862E-01 5.862E-01 72. 56 TH-228 74.82 142 10.28 4.348E+OO 1. 679E+OO 1.679E+OO 40.90 Page 3106 of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235010 Acquisition date 3-0CT-2016 08:06:48 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 285 17.10 .4. 595E+OO l.922E+OO 1.922E+OO 22.12 238.63 466 43.60* 5.102E+OO 1. llOE+OO l. llOE+OO 13.00 300.09 ------3.30 4.295E+OO ------Line Not Found ------TH-230 609.32 163 45.49* 2.455E+OO 7.735E-01 7.735E-01 24.04 1120.29 46 14.92 1.539E+OO 1. 061E+OO 1.061E+OO 36. 29 1764.49 ------15.30 l.045E+OO ------Line Not Found ------TH-232 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 111 11.27 3.903E+OO 1.334E+OO 1.334E+OO 35. 71 835.71 ------1. 61 1. 930E+OO ------Line Not Found ------911. 20 98 25.80* 1.806E+OO l.118E+00 1.118E+OO 25.05 968. 97 30 15.80 1.723E+OO 5. 8 62E-01 5.862E-01 72.56 U-234 609.32 163 45.49* 2.455E+OO 7.735E-01 7.735E-01 24.04 1120.29 46 14.92 l.539E+00 1.061E+OO 1. 061E+OO 36. 29 1764.49 ------15.30 1.045E+OO ------Line Not Found ------U-235 89. 96 86 3.47 5. 613E+OO 2.346E+OO 2.346E+OO 45.73 93.35 104 5.60 5.774E+OO 1.699E+OO 1.699E+OO 62.79 143.76 ------10. 96* 6.593E+OO ------Line Not Found ------163.33 ------5.08 6.352E+OO ------Line Not Found ------185. 72 104 57.20 5. 972E+OO 1.607E-01 1.607E-01 62.42 205.31 ------5.01 5.647E+OO ------Line Not Found ------AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 142 67.20* 4.348E+OO 2.568E-01 2.568E-01 40.90 ANH-511 511. 00 41 100.00* 2.815E+00 7.735E-02 7.735E-02 100.37 Flag: "*" Key line Page 3107of5809 Summary of Nuclide Activity Sample ID : G405235010 Acquisition date Page : 3 3-0CT-2016 08:06:48 Total number of lines in spectrum 40 Number of unidentified lines 8 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211

  • PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Hlife l.25E+09Y 83.79D 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600. OOY 1600.00Y 1. 41E+10Y 1600.00Y l.41E+l0Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 1. 41E+l0Y 2.45E+05Y 7.04E+08Y 7370.00Y l.OOE+09Y Decay 1. 00 11. 8 1. 56 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.548E+Ol 2.023E-02 9.114E-01 9 .114E-02 2.882E-01 3.045E-01 4.280E-01 3.107E+OO l.llOE+OO 7.735E-01 l.127E+OO 7.735E-01 2.604E+OO 7.735E-01 l.118E+OO l .118E+OO 1. llOE+OO 7.735E-01 l .118E+OO 7.735E-01 1.607E-01 2.568E-01 7.735E-02 3.430E+Ol 3.430E+Ol Decay Corr pCi7GRAM 1. 548E+Ol 2.379E-01 1.426E+OO 9 .114E-02 2.937E-01 3.103E-01 4.280E-01 3.107E+OO 1. llOE+OO 7.738E-01 l.128E+00 7.738E-01 2.604E+OO 7.738E-01 1.118E+OO 1.118E+OO 1. llOE+OO 7.735E-01 1.118E+OO 7.735E-01 1.607E-01 2.568E-01 7.735E-02 3.504E+Ol 3.504E+Ol 80.00% Decay Corr 2-Sigma Error 0.169E+Ol 5.243E-01 3.170E+OO 20.26E-02 0.887E-01 0.937E-01 0.849E-01 0.598E+OO 0.144E+OO 1.860E-01 0.217E+OO l.860E-01 1.237E+OO l.860E-01 0.280E+OO 0.280E+00 0.144E+OO 1.860E-01 0.280E+00 1. 8 60E-01 1.003E-01 1. 051E-01 7.764E-02 "M" Manually accepted 2-Sigma %Error 10.88 220.39 222.31 222.31 30.20 30.20 19.83 19.25 13. 00 24.04 19.25 24.04 47.53 24.04 25.05 25.05 13.00 24.04 25.05 24.04 62.42 40.90 100.37 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3108 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235010 Acquisition date : 3-0CT-2016 08:06:48 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.46 62 111 2.05 419.22 415 9 1.53E-02 70.4 5.58E+OO T 0 270.52 75 109 1. 57 541.41 534 14 1.88E-02 66.7 4.65E+OO T 0 281. 98 29 165 3.65 564.35 552 17 7.25E-03 **** 4. 51E+OO 0 328.59 27 50 1.14 657.65 654 7 6.97E-03 97.8 4.00E+OO T 0 381. 75 10 37 0.78 764.04 759 7 2.68E-03 **** 3.55E+OO 1 415.85 25 12 1. 67 832.30 829 13 6.54E-03 62.0 3.31E+OO T 1 418.05 25 27 1. 67 836.70 829 13 6.48E-03 92.0 3.30E+OO 0 498.95 11 12 1. 39 998.62 994 7 2.86E-03 **** 2.87E+OO 0 537.63 34 70 7.89 1076.05 1063 23 9.llE-03 **** 2. 71E+OO T 0 690.92 10 33 0.91 1382.84 1371 13 2.82E-03 **** 2.23E+OO 0 728.43 40 59 1. 37 1457.91 1450 16 l.09E-02 91.2 2.14E+OO T 0 777.17 22 18 1. 40 1555.47 1549 14 6.12E-03 91.3 2.04E+OO T 0 862.69 36 26 1. 64 1726.64 1718 18 9.81E-03 76.5 1.88E+OO 0 880.77 17 9 0.82 1762.82 1756 12 4.72E-03 85.6 1. 85E+OO T 0 925.88 12 15 5.21 1853.11 1843 16 3.23E-03 **** 1. 79E+OO T 0 957.60 8 29 4.25 1916.61 1903 15 2.29E-03 **** l.74E+00 7 965. 52 23 16 2.53 1932.45 1928 18 6.35E-03 78.6 l.73E+OO T 0 1227.79 6 16. 3.42 2457.39 2446 13 l.67E-03 **** 1.43E+OO 0 1331.39 15 0 1. 06 2664.73 2659 12 4.17E-03 51.6 1. 34E+OO T 0 1362.03 9 7 2.99 2726.06 2721 11 2.57E-03 **** 1.31E+OO T Flags: "T" = Tentatively Page 3109of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:09:59.02 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l *
  • Acquisition date 3-0CT-2016 08:06:48 Sensitivity 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.44 Half life ratio : ***** *
  • Sample date 10-DEC-2015 10:35:00 Nuclide Library : SOLID *
  • Sample ID G405235010 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4170E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO '* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 3.350E-01 2.374E-01 2.945E-02 3. lllE-02 2.597E-02 4.645E-02 6.062E-02 5.448E-02 6.062E-02 4.978E-01 6.062E-02 8.161E-02 8.161E-02 4.645E-02 6.060E-02 8.161E-02 6.060E-02 1.841E-01 4.776E-02 2.316E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 3110of5809 Le (pCi/GRAM l.031E+Ol 4.298E-02 O.OOOE+OO l.752E-02 O.OOOE+OO O.OOOE+OO 5.997E-02 4.189E-01 O.OOOE+OO 4.508E-02 4.980E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 . RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 3111 of 5809 5.610E+OO 3.483E-02 1.618E-01 2.142E+OO 8.583E+OO O.OOOE+OO 1.638E-01 O.OOOE+OO O.OOOE+OO 5.428E-01 7.361E+OO 7.618E-01 0.000E+OO 1.895E-01 4.940E+02 3 .132E-02 7.544E-Ol 2.236E+OO 1. 37 4E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 969E-02 4.534E-02 4.087E+OO 3. 651E-01 3 .'651E-01 2.456E-02 1.271E+OO 7.322E-02 1.768E-01 O.OOOE+OO 0.000E+OO 1.251E-01 1.474E+OO 9.710E-02 2.441E+02 O.OOOE+OO O.OOOE+OO 8.675E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.175E-02 0.000E+OO 5.102E-02 1.252E-01 O.OOOE+OO O.OOOE+OO 8.616E-02 O.OOOE+OO O.OOOE+OO 2.105E+Ol O.OOOE+OO 3.214E-01 4.693E-02 4.069E+OO 3.710E-02 O.OOOE+OO 7.706E+02 0.000E+OO 2.232E-02 7.233E-02 l.490E-01 1.033E-01 1.057E-01 1.434E+OO 4.950E-02 1.998E+01 1.977E-01 5.621E-02 2.312E-02 3.846E+OO 6.694E-01 2.692E+OO 2.985E+Ol NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 . RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3112 of 5809 9.753E+Ol 4. OllE-01 2.303E+OO 4.464E-02 3.470E+OO 3.870E-01 6.215E-01 7.072E-01 3. ll 7E-01 6.062E-01 1. 94 7E-01 1. 947E-01 3.992E-01 4.623E-01 6.062E-01 4.992E-02 2.623E-01 3.742E+OO 1.277E+OO 4.992E-02 O.OOOE+OO 1.277E+OO 2 .119E-01 3.004E+02 1. 229E-01 8.493E-02 5.780E-02 2.716E-02 3.394E-02 1.lOlE-01 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:10:04.79 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235010.CNF;l * *Acquisition date 3-0CT-2016 08:06:48 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.44 Half life ratio : ***** *
  • Sample date 10-DEC-2015 10:35:00 Nuclide Library : SOLID *
  • Sample ID G405235010 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.4170E+02 GRAM *
  • Quantity Err(%) : 1.4115E-03 % * *Wet wt corr 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * * '* Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.548E+Ol 1.840E+OO SC-46 2.379E-01 5.139E-01 BA-137M 2.937E-01 8.786E-02 CS-137 3.103E-01 9.281E-02 TL-208 4.280E-01 8.516E-02 PB-212 1. llOE+OO 1.533E-01 BI-214 7.738E-01 l.854E-01 PB-214 l.128E+OO 2.179E-01 RN-222 7.738E-01 1.854E-01 RA-224 3.884E-01 1.384E+OO RA-226 7.738E-01 1.854E-01 AC-228 1.118E+OO 2.804E-01 RA-228 l .118E+OO 2.804E-01 TH-228 1. llOE+OO 1.533E-01 TH-230 7.735E-01 l.853E-01 TH-232 1.118E+OO 2.804E-01 U-234 7.735E-01 l.853E-01 U-235 5.665E-02 2.136E-01 AM-243 l.494E-01 1.088E-01 ANH-511 7.735E-02 7.615E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3113 of 5809 Key-Line Activity (pCi/GRAM 1. 688E+OO 2.246E-02 -1. OOOE+41 -2.222E-02 l.361E+03 2.139E+02 5.688E-03 8.791E-02 1.000E+41 1.294E-02 K.L Act error ( 1. 96-sigma) l.184E+Ol 4.684E-02 3.866E+41 2.868E-02 l.431E+04 4.368E+02 6.780E-02 4.665E-01 5.403E+41 5.206E-02 TPU ( 1. 96-sigma) 1.840E+OO 5 .139E-01 8.786E-02 9.281E-02 8.516E-02 1.533E-01 l.854E-01 2.179E-01 1.854E-01 1.384E+OO 1.854E-01 2.804E-01 2.804E-01 1.533E-01 l.853E-01 2.804E-01 1.853E-01 2.136E-01 1. 088E-01 7.615E-02 TPU ( 1. 96-sigma) 1.186E+Ol 4.792E-02 O.OOOE+OO 3.038E-02 1.432E+04 4.473E+02 6.785E-02 4.682E-01 O.OOOE+OO 5.239E-02 NOT IDENT.
  • NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 -2.229E-01 6.007E-01 6.091E-01 NOT IDENT. FE-59 -4.196E+OO 7.288E+OO 7.530E+OO NOT IDENT. C0-60 6.396E-02 3.246E-02 4.342E-02 FAIL ABUN ZN-65 5.230E-02 2.045E-01 2.059E-01 NOT IDENT. GE-68 -4.752E-01 2.518E+OO 2.527E+OO NOT IDENT. AS-73 2.390E+OO 9.602E+OO 9.662E+OO NOT IDENT. AS-74 2 .106E+o3 6.005E+03 6.079E+03 SHORT HLIF SE-75 -8.366E-02 2.154E-01 2.187E-01 NOT IDENT. BR-77 1.137E+38 9.776E+38 O.OOOE+OO SHORT HLIF SR-82 l.331E+03 1.192E+03 1.335E+03 SHORT HLIF RB-83 -3.177E-02 6.447E-01 6.449E-01 NOT IDENT. KR-85 8.201E+OO 8.460E+OO 9.233E+OO NOT IDENT. SR-85 8.474E-01 8.758E-01 9.555E-01 NOT IDENT. RB-86 -l.586E+04 2.900E+04 2.987E+04 SHORT HLIF Y-88 4.586E-02 2.072E-01 2.082E-01 NOT IDENT. Y-91 -3.295E+Ol 5.892E+02 5.894E+02 NOT IDENT. NB-94 2.235E-02 3.465E-02 3.609E-02 NOT IDENT. NB-95 -2.932E-01 8.910E-01 9.008E-01 NOT IDENT. NB-95M 2.382E+OO 2.526E+OO 2.745E+OO NOT IDENT. ZR-95 1.093E+OO 1.412E+OO 1.495E+OO NOT IDENT. NB-97 1. 000E+41 l.512E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 8.363E+40 O.OOOE+OO SHORT HLIF M0-99 -3.736E+30 1.083E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.363E+42 O.OOOE+OO SHORT HLIF RH-101 -2.385E-02 3.749E-02 3.900E-02 NOT IDENT. RH-102 -4.469E-02 6.207E-02 6.525E-02 NOT IDENT. RU-103 3.193E+00 4.630E+OO 4.848E+OO FAIL ABUN RH-106 -4.160E-01 5.102E-01 5.436E-01 NOT IDENT. RU-106 -4.160E-01 5.102E-01 5.436E-01 NOT IDENT. AG-108M 6.887E-03 2.765E-02 2.782E-02 NOT IDENT. CD-109 1.426E+OO 3.109E+OO 3.174E+OO FAIL ABUN AG-llOM 7.324E-03 1.277E-01 1.278E-01 NOT IDENT. SN-113 -1.797E-01 2.264E-01 2.404E-01 NOT IDENT. CD-115 2.208E+38 l.854E+39 O.OOOE+OO SHORT HLIF SN-117M -6.889E+04 1.022E+05 l.068E+05 SHORT HLIF TE-123M 3.932E-02 1.466E-01 1.477E-01 NOT IDENT. SB-124 2.091E-01 1.723E+OO 1. 725E+OO NOT IDENT. SB-125 7.877E-02 l.031E-01 1.090E-01 NOT IDENT. TE-125M 4 .114E+Ol 2.824E+02 2.830E+02 NOT IDENT. I-126 9. 719E+05 8.215E+05 9.310E+05 SHORT HLIF SB-126 5.345E+05 8.831E+05 9.154E+05 SHORT HLIF SN-126 9 .114E-02 l.986E-01 2.028E-01 FAIL ABUN SB-127 -4.249E+21 l.884E+22 O.OOOE+OO SHORT HLIF I-131 -1.546E+09 4.262E+09 4.318E+09 SHORT HLIF I-132 1.000E+41 1.921E+42 O.OOOE+OO SHORT HLIF TE-132 1.165E+25 2.678E+26 O.OOOE+OO SHORT HLIF BA-133 -2.253E-02 4.415E-02 4.530E-02 NOT IDENT. I-133 -1.000E+41 2.154E+41 O.OOOE+OO SHORT HLIF CS-134 3.080E-02 5.429E-02 5.603E-02 NOT IDENT. CS-135 6.612E-02 1.344E-01 1. 376E-01 NOT IDENT. I-135 l.000E+41 7 .113E+41 O.OOOE+OO SHORT HLIF CS-136 4. 311E+04 2.769E+05 2.775E+05 SHORT HLIF CE-139 -l.225E-01 1.059E-01 l.195E-01 NOT IDENT. BA-140 2.989E+06 3.994E+06 4.215E+06 SHORT HLIF LA-140 -l.434E+05 4. 611E+05 4.656E+05 SHORT HLIF CE-141 -2.890E+Ol 2.762E+Ol 3.054E+Ol NOT IDENT. CE-143 1.000E+41 4.669E+41 O.OOOE+OO SHORT HLIF CE-144 -2.293E-01 4.018E-01 4.149E-01 NOT IDENT. PM-144 1. 911E-02 5.354E-02 5.423E-02 NOT IDENT. PR-144 1.643E+OO 4.643E+OO 4.702E+OO NOT IDENT. PM-146 7.738E-04 4.315E-02 4.315E-02 NOT IDENT. ND-147 -2.366E+06 3.238E+07 3.239E+07 SHORT HLIF PM-147 l .114E+02 8.989E+02 9.003E+02 NOT IDENT. PM-149 6.778E+39 2.648E+40 O.OOOE+OO SHORT HLIF EU-150 l.735E-02 2.585E-02 2.701E-02 FAIL ABUN EU-152 -1.553E-02 8.440E-02 8.469E-02 FAIL ABUN GD-153 -l.236E-01 1.840E-01 l.922E-01 NOT IDENT. EU-154 4.809E-02 l.136E-01 l.156E-01 NOT IDENT. EU-155 9.599E-02 1.157E-01 l.235E-01 NOT IDENT. TB-160 2.821E+00 2.373E+OO 2.693E+OO FAIL ABUN H0-166M -1.197E-02 6 .196E-02 6.219E-02 NOT IDENT. TM-171 -1.198E+OO 2.291E+Ol 2.292E+Ol NOT IDENT. HF-172 -l.589E-01 2.496E-01 2.597E-01 NOT IDENT. LU-172 -4.140E-02 7.402E-02 7.633E-02 FAIL ABUN LU-176 -2.567E-03 2.640E-02 2.643E-02 FAIL ABUN HF-181 6.322E-01 4.424E+OO 4.433E+OO NOT IDENT. TA-182 -3.562E-01 1.000E+OO 1. 013E+OO FAIL ABUN RE-183 -6.587E-01 3.103E+OO 3 .117E+OO NOT IDENT. Page 3114 of 5809 RE-184 1.787E+Ol 3.215E+Ol 3.315E+Ol NOT IDENT. W-188 4.322E+Ol 1.162E+02 1.178E+02 NOT IDENT. IR-192 -2.023E-01 4.751E-01 4.838E-01 FAIL ABUN HG-203 2.180E+00 2.403E+OO 2.597E+OO NOT IDENT. BI-207 3.199E-02 4.677E-02 4.894E-02 FAIL ABUN PB-210 3.202E-01 3.896E+OO 3.898E+OO NOT IDENT. BI-211 3.107E+OO 6.024E-01 1.525E+OO FAIL ABUN PB-211 3.286E-01 6.807E-01 6. 966E-01 NOT IDENT. BI-212 1.489E+OO 1.333E+OO l.492E+OO FAIL ABUN RN-219 5.262E-02 3.532E-01 3.540E-01 FAIL ABUN RA-223 5.300E-01 6.670E-01 7.085E-01 FAIL ABUN AC-227 -8.847E-02 2.259E-01 2.294E-01 NOT IDENT. TH-227 -8.847E-02 2.259E-01 2.294E-01 NOT IDENT. TH-229 -2.527E-01 4.572E-01 4. 712E-01 FAIL ABUN PA-231 l.SlOE-02 5.457E-01 5.458E-01 NOT IDENT. TH-231 5.300E-01 6.670E-01 7.085E-01 FAIL ABUN PA-233 -2.707E-02 5.937E-02 6.062E-02 NOT IDENT. PA-234 2.153E-02 3.0lOE-01 3.012E-01 FAIL ABUN PA-234M -1.253E+OO 4.257E+OO 4.294E+OO NOT IDENT. TH-234 -2.636E-01 1.458E+OO l.463E+OO FAIL ABUN NP-237 -2.707E-02 5.937E-02 6.062E-02 NOT IDENT. NP-238 3.888E+40 2.708E+41 O.OOOE+OO SHORT HLIF U-238 -2.636E-01 1.458E+OO 1.463E+OO FAIL ABUN NP-239 -1. 749E-01 2.655E-01 2.769E-01 NOT IDENT. PU-239 2.404E+02 3.355E+02 3.526E+02 NOT IDENT. AM-241 -9.236E-02 l.473E-01 1.531E-01 NOT IDENT. CM-243 -1.132E-01 1.097E-01 l.210E-01 NOT IDENT. BK-247 8.431E-03 7.090E-02 7.lOOE-02 NOT IDENT. CM-247 -2.331E-02 3.455E-02 3. 611E-02 NOT IDENT. CF-249 1. 601E-02 3.727E-02 3.796E-02 NOT IDENT. CF-251 5.780E-02 1.163E-01 1.192E-01 NOT IDENT. Page 3115 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 54.1856 87.09 145.3838 136.47 79.0660 45.60 74.3617 87.57 145. 4961 140.51 0.0000 46.54 69.2816 88.03 145.6035 143.76 89.5680 49. 72 0.0000 88.34 68.2860 144.24 85.9352 51. 35 67.9370 88.47 68.3002 145.44 110. 6419 51. 87 64.8281 89. 96 112. 5823 152.43 80.5468 52.39 63.8395 1093.63 91.3812 153.25 0.0000 52.97 73.5099 91.11 0.0000 323.87 74.4983 53.44 63.9880 92.59 91.6608 156.02 0.0000 54.07 61.9405 93.35 91. 7 688 158.56 0.0000 57.36 0.0000 94.56 81.2139 159.00 77.3884 57.53 62.4014 94.65 81. 224 7 162.33 82.6783 57.98 75.3828 94.67 81. 2274 162.66 0.0000 59.27 77.7448 94.87 81. 2522 163.33 71. 8994 59.32 85.3120 97.43 83.1077 165.86 82.1522 59.54 85.3506 98.43 84.3884 176.31 71.1835 60. 96 81. 2642 98.44 84.3895 176.60 0.0000 61.17 96.4746 99.53 83.3692' 177.52 69.5737 62.93 96. 8158 100 .11 81.1228 181.07 0.0000 63.29 106.6823 102.03 79.0276 181.52 74.1134 63.58 103.4757 103.18 97.7857 184.41 85.8591 64.28 93.8020 103.37 96.6488 143.76 72. 7105 66.73 105.2073 105.21 70.0518 193.51 75.8461 67.24 116.2796 105.31 70.0616 197.03 74.3699 125.81 107.5942 106.12 79.4950 198.01 65.7826 67.75 107.6077 106.47 87. 7224 201.83 89.4712 69.67 113.5081 109.28 75.1533 203.43 86.9934 70.83 92.7684 111. 00 80.0413 205.31 67. 9723 72.81 115.2734 111. 76 0.0000 210.85 61.7463 72. 87 124.1534 114. 06 68.5577 215.65 65. 9691 74.66 111. 2091 116. 30 0.0000 222.11 53.0750 74.82 111.2404 116.74 88. 9727 227.09 55.0794 74.97 111.2701 119.76 89.3297 227.38 58.6476 77 .11 111. 6913 121.12 77.5574 228.16 0.0000 78.74 112.0079 121.22 77.5674 228.18 66.6901 79.69 92.7446 121. 78 78.8186 116.74 66.6901 80.12 92.8127 122.06 77.6527 235.69 55.0331 80.19 0.0000 122.92 84.9149 235. 96 64.4429 80.57 92.8839 123.07 78.9505 238.63 64.5857 81. 00 92.9514 265.00 79.0125 238.98 0.0000 81. 07 92.9628 125.81 87.6315 240.99 64.7109 81.75 123.0918 127.23 92.5992 242.00 64.7644 83.79 115.9809 127.91 91.4755 244.70 59.4983 84.00 116.0217 129.30 74.7546 252.40 0.0000 85.43 144.9912 131. 20 100.3128 252.80 46.2753 86.55 145.2559 133.02 86.0026 254.15 0.0000 86.79 145.3125 133.52 93.3268 256.23 56.4086 86.94 145.3477 136. 00 81.4518 260.90 0.0000 Page 3116of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY . MDA COUNTS 264.66 48.0791 355.39 0.0000 584.27 19.7366 264.80 49.4583 356.01 39.4964 595.83 0.0000 265.00 38.4735 364.49 0.0000 427.87 28.7083 268.22 44. 0771 366.42 0.0000 602.52 0.0000 269.46 44 .1191 372.51 38.4192 604.72 23.2277 270.03 44.1377 375.0.5 41.4377 607.14 23.2507 271.23 44.1777 377.52 31.1245 609.32 28.8131 273.65 0.0000 356.01 44.6301 610.33 28.8258 276.40 59.1328 388.16 30.8228 614.28 18.3235 277.37 44.3818 388.63 0.0000 618.01 30.0300 277.60 44.3887 391.69 39.8535 620.36 14.4727 278.00 44.4023 264.66 29.0431 621.93 26.7363 279.20 44.4414 401.81 28.0598 630.19 0.0000 279.54 44.4531 402.40 38.0943 631. 29 26.8389 279.70 44.4580 404.85 31.1198 633.25 16.7877 280.46 44.4834 410.95 27.8021 634.78 0.0000 283.69 43.1955 413.71 33.2927 635.95 29.1305 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.4591 423.72 0.0000 645.85 21. 3727 285.90 0.0000 427.09 31. 5064 657.76 11.8672 287.50 45.6434 427.87 24.4023 657.90 0.0000 290.67 36.4117 433.94 27.5427 661. 66 22.6392 293.27 0.0000 439.40 27.6235 664.57 0.0000 351. 93 59. 0112 453.88 27.8350 666.33 0.0000 295. 96 59.0420 463.37 31.0797 666.50 0.0000 879.38 77.4596 468.07 30 .1163 667.71 0.0000 299.98 46.5221 473.00 0.0000 677.62 14.8070 300.09 46.5251 475.06 32.3074 685.70 0.0000 300 .13 49.3459 476.78 23.9906 695.00 0.0000 301.36 67.7329 477.60 25.0439 696. 49 17.2083 302.85 69.6866 482.18 28.2387 696. 51 17.2083 256.23 49.9689 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.2137 306.78 52.8805 497.08 11. 0627 697.49 18.3626 308.46 47 .2697 505.52 14.2817 702.65 20.6982 311. 90 47.3806 507.63 0.0000 706.68 26.4871 316.51 50.3819 511. 00 26.5170 711. 68 24.2291 319.41 0.0000 514.00 27.0854 720.70 0.0000 320.08 0.0000 514.00 27.0854 721. 93 0.0000 321.04 48.6281 520.40 24.5039 722.78 10.4268 323.87 42.4154 520.69 0.0000 722. 91 10. 4271 325.23 48.7640 522.65 0.0000 723. 31 10.4286 328.76 0.0000 527.90 0.0000 724 .19 13.9092 333.37 49.0255 528.26 32.0801 727.33 10.4440 333.97 30.2926 529.59 30.4946 733.00 13.9541 334.37 34.6289 529.87 0.0000 735.93 20.9531 338.28 41. 4673 531.02 0.0000 333.97 17.4707 338.32 41.4682 537.26 0.0000 739.50 0.0000 311. 90 39 .1116 546.56 0.0000 747.24 20.1622 340.48 39 .1116 552.55 20.5439 748.06 21. 0447 340.55 0.0000 563.25 19.5564 752.31 19.3205 344.28 33.8820 569.33 9658 753.82 0.0000 345.93 46.5156 946.00 25.0570 756.73 14.9528 351.06 33.0558 569.70 25.0599 756.80 14.9533 351. 93 33.0738 583.19 19. 7278 884.68 24.6914 Page 3117 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 26.4725 1274.44 12.3387 1620.50 4.3926 766.42 29.1258 1001.03 15.2065 1621. 92 2 .1969 766.84 28.2471 1002.74 10.4595 1678.03 0.0000 772. 60 0.0000 1004.73 13.3198 1690.97 3.3391 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 5.4152 778.90 17.7289 1028.54 0.0000 1063.66 12.6485 783.70 0.0000 1037.84 15.3643 1771.35 7.2293 785.37 15.1033 1038.76 0.0000 1791.20 0.0000 792.07 25.8237 631. 2 9 18.2903 1808.65 6.3680 794.95 22.2839 1048.07 0.0000 1810.72 0.0000 795.86 20.5075 1049.04 15.4121 1836.06 3.6564 810. 06 25.0862 1050.41 10.5999 810.29 25.0879 1063.66 10.6381 344.28 22.4007 1077.00 0.0000 810.76 22.4037 1077.34 15.5313 815.77 0.0000 1085.87 12.6485 1048.07 0.0000 1093.63 16.5746 832.01 17.1474 1099.45 21.4817 834.85 21. 6797 1112. 07 13.7163 835. 71 17.1683 1112. 84 16.6586 836.80 0.0000 1115. 54 15.6895 846.75 0.0000 1120.29 15.7090 846.77 17.2303 1120.55 15. 7100 856.80 0.0000 1221.41 17.2842 860.56 12.7529 1129. 67 14.7629 871.09 9 .1397 1131.51 0.0000 873.19 16.4625 1147.95 0.0000 875.33 0.0000 1173.23 17.9143 879.38 14.6621 1177.95 18.9316 880.51 14.6675 1189.05 15.9863 883.24 11. 0098 1204.77 20.0610 884.68 11. 0149 1221.41 16 .1143 889.28 8.8245 1231.02 19.3828 894.76 13.8121 1235.36 0.0000 898.04 15.6698 1238.28 23.2597 900. 72 21.2179 1260.41 0.0000 903.28 16.6185 1271.87 12.2329 911.20 9.2551 1274.44 10.2002 912.08 9.2575 1274.54 10.2008 923.98 0.0000 1291.59 14.3375 926.50 12.0875 1298.22 0.0000 929 .11 11. 9109 1312 .11 0.0000 937.49 21.4572 1332. 49 8.2705 944.13 0.0000 1362.66 0.0000 946.00 18.7054 1365.19 6.6652 949.00 25.4626 1368.63 0.0000 667.71 0.0000 1384.29 7.3213 962. 31 16.5408 1408. 01 6.3080 964.08 16.5494 1457.56 0.0000 966 .17 18.8177 1460.82 12.7595 911. 20 18.8330 1489.16 3.2087 968. 97 18.8330 1505.03 5.3656 '983. 53 0.0000 1584.12 9.8135 984.45 0.0000 1596.21 0.0000 Page 3118 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:10:36.59 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM33.CNF;235 Background date : Z-OCT-2016 11:02:02. Sample date 9-DEC-2015 10:13:00. Acquisition date : 3-0CT-2016 08:07:11. Sample ID G405235011 Sample quantity : 1.46502E+02 GRAM Detector name : GAM33 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.76 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 3 3 3 0 0 0 2 2 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3119of5809 Energy 63.53* 76.04* 87.05 89.79 92.69* 163.14* 185.81* 209.23 238.67* 241. 72 253 .11 269.69 271. 20 279.74 295.23 300.38 328.33* 338.46* 351. 84* 405.09 410.63 462.59 510.76* 583.10* 609.29* 653.95 661.69 726.96 769.04 805.86 825.89 860.69 880.86 894.48 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 7 274 70 43 61 15 95 33 343 100 24 31 28 20 176 15 48 60 263 27 18 48 20 114 215 5 85 23 14 12 12 19 15 24 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 123 283 193 127 148 63 125 73 74 88 48 58 54 108 69 57 48 70 51 28 44 33 52 41 24 29 30 20 19 17 8 18 14 14 0.83 3.34 1. 31 1. 01 1. 37 1. 35 1. 27 1.11 1.18 1. 48 0.65 1.25 1. 25 2.28 0.97 0.97 1. 22 0.81 1. 05 1. 67 1. 27 4.52 1. 21 1.20 1. 31 0.84 1. 51 2.41 1. 49 1. 03 1. 28 1. 98 4.75 0.62 127.17 152.16 174.15 179.62 185.41 326.13 371.42 418.20 477.02 483 .11 505.86 539.00 542.00 559.08 590.01 600.32 656.16 676.40 703.14 809.54 820.61 924.45 1020.71 1165.31 1217.67 1306.93 1322. 41 1452.90 1537.04 1610.67 1650.71 1720.32 1760.64 1787.88 124 146 168 168 168 324 367 415 472 472 502 534 534 551 584 596 653 671 697 805 815 917 1015 1158 1210 1298 1317 1447 1533 1605 1646 1713 1753 1779 6 1. 85E-03281.1 14 7. 61E-02 14. 4 24 1.94E-02 34.5 24 1.18E-02 44.1 24 l.70E-02 41.6 5 4.03E-03 90.4 11 2.63E-02 26.4 7 9.llE-03 47.0 17 9.52E-02 6.9 17 2.78E-02 20.4 8 6.54E-03 55.0 12 8.59E-03 44.7 12 7.68E-03 51.3 14 5.47E-03115.7 12 4.89E-02 12.1 8 4.27E-03 88.1 9 1.34E-02 30.9 10 1.65E-02 29.7 12 7.30E-02 8.3 9 7. 43E-03 41.1 11 5.00E-03 75.2 15 1.32E-02 30.3 13 5.55E-03 92.7 14 3.16E-02 15.6 14 5.99E-02 8.5 13 1.44E-03219.5 11 2.35E-02 16.7 10 6.43E-03 41.7 8 3.83E-03 63.6 9 3.19E-03 72.0 9 3.25E-03 54.2 11 5.18E-03 50.8 14 4.05E-03 60.5 18 6.75E-03 40.9 Fit 1. 69E+OO 1.29E+OO 2.12E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235011 Acquisition date 3-0CT-2016 08:07:11 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911.34* 93 18 1. 23 1821.60 1815 12 2.60E-02 14.0 36 0 934.66 28 8 1. 44 1868.25 1861 15 7.64E-03 28.9 37 0 967. 81 62 23 6.61 1934.54 1924 18 1.73E-02 21. 9 38 0 979.57 12 14 0.94 1958.08 1948 14 3.33E-03 72.2 39 0 1120.52* 53 16 1.17 2240.03 2234 13 1. 48E-02 21. 0 40 0 1166. 35 10 4 0.71 2331.73 2328 8 2. 67E-G\3 53.1 41 0 1195.46 11 9 1. 38 2389.97 2386 9 2.99E-03 62.5 42 0 1238.94 17 12 2.42 2476.97 2472 10 4.69E-03 46.0 43 0 1461. 02* 355 9 1. 87 2921.43 2913 17 9.85E-02 5.7 44 0 1592.82* 10 2 1. 63 3185.30 3182 7 2.80E-03 41. 0 45 0 1765.02* 30 0 1. 72 3530.12 3524 12 8.28E-03 19.5 Flag: "*" = Peak area was modified by background subtraction Page 3120of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:10:39 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 9-DEC-2015 10:13:00 G405235011 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:07:11 146.50 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA33 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 77 .11 PB-214 77 .11 PB-214 77 .11 PB-214 77 .11 PB-214 77 .11 PB-214 351. 93 Page 3121 of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 TH-228 77 .11 PB-212 77 .11 PB-214 77 .11 AM-243 74.66 TH-228 74.82 PB-212 74.82 TH-228 77 .11 PB-212 77 .11 BI-211 351.06 CAN 0 01:00:00.76 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235011 Acquisition date 3-0CT-2016 08:07:11 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40. 1460.82 10.66* 1.133E+OO 1.447E+Ol. 1.447E+Ol 11. 37 OK CD-109 88.03 3.70* 4.889E+OO 1.205E+OO l.888E+OO 142.57 OK SN-126 64.28 9.60 2.483E+OO l.819E-01 l.819E-01 562.28 OK 86.94 8.90 4.889E+OO 5.0lOE-01 5.0lOE-01 142 *. 57 OK 87.57 37.00* 4.889E+OO l.205E-01 l.205E-01 142.57 OK CS-135 268.22 16.00* 4.353E+OO 2.570E-01 2.570E-01 89.36 OK BA-137M 661.66 89.90* 2 .115E+OO 2.371E-01 2.416E-01 33.30 OK CS-137 661. 66 85.10* 2 .115E+OO 2.505E-01 2.553E-01 33.30 OK HG-203 70.83 3.69 3.364E+OO Line Not Found Absent 72. 87 6.19 3.591E+OO Line Not Found Absent 279.20 81. 56* 4.230E+OO 3.294E-02 2.813E+OO 231.47 OK TL-208 277.37 6.60 4.258E+OO Line Not Found Absent 583.19 85.00* 2.334E+00 3.090E-01 3.090E-01 31.11 OK 860.56 12.50 l.727E+00 4.495E-01 4.495E-01 101. 63 OK PB-212 74.82 10.28 3.925E+OO 2.323E+OO 2.323E+OO 56.07 OK 77 .11 17.10 3.925E+OO 1.397E+OO 1.397E+OO 56.07 OK 238.63 43.60* 4.775E+OO 9.622E-01 9.622E-01 13.75 OK 300.09 3.30 3.996E+00 6.688E-01 6.688E-01 176.29 OK BI-214 609.32 45.49* 2.255E+OO l.129E+OO 1.129E+OO 17.00 OK 1120.29 14.92 1.407E+OO 1.289E+OO 1. 290E+OO 41.98 OK 1764.49 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 OK PB-214 74.82 5.80 3.800E+OO Line Not Found <<INT Reject 77 .11 9.70 4.033E+OO Line Not Found <<INT Reject 87.09 3.41 4.892E+OO Line Not Found <<INT Reject 242.00 7.25 4. 727E+OO Line Not Found <<INT Reject 295.22 18.42 4.052E+OO 1.353E+OO l.353E+00 24.17 OK 351. 93 35.60* 3.513E+OO 1.187E+OO 1.187E+OO 16.59 OK RN-222 609.32 45.49* 2.255E+OO 1.129E+OO l.129E+OO 17.00 OK 1120.29 14.92 1. 407E+OO 1.289E+OO 1.290E+OO 41. 98 OK 1764.49 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 OK RA-224 240.99 4.10* 4. 731E+OO 6.267E-01 6.267E-01 216.97 OK RA-226 609.32 45.49* 2.255E+OO 1.129E+OO l.129E+OO 17.00 OK 1120.29 14.92 l.407E+00 1.289E+OO 1.290E+00 41. 98 OK 1764.49 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 OK AC-228 105.21 1.10 5.839E+00 Line Not Found Absent 338.32 11.27 3.627E+OO 8.265E-01 8.265E-01 59.37 OK 794.95 4.25 1.835E+OO Line Not Found Absent 835. 71 1. 61 1.766E+00 Line Not Found Absent 911.20 25.80* 1.653E+OO 1.133E+OO 1.133E+OO 28.05 OK 968. 97 15.80 1.578E+OO 1.282E+OO 1.282E+OO 43.90 OK RA-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.627E+OO 8.265E-01 8.265E-01 59.37 OK 794.95 4.25 1.835E+OO Line Not Found Absent 835.71 1. 61 1. 766E+OO Line Not Found Absent 911. 20 25.80* 1.653E+OO 1.133E+OO 1.133E+OO 28.05 OK 968.97 15.80 1. 578E+00 l.282E+OO 1.282E+OO 43.90 OK TH-228 74.82 10.28 3.925E+OO 2.323E+OO 2.323E+OO 56.07 OK 77 .11 17.10 3.925E+OO 1.397E+OO l.397E+OO 56.07 OK 238.63 43.60* 4.775E+OO 9.622E-01 9.622E-01 13.75 OK Page 3122of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235011 Acquisition date 3-0CT-2016 08:07:11 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 300.09 3.30 3 .. 996E+OO 6.688E-01 6.688E-01 176.29 OK TH-230 609.32 45.49* 2.255E+OO 1.129E+OO l.129E+OO 17.00 OK 1120.29 14.92 1.407E+OO l.289E+OO 1.289E+OO 41.98 OK 1764.49 15.30 9.589E-01 9.830E-01 9.830E-01 38.98 OK PA-231 283.69 1. 70 4.183E+OO Line Not Found Absent 301.36 5.35* 3. 996E+OO 4.125E-01 4.125E-01 176.29 OK TH-232 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.627E+OO 8.265E-01 8.265E-01 59.37 OK 835.71 1. 61 1.766E+OO Line Not Found Absent 911.20 25.80* 1.653E+OO 1.133E+OO 1.133E+OO 28.05 OK 968. 97 15.80 1.578E+OO 1.282E+OO 1.282E+OO 43.90 OK TH-234 63. 29 3.70* 2.483E+00 4.719E-01 4.719E-01 562.28 OK 92. 59 4.23 5.263E+OO 1. 738E+OO l.738E+OO 83.28 OK U-234 609.32 45.49* 2.255E+OO 1.129E+OO 1.129E+OO 17.00 OK 1120.29 14.92 1.407E+OO 1.289E+OO 1.289E+OO 41. 98 OK 1764.49 15.30 9.589E-01 9.830E-01 9.830E-01 38.98 OK U-235 89. 96 3.47 5.080E+OO 1.535E+OO 1.535E+OO 88.12 OK 93.35 5.60 5.263E+OO 1.312E+OO 1. 312E+OO 83.28 OK 143. 7 6 10. 96* 6.181E+OO Line Not Found Absent 163.33 5.08 5. 966E+OO 2.895E-01 2.895E-01 180.74 OK 185. 72 57.20 5.616E+OO 1. 761E-01 1. 761E-01 52.74 OK 205.31 5.01 5.295E+OO Line Not Found Absent U-238 63.29 3.70* 2.483E+OO 4.719E-01 4.719E-01 562.28 OK 92.59 4.23 5.263E+OO 1.738E+OO 1.738E+00 83.28 OK AM-243 43.53 5.90 2.461E-01 Line Not Found Absent 74.66 67.20* 3.925E+OO 3.554E-01 3.555E-01 56.07 OK ANH-511 511. 00 100.00* 2.593E+OO 4.207E-02 4.207E-02 185.33 OK Flag: "*" = Keyline Page 3123 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:10:40.68 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l *
  • Acquisition date 3-0CT-2016 08:07:11 Sensitivity : 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
  • Sample date 9-DEC-2015 10:13:00 Analyst initials: MXRl *
  • Sample ID G405235011 Sample Quantity 1.4650E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff'. File : DKA100: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1. 447E+Ol 1.613E+OO 6.678E-01 CD-109 1.888E+OO 2.638E+OO 2.312E+OO SN-126 l.205E-01 l.684E-01 1.485E-01 CS-135 2.570E-01 2.250E-01 2.458E-01 BA-137M 2.416E-01 7.886E-02 7.398E-02 CS-137 2.553E-01 8.331E-02 7.816E-02 HG-203 2. 813E+OO 6.381E+OO 4.499E+OO TL-208 3.090E-01 9.423E-02 6.624E-02 PB-212 9.622E-01 1.297E-01 8.860E-02 BI-214 1.129E+OO 1.881E-01 l.126E-01 PB-214 1.187E+OO 1. 931E-01 9.264E-02 RN-222 1.129E+OO 1.881E-01 1.126E-01 RA-224 6.267E-01 l.333E+00 9.496E-01 RA-226 1.129E+OO 1. 881E-01 l.126E-01 AC-228 l.133E+00 3 .115E-01 l.924E-01 RA-228 l.133E+00 3 .115E-01 l.924E-01 TH-228 9.622E-01 1.297E-01 8.860E-02 TH-230 l.129E+00 1.880E-01 l.125E-01 PA-231 4.125E-01 7.127E-01 6.999E-01 TH-232 l.133E+00 3 .115E-01 l.924E-01 TH-234 4.719E-01 2.600E+OO 2.657E+OO U-234 1.129E+OO l.880E-01 l.125E-01 U-235 6.013E-02 2.029E-01 3.875E-01 U-238 4. 719E-01 2.600E+OO 2.657E+OO AM-243 3.555E-01 l.953E-01 9.832E-02 ANH-511 4.207E-02 7.641E-02 5.558E-02 ----Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -5.945E-01 1.274E+Ol 2. 471E+Ol NOT IDENT. NA-22 -4.517E-02 3.949E-02 6.094E-02 NOT IDENT. NA-24 0.000E+OO l.335E+41 O.OOOE+OO SHORT HLIF AL-26 -5.270E-03 2.490E-02 5.224E-02 NOT IDENT. Page 3124of5809 SC-46 -6. 396E-02 3.082E-01 5.412E-01 FAIL ABUN V-48 O.OOOE+OO 1.507E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4. 031E+02 O.OOOE+OO SHORT HLIF MN-54 3.719E-03 6.319E-02 l.223E-01 NOT IDENT. C0-56 1.604E-02 4.266E-01 8.360E-01 FAIL ABUN MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 1.222E-02 4. 696E-02 9.024E-02 NOT IDENT. C0-58 -2.268E-01 4. 725E-01 8.438E-01 NOT IDENT. FE-59 -1.039E+OO 5.646E+OO 1.133E+Ol NOT IDENT. C0-60 -6.480E-03 3.547E-02 7.091E-02. NOT IDENT. ZN-65 7.180E-02 1.755E-01 3.441E-01 NOT IDENT. GE-68 l.522E+OO 2.297E+OO 5. lllE+OO NOT IDENT. AS-73 4.634E+00 1.069E+Ol 2.202E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.303E+03 O.OOOE+OO SHORT HLIF SE-75 6.535E-02 1. 891E-01 3.600E-01 FAIL ABUN BR-77 O.OOOE+OO 1. 785E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.736E+02 O.OOOE+OO SHORT HLIF RB-83 2.006E-01 5.353E-01 1.129E+OO NOT IDENT. KR-85 1.450E+OO 7.081E+OO 1.285E+Ol NOT IDENT. SR-85 1. 517E-01 7.411E-01 1.344E+OO NOT IDENT. RB-86 O.OOOE+OO 2.606E+04 O.OOOE+OO SHORT HLIF Y-88 -8.954E-02 2.715E-01 5 .115E-01 NOT IDENT. Y-91 -7.957E+Ol 5.157E+02 l.010E+03 NOT IDENT. NB-94 -3.468E-03 2.946E-02 5.606E-02 NOT IDENT. NB-95 -2.194E-01 1.070E+OO 1. 748E+OO NOT IDENT. NB-95M -7.068E-01 2.544E+OO 4.077E+OO NOT IDENT. ZR-95 7.376E-01 1. 301E+OO 2.776E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1.345E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.292E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 793E+41 O.OOOE+OO SHORT HLIF RH-101 -3.358E-02 3.564E-02 6.130E-02 NOT IDENT. RH-102 -l.877E-04 6.083E-02 1.178E-01 NOT IDENT. RU-103 -2.149E+OO 5.258E+OO 9.805E+OO FAIL ABUN RH-106 -l.854E-01 4.052E-01 7.438E-01 NOT IDENT. RU-106 -l.854E-01 4.052E-01 7.438E-01 NOT IDENT. AG-108M 6.948E-03 2. 791E-02 5.626E-02 NOT IDENT. AG-llOM 4. 396E-03 8. 931E-02 l.606E-01 NOT IDENT. SN-113 -l.097E-01 2. 371E-01 4. 431E-01 NOT IDENT. CD-115 O.OOOE+OO 2.202E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 0.000E+OO 9 .117E+04 O.OOOE+OO SHORT HLIF TE-123M -1.092E-01 1.297E-01 2.210E-01 NOT IDENT. SB-124 -9.972E-03 1.333E+OO 3.141E+OO NOT IDENT. SB-125 -8.818E-03 1.124E-01 2.172E-01 FAIL ABUN TE-125M 2.608E+02 2. 761E+02 5.574E+02 NOT IDENT. I-126 0.000E+OO 1.036E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.108E+06 O.OOOE+OO SHORT HLIF. SB-127 O.OOOE+OO 1. 788E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.369E+09 0.000E+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.099E+26 O.OOOE+OO SHORT HLIF BA-133 -1.680E-02 4.204E-02 7.083E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.235E-03 4.819E-02 9.439E-02 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 0.000E+OO 2.923E+05 O.OOOE+OO SHORT HLIF CE-139 2.759E-02 l.227E-01 2.131E-01 NOT IDENT. BA-140 O.OOOE+OO l.265E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.156E+05 O.OOOE+OO SHORT HLIF CE-141 -2.715E+OO 2.561E+Ol 4.689E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.121E+41 O.OOOE+OO SHORT HLIF CE-144 -1.632E-01 3.535E-01 6.338E-01 NOT IDENT. PM-144 9.472E-04 5.455E-02 l.054E-01 NOT IDENT. PR-144 1. 446E-01 4.746E+OO 9.187E+OO NOT IDENT. PM-146 -3.349E-02 4. 771E-02 8.562E-02 NOT IDENT. ND-147 0.000E+OO 2.826E+07 O.OOOE+OO SHORT HLIF PM-147 3.068E+02 8.045E+02 l.564E+03 NOT IDENT. PM-149 O.OOOE+OO 3.366E+40 O.OOOE+OO SHORT HLIF EU-150 1.228E-02 2.552E-02 4.849E-02 FAIL ABUN EU-152 2.065E-02 9.906E-02 1.979E-01 NOT IDENT. GD-153 -3.455E-02 2.178E-01 3.728E-01 NOT IDENT. EU-154 -1.059E-01 9.805E-02 l.551E-01 NOT IDENT. EU-155 -3.636E-02 l.082E-01 l.993E-01 FAIL ABUN TB-160 2.603E+00 3.089E+OO 3.609E+OO FAIL ABUN H0-166M 2.822E-02 5.407E-02 l.130E-01 FAIL ABUN TM-171 -7.373E+OO 2.694E+Ol 5.225E+Ol NOT IDENT. HF-172 7.132E-03 2.314E-01 4.345E-01 FAIL ABUN LU-172 8.715E-03 6.365E-02 1.355E-01 FAIL ABUN Page 3125 of 5809 LU-176 4 .116E-03 2.251E-02 4.560E-02 FAIL ABUN HF-181 1. 807E+OO 3.986E+OO 8.302E+OO NOT IDENT. TA-182 -3.295E-01 9.705E-01 1.828E+OO FAIL ABUN RE-183 1. 712E+OO 3.502E+00 7.147E+OO FAIL ABUN RE-184 1.509E+Ol 2.852E+Ol 6.0lOE+Ol FAIL ABUN W-188 -8.038E-01 1.136E+02 2.040E+02 FAIL ABUN IR-192 -l.862E-01 3.850E-01 7.339E-01 FAIL ABUN BI-207 4. 969E-02 5 .131E-02 l.159E-01 FAIL ABUN PB-210 3.479E+OO 5.166E+OO 1.090E+Ol NOT IDENT. BI-211 . 0. OOOE+OO 5.318E-01 8.701E-01 FAIL ABUN PB-211 1.262E+OO 1.016E+OO 1.464E+OO FAIL ABUN BI-212 9.324E-01 7.616E-01 1.165E+OO FAIL ABUN RN-219 1.905E-02 3.799E-01 6.826E-01 FAIL ABUN RA-223 -2.012E-01 6.095E-01 1.112E+OO FAIL ABUN AC-227 -1.880E-02 2.417E-01 3.986E-01 FAIL ABUN TH-227 -1.880E-02 2.417E-01 3.986E-01 FAIL ABUN TH-229 l.531E-01 4.706E-01 8.856E-01 FAIL ABUN TH-231 -2.012E-01 6.095E-01 1.112E+00 FAIL ABUN PA-233 1.608E-02 5.091E-02 l.053E-01 FAIL ABUN PA-234 -1. 94 7E-02 2.525E-01 4.826E-01 FAIL ABUN PA-234M -2.344E+00 4.564E+OO 8.080E+OO NOT IDENT. NP-237 l.608E-02 5. 091E-02 1.053E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 1.453E-01 2.540E-01 4.982E-01 NOT IDENT. PU-239 5.633E+Ol 3.310E+02 6.237E+02 NOT IDENT. AM-241 -1. OOlE-01 1. 674E-01 3 .119E-'01 NOT IDENT. CM-243 6.895E-02 9.505E-02 1.917E-01 NOT IDENT. BK-247 -2. 901E-02 7 .'847E-02 l.234E-01 NOT IDENT. CM-247 5.343E-03 3.533E-02 6. 431E-02 NOT IDENT. CF-249 2.814E-02 3.785E-02 7. 964E-02 FAIL ABUN CF-251 1.066E-01 1.181E-01 2.335E-01 NOT IDENT. Page 3126 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:10:37.60 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 341 10.66* 1.133E+OO 1.447E+Ol 1.447E+Ol 11. 37 CD-109 88.03 87 3.70* 4.889E+OO 2.452E+OO 3.842E+OO 68.99 SN-126 64.28 8 9.60 2.483E+OO 1. 819E-01 l.819E-01 562.28 86.94 87 8.90 4.889E+OO l.019E+OO 1.019E+OO 68.99 87.57 87 37.00* 4.889E+OO 2.452E-01 2.452E-01 68.99 CS-135 268.22 35 16.00* 4.353E+OO 2.570E-01 2.570E-01 89.36 BA-137M 661.66 88 89.90* 2 .115E+OO 2.371E-01 2.416E-01 33.30 CS-137 661.66 88 85.10* 2 .115E+OO 2.505E-01 2.553E-01 33.30 HG-203 70.83 ------3.69 3.364E+OO ------Line Not Found ------72.87 ------6.19 3.591E+OO ------Line Not Found ------279.20 22 81.56* 4.230E+OO 3.294E-02 2.813E+OO 231. 47 TL-208 277.37 ------6.60 4.258E+OO ------Line Not Found ------583.19 120 85.00* 2.334E+OO 3.090E-01 3.090E-01 31.11 860.56 19 12.50 1.727E+OO 4.495E-01 4.495E-01 101. 63 BI-211 72.87 ------1. 23 3.591E+OO ------Line Not Found ------351.06 290 12.92* 3.513E+OO 3.270E+OO, 3.270E+OO 16.59 PB-212 74.82 344 10.28 3.925E+OO 4.363E+OO 4.363E+OO 28.70 77 .11 344 17.10 3.925E+OO 2.623E+OO 2.623E+OO 28.70 238.63 391 43.60* 4.775E+OO 9.622E-01 9.622E-01 13.75 300.09 17 3.30 3.996E+OO 6.688E-01 6.688E-01 176.29 BI-214 609.32 226 45.49* 2.255E+OO 1.129E+OO 1.129E+OO 17.00 1120.29 53 14.92 l.407E+OO 1.289E+OO 1.290E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 PB-214 74.82 344 5.80 3.925E+OO 7.733E+OO 7.736E+OO 28.70 77 .11 344 9.70 3.925E+OO 4.624E+OO 4.626E+OO 28.70 87.09 87 3.41 4.889E+00 2.660E+OO 2.661E+OO 68.99 242.00 114 7.25 4.731E+OO 1.707E+OO 1. 708E+00 40.77 295.22 197 18.42 4.052E+OO l.353E+OO 1.353E+OO 24.17 351. 93 290 35.60* 3.513E+OO 1.187E+OO 1.187E+OO 16.59 RN-222 609.32 226 45.49* 2.255E+OO 1.129E+OO l.129E+OO 17.00 1120.29 53 14.92 1.407E+OO 1.289E+OO 1.290E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 RA-224 240.99 114 4.10* 4. 731E+OO 3.019E+OO 3.019E+OO 40.77 RA-226 609.32 226 45.49* 2.255E+OO 1.129E+OO l.129E+OO 17.00 1120.29 53 14.92 1.407E+OO 1.289E+OO l.290E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.833E-01 38.98 AC-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 66 11.27 3.627E+OO 8.265E-01 8.265E-01 59.37 794.95 ------4.25 1.835E+OO ------Line Not Found ------835.71 ------1. 61 1.766E+OO ------Line Not Found ------911.20 94 25.80* 1.653E+OO 1.133E+OO 1.133E+OO 28.05 968. 97 62 15.80 1.578E+OO 1.282E+OO 1.282E+OO 43.90 RA-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 66 11.27 3.627E+OO 8.265E-01 8.265E-01 59.37 794.95 ------4.25 1.835E+OO ------Line Not Found ------835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911. 20 94 25.80* 1.653E+OO 1.133E+OO 1.133E+OO 28.05 Page 3127 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235011 Acquisition date 3-0CT-2016 08:07:11 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968. 97 62 15.80 1. 57.8E+OO 1.282E+OO 1.282E+OO 43.90 TH-228 74.82 344 10.28 3.925E+OO 4.363E+OO 4.363E+OO 28.70 77 .11 344 17.10 3.925E+OO 2.623E+OO 2.623E+OO 28.70 238.63 391 43.60* 4.775E+OO 9.622E-01 9.622E-01 13.75 300.09 17 3.30 3. 996E+OO 6.688E-01 6.688E-01 176.29 TH-230 609.32 226 45.49* 2.255E+OO l.129E+OO 1.129E+OO 17.00 1120.29 53 14.92 1.407E+OO l.289E+OO 1.289E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.830E-01 38.98 PA-231 283.69 ------1. 70 4.183E+OO ------Line Not Found ------301.36 17 5.35* 3. 996E+OO 4.125E-01 4.125E-01 176.29 TH-232 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 66 11.27 3.627E+OO 8.265E-01 8.265E-01 59.37 835.71 ------1. 61 1.766E+OO ------Line Not Found ------911.20 94 25.80* 1.653E+OO l.133E+00 1.133E+OO 28.05 968. 97 62 15.80 1.578E+00 l.282E+OO 1.282E+00 43.90 TH-234 63.29 8 3.70* 2.483E+OO 4.719E-01 4.719E-01 562.28 92.59 75 4.23 5.263E+OO 1.738E+OO 1.738E+OO 83.28 U-234 609.32 226 45.49* 2.255E+OO l.129E+OO 1.129E+OO 17.00 1120.29 53 14.92 1.407E+OO 1.289E+00 '1.289E+OO 41. 98 1764.49 28 15.30 9.589E-01 9.830E-01 9.830E-01 38.98 U-235 89.96 53 3.47 5.080E+OO 1.535E+OO 1.535E+OO 88.12 93.35 75 5.60 5.263E+OO 1.312E+OO l.312E+00 83.28 143.76 ------10. 96* 6.181E+OO ------Line Not Found ------163.33 17 5.08 5. 966E+OO 2.895E-01 2.895E-01 180.74 185.72 110 57.20 5.616E+OO 1. 761E-01 1. 761E-01 52 .. 74 205.31 ------5.01 5.295E+OO ------Line Not Found ------U-238 63.29 8 3.70* 2.483E+OO 4.719E-01 4. 719E-01 562.28 92.59 75 4.23 5.263E+OO 1.738E+OO 1.738E+OO 83.28 AM-243 43.53 ------5.90 2.461E-01 ------Line Not Found ------74.66 344 67.20* 3.925E+OO 6.675E-01 6.675E-01 28.70 ANH-511 511. 00 21 100.00* 2.593E+OO 4.207E-02 4.207E-02 185.33 Flag: "*" Key line Page 3128of5809 Summary of Nuclide Activity Sample ID : G405235011 Acquisition date Page : 3 3-0CT-2016 08:07:11 Total number of lines in spectrum 45 Number of unidentified lines 10 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 u-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y 46.59D 1. 41E+10Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 57 1. 00 1. 00 1. 02 1. 02 85.4 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.447E+Ol 2.452E+OO 2.452E-01 2.570E-01 2.371E-01 2.505E-01 3.294E-02 3.090E-01 3.270E+OO 9.622E-01 1.129E+OO 1.187E+OO 1.129E+OO 3.019E+OO 1.129E+OO 1. 133E+OO 1.133E+OO 9.622E-01 1.129E+OO 4.125E-01 1.133E+OO 4.719E-01 1.129E+OO 1. 761E-01 4.719E-01 6.675E-01 4.207E-02 3.894E+Ol 3.894E+Ol Decay Corr pCi/GRAM 1.447E+Ol 3.842E+OO 2.452E-01 2.570E-01 2.416E-01 2.553E-01 2. 813E+OO 3.090E-01 3.270E+OO 9.622E-01 l.129E+OO 1.187E+OO 1.129E+OO 3.019E+OO 1.129E+OO 1'.133E+OO 1.133E+OO 9.622E-01 1.129E+OO 4.125E-01 1.133E+OO 4.719E-01 1.129E+OO 1. 761E-01 4.719E-01 6.675E-01 4.207E-02 4.312E+Ol 4.312E+Ol 77.78% Decay Corr 2-Sigma Error 0.165E+Ol 2.650E+OO 1. 691E-01 2. 296E-01 0.805E-01 0.850E-01 6.512E+OO 0. 961E-01 0.543E+OO l.323E-01 0.192E+OO 0.197E+OO 0.192E+OO 1. 231E+OO 0.192E+OO 0.318E+OO 0.318E+OO 1.323E-01 0.192E+OO 7.273E-01 0.318E+OO 26.53E-01 0.192E+OO 0.929E-01 26.53E-01 1.916E-01 7.797E-02 "M" Manually accepted 2-Sigma %Error 11. 37 68.99 68.99 89.36 33.30 33.30 231.47 31.11 16.59 13. 75 17.00 16.59 17.00 40.77 17.00 28.05 28.05 13. 75 17.00 176.29 28.05 562.28 17.00 52.74 562.28 28.70 185.33 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3129 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235011 Acquisition date : 3-0CT-2016 08:07:11 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.23 38 84 1.11 418.20 415 7 9. llE-03 94.0 5.23E+OO 0 253 .11 27 55 0.65 505.86 502 8 6.54E-03 **** 4.57E+OO T 1 271.20 31 60 1. 25 542.00 534 12 7.68E-03 **** 4.33E+OO T 0 328.33 53 .53 1. 22 656.16 653 9 1.34E-02 61. 8 3.72E+OO T 0 405.09 29 31 1. 67 809.54 805 9 7.43E-03 82.2 3.13E+OO T 0 410.63 20 48 1. 27 820.61 815 11 5.00E-03 **** 3.09E+OO T 0 462.59 51 36 4.52 924.45 917 15 l.32E-02 60.6 2. 81E+OO T 0 653.95 5 30 0.84 1306.93 1298 13 l.44E-03 **** 2.13E+OO 0 726. 96 24 20 2.41 1452.90 1447 10 6.43E-03 83.4 1. 97E+OO T 0 769.04 14 20 1. 49 1537.04 1533 8 3.83E-03 **** 1. 88E+OO 0 805.86 12 17 1. 03 1610.67 1605 9 3.19E-03 **** 1.82E+OO 0 825.89 12 8 1. 28 1650.71 1646 9 3.25E-03 **** 1. 78E+OO 0 880.86 15 15 4.75 1760.64 1753 14 4.05E-03 **** 1. 70E+OO T 0 894.48 25 14 0.62 1787.88 1779 18 6.75E-03 81. 8 1.68E+OO T 0 934.66 28 8 1. 44 1868.25 1861 15 7.64E-03 57.8 1.62E+OO 0 979.57 12 14 0.94 1958.08 1948 14 3.33E-03 **** l.56E+OO 0 1166. 35 9 4 0. 71 2331.73 2328 8 2.67E-03 **** 1.36E+OO 0 1195.46 11 9 1. 38 2389.97 2386 9 2.99E-03 **** l.34E+00 0 1238.94 17 12 2.42 2476.97 2472 10 4.69E-03 92.0 1. 30E+00 T 0 1592.82 10 1 1. 63 3185.30 3182 7 2.80E-03 82.0 1. 05E+OO Flags: "T" = Tentatively associated Page 3130 of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:11:03.48 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l *
  • Acquisition date 3-0CT-2016 08:07:11 Sensitivity 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
  • Sample date 9-DEC-2015 10:13:00 Nuclide Library : SOLID *
  • Sample ID G405235011 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.4650E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 HG-203 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-22 6 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2*. 762E-01 1.093E+OO 7.021E-02 1.126E-01 3.320E-02 3.507E-02 2. 071E+OO 2.954E-02 4.083E-02 4.936E-02 4.057E-02 4.936E-02 4.376E-01 4.936E-02 7.970E-02 7.970E-02 4.083E-02 4.934E-02 3.161E-01 7.970E-02 1. 24 7E+OO 4.934E-02 l.830E-01 l.247E+OO 4.625E-02 2.504E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3131 of 5809 Le (pCi/GRAM 1.113E+Ol 2.361E-02 O.OOOE+OO l.870E-02 2.209E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3132 of 5809 O.OOOE+OO O.OOOE+OO 5.340E-02 3.590E-01 O.OOOE+OO 4.215E-02 3.487E-01 4. 7 51E+OO 2.910E-02 l.492E-01 2.233E+OO l.022E+Ol O.OOOE+OO l.643E-01 O.OOOE+OO 0.000E+OO 4. 960E-01 5.753E+OO 6.020E-01 O.OOOE+OO 2.030E-01 4.349E+02 2.452E-02 7.787E-01 1. 885E+OO 1. 215E+00 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.859E-02 5.217E-02 4.323E+OO 3.156E-01 3.156E-01 2.546E-02 6. 716E-02 2.008E-01 O.OOOE+OO O.OOOE+OO l.023E-01 l.113E+OO 9.876E-02 2.618E+02 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.190E-02 O.OOOE+OO 4.127E-02 O.OOOE+OO O.OOOE+OO 9. 965E-02 O.OOOE+OO O.OOOE+OO 2.201E+Ol O.OOOE+OO 2.950E-01 4. 651E-02 4.056E+OO 3.854E-02 O.OOOE+OO 7.304E+02 O.OOOE+OO 2.217E-02 9 .107E-'02 l.755E-01 6.074E-02 9.292E-02 l.563E+OO 4.993E-02 2.415E+Ol 2.031E-01 5.724E-02 2.084E-02 SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3133of5809 3.718E+OO 7.934E-01 3.338E+OO 2.618E+Ol 9.347E+Ol 3.293E-01 5.145E-02 5.068E+OO 4.194E-01 6. 713E-01 5.287E-01 3.068E-01 5.083E-01 l.825E-01 l.825E-01 4.128E-01 5.083E-01 4.783E-02 2.048E-01 3.496E+OO 4.783E-02 O.OOOE+OO 2.340E-01 2.932E+02 l.454E-01 8. 965E-02 5.623E-02 2.899E-02 3.647E-02 l.094E-01 NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:11:16.35 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235011.CNF;l *
  • Acquisition date 3-0CT-2016 08:07:11 Sensitivity : 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
  • Sample date 9-DEC-2015 10:13:00 Nuclide Library : SOLID *
  • Sample ID G405235011 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4650E+02 GRAM *
  • Quantity Err(%) : 1.3652E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) K-40 1. 44 7E+Ol 1. 781E+OO 1. 781E+OO CD-109 1. 888E+OO 2.654E+OO 2.654E+OO SN-126 1.205E-01 1.693E-01 l.693E-01 CS-135 2.570E-01 2.257E-01 2.257E-01 BA-137M 2.416E-01 7.954E-02 7.954E-02 CS-137 2.553E-01 8.403E-02 8.403E-02 HG-203 2.813E+00 6.383E+OO 6.383E+OO TL-208 3.090E-01 9. 513E-02 9. 513E-02 PB-212 9.622E-01 l.392E-01 1.392E-01 BI-214 1.129E+OO l.942E-01 1.942E-01 PB-214 l.187E+OO l.992E-01 1.992E-01 RN-222 1.129E+OO 1.942E-01 l.942E-01 RA-224 6.267E-01 1.342E+OO 1.342E+OO RA-226 1.129E+OO l.942E-01 l.942E-01 AC-228 1.133E+OO 3.168E-01 3.168E-01 RA-228 1.133E+00 3.168E-01 3.168E-01 TH-228 9.622E-01 1.392E-01 l.392E-01 TH-230 1.129E+OO 1.941E-01 1. 941E-01 PA-231 4.125E-01 7.181E-01 7 .181E-01 TH-232 1.133E+OO 3.168E-01 3.168E-01 TH-234 4. 719E-01 2.602E+OO 2.602E+OO U-234 1.129E+OO 1.941E-01 1. 941E-01 U-235 6.013E-02 2.029E-01 2.029E-01 U-238 4.719E-01 2.602E+OO 2.602E+OO AM-24'3 3.555E-01 l.987E-01 1. '987E-01 ANH-511 4.207E-02 7.643E-02 7.643E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) BE-7 -5.945E-01 1.274E+Ol 1.274E+Ol NOT IDENT. NA-22 -4.517E-02 3.952E-02 4.446E-02 NOT IDENT. NA-24 -1.000E+41 1.404E+41 O.OOOE+OO SHORT HLIF AL-26 -5.270E-03 2.491E-02 2.502E-02 NOT IDENT. Page.3134 of 5809 SC-46 -6. 396E-02 3.083E-01 3. 096E-01 FAIL ABUN V-48 8.494E+03 1.508E+04 l.556E+04 SHORT HLIF CR-51 -7.144E+Ol 4. 031E+02 4.044E+02 SHORT HLIF MN-54 3.719E-03 6.319E-02 6. 321E-02 NOT IDENT. C0-56 1.604E-02 4.266E-01 4.267E-01 FAIL ABUN MN-56 1.000E+41 2.977E+42 O.OOOE+OO SHORT HLIF C0-57 1.222E-02 4. 696E-02 4.729E-02 NOT IDENT. C0-58 -2.268E-01 4.726E-01 4.835E-01 NOT IDENT. FE-59 -1.039E+OO 5.647E+OO 5.666E+OO NOT IDENT. C0-60 -6 .. 480E-03 3.547E-02 3.559E-02 NOT IDENT. ZN-65 7.180E-02 1.756E-01 1.785E-01 NOT IDENT. GE-68 1.522E+OO 2.298E+OO 2.398E+OO NOT IDENT. AS-73 4.634E+OO 1.073E+Ol 1.093E+Ol NOT IDENT. AS-74 7.799E+02 6.303E+03 6.313E+03 SHORT HLIF SE-75 6.535E-02 1.892E-01 l.914E-01 FAIL ABUN BR-77 1.325E+38 1.143E+39 O.OOOE+OO SHORT HLIF SR-82 6.801E+Ol 8.736E+02 8.741E+02 SHORT HLIF RB-83 2.006E-01 5.360E-01 5.435E-01 NOT IDENT. KR-85 1.450E+OO 7.082E+OO 7 .112E+OO NOT IDENT. SR-85 1. 517E-01 7. 411E-01 7.442E-01 NOT IDENT. RB-86 9.534E+03 2.607E+04 2.642E+04 SHORT HLIF Y-88 -8.954E-02 2.716E-01 2.745E-01 NOT IDENT. Y-91 -7.957E+Ol 5.157E+02 5.169E+02 NOT IDENT. NB-94 -3.468E-03 2.946E-02 2.951E-02 NOT IDENT. NB-95 -2.194E-01 1.070E+OO 1. 074E+OO NOT IDENT. NB-95M -7.068E-01 2.544E+OO 2.564E+OO NOT IDENT. ZR-95 7.376E-01 1.301E+OO 1.343E+OO NOT IDENT. NB-97 1.000E+41 2.701E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1.345E+41 O.OOOE+OO SHORT HLIF M0-99 3.932E+30 1.292E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1. 796E+41 O.OOOE+OO SHORT HLIF RH-101 -3.358E-02 3.615E-02 3.919E-02 NOT IDENT. RH-102 -1.877E-04 6.083E-02 6.083E-02 NOT IDENT. RU-103 -2.149E+OO 5.259E+OO 5.348E+OO FAIL ABUN RH-106 -1.854E-01 4.054E-01 4.139E-01 NOT IDENT. RU-106 -1.854E-01 4.054E-01 4.139E-01 NOT IDENT. AG-108M 6.948E-03 2.791E-02 2.809E-02 NOT IDENT. AG-llOM 4. 396E-03 8.931E-02 8.933E-02 NOT IDENT. SN-113 -l.097E-01 2.372E-01 2.423E-01 NOT IDENT. CD-115 1. 272E+38 2.202E+39 O.OOOE+OO SHORT HLIF SN-117M -3.348E+04 9.125E+04 9.249E+04 SHORT HLIF TE-123M -1.092E-01 l.298E-01 1. 388E-01 NOT IDENT. SB-124 -9.972E-03 1.333E+OO 1. 333E+OO NOT IDENT. SB-125 -8.818E-03 1.124E-01 l.125E-01 FAIL ABUN TE-125M 2.608E+02 2.765E+02 3.005E+02 NOT IDENT. I-126 9.615E+05 l.045E+06 1.131E+06 SHORT HLIF SB-126 5.093E+05 l.112E+06 1.135E+06 SHORT HLIF SB-127 -1.559E+22 2.787E+22 O.OOOE+OO SHORT HLIF I-131 -3. 096E+09 4.371E+09 4.589E+09 SHORT HLIF I-132 1.000E+41 2.179E+43 O.OOOE+OO SHORT HLIF TE-132 6. 791E+25 3 .112E+26 O.OOOE+OO SHORT HLIF BA-133 -1.680E-02 4.205E-02 4.273E-02 NOT IDENT. I-133 -1.000E+41 4.789E+41 O.OOOE+OO SHORT HLIF CS-134 5.235E-03 4.819E-02 4.825E-02 NOT IDENT. I-135 -1.000E+41 7.403E+41 O.OOOE+OO SHORT HLIF CS-136 1. 611E+05 2.928E+05 3.017E+05 SHORT HLIF CE-139 2.759E-02 1.228E-01 1.235E-01 NOT IDENT. BA-140 8.039E+05 1.266E+06 1.317E+06 SHORT HLIF LA-140 -3.472E+04 2.156E+05 2.162E+05 SHORT HLIF CE-141 -2.715E+OO 2.561E+Ol 2.564E+Ol NOT IDENT. CE-143 1.000E+41 l.126E+41 O.OOOE+OO SHORT HLIF CE-144 -1.632E-01 3.536E-01 3.612E-01 NOT IDENT. PM-144 9.472E-04 5.455E-02 5.455E-02 NOT IDENT. PR-144 1.446E-01 4.746E+OO 4.746E+OO NOT IDENT. PM-146 -3.349E-02 4.777E-02 5.0lOE-02 NOT IDENT. ND-147 -1. 2 97E+07 *2.827E+07 2.887E+07 SHORT HLIF PM-147 3.068E+02 8.047E+02 8.165E+02 NOT IDENT. PM-149 -9.900E+39 3.373E+40 O.OOOE+OO SHORT HLIF EU-150 1.228E-02 . 2. 552E-02 2. 611E-02 FAIL ABUN EU-152 2.065E-02 9.906E-02 9.950E-02 NOT IDENT. GD-153 -3.455E-02 2.178E-01 2.184E-01 NOT IDENT. EU-154 -1.059E-01 9.814E-02 1.091E-01 NOT IDENT. EU-155 -3.636E-02 l.082E-01 1.095E-01 FAIL ABUN TB-160 2.603E+OO 3.093E+OO 3.308E+OO FAIL ABUN H0-166M 2.822E-02 5.409E-02 5.556E-02 FAIL ABUN TM-171 -7.373E+OO 2.695E+Ol 2.715E+Ol NOT IDENT. HF-172 7.132E-03 2.314E-01 2.315E-01 FAIL ABUN LU-172 8.715E-03 6.365E-02 6.378E-02 FAIL ABUN Page 3135 of 5809 LU-176 4 .116E-03 2. 251E-02 2.258E-02 FAIL ABUN HF-181 1.807E+OO 3.986E+OO 4.069E+00 NOT IDENT. TA-182 -3.295E-01 9.706E-01 9.819E-01 FAIL ABUN RE-183 1. 712E+OO 3.512E+OO 3. 596E+OO FAIL ABUN RE-184 1.509E+Ol 2.875E+Ol 2.954E+Ol FAIL ABUN W-188 -8.038E-01 1.136E+02 l.136E+02 FAIL ABUN IR-192 -1. 8 62E-01 3. 851E-01 3.941E-01 FAIL ABUN BI-207 4. 969E-02 5.135E-02 5.602E-02 FAIL ABUN PB-210 3.479E+OO 5.176E+OO 5.408E+OO NOT IDENT. BI-211 3.2:70E+OO 5.514E-01 l.574E+OO FAIL ABUN PB-211 1. 2 62E+OO 1.018E+OO l.166E+OO FAIL ABUN BI-212 9.324E-01 7.631E-01 8. 712E-01 FAIL ABUN RN-219 l.905E-02 3.800E-01 3.801E-01 FAIL ABUN RA-223 -2.012E-01 6.097E-01 6.164E-01 FAIL ABUN AC-227 -1.880E-02 2.417E-01 2.419E-01 FAIL ABUN TH-227 -1.880E-02 2.417E-01 2.419E-01 FAIL ABUN TH-229 l.531E-01 4.707E-01 4.757E-01 FAIL ABUN TH-231 -2.012E-01 6.097E-01 6.164E-01 FAIL ABUN PA-233 l.608E-02 5.092E-02 5.143E-02 FAIL ABUN PA-234 -1.947E-02 2.535E-01 2.537E-01 FAIL ABUN PA-234M -2.344E+OO 4.566E+OO 4.686E+OO NOT IDENT. NP-237 l.608E-02 5.092E-02 5.143E-02 FAIL ABUN NP-238 -1.000E+41 2.592E+41 O.OOOE+OO SHORT HLIF NP-239 l.453E-01 2.543E-01 2.626E-01 NOT IDENT. PU-239 5.633E+Ol 3.310E+02 3.320E+02 NOT IDENT. AM-241 -1. OOlE-01 1. 675E-01 1.735E-01 NOT IDENT. CM-243 6.895E-02 9.527E-02 l.002E-01 NOT IDENT. BK-247 -2.901E-02 7.869E-02 7.977E-02 NOT IDENT. CM-247 5.343E-03 3.534E-02 3.542E-02 NOT IDENT. CF-249 2.814E-02 3.792E-02 3.999E-02 FAIL ABUN CF-251 1.066E-01 1.187E-01 l.281E-01 NOT IDENT. Page 3136 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 55 .1871 87.09 100.1593 136.47 54.8256 45.60 63. 9396 87.57 100.2393 140.51 0.0000 46.54 45.2391 88.03 100.3156 143.76 73.0133 49.72 0.0000 88.34 100.3668 144.24 78.5901 51. 35 54.3427 88.47 100.3881 145.44 80.9187 51. 87 59.1808 89. 96 100.6333 152.43 63.7006 52.39 55.4288 1093.63 100.7440 153.25 0.0000 52.97 47.8468 91.11 0.0000 323.87 82.8672 53.44 46.9400 92.59 101. 0610 156.02 0.0000 54.07 47.9658 93.35 101.1829 158.56 0.0000 57.36 0.0000 94.56 101.3773 159.00 70.9317 57.53 58.9665 94.65 101. 3915 162.33 61. 7769 57.98 56.1207 94.67 101.3945 162.66 0.0000 59.27 77.6215 94.87 89.6970 163.33 78.0598 59.32 77.6297 97.43 88.6699 165.86 63.5281 59.54 77.6657 98.43 79.0934 176.31 68.8257 60. 96 70.1079 98.44 79.0946 176:60 0.0000 61.17 70.1386 99.53 77.1419 177.52 53.9809 62.93 77.2373 100 .11 64.6891 181.07 0.0000 63.29 77.2941 102.03 73.2481 181.52 49.2057 63.58 77.3397 103.18 64.9881 184.41 75.5676 64.28 94 .1155 103.37 53.4731 143.76 56.7505 66.73 78.8135 105.21 68.3380 193.51 56.0229 67.24 89.7399 105.31 71.5024 197.03 64.4120 125.81 89.8170 106.12 65.2707 198.01 48.0619 67.75 93.7780 106.47 62.1442 201.83 57.6492 69.67 80.2560 109.28 53.9365 203.43 65.9847 70.83 84.7363 111. 00 86.9342 205.31 51. 9371 72.81 93.0257 111. 76 0.0000 210.85 64.8599 72.87 93.0364 114.06 77.7262 215.65 57.2007 74.66 84. 0096 116. 30 0.0000 222 .11 59.9297 74.82 84.0346 116.74 66. 2596 227.09 49.3582 74.97 84.0577 119. 76 70.8244 227.38 55.3915 77 .11 84.3845 121.12 60.2037 228.16 0.0000 78.74 84.6300 121. 22 58.0614 228.18 44.5851 79.69 88.8090 121. 78 63.4847 116.74 44.5851 80.12 71.3702 122.06 61.3557 235.69 56.5984 80.19 0.0000 122.92 64.6587 235. 96 56.6115 80.57 70.0787 123.07 64. 6715 238.63 46.2023 81. 00 86.3151 265.00 72.2748 238.98 0.0000 81. 07 86.3255 125.81 68.1507 240.99 46.2939 81.75 95.8808 127.23 87.7839 242.00 46.3334 83.79 77.2449 127.91 71. 5906 244.70 47.2519 84.00 77.2722 129.30 78.2380 252.40 0.0000 85.43 99.8819 131.20 87.1436 252.80 38.1355 86.55 100. 0696 133. 02 73.1504 254.15 0.0000 86.79 100.1092 133.52 71.0114 256.23 41.1194 86.94 100.1346 136. 00 48.2183 260.90 0.0000 Page 3137 of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 31. 0463 355.39 0.0000 584.27 22.8821 264.80 43.0562 356.01 34.4305 595.83 0.0000 265.00 43.0625 364.49 0.0000 427.87 26.0518 268.22 39.8496 366.42 0.0000 602.52 0.0000 269.46 39.8887 372. 51 38.3546 604.72 19.5730 .270. 03 39.9063 375.05 30 .. 3739 607.14 17.0816 271.23 39.9434 377.52 33.1037 609.32 17.0975 273.65 0.0000 356.01 24.2496 610.33 17.1045 276.40 38.8484 388.16 27.9140 614.28 24.1885 277.37 45.1472 388.63 0.0000 618.01 20.1888 277.60 45.1549 391.69 38.8008 620. 36 7. 0729 278.00 45.1692 264.66 19.0492 621.93 15.1666 279.20 45.2098 401. 81 25.8693 630.19 0.0000 279.54 45.2219 402.40 25.8786 631.29 20. 3011 279.70 45.2274 404.85 25.9151 633.25 24.3809 280.46 45.2527 410.95 24.6374 634.78 0.0000 283.69 45.3625 413. 71 24.6758 635.95 21.3572 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 45.4208 423. 72 0.0000 645.85 15.3168 285.90 .0.0000 427.09 31. 3078 657.76 12.3125 287.50 49.7032 427.87 35.0065 657.90 0.0000 290.67 40.5313 433.94 26.8052 661.66 25.6917 293.27 0.0000 439.40 20.3954 664.57 0.0000 351. 93 33.0411 453.88 38.3065 666.33 0.0000 295. 96 33.0586 463.37 21.5967 666.50 0.0000 879.38 30.5735 468.07 33.8862 667.71 0.0000 299.98 34.4298 473.00 0.0000 677. 62 14.4785 300.09 34.4331 475.06 32 .1192 685.70 0.0000 300.13 34.4339 476.78 21.7469 695.00 0.0000 301.36 29.3586 477.60 28.3777 696.49 18.7522 302.85 38.3340 482.18 18.9624 696. 51 18.7522 256.23 40.9375 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18.7581 306.78 35.0242 497.08 23.8810 697.49 19.8017 308.46 31.6448 505.52 17.2661 702.65 17.7519 311. 90 28.2916 507.63 0.0000 706.68 20.9172 316.51 32.6825 511.00 27.8920 711. 68 13.6215 319.41 0.0000 514.00 21. 6714 720.70 0.0000 320.08 0.0000 514.00 21.6714 721. 93 0.0000 321.04 37.0983 520.40 13.5260 722.78 17.3614 323.87 43.5668 520.69 0.0000 722.91 23.6755 325.23 41. 5303 522.65 0.0000 723.31 23.6792 328.76 0.0000 527.90 0.0000 724 .19 17. 3708 333.37 33.0583 528.26 16.4867 727. 33 15.8099 333.97 30.0254 529.59 19.4084 733.00 12.6743 334.37 36.5620 529.87 0.0000 735.93 15.8600 338.28 39.2752 531.02 0.0000 333.97 16.9271 338.32 39.2761 537.26 0.0000 739.50 0.0000 311. 90 51.1316 546.56 0.0000 747.24 11.6790 340.48 51.1316 552.55 12.7509 748.06 13.8067 340.55 0.0000 563.25 17.7407 752.31 11.7005 344.28 41.1824 569.33 22.7314 753.82 0.0000 345.93 29.4725 946.00 22.7333 756.73 10.6539 351.06 16.7209 569.70 20.7582 756.80 10.6543 351.93 16.7301 583.19 22.8718 884.68 30.7629 Page 3138 of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 24.0500 1274.44 10.3597 1620.50 2.0021 766.42 14.4327 1001.03 16.1374 1621.92 6.0077 766.84 14.4349 1002.74 14.9921 1678.03 0.0000 772. 60 0.0000 1004.73 13.8467 1690.97 2.0295 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.0287 778.90 21.4771 1028.54 0.0000 1063.66 9.2686 783.70 0.0000 1037.84 11. 6488 1771.35 2.0601 785.37 9.6866 1038.76 0.0000 1791.20 0.0000 792.07 17.2611 631.29 9.6337 1808.65 3 .1111 794.95 18.3579 1048.07 0.0000 1810.72 0.0000 795.86 15.1234 1049.04 14.8989 1836.06 7.2948 810.06 9 .1185 1050.41 14.9041 810.29 9 .1191 1063.66 9. 67 94 344.28 11. 9422 1077.00 0.0000 810.76 11. 9435 1077.34 9.7156 815.77 0.0000 1085.87 8.8531 1048.07 0.0000 1093.63 8.8715 832.01 12.0299 1099.45 10.6626 834.85 15.3250 1112. 07 14.2646 835. 71 16.4246 1112. 84 12.4841 836.80 0.0000 1115. 54 9.9948 846.75 0.0000 1120.29 12.5089 '846.77 12.0890 1120. 55 12.5098 856.80 0.0000 1221.41 12.5123 860.56 12.1438 1129. 67 10.7490 871.09 11.0775 1131. 51 0.0000 873.19 11. 0852 1147.95 0.0000 875.33 0.0000 1173.23 11. 77 65 879.38 11.1072 1177. 95 10.8838 880.51 11.1112 1189.05 12.7336 883.24 6.6726 1204.77 14.6104 884.68 8.3444 1221.41 18.3386 889.28 6.6855 1231.02 12.8678 894.76 5.5809 1235.36 0.0000 898.04 6.7041 1238.28 14.7324 900.72 15. 0969 1260.41 0.0000 903.28 10.0726 1271. 87 12.0677 911. 20 7.8536 1274.44 13.0037 912.08 7.8559 1274.54 13. 0037 923.98 0.0000 1291.59 6.5283 926.50 11. 2728 1298.22 0.0000 929 .11 6.7693 1312 .11 o. o*ooo 937.49 13.5732 1332.49 8.4743 944.13 0.0000 1362.66 0.0000 946.00 11.3403 1365.19 6.6403 949.00 10.2155 1368.63 0.0000 667. 71 0.0000 1384.29 5.7162 962. 31 15.3847 1408.01 1. 9155 964. 08 10.2620 1457.56 0.0000 966 .17 10.2682 1460.82 7.7505 911. 20 10.2766 1489.16 5.8477 968.97 10.2766 1505.03 7.8232 983.53 0.0000 1584.12 5.9630 984.45 0.0000 1596.21 0.0000 Page 3139 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:11:59.40 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : Z-OCT-2016 11:02:08. Sample date 10-DEC-2015 11:25:00 Acquisition date : 3-0CT-2016 08:07:40. Sample ID G405235012 Sample quantity 1.54640E+02 GRAM Detector name GAM36 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.35 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 0 0 0 0 8 8 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3140 of 5809 Energy 63.37* 74.74* 77.05* 87.48 93.40* 129.39 186.31* 238.68* 241. 61 258.46 277.51 291.35 295.32* 328.80* 338.53 352.01* 450.55 463.41 511. 7 5* 533.47 537.32 545.07 554.96 563.51 583.39* 609.42* 623.55* 633 .11 643.35 661. 56 679.66 726.74 772.05 816.20 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 17 107 181 62 67 47 86 371 107 52 34 11 101 7 51 158 9 35 54 17 11 18 7 10 81 107 11 10 6 79 11 23 21 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 99 127 142 167 162 86 125 31 37 41 38 42 52 37 35 34 22 17 46 9 11 23 11 16 25 17 9 39 11 12 7 13 19 4 0.73' 0.99 1.15 1. 42 1. 53 1.16 1.19 1.20 2.19 2.58 0.73 2.01 0.82 0.65 1. 22 1.12 0.49 1. 48 2.88 2.38 1. 20 3.44 0.72 0.57 1. 60 1. 02 3.28 5.34 0.91 1. 29 1. 08 4.32 4.63 2 .17 126. 71 149.46 154.07 174.93 186.78 258.76 372.60 477.34 483.20 516.90 555.00 582.69 590.62 657.57 677.04 704.00 901.07 926.78 1023.44 1066.89 1074.59 1090.08 1109.86 1126.95 1166. 71 1218.76 1247.01 1266.13 1286.60 1323.02 1359.22 1453.35 1543.94 1632.23 124 146 146 170 182 255 367 474 474 511 552 577 588 653 673 699 897 921 1014 1062 1072 1081 1108 1119 1162 1214 1242 1256 1282 1317 1354 1446 1533 1628 6 4.70E-03 98.4 19 2.98E-02 19.0 19 5.02E-02 13.5 8 1. 72E-02 38. 4 10 1.85E-02 39.4 8 1. 31E-02 37. 3 13 2.39E-02 29.8 15 1. 03E-01 5. 8 15 2.98E-02 19.2 11 1.44E-02 27.8 8 9.35E-03 36.2 8 3.lOE-03105.0 8 2.81E-02 16.1 6 1.82E-03155.6 9 1.41E-02 25.5 9 4.40E-02 10.5 8 2.40E-03100.2 11 9.58E-03 28.5 24 1. 51E-02 40. 6 10 4.67E-03 42.5 8 2.94E-03 61.3 16 5.00E-03 65.0 6 1.96E-03 85.0 10 2.69E-03 89.9 10 2.25E-02 16.4 11 2.97E-02 12.6 9 3.05E-03 59.1 14 2.90E-03130.0 6 1.54E-03107.0 12 2.20E-02 14.3 10 3.00E-03 56.1 13 6.47E-03 38.0 20 5.83E-03 56.3 8 3.17E-03 42.1 Fit 7.00E-01 1.99E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235012 Acquisition date 3-0CT-2016 08:07:40 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 905.10* 5 7 1. 39 1809.98 1804 9 1.28E-03116.l 36 0 911.73* 53 3 1. 67 1823.23 1817 14 1. 4 6E-02 16.3 37 0 9.34. 67 14 10 0.67 1869.10 1861 14 3.78E-03 57.2 38 0 951. 55 10 1 0.91 1902.84 1900 6 2.69E-03 37.6 39 0 970.47 9 24 0.68 1940.67 1933 12 2.50E-03113.9 40 0 1000.30* 16 4 3.42 2000.31 1993 15 4.55E-03 37.1 41 0 1120. 98* 22 6 2.21 2241. 57 2235 11 5.99E-03 31. 0 42 0 1202.26 7 12 1. 35 2404.06 2397 10 1. 89E-03104. 0 43 0 1208.67 13 9 1. 04 2416.88 2409 12 3.59E-03 54.1 44 0 1377.98 10 2 0.64 2755.32 2752 7 2.81E-03 38.3 45 0 1461.19* 205 3 1. 98 2921. 64 2916 12 5.68E-02 7.3 46 0 1588. 72 11 0 1. 50 3176.55 3171 10 3.06E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 3141of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:12:01 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 10-DEC-2015 11:25:00 G405235012 Acquisition date : Sample quantity Sample geometry. : 3-0CT-2016 08:07:40 154.64 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3142 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.35 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235012 Acquisition date 3-0CT-2016 08:07:40 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 . 1460.82 10.66* 6. 545E-01. 1.377E+Ol l.377E+Ol 14.53 OK CD-109 88.03 3.70* 4.307E+OO l.439E+OO 2.252E+OO 131.26 OK SN-126 64.28 9.60 2.480E+OO 4.564E-01 4.564E-01 196.78 OK 86.94 8.90 4.307E+00 5.984E-01 5.984E-01 131.26 10K 87.57 37.00* 4.307E+OO 1.439E-01 1.439E-01 131.26 OK BA-137M 661. 66 89.90* 1.335E+OO 3.381E-01 3.445E-01 28.51 OK CS-137 661. 66 85.10* 1.335E+OO 3.572E-01 3.639E-01 28.51 OK TL-208 277.37 6.60 3.040E+OO 9.409E-01 9.409E-01 72.30 OK 583.19 85.00* l.496E+OO 3. 313E-01 3.313E-01 32. 72 OK 860.56 12.50 l.058E+OO Line Not Found Absent PB-212 74.82 10.28 3.476E+OO 1.297E+OO 1.297E+OO 57.70 OK 77 .11 17.10 3. 651E+OO 1.828E+OO 1.828E+OO 27.04 OK 238.63 43.60* 3.499E+OO 1.385E+OO 1.385E+OO 11. 62 OK 300.09 3.30 2.819E+OO Line Not Found Absent BI-214 609.32 45.49* l.437E+OO 8.468E-01 8. 471E-01 25.22 OK 1120.29 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 OK 1764.49 15.30 5.419E-01 Line Not Found Absent PB-214 74.82 5.80 3.482E+OO Line Not Found <<INT Reject 77.11 9.70 3.651E+OO 3.222E+OO 3.224E+OO 27.04 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 3.455E+OO Line Not Found <<INT Reject 295.22 18.42 2.863E+OO 1.068E+OO 1.069E+OO 32.17 OK 351. 93 35.60* 2.414E+OO 1.0lOE+OO l.OlOE+OO 21. 06 OK RN-222 609.32 45.49* l.437E+OO 8.468E-01 8.471E-01 25.22 OK 1120. 29 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 OK 1764.49 15.30 5.419E-01 Line Not Found Absent RA-224 240.99 4.10* 3.460E+OO 2.410E+OO 2.410E+OO 73.01 OK RA-226 609.32 45.49* l.437E+OO 8.468E-01 8.471E-01 25.22 OK 1120.29 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 OK 1764.49 15.30 5.419E-01 Line Not Found Absent AC-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.507E+OO 9. 861E-01 9.861E-01 51. 02 OK 794.95 4.25 l.134E+OO Line Not Found Absent 835.71 1. 61 1.085E+OO Line Not Found Absent 911. 20 25.80* 1.005E+OO 1.007E+OO 1.007E+OO 32.55 OK 968. 97 15.80 9.513E-01 2.947E-01 2.947E-01 227. 71 OK RA-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11.27 2.507E+OO 9. 861E-01 9.861E-01 51.02 OK 794.95 4.25 1.134E+OO Line Not Found Absent 835. 71 1. 61 1.085E+OO Line Not Found Absent 911. 20 25.80* l.005E+OO 1. 007E+OO 1.007E+OO 32.55 OK 968. 97 15.80 9.513E-01 2.947E-01 2.947E-01 227.71 OK TH-228 74.82 10.28 3.476E+OO 1. 297E+OO 1. 297E+OO 57.70 OK 77 .11 17.10 3.651E+OO 1.828E+OO 1.828E+OO 27.04 OK 238.63 43.60* 3.499E+OO 1.385E+OO 1.385E+OO 11. 62 OK 300.09 3.30 2.819E+OO Line Not Found Absent TH-230 609.32 45.49* 1.437E+OO 8.468E-01 8.469E-01 25.22 OK 1120.29 14.92 8.367E-01 8.359E-01 8.359E-01 62.02 OK 1764.49 15.30 5.419E-01 Line Not Found Absent Page 3143 of5809 Nuclide Line Activity Report (continued) Sample ID : G405235012 Acquisition date Nuclide Type: Nuclide TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Energy 105.21 338.32 835.71 911.20 968. 97 63.29 92. 59 609.32 1120.29 1764.49 63.29 92.59 43.53 74.66 511. 00 %Abn 1.10 11. 27 1. 61 25.80* 15.80 3.70* 4.23 45.49* 14.92 15.30 3.70* 4.23 5.90 67.20* 100.00* Flag: "*" Key line Page 3144 of 5809 %Eff Uncorrected Decay Corr pCi/GRAM pCi/GRAM 4.933E+OO Line Not Found 2.507E+OO 9.861E-01 9.861E-01 1.085E+OO Line Not Found 1.005E+OO 1.007E+OO 1.007E+OO 9.513E-01 2.947E-01 2.947E-01 2.480E+OO 1.184E+OO 1.184E+OO 4.581E+OO 2.132E+OO 2.132E+OO 1.437E+OO 8.468E-01 8.469E-01 8.367E-01 8.359E-01 8.359E-01 5.419E-01 Line Not Found 2.480E+OO 1.184E+OO 1.184E+OO 4.581E+OO 2.132E+OO 2.132E+OO 5.957E-01 Line Not Found 3.476E+OO 1.984E-01 1.984E-01 1.688E+OO 1.698E-01 1.698E-01 Page : 3 3-0CT-2016 08:07:40 2-Sigma %Error Status Absent 51. 02 OK Absent 32.55 OK 227.71 OK 196. 78 OK 78.87 OK 25.22 OK 62.02 OK Absent 196.78 OK 78.87 OK Absent 57.70 OK 81. 23 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:12:02.63 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l * *Acquisition date 3-0CT-2016 08:07:40 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.35 Half life ratio : ***** *
  • Sample date 10-DEC-2015 11:25:00 Analyst initials: MXRl *
  • Sample ID G405235012 Sample Quantity 1.5464E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.'GAMMA]EFF GAM36 CAN.CNF;?
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.377E+Ol 1. 961E+OO CD-109 2.252E+OO 2.897E+OO SN-126 l.439E-01 l.852E-01 BA-137M 3.445E-01 9.625E-02 CS-137 3.639E-01 l.017E-01 TL-208 3.313E-01 l.063E-01 PB-212 1.385E+OO l.577E-01 BI-214 8.471E-01 2.094E-01 PB-214 1.0lOE+OO 2.084E-01 RN-222 8.471E-01 2.094E-01 RA-224 2.410E+OO 1. 725E+OO RA-226 8.471E-01 2.094E-01 AC-228 1.007E+OO 3.212E-01 RA-228 1.007E+OO 3.212E-01 TH-228 l.385E+OO l.577E-01 TH-230 8.469E-01 2.093E-01 TH-232 1.007E+OO 3.212E-01 TH-234 1.184E+OO 2.284E+OO U-234 8.469E-01 2.093E-01 U-238 l.184E+OO 2.284E+OO AM-243 l.984E-01 1.122E-01 ANH-511 l.698E-01 1.351E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 3145 of5809 Key-Line Activity (pCi/GRAM -1. 388E+Ol -4.322E-02 O.OOOE+OO -l.009E-02 -2.551E-01 O.OOOE+OO O.OOOE+OO 5.323E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1.167E+Ol 6.347E-02 l.309E+41 3.228E-02 4.008E-01 l.782E+04 4.461E+02 7.878E-02 MDA (pCi/GRAM 9.078E-01 2.471E+OO 1.636E-01 9.705E-02 l.025E-01 8.861E-02 8.974E-02 l.368E-01 l.489E-01 1. 368E-01 9.638E-01 1. 368E-01 2.979E-01 2.979E-01 8.974E-02 l.367E-01 2.979E-01 2.343E+OO l.367E-01 2.343E+OO 9. 921E-02 5.931E-02 MDA (pCi/GRAM 1.922E+Ol l .137E-01 O.OOOE+OO 6.799E-02 6.887E-01 O.OOOE+OO O.OOOE+OO 1.761E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 -1.022E-01 5.833E-01 1.126E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 l.567E-02 4.796E-02 9.727E-02 NOT IDENT. C0-58 -5.616E-03 5.973E-01 1.18 6E+OO NOT IDENT. FE-59 -2.197E+OO 8.186E+OO 1.643E+Ol NOT IDENT. C0-60 -7.445E-03 4.669E-02 9.734E-02 NOT IDENT. ZN-65 6.894E-02 2.498E-01 4.909E-01 NOT IDENT. GE-68 -2.026E+OO 3.020E+OO 4. 966E+OO NOT IDENT. AS-73 8.629E+OO 7.399E+OO 1.691E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.435E+03 O.OOOE+OO SHORT.HLIF SE-75 l.056E-01 2.387E-Ol 4.740E-01 NOT IDENT. BR-77 O.OOOE+OO l.599E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.092E+02 0.000E+OO SHORT HLIF RB-83 8.669E-02 8.817E-01 1.657E+OO NOT IDENT. KR-85 8.653E+OO 8.540E+OO 1.925E+Ol NOT IDENT. SR-85 8.904E-01 8.831E-01 1.990E+OO NOT IDENT. RB-86 O.OOOE+OO 3.260E+04 0.000E+OO SHORT HLIF Y-88 -7.223E-02 2. 296E-01 4.815E-01 NOT IDENT. Y-91 -3.935E+02 1. 253E+03 l.410E+03 NOT IDENT. NB-94 1.658E-02 3.730E-02 8.045E-02 NOT IDENT. NB-95 8.572E-02 1.014E+OO 1. 876E+00 NOT IDENT. NB-95M -1.658E-01 2.526E+00 4.394E+00 NOT IDENT. ZR-95 3.502E-01 1.303E+OO 2.921E+OO NOT IDENT. NB-97 O.OOOE+OO 1.282E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 705E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.134E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 2.476E-02 3.333E-02 6.615E-02 NOT IDENT. RH-102 -1. 7 54E-03 8.764E-02 l.725E-01 NOT IDENT. RU-103 3.893E+OO 6.051E+OO 1.359E+Ol FAIL ABUN RH-106 -2.134E-01 6.580E-01 1.129E+OO NOT IDENT. RU-106 -2.134E-01 6.580E-01 l.129E+00 NOT IDENT. AG-108M -1.346E-02 3.256E-02 6.309E-02 NOT IDENT. AG-llOM -1. 380E-02 l.418E-01 2.742E-01 NOT IDENT. SN-113 -5.246E-02 2.639E-01 5.281E-01 NOT IDENT. CD-115 0.000E+OO 2.097E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 9.397E+04 0.000E+OO SHORT HLIF TE-123M -2.052E-02 1.345E-01 2.575E-01 NOT IDENT. SB-124 1.113E+OO 1.542E+OO 5.188E+OO NOT IDENT. SB-125 1.032E-02 1.210E-01 2.500E-01 FAIL ABUN TE-125M 1. 784E+02 2.554E+02 5.388E+02 NOT IDENT. I-126 O.OOOE+OO 9.810E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.519E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1. 962E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.892E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.348E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.982E+26 O.OOOE+OO SHORT HLIF BA-133 1.368E-02 4.688E-02 9.169E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 1. 758E-02 7.139E-02 l.451E-01 FAIL ABUN CS-135 -1.049E-01 1.661E-01 2.880E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.804E+05 0.000E+OO SHORT HLIF CE-139 -3.431E-02 l.090E-01 2.052E-01 NOT IDENT. BA-140 O.OOOE+OO l.828E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.106E+05 O.OOOE+OO SHORT HLIF CE-141 -1.837E+Ol 2.366E+Ol 4.177E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 2. 411E-01 3.828E-01 7.848E-01 NOT IDENT. PM-144 -1.160E-02 6.810E-02 1.324E-01 NOT IDENT. PR-144 -1.054E+OO 5. 901E+OO 1.146E+Ol NOT IDENT. PM-146 3.331E-02 5.304E-02 1.090E-01 FAIL ABUN ND-147 O.OOOE+OO 3.694E+07 O.OOOE+OO SHORT HLIF PM-147 -1. 006E+OO 8.159E+02 1.615E+03 NOT IDENT. PM-149 O.OOOE+OO 2.955E+40 O.OOOE+OO SHORT HLIF EU-150 2.220E-02 3 .178E-02 6.420E-02 FAIL ABUN EU-152 -5.809E-02 1. 118E-01 1.922E-01 NOT IDENT. GD-153 3.292E-02 1.939E-01 3.679E-01 NOT IDENT. EU-154 -1.lOOE-01 1.548E-01 2.750E-01 NOT IDENT. EU-155 -7.153E-03 1.lOlE-01 2.180E-01 FAIL ABUN TB-160 4.382E-01 2.210E+OO 4.647E+OO FAIL ABUN H0-166M -8.789E-03 6.146E-02 l.223E-01 NOT IDENT. TM-171 -3.869E+00 l.748E+Ol 3.616E+Ol NOT IDENT. HF-172 2.282E-02 2.297E-01 4. 271E-01 FAIL ABUN LU-172 3.835E-03 9.394E-02 l.893E-01 FAIL ABUN LU-176 -1.853E-03 2. 811E-02 5.236E-02 FAIL ABUN HF-181 l.758E-03 5.398E+OO l.091E+Ol NOT IDENT. TA-182 -7.022E-01 1.215E+OO 2.238E+OO FAIL ABUN Page 3146 of 5809 RE-183 9. 966E-Ol 2. 722E+OO 5.807E+OO NOT IDENT. RE-184 -2.399E-01 4.279E+Ol 7.563E+Ol NOT IDENT. W-188 1. 029E+02 2 .117E+02 2. 611E+02 FAIL ABUN IR-192 l.705E-01 5.551E-Ol l.079E+OO FAIL ABUN HG-203 2.766E-01 2.749E+OO 4.866E+OO NOT IDENT. BI-207 5.891E-02 7.431E-02 l.631E-01 FAIL ABUN PB-210 -l.426E+OO 2.486E+OO 5.002E+OO NOT IDENT. BI-211 O.OOOE+OO 5.741E-01 9.598E-01 FAIL ABUN PB-211 -3.359E-01 8.036E-01 1. 563E+OO NOT IDENT. BI--,212 1.444E+OO 1.076E+OO 1. 556E+OO FAIL ABUN RN-219 -9. 572E-03 4.406E-01 8.983E-01 NOT IDENT. RA-223 -1. 789E-Ol 7.173E-01 l.292E+OO FAIL ABUN AC-227 -6.853E-03 2.432E-01 4.280E-01 NOT IDENT. TH-227 -6.853E-03 2.432E-01 4.280E-01 NOT IDENT. TH-229 -1. 7 59E-01 5.134E-01 9.485E-01 FAIL ABUN PA-231 3.236E-01 5.254E-01 1.054E+OO NOT IDENT. TH-231 -l.789E-01 7.173E-01 1. 292E+OO FAIL ABUN PA-233 4.224E-02 6.304E-02 l.309E-01 NOT IDENT. PA-234 7.189E-02 4.086E-01 8.216E-01 FAIL ABUN PA-234M 1.032E+Ol 7.498E+OO 1. 271E+Ol FAIL ABUN U-235 3.330E-02 1.935E-01 3.735E-01 FAIL ABUN NP-237 4.224E-02 6.304E-02 1.309E-01 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 -5. 313E-02 2.280E-01 4.446E-01 FAIL ABUN PU-239 O.OOOE+OO 6.481E+02 7.164E+02 FAIL ABUN AM-241 l.825E-02 1.297E-01 2. 712E-01 NOT IDENT. CM-243 5.526E-02 9.585E-02 2.007E-01 FAIL ABUN BK-247 7.357E-03 8.605E-02 1.636E-01 NOT IDENT. CM-247 l.727E-02 3.941E-02 8.481E-02 FAIL ABUN CF-249 2.069E-02 4.089E-02 8.909E-02 NOT IDENT. CF-251 4.467E-02 1.232E-01 2.449E-01 NOT IDENT. Page 3147of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:12:00.24 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 198 10.66* 6.545E-01 1.377E+Ol l.377E+Ol 14.53 CD-109 88.03 80 3.70* 4.307E+OO 2.424E+OO 3.792E+OO 76.83 SN-126 64.28 22 9.60 2.480E+OO 4.564E-01 4.564E-01 196. 78 86.94 80 8.90 4.307E+OO 1.008E+OO 1.008E+OO 76.83 87.57 80 37.00* 4.307E+OO 2.424E-01 2.424E-01 76.83 BA-137M 661. 66 84 89.90* 1.335E+OO 3.381E-01 3.445E-01 28.51 CS-137 661. 66 84 85.10* 1.335E+OO 3. 572E-01 3.639E-01 28.51 TL-208 277.37 39 6.60 3.040E+OO 9.409E-01 9.409E-01 72.30 583.19 87 85.00* l.496E+OO 3.313E-01 3.313E-01 32. 72 860.56 ------12.50 1.058E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 3.327E+OO ------Line Not Found ------351.06 179 12.92* 2.414E+OO 2.782E+OO 2.782E+OO 21. 06 PB-212 74.82 140 10.28 3.476E+OO 1.899E+OO 1.899E+OO 38.04 77 .11 235 17.10 3.651E+OO 1.828E+OO 1. 828E+00 27.04 238.63 435 43.60* 3.499E+OO 1.385E+OO 1.385E+OO 11. 62 300.09 ------3.30 2.819E+OO ------Line Not Found ------BI-214 609.32 114 45.49* l.437E+OO 8.468E-01 8.471E-01 25.22 1120.29 21 14.92 8.367E-01 8.359E-01 8.362E-01 62. 02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------PB-214 74.82 140 5.80 3.476E+OO 3.367E+OO 3.368E+OO 38.04 77 .11 235 9.70 3. 651E+OO 3.222E+OO 3.224E+OO 27.04 87.09 80 3.41 4.307E+00 2.630E+OO 2. 631E+OO 76.83 242.00 126 7.25 3.460E+OO 2.432E+OO 2.432E+OO 38.41 295.22 116 18.42 2.863E+OO 1.068E+OO l.069E+OO 32.17 351.93 179 35.60* 2.414E+OO 1.0lOE+OO 1.0lOE+OO 21. 06 RN-222 609.32 114 45.49* l.437E+OO 8.468E-01 8. 471E-01 25.22 1120.29 21 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------RA-224 240.99 126 4.10* 3.460E+OO 4.300E+OO 4.300E+OO 38.41 RA-226 609.32 114 45.49* l.437E+00 8.468E-01 8. 471E-01 25.22 1120.29' 21 14.92 8.367E-01 8.359E-01 8.362E-01 62.02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------AC-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 57 11. 27 2.507E+OO 9.861E-01 9.861E-01 51. 02 794.95 ------4.25 1.134E+OO ------Line Not Found ------835. 71 ------1. 61 1.085E+OO ------Line Not Found ------911. 20 54 25.80* 1.005E+OO 1.007E+OO 1.007E+OO 32.55 968. 97 9 15.80 9.513E-01 2.947E-01 2.947E-01 227.71 RA-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 57 11. 27 2.507E+00 9.861E-01 9.861E-01 51. 02 794.95 ------4.25 1.134E+OO ------Line Not Found ------835. 71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 54 25.80* 1.005E+OO 1.007E+OO 1.007E+OO 32.55 968.97 9 15.80 9.513E-01 2.947E-01 2.947E-01 227.71 TH-228 74.82 140 10.28 3.476E+OO 1. 899E+OO l.899E+OO 38.04 77 .11 235 17.10 3.651E+OO 1.828E+OO 1.828E+OO 27.04 238.63 435 43.60* 3.499E+OO 1.385E+OO 1.385E+OO 11. 62 Page 3148 of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235012 Acquisition date 3-0CT-2016 08:07:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 300.09 ------3.30 2.819E+OO ------Line Not Found ------TH-230 609.32 114 45.49* 1.437E+OO 8.468E-01 8.469E-01 25.22 1120.29 21 14.92 8.367E-01 8.359E-01 8.359E-01 62.02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------TH-232 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 57 11. 27 2.507E+OO 9.861E-01 9.861E-01 51. 02 835. 71 ------1. 61 l.085E+OO ------Line Not Found ------911. 20 54 25.80* 1.005E+OO 1.007E+OO 1.007E+OO 32.55 968. 97 9 15.80 9.513E-01 2.947E-01 2.947E-01 227.71 TH-234 63.29 22 3.70* 2.480E+OO 1.184E+OO 1.184E+OO 196.78 92.59 85 4.23 4.581E+OO 2.132E+OO 2.132E+OO 78.87 U-234 609.32 114 45.49* 1.437E+OO 8.468E-01 8.469E-01 25.22 1120.29 21 14.92 8.367E-01 8.359E-01 8.359E-01 62.02 1764.49 ------15.30 5.419E-01 ------Line Not Found ------U-238 63.29 22 3.70* 2.480E+OO 1.184E+OO l.184E+OO 196.78 92.59 85 4.23 4.581E+OO 2 .132E+OO 2.132E+OO 78.87 AM-243 43.53 ------5.90 5.957E-01 ------Line Not Found ------74.66 140 67.20* 3.476E+OO 2.906E-01 2.906E-01 38.04 ANH-51'1 511. 00 59 100.00* 1.688E+OO 1.698E-01 1.698E-01 81.23 Flag: "*" Key line Page 3149 of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235012 Acquisition date 3-0CT-2016 08:07:40 Total number of lines in spectrum 46 Number of unidentified lines 14 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1.41E+10Y 1600. OOY 1600. OOY 1600.00Y 1. 41E+10Y 1600.00Y 1. 41E+10Y 1. 41E+10Y *1. 41E+l0Y 7.54E+04Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 56 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.377E+Ol 2.424E+OO 2.424E-01 3.381E-01 3.572E-01 3. 313E-01 2.782E+OO 1.385E+OO 8.468E-01 1.0lOE+OO 8.468E-01 4.300E+OO 8.468E-01 1.007E+OO 1.007E+OO 1.385E+OO 8.468E-01 1.007E+OO 1.184E+OO 8.468E-01 l.184E+OO 2.906E-01 1.698E-01 3.841E+Ol 3. 841E+Ol Decay Corr pCi/GRAM 1.377E+Ol 3.792E+OO 2.424E-01 3.445E-01 3.639E-01 3.313E-01 2.782E+OO 1.385E+OO 8.471E-01 1.0lOE+OO 8. 471E-01 4.300E+00 8. 471E-01 1.007E+OO 1.007E+OO 1.385E+OO 8.469E-01 1.007E+OO 1.184E+OO 8.469E-01 1.184E+OO 2.906E-01 1.698E-01 3.979E+Ol 3.979E+Ol 69.57% Decay Corr 2-Sigma Error 0.200E+Ol 2.914E+OO 1. 863E-01 0.982E-01 l.037E-01 1.084E-01 0.586E+OO 0.161E+OO 2.136E-01 0.213E+OO 2.136E-01 1. 651E+OO 2.136E-01 0.328E+OO 0.328E+OO 0.161E+OO 2.136E-01 0.328E+OO 2.330E+OO 2.136E-01 2.330E+00 1.105E-01 1. 379E-01 "M" Manually accepted 2-Sigma %Error 14.53 76.83 76.83 28.51 28.51 32. 72 21. 06 11. 62 25.22 21. 06 25.22 38.41 25.22 32.55 32.55 11. 62 25.22 32.55 196.78 25.22 196.78 38.04 81. 23 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3150 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235012 Acquisition date : 3-0CT-2016 08:07:40 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.39 59 107 1.16 258.76 255 8 1. 31E-02 74.5 5.08E+OO T 0 186.31 103 150 1.19 372.60 367 13 2.39E-02 59.5 4.29E+OO T 0 258.46 60 48 2.58 516.90 511 11 1.44E-02 55.6 3.25E+OO 0 291.35 13 48 2.01 582.69 577 8 3. lOE-.03 **** 2.90E+OO T 0 328.80 7 42 0.65 657.57 653 6 1.82E-03 **** 2.58E+OO T 0 450.55 10 25 0.49 901.07 897 8 2.40E-03 **** 1. 90E+OO 0 463.41 38 18 1. 48 92 6. 78 921 11 9.58E-03 56.9 1.85E+OO T 0 533.47 18 10 2.38 1066.89 1062 10 4.67E-03 85.0 1. 62E+OO 0 537.32 11 12 1.20 1074.59 1072 8 2.94E-03 **** 1. 61E+OO T 0 545.07 19 25 3.44 1090.08 1081 16 5.00E-03 **** 1.59E+OO T 0 554. 96 8 12 0. 72 1109.86 1108 6 1. 96E-03 **** 1.57E+OO 0 563.51 10 18 0.57 1126.95 1119 10 2.69E-03 **** 1.54E+OO T 0 623.55 12 9 3.28 1247.01 1242 9 3.05E-03 **** 1.41E+OO 0 633 .11 11 41 5.34 1266.13 1256 14 2.90E-03 **** 1.39E+OO T 0 643.35 6 12 0.91 1286.60 1282 6 1. 54E-03 **** 1.37E+OO 0 679.66 11 8 1. 08 1359.22 1354 10 3.00E-03 **** l.30E+OO 0 726.74 24 13 4.32 1453.35 1446 13 6.47E-03 76.0 1.23E+OO T 0 772. 05 22 20 4.63 1543.94 1533 20 5.83E-03 **** 1.16E+OO T 0 816.20 12 4 2.17 1632.23 1628 8 3 .17E-03 84.1 1. llE+OO T 0 905.10 5 7 1. 39 1809.98 1804 9 1.28E-03 **** 1. OlE+OO 0 934.67 14 11 0.67 1869.10 1861 14 3.78E-03 **** 9.83E-01 0 951. 55 10 1 0.91 1902.84 1900 6 2.69E-03 75.2 9.68E-01 0 1000.30 17 4 3.42 2000.31 1993 15 4.55E-03 74.2 9.26E-01 T 0 1202.26 7 12 1. 35 2404.06 2397 10 1.89E-03 **** 7.85E-01 0 1208.67 13 9 1. 04 2416.88 2409 12 3.59E-03 **** 7.82E-01 0 1377. 98 10 2 0.64 2755.32 2752 7 2.81E-03 76. 7 6.92E-01 0 1588.72 11 0 1. 50 3176.55 3171 10 3.06E-03 60.3 6.03E-01 Flags: "T" = Tentatively associated Page 3151of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:12:15.07 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l * *Acquisition date 3-0CT-2016 08:07:40 Sensitivity 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.35 Half life ratio : ***** *
  • Sample date 10-DEC-2015 11:25:00 Nuclide Library : SOLID *
  • Sample ID G405235012 Ana1yst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.5464E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 3. 591E-01 1.167E+00 7.735E-02 4.279E-02 4.521E-02 3.898E-02 4.033E-02 6.647E-02 5.802E-02 4.332E-01 5.802E-02 1.231E-01 1. 231E-01 4.033E-02 5.BOOE-02 1. 231E-01 1.093E+OO 5.BOOE-02 1.093E+OO 4.656E-02 2.563E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 3152 of 5809 Le (pCi/GRAM 7.856E+OO 4.574E-02 0.000E+OO 2.149E-02 2.676E-01 O.OOOE+OO O.OOOE+OO 7.609E-02 4. 723E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3153of5809 O.OOOE+OO 4.519E-02 4.812E-01 6.780E+OO 3.833E-02 2.089E-01 1.971E+OO 7.853E+OO O.OOOE+OO 2.163E-01 O.OOOE+OO O.OOOE+OO 7.287E-01 8.642E+OO 8.932E-01 O.OOOE+OO l.522E-01 5.940E+02 3.489E-02 7. 931E-01 1.999E+OO 1.198E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.067E-02 7'.618E-02 5. 965E+OO 4.804E-01 4.804E-01 2.772E-02 1.167E-01 2.350E-01 O.OOOE+OO O.OOOE+OO l.188E-01 l.838E+OO 1.109E-01 2.504E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.096E-02 O.OOOE+OO 6.342E-02 1.302E-01 O.OOOE+OO O.OOOE+OO 9.416E-02 O.OOOE+OO O.OOOE+OO 1.920E+Ol O.OOOE+OO 3.666E-01 5.682E-02 4.914E+OO 4.835E-02 O.OOOE+OO 7.476E+02 O.OOOE+OO 2.924E-02 8.517E-02 1.718E-01 l.103E-01 1.014E-01 1.950E+OO 5 .117E-02 1.662E+Ol 1.970E-01 7.791E-02 2.352E-02 4.836E+OO 9.259E-01 2.700E+OO SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3154of5809 3.189E+Ol l.192E+02 4.885E-01 2.198E+OO 7.120E-02 2.298E+00 4.581E-01 6.957E-01 6.956E-01 4.004E-01 5.800E-01 l.918E-01 1.918E-01 4.365E-01 4.813E-01 5.800E-01 5.886E-02 3.535E-01 5.496E+OO l.739E-01 5.886E-02 O.OOOE+OO 2.048E-01 3.363E+02 1. 262E-01 9.330E-02 7.457E-02 3.793E-02 3.981E-02 l.134E-01 NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:12:20.75 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235012.CNF;l *
  • Acquisition date 3-0CT-2016 08:07:40 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.35 Half life ratio : ***** *
  • Sample date 10-DEC-2015 11:25:00 Nuclide Library : SOLID *
  • Sample ID G405235012 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.5464E+02 GRAM *
  • Quantity Err(%) : 1.2933E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 'Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1.377E+Ol 2.089E+OO 2.089E+OO CD-109 2.252E+OO 2.909E+OO 2.909E+OO SN-126 l.439E-01 l.858E-01 1.858E-01 BA-137M 3.445E-01 9.738E-02 9.738E-02 CS-137 3.639E-01 1. 029E-01 1.029E-01 TL-208 3.313E-01 l.072E-01 l.072E-01 PB-212 1.385E+OO 1.738E-01 1.738E-01 BI-214 8.471E-01 2.125E-01 2.125E-01 PB-214 1.0lOE+OO 2.126E-01 2.126E-01 RN-222 8.471E-01 2.125E-01 2.125E-01 RA-224 2.410E+OO 1.734E+OO 1. 734E+OO RA-226 8.471E-01 2.125E-01 2.125E-01 AC-228 l.007E+OO 3.253E-01 3.253E-01 RA-228 1.007E+OO 3.253E-01 3.253E-01 TH-228 1.385E+OO 1.738E-01 1.738E-01 TH-230 8.469E-01 2.124E-01 2.124E-01 TH-232 l.007E+OO 3.253E-01 3.253E-01 TH-234 l.184E+OO 2.299E+OO 2.299E+OO U-234 8.469E-01 2.124E-01 2.124E-01 U-238 1.184E+OO 2.299E+OO 2.299E+OO AM-243 l.984E-01 l.134E-01 l.134E-01 ANH-511 l.698E-01 l.353E-01 l.353E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-si'gma) (1.96-sigma) BE-7 -l.388E+Ol l.169E+Ol l.326E+Ol NOT IDENT. NA-22 -4.322E-02 6.349E-02 6. 641E-02 NOT IDENT. NA-24 l.OOOE+41 1.379E+41 O.OOOE+OO SHORT HLIF AL-26 -1.009E-02 3.229E-02 3.261E-02 NOT IDENT. SC-46 -2.551E-01 4.0lOE-01 4. l 71E-01 FAIL ABUN V-48 8.315E+03 l.782E+04 l.821E+04 SHORT HLIF CR-51 -4.712E+02 4.466E+02 4.945E+02 SHORT HLIF MN-54 5.323E-02 7.881E-02 8.238E-02 NOT IDENT. Page 3155 of5809 C0-56 -l.022E-01 5.833E-01 5.852E-01 NOT IDENT. MN-56 -l.000E+41 6.027E+41 O.OOOE+OO SHORT HLIF C0-57 l.567E-02 4. 796E-02 4.848E-02 NOT IDENT. C0-58 -5.616E-03 5.973E-01 5.973E-01 NOT IDENT. FE-59 -2.197E+OO 8.187E+OO 8.247E+OO NOT IDENT. C0-60 -7.445E-03 4.669E-02 4.681E-02 NOT IDENT. ZN-65 6.894E-02 2.498E-01 2.517E-01 NOT IDENT. GE-68 -2.026E+OO 3.021E+OO 3.157E+OO NOT IDENT. AS-73 8.629E+OO 7.609E+OO 8.546E+OO NOT IDENT. AS-74 3.007E+03 5.441E+03 5.607E+03 SHORT HLIF SE-75 1. 056E-01 2.388E-01 2.435E-01 NOT IDENT. BR-77 l.404E+38 1. 207E+39 O.OOOE+OO SHORT HLIF SR-82 2.194E+02 7.092E+02 7 .161E+02 SHORT HLIF RB-83 8.669E-02 8.818E-01 8.827E-01 NOT IDENT. KR-85 8.653E+OO 8.547E+OO 9.395E+OO NOT IDENT. SR-85 8.904E-01 8.838E-01 9.707E-01 NOT IDENT. RB-86 -1. 7 93E+04 3.261E+04 3.360E+04 SHORT HLIF Y-88 -7.223E-02 2.297E-01 2.320E-01 NOT IDENT. Y-91 -3.935E+02 l.253E+03 l.265E+03 NOT IDENT. NB-94 l.658E-02 3.731E-02 3.805E-02 NOT IDENT. NB-95 8. 572E-02 l.014E+00 l.015E+OO NOT IDENT. NB-95M -l.658E-01 2.526E+00 2.527E+OO NOT IDENT. ZR-95 3.502E-01 l.303E+OO l.313E+OO NOT IDENT. NB-97 l.OOOE+41 1. 283E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 1. 705E+41 O.OOOE+OO SHORT HLIF M0-99 -4.920E+30 l .134E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 2.885E+41 O.OOOE+OO SHORT HLIF RH-101 2.476E-02 3.363E-02 3.543E-02 NOT IDENT. RH-102 -l.754E-03 8.764E-02 8.765E-02 NOT IDENT. RU-103 3.893E+OO 6.053E+OO 6.303E+OO FAIL ABUN RH-106 -2.134E-01 6.581E-01 6.651E-01 NOT IDENT. RU-106 -2.134E-01 6.581E-01 6.651E-01 NOT IDENT. AG-108M -1. 34 6E-02 3.257E-02 3.313E-02 NOT IDENT. AG-llOM -l.380E-02 1. 418E-01 l.420E-01 NOT IDENT. SN-113 -5.246E-02 2.639E-01 2.650E-01 NOT IDENT. CD-115 l.366E+39 2 .111E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -4.365E+04 9.411E+04 9.615E+04 SHORT HLIF TE-123M -2.052E-02 l.345E-01 l.348E-01 NOT IDENT. SB-124 l .113E+OO l.543E+OO l.623E+OO NOT IDENT. SB-125 l.032E-02 l.210E-01 l.211E-01 FAIL ABUN TE-125M l.784E+02 2.556E+02 2.680E+02 NOT IDENT. I-126 l.202E+06 9.944E+05 l.132E+06 SHORT HLIF SB-126 9.405E+05 l.529E+06 l.587E+06 SHORT HLIF SB-127 -5. 551E+21 2.103E+22 O.OOOE+OO SHORT HLIF I-131 4.133E+09 4. 896E+09 5.238E+09 SHORT HLIF I-132 -l.OOOE+41 1. 841E+42 O.OOOE+OO SHORT HLIF TE-132 -l.162E+26 3.019E+26 O.OOOE+OO SHORT HLIF BA-133 l.368E-02 4.689E-02 4. 729E-02 FAIL ABUN I-133 -l.OOOE+41 4.249E+41 O.OOOE+OO SHORT HLIF CS-134 l.758E-02 7.139E-02 7.183E-02 FAIL ABUN CS-135 -l.049E-01 l.662E-01 1. 728E-01 NOT IDENT. I-135 -l.OOOE+41 7 .196E+41 O.OOOE+OO SHORT HLIF CS-136 2. 513E+o5 4.812E+05 4.943E+05 SHORT HLIF CE-139 -3. 431E-02 l.092E-01 l.103E-01 NOT IDENT. BA-140 l.521E+06 l.829E+06 l.953E+06 SHORT HLIF LA-140 9 .148E+o4 3.107E+05 3 .134E+05 SHORT HLIF CE-141 -l.837E+Ol 2.367E+Ol 2.508E+Ol NOT IDENT. CE-143 l.OOOE+41 2.575E+41 O.OOOE+OO SHORT HLIF CE-144 2. 411E-01 3.830E-01 3. 981E-01 NOT IDENT. PM-144 -l.160E-02 6. 811E-02 6. 831E-02 NOT IDENT. PR-144 -l.054E+OO 5.901E+00 5.920E+OO NOT IDENT. PM-146 3. 331E-02 5.310E-02 5.518E-02 FAIL ABUN ND-147 -3.489E+06 3.694E+07 3.697E+07 SHORT HLIF PM-147 -l.006E+OO 8.159E+02 8.159E+02 NOT IDENT. PM-149 -2.189E+40 2.993E+40 O.OOOE+OO SHORT HLIF EU-150 2.220E-02 3.179E-02 3.333E-02 FAIL ABUN EU-152 -5.809E-02 l.118E-01 l.149E-01 NOT IDENT. GD-153 3.292E-02 l.939E-01 l.945E-01 NOT IDENT. EU-154 -l.lOOE-01 l.548E-01 l.626E-01 NOT IDENT. EU-155 -7.153E-03 l.lOlE-01 l.lOlE-01 FAIL ABUN TB-160 4.382E-01 2. 211E+OO 2.219E+OO FAIL ABUN H0-166M -8.789E-03 6.146E-02 6.159E-02 NOT IDENT. TM-171 -3.869E+OO l.748E+Ol l.757E+Ol NOT IDENT. HF-172 2.282E-02 2.298E-01 2.300E-01 FAIL ABUN LU-172 3.835E-03 9.394E-02 9. 396E-02 FAIL ABUN LU-176 -l.853E-03 2.811E-02 2.812E-02 FAIL ABUN HF-181 1. 758E-03 5.398E+OO 5.398E+OO NOT IDENT. TA-182 -7.022E-01 l.216E+00 l.256E+OO FAIL ABUN Page 3156 of5809 RE-183 9. 966E-01 2.726E+OO 2.763E+OO NOT IDENT. RE-184 -2.399E-01 4.279E+Ol 4.279E+Ol NOT IDENT. W-188 1.029E+02 2.120E+02 2 .171E+02 FAIL ABUN IR-192 1.705E-01 5.552E-01 5.605E-01 FAIL ABUN HG-203 2.766E-01 2.749E+OO 2.751E+OO NOT IDENT. BI-207 5. 891E-02 7.435E-02 7.895E-02 FAIL ABUN PB-210 -1. 42 6E+00 2.489E+OO 2.571E+OO NOT IDENT. BI-211 2.782E+OO 5.873E-01 1.385E+OO FAIL ABUN PB-211 -3.359E-01 8.038E-01 8.179E-01 NOT IDENT. BI-212. 1.444E+OO 1. 078E+OO 1.259E+OO FAIL ABUN RN-219 -9.572E-03 4.406E-01 4.406E-01 NOT IDENT. RA-223 -1. 789E-01 7.173E-01 7.219E-01 FAIL ABUN AC-227 -6.853E-03 2.432E-01 2.432E-Ol NOT IDENT. TH-227 -6.853E-03 2.432E-01 2.432E-01 NOT IDENT. TH-229 -1. 7 59E-01 5.135E-01 5.195E-Ol FAIL ABUN PA-231 3.236E-01 5.299E-01 5.496E-01 NOT IDENT. TH-231 -1. 789E-01 7.173E-01 7.219E-01 FAIL ABUN PA-233 4.224E-02 6.307E-02 6.589E-02 NOT IDENT. PA-234 7.189E-02 4.168E-01 4.181E-01 FAIL ABUN PA-234M 1. 032E+Ol 7.512E+OO 8.835E+OO FAIL ABUN U-235 3.330E-02 1.935E-01 1.941E-01 FAIL ABUN NP-237 4.224E-02 6.307E-02 6.589E-02 FAIL ABUN NP-238 1.000E+41 2.226E+41 O.OOOE+OO SHORT HLIF NP-239 -5. 313E-02 2.280E-01 2.293E-01 FAIL ABUN PU-239 8.872E+02 6.493E+02 7.626E+02 FAIL ABUN AM-241 1.825E-02 l.297E-01 l.299E-01 NOT IDENT. CM-243 5.526E-02 9.599E-02 9.917E-02 FAIL ABUN BK-247 7.357E-03 8.607E-02 8.613E-02 NOT IDENT. CM-247 1. 727E-02 3.952E-02 4.028E-02 FAIL ABUN CF-249 2.069E-02 4.093E-02 4.198E-02 NOT IDENT. CF-251 4.467E-02 l.233E-01 l.249E-01 NOT IDENT. Page 3157of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 22.6668 87.09 101. 37 52 136.47 51.2710 45.60 47.2366 87.57 101.4831 140.51 0.0000 46.54 46.5986 88.03 95.4023 143.76 55.7815 49.72 0.0000 88.34 95.4673 144.24 49.9471 51. 35 48.1423 88.47 96.6735 145.44 57.8900 51. 87 47.4180 89. 96 81.6125 152.43 64.4565 52.39 47.4955 1093.63 95.9473 153.25 0.0000 52.97 37.9040 91.11 0.0000 323.87 52.6959 53.44 35.5365 92.59 76.7224 156.02 0.0000 54.07 54.2174 93.35 76.8464 158.56 0.0000 57.36 0.0000 94.56 77.0425 159.00 51. 0646 57.53 67.8678 94.65 77.0570 162.33 47.2847 57.98 51. 5819 94.67 77.0603 162.66 0.0000 59.27 54.2413 94.87 50.1997 163.33 53.3971 59.32 54.2491 97.43 54.0715 165.86 47.5214 59.54 56. 7511 98.43 51.4732 176.31 54.3619 60. 96 67.1668 98.44 51.4745 176.60 0.0000 61.17 53.9858 99.53 56 .1137 177.52 45.2038 62.93 65.6012 100 .11 52.5550 181.07 0.0000 63.29 65.6664 102.03 57.3052 181.52 46.8206 63.58 65. 7190 103.18 48.3192 184.41 37.3217 64.28 68.9016 103.37 47.4253 143.76 37.3848 66.73 62. 9265 105.21 60.4107 193.51 51. 3918 67.24 66.3724 105.31 60.4228 197.03 46.3499 125.81 63.0850 106.12 60.5175 198.01 36.9141 67.75 63. 0964 106.47 61. 4763 201.83 33.9077 69.67 50.7317 109.28 44.2800 203.43 53.0838 70.83 71.2358 111. 00 48.1255 205.31 46.8192 72.81 60.2305 111.76 0.0000 210.85 51.4124 72. 87 60. 2396 114.06 49.3305 215.65 39.8522 74.66 77.9192 116. 30 0.0000 222 .11 41.2326 74.82 77.9497 116.74 50. 5072 227.09 40. 3722 74.97 77.9789 119.76 48.9004 227.38 46.9341 77.11 78.3864 121.12 45.2476 228.16 0.0000 78.74 78.6933 121.22 51.8554 228.18 41.5138 79.69 78.8710 121. 78 48.1312 116.74 41.5138 80.12 78.9509 122.06 50.9875 235.69 35.2471 80.19 0.0000 122.92 50 .1185 235. 96 41.1335 80.57 79.0342 123.07 50.1315 238.63 26.5192 81. 00 79.1140 265.00 51.1317 238.98 0.0000 81. 07 79.1265 125.81 45.6176 240.99 26.5858 81. 75 71. 9946 127.23 39.3768 242.00 26.6144 83.79 70.0000 127.91 48.3243 244.70 31.1385 84.00 91. 0436 129.30 58.3165 252.40 0.0000 85.43 93.6808 131. 20 56.2649 252.80 25.7939 86.55 101.2532 133.02 50. 0211 254.15 0.0000 86.79 101.3067 133.52 53. 9133 256.23 25.5090 86.94 101.3409 136.00 54 .1321 260.90 0.0000 Page 3158of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 29.5087 355.39 0.0000 584.27 18.0336 264.80 29.5126 356.01 19.6787 595.83 0.0000 265.00 34.0594 364.49 0.0000 427.87 8.6158 268.22 41.0010 366.42 0.0000 602.52 0.0000 269.46 34. 2096 372. 51 22.4231 604.72 17.2683 278.03 33.0870 375.05 12.4814 607.14 8.6448. 271.23 21.7032 377.52 24.1755 609.32 10.5779 273.65 0.0000 356.01 15.9141 610.33 10.5833 276.40 18.3677 388.16 17.6453 614.28 17.3533 277.37 26.4281 388.63 0.0000 618.01 15.0681 277.60 26.4337 391.69 24.4304 620. 36 8.7034 278.00 26.4442 264.66 21.1980 621.93 13.0655 279.20 27.6255 401.81 22.9131 630.19 0.0000 279.54 27.6343 402.40 18.6775 631.29 19.4474 279.70 23.0322 404.85 25.5139 633.25 19.4661 280.46 24.5853 410.95 17.9371 634.78 0.0000 283.69 21. 9630 413.71 23. 9622 635.95 11. 6953 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 32.4186 423.72 0.0000 645.85 8.8143 285.90 0.0000 427.09 15.5475 657.76 7.3880 287.50 20.1078 427.87 19.8770 657.90 0.0000 290.67 26.7601 433.94 22.5622 661. 66 18.7511 293.27 0.0000 439.40 19.1609 664.57 0.0000 351.93 30.3767 453.88 13.1894 666.33 0.0000 295. 96 30.3965 463.37 15.9243 666.50 0.0000 879.38 43.7500 468.07 22.6274 667. 71 0.0000 299.98 37.5479 473.00 0.0000 677.62 13.4247 300.09 38. 7253 475.06 12.4779 685.70 0.0000 300.13 38.7263 476.78 16.0602 695.00 0.0000 301.36 27.0205 477.60 17.8536 696.49 14.0450 302.85 30.5862 482.18 20.5901 696. 51 14.0450 256.23 20.0277 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.0501 306.78 27.1518 497.08 10.8411 697.49 11. 0403 308.46 20.0983 505.52 12.2583 702.65 10.0602 311. 90 17.7873 507.63 0.0000 706.68 10.0789 316.51 26.1921 511. 00 13.6647 711.68 10.1017 319.41 0.0000 514.00 13.6890 720.70 0.0000 320.08 0.0000 514.00 13.6890 721. 93 0.0000 321.04 26.2942 520.40 15 .1143 722.78 15.2283 323.87 29.9522 520.69 0.0000 722. 91 18.2747 325.23 33.5850 522.65 0.0000 723.31 18.2783 328.76 0.0000 527.90 0.0000 724.19 18.2856 333.37 26.5681 528.26 12.1467 727.33 11.1902 333.97 24.1650 529.59 19.3389 733.00 10.1982 334.37 29.0076 529.87 0.0000 735.93 14. 2962 338.28 21.8260 531. 02 0.0000 333.97 6 .1311 338.32 21. 8265 537.26 0.0000 739.50 0.0000 311. 90 29.1533 546.56 0.0000 747.24 14.3669 340.48 29.1533 552.55 8. 3965 748.06 5.1329 340.55 0.0000 563.25 8.4459 752.31 9.2560 344.28 28.0249 569.33 12.2404 753.82 0.0000 345.93 17. 0813 946.00 12.2415 756.73 5.1522 351.06 23.2774 569.70 16.0094 756.80 5.1522 351. 93 23.2937 583.19 18.0236 884.68 10.8529 Page 3159 of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 7 65. 81 9.3098 1274.44 8.4689 1620.50 2. 0114 766.42 12.4165 1001.03 6.7861 1621. 92 2.0120 766.84 12.4185 1002.74 10.1851 1678.03 0.0000 772.60 0.0000 1004.73 5. 0960 1690.97 0.0000 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87. 0.0000 1764.49 3 .1130 778.90 8.7374 1028.54 0.0000 1063.66 3 .1166 783.70 0.0000 1037.84 5.7255 1771. 35 1.0391 785.37 7.3008 1038.76 0.0000 1791.20 0.0000 792.07 15.6885 631.29 8.0385 1808.65 2.0944 794.95 12.5654 1048.07 0.0000 1810.72 0.0000 795.86 13.6178 1049.04 9.1940 1836.06 2.1061 810.06 2.1073 1050.41 11. 4982 810.29 4.2148 1063.66 8.0835 344.28 5.2690 1077.00 0.0000 810.76 6.3235 1077.34 10.4385 815.77 0.0000 1085.87 5.8150 1048.07 0.0000 1093.63 6.9951 832.01 9.5665 1099.45 9.6364 834.85 7.4492 1112. 07 8.7946 835. 71 7.4517 1112. 84 4.3985 836.80 0.0000 1115. 54 8.4521 846.75 0.0000 1120.29 9.6989 846.77 10.6917 1120. 55 9.6995 856.80 0.0000 1221.41 9.8786 860.56 8.5993 1129.67 7.9585 871.09 10.7926 1131. 51 0.0000 873.19 7.5608 1147.95 0.0000 875.33 0.0000 1173.23 8. 9600 879.38 7.5788 1177.95 6.2809 880.51 9.7482 1189.05 10.8025 883.24 10.8427 1204.77 14.4697 884.68 11.9332 1221.41 12. 7225 889.28 8.6940 1231.02 13.6688 894.76 8. 7119 1235.36 0.0000 898.04 7.6320 1238.28 10.9578 900.72 4. 9113 1260.41 0.0000 903.28 9.8320 1271.87 6.4523 911.20 7.6694 1274.44 11. 0691 912.08 7.6719 1274.54 11. 0698 923.98 0.0000 1291.59 5.5609 926.50 8.8141 1298.22 0.0000 929 .11 8.2712 1312 .11 0.0000 937.49 9.9554 1332.49 5.6228 944.13 0.0000 1362.66 0.0000 946.00 11. 0954 1365.19 8.5073 949.00 11. 6625 1368.63 0.0000 667.71 0.0000 1384.29 2.8499 962.31 11.1597 1408.01 5.7345 964.08 5.0250 1457.56 0.0000 966 .17 6.7048 1460.82 4.8425 911. 20 11.1857 1489.16 1. 9504 968. 97 11.1857 1505.03 2.9370 983.53 0.0000 1584.12 4.7874 984.45 0.0000 1596.21 0.0000 Page 3160 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:13:37.83 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM41.CNF;ll9 Background date : Z-OCT-2016 11:02:18. Sample date 8-DEC-2015 11:23:00. Acquisition date : 3-0CT-2016 08:10:29. Sample ID G405235013 Sample quantity 1.44574E+02 GRAM Detector name : GAM41 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.06 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 0 2 0 3 3 4 3 5 3 6 3 7 3 8 3 9 0 10 0 11 0 12 0 13 4 14 4 .15 5 16 5 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 10 25 10 26 10 27 1 28 1 29 0 30 0 31 0 32 0 33 0 34 0 Page 3161of5809 Energy 46.50* 63.49* 74.86* 77.27* 84.07* 87.32 89.88 92. 86* 129.25 135.60 185.77* 209.76 238.91* 241.66 270.18 273.53 295.59 300.37 338.80 352.16* 411. 07 464.00 498.44 511.26* 516.70 519.03 521.78 524.48 583.87* 609.73* 636.18 662.05* 728.48* 782.60 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 66 96 289 372 49 113 51 101 46 38 116 95 384 97 49 19 134 43 67 206 20 17 14 84 16 10 16 16 105 142 7 345 32 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 113 276 219 110 212 156 126 135 122 121 126 73 42 55 61 44 66 79 95 53 36 39 22 24 6 3 3 4 33 23 16 38 20 2 0.88 0. 96 1. 55 0.90 1. 58 1. 23 0:93 1.13 0.60 2.98 0.94 2.39 1. 03 1. 67 2.10 1. 62 0.99 1. 34 0. 96 1.13 2.23 1. 57 0.95 4.01 1. 53 1. 21 1. 51 1. 81 1. 81 1. 24 0.49 1. 34 1. 91 1.12 93.30 127.26 149.99 154.81 168.41 174.91 180.04 185.98 258.74 271.43 371. 76 419.73 478.00 483.51 540.52 547.23 591.35 600.90 677.74 704.46 822.26 928.10 996. 98 1022.62 1033.49 1038.16 1043.66 1049.06 1167. 83 1219.55 1272. 45 1324 .18 1457.05 1565.29 90 122 143 143 161 161 161 161 255 267 367 414 470 470 535 535 585 596 672 697 816 924 992 1014 1014 1014 1041 1041 1161 1213 1267 1316 1452 1560 8 l.84E-02 32.5 11 2.66E-02 36.5 15 8.03E-02 10.8 8.32E+OO 15 1. 03E-01 6. 8 32 1.37E-02 53.8 1.02E+OO 32 3.15E-02 20.1 32 1.41E-02 37.5 32 2.80E-02 25.1 9 1.26E-02 46.1 10 1.06E-02 56.6 11 3.22E-02 21.7 12 2.65E-02 20.8 18 1.07E-01 5.8 1.45E+OO 18 2.70E-02 25.8 16 1.35E-02 34.1 1.73E+OO 16 5.36E-03 64.1 11 3.72E-02 14.6 12 1. 21E-02 43. 5 12 1. 87E-02 31.1 12 5. 72E-02 10 .1 9 5.52E-03 60.0 7 4.68E-03 67.5 8 3.99E-03 62.2 27 2.34E-02 20.4 2.44E+OO 27 4.40E-03 46.5 27 2.88E-03 42.9 12 4.40E-03 29.0 8.51E-01 12 4.36E-03 32.6 12 2.92E-02 14.9 13 3.94E-02 11.1 7 l.93E-03105.6 14 9.59E-02 6.6 12 8.77E-03 34.5 9 3.34E-03 36.3 Peak Search Report (continued) Page : 2 Sample ID : G405235013 Acquisition date 3-0CT-2016 08:10:29 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 8 61. 22 37 0 1. 48 1722.54 1716 14 1.03E-02 16.4 36 0 912.01* 61 17 1. 76 1824.14 1815 14 1. 69E-02 19.7 37 0 935.83 34 7 4.86 1871. 77 1864 16 9. 41E-.03 25.2 38 0 952.71 11 10 0.69 1905.55 1899 10 3.06E-03 61. 7 39 0 969.98* 33 13 1. 34 1940.09 1935 10 9.22E-03 28.l 40 0 1104 .14 13 21 4.41 2208.47 2198 17 3.55E-03 87.1 41 0 1121. 49 23 17 0.75 2243.17 2239 10 6.41E-03 39.6 42 0 1208.19 13 10 1. 54 2416.62 2411 10 3.61E-03 53.3 43 0 1211. 03 10 0 1. 24 2422.30 2420 6 2.78E-03 31. 6 44 0 1238.66 30 13 1. 50 2477.57 2470 13 8.33E-03 30.8 45 0 1378.39 8 4 0.61 2757.12 2752 9 2.18E-03 60.0 46 0 14 61. 77* 256 8 1. 76 2923.94 2915 16 7.lOE-02 6.8 47 0 1765.03 28 0 1. 05 3530.75 3524 12 7.78E-03 18.9 Flag: "*" = Peak area was modified by background subtraction Page 3162of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:13:39 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 8-DEC-2015 11:23:00 G405235013 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:10:29 144.57 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA41 0 01:00:00.00 1. 50 keV No Empirical 75.00 Interference Report Interfering Nuclide Page 3163 of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 74.66 74.82 74.82 351. 06 CAN 0 01:00:06.06 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235013 Acquisition date 3-0CT-2016 08:10:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 8.926E-01 1.342E+Ol 1.342E+Ol 13.57 OK RU-103 497.08 91.00* 2.367E+OO 3.686E-02 7.344E+OO 124.44 OK 610.33 5. 76 1.970E+OO 6.774E+OO l.350E+03 22.14 OK CD-109 88.03 3.70* 7.449E+OO 1.582E+OO 2.483E+OO 69.50 OK SN-126 64.28 9.60 7.794E+OO 8.387E-01 8.387E-01 72. 92 OK 86.94 8.90 7.449E+OO 6.579E-01 6.579E-01 69.50 OK 87.57 37.00* 7.449E+OO l.582E-01 1.582E-01 69.50 OK BA-137M 661.66 89.90* 1. 826E+OO l .132E+OO l.154E+OO 13.23 OK CS-137 661.66 85.10* 1. 826E+OO 1.196E+OO 1.219E+OO 13.23 OK TL-208 277.37 6.60 3.907E+OO Line Not Found Absent 583.19 85.00* 2.050E+OO 3.288E-01 3.288E-01 29.74 OK 860.56 12.50 1.433E+OO 1.085E+OO 1.085E+00 32.88 OK PB-210 46.54 4.25* 7.552E+OO 1.385E+OO 1.421E+OO 64.95 OK PB-212 74.82 10.28 7.683E+OO 1.726E+OO 1. 726E+OO 31. 59 OK 77 .11 17.10 7.644E+OO 1.836E+OO 1.836E+OO 13.51 OK 238.63 43.60* 4.382E+OO 1.184E+OO l.184E+OO 11. 68 OK 300.09 3.30 3.666E+OO 2. 071E+OO 2.071E+OO 86.98 OK BI-214 609.32 45.49* 1.970E+OO 8.578E-01 8.581E-01 22.14 OK 1120.29 14.92 l.127E+OO 7.033E-01 7.035E-01 79.28 OK 1764.49 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 OK PB-214 74.82 5.80 7.683E+OO Line Not Found <<INT Reject 77 .11 9.70 7.644E+00 3.237E+OO 3.238E+OO 13.51 OK 87.09 3.41 7.454E+OO Line Not Found <<INT Reject 242.00 7.25 4.340E+OO Line Not Found <<INT Reject 295.22 18.42 3.714E+OO 1.133E+OO 1.133E+OO 29.15 OK 351.93 35.60* 3.212E+OO 1.026E+OO 1.026E+OO 20.15 OK RN-222 609.32 45.49* l.970E+00 8.578E-01 8.581E-01 22.14 OK 1120.29 14.92 l.127E+00 7.033E-01 7.035E-01 79.28 OK 1764.49 15.30 7.618E-01 1.177E+OO l.177E+OO 37.80 OK RA-224 240.99 4.10* 4.345E+00 1.202E+OO 1.202E+OO 146.05 OK RA-226 609.32 45.49* 1.970E+OO 8.578E-01 8.581E-01 22.14 OK 1120.29 14.92 1.127E+OO 7.033E-01 7.035E-01 79.28 OK 1764.49 15.30 7.618E-01 1.177E+OO 1. l 77E+OO 37.80 OK AC-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.319E+OO 1. 031E+OO 1.031E+OO 62.23 OK 794.95 4.25 1.543E+OO Lin*e Not Found Absent 835.71 1. 61 1.473E+OO Line Not Found Absent 911.20 25.80* 1. 360E+OO 9.074E-01 9.074E-01 39.40 OK 968. 97 15.80 1.285E+OO 8.493E-01 8.493E-01 56. 29 OK RA-228 105.21 1.10 7.028E+00 Line Not Found Absent 338.32 11. 27 3.319E+OO 1. 031E+OO 1. 031E+OO 62.23 OK 794.95 4.25 l.543E+00 Line Not Found Absent 835.71 1. 61 1.473E+OO Line Not Found Absent 911. 20 25.80* 1.360E+OO 9.074E-01 9.074E-01 39.40 OK 968. 97 15.80 1.285E+OO 8.493E-01 8.493E-01 56.29 OK TH-228 74.82 10.28 7.683E+OO 1. 726E+OO 1. 726E+OO 31. 59 OK 77 .11 17.10 7.644E+OO l.836E+OO 1.836E+OO 13. 51 OK 238.63 43.60* 4.382E+00 1.184E+OO 1.184E+OO 11. 68 OK 300.09 3.30 3.666E+OO 2.071E+OO 2. 071E+OO 86.98 OK Page 3164of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235013 Acquisition date 3-0CT-2016 08:10:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-229 85.43 14.70 7 .. 517E+OO 2.864E-01 2.864E-01 107.55 OK 88.47 24.00 7.449E+OO 2.440E-01 2.440E-01 69.50 OK 193.51 4.41* 5.088E+OO Line Not Found Absent 210.85 2.80 4.815E+OO 4.207E+OO 4.208E+OO 41. 60 OK TH-230 609.32 45.49* l.970E+OO 8.578E-01 8.578E-01 22.14 OK 1120.29 14.92 1.127E+OO 7.033E-01 7.033E-01 79.28 OK 1764.49 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 OK PA-231 283.69 1. 70 3.838E+OO Line Not Found Absent 301.36 5.35* 3.666E+OO 1.277E+OO l.277E+OO 86.98 OK TH-232 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.319E+OO 1. 031E+OO 1. 031E+OO 62.23 OK 835. 71 1. 61 1. 4 73E+OO Line Not Found Absent 911. 20 25.80* l.360E+OO 9.074E-01 9.074E-01 39.40 OK 968.97 15.80 1.285E+OO 8.493E-01 8.493E-01 56. 29 OK TH-234 63.29 3.70* 7.794E+OO 2.176E+OO 2.176E+OO 72. 92 OK 92.59 4.23 7.325E+00 2.067E+OO 2.067E+OO 50.15 OK U-234 609.32 45.49* 1.970E+OO 8.578E-01 8.578E-01 22.14 OK 1120.29 14.92 l.127E+00 7.033E-01 7.033E-01 79.28 OK 1764.49 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 OK U-235 89. 96 3.47 7.393E+OO 1. 264E+OO 1.264E+OO 75.02 OK 93.35 5.60 7.325E+OO 1.562E+OO 1.562E+OO 50.15 OK 143.76 10. 96* 6.093E+OO Line Not Found Absent 163.33 5.08 5.667E+OO Line Not Found Absent 185. 72 57.20 5.227E+OO 2.333E-01 2.333E-01 43.44 OK 205.31 5.01 4.887E+OO Line Not Found Absent U-238 63.29 3.70* 7.794E+00 2.176E+OO 2.176E+OO 72.92 OK 92.59 4.23 7.325E+OO 2.067E+OO 2.067E+OO 50.15 OK AM-243 43.53 5.90 7. 421E+OO Line Not Found Absent 74.66 67.20* 7.683E+OO 2.640E-01 2. 641E-01 31. 59 OK ANH-511 511. 00 100.00* 2.313E+OO 2.004E-01 2.004E-01 40.73 OK Flag: "*" = Keyline Page 3165of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:13:40.80 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l *
  • Acquisition date 3-0CT-2016 08:10:29 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 11:23:00 Analyst initials: MXRl *
  • Sample ID G405235013 Sample Quantity 1.4457E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF 'GAM41 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 RU-103 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 t.J-238 AM-243 ANH-511 Activity (pCi/GRAM 1.342E+Ol 7.344E+OO 2.483E+OO l.582E-01 1.154E+OO 1.219E+OO 3.288E-01 1.421E+OO 1.184E+OO 8.581E-01 1.026E+OO 8.581E-01 1.202E+OO 8.581E-01 9.074E-01 9.074E-01 1.184E+OO 2.255E-01 8.578E-01 1.277E+OO 9.074E-01 2.176E+OO 8.578E-01 -2.341E-02 2.176E+OO 2. 641E-01 2.004E-01 Cnt uncert ( 1 . 96-sigma ) l.784E+OO 8.956E+OO 1.691E+OO l.078E-01 1.497E-01 1.581E-01 9.584E-02 9.045E-01 1.355E-01 1. 8 62E-01 2.026E-01 1. 8 62E-01 1. 720E+OO 1. 862E-01 3.503E-01 3.503E-01 l.355E-01 5.388E-01 1. 861E-01 1.089E+OO 3.503E-01 1.555E+OO 1. 861E-01 2.042E-01 1.555E+OO 8.175E-02 7.998E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3166 of 5809 Key-Line Activity (pCi/GRAM 5.147E+OO 6.027E-03 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.532E+Ol 5.947E-02 9.294E+40 MDA (pCi/GRAM 7.420E-01 1.390E+Ol 1.662E+OO l.058E-01 8.929E-02 9.433E-02 7.288E-02 7.952E-01 l.022E-01 l.233E-01 1.483E-01 l.233E-01 1.095E+OO 1.233E-01 2.775E-01 2.775E-01 1.022E-01 l.064E+00 1.233E-01 8.319E-01 2.775E-01 l.053E+OO 1.233E-01 3.984E-01 1.053E+OO 6.463E-02 5.635E-02 MDA (pCi/GRAM 2.985E+Ol l.193E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -3.212E-02 2.816E-02 l.889E-02 NOT IDENT. SC-46 -3. 272E-01 4.132E-01 7.148E-01 FAIL ABUN V-48 O.OOOE+OO 1. 692E+04 O.OOOE+OO SHORT HLIF CE-51 O.OOOE+OO 4.497E+02 O.OOOE+OO SHORT HLIF MN-54 -5.825E-04 6. 511E-02 l.318E-01 NOT IDENT. C0-56 -1. 37 5E-02 4.374E-01 8.986E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -l.237E-02 4.737E-02 9.132E-02 FAIL ABUN C0-58 -7.185E-02 6.447E-01 l.278E+OO NOT IDENT. FE-59 -6.747E-Ol 9.589E+OO l.633E+01 NOT IDENT. C0-60 -3. 631E-02 4.306E-02 6.830E-02 NOT IDENT. ZN-65 -2.634E-Ol 2.362E-01 3.465E-01 NOT IDENT. GE-68 -1. 572E+OO 3. ll 7E+OO 5.598E+OO NOT IDENT. AS-73 l.478E+OO 2.671E+OO 5.057E+OO NOT IDENT. AS-74 O.OOOE+OO 7.205E+03 O.OOOE+OO SHORT HLIF SE-75 1. 799E-02 2.404E-01 4.421E-01 FAIL ABUN BR-77 O.OOOE+OO 2.465E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.950E+02 0.000E+OO SHORT HLIF RB-83 6.204E-01 5.213E-01 l.469E+OO FAIL ABUN KR-85 l.119E+Ol 9.534E+OO l.858E+Ol NOT IDENT. SR-85 l. l 78E+OO l.007E+00 1. 963E+OO NOT IDENT. RB-86 O.OOOE+OO 3. 688E+o4 O.OOOE+OO SHORT HLIF Y-88 -l.347E-01 2.056E-01 3.668E-01 NOT IDENT. Y-91 -3.063E+02 8.498E+02 l.316E+03 NOT IDENT. NB-94 8.340E-03 3.899E-02 7.890E-02 NOT IDENT. NB-95 l.013E-Ol 9.653E-01 l.946E+OO NOT IDENT. NB-95M -7.221E-01 2.944E+OO 4.891E+OO NOT IDENT . ZR-95 -9.977E-02 . 1. 746E+OO 3.449E+OO NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO l.945E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.200E-02 3.861E-02 6.608E-02 NOT IDENT. RH-102 -l.545E-02 7.933E-02 l.354E-01 NOT IDENT. RH-106 l.730E-01 5.784E-01 l.138E+OO NOT IDENT. RU-106 l.730E-01 5.784E-01 l .138E+OO NOT IDENT. AG-108M 2.763E-03 3.302E-02 6.280E-02 NOT IDENT. AG-llOM -7.668E-04 l.217E-01 2.488E-01 NOT IDENT. SN-113 -3.029E-02 2.802E-01 5.205E-01 NOT IDENT. CD-115 O.OOOE+OO 4.226E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.991E+04 O.OOOE+OO SHORT HLIF TE-123M 8.356E-02 l.358E-01 2.757E-01 NOT IDENT. SB-124 2.379E+OO 2.789E+OO 6.999E+OO NOT IDENT. SB-125 4.677E-02 l.340E-01 2.598E-01 FAIL ABUN TE-125M 1. 899E+02 2.766E+02 5.623E+02 NOT IDENT. I-126 O.OOOE+OO 1. 277E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 384E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.687E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 5.620E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-.132 O.OOOE+OO 4.346E+26 O.OOOE+OO SHORT HLIF BA-133 4.340E-02 5.521E-02 l.024E-01 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.339E-02 6.894E-02 l.464E-01 NOT IDENT. CS-135 -2.247E-02 l.666E-01 2.804E-01 NOT IDENT. I-135 0.000E+OO l.753E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.130E+05 O.OOOE+OO SHORT HLIF CE-139 -5.176E-02 l.197E-01 2.244E-01 NOT IDENT. BA-140 O.OOOE+OO l.443E+06 O.OOOE+OO SHORT HLIF LA-140 0.000E+OO 5.563E+05 0.000E+OO SHORT HLIF CE-141 5.832E-01 2.697E+Ol 5.232E+Ol NOT IDENT. CE-143 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 1. 757E-01 5.043E-01 7.432E-01 NOT IDENT. PM-144 2.327E-02 5.848E-02 l.240E-01 NOT IDENT. PR-144 3. 672E-01 5.332E+OO l.077E+Ol NOT IDENT. PM-146 -2.107E-02 6.287E-02 l.120E-01 NOT I DENT*. ND-147 O.OOOE+OO 4.209E+07 O.OOOE+OO SHORT HLIF PM-147 2.230E+02 8.008E+02 l.603E+03 NOT IDENT. PM-149 O.OOOE+OO 5.423E+40 O.OOOE+OO SHORT HLIF EU-150 -8.134E-03 3.563E-02 5.804E-02 FAIL ABUN EU-152 3.350E-03 l .131E-01 2.047E-01 NOT IDENT. GD-153 -4.475E-03 1. 671E-01 2.972E-01 NOT IDENT. EU-154 l.715E-02 l.463E-01 2.940E-01 NOT IDENT. EU-155 7.484E-02 l.040E-01 2.129E-01 FAIL ABUN TB-160 2.176E+OO 2.275E+OO 5.141E+OO FAIL ABUN H0-166M 6.081E-04 5. 596E-02 l.142E-01 FAIL ABUN TM-171 3.640E+OO 5.817E+OO l. llOE+Ol NOT IDENT. HF-172 l .196E-01 2.625E-01 4.800E-01 FAIL ABUN Page 3167of5809 LU-172 8.250E-03 l.091E-01 2.140E-01 FAIL ABUN LU-176 1.038E-02 2.953E-02 5.763E-02 FAIL ABUN HF-181 -1.063E+OO 5. 596E+OO 1.019E+Ol NOT IDENT. TA-182 9.516E-02 1.177E+OO 2.317E+OO FAIL ABUN RE-183 7.378E-01 1.201E+OO 2.274E+OO NOT IDENT. RE-184 3.078E+Ol 3.738E+Ol 8.280E+Ol NOT IDENT. W-188 -7.409E+Ol l.425E+02 2.257E+02 FAIL ABUN IR-192 -4.557E-02 5.237E-01 9.865E-01 FAIL ABUN HG-203 2.099E+OO 2.455E+OO 5.095E+00 NOT IDENT. BI-207 4. 081E-04 6.198E-02 l.220E-01 FAIL ABUN BI-211 O.OOOE+OO 5.582E-01 8.632E-01 FAIL ABUN PB-211 7.339E-01 7.929E-01 l.593E+00 NOT IDENT. BI-212 1.510E+OO 1. 021E+OO 1.580E+OO FAIL ABUN RN-219 -2.732E-01 4.461E-01 7.790E-01 FAIL ABUN RA-223 l.967E-01 6. 671E-01 l.302E+OO FAIL ABUN AC-227 -2.352E-02 2.456E-01 4.663E-01 FAIL ABUN TH-227 -2.352E-02 2.456E-01 4.663E-01 FAIL ABUN TH-231 1. 967E-01 6.671E-01 1.302E+OO FAIL ABUN PA-233 2.532E-02 7.518E-02 l.459E-01 FAIL ABUN PA-234 -2.915E-02 3.071E-01 5.673E-01 NOT IDENT. PA-234M -2.595E+OO 4.341E+OO 7.673E+OO NOT IDENT. NP-237 2.532E-02 7.518E-02 1.459E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 3.233E-02 2.332E-01 4.625E-01 NOT IDENT. PU-239 O.OOOE+OO 6.271E+02 6.927E+02 FAIL ABUN AM-241 -4.753E-02 6.929E-02 1. 089E-01 NOT IDENT. CM-243 -4.333E-02 9.516E-02 1.821E-01 NOT IDENT. BK-247 5.619E-03 l.544E-01 FAIL ABUN CM-247 -1. 790E-02 4.179E-02 7.468E-02 NOT IDENT. CF-249 4.208E-04 4.683E-02 8.788E-02 NOT IDENT. CF-251 6.306E-02 l.157E-01 2.341E-01 NOT IDENT. Page 3168 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:13:38.63 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 246 10.66* 8.926E-01 1.342E+Ol 1.342E+Ol 13.57 RU-103 497.08 15 91.00* 2.367E+OO 3.686E-02 7.344E+OO 124.44 610.33 148 5.76 1. 970E+OO 6.774E+OO l.350E+03 22.14 CD-109 88.03 139 3.70* 7.449E+OO 2.626E+OO 4.121E+OO 40.24 SN-126 64.28 121 9.60 7.794E+OO 8.387E-01 8.387E-01 72. 92 86.94 139 8.90 7.449E+00 1.092E+OO 1.092E+OO 40.24 87.57 139 37.00* 7.449E+OO 2.626E-01 2.626E-01 40.24 BA-137M 661.66 358 89.90* l.826E+OO 1.132E+OO 1.154E+OO 13.23 CS-137 661.66 358 85.10* 1.826E+OO 1.196E+OO l.219E+00 13 .23 TL-208 277.37 ------6.60 3.907E+OO ------Line Not Found ------583.19 110 85.00* 2.050E+OO 3.288E-01 3.288E-01 29.74 860.56 37 12.50 1.433E+OO 1.085E+OO 1.085E+OO 32.88 PB-210 46.54 86 4.25* 7.552E+00 1.385E+OO 1.421E+OO 64.95 BI-211 72. 87 ------1. 23 7. 711E+OO ------Line Not Found ------351.06 226 12.92* 3.212E+OO 2.826E+OO 2.826E+00 20.15 PB-212 74.82 360 10.28 7.683E+OO 2. 365E+OO' 2.365E+OO 21. 67 77 .11 462 17.10 7.644E+OO 1.836E+OO 1.836E+OO 13.51 238.63 435 43.60* 4.382E+OO 1.184E+OO l.184E+OO 11. 68 300.09 48 3.30 3.666E+OO 2.071E+OO 2. 071E+OO 86.98 BI-214 609.32 148 45.49* 1.970E+OO 8.578E-01 8.581E-01 22.14 1120.29 23 14.92 1.127E+OO 7.033E-01 7.035E-01 79.28 1764.49 26 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 PB-214 74.82 360 5.80 7.683E+OO 4.192E+OO 4.193E+OO 21. 67 77 .11 462 9.70 7.644E+OO 3.237E+OO 3.238E+OO 13.51 87.09 139 3.41 7.449E+OO 2.849E+OO 2. 851E+OO 40.24 242.00 110 7.25 4.345E+OO 1.812E+OO 1. 813E+OO 51. 66 295.22 149 18.42 3.714E+OO l.133E+OO 1.133E+00 29.15 351. 93 226 35.60* 3.212E+OO 1.026E+OO 1.026E+OO 20.15 RN-222 609.32 148 45.49* l.970E+00 8.578E-01 8.581E-01 22.14 1120.29 23 14.92 1.127E+OO 7.033E-01 7.035E-01 79.28 1764.49 26 15.30 7.618E-01 1.177E+OO l.177E+OO 37.80 RA-224 240.99 110 4.10* 4.345E+OO 3.205E+OO 3.205E+OO 51. 66 RA-226 609.32 148 45.49* l.970E+00 8.578E-01 8.581E-01 22.14 1120.29 23 14.92 1.127E+OO 7.033E-01 7.035E-01 79.28 1764.49 26 15.30 7.618E-01 1.177E+OO l.177E+OO 37.80 AC-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 74 11. 27 3.319E+OO 1. 031E+OO 1.031E+OO 62.23 794.95 ------4.25 1.543E+00 ------Line Not Found ------835.71 ------1. 61 1.473E+OO ------Line Not Found ------911.20 61 25.80* 1.360E+OO 9.074E-01 9.074E-01 39.40 968. 97 33 15.80 1.285E+OO 8.493E-01 8.493E-01 56.29 RA-228 105. 21 ------1.10 7.028E+OO ------Line Not Found ------338.32 74 11. 27 3.319E+OO 1. 031E+OO 1.031E+OO 62.23 794.95 ------4.25 1.543E+OO ------Line Not Found ------835. 71 ------1. 61 1.473E+OO ------Line Not Found ------911.20 61 25.80* 1.360E+OO 9.074E-01 9.074E-01 39.40 968. 97 33 15.80 1.285E+OO 8.493E-01 8.493E-01 56.29 Page 3169of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235013 Acquisition date 3-0CT-2016 08:10:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error TH-228 74.82 360 10.28 7.683E+OO 2.365E+OO 2.365E+OO 21. 67 77 .11 462 17.10 7.644E+OO 1.836E+OO 1.836E+OO 13.51 238.63 435 43.60* 4.382E+OO 1.184E+OO 1.184E+OO 11. 68 300.09 48 3.30 3.666E+OO 2.071E+OO 2. 071E+OO 86.98 TH-229 85.43 61 14.70 7.517E+OO 2.864E-01 2.864E-01 107.55 88.47 139 24.00 7.449E+OO 4.049E-01 4.049E-01 40.24 193.51 ------4.41* 5.088E+OO ------Line Not Found ------210.85 109 2.80 4.815E+OO 4.207E+OO 4.208E+OO 41. 60 TH-230 609.32 148 45.49* 1.970E+OO 8.578E-01 8.578E-01 22.14 1120.29 23 14.92 l.127E+OO 7.033E-01 7.033E-01 79.28 1764.49 26 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 PA-231 283.69 ------1. 70 3.838E+OO ------Line Not Found ------301.36 48 5.35* 3.666E+OO 1.277E+OO 1.277E+OO 86.98 TH-232 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 74 11. 27 3.319E+00 1. 031E+OO 1. 031E+OO 62.23 835.71 ------1. 61 1. 473E+OO ------Line Not Found ------911.20 61 25.80* 1.360E+OO 9.074E-01 9.074E-01 39.40 968. 97 33 15.80 1.285E+OO 8.493E-01 8.493E-01 56.29 TH-234 63 .'29 121 3.70* 7.794E+00 2.176E+00 2.176E+OO 72. 92 92.59 123 4.23 7.325E+OO 2.067E+OO 2.067E+OO 50.15 U-234 609.32 148 45.49* 1.970E+OO 8.578E-01 8.578E-01 22.14 1120. 29 23 14.92 l.127E+OO 7.033E-01 7.033E-01 79.28 1764.49 26 15.30 7.618E-01 1.177E+OO 1.177E+OO 37.80 U-235 89. 96 62 3.47 7.393E+OO 1. 264E+OO l.264E+00 75.02 93.35 123 5.60 7.325E+OO 1.562E+OO 1.562E+OO 50.15 143.76 ------10. 96* 6.093E+00 ------Line Not Found ------163.33 ------5.08 5.667E+OO ------Line Not Found ------185.72 134 57.20 5.227E+OO 2.333E-01 2.333E-01 43.44 205.31 ------5.01 4.887E+OO ------Line Not Found ------U-238 63.29 121 3.70* 7.794E+OO 2.176E+OO 2.176E+00 72. 92 92.59 123 4.23 7.325E+OO 2.067E+OO 2.067E+OO 50.15 AM-243 43.53 ------5.90 7. 421E+OO ------Line Not Found ------74.66 360 67.20* 7.683E+OO 3.618E-01 3.618E-01 21.67 ANH-511 511. 00 89 100.00* 2. 313E+OO 2.004E-01 2.004E-01 40.73 Flag: "*" Key line Page 3170 of 5809 Surrunary of Nuclide Activity Sample ID : G405235013 Acquisition date Page : 3 3-0CT-2016 08:10:29 Total number of lines in spectrum 47 Number of unidentified lines 8 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 RU-103 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 39.26D 461. 40D 2.30E+05Y 30.08Y 30.08Y 1.41E+10Y 22.20Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600.00Y 1600. DOY 1.41E+10Y 1600. DOY 1. 41E+10Y 1.41E+10Y l.41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 199. 1. 57 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.342E+01 3.686E-02 2.626E+OO 2.626E-01 1.132E+OO 1.196E+OO 3.288E-01 l.385E+OO 2.826E+00 1.184E+OO 8.578E-01 1. 026E+OO 8.578E-01 3.205E+OO 8.578E-01 9.074E-01 9.074E-01 1.184E+00 4.049E-01 8.578E-01 1.277E+OO 9.074E-01 2.176E+OO 8.578E-01 2.333E-01 2.176E+OO 3.618E-01 2.004E-01 4.365E+Ol 4.365E+Ol Decay Corr pCi/GRAM 1.342E+Ol 7.344E+OO 4.121E+OO 2.626E-01 1.154E+OO 1.219E+OO 3.288E-01 1.421E+OO 2.826E+OO 1.184E+OO 8. 581E-01 1.026E+OO 8. 581E-01 3.205E+OO 8.581E-01 9.074E-01 9.074E-01 1.184E+OO 4.049E-01 8.578E-01 1.277E+00 9.074E-01 2.176E+OO 8.578E-01 2.333E-01 2.176E+OO 3.618E-01 2.004E-01 5.253E+Ol 5.253E+01 82.98% Decay Corr 2-Sigma Error 0.182E+Ol 9.139E+OO 1.658E+OO 1.057E-01 0.153E+OO 0.161E+OO 0.978E-01 0.923E+OO 0.570E+OO 0.138E+OO 1. 899E-01 0.207E+OO l.899E-01 1.656E+OO 1.899E-01 3.575E-01 3.575E-01 0.138E+OO 1.629E-01 1.899E-01 1.lllE+OO 3.575E-01 1.587E+OO 1.899E-01 1.014E-01 1.587E+OO 0.784E-01 0.816E-01 "M" Manually accepted 2-Sigma %Error 13.57 124.44 40.24 40.24 13.23 13.23 29.74 64.95 20.15 11. 68 22.14 20.15 22.14 51. 66 22.14 39.40 39.40 11. 68 40.24 22.14 86.98 39.40 72.92 22.14 43.44 72. 92 21. 67 40.73 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3171 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235013 Acquisition date : 3-0CT-2016 08:10:29 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.25 54 145 0.60 258.74 255 9 1.26E-02 92.2 6.43E+OO T 0 135.60 45 144 2.98 271.43 267 10 1.06E-02 **** 6.28E+OO T 5 270.18 55 68 2.10 540.52 535 16 1.35E-02 68.2 3.99E+OO T 5 273.53 22 49 1. 62 547.23 535 16 5.36E-03 **** 3 .. 95E+OO T 0 411. 07 22 39 2.23 822.26 816 9 5.52E-03 **** 2.81E+OO T 0 464.00 18 42 1. 57 928.10 924 7 4.68E-03 **** 2.52E+OO T 10 516.70 17 6 1. 53 1033.49 1014 27 4.40E-03 93.1 2.29E+OO 10 519.03 11 3 1. 21 1038.16 1014 27 2.88E-03 85.7 2.28E+OO T 1 521.78 17 3 1. 51 1043.66 1041 12 4.40E-03 58.0 2.27E+OO T 1 524.48 17 4 1. 81 1049.06 1041 12 4.36E-03 65.1 2.26E+OO 0 636.18 7 17 0.49 1272. 45 1267 7 1.93E-03 **** 1.89E+OO T 0 728.48 32 21 1. 91 1457.05 1452 12 8.77E-03 69.0 1.67E+OO T 0 782.60 12 2 1.12 1565.29 1560 9 3.34E-03 72.6 1.57E+OO T 0 935.83 34 7 4.86 1871. 77 1864 16 9.41E-03 50.4 1.33E+OO 0 952. 71 11 10 0.69 1905.55 1899 10 3.06E-03 **** 1. 31E+OO 0 1104 .14 13 21 4.41 2208.47 2198 17 3.55E-03 **** 1.14E+OO 0 1208.19 13 10 1. 54 2416.62 2411 10 3.61E-03 **** 1.05E+00 0 1211. 03 10 0 1. 24 2422.30 2420 6 2.78E-03 63.2 1. 05E+OO 0 1238.66 29 13 1. 50 2477.57 2470 13 8.33E-03 61. 6 1.03E+OO T 0 1378.39 8 4 0.61 2757.12 2752 9 2.18E-03 **** 9.39E-01 *Flags: "T" = Tentatively associated Page 3172 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:13:52.71 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l *
  • Acquisition date 3-0CT-2016 08:10:29 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 11:23:00 Nuclide Library : SOLID *
  • Sample ID G405235013 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4457E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 RU-103 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-22 6 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2. 969E-01 6.283E+OO 7.885E-01 5.018E-02 4.020E-02 4.247E-02 3.232E-02 3.735E-01 4.727E-02 5.365E-02 6.782E-02 5.365E-02 5.067E-01 5.365E-02 1.185E-01 1.185E-01 4.727E-02 4.992E-01 5.364E-02 3.787E-01 l.185E-01 5.007E-01 5.364E-02 1.882E-01 5.007E-01 3.087E-02 2.506E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3173 of 5809 Le (pCi/GRAM 1.353E+Ol 5.087E-02 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132

  • TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3174 of 5809 2.961E-01 O.OOOE+OO O.OOOE+OO 5.646E-02 3.769E-01 O.OOOE+OO 4.285E-02 5.500E-01 6.995E+OO 2.600E-02 1.442E-01 2.392E+OO 2.403E+OO O.OOOE+OO 2.037E-01 O.OOOE+OO O.OOOE+OO 6. 561E-01 8.530E+OO 9.009E-01 O.OOOE+OO l.159E-01 5.682E+02 3.530E-02 8.577E-01 2.274E+00 l.515E+00 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.105E-02 5.988E-02 5.038E-01 5.038E-01 2.841E-02 1.083E-01 2.371E-01 O.OOOE+OO O.OOOE+OO 1.291E-01 2.908E+OO 1.189E-01 2.663E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.731E-02 O.OOOE+OO 6.605E-02 l.288E-01 O.OOOE+OO O.OOOE+OO 1.048E-01 O.OOOE+OO O.OOOE+OO 2.465E+Ol O.OOOE+OO 3.498E-01 5.465E-02 4.747E+OO 5.123E-02 O.OOOE+OO 7.527E+02 O.OOOE+OO 2.673E-02 9.364E-02 l.402E-01 1.255E-01 1.008E-01 2. 272E+OO 4.932E-02 5.269E+OO 2.264E-01 9.378E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. 'SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247, CF-249 CF-251 Page 3175 of 5809 2.666E-02 4.601E+OO 1.004E+OO 1.082E+OO 3.656E+Ol l.034E+02 4.514E-01 2.348E+00 5.281E-02 4.143E-01 7.293E-01 7.262E-01 3.512E-01 5.983E-01 2.147E-01 2.147E-01 5.983E-01 6.763E-02 2.385E-01 3.158E+OO 6.763E-02 O.OOOE+OO 2.174E-01 3.282E+02 5.175E-02 8.592E-02 7.120E-02 3.383E-02 4.022E-02 1.091E-01 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL A.BUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:13:57.96 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235013.CNF;l *
  • Acquisition date 3-0CT-2016 08:10:29 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.06 Half life ratio : ***** *
  • Sample date 8-DEC-2015 11:23:00 Nuclide Library : SOLID *
  • Sample ID G405235013 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.4457E+02 GRAM *
  • Quantity Err ( % ) : 1. 3834E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) K-40 l.342E+Ol 2 .119E+OO 2 .119E+OO RU-103 7.344E+OO 8.980E+OO 8.980E+OO CD-109 2.483E+OO 1. 729E+OO 1. 729E+OO SN-126 l.582E-01 l.099E-01 l.099E-01 BA-137M l.154E+00 1.769E-01 1. 769E-01 CS-137 1.219E+00 1.868E-01 1.868E-01 TL-208 3.288E-01 9.987E-02 9.987E-02 PB-210 1. 421E+OO 9.219E-01 9.219E-01 PB-212 1.184E+OO 1. 759E-01 1. 759E-01 BI-214 8.581E-01 1.998E-01 l.998E-01 PB-214 1. 026E+OO 2.207E-01 2.207E-01 RN-222 8.581E-01 l.998E-01 l.998E-01 RA-224 1.202E+OO 1. 743E+OO 1. 743E+OO RA-226 8.581E-01 1.998E-01 l.998E-01 AC-228 9.074E-01 3.666E-01 3.666E-01 RA-228 9.074E-01 3.666E-01 3.666E-01 TH-228 1.184E+OO 1. 759E-01 1. 759E-01 TH-229 2.255E-01 5.392E-01 5.392E-01 TH-230 8.578E-01 1.997E-01 1.997E-01 PA-231 1.277E+OO 1.126E+OO l.126E+OO TH-232 9.074E-01 3.666E-01 3.666E-01 TH-234 2.176E+OO 1.645E+OO 1.645E+OO U-234 8.578E-01 1.997E-01 1.997E-01 U-235 -2.341E-02 2.042E-01 2.042E-01 U-238 2.176E+00 1.645E+OO AM-243 2.641E-01 8.817E-02 8.817E-02 ANH-511 2.004E-01 8.181E-02 8.181E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 5.147E+OO 1.533E+Ol 1.550E+Ol NOT IDENT. NA-22 6.027E-03 5.948E-02 5.954E-02 NOT IDENT. NA-24 -l.OOOE+41 1.029E+41 O.OOOE+OO SHORT HLIF Page 3176 of 5809 AL-26 -3.212E-02 2.826E-02 3.175E-02 NOT IDENT. SC-46 -3. 272E-01 4.148E-01 4.402E-01 FAIL ABUN V-48 1.217E+04 1. 700E+04 1. 787E+04 SHORT HLIF CR-51 2.275E+Ol 4.497E+02 4.499E+02 SHORT HLIF MN-54 -5.825E-04 6.511E-02 6. 511E-02 NOT IDENT. co-56 -1. 375E-02 4.374E-01 4.375E-01 FAIL ABUN MN-56 -l.OOOE+41 3.761E+42 O.OOOE+OO SHORT HLIF C0-57 -1.237E-02 4.739E-02 4. 772E-02 FAIL ABUN C0-58 -7.185E-02 6.448E-01 6.456E-01 NOT IDENT. FE-59 -6.747E-01 9.590E+OO 9.595E+OO NOT IDENT. C0-60 -3.631E-02 4.315E-02 4.615E-02 NOT IDENT. ZN-65 -2.634E-01 2.409E-01 2.686E-01 NOT IDENT. GE-68 -1. 572E+OO 3.128E+OO 3.207E+OO NOT IDENT. AS-73 l.478E+OO 2.692E+OO 2.773E+OO NOT IDENT. AS-74 -3.064E+03 7.213E+03 7.344E+03 SHORT HLIF SE-75 1. 799E-02 2.404E-01 2.405E-01 FAIL ABUN BR-77 2.152E+38 l.863E+39 O.OOOE+OO SHORT HLIF SR-82 -l.024E+02 7.950E+02 7. 964E+02 SHORT HLIF RB-83 6.204E-01 5.302E-01 5.995E-01 FAIL ABUN KR-85 1.119E+Ol 9.582E+OO 1.083E+Ol NOT IDENT. SR-85 1.178E+OO 1.012E+OO 1.143E+OO NOT IDENT. RB-86 -2.266E+04 3.708E+04 3.846E+04 SHORT HLIF Y-88 -l.347E-01 2.058E-01 2.146E-01 NOT IDENT. Y-91 -3.063E+02 8.502E+02 8. 613E+02 NOT IDENT. NB-94 8.340E-03 3.900E-02 3.918E-02 NOT IDENT. NB-95 1.013E-01 9.653E-01 9.664E-01 NOT IDENT. NB-95M -7. 221E-01 2.945E+OO 2. 963E+OO NOT IDENT. ZR-95 -9.977E-02 1.746E+OO 1. 746E+OO NOT IDENT. NB-97 1.000E+41 2.778E+41 0.000E+OO SHORT HLIF ZR-97 -1.000E+41 2.499E+41 O.OOOE+OO SHORT HLIF M0-99 4.076E+31 1.946E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 4.249E+41 O.OOOE+OO SHORT HLIF RH-101 -1.200E-02 3.870E-02 3.907E-02 NOT IDENT. RH-102 -1.545E-02 7.935E-02 7. 966E-02 NOT IDENT. RH-106 l.730E-01 5.786E-01 5.838E-01 NOT IDENT. RU-106 1.730E-01 5.786E-01 5.838E-01 NOT IDENT. AG-108M 2.763E-03 3.303E-02 3.305E-02 NOT IDENT. AG-llOM -7.668E-04 l.217E-01 1. 217E-01 NOT IDENT. SN-113 -3.029E-02 2.802E-01 2.805E-01 NOT IDENT. CD-115 -1.504E+39 4.236E+39 O.OOOE+OO SHORT HLIF SN-ll 7M l.323E+04 9.993E+04 1.001E+05 SHORT HLIF TE-123M 8.356E-02 l.360E-01 1. 411E-01 NOT IDENT. SB-124 2.379E+OO 2.795E+OO 2.994E+OO NOT IDENT. SB-125 4.677E-02 l.341E-01 l.357E-01 FAIL ABUN TE-125M 1.899E+02 2.774E+02 2.903E+02 NOT IDENT. I-126 l.085E+06 l.288E+06 1.378E+06 SHORT HLIF SB-126 -3.412E+05 l.385E+06 1.394E+06 SHORT HLIF SB-127 4.426E+21 2.755E+22 O.OOOE+OO SHORT HLIF I-131 4.091E+09 5.631E+09 5.925E+09 SHORT HLIF I-132 1.000E+41 l.893E+42 O.OOOE+OO SHORT HLIF TE-132 -1. 311E+26 4.380E+26 O.OOOE+OO SHORT HLIF BA-133 4.340E-02 5.534E-02 5.869E-02 NOT IDENT. I-133 l.000E+41 4.882E+42 O.OOOE+OO SHORT HLIF CS-134 5.339E-02 6.913E-02 7.321E-02 NOT IDENT. CS-135 -2.247E-02 l.667E-01 1.670E-01 NOT IDENT. I-135 l.000E+41 6.999E+41 O.OOOE+OO SHORT HLIF CS-136 -3. 018E+04 4.130E+05 4.132E+05 SHORT HLIF CE-139 -5.176E-02 l.202E-01 1.224E-01 NOT IDENT. BA-140 -5.974E+05 l.444E+06 1. 469E+06 SHORT HLIF LA-140 -4.657E+05 5.575E+05 5.957E+05 SHORT HLIF CE-141 5.832E-01 2.697E+Ol 2.697E+Ol NOT IDENT. CE-143 1.000E+41 3. 931E+41 O.OOOE+OO SHORT HLIF CE-144 1. 757E-01 5.048E-01 5.109E-01 NOT IDENT. PM-144 2.327E-02 5.853E-02 5.946E-02 NOT IDENT. PR-144 3.672E-01 5.333E+OO 5.335E+OO NOT IDENT. PM-146 -2.107E-02 6.291E-02 6.362E-02 NOT IDENT. ND-147 .7.793E+06 4.210E+07 4.224E+07 SHORT HLIF PM-147 2.230E+02 8.012E+02 8.075E+02 NOT IDENT. PM-149 1.902E+40 5.441E+40 O.OOOE+OO SHORT HLIF EU-150 -8.134E-03 3.563E-02 3.582E-02 FAIL ABUN EU-152 3.350E-03 l .131E-01 l.132E-01 NOT IDENT. GD-153 -4.475E-03 1. 671E-01 1. 671E-01 NOT IDENT. EU-154 l.715E-02 l.463E-01 1.465E-01 NOT IDENT. EU-155 7.484E-02 1.043E-01 1.097E-01 FAIL ABUN TB-160 2.176E+OO 2.289E+OO 2.491E+OO FAIL ABUN H0-166M 6.081E-04 5. 596E-02 5.596E-02 FAIL ABUN TM-171 3.640E+OO 5.838E+OO 6.064E+OO NOT IDENT. HF-172 1.196E-01 2.635E-01 2.690E-01 FAIL ABUN Page 3177 of 5809 LU-172 8.250E-03 1.091E-01 1.091E-01 FAIL ABUN LU-176 1.038E-02 2.955E-02 2. 991E-02 FAIL ABUN HF-181 -1.063E+OO 5.597E+OO 5.618E+OO NOT IDENT. TA-182 9.516E-02 1.177E+OO l.178E+OO FAIL ABUN RE-183 7.378E-01 1.209E+OO l.254E+OO NOT IDENT. RE-184 3.078E+Ol 3.824E+Ol 4.067E+Ol NOT IDENT. W-188 -7.409E+Ol 1.429E+02 1. 467E+02 FAIL ABUN IR-192 -4.557E-02 5.237E-01 5.241E-01 FAIL ABUN HG-203 2.099E+OO 2.461E+OO 2.637E+OO NOT IDENT. BI-207 4. 081E-04 6.198E-02 6.198E-02 FAIL ABUN BI-211 2.826E+OO 6.098E-01 1.413E+OO FAIL ABUN PB-211 7.339E-01 7.955E-01 8.616E-01 NOT IDENT. BI-212 l.510E+OO l.031E+OO l.235E+OO FAIL ABUN RN-219 -2.732E-01 4.478E-01 4.644E-01 FAIL ABUN RA-223 1. 967E-01 6.673E-01 6.732E-01 FAIL ABUN AC-227 -2.352E-02 2.456E-01 2.458E-01 FAIL ABUN TH-227 -2.352E-02 2.456E-01 2.458E-01 FAIL ABUN TH-231 1. 967E-01 6.673E-01 6.732E-01 FAIL ABUN PA-233 2.532E-02 7.522E-02 7.608E-02 FAIL ABUN PA-234 -2.915E-02 3.090E-01 3.092E-01 NOT IDENT. PA-234M -2.595E+OO 4.356E+OO 4. 511E+OO NOT IDENT. NP-237 2.532E-02 7.522E-02 7.608E-02 FAIL ABUN NP-238 l.OOOE+41 2.895E+41 O.OOOE+OO SHORT HLIF NP-239 3.233E-02 2.332E-01 2.337E-01 NOT IDENT. PU-239 6.937E+02 6.321E+02 7.053E+02 FAIL ABUN AM-241 -4.753E-02 6.959E-02 7. 281E-02 NOT IDENT. CM-243 -4.333E-02 9.531E-02 9.729E-02 NOT IDENT. BK-247 5.619E-03 8.955E-02 8.959E-02 FAIL ABUN CM-247 -1.790E-02 4.192E-02 4.269E-02 NOT IDENT. CF-249 4.208E-04 4.683E-02 4.683E-02 NOT IDENT. CF-251 6.306E-02 l.160E-01 l.194E-01 NOT IDENT. Page 3178 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 60.6064 87.09 114.3639 136.47 83.1355 45.60 74.9070 87.57 114. 4384 140.51 0.0000 46.54 79.7381 88.03 114. 5095 143.76 83.7465 49. 72 0.0000 88.34 114.5576 144.24 82.8953 51. 35 130.1865 88.47 114.5771 145.44 88.3471 51. 87 117.2815 89. 96 114.8056 152.43 88.9463 52.39 93.6784 1093.63 114. 9095 153.25 0.0000 52.97 94. 9655 91.11 0.0000 323.87 65.6973 53.44 98. 6113 92. 59 115.2042 156.02 0.0000 54.07 101.1032 93.35 115.3178 158.56 0.0000 57.36 0.0000 94.56 115.4990 159.00 59.6648 57.53 112.4989 94.65 115. 5122 162.33 68.0092 57.98 110.1909 94.67 115.5150 162.66 0.0000 59.27 105.6350 94.87 84.7611 163.33 73.5167 59.32 129.6541 97.43 92.6535 165.86 76.4147 59.54 148.9184 98.43 88.4496 176.31 70.6969 60. 96 136.4368 98.44 88.4507 176.60 0.0000 61.17 136.4847 99.53 78.8997 177.52 52.3886 62.93 123.1975 100 .11 90.8429 181.07 0.0000 63.29 123.2705 102.03 92.7610 181. 52 52.5683 63.58 123.3296 103.18 98.8568 184.41 74.8853 64.28 123.4711 103.37 105.6991 143.76 65.7124 66.73 155.5576 105.21 87.1400 193.51 67.9994 67.24 136. 2240 105.31 87.1509 197.03 73.7989 125.81 116.8447 106.12 96.6433 198.01 77.5964 67.75 116. 8572 106.47 100.9621 201.83 71. 2693 69.67 120.4660 109.28 84.1300 203.43 69.4819 70.83 159.8222 111. 00 100.6433 205.31 81. 8085 72.81 150.9000 111.76 0.0000 210.85 57.6076 72. 87 150.9141 114. 06 80.2818 215.65 48.3406 74.66 151.3204 116.30 0.0000 222 .11 57.1484 74.82 151.3561 116. 74 78.7951 227.09 60.2270 74.97 151. 38 99 119. 76 79.0622 227.38 62.1521 77 .11 151.8685 121.12 73.0903 228.16 0.0000 78.74 118. 8120 121. 22 73.0984 228.18 59.3183 79.69 133.8464 121.78 74.8852 116.74 59.3183 80.12 106.6470 122.06 83.6182 235.69 64.9319 80.19 0.0000 122.92 91.5439 235. 96 64.9443 80.57 134.0145 123.07 101.1507 238.63 51.0904 81. 00 142.3745 265.00 85.5117 238.98 0.0000 81. 07 142.3885 125.81 76.0887 240.99 51.1755 81. 75 115. 5944 127.23 89.3429 242.00 51.2122 83.79 115. 9250 127.91 95.9827 244.70 53.7295 84.00 115. 9591 129.30 81. 6389 252.40 0.0000 85.43 116.1876 131.20 73.8871 252.80 44.7820 86.55 114.2803 133.02 71. 3834 254.15 0.0000 86.79 114.3172 133.52 74.0657 256.23 46.8379 86.94 114. 3409 136.00 83.0953 260.90 0.0000 Page 3179 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 44.7474 355.39 0.0000 584.27 20.6689 264.80 45.6353 356.01 34.1957 595.83 0.0000 265.00 45.6410 364.49 0.0000 427.87 28.8839 2 68. 22 45.7375 366.42 0.0000 602.52 0.0000 269.46 37.4078 372.51 29.2703 604. 72 17.3572 . 270.03 37.4217 375.05 34 .. 5428 607.14 27.7959 271.23 37. 4511 377.52 34.5872 609.32 15.0683 273.65 0.0000 356.01 36.8037 610.33 15.0741 276.40 41. 5317 388.16 38.9918 614.28 29.6110 277.37 48.9783 388.63 0.0000 618.01 30.2328 277.60 48.9854 391. 69 36.9504 620.36 23.2764 278.00 45.1380 264.66 29.6936 621. 93 16.3026 279.20 31. 6999 401. 81 38.1995 630.19 0.0000 279.54 31. 707 0 402.40 38.2104 631. 29 22.4336 279.70 34.6831 404.85 24.2296 633.25 25.2554 280.46 32.7167 410.95 27.1799 634.78 0.0000 283.69 45.6986 413.71 27.2167 635.95 21.0667 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 39.7811 423.72 0.0000 645.85 16.7369 285.90 0.0000 427.09 32.2266 657.76 15.5687 287.50 41. 8248 427.87 33.3128 657.90 0.0000 290.67 50.8879 433.94 29.0978 661.66 27.4590 293.27 0.0000 439.40 22.6898 664.57 0.0000 351.93 46.5284 453.88 44.5960 666.3'3 0.0000 295. 96 46.5492 463.37 46.9726 666.50 0.0000 879.38 36.0959 468.07 39.4087 667.71 0.0000 299.98 34.6214 473.00 0.0000 677.62 13.3598 300.09 34.6235 475.06 47.2176 685.70 0.0000 300.13 34.6249 476.78 26.3740 695.00 0.0000 301.36 34.6502 477.60 26.3833 696.49 14.3418 302.85 46.7450 482.18 31.9441 696. 51 17.9272 256.23 52.8290 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.6219 306.78 44.3366 497.08 29.9331 697.49 22.4167 308.46 56.4853 505.52 21.6959 702.65 21. 5574 311.90 47.5039 507.63 0.0000 706.68 17.9883 316.51 40.5387 511. 00 21.7459 711. 68 13.5136 319.41 0.0000 514.00 21.7733 720.70 0.0000 320.08 0.0000 514.00 21.7733 721. 93 0.0000 321.04 39.6300 520.40 3.3586 722.78 16.8779 323.87 37.6594 520.69 0.0000 722. 91 17.3613 325.23 45.8377 522.65 0.0000 723.31 18.8106 328.76 0.0000 527.90 0.0000 724.19 18.8157 333.37 35.3058 528.26 18.5323 727. 33 21.7324 333.97 50.6732 529.59 21.3518 733.00 13.0636 334.37 43.0049 529.87 0.0000 735.93 17.2530 338.28 40.0212 531.02 0.0000 333.97 11. 8106 338.32 40.0220 537.26 0.0000 739.50 0.0000 311. 90 44.6939 546.56 0.0000 747.24 15.4929 340.48 44.6939 552.55 13. 6108 748.06 14.5850 340.55 0.0000 563.25 22.7799 752.31 22.8203 344.28 38.3012 569.33 22.8337 753.82 0.0000 345.93 41.7376 946.00 15.9847 756.73 18.2819 351.06 38.2375 569.70 15.9858 756.80 18.2819 351. 93 38.2556 583.19 20.6602 884.68 12.8259 Page 3180 of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.4171 1274.44 14.6750 1620.50 4.4641 766.42 15.5868 1001.03 10.7747 1621.92 4.4653 766.84 14. 6719 1002.74 11.,7 594 1678.03 0.0000 772.60 0.0000 1004.73 9.8044 1690.97 2.7114 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.9150 778.90 10.3086 1028.54 0.0000 1063.66 11. 9063 783.70 0.0000 1037.84 12.8524 1771. 35 3.6643 785.37 10.3291 1038.76 0.0000 1791.20 0.0000 792.07 26.7999 631.29 7.9263 1808.65 4.6082 794.95 10.1745 1048.07 0.0000 1810.72 0.0000 795.86 18.5040 1049.04 11.8967 1836.06 3.7029 810.06 14.8667 1050.41 15.8682 810.29 13.9384 1063.66 13.9299 344.28 14.8687 1077.00 0.0000 810.76 13.9407 1077.34 16.9709 815.77 0.0000 1085.87 12.0037 1048.07 0.0000 1093.63 16.0352 832.01 8.4172 1099.45 12.8461 834.85 12.1685 1112. 07 11. 0725 835. 71 13.1075 1112. 84 8.0542 836.80 0.0000 1115. 54 20.7246 846.75 0.0000 1120. 29 8.0684 846.77 9.3927 1120. 55 8:0688 856.80 0.0000 1221.41 19.1670 860.56 11.3163 1129. 67 15 .1611 871.09 11. 3503 1131.51 0.0000 873.19 8.5177 1147.95 0.0000 875.33 0.0000 1173.23 7.1465 879.38 9.4809 1177.95 11.2424 880. 5.1 11. 3804 1189.05 17.4182 883.24 18.0328 1204.77 18.0963 884.68 12.3434 1221. 41 13. 4158 889.28 15.2114 1231. 02 13.0003 894.76 8.5696 1235.36 0.0000 898.04 10.4834 1238.28 16.5723 900 .. 72 11. 4448 1260.41 0.0000 903.28 10.4985 1271.87 8.3462 911.20 11.4781 1274.44 10.4382 912.08 11. 4807 1274.54 10.4388 923.98 0.0000 1291. 59 6.2860 926.50 8.6446 1298.22 0.0000 929 .11 15.3789 1312 .11 0.0000 937.49 6.7434 1332.49 9.5092 944.13 0.0000 1362.66 0.0000 946.00 10.2992 1365.19 5.3183 949.00 9.2766 1368.63 0.0000 667.71 0.0000 1384.29 7.4742 962.31 25.2129 1408.01 2.1455 964. 08 18 .1101 1457.56 0.0000 966 .17 13.9781 1460.82 5.4190 911.20 34.1945 1489.16 6.5380 968. 97 34.1945 1505.03 1. 0 92 9 983.53 0.0000 1584.12 5.5441 984.45 0.0000 1596.21 0.0000 Page 3181 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:14:26.62 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG Background date : Z-OCT-2016 11:02:23. Sample date 8-DEC-2015 10:49:00. Acquisition date : 3-0CT-2016 08:11:15. Sample ID G405235014 Sample quantity : 1.53732E+02 GRAM Detector name : GAM43 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.71 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 4 4 0 0 0 3 3 6 6 0 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3182of5809 Energy 47.48 62.99* 74.87 76.92 90.01 92. 96* 109.22 186.07* 210.28 238.55* 241.44 266.97 270.06 277.80 295.37* 301.50 337.91 352.00* 434.31 440.31 444.15 463.30 510.77* 583 .13* 609.17* 661. 58 665.90 695.65 704.04 727.74 754.99 768.76 773.28 794.87 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 53 25 99 173 50 81 21 84 35 415 88 13 26 33 158 36 105 209 20 24 29 31 62 106 136 208 19 17 21 19 54 18 8 28 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 153 69 168 176 61 149 125 169 153 56 77 30 68 90 77 76 47 50 58 18 22 37 41 63 46 36 5 23 27 27 20 18 11 6 1. 50 0.84 1. 36 1. 29 0.94 1. 70 1. 34 1. 09 0.58 1. 08 1. 90 1. 36 1. 58 1. 33 1. 26 4.72 1.16 1. 20 4.44 2.02 2.03 0.88 2.24 1. 45 1. 43 1. 65 0.61 0.86 0.89 1. 03 8.83 1. 41 1. 41 1. 00 94.74 125.76 149.53 153.64 179.82 185.73 218.25 372.01 420.44 476.99 482.76 533.85 540.02 555.51 590.66 602.93 675.76 703.94 868.61 880.60 888.30 926.60 1021.56 1166. 31 1218.40 1323.25 1331.88 1391.39 1408.18 1455.59 1510.09 1537.65 1546.69 1589.88 90 124 145 145 178 178 214 366 412 472 472 532 532 549 584 596 670 700 861 87 6 876 924 1014 1160 1212 1318 1329 1386 1397 1448 1497 1532 1543 1585 13 1.47E-02 50.3 5 6.82E-03 56.7 13 2.74E-02 25.5 13 4.81E-02 15.3 16 1. 39E-02 25. 8 16 2. 24E-02 31. 9 9 5.70E-03101.0 12 2.34E-02 33.7 12 9.81E-03 72.0 18 1.15E-01 5. 7 18 2. 43E-02 31. 5 12 3.68E-03 62.7 12 7.35E-03 58.9 10 9.20E-03 56.8 13 4.40E-02 14.1 13 9.97E-03 53.3 10 2.91E-02 15.7 11 5.80E-02 9.6 16 5.63E-03 88.1 17 6.72E-03 42.2 17 8.07E-03 36.7 8 8.55E-03 39.5 15 1.72E-02 29.6 12 2.94E-02 18.1 13 3.78E-02 13.5 12 5.79E-02 9.0 7 5.28E-03 31.7 12 4.72E-03 62.3 18 5.95E-03 60.8 12 5.27E-03 59.4 27 1.51E-02 26.7 11 4.98E-03 54.8 8 2.35E-03 73.9 10 7.64E-03 26.4 Fit 2.30E+OO 1.43E+OO 1. 71E+OO 2.44E+00 1.57E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235014 Acquisition date 3-0CT-2016 08:11:15 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 799.01 9 5 0.56 1598.16 1595 8 2.62E-03 49.7 36 0 821.19 9 12 4.21 1642.52 1635 10 2.46E-03 86.4 37 0 910.92 96 6 1. 79 1822.01 1816. 11 2.65E-02 11. 3 38 0 935.10 12 21 0.80 1870.38 1859 14 3.33E-03 86. 0 39 0 969. 52 25 44 1.27 1939.21 1933 14 6.81E-03 61. 6 40 0 1031. 64 13 11 0.88 2063.48 2052 15 3.52E-03 64.1 41 0 1050.16 13 9 3.86 2100.52 2094 12 3.59E-03 54.1 42 0 1093.61 31 5 4.87 2187.43 2177 20 8.69E-03 25.0 43 0 1120.46 40 3 2.67 2241.12 2235 13 1.lOE-02 18.5 44 0 1155. 98 16 16 0.84 2312.18 2305 13 4.49E-03 56.9 45 0 1197. 74 8 13 0.71 2395.70 2387 13 2.32E-03 95.2 46 0 1376.00 2 0. 0 3.21 2752.25 2744 16 5.56E-03 22.4 47 0 1460.53* 335 4 2.38 2921.30 2913 15 9.30E-02 5.7 48 0 1764.33* 28 0 3.32 3528.90 3522 14 7.82E-03 20.0 49 0 1847.78 9 0 1. 07 3695.78 3692 9 2.50E-03 33.3 Flag: "*" = Peak area was modified by background subtraction Page 3183of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:14:28 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 8-DEC-2015 10:49:00 G405235014 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 08:11:15 153.73 GRAM Sample type. Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA43 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3184 of5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.71 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235014 Acquisition date 3-0CT-2016 08:11:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1. 002E+OO. 1.481E+Ol l.481E+Ol 11. 33 OK TE-125M 109.28 0.27* 5.555E+OO 8.391E+OO 3.138E+02 202.05 OK CS-135 268.22 16.00* 4.339E+OO l.078E-01 1.078E-01 125.35 OK BA-137M 661. 66 89.90* 1.974E+OO 6.050E-01 6.165E-01 18.01 OK CS-137 661. 66 85.10* 1.974E+OO 6.391E-01 6.513E-01 18.01 OK PR-144 696. 51 1.34* 1.892E+OO 3.437E+OO 7.130E+OO 124.51 OK 1489.16 0.28 9.838E-01 Line Not Found Absent HG-203 70.83 3.69 2.720E+OO Line Not Found Absent 72.87 6.19 2.941E+OO Line Not Found Absent 279.20 81.56* 4.200E+OO 3.048E-02 2.642E+OO 204.81 OK TL-208 277.37 6.60 4.205E+OO Line Not Found <<INT Reject 583.19 85.00* 2.199E+OO 2.958E-01 2.958E-01 36.14 OK 860.56 12.50 l.582E+OO Line Not Found Absent PB-210 46.54 4.25* 3.240E-01 2.540E+Ol 2.606E+Ol 100.60 OK PB-212 74.82 10.28 3.152E+OO l.248E+OO 1.248E+OO 80.16 OK 77 .11 17.10 3.363E+OO 1.907E+OO 1.907E+OO 30.68 OK 238.63 43.60* 4.740E+OO 1.147E+OO l.147E+00 11. 44 OK 300.09 3.30 3.919E+OO 1.548E+OO l.548E+00 106.58 OK BI-214 609.32 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 OK 1120.29 14.92 l.266E+OO 1.020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1.016E+OO 1. 017E+OO 39.95 OK PB-214 74.82 5.80 3.147E+OO Line Not Found <<INT Reject 77 .11 9.70 3.363E+OO 3.361E+OO 3.362E+OO 30.68 OK 87.09 3.41 4.287E+OO Line Not Found Absent 242.00 7.25 4.688E+OO Line Not Found <<INT Reject 295.22 18.42 3.989E+OO 1.205E+OO 1.205E+OO 28 .11 OK 351. 93 35.60* 3.425E+OO 9.411E-01 9.414E-01 19.18 OK RN-222 609.32 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 OK 1120. 29 14.92 1. 266E+OO 1.020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1.016E+OO 1. 017E+OO 39.95 OK RA-224 240.99 4.10* 4.697E+OO 4.607E-01 4.607E-01 377.38 OK RA-226 609.32 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 OK 1120.29 14.92 1.266E+OO 1.020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1.016E+OO 1. 017E+OO 39.95 OK AC-228 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.550E+OO 1.444E+OO 1.444E+OO 31. 44 OK 794.95 4.25 1.691E+OO l.935E+00 1. 935E+OO 52.79 OK 835. 71 1. 61 1.621E+OO Line Not Found Absent 911. 20 25.80* 1.508E+00 1.222E+OO 1.222E+OO 22.57 OK 968. 97 15.80 l.431E+OO 5.358E-01 5.358E-01 123.29 OK RA-228 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.550E+OO 1.444E+OO 1.444E+OO 31. 44 OK 794.95 4.25 1. 691E+OO 1.935E+OO 1.935E+00 52.79 OK 835.71 1. 61 1. 621E+OO Line Not Found Absent 911.20 25.80* 1.508E+OO 1.222E+OO 1.222E+OO 22.57 OK 968. 97 15.80 1. 431E+OO 5.358E-01 5.358E-01 123.29 OK TH-228 74.82 10.28 3.152E+OO 1.248E+OO 1.248E+OO 80.16 OK 77 .11 17 .10 3.363E+OO l.907E+OO 1.907E+OO 30.68 OK 238.63 43.60* 4.740E+OO 1.147E+OO 1.147E+OO 11. 44 OK Page 3185of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235014 Acquisition date 3-0CT-2016 08:11:15 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 3.919E+OO .1. 548E+OO 1.548E+OO 106.58 OK TH-230 609.32 45.49* 2 .118E+OO 7.335E-01 7.335E-01 27.01 OK 1120.29 14.92 1. 2 66E+OO 1.020E+OO 1.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1.016E+OO 1.016E+OO 39.95 OK PA-231 283.69 1. 70 4.127E+OO Line Not Found Absent 301.36 5.35* 3.919E+OO 9.549E-01 9.549E-01 106.58 OK TH-232 105.21 1.10 5. 396E+OO Line Not Found Absent 338.32 11. 27 3.550E+OO 1.444E+OO 1.444E+OO 31. 44 OK 835.71 1. 61 1. 621E+OO Line Not Found Absent 911.20 25.80* 1.508E+OO l.222E+OO 1.222E+OO 22.57 OK 968. 97 15.80 1.431E+OO 5.358E-01 5.358E-01 123.29 OK TH-234 63.29 3.70* l.836E+OO 2.324E+00 2.324E+00 113. 44 OK 92.59 4.23 4.722E+00 2.512E+OO 2.512E+OO 63.86 OK U-234 609.32 45.49* 2 .118E+OO 7.335E-01 7.335E-01 27.01 OK 1120.29 14.92 l.266E+OO l.020E+OO l.020E+OO 36.97 OK 1764.49 15.30 8.364E-01 1.016E+OO 1. 016E+OO 39.95 OK U-235 89. 96 3.47 4.512E+OO 1.994E+OO 1.994E+OO 51.66 OK 93.35 5.60 4. 722E+00 1. 897E+OO 1.897E+00 63. 86 OK 143:76 10.96* 6.023E+OO Line Not Found Absent 163.33 5.08 5.876E+OO Line Not Found Absent 185. 72 57.20 5.564E+OO 1.546E-01 1.546E-01 67.36 OK 205.31 5.01 5.260E+OO Line Not Found Absent U-238 63.29 3.70* l.836E+OO 2.324E+00 2.324E+00 113. 44 OK 92.59 4.23 4. 722E+OO 2.512E+OO 2.512E+OO 63.86 OK AM-243 43.53 5.90 l.216E-01 Line Not Found Absent 74.66 67.20* 3.152E+OO 1.910E-01 l.910E-01 80.16 OK ANH-511 511. 00 100.00* 2.466E+OO 1. 32 6E-01 1.326E-01 59.16 OK Flag: "*" = Keyline Page 3186 of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:14:29.63 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l, * *Acquisition date 3-0CT-2016 08:11:15 Sensitivity : 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.71 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:49:00 Analyst initials: MXRl *
  • Sample ID G405235014 Sample Quantity 1.5373E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA'. GAMMA] EFF GAM43 CAN. CNF; 7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.481E+Ol 1.644E+OO 6.863E-01 TE-125M 3 .138E+02 6.214E+02 5.267E+02 CS-135 l.078E-01 l.324E-01 2. 716E-01 BA-137M 6.165E-01 1.088E-01 7.973E-02 CS-137 6.513E-01 1.150E-01 8.423E-02 PR-144 7.130E+OO 8.700E+00 9.976E+OO HG-203 2.642E+OO 5.302E+OO 4.912E+OO TL-208 2.958E-01 l.048E-01 7.283E-02 PB-210 2.606E+Ol 2.569E+Ol 1.890E+Ol PB-212 1.147E+OO 1.286E-01 9.376E-02 BI-214 7.337E-01 1.942E-01 1.399E-01 PB-214 9.414E-01 l.770E-01 1.295E-01 RN-222 7.337E-01 1.942E-01 l.399E-01 RA-224 4.607E-01 1.704E+OO 1.005E+OO RA-226 7.337E-01 l.942E-01 l.399E-01 AC-228 1.222E+OO 2.702E-01 2.657E-01 RA-228 1.222E+OO 2.702E-01 2.657E-01 TH-228 1.147E+OO 1.286E-01 9.376E-02 TH-230 7.335E-01 l.942E-01 l.398E-01 PA-231 9.549E-01 9.974E-01 8.322E-01 TH-232 1.222E+OO 2.702E-01 2.657E-01 TH-234 2.324E+OO 2.583E+OO 3.466E+OO U-234 7.335E-01 l.942E-01 l.398E-01 U-235 -2.352E-02 l.788E-01 3.515E-01 U-238 2.324E+00 2.583E+OO 3.466E+OO AM-243 l.910E-01 1.500E-01 1.329E-01 ANH-511 1. 326E-01 7.689E-02 5.390E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -1.129E+Ol 1. 462E+Ol 2.444E+Ol NOT IDENT. NA-22 -8.378E-03 4.504E-02 8.932E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF Page 3187 of 5809 AL-26 -3.236E-02 3.683E-02 5.583E-02 NOT IDENT. SC-46 7.289E-02 3.221E-01 6.806E-01 FAIL ABUN V-48 O.OOOE+OO 1.413E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.006E+02 O.OOOE+OO SHORT HLIF MN-54 -1.942E-02 6.643E-02 l.240E-01 NOT IDENT. C0-56 -9.078E-02 5.059E-01 9.614E-01 NOT IDENT. MN-56 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF C0-57 3.139E-03 5.206E-02 9.550E-02 NOT IDENT. C0-58 -1.237E-01 5.755E-01 1.101E+OO NOT IDENT. FE-59 4.269E+OO 8.949E+OO 1.651E+Ol NOT IDENT. C0-60 2.219E-02 4.296E-02 9.516E-02 NOT IDENT. ZN-65 -1.444E-01 2.380E-01 3.342E-01 NOT IDENT. GE-68 5.698E-01 2.104E+OO 4.417E+OO NOT IDENT. AS-73 1.078E+OO 1.785E+Ol 3.442E+Ol NOT IDENT. AS-74 O.OOOE+OO 6. 601E+03 O.OOOE+OO SHORT HLIF SE-75 -1.310E-01 2.388E-01 3.840E-01 NOT IDENT. BR-77 0.000E+OO 2.356E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.819E+02 O.OOOE+OO SHORT HLIF RB-83 -1.294E-01 7.147E-01 1.395E+OO NOT IDENT. KR-85 -3.310E+OO 9.208E+OO 1.412E+Ol NOT IDENT. SR-85 -3.512E-01 9.735E-01 1.492E+OO NOT IDENT. RB-86 O.OOOE+OO 2.538E+04 O.OOOE+OO SHORT HLIF Y-88 -1.760E-01 1.823E-01 1. 968E-01 NOT IDENT. Y-91 -2.612E+02 6. 7 61E+02 1.259E+03 NOT IDENT. NB-94 5.865E-02 6.989E-02 6.659E-02 FAIL ABUN NB-95 7.046E-01 1.044E+OO 1.992E+OO NOT IDENT. NB-95M -1.012E+00 2.615E+OO 4.336E+OO NOT IDENT. ZR-95 1.957E+OO 1.629E+OO 3.655E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.583E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.482E+41 O.OOOE+OO SHORT HLIF RH-101 -3.795E-02 4.00lE-02 6.654E-02 NOT IDENT. RH-102 5.154E-02 5.776E-02 1.285E-01 NOT IDENT. RU-103 1.514E+OO 5.774E+OO 1.128E+Ol FAIL ABUN RH-106 2. 972E-01 4. 719E-01 1. 026E+OO FAIL ABUN RU-106 2. 972E-01 4.719E-01 1.026E+00 FAIL ABUN AG-108M 4.241E-02 7.319E-02 6.090E-02 FAIL ABUN CD-109 1. 734E+OO 1.563E+OO 2.901E+OO NOT IDENT. AG-110M -1.342E-01 1.085E-01 1.641E-01 NOT IDENT. SN-113 -2.478E-01 2.780E-01 4.697E-01 NOT IDENT. CD-115 O.OOOE+OO 3.293E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 9.876E+04 O.OOOE+OO SHORT HLIF TE-123M 1.303E-01 1. 351E-01 2.830E-01 NOT IDENT. SB-124 -3.031E-01 2.005E+OO 4. l 71E+OO NOT IDENT. SB-125 2.322E-02 1.247E-01 2.148E-01 FAIL ABUN I-126 O.OOOE+OO 9.035E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.424E+06 0.000E+OO SHORT HLIF SN-126 O.OOOE+OO 9. 931E-02 1. 962E-01 FAIL ABUN SB-127 O.OOOE+OO 2.142E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.700E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.120E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.875E+26 O.OOOE+OO SHORT HLIF BA-133 1.923E-03 4.564E-02 7.799E-02 FAIL ABUN I-133 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 6.553E-02 1.245E-01 FAIL ABUN I-135 O.OOOE+OO 1.833E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.236E+05 O.OOOE+OO SHORT HLIF CE-139 -1.909E-02 1.037E-01 2.027E-01 NOT IDENT. BA-140 O.OOOE+OO 1.438E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.120E+05 O.OOOE+OO SHORT HLIF CE-141 -2.980E+OO 2.395E+Ol 4.726E+Ol NOT IDENT. CE-143 O.OOOE+OO 8 .116E+40 O.OOOE+OO SHORT HLIF CE-144 -8.042E-02 3.852E-01 7.583E-01 NOT IDENT. PM-144 8.208E-02 l.002E-01 1.253E-01 FAIL ABUN PM-146 1. 728E-02 4.907E-02 9.645E-02 NOT IDENT. ND-147 O.OOOE+OO 3. 358E+o7 O.OOOE+OO SHORT HLIF PM-147 1.955E+02 9.309E+02 1.727E+03 NOT IDENT. PM-149 O.OOOE+OO 5.276E+40 O.OOOE+OO SHORT HLIF EU-150 2.285E-03 3.046E-02 5.200E-02 FAIL ABUN EU-152 -6.069E-02 1.084E-01 1.931E-01 NOT IDENT. GD-153 -8.930E-02 2.365E-01 3.882E-01 NOT IDENT. EU-154 -2.756E-02 1.142E-01 2.231E-01 NOT IDENT. EU-155 2.749E-02 1.236E-01 2.158E-01 NOT IDENT. TB-160 1.175E-01 1.916E+OO 3.810E+OO NOT IDENT. H0-166M -1. 54 7E-02 6.203E-02 1.175E-01 NOT IDENT. TM-171 -1.986E+Ol 4.678E+Ol 7. 968E+Ol NOT IDENT. HF-172 2.189E-01 2.466E-01 4.829E-01 FAIL ABUN Page 3188 of5809 LU-172 O.OOOE+OO 1. 244E-01 2. OOlE-01 FAIL ABUN LU-176 -4.830E-03 2.643E-02 4. 421E-02 NOT IDENT. HF-181 -1.802E+00 4.908E+00 8.702E+OO NOT IDENT. TA-182 9.192E-03 1.077E+OO 2.130E+00 FAIL ABUN RE-183 3.007E-01 5.700E+00 1. 096E+Ol NOT IDENT. RE-184 -6 .113E+00 3.426E+Ol 6.457E+Ol NOT IDENT. W-188 -3.102E+Ol l.259E+02 2.089E+02 FAIL ABUN IR-192 -2.127E-01 4. 731E-01 8.620E-01 FAIL ABUN BI-207 1. 715E-02 5.288E-02 l.075E-01 FAIL ABUN BI.-211 O.OOOE+OO 4.875E-01 8.259E-01 FAIL ABUN PB-211 -4.174E-01 6.882E-01 1.202E+OO NOT IDENT. BI-212 7. 965E-01 9.276E-01 l.307E+OO FAIL ABUN RN-219 l.993E-01 4.340E-01 8.510E-01 FAIL ABUN RA-223 -2.664E-01 6.167E-01 l.122E+OO FAIL ABUN AC-227 4.542E-02 2.299E-01 4.506E-01 NOT IDENT. TH-227 4.542E-02 2.299E-01 4.506E-01 NOT IDENT. TH-229 6.960E-02 4.526E-01 8.954E-01 FAIL ABUN TH-231 -2.664E-01 6.167E-01 1.122E+OO FAIL ABUN PA-233 2.563E-03 6.297E-02 1.204E-01 FAIL ABUN PA-234 1.054E-01 2.756E-01 5.773E-01 NOT IDENT. PA-234M 1. 875E+OO 5.187E+OO 1. 036E+Ol NOT IDENT. NP-237 2.563E-03 6.297E-02 l.204E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -1.186E-01 2.716E-01 4.776E-01 FAIL ABUN PU-239 l.003E+02 3.584E+02 6.616E+02 NOT IDENT. AM-241 8.840E-02 2.500E-01 4.899E-01 NOT IDENT. CM-243 3.917E-02 1.137E-01 2.158E-01 FAIL ABUN BK-247 -4.830E...:02* 8.371E-02 1.341E-01 NOT IDENT. CM-247 1.053E-03 3. 963E-02 7.438E-02 FAIL ABUN CF-249 4.493E-02 4.237E-02 8.790E-02 NOT IDENT. CF-251 5.042E-02 1.112E-01 2.257E-01 NOT IDENT. Page 3189of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:14:27.34 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 324 10.66* 1.002E+OO 1. 481E+Ol 1.481E+Ol 11.33 TE-125M 109.28 26 0.27* 5.555E+OO 8.391E+OO 3.138E+02 202.05 CS-135 268.22 15 16.00* 4.339E+OO 1.078E-01 l.078E-01 125.35 BA-137M 661.66 220 89.90* 1.974E+OO 6.050E-01 6.165E-01 18.01 CS-137 661. 66 220 85.10* 1.974E+OO 6. 391E-01 6.513E-01 18.01 PR-144 696. 51 18 1.34* 1. 8 92E+OO 3.437E+OO 7.130E+OO 124.51 1489.16 ------0.28 9.838E-01 ------Line Not Found ------HG-203 70.83 ------3.69 2.720E+00 ------Line Not Found ------72. 87 ------6.19 2. 941E+OO ------Line Not Found ------279.20 38 81.56* 4.200E+OO 5.442E-02 4.716E+OO 113. 61 TL-208 277.37 38 6.60 4.200E+OO 6. 725E-01 6.725E-01 113. 61 583.19 113 85.00* 2.199E+00 2.958E-01 2.958E-01 36.14 860.56 ------12.50 1. 582E+OO ------Line Not Found ------PB-210 46.54 72 4.25* 3.240E-01 2.540E+Ol 2.606E+Ol 100.60 BI-211 72. 87 ------1.23 2.941E+OO ------Line Not Found ------351.06 235 12.92* 3.425E+OO 2.593E+OO 2.593E+'OO 19.18 PB-212 74.82 128 10.28 3.152E+OO l.928E+OO l.928E+OO 50.94 77 .11 225 17.10 3.363E+OO 1.907E+OO l.907E+OO 30.68 238.63 486 43.60* 4.740E+OO l.147E+OO l.147E+OO 11. 44 300.09 41 3.30 3.919E+OO 1.548E+OO l.548E+OO 106.58 BI-214 609.32 145 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 1120.29 39 14.92 1. 2 66E+OO l.020E+00 l.020E+OO 36.97 1764.49 27 15.30 8.364E-01 l.016E+OO 1. Ol 7E+OO 39.95 PB-214 74.82 128 5.80 3.152E+OO 3.418E+OO 3.419E+OO 50.94 77 .11 225 9.70 3.363E+OO 3.361E+OO 3.362E+00 30.68 87.09 ------3.41 4.287E+OO ------Line Not Found ------242.00 102 7.25 4.697E+OO l.465E+OO l.466E+OO 62.99 295.22 181 18.42 3.989E+OO l.205E+OO l.205E+00 28 .11 351. 93 235 35.60* 3.425E+OO 9. 411E-01 9.414E-01 19.18 RN-222 609.32 145 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 1120.29 39 14.92 l.266E+OO l.020E+OO l.020E+OO 36.97 1764.49 27 15.30 8.364E-01 l.016E+OO l.017E+OO 39.95 RA-224 240.99 102 4.10* 4.697E+OO 2.591E+OO 2. 591E+OO 62.99 RA-226 609.32 145 45.49* 2 .118E+OO 7.335E-01 7.337E-01 27.01 1120.29 39 14.92 1.266E+OO 1.020E+OO l.020E+OO 36.97 1764.49 27 15.30 8.364E-01 1.016E+OO l.017E+OO 39.95 AC-228 105.21 ------1.10 5.396E+OO ------Line Not Found ------338.32 118 11. 27 3.550E+OO l.444E+OO l.444E+OO 31. 44 794.95 28 4.25 l.691E+00 1.935E+OO 1.935E+OO 52.79 835.71 ------1. 61 1. 621E+OO ------Line Not Found ------911.20 97 25.80* 1.508E+OO l.222E+OO l.222E+OO 22.57 968. 97 25 15.80 l.431E+OO 5.358E-01 5.358E-01 123.29 RA-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 118 11. 27 3.550E+OO 1.444E+OO l.444E+00 31. 44 794.95 28 4. 2-5 1.691E+OO l.935E+OO l.935E+OO 52.79 835. 71 ------1. 61 l.621E+OO ------Line Not Found ------911. 20 97 25.80* l.508E+OO l.222E+00 l.222E+OO 22.57 Page 3190 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235014 Acquisition date 3-0CT-2016 08:11:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 968. 97 25 15.80 1.431E+OO 5.358E-01 5.358E-01 123. 29 TH-228 74.82 128 10.28 3.152E+OO 1.928E+OO 1.928E+OO 50.94 77 .11 225 17.10 3.363E+OO 1.907E+OO 1.907E+OO 30.68 238.63 486 43.60* 4.740E+OO 1.147E+OO 1.147E+OO 11. 44 300.09 41 3.30 3.919E+OO 1.548E+OO 1.548E+OO 106.58 TH-230 609.32 145 45.49* 2.118E+OO 7.335E-01 7.335E-01 27.01 1120.29 39 14.92 1.266E+OO 1.020E+OO 1.020E+OO 36.97 1764.49 27 15.30 8.364E-01 1.016E+OO 1.016E+OO 39.95 PA-231 283.69 ------1. 70 4.127E+OO ------Line Not Found ------301.36 41 5.35* 3.919E+OO 9.549E-01 9.549E-01 106.58 TH-232 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 118 11.27 3.550E+00 1.444E+OO 1.444E+OO 31. 44 835. 71 ------1. 61 1.621E+OO ------Line Not Found ------911. 20 97 25.80* 1.508E+OO 1.222E+OO 1.222E+OO 22.57 968.97 25 15.80 1.431E+OO 5.358E-01 5.358E-01 123.29 TH-234 63.29 32 3.70* 1.836E+OO 2.324E+OO 2.324E+OO 113. 44 92.59 103 4.23 4. 722E+OO 2.512E+OO 2.512E+OO 63.86 U-234 609.32 145 45.49* 2 .118E+OO 7.335E-01 7.335E-01 27.01 1120.29 39 14.92 1.266E+OO 1.020E+OO 1.020E+OO 36.97 1764.49 27 15.30 8.364E-01 1.016E+OO 1.016E+OO 39.95 U-235 89. 96 64 3.47 4.512E+OO 1.994E+OO 1.994E+OO 51.66 93.35 103 5.60 4. 722E+OO 1.897E+OO 1.897E+OO 63.86 143.76 ------10. 96* 6.023E+OO ------Line Not Found ------163.33 ------5.08 5.876E+OO ------Line Not Found ------185. 72 101 57.20 5.564E+OO 1. 546E-01 1.546E-01 67.36 205.31 ------5.01 5.260E+OO ------Line Not Found ------U-238 63.29 32 3.70* 1.836E+OO 2.324E+OO 2.324E+OO 113. 44 92.59 103 4.23 4.722E+OO 2.512E+OO 2.512E+OO 63.86 AM-243 43.53 ------5.90 1.216E-01 ------Line Not Found ------74.66 128 67.20* 3.152E+OO 2.950E-01 2.950E-01 50.94 ANH-511 511.00 67 100.00* 2.466E+OO 1.326E-01 1.326E-01 59.16 Flag: "*" Key line Page 3191 of5809 Summary of Nuclide Activity Sample ID : G405235014 Acquisition date Page : 3 3-0CT-2016 08:11:15 Total number of lines in spectrum 49 Number of unidentified lines 10 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 TE-125M CS-135 BA-137M CS-137 PR-144 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 57.40D 2.30E+06Y 30.08Y 30.08Y 284.91D 46.59D 1. 41E+10Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+l0Y 1600. OOY 1.41E+10Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 37.4 1. 00 1. 02 1. 02 2.07 86.7 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.481E+Ol 8.391E+OO l.078E-01 6.050E-01 6.391E-01 3.437E+OO 5.442E-02 2.958E-01 2.540E+Ol 2.593E+OO l.147E+OO 7.335E-01 9. 411E-01 7.335E-01 2. 591E+OO 7.335E-01 l.222E+OO l.222E+00 1.147E+OO 7.335E-01 9.549E-01 l.222E+00 2.324E+OO 7.335E-01 l.546E-01 2.324E+OO 2.950E-01 l.326E-01 7.567E+Ol 7.567E+Ol Decay Corr _ pCi/GRAM 1.481E+Ol 3 .138E+02 1. 078E-01 6.165E-01 6.513E-01 7 .130E+OO 4.716E+OO 2.958E-01 2.606E+Ol 2.593E+OO 1.147E+OO 7.337E-01 9.414E-01 7.337E-01 2. 591E+OO 7.337E-01 l.222E+00 1.222E+OO 1.147E+OO 7.335E-01 9.549E-01 1.222E+OO 2.324E+OO 7.335E-01 1.546E-01 2.324E+00 2.950E-01 l.326E-01 3. 901E+o2 3.901E+02 79.59% Decay Corr 2-Sigma Error 0.168E+Ol 6.341E+02 l.351E-01 1. llOE-01 1.173E-01 8.877E+OO 5.358E+OO 1.069E-01 2.621E+Ol 0.497E+00 0.131E+OO l.982E-01 1. 806E-01 l.982E-01 1.632E+OO l.982E-01 0.276E+OO 0.276E+00 0 .131E+OO 1. 981E-01 10.18E-01 0.276E+OO 2.636E+00 1.981E-01 1. 041E-01 2.636E+OO l.503E-01 0.785E-01 "M" Manually accepted 2-Sigma %Error 11. 33 202.05 125.35 18.01 18.01 124.51 113. 61 36.14 100.60 19.18 11. 44 27.01 19.18 27.01 62.99 27.01 22.57 22.57 -11. 44 27.01 106.58 22.57 113. 44 27.01 67.36 113. 44 50.94 59.16 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3192of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235014 Acquisition date : 3-0CT-2016 08:11:15 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 210.28 42 181 0.58 420.44 412 12 9.81E-03 **** 5.18E+OO T 6 270.06 31 78 1. 58 540.02 532 12 7.35E-03 **** 4.30E+OO T 0 434.31 22 64 4.44 868.61 861 16 5.63E-03 **** 2.84E+OO T 2 440.31 27 20 2.02 880.60 876 17 6. 72E.,-03 84.4 2.81E+OO T 2 444.15 32 24 2.03 888.30 876 17 8.07E-03 73.5 2.79E+OO 0 463.30 34 41 0.88 926.60 924 8 8.55E-03 79.1 2.69E+OO T 0 665.90 20 5 0.61 1331.88 1329 7 5.28E-03 63.4 1. 96E+OO T 0 704.04 22 28 0.89 1408.18 1397 18 5.95E-03 **** 1. 87E+OO T 0 727.74 20 28 1. 03 1455.59 1448 12 5.27E-03 **** 1. 82E+OO T 0 754.99 56 21 8.83 1510.09 1497 27 1.51E-02 53.5 1.77E+OO T 0 768.76 19 19 1. 41 1537.65 1532 11 4.98E-03 **** 1. 74E+OO 0 773.28 9 11 1. 41 1546.69 1543 8 2.35E-03 **** 1. 73E+OO T 0 799.01 10 5 0.56 1598.16 1595 8 2.62E-03 99.5 l.68E+OO 0 821.19 9 13 4.21 1642.52 1635 10 2.46E-03 **** 1. 65E+OO 0 935.10 12 21 0.80 1870.38 1859 14 3.33E-03 **** 1. 48E+OO 0 1031.64 13 11 0.88 2063.48 2052 15 3.52E-03 **** 1.36E+OO 0 1050.16 13 9 3.86 2100.52 2094 12 3.59E-03 **** 1.34E+OO T 0 1093.61 31 5 4.87 2187.43 2177 20 8.69E-03 49.9 1.29E+OO T 0 1155. 98 16 16 0.84 2312.18 2305 13 4.49E-03 **** 1.23E+OO 0 1197.74 8 13 o. 71 2395.70 2387 13 2.32E-03 **** l.20E+00 0 1376.00 19 0 3.21 2752.25 2744 16 5.56E-03 44.7 1.06E+OO 0 1847.78 8 0 1. 07 3695.78 3692 9 2.50E-03 66.7 7.98E-01 Flags: "T" == Tentatively associated Page 3193 of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:14:41.62 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l *
  • Acquisition date 3-0CT-2016 08:11:15 Sensitivity 3.000 *
  • Detector ID : GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real .time: 0 01:00:00.71 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:49:00 Nuclide Library : SOLID *
  • Sample ID G405235014 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.5373E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 TE-125M CS-135 BA-137M CS-137 PR-144 HG-203 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.808E-01 2.457E+02 1.258E-01 3.598E-02 3.800E-02 4.433E+OO 2.280E+00 3.278E-02 8.795E+OO 4.352E-02 6.289E-02 5. 911E-02 6.289E-02 4.667E-01 6.289E-02 l.156E-01 1.156E-01 4.352E-02 6.286E-02 3.832E-01 1.156E-01 1.630E+00 6.286E-02 l.651E-01 1.630E+OO 6.306E-02 2.418E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3194 of 5809 Le (pCi/GRAM 1.098E+01 3.732E-02 O.OOOE+OO 1.978E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3195of5809 2.880E-01 0.000E+OO O.OOOE+OO 5.393E-02 4.186E-01 O.OOOE+OO 4.475E-02 4.739E-01 7.273E+00 4.076E-02 l.427E-01 1. 866E+00 1.607E+Ol O.OOOE+OO 1.767E-01 O.OOOE+OO O.OOOE+OO 6.277E-01 6.384E+OO 6.747E-01 O.OOOE+OO 3.998E-02 5.540E+02 2. 968E-02 8. 962E-01 2.017E+OO 1.646E+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.121E-02 5.740E-02 5.046E+OO 4.554E-01 4.554E-01 2.779E-02 l.382E+00 6.827E-02 2.142E-01 O.OOOE+OO O.OOOE+OO l.335E-01 1. 580E+OO 9.758E-02 O.OOOE+OO O.OOOE+OO 9.368E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.554E-02 O.OOOE+OO 5. 611E-02 O.OOOE+OO O.OOOE+OO 9.455E-02 O.OOOE+OO O.OOOE+OO 2.218E+Ol O.OOOE+OO 3.573E-01 5.627E-02 4. 396E-02 O.OOOE+OO 8 .112E+02 O.OOOE+OO 2.397E-02 8.881E-02 l.825E-01 9.356E-02 1.009E-01 1.650E+OO 5.200E-02 3.695E+Ol 2.273E-01 8.890E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3196 of5809 2.019E-02 3.910E+OO 9.356E-01 5.161E+OO 2.816E+Ol 9.609E+Ol 3.939E-01 4.684E-02 3.976E-01 5.410E-01 5.979E-01 3.914E-01 5.141E-01 2. 091E-01 2.091E-01 4.187E-01 5.141E-01 5.550E-02 2.503E-01 4.606E+OO 5.550E-02 O.OOOE+OO 2.234E-01 3.122E+02 2.312E-01 1.014E-01 6.175E-02 3.406E-02 4.064E-02 1.058E-01 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. 'FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:14:46.75 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235014.CNF;l *
  • Acquisition date 3-0CT-2016 08:11:15 Sensitivity : 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.71 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:49:00 Nuclide Library : SOLID *
  • Sample ID G405235014 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.5373E+02 GRAM *
  • Quantity Err(%) : 1.3010E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 6-SEP-2016 07:25:20' Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error *Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.481E+Ol l.817E+OO TE-125M 3 .138E+02 6.217E+02 CS-135 1.078E-01 l.326E-01 BA-137M 6.165E-01 l.120E-01 CS-137 6.513E-01 l.183E-01 PR-144 7.130E+OO 8.705E+OO HG-203 2.642E+OO 5.308E+OO TL-208 2.958E-01 1.055E-01 PB-210 2.606E+Ol 2.580E+Ol PB-212 1.147E+OO 1.425E-01 BI-214 7.337E-01 1. 968E-01 PB-214 9.414E-01 l.814E-01 RN-222 7.337E-01 1. 968E-01 RA-224 4.607E-01 1.710E+OO RA-226 7.337E-01 1. 968E-01 AC-228 l.222E+OO 2.774E-01 RA-228 1.222E+OO 2.774E-01 TH-228 1.147E+OO 1.425E-01 TH-230 7.335E-01 1. 967E-01 PA-231 9.549E-01 1.018E+OO TH-232 l.222E+OO 2.774E-01 TH-234 2.324E+OO 2.635E+OO U-234 7.335E-01 1. 967E-01 U-235 -2.352E-02 1.788E-01 U-238 2.324E+OO 2.635E+OO AM-243 1.910E-01 1. 511E-01 ANH-511 1. 326E-01 7.708E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3197 of5809 Key-Line Activity (pCi/GRAM -1.12 9E+Ol -8.378E-03 1.000E+41 K.L Act error ( 1. 96-sigma) 1.463E+Ol 4.504E-02 7.300E+41 TPU (1.96-sigma) 1.817E+OO 6.217E+02 1.326E-01 1.120E-01 l.183E-01 8.705E+00 5.308E+OO 1.055E-01 2.580E+Ol 1.425E-01 1. 968E-01 l.814E-01 1. 968E-01 1. 710E+OO 1. 968E-01 2.774E-01 2.774E-01 l.425E-01 l.967E-01 1.018E+OO 2.774E-01 2.635E+OO 1. 967E-01 1. 788E-01 2.635E+OO 1. 511E-01 7.708E-02 TPU (1. 96-sigma) 1.549E+Ol 4.520E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -3.236E-02 3.689E-02 3.967E-02 NOT IDENT. SC-46 7.289E-02 3.221E-01 3.238E-01 FAIL ABUN V-48 -9.700E+02 l.413E+04 l.414E+04 SHORT HLIF CR-51 3.430E+02 4.009E+02 4.296E+02 SHORT HLIF MN-54 -1.942E-02 6.643E-02 6.701E-02 NOT IDENT. C0-56 -9.078E-02 5.059E-01 5.076E-01 NOT IDENT. MN-56 -1.000E+41 5.573E+41 O.OOOE+OO SHORT HLIF C0-57 3.139E-03 5.206E-02 5.208E-02 NOT IDENT. C0-58 -1.237E-01 5.755E-01 5.782E-01 NOT IDENT. FE-59 4.269E+OO 8.955E+OO 9.159E+OO NOT I DENT .. C0-60 2.219E-02 4.296E-02 4. 411E-02 NOT IDENT. ZN-65 -1.444E-01 2.381E-01 2.468E-01 NOT IDENT. GE-68 5.698E-01 2.104E+OO 2.120E+OO NOT IDENT. AS-73 1. 07 8E+OO l.786E+Ol l.786E+Ol NOT IDENT. AS-74 4.392E+03 6. 611E+03 6.902E+03 SHORT HLIF SE-75 -1.310E-01 2.389E-01 2.460E-01 NOT IDENT. BR-77 2 .101E+38 1.819E+39 O.OOOE+OO SHORT HLIF SR-82 4.516E+02 7.822E+02 8.082E+02 SHORT HLIF RB-83 -1.294E-01 7.149E-01 7.173E-01 NOT IDENT. KR-85 -3.310E+OO 9.209E+OO 9.329E+OO NOT IDENT. SR-85 -3.512E-01 9.736E-01 9.864E-01 NOT IDENT. RB-86 6.876E+03 2.538E+04 2.557E+04 SHORT HLIF Y-88 -1.760E-01 1.827E-01 1.992E-01 NOT IDENT. Y-91 -2.612E+02 6.762E+02 6.864E+02 NOT IDENT. NB-94 5.865E-02 6.993E-02 7.476E-02 FAIL ABUN NB-95 7.046E-01 1.044E+OO 1. 091E+OO NOT IDENT. NB-95M -1.012E+OO 2.616E+OO 2.656E+00 NOT IDENT. *zR-95 l.957E+00 l.632E+OO 1.855E+OO NOT IDENT. NB-97 1.000E+41 5.763E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 3.376E+41 O.OOOE+OO SHORT HLIF M0-99 -4.810E+30 1.583E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.485E+41 O.OOOE+OO SHORT HLIF RH-101 -3.795E-02 4.059E-02 4.405E-02 NOT IDENT. RH-102 5.154E-02 5.791E-02 6.240E-02 NOT IDENT. RU-103 1.514E+00 5.775E+OO 5.815E+00 FAIL ABUN RH-106 2. 972E-01 4.723E-01 4.909E-01 FAIL ABUN RU-106 2. 972E-01 4.723E-01 4.909E-01 FAIL ABUN AG-108M 4.241E-02 7.321E-02 7.567E-02 FAIL ABUN CD-109 1.734E+OO 1. 570E+OO 1. 754E+OO NOT IDENT. AG-llOM -l.342E-01 l.087E-01 1.244E-01 NOT IDENT. SN-113 -2.478E-01 2.782E-01 2.997E-01 NOT IDENT. CD-115 3.730E+38 3.293E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 9.717E+04 9.943E+04 1.087E+05 SHORT HLIF TE-123M l.303E-01 1.352E-01 1.474E-01 NOT IDENT. SB-124 -3. 031E-01 2.005E+00 2.009E+OO NOT IDENT. SB-125 2.322E-02 l.247E-01 1.251E-01 FAIL ABUN I-126 l.455E+06 9.248E+05 1.134E+06 SHORT HLIF SB-126 -7.524E+05 1.431E+06 l.470E+06 SHORT HLIF SN-126 1.998E-01 1.00lE-01 1.347E-01 FAIL ABUN SB-127 6.591E+21 2.326E+22 O.OOOE+OO SHORT HLIF I-131 -3.823E+08 4.700E+09 4.703E+09 SHORT HLIF I-132 1.000E+41 l.852E+42 O.OOOE+OO SHORT HLIF TE-132 -1.155E+26 3.904E+26 O.OOOE+OO SHORT HLIF BA-133 1.923E-03 4.564E-02 4.565E-02 FAIL ABUN I-133 -1.000E+41 7.635E+41 O.OOOE+OO SHORT HLIF CS-134 1.267E-01 6.575E-02 8.708E-02 FAIL ABUN I-135 -l.OOOE+41 7.020E+41 O.OOOE+OO SHORT HLIF CS-136 -l.299E+04 4.236E+05 4.236E+05 SHORT HLIF CE-139 -1.909E-02 1.037E-01 1.041E-01 NOT IDENT. BA-140 3.127E+05 1.438E+06 l.445E+06 SHORT HLIF LA-140 -6.102E+05 5.128E+05 5.819E+05 SHORT HLIF CE-141 -2.980E+OO 2.395E+Ol 2.399E+Ol NOT IDENT. CE-143 l.OOOE+41 8.180E+40 O.OOOE+OO SHORT HLIF CE-144 -8.042E-02 3.852E-01 3.870E-01 NOT IDENT. PM-144 8.208E-02 l.003E-01 l.069E-01 FAIL ABUN PM-146 1.728E-02 4. 909E-02. 4.970E-02 NOT IDENT. ND-147 -4.681E+06 3.358E+07 3.364E+07 SHORT HLIF PM-147 1.955E+02 9.309E+02 9.351E+02 NOT IDENT. PM-149 -l.248E+40 5.284E+40 O.OOOE+OO SHORT HLIF EU-150 2.285E-03 3.046E-02 3.048E-02 FAIL ABUN EU-152 -6.069E-02 1.085E-01 l .119E-01 NOT IDENT. GD-153 -8.930E-02 2.365E-01 2.399E-01 NOT IDENT. EU-154 -2.756E-02 l.142E-01 l.149E-01 NOT IDENT. EU-155 2.749E-02 l.236E-01 l.242E-01 NOT IDENT. TB-160 1.17 5E-01 1. 916E+00 1.916E+OO NOT IDENT. H0-166M -l.547E-02 6.204E-02 6.243E-02 NOT IDENT. TM-171 -1. 98 6E+Ol 4.682E+Ol 4.767E+Ol NOT IDENT. HF-172 2.189E-01 2.492E-01 2.680E-01 FAIL ABUN Page 3198of5809 LU-172 2.541E-01 1.270E-01 1.710E-01 FAIL ABUN LU-176 -4.830E-03 2.643E-02 2.652E-02 NOT IDENT. HF-181 -1.802E+OO 4.908E+OO 4.975E+OO NOT IDENT. TA-182 9.192E-03 1.077E+OO l.077E+00 FAIL ABUN RE-183 3.007E-01 5.700E+00 5.702E+OO NOT IDENT. RE-184 -6 .113E+00 3.429E+Ol 3.440E+Ol NOT IDENT. W-188 -3.102E+01 1.259E+02 1.267E+02 FAIL ABUN IR-192 -2.127E-01 4.732E-01 4.828E-01 FAIL ABUN BI-207 1. 715E-02 5.288E-02 5.344E-02 FAIL ABUN BI-211. 2.593E+00 5.013E-01 1. 272E+OO FAIL ABUN PB-211 -4.174E-01 6.886E-01 7.138E-01 NOT IDENT. BI-212 7. 965E-01 9.284E-01 9.955E-01 FAIL ABUN RN-219 1.993E-01 4.347E-01 4.439E-01 FAIL ABUN RA-223 -2.664E-01 6.169E-01 6.285E-01 FAIL ABUN AC-227 4.542E-02 2.300E-01 2.309E-01 NOT IDENT. TH-227 4.542E-02 2.300E-01 2.309E-01 NOT IDENT. TH-229 6.960E-02 4.527E-01 4.537E-01 FAIL ABUN TH-231 -2.664E-01 6.169E-01 6.285E-01 FAIL ABUN PA-233 2.563E-03 6.297E-02 6.298E-02 FAIL ABUN PA-234 1.054E-01 3.009E-01 3.046E-01 NOT IDENT. PA-234M 1.875E+OO 5.188E+OO 5.256E+OO NOT IDENT. NP-237 2.563E-03 6.297E-02 6.298E-02 FAIL ABUN NP-238 -l.OOOE+41 2.329E+41 0.000E+OO SHORT HLIF NP-239 -1.186E-01 2.717E-01 2.770E-01 FAIL ABUN PU-239 1.003E+02 '3.585E+02 3.613E+02 NOT IDENT. AM-241 8.840E-02 2.501E-01 2.533E-01 NOT IDENT. CM-243 3.917E-02 1.137E-01 l.151E-01 FAIL ABUN BK-247 -4.830E-02 8.428E-02 8.704E-02 NOT IDENT. CM-247 l.053E-03 3. 963E-02 3. 963E-02 FAIL ABUN CF-249 4.493E-02 4.253E-02 4.710E-02 NOT IDENT. CF-251 5.042E-02 1.113E-01 1.136E-01 NOT IDENT. Page 3199 of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 64.4058 87.09 95.1059 136.47 89.5901 45.60 81.3972 87.57 82.9171 140.51 0.0000 46.54 60.1935 88.03 96.8296 143.76 79.5716 49.72 0.0000 88.34 96.8917 144.24 76.2396 51. 35 58.9820 88.47 96.9174 145.44 81.4648 51. 87 66.1055 89. 96 106.4733 152.43 81. 4309 52.39 61. 98 09 1093.63 82.2839 153.25 0.0000 52.97 64.9081 91.11 0.0000 323.87 77.3383 53.44 61. 4644 92.59 82.6084 156.02 0.0000 54.07 64.7612 93.35 82.7340 158.56 0.0000 57.36 0.0000 94.56 82.9328 159.00 68.3382 57.53 80.4045 94.65 82.9474 162.33 67.7803 57.98 85.8707 94.67 82.9507 162.66 0.0000 59.27 90.4818 94.87 82.9837 163.33 65.2611 59.32 82.9528 97.43 90.8392 165.86 68.9747 59.54 84.0801 98.43 73.7531 176.31 58.4133 60. 96 83.6789 98.44 73.7545 176.60 *o. 0000 61.17 83.7255 99.53 90.8130 177.52 63.8218 62. 93 90.2769 100 .11 81.4679 181.07 0.0000 63.29 82.7403 102.03 91. 2436 181.52 74.8339 63.58 81.3498 103.18 72.4389 184.41 79.5725 64.28 94.5941 103.37 72.4650 143.76 79.7011 66.73 91.1561 105.21 63.5730 193.51 65.9907 67.24 86.8734 105.31 63.5844 197.03 70.8041 125.81 92.4729 106.12 90.7423 198.01 78.1562 67.75 92.4883 106.47 90.8003 201.83 73.0265 69.67 113. 9450 109.28 64.8439 203.43 92.1826 70.83 90.2279 111. 00 77.0874 205.31 83.8582 72. 81 98.0849 111.76 0.0000 210.85 58.0999 72. 87 98.0990 114.06 79.9234 215.65 64.9001 74.66 115.3021 116. 30 0.0000 222 .11 72.8267 74.82 115.3446 116.74 81.5095 227.09 70.3987 74.97 115.3846 119. 76 61.1397 227.38 69.4811 77 .11 115.9520 121.12 74.7598 228.16 0.0000 78.74 100.9369 121. 22 74.7724 228.18 62.0220 79.69 87.5635 121. 78 72.3879 116.74 62.0220 80.12 84.6249 122.06 72.4217 235.69 69.6121 80.19 0.0000 122.92 83.5878 235. 96 73.8947 80.57 114. 9618 123.07 71.3128 238.63 56.0477 81. 00 122.6412 265.00 78.7690 238.98 0.0000 81. 07 122.6602 125.81 62.9874 240.99 56.1822 81. 75 108.0564 127.23 102.7431 242.00 56.2398 83.79 93.6820 127.91 86.7462 244.70 40.1436 84.00 99.4395 129.30 85. 6962 252.40 0.0000 85.43 173.1168 131.20 108.3770 252.80 52.0285 86.55 90.7850 133. 02 93.6951 254.15 0.0000 86.79 98 .1120 133.52 94.1851 256.23 51.2351 86.94 98.1432 136.00 92.0359 260.90 0.0000 Page 3200 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 57.0087 355.39 0.0000 584.27 26.1571 264.80 58.4790 356.01 34.7261 595.83 0.0000 265.00 58.4900 364.49 0.0000 427.87 30.2205 2 68. 22 52.8003 366.42 0.0000 602.52 0.0000 269.46 52.8607 372.51 38.3489 604.72 33.7700 270.03 52.8893 375 .. 05 42.6880 607.14 32.3404 271.23 61. 7734 377.52 37.4189 609.32 26.6724 273.65 0.0000 356.01 35.4405 610.33 26.6857 276.40 60. 0965 388.16 31.2403 614.28 29.5039 277.37 60.1499 388.63 0.0000 618.01 25.8629 277.60 60.1623 391.69 52.9159 620.36 24. 9681 278.00 62.1579 264.66 40.2068 621. 93 13.8817 279.20 56.2996 401. 81 35.8883 630.19 0.0000 279.54 54.8349 402.40 39.1663 631. 29 13.0152 279.70 54.8428 404.85 37.0526 633.25 26.9848 280.46 68.2293 410.95 32.8290 634.78 0.0000 283.69 56.5280 413.71 51.5277 635.95 13.0443 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 59.5947 423. 72 0.0000 645.85 18.7219 285.90 0.0000 427.09 24.3342 657.76 18.0738 287.50 52.7391 427.87 29.8801 657.90 0.0000 290.67 49.3953 433.94 28.3316 661. 66 28.6688 293.27 0.0000 439.40 6.6897 664.57 0.0000 351. 93 36.0667 453.88 27.0049 666.33 0.0000 295. 96 36.0901 463.37 28.8618 666.50 0.0000 879.38 24 .1143 468.07 25. 5396 667.71 0.0000 299.98 45.2692 473.00 0.0000 677.62 14.2497 300.09 45.2737 475.06 28.4973 685.70 0.0000 300 .13 45.2747 476.78 29.6679 695.00 0.0000 301.36 45.3223 477.60 38.8158 696.49 21. 4601 302.85 34.7913 482.18 32.0537 696. 51 21. 4601 256.23 36.3552 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 15.3340 306.78 40.9787 497.08 20.7872 697.49 15.3354 308.46 45.5960 505.52 26.1108 702.65 16.9077 311. 90 45.7278 507.63 0.0000 706.68 13.8582 316.51 45.9027 511. 00 25.6105 711. 68 23.1475 319.41 0.0000 514.00 36.7321 720.70 0.0000 320.08 0.0000 514.00 36.7321 721. 93 0.0000 321. 04 34.8114 520.40 29.8434 722. 78 12.4047 323.87 48.2326 520.69 0.0000 722.91 12.4055 325.23 48.2852 522.65 0.0000 723.31 13.9583 328.76 0.0000 527.90 0.0000 724 .19 15.5151 333.37 40.3282 528.26 24.6846 727.33 24.2752 333.97 45.0027 529.59 23.8203 733.00 18.1694 334.37 40.3600 529.87 0.0000 735.93 17.5424 338.28 52.9413 531. 02 0.0000 333.97 17.5540 338.32 52.9434 537.26 0.0000 739.50 0.0000 311. 90 43.6740 546.56 0.0000 747.24 15.6680 340.48 43.6740 552.55 23.2261 748.06 25.0773 340.55 0.0000 563.25 26.9522 752.31 12.7572 344.28 55.2752 569.33 28.8403 753.82 0.0000 345.93 45.9470 946.00 28.8428 756.73 12.7806 351.06 44. 0311 569.70 27.0428 756.80 12.7810 351.93 36.7168 583.19 27.2324 884.68 15.7769 Page 3201of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.3680 1274.44 17.1860 1620.50 5.0767 766.42 22 .1102 1001.03 17.2129 1621.92 4.0625 766.84 20.5347 1002.74 17.2227 1678.03 0.0000 772. 60 0.0000 1004.73 20.4652 1690.97 4.1234 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.1403 778.90 14.7397 1028.54 0.0000 1063.66 3.4933 783.70 0.0000 1037.84 11. 9762 1771. 35 1.4975 785.37 14.9203 1038.76 0.0000 1791.20 0.0000 792.07 15.9580 631.29 17.4688 1808.65 7.3931 794.95 11.1836 1048.07 0.0000 1810.72 0.0000 795.86 0.0000 1049.04 17.4824 1836.06 4.2477 810.06 18.0813 1050.41 17.4902 810.29 18.0829 1063.66 12.0742 344.28 18.0840 1077.00 0.0000 810.76 15.0719 1077.34 7.7165 815.77 0.0000 1085.87 21.2215 1048.07 0.0000 1093.63 15.5107 832.01 13.1702 1099.45 12.4312 834.85 18.2554 1112. 07 13. 3696 835.71 18.2615 1112. 84 11. 1444 836.80 0.0000 1115. 54 19.6292 846.75 0.0000 1120.29 14.5203 846.77 17.3201 1120.55 14. 5211 856.80 0.0000 1221.41 14.5242 860.56 19.4581 1129. 67 16.8008 871.09 18.5065 1131. 51 0.0000 873.19 15.4340 1147.95 0.0000 875.33 0.0000 1173.23 9.9833 879.38 13.4066 1177.95 19.0846* 880.51 13.4122 1189.05 12.5361 883.24 14.4584 1204.77 22.8943 884.68 21. 6985 1221. 41 17.4813 889.28 8.2800 1231.02 17.5277 894.76 13.4820 1235.36 0.0000 898.04 16.6128 1238.28 11. 0924 900. 72 18.7075 1260.41 0.0000 903.28 17.6843 1271.87 6.5304 911. 20 15.0223 1274.44 11.2025 912.08 16. 6963 1274.54 10.2690 923.98 0.0000 1291.59 11. 2541 926.50 10.0690 1298.22 0.0000 929 .11 10.0784 1312 .11 0.0000 937.49 18.5313 1332.49 7.5836 944.13 0.0000 1362.66 0.0000 946.00 10.5603 1365.19 8.6036 949.00 19.0278 1368.63 0.0000 667. 71 0.0000 1384.29 5.3366 962. 31 24.2732 1408.01 9.6631 964. 08 20.4018 1457.56 0.0000 966 .17 11. 9092 1460.82 6.8517 911.20 22.3516 1489.16 4.9272 968. 97 22.3516 1505.03 10.8802 983.53 0.0000 1584.12 4.0287 984.45 0.0000 1596.21 0.0000 Page 3202 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:15:15.21 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date : Z-OCT-2016 11:02:28. Sample date 8-DEC-2015 10:56:00. Acquisition date : 3-0CT-2016 08:11:39. Sample ID G405235015 Sample quantity : l.45075E+02 GRAM Detector name : GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.75 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 0 0 0 0 0 4 4 0 0 2 2 0 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 Page 3203 of 5809 Energy 62.79* 74.99 77.15* 87.17 93.06* 99.51* 185.90* 209.20 238.73* 241.60 271.00 284.47 295.41 299.91 321. 84 338.37 351.83* 414.86 482.23 511.09* 516.88 525.75 583.28* 609.36* 661.95 669.81 727. 83 738.40 768.61 772.60 794.46 861.16 871. 28 911.36* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 60 79 140 38 58 31 102 26 365 113 23 43 91 21 37 70 241 15 12 64 21 19 120 155 78 10 17 5 27 8 35 37 26 73 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 131 138 118 144 181 187 114 70 63 88 74 79 56 56 40 82 48 37 21 23 4 7 33 35 40 26 25 10 23 13 7 15 13 24 1. 00 1. 07 1. 07 1. 06 1. 03 3.33 0. 96 0.93 1.15 1. 78 1. 46 3.86 1. 42 1. 56 0.98 1. 05 1.19 2.38 1. 49 2.12 1. 80 1. 81 1. 30 1. 35 1.17 4.82 1. 36 0.89 1. 71 1. 38 1. 26 0.64 6.59 1. 06 126.04 150.43 154.76 174.81 186.60 199.50 372.34 418. 96 478.06 483.80 542.61 569.57 591.47 600.46 644.35 677.42 704.35 830.48 965.28 1023.03 1034.63 1052.37 1167. 51 1219.70 1324.93 1340.67 1456.78 1477.92 1538.38 1546.37 1590.12 1723.62 1743.86 1824.08 122 147 147 172 183 193 366 416 472 472 536 562 587 587 640 673 698 823 959 1015 1031 1031 1162 1213 1319 1330 1451 1474 1529 1543 1584 1714 1734 1819 9 1. 68E-02 37. 0 13 2.18E-02 25.3 1.29E+OO 13 3.89E-02 15.4 7 l.06E-02 54.1 10 1. 60E-02 46. 7 12 8.49E-03 92.2 12 2.83E-02 23.7 7 7.09E-03 57.9 19 1.0lE-01 6.5 1.12E+OO 19 3.14E-02 24.2 9 6.29E-03 71.7 15 1.20E-02 47.4 18 2.53E-02 17.9 1.56E+OO 18 5.84E-03 69.0 10 1.03E-02 36.0 11 l.95E-02 27.4 11 6.71E-02 8.6 10 4.05E-03 82.7 10 3.27E-03 80.2 16 l.76E-02 25.5 25 5.80E-03 29.6 l.60E+OO 25 5.21E-03 30.7 10 3.33E-02 13.0 15 4.31E-02 11.6 12 2.18E-02 19.2 12 2.80E-03107.3 10 4.66E-03 60.9 6 1. 25E-03116. 5 13 7.49E-03 41.3 7 2.35E-03 76.9 13 9.79E-03 22.5 20 1.03E-02 30.5 18 7.15E-03 38.8 11 2.02E-02 18.0 Peak Search Report (continued) Page : 2 Sample ID : G405235015 Acquisition date 3-0CT-2016 08:11:39 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 923.46 11 5 0.59 1848.31 1845 7 3.07E-03 45.4 36 5 964. 70 22 5 2.91 1930.84 1926 18 6.07E-03 27.5 1.67E+OO 37 5 968. 96* 44 5 1. 74 1939.36 1926 18 1. 23E-:-02 20.0 38 0 1005.15 8 12 0.92 2011. 81 2008 8 2.22E-03 82.9 39 0 1039.30 7 14 0.97 2080.16 2071 11 2.02E-03105.3 40 0 1041. 21 13 j_ 1. 51 2083.97 2081 6 3.50E-03 32.0 41 0 1084.19 13 14 0.73 2170.00 2162 14 3.61E-03 67 .1 42 0 1095.28 7 7 0.98 2192.21 2188 6 l.84E-03 76.1 43 0 1098.49 16 4 3.22 2198.64 2194 10 4.44E-03 35.6 44 0 1120.70 34 30 1. 56 2243.09 2237 15 9.44E-03 39.1 45 0 1154. 44 16 8 2.34 2310.63 2305 11 4.45E-03 42.6 46 0 1223.88 9 11 0.65 2449.62 2444 9 2.51E-03 74.6 47 0 1333.06 9 6 2.33 2668.18 2661 11 2.36E-03 63.5 48 0 1460.73* 384 4 2.05 2923.76 2915 16 1.07E-01 5.3 49 0 1764.90 24 2 2.03 3532.71 3528 11 6.61E-03 24.4 Flag: "*" = Peak area was modified by background subtraction Page 3204 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:15:17 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 10:56:00 G405235015 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:11:39 145.07 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA44 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3205 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.75 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235015 Acquisition date 3-0CT-2016 08:11:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.030E+OO 1. 738E+0.1 1.738E+Ol 10.57 OK CD-109 88.03 3.70* 4.453E+OO 8.036E-01 1.261E+OO 202.07 OK SN-126 64.28 9.60 1.986E+OO 2.070E+OO 2.070E+OO 73. 96 OK 86.94 8.90 4.453E+OO 3.341E-01 3. 341E-01 202.07 OK 87.57 37.00* 4.453E+OO 8.036E-02 8.036E-02 202.07 OK BA-137M 661.66 89.90* 1. 965E+OO 2.384E-01 2.430E-01 38.33 OK CS-137 661. 66 85.10* 1. 965E+OO 2.519E-01 2.567E-01 38.33 OK TL-208 277.37 6.60 4.074E+OO Line Not Found Absent 583.19 85.00* 2.178E+OO 3.520E-01 3.520E-01 26.04 OK 860.56 12.50 1. 591E+OO 9.740E-01 9.740E-01 60.95 OK BI-211 72. 87 1. 23 3.135E+OO Line Not Found Absent 351.06 12.92* 3.337E+OO 1.150E+OO 1.150E+OO 79.27 OK PB-212 74.82 10.28 3.357E+OO 1'.054E+OO 1.054E+OO 71. 86 OK 77 .11 17.10 3.576E+OO 1. 473E+OO 1.473E+OO 30.75 OK 238.63 43.60* 4.584E+OO 1.073E+OO 1. 073E+OO 12.92 OK 300.09 3.30 3.820E+OO 9.620E-01 9.620E-01 137. 97 OK BI-214 609.32 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 OK 1120.29 14.92 1.287E+OO 9.041E-01 9.044E-01 78.15 OK 1764.49 15:30 8.672E-01 8.753E-01 8.756E-01 48. 71 OK PB-214 74.82 5.80 3.340E+OO Line Not Found <<INT Reject 77 .11 9.70 3.576E+OO 2.597E+OO 2.598E+OO 30.75 OK 87.09 3.41 4.447E+OO Line Not Found <<INT Reject 242.00 7.25 4.538E+OO Line Not Found <<INT Reject 295.22 18.42 3.868E+OO 7.375E-01 7.378E-01 35.88 OK 351. 93 35.60* 3.336E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 OK 1120.29 14.92 1.287E+OO 9.041E-01 9.044E-01 78.15 OK 1764.49 15.30 8.672E-01 8.753E-01 8.756E-01 48.71 OK RA-224 240.99 4.10* 4.543E+OO 2.256E+OO 2.256E+OO 79.02 OK RA-226 609.32 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 OK 1120.29 14.92 1.287E+OO 9.041E-01 9.044E-01 78.15 OK 1764.49 15.30 8.672E-01 8.753E-01 8.756E-01 48. 71 OK AC-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.450E+OO 1. 031E+OO 1.031E+00 54.85 OK 794.95 4.25 1.697E+OO 2.579E+OO 2.579E+OO 45.09 OK 835.71 1. 61 1.630E+00 Line Not Found Absent 911.20 25.80* l.521E+OO 9.637E-01 9.637E-01 35.95 OK 968. 97 15.80 l.448E+OO 9.995E-01 9.995E-01 39.93 OK RA-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.450E+OO 1.031E+OO 1. 031E+OO 54.85 OK 794.95 4.25 l.697E+OO 2.579E+OO 2.579E+OO 45.09 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* 1. 521E+OO 9.637E-01 9.637E-01 35.95 OK 968. 97 15.80 1.448E+OO 9.995E-01 9.995E-01 39.93 OK TH-228 74.82 10.28 3.357E+OO l.054E+OO 1.054E+00 71. 86 OK 77 .11 17.10 3.576E+00 1.473E+OO l.473E+OO 30.75 OK 238.63 43.60* 4.584E+OO 1.073E+OO l.073E+OO 12. 92 OK 300.09 3.30 3.820E+OO 9.620E-01 9.620E-01 137.97 OK TH-230 609.32 45.49* 2.102E+OO 8.785E-01 8.785E-01 23.19 OK Page 3206 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235015 Acquisition date 3-0CT-2016 08:11:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 1.287E+OO 9. 041E-01 9.041E-01 78.15 .OK 1764.49 15.30 8.672E-01 8.753E-01 8.753E-01 48.71 OK PA-231 283.69 1. 70 3.991E+OO 3.676E+OO 3.676E+OO 94.84 OK 301.36 5.35* 3.820E+OO 5.934E-01 5.934E-01 137.97 OK TH-232 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.450E+OO 1. 031E+OO 1. 031E+OO 54.85 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* 1.521E+OO 9.637E-01 9.637E-01 35.95 OK 968.97 15.80 1.448E+OO 9.995E-01 9.995E-01 39.93 OK TH-234 63.29 3.70* 1.986E+OO 5.371E+OO 5. 371E+OO 73. 96 OK 92. 59 4.23 4.860E+OO 1. 783E+OO 1. 783E+OO 93.49 OK U-234 609.32 45.49* 2.102E+OO 8.785E-01 8.785E-01 23.19 OK 1120.29 14.92 1.287E+OO 9.041E-01 9.041E-01 78.15 OK 1764.49 15.30 8.672E-01 8.753E-01 8.753E-01 48.71 OK U-238 63.29 3.70* 1.986E+OO 5.371E+OO 5. 371E+OO 73. 96 OK 92. 59 4.23 4.860E+OO 1. 783E+OO 1.783E+OO 93.49 OK AM-243 43.53 5.90 1.573E-01 Line Not Found Absent 74.66 67.20* 3.357E+OO l.612E-01 l.612E-01 71. 86 OK ANH-511 511. 00 100.00* 2.430E+OO 1.437E-01 1.437E-01 51. 05 OK Flag: "*" = Keyline Page 3207 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:15:18.10 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l *
  • Acquisition date 3-0CT-2016 08:11:39 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:56:00 Analyst initials: MXRl *
  • Sample ID G405235015 Sample Quantity l.4507E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF' GAM44 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.738E+Ol 1.800E+OO CD-109 1.261E+OO 2.497E+OO SN-126 8.036E-02 1.591E-01 BA-137M -2. 430E-01 9.127E-02 CS-137 2.567E-01 9.642E-02 TL-208 3.520E-01 8.982E-02 BI-211 1.150E+OO 8.936E-01 PB-212 1.073E+OO 1.359E-01 BI-214 8.789E-01 l.997E-01 PB-214 l.155E+00 1. 947E-01 RN-222 8.789E-01 1.997E-01 RA-224 2.256E+OO 1.747E+OO RA-226 8.789E-01 l.997E-01 AC-228 9.637E-01 3.395E-01 RA-228 9.637E-01 3.395E-01 TH-228 1.073E+OO 1.359E-01 TH-230 8.785E-01 l.997E-01 PA-231 5.934E-01 8.023E-01 TH-232 9.637E-01 3.395E-01 TH-234 5.371E+OO 3.893E+OO U-234 8.785E-01 1. 996E-01 U-238 5.371E+OO 3.893E+OO AM-243 l.612E-01 l .135E-01 ANH-511 l.437E-01 7.188E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3208 of 5809 Key-Line Activity (pCi/GRAM -1.215E+OO -2.426E-02 O.OOOE+OO 1.487E-02 -2.499E-01 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1. 313E+Ol 5.689E-02 1. 960E+41 3.214E-02 3.789E-01 l.677E+04 MDA (pCi/GRAM 6.783E-01 2.713E+OO l.577E-01 7.562E-02 7.989E-02 6.522E-02 3.333E-01 9 .191E-02 1.300E-01 3.487E-01 l.300E-01 9.855E-01 l.300E-01 2.921E-01 2.921E-01 9.191E-02 l.300E-01 8 .. 249E-01 2. 921E-01 2.910E+OO l.300E-01 2.910E+OO l.148E-01 4.525E-02 MDA (pCi/GRAM 2.278E+Ol l.037E-01 O.OOOE+OO 7.812E-02 6.934E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 4.430E+02 O.OOOE+OO SHORT HLIF MN-54 -1.210E-02 8.120E-02 l.475E-01 NOT IDENT. C0-56 -1.lOlE-01 4.646E-01 8.533E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 5.235E-02 4.850E-02 9.989E-02 NOT IDENT. C0-58 1.616E-01 5.703E-01 1.163E+OO NOT IDENT. FE-59 l.183E+Ol 8.264E+OO 1. 373E+Ol FAIL ABUN C0-60 4.267E-02 5.311E-02 9.449E-02 FAIL ABUN ZN-65 1.012E-01 2.061E-01 4.006E-01 NOT IDENT. GE-68 2.101E+OO 2.449E+OO 5. 311E+O.O NOT IDENT. AS-73 2.130E+OO 1.516E+Ol 3.040E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.059E+03 O.OOOE+OO SHORT HLIF SE-75 -3.892E-03 2.215E-01 3.990E-01 NOT IDENT. BR-77 O.OOOE+OO 2.486E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 9.496E+02 O.OOOE+OO SHORT HLIF RB-83 3.473E-01 6.642E-01 l.294E+OO NOT IDENT. KR-85 6.488E+OO 5.028E+OO 1.124E+Ol NOT IDENT. SR-85 6.846E-01 5.313E-01 1.188E+OO NOT IDENT. RB-86 0.000E+OO 3.075E+04 O.OOOE+OO SHORT HLIF Y-88 -2.598E-02 2.676E-01 5.665E-01 NOT IDENT. Y-91 2 .110E+02 6.393E+02 l.306E+03 NOT IDENT. NB-94 2.033E-02 3.945E-02 7.873E-02 FAIL ABUN NB-95 1.164E-01 1. 067E+OO l.829E+OO NOT IDENT. NB-95M -1.639E+OO 2.828E+OO 4.342E+OO NOT IDENT. ZR-95 -9.700E-01 1.819E+OO 3 .138E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 810E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 1.974E-02 3.565E-02 6.993E-02 NOT IDENT. RH-102 7.340E-03 5.816E-02 1.156E-01 NOT IDENT. RU-103 -2.265E+OO 6.652E+OO 1.230E+Ol FAIL ABUN RH-106 2.279E-02 5.336E-01 1.037E+OO NOT IDENT. RU-106 2.279E-02 5.336E-01 l.037E+00 NOT IDENT. AG-108M l.552E-02 3.093E-02 6.332E-02 NOT IDENT. AG-llOM -1.230E-01 l.150E-01 1.947E-01 NOT IDENT. SN-113 -1.381E-01 2.528E-01 4.650E-01 NOT IDENT. CD-115 O.OOOE+OO 2.914E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.547E+04 O.OOOE+OO SHORT HLIF TE-123M 2.414E-02 1. 2 61E-01 2.394E-01 NOT IDENT. SB-124 -9.028E-01 1.943E+OO 3.543E+OO NOT IDENT. SB-125 2.405E-02 l.017E-01 2.058E-01 FAIL ABUN TE-125M -4.543E+Ol 2.972E+02 5.574E+02 NOT IDENT. I-126 O.OOOE+OO l.066E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.128E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.299E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.605E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 4.228E+26 O.OOOE+OO SHORT HLIF BA-133 5.431E-02 3.986E-02 8.526E-02 NOT IDENT. I-133 O.OOOE+OO l.388E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 7.462E-02 1.326E-01 FAIL ABUN CS-135 -2.155E-02 1.460E-01 2.585E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.293E+05 O.OOOE+OO SHORT HLIF CE-139 7.823E-02 l.206E-01 2.342E-01 NOT IDENT. BA-140 O.OOOE+OO l.205E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.009E+05 O.OOOE+OO SHORT HLIF CE-141 1.041E+OO 2. 691E+Ol 5.004E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.331E-01 3. 726E-01 6.609E-01 NOT IDENT. PM-144 -7.840E-03 6.171E-02 1.150E-01 NOT IDENT. PR-144 -6.812E-01 5.361E+OO 9.992E+OO NOT IDENT. PM-14.6 2.362E-02 4.484E-02 9.309E-02 NOT IDENT. ND-147 O.OOOE+OO 3.052E+07 O.OOOE+OO SHORT HLIF PM-147 -5.403E+Ol 8.382E+02 1. 57 9E+03 NOT IDENT. PM-149 O.OOOE+OO 9.295E+40 O.OOOE+OO SHORT HLIF EU-150 5.076E-06 2. 641E-02 4. 717E-02 FAIL ABUN EU-152 2.974E-02 8. 964E-02 l.835E-01 FAIL ABUN GD-153 1. 756E-01 1. 968E-01 3.800E-01 NOT IDENT. EU-154 -6.221E-02 1. 38 9E-01 2.524E-01 FAIL ABUN EU-155 -1.454E-02 1.127E-01 2.128E-01 FAIL ABUN TB-160 7.227E-01 l.782E+OO 3.904E+OO FAIL ABUN H0-166M -4.340E-03 5.857E-02 l. lllE-01 FAIL ABUN TM-171 1.593E+OO 3.750E+Ol 7.477E+Ol NOT IDENT. HF-172 -6.872E-02 2.293E-01 4.218E-01 FAIL ABUN LU-172 2.874E-02 1.066E-01 1. 947E-01 FAIL ABUN LU-176 7.255E-03 2.377E-02 4.854E-02 FAIL ABUN Page 3209 of 5809 HF-181 4.271E+OO 6.717E+OO 8.497E+OO FAIL ABUN TA-182 -1.841E-01 1.190E+OO 1.980E+OO FAIL ABUN RE-183 -2.181E-01 4.547E+OO 8.974E+OO NOT IDENT. RE-184 -8.667E+OO 2.909E+Ol 5.692E+Ol NOT IDENT. W-188 9.675E+OO 1.339E+02 2.221E+02 FAIL ABUN IR-192 1.295E-01 4.625E-01 9.399E-01 FAIL ABUN HG-203 -l.257E+OO 2.412E+OO 4.061E+OO NOT IDENT. BI-207 6.760E-02 5. OllE-02 l.207E-01 FAIL ABUN PB-210 -1. 268E-01 7.562E+OO 1.525E+Ol NOT IDENT. PB-211 1. 792E-01 7.193E-01 1.438E+OO NOT IDENT. BI-212 7.358E-01 8.783E-01 1.335E+OO FAIL ABUN RN-219 -2.098E-01 3.617E-01 6.640E-01 FAIL ABUN RA-223 -4.391E-01 6.307E-01 1. 017E+OO FAIL ABUN AC-227 -3.762E-01 2.657E-01 3. 996E-01 FAIL ABUN TH-227 -3.762E-01 2.657E-01 3. 996E-01 FAIL ABUN TH-229 -7.744E-02 4.848E-01 8.736E-01 FAIL ABUN TH-231 -4.391E-01 6.307E-01 1.017E+OO FAIL ABUN PA-233 5.431E-02 6.613E-02 1.385E-01 FAIL ABUN PA-234 l.529E-02 2.725E-01 5.620E-01 FAIL ABUN PA-234M 3.369E+OO 4.340E+OO 9.184E+OO NOT IDENT. U-235 1. 771E-02 1.940E-01 3.630E-01 FAIL ABUN NP-237 5.431E-02 6.613E-02 1.385E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 -1.136E-01 2.437E-01 4.440E-01 FAIL ABUN PU-239 -4.243E+Ol 3.300E+02 6.121E+02 FAIL ABUN AM-241 6.568E-02 2.020E-01 3.839E-01 NOT IDENT. CM-243 2.062E-02 1.056E-01 1.915E-01 FAIL ABUN BK-247 1.557E-03 7.712E-02 l.394E-01 NOT IDENT. CM-247 l.930E-02 3.194E-02 6.773E-02 NOT IDENT. CF-249 1.140E-02 3.678E-02 7.492E-02 NOT IDENT. CF-251 -6.705E-02 1.119E-01 l.944E-01 FAIL ABUN Page 3210of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:15:15.97 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 369 10.66* 1.030E+OO 1.738E+Ol 1.738E+Ol 10.57 CD-109 88.03 47 3.70* 4.453E+OO l.483E+OO 2.328E+OO 108.23 SN-126 64.28 76 9.60 1. 986E+OO 2.070E+OO 2.070E+OO 73. 96 86.94 47 8.90 4.453E+OO 6.167E-01 6.167E-01 108.23 87.57 47 37.00* 4.453E+OO l.483E-01 1.483E-01 108.23 BA-137M 661. 66 81 89.90* 1.965E+OO 2.384E-01 2.430E-01 38.33 CS-137 661. 66 81 85.10* 1. 965E+OO 2.519E-01 2.567E-01 38.33 TL-208 277.37 ------6.60 4.074E+OO ------Line Not Found ------583.19 126 85.00* 2.178E+OO 3.520E-01 3.520E-01 26.04 860.56 37 12.50 1.591E+OO 9.740E-01 9.740E-01 60.95 BI-211 72. 87 ------1.23 3.135E+OO ------Line Not Found ------351.06 265 12.92* 3.337E+OO 3.182E+OO 3.182E+OO 17.20 PB-212 74.82 98 10.28 3.357E+OO 1.470E+OO 1. 470E+OO 50.50 77 .11 174 17.10 3.576E+OO 1.473E+OO l.473E+OO 30.75 238.63 415 43.60* 4.584E+OO 1.073E+OO 1.073E+OO 12.92 300.09 23 3.30 3.820E+OO 9.620E-01 9.620E-01 137. 97 BI-214 609.32 162 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 1120.29 34 14.92 1.287E+OO 9.041E-01 9.044E-01 78.15 1764.49 22 15.30 8.672E-01 8.753E-01 8.756E-01 48.71 PB-214 74.82 98 5.80 3.357E+OO 2.605E+OO 2.606E+OO 50.50 77 .11 174 9.70 3.576E+OO 2.597E+OO 2.598E+00 30.75 87.09 47 3.41 4.453E+OO 1.609E+OO 1.610E+OO 108.23 242.00 128 7.25 4.543E+OO 2.013E+OO 2.014E+OO 48.32 295.22 102 18.42 3.868E+OO 7.375E-01 7.378E-01 35.88 351. 93 265 35.60* 3.337E+OO l.155E+OO 1.155E+OO 17.20 RN-222 609.32 162 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 1120.29 34 14.92 1.287E+OO 9. 041E-01 9.044E-01 78.15 1764.49 22 15.30 8.672E-01 8.753E-01 8.756E-01 48. 71 RA-224 240.99 128 4.10* 4.543E+OO 3.560E+OO 3.560E+OO 48.32 RA-226 609.32 162 45.49* 2.102E+OO 8.785E-01 8.789E-01 23.19 1120.29 34 14.92 1.287E+OO 9. 041E-01 9.044E-01 78.15 1764.49 22 15.30 8. 672E-01 8.753E-01 8.756E-01 48.71 AC-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 77 11. 27 3.450E+OO l.031E+OO 1.031E+OO 54.85 794.95 36 4.25 1.697E+OO 2.579E+OO 2.579E+OO 45.09 835.71 ------1.61 1.630E+OO ------Line Not Found ------911.20 73 25.80* 1.521E+OO 9.637E-01 9.637E-01 35.95 968.97 44 15.80 l.448E+OO 9.995E-01 9.995E-01 39.93 RA-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 77 11. 27 3.450E+OO l.031E+OO 1. 031E+OO 54.85 794.95 36 4.25 1.697E+OO 2.579E+OO 2.579E+OO 45.09 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911. 20 73 25.80* 1. 521E+OO 9.637E-01 9.637E-01 35.95 968.97 44 15.80 1.448E+OO 9.995E-01 9.995E-01 39.93 TH-228 74.82 98 10.28 3.357E+OO 1.470E+OO l.470E+OO 50.50 77 .11 174 17.10 3.576E+OO 1.473E+OO 1.473E+OO 30.75 238.63 415 43.60* 4.584E+OO l.073E+OO 1.073E+OO 12.92 Page 3211 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235015 Acquisition date 3-0CT-2016 08:11:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 300.09 23 3.30 3.820E+OO 9.620E-01 9.620E-Ol 137.97 TH-230 609.32 162 45.49* 2.102E+OO 8.785E-01 8.785E-01 23.19 1120.29 34 14.92 l.287E+OO 9. 041E-01 9.041E-01 78.15 1764.49 22 15.30 8.672E-01 8.753E-01 8.753E-01 48.71 PA-231 283.69 48 1. 70 3.991E+OO 3.676E+OO 3.676E+OO 94.84 301.36 23 5.35* 3.820E+OO 5.934E-01 5.934E-01 137.97 TH-232 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 77 11.27 3.450E+OO 1.031E+00 1.031E+OO 54.85 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911. 20 73 25.80* 1.521E+OO 9.637E-01 9.637E-01 35.95 968. 97 44 15.80 1.448E+00 9.995E-01 9.995E-01 39.93 TH-234 63.29 76 3.70* 1.986E+OO 5.371E+00 5. 371E+OO 73. 96 92.59 71 4.23 4.860E+OO l.783E+00 1.783E+OO 93.49 U-234 609.32 162 45.49* 2.102E+00 8.785E-01 8.785E-01 23.19 1120.29 34 14.92 1.287E+OO 9.041E-01 9. 041E-01 78.15 1764.49 22 15.30 8.672E-01 8.753E-01 8.753E-01 48.71 U-238 63.29 76 3.70* 1.986E+OO 5.371E+OO 5.371E+OO 73. 96 92.59 71 4.23 4.860E+OO l.783E+00 l.783E+00 93.49 AM-243 43'. 53 ------5.90 1.573E-01 ------Line Not Found ------74.66 98 67.20* 3.357E+OO 2.248E-01 2.248E-01 50.50 ANH-511 511. 00 67 100.00* 2.430E+OO l.437E-01 1.437E-01 51. 05 Flag: "*" Key line Page 3212 of 5809 Summary of Nuclide Activity Sample ID : G405235015 Acquisition date Page : 3 3-0CT-2016 08:11:39 Total number of lines in spectrum 49 Number of unidentified lines 10 Number of lines tentativel¥ identified by NID 39 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461.400 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1.41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600.00Y 1. 41E+l0Y l.41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 738E+Ol 1.483E+OO 1.483E-01 2.384E-01 2.519E-01 3.520E-01 3.182E+OO 1.073E+OO 8.785E-01 l.155E+OO 8.785E-01 3.560E+OO 8.785E-01 9.637E-01 9.637E-01 1.073E+OO 8.785E-01 5.934E-01 9.637E-01 5.371E+OO 8.785E-01 5. 371E+OO 2.248E-01 1.437E-01 4.889E+Ol 4.889E+Ol Decay Corr pCi/GRAM 1. 738E+Ol 2.328E+OO 1.483E-01 2.430E-01 2.567E-01 3.520E-01 3.182E+OO 1.073E+OO 8.789E-01 1.155E+OO 8.789E-01 3.560E+OO 8.789E-01 9.637E-01 9.637E-01 '1. 073E+OO 8.785E-01 5.934E-01 9.637E-01 5.371E+OO 8.785E-01 5.371E+OO 2.248E-01 1.437E-01 4.975E+Ol 4.975E+Ol 79.59% Decay Corr 2-Sigma Error 0.184E+Ol 2.519E+OO 1.605E-01 0.931E-01 0.984E-01 0.917E-01 0.547E+OO 0.139E+OO 2.038E-01 0.199E+OO 2.038E-01 1. 720E+OO 2.038E-01 3.464E-01 3.464E-01 0.139E+OO 2.037E-01 8.186E-01 3.464E-01 3.973E+00 2.037E-01 3.973E+00 1.135E-01 0.733E-01 "M" Manually accepted 2-Sigma %Error 10.57 108.23 108.23 38.33 38.33 26.04 17.20 12.92 23.19 17.20 23.19 48.32 23.19 35.95 35.95 12.92 23.19 137.97 35.95 73. 96 23.19 73.96 50.50 51. 05 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3213 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235015 Acquisition date : 3-0CT-2016 08:11:39 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 99.51 37 228 3.33 199.50 193 12 8.49E-03 **** 5.22E+OO T 0 185.90 118 132 0. 96 372.34 366 12 2.83E-02 47.5 5.40E+OO T 0 209.20 29 81 0.93 418. 96 416 7 7.09E-03 **** 5.03E+OO 0 271.00 25 84 1. 46 542.61 536 9 6.29E-03 -1:<*** 4.15E+OO T 0 321. 84 41 44 0.98 644.35 640 10 1. 03E-02 71. 9 3.60E+OO T 0 414.86 16 40 2.38 830.48 823 10 4.05E-03 **** 2.90E+OO T 0 482.23 13 23 1. 49 965.28 959 10 3.27E-03 **** 2.55E+OO T 2 516.88 22 4 1. 80 1034.63 1031 25 5.80E-03 59.2 2.41E+OO 2 525.75 20 7 1. 81 1052.37 1031 25 5.21E-03 61. 4 2.37E+OO 0 669.81 10 27 4.82 1340.67 1330 12 2.80E-03 **** l.95E+OO 0 727.83 17 26 1. 36 1456.78 1451 10 4.66E-03 **** 1.82E+OO T 0 738.40 5 10 0.89 1477.92 1474 6 l.25E-03 **** l.80E+OO T 0 768.61 28 24 1. 71 1538.38 1529 13 7.49E-03 82.6 1. 74E+OO 0 772.60 9 13 1. 38 1546.37 1543 7 2.35E-03 **** 1.74E+OO T 0 871.28 26 13 6.59 1743.86 1734 18 7.15E-03 77.6 1.58E+OO T 0 923.46 11 5 0.59 1848.31 1845 7 3.07E-03 90.7 1.50E+OO T 5 964.70 22 5 2.91 1930.84 1926 18 6.07E-03 55.0 l.45E+00 T 0 1005.15 8 12 0.92 2011. 81 2008 8 2.22E-03 **** 1. 41E+OO T 0 1039.30 7 14 0.97 2080.16 2071 11 2.02E-03 **** 1.37E+OO T 0 1041. 21 13 1 1. 51 2083.97 2081 6 3.50E-03 63.9 1.37E+OO 0 1084.19 13 14 0.73 2170.00 2162 14 3. 61E-03 **** 1.32E+OO 0 1095.28 7 7 0.98 2192.21 2188 6 1.84E-03 **** 1.31E+OO 0 1098.49 16 4 3.22 2198.64 2194 10 4.44E-03 71. 3 1. 31E+OO T 0 1154. 44 16 8 2.34 2310.63 2305 11 4.45E-03 85.3 1.26E+OO 0 1223.88 9 11 0.65 2449.62 2444 9 2. 51E-03 **** 1.20E+00 0 1333. 06 8 5 2.33 2668.18 2661 11 2.36E-03 **** 1. llE+OO T Flags: "T" = Tentatively associated Page 3214 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:15:39.45 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235015.CNF;l *
  • Acquisition date 3-0CT-2016 08:11:39 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:56:00 Nuclide Library : SOLID *
  • Sample ID G405235015 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4507E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2. 7 51E-01 l.287E+OO 7.438E-02 3.369E-02 3.559E-02 2.874E-02 1.499E-01 4. 231E-02 5.753E-02 1.683E-01 5.753E-02 4.537E-01 5.753E-02 l.280E-01 l.280E-01 4.231E-02 5.751E-02 3.768E-01 1.280E-01 1.356E+OO 5.751E-02 1.356E+OO 5.407E-02 1. 967E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3215of5809 Le (pCi/GRAM 1.006E+Ol 4.428E-02 O.OOOE+OO 3.078E-02 2.919E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 .AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3216of5809 6. 52 6E-02 3.615E-01 O.OOOE+OO 4.678E-02 5.009E-01 5.845E+OO 4.021E-02 1. 750E-01 2.300E+OO l.415E+Ol O.OOOE+OO l.829E-01 O.OOOE+OO O.OOOE+OO 5. 728E-01 4.899E+OO 5.175E-01 O.OOOE+OO 2.239E-01 5.751E+02 3.555E-02 8.093E-01 2.008E+00 1. 378E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.278E-02 5.050E-02 5.518E+OO 4.573E-01 4.573E-01 2.880E-02 8.291E-02 2.103E-01 O.OOOE+OO O.OOOE+OO 1.110E-01 1.255E+OO 9.237E-02 2.604E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.890E-02 0.000E+OO 5.983E-02 l.184E-01 O.OOOE+OO O.OOOE+OO 1.098E-01 O.OOOE+OO O.OOOE+OO 2.348E+Ol O.OOOE+OO 3.072E-01 5.076E-02 4.410E+OO 4.197E-02 O.OOOE+OO 7.344E+02 b.OOOE+OO 2.139E-02 8.342E-02 1.781E-01 l.076E-01 9.915E-02 1.684E+OO 4.844E-02 3.475E+Ol l.959E-01 8.575E-02 2.220E-02 3.776E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3217 of 5809 8.560E-01 4.187E+OO 2.414E+Ol l.020E+02 4.299E-01 1.840E+OO 5.319E-02 7.066E+00 6.545E-01 6.091E-01 2.952E-01 4.577E-01 1. 821E-01 1.821E-01 4.054E-01 4.577E-01 6.417E-02 2.410E-01 3.994E+OO 1.702E-01 6.417E-02 O.OOOE+OO 2.059E-01 2.863E+02 1. 789E-01 8. 901E-02 6.398E-02 3.049E-02 3.389E-02 8.954E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. .FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL* ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016.09:15:50.50 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARGHIVE.GAMMA]G405235015.CNF;l * *Acquisition date 3-0CT-2016 08:11:39 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:56:00 Nuclide Library : SOLID *
  • Sample ID G405235015 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity 1.4507E+02 GRAM *
  • Quantity Err(%) 1.3786E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) K-40 1.738E+Ol 2.015E+00 2.015E+OO CD-109 1.261E+00 2.503E+OO 2.503E+OO SN-126 8.036E-02 l.594E-01 1.594E-01 BA-137M 2.430E-01 9.187E-02 9.187E-02 CS-137 2.567E-01 9.705E-02 9.705E-02 TL-208 3.520E-01 9.105E-02 9.105E-02 BI-211 1.150E+OO 9.036E-01 9.036E-01 PB-212 1.073E+OO 1.473E-01 1.473E-01 BI-214 8.789E-01 2.032E-01 2.032E-01 PB-214 1.155E+OO 2.006E-01 2.006E-01 RN-222 8.789E-01 2.032E-01 2.032E-01 RA-224 2.256E+OO 1. 753E+OO 1. 753E+OO RA-226 8.789E-01 2.032E-01 2.032E-01 AC-228 9.637E-01 3.430E-01 3.430E-01 RA-228 9.637E-01 3.430E-01 3.430E-01 TH-228 1.073E+OO 1.473E-01 1.473E-01 TH-230 8.785E-01 2.032E-01 2.032E-01 PA-231 5.934E-01 8.122E-01 8.122E-01 TH-232 9.637E-01 3.430E-01 3.430E-01 TH-234 5.371E+OO 4.071E+OO 4.071E+OO U-234 8.785E-01 2.032E-01 2. 032E-Ol. U-238 5.371E+OO 4.071E+OO 4. 071E+OO AM-243 l.612E-01 1.142E-01 1.142E-01 ANH-511 l.437E-01 7.212E-02 7.212E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.215E+00 1.313E+Ol 1. 314E+Ol NOT IDENT. NA-22 -2.426E-02 5.690E-02 5.794E-02 NOT IDENT. NA-24 -l.OOOE+41 4.956E+41 O.OOOE+OO SHORT HLIF AL-26 1.487E-02 3.216E-02 3.285E-02 NOT IDENT. SC-46 -2.499E-01 3.790E-01 3.954E-01 FAIL ABUN V-48 1.113E+04 1.678E+04 1. 751E+04 SHORT HLIF Page 3218of5809 CR-51 -1.114E+02 4.431E+02 4.459E+02 SHORT HLIF MN-54 -1. 210E-02 8.120E-02 8 .138E-02 NOT IDENT. C0-56 -1.lOlE-01 4.647E-01 4.673E-01 FAIL ABUN MN-56 -1.000E+41 4.458E+41 0.000E+OO SHORT HLIF C0-57 5.235E-02 4.856E-02 5.399E-02 NOT IDENT. C0-58 1.616E-01 5.704E-01 5.750E-01 NOT IDENT. FE-59 1.183E+Ol 8.309E+OO 9.874E+OO FAIL ABUN C0-60 4.267E-02 5. 313E-02 5.650E-02 FAIL ABUN ZN-65 1.012E-01 2.061E-01 2. lllE-01 NOT IDENT. GE-68 2.lOlE+OO 2.450E+OO 2.627E+OO NOT IDENT. AS:-73 2.130E+OO 1.516E+Ol l.519E+Ol NOT IDENT. AS-74 -3.971E+02 6.059E+03 6.062E+03 SHORT HLIF SE-75 -3.892E-03 2.215E-01 2.215E-01 NOT IDENT. BR-77 1. 963E+38 l.700E+39 O.OOOE+OO SHORT HLIF SR-82 -2.631E+Ol 9.496E+02 9.497E+02 SHORT HLIF RB-83 3.473E-01 6.659E-01 6.841E-01 NOT IDENT. KR-85 6.488E+OO 5.035E+OO 5.823E+OO NOT IDENT. SR-85 6.846E-01 5.321E-01 6.151E-01 NOT IDENT. RB-86 7.865E+03 3.075E+04 3.095E+04 SHORT HLIF Y-88 -2.598E-02 2.676E-01 2.678E-01 NOT IDENT. Y-91 2 .110E+02 6.394E+02 6.464E+02 NOT IDENT. NB-94 2.033E-02 3.946E-02 4.051E-02 FAIL ABUN NB-95 1.164E-01 l.067E+OO 1.068E+OO NOT IDENT. NB-95M -1.639E+OO 2. 831E+OO 2.926E+OO NOT IDENT. ZR-95 -9.700E-01 1.820E+OO 1.872E+OO NOT IDENT. NB-97 -1.000E+41 l.940E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 3.690E+41 O.OOOE+OO SHORT HLIF M0-99 7.926E+31 1. 811E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 5.547E+41 O.OOOE+OO SHORT HLIF RH-101 1.974E-02 3.582E-02 3. 691E-02 NOT IDENT. RH-102 7.340E-03 5.817E-02 5.826E-02 NOT IDENT. RU-103 -2.265E+OO 6.653E+OO 6.730E+OO FAIL ABUN RH-106 2.279E-02 5.336E-01 5.337E-01 NOT IDENT. RU-106 2.279E-02 5.336E-01 5.337E-01 NOT IDENT. AG-108M l.552E-02 3.094E-02 3.172E-02 NOT IDENT. AG-llOM -l.230E-01 l .151E-01 1.278E-01 NOT IDENT. SN-113 -l.381E-01 2.529E-01 2.604E-01 NOT IDENT. CD-115 1.119E+39 2.921E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -8.680E+03 9.548E+04 9.556E+04 SHORT HLIF TE-123M 2.414E-02 1.261E-01 1. 2 66E-01 NOT IDENT. SB-124 -9.028E-01 1.944E+OO 1. 986E+OO NOT IDENT. SB-125 2.405E-02 1.017E-01 1.023E-01 FAIL ABUN TE-125M -4.543E+Ol 2.972E+02 2.979E+02 NOT IDENT. I-126 2.633E+05 l.066E+06 1.073E+06 SHORT HLIF SB-126 -l.938E+05 9 .135E+05 9.177E+05 SHORT HLIF SB-127 l.037E+22 2.705E+22 O.OOOE+OO SHORT HLIF I-131 7.678E+08 4.605E+09 4.618E+09 SHORT HLIF I-132 1.000E+41 l.933E+42 O.OOOE+OO SHORT HLIF TE-132 3.654E+26 4.481E+26 O.OOOE+OO SHORT HLIF BA-133 5.431E-02 3.992E-02 4.683E-02 NOT IDENT. I-133 -l.000E+41 2.280E+41 O.OOOE+OO SHORT HLIF CS-134 1. 689E-01 7.497E-02 1. 068E-01 FAIL ABUN CS-135 -2.155E-02 l.460E-01 1.463E-01 NOT IDENT. I-135 l.000E+41 l.052E+42 O.OOOE+OO SHORT HLIF CS-136 -4.493E+04 3.294E+05 3.300E+05 SHORT HLIF CE-139 7.823E-02 l.216E-01 1.266E-01 NOT IDENT. BA-140 -3.078E+05 l.205E+06 1.213E+06 SHORT HLIF LA-140 -3.037E+05 4.012E+05 4.239E+05 SHORT HLIF CE-141 1. 041E+OO 2.691E+Ol 2.692E+Ol NOT IDENT. CE-143 -l.OOOE+41 6.679E+41 O.OOOE+OO SHORT HLIF CE-144 -2.331E-01 3.728E-01 3.873E-01 NOT IDENT. PM-144 -7.840E-03 6. l 71E-02 6.181E-02 NOT IDENT. PR-144 -6.812E-01 5.361E+OO 5.369E+OO NOT IDENT. PM-146 2.362E-02 4.487E-02 4.612E-02 NOT IDENT. ND-147 -8.845E+06 3.053E+07 3.079E+07 SHORT HLIF PM-147 -5.403E+Ol 8.382E+02 8.386E+02 NOT IDENT. PM-149 1.000E+41 9.550E+40 0.000E+OO SHORT HLIF EU-150 5.076E-06 2.641E-02 2. 641E-02 FAIL ABUN EU-152 2.974E-02 8.966E-02 9.065E-02 FAIL ABUN GD-153 1. 756E-01 l.971E-01 2.124E-Ol NOT IDENT. EU-154 -6.221E-02 l.390E-01 1.418E-01 FAIL ABUN EU-155 -l.454E-02 1.127E-01 1.129E-01 FAIL ABUN TB-160 7.227E-01 1. 783E+OO 1.812E+OO FAIL ABUN H0-166M -4.340E-03 5.857E-02 5.860E-02 FAIL ABUN TM-171 1.593E+OO 3.750E+Ol 3.750E+Ol NOT IDENT. HF-172 -6. 872E-02 2.296E-01 2.317E-01 FAIL ABUN LU-172 2.874E-02 1.066E-01 l.074E-01 FAIL ABUN LU-176 7.255E-03 2.377E-02 2.400E-02 FAIL ABUN Page 3219 of 5809 HF-181 4.271E+OO 6. 720E+OO 6.990E+00 FAIL ABUN TA-182 -l.841E-01 l.190E+OO l.193E+OO FAIL ABUN RE-183 -2.181E-01 4.547E+OO 4.549E+OO NOT IDENT. RE-184 -8.667E+OO 2.917E+Ol 2.943E+Ol NOT IDENT. W-188 9.675E+OO 1. 339E+02 l.340E+02 FAIL ABUN IR-192 l.295E-01 4.625E-01 4.662E-01 FAIL ABUN HG-203 -l.257E+OO 2.413E+OO 2.478E+OO NOT IDENT. BI-207 6.760E-02 5.018E-02 5.870E-02 FAIL ABUN PB-210 -l.268E-01 7.562E+OO 7.562E+OO NOT IDENT. PB-211 1. 792E-01 7.194E-01 7.239E-01 NOT IDENT. BI-212 7.358E-01 8.791E-01 9.396E-01 FAIL ABUN RN-219 -2.098E-01 3.626E-01 3.747E-01 FAIL ABUN RA-223 -4.391E-01 6.312E-01 6.616E-01 FAIL ABUN AC-227 -3.762E-01 2.703E-01 3.191E-01 FAIL ABUN TH-227 -3.762E-01 2.703E-01 3 .191E-01 FAIL ABUN TH-229 -7.744E-02 4.848E-01 4.860E-01 FAIL ABUN TH-231 -4.391E-01 6.312E-01 6.616E-01 FAIL ABUN PA-233 5.431E-02 6.618E-02 7.056E-02 FAIL ABUN PA-234 l.529E-02 2.731E-01 2.732E-01 FAIL ABUN PA-234M 3.369E+OO 4.343E+OO 4. 601E+OO NOT IDENT. U-235 1. 771E-02 l.940E-01 l.942E-01 FAIL ABUN NP-237 5.431E-02 6.618E-02 7.056E-02 FAIL ABUN NP-238 4.718E+40 5.971E+41 O.OOOE+OO SHORT HLIF NP-239 -l.136E-01 2.439E-01 2.492E-01 FAIL ABUN PU-239 -4.243E+Ol 3.300E+02 3.306E+02 FAIL ABUN AM-241 6.568E-02 2.020E-01 2.042E-01 NOT IDENT. CM-243 2.062E-02 l.056E-01 1. 060E-01 FAIL ABUN BK-247 l.557E-03 7.712E-02 7.713E-02 NOT IDENT. CM-247 1. 930E-02 3.210E-02 3.326E-02 NOT IDENT. CF-249 l.140E-02 3.679E-02 3.715E-02 NOT IDENT. CF-251 -6.705E-02 l .121E-01 l.161E-01 FAIL ABUN Page 3220 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 53.8048 87.09 91.6306 136.47 51.5515 45.60 55.0496 87.57 91.7214 140.51 0.0000 46.54 53.4309 88.03 113 .1961 143.76 72.7363 49. 72 0.0000 88.34 113.2678 144.24 64. 0964 51. 35 61.4377 88.47 113. 2975 145.44 76.1780 51. 87 57. 9111 89. 96 85.2290 152.43 79.1334 52.39 54.3732 1093.63 85.3452 153.25 0.0000 52.97 49.0174 91.11 0.0000 323.87 60.5977 53.44 54.5368 92.59 92.9816 156.02 0.0000 54.07 56.4552 93.35 93.1204 158.56 0.0000 57.36 0.0000 94.56 93.3405 159.00 51.0144 57.53 57.9169 94.65 93.3568 162.33 57.9263 57.98 66.2709 94.67 93.3604 162.66 0.0000 59.27 65.2685 94.87 93. 3967 163.33 69.1578 59.32 65.2771 97.43 53.6324 165.86 60.4352 59.54 55.4562 98.43 53.7341 176.31 52.1754 60. 96 63.0852 98.44 53.7351 176.60 0.0000 61.17 63 .1197 99.53 53.8456 177.52 57.9345 62.93 62.4742 100 .11 53.9038 181. 07 0.0000 63.29 62.5314 102.03 51.3915 181.52 63.9297 63.58 62.5775 103.18 54.2102 184.41 46.9708 64.28 72.3566 103.37 54.2293 143.76 47.0459 66.73 56.4816 105.21 65.2930 193.51 59.0645 67.24 59.3797 105.31 65.3047 197.03 59.3073 125.81 76.4276 106.12 57.2249 198.01 76.8372 67.75 76.4399 106.47 57.2608 201.83 60.8042 69.67 71.1061 109.28 70.9057 203.43 59.7431 70.83 75.1046 111. 00 63.9044 205.31 64 .. 1734 72. 81 95.5101 111.76 0.0000 210.85 59.8451 72.87 95.5238 114. 06 56.9886 215.65 65.3049 74.66 87.2842 116. 30 0.0000 222 .11 66.9537 74.82 87.3162 116. 74 64.5340 227.09 57.6899 74. 97 87.3460 119. 76 65.9051 227.38 43.2806 77 .11 87.7675 121.12 60.8099 228.16 0.0000 78.74 80.0184 121. 22 60.8201 228.18 48.1299 79.69 60.7853 121. 7 8 52.4788 116.74 48.1299 80.12 55.6641 122.06 49.3527 235.69 64. 6696 80.19 0.0000 122.92 52.5761 235.96 64.6867 80.57 59.6057 123.07 56.7962 238.63 44.9978 81. 00 53.1765 265.00 56.8522 238.98 0.0000 81. 07 59.6703 125.81 63.3852 240.99 45.1039 81. 75 78.9186 127.23 62.4687 242.00 45 .1496 83.79 61.3217 127.91 71.0157 244.70 44.0469 84.00 58.7384 129.30 73.2946 252.40 0.0000 85.43 79.8615 131.20 68.1855 252.80 48.0954 86.55 91.5291 133.02 65.1709 254.15 0.0000 86.79 91. 5738 133. 52 72. 7055 256.23 65.5755 86.94 91.6029 136.00 62.2472 260.90 0.0000 Page 3221of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.1553 355.39 0.0000 584.27 20.0919 264.80 41.1614 356.01 16.1433 595.83 0.0000 265.00 41.1684 364.49 0.0000 427.87 28.0470 268.22 42.5425 366.42 0.0000 602.52 0.0000 269.46 45. 0967 372.51 32.6785 604. 72 15.6134 270.03 45 .1198 375.05 22.7351 607.14 25.0107 271.23 42.6608 377.52 26.4187 609.32 19.8218 273.65 0.0000 356.01 35.6881 610.33 19.8311 276.40 34.4570 388.16 25.6997 614.28 26.6673 277.37 37.0104 388.63 0.0000 618.01 19.9053 277.60 37.0176 391.69 38.6436 620.36 22.0254 278.00 35.3478 264.66 36.1047 621. 93 16.7943 279.20 40.4414 401. 81 29.6471 630.19 0.0000 279.54 50.5664 402.40 19.4641 631.29 14.7611 279.70 50.5737 404.85 30.6367 633.25 18. 9961 280.46 44.2819 410.95 32.1606 634.78 0.0000 283.69 29.6060 413.71 36.4221 635.95 16.9069 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 29.6509 423.72 0.0000 645.85 14.8625 285.90 0.0000 427.09 30.1478 657.76 17.6132 287.50 30.5544 427.87 22.6221 657.90 0.0000 290.67 40.8516 433.94 26.4955 661.66 22.4569 293.27 0.0000 439.40 28.4863 664.57 0.0000 351. 93 . 38.4485 453.88 21. 0798 666.33 0.0000 295. 96 38.4732 463.37 26.0211 666.50 0.0000 879.38 38.5593 468.07 23.1958 667.71 0.0000 299.98 38.6050 473.00 0.0000 677.62 14.0029 300.09 38.6087 475.06 21.3519 685.70 0.0000 300.13 38.6096 476.78 26.2315 695.00 0.0000 301.36 37.3616 477.60 20.4121 696.49 20.6375 302.85 39.9884 482.18 15.5944 696. 51 20.6382 256.23 38.2357 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.8184 306.78 33.6497 497.08 30.4765 697.49 21. 7334 308.46 42.3367 505.52 25.1903 702.65 21.7822 311. 90 38.1249 507.63 0.0000 706.68 17.4564 316.51 33.9203 511. 00 14.8639 711. 68 16.4008 319.41 0.0000 514.00 2.9778 720.70 0.0000 320.08 0.0000 514.00 2.9778 721. 93 0.0000 321.04 30.5524 520.40 13.4478 722.78 6.5918 323.87 39. 3713 520.69 0.0000 722. 91 8.2401 325.23 44.6696 522.65 0.0000 723.31 8.2416 328.76 0.0000 527.90 0.0000 724 .19 6.5957 333.37 27.5031 528.26 10.5047 727.33 12.1082 333.97 31.7490 529.59 18.0212 733.00 15.4475 334.37 33.0826 529.87 0.0000 735.93 9.9426 338.28 30.0862 531. 02 0.0000 333.97 15.4766 338.32 30.0869 537.26 0.0000 739.50 0.0000 311. 90 31. 9102 546.56 0.0000 747.24 12.2098 340.48 31.9102 552.55 21. 2854 748.06 16.6553 340.55 0.0000 563.25 23.4436 752.31 23.3584 344.28 28.4473 569.33 20.4500 753.82 0.0000 345.93 29.9072 946.00 20.4517 756.73 24.5155 351.06 26.8066 569.70 20.4541 756.80 24.5164 351.93 26.8237 583.19 18.5361 884.68 13. 4116 Page 3222 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 18.4551 1274.44 13.6844 1620.50 2.1527 766.42 18.4591 1001.03 7.3098 1621. 92 7.5370 766.84 18.4625 1002.74 13.1647 1678.03 0.0000 772.60 0.0000 1004.73 17.3817 1690.97 4.3708 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 8.8750 778.90 11. 2439 1028.54 0.0000 1063.66 7.7750 783.70 0.0000 1037.84 16.2733 1771.35 2.2219 785.37 16.9098 1038.76 0.0000 1791.20 0.0000 792.07 8.4775 631.29 9.2712 1808.65 2.2385 794.95 7. 9211 1048.07 0.0000 1810.72 0.0000 795.86 7.9240 1049.04 15.7736 1836.06 5.4015 810.06 15.9363 1050.41 10.2111 810.29 15.9380 1063.66 5.5928 344.28 10.2462 1077.00 0.0000 810.76 10.2477 1077.34 5.9906 815.77 0.0000 1085.87 13.5141 1048.07 0.0000 1093.63 15.0518 832.01 19.5151 1099.45 7.5391 834.85 21. 8342 1112. 07 13.2438 835.71 18.3932 1112.84 18.9233 836.80 0.0000 1115. 54 10.6060 846.75 0.0000 1120.29 17.0695 846.77 12.6982 1120.55 17.0706 856.80 0.0000 1221.41 17.0739 860.56 10.4429 1129. 67 11. 4111 871.09 10.4832 1131. 51 0.0000 873.19 10.4912 1147.95 0.0000 875.33 0.0000 1173.23 13.4830 879.38 9.6388 1177.95 13.5010 880.51 4.3831 1189.05 11. 608 9 883.24 18.4269 1204.77 14.5752 884.68 22.8262 1221. 41 15.6191 889.28 15.8291 1231.02 18.5964 894.76 14.0981 1235.36 0.0000 898.04 11. 4678 1238.28 19.6143 900.72 14.1279 1260.41 0.0000 903.28 13.2568 1271.87 13.8556 911.20 16.8395 1274.44 15.8457 912.08 16.8448 1274.54 15.8457 923.98 0.0000 1291. 59 8.9539 926.50 12.8312 1298.22 0.0000 929 .11 8.0266 1312 .11 0.0000 937.49 9.8388 1332.49 8.0444 944 .13 0.0000 1362.66 0.0000 946.00 11. 6618 1365.19 5. 0696 949.00 14.3677 1368.63 0.0000 667. 71 0.0000 1384.29 9.1692 962. 31 11.5461 1408.01 6.1487 964.08 9.0259 1457.56 0.0000 966 .17 9.0323 1460.82 6.2278 911.20 9.0408 1489.16 5.2246 968. 97 9.0408 1505.03 6. 292 6 983.53 0.0000 1584.12 7.4747 984.45 0.0000 1596.21 0.0000 Page 3223 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:16:33.43 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM12.CNF;467 Background date : Z-OCT-2016 11:00:40. Sample date 8-DEC-2015 11:29:00. Acquisition date : 3-0CT-2016 08:15:34. Sample ID G405235016 Sample quantity l.63118E+02 GRAM Detector name GAM12 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 9 9 9 9 9 0 3 3 0 4 4 0 0 0 0 3 3 0 0 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 Page 3224 of 5809 Energy 35.91* 37.68* 40.14 42.83 45.08 64.52* 75.00 77.26* 87.10 90.06 93.09* 154.32 157.46 185.62* 209.26 238.62* 241.60 258.15 271.20 295.06 338.33* 351.65* 408.91 432.57 443.52 446.21 462.58 491. 73 510.37* 569.42 583.20* 609.25* 662.19 727. 24 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 31 50 72 27 17 14 120 148 30 53 108 31 23 61 29 399 122 13 32 171 76 232 26 10 20 24 29 14 58 39 122 146 28 46 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 8 40 77 145 86 166 192 135 170 68 169 65 92 137 90 86 90 62 112 58 57 75 97 31 7 26 45 17 36 60 26 44 58 35 1.15 1. 86 1. 78 2.60 1.17 0.62 1. 69 1. 23 1. 23 1. 04 1. 90 1. 34 1. 37 1. 24 0.89 *i. 28 1. 92 1. 41 0.80 1. 30 1.10 1. 38 5.41 1. 27 1. 28 1. 74 3.05 1. 73 1. 35 0.81 1. 31 1. 55 1. 02 1. 52 71. 66 75.20 80 .11 85.49 90.00 128.86 149.83 154.36 174.04 179.95 186.01 308.48 314.75 371.06 418.35 477.07 483.04 516 .13 542.23 589.98 676.52 703.18 817.70 865.05 886.95 892.32 925.07 983.40 1020.67 1138.82 1166. 38 1218.51 1324.44 1454.59 68 68 68 68 68 124 143 143 171 178 178 306 312 367 415 472 472 512 536 586 672 697 805 861 885 885 918 979 1013 1132 1160 1213 1320 1448 25 8.49E-03 43.5 25 l.39E-02 41.4 25 2.00E-02 28.2 25 7.47E-03 90.1 25 4.85E-03 81.1 8 3.90E-03163.9 17 3.33E-02 24.8 17 4.lOE-02 16.1 8 8.20E-03 78.4 16 l.48E-02 24.7 16 3.0lE-02 26.9 6 8.54E-03 45.7 8 6.48E-03 73.6 10 l.70E-02 39.1 8 7.98E-03 60.2 19 l. llE-01 6. 5 19 3.40E-02 23.9 9 3.62E-03112.8 14 8.80E-03 73.9 10 4.75E-02 11.3 10 2.llE-02 22.3 12 6.46E-02 10.0 19 7.34E-03 92.5 8 2.74E-03100.0 17 5.51E-03 28.1 17 6.65E-03 45.9 14 8.03E-03 52.9 7 3.94E-03 55.4 16 1. 61E-02 31. 0 16 l.lOE-02 46.6 14 3.40E-02 13.0 15 4.04E-02 12.9 11 7.65E-03 56.8 16 l.27E-02 32.8 Fit 2. 41E+OO 1.17E+OO 1. 47E+00 1.02E+OO 3.17E+00 Peak Search Report (continued) Page : 2 Sample ID : G405235016 Acquisition date : 3-0CT-2016 08:15:34 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 795.02 25 11 1.10 1590. 21 1584 11 7.0lE-03 32.3 36 0 8 62. 42 39 30 4.43 1725.08 1717 19 1.08E-02 36.7 37. 0 889.39 12 14 3.27 1779.06. 1774 11 3.26E-03 68.0 38 0 911. 23* 78 20 1.10 1822. 78 1817 13 2.15E-02 16.7 39 0 969 .14 66 24 1. 25 1938. 66 1932 14 1.83E-02 20.l 40 0 996 .16 11 2 1.63 1992.73 1989 7 3.14E-03 35.4 41 0 1104.74 15 20 0.53 2210.06 2202 16 4.07E-03 73.2 42 0 1120.60 50 11 1. 39 2241. 80 2236 14 1. 39E-02 19. 8 43 0 1161.46 12 0 1. 60 2323. 58 2320 7 3.33E-03 28.9 44 0 1181.87 11 27 3.93 2364.44 2352 19 2.97E-03123.2 45 0 1187. 67 16 5 2.39 2376.05 2372 9 4.46E-03 34.8 46 0 1194.48 20 2 3.89 2389.67 2385 11 5.49E-03 27.5 47 0 1239.76 31 7 3.90 2480.31 2473 14 8.73E-03 25.2 48 0 1247.01 21 7 2.11 2494.83 2488 13 5.69E-03 33.8 49 0 1460.74 336 0 1.85 2922.71 2915 14 9.33E-02 5.5 50 0 1764.60 35 7 1. 38 3531.13 3523 13 9.58E-03 22.8 51 0 2042.49 5 5 0.51 4087.70 4081 10 1.39E-03 94.9 Flag: "*" = Peak area was modified by background subtraction Page 3225 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:16:36 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 11:29:00 G405235016 Acquisition date : Sample quantity Sample g.eometry : 3-0CT-2016 08:15:34 163.12 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA12 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3226 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235016 Acquisition date 3-0CT-2016 08:15:34 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.082E+OO l.303E+Ol 1.303E+Ol 10.91 OK SC-46 889.28 99.98* 1. 620E+OO 3.460E-02 4.135E-01 135.97 OK 1120.55 99.99 1.350E+OO l.715E-01 2.049E+OO 39.59 OK BA-137M 661. 66 89.90* 2.040E+OO 7.427E-02 7.569E-02 113. 58 OK CS-137 661.66 85.10* 2.040E+OO 7.846E-02 7. 996E-02 113. 58 OK TL-208 277.37 6.60 4.142E+OO Line Not Found Absent 583.19 85.00* 2.256E+OO 3.205E-01 3.205E-01 26.05 OK 860.56 12.50 l.662E+OO Line Not Found Absent PB-210 46.54 4.25* 3.130E-01 8.579E+OO 8.802E+OO 162.16 OK PB-212 74.82 10.28 3.186E+OO l.562E+OO 1.562E+OO 73.17 OK 77 .11 17.10 3.414E+OO l.571E+OO 1. 571E+OO 32.23 OK 238.63 43.60* 4.646E+OO l.093E+OO 1. 093E+OO 12.91 OK 300.09 3.30 3.888E+OO Line Not Found Absent BI-214 609.32 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 OK 1120.29 14.92 1.350E+OO l.149E+00 1.149E+OO 39.59 OK 1764.49 15.30 9.121E-01 1. 079E+OO 1. 079E+OO 45.69 OK PB-214 74.82 5.80 3.167E+OO Line Not Found <<INT Reject 77 .11 9.70 3.414E+OO 2.769E+OO 2.770E+OO 32.23 OK 87.09 3.41 4.297E+00 l.237E+OO l.238E+OO 156.88 OK 242.00 7.25 4.599E+OO Line Not Found <<INT Reject 295.22 18.42 3.9428+00 l.277E+OO 1.278E+OO 22.57 OK 351. 93 35.60* 3.413E+OO 1.017E+OO 1.018E+00 20.10 OK RN-222 609.32 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 OK 1120.29 14.92 l.350E+OO l.149E+OO l.149E+00 39.59 OK 1764.49 15.30 9 .121E-01 1.079E+OO 1. 079E+OO 45.69 OK RA-224 240.99 4.10* 4.604E+OO 1. 332E+OO 1.332E+OO 134.55 OK RA-226 609.32 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 OK 1120.29 14.92 l.350E+OO l.149E+OO l.149E+00 39.59 OK 1764.49 15.30 9.121E-01 1.079E+OO 1.079E+OO 45.69 OK AC-228 105.21 1.10 5.379E+OO Line Not Found Absent 338.32 11. 27 3.524E+OO 1. 021E+OO l.021E+OO 44.67 OK 794.95 4.25 1. 768E+OO l.623E+OO 1.623E+OO 64.54 OK 835. 71 1. 61 1. 701E+OO Line Not Found Absent 911. 20 25.80* 1.589E+OO 8.986E-01 8.986E-01 33.41 OK 968. 97 15.80 1.514E+OO l.298E+OO 1.298E+OO 40.27 OK RA-228 105.21 1.10 5.379E+OO Line Not Found Absent 338.32 11. 27 3.524E+OO l.021E+OO 1.021E+OO 44.67 OK 794.95 4.25 1. 768E+OO 1.623E+OO 1.623E+OO 64.54 OK 835. 71 1. 61 1. 701E+OO Line Not Found Absent 911. 20 25.80* 1. 589E+OO 8.986E-01 8.986E-01 33.41 OK 968. 97 15.80 1.514E+OO l.298E+OO 1.298E+OO 40.27 OK TH-228 74.82 10.28 3.186E+OO l.562E+OO 1.562E+OO 73.17 OK 77 .11 17.10 3.414E+OO 1.571E+OO 1.571E+OO 32.23 OK 238.63 43.60* 4.646E+OO 1.093E+OO 1.093E+OO 12.91 OK 300.09 3.30 3.888E+OO Line Not Found Absent TH-230 609.32 45.49* 2.179E+OO 7.334E-01 7.334E-01 25.80 OK 1120.29 14.92 1.350E+OO l.149E+OO 1.149E+OO 39.59 OK 1764.49 15.30 9.121E-01 1.079E+OO 1.079E+OO 45.69 OK TH-232 105.21 1.10 5.379E+OO Line Not Found Absent Page 3227 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235016 Acquisition date 3-0CT-2016 08:15:34 Nuclide Type: Nuclide Energy %Abn %Eff Uncorrected Decay Corr 2-Sigma pCi/GRAM pCi/GRAM %Error Status 338.32 11. 27 3.524E+OO l.021E+OO 1. 021E+OO 44.67 OK 835. 71 1. 61 1. 701E+OO Line Not Found Absent 911.20 25.80* 1. 589E+OO 8.986E-01 8.986E-01 33.41 OK 968. 97 15.80 1.514E+OO l.298E+OO 1.298E+OO 40.27 OK TH-234 63. 29 3. 70* . 2.058E+OO 1.166E+OO l.166E+OO 327.90 OK 92.59 4.23 4.733E+OO 3.299E+OO 3.299E+OO 53.76 OK U-234 609.32 45.49* 2.179E+OO 7.334E-01 7.334E-01 25.80 OK 1120.29 14.92 1.350E+OO 1.149E+OO 1.149E+OO 39.59 OK 1764.49 15.30 9.121E-01 1.079E+OO 1.079E+OO 45.69 OK U-235 89. 96 3.47 4.522E+OO 2.083E+OO 2.083E+OO 49.42 OK 93.35 5.60 4.733E+OO 2.492E+OO 2.492E+00 53.76 OK 143.76 10. 96* 5.929E+OO Line Not Found Absent 163.33 5.08 5.762E+OO Line Not Found Absent 185.72 57.20 5.452E+OO 1.120E-01 1.120E-01 78.16 OK 205.31 5.01 5.147E+OO Line Not Found Absent U-238 63.29 3.70* 2.058E+OO 1.166E+OO 1. 166E+OO 327.90 OK 92.59 4.23 4.733E+OO 3.299E+OO 3.299E+OO 53.76 OK AM-243 43.53 5.90 2.032E-01 1.471E+Ol l.471E+Ol 180.12 OK 74.66 67.20* 3.186E+OO 2.389E-01 2.390E-01 73.17 OK ANH-511 511. 00 100. 00** 2. 511E+OO 1.177E-01 1.177E-01 62.00 OK Flag: "*" = Keyline Page 3228 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:16:37.62 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l *
  • Acquisition date 3-0CT-2016 08:15:34 Sensitivity : 3.000 *
  • Detector ID GAM12 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 8-DEC-2015 11:29:00 Analyst initials: MXRl *
  • Sample ID G405235016 Sample Quantity 1.6312E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;13
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.303E+Ol 1.394E+OO 3.757E-01 SC-46 4.135E-01 5.510E-01 7.481E-01 BA-137M 7.569E-02 8.424E-02 8.137E-02 CS-137 7. 996E-02 8.900E-02 8. 596E-02 TL-208 3.205E-01 8 .181E-02 5.564E-02 PB-210 8.802E+OO 1.399E+Ol 1.482E+Ol PB-212 1.093E+OO 1.382E-01 9.363E-02 BI-214 7.336E-01 1.855E-01 1.137E-01 PB-214 1.018E+OO 2.004E-01 1.354E-01 RN-222 7.336E-01 1.855E-01 l.137E-01 RA-224 1.332E+OO 1.756E+OO 1.003E+OO RA-226 7.336E-01 1.855E-01 1.137E-01 AC-228 8.986E-01 2.943E-01 l.842E-01 RA-228 8.986E-01 2.943E-01 1.842E-01 TH-228 1.093E+OO 1.382E-01 9.363E-02 TH-230 7.334E-01 1.855E-01 1.136E-01 TH-232 8.986E-01 2.943E-01 1.842E-01 TH-234 1.166E+OO 3.747E+OO 3. 551E+OO U-234 7.334E-01 1.855E-01 1.136E-01 U-235 4.023E-02 1.760E-01 3.561E-01 U-238 1.166E+OO 3.747E+OO 3. 551E+OO AM-243 2.390E-01 1. 713E-01 1.220E-01 ANH-511 1.177E-01 7.154E-02 4.450E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -5.074E-01 1. 2 69E+Ol 2.412E+Ol NOT IDENT. NA-22 3.326E-02 4.387E-02 9.885E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 -1.662E-02 2.829E-02 4.921E-02 NOT IDENT. V-48 O.OOOE+OO l.393E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.755E+02 O.OOOE+OO SHORT HLIF MN-54 1. 791E-02 5.843E-02 1.232E-01 NOT IDENT. Page 3229 of 5809 C0-56 1. 676E-01 4.422E-01 9.416E-01 FAIL ABUN MN-56 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.561E-02 4.717E-02 9.092E-02 NOT IDENT. C0-58 -1.599E-01 4.577E-01 8.989E-01 NOT IDENT. FE-59 3.785E+00 5.186E+OO 1.151E+Ol NOT IDENT. C0-60 l.572E-02 3.574E-02 7.896E-02 NOT IDENT. ZN-65 -3.473E-02 l.851E-01 3.122E-01 NOT IDENT. GE-68 l.709E-01 2.145E+OO 4.394E+OO NOT IDENT. AS-73 -9.140E+OO 1.748E+Ol 3.136E+Ol NOT IDENT. AS-74 .O. OOOE+OO 6 .114E+03 O.OOOE+OO SHORT HLIF SE-75 -l.278E-02 1.970E-01 3.815E-01 NOT IDENT. BR-77 O.OOOE+OO 2.513E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.420E+02 O.OOOE+OO SHORT HLIF RB-83 2.473E-01 7.246E-01 1.428E+OO NOT IDENT. KR-85 7.898E+OO 6.575E+OO 1.362E+Ol NOT IDENT. SR-85 8.337E-01 6.948E-01 l.439E+OO NOT IDENT. RB-86 O.OOOE+OO 2. 513E+04 O.OOOE+OO SHORT HLIF Y-88 -1.189E-01 l.346E-01 1.009E-01 NOT IDENT. Y-91 l.635E+02 5.205E+02 1.077E+03 NOT IDENT. NB-94 1.764E-02 3.342E-02 6.702E-02 NOT IDENT. NB-95 -2.185E-03 8.650E-01 1.727E+OO NOT IDENT. NB-95M -1.185E+OO 2.737E+OO 4.532E+OO NOT IDENT. ZR-95 -4.0lOE-01 1.203E+OO 2.179E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 .O.OOOE+OO 6.034E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 711E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.426E+41 O.OOOE+OO SHORT HLIF RH-101 -2.472E-02 3.403E-02 6.454E-02 NOT IDENT. RH-102 4.147E-03 6.179E-02 1.181E-01 NOT IDENT. RU-103 7.210E-01 5.736E+OO 1.115E+Ol FAIL ABUN RH-106 -4. 231E-04 5 .113E-01 9.706E-01 NOT IDENT. RU-106 -4. 231E-04 5 .113E-01 9.706E-01 NOT IDENT. AG-108M 1.970E-02 3.860E-02 5.205E-02 FAIL ABUN CD-109 l.789E+00 2.751E+00 2.923E+OO FAIL ABUN AG-llOM 6.783E-03 l.103E-01 1.991E-01 NOT IDENT. SN-113 -9.909E-02 2.278E-01 4.167E-01 NOT IDENT. CD-115 O.OOOE+OO 3 .111E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1.682E+05 O.OOOE+OO SHORT HLIF TE-123M -3.086E-02 1.478E-01 2.567E-01 NOT IDENT. SB-124 -8.270E-01 2.224E+OO 4.163E+OO NOT IDENT. SB-125 5. 811E-02 1.160E-01 2.134E-01 FAIL ABUN TE-125M l.391E+02 2.888E+o2 5. 969E+02 NOT IDENT. I-126 O.OOOE+OO l.205E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.273E+06 O.OOOE+OO SHORT HLIF SN-126 l.140E-01 1.753E-01 1.916E-01 FAIL ABUN SB-127 O.OOOE+OO 2.169E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.777E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF TE-132 O.OOOE+OO 3.871E+26 O.OOOE+OO SHORT HLIF BA-133 1.772E-02 4.090E-02 7. 551E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 1. 063E-01 6. 721E-02 1.082E-01 FAIL ABUN CS-135 8. OllE-02 1.432E-01 2.662E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.416E+05 O.OOOE+OO SHORT HLIF CE-139 8.136E-03 1.051E-01 2.085E-01 NOT IDENT. BA-140 O.OOOE+OO 1.186E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.593E+05 O.OOOE+OO SHORT HLIF CE-141 -1.706E+Ol 2.422E+Ol 4.565E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.559E+40 O.OOOE+OO SHORT HLIF CE-144 8.743E-02 3.465E-01 7. 021E-01 NOT IDENT. PM-144 2.444E-03 4.852E-02 9.377E-02 NOT IDENT. PR-144 -6.480E-01 4.365E+00 8.130E+OO NOT IDENT. PM-146 -9. 711E-03 3.995E-02 7.109E-02 NOT IDENT. ND-147 O.OOOE+OO 3.585E+07 O.OOOE+OO SHORT HLIF PM-147 -2.014E+02 8.307E+02 l.635E+03 NOT IDENT. PM-149 O.OOOE+OO 4.587E+40 O.OOOE+OO SHORT HLIF EU-150 2.263E-02 2.525E-02 4.915E-02 FAIL ABUN EU-152 -4.763E-03 9.819E-02 1.874E-01 NOT IDENT. GD-153 3.764E-02 l.940E-01 3.607E-01 NOT IDENT. EU-154 7.458E-02 l.061E-01 2.380E-01 FAIL ABUN EU-155 1.808E-02 1.089E-01 2.221E-01 FAIL ABUN TB-160 -1.413E+OO 1.475E+OO 2.526E+OO FAIL ABUN H0-166M 2.079E-02 5.761E-02 l.144E-01 FAIL ABUN TM-171 -3.003E+Ol 4.271E+Ol 7.545E+Ol NOT IDENT. HF-172 -9.750E-02 2.359E-01 4.575E-01 NOT IDENT. LU-172 7.676E-02 5.341E-02 1.409E-01 FAIL ABUN LU-176 -6.849E-03 2.260E-02 4.256E-02 FAIL ABUN Page 3230 of 5809 HF-181 -2.950E+OO 4.400E+OO 7.685E+OO NOT IDENT. TA-182 3.397E-02 8.497E-01 1. 701E+OO FAIL ABUN RE-183 -3.033E+00 5.074E+OO 8.999E+OO NOT IDENT. RE-184 -9. 960E+00 2.832E+Ol 5. 441E+Ol NOT IDENT. W-188 1. 869E+Ol 1.254E+02 2.204E+02 FAIL ABUN IR-192 -2.217E-01 4.445E-01 7.900E-01 FAIL ABUN HG-203 -5.593E-01 2.547E+OO 4.813E+OO NOT IDENT. BI-207 -1.14 7E-02 4.946E-02 9.508E-02 FAIL ABUN BI-211 O.OOOE+OO 5.521E-01 8.615E-01 FAIL ABUN PB-211 7.166E-01 6.909E-01 l.458E+OO NOT IDENT. BI-212 O.OOOE+OO 1.137E+OO 1.394E+OO FAIL ABUN RN-219 -2.873E-01 4.540E-01 7.021E-01 FAIL ABUN RA-223 1.044E-01 5.387E-01 1.066E+00 FAIL ABUN AC-227 1.571E-01 2.269E-01 4.306E-01 NOT IDENT. TH-227 1.571E-01 2.269E-01 4.306E-01 NOT IDENT. TH-229 4.188E-01 4.920E-01 1. OllE+OO FAIL ABUN PA-231 -2.591E-01 4 .113E-01 7.474E-01 NOT IDENT. TH-231 1.044E-01 5.387E-01 l.066E+OO FAIL ABUN PA-233 -2.076E-02 5. 396E-02 l.008E-01 NOT IDENT. PA-234 -4. 241E-03 l.812E-01 3.856E-01 FAIL ABUN PA-234M -6.112E-01 3.785E+OO 7.418E+OO NOT IDENT. NP-237 -2.076E-02 5.396E-02 1.008E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 3.730E-02 2.438E-01 4.938E-01 NOT IDENT. PU-239 1. 282E+02 3 .112E+02 6.352E+02 NOT IDENT. AM-241 -8.076E-02 2.236E-01 4.049E-01 NOT IDENT. CM-243 -6.819E-02 9.733E-02 1.873E-01 NOT IDENT. BK-247 1.640E-02 6.957E-02 1.328E-01 NOT IDENT. CM-247 1.891E-02 3.598E-02 6. 701E-02 NOT IDENT. CF-249 4.479E-02 3.711E-02 8.006E-02 NOT IDENT. CF-251 7. 996E-02 l.141E-01 2.346E-01 NOT IDENT. Page 3231 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:16:34.41 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 327 10.66* 1.082E+OO 1.303E+Ol 1.303E+Ol 10.91 SC-46 889.28 12 99.98* 1.620E+OO 3.460E-02 4.135E-01 135.97 1120. 55 50 99.99 1.350E+OO 1. 715E-01 2.049E+OO 39.59 CD-109 88.03 39 3.70* 4.297E+OO 1.140E+OO 1. 789E+OO 156.88 SN-126 64.28 19 9.60 2.058E+OO 4.494E-01 4.494E-01 327.90 86. 94 39 8.90 4.297E+OO 4.741E-01 4.741E-01 156.88 87.57 39 37.00* 4.297E+OO 1.140E-01 1.140E-01 156.88 BA-137M 661.66 30 89.90* 2.040E+OO 7.427E-02 7.569E-02 113. 58 CS-137 661.66 30 85.10* 2.040E+OO 7.846E-02 7. 996E-02 113. 58 TL-208 277.37 ------6.60 4.142E+OO ------Line Not Found ------583.19 134 85.00* 2.256E+OO 3.205E-01 3.205E-01 26.05 860.56 ------12.50 1.662E+OO ------Line Not Found ------PB-210 46.54 25 4.25* 3.130E-01 8.579E+OO 8.802E+00 162.16 BI-211 72.87 ------1.23 2. 964E+OO ------Line Not Found ------351. 06 269 12.92* 3.413E+OO 2.803E+OO 2.803E+OO 20.10 PB-212 74.82 162 10.28 3.186E+OO 2.282E+00 2.282E+OO 49.58 77 .11 199 17.10 3.414E+00 1.571E+OO 1. 571E+OO 32.23 238.63 481 43.60* 4.646E+OO 1.093E+OO 1.093E+OO 12.91 300.09 ------3.30 3.888E+OO ------Line Not Found ------BI-214 609.32 158 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 1120.29 50 14.92 1.350E+OO 1.149E+OO 1.149E+00 39.59 1764.49 33 15.30 9.121E-01 1.079E+OO 1.079E+OO 45.69 PB-214 74.82 162 5.80 3.186E+OO 4.045E+OO 4.046E+OO 49.58 77 .11 199 9.70 3.414E+OO 2.769E+00 2.770E+00 32.23 87.09 39 3.41 4.297E+00 1.237E+OO 1.238E+OO 156. 8 8 242.00 147 7.25 4.604E+OO 2. 031E+OO 2.031E+OO 47.85 295.22 201 18.42 3.942E+OO 1.277E+OO 1.278E+OO 22.57 351. 93 269 35.60* 3.413E+00 1. 017E+OO 1.018E+OO 20.10 RN-222 609.32 158 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 1120.29 50 14.92 1.350E+OO 1.149E+OO 1.149E+OO 39.59 1764.49 33 15.30 9 .121E-01 1.079E+OO 1.079E+OO 45.69 RA-224 240.99 147 4.10* 4.604E+OO 3.591E+OO 3.591E+OO 47.85 RA-226 609.32 158 45.49* 2.179E+OO 7.334E-01 7.336E-01 25.80 1120.29 50 14.92 1.350E+OO 1.149E+OO 1.149E+00 39.59 1764.49 33 15.30 9.121E-01 1.079E+OO 1.079E+OO 45.69 AC-228 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 88 11. 27 3.524E+00 1. 021E+OO 1.021E+OO 44.67 794.95 26 4. 25 . 1. 768E+OO 1.623E+OO 1.623E+00 64.54 835.71 ------1. 61 1. 701E+OO ------Line Not Found ------911.20 80 25.80* 1.589E+OO 8.986E-01 8.986E-01 33.41 968. 97 67 15.80 1.514E+OO 1.298E+OO 1.298E+OO 40.27 RA-228 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 88 11. 27 3.524E+OO 1.021E+OO 1. 021E+OO 44.67 794.95 26 4.25 1. 768E+OO 1.623E+OO 1.623E+OO 64.54 835. 71 ------1. 61 1.701E+OO ------Line Not Found ------911. 20 80 25.80* 1. 58 9E+OO 8.986E-01 8.986E-01 33.41 968. 97 67 15.80 1.514E+00 1.298E+OO 1.298E+OO 40.27 Page 3232 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235016 Acquisition date 3-0CT-2016 08:15:34 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 162 10.28 3.186E+OO 2.282E+OO 2.282E+OO 49.58 77 .11 199 17.10 3.414E+OO 1. 571E+OO 1. 571E+OO 32.23 238.63 481 43.60* 4.646E+OO l.093E+OO l.093E+OO 12.91 300.09 ------3.30 3.888E+OO ------Line Not Found ------TH-230 609.32 158 45.49* 2.179E+OO 7.334E-01 7.334E-01 25.80 1120. 29 50 14.92 l.350E+OO l.149E+OO l.149E+OO 39.59 1764.49 33 15.30 9 .121E-Ol 1. 079E+OO l.079E+OO 45.69 TH-232 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 88 11. 27 3.524E+OO l.021E+OO 1. 021E+OO 44.67 835. 71 ------1. 61 1. 701E+OO ------Line Not Found ------911. 20 80 25.80* 1. 589E+OO 8.986E-01 8.986E-01 33.41 968. 97 67 15.80 l.514E+OO 1.298E+OO l.298E+OO 40.27 TH-234 63.29 19 3.70* 2.058E+OO l.166E+OO l.166E+OO 327.90 92.59 144 4.23 4.733E+OO 3.299E+OO 3.299E+OO 53.76 U-234 609.32 158 45.49* 2.179E+OO 7.334E-01 7.334E-01 25.80 1120.29 50 14.92 l.350E+OO l.149E+OO l.149E+OO 39.59 1764.49 33 15.30 9 .121E-01 1. 079E+OO l.079E+OO 45.69 U-235 89. 96 71 3.47 4.522E+OO 2.083E+OO 2.083E+OO 49.42 93.35 144 5.60 4.733E+OO 2.492E+OO 2.492E+OO 53.76 143.76 ------10.96* 5.929E+OO ------Line Not Found ------163.33 ------5.08 5.762E+OO ------Line Not Found ------185. 72 76 57.20 5.452E+OO l.120E-01 l.120E-01 78.16 205.31 ------5.01 5.147E+OO ------Line Not Found ------U-238 63.29 19 3.70* 2.058E+OO 1.166E+OO 1.166E+OO 327.90 92.59 144 4.23 4.733E+OO 3.299E+OO 3.299E+OO 53. 76 AM-243 43.53 38 5.90 2.032E-01 l.471E+Ol 1. 471E+Ol 180.12 74.66 162 67.20* 3.186E+OO 3.491E-01 3. 491E-01 49.58 ANH-511 511. 00 64 100.00* 2. 511E+OO 1. l 77E-01 l.177E-01 62.00 Flag: "*" Key line Page 3233 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235016 Acquisition date 3-0CT-2016 08:15:34 Total number of lines in spectrum 51 Number of unidentified lines 15 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 83.79D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y 1.41E+10Y 1600.00Y l.41E+l0Y 1.41E+10Y 1. 41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 12.0 1. 57 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.303E+Ol 3.460E-02 l.140E+OO 1.140E-01 7.427E-02 7.846E-02 3.205E-01 8.579E+OO 2.803E+OO 1.093E+OO 7.334E-01 1.017E+OO 7.334E-01 3. 591E+OO 7.334E-01 8.986E-01 8.986E-01 l.093E+00 7.334E-01 8.986E-01 1.166E+OO 7.334E-01 1.120E-01 1.166E+OO 3.491E-01 l.177E-01 4.225E+Ol 4.225E+Ol Decay Corr pCi/GRAM 1.303E+Ol 4.135E-01 1.789E+OO l.140E-01 7.569E-02 7. 996E-02 3.205E-01 8.802E+OO 2.803E+OO 1.093E+OO 7.336E-01 1.018E+OO 7.336E-01 3.591E+OO 7.336E-01 8.98'6E-01 8.986E-01 1.093E+OO 7.334E-01 8.986E-01 1.166E+OO 7.334E-01 l.120E-01 1.166E+OO 3.491E-01 l.177E-01 4.350E+Ol 4.350E+Ol 70.59% Decay Corr 2-Sigma Error 0.142E+Ol 5.622E-01 2.807E+OO 1. 789E-01 8. 596E-02 9.081E-02 0.835E-01 14.27E+OO 0.563E+OO 0 .141E+OO l.893E-01 0.205E+OO 1. 8 93E-01 1.718E+OO 1. 8 93E-01 3.003E-01 3.003E-01 0 .141E+OO 1.892E-01 3.003E-01 3.824E+OO 1. 892E-01 0.876E-01 3.824E+OO 1. 731E-01 0.730E-01 "M" Manually accepted 2-Sigma %Error 10.91 135.97 156.88 156.88 113. 58 113. 58 26.05 162.16 20.10 12.91 25.80 20.10 25.80 47.85 25.80 33.41 33.41 12.91 25.80 33.41 327. 90 25.80 78.16 327.90 49.58 62.00 Flags: "K" Keyline not found "E" = Manually eBited "A" = Nuclide specific abn. limit Page 3234 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235016 Acquisition date : 3-0CT-2016 08:15:34 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 9 35.91 44 11 1.15 71. 66 68 25 8.49E-03 87.0 2.40E-02 9 37.68 72 58 1. 86 75.20 68 25 l.39E-02 82.7 4. 91E-02 9 40.14 103 111 1. 78 80 .11 68 25 2.00E-02 56.4 l.06E-01 0 154.32 39 82 1. 34 308.48 306 6 8. 54E-03 91. 3 5.86E+OO T 0 157.46 29 115 1. 37 314.75 312 8 6.48E-03 **** 5.83E+OO T 0 209.26 35 110 0.89 418.35 415 8 7.98E-03 **** 5.09E+OO 0 258.15 16 74 1. 41 516.13 512 9 3.62E-03 **** 4.38E+OO 0 271.20 38 133 0.80 542.23 536 14 8.80E-03 **** 4.22E+OO T 0 408.91 30 110 5.41 817.70 805 19 7.34E-03 **** 3. OlE+OO 0 432.57 11 35 1. 27 865. 05 8 61 8 2.74E-03 **** 2.87E+OO T 2 443.52 22 8 1. 28 886.95 885 17 5.51E-03 56.2 2.82E+OO 2 446.21 27 30 1. 74 892.32 885 17 6.65E-03 91.8 2.80E+OO 0 462.58 32 51 3.05 925.07 918 14 8.03E-03 **** 2.72E+OO T 0 491. 73 16 19 1. 73 983.40 979 7 3.94E-03 **** 2.59E+OO T 0 569.42 43 65 0.81 1138.82 1132 16 1.lOE-02 93.2 2.30E+OO T 0 727. 24 49 38 1. 52 1454.59 1448 16 1.27E-02 65.7 l.90E+OO T 0 862.42 4i 31 4.43 1725.08 1717 19 l.08E-02 73.4 1. 66E+00 0 996 .16 12 2 1. 63 1992.73 1989 7 3.14E-03 70.9 1.48E+OO T 0 1104.74 15 21 0.53 2210.06 2202 16 4.07E-03 **** 1.37E+OO 0 1161.46 12 0 1. 60 2323.58 2320 7 3.33E-03 57.7 1.31E+00 0 1181. 87 11 27 3.93 2364.44 2352 19 2.97E-03 **** 1.29E+OO 0 1187. 67 16 '5 2.39 2376.05 2372 9 4.46E-03 69.5 1.29E+OO T 0 1194.48 20 2 3.89 2389.67 2385 11 5.49E-03 55.0 1.28E+OO 0 1239.76 31 7 3.90 2480.31 2473 14 8.73E-03 50.3 1.24E+OO T 0 1247.01 20 6 2 .11 2494.83 2488 13 5.69E-03 67.7 1.24E+OO 0 2042.49 5 5 0.51 4087.70 4081 10 1.39E-03 **** 7.90E-01 Flags: "T" = Tentatively associated Page 3235 or'5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:16:51.97 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l *
  • Acquisition date 3-0CT-2016 08:15:34 Sensitivity : 3.000 *
  • Detector ID GAM12 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 8-DEC-2015 11:29:00 Nuclide Library : SOLID *
  • Sample ID G405235016 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.6312E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;13
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.333E-01 3.270E-01 3.712E-02 3.921E-02 2.445E-02 6.990E+OO 4.355E-02 5.033E-02 6.229E-02 5.033E-02 4.667E-01 5.033E-02 7.656E-02 7.656E-02 4.355E-02 5.032E-02 7.656E-02 1.679E+OO 5.032E-02 l.678E-01 1.679E+OO 5.778E-02 1.967E-02 ----Non-Identified Nu6lides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 Page 3236 of 5809 Le (pCi/GRAM' l.089E+Ol 4.296E-02 O.OOOE+OO 1. 757E-02 O.OOOE+OO O.OOOE+OO 5.428E-02 4.148E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3237 of 5809 O.OOOE+OO 4.257E-02 3.800E-01 4.882E+OO 3.348E-02 l.344E-01 1.893E+OO 1. 4 72E+Ol O.OOOE+OO 1.760E-01 O.OOOE+OO O.OOOE+OO 6.490E-01 6.181E+OO 6.531E-Ol O.OOOE+OO O.OOOE+OO 4.719E+02 3.021E-02 7.729E-01 2.120E+OO 9.246E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.028E-02 5.275E-02 5.023E+OO 4.324E-01 4.324E-01 2.352E-02 1. 396E+OO 8. 716E-02 1. 887E-01 O.OOOE+OO O.OOOE+OO 1.205E-01 1.644E+OO 9.747E-02 2.816E+02 O.OOOE+OO O.OOOE+OO 9.158E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.446E-02 O.OOOE+OO 4.854E-02 1.234E-01 O.OOOE+OO 0.000E+OO 9.768E-02 O.OOOE+OO O.OOOE+OO 2.143E+Ol O.OOOE+OO 3.299E-01 4.105E-02 3.558E+OO 3.153E-02 O.OOOE+OO 7.674E+02 O.OOOE+OO 2.263E-02 8.631E-02 1.693E-01 1.032E-01 1.043E-01 1.033E+OO 5.106E-02 3.537E+Ol 2.150E-01 6.052E-02 1.944E-02 3.429E+OO SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3238 of 5809 7.361E-01 4.214E+00 2.349E+Ol 1.021E+02 3.594E-01 2.237E+OO 4.139E-02 4.161E-01 6.722E-01 6.466E-01 3.187E-01 4.883E-01 l.995E-01 l.995E-01 4.774E-01 3.420E-01 4.883E-01 4.586E-02 l.584E-01 3 .196E+00 4.586E-02 O.OOOE+OO 2.321E-01 2. 996E+02 1. 899E-01 8.741E-02 6.126E-02 3.054E-02 3.689E-02 1.104E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:16:58.06 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235016.CNF;l * *Acquisition date 3-0CT-2016 08:15:34 Sensitivity : 3.000 *
  • Detector ID GAM12 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio ***** *
  • Sample date 8-DEC-2015 11:29:00 Nuclide Library : SOLID *
  • Sample ID G405235016 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity 1.6312E+02 GRAM *
  • Quantity Err(%) 1.2261E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000. * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN '*
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;l3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.303E+Ol 1.552E+OO 1.552E+OO SC-46 4.135E-01 5.513E-01 5.513E-01 BA-137M 7.569E-02 8.431E-02 8. 431E-02 CS-137 7. 996E-02 8.906E-02 8.906E-02 TL-208 3.205E-01 8.295E-02 8.295E-02 PB-210 8.802E+OO 1.404E+Ol 1. 404E+Ol PB-212 1.093E+OO l.503E-01 l.503E-01 BI-214 7.336E-01 l.882E-01 l.882E-01 PB-214 1.018E+OO 2.050E-01 2.050E-01 RN-222 7.336E-01 1.882E-01 1. 882E-01 RA-224 1.332E+OO 1.764E+OO 1. 764E+OO RA-226 7.336E-01 l.882E-01 1. 882E-01 AC-228 8.986E-01 2.979E-01 2.979E-01 RA-228 8.986E-01 2.979E-01 2.979E-01 TH-228 1.093E+OO l.503E-01 l.503E-01 TH-230 7.334E-01 1.881E-01 1.881E-01 TH-232 8.986E-01 2.979E-01 2.979E-01 TH-234 1.166E+OO 3.756E+OO 3.756E+OO U-234 7.334E-01 1. 8 81E-01 l.881E-01 U-235 4.023E-02 l.760E-01 1. 760E-01 U-238 1.166E+OO 3.756E+OO 3.756E+OO AM-243 2.390E-01 1. 726E-01 1. 726E-01 ANH-511 1.177E-01 7.170E-02 7.170E-02 Non-Identified Nuclides Key-Line K.L Act error Activity TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -5.074E-01 l.269E+Ol 1. 2 69E+Ol NOT IDENT. NA-22 3.326E-02 4.388E-02 4.637E-02 NOT IDENT. NA-24 l.OOOE+41 4.275E+41 O.OOOE+OO SHORT HLIF AL-26 -1.662E-02 2.831E-02 2.929E-02 NOT IDENT. V-48 -7.597E+03 l.393E+04 1.435E+04 SHORT HLIF CR-51 4.549E+01 3.755E+02 3.761E+02 SHORT HLIF MN-54 1. 791E-02 5.844E-02 5.899E-02 NOT IDENT. Page 3239 of 5809 C0-56 1. 676E-01 4.423E-01 4.487E-01 FAIL ABUN MN-56 l.OOOE+41 2.640E+41 0.000E+OO SHORT HLIF C0-57 -2.561E-02 4.718E-02 4.857E-02 NOT IDENT. C0-58 -l.599E-01 4.578E-01 4.634E-01 NOT IDENT. FE-59 3.785E+OO 5.193E+OO 5.466E+OO NOT IDENT. C0-60 1. 572E-02 3.575E-02 3.644E-02 NOT IDENT. ZN-65 -3.473E-02 l.851E-01 l.857E-01 NOT IDENT. GE-68 1. 709E-01 2.145E+OO 2.146E+OO NOT IDENT. AS-73 -9.140E+OO 1. 758E+Ol l.806E+Ol NOT IDENT. AS-74 -8. 60.7E+02 6 .115E+03 6.127E+03 SHORT HLIF SE-75 -l.278E-02 l.971E-01 l.971E-01 NOT IDENT. BR-77 l.987E+38 1. 720E+39 O.OOOE+OO SHORT HLIF SR-82 1.105E+02 6.420E+02 6.439E+02 SHORT HLIF RB-83 2.473E-01 7.254E-01 7.339E-01 NOT IDENT. KR-85 7.898E+OO 6.583E+OO 7.484E+OO NOT IDENT. SR-85 8.337E-01 6.957E-01 7.907E-01 NOT IDENT. RB-86 3.294E+03 2.513E+04 2.517E+04 SHORT HLIF Y-88 -l.189E-01 1.348E-01 l.451E-01 NOT IDENT. Y-91 l.635E+02 5.205E+02 5.257E+02 NOT IDENT. NB-94 l.764E-02 3.343E-02 3.436E-02 NOT IDENT. NB-95 -2.185E-03 8.650E-01 8.650E-01 NOT IDENT. NB-95M -l.185E+OO 2.739E+OO 2.791E+OO NOT IDENT. ZR-95 -4.0lOE-01 l.203E+OO l.216E+OO NOT IDENT. NB-97 l.OOOE+41 3.541E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 6.048E+40 O.OOOE+OO SHORT HLIF M0-99 8.346E+31 1. 712E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 l.430E+41 O.OOOE+OO SHORT HLIF RH-101 -2.472E-02 3.432E_:02 3.609E-02 NOT IDENT. RH-102 4.147E-03 6.179E-02 6.182E-02 NOT IDENT. RU-103 7. 210E-01 , 5.736E+OO 5.745E+OO FAIL ABUN RH-106 -4.231E-04 5 .113E-01 5 .113E-01 NOT IDENT. RU-106 -4.231E-04 5 .113E-01 5 .113E-01 NOT IDENT. AG-108M l.970E-02 3.860E-02 3. 961E-02 FAIL ABUN CD-109 1. 789E+OO 2.755E+OO 2.870E+OO FAIL ABUN AG-llOM 6.783E-03 l.103E-01 l.103E-01 NOT IDENT. SN-113 -9.909E-02 2.279E-01 2.322E-01 NOT IDENT. CD-115 2.004E+39 3 .132E+39 O.OOOE+OO SHORT HLIF SN-ll 7M l.166E+05 l.688E+05 l.768E+05 SHORT HLIF TE-123M -3.086E-02 l.478E-01 l.485E-01 NOT IDENT. SB-124 -8.270E-01 2.224E+OO 2.255E+00 NOT IDENT. SB-125 5. 811E-02 1.160E-01 l.190E-01 FAIL ABUN TE-125M 1. 391E+02 2.889E+02 2.956E+02 NOT IDENT. I-126 2.344E+05 l.205E+06 l.210E+06 SHORT HLIF SB-126 -2.180E+05 l.273E+06 l.277E+06 SHORT HLIF SN-126 l.140E-01 1. 755E-01 l.828E-01 FAIL ABUN SB-127 4.336E+21 2.249E+22 O.OOOE+OO SHORT HLIF I-131 -3.454E+09 4.780E+09 5.027E+09 SHORT HLIF I-132 l.000E+41 1. 911E+42 O.OOOE+OO SHORT HLIF TE-132 -l.587E+25 3.871E+26 O.OOOE+OO SHORT HLIF BA-133 l.772E-02 4.091E-02 4.168E-02 NOT IDENT. I-133 l.OOOE+41 4.029E+41 O.OOOE+OO SHORT HLIF CS-134 l.063E-01 6.737E-02 8.266E-02 FAIL ABUN CS-135 8. OllE-02 l.433E-01 1.478E-01 NOT IDENT. I-135 l.OOOE+41 l.016E+42 O.OOOE+OO SHORT HLIF CS-136 -l.033E+04 2.416E+05 2.417E+05 SHORT HLIF CE-139 8.136E-03 l.051E-01 l.051E-01 NOT IDENT. BA-140 8.733E+05 l.187E+06 l.250E+06 SHORT HLIF LA-140 -2.688E+05 4.595E+05 4.752E+05 SHORT HLIF CE-141 -l.706E+Ol 2.423E+Ol 2.542E+Ol NOT IDENT. CE-143 l.OOOE+41 5.652E+40 O.OOOE+OO SHORT HLIF CE-144 8.743E-02 3.466E-01 3.488E-01 NOT IDENT. PM-144 2.444E-03 4.852E-02 4.853E-02 NOT IDENT. PR-144 -6.480E-01 4.365E+OO 4.375E+OO NOT IDENT. PM-146 -9. 711E-03 3.995E-02 4.019E-02 NOT IDENT. ND-147 7.457E+06 3.585E+07 3. 601E+07 SHORT HLIF PM-147 -2.014E+02 8.307E+02 8.357E+02 NOT IDENT. PM-149 2.545E+38 4.587E+40 O.OOOE+OO SHORT HLIF EU-150 2.263E-02 2.527E-02 2. 725E-02 FAIL ABUN EU-152 -4.763E-03 9.819E-02 9.822E-02 NOT IDENT. GD-153 3.764E-02 l.941E-01 l.948E-01 NOT IDENT. EU-154 7.458E-02 l.061E-01 l .113E-01 FAIL ABUN EU-155 l.808E-02 1. 089E-01 l.092E-01 FAIL ABUN TB-160 -l.413E+OO 1.477E+OO l.609E+OO FAIL ABUN H0-166M 2.079E-02 5.762E-02 5.838E-02 FAIL ABUN TM-171 -3.003E+Ol 4.280E+Ol 4.489E+Ol NOT IDENT. HF-172 -9.750E-02 2.365E-01 2.405E-01 NOT IDENT. LU-172 7.676E-02 5.397E-02 6.411E-02 FAIL ABUN LU-176 -6.849E-03 2.260E-02 2.281E-02 FAIL ABUN Page 3240 of 5809 HF-181 -2.950E+OO 4.402E+OO 4.599E+OO NOT IDENT. TA-182 3.397E-02 8.497E-01 8.498E-01 FAIL ABUN RE-183 -3.033E+00 5.097E+OO 5.277E+OO NOT IDENT. RE-184 -9. 960E+00 2.842E+Ol 2.877E+Ol NOT IDENT. W-188 1. 8 69E+Ol 1.254E+02 1.257E+02 FAIL ABUN IR-192 -2.217E-01 4.446E-01 4.557E-01 FAIL ABUN HG-203 -5.593E-01 2.547E+OO 2.560E+OO NOT IDENT. BI-207 -1.14 7E-02 4.946E-02 4.973E-02 FAIL ABUN BI-211 2.803E+OO 5.666E-01 1.385E+OO FAIL ABUN . PB-211 7.166E-01 6.919E-01 7.636E-01 NOT IDENT. BI-212 1.766E+00 1.140E+OO 1.391E+OO FAIL ABUN RN-219 -2.873E-01 4.555E-01 4.735E-01 FAIL ABUN RA-223 1.044E-01 5.388E-01 5.408E-01 FAIL ABUN AC-227 1. 571E-01 2.279E-01 2.386E-01 NOT IDENT. TH-227 1.571E-01 2.279E-Ol 2.386E-01 NOT IDENT. TH-229 4.188E-01 4.924E-01 5.274E-01 FAIL ABUN PA-231 -2.591E-01 4.150E-01 4.312E-01 NOT IDENT. TH-231 l.044E-01 5.388E-01 5.408E-01 FAIL ABUN PA-233 -2.076E-02 5.397E-02 5.478E-02 NOT IDENT. PA-234 -4.241E-03 l.813E-01 l.813E-01 FAIL ABUN PA-234M -6.112E-01 3.785E+OO 3.795E+OO NOT IDENT. NP-237 -2.076E-02 5.397E-02 5.478E-02 NOT IDENT. NP-238 -l.000E+41 2.160E+41 0.000E+OO SHORT HLIF NP-239 3.730E-02 2.439E-01 2.444E-01 NOT IDENT. PU-239 l.282E+02 3 .113E+02 3.166E+02 NOT IDENT. AM-241 -8.076E-02 2.237E-01 2.267E-01 NOT IDENT. CM-243 -6.819E-02 9.754E-02 l.023E-01 NOT IDENT. BK-247 l.640E-02 6. 965E-02 7.004E-02 NOT IDENT. CM-247 1.891E-02 3.612E-02 3.712E-02 NOT IDENT. CF-249 4.479E-02 3.730E-02 4.241E-02 NOT IDENT. CF-251 7.996E-02 l.145E-01 l.200E-01 NOT IDENT. Page 3241of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 43.8354 87.09 136.4134 136.47 78.0933 45.60 91. 2111 87.57 136.4821 140.51 0.0000 46.54 92.9732 88.03 136.5484 143.76 74.0322 49. 72 0.0000 88.34 82.4707 144.24 82.1883 51. 35 92.4033 88.47 82.4819 145.44 95.8253 51. 87 88.7731 89. 96 82.6099 152.43 64.0735 52.39 91. 3065 1093.63 83.9597 153.25 0.0000 52.97 95.0859 91.11 0.0000 323.87 87.3652 53.44 90.2060 92.59 84.1273 156.02 0.0000 54.07 76.6810 93.35 84.1922 158.56 0.0000 57.36 0.0000 94.56 84.2949 159.00 84.9359 57.53 83.2581 94.65 84.3028 162.33 71.4095 57.98 88.2817 94.67 84.3043 162.66 0.0000 59.27 85.9423 94.87 84.3212 163.33 84.2875 59.32 85.9478 97.43 72. 8314 165.86 71.5912 59.54 85.9728 98.43 68.9972 176.31 69.3436 60. 96 74.8979' 98.44 68.9980 176.60' 0.0000 61.17 83.2428 99.53 72.9813 177.52 68.4762 62.93 88.8544 100 .11 78.2382 181.07 0.0000 63.29 101.8330 102.03 67.9322 181.52 86.2916 63.58 101.8704 103.18 81. 9574 184.41 65.5423 64.28 101. 9606 103.37 81. 9722 143.76 71.6478 66.73 100.5957 105.21 76.8738 193.51 73.8857 67.24 98.1427 105.31 76.8809 197.03 96. 5510 125.81 100.7135 106.12 69.9451 198.01 76.9142 67.75 100.7220 106.47 71. 7171 201.83 84.6231 69.67 94.6472 109.28 80.6731 203.43 63. 0613 70.83 102.3605 111. 00 82.5569 205.31 72.0876 72.81 107.2447 111. 76 0.0000 210.85 73.7542 72.87 107.2525 114. 06 79.2632 215.65 76.8159 74.66 107.4760 116. 30 0.0000 222.11 65.6898 74.82 107.4954 116.74 78.5703 227.09 64.9287 74.97 107.5141 119.76 83.2048 227.38 65.8948 77 .11 107.7770 121.12 84.1890 228.16 0.0000 78.74 109.6757 121.22 83.3100 228.18 64.0148 79.69 112.3452 121. 78 84.2373 116.74 64.0148 80.12 109.8443 122.06 85.1445 235.69 82.0462 80.19 0.0000 122.92 85.2075 235. 96 71. 9818 80.57 108.6209 123.07 88.7690 238.63 59.5958 81. 00 108.6728 265.00 73.7167 238.98 0.0000 81. 07 121.4672 125.81 92.5356 240.99 59.6753 81.75 125.3965 127.23 95.3186 242.00 59.7093 83.79 107. 7211 127.91 90.9166 244.70 44.8501 84.00 107.7455 129.30 82.0982 252.40 0.0000 85.43 107.9108 131. 20 98.3156 252.80 56.1934 86.55 124.7601 133. 02 69.8195 254.15 0.0000 86.79 136.3697 133.52 75.2209 256.23 39.3118 86.94 136.3915 136.00 85.2424 260.90 0.0000 Page 3242 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 48.7539 355.39 0.0000 584.27 17.7370 264.80 47.7828 356.01 29.0410 595.83 0.0000 265.00 43.3016 364.49 0.0000 427.87 22.2843 268.22 42.4964 366.42 0.0000 602.52 0.0000 269.46 49.8555 372.51 25.6571 604.72 31.7958 270.03 49.8701 375.05 33.9037 607.14 26.7949 271.23 49.9022 377.52 28.7970 609.32 20.1094 273.65 0.0000 356.01 36.0923 610.33 20 .1160 276.40 54.4510 388.16 25.8265 614.28 30.2102 277.37 49.4720 388.63 0.0000 618.01 19.0427 277.60 49.4782 391.69 38.2789 620.36 20.1775 278.00 51.0595 264.66 46.7267 621. 93 22.4300 279.20 62.8815 401. 81 45.1904 630.19 0.0000 279.54 69.7707 402.40 26.4971 631. 2 9 22.4927 279.70 69.7765 404.85 29.1239 633.25 20.2559 280.46 62.9219 410.95 34.4086 634.78 0.0000 283.69 46.2848 413.71 31.3153 635.95 28.1555 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 54.2100 423. 72 0.0000 645.85 15.8132 285.90 0.0000 427.09 39.8748 657.76 22.1025 287.50 50.3214 427.87 28.3409 657.90 0.0000 290.67 50. 4013 433.94 37.8765 661. 66 36.3112 293.27 0.0000 439.40 30.3650 664.57 0.0000 351.93 53.4869 453.88 24.1'707 666.33 0.0000 295. 96 53.5067 463.37 31.9159 666.50 0.0000 879.38 35.7173 468.07 33.5694 667.71 0.0000 299.98 29.7852 473.00 0.0000 677.62 21.6587 300.09 29.7864 475.06 25.6421 685.70 0.0000 300.13 29.7870 476.78 34.2109 695.00 0.0000 301.36 50.6690 477.60 29.9431 696. 49 16.0445 302.85 54.6822 482.18 33.2062 696. 51 18.3366 256.23 30.8461 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.1942 306.78 42.8338 497.08 25.8447 697.49 17.1954 308.46 35.8901 505.52 19.4407 702.65 20.6638 311. 90 40.9424 507.63 0.0000 706.68 26.4328 316.51 41.0325 511. 00 19.4777 711. 68 18. 4134 319.41 0.0000 514.00 14.6234 720.70 0.0000 320.08 0.0000 514.00 14.6234 721. 93 0.0000 321. 04 44.1289 520.40 28.2249 722.78 24.2411 323.87 36.1531 520.69 0.0000 722. 91 24.2419 325.23 43.2108 522.65 0.0000 723.31 22.5135 328.76 0.0000 527.90 0.0000 724.19 22.5183 333.37 36.3127 528.26 21.7700 727. 33 17.3370 333.97 28.7551 529.59 26.1357. 733.00 17.3633 334.37 40.8708 529.87 0.0000 735.93 18.5352 338.28 50.5473 531.02 0.0000 333.97 18.5430 338.32 50.5483 537.26 0.0000 739.50 0.0000 311. 90 51.6101 546.56 0.0000 747.24 16.2678 340.48 51.6101 552.55 15.3621 748.06 18.5957 340.55 0.0000 563.25 26.4268 752.31 10.4718 344.28 46.6298 569.33 27.5818 753.82 0.0000 345.93 45.6500 946.00 27.5838 756.73 13.9785 351.06 44.7376 569.70 27.5859 756.80 13.9790 351.93 44.7546 583.19 17.7305 884.68 12.2547 Page 3243 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 24.5214 1274.44 7.4001 1620.50 3.1053 766.42 28.0283 1001.03 11. 6411 1621.92 1.0353 766.84 27.1553 1002.74 12.0423 1678.03 0.0000 772. 60 0.0000 1004.73 13.9009 1690.97 7.3226 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 .1025.87 0.0000 1764.49 2.1146 778.90 19.3326 1028.54 0.0000 1063.66 5.6436 783.70 0.0000 1037.84 9.3329 1771.35 4.2332 785.37 14. 9637 1038.76 0.0000 1791.20 0.0000 792.07 11. 2859 631.29 13.0900 1808.65 5.3195 794.95 12.3530 1048.07 0.0000 1810.72 0.0000 795.86 8.4727 1049.04 8.4194 1836.06 3.2040 810.06 11. 514 6 1050.41 11.2288 810.29 11. 5154 1063.66 17.8287 344.28 13.2875 1077.00 0.0000 810.76 13.2884 1077.34 12.2327 815.77 0.0000 1085.87 12.2542 1048.07 0.0000 1093.63 1. 8882 832.01 11. 5777 1099.45 4.5372 834.85 15.1505 1112. 07 15.1621 835.71 16.9364 1112. 84 15.1641 836.80 0.0000 1115.54 15.1729 846.75 0.0000 1120.29 17.0848 846.77 14. 3013 1120.55 17.085'9 856.80 0.0000 1221.41 17.0892 860.56 17.9364 1129. 67 17.1167 871.09 15.4128 1131. 51 0.0000 873.19 12.5935 1147.95 0.0000 875.33 0.0000 1173.23 7.6729 879.38 15.3144 1177.95 16.8953 880.51 11.7142 1189.05 7.6958 883.24 10.3048 1204.77 13. 5087 884.68 15.8748 1221.41 13.5505 889.28 16.2532 1231. 02 12.6057 894.76 23.1453 1235.36 0.0000 898.04 11.7626 1238.28 6.2141 900.72 19.0127 1260.41 0.0000 903.28 17.2124 1271.87 15.6309 911.20 8.1683 1274.44 7.8193 912.08 8.1700 1274.54 7.8193 923.98 0.0000 1291.59 8.8242 926.50 10.9292 1298.22 0.0000 929 .11 12.7584 1312 .11 0.0000 937.49 21.9133 1332.49 6. 9133 944.13 0.0000 1362.66 0.0000 946.00 7.3186 1365.19 8.9390 949.00 10.9852 1368.63 0.0000 667.71 0.0000 1384.29 3.9861 962.31 22.0356 1408.01 6.0029 964. 08 16.1659 1457.56 0.0000 966.17 23.5250 1460.82 2.0187 911.20 22.9881 1489.16 4.0562 968.97 22.9881 1505.03 11.1826 983.53 0.0000 1584.12 8.2349 984.45 0.0000 1596. 21 0.0000 Page 3244 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:17:28.73 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM16.CNF;440 Background date : Z-OCT-2016 11:00:50. Sample date 2-DEC-2015 10:02:00. Acquisition date : 3-0CT-2016 08:16:00. Sample ID G405235017 Sample quantity 1.48561E+02 GRAM Detector name : GAM16 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.55 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 3 3 1 1 1 0 0 0 0 0 0 6 6 0 0 0 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 Page 3245 of 5809 Energy 43.60 70.29 74.95 77.16 81. 32 87.09 90.10 92.57* 115. 21 144.07* 154.89 186.01* 209.13 228.05 238.69* 241.61 270.50 295.27* 300.49 328.07 338.67 351. 96* 467.98 511.26* 546.79 551.54 562.64 583.38* 609.48* 616.03 646.12 661.74 685.39 728.12* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 27 31 142 234 43 78 40 75 31 29 28 91 44 26 468 154 32 173 54 47 88 277 99 14 22 17 30 139 238 24 28 1437 17 45 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 145 189 189 170 71 205 194 183 183 133 180 207 129 123 91 150 155 117 113 89 118 133 201 104 12 21 30 68 38 37 13 68 23 25 0.86 1.22 1. 32 1. 32 1. 34 1.12 1.12 1.13 1. 66 1. 56 1. 75 1.19 1.18 1. 48 1.11 2.23 1. 06 1.10 3.35 1. 60 1. 00 1. 25 9.84 1.12 1. 71 1. 72 1.29 1. 74 1. 32 3.46 1. 47 1. 64 4. 96 1. 21 87.27 140.62 149.93 154.35 162.66 174.19 180.20 185.16 230.41 288.09 309. 72 371. 93 418.16 455.98 477.25 483.08 540.83 590.35 600.78 655.93 677 .11 703.68 935.63 1022.15 1093.19 1102.69 1124.88 1166. 34 1218.54 1231. 63 1291.80 1323.02 1370.30 1455.74 84 137 137 137 137 170 170 170 225 285 305 367 415 453 472 472 536 585 596 652 671 698 921 1016 1090 1090 1119 1161 1213 1226 1286 1316 1363 1449 7 7.36E-03 78.4 28 8.56E-03 71.5 2.06E+OO 28 3.95E-02 19.5 28 6.49E-02 12.7 28 1.18E-02 33.8 22 2.18E-02 31.6 2.52E+OO 22 1.lOE-02 59.7 22 2.09E-02 34.8 9 8.50E-03 82.3 7 8.0lE-03 70.3 9 7.66E-03 90.1 10 2.51E-02 32.3 7 1.21E-02 46.1 8 7.16E-03 77.0 19 1.30E-01 5.9 1.15E+OO 19 23.7 10 8.89E-03 74.9 12 4.81E-02 14.7 11 1.49E-02 40.8 9 1.32E-02 38.8 10 2.44E-02 25.6 13 7.68E-02 10.6 26 2.76E-02 40.4 13 3.87E-03167.9 16 6.23E-03 33.0 2.19E+OO 16 4.85E-03 46.5 12 8.33E-03 40.8 15 3.85E-02 15.6 13 6.60E-02 8.5 12 6.72E-03 53.8 11 7.79E-03 31.7 16 3.99E-01 2.9 15 4.80E-03 64.6 14 l.25E-02 28.0 Peak Search Report (continued) Page : 2 Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 1 742.92 18 22 1. 88 1485.34 1478 19 4.90E-03 60.0 4.56E+OO 36 1 745.25 23 24 1. 71 1490.00 1478 19 6.48E-03 42.3 37 0 768.89 15 32 1. 42 1537.26 1533 11 4.28E-03 74.1 38 0 782.30 8 10 1. 50 1564.08 1560 7 2.28E-03 73.4 39 0 785.92 14 14 0.68 1571.31 1567 9 3.93E-03 54.0 40 0 911. 42* 75 33 1. 34 1822.26 1816 14 2.08E-02 20.7 41 0 969.24* 63 13 1. 42 1937.87 1932 12 1.75E-02 17.8 42 0 1002.46 13 20 0.66 2004.30 1996 17 3.49E-03 88.4 43 0 1008.37 17 6 2.90 2016.12 2012 9 4.62E-03 37.2 44 0 1072. 24 12 8 2.30 2143.83 2139 8 3.39E-03 49.2 45 0 1110.46 10 17 1. 09 2220.28 2209 14 2.67E-03 97.7 46 0 1120.27 50 5 1. 62 2239.89 2235 10 l.40E-02 16.3 47 0 1221. 91 13 9 2.28 2443.16 2438 9 3.47E-03 51. 4 48 0 1411. 82 10 7 3.55 2822.96 2816 11 2.69E-03 65.1 49 0 1460.83* 424 7 2.42 2920.98 2914 14 1.18E-01 5.1 50 0 1588.32 9 2 1.11 3175.98 3172 8 2.56E-03 42.0 51 0 1593.67* 3 0 0.73 3186.67 3183 8 7.84E-04 99.9 52 0 1764.55 26 9 1. 64 3528.46 3522 12 7.24E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 3246 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:17:31 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 2-DEC-2015 10:02:00 G405235017 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:16:00 148.56 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA16 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3247 of 5809 PB-214 U-235 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 143.76 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 CE-141 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 145.44 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.55 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.215E+OO 1. 595E+Ol 1.595E+Ol 10.13 OK CD-109 88.03 3.70* 5.400E+OO 1.377E+OO 2.181E+OO 116. 66 OK SN-126 64.28 9.60 3.017E+OO Line Not Found Absent 86.94 8.90 5.400E+OO 5.725E-01 5. 725E-01 116. 66 OK 87.57 37.00* 5.400E+OO l.377E-01 l.377E-01 116. 66 OK BA-137M 661.66 89.90* 2.305E+OO 3.661E+OO 3.733E+OO 5.89 OK CS-137 661.66 85.10* 2.305E+OO 3.868E+OO 3.943E+OO 5.89 OK CE-141 145.44 48.29* 6.768E+OO 1. 517E-02 1.032E+Ol 517.35 OK TL-208 277.37 6.60 4.683E+OO Line Not Found Absent 583.19 85.00* 2.549E+OO 3.420E-01 3.420E-01 31.12 OK 860.56 12.50 l.874E+00 Line Not Found Absent BI-212 727. 33 6.67* 2.137E+OO 1.646E+OO 1. 646E+00 56.05 OK 785.37 1.10 2.013E+OO 3.316E+OO 3.316E+OO 108.05 OK 1620.50 1. 47 1.107E+OO Line Not Found Absent PB-212 74.82 10.28 4.288E+OO 1.388E+OO 1. 388E+OO 59.83 OK 77 .11 17.10 4.519E+OO 1.931E+OO 1. 931E+OO 25.39 OK 238.63 43.60* 5. 251E+OO 1.186E+OO 1.186E+OO 11. 79 OK 300.09 3.30 4.392E+OO 2.101E+OO 2 .101E+OO 81. 58 OK BI-214 609.32 45.49* 2.461E+OO 1.129E+00 1.130E+o*o 17.06 OK 1120. 29 14.92 1.519E+OO 1.112E+OO l .113E+OO 32.64 OK 1764.49 15.30 1.023E+OO 7.948E-01 7.951E-01 60.44 OK PB-214 74.82 5.80 4.274E+OO Line Not Found <<INT Reject 77 .11 9.70 4.519E+OO 3.404E+OO 3.406E+OO 25.39 OK 87.09 3.41 5.400E+OO Line Not Found <<INT Reject 242.00 7.25 5.198E+OO Line Not Found <<INT Reject 295.22 18.42 4.455E+OO 1.203E+OO 1.203E+OO 29. 37 OK 351. 93 35.60* 3.858E+OO 1.129E+OO 1.129E+OO 21.10 OK RN-222 609.32 45.49* 2.461E+OO l.129E+OO 1.130E+OO 17.06 OK 1120.29 14.92 1.519E+OO 1.112E+OO 1.113E+OO 32.64 OK 1764.49 15.30 1.023E+OO 7.948E-01 7.951E-01 60.44 OK RA-224 240.99 4.10* 5.204E+OO 2.048E+OO 2.048E+OO 101.21 OK RA-226 609.32 45.49* 2.461E+OO 1.129E+OO l .130E+OO 17.06 OK 1120.29 14.92 l.519E+OO l .112E+OO l .113E+00 32.64 OK 1764.49 15.30 l.023E+OO 7.948E-01 7.951E-01 60.44 OK AC-228 105.21 1.10 6.393E+OO Line Not Found Absent 338.32 11.27 3.983E+OO l.lOOE+OO l.lOOE+OO 51. 24 OK 794.95 4.25 l.995E+OO Line Not Found Absent 835. 71 1. 61 l.918E+OO Line Not Found Absent 911.20 25.80* l.791E+OO 8.287E-01 8.287E-01 41. 38 OK 968. 97 15.80 l.706E+00 l.188E+OO l.188E+OO 35.66 OK RA-228 105.21 1.10 6.393E+OO Line Not Found Absent 338.32 11.27 3.983E+OO l.lOOE+OO 1.lOOE+OO 51. 24 OK 794.95 4.25 l.995E+OO Line Not Found Absent 835.71 1. 61 l.918E+00 Line Not Found Absent 911. 20 25.80* 1. 791E+OO 8.287E-01 8.287E-01 41. 38 OK 968. 97 15.80 1. 706E+00 l.188E+OO 1.188E+OO 35.66 OK TH-228 74.82 10.28 4.288E+OO l.388E+OO l.388E+OO 59.83 OK 77 .11 17.10 4.519E+OO l.931E+OO 1. 931E+OO 25.39 OK 238.63 43.60* 5. 251E+OO l.186E+OO 1.186E+OO 11. 79 OK Page 3248 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3 .. 30 4.392E+OO 2. 101E+OO 2.101E+OO 81.58 OK TH-230 609.32 45.49* 2.461E+OO 1.129E+OO 1.129E+OO 17.06 OK 1120.29 14.92 1.519E+OO 1.112E+OO 1.112E+OO 32.64 OK 1764.49 15.30 1.023E+OO 7.948E-01 7.948E-01 60.44 OK PA-231 283.69 1. 70 4.600E+OO Line Not Found Absent 301.36 5.35* 4.392E+OO 1.296E+OO 1.296E+OO 81. 58 OK TH-232 105.21 1.10 6.393E+OO Line Not Found Absent 338.32 11. 27 3.983E+OO 1.lOOE+OO 1.lOOE+OO 51.24 OK 835.71 1. 61 1.918E+OO Line Not Found Absent 911.20 25.80* 1. 791E+OO 8.287E-01 8.287E-01 41. 38 OK 968. 97 15.80 1.706E+OO 1.188E+OO 1.188E+OO 35.66 OK U-234 609.32 45.49* 2.461E+OO l.129E+OO 1.129E+OO 17.06 OK 1120.29 14.92 1.519E+OO 1.112E+OO l .112E+OO 32.64 OK 1764.49 15.30 1.023E+OO 7.948E-01 7.948E-01 60.44 OK U-235 89. 96 3.47 5.617E+OO 1.286E+OO 1.286E+OO 119.50 OK 93.35 5.60 5.779E+OO 1.461E+OO 1. 461E+OO 69.70 OK 143.76 10.96* 6.770E+00 Line Not Found <<INT Reject 163.33 5.08 6. 541E+OO Line Not Found Absent 185.72 57.20 6.164E+OO l.'524E-01 1.524E-01 64.51 OK 205.31 5.01 5.819E+OO Line Not Found Absent AM-243 43.53 5.90 4.061E-01 7.398E+OO 7.398E+OO 156.85 OK 74.66 67.20* 4.288E+OO 2.124E-01 2.124E-01 59.83 OK ANH-511 511. 00 100.00* 2.836E+OO 2.662E-02 2.662E-02 335.79 OK Flag: "*" = Keyline Page 3249 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:17:32.19 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l * *Acquisition date 3-0CT-2016 08:16:00 Sensitivity : 3.000 *
  • Detector ID GAM16 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:02:00 Analyst initials: MXRl *
  • Sample ID G405235017 Sample Quantity 1.4856E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.595E+Ol 1.583E+OO CD-109 2 .181E+OO 2.493E+OO SN-126 1.377E-01 l.575E-01 BA-137M 3.733E+00 2.155E-01 CS-137 3.943E+00 2.277E-01 CE-141 1.032E+Ol 5.234E+Ol TL-208 3.420E-01 l.043E-01 BI-212 1.646E+OO 9.043E-01 PB-212 l.186E+OO 1.370E-01 BI-214 1.130E+OO 1.889E-01 PB-214 1.129E+OO 2.336E-01 RN-222 1.130E+OO 1.889E-01 RA-224 2.048E+OO 2.032E+OO RA-226 1.130E+OO 1.889E-01 AC-228 8.287E-01 3.361E-01 RA-228 8.287E-01 3.361E-01 TH-228 l.186E+OO 1.370E-01 TH-230 1.129E+OO 1.889E-01 PA-231 1.296E+OO 1.036E+OO TH-232 8.287E-01 3. 361E-01 U-234 1.129E+OO 1.888E-01 U-235 2.358E-01 3.250E-01 AM-243 2.124E-01 1.245E-01 ANH-511 2.662E-02 8.759E:-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3250 of 5809 Key-Line Activity (pCi/GRAM -1.574E+Ol 1. 795E-02 O.OOOE+OO -1.312E-02 -l.637E-01 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) l.907E+Ol 4.081E-02 1. 960E+41 2.477E-02 3.600E-01 l.669E+04 MDA (pCi/GRAM 7.018E-01 2.282E+00 l.450E-01 6.780E-02 7.163E-02 5.673E+Ol 7.041E-02 8.373E-01 9.442E-02 1.319E-01 l.450E-01 1.319E-01 l.012E+OO l.319E-01 2.509E-01 2.509E-01 9.442E-02 1.318E-01 9.476E-01 2.509E-01 1. 318E-01 3.932E-01 9.680E-02 6.092E-02 MDA (pCi/GRAM 3.305E+Ol 8.794E-02 O.OOOE+OO 4. 715E-02 6.771E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 5.920E+02 O.OOOE+OO SHORT HLIF MN-54 8.642E-03 5.258E-02 1. 096E-01 NOT IDENT. C0-56 -1. 079E-01 4.273E-01 8.351E-01 NOT IDENT. MN-56 O.OOOE+OO l.747E+41 O.OOOE+OO SHORT HLIF C0-57 -3.425E-02 5.374E-02 9.531E-02 NOT IDENT. C0-58 6.255E-02 5.612E-01 l.152E+OO NOT IDENT. FE-59 2.294E-01 5.868E+OO l.202E+Ol NOT IDENT. C0-60 -1.098E-02 4.174E-02 7.797E-02 NOT IDENT. ZN-65 3.965E-02 2. 081E-01 3.690E-01 NOT IDENT. GE-68 -3.464E-01 2.284E+OO 4.278E+OO NOT IDENT. AS-73 -5.475E+00 1.185E+Ol 2.252E+Ol NOT IDENT. AS-74 O.OOOE+OO 8.525E+03 O.OOOE+OO SHORT HLIF SE-75 5.271E-02 2.377E-01 4.707E-01 NOT IDENT. BR-77 O.OOOE+OO 1.459E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 8.459E+02 O.OOOE+OO SHORT HLIF RB-83 8.200E-02 7.940E-01 1.515E+OO FAIL ABUN KR-85 3.266E+OO 9.035E+OO 1.583E+Ol NOT IDENT. SR-85 3.647E-01 1.018E+OO 1. 782E+OO NOT IDENT. RB-86 O.OOOE+OO 3.267E+04 O.OOOE+OO SHORT HLIF Y-88 2.707E-01 2.425E-01 6.305E-01 NOT IDENT. Y-91 1.368E+02 6.350E+02 l.253E+03 NOT IDENT. NB-94 1.327E-04 3.108E-02 5.836E-02 NOT IDENT. NB-95 -7.649E-01 1.133E+OO 1.614E+OO NOT IDENT. NB-95M -l.446E+OO 3.106E+OO 4.802E+OO NOT IDENT. ZR-95 2.686E-01 1.355E+OO 2.674E+00 NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 8.862E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO ._SHORT HLIF RH-101 -1.537E-02 3.813E-02 6.854E-02 NOT IDENT. RH-102 3.642E-02 6.305E-02 1.274E-01 NOT IDENT. RU-103 -1. 921E+OO 7.841E+OO l.440E+Ol FAIL ABUN RH-106 2.697E-01 5.389E-01 1.043E+OO NOT IDENT. RU-106 2.697E-01 5.389E-01 1.043E+OO NOT IDENT. AG-108M -2.261E-02 3.506E-02 6.250E-02 NOT IDENT. AG-llOM -2.589E-03 9.860E-02 1. 967E-01 NOT IDENT. SN-113 3.590E-02 3.082E-01 5.891E-01 NOT IDENT. CD-115 O.OOOE+OO 2.519E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.593E+05 O.OOOE+OO SHORT HLIF TE-123M 1.244E-01 1. 4 65E-01 2.843E-01 NOT IDENT. SB-124 -4.188E-01 1.241E+OO 2.495E+OO FAIL ABUN SB-125 l.903E-02 1.310E-01 2.506E-01 NOT IDENT. TE-125M l .116E+02 3.124E+02 6.008E+02 NOT IDENT. I-126 O.OOOE+OO 1.154E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.556E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.164E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.013E+10 O.OOOE+OO SHORT HLIF I-132 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.866E+27 O.OOOE+OO SHORT HLIF BA-133 1.839E-02 4.905E-02 8.840E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3.845E-02 5.577E-02 1.123E-01 FAIL ABUN CS-135 -3.516E-02 1. 742E-01 2.998E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.870E+05 0.000E+OO SHORT HLIF CE-139 -8.036E-02 1.274E-01 2.203E-01 NOT IDENT. BA-140 O.OOOE+OO 1.994E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.766E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 9.806E+40 O.OOOE+OO SHORT HLIF CE-144 2.124E-02 4.147E-01 7.664E-01 FAIL ABUN PM-144 5.082E-02 6.697E-02 l.341E-01 NOT IDENT. PR-144 4.357E+OO 5.828E+OO 1.166E+Ol NOT IDENT. PM-146 -1. 414E-02 6.025E-02 l.107E-01 NOT IDENT. ND-147 0.000E+OO 5.686E+07 O.OOOE+OO SHORT HLIF PM-147 -5.660E+Ol 9.040E+02 1.675E+03 NOT IDENT. PM-149 O.OOOE+OO l.497E+41 O.OOOE+OO SHORT HLIF EU-150 -5.178E-03 3.255E-02 5.530E-02 FAIL ABUN EU-152 4.729E-02 l.016E-01 2.032E-01 NOT IDENT. GD-153 4.509E-03 2. 296E-01 3.994E-01 FAIL ABUN EU-154 4.386E-02 9.974E-02 2.149E-01 NOT IDENT. EU-155 8.891E-02 1.167E-01 2.305E-01 FAIL ABUN TB-160 -3.736E-01 l.738E+OO 3.409E+OO FAIL ABUN H0-166M -5.948E-02 5.689E-02 8.902E-02 FAIL ABUN TM-171 1. 293E+Ol 2.676E+Ol 5.419E+Ol NOT IDENT. HF-172 -5.917E-02 2.532E-01 4.616E-01 FAIL ABUN LU-172 3.339E-02 7.741E-02 1.616E-01 FAIL ABUN LU-176 1. 956E-03 2.670E-02 5.202E-02 FAIL ABUN HF-181 7.667E+OO 6.760E+OO 1.374E+Ol NOT IDENT. Page 3251of5809 TA-182 1. 036E+OO 1.043E+OO 2.021E+OO FAIL ABUN RE-183 -1. 266E+OO 3.408E+OO 6.517E+OO NOT IDENT. RE-184 2.583E+Ol 3.559E+Ol 7.658E+Ol NOT IDENT. W-188 2 .-142E+Ol 1.307E+02 2.337E+02 FAIL ABUN IR-192 -2.060E-02 5.417E-01 1.045E+OO FAIL ABUN HG-203 -1.17 8E-02 2.862E+OO 5.563E+OO FAIL ABUN BI-207 -4.538E-02 4.581E-02 7.574E-02 FAIL ABUN PB-210 -3.189E+OO 4. 672E+.00 8.184E+OO NOT IDENT. BI-211 O.OOOE+OO 6.434E-01 8.492E-01 FAIL ABUN PB-211 l.331E-01 8.190E-01 1.573E+OO NOT IDENT. RN-219 2.806E-01 4.653E-01 9.251E-01 FAIL ABUN RA-223 -1. 701E-01 7.430E-01 l.258E+OO FAIL ABUN AC-227 l.004E-01 2.473E-01 4. 962E-01 FAIL ABUN TH-227 l.004E-01 2.473E-01 4. 962E-01 FAIL ABUN TH-229 -3.999E-01 5.417E-01 9.153E-01 FAIL ABUN TH-231 -l.701E-01 7.430E-01 1.258E+OO FAIL ABUN PA-233 -3.135E-02 6.316E-02 l.178E-01 FAIL ABUN PA-234 -5.330E-02 2.582E-01 5.009E-01 NOT IDENT. PA-234M 4.560E+OO 7.901E+OO 8.386E+00 FAIL ABUN TH-234 -2.226E-01 1.357E+OO 2.661E+OO FAIL ABUN NP-237 -3.135E-02 6.316E-02 1.178E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 -2.226E-01 1.357E+OO 2.661E+OO FAIL ABUN NP-239 -1.084E-02 2.685E-01 4.624E-01 FAIL ABUN PU-239 l.448E+02 3.547E+02 6.714E+02 NOT IDENT. AM-241 -9.017E-02 1.586E-01 2.978E-01 NOT IDENT. CM-243 -9. 716E-02 1.023E-01 1. 792E-01 FAIL ABUN BK-247 2.00lE-02 7.981E-02 l.583E-01 NOT IDENT. CM-247 2.693E-04 4.349E-02 8.246E-02 NOT IDENT. CF-249 -9.102E-03 4.912E-02 9.167E-02 NOT IDENT. CF-251 4.402E-02 l.299E-01 2.407E-01 FAIL ABUN Page 3252 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:17:29.71 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 409 10.66* l.215E+OO 1.595E+Ol 1.595E+Ol 10.13 CD-109 88.03 98 3.70* 5.400E+OO 2.486E+OO 3.936E+OO 63.30 SN-126 64.28 ------9.60 3.017E+OO ------Line Not Found ------86.94 98 8.90 5.400E+OO 1.033E+OO l.033E+OO 63.30 87.57 98 37.00* 5.400E+OO 2.486E-01 2.486E-01 63.30 BA-137M 661. 66 1501 89.90* 2.305E+OO 3.661E+OO 3.733E+OO 5.89 CS-137 661.66 1501 85.10* 2.305E+OO 3.868E+OO 3.943E+OO 5.89 CE-141 145.44 35 48.29* 6.768E+OO 5.351E-02 3.643E+Ol 140.66 TL-208 277.37 ------6.60 4.683E+OO ------Line Not Found ------583.19 147 85.00* 2.549E+OO 3.420E-01 3.420E-01 31.12 860.56 ------12.50 1.874E+OO ------Line Not Found ------BI-211 72.87 ------1.23 4.060E+OO ------Line Not Found ------351.06 307 12.92* 3.858E+OO 3. lllE+OO 3. lllE+OO 21.10 BI-212 727. 33 46 6.67* 2 .137E+OO 1.646E+OO 1.646E+OO 56.05 785.37 15 1.10 2.013E+OO 3.316E+OO 3.316E+OO 108.05 1620.50 ------1. 47 1.107E+OO ------Line Not Found ------PB-212 74.82 180 10.28 4.288E+OO 2.067E+OO 2.067E+OO 39.02 77 .11 295 17.10 4.519E+OO 1. 931E+OO 1. 931E+OO 25.39 238.63 537 43.60* 5. 251E+OO 1.186E+OO 1.186E+OO 11. 79 300.09 60 3.30 4.392E+OO 2 .101E+OO 2.101E+OO 81. 58 BI-214 609.32 250 45.49* 2.461E+OO 1.129E+OO l .130E+OO 17.06 1120.29 50 14.92 1.519E+OO 1.112E+OO 1.113E+OO 32.64 1764.49 25 15.30 1.023E+OO 7.948E-01 7.951E-01 60.44 PB-214 74.82 180 5.80 4.288E+OO 3.663E+OO 3.665E+OO 39.02 77 .11 295 9.70 4.519E+OO 3.404E+OO 3.406E+OO 25.39 87.09 98 3.41 5.400E+OO 2.697E+00 2.698E+OO 63.30 242.00 176 7.25 5.204E+OO 2.361E+OO 2.362E+OO 47.35 295.22 195 18.42 4.455E+OO 1.203E+OO 1.203E+OO 29.37 351. 93 307 35.60* 3.858E+OO 1.129E+OO 1.129E+OO 21.10 RN-222 609.32 250 45.49* 2.461E+OO 1.129E+OO 1.130E+OO 17.06 1120.29 50 14.92 l.519E+OO 1.112E+OO 1.113E+OO 32.64 1764.49 25 15.30 1.023E+OO 7.948E-01 7. 951E-01 60.44 RA-224 240.99 176 4.10* 5.204E+OO 4.175E+OO 4.175E+OO 47.35 RA-226 609.32 250 45.49* 2.461E+OO 1.129E+OO 1.130E+OO 17.06 1120.29 50 14.92 l.519E+OO 1.112E+OO 1.113E+OO 32.64 1764.49 25 15.30 1.023E+OO 7.948E-01 7.951E-01 60.44 AC-228 105.21 ------1.10 6.393E+OO ------Line Not Found ------338.32 98 11. 27 3.983E+OO 1.lOOE+OO 1.lOOE+OO 51. 24 794.95 ------4.25 1.995E+OO ------Line Not Found ------835.71 ------1. 61 1.918E+OO ------Line Not Found ------911. 20 76 25.80* 1. 791E+OO 8.287E-01 8.287E-01 41. 38 968.97 63 15.80 1.706E+OO 1.188E+OO 1.188E+OO 35.66 RA-228 105.21 ------1.10 6.393E+OO ------Line Not Found ------338.32 98 11. 27 3.983E+OO 1.lOOE+OO 1.lOOE+OO 51. 24 794.95 ------4.25 l.995E+OO ------Line Not Found ------835. 71 ------1. 61 1.918E+OO ------Line Not Found ------911. 20 76 25.80* 1.791E+OO 8.287E-01 8.287E-01 41. 38 Page 3253 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968. 97 63 15. 8.0 1. 706E+OO 1.188E+OO 1.188E+OO 35.66 TH-228 74.82 180 10.28 4.288E+OO 2.067E+OO 2.067E+OO 39.02 77 .11 295 17.10 4.519E+OO 1. 931E+OO 1. 931E+OO 25.39 238.63 537 43.60* 5.251E+OO 1.186E+OO 1.186E+OO 11. 79 300.09 60 3.30 4.392E+OO 2. lOlE+OO 2. lOlE+OO 81. 58 TH-230 609.32 250 45.49* 2.461E+OO l.129E+OO 1.129E+OO 17.06 1120.29 50 14.92 1.519E+OO 1.112E+OO 1.112E+OO 32.64 1764.49 25 15.30 1.023E+OO 7.948E-01 7.948E-01 60.44 PA-231 283.69 ------1. 70 4.600E+OO ------Line Not Found ------301.36 60 5.35* 4.392E+OO 1. 296E+OO 1.296E+OO 81. 58 TH-232 105.21 ------1.10 6.393E+OO ------Line Not Found ------338.32 98 11.27 3.983E+OO 1.lOOE+OO 1.lOOE+OO 51. 24 835. 71 ------1. 61 1.918E+OO ------Line Not Found ------911. 20 76 25.80* 1. 791E+OO 8.287E-01 8.287E-01 41. 38 968.97 63 15.80 1. 706E+OO 1.188E+OO l.188E+OO 35.66 U-234 609.32 250 45.49* 2.461E+OO 1.129E+00 1.129E+00 17.06 1120.29 50 14.92 1.519E+OO 1.112E+OO 1.112E+OO 32.64 1764.49 25 15.30 1. 023E+OO 7.948E-01 7.948E-01 60.44 U-235 89. 96 50 3.47 5.617E+00 1.286E+OO 1.286E+OO 119. 50 93.35 94 5.60 5.779E+OO l.461E+OO l.461E+00 69.70 143.76 35 10. 96* 6.768E+OO 2.358E-01 2.358E-01 140.66 163.33 ------5.08 6.541E+OO ------Line Not Found ------185. 72 106 57.20 6.164E+OO l.524E-01 1.524E-01 64.51 205.31 ------5.01 5.819E+OO ------Line Not Found ------AM-243 43.53 35 5.90 4.061E-01 7.398E+OO 7.398E+OO 156.85 74.66 180 67.20* 4.288E+OO 3.162E-01 3.162E-01 39.02 ANH-511 511. 00 15 100.00* 2.836E+00 2.662E-02 2.662E-02 335.79 Flag: "*" Key line Page 3254 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235017 Acquisition date 3-0CT-2016 08:16:00 Total number of lines in spectrum 52 Number of unidentified lines 11 Number of lines tentatively identified by NID 41 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 32. 510 1.41E+l0Y 7.04E+08Y l.41E+l0Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y 1. 41E+l0Y 1.41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 58 1. 00 1. 02 1. 02 681. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.595E+Ol 2.486E+OO 2.486E-01 3.661E+OO 3.868E+OO 5.351E-02 3.420E-01 3. lllE+OO 1. 646E+OO 1.18 6E+00 1.129E+OO 1.129E+OO l.129E+OO 4.175E+OO 1.129E+OO 8. 287E.:...01 8.287E-01 1.186E+OO l.129E+OO 1. 296E+OO 8.287E-01 l.129E+OO 2.358E-01 3.162E-01 2.662E-02 4.905E+Ol 4.905E+Ol Decay Corr pCi/GRAM l.595E+Ol 3.936E+OO 2.486E-01 3.733E+OO 3.943E+OO 3.643E+Ol 3.420E-01 3. lllE+OO 1.646E+OO l.186E+OO l.130E+OO 1.129E+OO 1.130E+OO 4.175E+OO 1.130E+OO 8.287E-01 8.287E-01 1.186E+OO l.129E+OO 1. 296E+OO 8.287E-01 1.129E+OO 2.358E-01 3.162E-01 2.662E-02 8.702E+Ol 8.702E+Ol 78.85% Decay Corr 2-Sigma Error 0.162E+Ol 2.491E+OO 1.573E-01 0.220E+OO 0.232E+OO 5.124E+Ol 1.064E-01 0.657E+OO 0.923E+00 0.140E+00 0.193E+00 0.238E+00 0.193E+OO 1.977E+OO 0.193E+OO 3.430E-01 3.430E-01 0.140E+OO 0.193E+00 1.057E+OO 3.430E-01 0.193E+OO 3.317E-01 l.234E-01 8.938E-02 "M" Manually accepted 2-Sigma %Error 10.13 63.30 63.30 5.89 5.89 140.66 31.12 21.10 56.05 11. 79 17.06 21.10 17.06 47.35 17.06 41. 38 41. 38 11. 79 17.06 81. 58 41. 38 17.06 140.66 39.02 335.79 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3255 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235017 Acquisition date : 3-0CT-2016 08:16:00 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 70.29 39 241 1. 22 140.62 137 28 8.56E-03 **** 3.76E+OO T 3 81. 32 54 90 1. 34 162.66 137 28 1.18E-02 67.7 4.92E+OO T 0 115.21 37 224 1. 66 230.41 225 9 8.50E-03 **** 6.66E+OO T 0 154.89 .33 215 1. 75 309. 72 305 9 7. 66E-03 .**** 6.66E+OO T 0 209.13 51 150 1.18 418.16 415 7 1.21E-02 92.3 5.75E+00 0 228.05 30 142 1. 48 455.98 453 8 7.16E-03 **** 5.43E+OO T 0 270.50 36 176 1. 06 540.83 536 10 8.89E-03 **** 4.78E+OO T 0 328.07 53 99 1. 60 655.93 652 9 1. 32E-02 77. 6 4.09E+OO T 0 467.98 107 217 9.84 935.63 921 26 2.76E-02 80.8 3.05E+OO T 1 546.79 24 13 1. 71 1093.19 1090 16 6.23E-03 66.0 2.69E+OO T 1 551.54 19 22 1. 72 1102.69 1090 16 4.85E-03 92.9 2.67E+OO T 0 562.64 32 32 1. 29 1124.88 1119 12 8.33E-03 81.6 2.62E+OO T 0 616.03 25 39 3.46 1231.63 1226 12 6.72E-03 **** 2.44E+OO 0 646.12 29 14 1. 47 1291.80 1286 11 7.79E-03 63.3 2.35E+OO T 0 685.39 18 24 4. 96 1370.30 1363 15 4.80E-03 **** 2.24E+OO T 1 742.92 18 23 1. 88 1485.34 1478 19 4.90E-03 **** 2.lOE+OO 1 745.25 24 25 1. 71 1490.00 1478 19 6.48E-03 84.5 2.lOE+OO 0 768.89 16 33 1. 42 1537.26 1533 11 4.28E-03 **** 2.05E+OO 0 782.30 8 10 1. 50 1564.08 1560 7 2.28E-03 **** 2.02E+OO T 0 1002.46 13 20 0.66 2004.30 1996 17 3.49E-03 **** 1. 66E+OO T 0 1008.37 17 6 2.90 2016.12 2012 9 4.62E-03 74.3 1. 65E+00 0 1072.24 12 8 2.30 2143.83 2139 8 3.39E-03 98.4 1.57E+OO 0 1110. 46 10 17 1. 09 2220.28 2209 14 2.67E-03 **** 1.53E+OO 0 1221.91 12 8 2.28 2443.16 2438 9 3.47E-03 **** 1.41E+OO T 0 1411. 82 9 7 3.55 2822.96 2816 11 2.69E-03 **** 1.25E+OO 0 1588.32 9 2 1.11 3175.98 3172 8 2.56E-03 83.9 1.13E+OO 0 1593.67 3 0 0.73 3186.67 3183 8 7.84E-04 **** 1.12E+OO Flags: "T" = Tentatively associated Page 3256 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:17:46.16 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l * *Acquisition date 3-0CT-2016 08:16:00 Sensitivity 3.000 *
  • Detector ID GAM16 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:02:00 Nuclide Library : SOLID *
  • Sample ID G405235017 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.4856E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 2.979E-01 1. 084E+OO 6.885E-02 3.046E-02 3.218E-02 2.686E+Ol 3.197E-02 3.697E-01 4.409E-02 5.967E-02 6.734E-02 5. 967E-02 4.727E-01 5. 967E-02 l.105E-01 l.105E-01 4.409E-02 5. 965E-02 4.435E-01 1.105E-01 5.965E-02 1. 8 69E-01 4.585E-02 2.798E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3257 of 5809 Le (pCi/GRAM 1. 532E+Ol 3.766E-02 O.OOOE+OO l.671E-02 2.907E-01 O.OOOE+OO 0.000E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 . AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 3258 of 5809 4.766E-02 3.604E-01 O.OOOE+OO 4.492E-02 5.051E-01 5.077E+OO 3.314E-02 1.631E-01 1.839E+OO 1. 062E+Ol O.OOOE+OO 2.207E-01 O.OOOE+OO O.OOOE+OO 6.922E-01 7.311E+OO 8.230E-01 O.OOOE+OO 2.641E-01 5. 571E+02 2.600E-02 7.138E-01 2.252E+OO l.167E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.241E-02 5.758E-02 6.607E+OO 4.699E-01 4.699E-01 2.885E-02 8.616E-02 2.751E-01 O.OOOE+OO O.OOOE+OO l.345E-01 7.885E-01 1.164E-01 2.838E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.104E-02 O.OOOE+OO 5.074E-02 1.406E-01 O.OOOE+OO O.OOOE+OO 1.037E-01 0.000E+OO O.OOOE+OO O.OOOE+OO 3.631E-01 6.137E-02 5.334E+OO 5.150E-02 O.OOOE+OO 7.905E+02 O.OOOE+OO '2.579E-02 9.452E-02 l.897E-01 9.204E-02 1.092E-01 l.469E+OO 3.857E-02 2.560E+Ol 2.180E-01 7 .114E-02 2.425E-02 6.433E+OO 8.954E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 'CM-247 CF-249 CF-251 Page 3259 of 5809 3.054E+OO 3.426E+Ol l.087E+02 4.865E-01 2.604E+OO 3.191E-02 3.836E+OO 4.106E-01 7.323E-01 4. 316E-01 . 5.858E-01 2.330E-01 2.330E-01 4.307E-01 5.858E-01 5.455E-02 2. l 72E-01 3.697E+OO l.262E+OO 5.455E-02 O.OOOE+OO l.262E+OO 2.176E-01 3.189E+02 1.403E-01 8.400E-02 7.423E-02 3.839E-02 4.283E-02 l .138E-01 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:17:51.78 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235017.CNF;l *
  • Acquisition date 3-0CT-2016 08:16:00 Sensitivity : 3.000 *
  • Detector ID GAM16 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:02:00 Nuclide Library : SOLID *
  • Sample ID G405235017 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4856E+02 GRAM *
  • Quantity Err(%) : 1.3462E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * * *'Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.595E+Ol 1. 789E+OO 1. 789E+OO CD-109 2.lBlE+OO 2.509E+OO 2.509E+OO SN-126 l.377E-01 1.583E-01 1.583E-01 BA-137M 3.733E+OO 2.689E-01 2.689E-01 CS-137 3.943E+OO 2.838E-01 2.838E-01 CE-141 1.033E+Ol 5.238E+Ol 5.238E+Ol TL-208 3.420E-01 1.053E-01 1.053E-01 BI-212 1. 646E+OO 9.081E-01 9.081E-01 PB-212 1.186E+OO l.509E-01 l.509E-01 BI-214 1.130E+OO 1.951E-01 l.951E-01 PB-214 1.129E+OO 2.383E-01 2.383E-01 RN-222 1.130E+OO 1.951E-01 1.951E-01 RA-224 2.048E+OO 2.040E+OO 2.040E+OO RA-226 1.130E+OO 1.951E-01 1.951E-01 AC-228 8.287E-01 3.388E-01 3.388E-01 RA-228 8.287E-01 3.388E-01 3.388E-01 TH-228 1.186E+OO 1.509E-01 1.509E-01 TH-230 1.129E+OO 1.950E-01 1.950E-01 PA-231 l.296E+OO 1.073E+OO 1.073E+OO TH-232 8.287E-01 3.388E-01 3.388E-01 U-234 1.129E+OO l.950E-01 l.950E-01 U-235 2.358E-01 3.252E-01 3.252E-01 AM-243 2.124E-01 1.259E-01 1.259E-01 ANH-511 2.662E-02 8.760E-02 8.760E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -l.574E+Ol 1.908E+Ol 2.036E+Ol NOT IDENT. NA-22 1. 795E-02 4.082E-02 4.161E-02 NOT IDENT. NA-24 1.000E+41 3.054E+41 O.OOOE+OO SHORT HLIF AL-26 -l.312E-02 2.478E-02 2.548E-02 NOT IDENT. SC-46 -1.637E-01 3.601E-01 3.676E-01 FAIL ABUN V-48 -5.949E+03 1.669E+04 1.691E+04 SHORT HLIF Page 3260 of 5809 CR-51 4.574E+02 5.924E+02 6.272E+02 SHORT HLIF MN-54 8.642E-03 5.258E-02 5.273E-02 NOT IDENT. C0-56 -1. 079E-01 4.273E-01 4. 301E-01 NOT IDENT. MN-56 -1.000E+41 1. 748E+41 0.000E+OO SHORT HLIF C0-57 -3.425E-02 5.377E-02 5.594E-02 NOT IDENT. C0-58 6.255E-02 5.612E-01 5.619E-01 NOT IDENT. FE-59 2.294E-01 5.868E+OO 5.869E+OO NOT IDENT. C0-60 -1.098E-02 4.174E-02 4.203E-02 NOT IDENT. ZN-65 3. 965E-02 2.081E-01 2.089E-01 NOT IDENT. GE-68 -3.464E-01 2.284E+OO 2.289E+OO NOT IDENT. AS-73 -5.475E+OO l.190E+Ol l.215E+Ol NOT IDENT. AS-74 8.846E+02 8.526E+03 8.535E+03 SHORT HLIF SE-75 5.271E-02 2.378E-01 2.389E-01 NOT IDENT. BR-77 1.263E+39 l.116E+40 0.000E+OO SHORT HLIF SR-82 -l.850E+02 8.459E+02 8.500E+02 SHORT HLIF RB-83 8.200E-02 7.941E-01 7.950E-01 FAIL ABUN KR-85 3.266E+OO 9.036E+OO 9.155E+OO NOT IDENT. SR-85 3.647E-01 1.018E+OO 1. 031E+OO NOT IDENT. RB-86 2.978E+03 3.267E+04 3.270E+04 SHORT HLIF Y-88 2.707E-01 2.432E-01 2. 721E-01 NOT IDENT. Y-91 l.368E+02 6.350E+02 6.380E+02 NOT IDENT. NB-94 l.327E-04 3.108E-02 3 .108E-02
  • NOT IDENT. NB-95 -7.649E-01 1.133E+OO 1.185E+OO NOT IDENT. NB-95M -l.446E+OO 3.108E+00 3.175E+OO NOT IDENT. ZR-95 2.686E-01 l.355E+OO 1.360E+OO NOT IDENT. NB-97 -1.000E+41 6.378E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 4.159E+41 O.OOOE+OO SHORT HLIF M0-99 -4.977E+32 8.870E+32 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 2.536E+41 O.OOOE+OO SHORT HLIF RH-101 -l.537E-02 3.823E-02 3.886E-02 NOT IDENT. RH-102 3.642E-02 6.312E-02 6.522E-02 NOT IDENT. RU-103 -1. 921E+OO 7.842E+OO 7.889E+00 FAIL ABUN RH-106 2.697E-01 5.391E-01 5.527E-01 NOT IDENT. RU-106 2.697E-01 5.391E-01 5.527E-01 NOT IDENT. AG-108M -2.261E-02 3.507E-02 3.652E-02 NOT IDENT. AG-llOM -2.589E-03 9.860E-02 9.861E-02 NOT IDENT. SN-113 3.590E-02 3.082E-01 3.086E-01 NOT IDENT. CD-115 -2.042E+40 2.547E+40 O.OOOE+OO SHORT HLIF SN-ll 7M l.632E+04 l.593E+05 1.595E+05 SHORT HLIF TE-123M l.244E-01 l.466E-01 1.570E-01 NOT IDENT. SB-124 -4.188E-01 1.241E+OO 1.255E+OO FAIL ABUN SB-125 l.903E-02 l.310E-01 l.312E-01 NOT IDENT. TE-125M l .116E+02 3.124E+02 3 .165E+02 NOT IDENT. I-126 l.178E+06 l.166E+06 1. 281E+06 SHORT HLIF SB-126 -4 .101E+05 l.558E+06 1.569E+06 SHORT HLIF SB-127 9.203E+22 1. 739E+23 O.OOOE+OO SHORT HLIF I-131 -4.498E+09 1.013E+10 l.033E+l0 SHORT HLIF I-132 -1.000E+41 1.940E+42 O.OOOE+OO SHORT HLIF TE-132 1.900E+27 2.972E+27 O.OOOE+OO SHORT HLIF BA-133 l.839E-02 4.906E-02 4.975E-02 FAIL ABUN I-133 1.000E+41 6.660E+41 0.000E+OO SHORT HLIF CS-134 3.845E-02 5.579E-02 5.842E-02 FAIL ABUN CS-135 -3.516E-02 1.742E-01 1. 749E-01 NOT IDENT. I-135 1.000E+41 8.045E+41 O.OOOE+OO SHORT HLIF CS-136 1.181E+05 3. 872E+05 3.908E+05 SHORT HLIF CE-139 -8.036E-02 l.284E-01 l.334E-01 NOT IDENT. BA-140 -9.431E+05 1.995E+06 2.040E+06 SHORT HLIF LA-140 2.523E+05 2.769E+05 2.993E+05 SHORT HLIF CE-143 1.000E+41 9. 861E+40 O.OOOE+OO SHORT HLIF CE-144 2.124E-02 4.147E-01 4.148E-01 FAIL ABUN PM-144 5.082E-02 6.705E-02 7.085E-02 NOT IDENT. PR-144 4.357E+OO 5. 831E+OO 6.152E+OO NOT IDENT. PM-146 -l.414E-02 6.026E-02 6.060E-02 NOT IDENT. ND-147 3.804E+07 5.690E+07 5.943E+07 SHORT HLIF PM-147 -5.660E+Ol 9.040E+02 9.044E+02 NOT IDENT. PM-149 l.000E+41 1.514E+41 O.OOOE+OO SHORT HLIF EU-150 -5.178E-03 3.255E-02 3.264E-02 FAIL ABUN EU-152 4.729E-02 1.017E-01 l.039E-01 NOT IDENT. GD-153 4.509E-03 2.296E-01 2. 296E-01 FAIL ABON EU-154 4.386E-02 9.976E-02 l.017E-01 NOT IDENT. EU-155 8.891E-02 1.168E-01 1.235E-01 FAIL ABUN TB-160 -3.736E-01 1.738E+OO l.747E+OO FAIL ABUN H0-166M -5.948E-02 5.698E-02 6.297E-02 FAIL ABUN TM-171 1.293E+Ol 2.678E+Ol 2.741E+Ol NOT IDENT. HF-172 -5.917E-02 2.534E-01 2.548E-01 FAIL ABUN LU-172 3.339E-02 7.749E-02 7.894E-02 FAIL ABUN LU-176 1.956E-03 2.670E-02 2.672E-02 FAIL ABUN HF-181 7.667E+OO 6.769E+OO 7.600E+OO NOT IDENT. Page 3261of5809 TA-182 l.036E+OO l.044E+OO l.144E+OO FAIL ABUN RE-183 -l.266E+OO 3.414E+OO 3.461E+00 NOT IDENT. RE-184 2.583E+Ol 3.614E+Ol 3.797E+Ol NOT IDENT. W-188 2.142E+Ol l.307E+02 l.310E+02 FAIL ABUN IR-192 -2.060E-02 5.417E-01 5.418E-01 FAIL ABUN HG-203 -l. l 78E-02 2.862E+OO 2.862E+OO FAIL ABUN BI-207 -4.538E-02 4.585E-02 5.020E-02 FAIL ABUN PB-210 -3.189E+OO 4. 681E+OO 4.896E+00 NOT IDENT. BI-211 3. lllE+OO 6.584E-01 l.549E+OO FAIL ABUN PB-211 l.331E-01 8.190E-01 8. 212E-,-01 NOT IDENT. RN-219 2.806E-01 4.667E-01 4.835E-01 FAIL ABUN RA-223 -1. 701E-01 7.431E-01 7.470E-01 FAIL ABUN AC-227 l.004E-01 2.477E-01 2.518E-01 FAIL ABUN TH-227 l.004E-01 2.477E-01 2.518E-01 FAIL ABUN TH-229 -3.999E-01 5.421E-01 5.712E-01 FAIL ABUN TH-231 -l.701E-01 7.431E-01 7.470E-01 FAIL ABUN PA-233 -3.135E-02 6.318E-02 6.474E-02 FAIL ABUN PA-234 -5.330E-02 2.653E-01 2.664E-01 NOT IDENT. PA-234M 4.560E+OO 7.904E+OO 8.167E+OO FAIL ABUN TH-234 -2.226E-01 l.358E+OO l.362E+OO FAIL ABUN NP-237 -3.135E-02 6.318E-02 6.474E-02 FAIL ABUN NP-238 -l.OOOE+41 4.680E+41 O.OOOE+OO SHORT HLIF U-238 -2.226E-01 l.358E+OO l.362E+OO FAIL ABUN NP-239 -l.084E-02 2.685E-01 2.685E-01 FAIL ABUN PU-239 l.448E+02 3.548E+02 3.608E+02 NOT IDENT. AM-241 -9.017E-02 l.588E-01 l.639E-01 NOT IDENT. CM-243 -9.716E-02 l.027E-01 l .116E-01 FAIL ABUN BK-247 2. OOlE-02 7. 991E-02 8.042E-02 NOT IDENT. CM-247 2.693E-04 4.349E-02 4.349E-02 NOT IDENT. CF-249 -9.102E-03 4.912E-02 4.929E-02 NOT IDENT. CF-251 4.402E-02 l.300E-01 l.315E-01 FAIL ABUN Page 3262 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 79.2320 87.09 119.8780 136.47 102.8881 45.60 66.0009 87.57 119. 9950 140.51 0.0000 46.54 83.3537 88.03 120.1066 143.76 95.0439 49.72 0.0000 88.34 120.1814 144.24 95 .1101 51. 35 76.4709 88.47 120.2129 145.44 106.1085 51.87 79.3869 89. 96 120.5703 152.43 99.6056 52.39 80.4400 1093.63 120.7332 153.25 0.0000 52.97 83.3828 91.11 0.0000 323.87 77.1558 53.44 98.5032 92.59 121.1955 156.02 0.0000 54.07 86.4599 93.35 121. 3742 158.56 0.0000 57.36 0.0000 94.56 121. 6578 159.00 78.7979 57.53 88.2287 94.65 121. 6785 162.33 88.3239 57.98 83.5850 94.67 121. 6834 162.66 0.0000 59.27 99 .1194 94.87 105. 9118 163.33 76.9535 59.32 103.8985 97.43 118.8676 165.86 103. 7123 59.54 103.9584 98.43 94.5103 176.31 110.9338 60. 96 89.0256 98.44 94.5123 176.60 0.0000 61.17 89.0738 99.53 105 .1110 177.52 90.0499 62.93 109.6769 100 .11 95.8478 181.07 0.0000 63.29 99.1840 102.03 80.5030 181.52 89.3165 63.58 99.2559 103.18 78.5757 184.41 94.3469 64.28 104.2561 103.37 99.5633 143.76 116.9371 66.73 121. 7188 105.21 86.2235 193.51 106.0936 67.24 106. 3112 105.31 86.2385 197.03 106.5254 125.81 127.1895 106.12 76.8841 198.01 116. 2310 67.75 129.8065 106.47 84.3091 201. 83 108.3115 69.67 105.6253 109.28 87.9025 203.43 88.0097 70.83 105.9120 111. 00 101.9729 205.31 86.9865 72.81 106.3974 111.76 0.0000 210.85 105.3460 72.87 106.4122 114. 06 90.7600 215.65 86.7523 74.66 106.8456 116.30 0.0000 222 .11 109.4927 74.82 106.8835 116.74 85.8051 227.09 82.4432 74.97 106.9198 119.76 93.7783 227.38 82.4677 77 .11 107.4298 121.12 87.5036 228.16 0.0000 78.74 107.8130 121. 22 96 .1616 228.18 84.1865 79.69 108.0354 121. 78 98. 4114 116.74 84.1865 80.12 108.1351 122.06 108.1932 235.69 89.8220 80.19 0.0000 122.92 78.0068 235. 96 89.8462 80.57 108.2390 123.07 78.0255 238.63 66.7301 81. 00 108.3387 265.00 96. 5418 238.98 0.0000 81. 07 108.3551 125.81 102.3105 240.99 66.8872 81. 75 101. 8134 127.23 112.3561 242.00 66.9535 83.79 100.9048 127.91 97.1876 244.70 61. 67 69 84.00 100.9491 129.30 107.2458 252.40 0.0000 85.43 129.5977 131. 20 113.0492 252.80 65.1207 86.55 119.7465 133. 02 108.9595 254.15 0.0000 86.79 119.8050 133.52 106.8397 256.23 70.4243 86.94 119.8419 136.00 103.9212 260.90 0.0000 Page 3263 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 70.9803 355:39 0.0000 584.27 32.7950 2 64. 8 0 70.9887 356.01 48.3974 595.83 0.0000 265.00 71.0022 364.49 0.0000 427.87 26.6622 268.22 82.3652 366.42 0.0000 602.52 0.0000 269.46 75.5874 372.51 50.3789 604. 72 22.4415 270.03 75.6268 375.05 65.4242 607.14 25.6777 271.23 75.7092 377.52 61. 7944 609.32 30.5248 273.65 0.0000 356.01 63.9492 610.33 30.5399 276.40 66.5541 388.16 71. 6860 614.28 16.1041 277.37 75.2630 388.63 0.0000 618.01 29.0391 277.60 74.4119 391.69 64.2965 620.36 38.7627 278.00 75.3037 264.66 57.0789 621.93 20.6891 279.20 71.9191 401.81 52.3626 630.19 0.0000 279.54 70.2076 402.40 60.9557 631.29 21.6471 279.70 67.6168 404.85 57.2400 633.25 19.5007 280.46 66.7938 410.95 64.1770 634.78 0.0000 283.69 68. 7232 .413.71 51.8192 635.95 26.0332 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 51. 4029 423.72 0.0000 645.85 15.2567 285.90 0.0000 427.09 61.9505 657.76 37.8032 287.50 63.7161 427.87 54.2340 657.90 0.0000 290.67 55.1378 433.94 61. 2491 661.66 26.3438 293.27 0.0000 439.40 53.6561 664.57 0.0000 351. 93 61.9428 453.88 64.9674 666.33 0.0000 295. 96 61.9815 463.37 60.3919 666.50 0.0000 879.38 31.7205 468.07 60.5619 667.71 0.0000 299.98 71. 4551 473.00 0.0000 677.62 30.9565 300.09 71.4617 475.06 53.8352 685.70 0.0000 300.13 71. 4633 476.78 56.8840 695.00 0.0000 301. 36 71. 5375 477.60 71.8887 696.49 26.7559 302.85 78.2585 482.18 48.0537 696. 51 26.7559 256.23 65.0826 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 33.4558 306.78 62.1016 497.08 46.4492 697.49 31. 2288 308.46 71.9594 505.52 47.1793 702.65 22.3560 311. 90 63.2532 507.63 0.0000 706.68 22.3950 316.51 61.7016 511. 00 42.7438 711. 68 28.0538 319.41 0.0000 514.00 41.2861 720.70 0.0000 320.08 0.0000 514.00 41.2861 721. 93 0.0000 321.04 60 .1312 520.40 35.8061 722.78 15.2210 323.87 67.4622 520.69 0.0000 722.91 20.2954 325.23 55.3790 522.65 0.0000 723. 31 18.6075 328.76 0.0000 527.90 0.0000 724.19 16.9220 333.37 70.6859 528.26 39.0422 727.33 19.2039 333.97 67.9977 529.59 32.9010 733.00 18.6833 334.37 63.9380 529.87 0.0000 735.93 13.6045 338.28 65.4961 531. 02 0.0000 333.97 10.2100 338.32 65.4976 537.26 0.0000 739.50 0.0000 311. 90 46.4709 546.56 0.0000 747.24 29.0455 340.48 46.4709 552.55 40.5917 748.06 20.5100 340.55 0.0000 563.25 34.5388 752.31 26.2526 344.28 50.2600 569.33 34.6476 753.82 0.0000 345.93 65.8770 946.00 34.6503 756.73 13.7217 351.06 56.9469 569.70 31. 5039 756.80 11. 4351 351.93 56.9834 583.19 32.7773 884.68 15.4825 Page 3264 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 30.9880 1274.44 13.4728 1620.50 3.3085 766.42 30.9957 1001.03 13.4938 1621. 92 6.6189 766.84 24.1121 1002.74 13. 5013 1678.03 0.0000 772.60 0.0000 1004.7.3 0.0000 1690.97 2.2389 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764 .. 49 4.5459 778.90 12 .1141 1028.54 0.0000 1063.66 10.9230 783.70 0.0000 1037.84 13.2745' 1771.35 3.6418 785.37 8.6752 1038.76 0.0000 1791.20 0.0000 792.07 19. 7157 631.29 10.4582 1808.65 4.5862 794.95 15.0942 1048.07 0.0000 1810.72 0.0000 795.86 19.7455 1049.04 13.3207 1836.06 1.8443 810.06 14.8911 1050.41 11. 4229 810.29 15.7681 1063.66 20.0720 344.28 15.7692 1077.00 0.0000 810.76 15. 7714 1077.34 14.2605 815.77 0.0000 1085.87 16.3598 1048.07 0.0000 1093.63 13.5044 832.01 14 .1328 1099.45 9.6631 834.85 13.2637 1112. 07 24.8297 835.71 14.1528 1112. 8.4 23.2837 836.80 0.0000 1115. 54 17.0887 846.75 0.0000 1120.29 10.6952 846.77 15.9879 1120.55 10.6959 856.80 0.0000 1221.41 3 .1123 860.56 18.7480 1129. 67 12.6747 871.09 13.4427 1131. 51 0.0000 873.19 18.8345 1147.95 0.0000 875.33 0.0000 1173.23 21.7220 879.38 15.2812 1177.95 15.8184 880.51 17.0860 1189.05 18.8434 883.24 18.9031 1204.77 18.9269 884.68 17.1115 1221. 41 11. 0081 889.28 17.1399 1231. 02 21. 0705 894.76 18.9806 1235.36 0.0000 898.04 20.8129 1238.28 19.1021 900.72 22.6440 1260.41 0.0000 903.28 15.4120 1271.87 13.1880 911.20 18.1824 1274.44 8.1216 912.08 18.1879 1274.54 8.1216 923.98 0.0000 1291.59 8.1582 926.50 19.1934 1298.22 0.0000 929 .11 17.3811 1312 .11 0.000"0 937.49 16.5135 1332.49 13.3983 944 .13 0.0000 1362.66 0.0000 946.00 16.5619 1365.19 11. 4310 949.00 17.5000 1368.63 0.0000 667. 71 0.0000 1384.29 9. 3972 %2.31 19.0321 1408.01 3.3607 964.08 23.6984 1457.56 0.0000 966 .17 16.3040 1460.82 10.6366 911. 20 21.3267 1489.16 7.4952 968. 97 21.3267 1505.03 6.4482 983.53 0.0000 1584.12 3.5010 984.45 0.0000 1596.21 0.0000 Page 3265 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:18:22.92 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM27.CNF;330 Background date : Z-OCT-2016 11:01:30. Sample date 2-DEC-2015 10:19:00. Acquisition date : 3-0CT-2016 08:16:22. Sample ID G405235018 Sample quantity 1.55815E+02 GRAM Detector name GAM27 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.98 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 0 0 3 3 0 0 0 5 5 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3266 of 5809 Energy 63.29* 74.84* 77.20 83.74* 87.27 93.05* 95.46 105.45 136.89 186.02* 238.71* 241. 58 270.35 277.65 295.31* 300.02 328.39 338.51* 351.96* 394.83 408.86 510.67* 536.91 554.81 583.29* 609.62* 645.81 654.80 661. 7 6* 722. 27 726.97 755.46 811.35 816.68 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 67 201 260 26 108 63 48 40 52 66 469 129 46 39 178 40 55 60 297 21 47 34 43 18 124 142 23 19 951 16 50 20 12 40 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 266 278 172 199 183 168 152 97 137 204 86 131 93 136 71 68 75 103 84 61 52 100 53 38 54 65 26 34 64 17 23 18 19 15 0.82 1. 31 0.84 1. 52 1. 53 1. 21 1. 41 0.96 0.90 1. 01 1.11 2.06 1. 76 1. 46 1. 28 1. 63 2.34 1.16 1. 34 0.72 1.14 2.45 7.37 3.48 1. 44 1. 58 2.44 4.26 1. 43 3.38 1. 90 1. 54 1. 24 4.54 125.90 149.00 153.73 166.81 173.88 185.43 190.27 210.25 273.15 371.45 476.86 482.61 540.18 554.79 590.12 599.53 656.30 676.54 703.47 789.24 817.32 1021.02 1073.53 1109.35 1166.33 1219.03 12 91. 43 1309.43 1323.36 1444.45 1453.85 1510.85 1622.71 1633.37 122 144 144 165 171 182 182 208 270 366 469 469 536 548 585 585 651 671 697 786 813 1012 1065 1101 1160 1213 1286 1300 1316 1439 1449 1507 1616 1625 9 1. 8 6E-02 15 5.58E-02 15 7.21E-02 7 7.29E-03 7 2.99E-02 13 1. 7 5E-02 13 1.35E-02 6 l.llE-02 8 1. 45E-02 11 1.84E-02 21 1.30E-01 21 3.58E-02 9 1.29E-02 13 1. lOE-02 19 4.95E-02 19 l.12E-02 10 l.52E-02 10 l.66E-02 11 8.26E-02 8 5. 71E-03 9 1.30E-02 18 9.38E-03 19 1. 20E-02 13 4.98E-03 12 3.45E-02 13 3.95E-02 12 6.33E-03 15 5.38E-03 15 2.64E-01 10 4.40E-03 11 l.37E-02 9 5.56E-03 9 3.20E-03 19 l.12E,.-02 46.5 16.0 9.8 92.1 23.0 39.1 52.2 42.3 40.8 44.9 5.8 26.3 40.3 63.0 11. 3 39.7 32.7 35.0 8. 4 69.1 31. 3 77.7 42.8 75.4 15.1 14.6 51. 7 69.2 3.7 55.3 23.3 44.3 78.3 27.4 Fit 1.14E+OO 1.75E+OO l.03E+OO l.22E+00 Peak Search Report (continued) Page : 2 Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 862.01 24 43 4.86 1724.08 1713 19 6.75E-03 67.7 36 0 911.47* 105 28 2.30 1823.05 1815 14 2.92E-02 14.8 3.7 0 953.31 11 9 1. 71 1906.78 1900 9 3. llE-03 56.6 38 2 964. 7 4 34 16 2.24 1929.66 1923 22 9.46E-03 28.7 1.54E+OO 39 2 968.79* 51 9 1. 97 1937.77 1923 22 1.42E-02 20.1 40 0 1120.06* 49 35 2.52 2240.50 2234 14 1.36E-02 29.8 41 0 1150. 90 14 12 3.15 2302.21 2296 12 3.89E-03 56.2 42 0 1255.13 9 18 2.84 2510.82 2500 15 2.40E-03114.3 43 0 1301.45 7 21 2.68 2603.53 2591 14 2.04E-03145.3 44 0 1314.68 9 5 0.90 2629.99 2622 11 2.38E-03 63.0 45 0 1318. 32 12 5 2.18 2637.29 2632 10 3.33E-03 45.3 46 0 1339.26 5 11 0.51 2679.20 2668 14 l.48E-03136.7 47 0 1377. 72 17 7 1. 08 2756.18 2750 13 4.58E-03 40.3 48 0 1460.95* 423 11 1. 70 2922.75 2915 15 1. l 7E-01 5.2 49 0 1480.60 10 3 2. 96 2962.08 2956 12 2.74E-03 47.6 50 3 1588.20 13 1 2.90 3177.46 3174 16 3.53E-03 29.5 6.09E-01 51 3 1592.38 11 3 1. 91 3185.83 3174 16 3.02E-03 39.1 52 0 1764.60* 37 3 2.04 3530.55 3524 13 l.04E-02 20.4 53 0 1847.52 15 0 1. 98 3696.53 3690 11 4.17E-03 25.8 Flag: "*" = Peak area: was modified by background subtraction Page 3267 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:18:25 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 10:19:00 G405235018 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:16:22 155. 82 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA27 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3268 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86.94 SN-126 87.57 CD-109 88.03 RA-224 240.99 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.98 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1 .. 403E+OO 1.319E+Ol 1.319E+Ol 10.43 O.K C0-58 810.76 99.45* 2.251E+OO 2.571E-02 5.127E-01 156.68 OK CD-109 88.03 3.70* 7.568E+OO 1.379E+OO 2.183E+OO 81. 38 OK SN-126 64.28 9.60 5.536E+OO 8.091E-01 8.091E-01 93.09 OK 86.94 8.90 7.568E+OO 5.732E-01 5.732E-01 81. 38 OK 87.57 37.00* 7.568E+00 1.379E-01 1. 37 9E-01 81. 38 OK BA-137M 661. 66 89.90* 2.624E+OO 2.058E+OO 2.098E+OO 7.49 OK CS-137 661. 66 85.10* 2.624E+OO 2.174E+OO 2.216E+OO 7.49 OK EU-155 86.55 30.70 7.568E+OO l.662E-01 1.878E-01 81. 38 OK 105.31 21.10* 8.063E+OO l.433E-01 1.619E-01 84.59 OK TL-208 277.37 6.60 5.128E+OO 6.519E-01 6.519E-01 125.97 OK 583.19 85.00* 2.886E+OO 2.619E-01 2.619E-01 30.18 OK 860.56 12.50 2.150E+OO 4.481E-01 4.481E-01 135.31 OK PB-212 74.82 10.28 6.758E+OO 1.207E+OO 1.207E+OO 49.92 OK 77 .11 17.10 6.949E+OO 1. 37 6E+OO l.376E+OO 19.56 OK 238.63 43.60* 5.747E+OO 1.060E+OO 1.060E+OO 11. 65 OK 300.09 3.30 4.829E+OO l.402E+00 1.402E+OO 79.42 OK BI-214 609.32 45.49* 2. 791E+OO 5.775E-01 5.777E-01 29.30 OK 1120.29 14.92 1. 754E+OO 9.007E-01. 9.0lOE-01 59.54 OK 1764.49 15.30 1.177E+OO 9.458E-01 9.461E-01 40.84 OK PB-214 74.82 5.80 6.757E+OO Line Not Found <<INT Reject 77 .11 9.70 6.949E+OO 2.425E+OO 2.426E+OO 19.56 OK 87.09 3.41 7.559E+OO Line Not Found <<INT Reject 242.00 7.25 5.689E+OO Line Not Found <<INT Reject 295.22 18.42 4.889E+OO 1.099E+OO 1.lOOE+OO 22.56 OK 351.93 35.60* 4.262E+OO 1.069E+OO 1.070E+OO 16.86 OK RN-222 609.32 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 OK 1120.29 14.92 1. 754E+OO 9.007E-01 9.0lOE-01 59.54 OK 1764.49 15.30 1.177E+OO 9.458E-01 9.461E-01 40.84 OK RA-224 240.99 4 .'10* 5.697E+OO 1.181E+OO 1.181E+OO 144.23 OK RA-226 609.32 45.49* 2. 791E+OO 5.775E-01 5.777E-01 29.30 OK 1120. 29 14.92 1. 754E+OO 9.007E-01 9.0lOE-01 59.54 OK 1764.49 15.30 1.177E+OO 9.458E-01 9.461E-01 40.84 OK AC-228 105.21. 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 OK 338.32 11.27 4.394E+OO 6.612E-01 6.612E-01 69.99 OK 794.95 4.25 2.286E+OO Line Not Found Absent 835.71 1. 61 2.201E+OO Line Not Found Absent 911. 20 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 OK 968. 97 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 OK RA-228 105.21 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 OK 338.32 11.27 4.394E+OO 6.612E-01 6.612E-01 69.99 OK 794.95 4.25 2.286E+OO Line Not Found Absent 835.71 1. 61 2.201E+OO Line Not Found Absent 911. 20 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 OK 968. 97 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 OK TH-228 74.82 10.28 6.758E+OO 1.207E+OO l.207E+OO 49.92 OK 77 .11 17.10 6.949E+OO 1.376E+OO 1. 37 6E+OO 19.56 OK 238.63 43.60* 5.747E+OO 1.060E+OO 1.060E+OO 11. 65 OK 300.09 3.30 4.829E+OO l.402E+OO 1.402E+OO 79.42 OK Page 3269 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 2.791E+OO 5.775E-01 5.775E-01 29.30 OK. 1120.29 14.92 1. 754E+OO 9.007E-01 9.007E-01 59.54 OK 1764.49 15.30 l.177E+OO 9.458E-01 9.458E-01 40.84 OK PA-231 283.69 1. 70 5.044E+OO Line Not Found Absent 301.36 5.35* 4.829E+OO 8.646E-01 8.646E-01 79.42 OK TH-232 105.21 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 OK 338.32 11. 27 4.394E+OO 6.612E-01 6.612E-01 69.99 OK 835.71 1. 61 2. 201E+OO Line Not Found Absent 911.20 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 OK 968.97 15.80 l.966E+00 8.046E-01 8.046E-01 40.21 OK TH-234 63. 29 3.70* 5.536E+00 2.099E+OO 2.099E+OO 93.09 OK 92.59 4.23 7.800E+OO l.184E+OO 1.184E+OO 78 .13 OK U-234 609.32 45.49* 2.791E+OO 5.775E-01 5.775E-01 29.30 OK 1120.29 14.92 1. 754E+OO 9.007E-01 9.007E-01 59.54 OK 1764.49 15.30 l.177E+OO 9.458E-01 9.458E-01 40.84 OK U-238 63.29 3.70* 5.536E+OO 2.099E+OO 2.099E+00 93.09 OK 92.59 4.23 7.800E+OO 1.184E+OO 1.184E+OO 78.13 OK AM-243 43.53 5.90 2.021E+OO Line Not Found Absent 74.66 67.20* 6.758E+OO 1. 846E-01 '1.846E-01 49.92 OK ANH-511 511. 00 100.00* 3.192E+OO 5.553E-02 5.553E-02 155.34 OK Flag: "*" = Keyline Page 3270 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:18:26.16 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l *
  • Acquisition date 3-0CT-2016 08:16:22 Sensitivity 3.000 *
  • Detector ID GAM27 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.98 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:19:00 Analyst initials: MXRl *
  • Sample ID G405235018 Sample Quantity 1.5582E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr : 1.00000 Dry Weight : 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;l3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1 . 96-sigma ) K-40 1.319E+Ol 1.348E+OO C0-58 5.127E-Ol 7.873E-01 CD-109 2.183E+OO 1. 741E+OO SN-126 1.379E-01 1.lOOE-01 BA-137M 2.098E+OO l.540E-01 CS-137 2.216E+OO l.627E-01 EU-155 1. 619E-01 l.342E-01 TL-208 2.619E-01 7.747E-02 PB-212 l.060E+OO l.211E-01 BI-214 5.777E-01 1.659E-01 PB-214 1.070E+OO 1.767E-01 RN-222 5.777E-01 l.659E-01 RA-224 1.181E+OO 1.670E+OO RA-226 5.777E-01 l.659E-01 AC-228 9.737E-01 2. 821E-01 RA-228 9.737E-01 2.821E-01 TH-228 1.060E+OO 1. 211E-01 TH-230 5.775E-01 l.658E-01 PA-231 8.646E-01 TH-232 9.737E-01 2.821E-01 TH-234 2.099E+OO 1.915E+OO U-234 5.775E-01 l.658E-01 U-238 2.099E+OO 1.915E+OO AM-243 1. 846E-01 9.030E-02 ANH-511 5.553E-02 8.454E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3271 of 5809 Key-Line Activity (pCi/GRAM l.854E+OO -l.638E-02 O.OOOE+OO 3.874E-02 9.603E-02 K.L. Cnt Uncert ( 1. 96-sigma) l.400E+Ol 3.530E-02 1. 960E+41 2.728E-02 3.228E-01 MDA (pCi/GRAM 4.997E-01 9.769E-01 1.691E+OO 1. 071E-01 5.879E-02 6. 211E-02 1.553E-01 5.981E-02 8.503E-02 1. 211E-01 1.179E-01 1. 211E-01 9 .115E-01 1. 211E-01 2.043E-01 2.043E-01 8.503E-02 1.210E-01 7.896E-01 2.043E-01 1.443E+OO l.210E-01 1.443E+OO 6.479E-02 5.039E-02 MDA (pCi/GRAM 2.679E+Ol 6.409E-02 O.OOOE+OO 7.380E-02 6.731E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1.790E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.233E+02 O.OOOE+OO SHORT HLIF MN-54 5.415E-02 5.306E-02 l.183E-01 NOT IDENT. C0-56 -2.903E-01 4.017E-01 7.258E-01 NOT IDENT. MN-56 0.000E+OO 1.391E+41 O.OOOE+OO SHORT HLIF C0-57 -3.318E-03 4.215E-02 7.817E-02 FAIL ABUN FE-59 -3.865E+OO 6.688E+OO 1.197E+Ol NOT IDENT. C0-60 1.028E-02 2.364E-02 5.114E-02 NOT IDENT. ZN-65 6.215E-02 1. 965E-01 3.498E-01 NOT IDENT. GE-68 7"2.862E-01 2.015E+OO 3.890E+OO NOT IDENT. AS-73 -3.048E+OO 4.557E+OO 8.566E+OO NOT IDENT. AS-74 O.OOOE+OO 6.804E+03 O.OOOE+OO SHORT HLIF SE-75 -2.039E-01 l.943E-01 3.517E-01 FAIL ABUN BR-77 O.OOOE+OO 1.285E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.184E+02 O.OOOE+OO SHORT HLIF RB-83 -4.170E-01 6.969E-01 1. 231E+OO NOT IDENT. KR-85 -4.591E+OO 8.086E+OO 1.253E+Ol NOT IDENT. SR-85 -5.166E-01 9.109E-01 1.412E+OO NOT IDENT. RB-86 O.OOOE+OO 2.973E+04 O.OOOE+OO SHORT HLIF Y-88 l.816E-02 2.207E-01 4.719E-01 NOT IDENT. Y-91 3.156E+02 5.163E+02 1. 07 5E+03 NOT IDENT. NB-94 1.547E-02 2.817E-02 5.626E-02 NOT IDENT. NB-95 -5.483E-01 8.881E-01 l.498E+OO NOT IDENT. NB-95M -4.289E-01 2.602E+OO 4.544E+OO NOT IDENT. ZR-95 2.137E+OO 1. 856E+00 2.864E+00 FAIL ABUN NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 6.'460E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 8.920E+40 O.OOOE+OO SHORT HLIF RH-101 -l.392E-02 3.173E-02 5.698E-02 NOT IDENT. RH-102 3.331E-03 4.936E-02 9.487E-02 NOT IDENT. RU-103 5.173E+OO 6.562E+OO 1.333E+Ol FAIL ABUN RH-106 -2.414E-01 4.562E-01 8.008E-01 NOT IDENT. RU-106 -2.414E-01 4.562E-01 8.008E-01 NOT IDENT. AG-108M -2.565E-02 3.068E-02 5.325E-02 FAIL ABUN AG-110M -2.689E-02 8.626E-02 1.650E-01 NOT IDENT. SN-113 -8.626E-02 2.513E-01 4.150E-01 NOT IDENT. CD-115 0.000E+OO l.908E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.178E+05 O.OOOE+OO SHORT HLIF TE-123M -2.056E-02 l.222E-01 2.211E-01 NOT IDENT. SB-124 -6.167E-02 1.663E+OO 3. 451E+OO FAIL ABUN SB-125 4.597E-02 1.077E-01 2.124E-01 NOT IDENT. TE-125M 1.914E+02 2.394E+02 4.763E+02 NOT IDENT. I-126 O.OOOE+OO 1.295E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.594E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.653E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 8.587E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO l.314E+27 O.OOOE+OO SHORT HLIF BA-133 -4.407E-02 4.771E-02 7.565E-02 FAIL ABUN I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 3.050E-02 5.159E-02 1. 013E-01 NOT IDENT. CS-135 1. 794E-02 l.364E-01 2.444E-01 NOT IDENT. I-135 O.OOOE+OO 1.632E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.064E+05 O.OOOE+OO SHORT HLIF CE-139 9.394E-03 9.938E-02 l.834E-01 NOT IDENT. BA-140 O.OOOE+OO 4.235E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.524E+05 0.000E+OO SHORT HLIF CE-141 -1.689E+Ol 2.669E+Ol 4.643E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 2. 211E-01 3.517E-01 6.332E-01 NOT IDENT. PM-144 -l.013E-02 4.502E-02 8.228E-02 NOT IDENT. PR-144 -1.243E+OO 3.975E+OO 7.157E+OO NOT IDENT. PM-146 8. 201E-03 4.350E-02 8.424E-02 NOT IDENT. ND-147 O.OOOE+OO 4.887E+07 O.OOOE+OO SHORT HLIF PM-147 -3.412E+Ol 7.324E+02 1.361E+03 NOT IDENT. PM-149 O.OOOE+OO 1.237E+41 O.OOOE+OO SHORT HLIF EU-150 -l.696E-03 2.627E-02 4.539E-02 FAIL ABUN EU-152 1.567E-02 9.275E-02 l.811E-01 FAIL ABUN GD-153 -5.762E-02 1.549E-01 2.621E-01 NOT IDENT. EU-154 -3.713E-02 8.688E-02 1.589E-01 FAIL ABUN TB-160 1.226E+OO 1.504E+OO 3.373E+OO FAIL ABUN H0-166M 1.593E-03 4.615E-02 8.804E-02 FAIL ABUN TM-171 5.599E+OO 9.701E+OO 1.982E+Ol NOT IDENT. HF-172 8.408E-03 2.042E-01 3.808E-01 FAIL ABUN LU-172 -4.981E-03 6.783E-02 1.315E-01 FAIL ABUN LU-176 3.662E-03 2.207E-02 4.363E-02 FAIL ABUN HF-181 -8.016E-01 4.807E+00 8. 964E+OO NOT IDENT. Page 3272 of 5809 TA-182 8.139E-02 8. 541E-01 l.666E+OO FAIL ABUN RE-183 1.166E+OO 1. 691E+OO 3.450E+OO NOT IDENT. RE-184 9.775E+OO 2.902E+Ol 6.016E+Ol NOT IDENT. W-188 8.433E+00 l .113E+02 1. 983E+02 FAIL ABUN IR-192 3.218E-01 4.774E-01 9. 718E-01 FAIL ABUN HG-203 l.448E+OO 2.448E+OO 4.597E+OO NOT IDENT. BI-207 -l.332E-02 3. 611E-02 6.789E-02 FAIL ABUN PB-210 -4.432E-01 1.285E+OO 2.558E+OO NOT IDENT. BI-211 O.OOOE+OO 4.868E-01 7.353E-01 FAIL ABUN PB-211 3.733E-01 6. 982E-0.l l.277E+OO NOT IDENT. BI-212 O.OOOE+OO 6.990E-01 l.187E+OO FAIL ABUN RN-219 5.585E-03 3.627E-01 6.966E-01 FAIL ABUN RA-223 5.092E-01 5.614E-01 1.083E+OO FAIL ABUN AC-227 1.163E-01 2.215E-01 4.484E-01 FAIL ABUN TH-227 1.163E-01 2.215E-01 4.484E-01 FAIL ABUN TH-229 -4.498E-02 4.879E-01 8.695E-01 FAIL ABUN TH-231 5.092.E-01 5.614E-01 l.083E+OO FAIL ABUN PA-233 -5.449E-03 5.268E-02 1.020E-01 FAIL ABUN PA-234 l.837E-01 2.256E-01 4.892E-01 FAIL ABUN PA-234M -2.650E+OO 3.674E+OO 6.504E+OO NOT IDENT. U-235 l.255E-01 l.698E-01 3.256E-01 FAIL ABUN NP-237 -5.449E-03 5.268E-02 l.020E-01 FAIL ABUN NP-238 O.OOOE+OO 1.637E+41 O.OOOE+OO SHORT HLIF NP-239 2.723E-02 2 .115E-01 3.989E-01 FAIL ABUN PU-239 2.824E+02 2.898E+02 5.698E+02 NOT IDENT. AM-241 4.583E-03 8.366E-02 l.516E-01 NOT IDENT. CM-243 2.000E-02 7.881E-02 l.415E-01 FAIL ABUN BK-247 -7.230E-02 6.601E-02 l.191E-01 FAIL ABUN CM-247 1. 871E-02 3.313E-02 6.670E-02 FAIL ABUN CF-249 l.475E-02 3.654E-02 7.250E-02 NOT IDENT. CF-251 1.980E-02 l.136E-01 2.084E-01 NOT IDENT. Page 3273 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:18:23.76 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 409 10.66* l.403E+OO 1.319E+Ol l.319E+Ol 10.43 C0-58 810.76 12 99.45* 2.251E+OO 2.571E-02 5.127E-01 156.68 CD-109 88.03 139 3.70* 7.568E+OO 2.392E+OO 3.788E+OO 45.93 SN-126 64.28 89 9.60 5.536E+OO 8.091E-01 8.091E-01 93.09 86.94 139 8.90 7.568E+OO 9.944E-01 9.944E-01 45.93 87.57 139 37.00* 7.568E+OO 2.392E-01 2.392E-01 45.93 BA-137M 661. 66 1007 89.90* 2.624E+OO 2.058E+OO 2.098E+OO 7.49 CS-137 661.66 1007 85.10* 2.624E+00 2.174E+OO 2.216E+OO 7.49 EU-155 86.55 139 30.70 7.568E+OO 2.883E-01 3.258E-01 45.93 105.31 51 21.10* 8.063E+OO l.433E-01 l.619E-01 84.59 TL-208 277.37 46 6.60 5.128E+OO 6.519E-01 6.519E-01 125.97 583.19 133 85.00* 2.886E+00 2.619E-01 2.619E-01 30.18 860.56 25 12.50 2.150E+OO 4. 481E-01 4. 481E-01 135.31 BI-211 72.87 ------1. 23 6.585E+OO ------Line Not Found ------351.06 337 12.92* 4.262E+OO 2.946E+OO 2.946E+OO 16.86 PB-212 74.82 263 10.28 6.758E+00 1.827E+OO *1. 827E+OO 32.07 77 .11 339 17.10 6.949E+OO 1.376E+OO 1.376E+OO 19.56 238.63 551 43.60* 5.747E+OO 1.060E+OO 1.060E+OO 11. 65 300.09 46 3.30 4.829E+OO 1. 402E+OO l.402E+OO 79.42 BI-214 609.32 152 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 1120.29 49 14.92 1. 754E+OO 9.007E-01 9.0lOE-01 59.54 1764.49 35 15.30 l.177E+OO 9.458E-01 9.461E-01 40.84 PB-214 74.82 263 5.80 6.758E+OO 3.238E+OO 3.239E+OO 32.07 77 .11 339 9.70 6.949E+OO 2.425E+OO 2.426E+OO 19.56 87.09 139 3.41 7.568E+OO 2.595E+OO 2.596E+OO 45.93 242.00 152 7.25 5.697E+OO 1. 767E+OO 1.768E+OO 52. 67 295.22 205 18.42 4.889E+OO 1.099E+OO l.lOOE+OO 22.56 351. 93 337 35.60* 4. 2 62E+OO 1.069E+OO 1.070E+00 16.86 RN-222 609.32 152 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 1120.29 49 14.92 1.754E+OO 9.007E-01 9.0lOE-01 59.54 1764.49 35 15.30 l.177E+OO 9.458E-01 9.461E-01 40.84 RA-224 240.99 152 4.10* 5.697E+OO 3.125E+OO 3.125E+OO 52.67 RA-226 609.32 152 45.49* 2.791E+OO 5.775E-01 5.777E-01 29.30 1120.29 ' 49 14.92 1. 754E+OO 9.007E-01 9.0lOE-01 59.54 1764.49 35 15.30 1.177E+OO 9.458E-01 9.461E-01 40.84 AC-228 105.21 51 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 338.32 68 11.27 4.394E+OO 6.612E-01 6.612E-01 69.99 794.95 ------4.25 2.286E+OO ------Line Not Found ------835.71 ------1. 61 2.201E+OO ------Line Not Found ------911.20 107 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 968. 97 52 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 RA-228 105.21 51 1.10 8.063E+OO 2.748E+00 2.748E+OO 84.59 33,8. 32 68 11. 27 4.394E+OO 6.612E-01 6.612E-01 69.99 794.95 ------4.25 2.286E+OO ------Line Not Found ------835. 71 ------1. 61 2.201E+OO ------Line Not Found ------911.20 107 25.80* 2.060E+OO 9.737E-01 9.737E-01 29.57 968. 97 52 15.80 1. 966E+00 8.046E-01 8.046E-01 40.21 Page 3274 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 .263 10.28 6.758E+OO 1.827E+OO 1.827E+OO 32.07 77 .11 339 17.10 6.949E+OO 1.376E+OO l.376E+OO 19.56 238.63 551 43.60* 5.747E+OO 1.060E+OO 1.060E+OO 11. 65 300.09 46 3.30 4.829E+OO 1.402E+OO l.402E+OO 79.42 TH-230 609.32 152 45.49* 2.791E+OO 5.775E-01 5.775E-01 29.30 1120. 29 49 14.92 1. 754E+OO 9.007E-01 9.007E-01 59.54 1764.49 35 15.30 1.177E+OO 9.458E-01 9.458E-01 40.84 PA-231 283.69 ------1. 70 5.044E+OO ------Line Not Found ------301.36 46 5.35* 4.829E+OO 8.646E-01 8.646E-01 79.42 TH-232 105.21 51 1.10 8.063E+OO 2.748E+OO 2.748E+OO 84.59 338.32 68 11.27 4.394E+OO 6.612E-01 6.612E-01 69.99 835. 71 ------1. 61 2.201E+OO ------Line Not Found ------911. 20 107 25.80* 2.060E+00 9.737E-01 9.737E-01 29.57 968. 97 52 15.80 1. 966E+OO 8.046E-01 8.046E-01 40.21 TH-234 63.29 89 3.70* 5.536E+OO 2.099E+OO 2.099E+00 93.09 92.59 81 4.23 7.800E+OO 1.184E+OO 1.184E+OO 78.13 U-234 609.32 152 45.49* 2.791E+OO 5.775E-01 5.775E-01 29.30 1120. 29 49 14.92 1. 754E+OO 9.007E-01 9.007E-01 59.54 1764.49 35 15.30 1.177E+OO 9.458E-01 9.458E-01 40.84 U-238 63.29 89 3.70* 5.536E+OO 2.099E+OO 2.099E+OO 93.09 92.59 81 4.23 7.800E+OO 1.184E+OO 1.184E+OO 78.13 AM-243 43.53 ------5.90 2. 021E+OO ------Line Not Found ------74.66 263 67.20* 6.758E+OO 2.795E-01 2.795E-01 32.07 ANH-511 511. 00 37 100.00* 3.192E+OO 5.553E-02 5.553E-02 155.34 Flag: "*" Key line Page 3275 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235018 Acquisition date 3-0CT-2016 08:16:22 Total number of lines in spectrum 53 Number of unidentified lines 15 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 70.86D 461.40D 2.30E+05Y 30.08Y 30.08Y 4.75Y 1. 41E+10Y 7.04E+08Y l.41E+10Y 1600. DOY 1600. DOY 1600. DOY 1. 41E+10Y 1600. ODY 1.41E+10Y 1.41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 19.9 1. 58 1. 00 1. 02 1. 02 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.319E+Ol 2. 571E-02 2.392E+OO 2.392E-01 2.058E+OO 2.174E+OO 1.433E-01 2.619E-01 2.946E+OO 1.060E+OO 5.775E-01 1.069E+OO 5.775E-01 3.125E+00 5.775E-01 9.737E-01 9.737E-01 l.060E+00 5.775E-01 8.646E-01 9.737E-01 2.099E+OO 5.775E-01 2.099E+OO 2.795E-01 5.553E-02 4.095E+Ol 4.095E+Ol Decay Corr pCi/GRAM 1.319E+Ol 5.127E-01 3.788E+OO 2.392E-01 2.098E+OO 2.216E+OO 1.619E-01 2.619E-01 2.946E+OO 1.060E+00 5.777E-01 1. 070E+OO 5.777E-01 3.125E+OO 5.777E-01 9.737E-01 9.737E-01 1.060E+OO 5.775E-01 8.646E-01 9.737E-'01 2.099E+OO 5.775E-01 2.099E+OO 2.795E-01 5.553E-02 4.294E+Ol 4.294E+Ol 71. 70% Decay Corr 2-Sigma Error 0.138E+Ol 8.033E-01 l.740E+OO 1.099E-01 0.157E+OO 0.166E+OO l.369E-01 0.791E-01 0.497E+OO 0.124E+OO l.693E-01 0.180E+OO 1.693E-01 1.646E+OO 1.693E-01 2.879E-01 2.879E-01 0.124E+OO 1.692E-01 6.866E-01 2.879E-01 1.954E+OO l.692E-01 1.954E+OO 0. 896E-01 8.627E-02 "M" Manually accepted 2-Sigma %Error 10.43 156.68 45.93 45.93 7.49 7.49 84.59 30.18 16.86 11. 65 29.30 16.86 29.30 52. 67 29.30 29.57 29.57 11. 65 29.30 79.42 29.57 93.09 29.30 93.09 32.07 155.34 Flags: "K" "E" Keyline not found Manually edited "A" = Nuclide specific abn. limit Page 3276 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235018 Acquisition date : 3-0CT-2016 08:16:22 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.74 34 258 l. 52 166.81 165 7 7.29E-03 **** 7.38E+OO T 3 95.46 62 195 l. 41 190.27 182 13 1.35E-02 **** 7.87E+OO T 0 136.89 65 170 0.90 273.15 270 8 l. 45E-02 81. 7 7.87E+OO T 0 1.86.02 80 246 l. 01 371.45 366 11 1.84E-02 89.9 6.81E+OO T 0 270.35 54 108 l. 76 540.18 536 9 l.29E-02 80.7 5.23E+00 T 0 328.39 62 86 2.34 656.30 651 10 l.52E-02 65.3 4.50E+OO T 0 394.83 23 69 0.72 789.24 786 8 5.71E-03 **** 3.89E+00 0 408.86 52 58 1.14 817.32 813 9 l. 30E-02 62. 6 3.79E+OO 0 536.91 47 57 7.37 1073.53 1065 19 l.20E-02 85.6 3.07E+OO T 0 554.81 19 41 3.48 1109.35 1101 13 4.98E-03 **** 3.00E+OO 0 645.81 24 28 2.44 1291.43 1286 12 6.33E-03 **** 2.67E+OO T 0 654.80 21 36 4.26 1309.43 1300 15 5.38E-03 **** 2.64E+00 0 722. 27 17 18 3.38 1444.45 1439 10 4.40E-03 **** 2.46E+00 T 0 726. 97 52 24 l. 90 1453.85 1449 11 l.37E-02 46.5 2.44E+OO T 0 755.46 21 19 l. 54 1510.85 1507 9 5.56E-03 88.6 2.38E+OO T 0 816.68 42 15 4.54 1633.37 1625 19 1.12E-02 54.9 2.24E+OO T 0 953.31 11 9 l. 71 1906. 78 1900 9 3.llE-03 **** 1.99E+OO T 2 964.74 35 16 2.24 1929.66 1923 22 9.46E-03 57.3 1.97E+00 T 0 1150. 90 14 12 3.15 2302.21 2296 12 3.89E-03 **** 1. 72E+OO 0 1255.13 9 18 2.84 2510.82 2500 15 2.40E-03 **** 1.60E+OO 0 1301.45 7 20 2.68 2603.53 2591 14 2.04E-03 **** 1. 55E+OO 0 1314.68 8 5 0.90 2629.99 2622 11 2.38E-03 **** 1.54E+OO 0 1318.32 12 5 2.18 2637.29 2632 10 3.33E-03 90.5 1. 53E+OO 0 1339.26 5 10 0.51 2679.20 2668 14 l.48E-03 **** 1. 51E+OO 0 1377. 72 16 6 1. 08 2756.18 2750 13 4.58E-03 80.5 l.48E+OO 0 1480.60 10 3 2.96 2962.08 2956 12 2.74E-03 95.3 1.39E+OO 3 1588.20 12 1 2.90 3177.46 3174 16 3.53E-03 59.0 1.30E+OO 3 1592.38 10 3 l. 91 3185.83 3174 16 3.02E-03 78.1 1.30E+OO 0 1847.52 14 0 l. 98 3696.53 3690 11 4.17E-03 51.6 1.12E+OO Flags: "T" = Tentatively associated Page 3277 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:18:38.22 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l *
  • Acquisition date 3-0CT-2016 08:16:22 Sensitivity 3.000 *
  • Detector ID GAM27 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.98 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:19:00 Nuclide Library : SOLID *
  • Sample ID G405235018 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.5582E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;l3
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 EU-155 TL-208 PB-212' BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.059E-01 4.291E-01 8.062E-01 5.104E-02 2.650E-02 2.800E-02 7.300E-02 2. 717E-02 3.978E-02 5.525E-02 5.445E-02 5.525E-02 4.264E-01 5.525E-02 8. 966E-02 8.966E-02 3.978E-02 5.523E-02 3.683E-01 8. 966E-02 6.868E-01 5.523E-02 6.868E-01 3.084E-02 2.308E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3278 of 5809 Le (pCi/GRAM 1.236E+Ol 2.682E-02 O.OOOE+OO 3.121E-02 2. 968E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-'149 EU-150 EU-152 GD...:.153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 3279 of 5809 O.OOOE+OO 5.320E-02 3.152E-01 O.OOOE+OO 3.688E-02 5.212E+OO 2.073E-02 1. 572E-01 1.697E+OO 4.043E+OO O.OOOE+OO l.630E-01 O.OOOE+OO O.OOOE+OO 5.599E-01 5.749E+OO 6.477E-01 G.OOOE+OO 1.935E-01 4*. 801E+02 2.546E-02 6.709E-01 2.141E+OO 1.290E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.697E-02 4.229E-02 6.159E+OO 3.569E-01 3.569E-01 2.456E-02 7.234E-02 l.907E-01 O.OOOE+OO O.OOOE+OO 1.040E-01 1.346E+OO 9.855E-02 2.253E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.509E-02 O.OOOE+OO 4.613E-02 1.141E-01 O.OOOE+OO O.OOOE+OO 8.617E-02 O.OOOE+OO O.OOOE+OO 2.195E+Ol O.OOOE+OO 3.000E-01 3.636E-02 3.162E+OO 3.882E-02 O.OOOE+OO 6.429E+02 O.OOOE+OO 2.107E-02 8.440E-02 l.237E-01 6.668E-02 l.491E+OO 3.904E-02 9.380E+OO 1. 799E-01 5. 772E-02 2.028E-02 4.108E+OO 7.375E-01 SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3280 of 5809 1.636E+OO 2. 672E+Ol 9 .196E+Ol 4.545E-01 2.143E+OO 2.900E-02 l.215E+OO 3.554E-01 5.915E-01 5.528E-01 3.216E-01 5.038E-01 2. llOE-01 2. llOE-01 4 .113E-01 5.038E-01 4. 724E-02 2.170E-01 2.840E+OO 1. 54 6E-01 4. 724E-02 O.OOOE+OO 1.886E-01 2.711E+02 7.188E-02 6.651E-02 5.523E-02 3.090E-02 3.364E-02 9.851E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:18:43.44 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235018.CNF;l *
  • Acquisition date 3-0CT-2016 08:16:22 Sensitivity : 3.000 *
  • Detector ID GAM27 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.98 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:19:00 Nuclide Library : SOLID *
  • Sample ID G405235018 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.5582E+02 GRAM *
  • Quantity Err(%) : 1.2836E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-0CT-2016 0'6: 09: 32 Eff. Geometry : CAN ' *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;l3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.319E+Ol 1.514E+OO 1.514E+OO C0-58 5.127E-01 7.876E-01 7.876E-01 CD-109 2.183E+OO 1. 762E+OO 1. 762E+OO SN-126 l.379E-01 l. llOE-01 1. llOE-01 BA-137M 2.098E+OO l.785E-01 l.785E-01 CS-137 2.216E+OO l.885E-01 l.885E-01 EU-155 l.619E-01 1. 34 7E-01 1. 34 7E-01 TL-208 2.619E-01 7.827E-02 7.827E-02 PB-212 1.060E+00 l.338E-01 1.338E-01 BI-214 5.777E-01 1.677E-01 1.677E-01 PB-214 1.070E+OO 1.824E-01 1. 824E-01 RN-222 5.777E-01 1.677E-01 1.677E-01 RA-224 1.181E+OO 1.676E+OO 1.676E+OO RA-226 5.777E-01 1.677E-01 l.677E-01 AC-228 9.737E-01 2.865E-01 2.865E-01 RA-228 9.737E-01 2.865E-01 2.865E-01 TH-228 1.060E+OO 1.338E-01 l.338E-01 TH-230 5.775E-01 1.677E-01 1.677E-01 PA-231 8.646E-01 6.978E-01 6.978E-01 TH-232 9.737E-01 2.865E-01 2.865E-01 TH-234 2.099E+OO 1.971E+OO 1.971E+OO U-234 5.775E-01 1.677E-01 1.677E-01 U-238 2.099E+OO 1. 971E+OO 1.971E+OO AM-243 1. 846E-01 9.180E-02 9.180E-02 ANH-511 5.553E-02 '8.457E-02 8.457E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 1.854E+OO l.400E+Ol 1.403E+Ol NOT IDENT. NA-2,2 -1.638E-02 3.531E-02 3.607E-02 NOT IDENT. NA-24 -1.000E+41 5.275E+41 O.OOOE+OO SHORT HLIF AL-26 3.874E-02 2.739E-02 3.249E-02 NOT IDENT. SC-46 9.603E-02 3.228E-01 3.257E-01 FAIL ABUN Page 3281of5809 V-48 2.628E+03 1.790E+04 1. 794E+04 SHORT HLIF CR-51 -1.305E+02 4.233E+02 4.274E+02 SHORT HLIF MN-54 5.415E-02 5. 311E-02 5.845E-02 NOT IDENT. C0-56 -2.903E-01 4.019E-01 4.227E-01 NOT IDENT. MN-56 -l.000E+41 1.392E+41 O.OOOE+OO SHORT HLIF C0-57 -3.318E-03 4.215E-02 4.217E-02 FAIL ABUN FE-59 -3.865E+OO 6.694E+OO 6.917E+OO NOT IDENT. C0-60 1.028E-02 2.365E-02 2.410E-02 NOT IDENT. ZN-65 6.215E-02 1. 965E-01 l.985E-01 NOT IDENT. GE-68 -2.862E-01 2.015E+OO 2.019E+OO NOT.IDENT. AS-73 -3.048E+OO 4.600E+OO 4.801E+OO NOT IDENT. AS-74 7.101E+03 6.829E+03 7.543E+03 SHORT HLIF SE-75 -2.039E-01 1.945E-01 2.152E-01 FAIL ABUN BR-77 l.125E+39 9.939E+39 O.OOOE+OO SHORT HLIF SR-82 2.157E+02 7.184E+02 7.250E+02 SHORT HLIF RB-83 -4.170E-01 6.992E-01 7.241E-01 NOT IDENT. KR-85 -4.591E+OO 8.088E+OO 8.349E+OO NOT IDENT. SR-85 -5.166E-01 9. lllE-01 9.404E-01 NOT IDENT. RB-86 -l.055E+04 2.974E+04 3.012E+04 SHORT HLIF Y-88 l.816E-02 2.207E-01 2.209E-01 NOT IDENT. Y-91 3.156E+02 5.165E+02 5.357E+02 NOT IDENT. NB-94 1.547E-02 2.818E-02 2.903E-02 NOT IDENT. NB-95 -5.483E-01 8.884E-01 9.221E-01 NOT IDENT. NB-95M -4.289E-01 2.602E+OO 2.609E+OO NOT IDENT. ZR-95 2.137E+OO 1.858E+OO 2.093E+OO FAIL ABUN NB-97 l.000E+41 2.235E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.000E+41 2.432E+42 O.OOOE+OO SHORT HLIF M0-99 2. 651E+32 6.463E'+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 8.974E+40 0.000E+OO SHORT HLIF RH-101 -1.392E-02 3.183E-02 3.245E-02 NOT IDENT. RH-102 3.331E-03 4.936E-02 4.938E-02 NOT IDENT. RU-103 5.173E+OO 6.566E+00 6.968E+OO FAIL ABUN RH-106 -2.414E-01 4.564E-01 4.692E-01 NOT IDENT. RU-106 -2.414E-01 4.564E-01 4.692E-01 NOT IDENT. AG-108M -2.565E-02 3.070E-02 3.280E-02 FAIL ABUN AG-llOM -2.689E-02 8.627E-02 8.712E-02 NOT IDENT. SN-113 -8.626E-02 2.514E-01 2.543E-01 NOT IDENT. CD-115 -8.038E+37 l.908E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 5.614E+03 1.178E+05 l.178E+05 SHORT HLIF TE-123M -2.056E-02 1.222E-01 1. 22 6E-01 NOT IDENT. SB-124 -6.167E-02 l.663E+OO l.664E+OO FAIL ABUN SB-125 4.597E-02 1.077E-01 l.097E-01 NOT IDENT. TE-125M 1.914E+02 2.397E+02 2.548E+02 NOT IDENT. I-126 2.786E+05 l.295E+06 l.301E+06 SHORT HLIF SB-126 1.358E+05 1.595E+06 1. 596E+06 SHORT HLIF SB-127 -2. 715E+22 6.816E+22 O.OOOE+OO SHORT HLIF I-131 -9.392E+08 8.587E+09 8.598E+09 SHORT HLIF I-132 -l.OOOE+41 1. 962E+42 O.OOOE+OO SHORT HLIF TE-132 -2.444E+26 1.318E+27 O.OOOE+OO SHORT HLIF BA-133 -4.407E-02 4.774E-02 5 .171E-02 FAIL ABUN I-133 1.000E+41 2.749E+41 O.OOOE+OO SHORT HLIF CS-134 3.050E-02 5.161E-02 5.341E-02 NOT IDENT. CS-135 1.794E-02 1.364E-01 1.367E-01 NOT IDENT. I-135 1.000E+41 7.102E+41 O.OOOE+OO SHORT HLIF CS-136 -6.038E+04 4.065E+05 4.074E+05 SHORT HLIF CE-139 9.394E-03 9.940E-02 9.949E-02 NOT IDENT. BA-140 5.050E+06 4.240E+06 4.812E+06 SHORT HLIF LA-140 -1. 231E+05 4.524E+05 4.558E+05 SHORT HLIF CE-141 -1.689E+Ol 2.670E+Ol 2.776E+Ol NOT IDENT. CE-143 l.000E+41 2.263E+41 O.OOOE+OO SHORT HLIF CE-144 2. 211E-01 3.519E-01 3.657E-01 NOT IDENT. PM-144 -l.013E-02 4.503E-02 4.526E-02 NOT IDENT. PR-144 -l.243E+00 3.975E+OO 4.014E+OO NOT IDENT. PM-146 8. 201E-03 4.350E-02 4.366E-02 NOT IDENT. ND-147 7.012E+06 4.887E+07 4.897E+07 SHORT HLIF PM-147 -3.412E+Ol 7 .* 324E+02 7.326E+02 NOT IDENT. PM-149 1.000E+41 1.256E+41 0.000E+OO SHORT HLIF EU-150 -1.696E-03 2.627E-02 2.628E-02 FAIL ABUN EU-152 1.567E-02 9.276E-02 9.303E-02 FAIL ABUN GD-153 -5.762E-02 1. 549E-01 1. 571E-01 NOT IDENT. EU-154 -3. 713E-02 8.689E-02 8.849E-02 FAIL ABUN TB-160 1.226E+OO 1. 506E+OO 1.604E+OO FAIL ABUN H0-166M 1.593E-03 4.615E-02 4.615E-02 FAIL ABUN TM-171 5.599E+OO 9. 713E+OO l.004E+Ol NOT IDENT. HF-172 8.408E-03 2.042E-01 2.042E-01 FAIL ABUN LU-172 -4.981E-03 6.783E-02 6.787E-02 FAIL ABUN LU-176 3.662E-03 2.207E-02 2.213E-02 FAIL ABUN HF-181 -8.016E-01 4.807E+OO 4.820E+OO NOT IDENT. Page 3282 of 5809 TA-182 8.139E-02 8. 541E-01 8.549E-01 FAIL ABUN RE-183 1.166E+OO 1. 701E+OO 1. 781E+OO NOT IDENT. RE-184 9.775E+OO 2.912E+Ol 2.945E+Ol NOT IDENT. W-188 8.433E+OO l .113E+02 l.114E+02 FAIL ABUN IR-192 3.218E-01 4.776E-01 4.992E-01 FAIL ABUN HG-203 1. 448E+OO 2.449E+OO 2.534E+OO NOT IDENT. BI-207 -1.332E-02 3.611E-02 3.661E-02 FAIL ABUN PB-210 -4.432E-01 1.285E+OO 1.301E+OO NOT IDENT. BI-211 2.946E+00 5.046E-01 1. 421E+OO FAIL ABUN PB-211 3.733E-01 6.985E-01 7.185E-01 NOT IDENT. BI-212 1.534E+OO 7.033E-01 9.862E-01 FAIL ABUN RN-219 5.585E-03 3.627E-01 3.627E-01 FAIL ABUN RA-223 5.092E-01 5.623E-01 6.074E-01 FAIL ABUN AC-227 l.163E-01 2.221E-01 2.282E-01 FAIL ABUN TH-227 l.163E-01 2. 221E-01 2.282E-01 FAIL ABUN TH-229 -4.498E-02 4.879E-01 4.883E-01 FAIL ABUN TH-231 5.092E-01 5.623E-01 6.074E-01 FAIL ABUN PA-233 -5.449E-03 5.268E-02 5.274E-02 FAIL ABUN PA-234 1.837E-01 3.083E-01 3.193E-01 FAIL ABUN PA-234M -2.650E+OO 3.675E+OO 3.865E+OO NOT IDENT. U-235 1.255E-01 l.699E-01 1. 791E-01 FAIL ABUN NP-237 -5.449E-03 5.268E-02 5.274E-02 FAIL ABUN NP-238 -l.000E+41 1.638E+41 O.OOOE+OO SHORT HLIF NP-239 2. 723E-02 2 .115E-01 2 .119E-01 FAIL ABUN PU-239 2.824E+02 2. 901E+02 3.168E+o2 NOT IDENT. AM-241 4.583E-03 8.366E-02 8.368E-02 NOT IDENT. CM-243 2.000E-02 7.883E-02 7.935E-02 FAIL ABUN BK-247 -7.230E-02 6.760E-02 7.505E-02 FAIL ABUN CM-247 1. 871E-02 3.328E-02 3.434E-02 FAIL ABUN CF-249 1. 4 7 5E-02 3.656E-02 3. 716E-02 NOT IDENT. CF-251 1.980E-02 l.136E-01 1.140E-01 NOT IDENT. .1 Page 3283 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 87.8545 87.09 159.0519 136.47 79.3663 45.60 104.5483 87.57 138.2499 140.51 0.0000 46.54 100.0665 88.03 138.3703 143.76 89.3306 49.72 0.0000 88.34 165.0228 144.24 77.9277 51. 35 106.2390 88.47 165.0636 145.44 111. 3422 51. 87 93.8141 89. 96 111. 5187 152.43 84. 5711 52.39 88.1330 1093.63 134.8350 153.25 0.0000 52.97 102.8177 91.11 0.0000 323.87 92.8943 53.44 113.6281 92.59 133.2050 156.02 0.0000 54.07 94.3593 93.35 133.3905 158.56 0.0000 57.36 0.0000 94.56 133.6827 159.00 87.6228 57.53 96.1768 94.65 133.7039 162.33 90.3354 57.98 92.3545 94.67 133.7087 162.66 0.0000 59.27 109.0760 94.87 133.7572 163.33 97. 4961 59.32 109.0895 97.43 105.2203 165.86 77.7687 59.54 109.1482 98.43 86.8883 176.31 89.4882 60. 96 102.9268 98.44 86.8901 176.60 0.0000 61.17 100.3383 99.53 78.4929 177.52 94.3947 62.93 131. 2527 100 .11 92.1433 181.07 0.0000 63.29 131. 3635 102.03 83.1325 181.52 94.4334 63.58 131.4532 103.18 74.6791 184.41 98.7601 64.28 131.6682 103.37 74.7029 143.76 98.9077 66.73 101. 6488 105.21 82.1410 193.51 104.6367 67.24 125.8688 105.31 82.1544 197.03 106.2609 125.81 143.7539 106.12 96. 6983 198.01 91.7015 67.75 143.7757 106.47 96.7548 201.83 87.1683 69.67 123.1886 109.28 80.5203 203.43 94.6956 70.83 125.5269 111. 00 97.1129 205.31 77.6320 72. 81 143.6872 111.76 0.0000 210.85 87. 9971 72. 87 143.7056 114.06 89.9149 215.65 77.2219 74.66 130.6455 116. 30 0.0000 222 .11 90.2615 74.82 130.6895 116.74 96.9026 227.09 84.8273 74.97 130.7305 119.76 92.9318 227.38 78.1301 77 .11 131.3145 121.12 90.9081 228.16 0.0000 78.74 135.8712 121.22 97.5746 228.18 81. 5546 79.69 123.7582 121.78 97.6579 116.74 81. 5546 80.12 125.2416 122.06 95.4791 235.69 94.0040 80.19 0.0000 122.92 101.1614 235. 96 70.3099 80.57 119.8445 123.07 104.5201 238.63 70.4880 81. 00 128.2203 265.00 94.5997 238.98 0.0000 81. 07 117.8965 125.81 97.1342 240.99 70.6451 81. 75 120.1277 127.23 117.4769 242.00 70,7118 83.79 137.2469 127.91 113 .1153 244.70 55.0892 84.00 137.3033 129.30 98.7556 252.40 0.0000 85.43 100 .1345 131.20 133.9149 252.80 83.4650 86.55 100.3499 133. 02 87.2537 254.15 0.0000 86.79 158. 9603 133.52 88.8205 256.23 72.5024 86.94 159.0056 136.00 90.6445 260.90 0.0000 Page 3284 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 76.5256 355.39 0.0000 584.27 33.0334 264.80 73.0557 356.01 67.2539 595.83 0.0000 265.00 79.1584 364.49 0.0000 427.87 25.7744 268.22 62.8066 366.42 0.0000 602.52 0.0000 269.46 68.1135 372.51 44.4058 604. 72 27.4382 270.03 68.1469 375.05 59.6252 607.14 .37.1644 271.23 66.4675 377.52 65. 4119 609.32 36.6632 273.65 0.0000 356.01 40. 9371 610.33 36.6798 276.40 59.7352 388.16 47.7376 614.28 38.9092 277.37 59.7836 388.63 0.0000 618.01 25.9844 277.60 59.7961 391.69 50.2409 620. 36 28.1794 278.00 59.8154 264.66 56.7901 621.93 30.3698 279.20 50.1904 401.81 48.1628 630.19 0.0000 279.54 50.2055 402.40 42.3994 631.29 21.7847 279.70 54.1754 404.85 41. 9840 633.25 23.9846 280.46 51.5660 410. 95 . 50.8669 634.78 0.0000 283.69 60.9857 413.71 40.7644 635.95 17.4648 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 53.1079 423.72 0.0000 645.85 26.3135 285.90 0.0000 427.09 52.8475 657.76 13.2261 287.50 51. 4261 427.87 46.9980 657.90 0.0000 290.67 53.3374 433.94 62.8971 661. 66 28.1531 293.27 0.0000 439.40 65.0762 664.57 0.0000 351. 93 62.4577 453.88 42.7629 666.33 0.0000 295. 96 62.4961 463.37 61.9987 666.50 0.0000 879.38 62.6272 468.07 61.1638 667.71 0.0000 299.98 62.6984 473.00 0.0000 677.62 24.4573 300.09 62.7026 475.06 46.3070 685.70 0.0000 300.13 62.7055 476.78 51. 3901 695.00 0.0000 301.36 64.5601 477.60 45.3653 696.49 22.4129 302.85 61.9431 482.18 43.4610 696.51 23.5336 256.23 55. 0130 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.6623 306.78 54.9325 497.08 35.6672 697.49 24.6641 308.46 57.7096 505.52 19. 9630 702.65 22.4707 311. 90 54.2480 507 .. 63 0.0000 706.68 24.7590 316.51 55.3483 511. 00 40.0438 711.68 18.0436 319.41 0.0000 514.00 53. 9911 720.70 0.0000 320.08 0.0000 514.00 53. 9911 721. 93 0.0000 321.04 61.0036 520.40 44.3717 722.78 10 .1960 323.87 41.0605 520.69 0.0000 722.91 10 .1964 325.23 47.9530 522.65 0.0000 723. 31 10.1982 328.76 0.0000 527.90 0.0000 724.19 10.2019 333.37 67.5440 528.26 29.0117 727. 33 15.3221 333.97 57.9205 529.59 28.6175 733.00 17.7461 334.37 52 .. 4193 529.87 0.0000 735.93 22.7783 338.28 71.0157 531. 02 0.0000 333.97 20.5129 338.32 71.0173 537.26 0.0000 739.50 0.0000 311. 90 63.7399 546.56 0.0000 747.24 19.4494 340.48 63.7399 552.55 25.1787 748.06 13.7334 340.55 0.0000 563.25 44.2986 752.31 24.0736 344.28 59.2839 569.33 39.1424 753.82 0.0000 345.93 58.9832 946.00 39.1454 756.73 20.6704 351. 06 49.3327 569.70 39.1484 756.80 20.6711 351.93 49.3640 583.19 33.0170 884.68 18.4258 Page 3285 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 34.5728 1274.44 11. 2401 1620.50 9.8849 766.42 31.1232 1001.03 20.6378 1621. 92 14.2830 766.84 31.1287 1002.74 21. 5878 1678.03 0.0000 772. 60 0.0000 1004.73 19. 7227 1690.97 4.4578 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 .1025.87 0.0000 1764.49 3.6189 778.90 15.0577 1028.54 0.0000 1063.66 4.5288 783.70 0.0000 1037.84 16.1295 1771. 35 5.6622 785.37 17.4170 1038.76 0.0000 1791.20 0.0000 792.07 31.4308 631.29 17.1244 1808.65 0.9125 794.95 25.6380 1048.07 0.0000 1810.72 0.0000 795.86 25.6470 1049.04 22.8486 1836.06 6.4210 810.06 19.6896 1050.41 18. 0966 810.29 19.6909 1063.66 15.2998 344.28 19.6923 1077.00 0.0000 810.76 17.5842 1077.34 17.2815 815.77 0.0000 1085.87 17.3254 1048.07 0.0000 1093.63 18.3297 832.01 22.1527 1099.45 22.2251 834.85 14.1924 1112. 07 17.4573 835. 71 16.8587 1112. 84 24.3909 836.80 0.0000 1115. 54 21.7465 846.75 0.0000 1120.29 23.3320 846.77 23.1618 1120. 55 23.3335 856.80 0.0000 1221.41 23.3379 860.56 16 .1142 1129. 67 14.6210 871. 09 17.9712 1131. 51 0.0000 873.19 12.5892 1147.95 0.0000 875.33 0.0000 1173.23 17.7605 879.38 10.8142 1177.95 14.8196 880.51 17.1289 1189.05 20.8103 883.24 15.3404 1204.77 15.9229 884.68 20.7651 1221.41 18.9930 889.28 15. 3725 1231.02 23.0505 894.76 15.4016 1235.36 0.0000 898.04 14.5117 1238.28 27.1104 900.72 17.2489 1260.41 0.0000 903.28 17.2640 1271.87 9 .1165 911.20 17.3104 1274.44 13.1769 912.08 17.3156 1274.54 13.1769 923.98 0.0000 1291.59 16.2891 926.50 20.1470 1298.22 0.0000 929 .11 19.2479 1312 .11 0.0000 937.49 18.3820 1332. 49 3.2914 944 .13 0.0000 1362.66 0.0000 946.00 11. 5870 1365.19 14.5161 949.00 16.2374 1368. 63 0.0000 667.71 0.0000 1384.29 2.7777 962. 31 16.3083 1408.01 8.3804 964. 08 13.9069 1457.56 0.0000 966.17 13.9165 1460.82 7.4234 911.20 13.9288 1489.16 7.4717 968. 97 13.9288 1505.03 10.7117 983.53 0.0000 1584.12 6.9754 984.45 0.0000 1596.21 0.0000 Page 3286 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:21:30.20 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM11.CNF;517 Background date : Z-OCT-2016 11:00:34. Sample date 8-DEC-2015 14:30:00. Acquisition date : 3-0CT-2016 08:21:03. Sample ID G405235019 Sample quantity 1.75975E+02 GRAM Detector name : GAMll Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.63 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 0 0 0 0 0 0 2 2 4 4 4 4 4 0 0 0 0 0 1 1 0 0 0 0 0 0 6 6 0 0 0 Page 3287 of 5809 Energy 63.02* 74.87* 77.15* 83.89* 86.82 89.82 92.82* 185.56* 209.55 238.65* 241. 64 270.47 274.41 276.97 295.35* 300.14 338.45* 351.87* 415.66 428.86 469.33 491.68 494.93 498.75 510.95* 544.28 583.46* 609.42* 660. 96* 668.21 670. 7 5 701.59 727. 59* 747.05 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 26 137 212 45 58 64 59 175 50 400 100 56 40 20 182 38 83 248 34 10 25 15 16 32 18 12 160 167 23 28 9 16 40 20 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 272 156 134 165 157 123 156 124 127 90 95 52 44 72 55 53 87 51 112 41 25 25 18 23 45 22 29 44 18 19 11 38 18 17 1.13 0.88 0.91 1. 04 0.74 1. 37 1. 46 1. 20 1. 42 1. 03 1. 41 1. 75 1.20 1. 76 1. 36 1. 80 0.92 1. 32 7.63 1. 41 1. 81 1. 55 1. 55 3.26 1. 03 3.54 1. 56 1. 23 0.84 1. 54 1. 65 5.90 1. 92 1. 62 125.95 149.66 154.22 167.71 173.58 179.58 185.58 371.18 419.20 477.44 483.41 541.11 549.00 554.12 590.91 600.49 677.16 704.01 831.66 858.08 939.06 983.78 990.28 997.93 1022.34 1089.02 1167. 43 1219.36 1322.50 1337.00 1342.09 1403.77 1455.79 1494.74 122 146 146 165 172 177 182 365 414 473 473 537 537 537 586 586 672 698 813 851 935 977 977 993 1019 1081 1162 1214 1316 1333 1333 1395 1451 1490 11 7.13E-03127.l 14 3.80E-02 15.9 14 5.89E-02 11.0 7 1.26E-02 49.5 6 1.62E-02 36.4 6 1.78E-02 30.4 7 1. 65E-02 39. 8 13 4.85E-02 15.6 11 1.37E-02 46.2 15 1.llE-01 6.2 2.44E+OO 15 2.77E-02 21.6 27 1.57E-02 28.2 4.29E+OO 27 1. llE-02 31. l 27 5.44E-03 92.0 23 5.06E-02 9.9 3.06E+OO 23 1. 06E-02 45. 7 11 2.30E-02 24.7 12 6.89E-02 8.7 24 9.52E-03 84.0 9 2.79E-03120.8 9 6.91E-03 41.4 17 4.30E-03 63.8 1.99E+OO 17 4.46E-03 48.9 10 8.92E-03 32.8 9 4.92E-03 92.2 10 3.20E-03 82.5 14 4.45E-02 11.0 11 4.63E-02 11.2 11 6.49E-03 43.8 12 7.79E-03 27.8 9.15E+OO 12 2.38E-03 71.4 15 4.31E-03 89.8 11 l.12E-02 26.8 10 5.55E-03 45.0 Peak Search Report (continued) Page : 2 Sample ID : G405235019 Acquisition date 3-0CT-2016 08:21:03 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 768.97 24 27 2.85 1538.59 1533 11 6.59E-03 51. 5 36 0 817.97 15 14 3.22 1636.63 1631 11 4.13E-03 55.0 37 0 860 .. 97 28 12 1. 35 1722.66 1717 11 7.88E-03 31.1 38 0 911. 28* 87 19 2.09 1823.31 1817 15 2.41E-02 15.7 39 0 935.17 11 9 1. 29 1871.08 1867 8 3.18E-03 57.9 40 1 964. 79 26 20 1. 90 1930.35 1920 25 7.29E-03 33.5 1.53E+OO 41 1 968.79 50 15 1. 84 1938.35 1920 25 1.38E-02 21. 9 42 0 1003.33* 30 4 5.74 2007.44 2000 15 8.36E-03 25.3 43 0 1116.48 11 11 1. 51 2233.79 2225 12 3.03E-03 69.8 44 0 1120.37* 42 8 1. 39 2241.57 2237 10 1.17E-02 20.5 45 0 1153. 38 14 22 2.48 2307.60 2301 11 3.89E-03 70.2 46 0 1166 .18 10 7 2.27 2333.20 2329 7 2.78E-03 54.1 47 0 1336.20 9 4 0.68 2673.26 2669 8 2.36E-03 52.6 48 0 1377.44 18 5 2.28 2755.75 2750 10 5.00E-03 33.1 49 0 1415.36 12 0 0.83 2831.58 2827 9 3.33E-03 28.9 50 0 1460.91* 413 8 1. 73 2922.68 2915 14 l.15E-01 5.1 51 0 1509.86 7 5 1. 79 3020.57 3014 10 1.94E-03 70.7 52 0 1764.78* 32 3 2 .13 3530.35 3524 12 8.81E-03 22.1 53 0 1847.73 7 2 1. 26 3696. 23 3691 9 1. 90E-03 54.9 Flag: "*" = Peak area was modified by background subtraction Page 3288 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:21:32 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl 8-DEC-2015 14:30:00 G405235019 SOLID GAMMAll 0 01:00:00.00 1.50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 08:21:03 175.98 GRAM CAN 0 01:00:00.63 10.00 0.00 % Peak Energy 0.0% Interfering Interfered Nuclide Page 3289 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Nuclide RA-224 TH-229 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 85.43 86.94 87.57 88:03 74.66 74.82 74.82 351.06 Nuclide Line Activity Report Page : 2 Sample ID : G405235019 Acquisition date 3-0CT-2016 08:21:03 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.238E+OO 1.308E+Ol 1.308E+Ol 10.29 OK ZN-65 1115.54 50.60* 1.552E+OO 6.051E-02 l.418E-01 139.62 OK CD-109 88.03 3.70* 6.225E+OO 4.599E-01 7.215E-01 244.59 OK SN-126 64.28 9.60 3.845E+OO 4.320E-01 4.320E-01 254.25 OK 86.94 8.90 6.225E+OO l.912E-01 1.912E-01 244.59 OK 87.57 37.00* 6.225E+OO 4.599E-02 4.599E-02 244.59 OK BA-137M 661. 66 89.90* 2. 341E+OO 5.215E-02 5.314E-02 87.64 OK CS-137 661.66 85.10* 2.341E+OO 5.509E-02 5.614E-02 87.64 OK TL-208 277.37 6.60 4.720E+OO 3.303E-01 3.303E-01 183.91 OK 583.19 85.00* 2.581E+OO 3.483E-01 3.483E-01 21. 98 OK 860.56 12.50 l.906E+OO 5.387E-01 5.387E-01 62.18 OK PB-212 74.82 10.28 5.239E+OO 9.007E-01 9.007E-01 56.51 OK 77 .11 17.10 5.459E+OO 1.382E+OO 1.382E+OO 21. 98 OK 238.63 43.60* 5.299E+OO 9.269E-01 9.269E-01 12.41 OK 300.09 3.30 4.424E+OO 1.357E+OO 1.357E+OO 91. 45 OK BI-214 609.32 45.49* 2.494E+OO 6.972E-01 6.975E-01 22.43 OK 1120.29 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 OK 1764.49 15.30 1.040E+OO 8.093E-01 8.096E-01 44.16 OK PB-214 74.82 5.80 5.234E+OO Line Not Found <<INT Reject 77 .11 9.70 5.459E+OO 2.436E+OO 2.437E+OO 21. 98 OK 87.09 3.41 6.242E+OO -----Line Not Found <<INT Reject 242.00 7.25 5.244E+OO Line Not Found <<INT Reject 295.22 18.42 4.482E+OO 1.150E+OO 1.150E+OO 19.77 OK 351.93 35.60* 3.884E+OO 9.156E-01 9.159E-01 17.41 OK RN-222 609.32 45.49* 2.494E+OO 6. 972E-01 6.975E-01 22.43 OK 1120. 29 14.92 l.548E+OO 7.912E-01 7.915E-01 41. 03 OK 1764.49 15.30 l.040E+00 8.093E-01 8.096E-01 44.16 OK RA-224 240.99 4.10* 5.250E+OO 4.419E-01 4.419E-01 258.61 OK RA-226 609.32 45.49* 2.494E+OO 6.972E-01 6.975E-01 22.43 OK 1120.29 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 OK 1764.49 15.30 1.040E+OO 8.093E-01 8. 096E-01 44.16 OK AC-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 OK 794.95 4.25 2.028E+OO Line Not Found Absent 835.71 1. 61 l.951E+OO Line Not Found Absent 911. 20 25.80* 1.823E+OO 8.277E-01 8.277E-01 31. 41 OK 968. 97 15.80 1.738E+OO 8.072E-01 8. 072E-01 43.85 OK RA-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 OK 794.95 4.25 2.028E+OO Line Not Found Absent 835.71 1. 61 1.951E+OO Line Not Found Absent 911. 20 25.80* 1.823E+OO 8.277E-01 8.277E-01 31. 41 OK 968. 97 15.80 1.738E+OO 8.072E-01 8.072E-01 43.85 OK TH-228 74.82 10.28 5.239E+00 9.007E-01 9.007E-01 56.51 OK 77 .11 17.10 5.459E+OO l.382E+00 1.382E+OO 21. 98 OK 238.63 43.60* 5.299E+OO 9.269E-01 9.269E-01 12.41 OK 300.09 3.30 4.424E+OO 1.357E+OO 1.357E+OO 91. 45 OK TH-229 85.43 14.70 6.225E+OO 1.158E-01 1.158E-01 244.59 OK 88.47 24.00 6.409E+OO 2.491E-01 2.491E-01 60.75 OK Page 3290 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235019 Acquisition date 3-0CT-2016 08:21:03 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 193.51 4.41* 6.133E+OO Line Not Found Absent 210.85 2.80 5. 821E+OO 1. 651E+OO 1. 651E+OO 92.48 OK TH-230 609.32 45.49* 2.494E+OO 6. 972E-01 6. 972E-01 22.43 OK 1120.29 14.92 1.548E+OO 7.912E-01 7.912E-01 41. 03 OK 1764.49 15.30 1.040E+OO 8.093E-01 8.093E-01 44.16 OK PA-231 283.69 1. 70 4.630E+OO Line Not Found Absent 301.36 5.35* 4.424E+OO 8.372E-01 8.372E-01 91. 45 OK TH-232 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 OK 835.71 1. 61 1. 951E+OO Line Not Found Absent 911.20 25.80* 1.823E+OO 8.277E-01 8.277E-01 31. 41 OK 968. 97 15.80 l.738E+00 8. 072E-01 8.072E-01 43.85 OK TH-234 63.29 3.70* 3.845E+00 l.121E+OO 1.121E+OO 254.25 OK 92.59 4.23 6.570E+OO 1.273E+OO 1.273E+OO 79.53 OK U-234 609.32 45.49* 2.494E+OO 6. 972E-01 6.972E-01 22.43 OK 1120.29 14.92 l.548E+OO 7.912E-01 7.912E-01 41. 03 OK 1764.49 15.30 1.040E+OO 8.093E-01 8.093E-01 44.16 OK U-235 89. 96 3.47 6.409E+OO 1. 723E+OO 1.723E+OO 60.75 OK 93.35 5.60 6.570E+OO 9'. 616E-01 9.616E-01 79.53 OK 143.76 10. 96* 7.059E+OO Line Not Found Absent 163.33 5.08 6.731E+OO Line Not Found Absent 185.72 57.20 6.293E+00 2.677E-01 2.677E-01 31.14 OK 205.31 5.01 5.902E+OO Line Not Found Absent U-238 63.29 3.70* 3.845E+00 1.121E+OO 1.121E+OO 254.25 OK 92.59 4.23 6.570E+OO 1.273E+00 1.273E+OO 79.53 OK AM-243 43.53 5.90 9.310E-01 Line Not Found Absent 74.66 67.20* 5.239E+OO l.378E-01 1. 378E-01 56.51 OK ANH-511 511. 00 100.00* 2.868E+OO 3.004E-02 3.004E-02 184.44 OK Flag: "*" = Keyline Page 3291of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:21:33.25 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l * *Acquisition date 3-0CT-2016 08:21:03 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** * *Sample date 8-DEC-2015 1.4:30:00 Analyst initials: MXRl * *Sample ID G405235019 Sample Quantity 1.7598E+02 GRAM *
  • Batch Number 1596247. Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1. 308E+Ol 1.319E+OO 3.933E-01 ZN-65 l.418E-01 1.940E-01 2.419E-01 CD-109 7.215E-01 1. 729E+OO 1.412E+00 SN-126 4.599E-02 1.102E-01 9. 996E-02 BA-137M 5.314E-02 4.564E-02 4. 713E-02 CS-137 5.614E-02 4.822E-02 4.978E-02 TL-208 3.483E-01 7.503E-02 5.067E-02 PB-212 9.269E-01 1.127E-01 8.229E-02 BI-214 6.975E-01 l.533E-01 1.022E-01 PB-214 9.159E-01 l.562E-01 9. 511E-02 RN-222 6.975E-01 l.533E-01 *l.022E-01 RA-224 4.419E-01 1.120E+OO 8.823E-01 RA-226 6.975E-01 l.533E-01 1.022E-01 AC-228 8.277E-01 2.547E-01 l.987E-01 RA-228 8.277E-01 2.547E-01 1.987E-01 TH-228 9.269E-01 1.127E-01 8.229E-02 TH-229 -8.168E-02 3.649E-01 6.825E-01 TH-230 6. 972E-01 1.532E-01 1.022E-01 PA-231 8.372E-01 7.503E-01 6.279E-01 TH-232 8.277E-01 2.547E-01 l.987E-01 TH-234 l.121E+OO 2.793E+00 1.538E+OO U-234 6. 972E-01 1.532E-01 l.022E-01 U-235 -2.306E-02 l.394E-01 2.680E-01 U-238 1.121E+OO 2.793E+OO 1.538E+OO AM-243 1. 37 8E-01 7.631E-02 7.049E-02 ANH-511 3.004E-02 5.430E-02 4.182E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM BE-7 -2.030E+00 9.521E+OO 1.863E+Ol NOT IDENT. NA-22 -4.410E-03 3.432E-02 6.846E-02 NOT IDENT. NA-24 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 1. 871E-02 2.462E-02 6. 211E-02 NOT IDENT. Page 3292 of 5809 SC-46 3.402E-01 2.517E-01 6.183E-01 FAIL ABUN V-48 O.OOOE+OO 9.984E+03 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 3. ll 7E+02 O.OOOE+OO SHORT HLIF MN-54 -5.091E-03 5.301E-02 1.003E-01 NOT IDENT. C0-56 -1.179E-01 3.829E-01 7.025E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 4.973E-03 3.363E-02 6.752E-02 NOT IDENT. C0-58 -2.941E-01 3.921E-01 6.621E-01 NOT IDENT. FE-59 -1.537E+OO 4. 969E+OO 9.690E+OO NOT IDENT. C0--:60 -1.192E-02 4. 096E-02 6 .. 849E-02 NOT IDENT. GE-68 1.051E+OO 1.852E+OO 4.066E+OO NOT IDENT. AS-73 -6.730E-01 5.407E+OO 1.124E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.441E+03 O.OOOE+OO SHORT HLIF SE-75 -2.080E-02 l.573E-01 2.918E-01 NOT IDENT. BR-77 O.OOOE+OO l.978E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.237E+02 O.OOOE+OO SHORT HLIF RB-83 8.125E-03 5.009E-01 1.004E+OO NOT IDENT. KR-85 -1.717E+OO 5.560E+OO 9.456E+OO NOT IDENT. SR-85 -l.822E-01 5.869E-01 9.978E-01 NOT IDENT. RB-86 0.000E+OO 2.390E+04 O.OOOE+OO SHORT HLIF Y-88 l.539E-01 1.336E-01 4.012E-01 NOT IDENT. Y-91 1. 451E+02 4.130E+02 8. 711E+02 NOT IDENT. NB-94 3.236E-02 5.694E-02 4.936E-02 FAIL ABUN NB-95 4.936E-01 8.228E-01 l.545E+OO NOT IDENT. NB-95M 2.028E+OO 2.085E+00 3. 960E+OO NOT IDENT. ZR-95 2.861E-01 1.125E+OO 2.282E+OO NOT IDENT. NB-97 O.OOOE+OO 1.585E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT "HLIF M0-99 O.OOOE+OO 1.205E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -6.699E-03 2.612E-02 5.036E-02 NOT IDENT. RH-102 -1.461E-02 4.451E-02 8.412E-02 NOT IDENT. RU-103 8. 096E+OO 4.274E+OO 9.608E+OO FAIL ABUN RH-106 -2.769E-01 4.128E-01 7.376E-01 NOT IDENT. RU-106 -2.769E-01 4.128E-01 7.376E-01 NOT IDENT. AG-108M 6.667E-03 l.918E-02 4.064E-02 NOT IDENT. AG-llOM -4.382E-03 7.159E-02 l.392E-01 NOT IDENT. SN-113 -5.393E-02 1.605E-01 3.157E-01 NOT IDENT. CD-115 0.000E+OO 2.409E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 6.910E+04 O.OOOE+OO SHORT HLIF TE-123M -1.664E-02 9. 651E-02 1. 848E-01 NOT IDENT. SB-124 1.150E+00 1.310E+OO 3.577E+OO NOT IDENT. SB-125 6.234E-02 1. 477E-01 l.689E-01 FAIL ABUN TE-125M 8.779E+Ol 1. 970E+02 4.059E+02 NOT IDENT. I-126 O.OOOE+OO 7.461E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8.010E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1. 446E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3. 541E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 5.442E+40 0.000E+OO SHORT HLIF TE-132 O.OOOE+OO 3.044E+26 O.OOOE+OO SHORT HLIF BA-133 2.751E-03 3.202E-02 5.973E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 -1.254E-02 4. 511E-02 8.276E-02 NOT IDENT. CS-135 -1.282E-02 l.107E-01 1. 886E-01 NOT IDENT. I-135 O.OOOE+OO 1. 843E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2 .139E+05 O.OOOE+OO SHORT HLIF CE-139 9. 921E-02 8.832E-02 1. 845E-01 NOT IDENT. BA-140 O.OOOE+OO 1.032E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.577E+05 O.OOOE+OO SHORT HLIF CE-141 -1.223E+OO 1.804E+Ol 3.498E+Ol NOT IDENT. CE-143 O.OOOE+OO 9.385E+40 0.000E+OO SHORT HLIF CE-144 5.676E-02 2.533E-01 5.079E-01 NOT IDENT. PM-144 1. 962E-02 4.483E-02 8.540E-02 NOT IDENT. PR-144 1.786E+OO 3.906E+OO 7.461E+OO NOT IDENT. PM-146 4.898E-04 2.943E-02 6.0lOE-02 FAIL ABUN ND-147 0.000E+OO 2.339E+07 O.OOOE+OO SHORT HLIF PM-147 2. 411E+02 6.008E+02 l.227E+03 NOT IDENT. PM-149 0.000E+OO 3.548E+40 O.OOOE+OO SHORT HLIF EU-150 -5.887E-03 2.094E-02 3. 722E-02 FAIL ABUN EU-152 6.035E-03 7.271E-02 l.488E-01 FAIL ABUN GD-153 8.733E-03 1. 2 68E-01 2.560E-01 NOT IDENT. EU-154 -1. 2 68E-02 8.373E-02 l.664E-01 FAIL ABUN EU-155 2.673E-02 7.650E-02 1. 571E-01 FAIL ABUN TB-160 -1.163E+OO 1.475E+OO 2.444E+OO FAIL ABUN H0-166M -l.428E-02 4.819E-02 8.957E-02 FAIL ABUN TM-171 -1.285E+OO 1. 2 69E+Ol 2.648E+Ol NOT IDENT. HF-172 -8.547E-02 1. 759E-01 3.337E-01 FAIL ABUN LU-172 2.802E-02 6.473E-02 1.379E-01 FAIL ABUN Page 3293 of 5809 LU-176 -1. 290E-02 1. 860E-02 3.159E-02 FAIL ABUN HF-181 -1.802E+OO 3.171E+OO 5.940E+OO NOT IDENT. TA-182 4.024E-01 6.947E-01 1.513E+OO FAIL ABUN RE-183 6.868E-01 1.784E+OO 3.825E+OO NOT IDENT. RE-184 7.369E+OO 2.491E+Ol 5.015E+Ol NOT IDENT. W-188 -8.317E-01 9.107E+Ol l.564E+02 FAIL ABUN IR-192 l.873E-01 3.482E-01 6.921E-01 FAIL ABUN HG-203 7. 031E-01 1.858E+OO 3.612E+OO NOT IDENT. BI-207 l.043E-02 3.756E-02 7.951E-02 FAIL ABUN PB-210 l.166E+OO l.708E+00 3. 7.80E+OO NOT IDENT. BI-211 O.OOOE+OO 4.304E-01 6.421E-01 FAIL ABUN PB-211 -l .196E-01 5.261E-01 9.302E-01 NOT IDENT. BI-212 O.OOOE+OO 6.742E-01 i .117E+OO FAIL ABUN RN-219 5.979E-02 2.698E-01 5.614E-01 FAIL ABUN RA-223 -3.781E-02 4.420E-01 8. 962E-01 FAIL ABUN AC-227 -6.068E-02 1. 723E-01 3 .119E-01 FAIL ABUN TH-227 -6.068E-02 1. 723E-01 3 .119E-01 FAIL ABUN TH-231 -3. 781E-02 4.420E-01 8. 962E-01 FAIL ABUN PA-233 -5.017E-02 4.711E-02 7.543E-02 FAIL ABUN PA-234 2. 962E-02 2.102E-01 4.173E-01 NOT IDENT. PA-234M 3.362E+OO 3. lllE+OO 6. 960E+OO NOT IDENT. NP-237 -5.017E-02 4. 711E-02 7.543E-02 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 2.354E-02 1.642E-01 3.315E-01 FAIL ABUN PU-239 -2.539E+Ol 2.347E+02 4. 572E+02 NOT IDENT. AM-241 9.666E-03 8.947E-02 1. 750E-01 NOT IDENT. CM-243 -3.383E-03 6.738E-02 1.350E-01 FAIL ABUN BK-247 -1. 496E-02. 5.689E-02 l.036E-01 FAIL ABUN CM-247 -4.980E-03 2.489E-02 4.952E-02 FAIL ABUN CF-249 -6.187E-03 2.648E-02 5.266E-02 NOT IDENT. CF-251 4. 211E-02 8.575E-02 l.720E-01 NOT IDENT. Page 3294 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:21:30.92 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 405 10.66* 1.238E+OO 1.308E+Ol 1.308E+Ol 10.29 ZN-65 1115. 54 11 50.60* 1.552E+OO 6.051E-02 l.418E-01 139.62 CD-109 88.03 82 3.70* 6.225E+OO 1.519E+OO 2.384E+OO 72. 74 SN-126 64.28 37 9.60 3.845E+OO 4.320E-01 4.320E-01 254.25 86. 94 82 8.90 6.225E+OO 6.317E-01 6.317E-01 72.74 87.57 82 37.00* 6.225E+OO l.519E-01 1.519E-01 72. 74 BA-137M 661. 66 26 89.90* 2.341E+OO 5.215E-02 5.314E-02 87.64 CS-137 661. 66 26 85.10* 2.341E+OO 5.509E-02 5.614E-02 87.64 TL-208 277.37 24 6.60 4. 720E+OO 3.303E-01 3.303E-01 183.91 583.19 179 85.00* 2.581E+OO 3.483E-01 3.483E-01 21. 98 860.56 30 12.50 l.906E+OO 5.387E-01 5.387E-01 62.18 BI-211 72.87 ------1. 23 5.033E+OO ------Line Not Found ------351.06 297 12.92* 3.884E+OO 2.523E+OO 2.523E+OO 17.41 PB-212 74.82 196 10.28 5.239E+OO 1.549E+OO l.549E+OO 31. 79 77 .11 302 17 .10 5.459E+OO 1.382E+OO 1.382E+OO 21. 98 238.63 502 43.60* 5.299E+OO 9'. 269E-01 9.269E-01 12.41 300.09 46 3.30 4.424E+OO 1.357E+OO 1.357E+OO 91. 45 BI-214 609.32 185 45.49* 2.494E+OO 6. 972E-01 6.975E-01 22.43 1120.29 43 14.92 1.548E+00 7.912E-01 7.915E-01 41. 03 1764.49 30 15.30 1.040E+OO 8.093E-01 8.096E-01 44.16 PB-214 74.82 196 5.80 5.239E+00 2.746E+OO 2.747E+OO 31. 79 77 .11 302 9.70 5.459E+OO 2.436E+OO 2.437E+OO 21. 98 87.09 82 3.41 6.225E+OO 1.649E+OO 1.649E+OO 72. 74 242.00 125 7.25 5.250E+OO l.400E+OO l.400E+00 43.23 295.22 222 18.42 4.482E+OO 1.150E+OO 1.150E+OO 19.77 351.93 297 35.60* 3.884E+OO 9.156E-01 9.159E-01 17.41 RN-222 609.32 185 45.49* 2.494E+OO 6. 972E-01 6.975E-01 22.43 1120.29 43 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 1764.49 30 15.30 1.040E+OO 8.093E-01 8.096E-01 44.16 RA-224 240.99 125 4.10* 5.250E+OO 2.475E+OO 2.475E+OO 43.23 RA-226 609.32 185 45.49* 2.494E+OO 6. 972E-01 6.975E-01 22.43 1120.29 43 14.92 1.548E+OO 7.912E-01 7.915E-01 41. 03 1764.49 30 15.30 1.040E+OO 8.093E-01 8. 096E-01 44.16 AC-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 99 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 794.95 ------4.25 2.028E+OO ------Line Not Found ------835.71 ------1. 61 1. 951E+OO ------Line Not Found ------911. 20 91 25.80* l.823E+00 8.277E-01 8.277E-01 31. 41 968.97 52 15.80 1.738E+OO 8. 072E-01 8.072E-01 43.85 RA-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 99 11. 27 *4.0lOE+OO 9.376E-01 9.376E-01 49.50 794.95 ------4.25 2.028E+OO ------Line Not Found ------835.71 ------1. 61 l.951E+OO ------Line Not Found ------911. 20 91 25.80* 1.823E+OO 8.277E-01 8.277E-01 31. 41 968.97 52 15.80 1.738E+OO 8. 072E-01 8.072E-01 43.85 TH-228 74.82 196 10.28 5.239E+OO 1.549E+OO 1.549E+OO 31. 79 77 .11 302 17.10 5.459E+OO 1.382E+OO 1.382E+OO 21. 98 Page 3295 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235019 Acquisition date 3-0CT-2016 08:21:03 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 502 43.60* 5.299E+OO 9.269E-01 9.269E-01 12. 41 300.09 46 3.30 4.424E+OO l.357E+OO l.357E+OO 91. 45 TH-229 85.43 82 14.70 6.225E+OO 3.824E-01 3.825E-01 72. 74 88.47 90 24.00 6.409E+OO 2.491E-01 2.491E-01 60.75 193.51 ------4*_ 41* 6.133E+OO ------Line Not Found ------210.85 63 2.80 5.821E+OO l.651E+OO 1. 651E+OO 92.48 TH-230 609.32 185 45.49* 2.494E+OO 6.972E-01 6. 972E-01 22.43 1120.29 43 14.92 l.548E+OO 7.912E-01 7.912E-01 41. 03 1764.49 30 15.30 l.040E+OO 8.093E-01 8.093E-01 44.16 PA-231 283.69 ------1. 70 4.630E+OO ------Line Not Found ------301.36 46 5.35* 4.424E+OO 8.372E-01 8.372E-01 91.45 TH-232 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 99 11. 27 4.0lOE+OO 9.376E-01 9.376E-01 49.50 835.71 ------1. 61 l.951E+OO ------Line Not Found ------911. 20 91 25.80* l.823E+OO 8.277E-01 8.277E-01 31. 41 968. 97 52 15.80 1. 738E+OO 8.072E-01 8. 072E-01 43.85 TH-234 63.29 37 3.70* 3.845E+00 l.121E+OO l .121E+OO 254.25 92.59 83 4.23 6.570E+OO l.273E+OO l.273E+OO 79.53 U-234 609.32 185 45.49* 2.494E+OO 6. 972E-01 6. 972E-01 22.43 1120.29 43 14.92 l.548E+OO 7.912E-01 7.912E-01 41. 03 1764.49 30 15.30 l.040E+00 8.093E-01 8.093E-01 44.16 U-235 89. 96 90 3.47 6.409E+OO 1. 723E+OO 1. 723E+OO 60.75 93.35 83 5.60 6.570E+OO 9.616E-01 9.616E-01 79.53 143.76 ------10. 96* 7.059E+OO ------Line Not Found ------163.33 ------5.08 6. 731E+OO ------Line Not Found ------185.72 226 57.20 6.293E+OO 2.677E-01 2.677E-01 31.14 205.31 ------5.01 5.902E+OO ------Line Not Found ------U-238 63.29 37 3.70* 3.845E+OO l.121E+OO l.121E+00 254.25 92.59 83 4.23 6.570E+OO 1. 273E+00 l.273E+OO 79.53 AM-243 43.53 ------5.90 9.310E-01 ------Line Not Found ------74.66 196 67.20* 5.239E+OO 2.370E-01 2.370E-01 31. 79 ANH-511 511. 00 20 100.00* 2. 8 68E+OO 3.004E-02 3.004E-02 184.44 Flag: "*" Key line Page 3296 of 5809 Summary of Nuclide Activity Sample ID : G405235019 Acquisition date Page : 3 3-0CT-2016 08:21:03 Total number of lines in spectrum 53 Number of unidentified lines 13 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 ZN-65 . CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlif e 1.25E+09Y 244.06D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+10Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y l.41E+l0Y 1.41E+10Y l.41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y l.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 2.34 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.308E+Ol 6. 051E-02 1.519E+OO l.519E-01 5.215E-02 5.509E-02 3.483E-01 2.523E+OO 9.269E-01 6.972E-01 9.156E-01 6.972E-01 2.475E+OO 6.972E-01 8.277E-01 8.277E-01 9.269E-01 2. 491E-01 6. 972E-01 8. 372E-01 8.277E-01 1.121E+OO 6.972E-01 2.677E-01 1.121E+OO 2.370E-01 3.004E-02 3.287E+Ol 3.287E+Ol Decay Corr pCi/GRAM l.308E+Ol l.418E-01 2.384E+OO l.519E-01 5.314E-02 5.614E-02 3.483E-01 2.523E+OO 9.269E-01 6.975E-01 9.159E-01 6.975E-01 2.475E+OO 6.975E-01 8.277E-01 8.277E-01 9.269E-01 2. 491E-01 6. 972E-01 8.372E-01 8.277E-01 1.121E+OO 6. 972E-01 2.677E-01 1.121E+OO 2.370E-01 3.004E-02 3.382E+Ol 3.382E+Ol 75.47% Decay Corr 2-Sigma Error 0.135E+Ol 1. 979E-01 1. 734E+OO 1.105E-01 4.658E-02 4.920E-02 0.766E-01 0.439E+OO l.150E-01 l.564E-01 l.594E-01 1.564E-01 1.070E+OO 1.564E-01 2.599E-01 2.599E-01 l.150E-01 l.513E-01 1.564E-01 7.656E-01 2.599E-01 2.850E+OO 1.564E-01 0.834E-01 2.850E+00 0.754E-01 5.541E-02 "M" accepted 2-Sigma %Error 10.29 139.62 72.74 72.74 87.64 87.64 21. 98 17.41 12.41 22.43 17.41 22.43 43.23 22.43 31. 41 31. 41 12.41 60.75 22.43 91. 45 31. 41 254.25 22.43 31.14 254.25 31. 79 184.44 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3297 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235019 Acquisition date : 3-0CT-2016 08:21:03 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.89 64 233 1. 04 167.71 165 7 1.26E-02 98.9 6.02E+OO T 4 270.47 70 65 1. 75 541.11 537 27 1.57E-02 56.3 4.81E+OO T 4 274.41 49 54 1. 20 549.00 537 27 l. llE-02 62.2 4.75E+OO T 0 415.66 40 131 7.63 831.66 813 24 9. 52E-03. **** 3.39E+OO T 0 428.86 12 48 1. 41 858.08 851 9 2.79E-03 **** 3.30E+OO T 0 469.33 29 29 1. 81 939.06 935 9 6.91E-03 82.7 3.07E+OO T 1 491.68 18 29 1. 55 983.78 977 17 4.30E-03 **** 2. 96E+00 T 1 494.93 18 21 1. 55 990.28 977 17 4.46E-03 97.7 2.94E+OO 0 498.75 37 26 3.26 997.93 993 10 8.92E-03 65.7 2.92E+OO 0 544.28 13 25 3.54 1089.02 1081 10 3.20E-03 **** 2.73E+OO 6 668.21 31 21 1. 54 1337.00 1333 12 7.79E-03 55.5 2.32E+OO T 6 670. 7 5 9 12 1. 65 1342.09 1333 12 2.38E-03 **** 2. 31E+OO 0 701.59 17 41 5.90 1403.77 1395 15 4. 31E-03 **** 2.23E+OO T 0 727. 59 44 19 1. 92 1455.79 1451 11 1.12E-02 53.5 2.17E+OO T 0 747.05 22 18 1. 62 1494.74 1490 10 5.55E-03 89.9 2.13E+OO T 0 768.97 26 29 2.85 1538.59 1533 11 6.59E-03 **** 2.08E+OO 0 817.97 16 15 3.22 1636.63 1631 11 4.13E-03 **** 1.98E+OO T 0 935.17 12 9 1.29 1871. 08 1867 8 3.18E-03 **** 1. 79E+OO 1 964. 79 27 21 1. 90 1930.35 1920 25 7.29E-03 67.1 1. 74E+OO T 0 1003.33 31 4 5.74 2007.44 2000 15 8.36E-03 50.5 1.69E+OO T 0 1153.38 14 22 2;48 2307.60 2301 11 3.89E-03 **** 1.51E+OO 0 1166 .18 10 7 2.27 '2333.20 2329 7 2.78E-03 **** 1. 50E+OO 0 1336.20 8 3 0.68 2673.26 2669 8 2.36E-03 **** l.34E+00 0 1377.44 18 5 2.28 2755.75 2750 10 5.00E-03 66.2 l.30E+OO 0 1415.36 12 0 0.83 2831. 58 2827 9 3.33E-03 57.7 1. 27E+OO 0 1509.86 7 5 1. 79 3020.57 3014 10 1.94E-03 **** 1. 20E+OO 0 1847.73 6 2 1.26 3696.23 3691 9 1. 90E-03 **** 9.94E-01 Flags: "T" = Tentatively associated Page 3298 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:21:46.64 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA *
  • * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l *
  • Acquisition date 3-0CT-2016 08:21:.03 Sensitivity 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:30:00 Nuclide Library : SOLID *
  • Sample ID G405235019 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : 1.7598E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.523E-01 1.034E-01 6.630E-01 4. 723E-02 2.065E-02 2.lBlE-02 2.259E-02 3.846E-02 4.579E-02 4.312E-02 4.579E-02 4.124E-01 4.579E-02 8. 671E-02 8. 671E-02 3.846E-02 3.182E-01 4.577E-02 2.878E-01 8.671E-02 7.241E-01 4.577E-02 1.259E-01 7.241E-01 3.341E-02 1.880E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3299 of 5809 Le (pCi/GRAM 8.359E+00 2.897E-02 O.OOOE+OO 2.532E-02 2.709E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3300 of 5809 O.OOOE+OO O.OOOE+OO 4.422E-02 3.057E-01 O.OOOE+OO 3.156E-02 2.746E-01 4.135E+OO 2.937E-02 1.786E+OO 5.277E+OO O.OOOE+OO l.337E-01 O.OOOE+OO O.OOOE+OO 4.490E-01 4.212E+OO 4.444E-01 O.OOOE+OO l.595E-01 3.815E+02 2.199E-02 6.989E-01 l.860E+OO 1.007E+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 2.365E-02 3.690E-02 4.352E+OO 3.256E-01 3.256E-01 1.826E-02 5.950E-02 1.417E-01 O.OOOE+OO O.OOOE+OO 8.610E-02 1.432E+OO 7.687E-02 1.906E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 715E-02 O.OOOE+OO 3.684E-02 8.634E-02 O.OOOE+OO O.OOOE+OO 8.694E-02 O.OOOE+OO O.OOOE+OO 1.639E+Ol O.OOOE+OO 2.375E-01 3.795E-02 3.318E+OO 2.676E-02 O.OOOE+OO 5.753E+02 O.OOOE+OO 1. 701E-02 6.831E-02 1.203E-01 7.033E-02 7.370E-02 1.035E+OO 3.977E-02 1.243E+Ol l.563E-01 6.088E-02 l.428E-02 SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3301of5809 2.632E+00 6.638E-01 1. 796E+00 2.207E+Ol 7.154E+Ol 3.167E-01 l.666E+OO 3.476E-02 1. 776E+OO 3. 090E-01. 4.184E-01 5. l 72E-01 2.542E-01 4. llOE-01 l.430E-01 1.430E-01 4. llOE-01 3.398E-02 1.807E-01 3.064E+OO 3.398E-02 O.OOOE+OO l.547E-01 2.147E+02 8.212E-02 6.302E-02 4.760E-02 2.232E-02 2.374E-02 8.039E-02 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:21:51.99 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235019.CNF;l * *Acquisition date 3-0CT-2016 08:21:03 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.63 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:30:00 Nuclide Library : SOLID *
  • Sample ID G405235019 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : 1.7598E+02 GRAM *
  • Quantity Err(%) : 1.1365E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 * * , Dry Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) K-40 1.308E+Ol 1.485E+OO 1.485E+OO ZN-65 l.418E-01 1.940E-01 1.940E-01 CD-109 7.215E-01 1.743E+OO 1.743E+OO SN-126 4.599E-02 l. lllE-01 1. lllE-01 BA-137M 5.314E-02 4.570E-02 4.570E-02 CS-137 5.614E-02 4.828E-02 4.828E-02 TL-208 3.483E-01 7.648E-02 7.648E-02 PB-212 9.269E-01 l.230E-01 l.230E-01 BI-214 6.975E-01 1.562E-01 1.562E-01 PB-214 9.159E-01 l.608E-01 l.608E-01 RN-222 6.975E-01 l.562E-01 1.562E-01 RA-224 4.419E-01 l.128E+OO 1.128E+OO RA-226 6.975E-01 1.562E-01 1.562E-01 AC-228 8.277E-01 2.582E-01 2.582E-01 RA-228 8.277E-01 2.582E-01 2.582E-01 TH-228 9.269E-01 l.230E-01 l.230E-01 TH-229 -8.168E-02 3.649E-01 3.649E-01 TH-230 6.972E-01 1.561E-01 1.561E-01 PA-231 8. 372E-01 7.713E-01 7. 713E-01 TH-232 8.277E-01 2.582E-01 2.582E-01 TH-234 1.121E+OO 2.804E+00 2.804E+OO U-234 6. 972E-01 1.561E-01 1.561E-01 U-235 -2.306E-02 l.394E-01 1.394E-01 U-238 1.121E+OO 2.804E+OO 2.804E+OO AM-243 l.378E-01 7.780E-02 7.780E-02 ANH-511 3.004E-02 5.432E-02 5.432E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -2.030E+OO 9. 521E+OO 9.565E+OO NOT IDENT. NA-22 -4.410E-03 3.432E-02 3.437E-02 NOT IDENT. NA-24 1.000E+41 6.019E+41 O.OOOE+OO SHORT HLIF AL-26 1.871E-02 2.465E-02 2.605E-02 NOT IDENT. Page 3302 of 5809 SC-46 3.402E-01 2.521E-01 2.951E-01 FAIL ABUN V-48 3.854E+03 9.985E+03 1.014E+04 SHORT HLIF CR-51 1.703E+02 3 .118E+02 3. 211E+02 SHORT HLIF MN-54 -5.091E-03 5.301E-02 5.306E-02 NOT IDENT. C0-56 -1.17 9E-01 3.830E-01 3.866E-01 NOT IDENT. MN-56 -1.000E+41 3.138E+41 O.OOOE+OO SHORT HLIF C0-57 4.973E-03 3.363E-02 3.370E-02 NOT IDENT. C0-58 -2.941E-01 3.923E-01 4.141E-01 NOT IDENT. FE-59 -1.537E+OO 4.971E+OO 5.019E+OO NOT IDENT. C0-60 -1.192E-02 4.097E-02 4.13.2E-02 NOT IDENT. GE-68 1. 051E+OO 1.853E+OO 1.912E+OO NOT IDENT. AS-73 -6.730E-01 5.408E+OO 5.417E+OO NOT IDENT. AS-74 -1.108E+03 4.442E+03 4.470E+03 SHORT HLIF SE-75 -2.080E-02 l.573E-01 1.576E-01 NOT IDENT. BR-77 l.627E+38 1.407E+39 O.OOOE+OO SHORT HLIF SR-82 -6. 725E+02 5.246E+02 6.059E+02 SHORT HLIF RB-83 8.125E-03 5.009E-01 5.009E-01 NOT IDENT. KR-85 -1.717E+OO 5.561E+OO 5.614E+OO NOT IDENT. SR-85 -l.822E-01 5.869E-01 5.926E-01 NOT IDENT. RB-86 3.761E+03 2.391E+04 2.397E+04 SHORT HLIF Y-88 1. 539E-01 1.340E-01 1.509E-01 NOT IDENT. Y-91 1. 451E+02 4.130E+02 4.182E+o2 NOT IDENT. NB-94 3.236E-02 5.695E-02 5.879E-02-FAIL ABUN NB-95 4.936E-01 8. 231E-01 8.526E-01 NOT IDENT. NB-95M 2.028E+OO 2.091E+OO 2.282E+OO NOT IDENT. ZR-95 2. 861E-01 1.125E+OO l .132E+OO NOT IDENT. NB-97 -1.000E+41 1. 586E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 3.098E+42 O.OOOE+OO SHORT HLIF M0-99 -1.909E+31 1.205E+32 O.OOOE+OO SHORT HLIF TC-99M 1. 000E+41 2.402E+41 O.OOOE+OO SHORT HLIF RH-101 -6.699E-03 2.615E-02 2.633E-02 NOT IDENT. RH-102 -1. 461E-02 4.453E-02 4.501E-02 NOT IDENT. RU-103 8.096E+00 4.292E+00 5.634E+OO FAIL ABUN RH-106 -2.769E-01 4 .131E-01 4.316E-01 NOT IDENT. RU-106 -2.769E-01 4 .131E-01 4.316E-01 NOT IDENT. AG-108M 6.667E-03 1.918E-02 l.942E-02 NOT IDENT. AG-llOM -4.382E-03 7.159E-02 7.162E-02 NOT IDENT. SN-113 -5.393E-02 l.605E-01 1.623E-01 NOT IDENT. CD-115 -l.407E+39 2.423E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -4.171E+03 6. 911E+04 6. 913E+04 SHORT HLIF TE-123M -l.664E-02 9. 651E-02 9.680E-02 NOT IDENT. SB-124 1.150E+OO 1.312E+OO 1. 411E+OO NOT IDENT. SB-125 6.234E-02 1. 477E-01 1.503E-01 FAIL ABUN TE-125M 8.779E+Ol 1.970E+02 2.010E+02 NOT IDENT. I-126 4.452E+05 7.485E+05 7.750E+05 SHORT HLIF SB-126 2.165E+05 8.020E+05 8.079E+05 SHORT HLIF SB-127 -2.355E+21 l.481E+22 O.OOOE+OO SHORT HLIF I-131 1.211E+08 3.541E+09 3.542E+09 SHORT HLIF I-132 1.000E+41 1.848E+42 O.OOOE+OO SHORT HLIF TE-132 -2.159E+26 3.168E+26 O.OOOE+OO SHORT HLIF BA-133 2.751E-03 3.202E-02 3.205E-02 FAIL ABUN I-133 -1. OOOE+41 7.873E+41 O.OOOE+OO SHORT HLIF CS-134 -1.254E-02 4. 511E-02 4.546E-02 NOT IDENT. CS-135 -1. 282E-02 1.107E-01 l.109E-01 NOT IDENT. I-135 -l.000E+41 7.019E+41 O.OOOE+OO SHORT HLIF CS-136 3.372E+04 2.140E+05 2.145E+05 SHORT HLIF CE-139 9.921E-02 9.055E-02 1.0lOE-01 NOT IDENT. BA-140 -3.105E+05 l.032E+06 1.042E+06 SHORT HLIF LA-140 7.780E+04 2.578E+05 2. 601E+05 SHORT HLIF CE-141 -1.223E+OO 1.804E+Ol 1. 805E+Ol NOT IDENT. CE-143 l.000E+41 9.440E+40 O.OOOE+OO SHORT HLIF CE-144 5.676E-02 2.533E-01 2.546E-01 NOT IDENT. PM-144 1. 962E-02 4.485E-02 4.571E-02 NOT IDENT. PR-144 1. 786E+OO 3.907E+OO 3.989E+OO NOT IDENT. PM-146 4.898E-04 2.943E-02 2.943E-02 FAIL ABUN ND-147 4.458E+'06 2.339E+07 2.348E+07 SHORT HLIF PM-147 2. 411E+02 6.009E+02 6.107E+02 NOT IDENT. PM-149 -4.995E+39 3.550E+40 O.OOOE+OO SHORT HLIF EU-150 -5. 887E...:.03 2.094E-02 2. lllE-02 FAIL ABUN EU-152 6.035E-03 7.271E-02 7.276E-02 FAIL ABUN GD-153 8.733E-03 1.268E-01 l.269E-01 NOT IDENT. EU-154 -1.268E-02 8.373E-02 8.393E-02 FAIL ABUN EU-155 2.673E-02 7.652E-02 7.746E-02 FAIL ABUN TB-160 -1.163E+00 1.477E+OO 1.567E+OO FAIL ABUN H0-166M -l.428E-02 4.820E-02 4.863E-02 FAIL ABUN TM-171 -1.285E+OO 1.269E+Ol 1. 271E+Ol NOT IDENT. HF-172 -8.547E-02 1. 765E-01 l.806E-01 FAIL ABUN LU-172 2.802E-02 6.480E-02 6.602E-02 FAIL ABUN Page 3303 of 5809 LU-176 -1.290E-02 1. 860E-02 1.949E-02 FAIL ABUN HF-181 -1.802E+OO 3. l 72E+OO 3.274E+OO NOT IDENT. TA-182 4.024E-01 6.949E-01 7 .181E-01 FAIL ABUN RE-183 6.868E-01 l.787E+OO 1.814E+00 NOT IDENT. RE-184 7.369E+OO 2.498E+Ol 2.520E+Ol NOT IDENT. W-188 -8.317E-01 9.107E+Ol 9.107E+Ol FAIL ABUN IR-192 1. 873E-01 3.483E-01 3.584E-01 FAIL ABUN HG-203 7. 031E-01 1.858E+OO 1.885E+OO NOT IDENT. BI-207 1.043E-02 3.757E-02 3.786E-02 FAIL ABUN PB-210 l.166E+OO 1. 711E+OO 1. 790E+OO NOT IDENT. BI-211 2.523E+OO 4.449E-01 l.221E+OO FAIL ABUN PB-211 -1.196E-01 5.261E-01 5.289E-01 NOT IDENT. BI-212 1.286E+OO 6.773E-01 8.915E-01 FAIL ABUN RN-219 5.979E-02 2.699E-01 2.713E-01 FAIL ABUN RA-223 -3.781E-02 4.420E-01 4.423E-01 FAIL ABUN AC-227 -6.068E-02 1. 724E-01 1.746E-01 FAIL ABUN TH-227 -6.068E-02 l.724E-01 1.746E-01 FAIL ABUN TH-231 -3.781E-02 4.420E-01 4.423E-01 FAIL ABUN PA-233 -5.017E-02 4.717E-02 5.231E-02 FAIL ABUN PA-234 2.962E-02 2.129E-01 2.133E-01 NOT IDENT. PA-234M 3.362E+OO 3 .115E+OO 3.464E+OO NOT IDENT. NP-237 -5.017E-02 4. 717E-02 5.231E-02 FAIL ABUN NP-238 6.669E+40 3 .130E+41 O.OOOE+OO SHORT HLIF NP-239 2.354E-02 l.642E-01 l.646E-01 FAIL ABUN PU-239 -2.539E+Ol 2.347E+02 2.350E+02 NOT IDENT. AM-241 9.666E-03 8.947E-02 8.958E-02 NOT IDENT. CM-243 -3.383E-03 6.738E-02 6.740E-02 FAIL ABUN BK-247 -1.496E-02 5.697E-02 5.736E-02 FAIL ABUN CM-247 -4.980E-03 2.491E-02 2. 501E-02 FAIL ABUN CF-249 -6.187E-03 2.649E-02 2.663E-02 NOT IDENT. CF-251 4.211E-02 8.588E-02 8.795E-02 NOT IDENT. Page 3304 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 54.6419 87.09 97.7634 136.47 66.6544 45.60 66.8561 87.57 97.8610 140.51 0.0000 46.54 53.4742 88.03 79.1166 143.76 74.6378 49.72 0.0000 88.34 79.1666 144.24 67.4290 51. 35 77.5164 88.47 79.1877 145.44 74.8213 51. 87 91. 4366 89. 96 96.4491 152.43 77.6697 52.39 80.3444 1093.63 49.2376 153.25 0.0000 52.97 76.1527 91.11 0.0000 323.87 66.2886 53.44 82.3216 92.59 92.5236 156.02 0.0000 54.07 72.9207 93.35 87.5850 158.56 0.0000 57.36 0.0000 94.56 68.7085 159.00 66.7270 57.53 78.0111 94.65 68.7206 162.33 64.9000 57.98 69.3302 94.67 68. 7233 162.66 0.0000 59.27 77.4982 94.87 70.0234 163.33 91.6204 59.32 77.5086 97.43 79.6476 165.86 61.9985 59.54 75.2041 98.43 59.6093 176.31 62.8410 60.96 83.7444 98.44 59.6108 176.60 0.0000 61.17 83.7907 99.53 84.7841 177.52 57. 5110 62.93 86.2496 100 .11 89.6992 181.07 0.0000 63.29 86.3296 102.03 60.9827 181.52 45.0759 63.58 86.3936 103.18 74.6930 184.41 49.2490 64.28 86.5481 103.37 67.9268 143.76 49.3279 66.73 95.7601 105.21 66.2086 193.51 68.6006 67.24 70. 7119 105.31 69.1420 197.03 67.7733 125.81 80.3872 106.12 70.2191 198.01 78.9736 67.75 97.2010 106.47 74.1671 201.83 67.0322 69.67 94.9440 109.28 68.6558 203.43 90.6590 70.83 103.3682 111. 00 76.7348 205.31 56.8299 72.81 114 .1762 111. 76 0.0000 210.85 48.5305 72. 87 114.1924 114. 06 70.2205 215.65 61.2683 74.66 110.7022 116.30 0.0000 222 .11 57.1266 74.82 110.7428 116.74 61. 6003 227.09 57.4287 74.97 110. 7816 119.76 77.8911 227.38 58.5952 77 .11 111.3207 121.12 66.0564 228.16 0.0000 78.74 111. 7269 121. 22 66.0670 228.18 64.3937 79.69 85.1277 121.78 65.1260 116.74 64.3937 80.12 75.3291 122.06 65.1562 235.69 55.6245 80.19 0.0000 122.92 91. 34 71 235. 96 63.3677 80.57 85.2926 123.07 91.3694 238.63 68.5771 81. 00 74.2371 265.00 69.3490 238.98 0.0000 81. 07 74.2480 125.81 85.7244 240.99 68.7400 81. 75 91.7081 127.23 85.9189 242.00 68.8093 83.79 82.1522 127.91 67.7979 244.70 45.2175 84.00 82.1885 129.30 82.1445 252.40 0.0000 85.43 95.5518 131.20 87.4763 252.80 54.2221 86.55 95.7760 133.02 65.2832 254.15 0.0000 86.79 97.7023 133.52 64.3122 256.23 47.3059 86.94 97.7333 136.00 84.0270 260.90 0.0000 Page 3305 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 42.9170 355.39 0.0000 584.27 22.6846 264.80 42.9225 356.01 32.1663 595.83 0.0000 265.00 47.7014 364.49 0.0000 427.87 24.8596 268.22 41. 4650 366.42 0.0000 602.52 0.0000 269.46 37.1219 372. 51 28.6521 604. 72 26.9033 270.03 37.1417 375.05. 26.9648 607.14 20.9504 271.23 37.1824 377.52 27.0127 609.32 24. 9674 273.65 0.0000 356.01 32.3863 610.33 24.9797 276.40 37.3584 388.16 31. 6069 614.28 27.0308 277.37 37.3915 388.63 0.0000 618.01 21.0615 277.60 37.3990 391.69 30.8044 620.36 22.0904 278.00 37.4132 264.66 25.6818 621.93 28.1356 279.20 37.4530 401. 81 27.4750 630.19 0.0000 279.54 37.4653 402.40 31.0323 631.29 21.1974 279.70 37.4700 404.85 30.6402 633.25 15.1550 280.46 40.3178 410.95 26.7535 634.78 0.0000 283.69 37.2000 413.71 26.8030 635.95 13.1513 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 36.4471 423.72 0.0000 645.85 18.2944 285.90 0.0000 427.09 26.1385 657.76 19.9293 287.50 38.9482 427.87 26.1520 657.90 0.0000 290.67 39.0566 433.94 21.7280 661.66 16.8934 293.27 0.0000 439.40 21.8037 664.57 0.0000 351.93 40.4363 453.88 22.0029 666.33 0.0000 295.96 40.4625 463.37 28.5870 666.50 0.0000 879.38 40.5541 468.07 24.9697 667.71 0.0000 299.98 40.6024 473.00 0.0000 677.62 15.4700 300.09 40.6055 475.06 25.0752 685.70 0.0000 300.13 40.6075 476.78 28.8197 695.00 0.0000 301.36 40.6498 477.60 28.8336 696.49 15.6006 302.85 40.7011 482.18 27.9797 696. 51 15.6012 256.23 26.3490 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.0460 306.78 42.0735 497.08 5.6449 697.49 14.0471 308.46 33.4583 505.52 23.6343 702.65 22.9435 311. 90 47.2252 507.63 0.0000 706.68 29.7745 316.51 29.9392 511. 00 26.5528 711. 68 25.1279 319.41 0.0000 514.00 27.0724 720.70 0.0000 320.08 0.0000 514.00 27.0724 721. 93 0.0000 321.04 35.8937 520.40 23.8332 722.78 22.0920 323.87 42.6681 520.69 0.0000 722. 91 20.5156 325.23 55.2780 522.65 0.0000 723.31 14.2053 328.76 0.0000 527.90 0.0000 724.19 12.6318 333.37 45.5208 528.26 19.1496 727.33 12.6489 333.97 43.0126 529.59 19.1642 733.00 17.4339 334.37 50.6189 529.87 0.0000 735.93 7.4053 338.28 37.2342 531. 02 0.0000 333.97 13.7617 338.32 37.2351 537.26 0.0000 739.50 0.0000 311. 90 47.0461 546.56 0.0000 747.24 20.1960 340.48 47.0461 552.55 31.0443 748.06 19 .1396 340.55 0.0000 563.25 22.4394 752.31 14.0604 344.28 40.8076 569.33 20.5531 753.82 0.0000 345.93 39.8379 946.00 21.5345 756.73 16. 0071 351.06 31.6192 569.70 20.5574 756.80 16.0077 351.93 31.6403 583.19 22. 6715 884.68 27.2930 Page 3306 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.8870 1274.44 2.7970 1620.50 6.1919 766.42 20.8925 1001.03 7.0034 1621.92 5.1617 766.8.4 20.8957 1002.74 13 .1387 1678.03 0.0000 772.60 0.0000 1004.73 13.1470 1690.97 1.0477 776.52 0.0000 507. 63 0.0000 1750.46 0.0000 739.50 0. 0.000 1025.87 0.0000 1764 .. 49 1. 0638 778.90 10.7682 1028.54 0.0000 1063.66 3.4082 783.70 0.0000 1037.84 7.0869 1771.35 3.6525 785.37 22. 6722 1038.76 0.0000 1791.20 0.0000 792.07 23.8154 631.29 17. 7 67 3 1808.65 2.1466 794.95 19.5081 1048.07 0.0000 1810.72 0.0000 795.86 26.0195 1049.04 13.3356 1836.06 0.0000 810.06 13. 0825 1050.41 11.5623 810.29 14.1743 1063.66 13. 3969 344.28 14.174.8 1077.00 0.0000 810.76 15.2675 1077.34 11. 6599 815.77 0.0000 1085.87 11. 6908' 1048.07 0.0000 1093.63 14.4229 832.01 10.9949 1099.45 14.4482 834.85 19;8127 1112. 07 11. 6031 835.71 14.3140 1112. 84 14.5068 836.80 0.0000 1115. 54 11.6148 846.75 0.0000 1120.29 11. 6313 846.77 18.7964 1120.55 11.6320 856.80 0.0000 1221.41 14.5439 860.56 16.6711 1129. 67 20.9589 871.09 20.0830 1131. 51 0.0000 873.19 15.6321 1147.95 0.0000 875.33 0.0000 1173.23 10.1520 879.38 19.0254 1177.95 11. 0896 880.51 12.3155 1189.05 16.6882 883.24 11. 2069 1204.77 13.0370 884.68 12.3343 1221.41 11. 2266 889.28 4.4927 1231. 02 16.8849 894.76 9.0029 1235.36 0.0000 898.04 13.5205 1238.28 11.2793 900.72 12.4059 1260.41 0.0000 903.28 14.6747 1271. 87 16.1253 911.20 15.8480 1274.44 11. 3906 912.08 15.8531 1274.54 11. 3906 923.98 0.0000 1291.59 8.5820 926.50 14.7959 1298.22 0.0000 929 .11 14.8091 1312. 11 0.0000 937.49 '10.2825 1332.49 13.8788 944.13 0.0000 1362.66 0.0000 946.00 . 12. 6042 1365.19 6.8035 949.00 14. 9112 1368.63 0.0000 667.71 0.0000 1384.29 4.8828 962.31 12.6749 1408.01 9.8236 964.08 12.6825 1457.56 0.0000 966 .17 12.6914 1460.82 3.9802 911.20 12.7031 1489.16 6.0103 968. 97 12.7031 1505.03* 8.0435 983.53 0.0000 1584.12 9.2137 !'*) 984.45 0.0000 1596.21 0.0000 Page 3307 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:53:52.33 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM01.CNF;402 Background date : Z-OCT-2016 10:59:55. Sample date 8-DEC-2015 13:50:00. Acquisition date : 3-0CT-2016 08:53:24. Sample ID G405235020 Sample quantity : 1.70763E+02 GRAM Detector name GAMOl Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.37 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 5 5 5 2 2 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 35.35* 40.33* 45.15* 74.90 77.16* 87.73 92.89* 185.65* 209.98 216.83 238.63* 241. 71
  • 295.30* 338.55* 351.87* 388.82 463.85 511.04* 566.51*

583.08* 609.50* 636.61 727.70 737.71 768.80 785.79 860.90 904.69* 911. 34* 964.44 969.20 1063.09 1119.89* 1143.54 Page 3308 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 36 29 19 101 150 46 42 85 95 24 344 94 85 53 224 14 40 46 31 110 118 7 51 25 18 11 31 11 57 28 41 6 39 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 10 55 62 157 151 213 141 176 138 42 59 77 61 55 45 82 66 55 53 35 33 20 20 10 25 13 15 13 22 16 12 5 8 11 1. 84 1. 85 1.16 1. 45 1. 28 0.97 1.12 1. 41 5.43 1. 25 1.15 1. 80 0.84 0.86 1.27 2.33 4.43 1. 72 0.87 1. 53 1. 75 1. 40 3.47 3.50 0.62 1. 51 1. 86 4.40 1.13 1. 32 1. 61 1. 46 1. 43 0.53 71. 39 81. 37 91. 00 150.50 155.01 176.15 186.47 371. 96 420.62 434.33 477.92 484.09 591.25 677.74 704.36 778.26 928.29 1022.65 1133.56 1166.70 1219.53 1273.74 1455.87 1475.89 1538.04 1572. 02 1722.19 1809.75 1823.05 1929.20 1938.71 2126.44 2239.99 2287.27 67 67 67 143 143 170 183 366 413 431 471 471 587 673 699 766 920 1013 1127 1159 1215 1266 1446 1468 1531 1568 1715 1802 1817 1922 1934 2123 2234 2282 32 1.0lE-02 40.9 32 8.00E-03 63.5 32 5.17E-03 72.2 17 2.81E-02 26.0 17 4.16E-02 17.0 9 1.27E-02 59.7 8 1.16E-02 56.2 14 2.37E-02 35.8 18 2.65E-02 30.8 6 6.67E-03 47.3 21 9.55E-02 6.7 21 2.61E-02 24.6 9 2.37E-02 20.1 10 l.48E-02 30.5 12 6.22E-02 9.1 17 3.93E-03148.2 20 1.llE-02 52.1 20 1.27E-02 46.8 16 8.51E-03 56.9 17 3.06E-02 15.7 11 3.29E-02 13.2 11 2.07E-03120.1 16 1.41E-02 24.3 14 6.82E-03 34.5 12 4.86E-03 63.4 8 3.16E-03 63.4 15 8.61E-03 32.6 13 3.18E-03 72.3 11 1.59E-02 21.2 13 7.83E-03 34.9 10 1.13E-02 22.5 6 1. 77E-03 66. 2 11 1. 08E-02 21. 7 7 2.08E-03 80.4 Fit 3.54E+OO 1.02E+OO 1. 09E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235020 Acquisition date 3-0CT-2016 08:53:24 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1155.31 10 10 1. 46 2310.80 2305 10 2.78E-03 67.1 36 0 1173.52 5 4 0.52 2347.20 2346 4 1. 45E-03 74.2 37 0 1234.37 8 20 3.32 2468.87 2459 13 2.08E-03126.8 38 0 1254.20 10 0 1. 66 2508.50 2505 7 2.78E-03 31. 6 39 0 1285.78 11 0 1. 28 2571.64 2568 7 3.06E-03 30.2 40 0 1460.69* 257 9 2.06 2921.30 2915 12 7.15E-02 6.7 41 0 1493.39 12 0 1. 65 2986.67 2982 9 3.33E-03 28.9 42 0 1591. 81 10 0 1. 41 3183.40 3179 8 2.78E-03 31. 6 43 0 1729.55 11 0 1. 72 3458.73 3455 7 3.06E-03 30.2 44 0 1764.44* 21 3 1. 00 3528.46 3522 13 5.94E-03 29.1 Flag: "*" = Peak area was modified by background subtraction Page 3309 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:53:54 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 13:50:00 G405235020 Acquisition date : Sample quantity Sample.geometry Detector geometry: 3-0CT-2016 08:53:24 170.76 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAl 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3310of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.37 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235020 Acquisition date 3-0CT-2016 08:53:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 9 .. 709E-01 1.069E+Ol 1.069E+Ol 13. 46 OK CD-109 88.03 3.70* 4.617E+OO 1.021E+OO 1.602E+OO 1.91. 53 OK SN-126 64.28 9.60 2.409E+OO Line Not Found Absent 86.94 8.90 4.617E+OO 4.245E-01 4.245E-01 191.53 OK 87.57 37.00* 4.617E+OO l.021E-Ol 1.021E-01 191.53 OK TL-208 277.37 6.60 3.944E+OO Line Not Found Absent 583.19 85.00* 2.090E+OO 3.015E-01 3.015E-01 31. 39 OK 860.56 12.50 1.519E+OO 7.551E-01 7.551E-01 65.24 OK PB-210 46.54 4.25* 4.948E-01 5.729E+OO 5.877E+OO 144.32 OK BI-211 72. 87 1. 23 3.328E+OO Line Not Found Absent 351.06 12.92* 3.217E+00 9.887E-01 9.887E-01 89.78 OK BI-212 727.33 6.67* 1. 742E+OO 2.061E+OO 2. 061E+OO 48.56 OK 785.37 1.10 1.636E+OO 2.959E+OO 2.959E+OO 126.79 OK 1620.50 1. 47 8.816E-01 Line Not Found Absent PB-212 74.82 10.28 3.530E+OO 1.345E+OO 1.345E+OO 67.22 OK 77 .11 17.10 3.747E+OO l.433E+OO 1.433E+OO 34.06 OK 238.63 43.60* 4.455E+OO 9.612E-01 9.612E-01 13.33 OK 300.09 3.30 3.690E+OO Line Not Found Absent BI-214 609.32 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 OK 1120.29 14.92 1.223E+OO 9.517E-01 9.521E-01 43.42 OK 1764.49 15.30 8 .116E-01 7.200E-01 7.202E-01 58 .11 OK PB-214 74.82 5.80 3.522E+OO Line Not Found <<INT Reject 77 .11 9.70 3.747E+OO 2.527E+OO 2.528E+OO 34.06 OK 87.09 3.41 4.572E+OO Line Not Found <<INT Reject 242.00 7.25 4.406E+OO Line Not Found <<INT Reject 295.22 18.42 3. 741E+OO 6.557E-01 6.560E-01 40.21 OK 351. 93 35.60* 3. 216E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 OK 1120.29 14.92 1.223E+OO 9.517E-01 9. 521E-01 43.42 OK 1764.49 15.30 8 .116E-01 7.200E-01 7.202E-01 58 .11 OK RA-224 240.99 4.10* 4.410E+OO 1.655E+OO 1.655E+OO 88.30 OK RA-226 609.32 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 OK 1120.29 14.92 1.223E+OO 9.517E-01 9. 521E-01 43.42 OK 1764.49 15.30 8 .116E-01 7.200E-01 7.202E-01 58 .11 OK AC-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 OK 794.95 4.25 1. 621E+OO Line Not Found Absent 835.71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1.450E+OO 7.028E-01 7.028E-01 42.33 OK 968. 97 15.80 1.379E+OO 8.506E-01 8.506E-01 45.09 OK RA-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 OK 794.95 4.25 1. 621E+OO Line Not Found Absent 835.71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1.450E+OO 7.028E-01 7.028E-01 42.33 OK 968. 97 15.80 1.379E+OO 8.506E-01 8.506E-01 45.09 OK TH-228 74.82 10.28 3.530E+OO 1.345E+OO 1.345E+OO 67.22 OK 77 .11 17.10 3.747E+OO 1.433E+OO 1.433E+OO 34.06 OK 238.63 43.60* 4.455E+OO 9.612E-01 9.612E-01 13.33 OK Page 3311 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235020 Acquisition date 3-0CT-2016 08:53:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 3. 6.90E+OO Line Not Found Absent TH-230 609.32 45.49* 2.015E+OO 6.255E-01 6.255E-01 26.31 OK 1120.29 14.92 1.223E+OO 9.517E-01 9.517E-01 43.42 OK 1764.49 15.30 8.116E-01 7.200E-01 7.200E-01 58 .11 OK TH-232 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 OK 835.71 1. 61 i.557E+OO Line Not Found Absent 911.20 25.80* 1.450E+OO 7.028E-01 7.028E-01 42.33 OK 968. 97 15.80 1.379E+OO 8.506E-01 8.506E-01 45.09 OK U-234 609.32 45.49* 2.015E+OO 6.255E-01 6.255E-01 26.31 OK 1120.29 14.92 1.223E+OO 9.517E-01 9.517E-01 43.42 OK 1764.49 15.30 8 .116E-01 7.200E-01 7.200E-01 58 .11 OK AM-243 43.53 5.90 3.822E-01 Line Not Found Absent 74. 66. 67.20* 3.530E+OO 2.057E-01 2.057E-01 67.22 OK CF-249 252.80 2.50 4.256E+OO Line Not Found Absent 333.37 14.60 3.371E+OO Line Not Found Absent 388.16 66.00* 2.950E+OO 3.721E-02 3.727E-02 296.41 OK ANH-511 511. 00 100.00* 2.334E+OO 9.690E-02 9.690E-02 93.64 OK Flag: "*" = Keyline Page 3312of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:53:55.25 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l * *Acquisition date 3-0CT-2016 08:53:24 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.37 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:50:00 Analyst initials: MXRl * *Sample ID G405235020 Sample Quantity 1.7076E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1. 069E+Ol l.409E+OO 5.458E-01 CD-109 1.602E+OO 3.007E+OO 2. 651E+OO SN-126 1. 021E-01 1.917E-01 1.565E-01 TL-208 3.015E-01 9.276E-02 5.255E-02 PB-210 5.877E+OO 8.313E+OO 5.825E+OO BI-211 9.887E-01 8.698E-01 3.512E-01 BI-212 2. 061E+OO 9.807E-01 7.016E-01 PB-212 9.612E-01 1.255E-01 8.471E-02 BI-214 6.257E-01 l.613E-01 1. 341E-01 PB-214 1.015E+OO 1.814E-01 3.053E-01 RN-222 6.257E-01 1. 613E-01 1.341E-01 RA-224 1.655E+OO 1.432E+OO 9.080E-01 RA-226 6.257E-01 1. 613E-01 1.341E-01 AC-228 7.028E-01 2.916E-01 2.577E-01 RA-228 7.028E-01 2.916E-01 2.577E-01 TH-228 9.612E-01 l.255E-01 8. 471E-02 TH-230 6.255E-01 1. 613E-01 1. 341E-01 TH-232 7.028E-01 2.916E-01 2.577E-01 U-234 6.255E-01 1.613E-01 1. 341E-01 AM-243 2.057E-01 l.355E-01 9.483E-02 CF-249 3. 727E-02 l.083E-01 6.516E-02 ANH-511 9.690E-02 8.892E-02 4.329E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -4.924E+00 1.067E+Ol 1.994E+Ol NOT IDENT. NA-22 2.738E-02 4.452E-02 l.007E-01 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 l.405E-02 1.733E-02 5.652E-02 NOT IDENT. SC-46 4.814E-02 3.610E-01 7.244E-01 FAIL ABUN V-48 O.OOOE+OO 1.335E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 3.813E+02 O.OOOE+OO SHORT HLIF MN-54 2. 968E-02 5.948E-02 1.255E-01 NOT IDENT. Page 3313 of 5809 C0-56 1. 764E-01 4.299E-01 9.045E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -3.997E-02 4.279E-02 8.228E-02 NOT IDENT. C0-58 -2.614E-01 5.486E-01 9.853E-01 NOT IDENT. FE-59 -2.573E+OO 6.343E+OO l.130E+Ol NOT IDENT. C0-60 -2.207E-02 2.975E-02 5.307E-02 FAIL ABUN ZN-65 -2.641E-02 l.685E-01 2.802E-01 NOT IDENT. GE-68 -6.242E-01 2.138E+OO 3.931E+OO NOT IDENT. AS-73 2. 796E+00 1.080E+Ol 2.143E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.875E+03 O.OOOE+OO SHORT HLIF SE-75 5.865E-02 1. 871E-01 3.847E-01 NOT IDENT. BR-77 O.OOOE+OO 2.235E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.128E+02 O.OOOE+OO SHORT HLIF RB-83 -5.550E-04 5.099E-01 l.031E+OO NOT IDENT. KR-85 2.082E+OO 5.606E+OO 1.174E+Ol NOT IDENT. SR-85 2.176E-01 5.918E-01 1.239E+OO NOT IDENT. RB-86 0.000E+OO 2.610E+04 O.OOOE+OO SHORT HLIF Y-88 -4. 372E-02 2.273E-01 4.699E-01 NOT IDENT. Y-91 l.208E+02 4.561E+02 9.861E+02 NOT IDENT. NB-94 1.537E-02 3.167E-02 6.535E-02 NOT IDENT. NB-95 4.826E-01 9.693E-01 1.815E+OO NOT IDENT. NB-95M -1.840E-01 2.374E+OO 4.219E+OO NOT IDENT. ZR-95 -2.812E-01 l.414E+OO 2.659E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.531E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 851E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 7.438E-04 6. 716E-02 NOT IDENT. RH-102 -l.297E-02 4.933E-02 8. 361E-02 NOT IDENT. RU-103 -4.617E+OO 5.126E+OO 8.870E+OO FAIL ABUN RH-106 -4.426E-01 4.392E-01 7.218E-01 NOT IDENT. RU-106 -4.426E-01 4.392E-01 7.218E-01 NOT IDENT. AG-108M 7.609E-05 2.467E-02 4.916E-02 NOT IDENT. AG-110M 4.315E-02 8.373E-02 1.836E-01 NOT IDENT. SN-113 4.383E-02 2.244E-01 4.133E-01 NOT IDENT. CD-115 O.OOOE+OO 2.477E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 8.817E+04 O.OOOE+OO SHORT HLIF TE-123M 7.173E-02 l.193E-01 2.513E-01 NOT IDENT. SB-124 l.758E+OO 2.005E+00 5.217E+OO NOT IDENT. SB-125 1. 072E-02 8.474E-02 1.730E-01 FAIL ABUN TE-125M 9.450E+Ol 2. 968E+02 5.647E+02 NOT IDENT. I-126 O.OOOE+OO 7.657E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 341E+06 O.OOOE+OO SHORT HLIF . SB-127 O.OOOE+OO 2.012E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.540E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.687E+26 O.OOOE+OO SHORT HLIF BA-133 -4.435E-03 4.221E-02 7.404E-02 NOT IDENT. I-133 O.OOOE+OO l.823E+41 O.OOOE+OO SHORT HLIF CS-134 3.244E-02 4.509E-02 9.842E-02 NOT IDENT. CS-135 -7.638E-02 l.329E-01 2. 513E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2. 541E+o5 O.OOOE+OO SHORT HLIF BA-137M 3. 751E-02 3.609E-02 7.869E-02 NOT IDENT. CS-137 3. 962E-02 3.813E-02 8.313E-02 NOT IDENT. CE-139 -3.178E-02 9.683E-02 1.917E-01 NOT IDENT. BA-140 O.OOOE+OO l.208E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.755E+05 O.OOOE+OO SHORT HLIF CE-141 3 .115E-01 2.283E+Ol 4.630E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 1.498E-01 3.408E-01 7.123E-01 NOT IDENT. PM-144 4.402E-02 5.266E-02 l.146E-01 NOT IDENT. PR-144 3.809E+OO 4.572E+OO 9.951E+OO NOT IDENT. PM-146 -l.214E-02 3.260E-02 6.245E-02 NOT IDENT. ND-147 O.OOOE+OO 3.024E+07 O.OOOE+OO SHORT HLIF PM-147 -2.548E+02 7.513E+02 1.508E+03 NOT IDENT. PM-149 O.OOOE+OO 4.33iE+40 O.OOOE+OO SHORT HLIF EU-150 -1.270E-02 2.744E-02 4.574E-02 FAIL ABUN EU-152 -7.684E-02 8.370E-02 l.499E-01 FAIL ABUN GD-153 -1. 7 93E-01 l.938E-01 3.322E-01 NOT IDENT. EU-154 6.338E-02 1.083E-01 2.445E-01 NOT IDENT. EU-155 6.365E-02 1.031E-01 2.037E-01 FAIL ABUN TB-160 -7.199E-01 1.731E+OO 3.134E+OO FAIL ABUN H0-166M 2.188E-02 4.819E-02 1.026E-01 FAIL ABUN TM-171 6.729E+OO 2.542E+Ol 5.066E+Ol NOT IDENT. HF-172 -7.921E-02 2.098E-01 4.189E-01 NOT IDENT. LU-172 3.032E-02 6.454E-02 l.402E-01 FAIL ABUN LU-176 -1. 611E-02 2.231E-02 4.127E-02 FAIL ABUN Page 3314of5809 HF-181 2.602E+OO 3.542E+OO 7. 821E+OO NOT IDENT. TA-182 2.248E-01 8.492E-01 1.808E+OO FAIL ABUN RE-183 -5.144E-01 3.730E+OO 7.089E+OO NOT IDENT. RE-184 3.349E+Ol 4.743E+Ol 5.484E+Ol FAIL ABUN W-188 1.903E+Ol 1.140E+02 2.079E+02 NOT IDENT. IR-192 6.747E-02 4.262E-01 8. 613E-01 FAIL ABUN HG-203 -9.829E-01 2.254E+OO 4.310E+OO NOT IDENT. BI-207 3.053E-02 3. 961E-02 9.927E-02 FAIL ABUN PB-211 -1.031E-01 5.692E-01 1. lllE+OO NOT IDENT. RN-219 -1.239E-02 3.529E-01 6. 960E-01 NOT IDENT. RA-223 -3.173E-01 4.935E-01 9.193E-01 FAIL ABUN AC-227 2.433E-02 2.086E-01 4.208E-01 NOT IDENT. TH-227 2.433E-02 2.086E-01 4.208E-01 NOT I DENT.
  • TH-229 -3.639E-02 4.542E-01 9.037E-01 FAIL ABUN PA-231 1.156E-01 4.450E-01 8.958E-01 NOT IDENT. TH-231 -3.173E-01 4.935E-01 9.193E-01 FAIL ABUN PA-233 -1. 38 9E-02 5.283E-02 l.027E-01 NOT IDENT. PA-234 -l.350E-02 2. 696E-01 5.200E-01 NOT IDENT. PA-234M 1.356E+OO 4.383E+OO 9.216E+OO NOT IDENT. TH-234 -4.212E-01 1.464E+OO 2.801E+OO FAIL ABUN U-235 -7.525E-02 1. 741E-01 3.446E-01 FAIL ABUN NP-237 -l.389E-02 5.283E-02 l.027E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 611E+41 O.OOOE+OO SHORT HLIF U-238 -4.212E-01 1.464E+OO 2.801E+OO FAIL ABUN NP-239 -3.997E-02 2.683E-01 4.895E-01 NOT IDENT. PU-239 2.487E+02 3.152E+02 6.675E+02 NOT IDENT. AM-241 -2.316E-02 1.566E-01 2.979E-01 NOT IDENT. CM-243 1.022E-01 1.799E-01 NOT IDENT. BK-247 2.848E-02 6.512E-02 l.352E-01 NOT IDENT. CM-247 4.868E-03 3 .. 055E-02 6.195E-02 NOT IDENT. CF-251 -5.439E-02 l.037E-01 2.013E-01 NOT IDENT. Page 3315of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:53:53.04 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 252 10.66* 9.709E-01 1.069E+Ol l.069E+Ol 13.46 CD-109 88.03 63 3.70* 4.617E+OO 1.625E+OO 2.550E+OO 119. 39 SN-126 64.28 ------9.60 2.409E+OO ------Line Not Found ------86.94 63 8.90 4.617E+OO 6.758E-01 6.758E-01 119.39 87.57 63 37.00* 4.617E+OO 1.625E-01 1.625E-01 119.39 TL-208 277.37 ------6.60 3.944E+OO ------Line Not Found ------583.19 122 85.00* 2.090E+OO 3.015E-01 3.015E-01 31. 39 860.56 33 12.50 1.519E+OO 7. 551E-01 7. 551E-01 65.24 PB-210 46.54 27 4.25* 4.948E-01 5.729E+00 5.877E+OO 144.32 BI-211 72. 87 ------1. 23 3.328E+OO ------Line Not Found ------351.06 264 12.92* 3.217E+OO 2.795E+OO 2.795E+OO 18.24 BI-212 727.33 54 6.67* 1.742E+OO 2.061E+OO 2.061E+OO 48.56 .785.37 12 1.10 1.636E+OO 2.959E+OO 2.959E+OO 126.79 1620.50 ------1. 47 8.816E-01 ------Line Not Found ------PB-212 74.82 142 10.28 3.530E+OO l.714E+00 1.714E+OO 52.00 77 .'11 209 17.10 3.747E+OO 1.433E+OO 1.433E+OO 34.06 238.63 425 43.60* 4.455E+OO 9.612E-01 9.612E-01 13.33 300.09 ------3.30 3.690E+OO ------Line Not Found ------BI-214 609.32 130 45.49* 2.015E+00 6.255E-01 6.257E-01 26.31 1120.29 40 14.92 1. 223E+OO 9.517E-01 9. 521E-01 43.42 1764.49 20 15.30 8 .116E-01 7.200E-01 7.202E-01 58 .11 PB-214 74.82 142 5.80 3.530E+OO 3.039E+00 3.040E+OO 52.00 77 .11 209 9.70 3.747E+OO 2.527E+OO 2.528E+OO 34.06 87.09 63 3.41 4.617E+00 1. 764E+OO 1. 764E+OO 119. 39 242.00 116 7.25 4.410E+OO 1.592E+OO 1.592E+OO 49.21 295.22 103 18.42 3. 741E+OO 6.557E-01 6.560E-01 40.21 351. 93 264 35.60* 3.217E+OO 1.015E+OO l.015E+OO 18.24 RN-222 609.32 130 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 1120.29 40 14.92 1.223E+OO 9.517E-01 9.521E-01 43.42 1764.49 20 15.30 8.116E-01 7.200E-01 7.202E-01 58 .11 RA-224 240.99 116 4.10* 4.410E+OO 2.815E+OO 2.815E+OO 49.21 RA-226 609.32 130 45.49* 2.015E+OO 6.255E-01 6.257E-01 26.31 1120.29 40 14.92 1.223E+OO 9.517E-01 9.521E-01 43.42 1764.49 20 15.30 8 .116E-01 7.200E-01 7.202E-01 58.11 AC-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 794.95 ------4.25 1.621E+OO ------Line Not Found ------835.71 ------1. 61 l.557E+OO ------Line Not Found ------911. 20 60 25.80* 1.450E+OO 7.028E-01 7.028E-01 42.33 968.97 42 15.80 1.379E+OO 8.506E-01 8.506E-01 45.09 RA-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11.27 3.326E+OO 7.402E-01 7.402E-01 61.04 794.95 ------4.25 1. 621E+OO ------Line Not Found ------835.71 ------1. 61 1.557E+OO ------Line Not Found ------911.20 60 25.80* l.450E+OO 7.028E-01 7.028E-01 42.33 968. 97 42 15.80 1. 379E+OO 8.506E-01 8.506E-01 45.09 TH-228 74.82 142 10.28 3.530E+OO 1.714E+OO 1. 714E+00 52.00 Page 3316of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235020 Acquisition date 3-0CT-2016 08:53:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 . 209 17.10 3.747E+OO 1. 433E+OO l.433E+OO 34.06 238.63 425 43.60* 4.455E+OO 9.612E-01 9.612E-01 13.33 300.09 ------3.30 3.690E+OO ------Line Not Found ------TH-230 609.32 130 45.49* 2.015E+OO 6.255E-01 6.255E-01 26.31 1120.29 40 14.92 1.223E+OO 9.517E-01 9.517E-01 43.42 1764.49 20 15.30 8 .116E-01 7.200E-01 7.200E-01 58 .11 TH-232 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.326E+OO 7.402E-01 7.402E-01 61. 04 835.71 ------1. 61 1.557E+OO ------Line Not Found ------911. 20 60 25.80* 1.450E+OO 7.028E-01 7.028E-01 42.33 968.97 42 15.80 1.379E+OO 8.506E-01 8.506E-01 45.09 U-234 609.32 130 45.49* 2.015E+OO 6.255E-01 6.255E-01 26. 31 1120.29 40 14.92 1.223E+OO 9.517E-01 9.517E-01 43.42 1764.49 20 15.30 8.116E-01 7.200E-01 7.200E-01 58 .11 AM-243 43.53 ------5.90 3.822E-01 ------Line Not Found ------74.66 142 67.20* 3. 530E+OO. 2.623E-01 2.623E-01 52.00 CF-249 252.80 ------2.50 4.256E+OO ------Line Not Found ------333.37 ------14.60 3.371E+OO ------Line Not Found ------388.16 16 66.00* 2.950E+OO 3.721E-02 3.727E-02 296. 41 ANH-511 511. 00 51 100.00* 2.334E+OO 9.690E-02 9.690E-02 93.64 Flag: "*" Key line Page 3317 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235020 Acquisition date 3-0CT-2016 08:53:24 Total number of lines in spectrum 44 Number of unidentified lines 11 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-40 CD-109 SN-126 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 'TH-228 TH-230 TH-232 U-234 AM-243 CF-249 ANH-511 Hlife l.25E+09Y 461. 400 2.30E+05Y 1. 41E+l0Y 22.20Y 7.04E+08Y 1. 41E+10Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y 1.41E+10Y 1600.00Y 1.41E+10Y l.41E+l0Y 1. 41E+10Y 7.54E+04Y 1. 41E+10Y 2.45E+05Y 7370.00Y 351. OOY l.OOE+09Y Decay 1. 00 1. 57 1. 00 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 069E+Ol 1. 625E+OO 1.625E-01 3.015E-01 5.729E+OO 2.795E+OO 2.061E+OO 9.612E-01 6.255E-01 1.015E+OO 6.255E-01 2.815E+OO 6.255E-01 7.028E-01 7.028E-01 9.612E-01 6.255E-01 7.028E-01 6.255E-01 2.623E-01 3. 721E-02 9.690E-02 3.475E+Ol 3.475E+Ol Decay Corr pCi/GRAM 1.069E+Ol 2.550E+OO 1.625E-01 3.015E-01 5.877E+00 2.795E+OO 2.061E+OO 9.612E-01 6.257E-01 1.015E+OO 6.257E-01 2.815E+00 6.257E-01 7.028E-01 7.028E-01 9.612E-01 6.255E-01 7.028E-01 6.255E-01 2.623E-01 3. 727E-02 9.690E-02 3.582E+Ol 3.582E+Ol 75.00% Decay Corr 2-Sigma Error 0.144E+Ol 3.045E+OO 1.941E-01 0.947E-01 8.483E+OO 0.510E+OO 1.00lE+OO 1.281E-01 1.646E-01 0.185E+OO 1.646E-01 1.385E+OO 1.646E-01 2.975E-01 2.975E-01 1.281E-01 1.646E-01 2.975E-01 l.646E-01 1.364E-01 11. 05E-02 9.074E-02 "M" Manually accepted 2-Sigma %Error 13.46 119. 39 119. 39 31. 39 144.32 18.24 48.56 13.33 26.31 18.24 26.31 49.21 26.31 42.33 42.33 13.33 26.31 42.33 26.31 52.00 296.41 93.64 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3318 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235020 Acquisition date : 3-0CT-2016 08:53:24 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 35.35 55 15 1. 84 71. 39 67 32 l.OlE-02 81.7 4.02E-02 5 40.33 43 82 1. 85 81. 37 67 32 8.00E-03 **** 2.0lE-01 0 92.89 57 193 1.12 186.47 183 8 l.16E-02 **** 4.95E+OO T 0 185.65 108 223 1. 41 371.96 366 14 2.37E-02 71. 6 5.30E+OO T 0 209.98 119 172 5.43 420.62 413 18 2.65E-02 61. 5 4.90E+OO T 0 216.83 30 52 1. 25 434.33 431 6 6.67E-03 94.6 4.79E+OO T 0 463.85 45 75 4.43 928.29 920 20 l. llE-02 **** 2.53E+00 T 0 566.51 34 59 0.87 1133. 56 1127 16 8.51E-03 **** 2.14E+OO 0 636.61 8 21 1. 40 1273.74 1266 11 2.07E-03 **** 1.94E+OO T 0 737.71 26 11 3.50 1475.89 1468 14 6.82E-03 69.0 1. 72E+OO T 0 768.80 19 26 0.62 1538.04 1531 12 4.86E-03 **** 1. 67E+OO 0 904.69 12 14 4.40 1809.75 1802 13 3.18E-03 **** l.46E+OO T 0 964.44 29 16 1. 32 1929.20 1922 13 7.83E-03 69.8 l.38E+OO T 0 1063.09 7 5 1. 46 2126.44 2123 6 l.77E-03 **** l.28E+OO T 0 1143.54 8 11 0.53 2287.27 2282 7 2.08E-03 **** 1.20E+OO 0 1155.31 10 10 1. 46 2310.80 2305 10 2.78E-03 **** 1.19E+OO 0 1173.52 5 4 0.52 2347.20 2346 4 l.45E-03 **** 1.18E+OO T 0 1234.37 8 20 3.32 2468.87 2459 13 2.08E-03 **** 1.13E+OO T 0 1254.20 10 0 1. 66 2508.50 2505 7 2.78E-03 63.2 1. llE+OO 0 1285.78 11 0 1.28 2571.64 2568 7 3.06E-03 60.3 1.09E+OO 0 1493.39 12 0 1. 65 2986.67 2982 9 3.33E-03 57.7 9. 51E-01 0 1591.81 10 0 1. 41 3183.40 3179 8 2.78E-03 63.2 8 *. 97E-01 0 1729.55 10 0 1. 72 3458.73 3455 7 3.06E-03 60.3 8.28E-01 Flags: "T" = Tentatively associated Page 3319of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:54:10.66 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l *
  • Acquisition date 3-0CT-2016 08:53:24 Sensitivity 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.37 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:50:00 Nuclide Library : SOLID *
  • Sample ID G405235020 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : l.7076E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMOl CAN.'CNF;9
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-243 CF-249 ANH-511 Le (pCi/GRAM 2.147E-01 l.266E+OO 7.444E-02 2.278E-02 2.644E+OO l.605E-01 2.978E-01 3.908E-02 6.032E-02 l.472E-01 6.032E-02 4.189E-01 6.032E-02 l.125E-01 l.125E-01 3.908E-02 6.030E-02 l.125E-01 6.030E-02 4.462E-02 2.935E-02 l.898E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 3320 of 5809 Le (pCi/GRAM 8.769E+00 4.349E-02 0.000E+OO 2.069E-02 3.128E-01 O.OOOE+OO O.OOOE+OO 5.509E-02 3.935E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3321 of 5809 O.OOOE+OO 3.837E-02 4.200E-01 4. 727E+OO 2.014E-02 l.172E-01 1.644E+OO 1.002E+Ol O.OOOE+OO 1. 775E-.Ol O.OOOE+OO O.OOOE+OO 4.485E-01 5.218E+OO 5.506E-01 O.OOOE+OO 1. 807E-01 4.224E+02 2.923E-02 8.131E-01 1.963E+OO 1.158E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.167E-02 3.523E-02 3.864E+OO 3.058E-01 3.058E-01 2.200E-02 7.879E-02 1. 866E-01 O.OOOE+OO O.OOOE+OO 1.180E-01 2.139E+OO 7.700E-02 2.664E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.366E-02 O.OOOE+OO 4.337E-02 1.159E-01 O.OOOE+OO O.OOOE+OO 3.563E-02 3.764E-02 8.935E-02 0.000E+OO O.OOOE+OO 2.179E+Ol O.OOOE+OO 3.357E-01 5.125E-02 4.448E+OO 2.709E-02 0.000E+OO 7.058E+02 O.OOOE+OO 2.089E-02 6.742E-02 1.558E-01 l.054E-01 9.556E-02 1.326E+OO 4.488E-02 2.364E+Ol 1. 963E-01 5. 961E-02 l.877E-02 3.485E+OO SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-251 Page 3322 of 5809 7.829E-01 3.325E+00 2.353E+Ol 9.581E+Ol 3.945E-01 1.984E+OO 4.314E-02 4.974E-01 3.149E-01 4.139E-01 l.945E-01 l.945E-01 4.238E-01 4.158E-01 4.139E-01 4.676E-02 2.238E-01 4.068E+OO l.323E+00 l.623E-01 4.676E-02 O.OOOE+OO 1.323E+OO 2.306E-01 3.164E+02 l.392E-01 8. 411E-02 6.244E-02 2.793E-02 9.384E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL' ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:54:17.70 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235020.CNF;l *
  • Acquisition date 3-0CT-2016 08:53:24 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.37 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:50:00 Nuclide Library : SOLID *
  • Sample ID G405235020 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : 1.7076E+02 GRAM *
  • Quantity Err(%) : 1.1712E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 1.069E+Ol 1.516E+OO CD-109 l.602E+OO 3.012E+OO SN-126 1.021E-01 l.919E-01 TL-208 3.015E-01 9.364E-02 PB-210 5.877E+OO 8.343E+OO BI-211 9.887E-01 8.779E-01 BI-212 2. 061E+OO 9.862E-01 PB-212 9.612E-01 1.355E-01 BI-214 6.257E-01 l.635E-01 PB-214 1.015E+OO 1. 8 62E-01 RN-222 6.257E-01 l.635E-01 RA-224 1.655E+OO l.437E+OO RA-226 6.257E-01 l.635E-01 AC-228 7.028E-01 2.938E-01 RA-228 7.028E-01 2.938E-01 TH-228 9.612E-01 1.355E-01 TH-230 6.255E-01 1.635E-01 TH-232 7.028E-01 2.938E-01 U-234 6.255E-01 l.635E-01 AM-243 2.057E-01 1.363E-01 CF-249 3.727E-02 l.083E-01 ANH-511 9.690E-02 8.901E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 3323 of 5809 Key-Line Activity (pCi/GRAM -4.924E+OO 2.738E-02 l.000E+41 l.405E-02 4.814E-02 4.336E+03 -2.615E+02 2. 968E-02 K.L Act error ( 1. 96-sigma) 1.068E+Ol 4.453E-02 2.203E+42 l.736E-02 3.611E-01 1.335E+04 3.815E+02 5.950E-02 TPU (1. 96-sigma) 1.516E+OO 3.012E+OO 1.919E-01 9.364E-02 8.343E+OO 8.779E-01 9.862E-01 l.355E-01 l.635E-01 l.862E-01 1.635E-01 1.437E+OO l.635E-01 2.938E-01 2.938E-01 l.355E-01 1.635E-01 2.938E-01 l.635E-01 1.363E-01 1.083E-01 8. 901E-02 TPU (1.96-sigma) 1.090E+Ol 4.621E-02 O.OOOE+OO l.848E-02 3.617E-01 l.349E+04 3.993E+02 6.098E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1. 764E-01 4.299E-01 4.372E-01 NOT IDENT. MN-56 l.000E+41 2.437E+41 O.OOOE+OO SHORT HLIF C0-57 -3.997E-02 4.283E-02 4.646E-02 NOT IDENT. C0-58 -2.614E-01 5.487E-01 5.612E-01 NOT IDENT. FE-59 -2.573E+OO 6.346E+OO 6.451E+OO NOT IDENT. C0-60 -2.207E-02 2.976E-02 3.138E-02 FAIL ABUN ZN-65 -2.641E-02 1.685E-01 1. 689E-01 NOT IDENT. GE-68 -6.242E-01 2.138E+OO 2.156E+OO NOT IDENT. AS-73 2.796E+OO 1.081E+Ol 1.088E+Ol NOT IDENT. AS-74 1.607E+03 5. 877E+03 5.921E+03 SHORT HLIF SE-75 5.865E-02 1. 871E-01 1. 890E-01 NOT IDENT. BR-77 1. 712E+38 l.481E+39 O.OOOE+OO SHORT HLIF SR-82 -l.858E+02 6.129E+02 6.186E+02 SHORT HLIF RB-83 -5.550E-04 5.099E-01 5.099E-01 NOT IDENT. KR-85 2.082E+OO 5.607E+OO 5.685E+OO NOT IDENT. SR-85 2.176E-01 5.918E-01 5.999E-01 NOT IDENT. RB-86 -5.605E+03 2.610E+04 2.622E+04 SHORT HLIF Y-88 -4. 372E-02 2.273E-01 2.282E-01 NOT IDENT. Y-91 1.208E+02 4. 561E+02 4.594E+02 NOT IDENT. NB-94 l.537E-02 3.167E-02 3.242E-02 NOT IDENT. NB-95 4.826E-01 9.696E-01 9.937E-01 NOT IDENT. NB-95M -1.840E-01 2.374E+OO 2.375E+OO NOT IDENT. ZR-95 -2.812E-01 1.414E+OO 1.419E+OO NOT IDENT. NB-97 1.000E+41 1.668E+42 0.000E+OO SHORT HLIF ZR-97 1.000E+41 l.531E+41 O.OOOE+OO SHORT HLIF M0-99 -2.145E+31 1. 851E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 2.467E+41 O.OOOE+OO SHORT HLIF RH-101 7.438E-04 3.293E-02 3.294E-02 NOT IDENT. RH-102 -1.297E-02 4.934E-02 4. 969E-02 NOT IDENT. RU-103 -4.617E+OO 5 .131E+OO 5.537E+OO FAIL ABUN RH-106 -4.426E-01 4.400E-01 4.832E-01 NOT IDENT. RU-106 -4.426E-01 4.400E-01 4.832E-01 NOT IDENT. AG-108M 7.609E-05 2.467E-02 2.467E-02 NOT IDENT. AG-llOM 4.315E-02 8.376E-02 8.599E-02 NOT IDENT. SN-113 4.383E-02 2.245E-01 2.253E-01 NOT IDENT. CD-115 3. 351E+38 2.478E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 9.722E+03 8.818E+04 8.829E+04 SHORT HLIF TE-123M 7.173E-02 1.193E-01 l.236E-01 NOT IDENT. SB-124 1. 758E+OO 2.008E+OO 2.158E+OO NOT IDENT. SB-125 1. 072E-02 8.474E-02 8.488E-02 FAIL ABUN TE-125M 9.450E+Ol 2. 969E+02 2.999E+02 NOT IDENT. I-126 3.377E+05 7. 671E+05 7.820E+05 SHORT HLIF SB-126 -1.330E+05 1.341E+06 l.342E+06 SHORT HLIF SB-127 -3.836E+20 2.013E+22 O.OOOE+OO SHORT HLIF I-131 l.689E+09 4.541E+09 4.604E+09 SHORT HLIF I-132 -1.000E+41 1.877E+42 O.OOOE+OO SHORT HLIF TE-132 l.652E+26 3.747E+26 O.OOOE+OO SHORT HLIF BA-133 -4.435E-03 4.221E-02 4.226E-02 NOT IDENT. I-133 1.000E+41 2.568E+41 O.OOOE+OO SHORT HLIF CS-134 3.244E-02 4. 511E-02 4.743E-02 NOT IDENT. CS-135 -7.638E-02 1.330E-01 l.374E-01 NOT IDENT. I-135 -1.000E+41 9 .112E+41 O.OOOE+OO SHORT HLIF CS-136 -2. 013E+05 2.551E+05 2.707E+05 SHORT HLIF BA-137M 3.751E-02 3.613E-02 3.989E-02 NOT IDENT. CS-137 3. 962E-02 3.817E-02 4.214E-02 NOT IDENT. CE-139 -3.178E-02 9.704E-02 9.810E-02 NOT IDENT. BA-140 4 .119E+05 1.208E+06 l.223E+06 SHORT HLIF LA-140. 1.304E+05 3.755E+05 3.801E+05 SHORT HLIF CE-141 3 .115E-01 2.283E+Ol 2.283E+Ol NOT IDENT. CE-143 -l.000E+41 2.145E+41 O.OOOE+OO SHORT HLIF CE-144 1.498E-01 3.409E-01 3.476E-01 NOT IDENT. PM-144 4.402E-02 5.273E-02 5.634E-02 NOT IDENT. PR-144 3.809E+OO 4.575E+OO 4.886E+OO NOT IDENT. PM-146 -l.214E-02 3.261E-02 3.307E-02 NOT IDENT. ND-147 6.976E+06 3.024E+07 3.040E+07 SHORT HLIF PM-147 -2.548E+02 7.514E+02 7. 601E+02 NOT IDENT. PM-149 -2.895E+39 4.331E+40 O.OOOE+OO SHORT HLIF EU-150 -l.270E-02 2.745E-02 2.804E-02 FAIL ABUN EU-152 -7. 684E:.._02 8.381E-02 9.069E-02 FAIL ABUN GD-153 -l.793E-01 l.941E-01 2.103E-01 NOT IDENT. EU-154 6.338E-02 1.084E-01 l.121E-01 NOT IDENT. EU-155 6.365E-02 l.032E-01 1. 071E-01 FAIL ABUN TB-160 -7.199E-01 1. 731E+OO 1. 762E+OO FAIL ABUN H0-166M 2.188E-02 4.821E-02 4.921E-02 FAIL ABUN TM-171 6.729E+OO 2.543E+Ol 2. 561E+Ol NOT IDENT. HF-172 -7.921E-02 2.102E-01 2.132E-01 NOT IDENT. LU-172 3.032E-02 6.461E-02 6.604E-02 FAIL ABUN LU-176 -1.611E-02 2.232E-02 2.347E-02 FAIL ABUN Page 3324 of 5809 HF-181 2.602E+OO 3.544E+OO 3.733E+OO NOT IDENT. TA-182 2.248E-01 8.493E-01 8.553E-01 FAIL ABUN RE-183 -5.144E-01 3.731E+OO 3.738E+OO NOT IDENT. RE-184 3.349E+Ol 4.810E+Ol 5.042E+Ol FAIL ABUN W-188 1.903E+Ol l.141E+02 l.144E+02 NOT IDENT. IR-192 6.747E-02 4.262E-Ol 4.273E-01 FAIL ABUN HG-203 -9.829E-01 2.255E+OO 2.298E+OO NOT IDENT. BI-207 3.053E-02 3. 963E-02 4.195E-02 FAIL ABUN PB-211 -l.031E-01 5.692E-01 5. 711E-01 NOT IDENT. RN-219 -l.239E-02 3.529E-01 3.529E-01 NOT IDENT. RA-223 -3.173E-Ol 4.939E-01 5.142E-01 FAIL ABUN AC-227 2.433E-02 2.086E-01 2.089E-01 NOT IDENT. TH-227 2.433E-02 2.086E-01 2.089E-01 NOT IDENT. TH-229 -3.639E-02 4.542E-01 4.545E-01 FAIL ABUN PA-231 1.156E-01 4.457E-01 4.487E-01 NOT IDENT. TH-231 -3.173E-01 4.939E-01 5.142E-01 FAIL ABUN PA-233 -1. 38 9E-02 5.284E-02 5.321E-02 NOT IDENT. PA-234 -1.350E-02 2.701E-01 2.702E-01 NOT IDENT. PA-234M 1.356E+OO 4.383E+OO 4.426E+OO NOT IDENT. TH-234 -4.212E-01 1.467E+OO 1.479E+OO FAIL ABUN U-235 -7.525E-02 1.742E-01 1.774E-01 FAIL ABUN NP-237 -1. 389E-02 5.284E-02 5.321E-02 NOT IDENT. NP-238 -1.000E+41 l.612E+41 0.000E+OO SHORT HLIF U-238 -4.212E-01 1.467E+OO 1.479E+OO FAIL ABUN NP-239 -3.997E-02 2.684E-01 2.690E-01 NOT IDENT. PU-239 2.487E+02 3.154E+02 3.347E+02 NOT IDENT. AM-241 -2.316E-02 1.566E-01 1.569E-01 NOT IDENT. CM-243' -6.645E-02 l.024E-01 l.067E-01 NOT IDENT. BK-247 2.848E-02 6.537E-02 6.662E-02 NOT IDENT. CM-247 4.868E-03 3.056E-02 3.064E-02 NOT IDENT. CF-251 -5.439E-02 l.039E-01 l.067E-01 NOT IDENT. Page 3325 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 32.3526 87.09 125.0983 136.47 94.4772 45.60 32.4465 87.57 125.1552 140.51 0.0000 46.54 32.4883 88.03 149.1172 143.76 88.1912 49. 72 0.0000 88.34 137. 8120 144.24 93.3104 51. 35 67.7282 88.47 137.8284 145.44 84.8999 51. 87 61. 9311 89. 96 119. 3485 152.43 79.3401 52.39 59.6337 1093.63 119. 4240 153.25 0.0000 52.97 54.9971 91.11 0.0000 323.87 68.3325 53.44 63.2258 92.59 113.5360 156.02 0.0000 54.07 73.8219 93.35 113.6148 158.56 0.0000 57.36 0.0000 94. 56 66.8581 159.00 65.1254 57.53 71. 7839 94.65 66.8636 162.33 63.5516 57.98 80.0647 94.67 66.8648 162.66 0.0000 59.27 70.7545 94.87 78.2949 163.33 60.1563 59.32 70.7588 97.43 99.3207 165.86 70.5847 59.54 70.7774 98.43 81. 0000 176.31 74.5230 60. 96 89.8015 98.44 81.0010 176.60 0.0000 61.17 89.8235 99.53 78.6221 177.52 74.5790 62.93 82.9012 100 .11 77.4330 181. 07 0.0000 63.29 81.7507 102.03 91.1055 181. 52 62.5935 63.58 81. 7779 103.18 86.2669 184.41 71.4130 64.28 86.5877 103.37 86.2813 143.76 71. 4697 66.73 111.8036 105.21 61.7268 193.51 77.9338 67.24 108.2972 105.31 61. 7321 197.03 78.9725 125.81 98.8247 106.12 69.1874 198.01 63.2146 67.75 84.5427 106.47 86.5099 201.83 60.7147 69.67 77.9592 109.28 84.2374 203.43 51.7874 70.83 92.3938 111. 00 94.2822 205.31 46.2884 72.81 85.0064 111.76 0.0000 210.85 55.7204 72. 87 85. 0118 114. 06 104.4681 215.65 37.2465 74.66 85.1716 116. 30 0.0000 222 .11 67.6373 74.82 85.1857 116.74 93.4776 227.09 62.4648 74.97 85.1990 119.76 62.4683 227.38 56.2273 77 .11 85.3872 121.12 78.3773 228.16 0.0000 78.74 96.3708 121. 22 79.2174 228.18 57.1439 79.69 94.8553 121.78 85.0918 116.74 57.1439 80.12 94.8961 122.06 85 .1105 235.69 61.8532 80.19 0.0000 122.92 71. 8080 235. 96 57.8278 80.57 109.4209 123.07 71.8163 238.63 47.5838 81. 00 107.8581 265.00 71. 8504 238.98 0.0000 81. 07 107.8656 125.81 82.8474 240.99 47.6420 81. 75 106.3275 127.23 90.4771 242.00 47.6668 83.79 106.5403 127.91 82.1422 244.70 45.9313 84.00 106.5625 129.30 89.7806 252.40 0.0000 85.43 111.5607 131. 20 110.0755 252.80 56.9720 86.55 125.0338 133.02 81.6168 254.15 0.0000 86. 79 125.0621 133. 52 79.1222 256.23 48.0108 86.94 125.0802 136.00 88.5425 260.90 0.0000 Page 3326 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.8429 355.39 0.0000 584.27 14.3287 264.80 40.9360 356.01 35.5156 595.83 0.0000 265.00 40.9396 364.49 0.0000 427.87 22.6230 268.22 58.3164 366.42 0.0000 602.52 0.0000 269.46 43.7637 372.51 26.6926 604. 72 32.4305 270.03 45.5994 375.05 28.6279 607.14 21.6349 271. 23 52.9259 377.52 20.0588 609.32 26.8030 273.65 0.0000 356.01 24.4167 610.33 26.8104 276.40 49.3978 388.16 27.8135 614.28 20 .1300 277.37 48.5046 388.63 0.0000 618.01 20.6681 277.60 45.7642 391. 69 25.9305 620.36 14.4774 278.00 44.8578 264.66 28.9087 621. 93 21.7255 279.20 53.1265 401. 81 30.8496 630.19 0.0000 279.54 54.9670 402.40 26.0349 631. 2 9 12.4468 279.70 57. 7205 404.85 27.0236 633.25 3 .1134 280.46 43.0766 410.95 31. 9211 634.78 0.0000 283.69 37.6342 413. 71 28.0802 635.95 17.6558 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 49.6066 423. 72 0.0000 645.85 14.5793 285.90 0.0000 427.09 21. 4056 657.76 17.7609 287.50 48.7354 427.87 20.4386 657.90 0.0000 290.67 42.8208 433.94 24.3841 661. 66 16.7337 293.27 0.0000 439.40 20.5223 664.57 0.0000 351.93 33.2205 453.88 18.6614 666.33 0.0000' 295. 96 33.2314 463.37 20.6928 666.50 0.0000 879.38 52.6791 468.07 23.6865 667.71 0.0000 299.98 39.9507 473.00 0.0000 677.62 11. 5532 300.09 44.3916 475.06 24.7314 685.70 0.0000 300.13 44.3926 476.78 22.7660 695.00 0.0000 301.36 50.8945 477.60 23.7622 696.49 13. 7210 302.85 54.6319 482.18 13.8826 696. 51 13.7210 256.23 36.1396 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 15.8356 306.78 46.3796 497.08 26.9044 697.49 14.7804 308.46 31.5616 505.52 13.4887 702.65 17.9712 311. 90 39.0469 507.63 0.0000 706.68 9.5240 316.51 37.2624 511. 00 17.0157 711. 68 11. 6557 319.41 0.0000 514.00 17.0318 720.70 0.0000 320.08 0.0000 514.00 17.0318 721. 93 0.0000 321.04 35.4688 520.40 15.0586 722.78 23.9081 323.87 '37 .3812 520.69 0.0000 722. 91 23.9090 325.23 39.2725 522.65 0.0000 723. 31 15.9406 328.76 0.0000 527.90 0.0000 724 .19 10.6295 333.37 42.7862 528.26 18 .1150 727. 33 10.6380 333.97 46.4576 529.59 14.0951 733.00 6.3918 334.37 38.0174 529.87 0.0000 735.93 11. 7269 338.28 36.6688 531. 02 0.0000 333.97 11.7314 338.32 36.6696 537.26 0.0000 739.50 0.0000 311. 90 36.7021 546.56 0.0000 747.24 11.7600 340.48 36.7021 552.55 17.2366 748.06 12.8315 340.55 0.0000 563.25 10.6803 752.31 14.9855 344.28 41. 4729 569.33 25.4751 753.82 0.0000 345.93 27.3533 946.00 18.3428 756.73 16.0736 351. 06 37.8076 569.70 18.3442 756.80 16.0736 351. 93 37.8206 583.19 14.3241 884.68 12.8813 Page 3327 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.7199 1274.44 7.9100 1620.50 3.7656 766.42 22.5560 1001.03 10.1796 1621.92 4.7079 766.84 21.4844 1002.74 20.3665 1678.03 0.0000 772.60 0.0000 1004.73 18 .1107 1690.97 1.9015 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.8413 778.90 8.6188 1028.54 0.0000 1063.66 5.7664 783.70 0.0000 1037.84 7.9758 1771. 35 2.8835 785.37 14.0273 1038.76 0.0000 1791.20 0.0000 792.07 17.2917 631.29 5.7068 1808.65 0.0000 794.95 11. 8961 1048.07 0.0000 1810.72 0.0000 795.86 10.8171 1049.04 9.1348 1836.06 4.8471 810.06 16.2793 1050.41 2.2843 810.29 16.2805 1063.66 22.3295 344.28 18.4519 1077.00 0.0000 810.76 16.2823 1077.34 11. 4811 815.77 0.0000 1085.87 9.1999 1048.07 0.0000 1093.63 6.9102 832.01 16.3623 1099.45 12.6829 834.85 12.0066 1112. 07 10.4011 835. 71 14.1928 1112. 84 12. 7143 836.80 0.0000 1115. 54 10.4077 846.75 0.0000 1120.29 10.4172 846.77 10.9448 1120. 55 8.6816 856.80 0.0000 1221.41 13.8926 860.56 9.8811 1129. 67 10.4355 871.09 8.8037 1131. 51 0.0000 873.19 11. 0099 1147.95 0.0000 875.33 0.0000 1173.23 18.4070 879.38 14.3325 1177.95 16.0424 880.51 14.3357 1189.05 20.2177 883.24 15.4481 1204.77 9. 6962 884.68 7.7263 1221.41 11.4932 889.28 12.1539 1231. 02 17.7112 894.76 12.1682 1235.36 0.0000 898.04 6.6418 1238.28 21.2798 900.72 4.9843 1260.41 0.0000 903.28 14.6287 1271.87 11.5932 911.20 15.9861 1274.44 8.0294 912.08 13. 3242 1274.54 8.0299 923.98 0.0000 1291.59 7.1582 926.50 8.9102 1298.22 0.0000 929 .11 12.2582 1312 .11 0.0000 937.49 15.6292 1332. 49 8.1079 944.13 0.0000 1362. 66 0.0000 946.00 13.4204 1365.19 4.5285 949.00 8.9525 1368.63 0.0000 667.71 0.0000 1384.29 4.5422 962. 31 15.1496 1408.01 6.3831 964.08 15.1551 1457.56 0.0000 966 .17 0.0000 1460.82 4. 5972 911.20 6.7422 1489.16 7. 3872 968.97 6.7422 1505.03 7.4048 983.53 0.0000 1584.12 7.4922 984.45 0.0000 1596.21 0.0000 Page 3328 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:51:34.03 ******************************************************************************** *
  • GEL Laboratoiies LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621350.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM31.CNF;306 Background date : Z-OCT-2016 11:01:52. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 08:50:58. Sample ID G1203621350 Sample quantity : 1.75975E+02 GRAM Detector name : GAM31 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.18 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.22* 1 130 0.79 92.08 89 7 3.17E-04***** 2 0 54.71 24 187 1. 30 109.05 103 8 6.75E-03100.3 3 0 62.87* 29 119 1. 89 125.37 122 7 8.02E-03 73.9 4 0 187.22* 18 47 6.25 373.88 366 18 4.98E-03100.5 5 0 296.25* 10 24 1. 89 591. 79 586 9 2.85E-03 97.3 6 0 338.11* 17 8 0.93 675.45 671 8 4. 71E-03 42.2 7 0 397 .11 11 8 3.32 793."37 788 9 2.96E-03 58.8 8 0 408.80 8 22 1.17 816.72 813 11 2.31E-03123.8 9 0 416.83 23 11 5.28 832.78 825 15 6.38E-03 38.0 10 0 437.75 9 6 1. 73 874.59 871 8 2.40E-03 60.2 11 0 483.85 12 8 1. 86 966.73 960 10 3.42E-03 50.5 12 0 569.56 14 5 3.28 1138.04 1133 9 3.75E-03 39.3 13 0 609.71* 2 8 1. 53 1218.28 1214 8 5.07E-04344.1 14 0 702.13* 14 15 1. 58 1403.00 1396 15 3.84E-03 68.2 15 0 873.87 8 1 0.69 1746.26 1743 6 2.lOE-03 44.4 16 0 911. 55* 6 2 0.71 1821. 58 1817 8 L59E-03 75.0 17 0 1121.09 12 2 1. 86 2240.41 2236 9 3.33E-03 36.4 Flag: "*" = Peak area was modified by background subtraction Page 3329 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:51:35 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621350.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621350 SOLID GAMMA31 0 01:00:00.00 1. 50 keV No Linear 75.00 Acquisition date : Sample quantity Samp.le geometry Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 08:50:58 175.98 GRAM CAN 0 01:00:06.18 10.00 0.00 % Peak Energy 0.2% No interference correction performed Page 3330 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : Gl203621350 Acquisition date 3-0CT-2016 08:50:58 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error AS-73 53.44 36 10.30* 5.699E+OO 2.612E-01 3.141E-01 200.62 PB-210 46.54 2 4.25* 5.454E+OO 3.158E-02 3.164E-02 3576.45 BI-214 609.32 2 45.49* 1.433E+OO 1.328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------RN-222 609.32 2 45.49* 1.433E+OO 1.328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72. 77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------RA-226 609.32 2 45.49* 1.433E+OO 1.328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72. 77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------TH-230 609.32 2 45.49* 1.433E+OO l.328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------U-234 609.32 2 45.49* 1.433E+OO 1. 328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72. 77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------Flag: "*" = Keyline Page 3331 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:51:36.77 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621350.CNF;l *
  • Acquisition date 3-0CT-2016 08:50:58 Sensitivity : 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.18 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl * *Sample ID Gl203621350 Sample Quantity 1.7598E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;? * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) AS-73 3 .141E-01 6.176E-01 PB-210 3.164E-02 1.109E+OO BI-214 1.328E-02 8.955E-02 RN-222 1. 328E-02 8.955E-02 RA-226 l.328E-02 8.955E-02 TH-230 l.328E-02 8.955E-02 U-234 l.328E-02 8.955E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-2-6 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 Page 3332 of 5809 Key-Line Activity (pCi/GRAM 3.192E-01 -3.592E-03 O.OOOE+OO 1.400E-03 -3.065E-01 -5.700E-03 3.865E-02 2.452E-01 8.034E-03 2.805E-02 O.OOOE+OO -7.439E-03 l.836E-02 l.914E-02 -1.436E-02 -1.288E-02 4.670E-01 -2.636E-02 4.532E-03 -1.491E+Ol 1. 672E-01 4.340E-02 -1.712E+Ol K.L. Cnt Uncert ( 1. 96-sigma) 3.357E-01 3.315E-02 6.647E+08 2.822E-02 4.013E-01 3.058E-02 6.426E-02 3.834E-01 3.087E-02 3. 965E-02 l.398E+41 1. 511E-02 3.932E-02 6.225E-02 3.492E-02 8. 718E-02 8.860E-01 l .119E-01 3.091E-02 4.397E+Ol 2.487E-01 5.757E-02 9.643E+OO MDA 4.265E-01 8.948E-01 1.264E-01 1. 264E-01 l.264E-01 l.264E-01 1.264E-01 MDA (pCi/GRAM 7.599E-01 7.002E-02 O.OOOE+OO 7.048E-02 8.243E-01 6.534E-02 1.635E-01 8.556E-01 6.749E-02 9. 091E-02 O.OOOE+OO 2.905E-02 8.673E-02 l.525E-01 6.679E-02 l.630E-01 2.219E+OO 2.179E-01 6.271E-02 8.724E+Ol 6.368E-01 l.378E-01 l.474E+Ol NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

SR-85 -9.700E-02 5.458E-02 8.341E-02 NOT IDENT. RB-86 3.865E-01 7.697E-01 1.862E+OO NOT IDENT. Y-88 1.552E-03 3.319E-02 8.264E-02 NOT IDENT. Y-91 -4.665E+OO 1. 22 9E+Ol 2.485E+Ol NOT IDENT. NB-94 5.045E-02 6.744E-02 7.033E-02 FAIL ABUN NB-95 4.156E-02 3.015E-02 8.291E-02 NOT IDENT. NB-95M 1.991E-02 9.302E-02 1.864E-01 NOT IDENT. ZR-95 4.506E-02 6.228E-02 1.485E-01 NOT IDENT. NB-97 O.OOOE+OO 9.852E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 9.093E+08 0. OOOE-:t-00 SHORT HLIF M0-99 -3.081E+Ol 4.615E+Ol 7. 911E+Ol NOT IDENT. TC-99M O.OOOE+OO 6.015E+23 O.OOOE+OO SHORT HLIF RH-101 3.524E-03 1.662E-02 3.538E-02 NOT IDENT. RH-102 2.133E-02 3.833E-02 9.209E-02 NOT IDENT. RU-103 2.408E-02 3.125E-02 7.666E-02 FAIL ABUN RH-106 5.307E-02 2.699E-01 5.795E-01 NOT IDENT. RU-106 5.307E-02 2.699E-01 5.795E-01 NOT IDENT. AG-108M 8.855E-03 2.375E-02 4.941E-02 NOT IDENT. CD-109 -l.024E-01 3.376E-01 6.878E-01 NOT IDENT. AG-llOM 1.994E-02 3.936E-02 9.531E-02 NOT IDENT. SN-113 -9.468E-03 3.346E-02 6.481E-02 NOT IDENT. CD-115 -3.537E+Ol 4.899E+Ol 8. 714E+Ol NOT IDENT. SN-117M l.612E-02 4.783E-02 1.003E-01 NOT IDENT. TE-123M 1.619E-02 l.764E-02 3.994E-02 NOT IDENT. SB-124 5.479E-02 8. 481E-02 2.295E-01 NOT IDENT. SB-125 -l.106E-02 6. 651E-02 1.377E-01 NOT IDENT. TE-125M 2.479E-02 5.160E+OO 1. 079E+Ol NOT IDENT. I-126 9.312E-02 2.072E-01 4.891E-01 NOT IDENT. SB-126 -8.453E-02 l.438E-01 2.550E-01 NOT IDENT. SN-126 -2.219E-03 3.158E-02 6.630E-02 FAIL ABUN SB-127 -1. 671E+OO 3. 741E+OO 6.894E+OO NOT IDENT. I-131 2.471E-02 1. 526E-01 3.312E-01 NOT IDENT. I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 -2.105E+OO 1.983E+OO 3.185E+OO NOT IDENT. BA-133 7.285E-03 2.942E-02 6.533E-02 NOT IDENT. I-133 O.OOOE+OO 5.019E+05 O.OOOE+OO SHORT HLIF CS-134 l.823E-02 3.484E-02 7.903E-02 FAIL ABUN CS-135 -1.955E-02 1. 207E-01 2.270E-01 NOT IDENT. I-135 O.OOOE+OO 4.139E+22 O.OOOE+OO SHORT HLIF CS-136 2.886E-03' 1. 249E-01 2.698E-01 NOT IDENT. BA-137M 2.648E-02 2. 396E-02 6.339E-02 NOT IDENT. CS-137 2.797E-02 2.531E-02 6.697E-02 NOT IDENT. CE-139 -:2.293E-02 1. 8 62E-02 3.021E-02 NOT IDENT. BA-140 3.489E-02 3.009E-01 6.447E-01 NOT IDENT. LA-140 -3.715E-03 9 .130E-02 2.099E-01 NOT IDENT. CE-141 -2.091E-02 4.305E-02 7.643E-02 NOT IDENT. CE-143 O.OOOE+OO l.850E+03 0.000E+OO SHORT HLIF CE-144 4.573E-02 1.151E-01 2.477E-01 NOT IDENT. PM-144 6. 831E-03 2.977E-02 5.888E-02 NOT IDENT. PR-144 5 .181E-01 2.237E+OO 4.425E+OO NOT IDENT. PM-146 7.788E-03 3.754E-02 8.018E-02 NOT IDENT. ND-147 1.559E-01 5.305E-01 1.235E+OO NOT IDENT. PM-147 2.632E+02 3.763E+02 8.582E+02 NOT IDENT. PM-149 2.685E+02 3.623E+02 8.871E+02 NOT IDENT. EU-150 -1.003E-03 2.085E-02 3.981E-02 NOT IDENT. EU-152 7.826E-02 6.709E-02 1.670E-01 NOT IDENT. GD-153 -5.142E-03 4.189E-02 8.624E-02 NOT IDENT. EU-154 -7.019E-03 9.461E-02 2. 013E-01 FAIL ABUN EU-155 1.538E-02 4.702E-02 l.039E-01 NOT IDENT. TB-160 -6.873E-03 1.069E-01 2.338E-01 FAIL ABUN H0-166M 8.549E-03 5.779E-02 1.114E-01 NOT IDENT. TM-171 6.925E-01 4.164E+OO 8.585E+OO NOT IDENT. HF-172 -3.697E-02 l .130E-01 2.215E-01 FAIL ABUN LU-172 -l.494E-02 4.600E-02 9.335E-02 FAIL ABUN LU-176 9.537E-04 l.815E-02 3.933E-02 NOT IDENT. HF-181 1.492E-02 3.663E-02 8.333E-02 NOT IDENT. TA-182 -4.265E-02 l.358E-01 2.710E-01 FAIL ABUN RE-183 -2.075E-02 7.051E-02 1.432E-01 NOT IDENT. RE-184 1. 816E-02 l.288E-01 2.823E-01 NOT IDENT. W-188 -1.002E+OO 4.692E+OO 9.480E+OO FAIL ABUN IR-192 -2.401E-02 2.859E-02 5.361E-02 FAIL ABUN HG-203 -1.315E-02 3.176E-02 5.701E-02 NOT IDENT. BI-207 1.611E-02 2.576E-02 7.357E-02 FAIL ABUN TL-208 1. 739E-02 3.273E-02 7.812E-02 NOT IDENT. BI-211 -1.654E-01 1.816E-01 3.525E-01 NOT IDENT. PB-211 -2.lOlE-01 5.907E-01 1. 035E+OO NOT IDENT. BI-212 -l.201E-02 3.035E-01 6.548E-01 NOT IDENT. PB-212 -2.936E-02 4.572E-02 8.696E-02 NOT IDENT. Page 3333 of 5809 PB-214 5.843E-03 6.678E-02 1.460E-01 FAIL ABUN RN-219 1.143E-01 2.486E-01 5.883E-01 NOT IDENT. RA-223 -l.072E-01 4.903E-01 1.008E+OO FAIL ABUN RA-224 -9.417E-02 4.363E-01 8.415E-01 NOT IDENT. AC-227 -2. llOE-03 1.661E-01 3.281E-01 NOT IDENT. TH-227 -2. llOE-03 1.661E-01 3.281E-01 NOT IDENT. AC-228 9.592E-02 l.410E-01 3. OllE-01 FAIL ABUN RA-228 9.592E-02 1.410E-01 3. OllE-01 FAIL ABUN TH-228 -2.936E-02 4.572E-02 8. 696E-02 NOT IDENT. TH-229 -1.597E-01 3.437E-01 5.754E-01 NOT IDENT. PA-231 -9.458E-02 2.B99E-01 6.000E-01 NOT IDENT. TH-231 -1. 072E-01 4.903E-01 1.008E+OO FAIL ABUN TH-232 9.592E-02 1.410E-01 3. OllE-01 FAIL ABUN PA-233 -6 .134E-03 4.837E-02 l.012E-01 NOT IDENT. PA-234 -1.013E-01 1.891E-01 3.699E-01 FAIL ABUN PA-234M 2.789E+OO 4.242E+OO 9.882E+OO NOT IDENT. TH-234 8.671E-01 1.256E+OO l.287E+OO FAIL ABUN U-235 2.736E-04 l.196E-01 2. 296E-01 NOT IDENT. NP-237 -6.134E-03 4.837E-02 1.012E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 091E+02 O.OOOE+OO SHORT HLIF U-238 8.671E-01 1.256E+OO 1.287E+OO FAIL ABUN NP-239 -8.259E-02 l.465E-01 2.802E-01 NOT IDENT. PU-239 -1. 068E+Ol 1. 757E+02 3.606E+02 NOT IDENT. AM-241 5.273E-02 5.486E-02 1.138E-01 NOT IDENT. AM-243 5.730E-03 2.103E-02 4.489E-02 NOT IDENT. CM-243 2. 968E-03 5. 081E-02 1. 07 5E-01 NOT IDENT. BK-247 O.OOOE+OO 5.464E-02 l.077E-01 NOT IDENT. CM-247 1.874E-03 2.444E-02 5.355E-02 NOT IDENT. CF-249 -2.265E-02 2.734E-02 4.984E-02 NOT IDENT. CF-251 -8.210E-02 7. 8 61E-02 1.312E-01 NOT IDENT. ANH-511 -9.288E-02 5.292E-02 1.075E-01 NOT IDENT. Page 3334 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:51:34.86 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error AS-73 53.44 36 10.30* 5.699E+OO 2.612E-01 3 .141E-01 200.62 PB-210 46.54 2 4.25* 5.454E+OO 3.158E-02 3.164E-02 3576.45 BI-214 609.32 2 45.49* l.433E+OO l.328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------RN-222 609.32 2 45.49* 1.433E+OO 1.328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------RA-226 609.32 2 45.49* 1.433E+OO 1. 328E-02 l.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------TH-230 609.32 2 45.49* l.433E+OO 1.328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E-01 4.009E-01 72.77 1764.49 ------15.30 5. 813E-01 ------Line Not Found ------U-234 609.32 2 45.49* 1.433E+OO l.328E-02 1.328E-02 688.26 1120.29 12 14.92 8.735E-01 4.009E..:.01 4.009E-01 72.77 1764.49 ------15.30 5.813E-01 ------Line Not Found ------Flag: "*" = Keyline Page 3335 of 5809 Summary of Nuclide Activity Sample ID : Gl203621350 Acquisition date Page : 2 3-0CT-2016 08:50:58 Total number of lines in spectrum 17 Number of unidentified lines 6 Number of lines tentatively identified by NID 11 64. 71% Nuclide Type : Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlif e Decay pCi/GRAM pCi/GRAM 2-Sigma Error %Error Flags AS-73 80.30D 1.20 2.612E-01 3 .141E-01 6.302E-01 200.62 PB-210 22.20Y 1. 00 3.158E-02 3.164E-02 113.lE-02 3576.45 BI-214 1600.00Y 1. 00 l.328E-02 l.328E-02 9.138E-02 688.26 RN-222 1600.00Y 1. 00 l.328E-02 l.328E-02 9.138E-02 688.26 RA-226 1600.00Y 1. 00 l.328E-02 l.328E-02 9 .138E-02 688.26 TH-230 7.54E+04Y 1. 00 1. 328E-02 1. 328E-02 9.138E-02 688.26 U-234 2.45E+05Y 1. 00 1.328E-02 l.328E-02 9.138E-02 688.26 ------------------Total Activity 3.591E-01 4.122E-01 Grand Total Activity 3.591E-01 4.122E-01 Flags: "K" Key line not found "M" Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit Page 3336 of 5809 Unidentified Energy Lines Page : 3 Sample ID : Gl203621350 Acquisition date : 3-0CT-2016 08:50:58 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 62.87 42 174 1. 89 125.37 122 7 8.02E-03 **** 5.59E+OO T 0 187.22 23 61 6.25 373.88 366 18 4.98E-03 **** 3.89E+OO 0 296.25 13 29 1. 89 591. 79 586 9 2.85E-03 **** 2.66E+OO T 0 338 .11 20. 9 0.93 675.45 671 8 4. 71E-03 84.5 2.37E+OO T 0 397 .11 13 10 3.32 793.37 788 9 2. 96E-03 **** 2.06E+OO 0 408.80 10 25 1.17 816.72 813 11 2.31E-03 **** 2.0lE+OO 0 416.83 27 13 5.28 832.78 825 15 6.38E-03 75.9 1.97E+OO 0 437.75 10 7 1. 73 874.59 871 8 2.40E-03 **** 1.89E+OO 0 483.85 14 9 1. 86 966.73 960 10 3.42E-03 **** 1. 74E+OO 0 569.56 15 5 3.28 1138.04 1133 9 3.75E-03 78.6 1.52E+OO T 0 702.13 15 16 1. 58 1403.00 1396 15 3.84E-03 **** l.28E+OO T 0 873.87 8 2 0.69 1746.26 1743 6 2.lOE-03 88.8 1. 07E+OO T 0 911. 55 6 2 0.71 1821. 58 1817 8 1.59E-03 **** 1. 03E+OO T Flags: "T" = Tentatively associated Page 3337of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:51:48.60 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621350.CNF;l *
  • Acquisition date 3-0CT-2016 08:50:58 Sensitivity 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.18 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621350 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : 1.7598E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide AS-73 PB-210 BI-214 RN-222 RA-226 TH-230 U-234 Le (pCi/GRAM 1.999E-01 4.194E-01 5.396E-02 5.396E-02 5. 396E-02 5. 396E-02 5. 396E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 Page 3338 of 5809 Le (pCi/GRAM 3.362E-01 2.738E-02 O.OOOE+OO 2.497E-02 3. 331E-01 2.593E-02 6.632E-02 3. 851E-01 2. 811E-02 3.887E-02 O.OOOE+OO 1.295E-02 3.685E-02 5.980E-02 2.554E-02 6.733E-02 8.944E-01 9.282E-02 2.729E-02 3.931E+Ol 2.579E-01 5.910E-02 6.523E+00 3.690E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.* NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 PB-214 Page 3339 of 5809 7.630E-01 2.928E-02 8.869E+OO 3.046E-02 3.510E-02 8.343E-02 6.271E-02 O.OOOE+OO O.OOOE+OO 3.065E+Ol O.OOOE+OO 1.576E-02 3.823E-02 3.259E-02 2.449E-01 2.449E-01 2. ll 7E-02 3.106E-01 3.945E-02 2. 725E-02 3.294E+Ol 4.516E-02 1. 802E-02 8.890E-02 5.807E-02 4.804E+OO 2.014E-01 9. 785E...:.02 2.993E-02 2.857E+OO 1. 441E-01 O.OOOE+OO 1. 374E+OO 2.827E-02 O.OOOE+OO 3.333E-02 1.00lE-01 O.OOOE+OO 1.102E-01 2.670E-02 2.820E-02 1.303E-02 2.724E-01 7.436E-02 3. 371E-02 O.OOOE+OO 1.113E-01 2.455E-02 l.845E+OO 3.494E-02 5.062E-01 3.837E+02 3.842E+02 l.722E-02 7.355E-02 3.869E-02 7.908E-02 4.609E-02 9.409E-02 4.690E-02 4.045E+OO 9.909E-02 3.591E-02 1. 711E-02 3.551E-02 1.049E-01 6.749E-02 l.184E-01 4.036E+OO 2.317E-02 2.478E-02 2.807E-02 3.428E-02 1.555E-01 4.373E-01 2.549E-01 3.903E-02 6.544E-02 NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN RN-219 RA-223 RA-224 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3340 of 5809 2.486E-01 4. 411E-01 3.730E-01 1.424E-01 l.424E-01 1.283E-01 1.283E-01 3.903E-02 2.502E-01 2.559E-01 4. 411E-01 1.283E-01 4.429E-02 l.356E-01 4.205E+OO 6.122E-01 1.023E-01 4.429E-02 O.OOOE+OO 6.122E-01 l.243E-01 1. 596E+02 5.373E-02 2.069E-02 4.788E-02 4.679E-02 2.260E-02 2.049E-02 5.659E-02 5.009E-02 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:51:53.99 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621350.CNF;l *
  • Acquisition date 3-0CT-2016 08:50:58 Sensitivity : 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.18 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621350 Analyst initials: MXRl * *Batch Number 1596247 Sample Quantity : 1.7598E+02 GRAM *
  • Quantity Err(%) : 1.1365E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM AS-73 PB-210 BI-214 RN-222 RA-226 TH-230 U-234 3.141E-01 3.164E-02 1. 328E-02 1.328E-02 1.328E-02 1.328E-02 1.328E-02 Act Error ( 1. 96-sigma) 6.210E-01 1.109E+OO 8.955E-02 8.955E-02 8.955E-02 8.955E-02 8.955E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 . FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 Page 3341of5809 Key-Line Activity (pCi/GRAM 3.192E-01 -3.592E-03 2.666E+08 1.400E-03 -3.065E-01 -5.700E-03 3.865E-02 2.452E-01 8.034E-03 2.805E-02 1.000E+41 -7.439E-03 1.836E-02 l.914E-02 -l.436E-02 -1. 288E-02 4.670E-01 -2.636E-02 4.532E-03 -1. 491E+Ol 1. 672E-01 4.340E-02 -1.712E+Ol K.L Act error ( 1. 96-sigma) 3.360E-01 3.315E-02 6.648E+08 2.822E-02 4.017E-01 3.058E-02 6.427E-02 3.835E-01 3.087E-02 3. 967E-02 1.399E+41 1.512E-02 3.933E-02 6.227E-02 3.492E-02 8.718E-02 8.862E-01 1.119E-01 3. 091E-02 4.493E+Ol 2.488E-01 5.788E-02 9.669E+OO TPU (1. 96-sigma) 6.210E-01 1.109E+OO 8.955E-02 8.955E-02 8.955E-02 8.955E-02 8.955E-02 TPU ( 1. 96-sigma) 3.655E-01 3.319E-02 6.756E+08 2.822E-02 4.248E-01 3.068E-02 6.659E-02 3. 991E-01 3.108E-02 4.164E-02 O.OOOE+OO 1.548E-02 4.019E-02 6.286E-02 3.551E-02 8.737E-02 9.108E-01 l.125E-01 3.098E-02 4.543E+Ol 2.600E-01 6.109E-02 l.237E+Ol NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT . NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

SR-85 -9.700E-02 5.472E-02 7.005E-02 NOT IDENT. RB-86 3.865E-01 7.699E-01 7.893E-01 NOT IDENT. Y-88 1.552E-03 3.319E-02 3.320E-02 NOT IDENT. Y-91 -4.665E+OO l.229E+Ol 1. 247E+Ol NOT IDENT. NB-94 5.045E-02 6.748E-02 7.121E-02 FAIL ABUN NB-95 4.156E-02 3.020E-02 3.554E-02 NOT IDENT. NB-95M 1.991E-02 9.304E-02 9.347E-02 NOT IDENT. ZR-95 4.506E-02 6. 231E-02 6.554E-02 NOT IDENT. NB-97 -l.OOOE+41 9.861E+40 O.OOOE+OO SHORT HLIF ZR-97 -2. l 72E+08 9.093E+08 9.146E+08 SHORT HLIF M0-99 -3.081E+Ol 4.618E+Ol 4.822E+Ol NOT IDENT. TC-99M -2.273E+23 6.019E+23 O.OOOE+OO SHORT HLIF RH-101 3.524E-03 l.663E-02 1.671E-02 NOT IDENT. RH-102 2.133E-02 3.837E-02 3.956E-02 NOT IDENT. RU-103 2.408E-02 3.127E-02 3.310E-02 FAIL ABUN RH-106 5.307E-02 2.699E-01 2.710E-01 NOT IDENT. RU-106 5.307E-02 2.699E-01 2.710E-01 NOT IDENT. AG-108M 8.855E-03 2.375E-02 2.408E-02 NOT IDENT. CD-109 -1.024E-01 3.377E-01 3.408E-01 NOT IDENT. AG-llOM 1.994E-02 3.937E-02 4.038E-02 NOT IDENT. SN-113 -9.468E-03 3.347E-02 3.374E-02 NOT IDENT. CD-115 -3.537E+Ol 4.904E+Ol 5.156E+Ol NOT IDENT. SN-117M 1.612E-02 4.784E-02 4.839E-02 NOT IDENT. TE-123M 1.619E-02 1. 765E-02 l.910E-02 NOT IDENT. SB-124 5.479E-02 8.486E-02 8.838E-02 NOT IDENT. SB-125 -1.106E-02 6.651E-02 6.670E-02 NOT IDENT. TE-125M 2.479E-02 5.160E+OO 5.160E+OO NOT IDENT. I-126 . 9.312E-02 2.073E-01 2 .115E-01 NOT IDENT. SB-126 -8.453E-02 l.440E-01 1.490E-01 NOT I DENT .. SN-126 -2.219E-03 3.158E-02 3.159E-02 FAIL ABUN SB-127 -1. 671E+OO 3.745E+OO 3.820E+OO NOT IDENT. I-131 2.471E-02 l.526E-01 1.530E-01 NOT IDENT. I-132 1.000E+41 3.056E+41 O.OOOE+OO SHORT HLIF TE-132 -2.105E+OO 1.991E+OO 2.206E+OO NOT IDENT. BA-133 7.285E-03 2.942E-02 2. 960E-02 NOT IDENT. I-133 1. 472E+05 5.024E+05 5.068E+05 SHORT HLIF CS-134 1.823E-02 3.485E-02 3.580E-02 FAIL ABUN CS-135 -1.955E-02 1.207E-01 l.210E-01 NOT IDENT. I-135 9.213E+21 4.163E+22 O.OOOE+OO SHORT HLIF CS-136 2.886E-03 1.249E-01 l.249E-01 NOT IDENT. BA-137M 2.648E-02 2.399E-02 2.679E-02 NOT IDENT. CS-137 2.797E-02 2.534E-02 2. 831E-02 NOT IDENT. CE-139 -2.293E-02 l.918E-02 2.179E-02 NOT IDENT. BA-140 3.489E-02 3.009E-01 3.013E-01 NOT IDENT. LA-140 -3.715E-03 9.130E-02 9.132E-02 NOT IDENT. CE-141 -2.091E-02 4.306E-02 4.408E-02 NOT IDENT. CE-143 9.909E+02 1. 851E+03 1.904E+03 SHORT HLIF CE-144 4.573E-02 1.151E-01 1.170E-01 NOT IDENT. PM-144 6. 831E-03 2.978E-02 2.993E-02 NOT IDENT. PR-144 5 .181E-01 2.237E+00 2.249E+OO NOT IDENT. PM-146 7.788E-03 3.754E-02 3.770E-02 NOT IDENT. ND-147 l.559E-01 5.306E-01 5.352E-01 NOT IDENT. PM-147 2.632E+02 3.765E+02 3.947E+02 NOT IDENT. PM-149 2.685E+02 3.641E+02 3.837E+02 NOT IDENT. EU-150 -1.003E-03 2.085E-02 2.086E-02 NOT IDENT. EU-152 7.826E-02 6. 723E-02 7.593E-02 NOT IDENT. GD-153 -5.142E-03 4.189E-02 4 .196E-02 NOT IDENT. EU-154 -7.019E-03 9.461E-02 9.466E-02 FAIL ABUN EU-155 1.538E-02 4.703E-02 4.754E-02 NOT IDENT. TB-160 -6.873E-03 l.069E-01 1.070E-01 FAIL ABUN H0-166M 8.549E-03 5.779E-02 5.792E-02 NOT IDENT. TM-171 6.925E-01 4.165E+OO 4.176E+OO NOT IDENT. HF-172 -3.697E-02 1.132E-01 l.144E-01 FAIL ABUN LU-172 -1. 494E-02 4.602E-02 4.651E-02 FAIL ABUN LU-176 9.537E-04 l.815E-02 l.815E-02 NOT IDENT. HF-181 l.492E-02 3.663E-02 3.725E-02 NOT IDENT. TA-182 -4.265E-02 l.358E-01 1. 371E-01 FAIL ABUN RE-183 -2.075E-02 7.054E-02 7 .116E-02 NOT IDENT. RE-184 l.816E-02 1.288E-01 1.290E-01 NOT IDENT. W-188 -1.002E+OO 4.693E+OO 4.715E+OO FAIL ABUN IR-192 -2. 401E-02 2.861E-02 3.059E-02 FAIL ABUN HG-203 -1.315E-02 3.176E-02 3.231E-02 NOT IDENT. BI-207 l.611E-02 2.577E-02 2.677E-02 FAIL ABUN TL-208 1. 739E-02 3.274E-02 3.366E-02 NOT IDENT. BI-211 -1.654E-01 1.817E-01 1. 964E-01 NOT IDENT. PB-211 -2.lOlE-01 5.908E-01 5.983E-01 NOT IDENT. BI-212 -1.201E-02 3.035E-01 3.036E-01 NOT IDENT. PB-212 -2.936E-02 4.574E-02 4.762E-02 NOT IDENT. Page 3342 of 5809 PB-214 5.843E-03 6.678E-02 6.683E-02 FAIL ABUN RN-219 l.143E-01 2.490E-01 2.542E-01 NOT IDENT. RA-223 -1. 072E-01 4.904E-01 4.928E-01 FAIL ABUN RA-224 -9.417E-02 4.363E-01 4.384E-01 NOT IDENT. AC-227 -2. llOE-03 1. 661E-01 l.661E-01 NOT IDENT. TH-227 -2. llOE-03 1. 661E-01 1.661E-01 NOT IDENT. AC-228 9.592E-02 1.410E-01 1.475E-01 FAIL ABUN RA-228 9.592E-02 l.410E-01 l.475E-01 FAIL ABUN TH-228 -2.936E-02 4.574E-02 4.762E-02 NOT IDENT. TH-229 . -1. 597E-Ol 3.438E-01 3. 512E-01. NOT IDENT. PA-231 -9.458E-02 2.906E-01 2.937E-01 NOT IDENT. TH-231 -1. 072E-01 4.904E-01 4.928E-01 FAIL ABUN TH-232 9.592E-02 l.410E-01 1.475E-01 FAIL ABUN PA-233 -6.134E-03 4.837E-02 4.845E-02 NOT IDENT. PA-234 -1.013E-01 2.218E-01 2.264E-01 FAIL ABUN PA-234M 2.789E+OO 4.244E+OO 4.426E+OO NOT IDENT. TH-234 8.671E-01 1.270E+OO l.329E+OO FAIL ABUN U-235 2.736E-04 l .196E-01 l .196E-01 NOT IDENT. NP-237 -6.134E-03 4.837E-02 4.845E-02 NOT IDENT. NP-238 1. 300E+02 l.092E+02 1.239E+02 SHORT HLIF U-238 8.671E-01 1.270E+OO 1.329E+OO FAIL ABUN NP-239 -8.259E-02 l.467E-01 l.513E-01 NOT IDENT. PU-239 -1.068E+Ol 1. 757E+02 1.758E+02 NOT IDENT. AM-241 5.273E-02 5.500E-02 5. 991E-02. NOT IDENT. AM-243 5.730E-03 2.103E-02 2 .119E-02 NOT IDENT. CM-243 2. 968E-03 5.081E-02 5.082E-02 NOT IDENT. BK-247 0.000E+OO 5.464E-02 O.OOOE+OO NOT IDENT. CM-247 l.874E-03 2.444E-02 2.445E-02 NOT IDENT. CF-249 -2.265E-02 2.740E-02 2.924E-02 NOT IDENT. CF-251 -8.210E-02 7.915E-02 8.737E-02 . NOT IDENT. ANH-511 -9.288E-02 5.305E-02 6.759E-02 NOT IDENT. Page 3343 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 61.1367 87.09 24.8846 136.47 26.2474 45.60 74.4062 87.57 23.9529 140.51 22.1901 46.54 74.6438 88.03 27.8134 143.76 19.1170 49. 72 83.2346 88.34 27.8325 144.24 23.3827 51. 35 82. 5072 88.47 26.8802 145.44 22.3612 51. 87 90.7905 89. 96 30.8201 152.43 23.6748 52.39 75.1992 90.64 69.4468 153.25 16.1616 52.97 75.3346 91.11 71.4476 154.21 26.9741 53.44 75.4442 92.59 23.2454 156.02 29.2095 54.07 75.5899 93.35 28.1334 158.56 22.8024 57. 36 0.0000 94.56 74.8887 159.00 16.2978 57.53 77.2653 94.65 74.9028 162.33 24.0175 57.98 96.9305 94.67 74.9057 162.66 22.9367 59.27 78.5486 94.87 74.9374 163.33 16.3989 59.32 78.5596 97.43 27.3942 165.86 29.6231 59.54 69.0809 98.43 26.4698 176.31 20.0327 60.96 82.5148 98 .'44 26.4702 176.60 20.0404 61.17 82.5636 99.53 21.6160 177.52 26.7532 62.93 69.4417 100 .11 26.5596 181.07 25.3855 63.29 69.5109 102.03 16.7868 181.52 22.4124 63.58 71. 0718 103.18 21.7734 184.41 20.2470 64.28 68.7940 103.37 21.7816 185.72 20.2813 66.73 67.4261 105.21 16.8917 193.51 21. 2410 67.24 65.6922 105.31 16.8949 197.03 24.0005 67.68 54.8071 106.12 22.8937 198.01 16. 0196 67.75 54.8167 106.47 20.9170 201.83 21. 8423 69.67 39.4825 109.28 22.0305 203.43 17.2771 70.83 48.8088 111.00 31.1433 205.31 25. 3969 72. 81 40.7236 111.76 32.1936 210.85 12.7819 72. 87 40.7297 114. 06 24.2477 215.65 28.0437 74.66 41.8407 116. 30 16. 2311 222 .11 23.5422 74.82 41. 8569 116.74 28.4268 227.09 7.1020 74.97 44.6638 119.76 22.4560 227.38 18.9446 77 .11 40.2197 121.12 15.3477 228.16 27.2563 78.74 48.8274 121. 22 15.3503 228.18 27.2570 79.69 27.2919 121.78 21.5116 235.69 21. 5068 80.12 31. 0876 122.06 29.7208 235. 96 21.5132 80.19 31.0926 122.92 27. 7127 238.63 20.3761 80.57 33.0064 123.07 27. 7199 238.98 17.9855 81. 00 28.3195 123.68 25.6937 240.99 16.8224 81. 07 29.2683 125.81 28.8823 242.00 28.8691 81. 75 38.7706 127.23 19.6460 244.70 26.5386 83.79 24.7013 127.91 22.7743 252.40 12.1594 84.00 24.7132 129.30 20.7523 252.80 12.1645 85.43 31. 4680 131.20 23.9406 254.15 0.0000 86.55 37.2823 133.02 24.0125 256.23 14.6483 86.79 37.3019 133.52 20.8975 260.90 18. 3966 86.94 25.8333 136.00 24.1294 264.66 13.5412 Page 3344 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 13.5429 364.49 13.4250 600.60 12.4507 265.00 14.7770 366.42 15.2375 602.52 0.0000 268.22 21.0005 372.51 14.4079 604. 72 9.9816 269.46 23.4995 375.05 9.0222 607.14 7.8079 270.03 16.0873 377.52 12.6547 609.32 11.4646 271.23 27.2563 383.85 9.9898 610.33 9.3849 273.65 18.6273 388.16 14.5768 614.28 11. 2847 276.40 22. 4116 388.63 16.4048 618.01 9.4215 277.37 11.2162 391.69 12.0570 620.36 9.4329 277.60 11. 2187 400.66 6.8951 621.93 8.3913 278.00 12.4701 401.81 6.4407 630.19 0.0000 279.20 19.9746 402.40 9.2049 631. 2 9 4.2153 279.54 17.4833 404.85 13. 8315 633.25 9.4937 279.70 17.4859 410.95 5.5564 634.78 4.2227 280.46 13.7490 413. 71 5.5671 635.95 8.4502 283.69 13.3727 414.70 5.5709 636.99 8.4544 284.31 15.8894 423. 72 8.4088 645.85 7.4301 285.41 11. 7199 427.09 12.1737 657.76 11.7434 285.90 7.5377 427.87 11. 2434 657.90 0.0000 287.50 12.5815 433.94 8.4672 661.66 2.1392 290.67 13 .1231 439.40 12.7472 664.57 0.0000 293.27 0.0000 453.88 13. 3455 666.33 4.2878 295.22 16.0498 463.37 10.5499 666.50 3.2161 295.96 16.0606 468.07 14.4293 667.71 0.0000 298.58 12.7094 473.00 12.5443 677.62 8.6214 299.98 15.2703 475.06 12.5604 685.70 11.8992 300.09 15.2717 476.78 8.7050 695.00 6.5186 300 .13 15.2725 477.60 8.1288 696.49 6.5229 301.36 14.4399 482.18 7.7638 696. 51 6.5229 302.85 19.5621 487.02 13.1405 697.00 6.5244 304.50 12.7766 492.35 9.7654 697.30 9.7881 304.85 12.7805 497.08 4.8966 697.49 9.7888 306.78 14.5094 505.52 20.6702 702.65 9. 8119 308.46 15.3856 507.63 0.0000 706.68 9.8302 311. 90 18.0037 511. 00 28.6371 711. 68 6.5681 316.51 23.2399 514.00 48.4736 720.70 7.6938 319.41 18.9837 514.00 48.4736 721. 93 0.0000 320.08 18.9944 520.40 5.9578 722.78 2.2003 321.04 23.3306 520.69 5.9587 722.91 2.2004 323.87 19.0557 522.65 0.0000 723; 31 1.1004 325.23 16.4758 527.90 7.9782 724.19 2.2017 328.76 15.6552 528.26 7.9798 727. 33 4.4095 333.37 17.0248 529.59 3.9928 733.00 5.5257 333.97 14.4127 529.87 0.0000 735.93 4.4263 334.37 18.3494 531.02 4.9951 737.46 3.3219 338.28 14.0254 537.26 9.0234 739.50 8.8662 338.32 14.0257 546.56 0.0000 747.24 8. 8 962 340.48 13 .1723 552.55 12.1348 748.06 11.1243 340.55 13.1732 563.25 9.1545 752.31 5.5723 344.28 7.0469 569.33 4.0822 753.82 8.9215 345.93 15.8767 569.50 4.0825 756.73 4.4663 351.06 15.9415 569.70 4.0830 756.80 5.5831 351. 93 9.7488 583.19 4 .1126 763.94 8.9603 355.39 0.0000 584.27 12.3447 765.81 1.1209 356.01 11. 558 6 595.83 13.4549 7 66. 42 5.6061 Page 3345 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 6.7285 1002.74 6.4367 1678.03 0.0000 772.60 0.0000 1004.73 11. 0416 1690.97 1.1062 776.52 2.2520 1021.30 0.0000 1750.46 0.0000 777.92 4.5067 1025.87 0.0000 1764.49 3.3710 778.90 4.5085 1028.54 0.0000 1770.23 5.4000 783.70 4.5176 1037.84 7.4429 1771. 35 3.6010 785.37 2.2603 1038.76 0.0000 1791.20 0.0000 792.07 9.0664 1046.59 6.5313 1808.65 1. 8144 794.95 4.5386 1048.07 6.5343 1810.72 0.0000 795.86 5.6755 1049.04 10.2715 1836.06 1.8245 801.95 7. 9653 1050.41 8.4078 810.06 2.2834 1063.66 0.9382 810.29 5.7088 1077.00 3.7690 810.45 5.7092 1077.34 2.8271 810.76 6.8521 1085.87 4.7247 815.77 3.4329 1093.63 5.6836 818.51 5. 7277 1099.45 2.8469 832.01 6.9104 1112. 07 6.6689 834.85 3.4591 1112. 84 6.6706 835. 71 3.4603 1115.54 8.9015 836.80 0.0000 1120.29 9.1693 846.75 0.0000 1120.55 5.7316 846.77 5.7922 1121.30 3.0574 856.80 6.9778 1129. 67 6.7056 860.56 3.4940 1131.51 0.0000 871.09 8. 4196 1147.95 0.0000 873.19 1. 7 555 1173.23 4.8529 875.33 0.0000 1177.95 3.8877 879.38 6.1585 1189.05 1.9503 880.51 7.9217 1204.77 3.9185 883.24 7.0486 1221.41 5.9059 884.68 4.4078 1231. 02 2.9612 889.28 6.1816 1235.36 5.9297 894.76 7.0791 1238.28 3.9563 898.04 5.3159 1260.41 0.0000 900.72 12.4162 1271. 87 4.9924 903.28 7.9893 1274.44 4.9957 911.20 8.0126 1274.54 4. 9960 1093.63 4.2749 1291.59 5.0195 923.98 0.0000 1298.22 0.0000 926.50 4.4765 1312 .11 2.0190 929.11 4.4806 1332.49 6.0901 937.49 5.3930 1362.66 0.0000 944.13 2.7029 1365 .19 5 .1190 946.00 5.4095 1368.63 0.0000 949.00 3.6101 1384.29 3.0868 954.55 0.0000 1408.01 4.1406 962.31 3. 6272 1457.56 0.0000 964.08 5.4441 1460.82 5.2448 966.17 5.4481 1489.16 3.1686 968. 97 5.4534 1505.03 6.3618 983.53 2.7405 1584.12 5.4007 984.45 0.0000 1596.21 2.1663 996.26 9.1751 1620.50 2.1782 1001.03 4.5949 1621. 92 1.0895 Page 3346 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:54:48.92 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621351.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;477 Background date : Z-OCT-2016 11:00:07. Sample date 10-DEC-2015 14:20:00 Acquisition date : 3-0CT-2016 08:53:50. Sample ID G1203621351 Sample quantity : 1.41585E+02 GRAM Detector name : GAM05 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.64 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 0 0 2 2 2 0 4 4 4 0 0 2 2 0 0 0 0 1 1 0 0 2 2 0 0 0 0 0 0 0 0 Page 3347 of 5809 Energy 32.25 39.16 41. 51 45.75* 62.89* 74.47* 76.75* 79.29 83.50* 86.89* 89.44 92.28* 185.83* 208.97 238.32* 241.49 269.53 277.75 294.91* 327.78 337.92* 339.92* 351.75* 409.97 427.28 431.57 463.04 510.54* 530.48 583.24* 609.16* 623.99 661. 90 727.79 BACKGROUND CORRECTED.SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 26 44 22 88 47 260 485 33 44 143 93 134 138 27 486 123 49 18 186 32 100 29 267 30 18 32 28 76 14 118 184 25 163 49 121 91 84 180 239 182 135 127 112 172 185 174 134 90 60 92 83 68 68 37 54 40 76 29 35 35 41 68 30 49 18 28 81 30 0.67 0.83 0.84 0.73 0.89 0.81 0.81 1. 04 1. 39 1.11 1.29 1. 30 1. 24 1.18 0.95 1. 37 0.93 1. 32 1.12 1. 08 1. 37 1. 37 1. 09 1. 86 1. 62 1. 62 1.17 2.41 1.47 1.12 1. 20 1. 74 1. 42 2.05 66.34 80.15 84.85 93.31 127.57 150. 71 155.27 160.36 168.76 175.55 180.65 186.32 373.29 419.54 478.20 484.53 540.57 557.00 591.30 656.98 677.25 681.25 704.90 821.26 855.85 864.44 927.33 1022.27 1062.12 1167.58 1219.37 1249.01 1324.79 1456.49 63 76 76 88 124 147 147 147 167 172 172 172 369 416 474 474 536 552 587 654 671 671 700 818 848 848 922 1014 1054 1161 1215 1240 1319 1448 6 7.19E-03 12 1.22E-02 12 6.03E-03 10 2.44E-02 8 1.30E-02 20 7.23E-02 20 1. 35E-01 20 9.28E-03 5 1.22E-02 20 3.97E-02 20 2.59E-02 20 3.73E-02 11 3. 83E-02 7 7.43E-03 15 l.35E-01 15 3.40E-02 10 1.35E-02 8 5.00E-03 10 5.18E-02 6 8.82E-03 15 2.77E-02 15 7.98E-03 11 7.42E-02 7 8.43E-03 26 5.02E-03 26 8.90E-03 11 7.82E-03 17 2.12E-02 11 4.02E-03 10 3.28E-02 9 5.12E-02 14 7.05E-03 14 4.52E-02 17 1. 37E-02 70.8 35. 0 1. 94E+OO 70.2 31. 9 60.7 9.7 2.46E+OO 5.9 64.1 40.1 17.2 5.47E-01 27.7 20.7 19.2 62.5 5.3 9.67E-01 16.6 37.8 82.8 11. 2 35.2 16.0 6.51E+00 56.5 8.9 34.7 68.2 2.73E+OO 36.9 48.0 30.0 77.8 14.5 8. 6 48.4 14.1 29.0 Peak Search Report (continued) Page : 2 Sample ID : G1203621351 Acquisition date 3-0CT-2016 08:53:50 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 735.20 4 21 1. 06 1471.28 1466 9 1.17E-03200.0 36 0 754.89 9 17 0.61 1510.64 1506 8 2.61E-03 83.9 37 0 786.51 25 26 6.39 1573.84 1565 17 6.97E-03 50.3 38 0 795.16 12 25 0.73 1591.13 1587 10 3.33E-03 83.1 39 0 806.54 10 21 0.50 1613.88 1608 9 2.85E-03 87.9 40 0 815.54 7 18 1. 27 1631.86 1626 10 1. 88E-03122. 7 41 0 892.23 15 6 1. 85 1785.15 1780 9 4.09E-03 40.9 42 0 911.09* 112 12 1. 47 1822.85 1815 16 3.12E-02 11. 8 43 0 920.75 7 11 1. 40 1842.14 1836 9 1.94E-03 94.4 44 2 934.55 25 4 2.10 1869.73 1863 19 6.81E-03 29.6 9.47E-01 45 2 938.82 14 0 2 .11 1878.27 1863 19 4.00E-03 28.7 46 0 964. 48 31 11 0.73 1929.55 1924 11 8.61E-03 27.4 47 3 969 .17 51 4 1. 91 1938.93 1935 16 1. 42E-02 15.3 1.40E+OO 48 3 973.23 14 1 2.35 1947.04 1935 16 4.02E-03 33.2 49 0 1035.77 4 21 1. 05 2072.04 2064 10 l.14E-03210.2 50 0 1121.15* 39 23 1. 61 2242.70 2237 13 1.07E-02 31.7 51 0 1156. 90 7 8 1.13 2314.17 2311 7 1.95E-03 74.2 52 0 1230.25 13 18 3.83 2460.78 2449 15 3.48E-03 80.4 53 0 1238.71 33 17 2.38 2477.68 2471 11 9.29E-03 29.2 54 0 1280.62 16 3 1. 95 2561.44 2558 7 4.42E-03 31.5 *55 0 1377.31 17 0 1. 29 2754.71 2748 12 4.72E-03 24.3 56 0 1460.98* 471 4 1. 90 2921. 96 2913 15 1. 31E-01 4.7 57 0 1631. 06 12 0 1. 44 32 61. 92 3257 10 3.33E-03 28.9 58 0 1764.57 42 0 2.74 3528.79 3523 12 1.17E-02 15.4 Flag: "*" = Peak area was modified by background subtraction Page 3348 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:54:51 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621351.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 10-DEC-2015 14:20:00 Gl203621351 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:53:50 141.59 GRAM Sample .type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMAS 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3349 of 5809 Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 TH-229 85.43 SN-126 86.94 SN-126 87.57 CD-109 88.03 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.64 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G1203621351 Acquisition date 3-0CT-2016 08:53:50 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 .1460. 82 10.66* 1. 244E+OO l.807E+Ol 1 .. 807E+Ol 9.45 OK CD-109 88.03 3.70* 8.913E+OO l.624E+OO 2.540E+OO 61.32 OK SN-126 64.28 9.60 9.123E+OO 3.524E-01 3.524E-01 121.47 OK 86.94 8.90 8.913E+OO 6.751E-01 6.751E-01 61. 32 OK 87.57 37.00* 8.913E+OO l.624E-01 1.624E-01 61.32 OK CS-135 2 68. 22 16.00* 5.040E+OO 3.559E-01 3.559E-01 75.52 OK BA-137M 661. 66 89.90* 2.416E+OO 4.095E-01 4.173E-01 28.18 OK CS-137 661.66 85.10* 2.416E+OO 4.326E-01 4.408E-01 28.18 OK HG-203 70.83 3.69 9.006E+00 Line Not Found Absent 72.87 6.19 8.990E+OO Line Not Found Absent 279.20 81.56* 4.917E+OO 3.160E-03 2.654E-011398.35 OK TL-208 277.37 6.60 4.923E+OO Line Not Found <<INT Reject 583.19 85.00* 2.673E+OO 2.870E-01 2.870E-01 29.00 OK 860.56 12.50 1.959E+OO Line Not Found Absent PB-210 46.54 4.25* 9.655E+OO 1.443E+OO 1.480E+OO 63. 86 OK BI-212 727.33 6.67* 2.240E+OO 1. 795E+OO 1.795E+OO 57.93 OK 785.37 1.10 2.105E+OO 5.833E+00 5.833E+OO 100.60 OK 1620.50 1. 47 1.126E+OO Line Not Found Absent PB-212 74.82 10.28 8.980E+OO 1.122E+OO 1.122E+OO 34.81 OK 77 .11 17.10 8. 967E+00 2. 051E+OO 2. 051E+OO 11. 84 OK 238.63 43.60* 5.564E+OO 1.192E+00 1.192E+OO 10.57 OK 300.09 3.30 4.613E+OO Line Not Found Absent BI-214 609.32 45.49* 2.581E+OO 8. 641E-01 8.644E-01 17.29 OK 1120.29 14.92 1. 57 5E+OO 8.566E-01 8.569E-01 63.42 OK 1764.49 15.30 1.032E+OO l.329E+OO 1.329E+OO 30.86 OK PB-214 74.82 5.80 8.977E+OO Line Not Found <<INT Reject 77 .11 9.70 8. 967E+OO 3.616E+OO 3.618E+OO 11. 84 OK 87.09 3.41 8.912E+00 Line Not Found <<INT Reject 242.00 7.25 5.497E+OO Line Not Found <<INT Reject 295.22 18.42 4.680E+OO 1.264E+OO 1.265E+OO 22.46 OK 351. 93 35.60* 4.043E+00 1.070E+OO 1.070E+OO 17.74 OK RN-222 609.32 45.49* 2.581E+OO 8.641E-01 8.644E-01 17.29 OK 1120.29 14. 92 1.575E+OO 8.566E-01 8.569E-01 63.42 OK 1764.49 15.30 1.032E+OO 1.329E+OO 1.329E+oo 30.86 OK RA-224 240.99 4.10* 5.506E+OO 9.903E-01 9.903E-01 119.26 OK RA-226 609.32 45.49* 2.581E+OO 8.641E-01 8.644E-01 17.29 OK 1120.29 14.92 1.575E+OO 8.566E-01 8.569E-01 63.42 OK 1764.49 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 OK AC-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.180E+OO 1.223E+OO l.223E+OO 31. 98 OK 794.95 4.25 2.087E+OO 7.274E-01 7.274E-01 166.25 OK 835.71 1. 61 2.005E+00 Line Not Found Absent 911.20 25.80* 1.870E+OO 1.236E+OO l.236E+00 23.55 OK 968. 97 15.80 1.778E+OO 9.614E-01 9.614E-01 30.58 OK RA-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.180E+OO 1.223E+OO 1.223E+OO 31. 98 OK 794.95 4.25 2.087E+OO 7.274E-01 7.274E-01 166.25 OK 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.870E+OO 1.236E+OO 1.236E+OO 23.55 OK Page 3350 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G1203621351 Acquisition date 3-0CT-2016 08:53:50 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 968. 97 15.80 1.778E+OO 9.614E-01 9.614E-01 30.58 OK TH-228 74.82 10.28 8.980E+OO 1.122E+OO 1.122E+OO 34.81 OK 77 .11 17.10 8. 967E+OO 2.051E+OO 2.051E+OO 11. 84 OK 238.63 43.60* 5.564E+OO 1.192E+OO 1.192E+OO 10.57 OK 300.09 3.30 4.613E+OO Line Not Found Absent TH-229 85.43 14.70 8.913E+OO 4.088E-01 4.088E-01 61.32 OK 88.47 24.00 8.895E+OO 2.808E-01 2.808E-01 55.31 OK 193.51 4.41* 6.511E+OO Line Not Found Absent 210.85 2.80 6 .116E+OO Line Not Found Absent TH-230 609.32 45.49* 2.581E+OO 8.641E-01 8. 641E-01 17.29 OK 1120.29 14.92 1. 575E+OO 8.566E-01 8.566E-01 63.42 OK 1764.49 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 OK TH-232 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.180E+OO 1.223E+OO 1.223E+OO 31. 98 OK 835. 71 1. 61 2.005E+OO Line Not Found Absent 911. 20 25.80* 1.870E+OO 1.236E+OO 1.236E+OO 23.55 OK 968.97 15.80 1.778E+OO 9.614E-01 9.614E-01 30.58 OK TH-234 63.29 3.70* 9.123E+OO 9.143E-01 9.143E-01 121.47 OK 92.59 4.23 8.870E+OO 2.293E+OO 2.293E+OO 41. 31 OK U-234 609.32 45.49* 2.581E+00 8.641E-01 8. 641E-01 17.29 OK 1120.29 14.92 1.575E+OO 8.566E-01 8.566E-01 63.42 OK 1764.49 15.30 1.032E+OO 1.329E+OO 1.329E+00 30.86 OK U-235 89.96 3.47 8.895E+OO 1.942E+OO 1.942E+OO 55.31 OK 93.35 5.60 8.870E+OO 1.732E+OO l.732E+OO 41. 31 OK 143.76 10. 96* 7.808E+OO Line Not Found Absent 163.33 5.08 7.279E+OO Line Not Found Absent 185.72 57.20 6.697E+OO 2.183E-01 2.183E-01 38.33 OK 205.31 5.01 6.238E+OO Line Not Found Absent U-238 63.29 3.70* 9.123E+OO 9.143E-01 9.143E-01 121. 47 OK 92.59 4.23 8.870E+OO 2.293E+OO 2.293E+OO 41. 31 OK AM-243 43.53 5.90 9. 491E+OO Line Not Found Absent 74.66 67.20* 8.980E+OO 1.716E-01 1.716E-01 34.81 OK ANH-511 511. 00 100.00* 2.976E+OO 1.434E-01 1.434E-01 59.99 OK Flag: "*" = Keyline Page 3351 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:54:51.96 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621351.CNF;l *
  • Acquisition date 3-0CT-2016 08:53:50 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.64 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:20:00 Analyst initials: MXRl *
  • Sample ID G1203621351 Sample Quantity l.4159E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. Fil'e : DKAlOO: [CANBERRA.GAMMA]EFF GAM05' CAN.CNF;20
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.807E+Ol 1.673E+OO 5.312E-01 CD-109 2.540E+OO l.527E+00 1.161E+00 SN-126 l.624E-01 9.759E-02 7.417E-02 CS-135 3.559E-01 2.634E-01 2.149E-01 BA-137M 4.173E-01 1.152E-01 6.556E-02 CS-137 4.408E-01 l.217E-01 6.925E-02 HG-203 2.654E-01 3.637E+OO 3.759E+OO TL-208 2.870E-01 8.156E-02 6. 791E-02 PB-210 1. 480E+OO 9.261E-01 5.346E-01 BI-212 1. 795E+OO 1.019E+OO 7.345E-01 PB-212 1.192E+OO l.234E-01 8.005E-02 BI-214 8.644E-01 l.465E-01 9. 851E-02 PB-214 1.070E+OO 1. 8 61E-01 l.207E-01 RN-222 8.644E-01 l.465E-01 9.851E-02 RA-224 9.903E-01 1.157E+OO 8.588E-01 RA-226 8.644E-01 1.465E-01 9. 851E-02 AC-228 1.236E+OO 2.852E-01 2.059E-01 RA-228 1.236E+OO 2.852E-01 2.059E-01 TH-228 1.192E+OO 1.234E-01 8.005E-02 TH-229 -2.553E-01 4.379E-01 7. 714E-01 TH-230 8.641E-01 1.464E-01 9.848E-02 TH-232 1.236E+OO 2.852E-01 2.059E-01 TH-234 9.143E-01 l.088E+OO 8.558E-01 U-234 8.641E-01 1.464E-01 9.848E-02 U-235 . 7.009E-04 l.524E-01 2. 85'8E-01 U-238 9.143E-01 1.088E+OO 8.558E-01 AM-243 1. 716E-01 5.854E-02 4.948E-02 ANH-511 1.434E-01 8.432E-02 4.633E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 1.198E+00 1.188E+Ol 2.333E+Ol NOT IDENT. NA-22 -8.524E-03 4.026E-02 7.806E-02 NOT IDENT. Page 3352 of 5809 NA-24 O.OOOE+OO 1.218E+41 O.OOOE+OO SHORT HLIF AL-26 -l.819E-02 2.522E-02 3.887E-02 NOT IDENT. SC-46 2.973E-02 3.425E-01 6.047E-01 FAIL ABUN V-48 O.OOOE+OO 1.099E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 3.698E+02 O.OOOE+OO SHORT HLIF MN-54 2.230E-02 5.728E-02 l.160E-01 NOT IDENT. C0-56 -6.903E-02 4.712E-01 8.916E-01 FAIL ABUN MN-56 0.000E+OO 1. 960E+41 0.000E+OO SHORT HLIF C0-57 7.749E-03 3.492E-02 6.848E-02 NOT IDENT. C0-58 -1 .. 150E-01 6.885E-01 1.013E+OO NOT IDENT. FE-59 2.591E+OO 6.204E+OO 1.314E+Ol NOT IDENT. C0-60 6 .116E-03 3.470E-02 7.276E-02 NOT IDENT. ZN-65 -1.431E-01 2.130E-01 3.177E-01 NOT IDENT. GE-68 -2.938E-01 2 .118E+OO 4.172E+OO NOT IDENT. AS-73 -1.457E-01 1.670E+OO 3.358E+OO NOT IDENT. AS-74 0.000E+OO 4.936E+03 O.OOOE+OO SHORT HLIF SE-75 l.219E-02 1.742E-01 3.234E-01 NOT IDENT. BR-77 0.000E+OO 1. 219E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.493E+02 O.OOOE+OO SHORT HLIF RB-83 -2.829E-01 5.702E-01 l.045E+OO FAIL ABUN KR-85 1.970E+OO 5. 981E+OO 1.118E+Ol NOT IDENT. SR-85 2.0lOE-01 6.181E-01 1.155E+OO NOT IDENT. RB-86 O.OOOE+OO 2.381E+04 O.OOOE+OO SHORT HLIF Y-88 9.869E-02 l.990E-01 4.849E-01 NOT IDENT. Y-91 -4.783E+02 5.949E+02 1. 021E+03 NOT IDENT. NB-94 2. llOE-02 3.395E-02 6.849E-02 NOT IDENT. NB-95 -9.650E-01 9.129E-01 l.453E+OO NOT IDENT. NB-95M -1.421E+OO 2.144E+OO 3.333E+OO NOT IDENT. ZR-95 -4.361E-02 1.500E+OO 2.538E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 7.475E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.007E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 684E+41 O.OOOE+OO SHORT HLIF RH-101 -2.626E-02 2.720E-02 4.825E-02 NOT IDENT. RH-102 1.073E-02 4.765E-02 9.727E-02 NOT IDENT. RU-103 -3.534E+OO 4.918E+OO 8.768E+OO FAIL ABUN RH-106 2.090E-01 4.657E-01 9.522E-01 NOT IDENT. RU-106 2.090E-01 4.657E-01 9.522E-01 NOT IDENT. AG-108M -l.608E-02 2.313E-02 4.206E-02 NOT IDENT. AG-llOM -5.618E-02 8.945E-02 l.502E-01 FAIL ABUN SN-113 -7.373E-02 1. 739E-01 3.317E-01 NOT IDENT. CD-115 O.OOOE+OO 1.474E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 7.285E+04 O.OOOE+OO SHORT HLIF TE-123M -3.381E-02 l.057E-01 l.945E-01 NOT IDENT. SB-124 5. 851E-01 1.573E+OO 3.832E+OO NOT IDENT. SB-125 1.226E-01 1.638E-01 2.028E-01 FAIL ABUN TE-125M 3.826E+Ol 2.051E+02 4.006E+02 NOT IDENT. I-126 O.OOOE+OO 7.802E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.085E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.410E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.679E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.222E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.054E+26 O.OOOE+OO SHORT HLIF BA-133 1. 321E-02 3.586E-02 6.805E-02 FAIL ABUN I-133 O.OOOE+OO 1.526E+41 O.OOOE+OO SHORT HLIF CS-134 4.753E-02 7.744E-02 1.062E-01 FAIL ABUN I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.302E+05 O.OOOE+OO SHORT HLIF CE-139 5.537E-04 9.138E-02 1. 721E-01 NOT IDENT. BA-140 O.OOOE+OO 9.242E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.833E+05 O.OOOE+OO SHORT HLIF CE-141 1.082E+Ol 1. 897E+Ol 3.748E+Ol NOT IDENT. CE-143 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 4.280E-02 2.800E-01 5. 411E-01 FAIL ABUN PM-144 -l.650E-02 5. 341E-02 9.727E-02 NOT IDENT. PR-144 -l.460E+OO 4. 631E+OO 8.426E+OO NOT IDENT. PM-146 2.852E-02 4.088E-02 8. 571E-02 FAIL ABUN ND-147 O.OOOE+OO 4.757E+07 O.OOOE+OO SHORT HLIF PM-147 -2.543E+02 6.036E+02 l.126E+03 NOT IDENT. PM-149 O.OOOE+OO 2 .111E+40 O.OOOE+OO SHORT HLIF EU-150 -1.118E-02 2.838E-02 4.399E-02 FAIL ABUN EU-152 1.583E-02 8.325E-02 l.542E-01 FAIL ABUN GD-153 -3.971E-02 l.225E-Ol 2.322E-01 NOT IDENT. EU-154 -1.862E-02 9.932E-02 l.934E-01 NOT IDENT. EU-155 5.563E-02 8.219E-02 1.657E-01 FAIL ABUN TB-160 3.548E-01 1.808E+OO 3.530E+OO FAIL ABUN H0-166M -2.302E-02 5.423E-02 9.785E-02 FAIL ABUN TM-171 1.147E+OO 3.793E+OO 7.812E+OO NOT IDENT. Page 3353 of 5809 HF-172 1. 406E-01 1.800E-01 3.641E-01 FAIL ABUN LU-172 3.597E-02 8.218E-02 1. 708E-01 FAIL ABUN LU-176 -2.303E-02 2.340E-02 3. 722E-02 FAIL ABUN HF-181 -2.095E+OO 4.058E+OO 7.444E+OO NOT IDENT. TA-182 1.355E-01 8.576E-01 1. 568E+OO FAIL ABUN RE-183 -2.948E-02 8.280E-01 1.657E+OO NOT IDENT. RE-184 l.334E+Ol 2.908E+Ol 5.875E+Ol NOT IDENT. W-188 9.998E+Ol 1.138E+02 2.104E+02 FAIL ABUN IR-192 1.234E-01 4.267E-01 7.979E-Ol FAIL ABUN BI-207 1. 03.2E-03 4.267E-02 8.643E-02 FAIL ABUN BI-211 O.OOOE+OO 5.125E-01 8.430E-01 FAIL ABUN PB-211 2.983E-01 6.093E-01 1.254E+OO FAIL ABUN RN-219 -1.275E-01 3.364E-01 6.381E-01 NOT IDENT. RA-223 -2.049E-01 6.432E-01 1.013E+OO FAIL ABUN AC-227 2.618E-02 1.990E-01 3.709E-01 FAIL ABUN TH-227 2.618E-02 1.990E-01 3.709E-01 FAIL ABUN PA-231 -1.344E-01 4.492E-01 7.813E-01 NOT IDENT. TH-231 -2.049E-01 6.432E-01 1.013E+OO FAIL ABUN PA-233 3.083E-02 5.582E-02 1.074E-01 FAIL ABUN PA-234 1. 892E-01 2.740E-01 5.727E-01 NOT IDENT. PA-234M -6. 718E-01 4.014E+OO 7.941E+OO NOT IDENT. NP-237 3.083E-02 5.582E-02 l.074E-01 FAIL ABUN NP-238 O.OOOE+OO 1.938E+41 O.OOOE+OO SHORT HLIF NP-239 -1.725E-01 l.917E-01 3.446E-01 FAIL ABUN PU-239 l.092E+02 2.525E+02 4.958E+02 NOT IDENT. AM-241 2.777E-02 4.648E-02 9.007E-02 NOT IDENT. CM-243 -2.004E-02 6.947E-02 l.323E-01 FAIL ABUN BK-247 1. 205E-02 6.575E_..:02 1.145E-01 FAIL ABUN CM-247 -4.604E-03 3.008E-02 5.856E-02 FAIL ABUN CF-249 2.627E-02 3.068E-02 6.637E-02 NOT IDENT. CF-251 -2.207E-02 9.952E-02 1.827E-01 NOT IDENT. Page 3354 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:54:49.80 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Ef f pCi/GRAM pCi7GRAM %Error K-40 1460.82 452 10.66* 1.244E+OO l.807E+Ol 1.807E+Ol 9.45 CD-109 88.03 173 3.70* 8.913E+OO 2 .. 789E+OO 4.363E+OO 34.45 SN-126 64.28 58 9.60 9.123E+OO 3.524E-01 3.524E-01 121. 4 7 86.94 173 8.90 8.913E+OO l.160E+OO 1.160E+OO 34.45 87.57 173 37.00* 8.913E+OO 2.789E-01 2.789E-01 34.45 CS-135 268.22 54 16.00* 5.040E+OO 3.559E-01 3.559E-01 75.52 BA-137M 661. 66 168 89.90* 2.416E+OO 4.095E-01 4.173E-01 28.18 CS-137 661. 66 168 85.10* 2.416E+OO 4.326E-01 4.408E-01 28.18 HG-203 70.83 ------3.69 9.006E+OO ------Line Not Found ------72.87 ------6.19 8.990E+00 ------Line Not Found ------279.20 20 81.56* 4.917E+OO 2.638E-02 2.215E+OO 165.55 TL-208 277.37 20 6.60 4.917E+OO 3.260E-01 3.260E-01 165.55 583.19 123 85.00* 2.673E+OO 2.870E-01 2.870E-01 29.00 8 60. 56 ------12.50 1.959E+OO ------Line Not Found ------PB-210 46.54 112 4.25* 9.655E+OO 1.443E+OO l.480E+OO 63.86 BI-211 72. 87 ------1.23 8.990E+OO ------Line Not Found ------351.06 290 12.92* 4.043E+OO 2.948E+OO 2.948E+OO 17.74 BI-212 727.33 51 6.67* 2.240E+OO l.795E+OO 1. 795E+OO 57.93 785.37 25 1.10 2.105E+OO 5.833E+OO 5.833E+OO 100.60 1620.50 ------1. 47 1.126E+OO ------Line Not Found ------PB-212 74.82 319 10.28 8.980E+OO l.835E+00 1.835E+OO 19.40 77 .11 593 17 .10 8.967E+OO 2.051E+OO 2.051E+OO 11. 84 238.63 545 43.60* 5.564E+OO l.192E+OO 1.192E+OO 10.57 300.09 ------3.30 4. 613E+OO ------Line Not Found ------BI-214 609.32 191 45.49* 2. 581E+OO 8.641E-01 8.644E-01 17.29 1120.29 38 14.92 1. 575E+OO 8.566E-01 8.569E-01 63.42 1764.49 40 15.30 1.032E+OO 1.329E+OO l.329E+00 30.86 PB-214 74.82 319 5.80 8.980E+OO 3.252E+OO 3.253E+OO 19.40 77 .11 593 9.70 8. 967E+OO 3.616E+OO 3.618E+OO 11. 84 87.09 173 3.41 8.913E+00 3.026E+OO 3.028E+OO 34.45 242.00 137 7.25 5.506E+OO l.824E+OO 1.825E+OO 33.13 295.22 206 18.42 4.680E+OO l.264E+OO 1.265E+OO 22.46 351. 93 290 35.60* 4.043E+OO 1.070E+OO 1. 070E+OO 17.74 RN-222 609.32 191 45.49* 2.581E+OO 8.641E-01 8.644E-01 17.29 1120.29 38 14.92 l.575E+00 8.566E-01 8.569E-01 63.42 1764.49 40 15.30 1.032E+OO 1.329E+OO 1.329E+OO 30.86 RA-224 240.99 137 4.10* 5.506E+OO 3.226E+OO 3.226E+OO 33.13 RA-226 609.32 191 45.49* 2. 581E+OO 8.641E-01 8.644E-01 17.29 1120.29 38 14.92 1.575E+OO 8.566E-01 8.569E-01 63.42 1764.49 40 15.30 1. 032E+OO 1. 329E+OO 1. 329E+OO 30.86 AC-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 109 11. 27 4.180E+OO l.223E+OO 1.223E+OO 31. 98 794.95 12 4.25 2.087E+OO 7.274E-01 7.274E-01 166.25 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 112 25.80* 1. 870E+OO 1.236E+OO 1.236E+OO 23.55 968.97 51 15.80 1. 778E+OO 9.614E-01 9.614E-01 30.58 RA-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------Page 3355 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : Gl203621351 Acquisition date 3-0CT-2016 08:53:50 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 338.32 109 11. 27 4.180E+OO l.223E+00 l.223E+OO 31. 98 794.95 12 4.25 2.087E+00 7.274E-01 7.274E-01 166.25 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911. 20 112 25.80* 1.870E+OO 1.236E+00 1.236E+OO 23.55 968. 97 51 15.80 l.778E+OO 9.614E-01 9.614E-01 30.58 TH-228 74.82 319 10.28 8.980E+OO 1.835E+OO 1.835E+OO 19.40 77 .11 593 17.10 8.967E+OO 2. 051E+OO 2.051E+OO 11. 84 23-8. 63 545 43.60* 5.564E+OO l.192E+OO 1.192E+OO 10.57 300.09 ------3.30 4.613E+OO ------Line Not Found ------TH-229 85.43 173 14.70 8.913E+OO 7.021E-01 7.021E-01 34.45 88.47 113 24.00 8.895E+OO 2.808E-01 2.808E-01 55.31 193.51 ------4.41* 6. 511E+OO ------Line Not Found ------210.85 ------2.80 6 .116E+OO ------Line Not Found ------TH-230 609.32 191 45.49* 2.581E+OO 8. 641E-01 8.641E-01 17.29 1120.29 38 14.92 1.575E+OO 8.566E-01 8.566E-01 63.42 1764.49 40 15.30 1.032E+OO 1. 329E+00 1. 329E+OO 30.86 TH-232 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 109 11.27 4.180E+00 l.223E+00 1.223E+OO 31. 98 835.71 ------1. 61 2.005E+OO ------Line Not'Found ------911.20 112 -25.80* l.870E+00 1. 236E+00 1.236E+OO 23.55 968. 97 51 15.80 1. 778E+OO 9.614E-01 9.614E-01 30.58 TH-234 63.29 58 3.70* 9.123E+OO 9.143E-01 9.143E-01 121. 4 7 92.59 162 4.23 8.870E+00 2.293E+00 2.293E+OO 41. 31 U-234 609.32 191 45.49* 2.581E+OO 8.641E-01 8. 641E-01 17.29 1120.29 38 14.92 1.575E+00 8.566E-01 8.566E-01 63.42 1764.49 40 15.30 l.032E+OO 1.329E+OO l.329E+00 30.86 U-235 89. 96 113 3.47 8.895E+OO l.942E+00 l.942E+OO 55.31 93.35 162 5.60 8.870E+OO 1. 732E+00 1.732E+OO 41. 31 143.76 ------10. 96* 7.808E+00 ------Line Not Found ------163.33 ------5.08 7.279E+OO ------Line Not Found ------185. 72 158 57.20 6.697E+OO 2.183E-01 2.183E-01 38.33 205.31 ------5.01 6.238E+00 ------Line Not Found ------U-238 63.29 58 3.70* 9.123E+OO 9.143E-01 9.143E-01 121.47 92.59 162 4.23 8.870E+OO 2.293E+OO 2.293E+OO 41. 31 AM-243 43.53 ------5.90 9.491E+OO ------Line Not Found ------74.66 319 67.20* 8.980E+00 2.807E-01 2.807E-01 19.40 ANH-511 511. 00 80 100.00* 2.976E+OO 1.434E-01 1.434E-01 59.99 Flag: "*" Key line Page 3356 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : Gl203621351 Acquisition date 3-0CT-2016 08:53:50 Total number of lines in spectrum 58 Number of unidentified lines 16 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 HG-203 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA....:224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y 46.59D 1.41E+10Y 22.20Y 7.04E+08Y l.41E+l0Y l.41E+l0Y 1600. OOY 1600.00Y 1600. OOY 1.41E+10Y 1600. OOY l.41E+10Y 1. 41E+10Y l.41E+l0Y 7340.00Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1. 00E+09Y Decay 1. 00 1. 56 1. 00 1. 00 1. 02 1. 02 84.0 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.807E+Ol 2.789E+OO 2.789E-01 3.559E-01 4.095E-01 4.326E-01 2.638E-02 2.870E-01 1.443E+OO 2.948E+OO 1.795E+OO l.192E+OO 8. 641E-01 1.070E+OO 8. 641E-01 3.226E+OO 8. 641E-01 l.236E+00 1.236E+OO 1.192E+OO 2.808E-01 8. 641E-01 1.236E+OO 9.143E-01 8.641E-01 2.183E-01 9.143E-01 2.807E-01 l.434E-01 4.629E+Ol 4.629E+Ol Decay Corr pCi/GRAM 1.807E+Ol 4.363E+OO 2.789E-01 3.559E-01 4.173E-01 4.408E-01 2.215E+OO 2.870E-01 l.480E+OO 2.948E+OO 1.795E+OO 1.192E+OO 8.644E-01 1.070E+OO 8.644E-01 3.226E+OO 8.644E-01 1.236E+OO 1.236E+OO l.192E+OO 2.808E-01 8. 641E-01 1.236E+OO 9.143E-01 8.641E-01 2.183E-01 9.143E-01 2.807E-01 1.434E-01 5. OllE+Ol 5. OllE+Ol 72.41% Decay Corr 2-Sigma Error 0.171E+Ol 1.503E+OO 0. 961E-01 2.688E-01 l.176E-01 l.242E-01 3.667E+OO 0.832E-01 0.945E+OO 0.523E+OO 1.040E+OO 0.126E+00 l.495E-01 0.190E+OO l.495E-01 1.069E+OO l.495E-01 0. 291E+OO 0. 291E+OO 0.126E+OO l.553E-01 1. 494E-01 0.291E+OO 11. llE-01 l.494E-01 0.837E-01 ll. llE-01 0.545E-01 0.860E-01 "M" Manually accepted 2-Sigma %Error 9.45 34.45 34.45 75.52 28.18 28.18 165.55 29.00 63. 86 17.74 57.93 10.57 17.29 17.74 17.29 33.13 17.29 23.55 23.55 10.57 55.31 17.29 23.55 121.47 17.29 38.33 121.47 19.40 59.99 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3357 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G1203621351 Acquisition date : 3-0CT-2016 08:53:50 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 32.25 34 158 0.67 66.34 63 6 7.19E-03 **** 2.13E+OO 1 39.16 57 116 0.83 80.15 76 12 1. 22E-02 70.0 8.19E+OO 1 41. 51 28 107 0.84 84.85 76 12 6.03E-03 **** 9.lOE+OO 2 79.29 41 155 1. 04 160.36 147 20 9.28E-03 **** 8.95E+OO T 0 83.50 53 137 1. 39 168.76 167 5 1.22E-02 80.3 8.93E+OO T 0 208.97 30 102 1.18 419.54 416 7 7.43E-03 **** 6.16E+OO 0 327.78 35 41 1. 08 656.98 654 6 8.82E-03 70.5 4.29E+OO T 1 339.92 31 44 '1. 37 681.25 671 15 7.98E-03 **** 4.16E+OO T 0 409.97 33 31 1. 86 821. 26 818 7 8.43E-03 69.4 3.56E+OO T 2 427.28 19 37 1. 62 855.85 848 26 5.02E-03 **** 3.44E+OO T 2 431.57 34 37 1. 62 864.44 848 26 8.90E-03 73.7 3. 41E+OO 0 463.04 30 43 1.17 927.33 922 11 7.82E-03 96. 0 3.22E+OO T 0 530.48 15 31 1. 47 1062.12 1054 11 4.02E-03 **** 2.88E+OO T 0 623.99 26 29 1. 74 1249.01 1240 14 7.05E-03 96. 8 2.53E+00 0 735.20 4 21 1. 06 1471.28 1466 9 1. l 7E-03 **** 2.22E+OO T 0 754.89 10 17 0.61 1510.64 1506 8 2.61E-03 **** 2.18E+OO T 0 806.54 10 21 0.50 1613.88 1608 9 2.85E-03 **** 2.06E+OO 0 815.54 7 18 1. 27 1631.86 1626 10 1. 8 8E-03 **** 2.05E+00 T 0 892.23 15 6 1. 85 1785.15 1780 9 4.09E-03 81. 8 1. 90E+OO 0 920.75 7 11 1. 40 1842.14 1836 9 l.94E-03 **** 1. 85E+OO 2 934.55 24 4 2.10 1869.73 1863 19 6. 81E-03 59.2 1. 83E+OO 2 *'938.82 14 0 2 .11 1878.27 18 63 '19 4.00E-03 57.4 1. 83E+OO T 0 964.48 31 11 0.73 1929.55 1924 11 8. 61E-03 54.8 1. 79E+OO T 3 973.23 14 1 2.35 1947.04 1935 16 4.02E-03 66.4 1.77E+OO 0 1035.77 4 21 1. 05 2072.04 2064 10 1.14E-03 **** 1. 68E+OO 0 1156. 90 7 8 1.13 2314.17 2311 7 1.95E-03 **** 1. 53E+OO 0 1230.25 12 18 3.83 2460.78 2449 15 3.48E-03 **** 1.45E+OO T 0 1238. 71 33 16 2.38 2477.68 2471 11 9.29E-03 58.4 1.44E+00 T 0 1280.62 15 3 1. 95 2561.44 2558 7 4.42E-03 63.1 1.40E+OO 0 1377. 31 16 0 1. 29 2754.71 2748 12 4.72E-03 48.5 1. 31E+OO 0 1631. 06 11 0 1. 44 32 61. 92 3257 10 3.33E-03 57.7 1.12E+OO Flags: "T" = Tentatively associated Page 3358 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:55:04.27 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621351.CNF;l *
  • Acquisition date 3-0CT-2016 08:53:50 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.64 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:20:00 Nuclide Library : SOLID *
  • Sample ID Gl203621351 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.4159E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * * *.Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 HG-203 TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2 .113E-01 5.445E-01 3.478E-02 9.828E-02 2.935E-02 3.lOlE-02 1. 723E+OO 3.073E-02 2.481E-01 3.184E-01 3.695E-02 4.302E-02 5.519E-02 4.302E-02 3. 965E-01 4.302E-02 8.789E-02 8.789E-02 3.695E-02 3.597E-01 4.300E-02 8.789E-02 4.053E-01 4.300E-02 1. 341E-01 4.053E-01 2.348E-02 2.070E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3359 of 5809 Le (pCi/GRAM 1.058E+Ol 3.266E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-f47 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3360 of 5809 1.228E-02 2.576E-01 O.OOOE+OO O.OOOE+OO 5. 096E-02 3.927E-01 O.OOOE+OO 3.199E-02 4.411E-01 5.743E+OO 3.045E-02 l.378E-01 1. 791E+OO 1.576E+OO O.OOOE+OO 1.479E-01 O.OOOE+OO 0.000E+OO 4.616E-01 4.986E+OO 5.149E-01 O.OOOE+OO l.919E-01 4.467E+02 3.107E-02 6.411E-01 1.532E+00 1.114E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.253E-02 4.258E-02 3.874E+OO 4.256E-01 4.256E-01 l.863E-02 6.317E-02 l.474E-01 O.OOOE+OO O.OOOE+OO 9.044E-02 1. 484E+OO 9.258E-02 l.885E+02 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.088E-02 O.OOOE+OO 4.776E-02 O.OOOE+OO O.OOOE+OO 8.024E-02 O.OOOE+OO O.OOOE+OO 1. 759E+Ol O.OOOE+OO 2.532E-01 4.305E-02 3. 728E+OO 3.903E-02 O.OOOE+OO 5.240E+02 O.OOOE+OO 2.014E-02 7.008E-02 1.091E-01 8.106E-02 7.822E-02 1.547E+OO 4.300E-02 3.676E+OO l.711E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3361of5809 7.575E-02 1. 68 6E-02 3.340E+OO 6. 729E-01 7.826E-01 2.593E+Ol 9.768E+Ol 3.657E-01 3.722E-02 4.075E-01 5.730E-01 2.882E-01 4.635E-01 1.705E-01 1.705E-01 3.605E-01 4.635E-01 4.938E-02 2.530E-01 3.473E+OO 4.938E-02 O.OOOE+OO 1. 611E-01 2.334E+02 4.273E-02 6.190E-02 5.237E-02 2.645E-02 3.018E-02 8.510E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:55:09.89 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621351.CNF;l * *Acquisition date 3-0CT-2016 08:53:50 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.64 Half life ratio : ***** *
  • Sample date 10-DEC-2015 14:20:00 Nuclide Library : SOLID *
  • Sample ID G1203621351 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : l.4159E+02 GRAM *
  • Quantity Err(%) : 1.4126E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.807E+Ol 1.921E+OO CD-109 2.540E+OO 1.557E+OO SN-126 1.624E-01 9.918E-02 CS-135 3.559E-01 2.645E-01 BA-137M 4.173E-01 l.166E-01 CS-137 4.408E-01 l.232E-01 HG-203 2.654E-01 3.643E+OO TL-208 2.870E-01 8.247E-02 PB-210 1.480E+OO 9.379E-01 BI-212 1. 795E+OO 1.023E+OO PB-212 1.192E+OO 1.387E-01 BI-214 8.644E-01 1. 511E-01 PB-214 l.070E+OO 1.913E-01 RN-222 8.644E-01 1. 511E-01 RA-224 9.903E-01 1.168E+OO RA-226 8.644E-01 1. 511E-01 AC-228 1.236E+OO 2.921E-01 RA-228 1.236E+OO 2. 921E-01 TH-228 1.192E+OO l.387E-01 TH-229 -2.553E-01 4.381E-01 TH-230 8. 641E-01 1. 511E-01 TH-232 l.236E+OO 2. 921E-01 TH-234 9.143E-01 1.107E+OO U-234 8. 641E-01 1. 511E-01 U-235 7.009E-04 l.524E-01 U-238 9.143E-01 l.107E+°OO AM-243 1. 716E-01 6.106E-02 ANH-511 l.434E-01 8.452E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3362 of 5809 Key-Line Activity (pCi/GRAM 1.198E+OO -8.524E-03 K.L Act error ( 1. 96-sigma) 1.188E+Ol 4.027E-02 TPU ( 1. 96-sigma) l.921E+OO l.557E+OO 9.918E-02 2.645E-01 l.166E-01 l.232E-01 3.643E+OO 8.247E-02 9.379E-01 1.023E+OO l.387E-01 1. 511E-01 1. 913E-01 l.511E-01 1.168E+OO 1. 511E-01 2.921E-01 2. 921E-01 l.387E-01 4.381E-01 1. 511E-01 2.921E-01 l.107E+OO l.511E-01 1.524E_.:01 l.107E+OO 6.106E-02 8. 452E.:..02 TPU (1. 96-sigma) 1.189E+Ol NOT IDENT. 4.045E-02 NOT IDENT.

NA-24 -1.000E+41 1. 293E+41 0.000E+OO SHORT HLIF AL-26 -1. 819E-02 2.525E-02 2.655E-02 NOT IDENT. SC-46 2.973E-02 3.425E-01 3.428E-01 FAIL ABUN V-48 -5.603E+03 1.100E+04 1.128E+o4 SHORT HLIF CR-51 -3.415E+Ol 3.698E+02 3.701E+02 SHORT HLIF MN-54 2.230E-02 5.729E-02 5.816E-02 NOT IDENT. C0-56 -6.903E-02 4.712E-01 4. 722E-01 FAIL ABUN MN-56 -l.OOOE+41 7.515E+41 O.OOOE+OO SHORT HLIF C0-57 7.749E-03 3.493E-02 3.510E-02 NOT IDENT. C0-58 -1.150E.-01 6.885E-01 6.904E-Ol NOT IDENT. FE-59 2. 591E+OO 6.206E+OO 6.315E+OO NOT IDENT. C0-60 6.116E-03 3.470E-02 3.481E-02 NOT IDENT. ZN-65 -1.431E-01 2.130E-01 2.226E-01 NOT IDENT. GE-68 -2.938E-01 2 .118E+OO 2.122E+OO NOT IDENT. AS-73 -1.457E-01 1.670E+OO 1. 671E+OO NOT IDENT. AS-74 -5.065E+02 4.936E+03 4.941E+03 SHORT HLIF SE-75 l.219E-02 1.742E-01 1.743E-01 NOT IDENT. BR-77 1.177E+38 l.012E+39 O.OOOE+OO SHORT HLIF SR-82 5.163E+02 6.498E+02 6.902E+02 SHORT HLIF RB-83 -2.829E-01 5.715E-01 5.855E-01 FAIL ABUN KR-85 1. 970E+OO 5. 981E+OO 6.047E+OO NOT IDENT. SR-85 2.0lOE-01 6.181E-01 6.247E-01 NOT IDENT. RB-86 l.284E+03 2.381E+o4 2.381E+04 SHORT HLIF Y-88 9.869E-02 1.991E-01 2.040E-01 NOT IDENT. Y-91 -4.783E+02 5.952E+02 6.330E+02 NOT IDENT. NB-94 2. llOE-02 3.396E-02 3.527E-02 NOT IDENT. NB-95 -9.650E-01 9.139E-01 1.012E+OO NOT IDENT. NB-95M -1. 421E+OO 2.147E+00 2.241E+OO NOT IDENT. ZR-95 -4. 361E-02 1.500E+OO 1.500E+OO NOT IDENT. NB-97 l.000E+41 1.485E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 7.486E+40 O.OOOE+OO SHORT HLIF M0-99 -3.682E+30 1.007E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.687E+41 O.OOOE+OO SHORT HLIF RH-101 -2.626E-02 2. 761E-02 3.004E-02 NOT IDENT. RH-102 1.073E-02 4.766E-02 4.790E-02 NOT IDENT. RU-103 -3.534E+OO 4.920E+OO 5. l 72E+OO FAIL ABUN RH-106 2.090E-01 4.659E-01 4.753E-01 NOT IDENT. RU-106 2.090E-01 4.659E-01 4.753E-01 NOT IDENT. AG-108M -l.608E-02 2.314E-02 2.425E-02 NOT IDENT. AG-llOM -5.618E-02 8.950E-02 9.301E-02 FAIL ABUN SN-113 -7.373E-02 l.739E-01 1.771E-01 NOT IDENT. CD-115 -3.925E+38 1.476E+39 O.OOOE+OO SHORT HLIF SN-117M -5.892E+04 7. 318E+o4 7.785E+04 SHORT HLIF TE-123M -3. 381E-02 1.057E-01 l.068E-01 NOT IDENT. SB-124 5. 851E-01 1.574E+OO 1.595E+OO NOT IDENT. SB-125 1. 22 6E-01 l.639E-01 1.729E-01 FAIL ABUN TE-125M 3.826E+Ol 2. 051E+02 2.058E+02 NOT IDENT. I-126 4. 960E+05 7. 831E+05 8.144E+05 SHORT HLIF SB-126 2.163E+05 1.086E+06 1.090E+06 SHORT HLIF SB-127 1.259E+21 l.421E+22 O.OOOE+OO SHORT HLIF I-131 -2.082E+08 3.679E+09 3. 681E+09 SHORT HLIF I-132 -l.000E+41 l.840E+42 O.OOOE+OO SHORT HLIF TE-132 -2.398E+25 2.057E+26 O.OOOE+OO SHORT HLIF BA-133 1. 321E-02 3.587E-02 3.636E-02 FAIL ABUN I-133 l.000E+41 2.357E+41 O.OOOE+OO SHORT HLIF CS-134 4.753E-02 7.747E-02 8.038E-02 FAIL ABUN I-135 l.000E+41 1.080E+42 O.OOOE+OO SHORT HLIF CS-136 4.573E+04 2.303E+05 2.312E+05 SHORT HLIF CE-139 5.537E-04 9.138E-02 9.138E-02 NOT IDENT. BA-140 7.225E+05 9.247E+05 9.804E+05 SHORT HLIF LA-140 -5.438E+05 4.840E+05 5.425E+05 SHORT HLIF CE-141 1.082E+Ol 1.898E+Ol 1. 960E+Ol NOT IDENT. CE-143 1.000E+41 2.746E+41 O.OOOE+OO SHORT HLIF CE-144 4.280E-02 2.800E-01 2.807E-01 FAIL ABUN PM-144 -l.650E-02 5.342E-02 5.393E-02 NOT IDENT. PR-144 -l.460E+OO 4.631E+OO 4.678E+OO NOT IDENT. PM-146 2.852E-02 4.093E-02 4.290E-02 FAIL ABUN ND-147 3 .118E+07 4.760E+07 4. 963E+07 SHORT HLIF PM-147 -2.543E+02 6.037E+02 6.145E+02 NOT IDENT. PM-149 7.426E+39 2 .117E+40 O.OOOE+OO SHORT HLIF EU-150 -l .118E-02 2.839E-02 2.883E-02 FAIL ABUN EU-152 1.583E-02 8.325E-02 8.356E-02 FAIL ABUN GD-153 -3.971E-02 1.225E-01 1.238E-01 NOT IDENT. EU-154 -1. 862E-02 9.933E-02 9.968E-02 NOT IDENT. EU-155 5.563E-02 8.229E-02 8.602E-02 FAIL ABUN TB-160 3.548E-01 1.809E+OO 1.816E+OO FAIL ABUN H0-166M -2.302E-02 5.424E-02 5.523E-02 FAIL ABUN TM-171 1.147E+OO 3.795E+OO 3.830E+OO NOT IDENT. Page 3363 of 5809 HF-172 1.406E-01 1. 815E-01 1.922E-01 FAIL ABUN LU-172 3.597E-02 8.226E-02 8.384E-02 FAIL ABUN LU-176 -2.303E-02 2.342E-02 2.562E-02 FAIL ABUN HF-181 -2.095E+OO 4.059E+00 4.168E+OO NOT IDENT. TA-182 l.355E-01 8.576E-01 8.598E-01 FAIL ABUN RE-183 -2.948E-02 8.280E-01 8. 281E-01 NOT IDENT. RE-184 1.334E+Ol 2.926E+Ol 2.987E+Ol NOT IDENT. W-188 9.998E+Ol l.144E+02 1.229E+02 FAIL ABUN IR-192 1.234E-01 4.267E-01 4.303E-01 FAIL ABUN BI-207 1. 032E-0.3 4.267E-02 4.267E-02 FAIL ABUN BI-211 2.948E+OO 5.292E-01 l.430E+OO FAIL ABUN PB-211 2.983E-01 6.095E-01 6.242E-01 FAIL ABUN RN-219 -1.275E-01 3.368E-01 3.417E-01 NOT IDENT. RA-223 -2.049E-01 6.433E-01 6.499E-01 FAIL ABUN AC-227 2.618E-02 l.990E-01 l.994E-01 FAIL ABUN TH-227 2.618E-02 l.990E-01 l.994E-01 FAIL ABUN PA-231 -1.344E-01 4.501E-01 4.542E-01 NOT IDENT. TH-231 -2.049E-01 6.433E-01 6.499E-01 FAIL ABUN PA-233 3.083E-02 5.584E-02 5.754E-02 FAIL ABUN PA-234 l.892E-01 3.491E-01 3.594E-01 NOT IDENT. PA-234M -6. 718E-01 4.014E+00 4.025E+OO NOT IDENT. NP-237 3.083E-02 5.584E-02 5.754E-02 FAIL ABUN NP-238 -2.003E+39 1. 938E+41 O.OOOE+OO SHORT HLIF NP-239 -1.725E-01 1.922E-01 2.074E-01 FAIL ABUN PU-239 l.092E+02 2.525E+02 2.573E+02 NOT IDENT. AM-241 2.777E-02 4.653E-02 4.818E-02 NOT IDENT. CM-243 -2.004E-02 6.949E-02 7.008E-02 FAIL ABUN BK-247 1.205E-02 6.579E-02 6.602E-02 FAIL ABUN CM-247 -4.604E-03 3.009E-02 3.016E-02 FAIL ABUN CF-249 2.627E-02 3.075E-02 3.295E-02 NOT IDENT. CF-251 -2.207E-02 9.955E-02 1.000E-01 NOT IDENT. Page 3364 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 49.1228 87.09 76.1071 136.47 69.0987 45.60 55.7147 87.57 76.1977 140.51 0.0000 46.54 55.9163 88.03 76.2836 143.76 73.9265 49.72 0.0000 88.34 76.3411 144.24 68.0682 51. 35 80.6338 88.47 76.3656 145.44 65.2417 51. 87 66.5273 89.96 76.6420 152.43 64.0059 52.39 68.2366 1093.63 76. 7676 153.25 0.0000 52.97 71. 5557 91.11 0.0000 323.87 70.2094 53.44 70.8767 92.59 77.1247 156.02 0.0000 54.07 76.6183 93.35 77.2629 158.56 0.0000 57.36 0.0000 94.56 73.9057 159.00 65.6982 57.53 91.2452 94.65 73.9214 162.33 67.0594 57.98 97.8495 94.67 73.9246 162.66 0.0000 59.27 93 .1185 94.87 73.9586 163.33 64 .1113 59.32 93.1339 97.43 84.5951 165.86 63.3415 59.54 96. 4511 98.43 75. 7671 176.31 61.2300 60. 96 102.3334 98.44 75.7687 176.60 0.0000 61.17 99.1332 99.53 73.2425 177.52 66.5361 62.93 106.8018 100 .11 66.0944 181.07 0.0000 63.29 106. 9211 102.03 72.7411 181.52 55.7690 63.58 107.0168 103.18 86.5982 184.41 75.5991 64.28 106.6966 103.37 78. 4263 143.76 62.0645 66.73 103.0565 105.21 80.5711 193.51 77.6271 67.24 109.0391 105.31 77.8412 197.03 72.6567 125.81 109.1810 106.12 84.3984 198.01 58.8437 67.75 111. 7038 106.47 94.5602 201.83 78.5004 69.67 114.8485 109.28 80.3472 203.43 70.0454 70.83 114.3900 111. 00 77.8553 205.31 99.3868 72. 81 121.7988 111.76 0.0000 210.85 66.7343 72.87 121.8197 114. 06 58.7587 215.65 56.9250 74.66 115.6247 116. 30 0.0000 222 .11 46.3483 74.82 115.6755 116.74 90.9597 227.09 44.4104 74.97 115. 7233 119.76 78.2976 227.38 47.7576 77.11 116. 3987 121.12 69.0474 228.16 0.0000 78.74 116. 9072 121.22 69.0607 228.18 45.5807 79.69 117.2008 121. 78 71. 9765 116.74 45.5807 80.12 117.3326 122.06 62.5402 235.69 58.3278 80.19 0.0000 122.92 69.2880 235. 96 58.3469 80.57 117.4706 123.07 71. 2069 238.63 48.3986 81. 00 117.6024 265.00 72.2404 238.98 0.0000 81. 07 117. 6241 125.81 63.9442 240.99 48.5312 81. 75 62.3809 127.23 89.9520 242.00 48.5882 83.79 80.1266 127.91 76.6528 244.70 45.3381 84.00 88.8835 129.30 74.9293 252.40 0.0000 85.43 89.2041 131.20 73.2643 252.80 41.1784 86.55 76.0059 133.02 84.1472 254.15 0.0000 86.79 76.0509 133.52 67.7655 256.23 41.3350 86.94 76.0793 136. 00 70.0137 260.90 0.0000 Page 3365 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 37.0801 355.39 0.0000 584.27 31.0475 264.80 37.0859 356.01 26.5422 595.83 0.0000 265.00 35.5482 364.49 0.0000 427.87 32.8254 268.22 38.3849 366.42 0.0000 602.52 0.0000 269.46 38.4352 372. 51 29.8994 604.72 20.9359 270.03 38.4584 375.05 35. 9545 . 607.14 25.4564 271.23 46.6748 377.52 35.1685 609.32 15.9915 273.65 0.0000 356.01 31. 8993 610.33 19.5008 276.40 46.9275 388.16 21.6273 614.28 18.0396 277.37 46.9751 388.63 0.0000 618.01 18.0754 277.60 46.9861 391.69 26.8929 620.36 21.1154 278.00 43.8719 264.66 27.0815 621.93 18 .1143 279.20 40.7890 401.81 34.9748 630.19 0.0000 279.54 34.5254 402.40 31.4912 631.29 12.1362 279.70 34.5308 404.85 29.7977 633.25 22.2730 280.46 45.5538 410.95 33.0177 634.78 0.0000 283.69 39.0062 413.71 27.7926 635.95 19.2636 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 42.6270 423.72 0.0000 645.85 16.3060 285.90 0.0000 427.09 29.4067 657.76 29.2248 287.50 46.2756 427.87 29.4235 657.90 0.0000 290.67 38.0908 433.94 29.5538 661. 66 24.6592 293.27 0.0000 439.40 29.6699 664.57 0.0000 351. 93 40.6541 453.88 24.5248 666.33 0.0000 295. 96 40.6842 463.37 22.8577 666.50 0.0000 879.38 51.1849 468.07 26.4164 667.71 0.0000 299.98 44.4479 473.00 0.0000 677.62 21. 7 520 300.09 44.4524 475.06 31.3334 685.70 0.0000 300.13 44.4547 476.78 34.1380 695.00 0.0000 301.36 54.1310 477.60 30.4635 696.49 24.0463 302.85 37.3442 482.18 33.3347 696. 51 24.0472 256.23 37.4028 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.0566 306.78 49.5771 497.08 28.9862 697.49 23.0125 308.46 35.1225 505.52 35.2547 702.65 23.0706 311. 90 34.0225 507.63 0.0000 706.68 23 .1154 316.51 35.3898 511. 00 23.5850 711. 68 21.0645 319.41 0.0000 514.00 18.4312 720.70 0.0000 320.08 0.0000 514.00 18.4312 721. 93 0.0000 321. 04 34.3130 520.40 25.6223 722.78 23.8229 323.87 45.8703 520.69 0.0000 722.91 27. 0014 325.23 36.0857 522.65 0.0000 723.31 27.0066 328.76 0.0000 527.90 0.0000 724.19 20.6608 333.37 33.0469 528. 2 6 22.8867 727. 33 14.3245 333.97 47.9439 529.59 22.9053 733.00 12.7671 334.37 56.2295 529.87 0.0000 735.93 17.5789 338.28 41. 0748 531.02 0.0000 333.97 15.9918 338.32 41. 0758 537.26 0.0000 739.50 0.0000 311. 90 41.1543 546.56 0.0000 747.24 13.9225 340.48 41.1543 552.55 20.3215 748.06 18.2133 340.55 0.0000 563.25 22.3973 752.31 16.1023 344.28 30.0300 569.33 19.5451 753.82 0.0000 345.93 31.7440 946.00 19.5475 756.73 17.7481 351. 06 38. 5972 569.70 17.5942 756.80 17.7488 351.93 38.6263 583.19 30.5371 884.68 22.6628 Page 3366 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 34.5625 1274.44 12.4427 1620;50 6.3875 766.42 25.9287 1001. 03 15 .1349 1621.92 8.5195 766.84 20.5308 1002.74 17.8168 1678.03 0.0000 772.60 0.0000 1004.73 20.5033 1690.97 2.1642 77 6. 52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.10 00 778.90 20.8594 1028.54 0.0000 1063.66 12.1145 783.70 0.0000 1037.84 18.7599 1771.35 5.5081 785.37 15.2538 1038.76 0.0000 1791.20 0.0000 792.07 6.5566 631.29 14.4746 1808.65 4.4421 794.95 16.4124 1048. 07 0.0000 1810. 72 0.0000 795.86 16.4191 1049.04 9. 9600 1836.06 2 . 2.3 4 0 810.06 13.2163 1050.41 9.0588 810.29 16.5216 1063.66 12.7396 344.28 16.5228 1077.00 0.0000 810.76 17.6270 1077.34 13. 7137 815.77 0.0000 1085.87 20.1711 1048.07 0.0000 1093.63 15.6273 832.01 18.8981 1099.45 . 11. 9733 834.85 13. 3560 1112. 07 13.8730 835.71 17.8145 1112*. 84 16.6509 836.80 0.0000 1115.54. 23.7031 846.75 0.0000 1120.29 17.6188 846.77 15.6594 1120.55 17.6212 856.80 0.0000 1221.41 17.6246 860.56 19.1236 1129.67 19.5337 871.09 12.4269 1131.51 0.0000 873.19 18. 0911 1147.95 0.0000 875.33 . 0. 0000 1173.23 15.0898 879.38 14.7356 1177.95 18.8904 880.51 13.6084 1189.05 17.0607 883.24 13.6230 1204.77 26.6670 884.68 15.9027 1221.41 10.7208 889.28 10.2422 1231. 02 15.3604 894.76 5.1321 1235.36 0.0000 898.04 20.5554 1238.28 12. 5073 900.72 16.0041 1260.41 0.0000 903.28 13.7314 1271.87 13.6035 911'.20 11.4787 1274.44 10.6965 912.08 11. 4823 1274.54 10. 6965 923.98 0.0000 1291. 59 11. 72 68 926.50 12. 7013 1298.22 0.0000 929.11 19.0707 1312 .11 0.0000 937.49 9.2760 1332.49 6.9205 944.13 0.0000 1362.66 0.0000 946.00 11. 6325 1365.19 3.9907 949.00 15.1392 1368.63 0.0000 667.71 0.0000 1384.29 3.0086 962. 31 12.6400 1408.01 5.0464 964.08 8.4322 1457.56 0.0000 966.17 7.0322 1460.82 5 .1169 911. 20 8.4475 1489.16 6.1853 968. 97 8.4475 1505.03 3.1051 983.53 0.0000 1584.12 2 .1107 984.45 0.0000 1596.21 0.0000 ;', Page 3367 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:12:49.63 ********************************************************************************
  • GEL. Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621352.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM06.CNF;499 Background date : Z-OCT-2016 11:00:12. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 08:54:28. Sample ID G1203621352 Sample quantity : 1.15000E+02 GRAM Detector name GAM06 Detector geometry: CAN Elapsed live time: 0 00:15:00.00 Elapsed real time: 0 00:15:04.93 0.5% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596247 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 0 9 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 Energy 46.45* 57.98 59.52 79.75 88.05 122.00 176.42 207.48 263.19 344.80 422.27 624.76 652.88 661. 31 682.16 868.77 1004.49 1061.17 1070.41 1116. 07 1172.55 1331. 71 1447.49 1449.99 1494.41 1502.94 1559.77 1628 .13 1681. 09 1701.37 1741.41 1771.88 BACKGROUND CORRECTED SAMPLE PEAK *REPORT Area 5184 523 14681 39 2683 183 33 45 46 51 87 4 40 11922 40 65 51 22 51 129 7331 6678 17 19 11 19 10 9 9 7 12 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 5306 1986 1748 920 1645 893 496 455 538 355 507 431 218 534 198 373 391 263 227 276 305 136 11 7 15 4 6 12 6 16 3 0 0.95 1. 73 0.94 0.73 1. 02 0.97 1.25 0.62 1. 46 1.25 2.45 2. 97 1. 35 1. 47 1. 27 4.15 3.20 0.95 2.08 3.81 1. 87 2.00 2.03 2.03 3.00 1. 01 0.63 1.10 1. 40 1. 44 0.78 1. 00 92.64 115.68 118.76 159.19 175.76 243.61 352.38 414.45 525.79 688.90 843.76 1248.56 1304.78 1321.64 1363.33 1736.45 2007.88 2121.24 2139.72 2231.04 2344.00 2662.38 2894.00 2899.00 2987.87 3004.95 3118. 66 3255.44 3361.40 3401. 99 3482 .11 3543.09 87 113 113 157 170 240 351 413 524 686 841 1237 1301 1314 1359 1730 2001 2118 2134 2225 2338 2653 2889 2889 2976 2998 3111 3250 3356 3396 3476 3539 11 5.76E+00 3.1 12 5.81E-01 11.5 2.22E+OO 12 1. 63E+Ol 1. 0 6 4.33E-02123.8 12 2.98E+OO 3.6 8 2.03E-01 29.3 6 3.71E-02106.6 5 5.02E-02 72.0 7 5.13E-02 84.4 6 5.69E-02 60.0 8 9.63E-02 46.4 13 3.90E-03***** 7 4.42E-02 63.7 16 1. 32E+Ol 1. 0 8 4.42E-02 63.4 12 7.18E-02 61.2 13 5.64E-02 81.9 9 2.46E-02133.3 10 5.66E-02 57.6 12 1.43E-01 27.5 16 8.15E+00 1.3 18 7. 42E+OO 1. 3 19 1.89E-02 36.1 1.24E+OO 19 2.15E-02 38.0 14 1.27E-02 75.6 14 2.16E-02 30.5 12 1.15E-02 56.5 12 1.00E-02 83.9 9 1. 02E-02 59. 7 13 8.07E-03119.9 11 1.37E-02 38.4 9 1.22E-02 30.2 Flag: "*" = Peak area was modified by background subtraction Page 3368 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:12:51 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621352.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 Gl203621352 SOLID GAMMA6 0 00:15:00.00 1.50 keV No Empirical 75.00 Acquisition date : Sample quantity Sample geometry :. Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 08:54:28 115. 00 GRAM CAN 0 00:15:04.93 10.00 0.00 % Peak Energy 0.5% No interference correction performed Page 3369 of 5809 Nuclide Line Activity Report Sample ID : Gl203621352 Nuclide Type: Nuclide Energy Area C0-57 122.Q6 192 136.47 ------C0-60 1173.23 6983 1332.49 6325 ZN-65 1115.54 123 CD-109 88.03 2848 SN-126 64.28 ------86.94 2848 87.57 2848 BA-137M 661. 66 11644 CS-137 661. 66 11644 PM-147 121. 22 192 PB-210 46.54 5644 AM-241 59.54 15831 Flag: "*" Key line Page 3370 of 5809 %Abn 85.60* 10.68 99.85 99.98* 50.60* 3.70* 9.60 8.90 37.00* 89.90* 85.10* 0.00* 4.25* 35.90* Acquisition date Page : 2 3-0CT-2016 08:54:28 Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCi7GRAM %Error 6.177E+OO 9.479E-01 11. OOlE+OO 58.57 6.083E+OO ------Line Not Found ------1. 227E+OO 1. 488E+02 1.500E+02 2.57 1.092E+OO 1. 513E+02 1.525E+02 2.58 l.284E+OO 4.950E+OO 5.260E+OO 55.01 5.256E+OO 3.825E+02 3.950E+02 7.21 2. 772E+OO ------Line Not Found ------5.256E+OO 1.590E+02 l.590E+02 7.21 5.256E+OO 3.825E+Ol 3.825E+Ol 7.21 2.028E+00 l.667E+02 l.670E+02 2.03 2.028E+OO 1. 762E+02 1. 7 64E+02 2.03 6.177E+OO 2.847E+04 2.892E+04 58.57 6.123E-01 5.664E+03 5.674E+03 6.13 2.129E+OO 5.410E+02 5.410E+02 1. 91

... VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:12:52.47 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621352.CNF;l *
  • Acquisition date 3-0CT-2016 08:54:28 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:04.93 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
  • Sample ID G1203621352 Sample Quantity l.1500E+02 GRAM *
  • Batch Number 1596247 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM C0-57 1.00lE+OO 5.745E-01 5.328E-01 C0-60 l.525E+02 3.856E+00 8.177E-01 ZN-65 5.260E+OO 2.836E+OO 3.052E+OO CD-109 3.950E+02 2.790E+Ol l.577E+Ol SN-126 3.825E+Ol 2.702E+OO 1.536E+OO BA-137M l.670E+02 3.319E+OO 9.844E-01 CS-137 1. 764E+02 3.506E+OO 1.040E+OO PM-147 2.892E+04 l.660E+04 1.538E+04 PB-210 5.674E+03 3. 411E+02 1. 962E+02 AM-241 5.410E+02 1.014E+Ol 5. 631E+OO Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -l.880E+OO 6.849E+OO 1.196E+Ol NOT IDENT. NA-22 -2.590E-01 3.644E-01 6.230E-01 NOT IDENT. NA-24 O.OOOE+OO 6. 071E+09 O.OOOE+OO SHORT HLIF AL-26 l.211E-01 3.017E-01 6.159E-01 NOT IDENT. K-40 -4.385E-01 2.341E+OO 4.489E+OO NOT IDENT. SC-46 -l.583E-01 9.402E-01 1.566E+OO NOT IDENT. V-48 1.084E+OO 1.883E+OO 3. 451E+OO NOT IDENT. CR-51 3.819E+OO 6.398E+OO l.185E+Ol NOT IDENT. MN-54 -4.769E-01 7.182E-01 1.177E+OO NOT IDENT. C0-56 2.905E-01 8.260E-01 l.421E+OO FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-58 6.436E-01 7.617E-01 1. 351E+OO NOT IDENT. FE-59 1. 725E+OO 2.102E+OO 3.847E+OO NOT IDENT. GE-68 l.399E+Ol 2.657E+Ol 4.826E+Ol NOT IDENT. AS-73 l.201E+OO 2.460E+Ol 4.445E+Ol NOT IDENT. AS-74 -2.402E-02 1.812E+OO 3.171E+OO NOT IDENT. SE-75 5.714E-01 9.449E-01 1. 2 0 6E+OO FAIL ABUN BR-77 -3.457E+02 7.879E+02 1. 299E+03 NOT IDENT. SR-82 3.582E+00 6.844E+OO 1.202E+Ol NOT IDENT. RB-83 6.686E-01 l.276E+OO 2.292E+OO NOT IDENT. Page 3371of5809 KR-85 4.941E+Ol 1.076E+02 1.932E+02 NOT IDENT. SR-85 2.804E-01 6.088E-01 1.093E+OO NOT IDENT. RB-86 1.695E+Ol 2.054E+Ol 3.776E+Ol NOT IDENT. Y-88 -6.479E-02 3.626E-01 6.643E-01 NOT IDENT. Y-91 -7.015E+Ol 2.336E+02 4.149E+02 NOT IDENT. NB-94 -2.860E-01 5.000E-01 8.385E-01 NOT IDENT. NB-95 -2.712E-01 7.392E-01 1.242E+OO NOT IDENT. NB-95M -6.750E-01 1.829E+OO 3.021E+OO NOT IDENT. ZR-95 4.638E-01 1.240E+OO 2*. l 73E+OO NOT IDENT. .NB-97 O.OOOE+OO 8.509E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.297E+l0 O.OOOE+OO SHORT HLIF M0-99 -l.167E+03 l.028E+03 1.661E+03 NOT IDENT. TC-99M O.OOOE+OO 1.244E+25 O.OOOE+OO SHORT HLIF RH-101 -4.632E-02 3.549E-01 6.178E-01 NOT IDENT. RH-102 3.279E-01 8.920E-01 1. 58 OE+OO NOT IDENT. RU-103 9.859E-02 7.754E-01 l.374E+OO NOT IDENT. RH-106 4.659E-01 5.185E+OO 9.070E+OO NOT IDENT. RU-106 4.659E-01 5.185E+OO 9.070E+OO NOT IDENT. AG-108M 4.513E-02 5.714E-01 l.016E+00 NOT IDENT. AG-110M -3.650E-01 1.089E+00 1.803E+OO NOT IDENT. SN-113 -1.085E-01 7.783E-01 1.387E+OO NOT IDENT. CD-115 -2.673E+02 1.305E+03 2.279E+03 NOT IDENT. SN-117M 3.390E-01 8.872E-01 1.550E+OO NOT IDENT. TE-123M 1.288E-01 3.457E-01 6.040E-01 NOT IDENT. SB-124 8.470E-03 6.127E-01 1.222E+OO NOT IDENT. SB-125 -6.472E-01 l.680E+OO 2.950E+OO FAIL ABUN TE-125M 3.835E+Ol 1.170E+02 2.085E+02 NOT IDENT. I-126 -1. 72'4E+00 5. lOlE+OO 7. 724E+OO NOT IDENT. SB-126 1. 511E+OO 3.208E+OO 5.669E+OO NOT IDENT. SB-127 -3.088E+Ol 7.078E+Ol 1.060E+02 NOT IDENT. I-131 8.704E-01 3.204E+OO 5.820E+OO FAIL ABUN I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 -1. 951E+Ol 4.099E+Ol 6. 7 61E+Ol NOT IDENT. BA-133 -9.641E-02 6. 541E-01 1.175E+OO FAIL ABUN I-133 O.OOOE+OO l.400E+07 O.OOOE+OO SHORT HLIF CS-134 -1.044E-01 7.186E-01 1.217E+00 NOT IDENT. CS-135 -2.920E-01 2.333E+OO 3.855E+00 NOT IDENT. I-135 O.OOOE+OO 3.793E+23 O.OOOE+OO SHORT HLIF CS-136 2.977E+OO 3.047E+OO 5.642E+00 FAIL ABUN CE-139 1.644E-01 3.677E-01 6.421E-01 NOT IDENT. BA-140 l.513E+OO 5.983E+OO 1.065E+Ol FAIL ABUN LA-140 -2.759E-01 8.810E-01 1.605E+OO NOT IDENT. CE-141 7.074E-02 8.172E-01 1. 421E+OO NOT IDENT. CE-143 O.OOOE+OO 4.321E+04 O.OOOE+OO SHORT HLIF CE-144 -1.056E+OO 2.320E+OO 3.980E+OO FAIL ABUN PM-144 l.240E-01 5.391E-01 9.429E-01 NOT IDENT. PR-144 9.313E+OO 4.048E+Ol 7.080E+Ol NOT IDENT. PM-146 6.184E-01 8.485E-01 1.532E+OO NOT IDENT. ND-147 -9.575E+OO 1.364E+Ol 2.330E+Ol NOT IDENT. PM-149 -4.503E+03 9.654E+03 1.566E+04 NOT IDENT. EU-150 -1.570E-02 4.035E-01 7.303E-01 NOT IDENT. EU-152 1.510E+OO 1. 776E+OO 2.717E+OO FAIL ABUN GD-153 2.130E-01 9.702E-01 l.732E+00 NOT IDENT. EU-154 -7.977E-01 1. 021E+OO 1 .. 730E+OO FAIL ABUN EU-155 -6.607E-01 1.193E+OO 2.070E+OO FAIL ABUN TB-160 6.482E-01 2. 996E+OO 5.094E+OO FAIL ABUN H0-166M -9.997E-03 9.507E-01 1. 641E+OO FAIL ABUN TM-171 -2.081E+OO 4.953E+02 8.951E+02 NOT IDENT. HF-172 -7.571E-01 2.330E+OO 3.720E+OO FAIL ABUN LU-172 -7.722E-01 1.308E+OO 2.266E+OO FAIL ABUN LU-176 -l.151E-01 3.856E-01 6. 963E-01 FAIL ABUN HF-181 -6.184E-01 9.069E-01 1.561E+OO FAIL ABUN TA-182 -5.438E-02 1.912E+OO 3.480E+OO NOT IDENT. RE-183 O.OOOE+OO 6.232E+OO 1.224E+Ol FAIL ABUN RE-184 2.127E+00 3.138E+OO 5.420E+OO NOT IDENT. W-188 1. 266E+02 1.178E+02 2.030E+02 NOT IDENT. IR-192 -2.490E-01 5.280E-01 9.467E-01 NOT IDENT. HG-203 9.750E-02 6.268E-01 1.045E+OO NOT IDENT. BI-207 :....4.066E-01 1. 2 67E+OO 1. 816E+OO NOT IDENT. TL-208 -4.466E-02 5. 571E-01 9.726E-01 NOT IDENT. BI-211 7.282E-01 3.057E+OO 5.566E+OO NOT IDENT. PB-211 -1.244E+Ol 1.190E+Ol 2.052E+Ol NOT IDENT. BI-212 9.954E-01 7.923E+OO 1.374E+Ol NOT IDENT. PB-212 2.726E-01 8.007E-01 1.360E+OO NOT IDENT. BI-214 -3.289E-01 1.084E+OO 1.867E+OO NOT IDENT. PB-214 -3.957E-01 1.115E+OO l.990E+00 FAIL ABUN RN-219 2.822E+OO 6.745E+OO 1.223E+Ol NOT IDENT. RN-222 -3.289E-01 1.084E+OO 1.867E+OO NOT IDENT. Page 3372 of 5809 RA-223 3.803E+OO 9.421E+OO 1. 733E+Ol FAIL ABUN RA-224 1. 718E+OO 8.628E+OO l.455E+Ol NOT IDENT. RA-226 -3.289E-01 1.084E+OO l.867E+OO NOT IDENT. AC-227 -8.529E-01 3.698E+OO 6. llOE+OO FAIL ABUN TH-227 -8.529E-01 3.698E+OO 6. llOE+OO FAIL ABUN AC-228 2.703E-01 3.166E+OO 5.319E+OO NOT IDENT. RA-228 2.703E-01 3.166E+OO 5.319E+OO NOT IDENT. TH-228 2.726E-01 8.007E-01 1.360E+OO NOT IDENT. TH-229 -5.997E+OO 6.993E+OO l.152E+Ol FAIL ABUN TH-230 -3.289E-01 *I 1.084E+OO 1. 8 67E+OO NOT IDENT. PA-231 -7.971E+OO 6.634E+OO l.165E+Ol NOT IDENT. TH-231 3.803E+00 9.421E+OO 1.733E+Ol FAIL ABUN TH-232 2.703E-01 3.166E+OO 5.319E+OO NOT IDENT. PA-233 3.978E-01 9.528E-01 1. 757E+OO NOT IDENT. PA-234 4.267E+OO 6.913E+OO 1.263E+Ol NOT IDENT. PA-234M 3.551E+Ol 1.052E+02 1. 691E+02 NOT IDENT. TH-234 -2.388E+OO 1. 776E+Ol 2.978E+Ol NOT IDENT. U-234 -3.289E-01 1.084E+OO l.867E+OO NOT IDENT. U-235 -9.497E-01 2.290E+OO 3.917E+OO NOT IDENT. NP-237 3.978E-01 9.528E-01 1.757E+OO NOT IDENT. NP-238 O.OOOE+OO 3.268E+03 0.000E+OO SHORT HLIF U-238 -2.388E+OO 1. 776E+Ol 2.978E+Ol NOT IDENT. NP-239 4.059E-01 3.137E+00 5.528E+OO NOT IDENT. PU-239 -1.314E+03 3.882E+03 6.699E+03 NOT IDENT. AM-243 l.423E-02 6.129E-01 1.101E+OO NOT IDENT. CM-243 7.317E-02 1. 201E+OO 2.129E+OO NOT IDENT. BK-247 -4.071E-01 1.382E+OO 2.082E+OO NOT IDENT. CM-247 1. 264E-01 6.125E-01 1.103E+OO NOT IDENT. CF-249 3. 441E-02 6.706E-01 1.204E+OO NOT IDENT. CF-251 9.590E-01 2.005E+OO 2.687E+OO FAIL ABUN ANH-511 1. 798E-01 4.890E-01 8.844E-01 NOT IDENT. Page 3373 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:12:50.44 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 192 85.60* 6.177E+OO 9.479E-01 1. OOlE+OO 58.57 136.47 ------10.68 6.083E+OO ------Line Not Found ------C0-60 1173.23 6983 99.85 1.227E+OO l.488E+02 1.500E+02 2.57 1332.49 6325 99.98* 1.092E+OO l.513E+02 1.525E+02 2.58 ZN-65 1115. 54 123 50.60* 1.284E+OO 4.950E+00 5.260E+OO 55.01 CD-109 88.03 2848 3.70* 5.256E+OO 3.825E+02 3.950E+02 7.21 SN-126 64.28 ------9.60 2. 772E+OO ------Line Not Found ------86.94 2848 8.90 5.256E+OO 1.590E+02 l.590E+02 7.21 87.57 2848 37.00* 5.256E+OO 3.825E+Ol 3.825E+Ol 7.21 BA-137M 661.66 11644 89.90* 2.028E+OO 1.667E+02 1. 670E+02 2.03 CS-137 661. 66 11644 85.10* 2.028E+OO 1. 762E+02 l.764E+02 2.03 PM-147 121.22 192 0.00* 6.177E+OO 2.847E+04 2.892E+04 58.57 PB-210 46.54 5644 4.25* 6.123E-01 5.664E+03 5.674E+03 6.13 AM-241 59.54 15831 35.90* 2.129E+OO 5.410E+02 5.410E+02 1. 91 Flag: "*" Key line Page 3374 of 5809 Summary of Nuclide Activity Sample ID : Gl203621352 Acquisition date Page : 2 3-0CT-2016 08:54:28 Total number of lines in spectrum 32 Number of unidentified lines 16 Number of lines tentatively identified by NID 16 50.00% Nuclide Type : Uncorrected Decay Corr Decay Corr 2-Sigma Nuclide Hlife Decay pCi/GRAM pCi/GRAM 2-Sigma Error %Error Flags C0-57 271. 74D 1. 06 9.479E-01 1. OOlE+OO 0.586E+OO 58.57 C0-60 5.27Y 1. 01 1. 513E+02 l.525E+02 0.039E+02 2.58 ZN-65 244.06D 1. 06 4.950E+OO 5. 2 60E+OO 2.894E+00 55.01 CD-109 461.40D 1. 03 3.825E+02 3.950E+02 0.285E+02 7.21 SN-126 2.30E+05Y 1. 00 3.825E+Ol 3.825E+Ol 0.276E+Ol 7.21 BA-137M 30.08Y 1. 00 1. 667E+02 1.670E+02 0.034E+02 2.03 CS-137 30.08Y 1. 00 1. 762E+02 l.764E+02 0.036E+02 2.03 PM-147 2.62Y 1. 02 2.847E+04 2.892E+04 l.693E+04 58.57 PB-210 22.20Y 1. 00 5.664E+03 5.674E+03 0.348E+03 6.13 AM-241 432.60Y 1. 00 5.410E+02 5.410E+02 0.103E+02 1. 91 ------------------Total Activity 3.560E+04 3.607E+04 Grand Total Activity 3.560E+04 3.607E+04 Flags: "K" Keyline not found "M" Manually accepted "E" = Manually edited "A" = Nuclide specific abn. limit Page 3375of5809 Unidentified Energy Lines Page : 3 Sample ID : G1203621352 Acquisition date : 3-0CT-2016 08:54:28 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 9 57.98 565 2144 1. 73 115. 68 113 12 5.81E-01 23.0 1.92E+OO T 0 79.75 42 981 0.73 159.19 157 6 4.33E-02 **** 4.59E+OO T 0 176.42 35 512 1. 25 352.38 351 6 3.71E-02 **** 5.43E+OO T 0 207.46 46 466 0.62 414.45 413 5 5.Q2E-02 **** 4.90E+OO 0 263.19 47 546 1. 46 525.79 524 7 5.13E-02 **** 4.12E+OO T 0 344.80 51 356 1. 25 688.90 686 6 5.69E-02 **** 3.36E+OO T 0 422.27 86 505 2.45 843.76 841 8 9.63E-02 92.8 2.88E+OO T 0 624. 7 6 3 422 2.97 1248.56 1237 13 3.90E-03 **** 2.12E+OO 0 652.88 39 213 1. 35 1304.78 1301 7 4.42E-02 **** 2.05E+OO 0 682.16 39 193 1. 27 1363.33 1359 8 4.42E-02 **** 1.98E+OO 0 868.77 62 360 4.15 1736.45 1730 12 7.18E-02 **** 1. 61E+OO 0 1004.49 49 375 3.20 2007.88 2001 13 5.64E-02 **** 1. 41E+00 T 0 1061.17 21 251 0.95 2121.24 2118 9 2.46E-02 **** l.35E+OO 0 1070.41 49 217 2.08 2139.72 2134 10 5.66E-02 **** 1.33E+OO 1 1447.49 16 10 2.03 2894.00 2889 19 1. 89E-02 72 .2 1. OlE+OO 1 1449.99 18 6 2.03 2899.00 2889 19 2.15E-02 76.0 1. OlE+OO 0 1494.41 11 14 3.00 2987.87 2976 14 l.27E-02 **** 9.85E-01 0 1502.94 18 3 1. 01 3004.95 2998 14 2.16E-02 61. 0 9.80E-01 0 1559.77 10 5 0.63 3118. 66 3111 12 1. 15E-02 **** 9.49E-01 0 1628.13 8 11 1.10 3255.44 3250 12 1.00E-02 **** 9.15E-01 0 1681. 09 9 5 1. 40 3361. 40 3356 9 1. 02E-02 **** 8.92E-01 0 1701.37 7 15 1. 44 3401.99 3396 13 8.07E-03 **** 8.84E-01 0 1741.41 12 2 0.78 3482 .11 3476 11 1.37E-02 76.8 8.68E-01 0 1771.88 10 0 1. 00 3543.09 3539 9 1.22E-02 60.3 8.56E-01 T Flags: "T" = Tentatively associated Page 3376 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:13:04.08 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA '* * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621352.CNF;l *
  • Acquisition date 3-0CT-2016 08:54:28 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:04.93 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID Gl203621352 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.1500E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are vaiid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M CS-137 PM-147 PB-210 AM-241 Le (pCi/GRAM 2.593E-01 3.765E-01 1.469E+OO 7.698E+OO 7. 496E-01 4.730E-01 4. 996E-01 7.486E+03 9.676E+Ol 2.770E+OO ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54. C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 Page 3377 of 5809 Le (pCi/GRAM 5. 811E+OO 2.801E-01 O.OOOE+OO 2.663E-01 1.917E+OO 7.565E-01 1.664E+OO 5.753E+OO 5.664E-01 6.848E-01 O.OOOE+OO 6.504E-01 1.858E+OO 2.327E+Ol 2.192E+Ol 1.523E+OO 5.866E-01 6.322E+02 5.778E+OO 1.109E+OO 9.332E+Ol NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 Page 3378of5809 5.282E-01 1.821E+Ol 2.835E-01 1.930E+02 4. 011E-01 5. 962E-01 1.471E+00 1.042E+OO O.OOOE+OO O.OOOE+OO 7. 965E+02 0.000E+OO 3.004E-01 7.598E-01 6.652E-01 4.363E+OO 4.363E+OO 4.942E-01 8.694E-01 6.736E-01 1.099E+03 7.540E-01 2.937E-01 5.045E-01 1.433E+OO 1.014E+02 3. 696E+00 2. 720E+OO 5.076E+Ol 2.825E+OO O.OOOE+OO 3.291E+Ol 5.700E-01 O.OOOE+OO 5.843E-01 1. 874E+OO O.OOOE+OO 2. 722E+OO 3.123E-01 5.132E+OO 6.763E-01 6.910E-01 O.OOOE+OO 1.935E+OO 4.526E-01 3.398E+Ol 7.460E-01 1.122E+Ol 7.594E+03 3.545E-01 1.319E+OO 8.437E-01 7.761E-01 1.007E+OO 2.458E+OO 7.866E-01 4. 413E+02 1.808E+OO 1.090E+OO 3.379E-01 7.570E-01 1.615E+OO 6.057E+00 2.621E+OO 9.869E+Ol 4.589E-01 5.076E-01 8.733E-01 4.680E-01 2.701E+OO 9.949E+OO 6.592E+OO 6.619E-01 8.982E-01 9.651E-01 5.936E+OO 8.982E-01 8.413E+00 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF

  • NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3379 of 5809 7.078E+OO 8.982E-01 2. 967E+OO 2.967E+OO 2. 572E+OO 2. 572E+OO 6.619E-01 5.603E+OO 8.981E-01 5.64,9E+OO 8.413E+OO 2.572E+OO 8.532E-01 6.120E+OO 8 .161E+Ol l.453E+Ol 8. 981E-01 1.905E+OO 8.532E-01 O.OOOE+OO 1.453E+Ol 2.692E+OO 3.258E+03 5.374E-01 1. 036E+OO 1.012E+OO 5.353E-01 5.845E-01 1.306E+OO 4.282E-01 NOT IDENT. NOT*IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:13:09.17 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621352.CNF;l *
  • Acquisition date 3-0CT-2016 08:54:28 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:04.93 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621352 Analyst initials: MXRl *
  • Batch Number 1596247 Sample Quantity : 1.1500E+02 GRAM *
  • Quantity Err(%): 1.7391E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M CS-137 PM-147 PB-210 AM-241 1.00lE+OO l.525E+02 5.260E+00 3.950E+02 3.825E+Ol 1.670E+02 1. 764E+02 2.892E+04 5.674E+03 5.410E+02 Act Error ( 1. 96-sigma) 5.791E-01 1.247E+Ol 2.986E+OO 4.779E+Ol 4.161E+OO 1.418E+Ol 1.497E+Ol 1.673E+04 5.985E+02 4.310E+Ol Non-Identified Nuclides Key-Line Activity K.L Act error Nuclide (pCi/GRAM ( 1 . 96-sigma ) BE-7 -1.880E+OO 6.851E+OO NA-22 -2.590E-01 3.650E-01 NA-24 5.870E+08 6. 071E+09 AL-26 1. 211E-01 3.018E-01 K-40 -4.385E-01 2.341E+OO SC-46 -1.583E-01 9.404E-01 V-48 1.084E+OO 1.889E+00 CR-51 3.819E+OO 6. 40'8E+00 MN-54 -4.769E-01 7.202E-01 C0-56 2.905E-01 8.267E-01 MN-56 l.000E+41 2.766E+41 C0-58 6.436E-01 7.648E-01 FE-59 1. 725E+OO 2.126E+OO GE-68 1.399E+Ol 2.667E+Ol AS-73 1.201E+OO 2.461E+Ol AS-74 -2.402E-02 l.812E+OO SE-75 5.714E-01 9.464E-01 BR-77 -3.457E+02 8 .168E+o2 SR-82 3.582E+OO 6.854E+OO RB-83 6.686E-01 1.281E+OO Page 3380 of 5809 TPU ( 1. 96-sigma) 5. 791E-01 1.247E+Ol 2.986E+OO 4.779E+Ol 4.161E+OO 1.418E+Ol l.497E+Ol 1.673E+04 5.985E+02 4.310E+Ol TPU ( 1. 96-sigma) 6.903E+OO 3.833E-01 6.077E+09 3.067E-01 2.350E+OO 9.432E-01 1.952E+OO 6.635E+OO 7.516E-01 8.370E-01 O.OOOE+OO 8.180E-01 2.264E+OO 2. 741E+Ol 2.461E+Ol 1.812E+OO 9.809E-01 8.315E+02 7.041E+OO 1.316E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

KR-85 4.941E+Ol 1.076E+02 1.099E+02 NOT IDENT. SR-85 2.804E-01 6.092E-01 6.222E-01 NOT IDENT. RB-86 1.695E+Ol 2.073E+Ol 2.210E+Ol NOT IDENT. Y-88 -6.479E-02 3.626E-01 3.638E-01 NOT IDENT. Y-91 -7.015E+Ol 2.337E+02 2.358E+02 NOT IDENT. NB-94 -2.860E-01 5.006E-01 5.170E-01 NOT IDENT. NB-95 -2.712E-01 7.397E-01 7.497E-01 NOT IDENT. NB-95M -6.750E-01 1.831E+OO 1.856E+OO NOT IDENT. ZR-95 4.638E-01 1.241E+OO 1.258E+OO NOT IDENT. l.000E+41 8.549E+40

  • O.OOOE+OO SHORT HLIF ZR-97 -5.794E+09 1.298E+10 1.324E+10 SHORT HLIF M0-99 -l.167E+03 l.034E+03 1.160E+03 NOT IDENT. TC-99M -9.070E+24 1.248E+25 O.OOOE+OO SHORT HLIF RH-101 -4.632E-02 3.551E-01 3.557E-01 NOT IDENT. RH-102 3.279E-01 8.927E-01 9.049E-01 NOT IDENT. RU-103 9.859E-02 7.754E-01 7.767E-01 NOT IDENT. RH-106 4.659E-01 5.185E+OO 5.189E+OO NOT IDENT. RU-106 4.659E-01 5.185E+OO 5.189E+OO NOT IDENT. AG-108M 4.513E-02 5.714E-01 5.718E-01 NOT IDENT. AG-llOM -3.650E-01 1.090E+OO 1.103E+OO NOT IDENT. SN-113 -1.085E-01 7.783E-01 7.799E-01 NOT IDENT. CD-115 -2.673E+02 1.305E+03 1. 311E+03 NOT IDENT. SN-117M 3.390E-01 8.875E-01 9.006E-01 NOT IDENT. TE-123M 1.288E-01 3.459E-01 3.507E-01 NOT IDENT. SB-124 8.470E-03 6.127E-01 6.127E-01 NOT IDENT. SB-125 -6. 472E-01 1. 681E+OO 1.706E+00 FAIL ABUN TE-125M 3.835E+Ol 1.170E+02 1.183E+02 NOT IDENT. I-126 -1.724E'+OO 5.103E+OO 5.162E+OO NOT IDENT. SB-126 1. 511E+OO 3.214E+OO 3.285E+OO NOT IDENT. SB-127 -3.088E+Ol 7.089E+Ol 7.225E+Ol NOT IDENT. I-131 8.704E-01 3.204E+OO 3.228E+OO FAIL ABUN I-132 1.000E+41 3.538E+41 O.OOOE+OO SHORT HLIF TE-132 -l.951E+Ol 4.105E+Ol 4.198E+Ol NOT IDENT. BA-133 -9. 641E-02 6.542E-01 6.556E-01 FAIL ABUN I-133 -4.132E+06 1.402E+07 1.414E+07 SHORT HLIF CS-134 -l.044E-01 7.187E-01 7.202E-01 NOT IDENT. CS-135 -2.920E-01 2.333E+OO 2.337E+OO NOT IDENT. I-135 -2.706E+23 4.022E+23 O.OOOE+OO SHORT HLIF CS-136 2.977E+OO 3.092E+OO 3.370E+OO FAIL ABUN CE-139 l.644E-01 3.693E-01 3.767E-01 NOT IDENT. BA-140 1.513E+OO 5.984E+OO 6.023E+OO FAIL ABUN LA-140 -2.759E-01 8. 813E-01 8.900E-01 NOT IDENT. CE-141 7.074E-02 8.172E-01 8.178E-01 NOT IDENT. CE-143 -5.489E+02 4.321E+04 4.321E+04 SHORT HLIF CE-144 -1.056E+OO 2.322E+OO 2.370E+OO FAIL ABUN PM-144 1.240E-01 5.392E-01 5.421E-01 NOT IDENT. PR-144 9.313E+OO 4.048E+Ol 4.070E+Ol NOT IDENT. PM-146 6.184E-01 8.509E-01 8.954E-01 NOT IDENT. ND-147 -9.575E+OO 1.367E+Ol 1.433E+Ol NOT IDENT. PM-149 -4.503E+03 9.680E+03 9.891E+03 NOT IDENT. EU-150 -1.570E-02 4.035E-01 4.036E-01 NOT IDENT. EU-152 1.510E+OO 1. 782E+OO l.908E+OO FAIL ABUN GD-153 2.130E-01 9.703E-01 9.750E-01 NOT IDENT. EU-154 -7.977E-01 1.023E+OO 1.085E+OO FAIL ABUN EU-155 -6.607E-01 1.195E+OO 1. 231E+OO FAIL ABUN TB-160 6.482E-01 2.998E+OO 3.012E+OO FAIL ABUN H0-166M -9.997E-03 9.507E-01 9.507E-01 FAIL ABUN TM-171 -2.081E+OO 4.953E+02 4.953E+02 NOT IDENT. HF-172 -7. 571E-01 2.334E+OO 2.359E+OO FAIL ABUN LU-172 -7. 722E-01 1. 317E+OO 1.362E+OO FAIL ABUN LU-176 -1.151E-01 3.857E-01 3.892E-01 FAIL ABUN HF-181 -6.184E-01 9.085E-01 9.503E-01 FAIL ABUN TA-182 -5.438E-02 1.912E+OO 1.912E+OO NOT IDENT. RE-183 2.763E+Ol 6.890E+OO 1.423E+Ol FAIL ABUN RE-184 2.127E+OO 3.153E+OO 3.295E+00 NOT IDENT. W-188 L266E+02 l.191E+02 1. 321E+02 NOT IDENT. IR-192 -2.490E-01 5.285E-01 5.403E-01 NOT IDENT. HG-203 9.750E-02 6.268E-01 6.284E-01 NOT IDENT. BI-207 -4.066E-01 1.269E+OO 1.282E+OO NOT IDENT. TL-208 -4.466E-02 5.571E-01 5.575E-01 NOT IDENT. BI-211 7.282E-01 3.058E+OO 3.075E+OO NOT IDENT. PB-211 -1.244E+Ol 1.195E+Ol 1.320E+Ol NOT IDENT. BI-212 9.954E-01 7.924E+OO 7.937E+OO NOT IDENT. PB-212 2.726E-01 8. OllE-01 8.105E-01 NOT IDENT. BI-214 -3.289E-01 1.084E+OO 1.094E+OO NOT IDENT. PB-214 -3.957E-01 1.115E+OO 1.129E+OO FAIL ABUN RN-219 2.822E+OO 6.757E+OO 6.876E+OO NOT IDENT. RN-222 -3.289E-01 1.084E+OO 1.094E+OO NOT IDENT. Page 3381 of 5809 RA-223 3.803E+OO 9.430E+OO 9.584E+OO FAIL ABUN RA-224 1.718E+00 8.629E+OO 8.664E+OO NOT IDENT. RA-226 -3.289E-01 1.084E+OO 1.094E+OO NOT IDENT. AC-227 -8.529E-01 3.700E+OO 3.720E+OO FAIL ABUN TH-227 -8.529E-01 3.700E+OO 3. 720E+OO FAIL ABUN AC-228 2.703E-01 3.166E+OO 3.168E+OO NOT IDENT. RA-228 2.703E-01 3.166E+OO 3.168E+OO NOT IDENT. TH-228 2.726E-01 8. OllE-01 8.105E-01 NOT IDENT. TH-229 -5.997E+OO 7.008E+OO 7. 511E+OO FAIL ABUN TH-230 -3.289E-01 1.084E+OO 1.094E+OO NOT IDENT. PA-231 -7.971E+OO 6.881E+OO 7.763E+OO NOT IDENT. TH-231 3.803E+OO 9.430E+OO 9.584E+OO FAIL ABUN TH-232 2.703E-01 3.166E+OO 3.168E+OO NOT IDENT. PA-233 3.978E-01 9.535E-01 9.702E-01 NOT IDENT. PA-234 4.267E+OO 8.481E+OO 8. 696E+OO NOT IDENT. PA-234M 3.551E+Ol l.053E+02 l.065E+02 NOT IDENT. TH-234 -2.388E+OO 1.777E+Ol 1. 780E+Ol NOT IDENT. U-234 -3.289E-01 1.084E+OO 1.094E+OO NOT IDENT. U-235 -9.497E-01 2.291E+OO 2. 331E+OO NOT IDENT. NP-237 3.978E-01 9.535E-01 9.702E-01 NOT IDENT. NP-238 l.944E+03 3.280E+03 3.395E+03 SHORT HLIF U-238 -2.388E+OO 1.777E+Ol 1.780E+Ol NOT IDENT. NP-239 4.059E-01 3.137E+OO 3.142E+00 NOT IDENT. PU-239 -1.314E+03 3.883E+03 3.928E+03 NOT IDENT. AM-243 1. 423E-02 6.129E-01 6.130E-01 NOT IDENT. CM-243 7.317E-02 1.201E+00 l.202E+00 NOT IDENT. BK-247 -4.071E-01 1.385E+OO l.397E+OO NOT IDENT. CM-247 1.264E-0'1 6 .130E-01 6.156E-01 NOT IDENT. CF-249 3.441E-02 6.706E-01 6.708E-01 NOT IDENT. CF-251 9.590E-01 2.008E+OO 2.054E+00 FAIL ABUN ANH-511 1. 7 98E-01 4.893E-01 4.959E-01 NOT IDENT. Page 3382 of 5809
  • GEL Laboratories LLC *
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  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 1964 .1102 87.09 543.0725 136.47 408. 9632 45.60 1653.5233 87.57 543.6205 140.51 429.2876 46.54 1658.5250 88.03 544.1423 143.76 431. 3771 49. 72 1488.5717 88.34 544.4946 144.24 396.9384 51. 35 1543.0040 88.47 544.6424 145.44 411. 3519 51. 87 1583.8177 89. 96 412.7759 152.43 367.5838 52.39 1569.6459 90.64 422.3123 153.25 401. 0778 52.97 1610.8647 91.11 440.6485 154.21 408.0317 53.44 1625.3617 92.59 422.7026 156.02 394.0771 54.07 1638.0039 93.35 411.1242 158.56 394.4007 57.36 0.0000 94.56 434.3693 159.00 389.2594 57.53 1148.3273 94.65 434.4481 162.33 379.1556 57.98 1149.7538 94. 67 434.4652 162.66 376.0849 -59. 27 1153.8312 94.87 434.6365 163.33 398.0583 59.32 1153.9841 97.43 442.6662 165.86 391. 8196 59.54 1154.6753 98.43 438.6497 176.31 369.7046 60. 96 1159 .1030 98.44 438.6601 176.60 387.4492 61.17 1159.7546 99.53 452.2791 177.52 417.2925 62.93 516.2480 100 .11 468.4312 181.07 426.1812 63.29 523.9438 102.03 415 .1772 181.52 429.7448 63.58 517.1239 103.18 427.8779 184.41 455.7509 64.28 549.3857 103.37 428.0305 185. 72 477.6435 66.73 546.4628 105.21 448.2537 193.51 474.3121 67.24 558.9999 105.31 448.3368 197.03 443.5702 67.68 586.0448 106.12 402.5224 198.01 431.6502 67.75 586.1478 106.47 423.5623 201.83 418.8242 69.67 572.4478 109.28 412.7963 203.43 442.3439 70.83 547.4277 111. 00 415.0669 205.31 387.4597 72. 81 551.8744 111.76 438.6048 210.85 501.5160 72.87 567.6429 114. 06 428.3455 215.65 462.3163 74.66 553.3564 116. 30 421. 9538 222 .11 459.7844 74.82 553.5613 116.74 444.4453 227.09 448.2363 74.97 575.0912 119.76 433.5675 227.38 444.8740 77 .11 525.7336 121.12 438.6215 228.16 469. 7811 78.74 586.3143 121.22 438.6940 228.18 469.7933 79.69 557.8715 121.78 439.1027 235.69 464.0754 80.12 558.4072 122.06 439.3070 235. 96 448.8912 80.19 558.4934 122.92 439.9365 238.63 407.5923 80.57 584.9567 123.07 427.8218 238.98 446.7409 81. 00 599.3088 123.68 429.6140 240.99 416.8667 81. 07 599.4012 125.81 416.1079 242.00 406.6216 81. 75 605.3193 127.23 410.2280 244.70 387.5279 83.79 584.0486 127.91 400.4141 252.40 364.1497 84.00 608.2906 129.30 436.2925 252.80 373.8801 85.43 643.0718 131. 20 408.7134 254.15 0.0000 86.55 542.4550 133.02 425.4116 256.23 383. 5511 86.79 542.7246 133.52 430.9233 260.90 365.5590 86.94 542.8986 136.00 400.3504 264.66 452.5277 Page 3383 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 80 452.5847 364.49 350.5050 600.60 203.7072 265.00 428.4145 366.42 365.9636 602.52 0.0000 268.22 398.9092 372.51 352.5831 604.72 217.3263 269.46 392.0739 375.05 325.7884 607.14 209.4534 270.03 387.4072 1093.63 359.1870 609.32 220.8763 271.23 385.4047 3.83.85 359.9358 610.33 232. 1.934 273.65 385.0406 388.16 369.9822 614.28 212.2402 276.40 343.1299 388.63 379.0397 618.01 202.4070 277.37 381.4609 391.69 372.6921 620.36 207.7578 277.60 381.5369 400.66 340.7706 621. 93 207.9147 278.00 374.3156 401.81 343.7465 630.19 0.0000 279.20 363.6677 402.40 342.0808 631.29 196.5180 279.54 400.6453 404.85 386.0566 633.25 212.1441 279.70 400.7050 410.95 411.2686 634.78 190.6608 280.46 361. 6232 413. 71 350.1830 635.95 181.4857 283.69 386.1206 414.70 374.9927 636.99 206.3395 284.31 355.4736 423. 72 407.9309 645.85 220.6790 285.41 391.6548 427.09 381.0308 657.76 209.4159 285.90 358.4555 427.87 403.9958 657.90 0.0000 287.50 367.6336 433.94 419.4254 661. 66 199.3547 290.67 337.6343 439.40 449.5836 664.57 0.0000 293.27 0.0000 453.88 417.3255 666.33 177.3005 295.22 363.9128 463.37 441.3995 666.50 177.3143 295. 96 392.8271 468.07 412.5320 667.71 0.0000 298.58 341.2333 473.00 412.8260 677.62 176.6406 299.98 363.7502 475.06 433.2047 685.70 183.6218 300.09 363.7857 476.78 396.7338 695.00 178.0352 300 .13 363.7946 477.60 401.6665 696.49 181.3326 301.36 395.0905 482.18 368.5732 696. 51 181.3326 302.85 349.5919 487.02 359.1517 697.00 195.1631 304.50 354.2728 492.35 330.6612 697.30 176.0913 304.85 359.4114 497.08 291. 3271 697.49 182.4735 306.78 371.7444 505.52 287.9408 702.65 181. 82 67 308.46 391.6042 507.63 0.0000 706.68 166.1753 311.90 353.9734 511. 00 269.5263 711. 68 178.2801 316.51 351.1019 514.00 246.7615 720.70 169.3376 319.41 362.1230 514.00 246.7615 721. 93 0.0000 320.08 342.7983 520.40 260.2793 722.78 203.8155 321. 04 365.9975 520.69 271.0078 722. 91 208.1221 323.87 349.8250 522.65 0.0000 723. 31 203.8619 325.23 357.0263 527.90 248.7018 724 .19 177.1051 328.76 359.7583 528.26 249.7292 727. 33 178.4216 333.37 372. 2359 529.59 237.2157 733.00 150.8407 333.97 364.6896 529.87 0.0000 735.93 184.4707 334.37 375.1112 531.02 256.9429 737.46 166.2443 338.28 363.3517 537.26 224.4994 739.50 223.6520 338.32 378.8680 546.56 0.0000 747.24 202.7051 340.48 340.5182 552.55 206.6018 748.06 178.9178 340.55 340.5423 563.25 216. 7227 752.31 / 184.6647 344.28 352.9492 569.33 230.3890 753.82 189.1301 345.93 344.3108 569.50 230.4078 756.73 165.4212 351.06 342.6258 569.70 230.4266 756.80 165.4212 351. 93 360.2538 583.19 215.9798 763.94 203.0288 355.39 0.0000 584.27 217.0986 765.81 208.6420 356.01 361. 3740 595.83 199.1723 766.42 204.3258 Page 3384 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 199.9924 1002.74 220.8060 1678.03 0.0000 772.60 0.0000 1004.73 220.9492 1690.97 7.4952 776.52 179.9422 1021.30 0.0000 1750.46 0.0000 777.92 205.2921 1025.87 0.0000 1764.49 8.6982 778.90 183.4105 1028.54 0.0000 1770.23 3.4832 783.70 .202.4704 1037.84 221.5378 ., 1771. 35 1. 7421 785.37 198.2080 1038.76 0.0000 1791.20 0.0000 792.07 220.8252 1046.59 228.4980 1808.65 9.8734 794.95 195.6536 1048.07 210.4624 1810. 72 0.0000 795.86 201. 2546 1049.04 229.5901 1836.06 13.2363 801.95 191. 7670 1050.41 243.3003 810.06 201.2756 1063.66 222.4504 810.29 202.4098 1077.00 207.8109 810.45 182.4046 1077.34 218.8256 810.76 183.5370 1085.87 207.4609 815.77 215.1067 1093.63 233.7222 818.51 201.9458 1099.45 225.8444 832.01 229.9243 1112. 07 256.1380 834.85 248.1394 1112.84 260.6484 835.71 234.7423 1115. 54 219.5403 836.80 0.0000 1120. 29 149.9120 846.75 0.0000 1120. 55 139. 5313 846.77 218.8183 1121. 30 142.5375 856.80 260.4065 1129.67 147.9174 860.56 259.6470 1131. 51 0.0000 871.09 254.4022 1147.95 0.0000 873.19 252.8936 1173.23 156.4254 875.33 0.0000 1177.95 99.6445 879.38 239.7705 1189.05 85.1935 880.51 227.3083 1204.77 65.6098 883.24 257.2632 1221.41 56.3640 884.68 256.2565 1231. 02 39.2733 889.28 278.4573 1235.36 47.9523 894.76 312.3086 1238.28 46.0693 898.04 272.4497 1260.41 0.0000 900. 72 271.5594 1271.87 26.1546 903.28 251.0779 1274.44 37.8051 911.20 279.5171 1274.54 37.8051 912.08 258.8086 1291.59 34.0836 923.98 0.0000 1298.22 0.0000 926.50 272.9045 1312 .11 33.2903 929 .11 303.3849 1332.49 45.2813 937.49 291.4531 1362.66 0.0000 944.13 316.3708 1365.19 14.8901 946.00 296.4102 1368.63 0.0000 949.00 326.5671 1384.29 16.9575 954.55 0.0000 1408.01 17.0591 962. 31 272.4967 1457.56 0.0000 964. 08 302.6686 1460.82 12.1978 966 .17 281. 6951 1489.16 21. 2862 968.97 258.0931 1505.03 11. 5049 983.53 220.2847 1584.12 11.5062 984.45 0.0000 1596.21 12.5867 996.26 240.8478 1620.50 10.5450 1001.03 240.1547 1621. 92 14.0649 Page 3385 of 5809 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 2010 10/03/16 1596249 Batch# ________ _ Gamma Solid MJWC Product:, ________ _ Date: 10/03/16 Criteria: Yes No Comments Sample Solids are less than or equal to 100 m11 for GAB. n/a Samples have been blank corrected (If required). n/a Blank correction reoorted included flf reauJred), If activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. ./ If greater than 10* MDA/ MDC, error Is 400/o or less. If hRlnw th" MDA I Mnr "rrnr '" .. Instrument source check Is within limits. Instrument bka check ls within limit" ./ Method RDL/ LLD has been met. ./ If duolicate activities are: Less than 5* MDA/ MDC, then RPO Is 1000/o or less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO ls 0%, ./ Dr meets the client's reoulred RER accentance criteria. Tracer yield Is 15*1250/o
  • Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). n /,, Method blank ls less than the RDL/ LLD. ./ ""mnlna <'. SO/o of ln ... nct ac:tivltv\ Sample was run within hold time. I DER Sam Pie was correctlv Preserved If regulred. ./ Smears Taken for Radioactive batches. n/a Method Spike and LCS are within 75-125% ./ J or meets the client's contract accentance criteria l, No blank spaces on data forms. ./ All line outs Initialed and dated. tr.anst:ciatiao !:CCQc& am arnzaceot Aux data Is correct. ./ Client Special reaulrements oaoe has been checked, ./ Raw Data and/ or spectrum are included and nroaerlv statused. J MS, LCS, and Duplicate RPD/RER values uploaded to LIM5 and ./ va" oDa .. nrlfln,f Hit ./ entered lntll..til*P ./ 1563940 Batch Data Exception Reports (DER) completed if applicable. ./ ' DER 1563940 Batch Data Exception Reports (DER) second reviewed. / Disposition verified to be comnleted. aJL@..QLCorrectlon c;omp.lfil;e<i If *B"""ired n/a Review sample historical results if available ./ (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. l Primary Review Performed By:, _____ __ _ Page 3386 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER Mo.Day Yr. 03-0CT-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1596249 DATA EXCEPTION REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE HASL 300, 4.5.2.3/Ga-01-R Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

DER Report No.: 1563940 Revision No.: Type: Process Client Code: MJWC Samples 405235 021, 022, 023, 024, 025, 026, 027, 028, 029, 030, 031, Samples were analyzed in a timely manner upon receipt. Reporting 032, 033, 034, 035, 036, 037, 038, 039, 040, and 1203621355 (duplicate) results. were received outside of the holding period. Originator's Name: Data Validator/Group Leader: Spencer Collins 03-0CT-16 Michael Hilton 03-0CT-16 Page 1 Page 3387of5809

  • Gamma Spec Queue Sheet 09/13/2016 Batch #:1596249 Gamma LCS Isotope: Mixed Gamma Initials:_,_. _ Analyst: MXRl First Client DueDate:l0/04/2016 LCS Code: I i:;-t;t, Expiration Date: Prep Internal Due Date: 09/30/2016 Y I I \ 3 ( Vol: \
  • 0 Balance ID:. _ _____ _ Sample ID Client Descript Hazard Sealing Dateffime ion I Container ID Type Code Client Matrix Collect Date Geometry (I g F) Detector (if Applicable) 405235021-1 4.2B.R.2.3 SAMPLE MJWCOOl SOIL 08-DEC-1514:17:0etitf *rAtJ 161.305 g 7 I .q 117--1\ If 405235022-1 4.2B.R.l.3 40523:5il23-l 4.ZB.R.11.2 405235024-1 4.2B.R.2.2 SAMPLE MJWCOOl SOIL 08-DEC-15 13:43:00 161.105 g [")? l SAi\IPLE MJWCOOl SOIL 02-DEC-1510:40:00\l' I 141.404 g ! 'l I..\. I SAMPLE MJWCOOl SOIL OS-DEC-1514:13:00 Y'J ? 138.962 g '-'1
  • 405235025-1 4.2B.R.l.2 SAMPLE MJWCOOl SOIL 08-DEC-15 13:38:00 ft 138.244 g 2. 405235026-1 4.2C.R.1.3 SA.MP LE MJWCOOl SOIL 08-DEC-1510:15:00'(lt' I 155.202 g :xi 405235027-1 4.2C.R.l.4 -:0523:'.028-l 4.3.ARl.3 405235029-1 4.3.B.R.1.3 -105235030-1 4.3A.R.2.3 SAMPLE MJWCOOl SOIL OS-DEC-15 10:19:00 I 158.553 g CK I .$AMPLE MJWCOOl SOIL 23-1'\0\'-15 14:50:00 n; I 125.516 g I SAMPLE MJWCOOl. SOIL 23-NOV-1511:10:001'\f 151.202 g SAMPLE M.JWCOOl SOIL 23-NOV-15 14:44:00Rf 131.12 g 1o 405235031-1 -l.3.BR19.2 SAMPLE MJWCOOl SOIL 26-NOV-15 14:25:00"\l.'f-I 139.617 g I 32 405235032-1 4.3B.R.3.3 405235033-1 4.3B.R.3.4 SAl'rlPLE MJWCOOl SOIL 23-NOV-15 146.947 g SAMPLE MJWCOOl SOIL 166.788 g I 2$ 405235034-1 4.3.B.R.l.4 405235035-1 4.3B.R.2.3 405235036-l 4.38.R.2.4 405235037-1 4.4C.R.2.4 405235038-f 4.4C.R.l.3 -105235039-1 4.4C.R.1.4 405235040-1 4.4D.R.l.3 1203621354-1 MB 1203621355-1 DUP 4.4C.R. l.3{ 405 1203621356-1 LCS SAMPLE MJWCOOI SOIL 23-NOV-15 11:20:0°{"lR 152.487 g I 1...%'° SAl'rlPLE MJWCOOl SOIL 164.073 g 33)-5 r,,-').-\b SAMPLE MJWCOOI SOIL 162.257 g I 3C SAMPLE MJWCOOl SOIL 30-NOV-15 11:19:00 \ 178.756 g j I-Li I I SAMPLE MJWCOOl SOIL 30-NOV-15 J0:40:00"(l. I 170.192 g i SAMPLE MJWCOOl SOIL 30-NOY-15 10:43:00'fU? 175.326 g I SAMPLE MJWCOOI SOIL 30-NOV-15 13:23:00\RJ 172.014 g ,.., I MB QC ACCOUNT SOIL ti ln...\\c. 1lf-H: 235038) DUP QC ACCOUNT SOIL 30-NOV-15 110. Otft;"" I l.t LCS QC ACCOUNT SOIL 11.f rI. ... GEL Laboratories LLC, Radiochemistry Division ------..._ Data Reviewed By: Jr:J-3-I lo Page 1 of 1 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:58:09.35 ******************************************************************************** *
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM07.CNF;484 Background date : Z-OCT-2016 11:00:17. Sample date 8-DEC-2015 14:17:00. Acquisition date : 3-0CT-2016 08:57:41. Sample ID G405235021 Sample quantity 1.61305E+02 GRAM Detector name : GAM07 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.50 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 0 2 0 3 4 4 4 5 1 6 1 7 0 8 0 9 0 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 3 24 3 25 0 26 0 27 0 28 0 29 0 30 0 31 0 32 0 33 0 34 0 Page 3389 of 5809 Energy 62. 66* 70.49 74.85* 77.17 87.24 89.87 92.89* 115. 04 128.68 185.83* 209.68 238.46* 242.08 252.03 269.99 281. 65 295.17* 302.16*

338.46* 351.81* 463.69 485.37 510.66* 514.25 583.25* 609.13* 661.74 665.33 711. 67 728.14* 830.98 852.04 861.03 911. 88* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 18 19 124 210 75 30 74 15 48 83 74 288 70 24 60 26 128 44 50 192 16 40 25 19 103 146 46 16 8 13 12 8 27 91 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 180 1.05 125.81 125 1.37 141.47 170 1.31 150.19 140 1.07 154.82 114 1.16 174.95 136 1.02 180.21 155 1.47 186.26 86 0.60 230.55 176 0.63 257.81 133 1.20 372.09 97 1.48 419.78 122 1.21 477.32 104 1.02 484.57 37 0.92 504.47 112 4.94 540.38 38 1.60 563.70 81 1.17 590.72 84 4.80 604.69 63 0.91 677.29 71 1.32 703.97 31 1.37 927. 70 69 12.38 971.04 27 2. 04 1021. 61 20 2.04"1028.79 41 1.27 1166. 76 33 1. 48 1218. 51 34 1. 04 1323. 73 13 1.88 1330.89 28 0.78 1423.57 36 0.92 1456.50 11 1.50 1662.14 14 0.67 1704.25 29 1.54 1722.24 35 2.35 1823.92 122 140 146 146 172 172 183 228 253 366 414 474 482 501 530 558 584 597 672 698 922 957 1014 1014 1162 1213 1319 1328 1419 1449 1655 1694 1715 1815 9 4.88E-03143.9 6 5.38E-03 94.3 16 3.46E-02 20.9 2.90E+00 16 5.84E-02 11.l 11 2.08E-02 23.9 4.37E+OO 11 8.32E-03 62.4 9 2.07E-02 34.4 6 4.24E-03 99.2 11 1.33E-02 55.4 11 2.30E-02 30.0 11 2.05E-02 28.5 8 8.0lE-02 9.0 9 1. 94E-02 31. 3 6 6.78E-03 44.4 16 1. 67E-02 41. 4 11 7.12E-03 51.9 13 3.54E-02 17.2 16 1.22E-02 49.5 9 1.40E-02 32.4 14 5. 34E-02 11. 9 9 4.47E-03 67.5 30 1.lOE-02 62.7 20 7.03E-03 61.4 2.04E+00 20 5.24E-03 55.9 12 2.86E-02 16.2 14 4.07E-02 11.8 10 1. 29E-02 27. 9 8 4.31E-03 48.7 12 2.09E-03149.1 12 3.55E-03 99.6 11 3.25E-03 66.7 14 2.22E-03105.3 17 7.47E-03 50.3 22 2.53E-02 19.6 Peak Search Report (continued) Page : 2 Sample ID : G405235021 Acquisition date 3-0CT-2016 08:57:41 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 964. 23 23 11 1. 35 1928.61 1922 11 6.25E-03 35.3 36 0 968.59* 58 9 1. 50 1937.32 1933 10 1. 62E-02 16.9 37 0 .* 991. 95 13 1. 1. 04 1984.05 6 3.49E-03 32.1 38 0 1055.78 7 16 4.25 2111. 68 2103 13 1.93E-03125.6 39 0 1102.76 12 15 1. 34 2205.63 2200 10 3.33E-03 66.9 40 0 1119. 87 41 12 1. 95 2239.84 2231 16 1.14E-02 24.6 41 0 1128.91 14 2 3.21 2257.93 2253 9 3.86E-03 33.0 42 *o 1238' .14 12 9 0.64 2476.37 2473 7 3.43E-03 50.8 43 0 1376.74 20 3 1. 40 2753.54 2746 14 5.43E-03 30.4 44 0 1460.29* 304 7 1. 93 2920.63 2913 14 8.44E-02 6.1 45 0 1764.35* 29 3 1. 45 3528.71 3522 12 8.lOE-03 23.5 Flag: "*" = Peak area was modified by background subtraction Page 3390 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:58:11 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 14:17:00 G405235021 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:57:41 161. 30 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA7 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3391of5809 PB-214 PB-214 PB-214 PB-214 'PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 ** Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.50 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235021 Acquisition date 3-0CT-2016 08:57:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status .K-40 1460.82 l.122E+OO 1.148E+Ol l.148E+Ol 12.23 OK KR-85 514.00 0.43* 2.620E+OO 8.514E+OO 8.986E+OO 111. 77 OK SR-85 514.00 96. 00* 2.620E+OO 3.849E-02 9.489E-01 111. 77 OK CD-109 88.03 3.70* 5.745E+OO 1.334E+OO 2.093E+OO 80. 72 OK SN-126 64.28 9.60 3.624E+OO Line Not Found Absent 86.94 8.90 5.745E+OO 5.546E-01 5.546E-01 80. 72 OK 87.57 37.00* 5.745E+OO 1.334E-01 1.334E-01 80.72 OK BA-137M 661.66 89.90* 2 .138E+OO 1.205E-01 l.228E-01 55.70 OK CS-137 661.66 85.10* 2.138E+OO 1.273E-01 1. 2 97E-01 55.70 OK TL-208 277.37 6.60 4.377E+OO Line Not Found Absent 583.19 85.00* 2.365E+OO 2.589E-01 2.589E-01 32.49 OK 860.56 12.50 l.736E+00 5.982E-01 5.982E-01 100.52 OK PB-212 74.82 10.28 4.784E+00 1.070E+OO 1. 070E+OO 63.93 OK 77.11 17.10 4.995E+OO 1.533E+OO 1.533E+OO 22 .11 OK 238.63 43.60* 4.933E+OO 7.477E-01 7.477E-01 17.95 OK 300.09 3.30 4.103E+OO Line Not Found Absent BI-214 609.32 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 OK 1120.29 14.92 l.406E+00 9.123E-01 9.126E-01 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 OK PB-214 74.82 5.80 4.781E+OO Line Not Found <<INT Reject 77 .11 9.70 4.995E+OO 2.703E+OO 2.704E+OO 22 .11 OK 87.09 3.41 5.736E+OO Line Not Found <<INT Reject 242.00 7.25 4.877E+OO Line Not Found <<INT Reject 295.22 18.42 4.160E+OO 9.078E-01 9.082E-01 34.41 OK 351. 93 35.60* 3.593E+OO 8.043E-01 8.045E-01 23.81 OK RN-222 609.32 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 OK 1120.29 14.92 1.406E+OO 9.123E-01 9.126E-01 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 OK RA-224 240.99 4.10* 4.876E+OO 3.389E-01 3.389E-01 394.49 OK RA-226 609.32 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 OK 1120.29 14.92 l.406E+OO 9.123E-01 9.126E-01 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 OK AC-228 105.21 1.10 6.488E+00 Line Not Found Absent 338.32 11. 27 3. 711E+OO 6.479E-01 6.479E-01 64.74 OK 794.95 4.25 1.849E+OO Line Not Found Absent 835.71 1. 61 1.777E+OO Line Not Found Absent 911. 20 25.80* 1.658E+OO 1.020E+OO 1. 020E+OO 39.13 OK 968.97 15.80 1. 581E+OO 1.112E+OO 1.112E+OO 33.90 OK RA-228 105'. 21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.711E+OO 6.479E-01 6.479E-01 64.74 OK 794.95 4.25 1.849E+OO Line Not Found Absent 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.658E+OO 1.020E+OO 1. 020E+OO 39.13 OK 968. 97 15.80 1.581E+OO 1.112E+OO 1.112E+OO 33.90 OK TH-228 74.82 10.28 4.784E+OO 1.070E+OO 1.070E+OO 63.93 OK 77.11 17.10 4.995E+OO l.533E+00 1.533E+OO 22 .11 OK 238.63 43.60* 4.933E+OO 7.477E-01 7.477E-01 17.95 OK 300.09 3.30 4.103E+OO Line Not Found Absent TH-230 609.32 45.49* 2.284E+OO 7.086E-01 7.086E-01 23.69 OK Page 3392 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235021 Acquisition date 3-0CT-2016 08:57:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29' 14.92 1.406E+OO 9.123E-01 9.123E-01 c 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.919E-01 47.05 OK PA-231 283.69 1. 70 4.298E+OO Line Not Found Absent 301.36 5.35* 4.080E+OO l.090E+OO 1.090E+OO 99.01 OK TH-232 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11.27 3. 711E+OO 6.479E-01 6.479E-01 64.74 OK 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.658E+00 1.020E+OO 1.020E+OO 39.13 OK 968. 97 15.80 1.581E+OO 1.112E+OO 1.112E+OO 33.90 OK TH-234 63.29 3.70* 3.418E+OO 8.828E-01 8.828E-01 287.78 OK 92.59 4.23 6.053E+OO 1. 779E+OO 1. 779E+OO 68.74 OK U-234 609.32 45.49* 2.284E+OO 7.086E-01 7.086E-01 23.69 OK 1120.29 14.92 l.406E+OO 9.123E-01 9.123E-01 49 .11 OK 1764.49 15.30 9.423E-01 8.919E-01 8.919E-01 47.05 OK U-235 89. 96 3.47 5.897E+OO 8.997E-01 8.997E-01 124.84 OK 93.35 5.60 6.053E+OO 1.344E+OO 1.344E+OO 68.74 OK 143.76 10. 96* 6.563E+OO Line Not Found Absent 163.33 5.08 6.266E+OO Line Not Found Absent 185.72 57.20 5.856E+OO l.417E-01 1. 417E-01 59.94 OK 205.31 5.01 5.496E+OO Line Not Found Absent U-238 63.29 3.70* 3.418E+OO 8.828E-01 8.828E-01 287.78 OK 92.59 4.23 6.053E+OO 1. 779E+OO 1.779E+OO 68.74 OK AM-243 43.53 5.90 6.933E-01 Line Not Found Absent 74.66 67.20* 4.784E+00 1.637E-01 l.637E-01 63.93 OK ANH-511 511. 00 100.00* 2.635E+OO 4.932E-02 4.932E-02 122.78 OK Flag: "*" = Keyline Page 3393 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:58:12.27 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l *
  • Acquisition date 3-0CT-2016 08:57:41 Sensitivity : 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Analyst initials: MXRl *
  • Sample ID G405235021 Sample Quantity 1.6130E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 * *Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 l.148E+Ol 1.376E+OO 6.020E-01 KR-85 8.986E+OO 9.843E+OO 1.069E+Ol SR-85 9.489E-01 1. 039E+OO 1.129E+OO CD-109 2.093E+OO 1.656E+OO 1. 856E+OO SN-126 l.334E-01 1.055E-01 1.188E-01 BA-137M 1.228E-01 6.702E-02 6.972E-02 CS-137 1. 2 97E-01 7.080E-02 7.365E-02 TL-208 2.589E-01 8.244E-02 6.287E-02 PB-212 7.477E-01 1.315E-01 l.031E-01 BI-214 7.089E-01 1.646E-01 1.049E-01 PB-214 8.045E-01 1.877E-01 1. l 78E-01 RN-222 7.089E-01 1. 646E-01 l.049E-01 RA-224 3.389E-01 1.310E+OO 1.312E+OO RA-226 7.089E-01 1. 646E-01 l.049E-01 AC-228 1.020E+OO 3. 911E-01 2.008E-01 RA-228 1.020E+OO 3. 911E-01 2.008E-01 TH-228 7.477E-01 l.315E-01 1. 031E-01 TH-230 7.086E-01 1.645E-01 1.048E-01 PA-231 1.090E+OO 1.058E+OO 6.675E-01 TH-232 l.020E+00 3.911E-01 2.008E-01 TH-234 8.828E-01 2.490E+OO 1.888E+OO U-234 7.086E-01 l.645E-01 l.048E-01 U-235 3.069E-02 1.661E-01 3.129E-01 U-238 8.828E-01 2.490E+OO 1.888E+OO AM-243 1.637E-01 1. 026E-01 7.753E-02 ANH-511 4.932E-02 5.935E-02 4.372E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nµclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 2.392E+00 9.940E+OO 1. 8 66E+Ol NOT IDENT. NA-22 -4. 722E-03 3.491E-02 6.991E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 6.485E-03 3.382E-02 7.502E-02 FAIL ABUN Page 3394 of 5809 SC-46 -1.593E-02 2. 996E-01 6.153E-01 FAIL ABUN V-48 O.OOOE+OO 1.277E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.367E+02 O.OOOE+OO SHORT HLIF MN-54 5.176E-02 6.098E-02 1.269E-01 NOT IDENT. C0-56 -2.602E-01 4.253E-01 6.647E-01 FAIL ABUN MN-56 O.OOOE+OO l.702E+41 O.OOOE+OO SHORT HLIF C0-57 -3.235E-02 3.999E-02 7.039E-02 NOT IDENT. C0-58 -3.988E-01 5.759E-01 9.569E-01 NOT IDENT. FE-59 2.626E+OO 6.765E+OO l.300E+Ol NOT IDENT.
  • co-60 1.241E-02 3.036E-02 6.856E-02 NOT IDENT . ZN-65 5.526E-02 1. 769E-01 3.311E-01 NOT IDENT. GE-68 -4.394E-01 2.136E+00 4.149E+OO NOT IDENT. AS-73 -1. 865E+OO 6.599E+OO 1. 291E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.387E+03 O.OOOE+OO SHORT HLIF SE-75 -2.194E-01 2.022E-01 3.164E-01 NOT IDENT. BR-77 O.OOOE+OO 2. 331E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.800E+02 O.OOOE+OO SHORT HLIF RB-83 1.042E-02 5.040E-01 1.004E+OO NOT IDENT. RB-86 0.000E+OO 2.604E+04 O.OOOE+OO SHORT HLIF Y-88 3.393E-03 9.615E-02 2.683E-01 NOT IDENT. Y-91 1.990E+02 6.222E+02 1.242E+03 NOT IDENT. NB-94 -5.126E-03 2.760E-02 5 .135E-02 NOT IDENT. NB-95 -5.377E-01 8.952E-01 1.524E+OO NOT IDENT. NB-95M 1.132E+OO 1.907E+OO 3.707E+OO NOT IDENT. ZR-95 -5.668E-02 1.476E+OO 2. 771E+OO NOT IDENT. NB-97 O.OOOE+OO 1.082E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.168E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.603E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO l.738E+41 O.OOOE+OO SHORT HLIF RH-101 O.OOOE+OO 8.089E-02 5.978E-02 FAIL ABUN RH-102 -2.224E-02 5.089E-02 9.190E-02 NOT IDENT. RU-103 8.950E-02 4.626E+00 9.162E+OO FAIL ABUN RH-106 l.541E-01 4.129E-01 8.536E-01 NOT IDENT. RU-106 1.541E-01 4.129E-01 8.536E-01 NOT IDENT. AG-108M -6.525E-03 2.718E-02 5.150E-02 NOT IDENT. AG-llOM -3.167E-02 7.927E-02 1.533E-01 NOT IDENT. SN-113 -2.884E-02 2.214E-01 4.269E-01 NOT IDENT. CD-115 O.OOOE+OO 2.764E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 8.764E+04 O.OOOE+OO SHORT HLIF TE-123M -1.079E-01 1.253E-01 2.145E-01 NOT IDENT. SB-.124 1.146E-01 2 .131E+00 4.424E+OO NOT IDENT. SB-125 -5.414E-02 8.818E-02 1.605E-01 FAIL ABUN TE-125M 6.919E+Ol 2.305E+02 4.499E+02 NOT IDENT. I-126 O.OOOE+OO l.004E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.126E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1. 888E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.311E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 572E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.208E+26 O.OOOE+OO SHORT HLIF BA-133 -1.338E-02 4.086E-02 6.908E-02 FAIL ABUN I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 2.153E-02 5.269E-02 1.041E-01 NOT IDENT. CS-135 7.379E-02 1.144E-01 2.418E-01 NOT IDENT. I-135 O.OOOE+OO 1.868E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2. 951E+05 O.OOOE+OO SHORT HLIF CE-139 -1.250E-02 1.054E-01 1.927E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 021E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3 .117E+05 O.OOOE+OO SHORT HLIF CE-141 1.388E+Ol 2.089E+Ol 4.126E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.515E+41 O.OOOE+OO SHORT HLIF CE-144 -1.287E-01 3.429E-01 5.708E-01 NOT IDENT. PM-144 2.690E-02 4.832E-02 l.005E-01 NOT IDENT. PR-144 2.365E+OO 4.201E+OO 8.747E+OO NOT IDENT. PM-146 1.296E-02 3.715E-02 7.623E-02 NOT IDENT. ND-147 O.OOOE+OO 2.875E+07 O.OOOE+OO SHORT HLIF PM-147 *1. 924E+02 6.547E+02 1.282E+03 NOT IDENT. PM-149 O.OOOE+OO 3.886E+40 O.OOOE+OO SHORT HLIF EU-150 -1.312E-03 2.262E-02 4.017E-02 FAIL ABUN EU-152 .:.5.561E-02 7.338E-02 1. 339E-01 FAIL ABUN GD-153 -1.028E-01 1.661E-01 2.784E-01 FAIL ABUN EU-154 -1.158E-02 8.558E-02 1. 714E-01 NOT IDENT. EU-155 -3.814E-02 9.072E-02 1.676E-01 FAIL ABUN TB-160 6.524E-01 1.255E+OO 2.906E+OO FAIL ABUN H0-166M 3.408E-02 9. 961E-02 1.135E-01 FAIL ABUN TM-171 -1.794E-01 1.546E+Ol 3.096E+Ol NOT IDENT. HF-172 -1.lOlE-01 2.305E-01 3.809E-01 FAIL ABUN LU-172 -5.708E-02 7.403E-02 1.289E-01 FAIL ABUN LU-176 -8.387E-03 2.145E-02 3.656E-02 FAIL ABUN Page 3395 of 5809 HF-181 4.432E-01 3.660E+OO 7.316E+OO NOT IDENT. TA-182 6.389E-01 9.186E-01 1.966E+OO FAIL ABUN RE-183 -7.564E-01 2.314E+00 4.481E+OO NOT IDENT. RE-184 1. 372E+Ol 3.124E+Ol 6.567E+Ol NOT IDENT. W-188 1.904E+Ol 1.023E+02 1.882E+02 FAIL ABUN IR-192 1.089E-01 3.924E-01 7.923E-01 FAIL ABUN HG-203 -9 .161E-01 2.069E+OO 3.528E+OO FAIL ABUN BI-207 2. 596E-02 4.647E-02 9.988E-02 FAIL ABUN PB-210 1.035E+OO 2.467E+OO 5. 096E+OO NOT IDENT. BI-211 O.OOOE+OO 5.170E-01
  • 7. 320E-01 FAIL ABUN PB-211 2.257E-01 5.095E-01 1.070E+OO FAIL ABUN BI-212 4.770E-01 9.309E-01 1.119E+OO FAIL ABUN RN-219 -7.130E-02 3.350E-01 6.430E-01 FAIL ABUN RA-223 4.393E-02 5.413E-01 1.076E+OO FAIL ABUN AC-227 -4.093E-02 l.944E-01 3.828E-01 NOT IDENT. TH-227 -4.093E-02 1.944E-01 3.828E-01 NOT IDENT. TH-229 6.714E-02 4.220E-01 7.859E-01 FAIL ABUN TH-231 4.393E-02 5.413E-01 . 1. 07 6E+OO FAIL ABUN PA-233 8.350E-03 5.037E-02 1.019E-01 NOT IDENT. PA-234 8.053E-02 2.328E-01 5.005E-01 NOT IDENT. PA-234M -6.592E-01 3.983E+OO 7.916E+OO NOT IDENT. NP-237 8.350E-03 5.037E-02 1.019E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 9.356E-02 2.179E-01 4.002E-01 NOT IDENT. PU-239 O.OOOE+OO 7.337E+02 6 .161E+02 FAIL ABUN AM-241 -8.491E-03 1.182E-01 2 .151E-01 NOT IDENT. CM-243 2.499E-02 8.365E-02 1.642E-01 NOT IDENT. BK-247 -4. 9orn:..02 7.077E-02 1.171E-01 NOT IDENT. CM-247 -2.554E-03 2.981E-02 5.820E-02 NOT IDENT. CF-249 1. 748E-02 3.440E-02 7.092E-02 FAIL ABUN CF-251 1.018E-01 9.504E-02 1.944E-01 NOT IDENT. Page 3396 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:58:10.05 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 295 10.66* 1.122E+OO l.148E+Ol 1.148E+Ol 12.23 KR-85 514.00 21 0.43* 2.620E+OO 8.514E+OO 8.986E+OO 111. 77 SR-85 514.00 21 96. 00* 2.620E+OO 3.849E-02 9.489E-01 111. 77 CD-109 88.03 99 3.70* 5.745E+OO 2.171E+OO 3.406E+OO 47.80 SN-126 64.28 ------9.60 3.624E+OO ------Line Not Found ------86.94 99 8.90 5.745E+OO 9.024E-01 9.024E-01 47.80 87.57 99 37.00* 5.745E+OO 2 .171E-01 2.171E-01 47.80 BA-137M 661.66 50 89.90* 2.138E+OO l.205E-01 1. 228E-01 55.70 CS-137 661.66 50 85.10* 2.138E+OO l.273E-01 l.297E-01 55.70 TL-208 277.37 ------6.60 4.377E+OO ------Line Not Found ------583.19 112 85.00* 2.365E+OO 2.589E-01 2.589E-01 32.49 860.56 28 12.50 1. 736E+OO 5.982E-01 5.982E-01 100.52 BI-211 72. 87 ------1. 23 4.591E+OO ------Line Not Found ------351.06 221 12.92* 3.593E+OO 2.216E+OO 2.216E+OO 23.81 PB-212 74.82 167 10.28 4.784E+OO 1.582E+OO 1.582E+OO 41.77 77 .11 281 17.10 4.995E+OO' l.533E+OO 1.533E+OO 22 .11 238.63 346 43.60* 4.933E+OO 7.477E-01 7.477E-01 17.95 300.09 ------3.30 4.103E+OO ------Line Not Found ------BI-214 609.32 158 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 1120. 29 41 14.92 1. 406E+OO 9.123E-01 9.126E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 PB-214 74.82 167 5.80 4.784E+OO 2.805E+OO 2.806E+OO 41. 77 77 .11 281 9.70 4.995E+OO 2.703E+OO 2.704E+OO 22 .11 87.09 99 3.41 5.745E+OO 2.355E+OO 2.356E+OO 47.80 242.00 84 7.25 4.876E+OO 1.099E+OO l.lOOE+OO 62. 62 295.22 149 18.42 4.160E+OO 9.078E-01 9.082E-01 34.41 351.93 221 35.60* 3.593E+OO 8.043E-01 8.045E-01 23.81 RN-222 609.32 158 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 1120.29 41 14.92 1.406E+OO 9.123E-01 9.126E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 RA-224 240.99 84 4.10* 4.876E+OO 1.944E+OO 1.944E+OO 62. 62 RA-226 609.32 158 45.49* 2.284E+OO 7.086E-01 7.089E-01 23.69 1120.29 41 14.92 1.406E+OO 9.123E-01 9.126E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8.922E-01 47.05 AC-228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 58 11. 27 3. 711E+OO 6.479E-01 6.479E-01 64.74 794.95 ------4.25 1.849E+OO ------Line Not Found ------835.71 ------1. 61 1.777E+OO ------Line Not Found ------911. 20 94 25.80* 1.658E+00 l.020E+OO 1.020E+00 39.13 968.97 60 15.80 1. 581E+OO l .112E+OO 1.112E+OO 33.90 RA-228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 58 11. 27 3.711E+OO 6.479E-01 6.479E-01 64.74 794.95 ------4.25 1.849E+OO ------Line Not Found ------835.71 ------1. 61 1.777E+OO ------Line Not Found ------911.20 94 25.80* 1.658E+OO 1.020E+OO 1.020E+OO 39.13 968.97 60 15.80 1.581E+OO l .112E+OO 1.112E+OO 33.90 TH-228 74.82 167 10.28 4.784E+OO 1.582E+OO 1.582E+OO 41.77 Page 3397 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235021 Acquisition date 3-0CT-2016 08:57:41 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 281 J.7.10 4.995E+OO l.533E+OO 1.533E+OO .22.11 238.63 346 43.60* 4.933E+OO 7.477E-01 7.477E-01 17.95 300.09 ------3.30 4.103E+OO ------Line Not Found ------TH-230 609.32 158 45.49* 2.284E+OO 7.086E-01 7.086E-01 23.69 1120.29 41 14.92 l.406E+OO 9.123E-01 9.123E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8.919E-01 47.05 PA-231 283.69 ------1. 70 4.298E+OO ------Line Not Found ------301.36 51 5.35* 4.080E+OO 1.090E+OO 1.090E+OO 99.01 TH-232 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 58 11.27 3.711E+00 6.479E-01 6.479E-01 64.74 835.71 ------1. 61 1.777E+00 ------Line Not Found ------911.20 94 25.80* 1. 658E+OO 1.020E+OO 1.020E+OO 39.13 968. 97 60 15.80 1. 581E+OO 1.112E+OO 1.112E+OO 33.90 TH-234 63.29 24 3.70* 3.418E+OO 8.828E-01 8.828E-01 287.78 92.59 98 4.23 6.053E+OO 1. 779E+OO 1.779E+OO 68.74 U-234 609.32 158 45.49* 2.284E+OO 7.086E-01 7.086E-01 23.69 1120. 29 41 14.92 1.406E+OO 9.123E-01 9.123E-01 49 .11 1764.49 28 15.30 9.423E-01 8.919E-01 8.919E-01 47.05 U-235 89. 96 40 3.47 5.897E+OO '8. 997E-01 8.997E-01 124.84 93.35 98 5.60 6.053E+OO 1.344E+OO l.344E+00 68.74 143.76 ------10. 96* 6.563E+OO ------Line Not Found ------163.33 ------5.08 6.266E+OO ------Line Not Found ------185.72 102 57.20 5.856E+OO 1. 417E-01 1. 417E-01 59.94 205.31 ------5.01 5.496E+00 ------Line Not Found ------U-238 63.29 24 3.70* 3.418E+OO 8.828E-01 8.828E-01 287.78 92.59 98 4.23 6.053E+OO 1. 779E+OO 1. 77 9E+OO 68.74 AM-243 43.53 ------5.90 6.933E-01 ------Line Not Found ------74.66 167 67.20* 4.784E+OO 2. 421E-01 2.421E-01 41.77 ANH-511 511. 00 28 100.00* 2.635E+OO 4.932E-02 4.932E-02 122.78 Flag: "*" Key line Page 3398 of 5809 Summary of Nuclide Activity Sample ID : G405235021 Acquisition date Page : 3 3-0CT-2016 08:57:41 Total number of lines in spectrum 45 Number of unidentified lines 6 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 10.56Y 64.84D 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600.00Y 1600.00Y l.41E+l0Y 1600. OOY 1.41E+10Y l.41E+l0Y l.41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 06 24.7 1. 57 1. 00 1. 02. 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.148E+Ol 8.514E+OO 3.849E-02 2. l 71E+OO 2.171E-01 1.205E-01 1.273E-01 2.589E-01 2.216E+OO 7.477E-01 7.086E-01 8.043E-01 7.086E-01 1.944E+OO 7.086E-01 l.020E+00 1.020E+OO 7.477E-01 7.086E-01 l.090E+OO 1. 020E+OO 8.828E-01 7.086E-01 l.417E-01 8.828E-01 2.421E-01 4.932E-02 3.928E+Ol 3.928E+Ol Decay Corr pCi/GRAM 1.148E+Ol 8.986E+OO 9.489E-Ol 3.406E+OO 2. l 71E-Ol l.228E-01 l.297E-01 2.589E-01 2.216E+OO 7.477E-01 7.089E-01 8.045E-01 7.089E-01 1.944E+OO 7.089E-01 1.020E+OO 1.020E+OO 7.477E-01 7.086E-01 1.090E+OO l.020E+OO 8.828E-01 7.086E-01 l.417E-01 8.828E-01 2.421E-01 4.932E-02 4.190E+Ol 4.190E+Ol 86.67% Decay Corr 2-Sigma Error 0.140E+Ol 10.04E+OO 10.61E-01 l.628E+OO 1.038E-01 0.684E-01 0. 722E-01 0.841E-01 0.528E+OO l.342E-01 l.679E-01 l.915E-01 1.679E-01 1.218E+OO l.679E-01 0.399E+OO 0.399E+OO l.342E-01 1.679E-01 1. 07 9E+OO 0.399E+OO 25.40E-01 1. 679E-01 0.850E-01. 25.40E-01 1. OllE-01 6.056E-02 "M" Manually accepted 2-Sigma %Error 12.23 111. 77 111. 77 47.80 47.80 55.70 55.70 32.49 23.81 17.95 23.69 23.81 23.69 62. 62 23.69 39.13 39.13 17.95 23.69 99.01 39.13 287.78 23.69 59.94 287.78 41.77 122.78 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3399 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235021 Acquisition date : 3-0CT-2016 08:57:41 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 70.49 26 168 1. 37 141.47 140 6 5.38E-03 **** 4.34E+OO T 0 115.04 20 111 0.60 230.55 228 6 4.24E-03 **** 6.65E+OO T 0 128.68 61 224 0.63 257.81 253 11 l.33E-02 **** 6.69E+OO T 0 209.68 90. 118 1. 48 419.78 414 56.9 5.42E+OO T 0 252.03 29 44 0.92 504.47 501 6 6.78E-03 88.7 4.73E+OO T 0 269.99 71 132 4.94 540.38 530 16 1. 67E-02 82.7 4.47E+OO T 0 281. 65 30 45 1. 60 563.70 558 11 7.12E-03 **** 4.32E+OO T 0 463.69 18 34 1. 37 927.70 922 9 4.47E-03 **** 2.85E+OO T 0 485.37 44 77 12.38 971.04 957 30 1.lOE-02 **** 2.75E+OO 0 665.33 17 14 1. 88 1330.89 1328 8 4. 31E-03 97.3 2.13E+OO T 0 711. 67 8 30 0.78 1423.57 1419 12 2.09E-03 **** 2.02E+OO T 0 728.14 14 38 0.92 1456.50 1449 12 3.55E-03 **** 1.98E+OO T 0 830.98 12 12 1. 50 1662.14 1655 11 3.25E-03 **** 1. 79E+OO T 0 852.04 8 15 0.67 1704.25 1694 14 2.22E-03 **** 1. 7 5E+OO 0 964. 23 23 11 1. 35 1928.61 1922 11 6.25E-03 70.7 1.59E+OO T 0 991.95 13 1 1. 04 1984.05 1981 6 3.49E-03 64.1 l.55E+00 0 1055.78 7 16 4.25 2111. 68 2103 13 1.93E-03 **** l.47E+OO 0 1102.76 12 15 1. 34 2205.63 2200 10 3.33E-03 **** 1. 42E+OO 0 1128.91 14 2 3.21 2257.93 2253 9 3.86E-03 66.0 1.40E+OO T 0 1238.14 12 9 0.64 2476.37 2473 7 3.43E-03 **** 1.29E+OO T 0 1376.74 19 3 1. 40 2753.54 2746 14 5.43E-03 60.8 1.18E+OO Flags: "T" = Tentatively associated Page 3400 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:58:24.66 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l *
  • Acquisition date 3-0CT-2016 08:57:41 Sensitivity : 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Nuclide Library : SOLID *
  • Sample ID G405235021 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : l.6130E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.479E-01 4.737E+OO 5.003E-01 8.780E-01 5.622E-02 3.142E-02 3.319E-02 2.819E-02 4.843E-02 4.617E-02 5. 372E-02 4.617E-02 6.227E-01 4.617E-02 8.536E-02 8.536E-02 4.843E-02 4.615E-02 3.034E-01 8.536E-02 8.907E-01 4.615E-02 l.471E-01 8.907E-01 3.662E-02 1. 938E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3401of5809 Le (pCi/GRAM 8.209E+OO 2.866E-02 O.OOOE+OO 3.063E-02 2.621E-01 NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60
  • ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU--:150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3402 of 5809 O.OOOE+OO O.OOOE+OO 5.638E-02 2.782E-01 O.OOOE+OO 3.265E-02 4 .114E-01 5.652E+OO 2.844E-02 l.445E-01 1.779E+OO 6.035E+00 O.OOOE+OO 1. 441E-01 O.OOOE+OO O.OOOE+OO 4.395E-01 O.OOOE+OO 8.482E-02 5.566E+02 2.249E-02 6.748E-01 1.715E+OO 1.227E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0. O'OOE+OO 2.812E-02 3.985E-02 4.049E+OO 3.758E-01 3.758E-01 2.334E-02 6.463E-02 1. 947E-01 O.OOOE+OO O.OOOE+OO l.OOOE-01 1. 784E+OO 7.136E-02 2.106E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.138E-02 O.OOOE+OO 4.666E-02 1.117E-01 O.OOOE+OO O.OOOE+OO 9.022E-02 O.OOOE+OO O.OOOE+OO 1.936E+Ol O.OOOE+OO 2.664E-01 4.464E-02 3.884E+OO 3.426E-02 O.OOOE+OO 5.970E+02 O.OOOE+OO l.822E-02 5.987E-02 1.302E-01 7.027E-02 7.819E-02 1.231E+OO 5.083E-02 1. 447E+Ol l.783E-01 5.482E-02 1. 652E-02 3.261E+OO SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. **

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3403 of 5809 8.720E-01 2.099E+OO 2.925E+Ol 8.638E+Ol 3.621E-01 1.602E+OO 4.398E-02 2.396E+OO 3.519E-01 4. 804E-01. 5.105E-01 2.905E-01 4.950E-01 1. 764E-01 1. 764E-01 3.663E-01 4.950E-01 4.663E-02 2.170E-01 3.462E+OO 4.663E-02 O.OOOE+OO l.873E-01 2.920E+02 1. OllE-01 7.695E-02 5.366E-02 2.625E-02 3.244E-02 9;076E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. -FAIL ABUN NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:58:30.17 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235021.CNF;l *
  • Acquisition date 3-0CT-2016 08:57:41 Sensitivity : 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:17:00 Nuclide Library : SOLID *
  • Sample ID G405235021 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.6130E+02 GRAM *
  • Quantity Err ( % ) : 1. 2399E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.148E+Ol 1.501E+OO 1.501E+OO KR-85 8.986E+OO 9.849E+OO 9.849E+OO SR-85 9.489E-01 1.040E+OO 1.040E+OO CD-109 2.093E+00 1.672E+00 l.672E+00 SN-126 l.334E-01 1.064E-01 1.064E-01 BA-137M 1.228E-01 6. 723E-02 6. 723E-02 CS-137 1.297E-01 7.102E-02 7.102E-02 TL-208 2.589E-01 8.317E-02 8.317E-02 PB-212 7.477E-01 l.374E-01 l.374E-01 BI-214 7.089E-01 1.674E-01 l.674E-01 PB-214 8.045E-01 l.907E-01 1.907E-01 RN-222 7.089E-01 1.674E-01 1.674E-01 RA-224 3.389E-01 1.315E+OO 1.315E+OO RA-226 7.089E-01 1.674E-01 1.674E-01 AC-228 1. 020E+OO 3.946E-01 3.946E-01 RA-228 1.020E+OO 3.946E-01 3.946E-01 TH-228 7.477E-01 1.374E-01 1.374E-01 TH-230 7.086E-01 1. 673E-01 l.673E-01 PA-231 1.090E+OO 1.083E+OO 1.083E+OO TH-232 1.020E+OO 3.946E-01 3.946E-01 TH-234 8.828E-01 2.497E+OO 2.497E+OO U-234 7.086E-01 1. 673E-01 l.673E-01 U-235 3.069E-02 1.661E-01 l.661E-01 U-238 8.828E-01 2.497E+OO 2.497E+OO AM-243 1.637E-01 1.035E-01 l.035E-01 ANH-511 4.932E-02 5.938E-02 5.938E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 2.392E+OO 9.940E+00 9.999E+OO NOT IDENT. NA-22 -4.722E-03 3.491E-02 3.497E-02 NOT IDENT. NA-24 1.000E+41 2.950E+41 O.OOOE+OO SHORT HLIF AL-26 6.485E-03 3.382E-02 3.395E-02 FAIL ABUN Page 3404 of 5809 SC-46 -l.593E-02 2. 996E-01 2.997E-01 FAIL ABUN V-48 5.642E+03 l.277E+04 l.302E+04 SHORT HLIF CR-51 -2.792E+02 3.369E+02 3.597E+02 SHORT HLIF MN-54 5.176E-02 6.102E-02 6.532E-02 NOT IDENT. C0-56 -2.602E-01 4.254E-01 4.413E-01 FAIL ABUN MN-56 -l.OOOE+41 1. 703E+41 O.OOOE+OO SHORT HLIF C0-57 -3.235E-02 4.002E-02 4.259E-02 NOT IDENT. C0-58 -3.988E-01 5.762E-01 6.036E-01 NOT IDENT. FE-59 2.626E+OO 6.767E+OO 6.870E+OO NOT IDENT. C0-60
  • l.241E-02 3.036E-02 3.0a7E-02 NOT IDENT . ZN-65 5.526E-02 1. 769E-01 l.786E-01 NOT IDENT. GE-68 -4.394E-01 2.136E+OO 2.145E+OO NOT IDENT. AS-73 -1. 865E+OO 6.610E+OO 6.664E+OO NOT IDENT. AS-74 -4.685E+03 5.401E+03 5.799E+03 SHORT HLIF SE-75 -2.194E-01 2.025E-01 2.253E-01 NOT IDENT. BR-77 l.325E+38 l.147E+39 O.OOOE+OO SHORT HLIF SR-82 -1. 8llE+02 6.801E+02 6.849E+02 SHORT HLIF RB-83 l.042E-02 5.040E-01 5.040E-01 NOT IDENT. RB-86 -3.319E+03 2.604E+04 2.608E+04 SHORT HLIF Y-88 3.393E-03 9.615E-02 9.617E-02 NOT IDENT. Y-91 l.990E+02 6.223E+02 6.287E+02 NOT IDENT. NB-94 -5.126E-03 2.760E-02 2.770E-02 NOT IDENT. NB-95 -5.377E-01 8.955E-01 9.277E-01 NOT IDENT. NB-95M l.132E+OO l.909E+OO 1. 976E+OO NOT IDENT. ZR-95 -5.668E-02 l.476E+OO 1. 477E+OO NOT IDENT. NB-97 -l.OOOE+41 l.083E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 l.168E+41 O.OOOE+OO SHORT HLIF M0-99 8.480E+31 l.604E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 1. 741E+41 0.000E+OO SHORT HLIF RH-101 7.445E-02 8.201E-02 8. 861E-02 FAIL ABUN RH-102 -2.224E-02 5.092E-02 5.190E-02 NOT IDENT. RU-103 8.950E-02 4.626E+OO 4.626E+OO FAIL ABUN RH-106 l.541E-Ol 4.130E-01 4.188E-01 NOT IDENT. RU-106 l.541E-01 4 .130E-01 4.188E-01 NOT IDENT. AG-108M -6.525E-03 2.718E-02 2.734E-02 NOT IDENT. AG-llOM -3.167E-02 7.928E-02 8.056E-02 NOT IDENT. SN-ll3 -2.884E-02 2.214E-01 2.217E-01 NOT IDENT. CD-ll5 l.042E+39 2.770E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -4.146E+04 8.778E+04 8.975E+04 SHORT HLIF TE-123M -l.079E-01 l.254E-01 l.345E-01 NOT IDENT. SB-124 l.146E-01 2 .131E+OO 2.132E+OO NOT IDENT. SB-125 -5.414E-02 8.821E-02 9.152E-02 FAIL ABUN TE-125M 6.919E+Ol 2.306E+02 2.327E+02 NOT IDENT. I-126 l.053E+06 l.014E+06 l.120E+06 SHORT HLIF SB-126 -2.367E+04 l.126E+06 l.126E+06 SHORT HLIF SB-127 -7.599E+21 2.158E+22 O.OOOE+OO SHORT HLIF I-131 5.698E+08 4. 3llE+09 4.318E+09 SHORT HLIF I-132 l.000E+41 l.855E+42 O.OOOE+OO SHORT HLIF TE-132 -l.446E+26 3.261E+26 O.OOOE+OO SHORT HLIF BA-133 -l.338E-02 4.086E-02 4 .130E-02 FAIL ABUN I-133 -l.OOOE+41 4. ll5E+41 O.OOOE+OO SHORT HLIF CS-134 2.153E-02 5.270E-02 5.359E-02 NOT IDENT. CS-135 7.379E-02 l.145E-01 l.193E-01 NOT IDENT. I-135 -l.OOOE+41 7.026E+41 O.OOOE+OO SHORT HLIF CS-136 -6.716E+02 2. 951E+05 2. 951E+05 SHORT HLIF CE-139 -l.250E-02 l.054E-01 l.056E-01 NOT IDENT. BA-140 5.230E+05 1. 021E+06 l.048E+06 SHORT HLIF LA-140 -5.901E+04 3. ll 7E+05 3.129E+05 SHORT HLIF CE-141 1. 388E+Ol 2.090E+Ol 2.181E+Ol NOT IDENT. CE-143 1. OOOE+41 l.519E+41 0.000E+OO SHORT HLIF CE-144 -l.287E-01 3.430E-01 3.478E-01 NOT IDENT. PM-144 2.690E-02 4.834E-02 4.984E-02 NOT IDENT. PR-144 2.365E+OO 4.203E+OO 4.336E+OO NOT IDENT. PM-146 1. 296E-02 3. 716E-02 3.762E-02 NOT IDENT. ND-147 l.585E+07 2.876E+07 2. 964E+07 SHORT HLIF PM-147 l.924E-t02 6.547E+02 6.604E+02 NOT IDE.NT. PM-149 l.561E+40 3.901E+40 O.OOOE+OO SHORT HLIF EU-150 -l.312E-03 2.262E-02 2.263E-02 FAIL ABUN EU-152 7.345E-02 7.761E-02 FAIL ABUN GD-153 -l.028E-01 l.662E-01 l.725E-01 FAIL ABUN EU-154 -l.158E-02 8.558E-02 8.574E-02 NOT IDENT. EU-155 -3.814E-02 9.076E-02 9.238E-02 FAIL ABUN TB-160 6.524E-01 l.255E+OO 1. 289E+OO FAIL ABUN H0-166M 3.408E-02 9. 963E-02 l.008E-01 FAIL ABUN TM-171 -l.794E-01 l.546E+Ol l.546E+Ol NOT IDENT. HF-172 -l.lOlE-01 2.312E-Ol 2.364E-01 FAIL ABUN LU-172 -5.708E-02 7.426E-02 7.859E-02 FAIL ABUN LU-176 -8.387E-03 2.145E-02 2.178E-02 FAIL ABUN Page 3405 of 5809 HF-181 4.432E-01 3.661E+OO 3.666E+OO NOT IDENT. TA-182 6.389E-01 9.189E-01 9.630E-01 FAIL ABUN RE-183 -7.564E-01 2.317E+OO 2.342E+OO NOT IDENT. RE-184 1.372E+Ol 3.141E+Ol 3.201E+Ol NOT IDENT. W-188 1.904E+Ol l.023E+02 l.027E+02 FAIL ABUN IR-192 l.089E-01 3.924E-01 3.955E-01 FAIL ABUN HG-203 -9 .161E-01 2.069E+OO 2. llOE+OO FAIL ABUN BI-207 2. 596E-02 4.649E-02 4.794E-02 FAIL ABUN PB-210 l.035E+OO 2.468E+OO 2.512E+OO NOT IDENT. BI-211 2.216E+OO 5.264E-01 1.129E:+OO FAIL ABUN PB-211 2.257E-01 5. 096E-01 5 .196E-Ol FAIL ABUN BI-212 4.770E-01 9.312E-01 9.557E-01 FAIL ABUN RN-219 -7.130E-02 3. 351E-01 3.367E-01 FAIL ABUN RA-223 4.393E-02 5.413E-01 5.417E-01 FAIL ABUN AC-227 -4.093E-02 1.945E-01 l.953E-01 NOT IDENT. TH-227 -4.093E-02 1.945E-01 l.953E-01 NOT IDENT. TH-229 6.714E-02 4.220E-01 4.231E-01 FAIL ABUN TH-231 4.393E-02 5.413E-01 5.417E-01 FAIL ABUN PA-233 8.350E-03 5.037E-02 5.051E-02 NOT IDENT. PA-234 8.053E-02 2.504E-01 2.530E-01 NOT IDENT. PA-234M -6.592E-01 3.984E+OO 3.995E+OO NOT IDENT. NP-237 8.350E-03 5.037E-02 5.051E-02 NOT IDENT. NP-238 8. 921E+40 4.010E+41 O.OOOE+OO SHORT HLIF NP-239 9.356E-02 2.180E-01 2.221E-01 NOT IDENT. PU-239 6.753E+02 7.343E+02 7.949E+02 FAIL ABUN AM-241 -8.491E-03 1.182E-01 l.183E-01 NOT IDENT. CM-243 2.499E-02 8.368E-02 8.444E-02 NOT IDENT. BK-247 -4.901E-02 7.146E-02 7.480E-02 NOT IDENT. CM-247 -2.554E-03 2.982E-02 2.984E-02 NOT IDENT. CF-249 1. 748E-02 3.443E-02 3.532E-02 FAIL ABUN CF-251 1.018E-01 9.572E-02 1.061E-01 NOT IDENT. Page 3406 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 61.8428 87.09 102.2612 136.47 64.7451 45.60 62.2083 87.57 102.3518 140.51 0.0000 46.54 63.3312 88.03 102.4387 143.76 72.2641 49. 72 0.0000 88.34 102.4966 144.24 70.0137 51. 35 74.8469 88.47 102.5211 145.44 60.9278 51. 87 68.1345 89. 96 95.0544 152.43 64.9585 52.39 69.2008 1093.63 95.1711 153.25 0.0000 52.97 74.1842 91.11 0.0000 323.87 67.4298 53.44 75.2502 92. 59 70.7438 156.02 0.0000 54.07 73.4127 93.35 70.8389 158.56 0.0000 57.36 0.0000 94.56 53.9524 159.00 85.3753 57.53 81. 9412 94.65 53. 9609 162.33 76.3286 57.98 82.0299 94.67 53. 9628 162.66 0.0000 59.27 77.9876 94.87 53.9818 163.33 72.8937 59.32 77.9969 97.43 77.0515 165.86 75.4746 59.54 84.6510 98.43 69.6799 176.31 64.4645 60. 96 86.2613 98.44 69.6809 176.60 0.0000 61.17 84.9756 99.53 71.9578 177.52 43.0356 62.93 92.9871 100 .11 77.4036 181.07 0.0000 63.29 93.0635 102.03 78.7321 181.52 49.6352 63.58 93.1251 103.18 66.9956 184.41 67.4647 64.28 92.2697 103.37 67.0169 143.76 67.5621 66.73 99.4977 105.21 74.8086 193.51 59.6201 67.24 95.9074 105.31 74.8207 197.03 62.2862 125.81 90.2739 106.12 68.4049 198.01 47.6800 67.75 90.287:! 106.47 73.8754 201.83 56.4633 69.67 94.7226 109.28 61.1137 203.43 60.2459 70.83 93.6003 111. 00 75.5056 205.31 52.5605 72. 81 81.7303 111.76 0.0000 210.85 37.9917 72. 87 81.7407 114. 06 52.7769 215.65 51. 0373 74.66 97.0840 116. 30 0.0000 222 .11 62.6366 74.82 97 .1158 116.74 60.3543 227.09 57.9029 74.97 97.1461 119.76 56.5633 227.38 57.9190 77 .11 97.5672 121.12 53.3438 228.16 0.0000 78.74 97.8843 121. 22 54.4633 228.18 57. 9633 79.69 103.5927 121.78 71.1948 116.74 57. 9633 80.12 100.9149 122.06 73.4499 235.69 39.3399 80.19 0.0000 122.92 63.5144 235. 96 41.8882 80.57 101.0040 123.07 63.5284 238.63 81. 4395 81. 00 113.5508 265.00 69.1625 238.98 0.0000 81. 07 113.5666 125.81 85.0431 240.99 117.3233 81. 75 83.2068 127.23 74.0040 242.00 49.7807 83.79 84.9243 127.91 74.0765 244.70 47.3441 84.00 84.9584 129.30 74.2228 252.40 0.0000 85.43 94. 9630 131. 20 70.6635 252.80 39.9553 86.55 109.1559 133.02 67.8287 254.15 0.0000 86.79 102.2040 133.52 75.4181 256.23 49.9877 86. 94 102.2330 136.00 68.1088 260.90 0.0000 Page 3407 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 57.2988 355.39 0.0000 584.27 25.4238 264.80 57.3069 356.01 39.1041 595.83 0.0000 265.00 54.7110 364.49 0.0000 427.87 25.6182 268.22 37.4448 366.42 0.0000 602.52 0.0000 269.46 37.4841 372. 51 32. 0113 604.72 14.4377 270.03 37.5025 375.05. 23.5774 607.14 19.2715 271. 23 37.5401 377.52 32.1178 609.32 18.2195 273.65 0.0000 356.01 36.9941 610.33 18.2278 276.40 44.7173 388.16 30.4388 614.28 20.9457 277.37 47.3851 388.63 0.0000 618.01 21.5194 277.60 52. 6611 391. 69 38.1348 620.36 18.3108 278.00 40.8256 264.66 31. 6411 621. 93 14.0125 279.20 40.8663 401. 81 32.6235 630.19 0.0000 279.54 51. 4267 402.40 29.7563 631.29 19.4832 279.70 51.4327 404.85 20.1882 633.25 8.6667 280.46 44.8668 410.95 36.6702 634.78 0.0000 283.69 33.0780 413.71 29.9663 635.95 20.6081 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 34.4487 423.72 0.0000 645.85 17.4297 285.90 0.0000 427.09 21. 4396 657.76 21.3527 287.50 42.4707 427.87 30.2249 657.90 0.0000 290.67 38.5864 433.94 35.2273 661.66 27. 9695 293.27 0.0000 439.40 31. 4141 664.57 0.0000 351. 93 38.7263 453.88 21.7793 666.33 0.0000 295. 96 38.7493 l!63.37 21. 8971 666.50 0.0000 879.38 29.4564 468.07 19.1609 667.71 0.0000 299.98 33.5098 473.00 0.0000 677.62 11. 0429 300.09 33.5129 475.06 17.0315 685.70 0.0000 300.13 33.5144 476.78 18.0505 695.00 0.0000 301.36 33.5464 477.60 15.0488 696.49 14.4690 302.85 33.5854 482.18 21.1218 696. 51 14.4690 256.23 33.6281 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18.9272 306.78 36.3826 497.08 19.2648 697.49 22.2689 308.46 29.1430 505.52 18.3329 702.65 18. 9687 311. 90 36.0742 507.63 0.0000 706.68 16.7645 316.51 30.7696 511. 00 20.4285 711. 68 16.7987 319.41 0.0000 514.00 20.4606 720.70 0.0000 320.08 0.0000 514.00 20.4606 721.93 0.0000 321.04 36.3224 520.40 16.4232 722. 78 25.3107 323.87 42.7687 520.69 0.0000 722. 91 25.3125 325.23 51. 0086 522.65 0.0000 723.31 25.3162 328.76 0.0000 527.90 0.0000 724.19 20.2603 333.37 35.7357 528.26 20.6120 727. 33 19.1582 333.97 33.0015 529.59 24.7510 733.00 13.5542 334.37 31.6355 529.87 0.0000 735.93 18.0931 338.28 36.7814 531.02 0.0000 333.97 16. 9727 338.32 36.7830 537.26 0.0000 739.50 0.0000 311. 90 41.4441 546.56 0.0000 747.24 22. 7165 340.48 41.4441 552.55 20.8643 748.06 9.0895 340.55 0.0000 563.25 17.8280 752.31 21. 6232 344.28 35.0916 569.33 18.9324 753.82 0.0000 345.93 31. 0646 946.00 18.9338 756.73 20.5203 351.06 36.1872 569.70 15.7794 756.80 20.5210 351.93 36.2086 583.19 25.4102 884.68 19.4342 Page 3408 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 28.6001 1274.44 14.8569 1620.50 3.2587 766.42 26.3186 1001.03 14.8789 1621.92 5.4327 766.84 21. 7445 1002.74 19.5388 1678.03 0.0000 772.60 0.0000 1004.73 18.6200 1690.97 5.5096 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 O.QOOO 1025.87 0.0000 1764..49 3.3539 778.90 18.3952 1028.54 0.0000 1063.66 1.1192 783.70 0.0000 1037.84 11. 2844 1771.35 3.3583 785.37 20.7451 1038.76 0.0000 1791.20 0.0000 792.07 26.5741 631. 2 9 12.2573 1808.65 5. 4117 794.95 18.5059 1048.07 0.0000 1810.72 0.0000 795.86 19.6694 1049.04 9.0580 1836.06 0.9066 810.06 16.2832 1050.41 13.5923 810.29 16.2843 1063.66 12.3192 344.28 20.9385 1077.00 0.0000 810.76 20.9407 1077.34 14.2712 815.77 0.0000 1085.87 11. 4448 1048.07 0.0000 1093.63 19.1174 832.01 15.4747 1099.45 10.7242 834.85 11.2656 1112. 07 19.2188 835. 71 12.9126 1112. 84 7.6890 836.80 0.0000 1115. 54 12.3117 846.75 0.0000 1120.29 11. 557 6 846.77 15.5563 1120.55 11. 5591 856.80 0.0000 1221.41 4.6245 860.56 8.8815 1129. 67 12.3609 871.09 10. 6967 1131.51 0.0000 873.19 8.9203 1147.95 0.0000 875.33 0.0000 1173.23 23.4565 879.38 6.2577 1177.95 18.5930 880.51 12.5200 1189.05 15.7041 883.24 6.2658 1204.77 20.6988 884.68 13.4335 1221.41 12.8699 889.28 11. 6602 1231. 02 16.8713 894.76 15.2766 1235.36 0.0000 898.04 13.4944 1238.28 16.9035 900.72 20.7097 1260.41 0.0000 903.28 17.1225 1271.87 7.0205 911.20 10.8431 1274.44 8.0288 912.08 10.8461 1274.54 8.0288 923.98 0.0000 1291.59 9.0714 926.50 13.6226 1298.22 0.0000 929 .11 14.5430 1312 .11 0.0000 937.49 20. 9631 1332.49 5.0909 944.13 0.0000 1362.66 0.0000 946.00 10.9673 1365.19 5.1312 949.00 13. 7224 1368.63 0.0000 667. 71 0.0000 1384.29 7. 216.6 962.31 8.8198 1408. 01 2.0734 964.08 11.7664 1457.56 0.0000 966 .17 11. 0383 1460.82 7.3452 911.20 10.3'117 1489.16 3.1681 968*. 97 10.3117 1505.03 3.1793 983.53 0.0000 1584.12 8. 6240 984.45 0.0000 1596.21 0.0000 ,i*, Pa.ge 3409 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:58:59.00 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM18.CNF;511 Background date : Z-OCT-2016 11:01:02. Sample date 8-DEC-2015 13:43:00. Acquisition date : 3-0CT-2016 08:58:12. Sample ID G405235022 Sample quantity : 1.61105E+02 GRAM Detector name : GAM18 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.02 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 0 0 0 0 0 0 3. 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3410of5809 Energy 49.57 62.89* 74.91 77.20* 87.32 92.44* 129.60 143.83* 185.90* 208.76 238.82* 241.79 270.17 295.64* 300.66 338.90* 352.34* 453.32* 463.59 511. 57* 571. 35 583.63* 609.67* 641.46 662.21 667.87 683.97 708.81 728. 24 769.01 863.01 912.06* 969.92* 997.10 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 34 53 129 212 74 192 52 10 71 49 504 145 50 152 39 96 346 13 31 103 24 220 270 25 364 39 25 24 62 26 25 86 85 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 109 191 187 178 143 306 285 137 201 105 106 111 111 141 89 119 102 57 69 85 50 60 82 19 68 17 12 55 28 32 35 55 31 25 1. 03 2.02 1.14 1.15 1.17 1. 65 4.07 0.85 1. 52 1. 53 1. 21 1. 81 1. 55 1. 37 1. 47 1. 22 1. 48 1.11 1.13 2.85 2.91 1. 63 1. 72 3.12 1. 55 0.89 1. 33 4.85 1. 68 2.53 1. 35 1. 44 2.05 0.55 99.98 126.58 150.61 155.18 175.42 185.63 259.90 288.33 372.40 418.09 478.16 484.10 540.82 591. 71 601. 7 5 678.18 705.04 906.86 927.38 1023.28 1142. 77 1167. 31 1219.35 1282.88 1324.36 1335.69 1367.87 1417.52 1456.36 1537.84 1725.74 1823.79 1939.45 1993.80 97 122 146 146 173 179 252 285 366 415 473 473 535 585 597 671 697 900 924 1015 1135 1158 1211 1275 1316 1331 1363 1408 1449 1532 1716 1817 1933 1983 6 9.48E-03 51.4 9 1.47E-02 50.0 15 3.59E-02 19.7 15 5.90E-02 12.9 6 2.04E-02 28.3 15 5.33E-02 21.7 15 1.44E-02 72.5 7 2.88E-03194.l 12 l.97E-02 42.9 7 1. 35E-02 37. 8 16 1.40E-01 5.7 16 4.03E-02 16.9 12 1.40E-02 44.1 12 4.23E-02 17.8 10 1.08E-02 48.8 14 2.68E-02 26.7 16 9.61E-02 8.6 10 3. 71E-03113. 0 9 8.56E-03 51.5 23 2.85E-02 28.2 14 6.58E-03 67.8 16 6.12E-02 10.6 18 7.51E-02 10.1 13 6.86E-03 42.0 16 1. OlE-01 7. 3 13 1.08E-02 26.7 9 6.87E-03 33.2 17 6.54E-03 75.2 16 1. 73E-02 22. 8 11 7.19E-03 47.1 14 7.02E-03 53.5 11 2.39E-02 18.1 13 2.35E-02 17.9 12 2.28E-03130.3 Fit 1. 08E+00 9.60E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235022 Acquisition date 3-0CT-2016 08:58:12 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1054.81 8 47 5.05 2109.15 2091 23 2.30E-03215.8 36 0 1062.39 9 15 1. 04 2124.31 2116 11 2.48E-03 93.4 'J7 0 1065.22 .12 8 0.64 2129. n. 2126 8 3.22E-03 51.7 38 0 1121.22* 41 28 1. 63 2241. 92 2234 16 1. 14E-02 33. 8 39 0 1188 .16 15 18 0.54 2375.75 2368 14 4.23E-03 63.8 40 0 1239.27 20 27 3.66 2477.93 2470 12 5.58E-03 56.3 41 0 1270.17 37 11 8.03 2539.71 2529 21 1. OlE-02 27. 7 42 0 1314.97 14 0 1. 29 2629.29 2625 9 3.89E-03 26.7 43 0 1337 .14 11 18 0.96 2673.60 2663 16 2. 96E-03 98.0 44 0 1378.49 39 10 2.65 2756.28 2745 17 1.09E-02 23.6 45 0 1406.28 6 17 1. 31 2811. 83 2801 17 1.67E-03162.7 46 0 1411.65 5 6 0.61 2822.57 2817 9 l.34E-03106.2 47 0 1461.65* 587 6 2.57 2922.55 2911 24 1. 63E-01 4.3 48 0 1503.19 7 8 0.70 3005.60 2998 12 l.82E-03 98.7 49 0 1590.82 15 13 1.13 3180.82 3173 14 4.15E-03 58.8 50 0 1765.46* 66 0 1. 63 3530.04 3520 18 l.83E-02 13.2 Flag: "*" = Peak area was modified by background subtraction Page 3411of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:59:00 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 8-DEC-2015 13:43:00 G405235022 Acquisition date : Sample quantity : 3-0CT-2016 08:58:12 161.10 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA18 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 *74. 82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3412of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:01.02 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235022 Acquisition date 3-0CT-2016 08:58:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* L. 911E+OO l.305E+Ol l.305E+Ol 8.61 OK CD-109 88.03 3.70* 6.143E+OO 1.288E+OO 2.021E+OO 89.80 OK SN-126 64.28 9.60 3.037E+OO 1.155E+OO 1.155E+OO 100.06 OK 86.94 8.90 6.143E+OO 5.354E-01 5.354E-01 89.80 OK 87.57 37.00* 6.143E+OO 1.288E-01 1. 28 8E-01 89.80 OK BA-137M 661. 66 89.90* 3.370E+OO 5.994E-01 6.109E-01 14.57 OK CS-137 661.66 85.10* 3.370E+OO 6.332E-01 6.453E-01 14.57 OK TL-208 277.37 6.60 6.127E+OO Line Not Found Absent 583.19 85.00* 3.675E+00 3.568E-01 3.568E-01 21.15 OK 860.56 12.50 2.814E+OO Line Not Found Absent BI-211 72. 87 1.23 4.495E+OO Line Not Found Absent 351. 06 12.92* 5.217E+OO 6. 331E-01 6. 331E-01 140.40 OK PB-212 74.82 10.28 4.764E+OO l.217E+OO 1.217E+OO 54.80 OK 77 .11 17.10 5. 051E+OO 1.533E+OO 1.533E+OO 25.72 OK 238.63 43.60* 6.720E+OO 9.605E-01 9.605E-01 11. 41 OK 300.09 3.30 5.811E+OO 1.102E+OO l.102E+OO 97.69 OK BI-214 609.32 45.49* 3.566E+OO 8.388E-01 8. 391E-01 20.12 OK 1120.29 14.92 2.335E+OO 5.509E-01 5. 511E-01 67. 60 OK 1764.49 15.30 1.633E+OO 1.167E+OO 1.168E+OO 26.46 OK PB-214 74.82 5.80 4.752E+OO Line Not Found <<INT Reject 77 .11 9.70 5. 051E+OO 2.703E+00 2.704E+OO 25.72 OK 87.09 3.41 6.121E+00 Line Not Found <<INT Reject 242.00 7.25 6.668E+OO Line Not Found <<INT Reject 295.22 18.42 5.877E+OO 7.669E-01 7.672E-01 35.62 OK 351. 93 35.60* 5. 221E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 3.566E+OO 8.388E-01 8.391E-01 20.12 OK 1120.29 14.92 2.335E+OO 5.509E-01 5. 511E-01 67.60 OK 1764.49 15.30 l.633E+OO 1.167E+OO 1.168E+OO 26.46 OK RA-224 240.99 4.10* 6.671E+OO 1.597E+OO 1.597E+OO 69.38 OK RA-226 609.32 45.49* 3.566E+OO 8.388E-01 8. 391E-01 20.12 OK 1120.29 14.92 2.335E+OO 5.509E-01 5.511E-01 67. 60 OK 1764.49 15.30 1.633E+OO 1.167E+OO 1.168E+OO 26.46 OK AC-228 105.21 1.10 7.385E+OO Line Not Found Absent 338.32 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 OK 794.95 4.25 2.973E+OO Line Not Found Absent 835.71 1. 61 2. 872E+OO Line Not Found Absent 911. 20 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 OK 968. 97 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 OK RA-228 105.21 1.10 7.385E+OO Line Not Found Absent 338.32 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 OK 794.95 4.25 2.973E+OO Line Not Found Absent 835.71 1. 61 2. 872E+OO Line Not Found Absent 911. 20 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 OK 968. 97 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 OK TH-228 74.82 10.28 4.764E+OO 1.217E+OO 1.217E+OO 54.80 OK 77 .11 17.10 5. 051E+OO 1.533E+OO 1.533E+OO 25.72 OK 238.63 43.60* 6.720E+OO 9.605E-01 9.605E-01 11. 41 OK 300.09 3.30 5. 811E+OO 1.102E+OO 1.102E+OO 97.69 OK TH-230 609.32 45.49* 3.566E+OO 8.388E-01 8.388E-01 20.12 OK Page 3413 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235022 Acquisition date 3-0CT-2016 08:58:12 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 2. 3.35E+OO 5.509E-01 5.509E-01 67.60 OK4 1764.49 15.30 1.633E+OO 1.167E+OO 1.167E+OO 26.46 OK PA-231 283.69 1. 70 6.038E+OO Line Not Found Absent 301.36 5.35* 5. 811E+OO 6.797E-01 6.797E-01 97.69 OK TH-232 105.21 1.10 7.385E+OO Line Not Found Absent 338.32 11.27 5.359E+OO 8.573E-01 8.573E-01 53.48 OK 835.71 1. 61 2. 872E+OO Line Not Found Absent 911.20 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 OK 968. 97 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 OK TH-234 63.29 3.70* 3.037E+OO 2. 996E+OO 2. 996E+00 100.06 OK 92.59 4.23 6.582E+00 4.229E+00 4.229E+OO 43.37 OK U-234 609.32 45.49* 3.566E+OO 8.388E-01 8.388E-01 20.12 OK 1120.29 14.92 2.335E+OO 5.509E-01 5.509E-01 67.60 OK 1764.49 15.30 1.633E+OO 1.167E+OO 1.167E+OO 26.46 OK U-235 89.96 3.47 6.379E+00 Line Not Found Absent 93.35 5.60 6.582E+OO 3.195E+OO 3.195E+OO 43.37 OK 143.76 10. 96* 8.086E+OO 6. 871E-02 6. 871E-02 388.16 OK 163.33 5.08 7.938E+OO Line Not Found Absent 185. 72 57.20 7.616E+OO 9.318E-02 9.318E-02 85.87 OK 205.31 5.01 7.289E+OO Line Not Found Absent U-238 63.29 3.70* 3.037E+OO 2.996E+OO 2. 996E+OO 100.06 OK 92.59 4.23 6.582E+OO 4.229E+00 4.229E+OO 43.37 OK AM-243 43.53 5.90 3.443E-01 Line Not Found -----Absent 74.66 67.20* 4.764E+OO 1. 8 62E-01 l.862E-01 54.80 OK ANH-511 511. 00 100.00* 4.026E+OO 1.308E-01 l.308E-01 56.43 OK Flag: "*" = Keyline Page 3414of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:59:01.76 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l *
  • Acquisition date 3-0CT-2016 08:58:12 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 1.500 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.02 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:43:00 Analyst initials: MXRl *
  • Sample ID G405235022 Sample Quantity 1.6110E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.305E+Ol 1.101E+OO CD-109 2.021E+OO 1.778E+OO SN-126 1.288E-01 1.133E-01 BA-137M 6.109E-01 8.723E-02 CS-137 6.453E-01 9.215E-02 TL-208 3.568E-01 7.397E-02 BI-211 6. 331E-01 8.711E-01 PB-212 9.605E-01 1. 074E-01 BI-214 8.391E-01 l.655E-01 PB-214 9.970E-01 l.682E-01 RN-222 8.391E-01 l.655E-01 RA-224 1.597E+OO 1.086E+OO RA-22 6 8.391E-01 l.655E-01 AC-228 5.926E-01 2.107E-01 RA-228 5.926E-01 2.107E-01 TH-228 9.605E-01 1.074E-01 TH-230 8.388E-01 1.654E-01 PA-231 6.797E-01 6.507E-01 TH-232 5.926E-01 2.107E-01 TH-234 2. 996E+OO 2.938E+OO U-234 8.388E-01 1.654E-01 U-235 6.871E-02 2.614E-01 U-238 2.996E+OO 2.938E+OO AM-243 l.862E-01 9.999E-02 ANH-511 l.308E-01 7.232E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3415of5809 Key-Line Activity (pCi/GRAM -7. 641E+OO 3.943E-02 O.OOOE+OO -1.490E-02 6.926E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1.071E+Ol 3.860E-02 1. 779E+41 2.491E-02 3.070E-01 MDA (pCi/GRAM 3.806E-01 1. 651E+OO l.097E-01 5. 719E-02 6.041E-02 4.492E-02 2.554E-01 7.630E-02 8.939E-02 2.454E-01 8.939E-02 8.172E-01 8.939E-02 2.003E-01 2.003E-01 7.630E-02 8.936E-02 6.233E-01 2.003E-01 2 .115E+OO 8.936E-02 2.565E-01 2 .115E+OO 8.044E-02 3.680E-02 MDA (pCi/GRAM 1.808E+Ol 7.597E-02 O.OOOE+OO 4.378E-02 5.862E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1.065E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.331E+02 O.OOOE+OO SHORT HLIF MN-54 -3 .136E-02 4.802E-02 8.224E-02 NOT IDENT. C0-56 1.704E-02 3.528E-01 6.658E-01 FAIL ABUN MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 -l.302E-02 3.740E-02 6.907E-02 NOT IDENT. C0-58 -7.lOlE-02 3.817E-01 7.107E-01 NOT IDENT. FE-59 -4.991E-01 4.655E+OO 8. 911E+OO NOT IDENT. C0-60 2.140E-02 3.225E-02 6.121E-02 NOT IDENT. ZN-65 . 1.107E-01 1.388E-01 2. 641E-01 NOT IDENT. GE-68 -l.237E-01 1.867E+OO 3.553E+OO NOT IDENT. AS-73 -1.057E+OO 8. 772E+OO 1. 794E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.756E+03 O.OOOE+OO SHORT HLIF SE-75 1.514E-01 l.540E-01 2.998E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 917E+37 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 5.434E+02 O.OOOE+OO SHORT HLIF RB-83 -4.114E-02 5.068E-01 8.734E-01 NOT IDENT. KR-85 1.121E+Ol 5.744E+OO 1.269E+Ol NOT IDENT. SR-85 1.180E+OO 6.063E-01 1.340E+OO NOT IDENT. RB-86 O.OOOE+OO 2.255E+04 O.OOOE+OO SHORT HLIF Y-88 2.032E-02 l.233E-01 2.749E-01 NOT IDENT. Y-91 2.861E+02 4.316E+02 8.710E+02 NOT IDENT. NB-94 -1. 750E-02 2.858E-02 4.325E-02 NOT IDENT. NB-95 6.325E-01 6.446E-01 1.243E+OO NOT IDENT. NB-95M l.835E-01 l.983E+OO 3.507E+OO NOT IDENT. ZR-95 8.519E-02 1.015E+OO 1.956E+OO NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 1'. 081E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 34 7E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 1.447E-02 2.823E-02 5.500E-02 NOT IDENT. RH-102 l.531E-02 4. 391E-02 8.780E-02 NOT IDENT. RU-103 -8.813E-01 4.179E+OO 7.984E+OO FAIL ABUN RH-106 -2.326E-01 3.658E-01 6.570E-01 NOT IDENT. RU-106 -2.326E-01 3.658E-01 6.570E-01 NOT IDENT. AG-108M -3.131E-03 2.150E-02 3.932E-02 NOT IDENT. AG-llOM -2.253E-02 7.881E-02 1.412E-01 NOT IDENT. SN-113 -5.019E-02 l.896E-01 3.448E-01 NOT IDENT. CD-115 0.000E+OO 2.304E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.166E+04 O.OOOE+OO SHORT HLIF TE-123M 2.086E-03 l.104E-01 2.029E-01 NOT IDENT. SB-124 -3.345E-01 1.404E+OO 2.741E+OO NOT IDENT. SB-125 -4.372E-02 8.373E-02 l.468E-01 FAIL ABUN TE-125M 4.863E+Ol 2.185E+o2 4.261E+02 NOT IDENT. I-126 O.OOOE+OO 4.917E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.456E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.716E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.865E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 5.235E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.748E+26 O.OOOE+OO SHORT HLIF BA-133 8.277E-03 3.078E-02 5.433E-02 NOT IDENT. I-133 O.OOOE+OO 1.827E+41 O.OOOE+OO SHORT HLIF CS-134 3.357E-02 4.044E-02 8.303E-02 NOT IDENT. CS-135 8 .114E-02 1.129E-01 2.107E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.278E+05 O.OOOE+OO SHORT HLIF CE-139 -5.266E-02 9.230E-02 1.610E-01 NOT IDENT. BA-140 O.OOOE+OO 9. 051E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.185E+05 O.OOOE+OO SHORT HLIF CE-141 -9.646E+OO 2.254E+Ol 3.736E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -9.676E-02 3.061E-01 5.139E-01 NOT IDENT. PM-144 -2.033E-02 4.393E-02 7.904E-02 NOT IDENT. PR-144 -1. 7 40E+00 3.819E+OO 6.876E+OO NOT IDENT. PM-146 2.708E-02 5.998E-02 6.557E-02 FAIL ABUN ND-147 0.000E+OO 2.453E+07 O.OOOE+OO SHORT HLIF PM-147 -5.706E+Ol 6.450E+02 1.218E+03 NOT IDENT. PM-149 O.OOOE+OO 3.512E+40 O.OOOE+OO SHORT HLIF EU-150 1.750E-03 2.173E-02 3. 718E-02 FAIL ABUN EU-152 4 .113E-02 8.247E-02 1.470E-01 NOT IDENT. GD-153 4.647E-02 1.481E-01 2.739E-01 NOT IDENT. EU-154 9.519E-02 9.444E-02 1.856E-01 FAIL ABUN EU-155 6.081E-02 8.556E-02 1. 733E-01 FAIL ABUN TB-160 1. 774E-01 l.284E+00 2.476E+OO FAIL ABUN H0-166M 2.500E-02 5.246E-02 9.261E-02 FAIL ABUN TM-171 -1. 511E+OO 2.280E+Ol 4.364E+Ol NOT IDENT. HF-172 -4.209E-02 2 .115E-01 3.609E-01 FAIL ABUN LU-172 3.188E-02 5.934E-02 l.209E-01 FAIL ABUN Page 3416of5809 LU-176 -2.564E-03 1.836E-02 3.478E-02 FAIL ABUN HF-181 1.596E+OO 3 .138E+OO 6.153E+OO NOT IDENT. TA-182 5.369E-01 7. 361E-01 1.495E+00 FAIL ABUN RE-183 -1.204E+OO 2.910E+OO 5,768E+OO NOT IDENT. RE-184 -1.555E+Ol 2.253E+Ol 3.786E+Ol NOT IDENT. W-188 -5.736E+Ol 9.789E+Ol l.578E+02 FAIL ABUN IR-192 -1. 320E-01 3.467E-01 6. 411E-01 FAIL ABUN HG-203 l.057E+OO 1. 774E+OO 3.582E+OO NOT IDENT. BI-207 2.360E-02 4". 321E-02 7.362E-02 FAIL ABUN PB.,-210 -2.609E+OO 4.585E+DO 8.442E+.00 NOT IDENT. PB-211 -1.065E-01 5.620E-01 l.024E+OO NOT IDENT. BI-212 O.OOOE+OO 6.523E-01 9.123E-01 FAIL ABUN RN-219 -1.002E-01 2.939E-01 5.301E-01 FAIL ABUN RA-223 3.255E-01 4.306E-01 8.751E-01 FAIL ABUN AC-227 -l.191E-01 1.771E-01 3.270E-01 FAIL ABUN TH-227 -1.191E-01 l.771E-01 3.270E-01 FAIL ABUN TH-229 2. 710E-02 3.335E-01 6.695E-01 FAIL ABUN TH-231 3.255E-01 4.306E-01 8. 7 51E-01 FAIL ABUN PA-233 3.015E-02 4.366E-02 8.856E-02 FAIL ABUN PA-234 -5.054E-02 2.023E-01 3.845E-01 NOT IDENT. PA-234M 2.969E+OO 3.274E+OO 6.539E+OO NOT IDENT. NP-237 3.015E-02 4.366E-02 8.856E-02 FAIL ABUN NP-238 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -6.413E-02 1.986E-01 3.688E-01 NOT IDENT. PU-239 O.OOOE+OO 8. 641E+02 5.285E+02 FAIL ABUN AM-241 3.422E-02 1. 381E-01 2.661E-01 NOT IDENT. CM-243 -5.287E-02 7.496E-02 1.370E-01 NOT IDENT. BK-247 7.490E-02 5.094E-02 1.045E-01 NOT IDENT. CM-247 l.157E-02 2.629E-02 5.127E-02 NOT IDENT. CF-249 1.428E-02 2.762E-02 5.454E-02 NOT IDENT. CF-251 4.262E-02 8.960E-02 1.697E-01 NOT IDENT. Page 3417 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:58:59.70 Nuclide Line Activity Report
  • Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 570 10.66* 1. 911E+OO 1.305E+Ol 1.305E+Ol 8.61 CD-109 88.03 97 3.70* 6.143E+OO 1.995E+OO 3.129E+OO 56.59 SN-126 64.28 72 9.60 3.037E+OO l.155E+OO 1.155E+OO 100.06 86.94 97 8.90 6.143E+OO 8.292E-01 8.292E-01 56.59 87.57 97 37.00* 6.143E+OO 1.995E-01 l.995E-01 56.59 BA-137M 661.66 390 89.90* 3.370E+OO 5.994E-01 6.109E-01 14.57 CS-137 661.66 390 85.10* 3.370E+OO 6.332E-01 6.453E-01 14.57 TL-208 277.37 ------6.60 6.127E+OO ------Line Not Found ------583.19 239 85.00* 3.675E+OO 3.568E-01 3.568E-01 21.15 860.56 ------12.50 2.814E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 4.495E+OO ------Line Not Found ------351.06 397 12.92* 5.217E+00 2.746E+00 2.746E+OO 17.22 PB-212 74.82 173 10.28 4.764E+OO 1.650E+OO 1.650E+OO 39.33 77 .11 284 17.10 5. 051E+OO l.533E+OO 1.533E+OO 25.72 238.63 604 43.60* 6.720E+OO 9.605E-01 9.605E-01 11. 41 300.'09 45 3.30 5. 811E+00 1.102E+00 1.102E+OO 97.69 BI-214 609.32 292 45.49* 3.566E+OO 8.388E-01 8.391E-01 20.12 1120.29 41 14.92 2.335E+OO 5.509E-01 5. 511E-01 67.60 1764.49 63 15.30 l.633E+00 l.167E+00 1.168E+OO 26.46 PB-214 74.82 173 5.80 4.764E+OO 2.924E+OO 2.925E+OO 39.33 77 .11 284 9.70 5. 051E+OO 2.703E+00 2.704E+OO 25.72 87.09 97 3.41 6.143E+OO 2.164E+OO 2.165E+OO 56.59 242.00 173 7.25 6.671E+OO l.670E+OO 1. 670E+OO 33.76 295.22 178 18.42 5.877E+00 7.669E-01 7.672E-01 35.62 351. 93 397 35.60* 5.217E+00 9. 966E-01 9.970E-01 17. 22 RN-222 609.32 292 45.49* 3.566E+OO 8.388E-01 8. 391E-01 20.12 1120.29 41 14.92 2.335E+00 5.509E-01 5. 511E-01 67.60 1764.49 63 15.30 1.633E+OO l.167E+OO 1.168E+OO 26.46 RA-224 240.99 173 4.10* 6. 671E+OO 2.953E+OO 2.953E+00 33.76 RA-226 609.32 292 45.49* 3.566E+OO 8.388E-01 8. 391E-01 20.12 1120.29 41 14.92 2.335E+OO 5.509E-01 5. 511E-01 67.60 1764.49 63 15.30 1.633E+00 1.167E+OO 1.168E+OO 26.46 AC-228 105.21 ------1.10 7.385E+OO ------Line Not Found ------338.32 111 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 794.95 ------4.25 2.973E+OO ------Line Not Found ------835. 71 ------1. 61 2.872E+OO ------Line Not Found ------911. 20 89 25.80* 2.703E+00 5.926E-01 5.926E-01 36.28 968. 97 87 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 RA-228 105.21 ------1.10 7.385E+OO ------Line Not Found ------338.32 111 11. 27 5.359E+OO 8.573E-01 8.573E-01 53.48 794.95 ------4.25 2.973E+00 ------Line Not Found ------835.71 ------1. 61 2.872E+OO ------Line Not Found ------911. 20 89 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 968.97 87 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 TH-228 74.82 173 10.28 4.764E+OO 1.650E+OO l.650E+OO 39.33 77 .11 284 17.10 5. 051E+OO 1.533E+OO l.533E+00 25.72 238.63 604 43.60* 6.720E+OO 9.605E-01 9.605E-01 11. 41 Page 3418of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235022 Acquisition date 3-0CT-2016 08:58:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Ef f pCi/GRAM pCi/GRAM %Error 300.09 45 3.30 5. 811E+OO 1.102E+OO 1.102.E+OO 97. 69 TH-230 609.32 292 45.49* 3.566E+OO 8.388E-01 8.388E-01 20.12 1120.29 41 14.92 2.335E+OO 5.509E-01 5.509E-01 67.60 1764.49 63 15.30 l.633E+OO 1.167E+OO 1.167E+OO 26.46 PA-231 283.69 ------1. 70 6.038E+OO ------Line Not Found ------301.36 45 5.35* 5.811E+OO 6.797E-01 6.797E-01 97. 69 TH-232 105.21 ------1.10 7.385E+OO ------Line Not Found ------338.32 111 11.27 5.359E+OO 8.573E-01 8.573E-01 53.48 835.71 ------1. 61 2. 872E+OO ------Line Not Found ------911.20 89 25.80* 2.703E+OO 5.926E-01 5.926E-01 36.28 968. 97 87 15.80 2.589E+OO 9.865E-01 9.865E-01 35.85 TH-234 63.29 72 3.70* 3.037E+OO 2. 996E+OO 2.996E+OO 100.06 92.59 253 4.23 6.582E+OO 4.229E+OO 4.229E+OO 43.37 U-234 609.32 292 45.49* 3.566E+OO 8.388E-01 8.388E-01 20.12 1120.29 41 14.92 2.335E+OO 5.509E-01 5.509E-01 67.60 1764.49 63 15.30 1.633E+OO 1.167E+OO 1.167E+OO 26.46 U-235 89.96 ------3.47 6.379E+OO ------Line Not Found ------93.35 253 5.60 6.582E+OO 3.195E+OO 3.195E+OO 43.37 143.76 13 10. 96* 8.086E+OO 6. 871E-02 6.871E-02 388.16 163.33 ------5.08 7.938E+OO ------Line Not Found ------185. 72 87 57.20 7.616E+OO 9.318E-02 9.318E-02 85.87 205.31 ------5.01 7.289E+OO ------Line Not Found ------U-238 63.29 72 3.70* 3.037E+OO 2. 996E+OO 2. 996E+OO 100.06 92.59 253 4.23 6.582E+OO 4.229E+OO 4.229E+OO 43.37 AM-243 43.53 ------5.90 3.443E-01 ------Line Not Found ------74.66 173 67.20* 4.764E+OO 2.524E-01 2.524E-01 39.33 ANH-511 511. 00 113 100.00* 4.026E+OO 1.308E-01 l.308E-01 56.43 Flag: "*" Key line Page 3419of5809 Summary of Nuclide Activity Sample ID : G405235022 Acquisition date Page : 3 3-0CT-2016 08:58:12 Total number of lines in spectrum 50 Number of unidentified lines 17 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 'TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y 1. 41E+l0Y 1600. DOY 1600. DOY 1600.00Y l.41E+l0Y 1600.00Y l.41E+l0Y l.41E+l0Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.305E+Ol l.995E+OO l.995E-01 5.994E-01 6.332E-01 3.568E-01 2.746E+OO 9.605E-01 8.388E-01 9. 966E-01 8.388E-01 2.953E+OO 8.388E-01 5.926E-01 5.926E-01 9.605E-01 8.388E-01 6.797E-01 5.926E-01 2. 996E+00 8.388E-01 6. 871E-02 2. 996E+OO 2.524E-01 l.308E-01 3.854E+Ol 3.854E+Ol Decay Corr pCi7GRAM l.305E+Ol 3.129E+OO l.995E-01 6.109E-01 6.453E-01 3.568E-01 2.746E+OO 9.605E-01 8.391E-01 9.970E-01 8.391E-01 2.953E+OO 8. 391E-01 5.926E-01 5.926E-01 9.605E-01 8.388E-01 6.797E-01 5.926E-01 2. 996E+OO 8.388E-01 6. 871E-02 2.996E+OO 2.524E-01 l.308E-01 3.970E+Ol 3.970E+Ol 66.00% Decay Corr 2-Sigma Error 0 .112E+Ol 1. 771E+OO l.129E-01 0.890E-01 0.940E-01 0.755E-01 0.473E+OO 1. 096E-01 l.689E-01 l.717E-01 l.689E-01 0.997E+OO l.689E-01 2.150E-01 2.150E-01 1. 096E-01 l.688E-01 6.640E-01 2.150E-01 2.998E+OO l.688E-01 26.67E-02 2.998E+OO 0.993E-01 0.738E-01 "M" Manually accepted
  • 2-Sigma %Error 8.61 56.59 56.59 14.57 14.57 21.15 17.22 11. 41 20.12 17.22 20.12 33.76 20.12 36.28 36.28 11. 41 20.12 97.69 36.28 100.06 20.12 388.16 100.06 39.33 56.43 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3420 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235022 Acquisition date : 3-0CT-2016 08:58:12 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 49.57 48 152 1. 03 99.98 97 6 9.48E-03 **** 1. OlE+OO T 0 129.60 66 363 4.07 259.90 252 15 l.44E-02 **** 8.04E+OO T 0 208.76 59 127 1. 53 418.09 415 7 1.35E-02 75.7 7.23E+OO 0 270.17 60 131 1. 55 540.82. 535 l-2 1. 40E-02 88.3 6.23E+OO T 0 453.32 15 64 1.11 906.86 900 10 3.71E-03 **** 4.38E+OO T 0 463.59 34 77 1.13 927.38 924 9 8.56E-03 **** 4.31E+OO T 0 571.35 26 55 2.91 1142.77 1135 14 6.58E-03 **** 3.73E+OO 0 641.46 27 21 3.12 1282.88 1275 13 6.86E-03 84.0 3.44E+OO 0 667.87 42 18 0.89 1335.69 1331 13 1.08E-02 53.4 3.35E+OO T 0 683.97 26 13 1. 33 1367.87 1363 9 6.87E-03 66.4 3.30E+OO 0 708.81 25 59 4.85 1417.52 1408 17 6.54E-03 **** 3.22E+00 0 728.24 66 29 1. 68 1456.36 1449 16 1.73E-02 45.5 3.16E+OO T 0 769.01 27 34 2.53 1537.84 1532 11 7.19E-03 94.3 3.04E+00 0 863.01 26 36 1. 35 1725.74 1716 14 7.02E-03 **** 2.81E+OO 0 997.10 8 25 0.55 1993.80 1983 12 2.28E-03 **** 2.54E+OO T 0 1054.81 8 47 5.05 2109.15 2091 23 2.30E-03 **** 2.44E+OO 0 1062.39 9 15 1. 04 2124.31 2116 11 2.48E-03 **** 2.43E+00 T 0 1065.22 12 8 0.64 2129.97 2126 8 3.22E-03 **** 2.42E+00 0 1188.16 15 18 0.54 2375.75 2368 14 4.23E-03 **** 2.24E+OO T 0 1239.27 20 27 3.66 2477.93 2470 12 5.58E-03 **** 2.17E+OO T 0 1270.17 36 10 8.03 2539.71 2529 21 1. OlE-02 55.4 2.13E+OO 0 1314.97 14 0 1. 29 2629.29 2625 9 3.89E-03 53.5 2*. 07E+OO 0 1337.14 10 18 0. 96 2673.60 2663 16 2.96E-03 **** 2.05E+OO 0 1378.49 38 10 2.65 2756.28 2745 17 1. 09E-02 47.2 2.00E+OO 0 1406.28 6 17 1. 31 2811.83 2801 17 1.67E-03 **** 1.97E+OO 0 1411.65 5 6 0.61 2822.57 2817 9 l.34E-03 **** 1. 96E+OO 0 1503.19 6 8 0.70 3005.60 2998 12 1. 82E-03 **** 1. 87E+OO 0 1590.82 14 13 1.13 3180.82 3173 14 4.15E-03 **** 1. 78E+OO Flags: "T" = Tentatively associated Page 3421of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:59:13.78 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l * *Acquisition date 3-0CT-2016 08:58:12 Sensitivity 3.000 *
  • Detector ID . GAM18 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.02 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:43:00 Nuclide Library : SOLID *
  • Sample ID G405235022 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.6110E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.591E-01 7.788E-01 5.186E-02 2.641E-02 2.790E-02 2.037E-02 l.179E-01 3.588E-02 4.068E-02 1.192E-01 4.068E-02 3.843E-01 4.068E-02 9.093E-02 9.093E-02 3.588E-02 4.067E-02 2.903E-01 9.093E-02 9.973E-01 4.067E-02 1.206E-01 9.973E-01 3.806E-02 l.678E_.:.02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3422 of 5809 Le (pCi/GRAM 8.300E+OO 3.425E-02 O.OOOE+OO 1. 793E-02 2.651E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM'-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3423 of 5809 O.OOOE+OO 3.675E-02 2.994E-01 O.OOOE+OO 3.239E-02 3.137E-01 3.945E+OO 2.715E-02 1.194E-01 1.599E+OO 8. 396E+OO O.OOOE+OO 1.397E-01 O.OOOE+OO O.OOOE+OO 3. 960E-01 5.952E+OO 6.281E-01 O.OOOE+OO 1.091E-01 3. 969E+02 1. 962E-02 5.670E-01 1.651E+OO 8.787E-01 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 2.603E-02 4.002E-02 3.643E+OO 2.959E-01 2.959E-01 l.805E-02 6.324E-02 1.597E-01 O.OOOE+OO O.OOOE+OO 9.573E-02 1.123E+OO 6.747E-02 2.006E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.499E-02 O.OOOE+OO 3.817E-02 9. 872E-02 O.OOOE+OO O.OOOE+OO 7.568E-02 O.OOOE+OO 0.000E+OO 1. 765E+Ol O.OOOE+OO 2.413E-01 3.597E-02 3 .130E+OO 3.023E-02 0.000E+OO 5. 715E+02 O.OOOE+OO 1. 730E-02 6.862E-02 1. 289E-01 8.364E-02 8.171E-02 1.101E+OO 4.257E-02 2.041E+Ol 1. 703E-01 5.466E-02 1.615E-02 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IUENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3424 of 5809 2.815E+OO 6. 811E-01 2. 711E+OO 1.673E+Ol 7.344E+Ol 2. 967E-01 1. 676E+OO 3.321E-02 3.958E+OO 4. 7 SlE-01 4.255E-01 2.441E-01 4.076E-01 1.526E-01 1.526E-01 3.144E-01 4.076E-01 4.124E-02 1.719E-01 2. 968E+OO 4.124E-02 O.OOOE+OO 1. 734E-01 2.509E+02 1.254E-01 6.396E-02 4.872E-02 2.371E-02 2.522E-02 7.986E-02 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDEN.T. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:59:19.80 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235022.CNF;l *
  • Acquisition date 3-0CT-2016 08:58:12 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: O 01:00:01.02 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:43:00 Nuclide Library : SOLID *
  • Sample ID G405235022 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : l.6110E+02 GRAM *
  • Quantity Err ( % ) : 1. 2414E-03 % *
  • Wet wt corr 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) K-40 1.305E+Ol l.295E+OO 1. 295E+OO CD-109 2.021E+OO 1. 791E+OO 1. 791E+OO SN-126 1.288E-01 1.140E-01 l.140E-01 BA-137M 6.109E-01 9 .111E-02 9 .111E-02 CS-137 6.453E-01 9.623E-02 9.623E-02 TL-208 3.568E-01 7.551E-02 7. 551E-02 BI-211 6. 331E-01 8.810E-01 8.810E-01 PB-212 9.605E-01 1.188E-01 1.188E-01 BI-214 8.391E-01 l.694E-01 1.694E-01 PB-214 9.970E-01 1.733E-01 1. 733E-01 RN-222 8.391E-01 l.694E-01 1.694E-01 RA-224 1.597E+OO 1.093E+OO 1.093E+OO RA-226 8.391E-01 1.694E-01 1.694E-01 AC-228 5.926E-01 2.129E-01 2.129E::-01 RA-228 5.926E-01 2.129E-01 2.129E-01 TH-228 9.605E-01 1.188E-01 l.188E-01 TH-230 8.388E-01 l.693E-01 1.693E-01 PA-231 6.797E-01 6.667E-01 6.667E-01 TH-232 5.926E-01 2.129E-01 2.129E-01 TH-234 2.996E+OO 3.012E+OO 3.012E+OO U-234 8.388E-01 l.693E-01 1.693E-01 U-235 6. 871E-02 2.614E-01 2.614E-01 U-238 2. 996E+OO 3.012E+OO 3.012E+00 AM-243 l.862E-01 1.0lOE-01 1.0lOE-01 ANH-511 1.308E-01 7. 251E-02 7. 251E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) BE-7 -7.641E+OO 1. 072E+Ol 1.126E+Ol NOT IDENT. NA-22 3.943E-02 3.863E-02 4.252E-02 NOT IDENT. NA-24 l.000E+41 1.832E+41 O.OOOE+OO SHORT HLIF AL-26 -1.490E-02 2.493E-02 2.582E-02 NOT IDENT. SC-46 6.926E-02 3.070E-01 3.086E-01 FAIL ABUN Page 3425 of 5809 V-48 -1. 740E+03 1. 065E+04 1.068E+04 SHORT HLIF CR-51 8.068E+Ol 3. 331E+02 3. 351E+02 SHORT HLIF MN-54 -3.136E-02 4.804E-02 5.008E-02 NOT IDENT. C0-56 1. 704E-02 3.528E-01 3.529E-01 FAIL ABUN MN-56 1.000E+41 1. 8 61E+42 O.OOOE+OO SHORT HLIF C0-57 -l.302E-02 3.741E-02 3.786E-02 NOT IDENT. C0-58 -7.lOlE-02 3.817E-01 3.830E-01 NOT IDENT. FE-59 -4.991E-01 4.655E+OO 4. 661E+OO NOT IDENT. C0-60 2.140E-02 3.226E-02 3.367E-02 NOT IDENT. ZN-65 l.107E-01 1. 389E-01 1. 4 7 6E-01 NOT IDENT. GE-68 -l.237E-01 1. 8 67E+OO l.868E+OO NOT IDENT. AS-73 -l.057E+OO 8.775E+OO 8.788E+OO NOT IDENT. AS-74 -4.091E+03 4.768E+03 5 .113E+03 SHORT HLIF SE-75 l.514E-01 1.542E-01 1. 686E-01 NOT IDENT. BR-77 1. 714E+38 l.484E+39 0.000E+OO SHORT HLIF SR-82 -2.549E+Ol 5.434E+02 5.435E+02 SHORT HLIF RB-83 -4 .114E-02 5.068E-01 5.072E-01 NOT IDENT. KR-85 1.121E+Ol 5.762E+OO 7.665E+OO NOT IDENT. SR-85 1.180E+OO 6.082E-01 8.080E-01 NOT IDENT. RB-86 2.197E+03 2.255E+04 2.257E+04 SHORT HLIF Y-88 2.032E-02 l.233E-01 1.237E-01 NOT IDENT. Y-91 2.861E+02 4.317E+02 4.506E+02 NOT IDENT. NB-94 -1. 7 50E-02 2.859E-02 2. 966E-02 NOT IDENT. NB-95 6.325E-01 6. 451E-01 7.053E-01 NOT IDENT. NB-95M l.835E-01 1.983E+OO 1.985E+OO NOT IDENT. ZR-95 8.519E-02 1. 015E+OO 1.016E+OO NOT IDENT. NB-97 1.000E+41 3.265E+41 0.000E+OO SHORT HLIF ZR-97 1.000E+41 1. 082E+41 O.OOOE+OO SHORT HLIF M0-99 -4.397E+31 1. 34 7E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 7.343E+42 O.OOOE+OO SHORT HLIF RH-101 1. 44 7E-02 2.835E-02 2.910E-02 NOT IDENT. RH-102 1.531E-02 4.392E-02 4.446E-02 NOT IDENT. RU-103 -8.813E-01 4.179E+OO 4.198E+OO FAIL ABUN RH-106 -2.326E-01 3.661E-01 3.808E-01 NOT IDENT. RU-106 -2.326E-01 3.661E-01 3.808E-01 NOT IDENT. AG-108M -3.131E-03 2.150E-02 2.155E-02 NOT IDENT. AG-110M -2.253E-02 7. 881E-02 7.947E-02 NOT IDENT. SN-113 -5.019E-02 1. 896E-01 l.909E-01 NOT IDENT. CD-115 l.684E+38 2.304E+39 O.OOOE+OO SHORT HLIF SN-117M l.624E+04 8.168E+04 8.201E+04 SHORT HLIF TE-123M 2.086E-03 l.104E-01 l.104E-01 NOT IDENT. SB-124 -3.345E-01 1.404E+OO l.412E+00 NOT IDENT. SB-125 -4.372E-02 8.375E-02 8.604E-02 FAIL ABUN TE-125M 4.863E+Ol 2.185E+02 2 .196E+02 NOT IDENT. I-126 1. 560E+06 5.354E+05 8.839E+05 SHORT HLIF SB-126 -l.240E+04 9.456E+05 9.456E+05 SHORT HLIF SB-127 4.877E+21 1. 843E+22 O.OOOE+OO SHORT HLIF I-131 6.706E+08 3.865E+09 3.877E+09 SHORT HLIF I-132 1.000E+41 1.849E+42 O.OOOE+OO SHORT HLIF TE-132 -9.294E+25 2.774E+26 O.OOOE+OO SHORT HLIF BA-133 8.277E-03 3.078E-02 3. lOlE-02 NOT IDENT. I-133 1.000E+41 2.571E+41 O.OOOE+OO SHORT HLIF CS-134 3.357E-02 4.047E-02 4. 321E-02 NOT IDENT. CS-135 8 .114E-02 1.130E-01 l.188E-01 NOT IDENT. I-135 -1.000E+41 7.385E+41 O.OOOE+OO SHORT HLIF CS-136 1.520E+04 2.278E+05 2.279E+05 SHORT HLIF CE-139 -5.266E-02 9. 291E-02 9.589E-02 NOT IDENT. BA-140 -2.767E+05 9.052E+05 9.137E+05 SHORT HLIF LA-140 2.399E+05 3.187E+05 3.365E+05 SHORT HLIF CE-141 -9.646E+OO 2.255E+Ol 2. 296E+Ol NOT IDENT. CE-143 l.000E+41 2.342E+41 0.000E+OO SHORT HLIF CE-144 -9.676E-02 3.062E-01 3.093E-01 NOT IDENT. PM-144 -2.033E-02 4.395E-02 4.490E-02 NOT IDENT. PR-144 -1. 740E+00 3.820E+OO 3.900E+OO NOT IDENT. PM-146 2.708E-02 6. OOlE-02 6.124E-02 FAIL ABUN ND-147 7.700E+06 2.453E+07 2.478E+07 SHORT HLIF PM-147 -5.706E+Ol 6.450E+02 6.455E+02 NOT IDENT. PM-149 l.865E+39 3.512E+40 O.OOOE+OO SHORT HLIF EU-150 1. 750E-03 2.173E-02 2.174E-02 FAIL ABUN EU-152 4 .113E-02 8.250E-02 8.456E-02 NOT IDENT. GD-153 4.647E-02 1.482E-01 l.496E-01 NOT IDENT. EU-154 9.519E-02 9. 451E-02 1. 038E-01 FAIL ABUN EU-155 6.081E-02 8.567E-02 8.995E-02 FAIL ABUN TB-160 l.774E-01 1.284E+OO l.287E+OO FAIL ABUN H0-166M 2.500E-02 5.248E-02 5.368E-02 FAIL ABUN TM-171 -1. 511E+OO 2.280E+Ol 2.281E+Ol NOT IDENT. HF-172 -4.209E-02 2 .116E-01 2.124E-01 FAIL ABUN LU-172 3.188E-02 5.942E-02 6 .114E-02 FAIL ABUN Page 3426 of 5809 LU-176 -2.564E-03 1.836E-02 1. 840E-02 FAIL ABUN HF-181 1.596E+OO 3.139E+OO 3.220E+OO NOT IDENT. TA-182 5.369E-01 7.364E-01 7. 7 51E-01 FAIL ABUN RE-183 -1.204E+OO 2.916E+OO 2. 966E+OO NOT IDENT. RE-184 -1.555E+Ol 2.283E+Ol 2.389E+Ol NOT IDENT. W-188 -5.736E+Ol 9.810E+Ol l.014E+02 FAIL ABUN IR-192 -l.320E-01 3.467E-01 3.518E-01 FAIL ABUN HG-203 1.057E+OO 1. 774E+OO 1.837E+OO NOT IDENT. BI-207 2.360E-02 4.322E-02 4.451E-02 FAIL ABUN ** PB-210 -2. 609E+OO. 4. 591E+OO 4.740E+OO NOT IDENT. PB-211 -1.065E-01 5.620E-01 5.641E-01 NOT IDENT. BI-212 l.461E+OO 6.565E-01 9.301E-01 FAIL ABUN RN-219 -l.002E-Ol 2.942E-01 2.976E-Ol FAIL ABUN RA-223 3.255E-01 4.310E-01 4.553E-01 FAIL ABUN AC-227 -l.191E-01 l.778E-01 l.858E-01 FAIL ABUN TH-227 -1.191E-01 1.778E-01 l.858E-01 FAIL ABUN TH-229 2.710E-02 3.335E-01 3.337E-01 FAIL ABUN TH-231 3.255E-01 4.310E-01 4.553E-01 FAIL ABUN PA-233 3.015E-02 4.368E-02 4.575E-02 FAIL ABUN PA-234 -5.054E-02 2.104E-01 2 .116E-01 NOT IDENT. PA-234M 2.969E+OO 3.277E+OO 3.540E+OO NOT IDENT. NP-237 3.015E-02 4.368E-02 4.575E-02 FAIL ABUN NP-238 -l.000E+41 3.092E+41 O.OOOE+OO SHORT HLIF NP-239 -6.413E-02 1.987E-01 2.008E-01 NOT IDENT. PU-239 6. 081E+02 8.645E+02 9.069E+02 FAIL ABUN AM-241 3.422E-02 1. 381E-01 1. 38 9E-01 NOT IDENT. CM-243 -5.287E-02 7.512E-02 7.881E-02 NOT IDENT. BK-247 7.490E-02 5.313E-02 6.295E-02 NOT IDENT. CM-247 1.157E-02 2.636E-02 2.687E-02 NOT IDENT. CF-249 1.428E-02 2.765E-02 2.839E-02 NOT IDENT. CF-251 4.262E-02 8.973E-02 9.176E-02 NOT IDENT. Page 3427 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 78.8835 87.09 99.2838 136.47 81. 9702 45.60 78.9767 87.57 99.4423 140.51 0.0000 46.54 83.7918 88.03 92.3857 143.76 83.3391 49. 72 0.0000 88.34 92.4803 144.24 83.4283 51. 35 67.8268 88.47 92.5198 145.44 100.8383 51. 87 63.4697 89. 96 81. 7 622 152.43 89.5764 52.39 71.5876 1093.63 81. 9426 153.25 0.0000 52.97 68.3734 91.11 0.0000 323.87 95.7522 53.44 74.5267 92. 59 82.4554 156.02 0.0000 54.07 82.4875 93.35 82.6534 158.56 0.0000 57.36 0.0000 94.56 82.9681 159.00 91.9906 57.53 96.9429 94.65 82.9915 162.33 77.1796 57.98 91. 8914 94.67 82. 9965 162.66 0.0000 59.27 79.8124 94.87 83.0482 163.33 77.3343 59.32 79.8303 97.43 76.9550 165.86 98.0519 59.54 82.2595 98.43 88.3607 176.31 79.3060 60. 96 92.2402 98.44 88.3634 176.60 0.0000 61.17 92.3251 99.53 77.4449 177.52 72.1493 62. 93 91.2437 100.11 77.5789 181.07 0.0000 63.29 91.3844 102.03 76.9947 181.52 70.6317 63.58 91. 4974 103.18 83.4336 184.41 76.7848 64.28 95.9678 103.37 82.4493 143.76 76.9664 66.73 93.3158 105.21 73.5633 193.51 78.0345 67.24 101.1002 105.31 73.5844 197.03 76.8220 125.81 110. 4059 106.12 77.9102 198.01 82.8699 67.75 110. 4372 106.47 85.2663 201.83 85.1095 69.67 99.3351 109.28 80.7016 203.43 92.1643 70.83 115.8046 111. 00 89.5103 205.31 75.7603 72. 81 115.4553 111.76 0.0000 210.85 90.7033 72. 87 115.4818 114. 06 100.8759 215.65 80.9578 74.66 103.1418 116.30 0.0000 222.11 67.7126 74.82 103.2039 116.74 91. 9727 227.09 63.8013 74.97 103.2618 119. 76 79.7649 227.38 50.5314 77 .11 104.0834 121.12 80.0443 228.16 0.0000 78.74 104.7019 121. 22 80.0647 228.18 72.7827 79.69 85.3210 121.78 85. 5968 116.74 72.7827 80.12 84.1765 122.06 84.5734 235.69 84.8235 80.19 0.0000 122.92 86.9312 235. 96 87.5510 80.57 90.6986 123.07 90.2253 238.63 82.9361 81. 00 88.2778 265'.00 87.0978 238.98 0.0000 81. 07 88.2996 125.81 99. 2372 240.99 83.2206 81. 75 93.6419 127.23 88.9673 242.00 83.3422 83.79 86.2323 127.91 89 .1169 244.70 66.8419 84.00 91. 7885 129.30 89.4181 252.40 0.0000 85.43 116. 9193 131.20 89.8297 252.80 59.7890 86.55 109.5365 133.02 84. 6511 254.15 0.0000 86.79 109.6237 133. 52 87.7258 256.23 81. 3296 86.94 99.2336 136.00 86.3677 260.90 0.0000 Page 3428 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 42.0667 355.39 0.0000 584.27 32.0203 264.80 42.0740 356.01 39.0137 595.83 0.0000 265.00 33.6680 364.49 0.0000 427.87 45.6958 268.22 56.3538 366.42 0.0000 602.52 0.0000 269.46 62.0912 372.51 43.3748 604. 72 36.6539 270.03 62.1368 375.05 37.1206 607.14 41.3016 271.23 62.2349 377.52 55.2849 609.32 34.4663 273.65 0.0000 356.01 45.9998 610.33 34.4883 276.40 69.2989 388.16 40.8203 614.28 46.1016 277.37 71. 2860 388.63 0.0000 618.01 35.2087 277.60 69.4058 391.69 58.2034 620.36 33.7460 278.00 62.7827 264.66 44.5668 621. 93 37.6396 279.20 57.1619 401.81 52.2314 630.19 0.0000 279.54 68.6250 402.40 42.4611 631. 29 30.0956 279.70 68.6382 404.85 60.0175 633.25 29.1605 280.46 60.1174 410.95 58 .1596 634.78 0.0000 283.69 68.9854 413. 71 47.3051 635.95 31.1563 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 50.8909 423. 72 0.0000 645.85 43.8853 285.90 0.0000 427.09 50 .1013 657.76 33.1529 287.50 65.4641 427.87 53.4785 657.90 0.0000 290.67 75.3871 433.94 44.8031 661. 66 49 .. 0551 293.27 0.0000 439.40 42.7639 664.57 0.0000 ' 351. 93 58.3142 453.88 46'.1409 666.33 0.0000 295. 96 58.3667 463.37 63. 7292 666.50 0.0000 879.38 67.3337 468.07 44.9549 667. 71 0.0000 299.98 61.5824 473.00 0.0000 677.62 27.3842 300.09 61. 5901 475.06 42.8919 685.70 0.0000 300.13 61.5939 476.78 39.4681 695.00 0.0000 301.36 61. 6849 477.60 56.9184 696.49 42.3935 302.85 52. 9662 482.18 30. 3116 696. 51 42.3935 256.23 58.9673 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 38.3734 306.78 60 .1114 497.08 33.6159 697.49 40.3979 308.46 54.3051 505.52 35.6146 702.65 38.8957 311. 90 47.5840 507.63 0.0000 706.68 34.5178 316.51 59.7974 511. 00 35.7629 711. 68 34.2070 319.41 0.0000 514.00 35.8435 720.70 0.0000 320.08 0.0000 514.00 35.8435 721.93 0.0000 321.04 56.0991 520.40 33.1344 722.78 19.6682 323.87 46.2284 520.69 0.0000 722.91 26.2258 325.23 82.5322 522.65 0.0000 723. 31 26.2320 328.76 0.0000 527.90 0.0000 724.19 37.7265 333.37 68.5533 528.26 36.2244 727. 33 30.8084 333.97 57.9277 529.59 32.6338 733.00 26.3719 334.37 62.5285 529.87 0.0000 735.93 25.9424 338.28 58.1991 531. 02 0.0000 333.97 30.9796 338.32 58.2026 537.26 0.0000 739.50 0.0000 311. 90 58.3383 546.56 0.0000 747.24 30.1054 340.48 58.3383 552.55 31.3313 748.06 27.0029 340.55 0.0000 563.25 39.9214 752.31 30.1877 344.28 53.9505 569.33 37.2925 753.82 0.0000 345.93 60.2222 946.00 37.2961 756.73 25.0415 351.06 48.6457 569.70 37.3010 756.80 25.0422 351. 93 48.6906 583.19 31. 9974 884.68 21. 7852 Page 3429 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.1293 1274.44 24.8932 1620.50 10.4983 766.42 25.1697 1001.03 16.0342 1621. 92 10.5018 766.84 21. 8188 1002.74 27.1436 1678.03 0.0000 772.60 0.0000 1004.73 26.2295 1690.97 8.7477 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 .6.9294 778.90 26.3893 1028.54 0.0000 1063.66 5.0981 783.70 0.0000 1037.84 24.6835 1771. 35 3.3997 785.37 27.5361 1038.76 0.0000 1791.20 0.0000 792.07 42.5085 631. 2 9 17.4659 1808.65 12.0059 794.95 19.1569 1048.07 0.0000 1810.72 0.0000 795.86 24.4901 1049.04 19.0723 1836.06 4.0282 810.06 19.3035 1050.41 19.0820 810.29 20.3783 1063.66 0.0000 344.28 20.3794 1077.00 0.0000 810.76 21. 4557 1077.34 27.9606 815.77 0.0000 1085.87 24.1833 1048.07 0.0000 1093.63 22.3149 832.01 32.5223 1099.45 21.3909 834.85 33.6527 1112. 07 18.4536 835.71 35.8390 1112.84 19.5449 836.80 0.0000 1115. 54 17.9341 846.75 0.0000 1120.29 24.4983 846.77 26.2039 1120.55 24.5007 856.80 0.0000 1221.41 24.5081 860.56 20.8810 112 9. 67 31.6857 871.09 15.4625 1131.51 0.0000 873.19 22.1109 1147.95 0.0000 875.33 0.0000 1173.23 29.9700 879.38 19.9572 1177.95 22.0150 880.51 25.5142 1189.05 26.7891 883.24 29.9894 1204.77 25.2539 884.68 28.8977 1221.41 24.3832 889.28 26.7312 1231.02 29.1225 894.76 27.9144 1235.36 0.0000 898.04 20.1286 1238.28 31.6766 900. 72 17.9141 1260.41 0.0000 903.28 29.1437 1271.87 20.6670 911. 20 32.6223 1274.44 13.7897 912.08 39.0127 1274.54 13.7904 923.98 0.0000 1291.59 20.8018 926.50 21. 7459 1298.22 0.0000 929 .11 21.7711 1312 .11 0.0000 937.49 25.4933 1332.49 12.2944 944.13 0.0000 1362.66 0.0000 946.00 27.4153 1365 .19 10.6470 949.00 21.9609 1368. 63 0.0000 667.71 0.0000 1384.29 19.6340 962. 31 32.2101 1408.01 10.7866 964.08 30.6991 1457.56 0.0000 966 .17 35.3357 1460.82 8.7652 911. 20 35.0702 1489.16 17.4901 968. 97 35.0702 1505.03 11. 0967 983.53 0.0000 1584.12 16.2026 984.45 0.0000 1596.21 0.0000 Page 3430 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:59:48.23 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235023.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM24.CNF;330 Background date : Z-OCT-2016 11:01:18. Sample date 2-DEC-2015 10:40:00. Acquisition date : 3-0CT-2016 08:58:40. Sample ID G405235023 Sample quantity 1.41404E+02 GRAM Detector name : GAM24 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:02.00 0.1% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 2 2 2 4 4 4 4 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3431 of 5809 Energy 46.77* 63.47* 65.12* 73.16 75.05* 77. 2 6* 84.43* 87.31 90.04 92.84* 110. 08* 186.31* 209.29 238.71* 242.02 295.40 300.12 311.47 338.32 352.11* 464.13 511. 80* 583.38* 609.68* 662.16 670.22 727.02* 768.38* 786.48 794.86* 809.16 860.47 873.29 911. 42* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 16 40 12 37 201 2 68 48 106 61 111 9 92 27 450 117 186 44 25 105 306 19 1 139 205 135 26 33 14 20 29 10 17 25 71 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 158 1. 35 168 1. 23 159 0.94 230 1. 25 215 1.26 140 1. 04 135 1. 54 138 1.16 120 1. 07 144 1.19 136 1.28 137 1. 07 91 0.83 59 1. 24 94 2.03 50 1. 32 38 1. 54 100 5.35 80 1.23 56 1.47 67 1.15 100 2.36 36 1.35 56 1.76 53 1. 51 43 0.73 32 3.34 25 0.78 15 1. 4 6 12 1. 56 11 0. 91 21 0.90 35 10.38 31 1. 23 93.59 127.00 130.30 146.38 150.17 154.58 168.92 174.68 180.15 185.75 220.24 372.73 418. 71 477.56 484.17 590.97 600.42 623.13 676.84 704.43 928.53 1023.91 1167 .13 1219.74 1324.74 1340.86 1454.52 1537.26 1573.47 1590.24 1618.85 1721.52 1747.18 1823.47 89 123 123 143 143 143 165 165 165 165 219 368 416 471 471 586 596 613 670 699 923 1014 1161 1213 1316 1334 1447 1532 1570 1584 1614 1718 1733 1818 9 4.37E-03149.3 10 l.lOE-02 58.5 3.93E+OO 10 3.29E-03174.0 22 1.02E-02 76.1 2.62E+OO 22 5.58E-02 14.6 22 7.45E-02 9.9 27 l.33E-02 44.0 8.15E-01 27 2.95E-02 21.0 27 1.69E-02 31.l 27 3.07E-02 21.6 8 2.58E-03222.l 10 2.56E-02 27.0 7 7.47E-03 62.2 23 1.25E-01 5.6 1.69E+OO 23 3.25E-02 24.1 9 5.17E-02 10.0 8 l.23E-02 28.5 17 6.86E-03 95.7 14 2.91E-02 20.6 13 8.49E-02 7.8 12 5.23E-03 89.5 16 1.53E-04***** 11 3.87E-02 12.l 17 5.70E-02 11.2 18 3.74E-02 15.4 17 7.08E-03 61.8 16 9.29E-03 42.4 11 4.00E-03 73.0 11 5.69E-03 41.7 10 8.15E-03 30.0 8 2.84E-03 65.5 9 4.69E-03 54.1 28 7.03E-03 69.0 13 1.96E-02 20.8 Peak Search Report (continued) Page : 2 Sample ID : G405235023 Acquisition date 3-0CT-2016 08:58:40 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 964. 51 33 6 2.25 1929.71 1925 9 9.06E-03 22.6 36 0 . 968. 92* 54 6 2.22 1938.53 1934 11 l.51E-02 17.1 37 0 105.3. 71 18 6 1. 85 2108.19 2104 J.O 5.08E-03 33.0 38 0 1120.43* 41 19 2.21 2241.70 2236 11 1.13E-02 26.6 39 0 1161.19 10 12 1. 28 2323.27 2317 9 2.69E-03 74.7 40 0 1169.26 15 17 0.96 2339.43 2331 14 4.05E-03 66.2 41 0 1256.53 11 14 0.65 2514.06 2507 10 3.07E-03 71. 6 42 0 1281.19 14 11 1. 80 2563.42 2557 10 3. 81E-03 54.7 43 0 1322.81 5 3 1. 24 2646.70 2643 6 1.39E-03 70.7 44 0 1353.65 7 0 0.73 2708.43 2705 6 l.94E-03 37.8 45 0 1356.56 8 0 0.73 2714. 25 2711 6 2.22E-03 35.4 46 0 1377.81 22 3 2.85 2756.78 2751 11 6.19E-03 25.6 47 0 1408.39 15 3 1. 93 2817.97 2813 11 4.17E-03 33.6 48 0 1460.82* 352 4 2.44 2922.89 2915 15 9.79E-02 5.5 49 0 1588.14 12 2 1. 87 3177.70 3173 9 3.30E-03 36.7 50 0 1620.84 13 0 3.16 3243.15 3238 11 3. 61E-03 27.7 51 0 1764.52* 37 3 0.86 3530.73 3524 12 l.03E-02 20.0 Flag: "*" = Peak area was modified by background subtraction Page 3432 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 09:59:50 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235023.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 10:40:00 G405235023 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 08:58:40 141.40 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA24 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3433 of 5809 PB-214 PB-214 PB-214 PB-214 ps.:..214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.47 74.66 74.82 74.82 351.06 CAN 0 01:00:02.00 10.00 0.00 % Peak Energy 0.1%

Nuclide Line Activity Report Page : 2 Sample ID : G405235023 Acquisition date 3-0CT-2016 08:58:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.354E+OO cl. 243E+Ol 1.243E+Ol 11. 03 OK CD-109 88.03 3.70* 7.499E+OO 1. 317E+OO 2.086E+OO 80.27 OK TE-125M 109.28 0.27* 7.981E+OO 2.721E+OO 1.095E+02 444.12 OK SN-126 64.28 9.60 5.554E+OO 4.883E-01 4.883E-01 116. 90 OK 86.94 8.90 7.499E+OO 5.477E-01 5.477E-01 80.27 OK 87.57 37.00* 7.499E+OO 1. 317E-01 1.317E-01 80.27 OK BA-137M 661. 66 89.90* 2.532E+OO 3.236E-01 3.299E-01 30.82 OK CS-137 661. 66 85.10* 2.532E+OO 3.419E-01 3.486E-01 30.82 OK TL-208 277.37 6.60 5.023E+OO Line Not Found Absent 583.19 85.00* 2.790E+OO 3.245E-01 3.245E-01 24.30 OK 860.56 12.50 2.074E+OO 3.480E-01 3.480E-01 108.30 OK PB-210 46.54 4.25* 2.491E+OO 9.993E-01 1. 026E+OO 298.62 OK BI-212 727.33 6.67* 2.358E+OO 1.153E+OO l.153E+OO 84.77 OK 785.37 1.10 2.221E+OO 4.513E+OO 4.513E+OO 83.37 OK 1620.50 1. 47 1.233E+OO 3.617E+OO 3.617E+00 55.47 OK PB-212 74.82 10.28 6.749E+OO l.184E+OO 1.184E+OO 48.04 OK 77 .11 17.10 6.918E+OO 1. 472E+OO 1.472E+OO 19.84 OK 238.63 43.60* 5.637E+OO 1.091E+OO 1.091E+OO 11.14 OK 3.30 4. 720E+00 1.656E+OO 1.656E+OO 56.97 OK BI-214 609.32 45.49* 2.697E+OO 9. 213E-01 9.216E-01 22.32 OK 1120.29 14.92 1. 689E+OO 8.435E-01 8.438E-01 53.28 OK 1764.49 15.30 1.138E+OO l.066E+OO 1. 066E+OO 39.91 OK PB-214 74.82 5.80 6.730E+OO Line Not Found <<INT Reject 77 .11 9.70 6.918E+OO 2.595E+OO 2. 596E+OO 19.84 OK 87.09 3.41 7.489E+OO Line Not Found <<INT Reject 242.00 7.25 5.579E+OO Line Not Found <<INT Reject 295.22 18.42 4.779E+OO 1.238E+OO 1.239E+OO 20.01 OK 351. 93 35.60* 4.154E+OO l.193E+OO 1.193E+OO 15.55 OK RN-222 609.32 45.49* 2.697E+OO 9. 213E-01 9.216E-01 22.32 OK 1120. 29 14.92 l.689E+OO 8.435E-01 8.438E-01 53.28 OK 1764.49 15.30 1.138E+OO 1.066E+OO 1.066E+OO 39.91 OK RA-224 240.99 4.10* 5.579E+OO 8.509E-01 8.509E-01 179.75 OK RA-226 609.32 45.49* 2.697E+OO 9.213E-01 9.216E-01 22.32 OK 1120.29 14.92 1. 689E+OO 8.435E-01 8.438E-01 53.28 OK 1764.49 15.30 1.138E+OO 1.066E+OO l.066E+OO 39.91 OK AC-228 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11. 27 4.289E+OO 1.254E+OO 1.254E+OO 41. 25 OK 794.95 4.25 2.204E+OO 1.687E+OO l.687E+00 60.00 OK 835.71 1. 61 2.121E+OO Line Not Found Absent 911. 20 25.80* 1.985E+OO 7.334E-01 7.334E-01 41. 55 OK 968.97 15.80 1.893E+OO 9.598E-01 9.598E-01 34.24 OK RA-228 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11. 27 4.289E+OO 1.254E+OO l.254E+00 41. 25 OK 794.95 4.25 2.204E+00 1.687E+OO 1.687E+OO 60.00 OK 835.71 1. 61 2 .121E+OO Line Not Found Absent 911.20 25.80* 1.985E+OO 7.334E-01 7.334E-01 41. 55 OK 968.97 15.80 1.893E+OO 9.598E-01 9.598E-01 34.24 OK TH-228 74.82 10.28 6.749E+OO l.184E+00 l.184E+OO 48.04 OK 77 .11 17.10 6.918E+OO 1. 472E+OO 1. 472E+OO 19.84 OK Page 3434 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235023 Acquisition date 3-0CT-2016 08:58:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 238.63 5.637E+OO 1. 091E+OO 1.091E+OO ll .14 OK 300.09 3.30 4. 720E+OO 1.656E+OO 1. 656E+OO 56.97 OK TH-229 85.43 14.70 7. 361E+OO 2.859E-01 2.859E-01 87.98 OK 88.47 24.00 7.499E+OO 2. 031E-01 2.031E-01 80.27 OK 193.51 4.41* 6.531E+OO Line Not Found Absent 210.85 2.80 6.166E+OO Line Not Found Absent TH-230 609.32 45.49* 2.697E+OO 9.213E-01 9.213E-01 22.32 OK 1120. 29 14.92 1.689E+OO 8.435E-01 8.435E-01 53.28 OK 1764.49 15.30 l.138E+OO l.066E+OO 1.066E+OO 39.91 OK PA-231 283.69 1. 70 4.935E+OO Line Not Found Absent 301.36 5.35* 4.720E+OO 1.022E+OO l.022E+OO 56.97 OK TH-232 105.21 1.10 7.950E+OO Line Not Found Absent 338.32 11. 27 4.289E+OO 1.254E+OO 1.254E+OO 41. 25 OK 835.71 1. 61 2.121E+OO Line Not Found Absent 911.20 25.80* 1.985E+OO 7.334E-01 7.334E-01 41. 55 OK 968.97 15.80 1.893E+OO 9.598E-01 9.598E-01 34.24 OK PA-233 300.13 6.63 4.720E+OO 8.243E-01 8.243E-01 56.97 OK 311. 90 38.50* 4.582E+OO 8.161E-02 8.161E-02 191.33 OK 340.48 4.45 4.267E+OO -----Line Not Found Absent TH-234 63.29 3.70* 5.554E+OO 1.267E+OO 1.267E+OO 116. 90 OK 92.59 4.23 7.706E+OO 2.171E+OO 2.171E+OO 43.23 OK U-234 609.32 45.49* 2.697E+OO 9.213E-01 9.213E-01 22.32 OK 1120.29 14.92 1. 689E+OO 8.435E-01 8.435E-01 53.28 OK 1764.49 15.30 1.138E+OO 1.066E+OO 1.066E+00 39.91 OK U-235 89.96 3.47 7.610E+OO l.480E+OO 1.480E+OO 62.13 OK 93.35 5.60 7.706E+OO 1.640E+OO 1.640E+OO 43.23 OK 143.76 10.96* 7.620E+OO Line Not Found -----, Absent 163.33 5.08 7.206E+OO Line Not Found Absent 185.72 57.20 6.689E+OO l.465E-01 l.465E-01 54. 04* OK 205.31 5.01 6.280E+OO Line Not Found Absent U-238 63.29 3.70* 5.554E+OO 1.267E+OO 1.267E+OO 116. 90 OK 92.59 4.23 7.706E+OO 2.171E+OO 2.171E+OO 43.23 OK AM-243 43.53 5.90 1.694E+OO Line Not Found Absent 74.66 67.20* 6.749E+OO 1.812E-01 l.812E-01 48.04 OK ANH-511 511. 00 100.00* 3.088E+OO 9. 971E-04 9.971E-048945.20 OK Flag: "*" = Keyline Page 3435 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:59:51.05 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235023.CNF;l *
  • Acquisition date 3-0CT-2016 08:58:40 Sensitivity : 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:02.00 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:40:00 Analyst initials: MXRl *
  • Sample ID G405235023 Sample Quantity 1.4140E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;?
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM K-40 1.243E+Ol 1.344E+OO 4.832E-01 CD-109 2.086E+OO 1. 641E+OO 1. 487E+OO TE-125M l.095E+02 4.764E+02 4.587E+02 SN-126 l.317E-01 1. 036E-01 9.410E-02 BA-137M 3.299E-01 9. 966E-02 5.785E-02 CS-137 3.486E-01 l.053E-01 6. lllE-02 TL-208 3.245E-01 7. 72 6E-02 5.906E-02 PB-210 1.026E+OO 3.002E+OO 2.460E+00 BI-212 l.153E+OO 9.578E-01 7.389E-01 PB-212 1.091E+OO 1.192E-01 8.285E-02 BI-214 9.216E-01 2.016E-01 1.125E-01 PB-214 1.193E+OO l.819E-01 1. 07 5E-01 RN-222 9.216E-01 2.016E-01 1.125E-01 RA-224 8.509E-01 l.499E+OO 8.882E-01 RA-226 9.216E-01 2.016E-01 l.125E-01 AC-228 7.334E-01 2.986E-01 2. 451E-01 RA-228 7.334E-01 2.986E-01 2.451E-01 TH-228 1. 091E+OO 1.192E-01 8.285E-02 TH-229 4 .141E-01 4.432E-01 8.579E-01 TH-230 9.213E-01 2.015E-01 l.124E-01 PA-231 1.022E+OO 5.703E-01 7.210E-01 TH-232 7.334E-01 2.986E-01 2.451E-01 PA-233 8 .161E-02 l.530E-01 9.713E-02 TH-234 1.267E+00 1.451E+OO l.385E+00 U-234 9.213E-01 2.0lSE-01 l.124E-01 U-235 -7.143E-02 l.739E-01 3.090E-01 U-238 1. 267E+OO 1.451E+OO 1.385E+OO AM-243 l.812E-01 8.530E-02 6. 331E-02 ANH-511 9.971E-04 8.741E-02 5.169E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -4. 962E+OO 1.228E+Ol 2.252E+Ol NOT IDENT. Page 3436 of 5809 NA-22 l.243E-02 5.037E-02 9.585E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF AL-26 7. 081E-03 2.274E-02 5.523E-02 NOT IDENT. SC-46 -5.738E-01 3.732E-01 4.987E-01 FAIL ABUN V-48 0.000E+OO l.642E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4 .118E+02 0.000E+OO SHORT HLIF MN-54 -3.323E-02 6.726E-02 l.157E-01 NOT IDENT. C0-56 7.905E-02 4.295E-01 8.435E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF C(\-57 7.259.E-03 4.035E-02 560E-02 NOT IDENT. C0-58 2.659E-01 3.646E-01 8.222E-01 NOT IDENT. FE-59 -5.545E+OO 6.252E+OO 1.070E+Ol NOT IDENT. C0-60 7.350E-03 2.885E-02 6.330E-02 NOT IDENT. ZN-65 l.056E-01 1.649E-01 3.299E-01 NOT IDENT. GE-68 -2.103E-01 1. 881E+OO 3.763E+OO NOT IDENT. AS-73 3.431E+OO 4.973E+OO 9.828E+OO NOT IDENT. AS-74 0.000E+OO 7.107E+03 O.OOOE+OO SHORT HLIF SE-75 -9.210E-02 1. 883E-01 3.549E-01 NOT IDENT. BR-77 O.OOOE+OO l.270E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.798E+02 O.OOOE+OO SHORT HLIF RB-83 5.320E-02 6.081E-01 1.188E+OO NOT IDENT. KR-85 4.224E+OO 7.385E+OO 1.359E+Ol NOT IDENT. SR-85 4.720E-01 8.315E-01. 1.529E+OO NOT IDENT. RB-86 O.OOOE+OO 2.780E+04 O.OOOE+OO SHORT HLIF Y-88 2.103E-02 2.149E-01 4.626E-01 NOT IDENT. Y-91 2.930E+Ol 4.811E+02 9.673E+02 NOT IDENT. NB-94 5.166E-03 2.952E-02 5.700E-02 NOT IDENT. NB-95 -3.463E-01 9.430E-01 1. 461E+OO NOT IDENT. NB-95M -l.482E-01 2.294E+OO 4.049E+OO NOT IDENT. ZR-95 -5.707E-01 1.552E+OO 2.757E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 6.430E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.290E-02 3.143E-02 5.562E-02 NOT IDENT. RH-102 2.lOOE-02 5.312E-02 l.073E-01 NOT IDENT. RU-103 -l.115E-01 6.133E+OO 1.173E+Ol FAIL ABUN RH-106 -2.431E-01 4.526E-01 7.994E-01 NOT IDENT. RU-106 -2. 431E-01 4.526E-01 7.994E-01 NOT IDENT. AG-108M 6.719E-03 2.650E-02 5.237E-02 NOT IDENT. AG-llOM -5.599E-02 9.755E-02 l.651E-01 NOT IDENT. SN-113 2.579E-02 2.076E-01 4.091E-01 NOT IDENT. CD-115 O.OOOE+OO 1.904E+40 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1. 176E+05 O.OOOE+OO SHORT HLIF TE-123M 5.449E-02 1. 229E-01 2.315E-01 NOT IDENT. SB-124 1. 875E+OO 2.188E+OO 5.319E+OO NOT IDENT. SB-125 2.521E-02 9.217E-02 1. 840E-01 FAIL ABUN I-126 O.OOOE+OO l.484E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.467E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.558E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 7 .131E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.275E+27 O.OOOE+OO SHORT HLIF BA-133 6.630E-03 3.279E-02 6. 031E-02 NOT IDENT. I-133 O.OOOE+OO 1.431E+41 0.000E+OO SHORT HLIF CS-134 l. lllE-01 6.531E-02 1.171E-01 FAIL ABUN CS-135 -1.159E-01 1.189E-01 2 .139E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 3.586E+05 O.OOOE+OO SHORT HLIF CE-139 2.532E-02 l.080E-01 1. 988E-01 NOT IDENT. BA-140 0.000E+OO 1. 622E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.622E+05 O.OOOE+OO SHORT HLIF CE-141 7.869E+OO 2.563E+Ol 4.766E+Ol NOT IDENT. CE-143 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CE-144 -6.451E-02 3.266E-01 5.875E-01 NOT IDENT. PM-144 1.707E-03 4. 896E-02 9.367E-02 NOT IDENT. PR-144 l.488E-01 4.267E+OO 8.163E+OO NOT IDENT. PM-146 2.504E-02 3.878E-02 8.043E-02 NOT IDENT. ND-147 0 .'OOOE+OO 4.673E+07 O.OOOE+OO SHORT HLIF PM-147 3. 721E+02 6.950E+02 1. 340E+03 NOT IDENT. PM-149 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF EU-150 -8.459E-03 2.594E-02 4.347E-02 FAIL ABUN EU-152 -l.209E-02 8.335E-02 1.531E-01 FAIL ABUN GD-153 -l.662E-02 l.647E-01 2.796E-01 NOT IDENT. EU-154 2. 611E-02 l.224E-01 2.318E-01 FAIL ABUN EU-155 7.348E-02 8.533E-02 1. 696E-01 FAIL ABUN TB-160 l.838E-01 2.302E+OO 3.875E+OO FAIL ABUN H0-166M -9.090E-03 5.178E-02 9.582E-02 FAIL ABUN Page 3437of5809 TM-171 1.848E+OO 1.052E+Ol 2.043E+Ol NOT IDENT. HF-172 2.587E-02 l.950E-01 3.630E-01 FAIL ABUN LU-172 3.856E-02 7.593E-02 1.599E-01 FAIL ABUN LU-176 -7.838E-03 2.299E-02 3.883E-02 FAIL ABUN HF-181 -8.063E-01 4.423E+OO 8.338E+OO NOT IDENT. TA-182 9.328E-01 8.809E-01 1. 972E+OO FAIL ABUN RE-183 5.395E-01 1.747E+OO 3.407E+OO NOT IDENT. RE-184 3.575E+Ol 3.237E+Ol 7.099E+Ol NOT IDENT. W-188 -1.181E+02 1.134E+02 1.740E+02 FAIL ABUN IR-J...,92 1.622E-01 4.426E-01 8 . ..208E-01 FAIL ABUN HG-203 -l.083E-01 2.290E+OO 4.467E+OO FAIL ABUN BI-207 -3.287E-03 3.269E-02 6.685E-02 FAIL ABUN BI-211 O.OOOE+OO 5.009E-01 7.826E-01 FAIL ABUN PB-211 3.499E-01 5.572E-01 1.158E+OO NOT IDENT. RN-219 -6.484E-02 3.377E-01 6.414E-01 NOT IDENT. RA-223 1. 260E-01 5.033E-01 1.007E+OO FAIL ABUN AC-227 2.015E-01 2.012E-01 4.251E-01 FAIL ABUN TH-227 2.015E-01 2.012E-01 4. 251E-01 FAIL ABUN TH-231 l.260E-01 5.033E-01 1.007E+OO FAIL ABUN PA-234 -1.091E-01 2.326E-01 4.105E-01 FAIL ABUN PA-234M l.210E+00 3. 722E+OO 7. 801E+OO NOT IDENT. NP-237 8.161E-02 1.530E-01 9.516E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 7.289E-02 2.051E-01 3.896E-01 NOT IDENT. PU-239 1. 216E+02 3.023E+02 5.660E+02 NOT IDENT. AM-241 -1.082E-02 8.487E-02 1.480E-01 NOT IDENT. CM-243 -l.628E-03 7.335E-02 1.369E-01 NOT IDENT. BK-247 -2.981E-02 6.259E-02 l.181E-01 FAIL ABUN CM-247 1. 744E-02 2.802E-02 5.858E-02 NOT IDENT. CF-249 3.766E-03 3.437E-02 6. 724E-02 NOT IDENT. CF-251 1.701E-02 1.069E-01 1.953E-01 NOT IDENT. Page 3438 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:59:48.93 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 338 10.66* 1.354E+OO 1.243E+Ol 1.243E+Ol 11. 03 CD-109 88.03 128 3.70* 7.499E+OO 2.459E+OO 3.893E+OO 42.00 TE-125M 109.28 11 0.27* 7.981E+OO 2. 721E+OO 1.095E+02 444.12 SN-126 64.28 49 9.60 5.554E+OO 4.883E-01 4.883E-01 116. 90 86.94 128 8.90 7.499E+OO 1.022E+OO 1.022E+OO 42.00 87.57 128 37.00* 7.499E+OO 2.459E-01 2.459E-01 42'. 00 BA-137M 661. 66 139 89.90* 2.532E+OO 3.236E-01 3.299E-01 30.82 CS-137 661.66 139 85.10* 2.532E+OO 3.419E-01 3.486E-01 30.82 TL-208 277.37 ------6.60 5.023E+OO ------Line Not Found ------583.19 145 85.00* 2.790E+OO 3.245E-01 3.245E-01 24.30 860.56 17 12.50 2.074E+OO 3.480E-01 3.480E-01 108.30 PB-210 46.54 20 4.25* 2. 491E+OO 9.993E-01 1.026E+OO 298.62 BI-211 72.87 45 1. 23 6. 591E+OO 2.940E+OO 2.940E+OO 152.14 351.06 332 12.92* 4.154E+OO 3.287E+OO 3.287E+OO 15.55 BI-212 727.33 34 6.67* 2.358E+OO 1.153E+OO 1.153E+OO 84.77 785.37 21 1.10 2.221E+OO 4.513E+OO 4.513E+OO 83.37 1620.50 12 1. 47 1.233E+OO 3.617E+OO 3.617E+OO 55.47 PB-212 74.82 246 10.28 6.749E+OO 1. 883E+00 1. 883E+O,O 29 .29 77 .11 328 17.10 6.918E+OO 1. 472E+OO 1. 472E+OO 19.84 238.63 505 43.60* 5.637E+OO 1. 091E+OO 1. 091E+OO 11.14 300.09 49 3.30 4.720E+00 1.656E+OO 1.656E+00 56.97 BI-214 609.32 213 45.49* 2.697E+OO 9. 213E.-01 9.216E-01 22.32 1120. 29 40 14.92 1.689E+OO 8.435E-01 8.438E-01 53.28 1764.49 35 15.30 1.138E+OO 1.066E+OO 1.066E+OO 39.91 PB-214 74.82 246 5.80 6.749E+OO 3.337E+OO 3.338E+00 29.29 77 .11 328 9.70 6.918E+OO 2.595E+OO 2.596E+OO 19.84 87.09 128 3.41 7.499E+OO 2.668E+OO 2.669E+00 42.00 242.00 131 7.25 5.579E+OO 1. 719E+OO 1. 720E+OO 48.20 295.22 205 18.42 4.779E+OO l.238E+OO l.239E+OO 20.01 351.93 332 35.60* 4.154E+OO 1.193E+OO 1.193E+OO 15.55 RN-222 609.32 213 45.49* 2.697E+OO 9.213E-01 9.216E-01 22.32 1120.29 40 14.92 1. 689E+OO 8.435E-01 8.438E-01 53.28 1764.49 35 15.30 1.138E+OO 1. 066E+OO l.066E+OO 39.91 RA-224 240.99 131 4.10* 5.579E+OO 3.040E+OO 3.040E+OO 48.20 RA-226 609.32 213 45.49* 2.697E+OO 9.213E-01 9.216E-01 22.32 1120.29 40 14.92 1. 689E+OO 8.435E-01 8.438E-01 53.28 1764.49 35 15.30 1.138E+OO 1.066E+OO l.066E+OO 39.91 AC-228 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 114 11.27 4.289E+00 l.254E+OO l.254E+OO 41. 25 794.95 30 4.25 2.204E+OO l.687E+OO l.687E+OO 60.00 835.71 ------1. 61 2.121E+OO ------Line Not Found ------911.20 71 25.80* l.985E+00 7.334E-01 7.334E-01 41. 55 968. 97 54 15.80 l.893E+OO 9.598E-01 9.598E-01 34.24 RA-228 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 114 11.27 4.289E+OO l.254E+OO l.254E+OO 41.25 794.95 30 4.25 2.204E+OO 1.687E+OO l.687E+OO 60.00 835.71 ------1. 61 2 .121E+OO ------Line Not Found ------Page 3439 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235023 Acquisition date 3-0CT-2016 08:58:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911. 20 71 .25.80* 1.985E+OO 7.334E-01 7.334E-01 4:1..55 968. 97 54 1.893E+OO 9.598E-01 9.598E-01 34.24 TH-228 74.82 246 10.28 6.749E+OO 1.883E+OO 1. 883E+OO 29.29 77.11 328 17.10 6.918E+OO 1.472E+OO 1.472E+OO 19.84 238.63 505 43.60* 5.637E+OO 1.091E+OO 1.091E+OO 11.14 300.09 49 3.30 4. 720E+OO 1.656E+OO 1. 656E+OO 56.97 TH-229 85.43 58 14.70 7.361E+OO 2.859E-01 2.859E-01 87.98 88.47 128 24.00 7.499E+OO 3.790E-01 3.791E-01 42.00 193.51 ------4.41* 6.531E+00 ------Line Not Found ------210.85 ------2.80 6.166E+OO ------Line Not Found ------TH-230 609.32 213 45.49* 2.697E+OO 9.213E-01 9.213E-01 22.32 1120.29 40 14.92 1.689E+OO 8.435E-01 8.435E-01 53.28 1764.49 35 15.30 1.138E+OO 1.066E+OO 1.066E+OO 39.91 PA-231 283.69 ------1. 70 4.935E+OO ------Line Not Found ------301.36 49 5.35* 4.720E+OO 1.022E+OO 1.022E+OO 56.97 TH-232 105.21 ------1.10 7.950E+OO ------Line Not Found ------338.32 114 11.27 4.289E+00 1.254E+OO 1.254E+OO 41. 25 835.71 ------1. 61 2.121E+00 ------Line Not Found ------911.20 71 25.80* 1.985E+OO 7.334E-01 7.334E-01 41. 55 968. 97 54 15.80 1.893E+OO 9.598E-01 9.598E-01 34.24 PA-233 300.13 49 6.63 4. 720E+OO 8.243E-01 8.243E-01 56.97 311. 90 27 38.50* 4.582E+OO 8.161E-02 8 .161E-02 191.33 340.48 ------4.45 4.267E+00 ------Line Not Found ------TH-234 63.29 49 3.70* 5.554E+00 1. 2 67E+OO 1.267E+00 116. 90 92.59 133 4.23 7.706E+00 2.171E+OO 2.171E+OO 43.23 U-234 609.32 213 45.49* 2.697E+OO 9.213E-01 9.213E-01 22.32 1120.29 40 14.92 1. 689E+OO 8.435E-01 8.435E-01 53.28 1764.49 35 15.30 1.138E+OO 1. 066E+OO 1.066E+00 39.91 U-235 89. 96 74 3.47 7.610E+00 1.480E+OO 1.480E+OO 62 .13 93.35 133 5.60 7.706E+d0 1.640E+OO 1.640E+OO 43.23 143.76 ------10.96* 7.620E+OO ------Line Not Found ------163.33 ------5.08 7.206E+00 ------Line Not Found ------185. 72 106 57.20 6.689E+OO 1.465E-01 1.465E-01 54.04 205.31 ------5.01 6.280E+OO ------Line Not Found ------U-238 63.29 49 3.70* 5.554E+OO 1.267E+OO 1.267E+OO 116. 90 92.59 133 4.23 7.706E+00 2.171E+OO 2 .171E+OO 43.23 AM-243 43.53 ------5.90 1.694E+OO ------Line Not Found ------74.66 246 67.20* 6.749E+OO 2.880E-01 2. 881E-01 29.29 ANH-511 511. 00 1 100.00* 3.088E+OO 9. 971E-04 9. 971E-04 8945.20 Flag: "*" Key line Page 3440 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235023 Acquisition date 3-0CT-2016 08:58:40 Total number of lines in spectrum 51 Number of unidentified lines 14 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 PA-233 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y . 461.40D 57.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y l.41E+10Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 2.14E+06Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 58 40.2 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.243E+Ol 2.459E+OO 2.721E+OO 2.459E-01 3.236E-01 3.419E-01 3.245E-01 9.993E-01 3.287E+OO 1.153E+OO l.091E+OO 9.213E-01 1.193E+OO 9.213E-01 3.040E+OO 9.213E-01 7.334E-01 7.334E-01 1. 091E+OO 3.790E-01 9. 213E-01 1.022E+OO 7.334E-01 8 .161E-02 1.267E+OO 9. 213E-01 1. 465E_.:.01 1. 267E+OO 2.880E-01 9. 971E-04 4 .196E+Ol 4 .196E+Ol Decay Corr pCi/GRAM 1.243E+Ol 3.893E+OO 1.095E+02 2.459E-01 3.299E-01 3.486E-01 3.245E-01 1. 026E+OO 3.287E+OO 1.153E+OO 1.091E+OO 9.216E-01 1.193E+OO 9.216E-01 3.040E+OO 9.216E-01 7.334E-01 7.334E-01 1.091E+OO 3. 791E-01 9.213E-01 1.022E+OO 7.334E-01 8.161E-02 1. 267E+OO 9. 213E-01 l.465E-01 1.267E+OO 2.881E-01 9. 971E-04 1.502E+02 1.502E+02 72.55% . Decay Corr 2-Sigma Error 0.137E+Ol 1.635E+OO 4.862E+02 l.033E-01 1.017E-01 l.074E-01 0.788E-01 3.063E+OO 0. 511E+OO 0.977E+OO 0.122E+OO 2.057E-01 0.186E+OO 2.057E-01 l.465E+OO 2.057E-01 3.047E-01 3.047E-01 0.122E+OO l.592E-01 2.056E-01 0.582E+OO 3.047E-01 15.61E-02 l.481E+OO 2.056E-01 0.792E-01 l.481E+OO 0.844E-01 891.9E-04 "M" Manually accepted 2-Sigma %Error 11. 03 42.00 444.12 42.00 30.82 30.82 24.30 298.62 15.55 84.77 11.14 22.32 15.55 22.32 48.20 22.32 41. 55 41. 55 11.14 42.00 22.32 56.97 41. 55 191. 33 116. 90 22.32 54.04 116. 90 29.29 8945.20 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3441of5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235023 Acquisition date : 3-0CT-2016 08:58:40 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 2 65.12 15 197 0.94 130.30 123 10 3.29E-03 **** 5.76E+OO 0 209.29 30 103 0.83 418.71 416 7 7.47E-03 **** 6.20E+OO 0 464.13 20 71 1.15 928.53 923 12 5.23E-03 **** 3.33E+OO T 0 670.22 le 26 44 0.73 1340.86 1334 17 7.08E-OJ **** 2.51E+OO 0 768.38 15 25 0.78 1537.26 1532 11 4.00E-03 **** 2.26E+OO 0 809.16 10 11 0.91 1618.85 1614 8 2.84E-03 **** 2.17E+OO T 0 873.29 25 35 10.38 1747.18 1733 28 7.03E-03 **** 2.05E+OO T 0 964. 51 32 6 2.25 1929.71 1925 9 9.06E-03 45.1 1. 90E+OO T 0 1053. 71 18 6 1. 85 2108.19 2104 10 5.08E-03 66.1 1.77E+OO 0 1161.19 9 12 1. 28 2323.27 2317 9 2.69E-03 **** 1.64E+OO 0 1169.26 14 17 0. 96 2339.43 2331 14 4.05E-03 **** 1. 63E+OO 0 1256.53 11 14 0.65 2514.06 2507 10 3.07E-03 **** 1.54E+OO 0 1281.19 13 11 1. 80 2563.42 2557 10 3.81E-03 **** 1.51E+OO 0 1322.81 5 3 1.24 2646.70 2643 6 1.39E-03 **** 1. 4 7E+OO 0 1353. 65 7 0 0.73 2708.43 2705 6 1. 94E-03 75.6 1. 45E+OO 0 1356.56 8 0 0.73 2714.25 2711 6 2.22E-03 70.7 1. 44E+OO 0 1377.81 21 3 2.85 2756.78 2751 11 6.19E-03 51. 2 1. 42E+OO 0 1408.39 14 3 1. 93 2817.97 2813 11 4.17E-03 67.3 1. 40E+OO T 0 1588.14 11 2 1. 87 3177.70 3173 9 3.30E-03 73.4 1.26E+OO Flags: "T" = Tentatively associated Page 3442 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:02.50 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235023.CNF;l *
  • Acquisition date 3-0CT-2016 08:58:40 Sensitivity 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:02.00 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:40:00 Nuclide Library : SOLID *
  • Sample ID G405235023 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.4140E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN:CNF;7 * ***********************************************x*****x************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 PA-233 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1. 917E-01 7.002E-01 2.152E+02 4.432E-02 2.565E-02 2. 710E-02 2.644E-02 1.154E+OO 3.230E-01 3.839E-02 5.027E-02 4.876E-02 5.027E-02 4 .116E-01 5.027E-02 1.084E-01 1.084E-01 3.839E-02 4.030E-01 5.026E-02 3.310E-01 l.084E-01 4.435E-02 6. 551E-01 5.026E-02 l.455E-01 6. 551E-01 2.997E-02 2.347E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3443 of 5809 Le (pCi/GRAM 1.0lOE+Ol NOT IDENT. 4.199E-02 NOT IDENT.

NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 Page 3444 of 5809 O.OOOE+OO 2 .114E-02 2. 041E-01 O.OOOE+OO O.OOOE+OO 5. llOE-02 3.677E-01 O.OOOE+OO 3.538E-02 3.437E-01 4.470E+OO 2.615E-02 l.448E-01 l.599E+OO 4.651E+OO O.OOOE+OO l.632E-01 O.OOOE+OO O.OOOE+OO 5. 311E-01 6.214E+00 6.993E-01 O.OOOE+OO l.830E-01 4 .182E+02 2.547E-02 6.421E-01 l.880E+OO l.218E+00 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.614E-02 4.784E-02 5.298E+OO 3.506E-01 3.506E-01 2.386E-02 7.102E-02 l.857E-01 O.OOOE+OO O.OOOE+OO l.085E-01 2.228E+OO 8.342E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.709E-02 O.OOOE+OO 5.344E-02 9.791E-02 O.OOOE+OO O.OOOE+OO 9.327E-02 O.OOOE+OO O.OOOE+OO 2.243E+Ol O.OOOE+OO 2.755E-01 4.143E-02 3.610E+OO 3. 651E-02 O.OOOE+OO 6.282E+02 O.OOOE+OO l.993E-02 6. 966E-02 1. 317E-01 l.014E-01 7. 971E-02 l.715E+OO 4.228E-02 9.628E+00 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN s*HORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-231 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3445 of 5809 1. 700E-01 7.084E-02 l.771E-02 3.748E+OO 8.778E-01 l.607E+OO 3.168E+Ol 7.904E+Ol 3.754E-01 2.061E+00 2.780E-02 3.777E-01 5.266E-01 2.907E-01 4.616E-01 l.979E-01 l.979E-01 4.616E-01 l.738E-01 3.433E+OO 4.337E-02 O.OOOE+OO 1. 829E-01 2.678E+02 6.973E-02 6.380E-02 5.431E-02 2.654E-02 3.070E-02 9.136E-02 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:07.74 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235023.CNF;l *
  • Acquisition date 3-0CT-2016 08:58:40 Sensitivity : 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:02.00 Half life ratio : ***** *
  • Sample date 2-DEC-2015 10:40:00 Nuclide Library : SOLID *
  • Sample ID G405235023 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity l.4140E+02 GRAM *
  • Quantity Err ( % ) 1. 4144E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 07: 45: 20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.243E+Ol 1.492E+00 CD-109 2.086E+OO 1.665E+OO TE-125M 1.095E+02 4.765E+02 SN-126 1.317E-01 1.049E-01 BA-137M 3.299E-01 l.007E-01 CS-137 3.486E-01 l.063E-01 TL-208 3.245E-01 7.848E-02 PB-210 1.026E+OO 3.003E+OO BI-212 1.153E+OO 9.596E-01 PB-212 1. 091E+OO 1.323E-01 BI-214 9.216E-01 2.054E-01 PB-214 1.193E+OO 1.884E-01 RN-222 9.216E-01 2.054E-01 RA-224 8.509E-01 1.506E+OO RA-226 9.216E-01 2.054E-01 AC-228 7.334E-01 3.009E-01 RA-228 7.334E-01 3.009E-01 TH-228 1.091E+OO 1.323E-01 TH-229 4.141E-01 4.436E-01 TH-230 9.213E-01 2.053E-01 PA-231 l.022E+00 6.106E-01 TH-232 7.334E-01 3.009E-01 PA-233 8 .161E-02 1. 531E-01 TH-234 1. 267E+OO 1. 478E+OO U-234 9.213E-01 2.053E-Oi U-235 -7.143E-02 l.739E-01 U-238 l.267E+00 1.478E+OO AM-243 l.812E-01 8.708E-02 ANH-511 9.971E-04 8.741E-02 Non-Identified Nuclides Nuclide BE-7 Page 3446 of 5809 Key-Line Activity (pCi/GRAM -4.962E+OO K.L Act error ( 1. 96-sigma) 1. 228E+Ol TPU ( 1. 96-sigma) 1.492E+OO 1.665E+OO 4.765E+02 l.049E-01 1.007E-01 1.063E-01 7.848E-02 3.003E+OO 9. 596E-01 l.323E-01 2.054E-01 1.884E-01 2.054E-01 1.506E+OO 2.054E-01 3.009E-01 3.009E-01 1.323E-01 4.436E-01 2.053E-01 6.106E-01 3.009E-01 l.531E-01 1. 478E+OO 2.053E-01 1.739E-01 1.478E+OO 8.708E-02 8.741E-02 TPU ( 1. 96-sigma) l.248E+Ol NOT IDENT.

NA-22 l.243E-02 5.037E-02 5.069E-02 NOT IDENT. NA-24 -l.000E+41 2.535E+41 O.OOOE+OO SHORT HLIF AL-26 7. 081E-03 2.274E-02 2.296E-02 NOT IDENT. SC-46 -5.738E-01 3.740E-Ol 4.547E-01 FAIL ABUN V-48 -1.990E+03 1.642E+04 1.644E+04 SHORT HLIF CR-51 -3.344E+02 4.120E+02 4.387E+02 SHORT HLIF MN-54 -3.323E-02 6. 727E-02 6.892E-02 NOT IDENT. C0-56 7.905E-02 4.295E-01 4.310E-01 NOT IDENT. MN-56 1.000E+41 3.373E+41 0.000E+OO SHORT HLIF C0-57

  • 7.259E-03 4.035E-02 4. 0.48E-02 NOT IDENT. C0-58 2.659E-01 3.648E-01 3.840E-01 NOT IDENT. FE-59 -5.545E+OO 6. 2 65E+OO 6.745E+OO NOT IDENT. C0-60 7.350E-03 2.885E-02 2.904E-02 NOT IDENT. ZN-65 1.056E-01 l.650E-01 l.717E-01 NOT IDENT. GE-68 -2.103E-01 1.881E+OO 1.884E+OO NOT IDENT. AS-73 3.431E+OO 5.023E+OO 5.256E+OO NOT IDENT. AS-74 -2.915E+03 7 .111E+03 7.232E+03 SHORT HLIF SE-75 -9.210E-02 l.883E-01 l.928E-01 NOT IDENT. BR-77 1.163E+39 1.027E+40 O.OOOE+OO SHORT HLIF SR-82 6.237E+02 7.804E+02 8.295E+02 SHORT HLIF RB-83 5.320E-02 6.082E-01 6.087E-01 NOT IDENT. KR-85 4.224E+OO 7.386E+OO 7.628E+OO NOT IDENT. SR-85 4.720E-01 8.317E-01 8.585E-01 NOT IDENT. RB-86 -3.932E+03 2.780E+04 2.786E+04 SHORT HLIF Y-88 2.103E-02 2.149E-01 2.152E-01 NOT IDENT. Y-91 2.930E+Ol 4. 811E+02 4.813E+02 NOT IDENT. NB-94 5.166E-03 2.952E-02 2. 961E-02 NOT IDENT. NB-95 -3.463E-01 9.431E-01 9.559E-01 NOT IDENT. NB-95M -1.482E-01 2.295E+OO 2.295E+OO NOT IDENT. ZR-95 -5.707E-01 1.552E+OO 1.573E+OO NOT IDENT. NB-97 -1.000E+41 4.064E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 2.321E+41 O.OOOE+OO SHORT HLIF M0-99 -6.949E+32 6.450E+32 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 3.406E+41 O.OOOE+OO SHORT HLIF RH-101 -1.290E-02 3.152E-02 3.205E-02 NOT IDENT. RH-102 2.lOOE-02 5 .,315E-02 5.399E-02 NOT IDENT. RU-103 -l .115E-01 6.133E+OO 6.133E+OO FAIL ABUN RH-106 -2. 431E-01 4.528E-01 4.659E-01 NOT IDENT. RU-106 -2.431E-01 4.528E-01 4.659E-01 NOT IDENT. AG-108M 6.719E-03 2.650E-02 2.667E-02 NgT IDENT. AG-110M -5.599E-02 9.759E-02 1.008E-01 N T IDENT. SN-113 2.579E-02 2.076E-01 2.079E-01 NOT IDENT. CD-115 8.801E+38 1.904E+40 O.OOOE+OO SHORT HLIF SN-117M 2.188E+04 1.177E+05 1.181E+05 SHORT HLIF TE-123M 5.449E-02 l.229E-01 1.254E-01 NOT IDENT. SB-124 1.875E+OO 2.190E+OO 2.348E+OO NOT IDENT. SB-125 2.521E-02 9.218E-02 9.288E-02 FAIL ABUN I-126 1.099E+06 1.492E+06 l.572E+06 SHORT HLIF SB-126 6.407E+05 1.472E+06 1.500E+06. SHORT HLIF SB-127 2.035E+21 6.564E+22 O.OOOE+OO SHORT HLIF I-131 -5.209E+08 7.131E+09 7.135E+09 SHORT HLIF I-132 1.000E+41 1. 8 97E+42 O.OOOE+OO SHORT HLIF TE-132 9.883E+26 1.339E+27 O.OOOE+OO SHORT HLIF BA-133 6.630E-03 3.279E-02 3.293E-02 NOT IDENT. I-133 -1.000E+41 2.336E+41 O.OOOE+OO SHORT HLIF CS-134 1.111E-01 6.548E-02 8.243E-02 FAIL ABUN CS-135 -1.159E-01 1.191E-01 1. 301E-01 NOT IDENT. I-135 1.000E+41 l.020E+42 O.OOOE+OO SHORT HLIF CS-136 4.103E+05 3.614E+05 4.060E+05 SHORT HLIF CE-139 2.532E-02 1. 081E-01 1.087E-01 NOT IDENT. BA-140 -8.149E+05 l.622E+06 l.663E+06 SHORT HLIF LA-140 2.849E+05 4.624E+05 4.799E+05 SHORT HLIF CE-141 7.869E+OO 2.563E+Ol 2.587E+Ol NOT IDENT. CE-143 1.000E+41 2.129E+41 O.OOOE+OO SHORT HLIF CE-144 -6. 451E-02 3.266E-01 3.279E-01 NOT IDENT. PM-144 1. 707E:....03 4.896E-02 4.897E-02 NOT IDENT. PR-144 1. 488E-01 4.267E+OO 4.267E+OO NOT IDENT. PM-146 2.504E-02 3.883E-02 4.043E-02 NOT IDENT. ND-147 7.057E+06 4.673E+07 4.684E+07 SHORT HLIF PM-147 3.721E+02 6.952E+02 7 .151E+02 NOT IDENT. PM-149 1.000E+41 2.219E+41 O.OOOE+OO SHORT HLIF EU-150 -8.459E-03 2.595E-02 2.622E-02 FAIL ABUN EU-152 -l.209E-02 8.335E-02 8.353E-02 FAIL ABUN GD-153 -1.662E-02 1.647E-01 l.649E-01 NOT IDENT. EU-154 2. 611E-02 l.224E-01 1.230E-01 FAIL ABUN EU-155 7.348E-02 8.549E-02 9.168E-02 FAIL ABUN TB-160 1.838E-01 2.302E+OO 2.304E+OO FAIL ABUN H0-166M -9.090E-03 5.179E-02 5.195E-02 FAIL ABUN Page 3447 of 5809 TM-171 l.848E+OO l.052E+Ol l.055E+Ol NOT IDENT. HF-172 2.587E-02 1. 951E-01 l.954E-01 FAIL ABUN LU-172 3.856E-02 7.603E-02 7.799E-02 FAIL ABUN LU-176 -7.838E-03 2.299E-02 2.326E-02 FAIL ABUN HF-181 -8.063E-01 4.424E+OO 4.439E+OO NOT IDENT. TA-182 9.328E-01 8.816E-01 9.768E-01 FAIL ABUN RE-183 5.395E-01 1. 749E+OO 1. 766E+OO NOT IDENT. RE-184 3.575E+Ol 3.352E+Ol 3. 719E+Ol NOT IDENT. W-188 -l .181E+02 l.142E+02 1. 2 60E+02 FAIL ABUN IR-192 <j l.622E-01 4.427E-01 4.487.E-01 FAIL ABUN HG-20*3 -l.083E-01 2.290E+OO 2.290E+OO FAIL ABUN BI-207 -3.287E-03 3.269E-02 3.273E-02 FAIL ABUN BI-211 3.287E+OO 5.218E-01 1. 571E+OO FAIL ABUN PB-211 3.499E-01 5.574E-01 5.793E-01 NOT IDENT. RN-219 -6.484E-02 3.378E-01 3.391E-01 NOT IDENT. RA-223 1. 2 60E-01 5.034E-01 5.066E-01 FAIL ABUN AC-227 2.015E-01 2.030E-01 2.224E-01 FAIL ABUN TH-227 2.015E-01 2.030E-01 2.224E-01 FAIL ABUN TH-231 1. 260E-01 5.034E-01 5.066E-01 FAIL ABUN PA-234 -l.091E-01 2.640E-01 2.685E-01 FAIL ABUN PA-234M l.210E+OO 3. 722E+OO 3.762E+OO NOT IDENT. NP-237 8 .161E-02 l.531E-01 1. 574E-01 FAIL ABUN NP-238 1. OOOE+41 5.725E+41 O.OOOE+OO SHORT HLIF NP-239 7.289E-02 2.052E-01 2.078E-01 NOT IDENT. PU-239 l.216E+02 3.023E+02 3.073E+02 NOT IDENT. AM-241 -l.082E-02 8.488E-02 8.502E-02 NOT IDENT. CM-243 -l.628E-03 7.335E-02 7.336E-02 NOT IDENT. BK-247 -2.981E-02 6.287E-02 6.429E-02 FAIL ABUN CM-247 1. 744E-02 2.817E-02 2.925E-02 NOT IDENT. CF-249 3.766E-03 3.437E-02 3.441E-02 NOT IDENT. CF-251 1. 701E-02 l.069E-01 1. 072E-01 NOT IDENT. Page 3448 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 77.8223 87.09 87.6782 136.47 70.4387 45.60 76.2650 87.57 87.7463 140.51 0.0000 46.54 76.4388 88.03 87. 8113 143.76 90.5337 49. 72 0.0000 88.34 87.8554 144.24 88.2910 51. 35 83.2463 88.47 87.8737 145.44 78.0803 51. 87 96.2426 89. 96 88.0831 152.43 68.2890 52.39 84.4345 1093.63 88.1783 153.25 0.0000 52. 97 78.5760 91.11 0.0000 323.87 69.5856 53.44 82.6403 92.59 88.4489 156.02 0.0000 54.07 87.7402 93.35 88.5530 158.56 0.0000 57.36 0.0000 94.56 88.7188 159.00 64.1250 57.53 86.3865 94.65 91. 5938 162.33 73.7176 57.98 83.4515 94.67 91.5964 162.66 0.0000 59.27 92.7493 94.87 91.6244 163.33 76.1401 59.32 92.7591 97.43 91.9824 165.86 71.6473 59.54 92.8012 98.43 83.1249 176.31 68.8679 60.96 86.3271 98.44 83.1261 176.60 0.0000 61.17 86.3639 99.53 73.5299 177.52 66.5752 62.93 102.5824 100 .11 76.8399 181.07 0.0000 63.29 102.6558 102.03 64.0339 181. 52 77.9841 63.58 102.7151 103.18 68.4900 184.41 84.5928 64.28 102.8571 103.37 63.0715 143.76 75.5133 66.73 124.1539 105.21 64.3300 193.51 57. 9697 67.24 140.6631 105.31 61.0676 197.03 59.3756 125.81 129.8470 106.12 61.1385 198.01 65.4953 67.75 125.7635 106.47 66.6303 201.83 69.3809 69.67 112.5006 109.28 77. 4965 203.43 60.9512 70.83 141.6166 111. 00 84.6447 205.31 61.0565 72.81 104.8742 111.76 0.0000 210.85 67.0921 72.87 104.8858 114. 06 89.7849 215.65 59.1636 74.66 105.2252 116. 30 . 0. 0000 222 .11 60.7401 74.82 105.2553 116.74 69.7993 227.09 62.2467 74.97 105.2832 119.76 76.7543 227.38 62.2620 77 .11 105.6829 121.12 63.5192 228.16 0.0000 78.74 105.9836 121. 22 63.5275 228.18 41.1211 79.69 106.1568 121.78 63.5740 116.74 41.1211 80.12 106.2356 122.06 66.9447 235.69 57.6846 80.19 0.0000 122.92 71.4873 235. 96 57.6972 80.57 106.3168 123.07 71.5015 238.63 53.6354 81. 00 106.3949 265.00 71.5576 238.98 0.0000 81. 07 106.4073 125.81 69.5116 240.99 53.7396 81. 75 79.8976 127.23 92.1005 242.00 53.7845 83.79 87.2039 127.91 94.4285 244.70 53.9030 84.00 87.2342 129.30 92.3413 252.40 0.0000 85.43 87.4404 131. 20 99.3330 252.80 60.1886 86.55 87.6012 133.02 82.5873 254.15 0.0000 86.79 87.6353 133. 52 80.3744 256.23 41. 6518 86.94 87.6567 136.00 77.2118 260.90 0.0000 Page 3449 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 53.0492 355.39 0.0000 584.27 29.2097 264.80 53.0542 356.01 23.2386 595.83 0.0000 265.00 52.2072 364.49 0.0000 427.87 35.0902 268.22 57.4841 366.42 0.0000 602.52 0.0000 269.46 48.0908 372. 51 35.9023 604.72 31. 0156 270.03 38.6618 37.8010 607.14 21.7332 271.23 34.3970 377.52 26.7769 609.32 23.8254 273.65 0.0000 356.01 37. 9996 610.33 23.8348 276.40 44.8906 388.16 35.3080 614.28 23.3551 277.37 47.5140 388.63 0.0000 618.01 22. 8719 277.60 49.2511 391.69 30.7253 620.36 16.6504 278.00 50.1293 264.66 31. 8204 621.93 23.9499 279.20 48.4440 401.81 34.6514 630.19 0.0000 279.54 43.2648 402.40 22.4839 631.29 17.7706 279.70 43.2699 404.85 24.3914 633.25 26.1536 280.46 41.5625 410.95 32.0064 634.78 0.0000 283.69 39.9253 413.71 33.9419 635.95 24.0875 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 33.0235 423.72 0.0000 645.85 17.8750 285.90 0.0000 427.09 37.9923 657.76 23.7708 287.50 34.8140 427.87 27.5563 657.90 0.0000 290.67 53.6498 433.94 31. 4 605 661.66 20.6331 293.27 0.0000 439.40 30.5964 664.57 0.0000 351.93 38. 0714 453.88 23.1235 666.33 0.0000 295. 96 26.2695 463.37 27 .1102 666.50 0.0000 879.38 18.4229 468.07 33.4843 667.71 0.0000 299.98 27.6618 473.00 0.0000 677.62 19.1646 300.09 27.6638 475.06 17.5320 685.70 0.0000 300.13 27.6644 476.78 25.3462 695.00 0.0000 301.36 42.1924 477.60 31. 2083 696. 49 19.3037 302.85 35.6369 482.18 29.3250 696. 51 19.3037 256.23 27.7496 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 27.8916 306.78 42.3516 497.08 29.5410 697.49 22.5295 308.46 37.1012 505.52 29.6625 702.65 21.4982 311. 90 37.1884 507.63 0.0000 706.68 21.5308 316.51 31.9761 511. 00 32.7140 711. 68 18.3350 319.41 0.0000 514.00 28.2936 720.70 0.0000 320.08 0.0000 514.00 28.2936 721. 93 0.0000 321.04 35.6380 520.40 22.9027 722.78 14.6206 323.87 36.5982 520.69 0.0000 722. 91 14.6212 325.23 50.0334 522.65 0.0000 723.31 14.6234 328.76 0.0000 527.90 0.0000 724.19 14.6277 333.37 48.5057 528.26 20.9889 727.33 16.2720 333.97 47.1765 529.59 27.0022 733.00 17.9361 334.37 51.2330 529.87 0.0000 735.93 9.7939 338.28 39.6494 531.02 0.0000 333.97 6.5330 338.32 39.6503 537.26 0.0000 739.50 0.0000 311. 90 35.1938 546.56 0.0000 747.24 13 .1118 340.48 35.1938 552.55 23.2443 748.06 16.3947 340.55 0.0000 563.25 23.3566 752.31 19.7036 344.28 36.9078 569.33 30.5469 753.82 0.0000 345.93 28.0717 946.00 30.5493 756.73 24 .1198 351.06 31. 7971 569.70 24.4414 756.80 24.1207 351. 93 31.8142 583.19 24.5859 884.68 16.4874 Page 3450 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 23.0978 1274.44 9.7613 1620.50 3.0811 766.42 24.7522 1001.03 11. 5519 1621.92 6.5746 766.84 19.8047 1002.74 11. 557 5 1678.03 0.0000 772.60 0.0000 1004.73 15.1225 1690.97 3.1227 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0 .,0000 1025.87 0.0000 176l!.49 2 .1102 778.90 17.6790 1028.54 0.0000 1063.66 6.3373 783.70 0.0000 1037.84 15.2641 1771.35 3.1694 785.37 9. 9664 1038.76 0.0000 1791.20 0.0000 792.07 13.3193 631.29 13.5004 1808.65 2.1271 794.95 26.6650 1048.07 0.0000 1810.72 0.0000 795.86 16.6711 1049.04 5.7641 1836.06 4.2747 810.06 5.0255 1050.41 18.7408 810.29 5.0259 1063.66 9.0424 344.28 3.3507 1077.00 0.0000 810.76 3. 3511 1077.34 11.7995 815.77 0.0000 1085.87 11.8265 1048.07 0.0000 1093.63 14.5859 832.01 15.7494 1099.45 17.3475 834.85 25.8984 1112. 07 20.1537 835.71 18. 0215 1112. 84 21.9902 836.80 0.0000 1115. 54 10.2689 846.75 0.0000 1120.29 20.1967 846.77 13.5649 1120. 55 20.1980 856.80 0.0000 1221. 41 19.1001 860.56 19.3028 1129. 67 19.3260 871.09 12.5326 1131. 51 0.0000 873.19 12.5406 1147.95 0.0000 875.33 0.0000 1173.23 17.8676 879.38 18.8478 1177.95 14. 9072 880.51 17.1405 1189.05 14.0140 883.24 16.0120 1204.77 13.1310 884.68 19.4515 1221.41 10.3595 889.28 20.6257 1231. 02 20.7673 894.76 19.5131 1235.36 0.0000 898.04 12.6391 1238.28 19.8580 900.72 22.9997 1260.41 0.0000 903.28 10.3579 1271.87 10.4857 911.20 19.6127 1274.44 13.9890 912.08 19.6182 1274.54 13.9899 923.98 0.0000 1291.59 11. 4917 926.50 12.7501 1298.22 0.0000 929 .11 11. 6003 1312 .11 0.0000 937.49 22. 0963 1332.49 5.8004 944 .13 0.0000 1362.66 0.0000 946.00 11. 6593 1365.19 6. 8171 949.00 13.1282 1368.63 0.0000 667.71 0.0000 1384.29 1. 9561 962. 31 4.2177 1408. 01 5.8989 964.08 8.4398 1457.56 0.0000 966.17 0.0000 1460.82 4.9716 911. 20 9.8605 1489.16 8.0020 968. 97 9.8605 1505.03 9.0319 983.53 0.0000 1584.12 8.1577 984.45 0.0000 1596.21 0.0000 Page 3451 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:00:36.81 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM29.CNF;354 Background date : Z-OCT-2016 11:01:41. Sample date 8-DEC-2015 14:13:00. Acquisition date : 3-0CT-2016 08:59:12. Sample ID G405235024 Sample quantity 1.38962E+02 GRAM Detector name GAM29 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.43 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 2 0 5 5 0 0 1 1 3 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 3 3 Page 3452 of 5809 Energy 63.35* 72. 24 74.74* 77.19* 87.06 90.00 92.91* 128.68 185.79* 208.71 210.22 238.69* 241. 95 243.51 270.38 295.21* 300.42 327.86 338.30* 352.07* 438. 11 462.81 471.19 480.06 511. 21* 533.31 583.44* 603.29 609.37* 651.41 661. 67 727.72 795.15 799.26 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 17 48 139 219 68 53 lil 41 90 53 26 404 88 24 36 178 35 50 92 256 13 36 4 69 33 19 115 8 209 23 296 35 26 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 148 66 152 150 170 73 170 175 180 79 78 91 107 93 83 93 51 89 42 98 38 62 32 128 64 27 56 38 63 15 49 9 9 4 0.70 1. 21 1. 22 1.22 1.17 0.95 1. 47 0.89 1. 44 1.16 1.16 1.14 1. 59 1. 44 1. 43 1. 30 2.04 2.44 0.88 1. 42 0. 67 1. 93 0.53 7.12 1. 92 2.54 1. 43 0.64 1. 50 2.54 1. 48 0.97 2.04 2.04 126.67 144.42 149.42 154.32 174.02 179.90 185. 71 257.14 371.21 417.00 420.00 476.89 483.39 486.50 540.20 589.79 600.19 655.01 675.88 703.39 875.32 924.67 941. 41 959.14 1021. 39 1065.57 1165.76 1205.44 1217.59 1301. 62 1322.13 1454.18 1588.99 1597.21 124 143 143 143 172 178 178 253 366 413 413 472 472 472 536 582 596 650 673 697 872 918 939 944 1013 1059 1160 1199 1209 1298 1315 1449 1582 1582 7 4.76E-03126.2 23 1.32E-02 24.4 2.62E+OO 23 3.86E-02 17.6 23 6.08E-02 11.8 7 1.89E-02 34.1 13 l.48E-02 26.2 9.81E-01 13 3.07E-02 24.5 9 1.15E-02 59.6 13 2.51E-02 33.4 12 1.48E-02 31.5 3.60E+OO 12 7.31E-03 62.0 26 1.12E-01 6.3 2.81E+OO 26 2.45E-02 26.3 26 6.56E-03 88.0 9 1.00E-02 48.5 15 4.95E-02 14.1 8 9.85E-03 38.4 13 1. 38E-02 41. 6 7 2.56E-02 15.8 11 7.llE-02 9.8 8 3.61E-03 89.5 12 9.87E-03 47.7 6 1.22E-03210.9 34 l.91E-02 52.1 14 9.27E-03 62.0 11 5.24E-03 58.5 14 3.20E-02 17.2 9 2.23E-03143.5 18 5.80E-02 11.4 8 6.52E-03 35.6 14 8.22E-02 7.7 9 9.71E-03 22.9 19 7.19E-03 34.3 1.08E+OO 19 3.90E-03 38.4 Peak Search Report (continued) Page : 2 Sample ID : G405235024 Acquisition date 3-0CT-2016 08:59:12 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 835.84 12 17 2.48 1670.35 1664 10 3. 41E-03 69.5 36 0 860.94 14 22 0.90 1720.54 1716 10 3.84E-03 69.5 (37 0 911.32* 86 27 1. 45 1821.,29 . 1816 13 2.40E-02 16.6 38 0 933.01 12 16 1. 37 1864.68 1859 9 3.19E-03 68.7 39 0 954.17 17 30 6.47 1907.01 1892 20 4.67E-03 83.5 40 0 965.07 26 13 1. 94 1928.80 1924 9 7.14E-03 32.4 41 0 969. 22* 51 19 1. 50 1937.09 1933 12 1. 41E-02 22.7 42 0 1000.45* 16 15 0.88 1999.57 1993 14 4.48E-03 57.5 43 0 1052.34 6 23 1. 50 2103.36 2097 12 1.63E-03163.1 44 0 1093.39 13 11 2.16 2185.47 2179 12 3.66E-03 58.8 45 0 1120.44* 44 6 1. 61 2239.59 2234 11 1.23E-02 19.2 46 0 1148. 58 9 13 0.92 2295.89 2288 10 2.61E-03 77.6 47 0 1151.13 11 13 1. 35 2300.99 2298 8 3.15E-03 61.1 48 0 1300. 05 10 2 3.25 2598.97 2594 9 2.73E-03 42.0 49 0 1352 .11 10 4 1.16 2703.17 2698 9 2.74E-03 49.8 50 0 1378.52* 9 12 0.88 2756.02 2747 16 2.59E-03 91. 3 51 0 1425.60 16 0 4.00 2850.25 2845 11 4.44E-03 25.0 52 0 1460.87* 360 13 1. 77 2920. 86 2912 14 1.00E-01 5.7 53 0 1508 .11 10 3 0.64 3015.41 3009 10 2.84E-03 42.9 54 0 1729.99 12 2 1. 93 3459.68 3454 9 3.40E-03 35.6 55 0 1764.73* 37 0 1. 36 3529.26 3524 10 1. 03E..:.02 18.1 56 0 1871.53 6 0 0.99 3743.17 3739 7 1. 67E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 3453 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:00:38 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 8-DEC-2015 14:13:00 G405235024 Acquisition date : Sample quantity Sampla geometry Detector geometry: 3-0CT-2016 08:59:12 138. 96 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA29 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 . 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3454 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:01.43 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235024 Acquisition date 3-0CT-2016 08:59:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.347E+OO 1.298E+Ol l.298E+Ol 11. 35 cOK MN-54 834.85 99.98* 2.116E+OO 3.152E-02 6.135E-02 138. 96 OK CD-109 88.03 3.70* 6.255E+OO 7.744E-01 l.215E+OO 172.03 OK SN-126 64.28 9.60 3.603E+OO 3.278E-01 3.278E-01 252.49 OK 86.94 8.90 6.255E+OO 3.219E-01 3.219E-01 172. 03 OK 87.57 37.00* 6.255E+OO 7.744E-02 7.744E-02 172.03 OK CS-134 563.25 8.34 2.846E+OO Line Not Found Absent 569.33 15.37 2.823E+OO Line Not Found Absent 604. 72 97. 62 2.703E+OO 1.695E-02 2.231E-02 286.91 OK 795.86 85.46* 2.197E+OO 7.517E-02 9.896E-02 68.70 OK 801. 95 8.69 2.183E+OO Line Not Found Absent 1365.19 3.02 1.430E+OO Line Not Found Absent BA-137M 661.66 89.90* 2.522E+OO 7.232E-01 7.370E-01 15.36 OK CS-137 661. 66 85.10* 2.522E+OO 7.640E-01 7.785E-01 15.36 OK TL-208 277.37 6.60 4.914E+OO Line Not Found Absent 583.19 85.00* 2.772E+OO 2.734E-01 2.734E-01 34.39 OK 860.56 12*. 50 2.069E+OO 2.895E-01 2.895E-01 139.00 OK PB-212 74.82 10.28 5.094E+OO l.050E+OO 1.050E+OO 60.99 OK 77 .11 17.10 5.365E+OO 1.557E+OO 1.557E+OO 23.57 OK 238.63 43.60* 5.495E+OO 1.013E+00 1.013E+OO 12.55 OK 300.09 3.30 4.622E+OO 1.373E+OO 1.373E+OO 76.89 OK BI-214 609.32 45.49* 2.683E+OO 9.538E-01 9. 541E-01 22.80 OK 1120. 29 14.92 l.685E+OO 9.323E-01 9.326E-01 38.48 OK 1764.49 15.30 l.129E+OO l.090E+00 1. 091E+OO 36.10 OK PB-214 74.82 5.80 5.103E+00 Line Not Found <<INT Reject 77 .11 9.70 5.365E+OO 2.745E+OO 2.746E+00 23.57 OK 87.09 3.41 6.257E+OO Line Not Found <<INT Reject 242.00 7.25 5.441E+OO Line Not Found <<INT Reject 295.22 18.42 4.685E+OO l.219E+OO 1.220E+OO 28.25 OK 351. 93 35.60* 4.086E+OO 1. 026E+00 1.026E+OO 19.69 OK RN-222 609.32 45.49* 2.683E+OO 9.538E-01 9. 541E-01 22.80 OK 1120. 29 14.92 1.685E+OO 9.323E-01 9.326E-01 38.48 OK 1764.49 15.30 1.129E+OO l.090E+OO 1.091E+OO 36.10 OK RA-224 240.99 4.10* 5. 441E+OO 2.178E-01 2.178E-01 638.47 OK RA-226 609.32 45.49* 2.683E+OO 9.538E-01 9.541E-01 22.80 OK 1120.29 14.92 1.685E+OO 9.323E-01 9.326E-01 38.48 OK 1764.49 15.30 1.129E+OO 1.090E+OO 1.091E+OO 36.10 OK AC-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 1.134E+OO 1.134E+OO 31. 65 OK 794.95 4.25 2.197E+OO 1.512E+OO 1.512E+OO 68.70 OK 835.71 1. 61 2.116E+OO l.957E+00 1.957E+OO 138. 96 OK 911.20 25.80* 1.981E+OO 9.123E-01 9.123E-01 33.21 OK 968. 97 15.80 1. 889E+OO 9.088E-01 9.088E-01 45.33 OK RA-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 1.134E+OO 1.134E+OO 31. 65 OK 794.95 4.25 2.197E+OO 1.512E+OO 1.512E+OO 68.70 OK 835.71 1. 61 2 .116E+OO 1.957E+OO 1.957E+OO 138. 96 OK 911.20 25.80* 1.981E+OO 9.123E-01 9.123E-01 33.21 OK 968. 97 15.80 1.889E+OO 9.088E-01 9.088E-01 45.33 OK Page 3455 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235024 Acquisition date 3-0CT-2016 08:59:12 Nuclide* Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 5.094E+OO 1.050E+OO 1.050E+OO 60.99 Ori 77 .11 17.10 5.365E+OO 1.557E+OO l.557E+OO 23.57 OK 238.63 43.60* 5.495E+OO 1.013E+OO 1.013E+OO 12.55 OK 300.09 3.30 4.622E+OO 1.373E+OO l.373E+OO 76. 89 OK TH-230 609.32 45.49* 2. 683E+OO 9.538E-01 9.538E-01 22.80 OK 1120. 29 14.92 1.685E+OO 9.323E-01 9.323E-01 38.48 OK 1764.49 15.30 1.129E+OO 1.090E+OO l.090E+OO 36.10 OK PA-231 283.69 1. 70 4.831E+OO Line Not Found Absent 301.36 5.35* 4.622E+00 8.467E-01 8.467E-01 76. 89 OK TH-232 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 1.134E+OO 1.134E+OO 31. 65 OK 835.71 1. 61 2 .116E+OO 1.957E+OO 1.957E+00 138. 96 OK 911.20 25.80* 1.981E+OO 9.123E-01 9.123E-01 33.21 OK 968. 97 15.80 1.889E+OO 9.088E-01 9.088E-01 45.33 OK TH-234 63.29 3.70* 3.603E+OO 8.506E-01 8.506E-01 252.49 OK 92.59 4.23 6.639E+OO 2.536E+OO 2.536E+OO 48.92 OK U-234 609.32 45.49* 2.683E+OO 9.538E-01 9.538E-01 22.80 OK 1120.29 14.92 1.685E+OO 9.323E-01 9.323E-01 38.48 OK 1764.49 15.30 1.129E+OO 1.090E+OO 1.090E+OO 36.10 OK U-235 89. 96 3.47 6.460E+OO l.538E+OO 1.538E+OO 52.32 OK 93.35 5.60 6.639E+OO 1.916E+OO 1.916E+OO 48.92 OK 143.76 10. 96* 7.247E+00 Line Not Found Absent 163.33 5.08 6.922E+OO Line Not Found Absent 185. 72 57.20 6.480E+OO 1.493E-01 1.493E-01 66.77 OK 205.31 5.01 6.095E+OO Line Not Found Absent U-238 63.29 3.70* 3.603E+OO 8.506E-01 8.506E-01 252.49 OK 92. 59 4.23 6.639E+OO 2.536E+OO 2.536E+OO 48.92 OK AM-243 43.53 5.90 7.707E-01 Line Not Found Absent 74.66 67.20* 5.094E+OO l.607E-01 1.607E-01 60.99 OK ANH-511 511.00 100.00* 3.064E+OO 6.163E-02 6.163E-02 123.96 OK Flag: "*" = Keyline Page 3456 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:39.74 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l *
  • Acquisition date 3-0CT-2016 08:59:12 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.43 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:13:00 Analyst initials: MXRl *
  • Sample ID G405235024 Sample Quantity 1.3896E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.298E+Ol 1.444E+OO MN-54 6.135E-02 8.355E-02 CD-109 1.215E+OO 2.048E+OO SN-126 7.744E-02 1.306E-01 CS-134 9.896E-02 6.662E-02 BA-137M 7.370E-01 l.109E-01 CS-137 7.785E-01 l.172E-01 TL-208 2.734E-01 9.212E-02 PB-212 1.013E+OO 1.246E-01 BI-214 9.541E-01 2.132E-01 PB-214 1.026E+OO 1.980E-01 RN-222 9.541E-01 2.132E-01 RA-224 2.178E-01 1.363E+OO RA-226 9. 541E-01 2.132E-01 AC-228 9.123E-01 2. 969E-01 RA-228 9.123E-01 2.969E-01 TH-228 1. 013E+OO 1.246E-01 TH-230 9.538E-01 2.132E-01 PA-231 8.467E-01 6.380E-01 TH-232 9.123E-01 2. 969E-01 TH-234 8.506E-01 2.105E+OO U-234 9.538E-01 2 .132E-01 U-235 3. 851E-02 1.724E-01 U-238 8.506E-01 2.105E+OO AM-243 l.607E-01 9.604E-02 ANH-511 6.163E-02 7.487E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3457 of 5809 Key-Line Activity (pCi/GRAM 9. 431E+OO 7.646E-03 O.OOOE+OO 2.291E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1.239E+Ol 3.797E-02 1. 960E+41 2.462E-02 MDA (pCi/GRAM 6. 781E-01 l.027E-01 2. ll 7E+OO 1. 356E-01 7.303E-02 5.493E-02 5.803E-02 6.244E-02 8.337E-02 l.065E-01 l.278E-01 1.065E-01 8.935E-01 1. 065E-01 2.203E-01 2.203E-01 8.337E-02 l.064E-01 8.399E-01 2.203E-01 1.985E+OO 1.064E-01 3.178E-01 1.985E+OO 8.528E-02 5.255E-02 MDA (pCi/GRAM 2.423E+Ol 7.704E-02 O.OOOE+OO 6.743E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 -2.693E-01 3.440E-01 5.743E-01 FAIL ABUN V-48 O.OOOE+OO 1.129E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 3.959E+02 O.OOOE+OO SHORT HLIF C0-56 -2.534E-01 3.559E-01 6.065E-01 NOT IDENT. MN-56 O.OOOE+OO l.395E+41 O.OOOE+OO SHORT HLIF C0-57 l.558E-02 4.338E-02 8.298E-02 NOT IDENT. C0-58 2.225E-01 5.020E-01 1.047E+OO NOT IDENT. FE-59 2 .115E+OO 4.555E+OO 1.006E+Ol NOT IDENT. C0-60 l.120E-02 4.075E-02 8.128E-02 NOT IDENT. ZN-65 1.345E-01 1.373E-01 3. OlOE-01

  • NOT IDENT. GE-68 -l.424E-02 2.313E+OO 4.389E+OO NOT IDENT. AS-73 8.773E+OO 8.373E+OO 1.723E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.409E+03 O.OOOE+OO SHORT HLIF SE-75 -8.318E-02 2.192E-01 3.769E-01 NOT IDENT. BR-77 O.OOOE+OO 2.210E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 4.547E+02 O.OOOE+OO SHORT HLIF RB-83 6.235E-01 5.286E-01 l.200E+OO NOT IDENT. KR-85 3.208E+OO 6.712E+OO l.261E+Ol NOT IDENT. SR-85 3.371E-01 7.086E-01 1.331E+OO NOT IDENT. RB-86 O.OOOE+OO 2.726E+04 O.OOOE+OO SHORT HLIF Y-88 -4.574E-02 2.182E-01 4.409E-01 NOT IDENT. Y-91 -3.038E+02 4.663E+02 7.730E+02 NOT IDENT. NB-94 -1.188E-02 3.102E-02 5.650E-02 NOT IDENT. NB-95 -7.194E-01 7.903E-01 1.315E+OO NOT IDENT. NB-95M 1. 462E+OO 2.276E+OO 4.075E+OO NOT IDENT. ZR-95 1. 729E+OO 1. 232E+OO 2.873E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 040E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.444E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 6.146E-02 7.180E-02 6.150E-02 FAIL ABUN RH-102 -2.658E-03 5.395E-02 1.045E-01 NOT IDENT. RU-103 -1.204E+OO 4.498E+OO 8.645E+OO FAIL ABUN RH-106 2.714E-01 3.874E-01 8.462E-01 NOT IDENT. RU-106 2.714E-01 3.874E-01 8.462E-01 NOT IDENT. AG-108M 2.457E-03 2.876E-02 5.137E-02 NOT IDENT. AG-llOM 8.045E-03 8.857E-02 1. 747E-01 NOT IDENT. SN-113 -5.652E-02 2.109E-01 4.040E-01 NOT IDENT. CD-115 O.OOOE+OO 2.793E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.367E+04 O.OOOE+OO SHORT HLIF TE-123M 1.418E-02 1.339E-01 2.462E-01 NOT IDENT. SB-124 4.256E-01 1.338E+OO 3.388E+OO NOT IDENT. SB-125 -4.288E-03 l.060E-01 2.054E-01 FAIL ABUN TE-125M -2.771E+02 2.477E+02 4.197E+02 NOT IDENT. I-126 O.OOOE+OO 8.877E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8. 696E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.022E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 5.128E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.771E+26 O.OOOE+OO SHORT HLIF BA-133 -6.492E-03 4.293E-02 7.464E-02 NOT IDENT. I-133 O.OOOE+OO 9.586E+40 O.OOOE+OO SHORT HLIF CS-135 -2.064E-02 l.533E-01 2.480E-01 NOT IDENT. I-135 O.OOOE+OO 1.675E+41 O.OOOE+OO SHORT HLIF CS-136 0.000E+OO 2.467E+05 O.OOOE+OO SHORT HLIF CE-139 -8.108E-02 1.058E-01 l.805E-01 NOT IDENT. BA-140 O.OOOE+OO 1.274E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.585E+05 O.OOOE+OO SHORT HLIF CE-141 3. 964E+OO 2.230E+Ol 4.161E+Ol NOT IDENT. CE-143 O.OOOE+OO 8.562E+40 O.OOOE+OO SHORT HLIF CE-144 4.415E-03 3.617E-01 6.655E-01 NOT IDENT. PM-144 2.748E-02 5. 811E-02 1.165E-01 NOT IDENT. PR-144 2.387E+OO 5.048E+OO l.012E+Ol NOT IDENT. PM-146 2.273E-02 4.257E-02 8.737E-02 NOT IDENT. ND-147 O.OOOE+OO 3.268E+07 O.OOOE+OO SHORT HLIF PM-147 -2.367E+02 7.745E+02 l.403E+03 NOT IDENT. PM-149 O.OOOE+OO 4.543E+40 O.OOOE+OO SHORT HLIF EU-150 1. 741E-02 2.574E-02 4.919E-02 FAIL ABUN EU-152 -7.064E-02 8.836E-02 l.612E-01 FAIL ABUN . GD-153 6. 911E-03 1.562E-01 2.942E-01 NOT IDENT. EU-154 1.656E-02 9.259E-02 1.872E-01 NOT IDENT. EU-155 1.163E-01 l.025E-01 2.067E-01 FAIL ABUN TB-160 -l.887E-03 1.843E+OO 3.530E+OO FAIL ABUN H0-166M -l.095E-02 4.703E-02 8.884E-02 FAIL ABUN TM-171 -6.546E+00 l.997E+Ol 3.758E+Ol NOT IDENT. HF-172 1.328E-01 2.274E-01 4 .114E-01 FAIL ABUN LU-172 8.750E-02 l.009E-01 l.382E-01 FAIL ABUN LU-176 1.356E-02 2.450E-02 4.642E-02 FAIL ABUN Page 3458 of 5809 HF-181 -1.184E+OO 3.796E+OO 6.425E+OO NOT IDENT. TA-182 -1.535E-01 8.0lOE-01 1.468E+OO FAIL ABUN RE-183 -l.494E-01 2.816E+OO 5.376E+OO NOT IDENT. RE-184 1.433E+Ol 2.680E+Ol 5.620E+Ol NOT IDENT. W-188 -4.208E+Ol 1.163E+02 1. 819E+02 FAIL ABUN IR-192 1.969E-01 5.028E-01 9.290E-01 FAIL ABUN HG-203 -1.693E+OO 2.470E+OO 4.085E+OO FAIL ABUN BI-207 -1.873E-02 5.148E-02 9 .119E-02 FAIL ABUN PB-210 -3.241E-Ol 3.128E-f-OO 6.038E+OO NOT IDENT. BI--:211 O.OOOE+OO 5.453E-.Ol 8.020E-01 FAIL ABUN PB-211 l.292E-01 6.637E-01 1.316E+OO NOT IDENT. BI-212 O.OOOE+OO 5.512E-01 1.133E+OO FAIL ABUN RN-219 -1.207E-01 3.592E-01 6.807E-01 FAIL ABUN RA-223 3.231E-01 5.187E-01 l.008E+OO FAIL ABUN AC-227 -l.829E-01 2.270E-01 3.725E-01 FAIL ABUN TH-227 -l.829E-01 2.270E-01 3.725E-01 FAIL ABUN TH-229 3.173E-03 4.456E-01 8.095E-01 FAIL ABUN TH-231 3. 231E-01 5.187E-01 1.008E+OO FAIL ABUN PA-233 -2.598E-02 6.275E-02 l.058E-01 FAIL ABUN PA-234 -1.214E-01 2.758E-01 4.254E-01 NOT IDENT. PA-234M 5.576E+OO 6.280E+OO 8.564E+OO FAIL ABUN NP-237 -2.598E-02 6.275E-02 l.058E-01 FAIL ABUN NP-238 O.OOOE+OO 1.244E+41 O.OOOE+OO SHORT HLIF NP-239 4.189E-02 2.277E-01 4.292E-01 NOT IDENT. PU-239 5.574E+02 6.512E+02 6. 596E+02 FAIL ABUN AM-241 1. 625E-02 l.317E-01 2.537E-01 NOT IDENT. CM-243 -6.249E-02 9.406E-02 1.667E-01 NOT IDENT. BK-247 -8.779E-03 7.529E-02 l.332E-01 NOT IDENT. CM-247 2.728E-02 3.317E-02 6.974E-02 NOT IDENT. CF-249 -9 .112E-03 3.637E-02 6.950E-02 NOT IDENT. CF-251 8.050E-03 l.058E-01 l.946E-01 NOT IDENT. Page 3459 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:00:37.59 Nuclide Line Activity Report ** Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 345 10.66* 1. 34 7E+OO 1. 2 98E+Ol 1.298E+Ol 11. 35 MN-54 834.85 12 99.98* 2 .116E+OO 3.152E-02 6.135E-02 138. 96 CD-109 88.03 81 3.70* 6.255E+OO 1.898E+OO 2.978E+OO 68.17 SN-126 64.28 21 9.60 3.603E+OO 3.278E-01 3.278E-01 252.49 86.94 81 8.90 6.255E+OO 7.890E-01 7.890E-01 68.17 87.57 81 37.00* 6.255E+OO l.898E-01 l.898E-01 68.17 CS-134 563.25 ------8.34 2.846E+OO ------Line Not Found ------569.33 ------15.37 2.823E+OO ------Line Not Found ------604. 72 8 97.62 2.703E+00 l.695E-02 2. 231E-02 286.91 795.86 26 85.46* 2.197E+OO 7.517E-02 9. 896E-02 68.70 801.95 ------8.69 2.183E+OO ------Line Not Found ------1365.19 ------3.02 1.430E+OO ------Line Not Found ------BA-137M 661.66 303 89.90* 2.522E+OO 7.232E-01 7.370E-01 15.36 CS-137 661.66 303 85.10* 2.522E+00 7.640E-01 7.785E-01 15.36 TL-208 277.37 ------6.60 4.914E+00 ------Line Not Found ------583'.19 119 85.00* 2.772E+OO 2.734E-01 2.734E-01 34.39 860.56 14 12.50 2.069E+OO 2.895E-01 2.895E-01 139. 00 BI-211 72.87 58 1. 23 4.798E+OO 5.284E+OO 5.284E+OO 48.75 351.06 276 12.92* 4.086E+OO 2.826E+OO 2.826E+OO 19.69 PB-212 74.82 168 10.28 5.094E+OO 1.738E+OO 1. 738E+OO 35.12 77 .11 264 17.10 5.365E+OO 1.557E+OO 1.557E+OO 23.57 238.63 449 43.60* 5.495E+00 l.013E+00 1.013E+OO 12.55 300.09 39 3.30 4.622E+OO 1.373E+OO 1.373E+OO 76. 89 BI-214 609.32 215 45.49* 2.683E+OO 9.538E-01 9.541E-01 22.80 1120.29 43 14.92 1.685E+OO 9.323E-01 9.326E-01 38.48 1764.49 35 15.30 1.129E+OO l.090E+00 1.091E+OO 36.10 PB-214 74.82 168 5.80 5.094E+OO 3.081E+OO 3.082E+00 35.12 77 .11 264 9.70 5.365E+OO 2.745E+OO 2.746E+OO 23.57 87.09 81 3.41 6.255E+OO 2.059E+OO 2.060E+OO 68.17 242.00 98 7.25 5.441E+00 1.342E+OO 1.343E+OO 52.67 295.22 195 18.42 4.685E+OO 1.219E+OO 1.220E+OO 28.25 351. 93 276 35.60* 4.086E+OO l.026E+OO l.026E+OO 19.69 RN-222 609.32 215 45.49* 2.683E+OO 9.538E-01 9.541E-01 22.80 1120.29 43 14.92 1.685E+00 9.323E-01 9.326E-01 38.48 1764.49 35 15.30 1.129E+00 1.090E+OO 1. 091E+OO 36.10 RA-224 240.99 98 4.10* 5.441E+OO 2.374E+OO 2.374E+00 52. 67 RA-226 609.32 215 45.49* 2.683E+OO 9.538E-01 9.541E-01 22.80 1120.29 43 14.92 l.685E+OO 9.323E-01 9.326E-01 38.48 1764.49 35 15.30 1.129E+OO l.090E+00 1. 091E+OO 36.10 AC-228 105.21 ------1.10 7.155E+00 ------Line Not Found ------338.32 100 11. 27 4.215E+OO l.134E+OO l.134E+00 31. 65 794.95 26 4.25 2.197E+OO 1.512E+OO 1.512E+OO 68.70 835. 71 12 1. 61 2 .116E+OO 1.957E+OO l.957E+00 138. 96 911. 20 86 25.80* 1.981E+OO 9.123E-01 9.123E-01 33.21 968. 97 50 15.80 l.889E+OO 9.088E-01 9.088E-01 45.33 RA-228 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 100 11.27 4.215E+OO 1.134E+OO 1.134E+OO 31. 65 Page 3460 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235024 Acquisition date 3-0CT-2016 08:59:12 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 26 4.25 2.197E+OO l.512E+OO 1. 512E+OO 68.70 835.71 12 1. 61 2 .116E+OO 1.957E+OO 1.957E+OO 138. 96 911.20 86 25.80* 1.981E+OO 9.123E-01 9.123E-01 33.21 968.97 50 15.80 1.889E+OO 9.088E-01 9.088E-01 45.33 TH-228 74.82 168 10.28 5.094E+OO 1.738E+OO 1. 738E+OO 35.12 77 .11 264 17.10 5.365E+OO 1.557E+OO 1.557E+OO 23.57 238.63 449 43.60* 5.495E+OO l.013E+OO 1.013E+OO 12.55 300.09 39 3.30 4.622E+OO 1.373E+OO l.373E+OO 76.89 TH-230 609.32 215 45.49* 2.683E+OO 9.538E-01 9.538E-01 22.80 1120.29 43 14.92 l.685E+OO 9.323E-01 9.323E-01 38.48 1764.49 35 15.30 1.129E+OO 1.090E+OO 1.090E+OO 36.10 PA-231 283.69 ------1. 70 4.831E+OO ------Line Not Found ------301.36 39 5.35* 4.622E+OO 8.467E-01 8.467E-01 76.89 TH-232 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 100 11. 27 4.215E+OO 1.134E+OO 1.134E+OO 31. 65 835. 71 12 1. 61 2 .116E+OO 1.957E+OO 1.957E+OO 138. 96 911.20 86 25.80* 1. 981E+OO 9.123E-01 9.123E-01 33.21 968.97 50 15.80 1.889E+OO 9.088E-01 9.088E-01 45.33 TH-234 63.29 21 3.70* 3.603E+OO 8.506E-01 8.506E-01 252.49 92.59 132 4.23 6.639E+OO 2.536E+OO 2.536E+OO 48.92 U-234 609.32 215 45.49* 2.683E+OO 9.538E-01 9.538E-01 22.80 1120.29 43 14.92 1.685E+OO 9.323E-01 9.323E-01 38.48 1764.49 35 15.30 1.129E+OO 1.090E+OO 1.090E+OO 36.10 U-235 89. 96 64 3.47 6.460E+OO 1.538E+OO 1.538E+OO 52.32 93.35 132 5.60 6.639E+OO 1.916E+OO l.916E+OO 48.92 143.76 ------10. 96* 7.247E+OO ------Line Not Found ------163.33 ------5.08 6.922E+OO ------Line Not Found ------185. 72 102 57.20 6.480E+OO 1.493E-01 l.493E-01 66.77 205.31 ------5.01 6.095E+OO ------Line Not Found ------U-238 63.29 21 3.70* 3.603E+OO 8.506E-01 8.506E-01 252.49 92.59 132 4.23 6.639E+OO 2.536E+OO 2.536E+OO 48.92 AM-243 43.53 ------5.90 7.707E-01 ------Line Not Found ------74.66 168 67.20* 5.094E+OO 2.659E-01 2.659E-01 35.12 ANH-511 511. 00 35 100.00* 3.064E+OO 6.163E-02 6.163E-02 123. 96 Flag: "*" Key line Page 3461 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235024 Acquisition date 3-0CT-2016 08:59:12 Total number of lines in spectrum 56 Number of unidentified lines 16 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 MN-54 CD-109 SN-126 CS-134 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 312.05D 461. 40D 2.30E+05Y 2.07Y 30.08Y 30.08Y l.41E+10Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1.41E+10Y 1600.00Y l.41E+l0Y 1. 41E+l0Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 95 1. 57 1. 00 1. 32 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.298E+Ol 3.152E-02 1.898E+OO 1. 898E-01 7.517E-02 7.232E-01 7.640E-01 2.734E-01 2.826E+OO l.013E+OO 9.538E-01 1.026E+OO 9.538E-01 2.374E+OO 9.538E-01 9.123E-01 9.123E-01 1. 013E+OO 9.538E-01 8.467E-01 9.123E-01 8.506E-01 9.538E-01 l.493E-01 8.506E-01 2.659E-01 6.163E-02 3. 572E+Ol 3.572E+Ol Decay Corr pCi/GRAM 1.298E+Ol 6.135E-02 2.978E+OO 1. 898E-01 9.896E-02 7.370E-01 7.785E-01 2.734E-01 2.826E+OO l.013E+OO 9. 541E-01 1.026E+OO 9. 541E-01 2.374E+OO 9. 541E-01 9.'123E-01 9.123E-01 1.013E+OO 9.538E-01 8.467E-01 9.123E-01 8.506E-01 9.538E-01 l.493E-01 8.506E-01 2.659E-01 6.163E-02 3.689E+Ol 3.689E+Ol 71.43% Decay Corr 2-Sigma Error 0.147E+Ol 8.525E-02 2.030E+OO 1.294E-01 6.798E-02 1.132E-01 1.196E-01 0.940E-01 0.556E+00 0.127E+00 2.176E-01 0.202E+OO 2.176E-01 l.250E+00 2.176E-01 3.029E-01 3.029E-01 0.127E+00 2.175E-01 6.510E-01 3.029E-01 21.48E-01 2.175E-01 0.997E-01 21.48E-01 0.934E-01 7.640E-02 "M" Manually accepted
  • 2-Sigma %Error 11. 35 138. 96 68.17 68.17 68.70 15.36 15.36 34.39 19.69 12.55 22.80 19.69 22.80 52.67 22.80 33.21 33.21 12.55 22.80 76.89 33.21 252.49 22.80 66.77 252.49 35.12 123. 96 Flags: "K" Keyline not found "E" = Manually "A" = Nuclide specific abn. limit Page 3462 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235024 Acquisition date : 3-0CT-2016 08:59:12 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 128.68 48 203 0.89 257.14 253 9 l.15E-02 **** 7.39E+OO T 1 208.71 60 89 1.16 417.00 413 12 1. 48E-02 63.0 6.03E+OO 1 210.22 30 87 1.16 420.00 413 12 7.31E-03 **** 6.00E+OO T 3 .. 243.51 26 103 1. 44 486.50 4 72 6.56E-03 **** 5.42E+OO T 0 270.38 40 91 1. 43 540.20 536 9 1. OOE-02 97.0 5.0lE+OO T 0 327.86 54 97 2.44 655.01 650 13 1. 38E-02 83.2 4.32E+OO T 0 438 .11 14 40 0.67 875.32 872 8 3.61E-03 **** 3.45E+OO T 0 462. 81 38 66 1. 93 924.67 918 12 9.87E-03 95.3 3.31E+OO T 0 471.19 5 33 0.53 941.41 939 6 1. 22E-03 **** 3.26E+OO 0 480.06 72 135 7.12 959.14 944 34 1. 91E-02 **** 3.21E+OO 0 533.31 20 28 2.54 1065.57 1059 11 5.24E-03 **** 2.97E+OO 0 651. 41 24 15 2.54 1301. 62 1298 8 6.52E-03 71. 3 2.55E+OO 0 727. 72 36 9 0.97 1454.18 1449 9 9.71E-03 45.9 2.35E+OO T 3 799.26 14 4 2.04 1597.21 1582 19 3.90E-03 76.7 2.19E+OO 0 933.01 11 15 1. 37 1864.68 1859 9 3.19E-03 **** 1.95E+OO 0 954.17 17 30 6.47 1907.01 1892 20 4.67E-03 **** 1. 91E+OO T 0 965. 07 26 13 1. 94 1928.80 1924 9 7.14E-03 64.8 1.90E+OO T 0 1000.45 16 15 0.88 1999.57 1993 14 4.48E-03 **** 1. 84E+OO T 0 1052.34 6 23 1.50 2103.36 2097 12 l.63E-03 **** 1.77E+OO 0 1093.39 13 11 2.16 2185.47 2179 12 3.66E-03 **** 1. 72E+OO T 0 1148.58 9 12 0.92 2295.89 2288 10 2. 61E-03 **** 1. 65E+OO T 0 1151.13 11 12 1. 35 2300.99 2298 8 3.15E-03 **** 1.65E+OO 0 1300.05 10 2 3.25 2598.97 2594 9 2.73E-03 84.0 1.49E+OO 0 1352 .11 10 4 1.16 2703.17 2698 9 2.74E-03 99.7 1.44E+OO 0 1378.52 9 11 0.88 2756.02 2747 16 2.59E-03 **** 1.42E+OO 0 1425.60 15 0 4.00 2850.25 2845 11 4.44E-03 50.0 1.38E+OO 0 1508 .11 10 3 0.64 3015.41 3009 10 2.84E-03 85.8 1.31E+OO 0 1729.99 12 2 1. 93 3459.68 3454 9 3.40E-03 71. 3 1. 15E+OO 0 1871.53 6 0 0.99 3743.17 3739 7 l.67E-03 81. 6 1. 06E+OO Flags: "T" = Tentatively associated Page 3463 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:51.61 *******************************************************************************
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  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l * *Acquisition date 3-0CT-2016 08:59:12 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.43 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:13:00 Nuclide Library : SOLID *
  • Sample ID G405235024 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.3896E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 CD-109 SN-126 CS-134 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2. 881E-01 4.454E-02 l.007E+OO 6.452E-02 3.132E-02 2.412E-02 2.548E-02 2.806E-02 3.853E-02 4. 714E-02 5.875E-02 4. 714E-02 4.129E-01 4. 714E-02 9.568E-02 9.568E-02 3.853E-02 4.712E-02 3.894E-01 9.568E-02 9.342E-01 4. 712E-02 l.493E-01 9.342E-01 4.039E-02 2.384E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3464 of 5809 Le (pCi/GRAM 1.101E+Ol 3.249E-02 O.OOOE+OO 2.707E-02 2.434E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 . TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3465 of 5809 O.OOOE+OO O.OOOE+OO 2. 511E-01 O.OOOE+OO 3.889E-02 4.590E-01 4.218E+OO 3.504E-02 1.303E-01 1. 911E+OO 8.142E+OO O.OOOE+OO l.742E-01 O.OOOE+OO O.OOOE+OO 5.388E-01 5.708E+OO 6.025E-01 O.OOOE+OO 1.729E-01 3.244E+02 2.517E-02 5.733E-01 1. 896E+OO 1.283E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.895E-02 4.632E-02 3.800E+OO 3.735E-01 3.735E-01 2.330E-02 7.581E-02 1.833E-01 O.OOOE+OO O.OOOE+OO 1.157E-01 1.282E+OO 9.389E-02 1. 952E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.417E-02 O.OOOE+OO l.147E-01 O.OOOE+OO O.OOOE+OO 8.398E-02 O.OOOE+OO O.OOOE+OO 1.950E+Ol O.OOOE+OO 3.134E-01 5.283E-02 4.589E+OO 3.988E-02 O.OOOE+OO 6.563E+02 O.OOOE+OO 2.273E-02 7.354E-02 1.380E-01 7.882E-02 9.764E-02 1. 551E+OO 3.867E-02 1. 766E+Ol 1.933E-01 5.989E-02 2.144E-02 2.822E+OO SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3466 of 5809 6.275E-01 2.531E+OO 2.466E+Ol 8.316E+Ol 4.303E-01 l.879E+OO 3.988E-02 2.854E+OO 3.869E-01 6.039E-01 5.190E-01 3.095E-01 4.607E-01 l.710E-01 l.710E-01 3.776E-01 4.607E-01 4.856E-02 l.807E-01 3.806E+OO 4.856E-02 O.OOOE+OO 2.0lSE-01 3.134E+02 l.197E-01 7.807E-02 6.165E-02 3.205E-02 3.175E-02 9.068E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:00:56.72 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235024.CNF;l * *Acquisition date 3-0CT-2016 08:59:12 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.43 Half life ratio : ***** *
  • Sample date 8-DEC-2015 14:13:00 Nuclide Library : SOLID *
  • Sample ID G405235024 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.3896E+02 GRAM *
  • Quantity Err(%) : 1.4392E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016'09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 1.298E+Ol 1. 596E+OO MN-54 6.135E-02 8.359E-02 CD-109 1.215E+OO 2.062E+OO SN-126 7.744E-02 1.314E-01 CS-134 9. 896E-02 6.675E-02 BA-137M 7.370E-01 1.154E-01 CS-137 7.785E-01 1.219E-01 TL-208 2.734E-01 9.285E-02 PB-212 1.013E+OO 1.356E-01 BI-214 9.541E-01 2 .171E-01 PB-214 1.026E+OO 2.025E-01 RN-222 9.541E-01 2 .171E-01 RA-224 2.178E-01 1.370E+OO RA-226 9.54iE-01 2.171E-01 AC-228 9.123E-01 3.006E-01 RA-228 9.123E-01 3.006E-01 TH-228 1.013E+OO 1. 356E-01 TH-230 9.538E-01 2 .171E-01 PA-231 8.467E-01 6. 631E-01 TH-232 9.123E-01 3.006E-01 TH-234 8.506E-01 2 .113E+OO U-234 9.538E-01 2.171E-01 U-235 3.851E-02 1. 724E-01 U-238 8.506E-01 2 .113E+OO AM-243 1.607E-01 9.746E-02 ANH-511 6.163E-02 7. 491E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3467 of 5809 Key-Line Activity (pCi/GRAM 9.431E+OO 7.646E-03 1.000E+41 2.291E-02 K.L Act error ( 1. 96-sigma) 1.240E+Ol 3.797E-02 4.382E+41 2.466E-02 TPU ( 1. 96-sigma) 1. 596E+OO 8.359E-02 2.062E+OO l.314E-01 6.675E-02 1.154E-01 1.219E-01 9.285E-02 1.356E-01 2.171E-01 2.025E-01 2.171E-01 1.370E+OO 2 .171E-01 3.006E-01 3.006E-01 1.356E-01 2 .171E-01 6.631E-01 3.006E-01 2 .113E+00 2 .171E-01 1.724E-01 2 .113E+OO 9.746E-02 7.491E-02 TPU (1.96-sigma) 1.310E+Ol 3.813E-02 O.OOOE+OO 2.674E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 -2.693E-01 3.442E-01 3.650E-01 FAIL ABUN V-48 -9.055E+03 1.129E+04 1.201E+04 SHORT HLIF CR-51 -3.470E+02 3. 961E+02 4.259E+02 SHORT HLIF C0-56 -2.534E-01 3.561E-01 3.739E-01 NOT IDENT. MN-56 -l.000E+41 1.396E+41 O.OOOE+OO SHORT HLIF C0-57 l.558E-02 4.339E-02 4.395E-02 NOT IDENT. C0-58 2.225E-01 5.021E-01 5.120E-01 NOT IDENT. FE-59 2 .115E+OO 4.558E+OO 4.657E+OO NOT IDENT. C0-60 1.120E-02 4.076E-02 4.107E-02 NOT IDENT. ZN-65 1 ... 345E-01 1.374E-01 1.501E-01 NQT IDENT. GE-68 -l.424E-02 2. 313E+OO 2.313E+OO NOT IDENT. AS-73 8.773E+OO 8.566E+OO 9.434E+OO NOT IDENT. AS-74 -3. 451E+03 5.416E+03 5.635E+03 SHORT HLIF SE-75 -8.318E-02 2.192E-01 2.224E-01 NOT IDENT. BR-77 1. 798E+38 1.556E+39 O.OOOE+OO SHORT HLIF SR-82 -2.266E+Ol 4.547E+02 4.548E+02 SHORT HLIF RB-83 6.235E-01 5.355E-01 6.047E-01 NOT IDENT. KR-85 3.208E+00 6.713E+OO 6.867E+00 NOT IDENT. SR-85 3.371E-01 7.088E-01 7.249E-01 NOT IDENT. RB-86 -3.282E+03 2.726E+04 2.730E+04 SHORT HLIF Y-88 -4.574E-02 2.182E-01 2.192E-01 NOT IDENT. Y-91 -3.038E+02 4.664E+02 4.861E+02 NOT IDENT. NB-94 -l.188E-02 3.103E-02 3.149E-02 NOT IDENT. NB-95 -7.194E-01 7.909E-01 8.548E-01 NOT IDENT. NB-95M l.462E+00 2.279E+OO 2. 372E+OO NOT IDENT. ZR-95 1. 729E+OO 1.235E+00 1.460E+OO NOT IDENT. NB-97 -1. OOOE+41 l.041E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 2.148E+41 O.OOOE+OO SHORT HLIF M0-99 -3.130E+31 1.445E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 3.986E+41 O.OOOE+OO SHORT HLIF RH-101 6.146E-02 7.266E-02 7.776E-02 FAIL ABUN RH-102 -2.658E-03 5.395E-02 5.397E-02 NOT IDENT. RU-103 -1.204E+00 4.498E+OO 4. 531E+OO FAIL ABUN RH-106 2. 714E-01 3.877E-01 4.066E-01 NOT IDENT. RU-106 2.714E-01 3.877E-01 4.066E-01 NOT IDENT. AG-108M 2.457E-03 2.876E-02 2.878E-02 NOT IDENT. AG-llOM 8.045E-03 8.857E-02 8.865E-02 NOT IDENT. SN-113 -5.652E-02 2.109E-01 2.125E-01 NOT IDENT. CD-115 1.278E+38 2.793E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 2.248E+04 9.371E+04 9.426E+04 SHORT HLIF TE-123M l.418E-02 1.339E-01 l.340E-01 NOT IDENT. SB-124 4.256E-01 1.338E+OO 1.352E+OO NOT IDENT. SB-125 -4.288E-03 l.060E-01 1.060E-01 FAIL ABUN TE-125M -2.771E+02 2.482E+02 2.779E+02 NOT IDENT. I-126 -9.604E+04 8.878E+05 8.889E+05 SHORT HLIF SB-126 6.220E+04 8.697E+05 8.701E+05 SHORT HLIF SB-127 -1.280E+22 2.680E+22 O.OOOE+OO SHORT HLIF I-131 6.239E+09 5.136E+09 5.855E+09 SHORT HLIF I-132 l.OOOE+41 1.898E+42 0.000E+OO SHORT HLIF TE-132 1.837E+26 3.844E+26 O.OOOE+OO SHORT HLIF BA-133 -6.492E-03 4.293E-02 4.303E-02 NOT IDENT. I-133 -1. OOOE+41 2.047E+41 O.OOOE+OO SHORT HLIF CS-135 -2.064E-02 l.533E-01 1.536E-01 NOT IDENT. I-135 1.000E+41 6.978E+41 O.OOOE+OO SHORT HLIF CS-136 2.233E+05 2.479E+05 2.676E+05 SHORT HLIF CE-139 -8.108E-02 1. 071E-01 1.132E-01 NOT IDENT. BA-140 2.003E+05 1.274E+06 1.277E+06 SHORT HLIF LA-140 3.376E+04 3.585E+05 3.589E+05 SHORT HLIF CE-141 3. 964E+OO 2.230E+Ol 2.237E+Ol NOT IDENT. CE-143 l.OOOE+41 8.622E+40 O.OOOE+OO SHORT HLIF CE-144 4.415E-03 3.617E-01 3.617E-01 NOT IDENT. PM-144 2.748E-02 5. 813E-02 5.944E-02 NOT IDENT. PR-144 2.387E+OO 5.049E+OO 5.162E+OO NOT IDENT. PM-146 2.273E-02 4.260E-02 4.381E-02 NOT IDENT. ND-147 6.708E+06 3.269E+07 3.282E+07 SHORT HLIF PM-147 -2.367E+02 7.746E+02 7.819E+02 NOT IDENT. PM-149 -4.743E+40 4.661E+40 O.OOOE+OO SHORT HLIF EU-150 l.741E-02 2.575E-02 2.692E-02 FAIL ABUN EU-152 -7.064E-02 '8.845E-02 9.401E-02 FAIL ABUN GD-153 6. 911E-03 l.562E-01 l.562E-01 NOT IDENT. EU-154 1.656E-02 9.259E-02 9.289E-02 NOT IDENT. EU-155 1.163E-01 l.029E-01 l.155E-01 FAIL ABUN TB-160 -1. 887E-03 l.843E+00 1.843E+OO FAIL ABUN H0-166M -l.095E-02 4.704E-02 4.729E-02 FAIL ABUN TM-171 -6.546E+OO 1.998E+Ol 2.020E+Ol NOT IDENT. HF-172 1.328E-01 2.284E-01 2.361E-01 FAIL ABUN LU-172 8.750E-02 l.013E-01 l.087E-01 FAIL ABUN LU-176 l.356E-02 2.450E-02 2.525E-02 FAIL ABUN Page 3468 of 5809 HF-181 -l.184E+OO 3.796E+OO 3.834E+OO NOT IDENT. TA-182 -l.535E-01 8.0lOE-01 8.040E-01 FAIL ABUN RE-183 -1.494E-01 2.816E+OO 2.817E+00 NOT IDENT. RE-184 l.433E+Ol 2.701E+Ol 2.778E+Ol NOT IDENT. W-188 -4.208E+Ol 1.164E+02 l.180E+02 FAIL ABUN IR-192 1. 969E-01 5.029E-01 5.106E-01 FAIL ABUN HG-203 -l.693E+OO 2.471E+00 2.586E+OO FAIL ABUN BI-207 -1.873E-02 5.149E-02 5.218E-02 FAIL ABUN PB-210 -3.241E-01 3.128E+OO 3.131E+OO NOT IDENT. * . BI-211 2.826E+OO . 5.597E-01 . 1.392E+OO FAIL ABUN PB-211 1.292E-01 6.637E-01 6.662E-01 NOT IDENT. BI-212 1. 22 6E+OO 5.547E-01 7.831E-Ol FAIL ABUN RN-219 -l.207E-01 3.595E-01 3.636E-01 FAIL ABUN RA-223 3.231E-01 5.190E-01 5.391E-01 FAIL ABUN AC-227 -l.829E-01 2.282E-01 2.427E-01 FAIL ABUN TH-227 -1.829E-01 2.282E-01 2.427E-01 FAIL ABUN TH-229 3.173E-03 4.456E-01 4.456E-01 FAIL ABUN TH-231 3.231E-01 5.190E-01 5.391E-01 FAIL ABUN PA-233 -2.598E-02 6.276E-02 6.384E-02 FAIL ABUN PA-234 -1.214E-01 3.088E-01 3.136E-01 NOT IDENT. PA-234M 5.576E+OO 6.285E+OO 6.769E+OO FAIL ABUN NP-237 -i. 598E-02 6.276E-02 6.384E-02 FAIL ABUN NP-238 -l.000E+41 1.245E+41 O.OOOE+OO SHORT HLIF NP-239 4.189E-02 2.277E-01 2.285E-01 NOT IDENT. PU-239 5.574E+02 6.517E+02 6.985E+02 FAIL ABUN AM-241 1.625E-02 1.318E-01 1.320E-01 NOT IDENT. CM-243 -6.249E-02 9.424E-02 9.836E-02 NOT IDENT. BK-247 -8.779E-03 7.531E-02 7.542E-02 NOT IDENT. CM-247 2.728E-02 3.349E-02 3.567E-02 NOT IDENT. CF-249 -9.112E-03 3.637E-02 3. 661E-02 NOT IDENT. CF-251 8.050E-03 1.058E-01 1.058E-01 NOT IDENT. Page 3469 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 93.1266 87.09 126.8845 136.47 79.2768 45.60 75.3984 87.57 126. 9696 140.51 0.0000 46.54 85.1069 88.03 127.0510 143.76 66.7467 49. 72 0.0000 88.34 53.3025 144.24 72. 2530 51. 35 99.4402 88.47 53.3120 145.44 70.1484 51. 87 94.7076 89. 96 95.8847 152.43 84.9860 52.39 88.9976 1093.63 78.1500 153.25 0.0000 52.97 81. 3484 91.11 0.0000 323.87 59.7044 53.44 71. 727 6 92.59 78.3567 156.02 0.0000 54.07 78.6056 93.35 78.4365 158.56 0.0000 57.36 0.0000 94.56 70.2936 159.00 78.8631 57.53 86.9195 94.65 70.3019 162.33 76.8838 57.98 87. 9672 94.67 70.3040 162.66 0.0000 59.27 96.0067 94.87 67.5644 163.33 69.1483 59.32 91.1165 97.43 74.7098 165.86 78.2555 59.54 91.1520 98.43 78. 9630 176.31 59.8159 60.96 90.39'65 98.44 78.9641 176.60 0.0000 61.17 90.4295 99.53 80.1153 177.52 61. 0096 62.93 85.7740 100 .11 83.2990 181.07 0.0000 63.29 85.8270 102.03 84.5466 181.52 58.9570 63.58 85.8691 103.18 76.3071 184.41 65.9253 64.28 77.7359 103.37 89.9171 143.76 65.9996 66.73 88.6375 105.21 67.0693 193.51 64.1467 67.24 104.6004 105.31 68.1257 197.03 75.8241 125.81 99.3759 106.12 82.8815 198.01 79.3348 67.75 99.3866 106.47 78.7193 201.83 70.3563 69.67 94.3792 109.28 86.3624 203.43 63.5182 70.83 117.1937 111. 00 81. 2650 205.31 50.8918 72.81 106.2046 111.76 0.0000 210.85 55.7644 72.87 106.2143 114. 06 92.1537 215.65 62.9723 74.66 106.5095 116. 30 0.0000 222 .11 66.8030 74.82 106.5354 116.74 74.3798 227*. 09 52.9383 74.97 106.5596 119.76 69.3080 227.38 54.1266 77 .11 106.9074 121.12 77.9590 228.16 0.0000 78.74 107.1686 121. 22 77.9674 228.18 60.0466 79.69 107.3190 121.78 83.3606 116.74 60.0466 80.12 107.3869 122.06 66.2823 235.69 45.7798 80.19 0.0000 122.92 66.3466 235. 96 45.7886 80.57 107.4581 123.07 65.2872 238.63 49.8333 81. 00 107.5260 265.00 83.5391 238.98 0.0000 81. 07 107.5374 125.81 65.8452 240.99 49.9186 81. 75 107.6433 127.23 86.0193 242.00 49.9551 83.79 101.8501 127.91 94.6924 244.70 50.0519 84.00 85.5797 129.30 94.8361 252.40 0.0000 85.43 119. 7834 131. 20 96.4720 252.80 57.5317 86. 55 113.1557 133. 02 96.2994 254.15 0.0000 86. 79 113.1937 133.52 86.6077 256.23 58.8709 86. 94 126.8580 136.00 93.3486 260.90 0.0000 Page 3470 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 58.0034 355.39 0.0000 584.27 26.4950 264.80 58.0093 356.01 42.1674 595.83 0.0000 265.00 54.3906 364.49 0.0000 427.87 29.9952 268.22 53.2987 366.42 0.0000 602.52 0.0000 269.46 38.7949 372.51 37.8215 604. 72 22.8896 270.03 38.8096 375.05 46.4799 607.14 " 20.0464 271.23 38.8408 377.52 49.1270 609.32 20. 0626 273.65 0.0000 356.01 30.2668 610.33 20.0703 276.40 43.8464 388.16 41. 6016 614.28 18.6645 277.37 42.6552 388.63 0.0000 618.01 15.3359 277.60 42.6616 391.69 36.4689 620.36 23.0244 278.00 42.6733 264.66 37.5095 621. 93 11. 5190 279.20 58.5688 401.81 39.2770 630.19 0.0000 279.54 57.3616 402.40 29.6850 631. 29 21.1908 279.70 57.3673 404.85 38.4633 633.25 12.5308 280.46 47.6265 410.95 28.9361 634.78 0.0000 283.69 40.3839 413.71 32.4887 635.95 19.2977 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 37.9790 423. 72 0.0000 645.85 26.1453 285.90 0.0000 427.09 39.7742 657.76 27.7161 287.50 40.4836 427.87 38.9055 657.90 0.0000 290.67 45.8919 433.94 30.5946 661. 66 17.5291 293.27 0.0000 439.40 28.0079 664.57 0.0000 351.93 32.8743 453.88 28.6471 666.33 0.0000 295. 96 32.8898 463.37 29.6726 666.50 0.0000 879.38 19.7666 468.07 25.2309 667. 71 0.0000 299.98 37.9187 473.00 0.0000 677.62 21.5452 300.09 37.9215 475.06 21. 6953 685.70 0.0000 300 .13 37.9225 476.78 21.7124 695.00 0.0000 301.36 54.4521 477.60 21. 7202 696.49 24.6440 302.85 39.6377 482.18 21. 7651 696. 51 24.6440 256.23 44.6385 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 28.5953 306.78 38.4927 497.08 20.9958 697.49 27.6104 308.46 44.7473 505.52 27.4866 702.65 27.6593 311. 90 47.3318 507.63 0.0000 706.68 10.8809 316.51 44. 9659 511. 00 32.1432 711. 68 17.8352 319.41 0.0000 514.00 23.4487 720. 70 0.0000 320.08 0.0000 514.00 23.4487 721. 93 0.0000 321. 04 47.5928 520.40 11. 9870 722.78 10.4427 .323.87 27.6000 520.69 0.0000 722. 91 17.9026 325.23 35.1555 522.65 0.0000 723. 31 17.9048 328.76 0.0000 527.90 0.0000 724 .19 14.9249 333.37 39.1076 528.26 16.6523 727. 33 9. 9605 333.97 36. 5969 529.59 16. 6611 733.00 12.9725 334.37 36.6058 529.87 0.0000 735.93 13.9840 338.28 43.0136 531. 02 0.0000 333.97 8*. 9941 338.32 43.0146 537.26 0.0000 739.50 0.0000 311. 90 40.5342 546.56 0.0000 747.24 19.0487 340.48 40.5342 552.55 19.6226 748.06 17.0477 340.55 0.0000 563.25 23.4609 752.31 16.0671 344.28 49.9313 569.33 20.6957 753.82 0.0000 345.93 40.6602 946.00 23.5199 756.73 8.0452 351. 06 43.3259 569.70 23.5209 756.80 8.0452 351.93 43.3477 583.19 26.4836 884.68 19.1515 Page 3471 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 7 65. 81 27.2318 1274.44 12.9336 1620.50 6.4706 766.42 25.2187 1001.03 12.9497 1621.92 3.6985 766.84 25.2228 1002.74 14.5750 1678.03 0.0000 772.60 0.0000 1004.73 12. 9624 1690.97 1. 8718 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50. 0.0000 ' 1025 .. 87 0.0000 1764.49
  • 0.9477 778.90 10.1278 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 18.5204 1771. 35 0.9488 785.37 20. 2962 1038.76 0.0000 1791.20 0.0000 792.07 16.7793 631. 29 13 .1016 1808.65 0.9547 794.95 12.2144 1048.07 0.0000 1810.72 0.0000 795.86 12.2178 1049.04 4.9160 1836.06 5.7539 810.06 10.2258 1050.41 11. 4750 810.29 10.2266 1063.66 20.8338 344.28 12.2725 1077.00 0.0000 810.76 12.2739 1077.34 15.4025 815.77 0.0000 1085.87 18.7432 1048.07 0.0000 1093.63 9.9412 832.01 18.5295 1099.45 5.5310 834.85 14.4238 1112. 07 16.6431 835.71 14.4278 1112. 84 17.7565 836.80 0.0000 1115. 54 4. 9969 846.75 0.0000 1120.29 8.8939 846.77 14.4751 1120. 55 8.8945 856.80 0.0000 1221.41 10. 0078 860.56 14.5338 1129. 67 12.2568 871.09 17.7028 1131.51 0.0000 873.19 15.6293 1147.95 0.0000 875.33 0.0000 1173.23 15.7591 879.38 17.7450 1177.95 15.7762 880.51 18.7947 1189.05 9.0378 883.24 14.6295 1204.77 15.8730 884.68 13.5903 1221.41 13.6563 889.28 18.8423 1231. 02 19.3879 894.76 18.8716 1235.36 0.0000 898.04 14.6916 1238.28 20.5620 900. 72 17.8529 1260.41 0.0000 903.28 10.5094 1271. 87 11. 5072 911.20 14.7463 1274.44 8. 0596 912.08 14.7497 1274.54 8.0601 923.98 0.0000 1291. 59 10. 4011 926.50 5.2889 1298.22 0.0000 929.11 12.7026 1312 .11 0.0000 937.49 17.8247 1332.49 10.4912 944.13 0.0000 1362.66 0.0000 946.00 15.9515 1365.19 10.5630 949.00 13.8363 1368.63 0.0000 667.71 0.0000 1384.29 8.4832 962. 31 12.8179 1408.01 8.8788 964.08 9.6178 1457.56 0.0000 966 .17 6.4155 1460.82 10.7666 911.20 14.4459 1489.16 4.5105 968.97 14.4459 1505.03 2.8955 983.53 0.0000 1584.12 8.2645 984.45 0.0000 1596.21 0.0000 Page 3472 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:01:37.87 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM02.CNF;493 Background date : Z-OCT-2016 11:00:01. Sample date 8-DEC-2015 13:38:00. Acquisition date : 3-0CT-2016 09:01:15. Sample ID G405235025 Sample quantity : 1 .. 38244E+02 GRAM Detector name : GAM02 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.48 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 3 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 72.58* 74.86* 77.02 87.50 92.77* 185.73* 238.46* 242.28 270.66 278.10 295.35 299.97 338.51* 351.90* 457.37 462.66 517. 62 583.23* 609.31* 661.52* 709.24 727. 23 769.76 891. 86 911.10* 941.84 965.23* 968.88* 1120 .15* 1228.04 1258.08 1460.57* 1764.70* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 8 86 165 30 60 76 324 79 69 28 148 27 88 200 40 41 40 90 161 1629 14 37 17 11 83 17 10 33 34 7 25 306 25 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 75 183 168 232 244 182 189 134 180 154 169 91 105 103 63 72 66 62 51 34 23 21 34 12 14 19 27 15 18 23 23 11 3 1.14 1.14 0.95 0.94 1. 33 1. 47 1.11 1. 24 3.44 1. 63 1.13 1. 41 1. 56 1. 36 1. 75 2.74 2.35 1. 50 1. 59 1. 56 5.22 2.30 2.83 3.64 2.19 3.94 0.66 1. 54 1. 42 2.58 4.37 2.50 2.33 144.66 149.21 153.52 174.46 185.00 370.75 476.11 483.75 540.46 555.32 589.79 599.04 676.04 702.80 913.56 924.15 1033.97 1165. 09 1217.22 1321.56 1416.93 1452.88 1537.87 1781.91 1820.35 1881. 79 1928.54 1935.83 2238.18 2453.83 2513.88 2918.62 3526.57 143 143 143 169 181 366 471 481 531 550 583 596 672 697 910 920 1029 1158 1210 1313 1409 1448 1527 1775 1815 1874 1921 1932 2229 2443 2501 2911 3520 15 2.19E-03162.l 2.95E+OO 15 2.40E-02 29.3 15 4.59E-02 14.3 8 8.38E-03 89.8 10 l.68E-02 54.2 11 2.lOE-02 38.3 10 9.0lE-02 9.8 9 2.20E-02 29.9 16 1.93E-02 45.3 11 7.78E-03 87.9 13 4.12E-02 19.8 8 7.40E-03 65.2 12 2.45E-02 25.6 10 5.55E-02 12.0 9 1.llE-02 38.6 8 1.14E-02 39.l 13 1.llE-02 44.5 14 2.50E-02 21.7 15 4.48E-02 12.8 15 4.52E-01 2.6 15 3.75E-03 81.3 11 1. 02E-02 29. 5 15 4.74E-03 78.1 12 3.06E-03 69.8 11 2.30E-02 14.5 16 4.64E-03 64.5 12 2.86E-03108.1 11 9.21E-03 28.7 14 9.43E-03 32.5 12 l.90E-03153.8 24 7.03E-03 54.8 15 8.51E-02 6.3 12 6.90E-03 27.5 Flag: "*" = Peak area was modified by background subtraction Page 3473 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:01:39 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 13:38:00 G405235025 Acquisition date : Sample quantity Sample geomet:i<y Detector geometry: 3-0CT-2016 09:01:15 138.24 GRAM Sample typEE? Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA2 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3474of5809 PB-214 PB-214 PB-214 PB-214 TL-208 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 277.37 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 HG-203 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 279.20 74.66 74.82 74.82 351.06 CAN 0 01:00:00.48 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235025 Acquisition date 3-0CT-2016 09:01:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.060E+0() 1.410E+Ol 1.410E+Ol 12. 62 OK BA-137M 661.66 89.90* 2.016E+OO 4.997E+OO 5.092E+OO 5.22 OK CS-137 661.66 85.10* 2.016E+OO 5.279E+OO 5.379E+OO 5.22 OK HG-203 70.83 3.69 3.355E+OO Line Not Found Absent 72.87 6.19 3.544E+OO 2.360E-01 2.043E+Ol 324.14 OK 279.20' 81.56* 4.164E+OO 2.751E-02 2.381E+OO 315.48 OK TL-208 277.37 6.60 4.173E+OO Line Not Found <<INT Reject 583.19 85.00* 2.233E+OO 2.666E-01 2.666E-01 43.48 OK 860.56 12.50 1.634E+OO Line Not Found Absent PB-212 74.82 10.28 3.779E+OO 7.765E-01 7.765E-01 115. 07 OK 77 .11 17.10 3.992E+OO 1.584E+OO 1.584E+OO 28. 65 OK 238.63 43.60* 4.703E+OO 9.530E-01 9.530E-01 19.57 OK 300.09 3.30 3. 911E+OO 1.222E+OO 1.222E+OO 130.41 OK BI-214 609.32 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 OK 1120.29 14.92 1.323E+OO 9.153E-01 9.156E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 OK PB-214 74.82 5.80 3.775E+OO Line Not Found <<INT Reject 77 .11 9.70 3.992E+OO 2.792E+OO 2.793E+OO 28.65 OK '87. 09 3.41 4.866E+OO 1.178E+OO 1.178E+OO 179.68 OK 242.00 7.25 4. 651E+OO Line Not Found <<INT Reject 295.22 18.42 3.962E+00 1.206E+OO 1.206E+OO 39.65 OK 351.93 35.60* 3.416E+OO 9.612E-01 9.615E-01 23.99 OK RN-222 609.32 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 OK 1120.29 14.92 1.323E+OO 9.153E-01 9.156E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 OK RA-224 240.99 4.10* 4.647E+OO 3.704E-01 3.704E-01 464.33 OK RA-226 609.32 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 OK 1120.29 14.92 1.323E+OO 9.153E-01 9.156E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 OK AC-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3. 531E+OO 1.301E+OO 1. 301E+OO 51.16 OK 794.95 4.25 1.740E+OO Line Not Found Absent 835.71 1. 61 1.672E+OO Line Not Found Absent 911.20 25.80* 1. 561E+OO 1.114E+OO 1.114E+OO 28.98 OK 968. 97 15.80 l.487E+OO 7.606E-01 7.606E-01 57.36 OK RA-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3. 531E+OO 1.301E+OO 1. 301E+OO 51.16 OK 794.95 4.25 1. 740E+OO Line Not Found Absent 835.71 1. 61 1.672E+OO Line Not Found Absent 911.20 25.80* 1.561E+OO 1.114E+OO 1.114E+00 28.98 OK 968. 97 15.80 1.487E+OO 7.606E-01 7.606E-01 57.36 OK TH-228 74.82 10.28 3.779E+OO 7.765E-01 7.765E-01 115. 07 OK 77 .11 17.10 3.992E+OO 1.584E+OO 1.584E+OO 28.65 OK 238.63 43.60* 4.703E+00 9.530E-01 9.530E-01 19.57 OK 300.09 3.30 3. 911E+OO 1.222E+OO l.222E+00 130.41 OK TH-230 609.32 45.49* 2.154E+OO 9.207E-01 9.207E-01 25.70 OK 1120.29 14.92 1.323E+OO 9.153E-01 9.153E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.290E-01 55.03 OK PA-231 283.69 1. 70 4.097E+OO Line Not Found Absent Page 3475 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235025 Acquisition date Page : 3 3-0CT-2016 09:01:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 301.36 5.35* 3. 911E+OO 7. 540E-01 7.540E-01 130.41 OK TH-232 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.531E+OO 1.301E+OO l.301E+OO 51.16 OK 835. 71 1. 61 1. 672E+OO Line Not Found Absent 911.20 25.80* 1. 561E+OO 1.114E+OO l .114E+OO 28.98 OK 968. 97 15.80 1. 487E+OO 7.606E-01 7.606E-01 57.36 OK U-234 609.32 45.49* 2.154E+OO 9.207E-01 9.207E-01 25.70 OK 1120.29 14.92 1.323E+OO 9.153E-01 9.153E-01 64. 96 OK 1764.49 15.30 8.930E-01 9.290E-01 9.290E-01 55.03 OK AM-243 43.53 5.90 2.878E-01 Line Not Found Absent 74.66 67.20* 3.779E+OO 1.188E-01 1.188E-01 115. 07 OK Flag: "*" = Keyline Page 3476of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:01:40.65 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l *
  • Acquisition date 3-0CT-2016 09:01:15 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:38:00 Analyst initials: MXRl *
  • Sample ID G405235025 Sample Quantity 1.3824E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.410E+Ol 1. 743E+OO BA-137M 5.092E+OO 2.603E-01 CS-137 5.379E+OO 2.750E-01 HG-203 2.381E+OO 7.361E+OO TL-208 2.666E-01 l .136E-01 PB-212 9.530E-01 l.828E-01 BI-214 9.210E-01 2.320E-01 PB-214 9.615E-01 2.261E-01 RN-222 9.210E-01 2.320E-01 RA-224 3.704E-01 1.686E+OO RA-226 9.210E-01 2.320E-Ol AC-228 1.114E+OO 3.165E-01 RA-228 1.114E+OO 3.165E-01 TH-228 9.530E-01 l.828E-01 TH-230 9.207E-01 2.319E-01 PA-231 7.540E-01 9.636E-01 TH-232 l .114E+OO 3.165E-01 U-234 9.207E-01 2.319E-01 AM-243 l.188E-01 1.340E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3477 of 5809 Key-Line Activity (pCi/GRAM 1.116E+Ol 2.517E-02 O.OOOE+OO -l.146E-02 7.694E-02 O.OOOE+OO O.OOOE+OO 8.808E-03 -2.099E-01 O.OOOE+OO -5.256E-02 K.L. Cnt Uncert ( 1 . '96-sigma ) 2.205E+Ol 5:260E-02 7.426E+40 3.389E-02 4.747E-01 1.589E+04 5.855E+02 7.637E-02 5.713E-01 1. 960E+41 6.336E-02 MDA (pCi/GRAM 7.327E-01 8.412E-02 8.887E-02 6 .196E+OO 7.886E-02 1.378E-01 1.646E-01 l.913E-01 l.646E-01 1.667E+OO 1.646E-01 3.234E-01 3.234E-01 1.378E-01 l.645E-01 1.125E+OO 3.234E-01 1.645E-01 1.270E-01 MDA (pCi/GRAM 4.168E+Ol l .115E-01 0.000E+OO 6.708E-02 8.380E-01 O.OOOE+OO O.OOOE+OO l.515E-01 1.061E+OO O.OOOE+OO l.059E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 6.041E-02 6.614E-01 1.327E+OO NOT IDENT. FE-59 l.134E+00 7.697E+OO l.540E+Ol NOT IDENT. C0-60 2.904E-03 5.003E-02 9.793E-02 NOT IDENT. ZN-65 8.404E-02 2.056E-01 3.882E-01 NOT IDENT. GE-68 -5.071E-01 2.600E+OO 4.934E+00 NOT IDENT. AS-73 2.324E+OO 1.603E+Ol 3.032E+Ol NOT IDENT. AS-74 O.OOOE+OO 8.622E+03 O.OOOE+OO SHORT HLIF SE-75 -2. 396E-01 3.288E-01 5.183E-01 FAIL ABUN BR-77 0.000E+OO 3.268E+37 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 8.797E+02 O.OOOE+OO SHOR.T HLIF RB-83 2.277E-01 1. 076E+OO 1.813E+OO NOT IDENT. KR-85 -4.606E+Ol 1. 729E+Ol 1.942E+Ol NOT IDENT. SR-85 -4.867E+OO 1.827E+OO 2.052E+OO NOT IDENT. RB-86 O.OOOE+OO 3.100E+04 O.OOOE+OO SHORT HLIF Y-88 5.231E-02 l.540E-01 4.248E-01 NOT IDENT. Y-91 -3.265E+02 6.188E+02 l.080E+03 NOT IDENT. NB-94 l.383E-02 3.938E-02 7.290E-02 NOT IDENT. NB-95 -5.155E-01 1. 065E+OO l.735E+OO NOT IDENT. NB-95M -5.541E-01 3.365E+OO 5.660E+OO NOT IDENT. ZR-95 -4.858E-02 1.638E+OO 3.231E+00 NOT IDENT. NB-97 O.OOOE+OO l.364E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 7.813E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.977E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.347E-02 4.720E-02 8.212E-02 NOT IDENT. RH-102 -5.587E-02 7.999E-02 l.320E-01 NOT IDENT. RU-103 5.291E+OO 8.698E+OO 1.691E+Ol FAIL ABUN RH-106 3.664E-01 6.435E-01 1.277E+OO NOT IDENT. RU-106 3.664E-01 6.435E-01 1.277E+OO NOT IDENT. AG-108M -1. 789E-02 4.639E-02 8.208E-02 NOT IDENT. CD-109 1. 703E+OO 2.999E+OO 2.952E+OO FAIL ABUN AG-110M 3.027E-02 1. 070E-01 2.175E-01 NOT IDENT. SN-113 3.862E-01 3.802E-01 7.527E-01 NOT IDENT. CD-115 O.OOOE+OO 4.476E+39 O.OOOE+OO SHORT HLIF SN-117M 0.000E+OO l.285E+05 O.OOOE+OO SHORT HLIF TE-123M -3.518E-02 1. 753E-01 3.357E-01 NOT IDENT. SB-124 -5.349E-01 1.858E+OO 3.847E+OO NOT IDENT. SB-125 1. 483E-01 l.868E-01 3.607E-01 FAIL ABUN TE-125M 8. 963E+Ol 3.866E+02 7.050E+02 NOT IDENT. I-126 O.OOOE+OO 1.165E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.430E+06 O.OOOE+OO SHORT HLIF SN-126 1. 086E-01 l.912E-01 l.943E-01 FAIL ABUN SB-127 O.OOOE+OO 2.622E+22 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 7.924E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.277E+26 O.OOOE+OO SHORT HLIF BA-133 1.067E-03 6.629E-02 l.106E-01 NOT IDENT. I-133 O.OOOE+OO 1.258E+41 O.OOOE+OO SHORT HLIF CS-134 6.142E-02 5.941E-02 l.307E-01 NOT IDENT. CS-135 1.531E-01 l.950E-01 3.867E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 4.086E+05 O.OOOE+OO SHORT HLIF CE-139 2.862E-02 1. 241E-01 2.455E-01 NOT IDENT. BA-140 0.000E+OO l.987E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.069E+05 O.OOOE+OO SHORT HLIF CE-141 -4.192E+Ol 3.231E+Ol 5.107E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 280E+41 O.OOOE+OO SHORT HLIF CE-144 -2.177E-01 4. 719E-01 8.085E-01 NOT IDENT. PM-144 1.131E-02 6. 551E-02 l.314E-01 NOT IDENT. PR-144 9.825E-01 5.690E+OO 1.141E+Ol NOT IDENT. PM-146 -3.209E-03 8.445E-02 1.366E-01 NOT IDENT. ND-147 O.OOOE+OO 4.732E+07 O.OOOE+OO SHORT HLIF PM-147 3 .119E+02 1. 017E+03 1.873E+03 NOT IDENT. PM-149 O.OOOE+OO 6.279E+40 O.OOOE+OO SHORT HLIF EU-150 1.919E-02 4.046E-02 7.085E-02 FAIL ABUN EU-152 2. 596E-02 1.42'1E-01 2.429E-01 FAIL ABUN GD-153 -5.715E-02 2.777E-01 4. 591E-01 NOT IDENT. EU-154 6.448E-02 1.295E-01 2. 7 51E-01 NOT IDENT. EU-155 7.081E-02 l.415E-01 2.650E-01 FAIL ABUN TB-160 1.360E+OO 2 .113E+OO 4.563E+OO FAIL ABUN H0-166M -l.342E-02 6.223E-02 1.058E-01 FAIL ABUN TM-171 -1.346E+Ol 3.933E+Ol 7.211E+Ol NOT IDENT. HF-172 -2.579E-02 3.085E-01 5.465E-01 NOT IDENT. LU-172 2.066E-02 9.199E-02 l.848E-01 FAIL ABUN LU-176 -9.477E-03 3.347E-02 6.151E-02 FAIL ABUN HF-181 1.524E+OO 7.273E+OO 1.350E+Ol NOT IDENT. TA-182 -3.884E-01 1. 341E+OO 2.081E+OO FAIL ABUN RE-183 -1.506E+OO 5.135E+OO 9.379E+OO NOT IDENT. Page 3478 of 5809 RE-184 8 .. 722E+00 3.298E+Ol 6.799E+Ol NOT IDENT. W-188 9.662E+Ol l.655E+02 2.960E+02 NOT IDENT. IR-192 *-3 .103E-02 6.270E-01 l.174E+OO FAIL ABUN BI-207 l.700E-02 4.652E-02 9.940E-02 FAIL ABUN PB-210 l.178E+00 6.676E+00 1. 269E+Ol NOT IDENT. BI-211 O.OOOE+OO 6.228E-01 9.734E-01 FAIL ABUN PB-211 -4.126E-01 l.098E+00 l.953E+OO NOT IDENT. BI-212 O.OOOE+OO 9.447E-01 1.529E+OO FAIL ABUN RN-219 -1.423E-01 6.267E-01 l.129E+OO FAIL ABUN R.t\-223 3.427E-01 8.308E-01 .l.603E+OO FAIL ABUN AC-227 3.517E-02 2.972E-01 5.691E-01 FAIL ABUN TH-227 3.517E-02 2. 972E-01 5.691E-01 FAIL ABUN TH-229 -3.194E-01 6.313E-01 1.173E+OO FAIL ABUN TH-231 3.427E-01 8.308E-01 1.603E+OO FAIL ABUN PA-233 -5.642E-02 7.810E-02 1.381E-01 FAIL ABUN PA-234 -l.635E-01 3.451E-01 5.308E-01 NOT IDENT. PA-234M -5 .196E+OO 5.090E+OO 8.894E+OO NOT IDENT. TH-234 l.896E+OO l.987E+OO 4.038E+OO FAIL ABUN U-235 5.759E-02 2.464E-01 4.461E-01 FAIL ABUN NP-237 -5.642E-02 7. 810E-02 1.381E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 l.896E+OO 1.987E+OO 4.038E+OO FAIL ABUN NP-239 1.878E-01 3.205E-01 5.998E-01 FAIL ABUN PU-239 -2.524E+Ol 4.323E+02 7.636E+02 NOT IDENT. AM-241 -3. 896E-02 2.244E-Ol 4.127E-01 NOT IDENT. CM-243 4.668E-02 1. 316E-01 2.440E-Ol FAIL ABUN BK-247 -7.946E-02 1.143E-01 1.809E-01 NOT IDENT. CM-247 4. 401E-03 5.597E-02 1. 036E-01 FAIL' ABUN CF-249 -4.305E-02 5.805E-02 l.004E-01 NOT IDENT. CF-251 -7.255E-02 l.350E-01 2.527E-01 NOT IDENT. ANH-511 -3.056E-02 6.123E-02 1. 218E-01 NOT IDENT. Page 3479 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:01:38.57 Nuclide Line Activity Report Nuclide Type:

  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 293 10.66* 1. 060E+OO l.410E+Ol l.410E+Ol 12.62 CD-109 88.03 36 3.70* 4.866E+OO 1. 086E+OO l.703E+OO 179.68 SN-126 64.28 ------9.60 2.600E+OO ------Line Not Found ------86.94 36 8.90 4.866E+OO 4.513E-01 4. 513E-01 179.68 87.57 36 37.00* 4.866E+OO 1. 086E-01 1. 086E-01 179.68 BA-137M 661.66 1667 89.90* 2.016E+OO 4.997E+OO 5.092E+OO 5.22 CS-137 661. 66 1667 85.10* 2.016E+00 5.279E+OO 5.379E+OO 5.22 HG-203 70.83 ------3.69 3.355E+OO ------Line Not Found ------72.87 10 6.19 3.544E+OO 2.360E-01 2.043E+Ol 324.14 279.20 31 81.56* 4.164E+OO '4.909E-02 4.248E+OO 175.76 TL-208 277.37 31 6.60 4.164E+OO 6.066E-01 6.066E-01 175.76 583.19 93 85.00* 2.233E+00 2.666E-01 2.666E-01 43.48 860.56 ------12.50 l.634E+OO ------Line Not Found ------BI-211 72.87 10 1. 23 3.544E+OO l.188E+00 1.188E+OO 324.14 351.06 215 12.92* 3.416E+OO 2.648E+OO 2.648E+OO 23.99 PB-212 74.82 '104 10.28 3.779E+OO 1.456E+OO 1.456E+OO 58.65 77 .11 199 17.10 3.992E+00 1.584E+OO 1.584E+OO 28.65 238.63 360 43.60* 4.703E+OO 9.530E-01 9.530E-01 19.57 300.09 29 3.30 3. 911E+OO 1.222E+OO l.222E+OO 130.41 BI-214 609.32 166 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 1120.29 33 14.92 1. 323E+00 9.153E-01 9.156E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 PB-214 74.82 104 5.80 3.779E+OO 2.581E+OO 2.581E+OO 58.65 77 .11 199 9.70 3.992E+00 2.792E+OO 2.793E+00 28.65 87.09 36 3.41 4.866E+00 l.178E+OO l.178E+OO 179.68 242.00 88 7.25 4.647E+OO 1.415E+00 1.416E+OO 59.86 295.22 162 18.42 3.962E+00 1.206E+OO 1.206E+OO 39.65 351. 93 215 35.60* 3.416E+00 9.612E-01 9.615E-01 23.99 RN-222 609.32 166 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 1120.29 33 14.92 1. 323E+OO 9.153E-01 9.156E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 RA-224 240.99 88 4.10* 4.647E+OO 2.502E+OO 2.502E+OO 59.86 RA-226 609.32 166 45.49* 2.154E+OO 9.207E-01 9.210E-01 25.70 1120.29 33 14.92 1. 323E+OO 9.153E-01 9.156E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.293E-01 55.03 AC-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 95 11. 27 3. 531E+OO 1. 301E+OO 1. 301E+OO 51.16 794.95 ------4.25 1. 740E+OO ------Line Not Found ------835. 71 ------1. 61 1. 672E+00 ------Line Not Found ------911. 20 83 25.80* 1. 561E+OO 1.114E+OO 1.114E+OO 28.98 968. 97 33 15.80 l.487E+OO 7.606E-01 7.606E-01 57.36 RA-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 95 11. 27 3. 531E+OO 1. 301E+OO 1.301E+OO 51.16 794.95 ------4.25 1. 740E+OO ------Line Not Found ------835. 71 ------1. 61 1. 672E+OO ------Line Not Found ------911. 20 83 25.80* 1. 561E+OO 1.114E+OO l.114E+00 28.98 968. 97 33 15.80 1.487E+OO 7.606E-01 7.606E-01 57.36 Page 3480 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235025 Acquisition date 3-0CT-2016 09:01:15 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 '74. 82 104 .J.0.28 3.779E+OO 1.456E+OO 1.456E+OO
  • 58.65 77 .11 199 17.10 3.992E+OO 1.584E+OO 1.584E+OO 28.65 238.63 360 43.60* 4.703E+OO 9.530E-01 9.530E-01 19.57 300.09 *29 3.30 3. 911E+OO 1.222E+OO 1.222E+OO 130.41 TH-230 609.32 166 45.49* 2.154E+OO 9.207E-01 9.207E-01 25.70 1120.29 33 14.92 l.323E+OO 9.153E-01 9.153E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.290E-01 55.03 PA-231 283.69 ------1. 70 4.097E+OO ------Line Not Found ------301.36 29 5.35* 3. 911E+OO 7.540E-01 7.540E-01 130. 41 TH-232 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 95 11. 27 3.531E+OO 1. 301E+OO 1.301E+OO 51.16 835. 71 ------1. 61 1.672E+00 ------Line Not Found ------911. 20 83 25.80* 1.561E+OO 1.114E+OO 1.114E+OO 28.98 968. 97 33 15.80 1.487E+00 7.606E-01 7.606E-01 57.36 U-234 609.32 166 45.49* 2.154E+OO 9.207E-01 9.207E-01 25.70 1120.29 33 14.92 1.323E+OO 9.153E-01 9.153E-01 64. 96 1764.49 23 15.30 8.930E-01 9.290E-01 9.290E-01 55.03 AM-243 43.53 ------5.90 2.878E-01 ------Line Not Found ------74.66 104 67.20* 3.779E+OO 2.227E-01 2.227E-01 58.65 Flag: "*" Key line Page 3481of5809 Surrunary of Nuclide Activity Sample ID : G405235025 Acquisition date Page : 3 3-0CT-2016 09:01:15 Total number of lines in spectrum 33 Number of unidentified lines 8 Number of lines tentatively identified by NID 25 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 Hlife l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 46.59D l.41E+10Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 2.45E+05Y 7370.00Y Decay 1. 00 1. 57 1. 00 1. 02 1. 02 86.6 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.410E+Ol 1. 086E+OO 1. 08 6E-01 4.997E+OO 5.279E+OO 4.909E-02 2.666E-01 2.648E+00 9.530E-01 9.207E-01 9.612E-01 9.207E-01 2.502E+OO 9.207E-01 1.114E+OO 1.114E+OO 9.530E-01 9.207E-01 7.540E-01 1.114E+OO 9.207E-01 2.227E-01 4.283E+Ol 4.283E+Ol Decay Corr pCi7GRAM 1.410E+Ol 1. 703E+OO 1. 086E-01 5.092E+OO 5.379E+OO 4.248E+OO 2.666E-01 2.648E+OO 9.530E-01 9.210E-01 9.615E-01 9.210E-01 2.502E+OO 9.210E-01 1.114E+OO 1.114E+OO' 9.530E-01 9.207E-01 7.540E-01 1.114E+00 9.207E-01 2.227E-01 4.784E+Ol 4.784E+Ol 75.76% Decay Corr 2-Sigma Error 0.178E+Ol 3.060E+OO 1.951E-01 0.266E+OO 0.281E+OO 7.467E+OO l.159E-01 0.635E+OO l.865E-01 2.367E-01 2.307E-01 2.367E-01 1. 498E+OO 2.367E-01 0.323E+OO 0.323E+OO 1.865E-01 2.366E-01 9.833E-01 0.323E+OO 2.366E-01 1. 306E-01 "M" Manually accepted 2-Sigma %Error 12.62 179.68 179.68 5.22 5.22 175.76 43.48 23.99 19.57 25.70 23.99 25.70 59.86 25.70 28.98 28.98 19.57 25.70 130.41 28.98 25.70 58.65 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3482 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235025 Acquisition date : 3-0CT-2016 09:01:15 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 92.77 72 290 1. 33 185.00 181 10 1.68E-02 **** 5.21E+OO T 0 185.73 86 206 1. 47 370.75 366 11 2.lOE-02 76.6 5.56E+OO T 0 270.66 76 197 3.44 540.46 531 16 1.93E-02 90.5 4.26E+OO T 0 457.37
  • 42 66 1. 75 913.56 910 9 1. llF.;-02 77.2 2.73E+OO 0 462.66 43 76 2.74 924.15 920 8 1. 14E-02 78.2 2.71E+OO T 0 517. 62 42 69 2.35 1033.97 1029 13 1. llE-02 88.9 2.46E+OO 0 709.24 14 23 5.22 1416.93 1409 15 3.75E-03 **** 1. 91E+OO 0 727.23 37 21 2.30 1452.88 1448 11 1. 02E-02 59.1 1.87E+OO T 0 769.76 17 34 2.83 1537.87 1527 15 4.74E-03 **** 1. 7 9E+OO 0 891.86 11 12 3.64 1781.91 1775 12 3.06E-03 **** 1.59E+OO 0 941. 84 17 19 3.94 1881.79 1874 16 4.64E-03 **** 1.52E+OO 0 965. 23 10 27 0.66 1928.54 1921 12 2.86E-03 **** 1.49E+OO T 0 1228 .. 04 7 22 2.58 2453.83 2443 12 1.90E-03 **** l.23E+OO 0 1258.08 25 22 4.37 2513.88 2501 24 7.03E-03 **** 1.20E+OO Flags: "T" = Tentatively associated Page 3483 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:01:52.92 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l *
  • Acquisition date 3-0CT-2016 09:01:15 Sensitivity 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:38:00 Nuclide Library : SOLID *
  • Sample ID G405235025 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.3824E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;15
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 BA-137M CS-137 HG-203 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 Le (pCi/GRAM 3.012E-01 3.786E-02 4.000E-02 2.905E+OO .3.549E-02 , 6. 521E-02 7.465E-02 8.946E-02 7.465E-02 7. 941E-01 7.465E-02 1.433E-01 1.433E-01 6.521E-02 7.463E-02 5.264E-01 1.433E-01 7.463E-02 6.046E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 3484 of 5809 Le (pCi/GRAM 1.949E+Ol 4.802E-02 O.OOOE+OO 2. 511E-02 3.633E-01 0.000E+OO O.OOOE+OO 6.712E-02 4.642E-01 O.OOOE+OO 4.982E-02 5.814E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 -RE-183 RE-184 Page 3485 of 5809 6.660E+00 4.180E-02 l.683E-01 2.104E+OO l.437E+Ol O.OOOE+OO 2.423E-01 O.OOOE+OO O.OOOE+OO 8.308E-01 8.978E+OO 9.483E-01 O.OOOE+OO 1.520E-01 4.607E+02 3.256E-02 7.606E-01 2.664E+OO 1.421E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.889E-02 5.860E-02 7.810E+OO 5.762E-01 '5.762E-01 3. 813E-02 1.410E+OO 9.403E-02 3.538E-01 O.OOOE+OO O.OOOE+OO 1.592E-01 1.399E+OO l.697E-01 3.345E+02 O.OOOE+OO O.OOOE+OO 9.289E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0-. OOOE+OO 5.149E-02 O.OOOE+OO 5.876E-02 l.823E-01 O.OOOE+OO O.OOOE+OO 1.154E-01 O.OOOE+OO O.OOOE+OO 2.399E+Ol O.OOOE+OO 3.810E-01 5.882E-02 5.109E+OO 6.367E-02 O.OOOE+OO 8.819E+02 O.OOOE+OO 3.320E-02 1.130E-01 2.180E-01 l.186E-01 l.254E-01 2.009E+OO 4.563E-02 3.411E+Ol 2.583E-01 8.060E-02 2.865E-02 6.270E+OO 9.043E-01 4.448E+OO 2. 960E+Ol NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABDN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3486 of 5809 1.388E+02 5.462E-01 4.238E-02 5.988E+OO 4.698E-01 9.107E-01 7.049E-01 5.273E-01 7.501E-01 2.666E-01 2.666E-01 5.548E-01 7.501E-01 6.388E-02 2.246E-01 3.838E+OO 1.935E+OO 2. ll 7E-01 6.388E-02 O.OOOE+OO 1.935E+OO 2.840E-01 3. 621E+02 l.956E-01 l.154E-01 8.460E-02 4.836E-02 4.'657E-02 1.186E-01 5.790E-02 NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:01:58.87 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235025.CNF;l *
  • Acquisition date 3-0CT-2016 09:01:15 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
  • Sample date 8-DEC-2015 13:38:00 Nuclide Library : SOLID *
  • Sample ID G405235025 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.3824E+02 GRAM *
  • Quantity Err(%) : 1.4467E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) K-40 l.410E+Ol 1.892E+OO 1. 892E+OO BA-137M 5.092E+OO 3.404E-01 3.404E-01 CS-137 5.379E+OO 3.592E-01 3.592E-01 HG-203 2.381E+OO 7.365E+OO 7.365E+OO TL-208 2.666E-01 1.142E-01 l.142E-01 PB-212 9.530E-01 l.897E-01 1.897E-01 BI-214 9.210E-01 2.353E-01 2.353E-01 PB-214 9.615E-01 2.296E-01 2. 296E-01 RN-222 9.210E-01 2.353E-01 2.353E-01 RA-224 3.704E-01 1.692E+OO 1.692E+OO RA-226 9.210E-01 2.353E-01 2.353E-01 AC-228 1.114E+OO 3.216E-01 3.216E-01 RA-228 l .114E+OO 3.216E-01 3.216E-01 TH-228 9.530E-01 1. 8 97E-01 1.897E-01 TH-230 9.207E-01 2.352E-01 2.352E-01 PA-231 7.540E-01 9.770E-01 9.770E-01 TH-232 1.114E+OO 3.216E-01 3.216E-01 U-234 9.207E-01 2.352E-01 2.352E-01 AM-243 1.188E-01 1.348E-01 l.348E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-s'igma) (1.96-sigma) BE-7 1.116E+Ol 2.205E+Ol 2.262E+Ol NOT IDENT. NA-22 2.517E-02 5.261E-02 5.382E-02 NOT IDENT. NA-24 -1. OOOE+41 8.612E+40 O.OOOE+OO SHORT HLIF AL-26 -l.146E-02 3.390E-02 3.429E-02 NOT IDENT. SC-46 7.694E-02 4.747E-01 4.760E-01 FAIL ABUN V-48 -6.158E+03 l.590E+04 1.614E+04 SHORT HLIF CR-51 8.994E+Ol 5.855E+02 5.869E+02 SHORT HLIF MN-54 8.808E-03 7.638E-02 7.648E-02 NOT IDENT. C0-56 -2.099E-01 5.714E-01 5.792E-01 NOT IDENT. MN-56 -l.OOOE+41 2.750E+41 O.OOOE+OO SHORT HLIF C0-57 -5.256E-02 6.340E-02 6.769E-02 NOT IDENT. Page 3487 of 5809 C0-58 6.041E-02 6.614E-01 6.619E-01 NOT IDENT. FE-59 l.134E+OO 7.697E+OO 7.714E+OO NOT IDENT. C0-60 2.904E-03 5.003E-02 5.005E-02 NOT IDENT. ZN-65 8.404E-02 2.056E-01 2.091E-01 NOT IDENT. GE-68 -5.071E-01 2.600E+OO 2.610E+OO NOT IDENT. AS-73 2.324E+OO l.604E+Ol l.607E+Ol NOT IDENT. AS-74 -3.375E+03 8.626E+03 8.759E+03 SHORT HLIF SE-75 -2. 396E-01 3.290E-01 3.463E-01 FAIL ABUN BR-77 l.704E+38 l.475E+39 O.OOOE+OO SHORT HLIF SR-82 2.385E+02 8.798E+02 8.864E+02 SHORT HLIF.c RB-83 2.277E-01 l.077E+OO l.081E+OO NOT IDENT. KR-85 -4.606E+Ol 1. 740E+Ol 2.709E+Ol NOT IDENT. SR-85 -4.867E+OO l.838E+OO 2.862E+OO NOT IDENT. RB-86 -8.835E+02 3.100E+04 3.100E+04 SHORT HLIF Y-88 5.231E-02 l.540E-01 l.558E-01 NOT IDENT. Y-91 -3.265E+02 6.189E+02 6.362E+02 NOT IDENT. NB-94 l.383E-02 3.939E-02 3.988E-02 NOT IDENT. NB-95 -5.155E-01 l.065E+OO l.090E+OO NOT IDENT. NB-95M -5.541E-01 3.366E+OO 3.375E+OO NOT IDENT. ZR-95 -4.858E-02 l.638E+OO l.638E+OO NOT IDENT. NB-97 l.000E+41 l.365E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 7.823E+40 O.OOOE+OO SHORT HLIF M0-99 5.166E+31 l.977E+32 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 2.763E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 347E-02 4. 726E-02 4.765E-02 NOT IDENT. RH-102 -5.587E-02 8.012E-02 8.399E-02 NOT IDENT. RU-103 5.291E+OO 8.701E+OO 9.022E+OO FAIL ABUN 'RH-106 3.664E-01 6.439E-01 6.647E-01 NOT IDENT. RU-106 3.664E-01 6.439E-01 6.647E-01 NOT IDENT. AG-108M -1. 789E-02 4.640E-02 4.709E-02 NOT IDENT. CD-109 l.703E+OO 3.002E+OO 3.099E+OO FAIL ABUN AG-llOM 3.027E-02 l.070E-01 l.078E-01 NOT IDENT. SN-ll3 3.862E-01 3.805E-01 4.185E-01 NOT IDENT. CD-ll5 -l.930E+39 4.489E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -l.162E+04 l.285E+05 l.286E+05 SHORT HLIF TE-123M -3.518E-02 1. 753E-01 l.760E-01 NOT IDENT. SB-124 -5.349E-01 l.859E+OO l.874E+OO NOT IDENT. SB-125 l.483E-01 1. 869E-01 l.985E-01 FAIL ABUN TE-125M 8. 963E+Ol 3.866E+02 3.887E+02 NOT IDENT. I-126 7.253E+05 l.169E+06 l.214E+06 SHORT HLIF SB-126 5.661E+05 l.434E+06 l.457E+06 SHORT HLIF SN-126 l.086E-01 l.913E-01 l.974E-01 FAIL ABUN SB-127 -2.502E+21 2.644E+22 O.OOOE+OO SHORT HLIF I-131 -l.906E+08 7.924E+09 7.925E+09 SHORT HLIF I-132 1. 000E+41 1. 906E+42 O.OOOE+OO SHORT HLIF TE-132 -2.869E+26 5.404E+26 O.OOOE+OO SHORT HLIF BA-133 l.067E-03 6.629E-02 6.629E-02 NOT IDENT. I-133 -l.000E+41 2.203E+41 O.OOOE+OO SHORT HLIF CS-134 6.142E-02 5.947E-02 6.560E-02 NOT IDENT. CS-135 l.531E-01 l.952E-01 2.071E-01 NOT IDENT. I-135 -l.000E+41 9.774E+41 0.000E+OO SHORT HLIF CS-136 -4.679E+04 4.086E+05 4.091E+05 SHORT HLIF CE-139 2.862E-02 l.242E-01 l.249E-01 NOT IDENT. BA-140 -2.192E+05 l.987E+06 l.990E+06 SHORT HLIF LA-140 -3.699E+04 5.069E+05 5. 072E+05 SHORT HLIF CE-141 -4.192E+Ol 3.236E+Ol 3.748E+Ol NOT IDENT. CE-143 l.000E+41 l.284E+41 O.OOOE+OO SHORT HLIF CE-144 -2.177E-01 4. 721E-01 4.822E-01 NOT IDENT. PM-144 l.131E-02 6.551E-02 6.571E-02 NOT IDENT. PR-144 9.825E-01 5.690E+OO 5.708E+00 NOT IDENT. PM-146 -3.209E-03 8.445E-02 8.446E-02 NOT IDENT. ND-147 -2.152E+07 4.733E+07 4.832E+07 SHORT HLIF PM-147 3. ll9E+02 l.017E+03 l.027E+03 NOT IDENT. PM-149 2.724E+40 6.307E+40 O.OOOE+OO SHORT HLIF EU-150 l.919E-02 4.047E-02 4.138E-02 FAIL ABUN EU-152 2. 596E-02 l.421E-01 1. 426E-01 FAIL ABUN GD-153 -5.715E-02 2.777E-01 2.789E-01 NOT IDENT. EU-154 6.448E-02 l.296E-01 l.328E-01 NOT IDENT. EU-155 7. 081E-02 l.416E-01 l.452E-01 FAIL ABUN TB-160 l.360E+OO 2. ll5E+OO 2.202E+OO FAIL ABUN H0-166M -l.342E-02 6.223E-02 6.253E-02 FAIL ABUN TM-171 -l.346E+Ol 3.935E+Ol 3.981E+Ol NOT IDENT. HF-172 -2.579E-02 3.085E-01 3.087E-01 NOT IDENT. LU-172 2.066E-02 9.201E-02 9.248E-02 FAIL ABUN LU-176 -9.477E-03 3.348E-02 3.375E-02 FAIL ABUN HF-181 l.524E+00 7.273E+OO 7.305E+OO NOT IDENT. TA-182 -3.884E-01 1. 341E+OO l.353E+OO FAIL ABUN RE-183 -l.506E+00 5.140E+OO 5.185E+OO NOT IDENT. Page 3488 of 5809 RE-184 8.722E+OO 3.304E+Ol 3.327E+Ol NOT IDENT. W-188 9.662E+Ol l.659E+02 l.715E+02 NOT IDENT. IR-192 -3.103E-02 6.270E-01 6.272E-01 FAIL ABUN BI-207 1. 700E-02 4.653E-02 4.715E-02 FAIL ABUN PB-210 1.178E+OO 6.676E+OO 6.698E+OO NOT IDENT. BI-211 2.648E+OO 6.340E-01 1.352E+OO FAIL ABUN PB-211 1.098E+OO 1.114E+OO NOT IDENT. BI-212 1.632E+OO 9.483E-01 l.200E+OO FAIL ABUN RN-219 -1.423E-01 6.270E-01 6.303E-01 FAIL ABUN RA-22.;3 3.427E-01 8.310E-01 8.'153E-01 FAIL ABUN AC-227 3.517E-02 2.973E-01 2.977E-01 FAIL ABUN TH-227 3.517E-02 2.973E-01 2.977E-01 FAIL ABUN TH-229 -3.194E-01 6.315E-01 6.477E-01 FAIL ABUN TH-231 3.427E-01 8.310E-01 8.453E-01 FAIL ABUN PA-233 -5.642E-02 7.815E-02 8.218E-02 FAIL ABUN PA-234 -1.635E-01 3.925E-01 3.994E-01 NOT IDENT. PA-234M -5 .196E+OO 5.095E+OO 5.608E+OO NOT IDENT. TH-234 1. 896E+OO 2. 031E+OO 2.204E+OO FAIL ABUN U-235 5.759E-02 2.464E-01 2.478E-01 *FAIL ABUN NP-237 -5.642E-02 7.815E-02 8.218E-02 FAIL ABUN NP-238 -5.579E+40 5.144E+41 O.OOOE+OO SHORT HLIF U-238 1. 896E+OO 2. 031E+OO 2.204E+OO FAIL ABUN NP-239 1. 878E-01 3.209E-01 3.319E-01 FAIL ABUN PU-239 -2.524E+Ol 4.323E+02 4.325E+02 NOT IDENT. AM-241 -3. 896E-02 2.244E-01 2. 251E-01 NOT IDENT. CM-243 4.668E-02 1. 317E-01 1.333E-01 FAIL ABUN BK-247 -7.946E-02 l.155E-01 1.209E-01 NOT IDENT. CM-247 4.401E-03 5.598E-02 5. 601E-02 FAIL ABUN . CF-249 -4.305E-02 5.816E-02 6 .131E-02 NOT IDENT. CF-251 -7.255E-02 l.353E-01 1.392E-01 NOT IDENT. ANH-511 -3.056E-02 6.124E-02 6.277E-02 NOT IDENT. Page 3489 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 91. 4849 87.09 139.2739 136.47 93.5441 45.60 82.8264 87.57 148.3922 140.51 0.0000 46.54 84.0705 88.03 154.5189 143.76 93.2419 49.72 0.0000 88.34 154.6079 144.24 76.1140 51. 35 94.5186 88.47 132.8742 145.44 118.0415 51. 87 110. 2482 89. 96 124.2040 152.43 107.9469 52.39 112.4799 1093.63 133. 4018 153.25 0.0000 52.97 110.5624 91.11 0.0000 323.87 103.2168 53.44 105.4741 92.59 133.8708 156.02 0.0000 54.07 103.5515 93.35 134. 0527 158.56 0.0000 57.36 0.0000 94.56 92.5958 159.00 116.7635 57.53 107. 6116 94.65 92.6107 162.33 91. 2813 57.98 121. 4591 94.67 92.6138 162.66 0.0000 59.27 114.4208 94.87 92.6461 163.33 99.7768 59.32 114.4344 97.43 114.4188 165.86 76.5332 59.54 115.5547 98.43 99.7156 176.31 83.4392 60. 96 145. 7276 98.44 99.7176 176.60 0.0000 61.17 144.7350 99.53 101.0518 177.52 91.2282 62.93 97.2415 100 .11 120.6917 181.07 0.0000 63. 29 98.3912 102.03 110.7048 181.52 79.6532 63.58 118.7903 103.18 97.0526 184.41 92.8004 64.28 129.6987 103.37 92.4603 143.76 92.9355 66.73 101. 3129 105.21 89.2633 193.51 115.4266 67.24 116. 5331 105.31 89.2780 197.03 114 .1199 125.81 119.8861 106.12 106.8116 198.01 112.4944 67.75 119.9039 106.47 91. 7711 201. 83 106.8195 69.67 131. 6160 109.28 107.3577 203.43 108.7510 70.83 121. 7933 111. 00 119. 3530 205.31 91. 3883 72. 81 128.8554 111.76 0.0000 210.85 119. 3033 72. 87 128.8716 114. 06 89.3576 215.65 103.0092 74.66 129.3515 116.30 0.0000 222 .11 90.2624 74.82 129.3938 116.74 88.5469 227.09 97.8831 74.97 129.4343 119.76 86.5811 227.38 97.9097 77 .11 129.9988 121.12 78.4384 228.16 0.0000 78.74 113.4760 121.22 78.4500 228.18 93.4904 79.69 126.9782 121. 78 105.8769 116.74 93.4904 80.12 118.2194 122.06 107 .1112 235.69 90.9882 80.19 0.0000 122.92 85.7977 235. 96 91. 0117 80.57 109.4493 123.07 85.8170 238.63 103.4934 81. 00 118. 4237 265.00 90.6657 238.98 0.0000 81. 07 118.4399 125.81 101. 7189 240.99 133.7436 81. 75 110.0721 127.23 115.1180 242.00 133.8677 83.79 122.0399 127.91 98.4273 244.70 75.3162 84.00 122.0883 129.30 114.2577 252.40 0.0000 85.43 135.8557 131.20 121. 8023 252.80 81.8441 86.55 139 .1339 133. 02 96.7249 254.15 0.0000 86.79 139 .1963 133. 52 102.8415 256.23 71.0243 86.94 139.2351 136. 00 94.6971 260.90 0.0000 Page 3490 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 89.2012 355.39 0.0000 584.27 27.2334 264.80 89.2129 356.01 61. 3036 595.83 0.0000 265.00 89.2285 364.49 0.0000 427.87 37.7346 268.22 71. 7 661 366.42 0.0000 602.52 0.0000 269.46 71. 8413 372.51 70.5640 604. 72 34.3689 270.03. 71. 87 57 375,.05 76.7422 607.14 39. 569.,2 271.23 71. 9494 377.52 61. 6962 609.32 32.1460 273.65 0.0000 356.01 54.8438 610.33 32.1608 276.40 76.9551 388.16 71. 2946 614.28 31. 0682 277.37 75.1383 388.63 0.0000 618.01 31.1210 277.60 75.1530 391.69 58.1863 620.36 31.1539 278.00 75.1774 264.66 57.4936 621. 93 20.7847 279.20 75.2523 401.81 71. 9198 630.19 0.0000 279.54 71.9802 402.40 64.7509 631.29 31.3077 279.70 71.9896 404.85 73.0859 633.25 18.5690 280.46 81.9218 410.95 61.9983 634.78 0.0000 283.69 67.9775 413.71 71.4202 635.95 32.5345 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 67.1273 423.72 0.0000 645.85 24.5077 285.90 0.0000 427.09 70.9620 657.76 23.9312 287.50 80.5003 427.87 64.7322 657.90 0.0000 290.67 61. 2417 433.94 66.0146 661. 66 27.3208 293.27 0.0000 439.40 68.3312 664.57 0.0000 351. 93. 75.7589 453.88 63. 6096 666.33 0.0000 295. 96 75.8042 463.37 71.9508 666.50 0.0000 879.38 68.7949 468.07 66.2635 667.71 0.0000 299.98 61.6970 473.00 0.0000 677.62 20.4086 300.09 61. 7023 475.06 72. 9611 685.70 0.0000 300.13 61. 7036 476.78 64.4385 695.00 0.0000 301.36 70.3822 477.60 58.0210 696.49 22.3587 302.85 67.5869 482.18 52.7823 696. 51 22.3587 256.23 57.5952 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 21.4717 306.78 68.2742 497.08 38. 0078 697.49 19.6837 308.46 56.8081 505.52 45.8153 702.65 18.6494 311. 90 61.7852 507.63 0.0000 706.68 22.9914 316.51 61.0338 511. 00 59.0762 711. 68 15.8388 319.41 0.0000 514.00 136.4188 720. 70 0.0000 320.08 0.0000 514.00 136.4188 721. 93 0.0000 321.04 80.6832 520.40 36.2791 722. 78 24.5877 323.87 61. 3696 520.69 0.0000 722.91 28.9287 325.23 85.8104 522.65 0.0000 723.31 .28.9336 328.76 0.0000 527.90 0.0000 724 .19 24.6019 333.37 60.0333 528.26 41. 9460 727.33 19.0178 333.97 61.8259 529.59 35.3477 733.00 14.5229 334.37 61.8439 529.87 0.0000 735.93 23.6268 338.28 61.0350 531.02 0.0000 333.97 19.0947 338.32 61.0363 537.26 0.0000 739.50 0.0000 311. 90 61; 1309 546.56 0.0000 747.24 16.4301 340.48 61.1309 552.55 40.2275 748.06 13.6958 340.55 0.0000 563.25 42.6866 752.31 24.6937 344.28 54.8699 569.33 42.8134 753.82 0.0000 345.93 60.5762 946.00 42.8165 756.73 18.3228 351.06 69.5372 569.70 38.3136 756.80 19.2395 351. 93 69.5785 583.19 27.2197 884.68 14.6992 Page 3491of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 19.1229 1274.44 12.9381 1620.50 3.7273 766.42 20.2309 1001.03 17.9407 1621. 92 3.7285 766.84 20.2336 1002.74 15.9561 1678.03 0.0000 772.60 0.0000 1004.73 10.9765 1690.97 3.7814 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 0.9591 778.90 19.4030 1028.54 0.0000 1063.66 9.6021 783.70 0.0000 1037.84 19.1508 1771. 35 1.9208 785.37 17.5980 1038.76 0.0000 1791.20 0.0000 792.07 18.5706 631. 29 12.1274 1808.65 4.8364 794.95 19.5202 1048.07 0.0000 1810.72 0.0000 795.86 13.9476 1049.04 21. 2384 1836.06 0. 9723 810.06 16.8250 1050.41 22.2592 810.29 15.8918 1063.66 8.1260 344.28 15.8929 1077.00 0.0000 810.76 15.8944 1077.34 13.2579 815.77 0.0000 1085.87 11. 2457 1048.07 0.0000 1093.63 13.3206 832.01 18.8440 1099.45 12.3164 834.85 18.8635 1112. 07 15.1071 835.71 23.5863 1112. 84 18.1328 836.80 0.0000 1115. 54 9.8982 846.75 0.0000 1120.29 16.5195 846.77 20.8378 1120.55 1'6.5205 856.80 0.0000 1221. 41 9.9141 860.56 7.6143 1129. 67 10.3516 871.09 18.1500 1131.51 0.0000 873.19 19 .1193 1147.95 0.0000 875.33 0.0000 1173.23 10.4767 879.38 11.4961 1177.95 17.8332 880.51 18.2091 1189.05 12. 62 62 883.24 10.5518 1204.77 16.9063 884.68 10. 9685 1221.41 18.6785 889.28 10.7659 1231. 02 18. 7258 894.76 24.6539 1235.36 0.0000 898.04 9.9166 1238.28 15.9897 900. 72 15.4395 1260.41 0.0000 903.28 12.5557 1271. 87 18.2783 911.20 20.3361 1274.44 8.6074 912.08 24.7977 1274.54 8.6074 923.98 0.0000 1291.59 8.6445 926.50 15.5728 1298.22 0.0000 929 .11 16.5601 1312 .11 0.0000 937.49 15.6289 1332.49 10.9161 944.13 0.0000 1362.66 0.0000 946.00 15.6724 1365.19 4.4011 949.00 16.9948 1368.63 0.0000 667. 71 0.0000 1384.29 6. 6317 962. 31 18.9053 1408.01 11.1151 964. 08 26.7982 1457.56 0.0000 966 .17 0.0000 1460.82 7.2008 911. 20 12.6305 1489.16 4.5293 968.97 12.6305 1505.03 5.4542 983.53 0.0000 1584.12 9.2476 984.45 0.0000 1596.21 0.0000 Page 3492 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:02:27.59 ******************************************************************************** *
  • GEL Laboratories LL"c *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM30.CNF;300 Background date : Z-OCT-2016 11:01:47. Sample date 8-DEC-2015 10:15:00. Acquisition date : 3-0CT-2016 09:01:37. Sample ID G405235026 Sample quantity 1.55202E+02 GRAM Detector name : GAM30 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.46 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 4 4 4 4 5 5 0 0 0 5 5 1 1 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3493 of 5809 Energy 63.60* 74.83 77.11* 84.35* 87.28 89.75 92.88* 140.12* 143.67* 164.59 186.09* 209.99 238.66* 241. 78 269.13 270.63 277.77 290.40 295.09* 300.23 307.04 338.45* 352.13* 412.99 486.39 511. 00* 565.29 583.49* 609.62* 648.41 661.77 723 .15 727.63 764.91 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 33 152 193 31 109 59 91 28 36 20 57 29 378 80 21 42 28 19 146 32 22 91 224 29 19 . 22 12 130 157 19 64 12 65 4 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 153 174 156 183 125 96 120 52 120 126 131 150 83 96 33 42 63 24 65 52 69 49 79 9 32 59 27 33 47 20 20 10 11 15 1. 01 1.19 0.93 1. 47 1.10 1. 07 1. 49 1. 03 1. 75 1. 55 1. 05 1. 30 1. 09 1. 57 1.21 1. 21 1. 21 1. 33 1. 37 1. 82 1. 83 1.16 1. 06 0.92 3.61 2.58 4.36 1. 67 1. 36 3.48 1. 68 1. 37 1. 67 0.56 12 6. 92 149.38 153.94 168.43 174.28 179.22 185.49 279.98 287.07 328.92 371.92 419.73 477.07 483.31 538.00 541.00 555.29 580.56 589.93 600.22 613. 84 676.66 704.02 825.76 972.59 1021.81 1130.42 1166. 83 1219.10 1296.69 1323.42 1446.22 1455.17 1529.75 124 145 145 163 163 163 163 278 278 320 366 414 472 472 535 535 550 578 583 596 596 672 699 823 966 1016 1122 1161 1214 1290 1318 1443 1450 1522 8 9.21E-03 68.8 14 4.23E-02 16.4 1.79E+OO 14 5.35E-02 12.7 28 8.48E-03 77.1 1.85E+OO 28 3.04E-02 19.1 28 1.65E-02 29.5 28 2.53E-02 27.8 16 7.68E-03 42.6 l.77E+00 16 9.91E-03 62.0 11 5. 61E-03111. 0 11 l.58E-02 42.3 13 8.18E-03 89.0 25 1.05E-01 6.6 1.34.E+OO 25 2.21E-02 25.9 13 5.92E-03 44.1 3.06E+OO 13 l.16E-02 31.0 9 7.70E-03 55.1 5 5.15E-03 46.5 13 4.07E-02 14.2 24 8.96E-03 45.8 1.51E+OO 24 6.08E-03 74.9 11 2.54E-02 18.3 11 6.21E-02 10.2 8 7.93E-03 26.7 11 5.29E-03 62.5 13 5.99E-03 89.1 13 3.28E-03 98.1 10 3.61E-02 12.3 13 4.37E-02 12.3 12 5.36E-03 52.3 13 l.76E-02 19.1 7 3.43E-03 53.3 14 l.80E-02 16.4 10 1.llE-03187.9 Peak Search Report (continued) Page : 2 Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 767.85 23 7 1.19 1535.64 1531 9 6.44E-03 29.0 36 0 795.50 19 28 2.00 1590.95 1582 14 5.28E-03 63.4 37 0 860.66 24 19 1. 23 1721.31 171A 13 6.54E-03 43.8 38 0 911. 55 99 35 1. 49 1823.13 1815 14 2.75E-02 16.2 39 0 956.30 22 8 3.97 1912.65 1906 15 5.97E-03 35.2 40 0 966. 07* 5 18 1. 33 1932.21 1926 10 l.48E-03164.5 41 0 969.48* 61 10 1. 64 1939.03 1935 10 1.70E-02 16.4 42 0 1015.29 7 20 3.21 2030.68 2019 16 1.85E-03155.6 43 0 1072. 58 15 7 1. 22 2145.31 2140 10 4.29E-03 41. 3 44 0 1120.76* 39 17 0.87 2241.70 2237 10 1.09E-02 26.1 45 0 1363.20 11 0 0.66 2726.82 2721 11 3.06E-03 30.2 46 0 1373.89 6 2 0.80 2748.20 2745 7 1.68E-03 54.9 47 0 1461.18* 371 0 1. 70 2922.88 2916 14 1. 03E-01 5.2 48 0 1509.43 8 3 3.81 3019.44 3012 11 2.23E-03 53.6 49 . 0 1589.74 10 6 1. 03 3180.15 3172 12 2.78E-03 58.3 50 0 1765.19* 41 0 1. 21 3531.27 3525 13 l.14E-02 16.6 Flag: "*" = Peak area was modified by background subtraction Page 3494 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:02:29 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 8-DEC-2015 10:15:00 G405235026 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:01:37 155.20 GRAM Sample type Detector name : Elapsed live time; Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA30 0 01:00:00.00 1. 50 keV No Empirical 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3495 of 5809 Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------N*uclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:01.46 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status * < K-40 1460.82 10 .. 66* 1.307E+OO 1.245E+Ol 1.245E+Ol 10.48 OK NB-95 765.81 99.81* 2.266E+OO 8.910E-03 2.292E-01 375.83 OK CD-109 88.03 3.70* 6.554E+OO 1. 930E+OO 3.028E+OO 57.12 OK SN-126 64.28 9.60 3.928E+OO 5.635E-01 5.636E-01 137.56 OK 86.94 8.90 6.554E+OO 8.022E-01 8.022E-01 57.12 OK 87.57 37.00* 6.554E+OO l.930E-01 1.930E-01 57.12 OK CS-135 268.22 16.00* 4.925E+OO 1.519E-01 1.519E-01 88.27 OK BA-137M 661.66 89.90* 2.541E+OO 1.423E-01 1. 450E-01 38 .11 OK CS-137 661.66 85.10* 2.541E+OO 1.503E-01 1.532E-01 38 .11 OK CE-139 165.86 80.00* 6.725E+OO 2.208E-02 1.000E-01 221.95 OK HG-203 70.83 3.69 4.957E+OO Line Not Found Absent 72. 87 6.19 5.213E+OO Line Not Found Absent 279.20 81.56* 4.815E+00 1.615E-02 1.400E+OO 271.55 OK TL-208 277.37 6.60 4.820E+OO Line Not Found <<INT Reject 583.19 85.00* 2.799E+OO 2.834E-01 2.834E-01 24.60 OK 860.56 12.50 2.058E+OO 4.553E-01 4.553E-01 87.56 OK PB-212 74.82 10.28 5.442E+OO 1.179E+OO 1.179E+OO 49.56 OK 77 .11 17.10 5. 691E+OO 1. 248E+00 1. 248E+OO 25.50 OK 238 .'63 43.60* 5.357E+OO 9.204E-01 9.204E-01 13.13 OK 300.09 3.30 4.554E+OO 1.192E+00 1.192E+OO 91. 66 OK BI-214 609.32 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 OK 1120.29 14.92 1.645E+OO 7. 714E-01 7.717E-01 52.15 OK 1764.49 15.30 1.121E+OO 1.092E+OO 1.093E+OO 33.24 OK PB-214 74.82 5.80 5.442E+OO Line Not Found <<INT Reject 77 .11 9.70 5.691E+00 2.200E+OO 2.201E+OO 25.50 OK 87.09 3.41 6.542E+OO Line Not Found <<INT Reject 242.00 7.25 5.305E+OO Line Not Found <<INT Reject 295.22 18.42 4. 611E+OO 9.588E-01 9. 591E-01 28.38 OK 351. 93 35.60* 4.059E+00 8.465E-01 8.468E-01 20.43 OK -RN-222 609.32 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 OK 1120.29 14.92 1.645E+OO 7. 714E-01 7.717E-01 52.15 OK 1764.49 -15.30 1.121E+OO 1.092E+OO 1.093E+OO 33.24 OK RA-224 240.99 4.10* 5.309E+00 3.817E-01 3.817E-01 308.85 OK RA-226 609.32 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 OK 1120.29 14.92 1.645E+OO 7.714E-01 7.717E-01 52.15 OK 1764.49 15.30 1.121E+OO 1.092E+OO 1.093E+OO 33.24 OK AC-228 105.21 1.10 7.278E+00 .. -----Line Not Found Absent 338.32 11.27 4.177E+OO 1. 064E+OO 1.064E+OO 36.57 OK 794.95 4.25 2 .196E+OO 1. 021E+OO 1.021E+OO 126.75 OK 835.71 1. 61 2.109E+OO Line Not Found Absent 911. 20 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 OK 968.97 15.80 1. 863E+00 1.019E+OO 1.019E+OO 32.73 OK RA-228 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 1.064E+OO 1.064E+OO 36.57 OK 794.95 4.25 2.196E+OO 1.021E+OO 1. 021E+OO 126.75 OK 835.71 1. 61 2.109E+OO Line Not Found Absent 911. 20 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 OK 968.97 15.80 1. 863E+OO 1.019E+OO 1.019E+OO 32.73 OK TH-228 74.82 10.28 5.442E+OO 1.179E+OO 1.179E+OO 49.56 OK Page 3496 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77 .11 1.7 .10 5.691E+OO 1.248E+OO l.248E+OO 25 .. 50 OK 238.63 43.60* 5.357E+OO 9.204E-01 9.204E-01 13.13 OK 300.09 3.30 4.554E+OO 1.192E+OO 1.192E+OO 91. 66 OK TH-229 85.43 14.70 6.345E+OO 2.049E-01 2.049E-01 154.20 OK 88.47 24.00 6.554E+OO 2.975E-01 2.975E-01 57.12 OK 193.51 4.41* 6.145E+OO Line Not Found Absent 210.85 2.80 5.837E+OO l.036E+OO l.036E+OO 177.94 OK TH-230 609.32 45.49* 2.707E+OO 6.600E-01 6.600E-01 24.57 OK 1120.29 14.92 1.645E+OO 7. 714E-01 7.714E-01 52.15 OK 1764.49 15.30 1.121E+OO 1.092E+OO 1.092E+OO 33.24 OK PA-231 283.69 1. 70 4.743E+OO Line Not Found Absent 301.36 5.35* 4.554E+OO 7.353E-01 7.353E-01 91.66 OK TH-232 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11.27 4.177E+OO 1.064E+OO 1.064E+OO 36.57 OK 835. 71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 OK 968. 97 15.80 1. 863E+OO 1.019E+OO 1.019E+OO 32.73 OK TH-234 63.29 3.70* 3.928E+OO 1.462E+OO 1.462E+OO 137.56 OK 92.59 4.23 6.875E+OO I.939E+OO 1.939E+OO 55.61 OK U-234 609.32 45.49* 2.707E+OO 6.600E-01 6.600E-01 24.57 OK 1120.29 14.92 1.645E+OO 7. 714E-01 7.714E-01 52.15 OK 1764.49 15.30 1.121E+OO 1.092E+OO 1.092E+OO 33.24 OK U-235 89.96 3.47 6.708E+OO 1.584E+OO 1.584E+OO 58.92 OK 93.35 5.60 6.875E+OO l.465E+OO 1. 465E+OO 55.61 OK 143.76 10. 96* 7.122E+OO 2.726E-01 2.726E-01 123.99 OK 163.33 5.08 6.725E+OO 3.477E-01 3.477E-01 221.95 OK 185.72 57.20 6.291E+OO 9.212E-02 9.212E-02 84.53 OK 205.31 5.01 5.922E+OO Line Not Found Absent U-238 63.29 3.70* 3.928E+OO 1.462E+OO 1.462E+OO 137.56 OK 92.59 4.23 6.875E+OO 1.939E+OO l.939E+OO 55.61 OK AM-243 43.53 5.90 8.765E-01 Line Not Found Absent 74.66 67.20* 5.442E+OO l.804E-01 l.804E-01 49.56 OK ANH-511 511. 00 100.00* 3. 091E+OO 3.668E-02 3.668E-02 178.21 OK Flag: "*" = Keyline Page 3497 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:02:30.67 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l *
  • Acquisition date 3-0CT-2016 09:01:37 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.46 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:15:00 Analyst initials: MXRl *
  • Sample ID G405235026 Sample Quantity 1.5520E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 11-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.245E+Ol 1.278E+OO NB-95 2.292E-01 8.440E-01 CD-109 3.028E+00 1.695E+OO SN-126 1.930E-01 1.080E-01 CS-135 1.519E-01 1.314E-01 BA-137M l.450E-01 5.415E-02 CS-137 1.532E-01 5. 720E-02 CE-139 1.000E-01 2.175E-01 HG-203 1.400E+OO 3. 727E+OO TL-208 2.834E-01 6.830E-02 PB-212 9.204E-01 1.185E-01 BI-214 6.602E-01 1.590E-01 PB-214 8.468E-01 1.695E-01 RN-222 6.602E-01 1.590E-01 RA-224 3.817E-01 1.155E+OO RA-226 6.602E-01 1.590E-01 AC-228 9.663E-01 3.064E-01 RA-228 9.663E-01 3.064E-01 TH-228 9.204E-01 1.185E-01 TH-229 -2.684E-01 4.158E-01 TH-230 6.600E-01 1. 589E-01 PA-231 7.353E-01 6.605E-01 TH-232 9.663E-01 3.064E-01 TH-234 1.462E+OO 1. 971E+OO U-234 6.600E-01 1. 589E-01 U-235 2.726E-01 3.313E-01 U-238 1.462E+OO 1.971E+OO AM-243 1.804E-01 8.762E-02 ANH-511 3.668E-02 6.406E-02 Non-Identified Nuclides Nuclide BE-7 Page 3498 of 5809 Key-Line Activity (pCi/GRAM -4.614E+OO K.L. Cnt Uncert ( 1. 96-sigma) 8.882E+00 MDA (pCi/GRAM 3.163E-01 1.532E-01 1.577E+00 1.009E-01 2.124E-01 4.720E-02 4.986E-02 1.662E-01 4.277E+OO 5.062E-02 8.444E-02 9.413E-02 1.073E-01 9.413E-02 9.046E-01 9.413E-02 1. 963E-01 1. 963E-01 8.444E-02 7.241E-01 9.409E-02 5.885E-01 1. 963E-01 1.588E+OO 9.409E-02 2.892E-01 1.588E+OO 6.903E-02 4.362E-02 MDA (pCi/GRAM 1.663E+Ol NOT IDENT.

NA-22 1. 327E-02 3.109E-02 7.054E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF AL-26 l.336E-02 2.580E-02 6.224E-02 NOT IDENT. SC-46 8.247E-02 2.832E-01 5.857E-Ol FAIL ABUN V-48 O.OOOE+OO 1.349E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.244E+02 O.OOOE+OO SHORT HLIF MN-54 4. 931E-03 4.362E-02 8.809E-02 NOT IDENT. C0-56 6.270E-02 3.105E-01 6.442E-01 NOT IDENT. MN-56 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-.57 9.927E-03 3.585E-02 1.029E-02 NOT IDENT. C0-58 2. 969E-01 4.248E-01 9.347E-01 NOT IDENT. FE-59 -1.656E-01 5.760E+OO 1. 096E+Ol NOT IDENT. C0-60 -2.654E-02 2.919E-02 4.943E-02 NOT IDENT. ZN-65 -1.207E-01 1.907E-01 2. 716E-01 NOT IDENT. GE-68 l.598E-01 1.561E+OO 3.032E+OO NOT IDENT. AS-73 l.152E+OO 5.597E+OO l.145E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.379E+03 O.OOOE+OO SHORT HLIF SE-75 -1.264E-01 l.845E-01 3 .115E-01 NOT IDENT. BR-77 O.OOOE+OO 2.207E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.523E+02 O.OOOE+OO SHORT HLIF RB-83 -3.046E-01 5.354E-01 9.842E-01 NOT IDENT. KR-85 1.452E+OO 6.449E+OO 1.169E+Ol NOT IDENT. SR-85 l.519E-01 6.820E-01 1.236E+OO NOT IDENT. RB-86 O.OOOE+OO l.887E+04 O.OOOE+OO SHORT HLIF Y-88 -4.737E-02 1. 700E-01 3.548E-01 NOT IDENT. Y-91 3.774E+Ol 4.010E+02 7.854E+02 NOT IDENT. NB-94 1.287E-02 2.468E-02 5 .133E-02 NOT IDENT. NB-95M -1.045E+OO 2.239E+OO 3.605E+OO NOT IDENT. ZR-95 -7.945E-01 1.065E+OO 1.829E+OO FAIL ABUN NB-97 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.434E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 1.054E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 8.347E+40 O.OOOE+OO SHORT HLIF RH-101 -2.137E-02 2.686E-02 4.761E-02 NOT IDENT. RH-102 3.756E-02 4.175E-02 9.383E-02 FAIL ABUN RU-103 -2.637E+OO 3.888E+OO 7.093E+OO FAIL ABUN RH-106 3.137E-01 3. 596E-01 8.013E-01 NOT IDENT. RU-106 3.137E-01 3. 596E-01 8.013E-01 NOT IDENT. AG-108M 5.223E-04 1.928E-02 3.910E-02 FAIL ABUN AG-110M -2.162E-02 7.255E-02 1.353E-01 FAIL ABUN SN-113 -7.688E-02 1. 636E-01 3.126E-01 NOT IDENT. CD-115 0.000E+OO 2.473E+39 O.OOOE+OO SHORT HLIF SN-117M 0.000E+OO 8.694E+04 O.OOOE+OO SHORT HLIF TE-123M -5.563E-02 l.164E-01 1. 911E-01 NOT IDENT. SB-124 -5.007E-01 1.075E+OO 2 .113E+OO FAIL ABUN SB-125 -3.335E-03 7.016E-02 l.414E-01 NOT IDENT. TE-125M 1.695E+02 2.106E+02 4.239E+02 NOT IDENT. I-126 O.OOOE+OO 7.471E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.062E+06 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 1.328E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.850E+09 0.000E+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.058E+26 O.OOOE+OO SHORT HLIF BA-133 -1.023E-02 3.653E-02 6.349E-02 FAIL ABUN I-133 O.OOOE+OO 1.294E+41 O.OOOE+OO SHORT HLIF CS-134 6.688E-02 8.308E-02 9.467E-02 FAIL ABUN I-135 0.000E+OO 1.057E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 2.083E+05 O.OOOE+OO SHORT HLIF BA-140 O.OOOE+OO 9.168E+05 O.OOOE+OO SHORT HLIF LA-140 0.000E+OO 2.511E+05 O.OOOE+OO SHORT HLIF CE-141 1. 2 69E+OO 2 .115E+Ol 3.988E+Ol NOT IDENT. CE-143 O.OOOE+OO 7.451E+40 O.OOOE+OO SHORT HLIF CE-144 -2.300E-01 2.824E-01 4.997E-01 NOT IDENT. PM-144 -2.303E-02 4.145E-02 7.676E-02 NOT IDENT. PR-144 -2.013E+OO 3.599E+OO 6.661E+OO NOT IDENT. PM-146 6. 8'08E-03 3.245E-02 6.656E-02 NOT IDENT. ND-147 O.OOOE+OO 2.604E+07 O.OOOE+OO SHORT HLIF PM-147 -5.319E+02 6.518E+02 l.157E+03 NOT IDENT. PM-149 O.OOOE+OO 4. 001E+40 O.OOOE+OO SHORT HLIF EU-150 1. 286E-02 1. 963E-02 3. 896E-02 FAIL ABUN EU-152 -9.259E-02 6.418E-02 1. 086E-01 NOT IDENT. GD-153 -2. 272E-01 l.255E-01 2.007E-01 NOT IDENT. EU-154 3.051E-02 7.569E-02 l.714E-01 FAIL ABUN EU-155 8.181E-02 7.943E-02 1.657E-01 FAIL ABUN TB-160 l.600E-01 l.668E+OO 3.253E+O'O FAIL ABUN H0-166M -2.302E-02 4.155E-02 7.466E-02 NOT IDENT. TM-171 -6.472E+OO 1.393E+Ol 2.693E+Ol NOT IDENT. HF-172 -8.490E-03 l.795E-01 3.407E-Ol FAIL ABUN Page 3499 of 5809 LU-172 1. 469E-03 7.094E-02 1.347E-01 FAIL ABUN LU-176 2. 8 91E-02 4.244E-02 4.162E-02 FAIL ABUN HF-181 1. 970E+OO 3.380E+OO 6.703E+OO NOT IDENT. TA-182 -4.880E-01 6.779E-01 1.222E+OO FAIL ABUN RE-183 -8.280E-01 2.007E+OO 3.871E+OO NOT IDENT. RE-184 -1.644E+Ol 2.388E+Ol 4.063E+Ol NOT IDENT. W-188 1.085E+02 9.881E+Ol 1. 811E+02 FAIL ABUN IR-192 -8.973E-02 3.174E-01 6.287E-01 FAIL ABUN BI-207 -4.942E-03 3.758E-02 7.097E-02 FAIL ABUN PB-210 8.066E-01 1.978E+OO 4. l33E+OO NOT IDENT. BI-211 O.OOOE+OO 4.669E-01 6.745E-01 FAIL ABUN PB-211 2.926E-02 4.865E-01 9.838E-01 NOT IDENT. BI-212 O.OOOE+OO 6.702E-01 1.233E+OO FAIL ABUN RN-219 6.479E-02 2.920E-01 5.973E-01 FAIL ABUN RA-223 -5.056E-02 4.lOlE-01 8.231E-01 FAIL ABUN AC-227 9.580E-03 2.097E-01 3.847E-01 FAIL ABUN TH-227 9.580E-03 2.097E-01 3.847E-01 FAIL ABUN TH-231 -5.056E-02 4. lOlE-01 8.231E-01 FAIL ABUN PA-233 -2.204E-02 4.683E-02 8.043E-02 FAIL ABUN PA-234 -1. 747E-01 2.018E-01 3.248E-01 NOT IDENT. PA-234M 1.140E+OO 2.777E+OO 5.945E+OO FAIL ABUN NP-237 -2.204E-02 4.683E-02 8.043E-02 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 l.059E-01 1.852E-01 3.714E-01 FAIL ABUN PU-239 -8. 761E+OO 2.558E+02 4.846E+02 FAIL ABUN AM-241 2.073E-02 9.276E-02 1. 876E-01 NOT IDENT. CM-243 -2.230E-02 7.324E-02 1.378E-01 FAIL ABUN BK-247 -3. 012E-02. 6.189E-02 1. 072E-01 FAIL ABUN CM-247 4. 372E-03 2.660E-02 5.413E-02 FAIL ABUN CF-249 2.169E-02 2.702E-02 5.900E-02 NOT IDENT. CF-251 -7.413E-02 9. 965E-02 1.731E-01 NOT IDENT. Page 3500 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:02:28.38 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 359 10.66* 1.307E+OO 1.245E+Ol 1.245E+Ol 10.48 NB-95 765.81 4 99.81* 2.266E+OO 8.910E-03 2.292E-01 375.83 CD-109 88.03 141 3.70* 6.554E+OO 2.813E+OO 4.415E+OO 38.15 SN-126 64.28 44 9.60 3.928E+OO 5.635E-01 5.636E-01 137.56 86.94 141 8.90 6.554E+OO 1.170E+OO 1.170E+OO 38.15 87.57 141 37.00* 6.554E+OO 2.813E-01 2.813E-01 38.15 CS-135 268.22 25 16.00* 4.925E+OO l.519E-01 l.519E-01 88.27 BA-137M 661. 66 67 89.90* 2. 541E+OO l.423E-01 l.450E-01 38 .11 CS-137 661. 66 67 85.10* 2. 541E+OO 1.503E-01 1.532E-01 38 .11 CE-139 165.86 25 80.00* 6.725E+OO 2.208E-02 1.000E-01 221. 95 HG-203 70.83 ------3.69 4.957E+OO ------Line Not Found ------72. 87 ------6.19 5.213E+OO ------Line Not Found ------279.20 32 81. 56* 4.815E+OO 3.949E-02 3.425E+OO 110 .14 TL-208 277.37 32 6.60 4.815E+OO 4.880E-01 4.880E-01 110 .14 583.19 139 85.00* 2.799E+OO 2.834E-01 2.834E-01 24.60 860.56 24 12.50 2.058E+OO 4.553E-01 4.553E-01 87.56 BI-211 72. 87 ------1. 23 5.213E+OO ------Line Not Found ------351. 06 253 12.92* 4.059E+OO 2.332E+OO 2.332E+OO 20.43 PB-212 74.82 199 10.28 5.442E+OO 1. 720E+OO 1.720E+OO 32.78 77 .11 251 17 .10 5.691E+OO 1.248E+OO l.248E+OO 25.50 238.63 444 43.60* 5.357E+OO 9.204E-01 9.204E-01 13 .13 300.09 37 3.30 4.554E+OO 1.192E+OO l.192E+OO 91. 66 BI-214 609.32 168 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 1120.29 39 14.92 1.645E+OO 7.714E-01 7.717E-01 52.15 1764.49 39 15.30 1.121E+OO 1.092E+OO 1.093E+OO '33.24 PB-214 74.82 199 5.80 5.442E+OO 3.049E+OO 3.050E+OO 32.78 77 .11 251 9.70 5.691E+OO 2.200E+OO 2.201E+OO 25.50 87.09 141 3.41 6.554E+OO 3.052E+OO 3.054E+OO 38.15 242.00 93 7.25 5.309E+OO 1.175E+OO 1.175E+OO 51. 81 295.22 168 18.42 4. 611E+OO 9.588E-01 9.591E-01 28.38 351.93 253 35.60* 4.059E+OO 8.465E-01 8.468E-01 20.43 RN-222 609.32 168 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 1120.29 39 14. 92 1.645E+OO 7.714E-Ol 7.717E-01 52.15 1764.49 39 15.30 1.121E+OO 1.092E+OO 1.093E+OO 33.24 RA-224 240.99 93 4.10* 5.309E+OO 2.077E+OO 2.077E+OO 51. 81 RA-226 609.32 168 45.49* 2.707E+OO 6.600E-01 6.602E-01 24.57 1120.29 39 14.92 1.645E+OO 7. 714E-01 7.717E-01 52.15 1764.49 39 15.30 1.121E+OO 1.092E+OO 1.093E+OO 33.24 AC-228 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 104 11. 27 4.177E+OO 1.064E+OO 1.064E+OO 36.57 794.95 20 4.25 2 .196E+OO 1.021E+OO 1.021E+OO 126.75 835. 71 ------1. 61 2.109E+OO ------Line Not Found ------911. 20 101 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 968.97 62 15.80 1.863E+OO 1.019E+OO 1.019E+OO 32.73 RA-228 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 104 11. 27 4.177E+OO 1.064E+OO l.064E+OO 36.57 794.95 20 4.25 2 .196E+OO 1. 021E+OO 1.021E+OO 126.75 Page 3501of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235026 Acquisition date 3-0CT-2016 09:01:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 835.71 ------1.61 2.109E+OO ------Line Not Found ---""--911.20 101 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 968.97 62 15.80 l.863E+OO l.019E+OO 1.019E+OO 32.73 TH-228 74.82 199 10.28 5.442E+OO 1. 720E+OO 1. 720E+OO 32.78 77 .11 251 17.10 5.691E+OO 1.248E+OO l.248E+OO 25.50 238.63 444 43.60* 5.357E+OO 9.204E-01 9.204E-01 13 .13 300.09 37 3.30 4.554E+OO 1.192E+OO 1.192E+OO 91. 66 TH-229 85.43 40 14.70 6.345E+OO 2.049E-01 2.049E-01 154.20 88.47 141 24.00 6.554E+00 4.337E-01 4.337E-01 38.15 193.51 ------4.41* 6.145E+OO ------Line Not Found ------210.85 35 2.80 5.837E+OO 1.036E+OO l.036E+OO 177.94 TH-230 609.32 168 45.49* 2.707E+OO 6.600E-01 6.600E-01 24.57 1120.29 39 14.92 1. 645E+OO 7. 714E-01 7. 714E-01 52.15 1764.49 39 15.30 l .121E+OO 1.092E+OO 1.092E+OO 33.24 PA-231 283.69 ------1. 70 4.743E+OO ------Line Not Found ------301.36 37 5.35* 4.554E+OO 7.353E-01 7.353E-01 91. 66 TH-232 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 104 11. 27 4.177E+OO 1. 064E+OO l.064E+00 36.57 835.71 ------1. 61 2.109E+00 ------Line Not Found ------911. 20 101 25.80* 1. 962E+OO 9.663E-01 9.663E-01 32.35 968.97 62 15.80 1. 8 63E+OO 1.019E+OO 1.019E+OO 32.73 TH-234 63.29 44 3.70* 3.928E+OO l.462E+00 1.462E+OO 137.56 92.59 117 4.23 6.875E+OO 1.939E+OO 1.939E+OO 55.61 U-234 609.32 168 45.49* 2.707E+OO 6.600E-01 6.600E-01 24.57 1120.29 39 14.92 1.645E+OO 7. 714E-01 7. 714E-01 52.15 1764.49 39 15.30 l.121E+OO 1.092E+OO 1.092E+OO 33.24 U-235 89. 96 76 3.47 6.708E+OO 1.584E+OO 1.584E+OO 58.92 93.35 117 5.60 6.875E+00 1.465E+OO l.465E+00 55.61 143.76 44 10. 96* 7.122E+OO 2.726E-01 2.726E-01 123.99 163.33 25 5.08 6. 725E+00 3.477E-01 3.477E-01 221. 95 185.72 69 57.20 6.291E+00 9.212E-02 9.212E-02 84.53 205.31 ------5.01 5.922E+OO ------Line Not Found ------U-238 63.29 44 3.70* 3.928E+OO 1.462E+OO 1. 4 62E+OO 137.56 92.59 117 4.23 6.875E+OO 1.939E+OO 1.939E+OO 55.61 AM-243 43.53 ------5.90 8.765E-01 ------Line Not Found ------74.66 199 67.20* 5.442E+OO 2. 631E-01 2.632E-01 32.78 ANH-511 511. 00 23 100.00* 3.091E+OO 3.668E-02 3.668E-02 178. 21 Flag: "*" Key line Page 3502 of 5809 Summary of Nuclide Activity Sample ID : G405235026 Acquisition date Page : 3 3-0CT-2016 09:01:37 Total number of lines in spectrum 50 Number of unidentified lines 8 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 NB-95 CD-109 SN-126 CS-135 BA-137M CS-137 CE-139 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 64.03D 461.40D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y 137.64D 46.59D l.41E+l0Y 7.04E+08Y 1.41E+lOY 1600. OOY 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y 1. 41E+l0Y 1. 41E+10Y 1. 41E+lOY 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+lOY 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1. OOE+09Y Decay 1. 00 25.7 1. 57 1. 00 1. 00 1. 02 1. 02 4.53 86.7 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.245E+Ol 8.910E-03 2.813E+OO 2.813E-01 1.519E-01 l.423E-01 1.503E-01 2.208E-02 3.949E-02 2.834E-01 2.332E+00 9.204E-01 6.600E-01 8.465E-01 6.600E-01 2.077E+OO 6.600E-01 9.663E-01 9.663E-01 9.204E-01 4.337E-01 6.600E-01 7.353E-01 9.663E-01 1.462E+OO 6.600E-01 2. 726E-01 1.462E+OO 2.631E-01 3.668E-02 3.430E+Ol 3.430E+Ol Decay Corr pCi/GRAM l.245E+Ol 2.292E-01 4.415E+OO 2. 813E-01 1.519E-01 1.450E-01 l.532E-01 l.OOOE-01 3.425E+OO 2.834E-01 2.332E+OO 9.204E-01 6.602E-01 8.468E-01 6.602E-01 2.077E+OO 6.602E-01 9.663E-01 9.663E-01 9.204E-01 4.337E-01 6.600E-01 7.353E-01 9.663E-01 l.462E+OO 6.600E-01 2.726E-01 1.462E+OO 2.632E-01 3.668E-02 3.959E+Ol 3.959E+Ol 84.00%

  • Decay Corr 2-Sigma Error 0 .130E+Ol 8.613E-01 1. 684E+OO l.073E-01 1. 341E-01 0.553E-01 0.584E-01 2.220E-01 3.772E+OO 0.697E-01 0.476E+OO 1.209E-01 1.622E-01 1.730E-01 1.622E-01 1. 07 6E+OO 1.622E-01 3.127E-01 3.127E-01 1.209E-01 l.655E-01 l.622E-01 6.740E-01 3.127E-01 2. OllE+OO l.622E-01 3.380E-01 2. OllE+OO 0.863E-01 6.537E-02 "M" Manually accepted 2-Sigma %Error 10.48 375.83 38.15 38.15 88.27 38 .11 38 .11 221.95 110 .14 24.60 20.43 13 .13 24.57 20.43 24.57 51. 81 24.57 32.35 32.35 13.13 38.15 24.57 91. 66 32.35 137.56 24.57 123.99 137.56 32.78 178.21 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3503 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235026 Acquisition date : 3-0CT-2016 09:01:37 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 140.12 34 65 1. 03 279.98 278 16 7.68E-03 85.2 7.18E+OO T 1 270.63 48 49 1. 21 541.00 535 13 1.16E-02 62.1 4.91E+OO T 0 290.40 21 28 1. 33 580.56 578 5 5.15E-03 92.9 4.66E+OO T 4 307.04
  • 25 79 1. 83 613.84 596 24 6.08E-03, **** 4.48E+OO T 0 412.99 32 10 0.92 825.76 823 8 7.93E-03 53.3 3.61E+OO T 0 486.39 21 35 3.61 972. 59 966 11 5.29E-03 **** 3.21E+OO T 0 565.29 13 29 4.36 1130. 42 1122 13 3.28E-03 **** 2.87E+OO 0 648.41 20 21 3.48 1296.69 1290 12 5.36E-03 **** 2.58E+OO 0 723.15 13 10 1. 37 1446.22 1443 7 3.43E-03 **** 2.37E+OO T 0 727.63 68 12 1. 67 1455.17 1450 14 1.80E-02 32.8 2.36E+OO T 0 767.85 24 7 1.19 1535.64 1531 9 6.44E-03 58.0 2.26E+OO T 0 956.30 22 8 3.97 1912.65 1906 15 5.97E-03 70.3 1. 88E+OO 0 966.07 5 18 1. 33 1932.21 1926 10 1.48E-03 **** 1.87E+OO T 0 1015.29 7 21 3.21 2030.68 2019 16 1.85E-03 **** 1.79E+OO 0 1072. 58 16 7 1. 22 2145.31 2140 10 4.29E-03 82.6 1. 71E+OO 0 1363.20 11 0 0.66 2726.82 2721 11 3.06E-03 60.3 1.39E+OO T 0 1373.89 6 2 0.80 2748.20 2745 7 1.68E-03 **** 1.38E+OO 0 1509.43 8 3 3.81 3019.44 3012 11 2.23E-03 **** 1.27E+OO 0 1589.74 10 6 1. 03 3180.15 3172 12 2.78E-03 **** 1. 22E+OO Flags: "T" = Tentatively associated Page 3504 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:02:42.32 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l *
  • Acquisition date 3-0CT-2016 09:01:37 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.46 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:15:00 Nuclide Library : SOLID *
  • Sample ID G405235026 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.5520E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 NB-95 CD-109 SN-126 CS-135 BA-137M CS-137 CE-139 HG-203 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.108E-01 O.OOOE+OO 7.432E-01 4.756E-02 9.751E-02 2.060E-02 2.176E-02 7. 722E-02 1.987E+00 2.248E-02 3.927E-02 4.159E-02 4.891E-02 4.159E-02 4.208E-01 4.159E-02 8.499E-02 8.499E-02 3.927E-02 3.365E-01 4.158E-02 2.660E-01 8.499E-02 7.444E-01 4.158E-02 1.357E-01 7.444E-01 3.258E-02 1. 962E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3505 of 5809 Le* (pCi/GRAM 7.320E+OO NOT IDENT. 2.967E-02 NOT IDENT.

NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57

  • C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3506 of 5809 O.OOOE+OO 2.515E-02 2.530E-01 O.OOOE+OO O.OOOE+OO 3.787E-02 2.747E-01 O.OOOE+OO 3.276E-02 4.088E-01 4. 727E+OO 1.951E-02 1.172E-01 1.255E+OO 5.324E+OO O.OOOE+OO l.425E-01 0.000E+OO O.OOOE+OO 4. 371E-01 5. 311E+OO 5.615E-01 O.OOOE+OO l.348E-01 3. 351E+02 2.289E-02 1.670E+OO 7. 7'56E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.214E-02 4.160E-02 3.075E+OO 3.562E-01 3.562E-01 1. 739E-02 5. 716E-02 l.393E-01 O.OOOE+OO O.OOOE+OO 8.863E-02 6.794E-01 6.271E-02 1.987E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.886E-02 O.OOOE+OO 4.264E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 1. 872E+Ol O.OOOE+OO 2.319E-01 3.348E-02 2.904E+OO 2.985E-02 O.OOOE+OO 5.373E+02 O.OOOE+OO 1.777E-02 4.778E-02 9.219E-02 7.196E-02 7.769E-02 1.432E+00 3.216E-02 l.250E+Ol l.590E-01 5.883E-02 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3507 of 5809 1.918E-02 2.999E+OO 5.123E-01 1. 802E+OO 1. 716E+Ol 8.333E+Ol 2.828E-Ol 3.022E-02 1.928E+OO 3. 244E-01. 4.428E-01 5.742E-01 2.707E-01 3.718E-Ol 1.781E-01 1. 781E-01 3.718E-01 3.620E-02 1.332E-01 2.535E+OO 3.620E-02 O.OOOE+OO 1. 738E-01 2.272E+02 8.774E-02 6.415E-02 4.899E-02 2.450E-02 2.676E-02 8.032E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:02:47.56 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235026.CNF;l * *Acquisition date 3-0CT-2016 09:01:37 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.46 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:15:00 Nuclide Library : SOLID *
  • Sample ID G405235026 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.5520E+02 GRAM *
  • Quantity Err(%) : 1.2886E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.245E+Ol l.693E+OO NB-95 2.292E-01 8.443E-01 CD-109 3.028E+OO 1. 733E+00 SN-126 l.930E-01 1.099E-01 CS-135 1.519E-01 1.322E-01 BA-137M l.450E-01 5.533E-02 CS-137 l.532E-01 5.845E-02 CE-139 1.000E-01 2.185E-01 HG-203 l.397E+OO 3.740E+OO TL-208 2.834E-01 7.214E-02 PB-212 9.204E-01 1.404E-01 BI-214 6.602E-01 l.678E-01 PB-214 8.468E-01 1.834E-01 RN-222 6.602E-01 l.678E-01 RA-224 3.817E-01 1.172E+OO RA-226 6.602E-01 1.678E-01 AC-228 9.663E-01 3.348E-01 RA-228 9.663E-01 3.348E-01 TH-228 9.204E-01 1.404E-01 TH-229 -2.684E-01 4.162E-01 TH-230 6.600E-01 1.677E-01 PA-231 7.353E-01 6.809E-01 TH-232 9.663E-01 3.348E-01 TH-234 l.462E+OO 1.998E+OO U-234 6.600E-01 1. 677E-01' U-235 2.726E-01 3.319E-01 U-238 1.462E+OO 1.998E+OO AM-243 1. 804E-01 8.950E-02 ANH-511 3.668E-02 6.413E-02 Non-Identified Nuclides Nuclide BE-7 Page 3508 of 5809 Key-Line Activity (pCi/GRAM -4.614E+00 K.L Act error ( 1. 96-sigma) 8. 891E+OO TPU ( 1. 96-s igma) 1.693E+OO 8.443E-01 1.733E+OO 1.099E-01 1.322E-01 5.533E-02 5.845E-02 2.185E-01 3.740E+OO 7.214E-02 1. 404E-01 1.678E-01 1.834E-01 1. 678E-01 l .172E+OO 1.678E-01 3.348E-01 3.348E-01 l.404E-01 4.162E-01 1.677E-01 6.809E-01 3.348E-01 l.998E+OO 1.677E-01 3.319E-01 1.998E+OO 8.950E-02 6.413E-02 TPU ( 1. 96-sigma) 9.131E+OO NOT IDENT.

NA-22 1.327E-02 3 .111E-02 3.168E-02 NOT IDENT. NA-24 -1. OOOE+41 9. 771E+41 O.OOOE+OO SHORT HLIF AL-26 1.336E-02 2.581E-02 2.651E-02 NOT IDENT. SC-46 8.247E-02 2.834E-01 2.858E-01 FAIL ABUN V-48 1.525E+03 l.349E+04 l.351E+04 SHORT HLIF CR-51 2.408E+02 3.250E+02 3.427E+02 SHORT HLIF MN-54 4.931E-03 4.363E-02 4.368E-02 NOT IDENT. C0-56 6.270E-02 3.106E-01 3 .119E-01 NOT IDENT. MN-56 1.000E+41 4.953E+41 O.OOOE+OO SHORT HLIF C0-57

  • 9.927E-03 3.586E-02 3.6:1,4E-02 NOT IDENT. C0-58 2. 969E-01 4.260E-01 4.466E-01 NOT IDENT. FE-59 -1. 656E-01 5.760E+OO 5.761E+OO NOT IDENT. C0-60 -2.654E-02 2.927E-02 3.163E-02 NOT IDENT. ZN-65 -l.207E-01 l.922E-01 l.997E-01 NOT IDENT. GE-68 1. 598E-01 1. 561E+OO 1.563E+OO NOT IDENT. AS-73 l.152E+OO 5.602E+OO 5.626E+OO NOT IDENT. AS-74 -4.053E+02 4.379E+03 4.383E+03 SHORT HLIF SE-75 -l.264E-01 1.848E-01 l.934E-01 NOT IDENT. BR-77 1.715E+38 1.485E+39 0.000E+OO SHORT HLIF SR-82 -2.361E+02 5.529E+02 5.630E+02 SHORT HLIF RB-83 -3.046E-01 5.375E-01 5.548E-01 NOT IDENT. KR-85 1.452E+OO 6.450E+OO 6.483E+OO NOT IDENT. SR-85 1.519E-01 6.821E-01 6.856E-01 NOT IDENT. RB-86 1.932E+03 1.887E+04 1.889E+04 SHORT HLIF Y-88 -4.737E-02 1.701E-01 1.714E-01 NOT IDENT. Y-91 3.774E+Ol 4.010E+02 4. 013E+02 NOT IDENT. NB-94 l.287E-02 2.471E-02 2.538E-02 NOT IDENT. NB-95M -1.045E+OO 2.241E+OO 2.290E+OO NOT IDENT. ZR-95 -7.945E-01 1.067E+OO 1.126E+OO FAIL ABUN NB-97 l.000E+41 9.568E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.437E+41 O.OOOE+OO SHORT HLIF M0-99 7.432E+31 l.057E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 8. 421E+40 0.000E+OO SHORT HLIF RH-101 -2.137E-02 2. 716E-02 2.882E-02 NOT IDENT. RH-102 3.756E-02 4.194E-02 4.523E-02 FAIL ABUN RU-103 -2.637E+OO 3.895E+OO 4. 072E+OO FAIL ABUN RH-106 3 .137E-01 3.607E-01 3.875E-01 NOT IDENT. RU-106 3 .137E-01 3.607E-01 3.875E-01 NOT IDENT. AG-108M 5.223E-04 1.928E-02 l.928E-02 FAIL ABUN AG-110M -2.162E-02 7.261E-02 7.326E-02 FAIL ABUN SN-113 -7.688E-02 1.637E-01 1.673E-01 NOT IDENT. CD-115 -1.509E+38 2.473E+39 O.OOOE+OO SHORT HLIF SN-117M -3.098E+04 8.704E+04 8.815E+04 SHORT HLIF TE-123M -5.563E-02 1.165E-01 1.191E-01 NOT IDENT. SB-124 -5.007E-01 1. 076E+OO 1.099E+OO FAIL ABUN SB-125 -3.335E-03 7.016E-02 7.018E-02 NOT IDENT. TE-125M l.695E+02 2 .110E+02 2.244E+02 NOT IDENT. I-126 -5.215E+05 7.512E+05 7. 871E+05 SHORT HLIF SB-126 2.268E+05 l.063E+06 1.068E+06 SHORT HLIF SB-127 3.067E+21 l.394E+22 0.000E+OO SHORT HLIF I-131 -1.018E+09 3.851E+09 3.879E+09 SHORT HLIF I-132 -1.000E+41 1. 892E+42 O.OOOE+OO SHORT HLIF TE-132 -1.218E+26 3.099E+26 O.OOOE+OO SHORT HLIF BA-133 -1.023E-02 3.653E-02 3.682E-02 FAIL ABUN I-133 1. OOOE+41 2.226E+41 O.OOOE+OO SHORT HLIF CS-134 6.688E-02 8.339E-02 8.867E-02 FAIL ABUN I-135 -1.000E+41 6.860E+41 O.OOOE+OO SHORT HLIF CS-136 -3.178E+04 2.084E+05 2.089E+05 SHORT HLIF BA-140 8.059E+05 9.192E+05 9.884E+05 SHORT HLIF LA-140 -4.952E+04 2. 511E+05 2.521E+05 SHORT HLIF CE-141 l.269E+OO 2.115E+Ol 2 .115E+Ol NOT IDENT. CE-143 l.OOOE+41 7.553E+40 0.000E+OO SHORT HLIF CE-144 -2.300E-01 2.830E-01 3.014E-01 NOT IDENT. PM-144 -2.303E-02 4 .151E-02 4.279E-02 NOT IDENT. PR-144 -2.013E+OO 3.603E+OO 3.715E+OO NOT IDENT. PM-146 6.808E_.:03 3.246E-02 3. 261E-02 NOT IDE.NT. ND-147 l.454E+07 2.607E+07 2.688E+07 SHORT HLIF PM-147 -5.319E+02 6.529E+02 6.955E+02 NOT IDENT. PM-149 -3.301E+40 4.073E+40 O.OOOE+OO SHORT HLIF EU-150 1.286E-02 1. 966E-02 2.050E-02 FAIL ABUN EU-152 -9.259E-02 6.473E-02 7.702E-02 NOT IDENT. GD-153 -2. 272E-01 1. 2 67E-01 l.629E-01 NOT IDENT. EU-154 3.051E-02 7.574E-02 7.698E-02 FAIL ABUN EU-155 8.181E-02 7.973E-02 8.785E-02 FAIL ABUN TB-160 1.600E-01 1.668E+OO 1.670E+OO FAIL ABUN H0-166M -2.302E-02 4.161E-02 4.288E-02 NOT IDENT. TM-171 -6. 4 72E+OO l.394E+Ol 1.425E+Ol NOT IDENT. HF-172 -8.490E-03 1.795E-01 1. 795E-01 FAIL ABUN Page 3509 of 5809 LU-172 1. 469E-03 7.094E-02 7.095E-02 FAIL ABUN LU-176 2. 891E-02 4. 251E-02 4.446E-02 FAIL ABUN HF-181 1.970E+OO 3.384E+OO 3.498E+OO NOT IDENT. TA-182 -4.880E-01 6.794E-01 7.142E-01 FAIL ABUN RE-183 -8.280E-01 2. OllE+OO 2.045E+OO NOT IDENT. RE-184 -1.644E+Ol 2.430E+Ol 2.540E+Ol NOT IDENT. W-188 l.085E+02 9.984E+Ol l .112E+02 FAIL ABUN IR-192 -8.973E-02 3.175E-01 3.201E-01 FAIL ABUN BI-207 -4.942E-03 3.759E-02 3.766E-02 FAIL ABUN PB-210 8.066E-01 1.979E+OO 2.012E:+OO NOT IDENT. BI-211 2.332E+OO 5.065E-01 l.167E+OO FAIL ABUN PB-211 2.926E-02 4.865E-01 4.866E-01 NOT IDENT. BI-212 2.085E+OO 6.993E-01 l. l 72E+OO FAIL ABUN RN-219 6.479E-02 2.922E-01 2.936E-01 FAIL ABUN RA-223 -5.056E-02 4.102E-01 4.108E-01 FAIL ABUN AC-227 9.580E-03 2.097E-01 2.098E-01 FAIL .ABUN TH-227 9.580E-03 2.097E-01 2.098E-01 FAIL ABUN TH-231 -5.056E-02 4.102E-01 4.108E-01 FAIL ABUN PA-233 -2.204E-02 4.687E-02 4.791E-02 FAIL ABUN PA-234 -1. 747E-01 2.851E-01 2.958E-01 NOT IDENT. PA-234M 1.140E+OO 2.783E+OO 2.831E+OO FAIL ABUN NP-237 -2.204E-02 4.687E-02 4.791E-02 FAIL ABUN NP-238 l.OOOE+41 2.741E+41 O.OOOE+OO SHORT HLIF NP-239 1.059E-01 l.855E-01 l.915E-01 FAIL ABUN PU-239 -8.761E+OO 2.558E+02 2.559E+02 FAIL ABUN AM-241 2.073E-02 9.278E-02 9.325E-02 NOT IDENT. CM-243 -2.230E-02 7.328E-02 7.397E-02 FAIL ABUN BK-247 -3.012E-02 6.222E-02 6.368E-02 FAIL ABUN CM-247 4. 372E-03 2.661E-02 2.668E-02 FAIL ABUN CF-249 2.169E-02 2.712E-02 2.883E-02 NOT IDENT. CF-251 -7.413E-02 1.00lE-01 l.055E-01 NOT IDENT. Page 3510of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 49.1170 87.09 89.5969 136.47 69.9026 45.60 67.0512 87.57 89.6634 140.51 0.0000 46.54 50.3978 88.03 89. 7272 143.76 76.9943 49.72 0.0000 88.34 89.7700 144.24 77.0366 51. 35 49.0542 88.47 89.7883 145.44 77.1395 51. 87 60.4421 89. 96 89.9934 152.43 59.1218 52.39 66.1823 1093.63 90.0864 153.25 0.0000 52.97 51.1179 91.11 0.0000 323.87 81.1746 53.44 54. 0115 92.59 90.3519 156.02 0.0000 54.07 70.2134 93.35 90.4545 158.56 0.0000 57.36 0.0000 94.56 66.5202 159.00 66.1533 57.53 70.7147 94.65 66.5291 162.33 60. 8511 57.98 69.8221 94.67 66. 5311 162.66 0.0000 59.27 65.2073 94.87 52.9688 163.33 60.9141 59.32 65.2138 97.43 78. 7289 165.86 57.7415 59.54 65.2421 98.43 59.3877 176.31 60.5934 60. 96 76.9696 98.44 59.3886 176.60 0.0000 61.17 77.0010 99.53 47.1750 177.52 73.0228 62.93 75.3307 100 .11 64.6626 181. 07 0.0000 63.29 75.3825 102.03 67.9260 181.52 58.6452 63.58 75.4238 103.18 68.0358 184.41 58.8079 64.28 75.5238 103.37 68.0539 143.76 58.8809 66.73 75.2205 105.21 52. 7214 193.51 72.9990 67.24 75.2913 105.31 52.7288 197.03 62.9358 125.81 74.0523 106.12 63.1380 198.01 53.8295 67.75 74.0616 106.47 79.7370 201.83 51. 7168 69.67 89.9659 109.28 54.0541 203.43 50.6393 70.83 78.3929 111. 00 64.5978 205.31 70.7061 72.81 93.0885 111. 76 0.0000 210.85 57.9216 72.87 93.0979 114. 06 72.1817 215.65 56.9987 74.66 93.7157 116. 30 0.0000 222 .11 50.2942 74.82 93.7410 116. 74 57. 7372 227.09 54.0263 74.97 93.7650 119. 76 56.9066 227.38 62.2630 77 .11 94.1063 121.12 74.9500 228.16 0.0000 78.74 98.0050 121.22 74.9597 228.18 44.6710 79.69 109.4335 121. 7 8 64.4472 116.74 44. 6710 80.12 97.5641 122.06 57. 0718 235.69 59.9262 80.19 0.0000 122.92 67. 7134 235. 96 59.9394 80.57 97.6366 123.07 70.9007 238.63 59.2773 81. 00 109.6685 265.00 61.4232 238.98 0.0000 81. 07 109.6811 125.81 65.8320 240.99 59.3887 81. 75 97.1588 127.23 77.6466 242.00 59.4360 83.79 89.1317 127.91 58.5495 244.70 59.5627 84.00 89.1616 129.30 72. 5104 252.40 0.0000 85.43 89.3640 131. 20 68.4004 252.80 43.1554 86.55 89.5215 133.02 74.9753 254.15 0.0000 86.79 89.5548 133.52 70.7333 256.23 51.6819 86.94 89.5758 136.00 68.7891 260.90 0.0000 Page 3511of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 52. 0113 355.39 0.0000 584.27 15.8474 264.80 47.1778 356.01 38.5675 595.83 0.0000 2 65. 00 47.1849 3.64.49 0.0000 427.87 20.3070 268.22 42.0416 366.42 0.0000 602.52 0.0000 269.46 35.2013 372.51 34.6191 604. 72 17.4353 270.03 35.2163 375.05i 22.5358 607.14 18.9073 271.23 35.2473 377.52 29.5120 609.32 19.4092 273.65 0.0000 356.01 29.6200 610.33 19.4173 276.40 37.8200 '388.16 20.9595 614.28 11.6689 277.37 37.8456 388.63 0.0000 618.01 19.4775 277.60 37.8522 391. 69 28.8763 620.36 19.4954 278.00 37.8636 264.66 27.2625 621. 93 11.7051 279.20 57.0473 401.81 28.1602 630.19 0.0000 279.54 57.0616 402.40 28.1693 631.29 10.7695 279.70 39.1318 404.85 26.4441 633.25 19.5964 280.46 42.4161 410.95 21. 22 61 634.78 0.0000 283.69 34.3378 413. 71 33.6582 635.95 18.6359 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.5189 423.72 0.0000 645.85 17.7239 285.90 0.0000 427.09 21. 4106 657.76 16.3221 287.50 29.5115 427.87 21. 4194 657.90 0.0000 290.67 22.1830 433.94 21. 4878 661.66 15.8509 293.27 0.0000 439.40 19.7531 664.57 0.0000 351.93 19.7803 453.88 22.6140 666.33 0.0000 295. 96 19.7905 463.37 26.3574 666.50 0.0000 879.38 27.2603 468.07 24.5967 667. 71 0.0000 299.98 29.7671 473.00 0.0000 677. 62 14.9506 300.09 29.7693 475.06 18.2825 685.70 0.0000 300 .13 29.7700 476.78 28.3618 695.00 0.0000 301.36 29.7949 477.60 24.7121 696. 49 18.0674 302.85 29.8250 482.18 16. 5114 696. 51 18.0674 256.23 29.8586 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.0685 306.78 29.9041 497.08 22.1729 697.49 17.0699 308.46 29.9377 505.52 16.6959 702.65 15.0897 311. 90 35.0077 507.63 0.0000 706.68 19.1423 316.51 30.9335 511. 00 26.9677 711.68 19.1770 319.41 0.0000 514.00 29.3326 720.70 0.0000 320.08 0.0000 514.00 29.3326 721.93 0.0000 321. 04 30.1868 520.40 28.9528 722.78 21. 2803 323.87 31.0817 520.69 0.0000 722.91 21. 2811 325.23 49.6072 522.65 0.0000 723. 31 19.7642 328.76 0.0000 527.90 0.0000 724 .19 3.0416 333.37 23.3268 528.26 24.3697 727. 33 4.5674 333.97 25.3644 529.59 18.7573 733.00 6.1023 334.37 31. 7139 529.87 0.0000 735.93 19.3440 338.28 28.8245 531. 02 0.0000 333.97 8.1491 338.32 28.8252 537.26 0.0000 739.50 0.0000 311. 90 30.5618 546.56 0.0000 747.24 17.3763 340.48 30.5618 552.55 28.4241 748.06 10.2242 340.55 0.0000 563.25 15.2305 752.31 16.3828 344.28 38.2928 569.33 15.7474 753.82 0.0000 345.93 27.2578 946.00 18.6121 756.73 18.4592 351.06 35.8887 569.70 18.6137 756.80 19.4855 351.93 35.9075 583.19 21.1200 884.68 12.3369 Page 3512of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 0.0000 1274.44 8.8366 1620.50 1. 9110 766.42 0.0000 1001.03 7.7423 1621. 92 2.8674 766.84 13.8928 1002.74 7.7460 1678.03 0.0000 772.60 0.0000 1004.73 13.2861 1690.97 2.9046 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 O.QOOO 1025.87 0.0000 1764..49 0.0000 778.90 14.4666 1028.54 0.0000 1063.66 4.7142 783.70 0.0000 1037.84 17.8763 1771.35 1. 9646 785.37 14.4979 1038.76 0.0000 1791.20 0.0000 792.07 12.4546 631.29 15.6794 1808.65 2. 9663 794.95 14.5446 1048.07 0.0000 1810.72 0.0000 795.86 14.5492 1049.04 6.7241 1836.06 3.9739 810.06 9.3970 1050.41 6.7266 810.29 11.4861 1063.66 12.3759 344.28 8.3538 1077.00 0.0000 810.76 9.3988 1077.34 5.0812 815.77 0.0000 1085.87 14. 7118 1048.07 0.0000 1093.63 15.8753 832.01 10.5155 1099.45 13.6279 834.85 11. 5778 1112. 07 21.6471 835.71 6.3169 1112.84 19.3726 836.80 0.0000 1115. 54 22.2374 846.75 0.0000 '1120.29 17 .12 65 846.77 9.5087 1120.55 17.1277 856.80 0.0000 1221. 41 17.1301 860.56 9.5500 1129.67 9.1556 871.09 11. 7108 1131. 51 0.0000 873.19 20.2408 1147.95 0.0000 875.33 0.0000 1173.23 15.0408 879.38 17.0775 1177.95 11. 5837 880.51 16.0156 1189.05 19.7448 883.24 16.0291 1204.77 10.4934 884.68 12.8291 1221.41 15.8027 889.28 10.7060 1231.02 13.1992 894.76 16.0858 1235.36 0.0000 898.04 12.8813 1238.28 11. 4591 900.72 10.7430 1260.41 0.0000 903.28 17.2025 1271.87 7.9953 911.20 14.0103 1274.44 6.2224 912.08 14.0140 1274.54 6.2224 923.98 0.0000 1291. 59 9.8163 926.50 8. 6611 1298.22 0.0000 929 .11 8.6676 1312 .11 0.0000 937.49 10.8614 1332.49 11.7083 944.13 0.0000 1362.66 0.0000 946.00 15.2436 1365.19 2.9029 949.00 10.8980 1368.63 0.0000 667.71 0.0000 1384.29 2.7328 962.31 9.8459 1408.01 9.1559 964.08 13.1348 1457.56 0.0000 966.17 0.0000 1460.82 1.8516 911.20 18.0851 1489.16 4.6558 968. 97 18.0851 1505.03 7.4731 983.53 0.0000 1584.12 1.5182 984.45 0.0000 1596.21 0.0000 Page 3513of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:08:36.16 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM08.CNF;320 Background date : Z-OCT-2016 11:00:23. Sample date 8-DEC-2015 10:19:00. Acquisition date : 3-0CT-2016 09:08:01. Sample ID G405235027 Sample quantity 1.58553E+02 GRAM Detector name : GAM08 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.68 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 1 1 0 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 74.88* 76.98* 83.55* 87.08* 92.62* 129.17 185.97* 209.64 238.61* 241. 91 295.39* 300.66 328.15 338.63* 351. 96* 384.53 406.41 468.34 511. 08* 576.94 583.60* 609.17* 628.44 663.83 669 .11 727.14* 797.54 829.90 859.90* 911. 33* 961.41* 969.81* 994.04 1001.96* Page 3514of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 97 150 49 47 24 33 85 39 312 74 119 32 37 67 158 53 57 11 52 8 119 148 9 29 14 32 5 20 21 65 5 39 10 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 130 111 147 90 216 96 66 74 54 66 46 69 31 76 47 76 75 24 66 14 24 26 14 24 4 23 32 0 10 30 6 32 7 13 1.18 1. 04 1. 67 0.91 1.16 1. 54 1. 66 1. 01 1.16 1. 79 1. 31 1. 07 1. 86 1. 43 1.16 9.77 10.03 0.93 2.48 0.59 1. 84 1. 68 1. 01 5.39 0.58 1. 27 1. 21 1. 99 2.66 1. 62 0.94 1. 03 2.90 1. 86 150.02 154.22 167.36 174.43 185.52 258.64 372.30 419.67 477.63 484.23 591.23 601.77 656.77 677.75 704.42 769.59 813.36 937.28 1022.78 1154. 56 1167.88 1219.03 1257.59 1328.40 1338.96 1455.07 1595.91 1660.65 1720.67 1823.57 1923.75 1940.57 1989.03 2004.89 146 146 165 172 181 255 367 416 472 472 587 597 653 672 699 759 801 931 1014 1150 1161 1211 1254 1319 1336 1449 1589 1656 1713 1815 1921 1930 1979 1999 12 2.71E-02 22.2 12 4.17E-02 14.4 8 1. 37E-02 45 .1 5 1. 31E-02 34. 2 10 6.60E-03123.0 8 9.21E-03 54.3 11 2.36E-02 23.1 8 1.08E-02 41.6 29 8.66E-02 7.0 29 2.05E-02 28.4 9 3.31E-02 14.2 11 8.95E-03 52.2 9 1. 03E-02 31.1 13 1.85E-02 30.3 12 4.38E-02 12.1 23 1. 47E-02 44. 7 27 1.59E-02 44.0 8 3.07E-03 82.4 22 1.45E-02 46.0 8 2.18E-03 90.2 17 3.30E-02 13.5 15 4.llE-02 11.4 6 2.60E-03 70.4 17 8.17E-03 43.2 8 3.89E-03 36.4 13 8.92E-03 36.8 10 l.43E-03210.7 11 5.56E-03 22.4 14 5.83E-03 40.9 15 1.80E-02 22.6 6 1.39E-03 98.6 19 1. 08E-02 39. 3 13 2.81E-03 61.0 10 2. 98E-03 72. 8 Fit 9.93E-01 1.55E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235027 Acquisition date 3-0CT-2016 09:08:01 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1071.27 13 8 1. 78 2143.54 2138 11 3.63E-03 50.6 36 0 1120.39* 26 25 2.18 2241. 82 2231 17 7.19E-03 49.4 J7 0 1150. 35 7 4 1. 24 2301.14 2297 9 2.02E-03 63.2 38 0 1154. 66 16 2 1. 98 2310.36 2306 9 4.35E-03 30.7 39 0 1173.23 12 2 1. 50 2347.51 2344 8 3.26E-03 36.1 40 0 1302.27 4 *6 0.81 2605.66 2600 8 1. lOE-03118. 7 41 0 1460.80 315 4 2.30 2922.80 2915 14 8.75E-02 5.8 42 0 1728.85 19 0 1. 76 3459.00 3452 12 5.28E-03 22.9 43 0 1764.94* 19 4 1. 68 3531.20 3523 13 5.22E-03 33.6 Flag: "*" = Peak area was modified by background subtraction Page 3515of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:08:38 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 8-DEC-2015 10:19:00 G405235027 Acquisition date : Sample quantity Sample.geometry : 3-0CT-2016 09:08:01 158.55 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAS 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3516 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.68 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235027 Acquisition date 3-0CT-2016 09:08:01 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 9..671E-01 1.404E+Ol 1.404E+Ol 11. 55 OK CD-109 88.03 3.70* 4.287E+OO 9.133E-01 l.433E+OO 141.09 OK SN-126 64.28 9.60 2.248E+OO Line Not Found Absent 86.94 8.90 4.287E+OO 3.797E-01 3.797E-01 141.09 OK 87.57 37.00* 4.287E+OO 9.133E-02 9.134E-02 141.09 OK TL-208 277.37 6.60 3. 710E+OO Line Not Found Absent 583.19 85.00* 2.006E+OO 3.567E-01 3.567E-01 27.01 OK 860.56 12.50 1. 479E+OO 5.555E-01 5.555E-01 81. 86 OK PB-212 74.82 10.28 3.324E+OO 1.222E+OO 1.222E+OO 66.34 OK 77 .11 17.10 3.513E+OO l.567E+OO 1.567E+OO 28.77 OK 238.63 43.60* 4.174E+OO 9. 631E-01 9.631E-01 14.09 OK 300.09 3.30 3.474E+OO 1.544E+OO 1.544E+OO 104.34 OK BI-214 609.32 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 OK 1120.29 14.92 1.202E+OO 6.847E-01 6.850E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 OK PB-214 74.82 5.80 3.318E+OO Line Not Found <<INT Reject 77 .11 9.70 3. 513E+OO 2.762E+OO 2.763E+OO 28.77 OK 87.09 3.41 4.288E+OO Line Not Found <<INT Reject 242.00 7.25 4 .130E+OO Line Not Found <<INT Reject 295.22 18.42 3.524E+OO 1.009E+OO 1.009E+OO 28.32 OK 351.93 35.60* 3.045E+OO 7.856E-01 7.858E-01 24.22 OK RN-222 609.32 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 OK 1120.29 14.92 l.202E+OO 6.847E-01 6.850E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 OK RA-224 240.99 4.10* 4 .131E+OO 6.650E-01 6.650E-01 222.68 OK RA-226 609.32 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 OK 1120.29 14.92 l.202E+OO 6.847E-01 6.850E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 OK AC-228 105.21 1.10 5.138E+OO Line Not Found Absent 338.32 11.27 3.146E+OO 1.020E+OO 1.020E+OO 60.55 OK 794.95 4.25 1.572E+OO Line Not Found Absent 835.71 1. 61 1.512E+OO Line Not Found Absent 911. 20 25.80* l.414E+OO 8.645E-01 8.645E-01 45.16 OK 968. 97 15.80 1.347E+OO 8. 811E-01 8. 811E-01 78.68 OK RA-228 105.21 1.10 5.138E+OO Line Not Found Absent 338.32 11. 27 3.146E+OO 1.020E+OO 1.020E+OO 60.55 OK 794.95 4.25 1. 572E+OO Line Not Found Absent 835. 71 1. 61 1.512E+OO Line Not Found Absent 911. 20 25.80* l.414E+OO 8.645E-01 8.645E-01 45.16 OK 968.97 15.80 1. 34 7E+OO 8. 811E-01 8.811E-01 78.68 OK TH-228 74.82 10.28 3.324E+OO 1.222E+OO l.222E+OO 66.34 OK 77 .11 17.10 3.513E+OO 1.567E+OO 1.567E+OO 28.77 OK 238.63 43.60* 4.174E+OO 9.631E-01 9. 631E-01 14.09 OK 300.09 3.30 3.474E+OO 1.544E+OO 1.544E+OO 104.34 OK TH-230 609.32 45.49* 1.938E+OO 8.533E-01 8.533E-01 22.78 OK 1120.29 14.92 1.202E+OO 6.847E-01 6.847E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.740E-01 67.14 OK PA-231 283.69 1. 70 3.643E+OO Line Not Found Absent 301.36 5.35* 3.474E+OO 9. 521E-01 9. 521E-01 104.34 OK Page 3517of5809 Nuclide Line Activity Report (continued) Sample ID : G405235027 Acquisition date Page : 3 3-0CT-2016 09:08:01 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-232 105.21 1.10 5 .1.38E+OO Line Not Found Absent 338.32 11.27 3.146E+OO 1.020E+00 1.020E+OO 60.55 OK 835.71 1. 61 1.512E+OO Line Not Found Absent 911.20 25.80* 1.414E+OO 8.645E-01 8.645E-01 45.16 OK 968. 97 15.80 1.347E+OO 8. 811E-01 8. 811E-01 78.68 OK U-234 609.32 45.49* 1.938E+OO 8.533E-01 8.533E-01 22.78 OK 1120.29 14.92 l.202E+OO 6.847E-01 6.847E-01 98.80 OK 1764.49 15.30 8.178E-01 6.740E-01 6.740E-01 67.14 OK AM-243 43.53 5.90 2.327E-01 Line Not Found Absent 74.66 67.20* 3.324E+OO 1.870E-01 1.870E-01 66.34 OK ANH-511 511. 00 100.00* 2.233E+OO 1.215E-01 l.215E-01 91. 93 OK Flag: "*" = Keyline Page 3518of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:08:39.77 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l * *Acquisition date 3-0CT-2016 09:08:01 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:19:00 Analyst initials: MXRl *
  • Sample ID G405235027 Sample Quantity 1.5855E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.404E+Ol 1.589E+OO 7.692E-01 CD-109 1.433E+OO 1.982E+OO 2.309E+OO SN-126 9.134E-02 1.263E-01 1.579E-01 TL-208 3.567E-01 9.441E-02 6.442E-02 PB-212 9.631E-01 l.330E-01 l.031E-01 BI-214 8.536E-01 1.906E-01 l.144E-01 PB-214 7.858E-01 1.865E-01 l.262E-01 RN-222 8.536E-01 l.906E-01 1.144E-01 RA-224 6.650E-01 l.451E+OO 1.106E+OO RA-22 6 8.536E-01 l.906E-01 l.144E-01 AC-228 8.645E-01 3.826E-01 2. 701E-01 RA-228 8.645E-01 3.826E-01 2. 701E-01 TH-228 9.631E-01 l.330E-01 1. 031E-01 TH-230 8.533E-01 1.905E-01 1.143E-01 PA-231 9.521E-01 9.735E-01 8.617E-01 TH-232 8.645E-01 3.826E-01 2. 701E-01 U-234 8.533E-01 l.905E-01 l.143E-01 AM-243 l.870E-01 1.216E-01 1.125E-01 ANH-511 1.215E-01 l.095E-01 5.481E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 6.504E+OO l.145E+Ol 2.425E+Ol NOT IDENT. NA-22 4.213E-02 4.337E-02 1. 038E-01 NOT IDENT. NA-24 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF AL-26 2.021E-02 3.844E-02 9.064E-02 NOT IDENT. SC-46 -2.279E-01 3.905E-01 7 .114E-01 FAIL ABUN V-48 O.OOOE+OO l.140E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 4.416E+02 O.OOOE+OO SHORT HLIF MN-54 2.085E-02 6.875E-02 l.308E-01 NOT IDENT. C0-56 2.340E-01 4.575E-01 1.002E+OO NOT IDENT. MN-56 O.OOOE+OO l.941E+41 O.OOOE+OO SHORT HLIF C0-57 -1.60/E-02 5.053E-02 9.168E-02 NOT IDENT. Page 3519of5809 C0-58 2.274E-01 5.281E-01 1.163E+OO NOT IDENT. FE-59 -8.323E-01 6. 966E+OO 1.358E+Ol NOT IDENT. C0-60 -2.168E-02 4.226E-02 7.539E-02 FAIL ABUN ZN-65 -l.915E-02 2.638E-01 4.365E-01 NOT IDENT. GE-68 l.983E+00 2. 631E+OO 5. 691E+OO NOT IDENT. AS-73 -6.587E+OO 1.307E+Ol 2.458E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.045E+03 O.OOOE+OO SHORT HLIF SE-75 l.870E-01 2.150E-01 4.561E-01 NOT IDENT. BR-77 O.OOOE+OO 2.479E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.164E+02 O.OOOE+OO ' SHORT HLIF RB-83 4 .196E-01 7.599E-01 1. 501E+OO NOT IDENT. KR-85 3.660E+OO 7.482E+OO 1.513E+Ol NOT IDENT. SR-85 3.810E-01 7.908E-01 1.598E+OO NOT IDENT. RB-86 O.OOOE+OO 3.471E+04 O.OOOE+OO SHORT HLIF Y-88 -8.357E-02 2.283E-01 4.508E-01 NOT IDENT. Y-91 -2.909E+02 5.701E+02 1.012E+03 NOT IDENT. NB-94 2.014E-02 3.428E-02 7.343E-02 NOT IDENT. NB-95 -8.599E-01 9.997E-01 1.764E+OO NOT IDENT. NB-95M -2.035E+OO 2.808E+OO 4.596E+OO NOT IDENT. ZR-95 2.936E-01 1.234E+OO 2.664E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.306E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.891E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 9. 131E-03 3.689E-02 6.517E-02 NOT IDENT. RH-102 l.055E-02 6.795E-02 l.197E-01 NOT IDENT. RU-103 4.992E-01 5.610E+OO 1.108E+Ol FAIL ABUN RH-106 -8.768E-02 5'. 710E-01 1.056E+OO NOT IDENT. RU-106 -8.768E-02 5.710E-01 1.056E+OO NOT IDENT. AG-108M 6.716E-03 2.641E-02 5.349E-02 NOT IDENT. AG-110M -3.887E-02 8.707E-02 l.649E-01 NOT IDENT. SN-113 1.470E-01 2.612E-01 4.943E-01 NOT IDENT. CD-115 0.000E+OO 3.789E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1.062E+05 O.OOOE+OO SHORT HLIF TE-123M -9.638E-03 l.360E-01 2.481E-01 NOT IDENT. SB-124 7.086E-02 1. 721E+OO 4.004E+OO NOT IDENT. SB-125 -3.865E-02 l.081E-01 2.002E-01 NOT IDENT. TE-125M 1.640E+Ol 3.259E+02 6.058E+02 NOT IDENT. I-126 O.OOOE+OO 7.697E+05 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO l.382E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.081E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 5.044E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 7.139E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4.310E+26 O.OOOE+OO SHORT HLIF BA-133 8. 272E-03 4.338E-02 7.863E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.493E-02 6.034E-02 1.336E-01 NOT IDENT. CS-135 1.302E-02 l.510E-01 2.983E-01 NOT IDENT. I-135 O.OOOE+OO l.050E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.149E+05 O.OOOE+OO SHORT HLIF BA-137M 5.530E-02 4.183E-02 8.721E-02 NOT IDENT. CS-137 5.842E-02 4.419E-02 9.213E-02 NOT IDENT. CE-139 4.175E-02 1. 267E-01 2.372E-01 NOT IDENT. BA-140 O.OOOE+OO 1.417E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.892E+05 O.OOOE+OO SHORT HLIF CE-141 -8.205E+00 2.795E+Ol 4.990E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.864E+41 O.OOOE+OO SHORT HLIF CE-144 7.581E-03 3.674E-01 6.760E-01 NOT IDENT. PM-144 9.004E-03 6.253E-02 1.271E-01 NOT IDENT. PR-144 7.316E-01 5.425E+OO 1.102E+Ol NOT IDENT. PM-146 -4.860E-02 4.515E-02 7.404E-02 NOT IDENT. ND-147 O.OOOE+OO 3.516E+07 O.OOOE+OO SHORT HLIF PM-147 l.708E+02 8.258E+02 1.581E+03 NOT IDENT. PM-149 O.OOOE+OO 5.024E+40 O.OOOE+OO SHORT HLIF EU-150 -3.078E-03 2.875E-02 4. 961E-02 FAIL ABUN EU-152 -2.251E-02 9.157E-02 l.560E-01 NOT IDENT. GD-153 -2.881E-02 1.927E-01 3.602E-01 NOT IDENT. EU-154 1.033E-01 l.063E-01 2.544E-01 NOT IDENT. EU-155 1. 34 7E-01 1.234E-01 2.515E-01 FAIL ABUN TB-160 -8.125E-01 1.959E+OO 3.684E+OO FAIL ABUN H0-166M -2.912E-02 4.958E-02 9.285E-02 NOT IDENT. TM-171 -3.054E+OO 3.295E+Ol 6.422E+Ol NOT IDENT. HF-172 -5.277E-02 2.759E-01 4.622E-01 FAIL ABUN LU-172 -l.452E-02 8.554E-02 1.670E-01 FAIL ABUN LU-176 -1.481E-03 2.347E-02 4.603E-02 FAIL ABUN HF-181 -3.218E-01 4.122E+OO 7. 960E+OO NOT IDENT. TA-182 -l.921E-02 9.545E-01 1.863E+OO FAIL ABUN RE-183 -2.253E+OO 3.904E+OO 7.300E+OO NOT IDENT. Page 3520 of 5809 RE-184 -2.091E+Ol 3.319E+Ol 5.698E+Ol NOT IDENT. W-188 -l.239E+02 l.328E+02 2. 051E+02 NOT IDENT. IR-192 -5.255E-01 4.755E-01 8.214E-01 FAIL ABUN HG-203 -9. 311E-01 2.515E+OO 4.758E+OO NOT IDENT. BI-207 -2.076E-02 4. 967E-02 9.162E-02 FAIL ABUN PB-210 3.177E+OO 6.242E+OO l.286E+Ol NOT IDENT. BI-211 O.OOOE+OO 5.137E-01 7.917E-01 FAIL ABUN PB-211 5.463E-01 6.832E-01 l.447E+OO NOT IDENT. BI-212 l.426E+OO l.028E+OO l.486E+OO FAIL ABUN RN.,.-219 l.594E-Ol 3. 681E-Dl 7.573E-01 NOT IDENT. RA-223 2.525E-01 6.153E-01 l.135E+OO FAIL ABUN AC-227 5.033E-02 2.330E-01 4.692E-01 FAIL ABUN TH-227 5.033E-02 2.330E-01 4.692E-01 FAIL ABUN TH-229 -l.659E-01 4.541E-01 8.847E-01 FAIL ABUN TH-231 2.525E-Ol 6.153E-01 l.135E+OO FAIL ABUN PA-233 1. 298E-02 5.757E-02 l.162E-01 FAIL ABUN PA-234 -3.659E-02 2.617E-01 5.191E-01 NOT IDENT. PA-234M 4.681E+OO 6.678E+OO l.131E+Ol FAIL ABUN TH-234 -8.951E-01 l.646E+OO 3.154E+OO FAIL ABUN U-235 -l.495E-02 2.094E-01 3.874E-01 FAIL ABUN NP-237 1. 298E-02 5.757E-02 l.162E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF U-238 -8.951E-01 1. 646E+OO 3.154E+OO FAIL ABUN NP-239 4.169E-02 2.647E-01 5.019E-01 NOT IDENT. PU-239 5.725E+02 6.099E+02 7.002E+02 FAIL ABUN AM-241 l.133E-01 l.732E-01 3.575E-01 NOT IDENT. CM-243 -7.545E-02 1. 075E-01 1.904E-01 NOT IDENT. BK-247 5. 725E-02 7.294E-02 1.542E-01 FAIL ABUN CM-247 2.614E-02 3.534E-02 7.457E-02 NOT IDENT. CF-249 l.604E-02 4.279E-02 8.566E-02 NOT IDENT. CF-251 -1.970E-02 l.169E-01 2.321E-01 NOT IDENT. Page 3521 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:08:36.97 Nuclide Line Activity Report .. Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 306 10.66* 9.671E-01 1.404E+Ol l.404E+Ol 11. 55 CD-109 88.03 62 3.70* 4.287E+OO 1.843E+OO 2.892E+OO 68.45 SN-126 64.28 ------9.60 2.248E+OO ------Line Not Found ------86.94 62 8.90 4.287E+OO 7.662E-01 7.662E-01 68.45 87.57 62 37.00* 4.287E+OO 1.843E-01 l.843E-01 68.45 TL-208 277.37 ------6.60 3.710E+OO ------Line Not Found ------583.19 128 85.00* 2.006E+OO 3.567E-01 3.567E-01 27.01 860.56 22 12.50 1.479E+OO 5.555E-01 5.555E-01 81.86 BI-211 72. 87 ------1. 23 3 .135E+OO ------Line Not Found ------351.06 180 12.92* 3.045E+OO 2.165E+OO 2.165E+OO 24.22 PB-212 74.82 129 10.28 3.324E+OO 1. 791E+OO l.791E+00 44.36 77 .11 199 17.10 3.513E+OO 1.567E+OO 1.567E+OO 28.77 238.63 370 43.60* 4.174E+OO 9.631E-01 9. 631E-01 14.09 300.09 37 3.30 3.474E+OO 1.544E+OO 1.544E+00 104.34 BI-214 609.32 159 45.49* 1.938E+OO 8.533E-01 8.536E-01 22.78 1120.'29 26 14.92 1.202E+OO 6.847E-01 6.850E-01 98.80 1764.49 18 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 PB-214 74.82 129 5.80 3.324E+OO 3.175E+OO 3.176E+OO 44.36 77 .11 199 9.70 3. 513E+OO 2.762E+OO 2.763E+OO 28.77 87.09 62 3.41 4.287E+OO 2.000E+OO 2.000E+OO 68.45 242.00 88 7.25 4.131E+OO 1.385E+OO 1.385E+OO 56.85 295.22 138 18.42 3.524E+OO 1.009E+OO l.009E+00 28.32 351. 93 180 35.60* 3.045E+OO 7.856E-01 7.858E-01 24.22 RN-222 609.32 159 45.49* 1.938E+00 8.533E-01 8.536E-01 22.78 1120.29 26 14.92 1.202E+00 6.847E-01 6.850E-01 98.80 1764.49 18 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 RA-224 240.99 88 4.10* 4 .131E+OO 2.449E+OO 2.449E+OO 56.85 RA-226 609.32 159 45.49* 1.938E+00 8.533E-01 8.536E-01 22.78 1120.29 26 14.92 1.202E+OO 6.847E-01 6.850E-01 98.80 1764.49 18 15.30 8.178E-01 6.740E-01 6.743E-01 67.14 AC-228 105.21 ------1.10 5.138E+OO ------Line Not Found ------338.32 76 11. 27 3.146E+OO l.020E+00 1.020E+OO 60.55 794.95 ------4.25 1. 572E+OO ------Line Not Found ------835.71 ------1. 61 1.512E+OO ------Line Not Found ------911.20 67 25.80* 1.414E+OO 8.645E-01 8.645E-01 45.16 968.97 40 15.80 1.347E+OO 8. 811E-01 8. 811E-01 78.68 RA-228 105.21 ------1.10 5.138E+OO ------Line Not Found ------338.32 76 11. 27 3.146E+OO 1.020E+OO 1.020E+OO 60.55 794.95 ------4.25 l.572E+00 ------Line Not Found ------835. 71 ------1. 61 1. 512E+OO ------Line Not Found ------911. 20 67 25.80* 1.414E+OO 8.645E-01 8.645E-01 45.16 968. 97 40 15.80 1. 347E+OO 8. 811E-01 8. 811E-01 78.68 TH-228 74.82 129 10.28 3.324E+OO 1. 791E+OO 1. 791E+OO 44.36 77 .11 199 17.10 3. 513E+OO 1.567E+00 1.567E+OO 28.77 238.63 370 43.60* 4.174E+OO 9.631E-01 9.631E-01 14.09 300.09 37 3.30 3.474E+OO 1.544E+OO 1.544E+OO 104.34 TH-230 609.32 159 45.49* 1.938E+OO 8.533E-01 8.533E-01 22.78 Page 3522 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235027 Acquisition date Page : 2 3-0CT-2016 09:08:01 Nuclide Type: Nuclide PA-231 TH-232 U-234 AM-243 ANH-511 Flag: "*" Page 3523 of 5809 Energy 1120.29 1764.49 283.69 301.36 105.21 338.32 835.71 911. 20 968. 97 609.32 1120.29 1764.49 43.53 74.66 511.00 Key line Area %Abn 26 14.92 18 15.30 ------1. 70 37 5.35* ------1.10 76 11. 27 ------1. 61 67 25.80* 40 15.80 159 45.49* 26 14.92 18 15.30 ------5.90 129 67.20* 57 100.00* Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCi/GRAM %Error 1.202E+OO 6.847E-01 6.847.E-01 98.80 8.178E-01 6.740E-01 6.740E-01 67.14 3.643E+OO ------Line Not Found ------3.474E+OO 9.521E-01 9.521E-01 104.34 5.138E+OO ------Line Not Found ------3.146E+OO 1.020E+OO 1.020E+OO 60.55 l.512E+OO ------Line Not Found ------1.414E+OO 8.645E-01 8.645E-01 45.16 1. 34 7E+OO 8.811E-01 8. 811E-01 78.68 1.938E+OO 8.533E-01 8.533E-01 22.78 1.202E+OO 6.847E-01 6.847E-01 98.80 8.178E-01 6.740E-01 6.740E-01 67.14 2.327E-01 ------Line Not Found ------3.324E+OO 2.740E-01 2.740E-01 44.36 2.233E+OO l.215E-01 1.215E-01 91. 93 Page : 3 Summary of Nuclide Activity Sample ID : G405235027 Acquisition date 3-0CT-2016 09:08:01 Total number of lines in spectrum 43 Number of unidentified lines 11 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 . PA-231 TH-232 U-234 AM-243 ANH-511 Hlife l.25E+09Y 461. 40D 2.30E+05Y 1.41E+l0Y 7.04E+08Y l.41E+10Y 1600. OOY 1600. OOY 1600. OOY 1.41E+l0Y 1600.00Y l.41E+l0Y 1. 41E+lOY l.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 57 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.404E+Ol 1.843E+OO 1.843E-01 3.567E-01 2.165E+OO 9. 631E-01 8.533E-01 7.856E-01 8.533E-01 2.449E+00 8.533E-01 8.645E-01 8.645E-01 9. 631E-01 8.533E-01 9.521E-01 8.645E-01 8.533E-01 2.740E-01 1. 215E-01 3.195E+Ol 3.195E+Ol Decay Corr pCi/GRAM l.404E+Ol 2.892E+OO l.843E-01 3.567E-01 2.165E+OO 9. 631E-01 8.536E-01 7.858E-01 8.536E-01 2.449E+OO 8.536E-01 8.645E-01 8.645E-01 9.631E-01 8.533E-01 9. 521E-01 8.645E-01 8.533E-01 2.740E-01 1.215E-01 3.300E+Ol 3.300E+Ol 74.42% Decay Corr 2-Sigma Error 0.162E+Ol 1. 980E+OO 1. 2 61E-01 0.963E-01 0.524E+OO 1.357E-01 1.945E-01 1.903E-01 1.945E-01 1.392E+OO l.945E-01 3.904E-01 3.904E-01 1.357E-01 1.944E-01 9.934E-01 3.904E-01 1.944E-01 l.216E-01 1. ll 7E-01 "M" Manually accepted " 2-Sigma %Error 11. 55 68.45 68.45 27.01 24.22 14.09 22.78 24.22 22.78 56. 85 22.78 45.16 45.16 14.09 22.78 104.34 45.16 22.78 44.36 91. 93 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3524 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235027 Acquisition date : 3-0CT-2016 09:08:01 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.55 65 194 1. 67 167.36 165 8 1. 37E-02 90. 3 4.04E+OO T 0 92. 62 31 281 1.16 185.52 181 10 6.60E-03 **** 4.62E+OO T 0 129.17 42 121 1. 54 258.64 255 8 9.21E-03 **** 5.48E+OO T 0 J.85.97 104 80 1. 66 372. 30. 367 ii 2.36E-02 46.3 4.93E+OO T 0 209.64 47 89 1. 01 419.67 416 8 1. 08E-02 83. 3 4.58E+OO T 0 328.15 43 35 1. 86 656.77 653 9 1. 03E-02 62. 2 3.23E+OO T 0 384.53 60 86 9.77 769.59 759 23 l.47E-02 89.3 2.83E+OO T 0 406.41 64 84 10.03 813.36 801 27 l.59E-02 88.0 2.70E+OO 0 468.34 12 26 0.93 937.28 931 8 3.07E-03 **** 2.40E+OO T 0 576.94 8 15 0.59 1154.56 1150 8 2.18E-03 **** 2.02E+OO 0 628.44 10 15 1. 01 1257.59 1254 6 2.60E-03 **** 1. 89E+OO 0 663.83 31 25 5.39 1328.40 1319 17 8.17E-03 86.4 1. 81E+OO T 0 669 .11 15 4 0.58 1338.96 1336 8 3.89E-03 72.8 1. 80E+OO T 0 727.14 34 24 1. 27 1455.07 1449 13 8.92E-03 73.6 1.69E+OO T 0 797.54 5 33 1. 21 1595.91 1589 10 l.43E-03 **** 1. 57E+OO 0 829.90 21 0 1. 99 1660.65 1656 11 5.56E-03 44.7 1. 52E+OO 0 961. 41 5 6 0.94 1923.75 1921 6 l.39E-03 **** 1.36E+OO T 0 994.04 10 7 2.90 1989.03 1979 13 2.81E-03 **** 1. 32E+OO 0 lOO:I. 96 11 13 1. 86 2004.89 1999 10 2.98E-03 **** 1. 31E+OO T 0 1071. 27 13 8 1. 78 2143.54 2138 11 3.63E-03 **** 1.25E+OO 0 1150.35 7 4 1. 24 2301.74 2297 9 2.02E-03 **** 1.18E+OO 0 1154. 66 16 2 1. 98 2310.36 2306 9 4. 35E-03 61. 3 1'.17E+OO 0 1173.23 12 2 1. 50 2347.51 2344 8 3.26E-03 72.2 1.16E+OO T 0 1302.27 4 6 0.81 2605.66 2600 8 1.lOE-03 **** 1. 06E+OO 0 1728.85 18 0 1. 76 3459.00 3452 12 5.28E-03 45.9 8.34E-01 Flags: "T" = Tentatively associated Page 3525 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:08:51.75 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l * *Acquisition date 3-0CT-2016 09:08:01 Sensitivity 3.000 *
  • Detector ID GAM08 . Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:19:00 Nuclide Library : SOLID *
  • Sample ID G405235027 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.5855E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Le (pCi/GRAM 3.220E-01 1.087E+OO 7.460E-02 2.833E-02 4.785E-02 4. 968E-02 5.694E-02 4. 968E-02 5.131E-01 4.968E-02 1.171E-01 1.171E-01 4.785E-02 4. 966E-02 3.946E-01 1.171E-01 4. 966E-02 5.314E-02 2.443E-02 ' ____ Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 3526 of 5809 Le (pCi/GRAM 1. 078E+Ol 4.445E-02 0.000E+OO 3. 727E-02 3.013E-01 0.000E+OO 0.000E+OO 5.699E-02 4.363E-01 O.OOOE+OO 4.267E-02 5.015E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106' AG-108M AG-llOM SN-l13 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD'-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 3527 of 5809 5.782E+OO 3.078E-02 l.933E-01 2.495E+OO 1.144E+Ol O.OOOE+OO 2. l12E-01 O.OOOE+OO O.OOOE+OO 6.756E-01 6.840E+OO 7.223E-01 O.OOOE+OO 1.677E-01 4.292E+02 3.291E-02 7.773E-01 2.131E+OO l.141E+OO O.OOOE+OO 0.000E+OO 0.000E+OO 0.000E+OO 3.039E-02 5.256E-02 4.899E+OO 4.669E-01 4.669E-01 2.386E-02 6.812E-02 2.247E-01 O.OOOE+OO O.OOOE+OO l.152E-01 l.499E+OO 8.945E-02 2.847E+02 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.553E-02 O.OOOE+OO 6.039E-02 1. 381E-01 O.OOOE+OO O.OOOE+OO 3.949E-02 4.172E-02 1. l12E-01 O.OOOE+OO O.OOOE+OO 2.339E+Ol O.OOOE+OO 3.146E-01 5.683E-02 4.925E+OO 3.240E-02 O.OOOE+OO 7.353E+02 O.OOOE+OO 2.257E-02 6.952E-02 1. 684E-01 l.090E-01 l.186E-01 1.576E+OO 3.931E-02 3.00lE+Ol 2.161E-01 7.206E-02 2.091E-02 3.504E+00 7.998E-01 3.393E+OO 2.420E+Ol NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3528 of 5809 9.332E+Ol 3.699E-01 2.185E+OO 3. 872E-02 6.036E+OO 3.790E-01 6.584E-01 6.844E-01 3.415E-01 5.161E-01 2.166E-01 2.166E-01 4.103E-01 5.161E-01 5.293E-02 2.198E-01 5.067E+00 l.489E+OO 1. 822E-01 5.293E-02 O.OOOE+OO 1.489E+OO 2.348E-01 3.303E+02 1. 674E-01 8.855E-02 7.124E-02 3.388E-02 3.921E-02 1.082E-01 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. .FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:08:57.24 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235027.CNF;l * *Acquisition date 3-0CT-2016 09:08:01 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 8-DEC-2015 10:19:00 Nuclide Library : SOLID *
  • Sample ID G405235027 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity 1.5855E+02 GRAM *
  • Quantity Err(%) 1.2614E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;14
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.404E+Ol 1. 750E+OO 1. 750E+OO CD-109 1.433E+OO 1.994E+OO 1.994E+OO SN-126 9.134E-02 1. 2 69E-01 1.269E-01 TL-208 3.567E-01 9.562E-02 9.562E-02 PB-212 9. 631E-01 l.425E-01 l.425E-01 BI-214 8.536E-01 1. 941E-01 1. 941E-01 PB-214 7.858E-01 l.893E-01 1. 893E-01 RN-222 8.536E-01 1. 941E-01 1. 941E-01 RA-224 6.650E-01 1.456E+OO 1.456E+OO RA-226 8.536E-01 1.941E-01 1,941E-01 AC-228 8.645E-01 3. 851E-01 3.851E-01 RA-228 8.645E-01 3.851E-01 3.851E-01 TH-228 9. 631E-01 1.425E-01 1.425E-01 TH-230 8.533E-01 l.940E-01 l.940E-01 PA-231 9. 521E-01 9.945E-01 9.945E-01 TH-232 8.645E-01 3.851E-01 3.851E-01 U-234 8.533E-01 1. 940E-01 1.940E-01 AM-243 1.870E-01 l.226E-01 1.226E-01 ANH-511 1.215E-01 1. 096E-01 1. 096E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM * ( 1 . 9 6-sigma ) ( 1. 96-sigma) BE-7 6.504E+00 1.145E+Ol 1.182E+Ol NOT IDENT. NA-22 4.213E-02 4.339E-02 4.737E-02 NOT IDENT. NA-24 l.OOOE+41 5.665E+41 O.OOOE+OO SHORT HLIF AL-26 2.021E-02 3.846E-02 3.952E-02 NOT IDENT. SC-46 -2.279E-01 3.906E-01 4.039E-01 FAIL ABUN V-48 -6.902E+02 l.140E+04 1.141E+04 SHORT HLIF CR-51 2.475E+02 4.417E+02 4.556E+02 SHORT HLIF MN-54 2.085E-02 6.875E-02 6.939E-02 NOT IDENT. C0-56 2.340E-01 4.576E-01 4.696E-01 NOT IDENT. MN-56 1.000E+41 l.941E+41 O.OOOE+OO SHORT HLIF C0-57 -1.607E-02 5.054E-02 5.106E-02 NOT IDENT. Page 3529 of 5809 C0-58 2.274E-01 5.282E-01 5.381E-01 NOT IDENT. FE-59 -8.323E-01 6.966E+00 6.976E+OO NOT IDENT. C0-60 -2.168E-02 4.227E-02 4.338E-02 FAIL ABUN ZN-65 -l.915E-02 2.638E-01 2.639E-01 NOT IDENT. GE-68 1.983E+OO 2.632E+OO 2.780E+OO NOT IDENT. AS-73 -6.587E+OO 1.314E+Ol 1. 34 7E+Ol NOT IDENT. AS-74 -7.177E+02 7.045E+03 7.053E+03 SHORT HLIF SE-75 l.870E-01 2.152E-01 2. 311E-01 NOT IDENT. BR-77 1. 795E+38 l.554E+39 O.OOOE+OO SHORT HLIF SR-82 6.165E+02 6.195E+02 SHQRT HLIF RB-83 4 .196E-01 7. 621E-01 7.852E-01 NOT IDENT. KR-85 3.660E+OO 7.484E+OO 7.664E+OO NOT IDENT. SR-85 3.810E-01 7.909E-01 8.094E-01 NOT IDENT. RB-86 1.391E+04 3.471E+04 3.527E+04 SHORT HLIF Y-88 -8.357E-02 2.284E-01 2.315E-01 NOT IDENT. Y-91 -2.909E+02 5.702E+02 5.851E+02 NOT IDENT. NB-94 2.014E-02 3.429E-02 3.547E-02 NOT IDENT. NB-95 -8.599E-01 1.000E+OO 1.073E+OO NOT IDENT. NB-95M -2.035E+OO 2.813E+OO 2.959E+OO NOT IDENT. ZR-95 2.936E-01 1.234E+OO 1.241E+OO NOT IDENT. NB-97 -1.000E+41 4.063E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1. 307E+41 O.OOOE+OO SHORT HLIF M0-99 -1.083E+32 1.892E+32 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 2.129E+41 O.OOOE+OO SHORT HLIF RH-101 9 .131E-03 3.693E-02 3. 716E-02 NOT IDENT. RH-102 l.055E-02 6.795E-02 6.812E-02 NOT IDENT. RU-103 4.992E-01 5.610E+OO 5.615E+OO FAIL ABUN RH-106 -8.768E-02 5.711E-01 5.724E-01 NOT IDENT. RU-106 -8.768E-02 5. 711E-01 5.724E-01 NOT IDENT. AG-108M 6.716E-03 2.641E-02 2.658E-02 NOT IDENT. AG-llOM -3.887E-02 8.709E-02 8.884E-02 NOT IDENT. SN-113 1.470E-01 2.613E-01 2.695E-01 NOT IDENT. CD-115 -1. 921E+39 3.805E+39 O.OOOE+OO SHORT HLIF SN-117M -7.708E+04 1.066E+05 1.121E+05 SHORT HLIF TE-123M -9.638E-03 1.360E-01 1.361E-01 NOT IDENT. SB-124 7.086E-02 1. 721E+OO 1. 721E+OO NOT IDENT. SB-125 -3.865E-02 1.082E-01 1. 096E-01 NOT IDENT. TE-125M 1.640E+Ol 3.259E+02 3.260E+02 NOT IDENT. I-126 8.055E+05 7.774E+05 8.580E+05 SHORT HLIF SB-126 1.356E+06 1.405E+06 1.533E+06 SHORT HLIF SB-127 -1. 77 9E+22 3.212E+22 O.OOOE+OO SHORT HLIF I-131 2.690E+09 5.045E+09. 5.189E+09 SHORT HLIF I-132 l.000E+41 1.850E+42 O.OOOE+OO SHORT HLIF TE-132 2.099E+26 4.394E+26 O.OOOE+OO SHORT HLIF BA-133 8.272E-03 4.338E-02 4.354E-02 FAIL ABUN I-133 -l.000E+41 7.469E+41 0.000E+OO SHORT HLIF CS-134 6.493E-02 6.040E-02 6.712E-02 NOT IDENT. CS-135 l.302E-02 1.510E-01 1. 511E-01 NOT IDENT. I-135 -1.000E+41 6.858E+41 O.OOOE+OO SHORT HLIF CS-136 8.062E+04 3.150E+05 3 .171E+05 SHORT HLIF BA-137M 5.530E-02 4.190E-02 4.875E-02 NOT IDENT. CS-137 5.842E-02 4.426E-02 5.150E-02 NOT IDENT. CE-139 4.175E-02 1.270E-01 1.284E-01 NOT IDENT. BA-140 l.265E+06 l.418E+06 l.529E+06 SHORT HLIF LA-140 -4.856E+05 4.898E+05 5.365E+05 SHORT HLIF CE-141 -8.205E+OO 2.795E+Ol 2.819E+Ol NOT IDENT. CE-143 1.000E+41 1.867E+41 O.OOOE+OO SHORT HLIF CE-144 7.581E-03 3.674E-01 3.674E-01 NOT IDENT. PM-144 9.004E-03 6.254E-02 6.267E-02 NOT IDENT. PR-144 7.316E-01 5.425E+OO 5.435E+OO NOT IDENT. PM-146 -4.860E-02 4.529E-02 5. 031E-02 NOT IDENT. ND-147 1.296E+07 3.517E+07 3.565E+07 SHORT HLIF PM-147 1.708E+02 8.259E+02 8.294E+02 NOT IDENT. PM-149 -4.055E+40 5.102E+40 O.OOOE+OO SHORT HLIF EU-150 -3.078E-03 2.875E-02 2.878E-02 FAIL ABUN EU-152 -2. 251E-02 9.158E-02 9.214E-02 NOT IDENT. GD-153 -2.881E-02 1.927E-01 1.931E-01 NOT IDENT. EU-154 1.033E-01 1.064E-01 1.161E-01 NOT IDENT. EU-155 1. 34 7E-01 l.237E-01 1.378E-01 FAIL.ABUN TB-160 -8.125E-01 1. 960E+OO 1.994E+OO FAIL ABUN H0-166M -2.912E-02 4. 960E-02 5.131E-02 NOT IDENT. TM-171 -3.054E+OO 3.295E+Ol 3.298E+Ol NOT IDENT. HF-172 -5.277E-02 2.761E-01 2. 771E-01 FAIL ABUN LU-172 -1.452E-02 8.555E-02 8.580E-02 FAIL ABUN LU-176 -l.481E-03 2.347E-02 2.348E-02 FAIL ABUN HF-181 -3.218E-01 4.122E+OO 4.124E+OO NOT IDENT. TA-182 -1.921E-02 9.545E-01 9.546E-01 FAIL ABUN RE-183 -2.253E+OO 3.920E+OO 4.050E+OO NOT IDENT. Page 3530 of 5809 RE-184 -2.091E+Ol 3.356E+Ol 3.486E+Ol NOT IDENT. W-188 -1.239E+02 1.335E+02 1.447E+02 NOT IDENT. IR-192 -5.255E-01 4.760E-01 5.317E-01 FAIL ABUN HG-203 -9. 311E-01 2.516E+OO 2.550E+00 NOT IDENT. BI-207 -2.076E-02 4. 968E-02 5.055E-02 FAIL ABUN PB-210 3.177E+OO 6.249E+OO 6.411E+OO NOT IDENT. BI-211 2.165E+OO 5.227E-01 l.107E+OO FAIL ABUN PB-211 5.463E-01 6.838E-01 7.268E-01 NOT IDENT. BI-212 1.426E+OO l.031E+OO l.215E+OO FAIL ABUN RN-219 1.594E-01 3.687E-01 3.756E-01 NOT IDENT. RA-223 2.525E-01 6.155E-01 6.259E-01 FAIL ABUN AC-227 5.033E-02 2.331E-01 2.342E-01 FAIL ABUN TH-227 5.033E-02 2.331E-01 2.342E-01 FAIL ABUN TH-229 -1.659E-01 4.541E-01 4.603E-01 FAIL ABUN TH-231 2.525E-01 6.155E-01 6.259E-01 FAIL ABUN PA-233 l.298E-02 5.757E-02 5.787E-02 FAIL ABUN PA-234 -3.659E-02 2.651E-01 2.656E-01 NOT IDENT. PA-234M 4.681E+OO 6.681E+OO 7.007E+OO FAIL ABUN TH-234 -8. 951E-01 1.658E+OO 1.707E+OO FAIL ABUN U-235 -l.495E-02 2.094E-01 2.095E-01 FAIL ABUN NP-237 1.298E-02 5.757E-02 5.787E-02 FAIL ABUN NP-238 1.000E+41 3.059E+41 O.OOOE+OO SHORT HLIF U-238 -8. 951E-01 1.658E+OO l.707E+OO FAIL ABUN NP-239 4.169E-02 2.647E-01 2.654E-01 NOT IDENT. .PU-239 5.725E+02 6.104E+02 6.628E+02 FAIL ABUN AM-241 1.133E-01 1.734E-01 1.807E-01 NOT IDENT. CM-243 -7.545E-02 l.078E-01 1.130E-01 NOT IDENT. BK-247 5. 725E-02 7.384E-02 7.822E-02 FAIL ABUN CM-247 2.614E-02 3.561E-02 3.751E-02 NOT IDENT. CF-249 1.604E-02 4.281E-02 4.342E-02 NOT IDENT. CF-251 -1.970E-02 1.170E-01 1.173E-01 NOT IDENT. Page 3531 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 48.7462 87.09 107.2032 136.47 64.4216 45.60 68.0586 87.57 98.4812 140.51 0.0000 46.54 66.2352 88.03 86.0623 143.76 74.7101 49. 72 0.0000 88.34 86.1123 144.24 71.1410 51. 35 68.1366 88.47 86.1331 145.44 82.1248 51.87 71.2863 89. 96 86.3730 152.43 63.3821 52.39 65.2659 1093.63 90.1777 153.25 0.0000 52.97 68.4295 91.11 0.0000 323.87 70.8574 53.44 66.4684 92.59 99. 0311 156.02 0.0000 54.07 68.6258 93.35 99.1683 158.56 0.0000 57.36 0.0000 94.56 68.4899 159.00 58.9988 57.53 77.4974 94.65 68.5007 162.33 77.7589 57.98 71. 3771 94. 67 68.5035 162.66 0.0000 59.27 58.1129 94.87 68.5278 163.33 63.0255 59.32 58.1202 97.43 72. 9554 165.86 66.9405 59.54 58.1512 98.43 68.5859 176.31 62.7602 60. 96 87.5264 98.44 68.5873 176.60 0.0000 61.17 90.6978 99.53 68.7176 177.52 67.8766 62.93 78.5145 100 .11 75.5524 181.07 0.0000 63.29 89.0581 102.03 74.6705 181.52 58.0889 63.58 83.8760 103.18 72.5488 184.41 63.3484 64.28 86.1129 103.37 75.9741 143.76 63.4422 66.73 89.7652 105.21 64.8352 193.51 62.2866 67.24 91. 9828 105.31 63.7084 197.03 59.9562 125.81 85.7238 106.12 66.0726 198.01 60.0195 67.75 81. 5029 106.47 75.2299 201.83 67.1526 69.67 80.7883 109.28 73.2876 203.43 64.6797 70.83 93.7813 111. 00 67.7502 205.31 71. 2887 72.81 88.4735 111.76 0.0000 210.85 56.0563 72.87 88.4848 114.06 68.0819 215.65 61.1354 74.66 95.6258 116. 30 0.0000 222 .11 60.6537 74.82 95.6578 116.74 67.2099 227.09 64.4847 74.97 95.6876 119.76 57.0462 227.38 63. 6196 77 .11 96 .1134 121.12 54. 8311 228.16 0.0000 78.74 85.2374 121. 22 54.8397 228.18 54.8258 79.69 88. 2962 121.78 58.3893 116.74 54.8258 80.12 67.3655 122.06 67.7603 235.69 72.1464 80.19 0.0000 122.92 69.0182 235.96 64.1470 80.57 67.4265 123.07 65.5233 238.63 55. 3771 81. 00 82.7226 265.00 67.9258 238.98 0.0000 81. 07 89.9916 125.81 73.6240 240.99 55.5000 81. 75 82.8455 127.23 58.0801 242.00 55.5524 83.79 97.7704 127.91 73.8515 244.70 55.6918 84.00 97.8106 129.30 63.7666 252.40 0.0000 85.43 83.4416 131. 20 50.5221 252.80 45.6083 86.55 95.3570 133.02 55.4024 254.15 0.0000 86.79 95.4000 133. 52 57.0264 256.23 44.4780 86.94 95.4277 136.00 60.8030 260.90 0.0000 Page 3532 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 36.5804 355.39 0.0000 584.27 17.9180 264.80 39.3283 356.01 26.5155 595.83 0.0000 265.00 35.6762 364.49 0.0000 427.87 25.9574 268.22 50.4536 366.42 0.0000 602.52 0.0000 269.46 39.4875 372.51 32.7784 604.72 11. 8732 270.03 44.1016 375.05 31. 8405 607.14 271.23 43.2268 377.52 26.9099 609.32 14.7313 273.65 0.0000 356.01 33.0289 610.33 14.7387 276.40 30.4850 388.16 33.1229 614.28 8.5184 277.37 40.6798 388.63 0.0000 618.01 15.9283 277.60 45. 3114 391.69 24.1450 620. 36 20.5020 278.00 42. 5513 264.66 18.2142 621.93 21. 6564 279.20 40.7424 401.81 22.2784 630.19 0.0000 279.54 41.6803 402.40 22.2865 631.29 15.4528 279.70 46.3175 404.85 22.3214 633.25 13.7480 280.46 40.7854 410.95 22.4078 634.78 0.0000 283.69 29.7422 413.71 18.3655 635.95 24.0881 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 46.5383 423.72 0.0000 645.85 27.6514 285.90 0.0000 427.09 28.8061 657.76 15.6357 287.50 41.0244 427.87 28.8197 657.90 0.0000 290.67 53.2833 433.94 19.6285 661. 66 12.1821 293.27 0.0000 439.40 19.6927 664.57 0.0000 ' 351. 93 28.1476 453.88 666.33 0.0000 295.96 28.1641 463.37 25.2271 666.50 0.0000 879.38 22.5786 468.07 30.0377 667. 71 0.0000 299.98 39.5570 473.00 0.0000 677.62 17.5226 300.09 39.5604 475.06 22. 2211 685.70 0.0000 300.13 39.5613 476.78 16.9466 695.00 0.0000 301.36 39.6006 477.60 14.8351 696.49 22.0787 302.85 38.2308 482.18 19.1224 696. 51 22.0795 256.23 46.7879 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 26.5036 306.78 34.0884 497.08 17.1377 697.49 26.5054 308.46 37.9256 505.52 11.2981 702.65 17.7087 311. 90 31.3726 507.63 0.0000 706.68 20.3987 316.51 45.7949 511. 00 22.6626 711. 68 15.9972 319.41 0.0000 514.00 22.6987 720.70 0.0000 320.08 0.0000 514.00 22.6987 721. 93 0.0000 321. 04 38.2943 520.40 19.5220 722. 78 25.7115 323.87 24.4650 520.69 0.0000 722. 91 25.7133 325.23 17.2870 522.65 0.0000 723. 31 25.7177 328.76 0.0000 527.90 0.0000 724 .19 20.0095 333.37 36.7162 528.26 25.0468 727.33 15.2050 333.97 36.2488 529.59 23.9748 733.00 24.3835 334.37 42.0610 529.87 0.0000 735.93 16.1554 338.28 39.7580 531.02 0.0000 333.97 14.3691 338.32 39.7588 537.26 0.0000 739.50 0.0000 311. 90 39.8214 546.56 0.0000 747.24 19.8348 340.48 39.8214 552.55 19.8464 748.06 18.0371 340.55 0.0000 563.25 18.8442 752.31 11. 7 440 344.28 26.2958 569.33 25.5708 753.82 0.0000 345.93 30.2274 946.00 25.5736 756.73 9.9543 351.06 28.3805 569.70 23.3516 756.80 9.9547 351. 93 28.3982 583.19 17.9089 884.68 13. 6125 Page 3533 of 5809 ENERGY MDA COUNTS ENERGY MDA c;:OUNTS ENERGY MDA COUNTS 765.81 29.9687 1274.44 3.9359 1620.50 3.6908 766.42 21.8005 1001.03 10.8399 1621.92 0.0000 766.84 19. 9872 1002.74 18.9305 1678.03 0.0000 772.60 0.0000 1004.73 17.3637 1690.97 2.8085 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 .2. 8500 778.90 13.6913 1028.54 0.0000 1063.66 12.3633 783.70 0.0000 1037.84 13.9530 1771.35 2.8538 785.37 11.8947 1038.76 0.0000 1791.20 0.0000 792.07 14.6772 631.29 4.9966 1808.65 3.8324 794.95 17.6314 1048.07 0.0000 1810.72 0.0000 795.86 15.6169 1049.04 13.0008 1836.06 4.8157 810.06 12.0058 1050.41 14.0068 810.29 10.1594 1063.66 14.0624 344.28 10.1601 1077.00 0.0000 810.76 9.2374 1077.34 9.2204 815.77 0.0000 1085.87 12.1326 1048.07 0.0000 1093.63 13.1730 832.01 16.3851 1099.45 12.1802 834.85 11.9289 1112. 07 17.9298 835.71 14.9155 1112. 84 22.8252 836.80 0.0000 1115. 54 21.2113 846.75 0.0000 1120.29 15.3168 8'46.77 10.2954 1120.55 15.3177 856.80 0.0000 1221. 41 14.7085 860.56 9.4055 1129. 67 10.2386 871.09 13.2164 1131. 51 0.0000 873.19 18.8947 1147.95 0.0000 875.33 0.0000 1173.23 10.3638 879.38 16.0947 1177.95 13.2828 880.51 11.3654 1189.05 9.3675 883.24 12.3244 1204.77 15.6793 884.68 11. 3818 1221.41 12.5991 889.28 16.1502 1231.02 15.7892 894.76 18.0839 1235.36 0.0000 898.04 11. 4342 1238.28 8.4370 900. 72 14.3060 1260.41 0.0000 903.28 17.4548 1271.87 9.5746 911.20 14.3568 1274.44 4.2583 912.08 14.3610 1274.54 4.2583 923.98 0.0000 1291.59 9.6229 926.50 8.6583 1298.22 0.0000 92 9 .11 14.4429 1312 .11 0.0000 937.49 13.5176 1332.49 9.7224 944 .13 0.0000 1362.66 0.0000 946.00 11. 6191 1365.19 5.4446 949.00 12.5997 1368.63 0.0000 667. 71 0.0000 1384.29 6.5636 962.31 11. 6807 1408.01 7.7007 964. 08 15.5830 1457.56 0.0000 966 .17 20.7917 1460.82 8.9097 911.20 16.7228 1489.16 2.2418 968. 97 16.7228 1505.03 2.2498 983.53 0.0000 1584.12 14.6500 984.45 0.0000 1596.21 0.0000 Page 3534 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:09:27.24 ********************************************************************************
  • 4 GEL Laboratories LLC i *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM09.CNF;335 Background date : Z-OCT-2016 11:00:29. Sample date 23-NOV-2015 14:50:00 Acquisition date : 3-0CT-2016 09:08:29. Sample ID G405235028 Sample quantity 1.25516E+02 GRAM Detector name : GAM09 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.50 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 5 5 2 2 0 0 0 0 0 0

0 0 2 2 0 0 0 2 2 0 0 2 2 0 0 0 8 8 0 0 0 0 0 0 Page 3535 of 5809 Energy 63.45* 66.17* 75.00 77 .13 87.01 92.87* 106.39 119. 81 129.51 143.90* 186.28* 209.07 238. 72* 241.86 252.87 271.22 295.22* 300.05 301.81 310.57 338.61* 351.87* 354.59 438.55 463. 64 478.15* 510.76* 516.91 528.48 558.41* 564.80 578.37 583.01* 609.05* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 46 22 99 148 36 71 23 17 25 28 52 76 400 95 17 26 132 43 18 20 61 230 25 10 25 14 23 17 8 14 37 11 119 182 60 106 123 96 162 126 48 78 115 86 156 95 67 55 52 77 44 40 44 13 78 25 15 14 46 18 30 16 13 11 33 12 14 13 1.18 1. 34 1. 03 0.90 1. 27 0.94 1. 36 1. 33 0.56 1. 04 1. 07 1. 25 1. 01 1. 33 1. 06 3.19 1. 06 1. 41 1. 41 1. 32 1. 09 1. 08 1. 47 0. 72 1. 00 0.63 2.90 1. 99 1. 60 1. 80 8.03 0.66 1. 62 1. 22 126.57 132.01 149.68 153.94 173.71 185.45 212.49 239.35 258.74 287.53 372. 33 417.93 477.25 483.54 505.57 542.28 590.30 599.98 603.49 621. 03 677.12 703.66 709.11 877.10 927.29 956.32 1021. 58 1033.88 1057.04 1116.93 1129.72 1156.86 1166.15 1218.25 124 124 146 146 171 182 210 236 254 284 367 412 472 472 501 536 585 596 596 619 672 698 698 874 921 951 1015 1015 1052 1114 1121 1150 1160 1211 13 1.26E-02 13 6.21E-03 14 2.74E-02 14 4. llE-02 7 9.87E-03 8 1. 96E-02 5 6.35E-03 7 4.81E-03 10 6.94E-03 8 7.69E-03 11 1.46E-02 13 2.lOE-02 16 1. llE-01 16 2.64E-02 8 4.69E-03 11 7. 35E-03 11 3. 66E-02 14 1.19E-02 14 4.87E-03 5 5.64E-03 12 1.68E-02 15 6.39E-02 15 6.92E-03 7 2.78E-03 12 7.02E-03 10 3.99E-03 23 6.50E-03 23 4.60E-03 7 2.28E-03 7 3.95E-03 21 l.03E-02 10 2.93E-03 11 3. 32E-02 13 5.05E-02 31. 4 1.14E+OO 85.3 19.9 2.89E+OO 12.9 61. 6 32.l 51.1 87.5 82.7 62.4 50.5 28.8 5.9 2.09E+OO 18.9 77.9 67.1 13 .2 30.7 l.09E+OO 75.5 34.9 31. 8 7.4 4.86E-01 37.7 69.6 56.8 62.1 67.7 l.65E+OO 49.8 82.4 51. 0 41. 5 69.9 11. 2 8. 7 Peak Search Report (continued) Page : 2 Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 613.75 7 14 0.89 1227.64 1223 6 2.06E-03 86.5 36 0 650 .11 10 14 1. 37 1300.41 1295 8 2.82E-03 70.9 37 0 66J.. 42 40 29 1.10 1323.03 1318 u 1. llE-02 30.2 38 0 703.29 18 14 1. 79 1406.82 1401 10 5.05E-03 45.8 39 0 727.30 41 15 1. 48 1454.86 1449 13 1.15E-02 25.1 40 0 763.48 10 7 0.57 1527.25 1524 6 2. 71E-03 54.4 41 0 772.21 13 18 0.52 1544.73 1538 10 3.67E-03 68.0 42 0 786.69 27 7 3.56 1573.70 1568 13 7.36E-03 27.8 43 0 794.71 19 20 3.02 1589.74 1585 11 5.32E-03 50.1 44 0 906.46 10 8 0.54 1813.34 1806 10 2.83E-03 59.5 45 0 910.92* 61 10 1. 51 1822.27 1818 10 l.70E-02 16.7 46 0 928.71 11 10 3.73 1857.87 1850 13 3.15E-03 64.0 47 0 933.91 22 5 1. 90 1868.28 1863 10 6.17E-03 28.3 48 0 969. 07 60 8 1. 31 1938.63 1933 13 1. 67E-02 16.6 49 0 1003.12 15 19 2.89 2006.77 2000 13 4.04E-03 71. 4 50 0 1078.97* 15 6 3.30 2158.55 2152 11 4.09E-03 41. 6 51 0 1097.54 7 6 0.75 2195.69 2191 8 2.02E-03 68.8 52 0 1119. 96 39 6 1. 88 2240.55 2235 12 1.08E-02 20.4 53 0 1124.78 10 4 0.83 2250.21 2247 7 2.64E-03 46.0 54 0 1138. 08 4 16 0.45 2276.82 2271 12 l.24E-03180.2 55 0 1156.29 13 '20 3.87 2313.25 2302 16 3.74E-03 79.0 56 0 1180.73 10 12 0.61 2362.16 2356 9 2.66E-03 75.5 57 0 1378.46 7 6 1. 23 2757.82 2752 8 1. 92E-03 72. 2 58 0 1460.16* 313 0 1. 95 2921. 32 2914 15 8.69E-02 5.7 59 0 1587.68 6 5 0.87 3176.50 3169 10 1. 67E-03 80.8 60 0 1763.90* 30 0 2.05 3529.12 3521 15 8.22E-03 19.8 Flag: "*" = Peak area was modified by background subtraction Page 3536 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:09:29 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 23-NOV-2015 14:50:00 G405235028 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:08:29 125.52 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA9 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3537of5809 PB-214 PB-214 PB-214 PB-214 PB.:..214 PB-214 PB-214 PB-214 PB-214 Line 87.09 87.09 87.09 87.09 242.00 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide EU-155 SN-126 SN-126 CD-109 RA-224 AM-243 TH-228 PB-212 BI-211 Line 86.55 86.94 87.57 88.03 240.99 74.66 74.82 74.82 351.06 CAN 0 01:00:00.50 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status BE-7 477.60 10.44* 2.792E+OO .2. 997E-01 1.808E+Ol 124.28 OK K-40 1460.82 10.66* l.146E+OO 1.455E+Ol 1.455E+Ol 11. 45 OK CD-109 88.03 3.70* 4.842E+OO 3.338E-01 5.357E-01 497.78 OK SN-126 64.28 9.60 2.286E+OO 1.416E+OO 1.416E+OO 62. 78 OK 86.94 8.90 4.842E+OO 1.388E-01 1.388E-01 497.78 OK 87.57 37.00* 4.842E+OO 3.338E-02 3.339E-02 497.78 OK BA-137M 661. 66 89.90* 2.157E+OO 1.226E-01 l.250E-01 60.39 OK CS-137 661.66 85.10* 2.157E+00 l.295E-01 1.321E-01 60.39 OK PM-147 121.22 0.00* 6.261E+OO 6.398E+02 8.035E+02 175.07 OK EU-155 86.55 30.70 4.842E+OO 4.024E-02 4.563E-02 497.78 OK 105.31 21.10* 5.939E+OO l.210E-01 1.373E-01 102.30 OK TL-208 277.37 6.60 4.352E+OO Line Not Found Absent 583.19 85.00* 2.382E+OO 3.546E-01 3.546E-01 22.39 OK 860.56 12.50 1. 758E+OO Line Not Found Absent BI-211 72.87 1. 23 3.448E+OO Line Not Found Absent 351.06 12.92* 3.589E+OO 9.525E-02 9.525E-02 958.15 OK BI-212 727.33 6.67* 2.003E+OO 1.843E+OO l.843E+00 50.28 OK 785.37 1.10 1.885E+OO 7.548E+00 7.548E+OO 55.52 OK 1620.50 1. 47 l.045E+OO Line Not Found Absent PB-212 74.82 10.28 3.689E+OO l.148E+00 1.148E+OO 62.52 OK 77 .11 17.10 3.920E+OO 1.490E+OO 1.490E+OO 25. 72 OK 238.63 43.60* 4. 881E+OO 1.192E+OO l.192E+OO 11. 89 OK 300.09 3.30 4.087E+OO 1.991E+OO 1. 991E+OO 61. 31 OK BI-214 609.32 45.49* 2.302E+OO 1.041E+OO 1.041E+OO 17.44 OK 1120.29 14.92 1.429E+OO 1.057E+OO 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 l.123E+OO 1.124E+OO 39.59 OK PB-214 74.82 5.80 3.669E+OO Line Not Found <<INT Reject 77 .11 9.70 3.920E+00 2.627E+00 2.628E+OO 25. 72 OK 87.09 3.41 4.849E+OO Line Not Found <<INT Reject 242.00 7.25 4.832E+OO Line Not Found <<INT Reject 295.22 18.42 4 .141E+OO 1.082E+OO 1.083E+OO 26. 47 OK 351.93 35.60* 3.588E+00 Line Not Found <<INT Reject RN-222 609.32 45.49* 2.302E+OO 1. 041E+OO 1.041E+OO 17.44 OK 1120.29 14.92 1. 429E+OO 1.057E+OO 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 l.123E+OO 1.124E+OO 39.59 OK RA-224 240.99 4.10* 4.834E+OO l.125E+OO 1.125E+OO 111. 80 OK RA-226 609.32 45.49* 2.302E+OO 1.041E+OO l.041E+00 17.44 OK 1120.29 14.92 1.429E+OO 1.057E+OO 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 l.123E+OO 1.124E+OO 39.59 OK AC-228 105.21 1.10 5.939E+00 2.322E+00 2.322E+OO 102.30 OK 338.32 11. 27 3.704E+OO 9.016E-01 9.016E-01 63.62 OK 794.95 4.25 l.870E+00 l.422E+00 1.422E+OO 100.12 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 OK 968. 97 15.80 1.603E+OO l.383E+00 1.383E+OO 33.25 OK RA-228 105.21 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 OK 338.32 11.27 3.704E+00 9.016E-01 9.016E-01 63.62 OK 794.95 4.25 1. 870E+00 1.422E+OO 1.422E+OO 100.12 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent Page 3538 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status 911. 20 25.80* 1.682E+OO 8.265E-01 8.265E-01 OK 968. 97 15.80 1.603E+OO 1.383E+OO 1.383E+OO 33.25 OK TH-228 74.82 10.28 3.689E+OO l.148E+OO l.148E+OO 62.52 OK 77 .11 17.10 3.920E+OO 1.490E+OO 1.490E+OO 25.72 OK 238.63 43.60* 4.881E+OO 1.192E+OO 1.192E+OO 11. 89 OK 300.09 3.30 4.087E+OO 1.991E+OO 1.991E+OO 61. 31 OK TH-230 609.32 45.49* 2.302E+00 1.041E+OO 1. 041E+OO 17.44 OK 1120.29 14.92 1.429E+00 1.057E+OO l.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 l.123E+OO 1.123E+OO 39.59 OK PA-231 283.69 1. 70 4.275E+OO Line Not Found Absent 301.36 5.35* 4.068E+OO 5.038E-01 5.038E-01 150.97 OK TH-232 105.21 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 OK 338.32 11. 27 3.704E+OO 9.016E-01 9.016E-01 63.62 OK 835.71 1. 61 1. 799E+OO Line Not Found Absent 911. 20 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 OK 968.97 15.80 1.603E+OO 1.383E+OO l.383E+OO 33.25 OK PA-233 300.13 6.63 4.087E+OO 9.909E-01 9.909E-01 61. 31 OK 311.90 38.50* 3.975E+OO 8.293E-02 8.293E-02 69.73 OK 340.48 4.45 3.687E+OO -----Line Not Found Absent TH-234 63.29 3.70* 2.286E+OO 3.673E+OO 3.673E+OO 62.78 OK 92.59 4.23 5.269E+OO 2.122E+OO 2.122E+OO 64.22 OK U-234 609.32 45.49* 2.302E+OO l.041E+OO 1. 041E+OO 17.44 OK 1120.29 14.92 1.429E+OO 1.057E+OO 1.057E+OO 40.70 OK 1764.49 15.30 9.659E-01 1.123E+OO 1.123E+OO 39.59 OK U-235 89.96 3.47 5.068E+OO Line Not Found Absent 93.35 5.60 5.269E+OO l.603E+OO 1.603E+OO 64.22 OK 143.76 10. 96* 6.310E+OO 2.613E-01 2. 613E-01 124.72 OK 163.33 5.08 6. 096E+OO Line Not Found Absent 185.72 57.20 5.735E+OO 1.027E-01 1. 027E-01 101.07 OK 205.31 5.01 5.415E+OO Line Not Found Absent U-238 63.29 3.70* 2.286E+OO 3.673E+OO 3.673E+OO 62. 78 OK 92.59 4.23 5.269E+OO 2.122E+OO 2.122E+OO 64.22 OK AM-243 43.53 5.90 1. 969E-01 Line Not Found Absent 74.66 67.20* 3.689E+OO 1.756E-01 1. 757E-01 62.52 OK ANH-511 511. 00 100.00* 2.647E+OO 5.361E-02 5.361E-02 135. 49 OK Flag: "*" = Keyline Page 3539 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:09:30.25 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l * *Acquisition date 3-0CT-2016 09:08:29 Sensitivity : 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:50:00 Analyst initials: MXRl *
  • Sample ID G405235028 Sample Quantity 1.2552E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-s igma) (pCi/GRAM BE-7 1.808E+Ol 2.202E+Ol 2.537E+Ol K-40 1.455E+Ol l.633E+00 5.780E-01 CD-109 5.357E-01 2.613E+OO 2.642E+OO SN-126 3.339E-02 1.629E-01 l.567E-01 BA-137M 1.250E-01 7.400E-02 6.889E-02 CS-137 1.321E-01 7.818E-02 7.278E-02 PM-147 8.035E+02 1. 37 9E+03 1. 471E+03 EU-155 1.373E-01 1. 37 6E-01 l.936E-01 TL-208 3.546E-01 7.780E-02 5.179E-02 BI-211 9.525E-02 8.943E-01 2. 961E-01 BI-212 1.843E+OO 9.080E-01 8.217E-01 PB-212 1.192E+00 l.388E-01 1.019E-01 BI-214 1.041E+OO 1. 780E-01 1.173E-01 PB-214 l.117E+00 l.628E-01 3.643E-01 RN-222 1.041E+OO 1. 780E-01 1.173E-01 RA-224 1.125E+OO 1. 232E+OO 1.092E+OO RA-226 1.041E+OO 1. 780E-01 1.173E-01 AC-228 8.265E-01 2.699E-01 2.702E-01 RA-228 8.265E-01 2.699E-01 2.702E-01 TH-228 1.192E+OO l.388E-01 1.019E-01 TH-230 1. 041E+OO 1. 779E-01 1.173E-01 PA-231 5.038E-01 7.453E-01 7.462E-01 TH-232 8.265E-01 2.699E-01 2.702E-01 PA-233 8.293E-02 5.667E-02 9.811E-02 TH-234 3.673E+OO 2.26dE+OO 2.660E+OO U-234 1. 041E+OO 1. 779E-01 1.173E-01 U-235 2. 613E-01 3.194E-01 3.047E-01 U-238 3.673E+OO 2.260E+OO 2.660E+OO AM-243 1. 757E-01 1. 076E-01 l.018E-01 ANH-511 5.361E-02 7. 119E-02 4.918E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM Page 3540 of 5809 NA-22 1. 756E-02 4.724E-02 1.033E-01 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 -2.615E-02 3.992E-02 6.817E-02 NOT IDENT. SC-46 -1. 364E-01 3.834E-01 7.040E-01 FAIL ABUN V-48 O.OOOE+OO 2.257E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.119E+02 O.OOOE+OO SHORT HLIF MN-54 3.315E-02 6.476E-02 l.373E-01 NOT IDENT. C0-56 -5.328E-02 5.071E-01 9.791E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF C0-57 -l.256E-02 4.967E-02 .S.579E-02 NOT IDENT. C0-58 -1.170E-01 6.807E-01 l.291E+OO NOT IDENT. FE-59 1. 602E+OO 7.670E+OO 1.466E+Ol NOT IDENT. C0-60 -2.154E-03 3.686E-02 7.673E-02 NOT IDENT. ZN-65 9.149E-02 1.921E-01 3.738E-01 NOT IDENT. GE-68 4.253E-01 2.527E+OO 5.191E+OO NOT IDENT. AS-73 4.979E+OO 1.469E+Ol 3.036E+Ol NOT IDENT. AS-74 O.OOOE+OO 1. 023E+04 O.OOOE+OO SHORT HLIF SE-75 -7.611E-02 2.177E-01 3.834E-01 FAIL ABUN BR-77 O.OOOE+OO l.945E+39 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 1.280E+03 0.000E+OO SHORT HLIF RB-83 -3.059E-02 6.694E-01 1. 212E+00 FAIL ABUN KR-85 6.317E+OO 7.064E+OO 1.526E+Ol NOT IDENT. SR-85 7.776E-01 8.727E-01 1.885E+OO NOT IDENT. RB-86 O.OOOE+OO 5.587E+04 O.OOOE+OO SHORT HLIF Y-88 1.465E-01 2.634E-01 6.554E-01 NOT IDENT. Y-91 -5.891E+02 7.282E+02 1.267E+03 NOT IDENT. NB-94 5.270E-02 4.734E-02 7.625E-02 FAIL ABUN NB-95 -1.152E+OO l.662E+OO 2 .151E+OO NOT IDENT. NB-95M 9.905E-01 3.326E+OO 5.763E+OO NOT IDENT. ZR-95 -1.217E+OO 1.834E+OO 3.156E+OO NOT IDENT. NB-97 O.OOOE+OO 1.486E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.540E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 8 .116E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 4.562E-03 3 .112E-02 5.643E-02 NOT IDENT. RH-102 -4.028E-03 5.142E-02 l.020E-01 NOT IDENT. RU-103 -7.032E+OO ' 7. 433E+OO 1.280E+Ol FAIL ABUN RH-106 1.548E-01 5.407E-01 l.101E+OO NOT IDENT. RU-106 l.548E-01 5.407E-01 1.101E+OO NOT IDENT. AG-108M l.214E-02 2.629E-02 5.542E-02 FAIL ABUN AG-llOM 5.191E-02 9.494E-02 2.0BBE-01 FAIL ABUN SN-113 5.300E-02 2. 431E-01 4. 966E-01 NOT IDENT. CD-115 0.000E+OO l.614E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 2.047E+05 O.OOOE+OO SHORT HLIF TE-123M -8.00lE-02 l.355E-01 2.405E-01 NOT IDENT. SB-124 -l.427E+OO 2.073E+OO 3.444E+OO NOT IDENT. SB-125 1. 741E-02 1.128E-01 2.259E-01 FAIL ABUN TE-125M 7.959E+Ol 3.427E+02 6.264E+02 NOT IDENT. I-126 O.OOOE+OO 2.574E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.566E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.398E+23 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 1.842E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.253E+27 O.OOOE+OO SHORT HLIF BA-133 O.OOOE+OO 5.448E-02 6. 917E-02 FAIL ABUN I-133 O.OOOE+OO l.614E+41 O.OOOE+OO SHORT HLIF CS-134 9.440E-02 9.262E-02 1.315E-01 FAIL ABUN CS-135 l.502E-02 l.440E-01 2.481E-01 NOT IDENT. I-135 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 7.482E+05 O.OOOE+OO SHORT HLIF CE-139 -l.851E-02 l .115E-01 2.061E-01 NOT IDENT. BA-140 O.OOOE+OO 2. 611E+06 O.OOOE+OO SHORT HLIF LA-140 0.000E+OO 8.833E+05 O.OOOE+OO SHORT HLIF CE-141 1.848E+Ol 3 .181E+Ol 5.958E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.757E-01 3.593E-01 5.769E-01 NOT IDENT. PM-144 4.00BE-03 6.903E-02 1.327E-01 FAIL ABUN PR-144 3.695E-01 6.046E+OO 1.162E+Ol NOT IDENT. PM-146 6 .*640E-03 3.953E-02 8. llOE-02 NOT IDENT. ND-147 O.OOOE+OO 9.701E+07 O.OOOE+OO SHORT HLIF PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 2.547E-02 2.832E-02 5.375E-02 FAIL ABUN EU-152 -l.123E-03 9.637E-02 l.745E-01 NOT IDENT. GD-153 -1. 396E-01 l.842E-01 3. 311E-01 NOT IDENT. EU-154 4.025E-02 1.144E-01 2. 496E-01 NOT IDENT. TB-160 -1. 721E-01 2.134E+OO 4 .117E+OO FAIL ABUN H0-166M -6.627E-06 5.425E-02 l.067E-01 NOT IDENT. TM-171 -3.799E+Ol 3.069E+Ol 5.512E+Ol FAIL ABUN Page 3541 of 5809 HF-172 -9.466E-02 2. 221E-01 3.752E-01 FAIL ABUN LU-172 8.053E-03 1.025E-01 1.754E-01 FAIL ABUN LU-176 1.258E-03 2.585E-02 4.393E-02 FAIL ABUN HF-181 -2.856E+OO 5.271E+OO 8. 511E+00 NOT IDENT. TA-182 -2.635E-01 1. 203E+OO 2.305E+OO* FAIL ABUN RE-183 -1.317E+OO 4.465E+OO 8. 714E+OO FAIL ABUN RE-184 -1.442E+Ol 4.071E+Ol 6.438E+Ol NOT IDENT. W-188 -4.982E+Ol 1.307E+02 2. 071E+02 FAIL ABUN IR-192 2.345E-01 5.058E-01 9.876E-01 FAIL ABUN -1. 792E+OO 3. 411E+OO 5 . .S06E+00 NOT IDENT. BI-207 -1.288E-02 5.720E-02 1.054E-01 FAIL ABUN PB-210 4.970E+OO 7.193E+OO 1.502E+Ol NOT IDENT. PB-211 l.667E-01 5.689E-01 l.190E+OO NOT IDENT. RN-219 -9.467E-02 3.489E-01 6.765E-01 FAIL ABUN RA-223 -1.686E-01 6.674E-01 1.164E+OO FAIL ABUN AC-227 -l.360E-01 2.527E-01 3.935E-01 FAIL ABUN TH-227 -1. 360E-01 2.527E-01 3.935E-01 FAIL ABUN TH-229 3.335E-02 4.608E-01 8.606E-01 FAIL ABUN TH-231 -1.686E-01 6.674E-01 1.164E+OO FAIL ABUN PA-234 l.703E-01 2.931E-01 6.240E-01 NOT IDENT. PA-234M 3.661E-01 6.507E+OO 1.145E+Ol NOT IDENT. NP-237 8.293E-02 5.667E-02 l.027E-01 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 -1.455E-01 2.759E-01 4.615E-01 FAIL ABUN PU-239 4 .101E+02 6.648E+02 6. 211E+02 FAIL ABUN AM-241 l.354E-02 l.698E-01 3.410E-01 NOT IDENT. CM-243 -5.031E-02 1.030E-01 1. 7 SlE-01 NOT IDENT. BK-247 1.326E-02 6.734E-02 1. 27 6E-01 FAIL ABUN CM-247 -2.270E-02 3.109E-02 5.675E-02 NOT IDENT. CF-249 -l.524E-02 4.413E-02 7.493E-02 FAIL ABUN CF-251 7.SlOE-02 1.124E-01 2.225E-01 NOT IDENT. Page 3542 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:09:27.99 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error BE-7 477.60 15 10.44* 2.792E+OO 2.997E-01 1.808E+Ol 124.28 K-40 1460.82 297 10.66* 1.146E+OO 1.455E+Ol 1.455E+Ol 11. 45 CD-109 88.03 40 3.70* 4.842E+OO 1.331E+OO 2.136E+OO 123.24 SN-126 64.28 52 9.60 2.286E+OO l.416E+OO 1.416E+OO 62.78 86.94 40 8.90 4.842E+OO 5.535E-01 5.535E-01 123.24 87.57 40 37.00* 4.842E+OO 1. 331E-01 1. 331E-01 123.24 BA-137M 661.66 40 89.90* 2.157E+OO 1. 22 6E-01 1.250E-01 60.39 CS-137 661.66 40 85.10* 2.157E+OO l.295E-01 1.321E-01 60.39 PM-147 121. 22 19 0.00* 6.261E+OO 6.398E+02 8.035E+02 175.07 EU-155 86.55 40 30.70 4.842E+OO 1.605E-01 1. 820E-01 123.24 105.31 25 21.10* 5.939E+OO 1.210E-01' 1.373E-01 102.30 TL-208 277.37 ------6.60 4.352E+OO ------Line Not Found ------583.19 120 85.00* 2.382E+OO 3.546E-01 3.546E-01 22.39 860.56 ------12.50 1. 758E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 3.448E+OO ------Line Not Found ------351.06 239 12.92* 3.589E+OO 3.077E+OO 3.077E+OO 14.87 BI-212 727.33 41 6.67* 2.003E+OO 1.843E+OO 1.843E+OO 50.28 785.37 26 1.10 1.885E+OO 7.548E+OO 7.548E+OO 55.52 1620.50 ------1. 47 1.045E+OO ------Line Not Found ------PB-212 74.82 112 10.28 3.689E+OO 1.759E+OO 1.759E+OO 39.77 77 .11 167 17.10 3.920E+OO 1.490E+OO 1.490E+00 25.72 238.63 424 43.60* 4. 881E+OO 1.192E+OO 1.192E+OO 11. 89 300.09 45 3.30 4.087E+OO 1. 991E+OO 1.991E+OO 61. 31 BI-214 609.32 182 45.49* 2.302E+OO 1.041E+OO 1. 041E+OO 17.44 1120.29 38 14.92 1. 429E+OO 1.057E+OO 1.057E+00 40.70 1764.49 28 15.30 9.659E-01 1.123E+OO 1.124E+OO 39.59 PB-214 74.82 112 5.80 3.689E+OO 3 .117E+OO 3 .119E+OO 39.77 77 .11 167 9.70 3.920E+OO 2.627E+OO 2.628E+OO 25.72 87.09 40 3.41 4.842E+OO 1.445E+OO 1.445E+OO 123.24 242.00 101 7.25 4.834E+OO 1.718E+OO 1. 719E+OO 37.88 295.22 138 18.42 4 .141E+OO 1.082E+OO 1.083E+OO 26.47 351.93 239 35.60* 3.589E+OO 1.117E+OO 1.117E+OO 14.87 RN-222 609.32 182 45.49* 2.302E+OO 1. 041E+OO 1.041E+OO 17.44 1120.29 38 14.92 1.429E+OO 1.057E+OO 1.057E+OO 40.70 1764.49 28 15.30 9.659E-01 1.123E+OO 1.124E+OO 39.59 RA-224 240.99 101 4.10* 4.834E+OO 3.039E+OO 3.039E+OO 37.88 RA-226 609.32 182 45.49* 2.302E+OO 1. 041E+OO 1. 041E+OO 17.44 1120.29 38 14.92 l.429E+OO 1.057E+OO 1.057E+OO 40.70 1764.49 28 15.30 9.659E-01 1.123E+OO l.124E+OO 39.59 AC-228 105.21 25 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 338.32 63 11. 27 3.704E+OO 9.016E-01 9.016E-01 63. 62 794.95 19 4.25 1. 870E+OO 1.422E+OO 1.422E+OO 100.12 835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 60 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 968. 97 59 15.80 1.603E+OO 1.383E+OO l.383E+OO 33.25 RA-228 105.21 25 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 338.32 63 11. 27 3.704E+OO 9.016E-01 9.016E-01 63.62 Page 3543 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 19 4.25 l.870E+OO 1.422E+OO 1.422E+OO lOQ.12 835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 60 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 968. 97 59 15.80 1.603E+OO 1.383E+OO 1.383E+OO 33.25 TH-228 74.82 112 10.28 3.689E+OO 1.759E+OO 1.759E+OO 39.77 77 .11 167 17.10 3.920E+OO 1.490E+OO 1.490E+OO 25. 72 238.63 424 43.60* 4.881E+OO l.192E+OO 1.192E+OO 11. 89 300.09 45 3.30 4.087E+OO 1.991E+OO 1.991E+OO 61. 31 TH-230 609.32 182 45.49* 2.302E+00 1.041E+OO 1.041E+OO 17.44 1120.29 38 14.92 1.429E+00 l.057E+OO 1.057E+OO 40.70 1764.49 28 15.30 9.659E-01 1.123E+OO 1.123E+OO 39.59 PA-231 283.69 ------1. 70 4.275E+OO ------Line Not Found ------301.36 18 5.35* 4.068E+OO 5.038E-01 5.038E-01 150.97 TH-232 105.21 25 1.10 5.939E+OO 2.322E+OO 2.322E+OO 102.30 338.32 63 11. 27 3.704E+OO 9.016E-01 9.016E-01 63.62 835. 71 ------1. 61 1. 799E+00 ------Line Not Found ------911. 20 60 25.80* 1.682E+OO 8.265E-01 8.265E-01 33.32 968. 97 59 15.80 1.603E+OO 1.383E+OO 1.383E+OO 33.25 PA-233 300.13 45 6.63 4.087E+OO 9.909E-01 9.909E-01 61. 31 311. 90 21 38.50* 3.975E+00 8.293E-02 8.293E-02 69.73 340.48 ------4.45 3.687E+OO ------Line Not Found ------TH-234 63.29 52 3.70* 2.286E+OO 3.673E+OO 3.673E+OO 62.78 92.59 79 4.23 5.269E+OO 2.122E+OO 2.122E+OO 64.22 U-234 609.32 182 45.49* 2.302E+00 1. 041E+OO 1. 041E+OO 17.44 1120.29 38 14.92 1.429E+OO 1.057E+OO l.057E+00 40.70 1764.49 28 15.30 9.659E-01 l.123E+OO 1.123E+OO 39.59 U-235 89. 96 ------3.47 5.068E+OO ------Line Not Found ------93.35 79 5.60 5.269E+OO 1.603E+OO l.603E+00 64.22 143.76 30 10.96* 6.310E+OO 2.613E-01 2.613E-01 12.4.72 163.33 ------5.08 6.096E+00 ------Line Not Found ------185.72 56 57.20 5.735E+00 l.027E-01 l.027E-01 101.07 205.31 ------5.01 5.415E+00 ------Line Not Found ------U-238 63.29 52 3.70* 2.286E+OO 3.673E+OO 3.673E+OO 62.78 92.59 79 4.23 5.269E+OO 2.122E+OO 2.122E+OO 64.22 AM-243 43.53 ------5.90 1. 969E-01 ------Line Not Found ------74.66 112 67.20* 3.689E+OO 2.691E-01 2.691E-01 39.77 ANH-511 511. 00 24 100.00* 2.647E+OO 5.361E-02 5.361E-02 135.49 Flag: "*" Key line Page 3544 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235028 Acquisition date 3-0CT-2016 09:08:29 Total number of lines in spectrum 60 Number of unidentified lines 16 Number of lines tentatively identified by NID 44 Nuclide Type : Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 PM-147 EU-155 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 PA-233 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 53.22D l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 2.62Y 4.75Y 1. 41E+l0Y 7.04E+08Y l.41E+l0Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1.41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+10Y 2.14E+06Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 60.3 1. 00 1. 60 1. 00 1. 02 1. 02 1.26 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 2.997E-01 l.455E+Ol l.331E+OO 1. 331E-01 1. 22 6E-01 l.295E-01 6.398E+02 1. 210E-01 3.546E-01 3.077E+OO 1. 843E+OO 1.192E+OO 1.041E+OO 1. ll 7E+OO l.041E+OO 3.039E+OO 1. 041E+OO 8.265E-01 8.265E-01 1.192E+OO 1. 041E+OO 5.038E-01 8.265E-01 8.293E-02 3.673E+OO 1.041E+OO 2. 613E-01 3.673E+OO 2.691E-01 5.361E-02 6.845E+02 6.845E+02 Decay Corr pCi/GRAM 1. 808E+Ol l.455E+Ol 2.136E+OO l.331E-01 l.250E-01 1. 321E-01 8.035E+02 l.373E-01 3.546E-01 3.077E+OO 1.843E+OO l.192E+OO 1. 041E+OO 1.117E+OO 1. 041E+OO 3.039E+OO 1. 041E+OO 8.265E-01 8.265E-01 1.192E+OO 1.041E+OO 5.038E-01 8.265E-01 8.293E-02 3.673E+OO 1.041E+OO 2.613E-01 3.673E+OO 2.691E-01 5.361E-02 8.668E+02 8.668E+02 73.33% Decay Corr 2-Sigma Error 2.247E+Ol 0.167E+Ol 2.633E+OO l.641E-01 0.755E-01 0.798E-01 14.07E+02 l.404E-01 0.794E-01 0.458E+OO 0.927E+OO 0.142E+OO 0.182E+OO 0.166E+OO 0.182E+OO l .151E+OO 0.182E+OO 2.754E-01 2.754E-01 0.142E+OO 0.182E+OO 7.605E-01 2.754E-01 5.783E-02 2.306E+OO 0.182E+OO 3.259E-01 2.306E+OO l.070E-01 7.264E-02 "M" Manually accepted 2-Sigma %Error 124.28 11. 45 123.24 123.24 60.39 60.39 175.07 102.30 22.39 14.87 50.28 11. 89 17.44 14.87 17.44 37.88 17.44 33.32 33.32 11. 89 17.44 150.97 33.32 69.73 62. 78 17.44 124.72 62.78 39.77 135.49 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3545 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235028 Acquisition date : 3-0CT-2016 09:08:29 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 5 66.17 25 121 1. 34 132. 01 124 13 6.21E-03 **** 2.63E+OO T 0 129.51 27 126 0.56 258.74 254 10 6.94E-03 **** 6.34E+OO T 0 209.07 81 102 1. 25 417.93 412 13 2.lOE-02 57.7 5.35E+OO 0 252.87 18 55 1. 06 505.57 501 8 4.69E-OJ **** 4.68E+OO T 0 271.22 28 81 3.19 542.28 536 11 7.35E-03 **** 4.43E+OO T 2 354.59 26 16 1. 47 709.11 698 15 6.92E-03 75.3 3.57E+OO T 0 438.55 10 14 0. 72 877.10 874 7 2.78E-03 **** 3.00E+OO T 0 463.64 26 47 *1. 00 927.29 921 12 7.02E-03 **** 2.86E+OO T 8 516.91 17 17 1. 99 1033.88 1015 23 4.60E-03 99.7 2.62E+OO 0 528.48 8 13 1. 60 1057.04 1052 7 2.28E-03 **** 2.58E+OO T 0 558.41 14 11 1. 80 1116. 93 1114 7 3.95E-03 **** 2.47E+OO 0 564.80 37 33 8.03 1129.72 1121 21 1. 03E-02 83.0 2.44E+OO 0 578.37 11 13 0.66 1156.86 1150 10 2.93E-03 **** 2.40E+00 0 613.75 7 14 0.89 1227.64 1223 6 2.06E-03 **** 2.29E+OO T 0 650 .11 10 14 1. 37 1300. 41 1295 8 2.82E-03 **** 2.19E+OO 0 703.29 18 14 1. 79 1406.82 1401 10 5.05E-03 91. 7 2.06E+OO T 0 763.48 10 7 0.57 1527.25 1524 6 2. 71E-03 **** l.93E+OO T 0 772. 21 13 18 0.52 1544.73 1538 10 3.67E-03 **** l.91E+OO T 0 906.46 10 8 0.54 1813.34 1806 10 2.83E-03 **** 1. 69E+OO 0 928.71 11 9 3.73 1857.87 1850 13 3.15E-03 **** 1. 66E+OO T 0 933.91 22 5 1. 90 1868.28 1863 10 6.17E-03 56.6 1. 65E+OO 0 1003.12 14 19 2. 89 . 2006.77 2000 13 4.04E-03 **** 1. 56E+OO T' 0 1078.97 14 5 3.30 2158.55 2152 11 4.09E-03 83.1 l.47E+OO 0 1097.54 7 6 0.75 2195.69 2191 8 2.02E-03 **** 1. 45E+OO 0 1124. 78 9 3 0.83 2250.21 2247 7 2.64E-03 92 .1 l.42E+OO 0 1138.08 4 15 0.45 2276.82 2271 12 l.24E-03 **** l.41E+OO 0 1156.29 13 19 3.87 2313.25 2302 16 3.74E-03 **** l.39E+OO 0 1180.73 9 12 0.61 2362.16 2356 9 2.66E-03 **** l.37E+OO 0 1378.46 7 6 1. 23 2757.82 2752 8 l.92E-03 **** l.20E+OO 0 1587.68 6 5 0.87 3176.50 *3169 10 l.67E-03 **** 1. 06E+OO Flags: "T" = Tentatively associated Page 3546 of 5809

. c VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:09:42.84 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * *******************************************************************************
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l *
  • Acquisition date 3-0CT-2016 09:08:29 Sensitivity 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:50:00 Nuclide Library : SOLID *
  • Sample ID G405235028 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.2552E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN:CNF;16
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 PM-147 EU-155 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 PA-233 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.099E+Ol 2.228E-01 1. 247E+OO 7.373E-02 3.015E-02 3.186E-02 6.771E+02 8.918E-02 2.185E-02 1.303E-01 3.498E-01 4.705E-02 5.086E-02 1. 758E-01 5.086E-02 5.046E-01 5.086E-02 1.164E-01 1.164E-01 4.705E-02 5.084E-02 3.353E-01 1.164E-01 4.365E-02 1.230E+OO 5.084E-02 1.403E-01 1.230E+OO 4.748E-02 2.149E-02 ----Non-Identified Nuclides Nuclide NA-22 Le (pCi/GRAM 4.375E-02 NOT IDENT. Page 3547 of 5809 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 cs...:135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 Page 3548 of 5809 O.OOOE+OO 2.552E-02 2.878E-01 0.000E+OO O.OOOE+OO 5.955E-02 4.124E-01 O.OOOE+OO 3.944E-02 5.488E-01 5.998E+OO 3.105E-02 1.596E-01 2.214E+OO 1.400E+Ol O.OOOE+OO 1. 725E-01 O.OOOE+OO O.OOOE+OO 5.185E-01 6.874E+OO 8.490E-01 O.OOOE+OO 2.601E-01 5.371E+02 3.416E-02 9.476E-01 2.677E+OO 1.345E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.590E-02 4.337E-02 5.538E+OO 4.852E-01 4.852E-01 2. 471E-02 8.884E-02 2.227E-01 O.OOOE+OO O.OOOE+OO 1.102E-01 1. 089E+OO 1.018E-01 2.903E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.063E-02 O.OOOE+OO 5.896E-02 l.125E-01 O.OOOE+OO O.OOOE+OO 9.472E-02 O.OOOE+OO O.OOOE+OO 2.755E+Ol O.OOOE+OO 2.630E-01 5.912E-02 5.181E+OO 3. 572E-02 O.OOOE+OO O.OOOE+OO 2.455E-02 7.841E-02 l.527E-01 l.056E-01 1.739E+OO 4.597E-02 2.493E+Ol 1. 716E-01 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-172 LU-176 HF-181 TA-l82 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3549 of 5809 7.553E-02 1. 977E-02 3.624E+OO 1.00lE+OO 4.009E+00 2.620E+Ol 9.241E+Ol 4.449E-01 2.651E+OO 4.529E-02 6.984E+OO 5.268E-01 2. 996E-01 5.283E-01 1. 780E-Ol 1. 780E-01 3. 969E-01 5.283E-01 2.706E-01 5.107E+OO 4.592E-02 O.OOOE+OO 2.139E-01 2.898E+02 l.573E-01 8.054E-02 5.770E-02 2.482E-02 3.370E-02 1. 031E-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:09:48.76 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235028.CNF;l *
  • Acquisition date 3-0CT-2016 09:08:29 Sensitivity : 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.50 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:50:00 Nuclide Library : SOLID *
  • Sample ID G405235028 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : l.2552E+02 GRAM *
  • Quantity Err(%) : 1.5934E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * -*
  • CALIBRATION INFORMATION * * '* Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;l6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) BE-7 1. 808E+Ol 2.204E+Ol 2.204E+Ol K-40 1.455E+Ol 1.800E+OO l.800E+OO CD-109 5.357E-01 2.621E+OO 2.621E+OO SN-126 3.339E-02 1.633E-01 1.633E-01 BA-137M 1.250E-01 7.420E-02 7.420E-02 CS-137 1. 321E-01 7.838E-02 7.838E-02 PM-147 8.035E+02 1.379E+03 l.379E+03 EU-155 1. 373E-01 1. 37 9E-01 1.379E-01 TL-208 3.546E-01 7.924E-02 7.924E-02 BI-211 9.525E-02 9.126E-01 9.126E-01 BI-212 1.843E+OO 9.128E-01 9.128E-01 PB-212 1.192E+OO 1.524E-01 1.524E-01 BI-214 1. 041E+OO l.835E-01 1.835E-01 PB-214 1.117E+OO 1.693E-01 l.693E-01 RN-222 1.041E+OO 1.835E-01 1.835E-01 RA-224 1.125E+OO l.240E+00 1.240E+OO RA-226 1.041E+OO l.835E-01 l.835E-01 AC-228 8.265E-01 2.732E-01 2.732E-01 RA-228 8.265E-01 2.732E-01 2.732E-01 TH-228 1.192E+OO 1.524E-01 1.524E-01 TH-230 1.041E+OO l.834E-01 1.834E-01 PA-231 5.038E-01 7.530E-01 7.530E-01 TH-232 8.265E-01 2.732E-01 2.732E-01 PA-233 8.293E-02 5. 681E-02 5.681E-02 TH-234 3.673E+00 2.402E+OO 2.402E+OO U-234 l.041E+OO l.834E-01 l.834E-01 U-235 2.613E-01 3 .196E-01 3 .196E-01 U-238 3.673E+00 2.402E+OO 2.402E+OO AM-243 l.757E-01 l.088E-01 l.088E-01 ANH-511 5.361E-02 7.122E-02 7.122E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma ) Page 3550 of 5809 NA-22 1.756E-02 4.725E-02 4. 791E-02 NOT IDENT. NA-24 -1.000E+41 l.020E+42 O.OOOE+OO SHORT HLIF AL-26 -2.615E-02 3. 996E-02 4.166E-02 NOT IDENT. SC-46 -1. 364E-01 3.835E-01 3.884E-01 FAIL ABUN V-48 1.045E+04 2.257E+04 2.306E+04 SHORT HLIF CR-51 2.576E+02 6.120E+02 6.229E+02 SHORT HLIF MN-54 3.315E-02 6.478E-02 6.648E-02 NOT IDENT. C0-56 -5.328E-02 5.071E-01 5.077E-01 NOT IDENT. MN-56 -l.OOOE+41 l.094E+42 0.000E+OO SHORT HLIF C0-57 * -1.256E-02 4. 968E-02 5. 0.00E-02 NOT IDENT. C0-58 -1.170E-01 6.807E-01 6.827E-01 NOT IDENT. FE-59 1.602E+OO 7. 671E+OO 7.705E+OO NOT IDENT. C0-60 -2.154E-03 3.686E-02 3.687E-02 NOT IDENT. ZN-65 9.149E-02 1.921E-01 1. 965E-01 NOT IDENT. GE-68 4.253E-01 2.527E+OO 2.534E+OO NOT IDENT. AS-73 4.979E+OO 1.473E+Ol 1.490E+Ol NOT IDENT. AS-74 l.334E+02 1.023E+04 l.023E+04 SHORT HLIF SE-75 -7.611E-02 2.177E-01 2.204E-01 FAIL ABUN BR-77 1.670E+40 1. 517E+41 O.OOOE+OO SHORT HLIF SR-82 2.876E+02 1.280E+03 1.287E+03 SHORT HLIF RB-83 -3.059E-02 6.694E-01 6.695E-01 FAIL ABUN KR-85 6.317E+OO 7.069E+OO 7.621E+OO NOT IDENT. SR-85 7.776E-01 8.733E-01 9.410E-01 NOT IDENT. RB-86 -2.782E+03 5.587E+04 5.588E+04 SHORT HLIF Y-88 1.465E-01 2.636E-01 2. 718E-01 NOT IDENT. Y-91 -5. 891E+02 7.285E+02 7.754E+02 NOT IDENT. NB-94 5.270E-02 4.740E-02 5.302E-02 FAIL ABUN NB-95 -1.152E+OO 1.662E+OO 1.742E+00 NOT IDENT. NB-95M 9.905E-01 3.326E+OO 3.356E+OO NOT IDENT. ZR-95 -1. 217E+OO 1.835E+OO 1.915E+OO NOT IDENT. NB-97 1.000E+41 l.487E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 l.540E+41 O.OOOE+OO SHORT HLIF M0-99 3.489E+33 8.120E+33 O.OOOE+OO SHORT HLIF TC-99M 1. OOOE+41 2.294E+41 O.OOOE+OO SHORT HLIF RH-101 4.562E-03 3 .113E-02 3.120E-02 NOT IDENT. RH-102 -4.028E-03 5.142E-02 5.145E-02 NOT IDENT. RU-103 -7.032E+OO 7.441E+OO 8.088E+OO FAIL ABUN RH-106 l.548E-01 5.408E-01 5.453E-01 NOT IDENT. RU-106 l.548E-01 5.408E-01 5.453E-01 NOT IDENT. AG-108M 1. 214E-02 2.630E-02 2.686E-02 FAIL ABUN AG-llOM 5 .191E-02 9.498E-02 9.782E-02 FAIL ABUN SN-113 5.300E-02 2.431E-01 2.443E-01 NOT IDENT. CD-115 1.000E+41 1.625E+41 O.OOOE+OO SHORT HLIF SN-ll 7M -1. 501E+05 2.055E+05 2.164E+05 SHORT HLIF TE-123M -8.00lE-02 l.355E-01 l.403E-01 NOT IDENT. SB-124 -l.427E+OO 2.075E+OO 2.172E+OO NOT IDENT. SB-125 1. 741E-02 1.128E-01 l.130E-01 FAIL ABUN TE-125M 7.959E+Ol 3.427E+02 3.446E+02 NOT IDENT. I-126 -2.242E+06 2.593E+06 2.783E+06 SHORT HLIF SB-126 -1. 7 66E+05 2.566E+06 2.567E+06 SHORT HLIF SB-127 -3. 841E+22 3.443E+23 O.OOOE+OO SHORT HLIF I-131 -l.353E+l0 l.843E+10 1. 941E+10 SHORT HLIF I-132 l.OOOE+41 2.096E+42 O.OOOE+OO SHORT HLIF TE-132 1. 051E+28 l.028E+28 O.OOOE+OO SHORT HLIF BA-133 7.383E-02 5.457E-02 6.392E-02 FAIL ABUN I-133 l.OOOE+41 2.492E+41 O.OOOE+OO SHORT HLIF CS-134 9.440E-02 9.271E-02 1.020E-01 FAIL ABUN CS-135 1. 502E-02 1.441E-01 l.442E-01 NOT IDENT. I-135 -1.000E+41 2.766E+42 O.OOOE+OO SHORT HLIF CS-136 -4.440E+05 7.498E+05 7. 761E+05 SHORT HLIF CE-139 -1. 851E-02 l .116E-01 1.119E-01 NOT IDENT. BA-140 -l.436E+06 2.612E+06 2.691E+06 SHORT HLIF LA-140 9.574E+03 8.833E+05 8.834E+05 SHORT HLIF CE-141 1. 848E+Ol 3.182E+Ol 3.289E+Ol NOT IDENT. CE-143 1.000E+41 2.630E+41 O.OOOE+OO SHORT HLIF CE-144 -2.757E:...01 3.596E-01 3.805E-01 NOT IDENT. PM-144 4.008E-03 6.903E-02 6.906E-02 FAIL ABUN PR-144 3.695E-01 6.046E+OO 6.049E+OO NOT IDENT. PM-146 6.640E-03 3.953E-02 3. 965E-02 NOT IDENT. ND-147 2.722E+07 9.703E+07 9.780E+07 SHORT HLIF PM-149 -1.000E+41 2 .133E+41 O.OOOE+OO SHORT HLIF EU-150 2.547E-02 2.834E-02 3.058E-02 FAIL ABUN EU-152 -1.123E-03 9.637E-02 9.637E-02 NOT IDENT. GD-153 -1. 396E-01 l.844E-01 1.949E-01 NOT IDENT. EU-154 4.025E-02 l.144E-01 1.158E-Ol NOT IDENT. TB-160 -1.721E-01 2.134E+00 2.135E+OO FAIL ABUN H0-166M -6.627E-06 5.425E-02 5.425E-02 NOT IDENT. TM-171 -3.799E+Ol 3.088E+Ol 3.531E+Ol FAIL ABUN Page 3551of5809 HF-172 -9.466E-02 2.226E-01 2.267E-01 FAIL ABUN LU-172 8.053E-03 1.025E-01 1.025E-01 FAIL ABUN LU-176 l.258E-03 2.585E-02 2.585E-02 FAIL ABUN HF-181 -2.856E+OO 5. 272E+OO 5.427E+OO NOT IDENT. TA-182 -2.635E-01 1.203E+OO l.209E+OO FAIL ABUN RE-183 -1.317E+OO 4.470E+OO 4.509E+OO FAIL ABUN RE-184 -1.442E+Ol 4.087E+Ol 4.138E+Ol NOT IDENT. W-188 -4.982E+Ol l.308E+02 1.327E+02 FAIL ABUN IR-192 2.345E-01 5.059E-01 5.168E-01 FAIL ABUN HG-203 * -1. 792E+OO 3.412E+OO 3. 506.E+OO NOT IDENT . BI-207 -1.288E-02 5.720E-02 5.750E-02 FAIL ABUN PB-210 4.970E+OO 7.208E+OO 7.548E+OO NOT IDENT. PB-211 1.667E-01 5.689E-01 5.739E-01 NOT IDENT. RN-219 -9.467E-02 3.491E-01 3.517E-01 FAIL ABUN RA-223 -1. 68 6E-01 6.675E-01 6. 718E-01 FAIL ABUN AC-227 -1.360E-01 2.533E-01 2.606E-01 FAIL ABUN TH-227 -l.360E-01 2.533E-01 2.606E-01 FAIL ABUN TH-229 3.335E-02 4.608E-01 4.611E-01 FAIL ABUN TH-231 -l.686E-01 6.675E-01 6.718E-01 FAIL ABUN PA-234 1. 703E-01 3.519E-01 3.602E-01 NOT IDENT. PA-234M 3.661E-01 6.507E+OO 6.509E+OO NOT IDENT. NP-237 8.293E-02 5.681E-02 6.801E-02 FAIL ABUN NP-238 1.000E+41 4.439E+41 O.OOOE+OO SHORT HLIF NP-239 -1.455E-01 2.761E-01 2.838E-01 FAIL ABUN PU-239 4.101E+02 6.650E+02 6.903E+02 FAIL ABUN AM-241 1.354E-02 l.698E-01 1.699E-01 NOT IDENT. CM-243 -5.031E-02 1.031E-01 l.056E-01 NOT IDENT. BK-247 1. 32 6E-02 6.740E-02 6.766E-02 FAIL ABUN CM-247 -2.270E-02 3.132E-02 3.295E-02 NOT IDENT. CF-249 -1.524E-02 4.415E-02 4.468E-02 FAIL ABUN CF-251 7.510E-02 l.127E-01 1.177E-01 NOT IDENT. Page 3552 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 74.66 38.0285 105.31 84.7366 131.20 51.9924 879.38 51. 5907 86.79 84.7818 133.02 39.4293 46.54 36.0719 86.94 84.8099 133.52 50.9180 228.16 0.0000 87.09 84.8380 136.00 41.2183 52.39 31.0659 87.57 84.9283 136.47 46.0459 1093.63 38.2976 88.03 95.8227 739.50 0.0000 52.39 50.3473 306.78 95.8877 140.51 0.0000 125.81 48.8370 88.47 95.9152 143.76 45.6080 53.44 40.8900 143.76 51.0469 144.24 45. 6417 54.07 30.5259 90.64 89.9037 145.44 38.9160 293.27 0.0000 531. 02 0.0000 152.43 51.1280 482.18 46.2649 92.59 72.5764 1048.07 0.0000 57.98 49.5762 93.35 72.6928 154.21 47.3188 59.27 46.4984 94.56 50.9549 158.56 0.0000 59.32 46.5051 311. 90 50. 9641 159.00 51.6207 59.54 46.5343 946.00 50. 9663 162.33 48.8744 60. 96 43. 7166 94.87 50.9877 537.26 0.0000 61.17 44.8360 97.43 57.2173 163.33 40.9531 62.93 50.2762 98.43 47.4797 165.86 46.1109 63.29 50.3260 98.44 47.4805 427.87 48.8064 290.67 50.3659 103.37 55.6658 176. 60 0.0000 87.57 50.4621 116.74 55.6658 177.52 40.7379 66.73 50.7949 100 .11 55.7306 181.07 0.0000 67.24 50.8633 102.03 45 .1160 181.52 55.9688 67. 68 55.6529 103.18 59.0852 184.41 61.6599 1221. 41 55.6625 103.37 54.2821 185.72 61.7642 97.43 61.5354 911. 20 42. 3711 193.51 45.7422 279.20 64.8037 105.31 46.0118 197.03 42.8093 1063.66 76.6875 106.12 50.0250 198.01 38.6796 72.87 76.6992 106.47 50.0586 201.83 38.8597 351.06 76.6992 109.28 48.8017 203.43 43.1440 74.66 64.5773 111. 00 56.9150 205.31 42.1863 238.63 64.6028 111.76 0.0000 210.85 33.9702 351. 93 64.6028 114.06 65.5458 215.65 41. 6321 238.63 64.6028 116. 30 0.0000 222 .11 38.7131 74.97 64.6266 116.74 65.5556 227.09 43.2538 77 .11 64. 9623 119.76 45.7012 227.38 42.1861 78.74 65.2151 264.66 44.8759 228.16 0.0000 256.23 68.8013 121. 22 44.8835 228.18 25.9838 133. 52 67. 7230 344.28 53.6634 235.69 50.9384 364.49 0.0000 122.06 48.6953 235.96 64.0557 711. 68 62.0486 122.92 43.7662 238.63 49.2737 356.01 56.3597 1274.44 40.0251 238.98 0.0000 323.87 48.3164 123.68 41.3195 240.99 49.3973 81. 75 65.6755 125.81 46. 4973 242.00 49.4501 83.79 61.3519 127.23 39.0512 244.70 30.8561 265.00 61.3810 127.91 45.4021 685.70 0.0000 193.51 75.5212 129.30 45.5076 388.16 38.8943 Page 3553 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 507.63 0.0000 345.93 21. 7 535 569.50 25.1686 256.23 40.1451 351.06 18.2021 569.70 25.1708 527.90 0.0000 351. 93 18.2149 583.19 9. 8596 2 64. 66 32. 6117 355.39 0.0000 584.27 14.0930 264.80 31. 4915 356.01 27.6132 595.83 0.0000 265.00 26.9978 364. 4Sil 0.0000 600.60 17.0566 . 268.22 30.0928 366.42 0.0000 602.52 0.0000 269.46 38.4150 372. 51 27.1435 604. 72 15.6688 270.03 38.4357 375.05 19.7788 607.14 14.2621 401. 81 38.4803 377.52 24.7693 609.32 14.2780 273.65 0.0000 383.85 27.3745 610.33 0.0000 276.40 50.0465 388.16 32.4548 614.28 8.5884 583.19 28.4615 666.33 0.0000 618.01 22.9463 277.60 27.3289 391.69 22.5269 884.68 15.3151 402.40 30.7565 400.66 18.4743 621.93 15.3275 279.20 46.7581 401.81 23.5316 630.19 0.0000 279.54 44.4915 402.40 25.2234 631.29 11.5493 279.70 44.4975 404.85 16.8449 633.25 17.3408 280.46 41.1042 410.95 27.9136 634.78 0.0000 301.36 32.0674 413. 71 28.8148 635.95 12.5409 284.31 0.0000 720.70 0.0000 636.99 0.0000 285.41 34.4128 423. 72 0.0000 1690.97 23.2646 285.90 0.0000 427.09 23.9497 657.76 5.8499 287.50 28.7331 427.87 25.6738 657.90 0.0000 290.67 29.2012 433.94 17.1863 661.66 16.6057 293.27 0.0000 439.40 15.5240 664.57 0.0000 295.22 21. 6061 453.88 16.5427 666.33 0.0000 316.51 21. 6204 463.37 13.1400 666.50 0.0000 298.58 20.8976 468.07 21. 08 64 667.71 0.0000 299.98 26.3488 473.00 0.0000 677.62 15.7474 300.09 26.3508 631. 29 18.5322 685.70 0.0000 300.13 26.3522 696. 49 14.1348 695.00 0.0000 311. 90 26.3522 477.60 14.1419 696.49 21. 8433 301.36 26.3813 482.18 17.2847 696. 51 21. 8433 302.85 26.4159 487.02 0.0000 697.00 0.0000 304.50 31.1230 492.35 0.0000 697.30 23.8379 304.85 0.0000 497.08 25.0452 697.49 23.8398 306.78 26.5079 505.52 12.1366 702.65 16.9260 308.46 26.5473 507.63 0.0000 706.68 13.4659 311.90 21.9280 511. 00 16.2345 711. 68 12. 9968 316.51 21.2294 514.00 16.2634 720.70 0.0000 319.41 0.0000 514.00 16.2634 721. 93 0.0000 320.08 0.0000 520.40 12.2432 722.78 9.0425 321. 04 28.4150 520.69 0.0000 722.91 9.0428 323.87 36.7907 667. 71 0.0000 723.31 13.5670 325.23 33.2688 527.90 0.0000 756.73 21.1119 1596.21 0.0000 528.26 10.9321 727.33 11. 0743 333.37 25.1214 529.59 25.9835 733.00 15.1392 333.97 22.3410 529.87 0.0000 735.93 10.1058 334.37 23.9447 531. 02 0.0000 737.46 17.1909 338.28 27.6248 537.26 0.0000 739.50 0.0000 338.32 27.6255 1260.41 0.0000 747.24 15.2332 340.48 27.6740 552.55 17.5481 748.06 13.2068 340.55 0.0000 795.86 18. 1154 752.31 16.2845 344.28 26.5527 569.33 25.1664 753.82 0.0000 Page 3554 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 756.73 18.3545 968. 97 14.3864 1505.03 8. 7133 756.80 18.3552 983.53 0.0000 1584.12 4.7341 763.94 21.4802 984.45 0.0000 1596.21 0.0000 765.81 30.7092 996.26 13.4053 1620.50 5.9667 1001.03 15.3589 1001.03 16.7841 1621. 92 1.9895 766.84 12 . .,2891 1002.74 10.0763 0.0000 772. 60 0.0000 1004.73 3.3610 1690.97 4.0400 776.52 0.0000 1021.30 0.0000 1750.46 0.0000 777.92 0.0000 1025.87 0.0000 1764.49 2.0519 778.90 12.3521 1028.54 0.0000 1770.23 3.0817 783.70 0.0000 1037.84 9.0625 1771.35 1.0274 785.37 11. 3531 1038.76 0.0000 1791.20 0.0000 903.28 6.2097 1046.59 7.9525 1808.65 5.1770 794.95 14.5064 1048.07 0.0000 1810.72 0.0000 795.86 14.5121 1049.04 15.9175 1836.06 2.0823 801.95 12.4702 1050.41 10.2371 810.06 8.3408 1063.66 12.5657 810.29 10.4268 1077.00 0.0000 810.45 10.4277 1077.34 8.0317 810.76 12.5146 1085.87 5.7524 815.77 0.0000 1093.63 12.1099 818.51 0.0000 1099.45 5.1995 832.01 10.5180 1112. 07 10.4399 834.85 9. 47 68 1112. 84 6.9614 835. 71 10.5334 1115. 54 6. 9673 836.80 0.0000 1120. 29 6.9775 846.75 0.0000 1120.55 6.9780 846.77 10.5790 1121.30 3.4897 856.80 0.0000 1808.65 9.7966 860.56 18. 0812 1131.51 0.0000 871. 09 12.8145 1147.95 0.0000 873.19 7.4811 1332.49 11. 5218 875.33 0.0000 1177.95 11. 3602 879.38 10. 7125 1189.05 14.2471 880.51 5.3585 1204.77 18.7852 883.24 10.7279 1221. 41 17.0773 884.68 6.4404 1231. 02 11. 7170 889.28 9.6771 1235.36 0.0000 894.76 10.7743 1238.28 15.3533 1836.06 9.7090 1260. 41 0.0000 900.72 9.7185 1271.87 6.3818 903.28 9. 7277 1274.44 7.2988 911.20 13.0083 1274.54 7.2988 912.08 14.6393 1291. 59 11. 0002 984.45 0.0000 1298.22 0.0000 926.50 8.1757 1312 .11 0.0000 929 .11 8.1833 1332. 49 6.4877 937.49 6.5664 1362.66 0.0000 983.53 0.0000 1365.19 4.6744 946.00 8.7819 1368.63 0.0000 949.00 8.7913 1384.29 4.6976 954.55 0.0000 1408.01 3.7808 962. 31 19.8735 1457.56 0.0000 964.08 8.2858 1460.82 3. 8311 966 .17 14.9255 1489.16 3.8577 Page 3555 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:10:18.82 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM19.CNF;561 Background date : Sample date 23-NOV-2015 11:10:00 Acquisition date : Z-OCT-2016 11:01:07. 3-0CT-2016 09:08:53. 1.51202E+02 GRAM CAN Sample ID G405235029 Sample quantity Detector name : GAM19 Detector geometry: Elapsed live time: 0 01:00:00.00 Elapsed real time: Energy tolerance 1.50000 keV Analyst Initials Abundance limit 75.00000 Sensitivity Batch ID 1596249 Detector SN# 0 01:00:00.76 0.0% MXRl 3.00000 Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 0 5 5 0 0 0 0 4 4 0 0 1 1 0 0 0 0 0 0 0 0 1 1 0 8 8 0 0 0 0 4 Page 3556 of 5809 Energy 62.52* 74.69* 77.07* 86.79 89.88 92.81* 129.14 143.25* 186.00* 209.48 238.55* 241.66 255.93 274.31 295.16* 300.36 338.55 351. 84* 410.33 510.76* 583.11* 609.54* 625.69 661. 59 723.01* 726.99 748.16 781.40 785.81 804.73 859.99 911. 02* 946.99 963.76 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 22 131 207 70 58 74 51 37 71 40 403 146 14 82 139 31 56 269 29 49 124 151 17 108 15 27 14 13 17 17 26 74 22 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 186 171 123 244 102 173 116 123 143 105 73 103 80 203 75 75 63 58 68 47 29 43 8 24 35 33 10 16 18 24 10 22 13 15 0.54 1. 30 1. 07 1. 00 1.14 1. 56 0.79 2.78 1. 49 0.91 1.10 2.07 0.57 8.38 1. 62 1. 63 1. 51 1. 32 2.16 2.14 1. 75 1. 53 0.91 1. 26 1. 98 1. 98 1. 39 2.20 2.29 1. 55 1. 80 1. 31 4.32 2.84 125.82 150.19 154.93 174.38 180.56 186.43 259.12 287.35 372.89 419.88 478.04 484.25 512.80 549.58 591.29 601.70 678.12 704.70 821. 74 1022.67 1167. 44 1220.32 1252.65 1324.47 1447.36 1455.34 1497.69 1564.19 1573.03 1610.87 1721.45 1823.55 1895.53 1929.07 121 143 143 168 178 178 256 283 369 416 470 470 509 533 586 586 674 698 812 1016 1162 1212 1249 1319 1440 1440 1494 1561 1561 1605 1717 1818 1886 1920 10 6.15E-03119.5 18 3.65E-02 19.8 18 5.76E-02 11.1 11 l.93E-02 45.1 13 l.62E-02 28.4 13 2.04E-02 35.9 8 1.41E-02 39.2 9 l.03E-02 57.4 11 1.98E-02 35.7 10 1.llE-02 50.9 24 1.12E-01 6.2 24 4.06E-02 20.7 9 3.79E-03121.7 28 2.28E-02 50.4 26 3.86E-02 14.6 26 8.50E-03 56.7 9 1.55E-02 29.5 13 7.47E-02 8.6 13 7.98E-03 62.1 16 l.35E-02 39.7 12 3.46E-02 12.7 14 4.20E-02 12.4 8 4.72E-03 37.7 11 2.99E-02 13.1 27 4.06E-03 83.9 27 7.39E-03 48.0 10 3.92E-03 52.6 17 3.50E-03 54.1 17 4.83E-03 52.7 12 4.61E-03 64.1 12 7.35E-03 30.0 12 2.06E-02 17.5 17 6.21E-03 42.2 23 4.95E-03 56.9 Fit 2.59E+OO 4.40E-01 5.95E-01 1. 62E+OO 1.19E+OO 2.80E+OO 3.57E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 4 968.62 53 6 1. 82 1938.81 1920 23 1. 46E-02 16.2 36 0 1063.76* 10 22 1. 73 2129.16 2121 15 2.67E-03160.0 .37 0 1120.42 41 14 1. 66 2242 .. 54 2237 11 1.14E-02 23. 4 38 0 1134.69 13 15 3.50 2271. 08 2263 15 3.61E-03 70.6 39 0 1143.20 15 12 3.51 2288.11 2282 12 4.16E-03 53.0 40 0 1168.70 19 12 1. 24 2339.14 2333 13 5.26E-03 45.2 41 0 1200.59 13 9 3.91 2402.95 2394 14 3.55E-03 59.9 42 3 1203.95 11 2 1. 89 2409.67 2407 13 3.16E-03 28.6 1.41E-01 43 3 1207.52 13 1 2.05 2416.82 2407 13 3.70E-03 28.3 44 0 1236.70 32 28 8.17 2475.21 2464 27 8.92E-03 48.5 45 0 1263.32 9 8 1. 37 2528.47 2521 12 2. 57E-03 71. 8 46 1 1272.80 20 6 2.30 2547.42 2542 19 5.48E-03 31.7 2 .13E+OO 47 1 1275.58 15 7 2.09 2553.00 2542 19 4. 30E-03 41. 9 48 0 1280.93 7 4 1. 39 2563.69 2560 7 1. 81E-03 61. 8 49 0 1460.59 368 3 1. 93 2923.18 2916 14 1.02E-01 5.3 50 0 1511. 05 7 5 1. 34 3024.14 3017 10 1. 94E-03 70. 7 51 0 1764.29* 34 0 3.25 3530.84 3522 15 9.40E-03 18.4 Flag: "*" = Peak area was modified by background subtraction Page 3557 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:10:20 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 23-NOV-2015 11:10:00 G405235029 Acquisition date : Sample quantity Sampla geometry Detector geometry: 3-0CT-2016 09:08:53 151.20 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA19 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 . 87. 09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 3558 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 TH-229 85.43 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.76 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status NA-22 1274.54 99.94* ;J_.297E+OO 5.808E-02 7.308E-02 83.90 .OK K-40 1460.82 10.66* l.161E+OO 1.424E+Ol l.424E+Ol 10.65 OK Y-91 1204.77 0.26* 1. 358E+00 1.576E+Ol 6.574E+02 57.20 OK CD-109 88.03 3.70* 5.459E+00 1.234E+OO 1.980E+OO 160.25 OK SN-126 64.28 9.60 3.426E+OO Line Not Found Absent 86.94 8.90 5.459E+OO 5.128E-01 5.128E-01 160.25 OK 87.57 37.00* 5.459E+OO 1.234E-01 1.234E-01 160.25 OK BA-137M 661. 66 89.90* 2.164E+00 2.887E-01 2.945E-01 26.26 OK CS-137 661. 66 85.10* 2.164E+00 3.050E-01 3. lllE-01 26.26 OK TL-208 277.37 6.60 4.415E+OO Line Not Found Absent 583.19 85.00* 2.392E+OO 3. 231E-01 3. 231E-01 25.47 OK 860.56 12.50 1. 764E+00 6.089E-01 6.089E-01 60.00 OK BI-211 72.87 1. 23 4.361E+OO Line Not Found Absent 351.06 12.92* 3.630E+OO 3.842E-01 3.842E-01 255.35 OK BI-212 727. 33 6.67* 2.0lOE+OO 1.025E+OO 1.025E+OO 95.99 OK 785.37 1.10 1. 892E+OO 4.277E+OO 4.277E+OO 105.50 OK 1620.50 1. 47 1.063E+OO Line Not Found Absent PB-212 74.82 10.28 4.533E+OO 1.224E+OO l.224E+OO 59.67 OK 77 .11 17.10 4.743E+OO 1. 624E+O'O 1.624E+OO 22.16 OK 238.63 43.60* 4. 961E+OO 1.074E+OO 1. 074E+OO 12.45 OK 300.09 3.30 4.139E+OO 1.262E+OO 1.262E+OO 113. 35 OK BI-214 609.32 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 OK 1120.29 14.92 1.437E+OO 9.465E-01 9.468E-01 46.85 OK 1764.49 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 OK PB-214 74.82 5.80 4.544E+OO Line Not Found <<INT Reject 77 .11 9.70 4.743E+OO 2.862E+00 2.863E+OO 22.16 OK 87.09 3.41 5.478E+OO Line Not Found <<INT Reject 242.00 7.25 4.908E+OO Line Not Found <<INT Reject 295.22 18.42 4.198E+OO 1.015E+OO 1.016E+OO 29.18 OK 351.93 35.60* 3.629E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 OK 1120.29 14.92 l.437E+OO 9.465E-01 9.468E-01 46.85 OK 1764.49 15.30 9. 8 62E-01 1.052E+OO l.052E+OO 36.70 OK RA-224 240.99 4.10* 4.913E+OO 2.381E+OO 2.381E+OO 75.98 OK RA-226 609.32 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 OK 1120.29 14.92 l.437E+00 9.465E-01 9.468E-01 46.85 OK 1764.49 15.30 9.862E-01 1.052E+OO l.052E+OO 36.70 OK AC-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11.27 3.748E+OO 7.358E-01 7.358E-01 58.98 OK 794.95 4.25 1.875E+OO Line Not Found Absent 835.71 1. 61 1.803E+OO Line Not Found Absent 911. 20 25.80* 1.687E+OO 8.586E-01 8.586E-01 35.02 OK 968.97 15.80 1.609E+OO 1.038E+OO 1.038E+OO 32.48 OK RA-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11.27 3.748E+OO 7.358E-01 7.358E-01 58.98 OK 794.95 4.25 1. 875E+OO Line Not Found Absent 835. 71 1. 61 1.803E+OO Line Not Found Absent 911. 20 25.80* l.687E+OO 8.586E-01 8.586E-01 35.02 OK 968.97 15.80 l.609E+OO 1.038E+OO 1.038E+OO 32.48 OK Page 3559 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi7GRAM %Error Status TH-228 74.82 10.28 4.E33E+OO 1.224E+OO 1.224E+OO 59.67 0:1.\ 77.11 17.10 4.743E+OO 1.624E+00 1.624E+OO 22.16 OK 238.63 43.60* 4. 961E+OO 1.074E+OO l.074E+OO 12.45 OK 300.09 3.30 4.139E+OO 1.262E+OO 1.262E+OO 113. 35 OK TH-229 85.43 14.70 5.459E+OO 3.105E-01 3.105E-01 160.25 OK 88.47 24.00 5.640E+OO 2.705E-01 2.705E-01 56.87 OK 193.51 4.41* 5. 711E+00 Line Not Found Absent 210.85 2.80 5.435E+OO 1.529E+OO 1.529E+OO 101.84 OK TH-230 609.32 45.49* 2.309E+OO 7.574E-01 7.574E-01 24.87 OK 1120.29 14.92 1.437E+OO 9.465E-01 9.465E-01 46.85 OK 1764.49 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 OK PA-231 283.69 1. 70 4.336E+OO Line Not Found Absent 301.36 5.35* 4 .139E+OO 7.782E-01 7.782E-01 113. 35 OK TH-232 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 OK 835.71 1. 61 1.803E+OO Line Not Found Absent 911.20 25.80* 1.687E+OO 8.586E-01 8.586E-01 35.02 OK 968. 97 15.80 1.609E+OO 1.038E+OO l.038E+00 32.48 OK TH-234 63.29 3.70* 3.208E+OO 1.207E+OO 1.207E+OO 239.06 OK 92.59 4.23 5.793E+OO 1.879E+OO 1.879E+OO 71.76 OK U-234 609.32 45.49* 2.309E+00 7.574E-01 7.574E-01 24.87 OK 1120.29 14.92 1.437E+OO 9.465E-01 9.465E-01 46.85 OK 1764.49 15.30 9.862E-01 l.052E+00 1.052E+OO 36.70 OK U-235 89. 96 3.47 5.640E+OO 1.871E+OO 1. 871E+OO 56. 87 OK 93.35 5.60 5.793E+OO 1.419E+OO l.419E+OO 71. 76 OK 143.76 10. 96* 6.467E+00 3.153E-01 3.153E-01 114. 8 6 OK 163.33 5.08 6.216E+OO Line Not Found Absent 185. 72 57.20 5. 841E+OO 1.258E-01 1.258E-01 71. 50 OK 205.31 5.01 5.506E+OO Line Not Found Absent U-238 63.29 3.70* 3.208E+OO l.207E+00 1.207E+OO 239.06 OK 92.59 4.23 5.793E+OO 1.879E+00 1.879E+OO 71.76 OK AM-243 43.53 5.90 5.190E-01 Line Not Found Absent 74.66 67.20* 4.533E+OO l.873E-01 l.873E-01 59.67 OK ANH-511 511. 00 100.00* 2.663E+OO 9.783E-02 9.783E-02 79.36 OK Flag: "*" = Keyline Page 3560 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:10:21.79 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  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l * *Acquisition date 3-0CT-2016 09:08:53 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:10:00 Analyst initials: MXRl *
  • Sample ID G405235029 Sample Quantity 1.5120E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) NA-22 7.308E-02 6.009E-02 K-40 1.424E+Ol 1. 486E+OO Y-91 6.574E+02 3.685E+02 CD-109 1.980E+OO 3.109E+OO SN-126 l.234E-01 1.937E-01 BA-137M 2.945E-01 7.580E-02 CS-137 3. lllE-01 8.007E-02 TL-208 3.231E-01 8.062E-02 BI-211 3.842E-01 9.615E-01 BI-212 1.025E+OO 9.640E-01 PB-212 1.074E+OO 1.310E-01 BI-214 7.577E-01 1.846E-01 PB-214 1.155E+OO l.937E-01 RN-222 7.577E-01 1.846E-01 RA-224 2.381E+00 1. 773E+OO RA-226 7.577E-01 1. 846E-01 AC-228 8.586E-01 2.947E-01 RA-228 8.586E-01 2.947E-01 TH-228 1.074E+OO 1.310E-01 TH-229 1.099E-01 4.780E-01 TH-230 7.574E-01 l.846E-01 PA-231 7.782E-01 8.644E-01 TH-232 8.586E-01 2.947E-01 TH-234 1.207E+OO 2.828E+OO U-234 7.574E-01 1.846E-01 U-235 3.153E-01 3.549E-01 U-238 l.207E+00 2.828E+OO AM-243 1. 873E-01 . l.095E-01 ANH-511 9.783E-02 7.608E-02 Non-Identified Nuclides Nuclide BE-7 Page 3561of5809 Key-Line Activity (pCi/GRAM -1.453E+Ol K.L. Cnt Uncert ( 1. 96-sigma) 1.671E+Ol MDA (pCi/GRAM 8.499E-02 5.018E-01 9.545E+02 1.938E+OO 1. 371E-01 6.679E-02 7.055E-02 6.673E-02 3.653E-01 9.073E-01 9.802E-02 l.440E-01 3.270E-01 l.440E-01 1. 051E+OO l.440E-01 2.737E-01 2.737E-01 9.802E-02 9.407E-01 1.439E-01 8.855E-01 2.737E-01 2.050E+OO 1.439E-01 3.256E-01 2.050E+OO 8.635E-02 5. 772E-02 MDA (pCi/GRAM 2.797E+Ol NOT IDENT.

NA-24 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF AL-26 5.527E-03 1. 712E-02 4.800E-02 NOT IDENT. SC-46 4.859E-02 4.254E-01 8.598E-01 FAIL ABUN V-48 O.OOOE+OO 2.902E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.549E+02 O.OOOE+OO SHORT HLIF MN-54 5.341E-02 7.338E-02 l.554E-01 NOT IDENT. C0-56 -1.196E-01 5.202E-01 1.002E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.255E-02 4.811E-02 9.420E-02 NOT IDENT. C0-58 , -4. 650E-03 7.415E-01 1. 366E+OO

  • NOT IDENT. FE-59 -3.147E+OO 7.184E+OO 1.322E+Ol NOT IDENT. C0-60 1. 764E-03 3.682E-02 7.433E-02 NOT IDENT. ZN-65 -l.572E-01 l.983E-01 2.720E-01 NOT IOENT. GE-68 -9.278E-01 2.040E+OO 3. 7 51E+OO NOT IDENT. AS-73 -5.050E-01 9.791E+OO 1.836E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.046E+04 O.OOOE+OO SHORT HLIF SE-75 -l.882E-02 2.424E-01 4.155E-01 NOT IDENT. BR-77 O.OOOE+OO 1.919E+39 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 1.113E+03 O.OOOE+OO SHORT HLIF RB-83 1. 073E-01 7.244E-01 1.401E+OO NOT IDENT. KR-85 -3.223E-01 8.982E+OO 1.473E+Ol NOT IDENT. SR-85 -4.160E-02 1.112E+OO 1.823E+OO NOT IDENT. RB-86 O.OOOE+OO 4.141E+04 O.OOOE+OO SHORT HLIF Y-88 8.967E-02 2.204E-01 5.349E-01 NOT IDENT. NB-94 4.531E-03 3.256E-02 6.536E-02 NOT IDENT. NB-95 3.129E-01 1.035E+OO 2.106E+OO NOT IDENT. NB-95M -5.126E-02 3.181E+OO 5.462E+OO NOT IDENT. ZR-95 4.002E-01 1. 703E+00 3.490E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 9.997E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 7.075E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 348E+41 O.OOOE+OO SHORT HLIF RH-101 -6.025E-03 3.588E-02 6.334E-02 NOT IDENT. RH-102 2.108E-02 5.714E-02 l.140E-01 NOT IDENT. RU-103 5.562E+OO 8.283E+00 1. 671E+Ol FAIL ABUN RH-106 -1.176E-01 5.939E-01 9.486E-01 NOT IDENT. RU-106 -1.176E-01 5.939E-01 9.486E-01 NOT IDENT. AG-108M -l.943E-03 2.940E-02 5.510E-02 FAIL ABUN AG-llOM -6.504E-02 9.867E-02 1. 764E-01 NOT IDENT. SN-113 -1.233E-01 2.916E-01 5.249E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1.975E+05 O.OOOE+OO SHORT HLIF TE-123M -2.844E-02 l.300E-01 2.524E-01 NOT IDENT. SB-124 1.719E-01 2.269E+OO 5.036E+OO FAIL ABUN SB-125 -6. 711E-02 1.221E-01 2.154E-01 NOT IDENT. TE-125M 3. 728E+Ol 3.485E+02 6.358E+02 NOT IDENT. I-126 O.OOOE+OO 1.936E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.089E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.556E+23 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 2.150E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.138E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. 068E+28 O.OOOE+OO SHORT HLIF BA-133 -7.632E-03 4.557E-02 7.581E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 4.499E-02 5.828E-02 1.230E-01 NOT IDENT. CS-135 2.104E-02 l.352E-01 2.635E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 7.600E+05 O.OOOE+OO SHORT HLIF CE-139 -2.342E-02 l.250E-01 2.409E-01 NOT IDENT. BA-140 O.OOOE+OO 3.081E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO l.063E+06 0.000E+OO SHORT HLIF CE-141 -2.317E+OO 3.524E+Ol 6.223E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.226E+41 O.OOOE+OO SHORT HLIF CE-144 1.442E-01 4.299E-01 7.843E-01 NOT IDENT. PM-144 -l.616E-02 5.745E-02 1.112E-01 NOT IDENT. PR-144 -1.415E+OO 5.030E+OO 9.733E+OO NOT IDENT. PM-146 3.302E-02 4.418E-02 9.098E-02 FAIL ABUN ND-147 O.OOOE+OO 9.122E+07 O.OOOE+OO SHORT HLIF PM-147 -3.599E+02 8.051E+02 1.558E+03 NOT IDENT. PM-149 O.OOOE+OO 1.350E+41 O.OOOE+OO SHORT HLIF EU-150 -5.813E-03 2.843E-02 4.715E-02 FAIL ABUN EU-152 2.077E-02 9.563E-02 1.859E-01 FAIL ABUN GD-153 6.480E-02 2.002E-01 3.735E-01 NOT IDENT. EU-154 l.778E-01 1.462E-01 2.544E-01 FAIL ABUN EU-155 2.016E-02 l.094E-01 2.020E-01 FAIL ABUN TB-160 1.846E+00 2.382E+OO 5.125E+OO FAIL ABUN H0-166M -l.935E-02 4.932E-02 9.416E-02 FAIL ABUN TM-171 -5.108E+00 1.995E+Ol 3.692E+Ol NOT IDENT. Page 3562 of 5809 HF-172 2.179E-02 2.578E-01 4.644E-01 FAIL ABUN LU-172 -3.290E-02 7.642E-02 l.395E-01 FAIL ABUN LU-176 l.887E-03 2.750E-02 4.748E-02 NOT IDENT. HF-181 l.695E-01 5.978E+OO l.128E+Ol NOT IDENT. TA-182 -7.827E-01 l.081E+OO l.834E+00 FAIL ABUN RE-183 -3.873E-01 3.611E+OO 6.168E+OO NOT IDENT. RE-184 l.204E+Ol 4.234E+Ol 8.666E+Ol NOT IDENT. W-188 -2.611E+Ol l.555E+02 2.594E+02 FAIL ABUN IR-192 -l.159E-01 5.398E-01 1. OllE+OO FAIL ABUN HG-.203 -l.561E+OO 3.603Et00 5.903E+OO NOT IDENT. BI-207 4.348E-02 l.364E-01 2.539E-01 FAIL ABUN PB-210 -1. 349E+OO 3.389E+OO 6.214E+OO NOT IDENT. PB-211 -2.626E-01 8.082E-01 l.296E+OO NOT IDENT. RN-219 5.338E-02 4.152E-01 7.924E-01 NOT IDENT. RA-223 8.816E-02 6.105E-01 l.178E+OO FAIL ABUN AC-227 1. 748E-01 4.169E-01 4.780E-01 FAIL ABUN TH-227 1. 748E-01 4.169E-01 4.780E-01 FAIL ABUN TH-231 8.816E-02 6.105E-01 l.178E+OO FAIL ABUN PA-233 2.158E-03 6. 096E-02 l.168E-01 FAIL ABUN PA-234 5. 719E-01 4.732E-01 5. 968E-01 FAIL ABUN PA-234M -1. 459E+OO 4. 351E+OO 8.286E+OO NOT IDENT. NP-237 2.158E-03 6. 096E-02 l.168E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF NP-239 1. 473E-01 2.327E-01 4.827E-01 NOT IDENT. -PU-239 O.OOOE+OO 5.744E+02 6.895E+02 FAIL ABUN AM-241 -3.107E-02 l.379E-01 2.326E-01 NOT IDENT. CM-243 l.986E-02 9.940E-02 l.840E-01 NOT IDENT. BK-247 -l.230E-02 7.877E-02 l.335E-01 NOT IDENT. CM-247 l.685E-03 3.922E-02 7.085E-02 NOT IDENT. CF-249 l.638E-03 4. 231E-02 7.992E-02 NOT IDENT. CF-251 4.163E-02 l.130E-01 2.261E-01 NOT IDENT. Page 3563 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:10:19.56 Nuclide Line Activity Report .. Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error NA-22 1274.54 15 99.94* l.297E+OO 5.808E-02 7.308E-02 83.90 K-40 1460.82 355 10.66* 1.161E+OO 1.424E+Ol 1.424E+Ol 10.65 Y-91 1204.77 11 0.26* 1.358E+OO 1. 576E+Ol 6.574E+02 57.20 CD-109 88.03 88 3.70* 5.459E+OO 2.169E+OO 3.482E+OO 90.26 SN-126 64.28 ------9.60 3.426E+00 ------Line Not Found ------86.94 88 8.90 5.459E+OO 9.018E-01 9.018E-01 90.26 87.57 88 37.00* 5.459E+OO 2.169E-01 2.169E-01 90.26 BA-137M 661. 66 113 89.90* 2.164E+OO 2.887E-01 2.945E-01 26.26 CS-137 661.66 113 85.10* 2.164E+OO 3.050E-01 3. lllE-01 26.26 TL-208 277.37 ------6.60 4.415E+OO ------Line Not Found ------583.19 132 85.00* 2.392E+OO 3.231E-01 3. 231E-01 25.47 860.56 27 12.50 1. 764E+OO 6.089E-01 6.089E-01 60.00 BI-211 72. 87 ------1.23 4.361E+OO ------Line Not Found ------351. 06 300 12.92* 3.630E+OO 3.182E+OO 3.182E+OO 17 .11 BI-212 727. 33 28 6.67* 2.0lOE+OO 1.025E+OO l.025E+00 95.99 785'. 37 18 1.10 1. 892E+OO 4.277E+00 4.277E+OO 105.50 1620.50 ------1. 47 1.063E+OO ------Line Not Found ------PB-212 74.82 169 10.28 4.533E+OO 1.797E+OO 1. 797E+00 39.57 77 .11 265 17 .10 4.743E+OO 1.624E+OO 1.624E+OO 22.16 238.63 468 43.60* 4.961E+00 1.074E+OO 1.074E+00 12.45 300.09 35 3.30 4.139E+00 1.262E+OO 1.262E+00 113. 35 BI-214 609.32 160 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 1120.29 41 14.92 1.437E+OO 9.465E-01 9.468E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 PB-214 74.82 169 5.80 4.533E+OO 3.185E+OO 3.186E+OO 39.57 77 .11 265 9.70 4.743E+00 2.862E+OO 2.863E+OO 22.16 87.09 88 3.41 5.459E+OO 2.354E+OO 2.355E+OO 90. 26 242.00 169 7.25 4.913E+OO 2.362E+OO 2.362E+OO 41. 46 295.22 158 18.42 4.198E+OO 1.015E+OO 1.016E+OO 29.18 351. 93 300 35.60* 3.630E+OO 1.155E+00 1.155E+OO 17 .11 RN-222 609.32 160 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 1120. 29 41 14.92 1.437E+OO 9.465E-01 9.468E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO 1. 052E+OO 36.70 RA-224 240.99 169 4.10* 4.913E+OO 4.176E+OO 4.176E+OO 41.46 RA-226 609.32 160 45.49* 2.309E+OO 7.574E-01 7.577E-01 24.87 1120.29 41 1'4. 92 1.437E+OO 9.465E-01 9.468E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 AC-228 105.21 ------1.10 6.259E+00 ------Line Not Found ------338.32 63 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 794.95 ------4.25 1.875E+OO ------Line Not Found ------835.71 ------1. 61 1. 803E+OO ------Line Not Found ------911.20 75 25.80* 1.687E+00 8.586E-01 8.586E-01 35.02 968. 97 53 15.80 1. 609E+OO 1.038E+OO 1.038E+OO 32.48 RA-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 63 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 794.95 ------4.25 1. 875E+OO ------Line Not Found ------835. 71 ------1. 61 1. 803E+OO ------Line Not Found ------Page 3564 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911.20 75 25.80* 1.687E+OO 8.586E-01 8.58.6E-01 35.02 968. 97 53 15.80 1.609E+OO 1. 038E+OO 1.038E+OO 32.48 TH-228 74.82 169 10.28 4.533E+OO 1. 797E+OO 1.797E+OO 39.57 77 .11 265 17.10 4.743E+OO 1. 624E+OO 1.624E+OO 22.16 238.63 468 43.60* 4. 961E+OO 1. 074E+OO l.074E+OO 12.45 300.09 35 3.30 4.139E+OO 1. 262E+OO 1.262E+OO 113.35 TH-229 85.43 88 14.70 5.459E+OO 5.460E-01 5.460E-01 90.26 88.47 74 24.00 5.640E+OO 2.705E-01 2.705E-01 56.87 193.51 ------4.41* 5. 711E+OO ------Line Not Found ------210.85 47 2.80 5.435E+OO 1. 529E+OO 1. 529E+OO 101.84 TH-230 609.32 160 45.49* 2.309E+OO 7.574E-01 7.574E-01 24.87 1120.29 41 14.92 1.437E+OO 9.465E-01 9.465E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 PA-231 283.69 ------1. 70 4.336E+OO ------Line Not Found ------301.36 35 5.35* 4.139E+OO 7.782E-01 7.782E-01 113. 35 TH-232 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 63 11. 27 3.748E+OO 7.358E-01 7.358E-01 58.98 835.71 ------1. 61 1.803E+OO ------Line Not Found ------911.20 75 25.80* 1.687E+OO 8.586E-01 8.586E-01 35.02 968. 97 53 15.80 1.609E+OO 1.038E+OO 1.038E+OO 32.48 TH-234 63.29 29 3.70* 3.208E+OO l.207E+OO 1.207E+OO 239.06 92.59 93 4.23 5.793E+OO 1.879E+OO l.879E+OO 71. 76 U-234 609.32 160 45.49* 2.309E+OO 7.574E-01 7.574E-01 24.87 1120.29 41 14.92 1.437E+OO 9.465E-01 9.465E-01 46.85 1764.49 32 15.30 9.862E-01 1.052E+OO 1.052E+OO 36.70 U-235 89.96 74 3.47 5.640E+OO 1. 871E+OO 1. 871E+OO 56.87 93.35 93 5.60 5.793E+OO l.419E+OO l.419E+OO 71. 76 143.76 45 10.96* 6.467E+OO 3.153E-01 3.153E-01 114.86 163.33 ------5.08 6.216E+OO ------Line Not Found ------185.72 85 57.20 5.841E+OO 1.258E-01 l.258E-01 71. 50 205.31 ------5.01 5.506E+OO ------Line Not Found ------U-238 63.29 29 3.70* 3.208E+OO 1.207E+OO 1.207E+OO 239.06 92.59 93 4.23 5.793E+OO 1. 879E+OO 1.879E+OO 71. 76 AM-243 43.53 ------5.90 5.190E-01 ------Line Not Found ------74.66 169 67.20* 4.533E+OO 2.749E-01 2.749E-01 39.57 ANH-511 511. 00 52 100.00* 2.663E+00 9.783E-02 9.783E-02 79.36 Flag: "*" Key line Page 3565 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235029 Acquisition date 3-0CT-2016 09:08:53 Total number of lines in spectrum 51 Number of unidentified lines 11 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide NA-22 K-40 Y-91 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 2.60Y l.25E+09Y 58.510 461.40D 2.30E+05Y 30.08Y 30.08Y 1.41E+10Y 7.04E+08Y l.41E+l0Y 1. 41E+10Y 1600.00Y 1600.00Y 1600. OOY l.41E+l0Y 1600. OOY 1. 41E+l0Y 1. 41E+l0Y 1.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 26 1. 00 41. 7 1. 60 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 5.808E-02 1. 424E+Ol 1. 576E+Ol 2.169E+OO 2.169E-01 2.887E-01 3.050E-01 3.231E-01 3.182E+OO l.025E+OO l.074E+00 7.574E-01 l.155E+OO 7.574E-01 4.176E+00 7.574E-01 8.586E-01 8.586E-01 1. 074E+OO 2.705E-01 7.574E-01 7.782E-01 8.586E-01 l.207E+00 7.574E-01 3.153E-01 1. 207E+OO 2.749E-01 9.783E-02 5.556E+Ol 5.556E+Ol Decay Corr pCi/GRAM 7.308E-02 1.424E+Ol 6.574E+02 3.482E+OO 2.169E-01 2.945E-01 3. lllE-01 3.231E-01 3.182E+OO 1.025E+OO 1.074E+OO 7.577E-01 1. 155E+OO 7.577E-01 4.176E+OO 7.'577E-01 8.586E-01 8.586E-01 l.074E+00 2.705E-01 7.574E-01 7.782E-01 8.586E-01 l.207E+00 7.574E-01 3.153E-01 1.207E+00 2.749E-01 9.783E-02 6.986E+02 6.986E+02 78.43% Decay Corr 2-Sigma Error 6.132E-02 0.152E+Ol 3.760E+02 3.142E+OO l.958E-01 0.773E-01 0.817E-01 0.823E-01 0.544E+OO 0.984E+OO 0.134E+OO l.884E-01 0.198E+OO 1.884E-01 1. 731E+OO 1.884E-01 3.007E-01 3.007E-01 0.134E+OO 1.539E-01 l.883E-01 8.821E-01 3.007E-01 2.886E+00 l.883E-01 3. 621E-01 2.886E+OO 1.088E-01 7.763E-02 "M" Manually accepted
  • 2-Sigma %Error 83.90 10.65 57.20 90. 26 90. 26 26.26 26.26 25.47 17 .11 95.99 12.45 24.87 17 .11 24.87 41. 46 24.87 35.02 35.02 12.45 56.87 24.87 113. 35 35.02 239.06 24.87 114.86 239.06 39.57 79.36 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3566 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235029 Acquisition date : 3-0CT-2016 09:08:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.14 62 143 0.79 259.12 256 8 1.41E-02 78.5 6.54E+OO T 0 255.93 16 93 0.57 512.80 509 9 3.79E-03 **** 4.70E+OO T 0 274.31 94 232 8.38 549.58 533 28 2.28E-02 **** 4.45E+OO T 0 1410.33 32 75 2.16 821. 74 812 .13 7.98E-03 **** 3.19E+OO T 0 625.69 18 8 0.91 1252.65 1249 8 4. 72E-03 75.3 2.26E+OO 1 723. 01 15 36 1. 98 1447.36 1440 27 4.06E-03 **** 2.02E+OO T 0 748.16 15 10 1. 39 1497.69 1494 10 3.92E-03 **** 1.97E+OO T 8 781.40 13 16 2.20 1564.19 1561 17 3.50E-03 **** 1.90E+OO 0 804.73 17 25 1. 55 1610.87 1605 12 4.61E-03 **** 1. 86E+OO 0 946.99 23 13 4.32 1895.53 1886 17 6.21E-03 84.4 1. 64E+OO T 4 963. 76 18 15 2.84 1929.07 1920 23 4.95E-03 **** 1. 62E+OO T 0 1063.76 10 22 1. 73 2129.16 2121 15 2.67E-03 **** 1.50E+OO T 0 1134. 69 13 15 3.50 2271.08 2263 15 3. 61E-03 **** 1.42E+OO 0 1143.20 15 12 3.51 2288.11 2282 12 4.16E-03 **** 1.41E+OO 0 1168. 70 19 12 1. 24 2339.14 2333 13 5.26E-03 90.3 1.39E+OO 0 1200.59 13 9 3.91 2402.95 2394 14 3.55E-03 **** 1.36E+OO 3 1207.52 13 1 2.05 2416.82 2407 13 3.70E-03 56.6 1.35E+OO 0 1236.70 32 27 8.17 2475.21 2464 27 8.92E-03 97.0 1.33E+OO T 0 1263.32 9 8 1.37 2528.47 2521 12 2.57E-03 **** 1. 31E+OO 1 1272.80 19 6 2.30 2547.42 2542 19 5.48E-03 63.4 1.30E+OO T 0 1280.93 6 3 1. 39 2563.69 2560 7 1.81E-03 **** 1.29E+OO 0 1511. 05 7 5 1. 34 3024.14 3017 10 1.94E-03 **** 1.13E+OO Flags: "T" = Tentatively associated Page 3567 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:10:34.27 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l *
  • Acquisition date 3-0CT-2016 09:08:53 Sensitivity 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:10:00 Nuclide Library : SOLID *
  • Sample ID G405235029 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.5120E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide NA-22 K-40 Y-91 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.592E-02 1.963E-01 3.970E+02 9.125E-01 6.504E-02 2.978E-02 3.146E-02 2.997E-02 l.678E-01 4.024E-01 4.576E-02 6.542E-02 1.582E-01 6.542E-02 4.905E-01 6.542E-02 1.212E-01 l.212E-01 4.576E-02 4.423E-01 6.540E-02 4. lllE-01 l.212E-01 9.659E-01 6.540E-02 1.528E-01 9.659E-01 4.080E-02 2.626E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-24 Page 3568 of 5809 Le (pCi/GRAM l.256E+Ol NOT IDENT. O.OOOE+OO SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 NB-94 NB-95 NB-95M ZR-95 NB-97 . ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3569 of 5809 l.701E-02 3.761E-01 O.OOOE+OO O.OOOE+OO 7.005E-02 4.361E-01 O.OOOE+OO 4.424E-02 6.015E-01 5. 496E+OO 3.llOE-02 l .132E-01 1.556E+OO 8.631E+OO O.OOOE+OO 1. 917E-01 O.OOOE+OO 0.000E+OO 6.265E-01 6.727E+OO 8.326E-01 O.OOOE+OO 2.123E-01 2.934E-02 9.456E-01 2.560E+OO 1.549E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.975E-02 5.057E-02 7.631E+OO 4.193E-01 4.193E-01 2.503E-02 7. 513E-02 2.409E-01 O.OOOE+OO O.OOOE+OO 1.178E-01 1.998E+OO 9.828E-02 2.992E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.459E-02 O.OOOE+OO 5.580E-02 1.221E-01 O.OOOE+OO O.OOOE+OO 1.135E-01 O.OOOE+OO O.OOOE+OO 2.923E+Ol O.OOOE+OO 3.710E-01 4.951E-02 4.335E+OO 4.144E-02 0.000E+OO 7.308E+02 O.OOOE+OO 2.162E-02 8.553E-02 1. 765E-01 l.112E-01 9.483E-02 2.294E+OO 4.085E-02 1. 728E+Ol 2.189E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT .. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-24i CM-243 BK-247 CM-247 CF-249 CF-251 Page 3570 of 5809 5.959E-02 2.190E-02 5.107E+OO 7.907E-01 2.900E+OO 3.830E+Ol 1.203E+02 4.643E-01 2.739E+OO 1. 208E-01 2.914E+OO 5. 911E-01 3.638E-01 5.439E-01 2.233E-01 2.233E-01 5.439E-01 5.388E-02 2.637E-01 3.626E+OO 5.388E-02 O.OOOE+OO 2.275E-01 3.275E+02 l.091E-01 8.638E-02 6.165E-02 3.244E-02 3.680E-02 1.062E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:10:40.06 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235029.CNF;l *
  • Acquisition date 3-0CT-2016 09:08:53 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.76 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:10:00 Nuclide Library : SOLID *
  • Sample ID G405235029 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity 1.5120E+02 GRAM *
  • Quantity Err(%) 1.3227E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1 . 96-sigma ) (1.96-sigma) NA-22 7.308E-02 6.015E-02 6.015E-02 K-40 l.424E+Ol 1.663E+OO 1.663E+OO Y-91 6.574E+02 3.693E+02 3.693E+02 CD-109 1.980E+OO 3 .119E+OO 3 .119E+OO SN-126 l.234E-01 1.942E-01 1.942E-01 BA-137M 2.945E-01 7.686E-02 7.686E-02 CS-137 3. lllE-01 8 .119E-02 8 .119E-02 TL-208 3. 231E-01 8.180E-02 8. lBOE-02 BI-211 3.842E-01 9.768E-01 9.768E-01 BI-212 1.025E+OO 9.654E-01 9.654E-01 PB-212 1.074E+OO 1.428E-01 l.428E-01 BI-214 7.577E-01 1. 875E-01 1. 875E-01 PB-214 1.155E+OO 1. 996E-01 1. 996E-01 RN-222 7.577E-01 1.875E-01 1. 875E-01 RA-224 2. 381E+OO 1. 781E+OO 1. 781E+OO RA-226 7.577E-01 1.875E-01 1. 875E-01 AC-228 8.586E-01 2.980E-01 2.980E-01 RA-228 8.586E-01 2.980E-01 2.980E-01 TH-228 1.074E+OO 1.428E-01 1.428E-01 TH-229 l.099E-01 4.781E-01 4.781E-01 TH-230 7.574E-01 l.874E-01 1. 874E-01 PA-231 7.782E-01 8.802E-01 8.802E-01 TH-232 8.586E-01 2.980E-01 2.980E-01 TH-234 l.207E+OO 2.841E+OO 2.841E+OO U-234 7.574E-01 l.874E-01 l.874E-01 U-235 3.153E-01 3.553E-01 3.553E-01 U-238 1.207E+OO 2.841E+OO 2.841E+OO AM-243 l.873E-01 l.107E-Ol l.107E-01 ANH-511 9.783E-02 7.619E-02 7.619E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.453E+Ol 1. 672E+Ol 1. 796E+Ol NOT IDENT. Page 3571 of 5809 NA-24 1.000E+41 3.370E+41 O.OOOE+OO SHORT HLIF AL-26 5.527E-03 1.712E-02 l.730E-02 NOT IDENT. SC-46 4.859E-02 4.254E-01 4.259E-01 FAIL ABUN V-48 8.593E+03 2.902E+04 2.927E+04 SHORT HLIF CR-51 2.128E+02 6.550E+02 6.619E+02 SHORT HLIF MN-54 5.341E-02 7.342E-02 7. 727E-02 NOT IDENT. C0-56 -1.196E-01 5.203E-01 5.230E-01 NOT IDENT. MN-56 -1.000E+41 4.574E+41 0.000E+OO SHORT HLIF C0-57 -1.255E-02 4. 811E-02 4.844E-02 NOT IDENT. C0-58 -4 ..,650E-03 7.415E-01 7.415E-01 NQT IDENT. FE-59 -3.147E+OO 7.188E+OO 7.326E+OO NOT IDENT. C0-60 1. 764E-03 3.682E-02 3.683E-02 NOT IDENT. ZN-65 -1.572E-01 l.984E-01 2.107E-01 NOT IDENT. GE-68 -9.278E-01 2.040E+OO 2.083E+OO NOT IDENT. AS-73 -5.050E-01 9.792E+OO 9.795E+OO NOT IDENT. AS-74 6.443E+03 l.048E+04 l.087E+04 SHORT HLIF SE-75 -1.882E-02 2.424E-01 2.426E-01 NOT IDENT. BR-77 1.573E+40 1.430E+41 O.OOOE+OO SHORT HLIF SR-82 3.226E+02 1.113E+03 l.123E+03 SHORT HLIF RB-83 l.073E-01 7.245E-01 7.261E-01 NOT IDENT. KR-85 -3.223E-01 8.982E+OO 8.983E+OO NOT IDENT. SR-85 -4.160E-02 1.112E+OO 1.112E+OO NOT IDENT. RB-86 -l.883E+04 4.142E+04 4.228E+04 SHORT HLIF Y-88 8. 967E-02 2.205E-01 2.242E-01 NOT IDENT. NB-94 4.531E-03 3.256E-02 3.263E-02 NOT IDENT. NB-95 3.129E-01 1.035E+OO l.045E+00 NOT IDENT. NB-95M -5.126E-02 3.181E+OO 3 .181E+OO NOT IDENT. ZR-95 4.002E-01 1.703E+OO 1. 713E+00 FAIL ABUN NB-97 -1.000E+41 2.803E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 1. 001E+41 O.OOOE+OO SHORT HLIF M0-99 2.584E+33 7.077E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 l.352E+41 O.OOOE+OO SHORT HLIF RH-101 -6.025E-03 3.589E-02 3.600E-02 NOT IDENT. RH-102 2.108E-02 5.717E-02 5.795E-02 NOT IDENT. RU-103 5.562E+OO 8.287E+OO 8.658E+OO FAIL ABUN RH-106 -1.176E-01 5.939E-01 5. 963E-01 NOT IDENT. RU-106 -1.176E-01 5.939E-01 5. 963E-01 NOT IDENT. AG-108M -l.943E-03 2.940E-02 2.941E-02 FAIL ABUN AG-llOM -6.504E-02 9.872E-02 1.030E-01 NOT IDENT. SN-113 -1.233E-01 2.916E-01 2. 969E-01 NOT IDENT. CD-115 -1.000E+41 2.080E+41 0.000E+OO SHORT HLIF SN-117M -4.185E+04 1. 976E+05 l.985E+05 SHORT HLIF TE-123M -2.844E-02 1.300E-01 l.307E-01 NOT IDENT. SB-124 1. 719E-01 2.269E+OO 2.271E+OO FAIL ABUN SB-125 -6. 711E-02 1. 221E-01 l.258E-01 NOT IDENT. TE-125M 3.728E+Ol 3.486E+02 3.490E+02 NOT IDENT. I-126 3.262E+05 l.936E+06 l.942E+06 SHORT HLIF SB-126 8.123E+04 3.089E+06 3.089E+06 SHORT HLIF SB-127 -1.859E+23 4.455E+23 0.000E+OO SHORT HLIF I-131 3.083E+09 2.150E+l0 2 .155E+l0 SHORT HLIF I-132 -l.000E+41 l.944E+42 O.OOOE+OO SHORT HLIF TE-132 -3.774E+27 1. 080E+28 O.OOOE+OO SHORT HLIF BA-133 -7.632E-03 4.557E-02 4.570E-02 NOT IDENT. I-133 -l.000E+41 7.518E+41 O.OOOE+OO SHORT HLIF CS-134 4.499E-02 5.831E-02 6.174E-02 NOT IDENT. CS-135 2.104E-02 l.352E-01 l.355E-01 NOT IDENT. I-135 1.000E+41 7.389E+41 O.OOOE+OO SHORT HLIF CS-136 9.174E+04 7. 601E+05 7.612E+05 SHORT HLIF CE-139 -2.342E-02 1. 251E-01 l.255E-01 NOT IDENT. BA-140 8.583E+04 3.081E+06 3. 081E+06 SHORT HLIF LA-140 -8.895E+05 1. 064E+06 l.137E+06 SHORT HLIF CE-141 -2.317E+00 3.524E+Ol 3.525E+Ol NOT IDENT. CE-143 l.OOOE+41 1.230E+41 O.OOOE+OO SHORT HLIF CE-144 l.442E-01 4.300E-01 4.348E-01 NOT IDENT. PM-144 -l.616E-02 5.746E-02 5.792E-02 NOT IDENT. PR-144 -1.415E+OO *5. 030E+OO 5.070E+00 NOT IDENT. PM-146 3.302E-02 4.424E-02 4.668E-02 FAIL ABUN ND-147 4.440E+07 9.125E+07 9.342E+07 SHORT HLIF PM-147 -3.599E+02 8.053E+02 8.214E+02 NOT IDENT. PM-149 -1.000E+41 1.368E+41 O.OOOE+OO SHORT HLIF EU-150 -5.813E-03 2.843E-02 2.855E-02 FAIL ABUN EU-152 2.077E-02 9.564E-02 9.609E-02 FAIL ABUN GD-153 6.480E-02 2.002E-01 2.023E-01 NOT IDENT. EU-154 1.778E-01 1. 464E-01 l.669E-01 FAIL ABUN EU-155 2.016E-02 l.094E-01 l.098E-01 FAIL ABUN TB-160 1.846E+00 2.384E+OO 2.525E+OO FAIL ABUN H0-166M -1.935E-02 4.933E-02 5.009E-02 FAIL ABUN TM-171 -5.108E+OO 1.996E+Ol 2.009E+Ol NOT IDENT. Page 3572 of 5809 HF-172 2.179E-02 2.579E-01 2.581E-01 FAIL ABUN LU-172 -3.290E-02 7.649E-02 7.791E-02 FAIL ABUN LU-176 l.887E-03 2.750E-02 2.751E-02 NOT IDENT. HF-181 1.695E-01 5.978E+OO 5.978E+OO NOT IDENT. TA-182 -7.827E-01 1. 081E+OO l.138E+OO FAIL ABUN RE-183 -3.873E-01 3.612E+OO 3.616E+OO NOT IDENT. RE-184 l.204E+Ol 4.245E+Ol 4.279E+Ol NOT IDENT. W-188 -2. 611E+Ol l.556E+02 1.560E+02 FAIL ABUN IR-192 -l.159E-01 5.398E-01 5.423E-01 FAIL ABUN HG-203 -1.561E+OO. 3.604E+OO '! 3. 672E+OO NOT IDENT. BI-207 4.348E-02 1.364E-01 1.378E-01 FAIL ABUN PB-210 -1.349E+OO 3.391E+OO 3.445E+OO NOT IDENT. PB-211 -2.626E-01 8.083E-01 8.170E-01 NOT IDENT. RN-219 5.338E-02 4.152E-01 4.159E-01 NOT IDENT. RA-223 8.816E-02 6.105E-01 6 .118E-01 FAIL ABUN AC-227 1.748E-01 4.176E-01 4.249E-01 FAIL ABUN TH-227 l.748E-01 4.176E-01 4.249E-01 FAIL ABUN TH-231 8.816E-02 6.105E-01 6.118E-01 FAIL ABUN PA-233 2.158E-03 6.096E-02 6. 096E-02 FAIL ABUN PA-234 5. 719E-01 8.074E-01 8.476E-01 FAIL ABUN PA-234M -l.459E+OO 4.352E+OO 4.401E+OO NOT IDENT. NP-237 2.158E-03 6.096E-02 6. 096E-02 FAIL ABUN NP-238 l.000E+41 3.756E+41 O.OOOE+OO SHORT HLIF NP-239 1.473E-01 2.330E-01 2.423E-01 NOT IDENT. PU-239 7.470E+02 5.753E+02 6.666E+02 FAIL ABUN AM-241 -3.107E-02 1. 37 9E-01 1.386E-01 NOT IDENT. CM-243 l.986E-02 9.941E-02 9.982E-02 NOT IDENT. BK-247 -l.'230E-02 7.881E-02 7.900E-02 NOT IDENT. CM-247 l.685E-03 3.922E-02 3.922E-02 NOT IDENT. CF-249 l.638E-03 4. 231E-02 4.232E-02 NOT IDENT. CF-251 4.163E-02 l.131E-01 l.147E-01 NOT IDENT. Page 3573 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 53.6616 879.38 112.8485 482.18 100.1077 45.60 62. 8962 87.57 112.8741 133.52 92.4598 46.54 79.9083 87.09 112.8991 264.66 89.2840 49. 72 0.0000 87.57 112.9795 122.06 100.4969 51. 35 69.3568 88.03 87.2150 140.51 0.0000 51. 87 78.5368 88.34 87.2545 143.76 77.0593 52.39 77.4805 193.51 87. 2715 144.24 81.8637 52.97 75.2901 89. 96 92.3206 145.44 81. 9684 53.44 83.3542 90.64 92.4122 152.43 110.0975 125.81 70.8834 91.11 0.0000 153.25 0.0000 57.36 0.0000 63.29 92.6714 154.21 88.4151 57.53 81. 7246 143.76 92.7717 156.02 0.0000 57.98 86.0189 94.56 89.6704 158.56 0.0000 1093.63 87.7696 94.65 92.9427 159.00 70.3743 57.98 87.7779 94.67 92.9456 162.33 73.2574 59.54 83.1923 94.87 92.9717 162.66 0.0000 60. 96 77. 23'44 97.43 83.4825 163.33 66.2621 61.17 88.0817 311. 90 78.6802 165.86 92 .1119 62.93 88.3663 946.00 78.6816 176.31 78.7268 63.29 88.4241 99.53 75.1051 1048.07 0.0000 63.58 88.4705 1221.41 107.2021 177.52 71.6512 64.28 97.9062 265.00 79.0664 739.50 0.0000 66.73 112.3799 103.18 73.0014 181.52 78.2110 67.24 106.6219 103.37 73.0199 711.68 63.5464 67.68 103.1861 116.74 73.0199 185.72 78.5128 67.75 96.1619 105.21 74.4388 193.51 77.2448 69.67 106.6782 105.31 74.4484 197.03 88.4233 70.83 111. 6041 106.12 78.2544 127.23 71.1644 72.81 98.1750 106.47 78.2900 306.78 85.1299 279.20 98.1851 109.28 82.3177 203.43 78.8307 72. 87 98.1851 111. 00 88.7489 205.31 68.8576 74.66 98.4751 228.16 0.0000 210.85 71.0243 74.82 98.5004 114.06 85.3279 215.65 72. 2339 1063.66 98.5245 116. 30 0.0000 222 .11 80.0616 238.63 98.8665 116.74 73.8615 2 90. 67 77.5769 351. 93 98.8665 119.76 81. 7165 177.52 74.7908 78.74 98.7248 121.12 86.9136 228.16 0.0000 79.69 86.1152 121.22 86.9241 228.18 74.8381 80.12 86.1735 121. 78 86.1382 235.69 74.8086 80.19 0.0000 122.06 86.1673 256.23 65.8828 80.57 95.8154 122.92 83.7191 238.63 66.0181 81. 00 97.4775 123.07 86. 2711 238.98 0.0000 81. 07 110.2734 123.68 82.9482 240.99 66.1377 81. 75 100.7908 125.81 87.8240 242.00 66.1883 323.87 93.0818 127.23 84.1448 344.28 66.3235 84.00 93 .1119 127.91 88.0399 252.40 0.0000 85.43 112. 6192 129.30 85.1990 252.80 48.6146 86.55 112.8086 131.20 96. 0583 254.15 0.0000 Page 3574 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 256.23 56.3820 351. 93 42.7203 583.19 26.1651 260.90 0.0000 507.63 0.0000 584.27 26.1773 264.66 49.0348 356.01 39.7633 595.83 0.0000 264.80 51.9247 364.49 0.0000 600.60 28.6407 265.00 51. 9313 366.42 0.0000 602.52 0.0000 268.22 50.1232 372. 51 32.9355 604. 72 30.9825 269.46 50.1666 129.30 38.1359 607.14 33.3094 270.03 50.1867 377.52 35.0922 609.32 33.3377 271.23 50.2290 383.85 45.5737 497.08 33.3507 273.65 0.0000 388.16 44.6429 433.94 10.3663 356.01 50.4110 388.63 0.0000 696. 49 23.0705 277.37 50.4448 391.69 49.9297 620.36 11. 5454 277.60 50.4533 400.66 39.7194 621. 93 22.5278 278.00 50.4670 401.81 39.7434 667.71 0.0000 279.20 61.1927 402.40 38.9195 631. 29 16.2319 279.54 64.1215 404.85 42.4273 453.88 23.2064 279.70 64.1295 410.95 39.4104 595.83 0.0000 280.46 55.4136 413.71 52.0973 635.95 24.3915 283.69 58.4583 414.70 0.0000 636.99 0.0000 364.49 0.0000 423. 72 0.0000 645.85 30.3132 285.41 56.5757 404.85 39.2116 884.68 32.3224 285.90 0.0000 427.87 46.6479 657.90 0.0000 402.40 46.8877 433.94 34.0306 661.66 22.8698 290.67 52.8618 333.97 33.0573 664.57 0.0000 293.27 0.0000 453.88 23.6288 666.33 0.0000 295.22 55.9679 463.37 20.5006 720.70 0.0000 295. 96 55.9946 468.07 25.9541 667.71 0.0000 298.58 56.0920 685.70 0.0000 677. 62 17.6953 299.98 56.1430 475.06 34.7207 685.70 0.0000 300.09 56.1476 476.78 33.6628 695.00 0.0000 300.13 56.1488 477.60 40.1940 696. 49 23.1610 301.36 56.1940 482.18 30.4826 696. 51 23.1610 302.85 56.2485 1596.21 0.0000 697.00 0.0000 304.50 47.4180 527.90 0.0000 697.30 21.3853 537.26 0.0000 497.08 26.3081 697.49 22.2778 306.78 46.0043 505.52 19.8073 702.65 24.1046 316.51 43.5775 507.63 0.0000 706.68 24.1383 311. 90 46.6519 511. 00 34 .1964 711. 68 18.8076 316.51 46.7877 514.00 38.1078 720.70 0.0000 531. 02 0.0000 514.00 38.1078 721. 93 0.0000 320.08 0.0000 520.40 22.1549 1690.97 20.6788 427.87 48.9183 238.98 0.0000 722.91 20.6795 323.87 46.0037 522.65 0.0000 1274.44 20.6823 325.23 54.0505 527.90 0.0000 724.19 20.6886 328.76 0.0000 528.26 25.5662 727.33 20.7111 388.16 51.9065 520.40 28.9178 733.00 14.4360 333.97 45.2838 529.87 0.0000 735.93 25.8048 334.37 49.8243 531.02 0.0000 737.46 14.4580 338.28 45.4019 537.26 0.0000 739.50 0.0000 911.20 45.4037 546.56 0.0000 747.24 20.3089 340.48 45.4623 552.55 22.4650 748.06 16.3240 340.55 0.0000 563.25 33.8489 752.31 24.7023 344.28 40.5029 795.86 31. 6732 753.82 0.0000 345.93 36.4885 569.50 29.4129 756.73 18.1909 351.06 42.6990 569.70 29.4150 756.80 19.1005 Page 3575of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 763.94 26.4406 984.45 0.0000 1596.21 0.0000 765.81 21. 8950 996.26 16.6176 1620.50 3.3697 766.42 13.6871 1001.03 15.6606 1621.92 3.3706 766.84 14.6016 1002.74 16.6467 1678.03 0.0000 772. 60 0.0000 1004.73 17.6358 1690.97 4.5510 776.52, 0.0000
  • 1021.30 0.0000 1750.46 777.92 0.0000 1025.87 0.0000 1764.49 1. 8441 778.90 20.5235 1028.54 0.0000 1770.23 11. 0760 783.70 0.0000 846.77 11. 8 616 1771.35 3.4618 727. 33 14.6909 1038.76 0.0000 1791.20 0.0000 792.07 25.7655 1046.59 16.8423 1808.65 0.9291 794.95 23.0263 1048.07 0.0000 846.75 0.0000 795.86 21.1898 1049.04 19.8267 1836.06 2.8000 801.95 19.2010 621. 93 19.8340 810.06 20.7313 1063.66 10.9463 810.29 19.2518 1077.00 0.0000 810.45 18.5126 1077.34 11. 9832 810.76 18.5144 1085.87 11. 0087 815.77 0.0000 1093.63 16.0439 818.51 0.0000 1099.45 12.0513 832.01 19.5709 1112. 07 11. 0819 834.85 18.6554 1112.84 13. 0992 835.71 21.4593 1115. 54 17.7461 1260.41 0.0000 609.32 11.1041 846.75 0.0000 889.28 11.104 7 846.77 17.7876 1121.30 11. 3094 856.80 0.0000 1129. 67 14.5705 860.56 14.1023 1131.51 0.0000 702.65 16.0335 1147.95 0.0000 873.19 12.2688 1173.23 6.5445 529.87 0.0000 1177.95 16.3799 879.38 15.1279 1189.05 13.3436 880.51. 17.0250 1204.77 8.2422 883.24 18.9319 1221.41 21.7191 884.68 17.9928 1231. 0,2 18.2435 889.28 15.1729 1235.36 0.0000 903.28 18.0468 1238.28 10.3827 898.04 18.0641 1260.41 0.0000 900. 72 19.0302 1271.87 10.0441 903.28 16.1876 1274.44 10.0500 911.20 20.0425 1274.54 10.0500 912.08 20.0477 1099.45 4.2034 923.98 0.0000 1298.22 0.0000 926.50 16.2970 1312 .11 0.0000 929 .11 13.4313 1332.49 8.4824 937.49 19.2334 1362.66 0.0000 944 .13 0.0000 1365.19 9.6103 946.00 10.6039 1368. 63 0.0000 949.00 10.8059 1384.29 6.4325 954.55 0.0000 1408.01 8. 6196 962. 31 8.7157 1457.56 0.0000 964.08 8.7201 1460.82 4.3564 966 .17 8.7251 696. 51 5.4764 968.97 9.3141 1505.03 5.2740 983.53 0.0000 1584.12 11.1560 Page 3576 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:11:09.21 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date : Z-OCT-2016 11:01:13. Sample date 23-NOV-2015 14:44:00 Acquisition date : 3-0CT-2016 09:09:22. Sample ID G405235030 Sample quantity : l.31120E+02 GRAM Detector name GAM20 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:15.23 0.4% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 3 3 3 3 3 0 0 0 4 4 0 1 1 0 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 63.17* 74.94 77.25 87.53 90.08* 92.88* 129.39 131.32 161.55 186.00* 208.97 238.54* 241.80 270.50 295.18* 300.19 327.64 338.27* 351. 92* 355.92* 416.83 463.17 510.97* 583.15* 609.31* 657.26 661.74* 710. 81 727. 71 860.58 911.09* 922.69 969. 00 1001.87* Page 3577 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 43 159 261 112 53 129 41 24 27 133 59 490 131 21 162 38 36 68 231 13 il 34 40 175 164 19 26 10 37 32 86 17 57 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 187 178 153 173 130 138 111 93 63 130 86 48 65 75 65 69 51 '60 50 34 17 27 53 18 50 9 11 14 39 20 16 10 24 3 1. 39 1.17 1.22 1. 32 1.19 1. 48 1. 36 1.14 1. 56 1. 69 1.23 1.21 1. 85 2.05 1. 27 1. 51 1. 31 1. 03 1. 55 1. 56 1. 33 1. 62 1. 72 1. 56 1. 46 1. 53 0.62 1. 33 1. 38 1. 75 1. 67 4.74 2.10 1. 31 126.50 150.02 154.64 175.17 180.28 185.86 258.84 2 62. 7 0 323.13 372.01 417.91 477.02 483.56 540.93 590.27 600.27 655.16 676.42 703.72 711. 72 833.50 92 6 .18 1021. 77 1166 .14 1218.47 1314.39 1323.34 1421.52 1455.33 1721.19 1822.28 1845.49 1938.18 2003.97 123 145 145 171 171 171 254 254 321 366 415 472 472 539 585 585 650 671 699 699 830 922 1016 1157 1213 1306 1319 1417 1449 1712 1815 1837 1933 2000 9 l.20E-02 60.3 15 4.42E-02 15.9 1.23E+OO 15 7.26E-02 10.4 21 3.llE-02 21.2 2.21E+OO 21 l.46E-02 38.5 21 3.59E-02 21.1 12 l.13E-02 47.8 l.57E+00 12 6.80E-03 72.2 6 7.50E-03 50.3 13 3.69E-02 20.5 9 1. 64E-02 30. 9 26 l.36E-01 5.2 1.lOE+OO 26 3.63E-02 18.0 8 5.75E-03 77.9 20 4.51E-02 11.4 2.45E+OO 20 l.07E-02 41.5 9 9.89E-03 38.0 10 l.88E-02 24.9 17 6.40E-02 8.7 5.15E+OO 17 3.59E-03101.2 6 3.14E-03 64.3 11 9.55E-03 33.0 13 l.llE-02 47.3 18 4.87E-02 9.6 13 4.57E-02 12.0 14 5.14E-03 43.5 9 7. 23E-03 31. 7 9 2.76E....:03 77.6 12 1. 03E-02 37. 4 17 8.87E-03 37.4 13 2. 38E-02 14. 7 12 4.81E-03 42.4 11 1. 59E-02 21. 4 7 2.81E-03 48.7 Peak Search Report (continued) Page : 2 Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1121.07 37 37 1. 65 2242.58 2237 15 l.04E-02 37.9 36 0 1238.15 21 11 2.37 2477.01 2472 9 5.79E-03 36.3 37 0 14n .30 6 4 1. 39 2865.83 2861
  • 8 1.67E-03 70.7 38 0 1460.87* 386 0 2.07 2923.05 2916 13 l.07E-01 5.1 39 0 1504.53 8 3 0.56 3010.52 3004 10 2.31E-03 49.9 40 0 1729.83 18 2 1. 32 3461.94 3457 10 4.92E-03 28.9 41 0 1764.61 44 12 2.38 3531.63 3522 15 1.23E-02 22.4 42 0 1846.37 16 0 1. 04 3695.50 3690 11 4.44E-03 25.0 Flag: "*" = Peak area was modified by background subtraction Page 3578 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:11:11 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID Sample.type Detector name : 23-NOV-2015 14:44:00 G405235030 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:09:22 131.12 GRAM Elapsed live time: Energy tolerance : Errors propagated: Efficiency type : Abundance limit SOLID GAMMA20 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3579 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:15.23 10.00 0.00 % Peak Energy 0.4%

Nuclide Line Activity Report Page : 2 Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.312E+OO 4 1. 507E+Ol. 1.507E+Ol 10.25 OK CD-109 88.03 3.70* 6.859E+OO 1.859E+OO 2.983E+OO 67.66 OK SN-126 64.28 9.60 4. 772E+OO 6.364E-01 6.364E-01 120.63 OK 86.94 8.90 6.859E+OO 7.727E-01 7. 727E-01 67.66 OK 87.57 37.00* 6.859E+OO l.859E-01 1. 859E-01 67.66 OK BA-137M 661. 66 89.90* 2.464E+OO 6.788E-02 6.924E-02 63.43 OK CS-137 661.66 85.10* 2.464E+OO 7.170E-02 7.314E-02 63.43 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.720E+OO 4.419E-01 4.419E-01 19.14 OK 860.56 12.50 2. OllE+OO 7.206E-01 7.206E-01 74. 72 OK PB-212 74.82 10.28 6.006E+OO 1.071E+OO 1.071E+OO 52.68 OK 77 .11 17.10 6.195E+OO 1.641E+OO 1. 641E+OO 20.71 OK 238.63 43.60* 5.554E+OO 1.253E+OO 1.253E+OO 10.39 OK 300.09 3.30 4.645E+00 1.532E+OO l.532E+OO 82.97 OK BI-214 609.32 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 OK 1120.29 14.92 1.635E+OO 8.518E-01 8. 521E-01 75.87 OK 1764.49 15.30 l.106E+00 1.404E+OO 1.405E+OO 44.86 OK PB-214 74.82 5.80 5.996E+OO Line Not Found <<INT Reject 77 .11 9.70 6.195E+OO 2.893E+OO 2.894E+OO 20.71 OK 87.09 3.41 6.836E+OO Line Not Found <<INT Reject 242.00 7.25 5.495E+OO Line Not Found <<INT Reject 295.22 18.42 4.708E+OO l.144E+00 1.144E+OO 22.73 OK 351.93 35.60* 4.083E+OO 9.572E-01 9.576E-01 17.36 OK RN-222 609.32 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 OK 1120. 29 14.92 l.635E+OO 8.518E-01 8. 521E-01 75.87 OK 1764.49 15.30 1.106E+OO 1.404E+OO 1.405E+OO 44.86 OK RA-224 240.99 4.10* 5.498E+OO l.568E+OO 1.568E+OO 87.46 OK RA-226 609.32 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 OK 1120.29 14.92 1. 635E+OO 8.518E-01 8. 521E-01 75.87 OK 1764.49 15.30 1.106E+OO 1.404E+OO 1.405E+OO 44.86 OK AC-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11.27 4.217E+OO 8.632E-01 8.632E-01 49.76 OK 794.95 4.25 2.138E+OO Line Not Found Absent 835.71 1. 61 2.057E+00 Line Not Found Absent 911.20 25.80* l.924E+00 9.747E-01 9.747E-01 29.48 OK 968. 97 15.80 1.834E+OO 1. llOE+OO 1. llOE+OO 42.70 OK RA-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.217E+00 8.632E-01 8.632E-01 49.76 OK 794.95 4.25 2.138E+OO Line Not Found Absent 835.71 1. 61 2.057E+OO Line Not Found Absent 911. 20 25.80* 1.924E+OO 9.747E-01 9.747E-01 29.48 OK 968. 97 15.80 l.834E+OO 1. llOE+OO 1. llOE+OO 42.70 OK TH-228 74.82 10.28 6.006E+OO 1.071E+OO 1. 071E+OO 52.68 OK 77 .11 17.10 6.195E+OO 1.641E+OO 1.641E+OO 20.71 OK 238.63 43.60* 5.554E+OO 1.253E+OO 1.253E+OO 10.39 OK 300.09 3.30 4.645E+OO 1.532E+OO l.532E+00 82.97 OK TH-230 609.32 45.49* 2.628E+OO 7.998E-01 7.998E-01 24.10 OK 1120.29 14.92 1.635E+OO 8.518E-01 8.518E-01 75.87 OK 1764.49 15.30 1.106E+00 1.404E+OO l.404E+00 44.86 OK Page 3580 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status PA-231 283.69

  • 1. 70 4.860E+OO Line Not Found Absent 301.36 5.35* 4.645E+OO 9.449E-01 9.449E-01 82.97 OK TH-232 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.217E+OO 8.632E-01 8.632E-01 49.76 OK 835.71 1. 61 2.057E+OO Line Not Found Absent 911.20 25.80* 1.924E+OO 9.747E-01 9.747E-01 29.48 OK 968. 97 15.80 1.834E+OO 1. llOE+OO 1. llOE+OO 42.70 OK TH-234 63.29 3.70* 4.772E+OO 1.651E+OO 1. 651E+OO 120.63 OK 92.59 4.23 7.103E+OO 2.828E+OO 2.828E+OO 42.14 OK U-234 609.32 45.49* 2.628E+OO 7.998E-01 7.998E-01 24.10 OK 1120.29 14.92 1.635E+OO 8.518E-01 8.518E-01 75.87 OK 1764.49 15.30 1.106E+OO 1.404E+OO 1.404E+OO 44. 86 OK U-235 89.96 3.47 6.984E+OO 1.434E+OO 1.434E+OO 77.01 OK 93.35 5.60 7.103E+OO 2.136E+OO 2.136E+OO 42.14 OK 143.76 10. 96* 7.370E+OO Line Not Found Absent 163.33 5.08 7.024E+OO Line Not Found Absent 185. 72 57.20 6.563E+OO 2.227E-01 2.227E-01 41. 06 OK 205.31 5.01 6.171E+OO Line Not Found Absent U-238 63.29 3.70* 4.772E+OO '1.651E+OO 1. 651E+OO 120.63 OK 92.59 4.23 7.103E+OO 2.828E+OO 2.828E+OO 42.14 OK AM-243 43.53 5.90 1.315E+OO Line Not Found Absent 74.66 67.20* 6.006E+OO 1.639E-01 1.639E-01 52.68 OK ANH-511 511. 00 100.00* 3.019E+OO 7.810E-02 7.810E-02 94.68 OK Flag: "*" = Keyline Page 3581of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:11:12.14 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l * *Acquisition date 3-0CT-2016 09:09:22 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:15.23 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:44:00 Analyst initials: MXRl *
  • Sample ID G405235Q30 Sample Quantity 1.3112E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.507E+Ol l.514E+OO CD-109 2.983E+OO l.978E+OO SN-126 1.859E-01 1.233E-01 BA-137M 6.924E-02 4.304E-02 CS-137 7.314E-02 4.546E-02 TL-208 4.419E-01 8.288E-02 PB-212 1.253E+OO 1. 27 6E-01 BI-214 8. OOlE-01 1. 889E-01 PB-214 9.576E-01 1. 629E-01 RN-222 8.00lE-01 l.889E-01 RA-224 l.568E+00 1. 344E+OO RA-226 8. OOlE-01 l.889E-01 AC-228 9.747E-01 2.816E-01 RA-228 9.747E-01 2.816E-01 TH-228 1.253E+OO 1. 27 6E-01 TH-230 7.998E-01 1.889E-01 PA-231 9.449E-01 7.683E-01 TH-232 9.747E-01 2.816E-01 TH-234 1.651E+OO 1. 952E+OO U-234 7.998E-01 1.889E-01 U-235 -2.216E-02 1.820E-01 U-238 1.651E+OO 1.952E+OO AM-243 1. 639E-01 8.461E-02 ANH-511 7.810E-02 7. 24.7E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3582 of 5809 Key-Line Activity (pCi/GRAM -5.191E+OO -2.891E-02 O.OOOE+OO 3.919E-03 5.750E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.334E+Ol 4.082E-02 1.960E+41 1. 766E-02 3.774E-01 2.440E+04 MDA (pCi/GRAM 3.783E-01 1. 87 6E+OO 1.173E-01 5.190E-02 5.483E-02 4.272E-02 8. 896E-02 1.294E-01 1.188E-01 1.294E-01 9.536E-01 1.294E-01 2.158E-01 2.158E-01 8. 896E-02 l.294E-01 7.239E-01 2.158E-01 1.661E+OO 1. 2 94E-01 3.210E-01 1. 661E+OO 7.554E-02 5.562E-02 MDA (pCi/GRAM 2.434E+Ol 7.116E-02 O.OOOE+OO 4.726E-02 7.455E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 5.321E+02 O.OOOE+OO SHORT HLIF MN-54 3.804E-02 5.866E-02 l.238E-01 NOT IDENT. C0-56 2.432E-02 4.637E-01 8.989E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -5.382E-02 5. 013E-02 8.085E-02 NOT IDENT. C0-58 -2.598E-01 6.789E-01 1.196E+OO NOT IDENT. FE-59 2.421E-01 8.558E+OO 1.708E+Ol NOT IDENT. C0-60 2.369E-02 3. 601E-02 8.216E-02 NOT IDENT. ZN-65 6.554E-02 1.670E-01 3.266E-01 NOT IDENT. -5. 813E-01 2.548E+OO
  • 4.883E+OO NOT IDENT . AS-73 2.459E+OO 6.369E+OO 1.214E+Ol NOT IDENT. AS-74 O.OOOE+OO 1. 068E+04 O.OOOE+OO SHORT HLIF SE-75 -5.855E-02 2.090E-01 3.937E-01 NOT IDENT. BR-77 O.OOOE+OO 1. 790E+39 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 1.060E+03 O.OOOE+OO SHORT HLIF RB-83 -2.797E-01 7.158E-01 1.294E+OO NOT IDENT. KR-85 2.480E+OO 7.227E+OO 1.297E+Ol NOT IDENT. SR-85 3.059E-01 8.933E-01 1.603E+OO NOT IDENT. RB-86 O.OOOE+OO 5.102E+04 O.OOOE+OO SHORT HLIF Y-88 -6.971E-02 2.168E-01 4.233E-01 NOT IDENT. Y-91 -l.463E+02 5.109E+02 9.832E+02 NOT IDENT. NB-94 -6.041E-03 3. 051E-02 5.576E-02 NOT IDENT. NB-95 -3.666E-01 l.205E+OO 2.121E+OO NOT IDENT. NB-95M 2.424E+OO 2.635E+OO 5.031E+OO NOT IDENT. ZR-95 -8.124E-01 1.394E+00 2.384E+OO NOT IDENT. NB-97 O.OOOE+OO 8.517E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 6.694E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 8.237E-03 3.475E-02 5.858E-02 NOT IDENT. RH-102 -4.122E-03 6.028E-02 1.129E-01 NOT IDENT. RU-103 -1.577E+OO 6. 996E+OO 1.300E+Ol FAIL ABUN RH-106 -1.630E-01 5.076E-01 9.176E-01 NOT IDENT. RU-106 -1.630E-01 5.076E-01 9.176E-01 NOT IDENT. AG-108M 1.808E-02 2.465E-02 5.173E-02 NOT IDENT. AG-llOM 2.838E-02 8.461E-02 1.756E-01 FAIL ABUN SN-113 5.595E-02 2.420E-01 4.747E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 2.242E+05 O.OOOE+OO SHORT HLIF TE-123M 5.483E-02 1.550E-01 2.624E-01 NOT IDENT. SB-124 9.869E-02 1.958E+OO 4.383E+OO NOT IDENT. SB-125 2.725E-02 9.345E-02 1.864E-01 FAIL ABUN TE-125M -1.420E+02 3.103E+02 5.351E+02 NOT IDENT. I-126 O.OOOE+OO 1. 881E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.675E+06 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 2.891E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.492E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.342E+27 O.OOOE+OO SHORT HLIF BA-133 3.287E-02 6.517E-02 7.453E-02 FAIL ABUN I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 5.534E-02 5.875E-02 l.214E-01 NOT IDENT. CS-135 8.038E-02 1. 421E-01 2.623E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 5.874E+05 O.OOOE+OO SHORT HLIF CE-139 -4.901E-02 1.118E-01 1. 8 90E-01 NOT IDENT. BA-140 O.OOOE+OO 2.717E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 8.756E+05 O.OOOE+OO SHORT HLIF CE-141 -4.732E+Ol 3.413E+Ol 5.290E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.204E+41 O.OOOE+OO SHORT HLIF CE-144 -l.732E-01 4.037E-01 6.288E-01 NOT IDENT. PM-144 4.007E-02 5. 701E-02 1.174E-01 NOT IDENT. PR-144 3.477E+OO 4.986E+OO 1.026E+Ol NOT IDENT. PM-146 -1.605E-02 3.918E-02 7.140E-02 NOT IDENT. ND-147 O.OOOE+OO 7 .119E+07 0.000E+OO SHORT HLIF PM-147 3:755E+02 7.836E+02 1.464E+03 NOT IDENT. PM-149 0.000E+OO 1.960E+41 O.OOOE+OO SHORT HLIF EU-150 -8.685E-03 2.611E-02 4.296E-02 FAIL ABUN EU-152 5.652E-02 8.423E-02 1.733E-01 NOT IDENT. GD-153 -1.544E-02 l.937E-01 3.200E-01 NOT IDENT. EU-154 -5.707E-02 9.728E-02 1. 749E-01 NOT IDENT. EU-155 1. 721E-02 l.027E-01 1.873E-01 FAIL ABUN TB-160 1.611E+OO 2.126E+OO 4.514E+OO FAIL ABUN H0-166M 4.534E-02 6.894E-02 9.764E-02 FAIL ABUN TM-171 9.197E-01 l.300E+Ol 2.426E+Ol NOT IDENT. HF-172 -7.889E-02 2.624E-01 4.157E-01 FAIL ABUN LU-172 -1.581E-03 8.202E-02 1.616E-01 FAIL ABUN LU-176 -9.895E-03 2.278E-02 4.200E-02 FAIL ABUN Page 3583 of 5809 HF-181 -5.063E-01 4.960E+00 9.421E+OO NOT IDENT. TA-182 3.245E-01 1.046E+OO 2.133E+OO FAIL ABUN RE-183 2.875E-01 2.455E+OO 4.555E+OO FAIL ABUN RE-184 3.007E+Ol 4. 311E+Ol 8.915E+Ol NOT IDENT. W-188 -4.717E+Ol 1. 309E+02 2.163E+02 FAIL ABUN IR-192 -3. 451E-02 4.503E-01 8.673E-01 FAIL ABUN HG-203 -1. 845E+OO 2.597E+OO 4.678E+OO NOT IDENT. BI-207 -4.604E-02 4 .113E-02 6.609E-02 FAIL ABUN PB-210 1.033E+OO l.856E+OO 3.617E+OO NOT IDENT. BI-211 O.OOOE+OO 4.488E-01 8,123E-01 FAIL ABUN PB-211 -4.082E-01 6.342E-01 1.123E+OO NOT IDENT. BI-212 l.398E+OO 1. 024E+OO 1. 446E+OO FAIL ABUN RN-219 1. 717E-01 3.548E-01 7.156E-01 FAIL ABUN RA-223 -2.322E-01 5. 966E-01 9.761E-01 FAIL ABUN AC-227 l.576E-01 2 .'lOlE-01 4.310E-01 FAIL ABUN TH-227 l.576E-01 2.lOlE-01 4.310E-01 FAIL ABUN TH-229 -3.144E-01 4.163E-01 7.625E-01 FAIL ABUN TH-231 -2.322E-01 5. 966E-01 9.761E-01 FAIL ABUN PA-233 5.683E-03 5.437E-02 1.059E-01 FAIL ABUN PA-234 4.956E-02 2.242E-01 4.775E-01 FAIL ABUN PA-234M 3.779E+OO 3.610E+OO 8.733E+OO FAIL ABUN NP-237 5.683E-03 5.437E-02 1.059E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF NP-239 8.044E-02 2.107E-01 3.936E-01 NOT IDENT. PU-239 5.533E+02 5.183E+02 6. 391E+02 FAIL ABUN AM-241 1.108E-01 1.030E-01 1. 921E-01 NOT IDENT. CM-243 5.665E-03 8.751E-02 1.591E-01 NOT IDENT. BK-247 -7.044E-03 6.SOlE-02 l.246E-01 NOT IDENT. CM-247 2. 966E-02 3.276E-02 6.874E-02 NOT IDENT. CF-249 -4.716E-03 3.330E-02 6.312E-02 NOT IDENT. CF-251 8. 311E-02 l.055E-01 2.163E-01 NOT IDENT. Page 3584 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:11:09.92 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 368 10.66* l.312E+OO l.507E+Ol l.507E+Ol 10.25 CD-109 88.03 129 3.70* 6.859E+OO 2.913E+OO 4.675E+OO 42.38 SN-126 64.28 51 9.60 4. 772E+OO 6.364E-01 6.364E-01 120.63 86.94 129 8.90 6.859E+OO 1. 211E+OO 1. 211E+OO 42.38 87.57 129 37.00* 6.859E+OO 2.913E-01 2.913E-01 42.38 BA-137M 661.66 26 89.90* 2.464E+OO 6.788E-02 6.924E-02 63.43 CS-137 661. 66 26 85.10* 2.464E+OO 7.170E-02 7.314E-02 63.43 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 178 85.00* 2. 720E+OO 4.419E-01 4.419E-01 19.14 860.56 32 12.50 2. OllE+OO 7.206E-01 7.206E-01 74.72 BI-211 72.87 ------1. 23 5.823E+OO ------Line Not Found ------351.06 243 12.92* 4.083E+OO 2.638E+00 2.638E+OO 17.36 PB-212 74.82 185 10.28 6.006E+OO l.717E+OO l.717E+OO 31. 74 77 .11 304 17.10 6.195E+OO l.641E+OO 1. 641E+OO 20.71 238.63 530 43.60* 5.554E+OO l.253E+OO l.253E+OO 10.39 300.09 41 3.30 4.645E+OO 'l. 532E+OO l.532E+OO 82.97 BI-214 609.32 167 45.49* 2.628E+OO 7.998E-Ol 8.00lE-01 24.10 1120.29 36 14.92 l.635E+OO 8.518E-01 8. 521E-01 75.87 1764.49 42 15.30 l.106E+OO l.404E+OO l.405E+OO 44.86 PB-214 74.82 185 5.80 6.006E+OO 3.043E+OO 3.044E+OO 31. 74 77 .11 304 9.70 6.195E+OO 2.893E+OO 2.894E+OO 20. 71 87.09 129 3.41 6.859E+OO 3 .161E+OO 3.162E+OO 42.38 242.00 141 7.25 5.498E+OO 2. 031E+OO 2.032E+OO 35.98 295.22 173 18.42 4.708E+OO l.144E+OO l.144E+OO 22.73 351. 93 243 35.60* 4.083E+OO 9. 572E-01 9.576E-01 17.36 RN-222 609.32 167 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 1120.29 36 14.92 l.635E+OO 8.518E-01 8.521E-01 75.87 1764.49 42 15.30 l.106E+OO l.404E+OO l.405E+OO 44.86 RA-224 240.99 141 4.10* 5.498E+OO 3.591E+OO 3.591E+OO 35.98 RA-226 609.32 167 45.49* 2.628E+OO 7.998E-01 8. OOlE-01 24.10 1120.29 36 14.92 l.635E+OO 8.518E-01 8. 521E-01 75.87 1764.49 42 15.30 l.106E+OO l.404E+OO l.405E+OO 44.86 AC-228 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 72 11. 27 4.217E+OO 8.632E-01 8.632E-01 49.76 794.95 ------4.25 2.138E+OO ------Line Not Found ------835.71 ------1. 61 2.057E+OO ------Line Not Found ------911.20 84 25.80* 1. 924E+OO 9.747E-01 9.747E-01 29.48 968.97 56 15.80 l.834E+OO l. llOE+OO l. llOE+OO 42.70 RA-228 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 72 11. 27 4.217E+OO 8.632E-01 8.632E-01 49.76 794.95 ------4.25 2.138E+OO ------Line Not Found ------835.71 ------1. 61 2.057E+OO ------Line Not Found ------911.20 84 25.80* l.924E+OO 9.747E-01 9.747E-01 29.48 968. 97 56 15.80 l.834E+OO l.llOE+OO l. llOE+OO 42.70 TH-228 74.82 185 10. 28 6.006E+OO l.717E+OO l.717E+OO 31. 74 77.11 304 17.10 6.195E+OO 1. 641E+OO 1. 641E+OO 20.71 238.63 530 43.60* 5.554E+OO l.253E+OO l.253E+OO 10.39 Page 3585 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235030 Acquisition date 3-0CT-2016 09:09:22 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 300.09 41 3.. 30 4.645E+OO 1.532E+OO 1.532E+OO 8.2. 97 TH-230 609.32 167 45.49* 2.628E+OO 7.998E-01 7.998E-01 24.10 1120.29 36 14.92 1.635E+OO 8.518E-01 8.518E-01 75.87 1764.49 42 15.30 1.106E+OO 1.404E+OO l.404E+OO 44.86 PA-231 283.69 ------1. 70 4.860E+OO ------Line Not Found ------301.36 41 5.35* 4.645E+OO 9.449E-01 9.449E-01 82.97 TH-232 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 72 11. 27 4.217E+OO 8.632E-01 8.632E-01 49.76 835. 71 ------1. 61 2.057E+OO ------Line Not Found ------911. 20 84 25.80* 1.924E+OO 9.747E-01 9.747E-01 29.48 968. 97 56 15.80 1.834E+OO 1. llOE+OO 1. llOE+OO 42.70 TH-234 63.29 51 3.70* 4.772E+OO l.651E+00 1. 651E+OO 120.63 92.59 148 4.23 7.103E+OO 2.828E+OO 2.828E+OO 42.14 U-234 609.32 167 45.49* 2.628E+00 7.998E-01 7.998E-01 24.10 1120. 29 36 14.92 1.635E+OO 8.518E-01 8.518E-01 75.87 1764.49 42 15.30 1. 106E+OO 1. 404E+OO 1.404E+OO 44.86 U-235 89. 96 61 3.47 6.984E+00 l.434E+00 1.434E+OO 77.01 93.35 148 5.60 7.103E+OO 2.136E+OO 2.136E+OO 42.14 143.76 ------10.96* 7.370E+OO ------Line Not Found ------163.33 ------5.08 7.024E+OO ------Line Not Found ------185. 72 146 57.20 6.563E+OO 2.227E-01 2.227E-01 41. 06 205.31 ------5.01 6.171E+OO ------Line Not Found ------U-238 63.29 51 3.70* 4.772E+OO 1. 651E+OO 1. 651E+OO 120.63 92.59 148 4.23 7.103E+OO 2.828E+OO 2.828E+OO 42.14 AM-243 43.53 ------5.90 1.315E+OO ------Line Not Found ------74.66 185 67.20* 6.006E+00 2.626E-01 2.626E-01 31. 74 ANH-511 511. 00 41 100.00* 3.019E+OO 7.810E-02 7.810E-02 94.68 Flag: "*" Key line Page 3586 of 5809 Summary of Nuclide Activity Sample ID : G405235030 Acquisition date Page : 3 3-0CT-2016 09:09:22 Total number of lines in spectrum 42 Number of unidentified lines 5 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+10Y 1.41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 60 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.507E+Ol 2.913E+OO 2.913E-01 6.788E-02 7.170E-02 4.419E-01 2.638E+OO 1.253E+OO 7.998E-01 9. 572E-01 7.998E-01 3. 591E+OO 7.998E-01 9.747E-01 9.747E-01 1.253E+OO 7.998E-01 9.449E-01 9.747E-01 1.651E+OO 7.998E-01 2.227E-01 1.651E+OO 2.626E-01 7.810E-02 4.029E+Ol 4.029E+Ol Decay Corr pCi/GRAM l.507E+Ol 4.675E+OO 2.913E-01 6.924E-02 7.314E-02 4.419E-01 2.638E+OO l.253E+OO 8.00lE-01 9.576E-01 8.00lE-01 3.591E+00 8. OOlE-01 9.747E-01 9.747E-01 1.253E+OO 7.998E-01 9.449E-01 9.747E-01 1.651E+OO 7.998E-01 2.227E-01 1.651E+OO 2.626E-01 7.810E-02 4.205E+Ol 4.205E+Ol 88.10% ' Decay Corr 2-Sigma Error 0.155E+Ol 1.981E+00 l.235E-01 4.392E-02 4.639E-02 0.846E-01 0.458E+OO 0.130E+OO 1.928E-01 1.663E-01 1.928E-01 1. 292E+OO 1.928E-01 2.873E-01 2.873E-01 0.130E+00 1.927E-01 7.840E-01 2.873E-01 1.992E+OO l.927E-01 0.914E-01 1.992E+OO 0.834E-01 7.395E-02 "M" Manually accepted 2-Sigma %Error 10.25 42.38 42.38 63.43 63.43 19.14 17.36 10.39 24.10 17.36 24.10 35.98 24.10 29.48 29.48 10.39 24.10 82.97 29.48 120.63 24.10 41. 06 120.63 31. 74 94.68 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3587 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235030 Acquisition date : 3-0CT-2016 09:09:22 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 129.39 46 125 1. 36 258.84 254 12 1.13E-02 95.6 7.54E+OO T 3 131.32 28 105 1.14 262. 70 254 12 6.80E-03 **** 7.52E+OO T 0 161. 55 30 70 1. 56 323.13 321 6 7.50E-03 **** 7.06E+OO T 0 208.97 64 94 1. 23 417.91 415 9 l.64E-Q2 61. 7 6.lOE+OO 0 270.50 22 81 2.05 540.93 539 8 5.75E-03 **** 5.05E+OO T 0 327.64 38 54 1. 31 655.16 650 9 9.89E-03 76.1 4.33E+OO T 1 355.92 14 35 1. 56 711. 72 699 17 3.59E-03 **** 4.05E+OO T 0 416.83 12 17 1.33 833.50 830 6 3.14E-03 **** 3.56E+OO 0 463.17 36 28 1. 62 926.18 922 11 9.55E-03 66.1 3,27E+OO T 0 657.26 19 10 1. 53 1314.39 1306 14 5.14E-03 86.9 2.48E+OO T 0 710.81 10 14 1. 33 1421.52 1417 9 2.76E-03 **** 2.33E+00 T 0 727.71 37 39 1. 38 1455.33 1449 12 1. 03E-02 74.7 2.29E+OO T 0 922.69 17 10 4.74 1845.49 1837 12 4.81E-03 84.8 1. 91E+OO T 0 1001.87 10 3 1. 31 2003.97 2000 7 2.81E-03 97.5 1.79E+OO T 0 1238.15 20 11 2.37 2477.01 2472 9 5.79E-03 72.6 1. 51E+00 T 0 1432.30 6 4 1. 39 2865.83 2861 8 1. 67E-03 **** 1.33E+00 0 1504.53 8 3 0.56 3010.52 3004 10 2.31E-03 99.9 1.28E+OO T 0 1729,.83 17 2 1. 32 3461. 94 3457 10 4.92E-03 57.9 1.13E+OO 0 1846.37 15 0 1. 04 3695.50 3690 11 4.44E-03 50.0 1. 06E+OO Flags: "T" = Tentatively associated Page 3588 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:11:23.75 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l * *Acquisition date 3-0CT-2016 09:09:22 Sensitivity 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:15.23 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:44:00 Nuclide Library : SOLID *
  • Sample ID G405235030 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.3112E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.337E-01 8.871E-01 5.546E-02 2.234E-02 2.360E-02 1. 796E-02 4.120E-02 5.814E-02 5.393E-02 5.814E-02 4.416E-01 5.814E-02 9.220E-02 9.220E-02 4.120E-02 5.812E-02 3.300E-01 9.220E-02 7.849E-01 5.812E-02 1. 506E-01 7.849E-01 3.576E-02 2. 521E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3589 of 5809 Le (pCi/GRAM 1.074E+01 2.894E-02 O.OOOE+OO 1. 646E-02 3.189E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3590 of 5809 5.427E-02 3.847E-01 O.OOOE+OO 3.766E-02 5.167E-01 7.425E+OO 3.496E-02 l.404E-01 2.121E+OO 5.709E+OO O.OOOE+OO 1.806E-01 O.OOOE+OO O.OOOE+OO 5.732E-01 5.846E+00 7.226E-01 O.OOOE+OO 1.551E-01 4.109E+02 2.454E-02 9.533E-01 2.343E+OO 9. 960E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.742E-02 5.004E-02 5.773E+OO 4.039E-01 4.039E-01 2.333E-02 7.472E-02 2.157E-01 O.OOOE+OO O.OOOE+OO 1.229E-01 1.662E+OO 8.378E-02 2.498E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.393E-02 O.OOOE+OO 5.498E-02 1.214E-01 O.OOOE+OO O.OOOE+OO 8. 751E-02 O.OOOE+OO O.OOOE+OO 2.459E+Ol O.OOOE+OO 2.937E-01 5.263E-02 4.600E+OO 3.163E-02 O.OOOE+OO 6.855E+02 O.OOOE+OO l.951E-02 7.919E-02 1.506E-01 7.132E-02 8.785E-02 1.989E+OO 4.260E-02 1.137E+Ol 1.949E-01 7.063E-02 1.915E-02 4.179E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3591of5809 9.395E-01 2.146E+OO 3.956E+Ol 9.873E+Ol 3.923E-01 2.125E+OO 2.681E-02 1.708E+OO 3.913E-01 5.042E-Ql 6.719E-01 3.252E-01 4.426E-01 1. 996E-01 l.996E-01 3.530E-01 4.426E-01 4.838E-02 2.040E-01 3.848E+OO O.OOOE+OO 1.834E-01 3.027E+02 9.077E-02 7.428E-02 5.714E-02 3.138E-02 2.838E-02 l.013E-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:11:28.93 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235030.CNF;l *
  • Acquisition date 3-0CT-2016 09:09:22 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:15.23 Half life ratio : ***** *
  • Sample date 23-NOV-2015 14:44:00 Nuclide Library : SOLID *
  • Sample ID G405235030 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.3112E+02 GRAM *
  • Quantity Err ( % ) : 1. 5253E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * * .
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;15 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma ) K-40 1.507E+Ol 1. 706E+OO 1. 706E+OO CD-109 2.983E+OO 2.004E+OO 2.004E+OO SN-126 1. 859E-01 1.245E-01 l.245E-01 BA-137M 6.924E-02 4.314E-02 4.314E-02 CS-137 7.314E-02 4.557E-02 4.557E-02 TL-208 4.419E-01 8.498E-02 8.498E-02 PB-212 l.253E+OO l.437E-01 1.437E-01 BI-214 8.00lE-01 1. 920E-01 l.920E-01 PB-214 9.576E-01 l.677E-01 1.677E-01 RN-222 8.00lE-01 1.920E-01 l.920E-01 RA-224 1. 568E+OO 1.353E+OO 1. 353E+OO RA-226 8. OOlE-01 l.920E-01 1.920E-01 AC-228 9.747E-01 2.860E-01 2.860E-01 RA-228 9.747E-01 2.860E-01 2.860E-01 TH-228 1.253E+OO 1.437E-01 l.437E-01 TH-230 7.998E-01 1.920E-01 1. 920E-01 PA-231 9.449E-01 7.944E-01 7.944E-01 TH-232 9.747E-01 2.860E-01 2.860E-01 TH-234 1. 651E+OO 1.986E+OO 1. 986E+OO U-234 7.998E-01 l.920E-01 l.920E-01 U-235 -2.216E-02 1.820E-01 1.820E-01 U-238 1.651E+OO 1.986E+OO 1. 986E+OO AM-243 l.639E-01 8.612E-02 8.612E-02 ANH-511 7.810E-02 7.254E-02 7.254E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) (1. 96-sigma) BE-7 -5.191E+OO 1.335E+Ol 1.355E+Ol NOT IDENT. NA-22 -2.891E-02 4.083E-02 4.286E-02 NOT IDENT. NA-24 l.OOOE+41 6.080E+41 O.OOOE+OO SHORT HLIF AL-26 3.919E-03 l.766E-02 1. 775E-02 NOT IDENT. SC-46 5.750E-02 3.774E-01 3.782E-01 FAIL ABUN V-48 -6.282E+03 2.441E+04 2.457E+04 SHORT HLIF Page 3592 of 5809 CR-51 4.764E+02 5.325E+02 5.742E+02 SHORT HLIF MN-54 3.804E-02 5.868E-02 6.114E-02 NOT IDENT. C0-56 2.432E-02 4.637E-01 4.638E-01 FAIL ABUN MN-56 l.OOOE+41 l.548E+42 O.OOOE+OO SHORT HLIF C0-57 -5.382E-02 5.019E-02 5.574E-02 NOT IDENT. C0-58 -2.598E-01 6.790E-01 6.890E-01 NOT IDENT. FE-59 2.421E-01 8.558E+OO 8.558E+OO NOT IDENT. C0-60 2.369E-02 3.602E-02 3.757E-02 NOT IDENT. ZN-65 6.554E-02 1. 670E-01 l.696E-01 NOT IDENT. GE-68. -5.813E-01 2.548E+OO NOT IDENT. AS-73 2.459E+OO 6.389E+OO 6.485E+OO NOT IDENT. AS-74 -2.231E+03 l.068E+04 l.073E+04 SHORT HLIF SE-75 -5.855E-02 2.090E-01 2.107E-01 NOT IDENT. BR-77 1. 758E+40 l.597E+41 O.OOOE+OO SHORT HLIF SR-82 -5.368E+02 1. 060E+03 l.087E+03 SHORT HLIF RB-83 -2.797E-01 7.168E-01 7.278E-01 NOT IDENT. KR-85 2.480E+OO 7.228E+OO 7. 313E+OO NOT IDENT. SR-85 3.059E-01 8.934E-01 9.040E-01 NOT IDENT. RB-86 -l.417E+04 5.102E+04 5.142E+04 SHORT HLIF Y-88 -6. 971E-02 2.169E-01 2.191E-01 NOT IDENT. Y-91 -l.463E+02 5.109E+02 5.152E+02 NOT IDENT. NB-94 -6. 041E-03 3. 051E-02 3.064E-02 NOT IDENT. NB-95 -3.666E-01 l.205E+00 l.217E+00 NOT IDENT. NB-95M 2.424E+OO 2.642E+OO 2.859E+OO NOT IDENT. ZR-95 -8.124E-01 l.395E+OO l.442E+OO NOT IDENT. NB-97 l.OOOE+41 8.528E+40 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 2. 811E+41 O.OOOE+OO SHORT HLIF M0-99 -5.817E+33 6.707E+33 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 2.102E+41 O.OOOE+OO SHORT HLIF RH-101 8.237E-03 3.478E-02 3.498E-02 NOT IDENT. RH-102 -4.122E-03 6.028E-02 6. 031E-02 NOT IDENT. RU-103 -l.577E+OO 6. 996E+OO 7.032E+OO FAIL ABUN RH-106 -l.630E-01 5.077E-01 5.130E-01 NOT IDENT. RU-106 -l.630E-01 5.077E-01 5.130E-01 NOT IDENT. AG-108M 1. 808E-02 2.466E-02 2.597E-02 NOT IDENT. AG-llOM 2.838E-02 8.462E-02 8.558E-02 FAIL ABUN SN-113 5.595E-02 2.420E-01 2.433E-01 NOT IDENT. CD-115 l.OOOE+41 2.668E+41 O.OOOE+OO SHORT HLIF SN-ll 7M l.581E+05 2.251E+05 2.361E+05 SHORT HLIF TE-123M 5.483E-02 l.550E-01 l.570E-01 NOT IDENT. SB-124 9.869E-02 l.958E+OO l.958E+OO NOT IDENT. SB-125 2.725E-02 9. 3.46E-02 9.426E-02 FAIL ABUN TE-125M -l.420E+02 3.104E+02 3.170E+02 NOT IDENT. I-126 3.392E+05 l.882E+06 l.888E+06 SHORT HLIF SB-126 5.891E+05 2.677E+06 2.690E+06 SHORT HLIF SB-127 -2.647E+23 4.791E+23 O.OOOE+OO SHORT HLIF I-131 l.256E+l0 l.493E+l0 l.597E+l0 SHORT HLIF I-132 l.OOOE+41 2.546E+42 O.OOOE+OO SHORT HLIF TE-132 2.590E+27 8.415E+27 O.OOOE+OO SHORT HLIF BA-133 3.287E-02 6.519E-02 6.685E-02 FAIL ABUN I-133 -l.OOOE+41 3.947E+41 O.OOOE+OO SHORT HLIF CS-134 5.534E-02 5.880E-02 6.387E-02 NOT IDENT. CS-135 8.038E-02 l.422E-01 l.467E-01 NOT IDENT. I-135 -l.OOOE+41 l.129E+42 O.OOOE+OO SHORT HLIF CS-136 l.009E+04 5.874E+05 5.874E+05 SHORT HLIF CE-139 -4.901E-02 l.122E-01 l.143E-01 NOT IDENT. BA-140 -3.097E+05 2.717E+06 2. 721E+06 SHORT HLIF LA-140 -6.788E+05 8.762E+05 9.281E+05 SHORT HLIF CE-141 -4.732E+Ol 3.419E+Ol 4.030E+Ol NOT IDENT. CE-143 l.OOOE+41 l.209E+41 O.OOOE+OO SHORT HLIF CE-144 -l.732E-01 4.038E-01 4 .113E-01 NOT IDENT. PM-144 4.007E-02 5.707E-02 5.986E-02 NOT IDENT. PR-144 3.477E+OO 4.989E+OO 5.229E+OO NOT IDENT. PM-146 -l.605E-02 3.920E-02 3.986E-02 NOT IDENT. ND-147 -5.655E+07 7.126E+07 7.568E+07 SHORT HLIF PM-147 3.755E+02 7.838E+02 8. 018E+02 NOT IDENT. PM-149 -l.OOOE+41 2.231E+41 O.OOOE+OO SHORT HLIF EU-150 -8.685E-03 2. 611E-02 2.640E-02 FAIL ABUN EU-152 5.652E-02 8.429E-02 8.806E-02 NOT IDENT. GD-153 -l.544E-02 l.937E-01 l.938E-01 NOT IDENT. EU-154 -5.707E-02 9.730E-02 1. 006E-01 NOT IDENT. EU-155 1. 721E-02 l.027E-01 l.030E-Ol FAIL ABUN TB-160 l.611E+OO 2.128E+OO 2.249E+OO FAIL ABUN H0-166M 4.534E-02 6.898E-02 7.194E-02 FAIL ABUN TM-171 9.197E-01 l.300E+Ol l.301E+Ol NOT IDENT. HF-172 -7.889E-02 2.627E-Ol 2.651E-01 FAIL ABUN LU-172 -1. 581E-03 8.202E-02 8.202E-02 FAIL ABUN LU-176 -9.895E-03 2.279E-02 2.322E-02 FAIL ABUN Page 3593 of 5809 HF-181 -5.063E-01 4. 960E+OO 4. 966E+OO NOT IDENT. TA-182 3.245E-01 1.046E+OO 1.056E+OO FAIL ABUN RE-183 2.875E-01 2.456E+OO 2.459E+OO FAIL ABUN RE-184 3.007E+Ol 4.376E+Ol 4.581E+Ol NOT IDENT. W-188 -4.717E+Ol 1. 310E+02 l.327E+02 FAIL ABUN IR-192 -3.451E-02 4.503E-01 4.505E-01 FAIL ABUN HG-203 -1.845E+OO 2.598E+OO 2.728E+OO NOT IDENT. BI-207 -4.604E-02 4.117E-02 4. 611E-02 FAIL ABUN PB-210 1.033E+OO 1.858E+OO 1.916E+OO NOT IDENT. BI-211 c 2.638E+OO 4.639E-01 1. 27 6E+OO FAIL ABUN PB-211 -4.082E-01 6.345E-01 6.607E-01 NOT IDENT. BI-212 1.398E+OO 1.026E+OO 1.204E+OO FAIL ABUN RN-219 1.717E-01 3.554E-01 3.638E-01 FAIL ABUN RA-223 -2.322E-01 5. 968E-01 6.059E-01 FAIL ABUN AC-227 1. 576E-01 2. lllE-01 2.228E-01 FAIL ABUN TH-227 1. 576E-01 2. lllE-01 2.228E-01 FAIL ABUN TH-229 -3.144E-01 4.166E-01 4.400E-01 FAIL ABUN TH-231 -2.322E-01 5. 968E-01 6.059E-01 FAIL ABUN PA-233 5.683E-03 5.437E-02 5.444E-02 FAIL ABUN PA-234 4.956E-02 2.312E-01 2.323E-01 FAIL ABUN PA-234M 3.779E+00 3.614E+OO 3.995E+OO FAIL ABUN NP-237 5.683E-03 5.437E-02 5.444E-02 FAIL ABUN NP-238 1.000E+41 1.834E+42 O.OOOE+OO SHORT HLIF NP-239 8.044E-02 2.108E-01 2.139E-01 NOT IDENT. PU-239 5.533E+02 5.189E+02 5.757E+02 FAIL ABUN AM-241 1.108E-01 1.033E-01 1.148E-01 NOT IDENT. CM-243 5.665E-03 8.751E-02 8.755E-02 NOT IDENT. BK-247 -7.044E-03 6.502E-02 6.510E-02 NOT IDENT. CM-247 2.966E-02 3.314E-02 3.574E-02 NOT IDENT. CF-249 -4.716E-03 3.330E-02 3.337E-02 NOT IDENT. CF-251 8. 311E-02 l.059E-01 1.123E-01 NOT IDENT. Page 3594 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 72.2845 87.09 101. 5767 136.47 53.1785 45.60 72.5864 87.57 101.6419 140.51 0.0000 46.54 70.5825 88.03 101.7051 143.76 74.2628 49.72 0.0000 88.34 101. 7472 144.24 70.6432 51. 35 86.3422 88.47 101.7645 145.44 90. 2372 51. 87 79.9433 89. 96 101. 9658 152.43 73.6569 52.39 73.5314 1093.63 102.0568 153.25 0.0000 52.97 70.3618 91.11 0.0000 323.87 78.6992 53.44 73.6720 92.59 102.3162 156.02 0.0000 54.07 80.2634 93.35 102.4167 158.56 0.0000 57.36 0.0000 94.56 72.2255 159.00 59.2881 57.53 91.6674 94.65 72.2341 162.33 69.3796 57.98 85.1854 94.67 72.2360 162.66 0.0000 59.27 68.5909 94.87 72.2542 163.33 57.8691 59.32 68.5966 97.43 81. 7423 165.86 62.1437 59.54 68.6222 98.43 75.2817 176.31 56.8617 60. 96. 87.8125 98.44 75.2827 176.60 0.0000 61.17 87.8433 99.53 . 80.0234 177.52 56.0841 62.93 98.0102 100 .11 77.7596 181.07 0.0000 63.29 98.0681 102.03 67.4731 181.52 49.1356 63.58 98 .1144 103.18 66.4024 184.41 63.1470 64.28 98.2260 103.37 64. 0872 143.76 63.2164 66.73 113.7548 105.21 72.4037 193.51 67.8630 67.24 110.8887 105.31 72.4122 197.03 69.7564 125.81 110. 9657 106.12 71. 3131 198.01 59.5944 67.75 110.9779 106.47 72.5125 201.83 63.1910 69.67 134.6849 109.28 77.4462 203.43 51.3000 70.83 112.9942 111. 00 65.8433 205.31 52.6601 72.81 128.2459 111.76 0.0000 210.85 73.5235 72. 87 128.2573 114. 06 57.8152 2'15. 65 68.1823 74.66 105.4215 116. 30 0.0000 222 .11 56.3698 74.82 105.4466 116.74 54.4400 227.09 47.0017 74.97 105.4696 119. 76 78.3720 227.38 47.0116 77 .11 105.8002 121.12 60.6504 228.16 0.0000 78.74 96.2715 121.22 60. 6571 228.18 41.8125 79.69 111. 4645 121. 78 83.3060 116.74 41.8125 80.12 120.5754 122.06 89.2834 235.69 42.0386 80.19 0.0000 122.92 65.5357 235. 96 42.0464 80.57 110.0948 123.07 60.7796 238.63 52.6575 81. 00 101.1073 265.00 69.1675 238.98 0.0000 81. 07 98.0991 125.81 84.4660 240.99 52.7448 81. 75 135.9586 127.23 65.4401 242.00 52.7820 83.79 115.1349 127.91 71. 8764 244.70 52.8809 84.00 124.2604 129.30 76.7803 252.40 0.0000 85.43 139.6874 131. 20 76.9326 252.80 51.4025 86.55 101.5027 133.02 73.8665 254.15 0.0000 86.79 101.5353 133.52 78.7248 256.23 39.0854 86.94 101.5564 136.00 68.8573 260.90 0.0000 Page 3595 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 46.4511 355.39 0.0000 584.27 9.3977 264.80 46.4553 356.01 33.0026 595.83 0.0000 265.00 42.8877 364.49 0.0000 427.87 22.0621 268.22 40.2914 366.42 0.0000 602.52 0.0000 269.46 49.7334 372.51 31. 3887 604.72 15.7825 270.03 44.3730 375.0.5 25. 7157. 607.14 30. 0134 271.23 36.7817 377.52 39.0998 609.32 26.3489 273.65 0.0000 356.01 27.7456 610.33 26.3590 276.40 37.8044 388.16 28.7653 614.28 25.3408 277.37 29.7216 388.63 0.0000 618.01 25.3750 277.60 28.8255 391.69 29.7771 620.36 13.7570 278.00 32.4368 264.66 25.0859 621.93 22.2347 279.20 45.0857 401.81 26.0656 630.19 0.0000 279.54 50.5062 402.40 23.1763 631. 29 21.2476 279.70 54.1199 404.85 35.7730 633.25 14.8835 280.46 49.6334 410.95 39.7588 634.78 0.0000 283.69 40.6915 413.71 13.1089 635.95 25.5391 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 47.9773 423.72 0.0000 645.85 20.2896 285.90 0.0000 427.09 24.4314 657.76 14.4767 287.50 32.6309 427.87 22.4848 657.90 0.0000 290.67 43.5938 433.94 18.6277 661. 66 12.8853 293.27 0.0000 439.40 25.5551 664.57 0.0000 351. 93 36.4290 453.88 25. 7255 666.33 0.0000 295.96 36.4461 463.37 21.8608 666.50 0.0000 879.38 36.5039 468.07 25.3916 667.71 0.0000 299.98 36.5348 473.00 0.0000 677.62 17.2747 300.09 36.5373 475.06 13.9835 685.70 0.0000 300.13 36.5381 476.78 20.9910 695.00 0.0000 301.36 35.6508 477.60 23.9980 696.49 16.2982 302.85 41.1722 482.18 22.0421 696. 51 16.2982 256.23 50.8298 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.3893 306.78 43.1034 497.08 24.2002 697.49 17.3906 308.46 37.6384 505.52 25.8045 702.65 20.6862 311. 90 35.8754 507.63 0.0000 706.68 22.8944 316.51 31.3604 511. 00 31. 4421 711. 68 16.3800 319.41 0.0000 514.00 22.8497 720.70 0.0000 320.08 0.0000 514.00 22.8497 721. 93 0.0000 321. 04 36.0666 520.40 25.4557 722. 78 18.0831 323.87 38.9042 520.69 0.0000 722. 91 18.0838 325.23 25.0291 522.65 0.0000 723. 31 19.7307 328.76 0.0000 527.90 0.0000 724.19 19.7366 333.37 33.5259 528.26 16.3438 727. 33 23.0491 333.97 39.1272 529.59 16.3529 733.00 18.4728 334.37 47.5220 529.87 0.0000 735.93 14.3081 338.28 39.2212 531.02 0.0000 333.97 9.9104 338.32 39.2220 537.26 0.0000 739.50 0.0000 311. 90 44.8789 546.56 0.0000 747.24 27.6143 340.48 44.8789 552.55 26.8178 748.06 17.6777 340.55 0.0000 563.25 14. 5013 752.31 17.7012 344.28 27.1710 569.33 25.9562 753.82 0.0000 345.93 42.2003 946.00 29.0721 756.73 14.4023 351.06 32.9143 569.70 29.0744 756.80 14.4028 351.93 32.9300 583.19 9.3937 884.68 22.2078 Page 3596 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 31.1081 1274.44 7 .1118 1620.50 5.0671 766.42 24.4474 1001.03 11.5706 1621. 92 5.0684 766.84 22.2274 1002.74 12.8224 1678.03 0.0000 772.60 0.0000 1004.73 5.7016 1690.97 3.0775 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 17(ii4.49 6.2307 778.90 10.0397 1028.54 0.0000 1063.66 2.7718 783.70 0.0000 1037.84 12.5764 1771. 35 6.2380 785.37 17.8835 1038.76 0.0000 1791.20 0.0000 792.07 27.9999 631.29 13.5040 1808.65 1.0460 794.95 25.7823 1048.07 0.0000 1810.72 0.0000 795.86 17.9408 1049.04 9.9083 1836.06 4.2021 810.06 13.5127 1050.41 10.8127 810.29 14.6398' 1063.66 16.2719 344.28 18.0189. 1077.00 0.0000 810.76 18.0208 1077.34 17.2327 815.77 0.0000 1085.87 14.5420 1048.07 0.0000 1093.63 16.3894 832.01 17. 0007 1099.45 14.5889 834.85 10.2089 1112. 07 10.9739 835.71 12.4806 1112. 84 10.0614 836.80 0.0000 1115. 54 8.7867 846.75 0.0000 1120. 29 16.4927 846.77 11. 3822 1120.55 16.4938 856.80 0.0000 1221. 41 16.4971 860.56 9.1419 1129. 67 13.7741 871.09 19.4847 1131. 51 0.0000 873.19 12.6154 1147.95 0.0000 875.33 0.0000 1173.23 11.1299 879.38 10.3396 1177.95 10.2131 880.51 13.7905 1189.05 14.8926 883.24 17.2510 1204.77 11. 2083 884.68 8.0539 1221.41 14.9990 889.28 10.3682 1231. 02 10.3333 894.76 19.6141 1235.36 0.0000 898.04 13.8579 1238.28 18.0645 900.72 25.4250 1260.41 0.0000 903.28 12.7214 1271.87 13.2677 911.20 11. 5898 1274.44 11.3782 912.08 13. 9111 1274.54 12 .. 3264 923.98 0.0000 1291.59 6.6612 926.50 3.4915 1298.22 0.0000 929 .11 8.1524 1312.11 0.0000 937.49 19.2594 1332.49 5.7583 944.13 0.0000 1362.66 0.0000 946.00 9.6515 1365.19 9.6606 949.00 15.8060 1368.63 0.0000 667.71 0.0000 1384.29 6.7881 962. 31 21.1487 1408.01 6.8201 964.08 18.3371 1457.56 0.0000 966 .17 22.5813 1460.82 1.9685 911. 20 23.8335 1489.16 4.9478 968. 97 2.3.8335 1505.03 12.7039 983.53 0.0000 1584.12 8.0552 984.45 0.0000 1596.21 0.0000 Page 3597 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:11:57.99 ******************************************************************************** *
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM32.CNF;277 Background date : Z-OCT-2016 11:01:57. Sample date 26-NOV-2015 14:25:00 Acquisition date : 3-0CT-2016 09:09:51. Sample ID G405235031 Sample quantity l.39617E+02 GRAM Detector name : GAM32 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.58 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 1 1 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 0 0 Page 3598 of 5809 Energy 75.28 77.48 87.22 93.20* 144.44 186.03* 208.93 239.03* 242 .11 271.27 295.94* 328.63 338.57 352.65* 367.02 463. 71 511. 32* 563.44 572.16 583.88* 609.76* 627.98 662.26 666.32 670.67 717.06 727. 72* 768.71 785.95 799.40 883.49 911.73* 961. 54 965. 08* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 98 171 50 62 41 74 45 405 76 33 159 64 78 230 18 15 49 27 19 97 181 16 65 17 9 12 20 33 14 25 9 71 11 14 122 124 186 172 124 173 123 66 93 108 98 57 84 90 36 28 54 12 26 45 40 18 11 9 11 19 11 23 7 50 2 26 5 9 1.19 1. 29 1. 07 1.17 1. 75 1. 48 0.93 1. 28 1. 59 2.19 1.21 1. 61 1.14 1. 30 2.46 0.67 1. 45 1. 81 1. 44 1.17 1.13 0.82 1. 79 1. 80 0.67 4.54 1. 31 6.07 1. 61 4.04 1. 23 1. 24 0.81 0.96 151.77 156.18 17 5. 66 187.61 290.10 373.27 419.07 479.27 485.43 543.76 593 .11 658.48 678.37 706.53 735.27 928.65 1023.88 1128 .11 1145.56 1169. 00 1220.77 1257.20 1325.76 1333.89 1342.59 1435.36 1456.69 1538.68 1573.15 1600.05 1768.23 1824. 72 1924.35 1931.43 148 148 171 184 284 367 413 472 472 536 586 652 671 699 730 925 1017 1123 1140 1163 1215 1250 1317 1317 1338 1427 1452 1531 1569 1583 1764 1819 1921 1927 13 2.71E-02 13 4.74E-02 9 1.40E-02 8 l.72E-02 10 l.13E-02 14 2.06E-02 12 l.24E-02 19 1.12E-01 19 2.12E-02 13 9.lOE-03 14 4.42E-02 15 1.77E-02 12 2.18E-02 16 6.39E-02 11 4.95E-03 9 4.17E-03 15 1.36E-02 12 7.50E-03 14 5.32E-03 13 2. 71E-02 13 5.02E-02 12 4.50E-03 22 1.81E-02 22 4.76E-03 7 2.36E-03 13 3.45E-03 9 5.44E-03 15 9.03E-03 9 3.77E-03 29 6.94E-03 8 2.54E-03 13 1. 96E-02 7 2.99E-03 9 4.0lE-03 20.7 4.09E+OO 14.4 50.9 40.8 54.1 40.1 51. 9 6.1 2.21E+OO 26. 8 68.3 15.5 28.6 26.0 11. 6 69.2 67.9 40.0 32.1 65.0 17.7 10.5 57.9 16. 7 8. OlE-01 40.1 71. 9 78.2 40.2 36.3 44.3 84.3 42.4 19.4 49.4 48.5 Peak Search Report (continued) Page : 2 Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969.78 48 15 1. 70 1940.82 1936 13 1.32E-02 22.6 36 0 1054.10 7 17 3.99 2109.46 2100 11 l.81E-03127.2 37 0 1115. 94 14 9. 1. 62 2233.14 2228 9 3.89E-03 47.0 38 0 1120.87* 42 11 2.43 2243.02 2238 11 l.16E-02 22.1 39 0 1175.28 8 7 1. 28 2351. 84 2345 9 2.22E-03 68.7 40 7 1191. 67 20 11 2.92 2384.61 2381 12 5.64E-03 31. 6 5.19E+OO 41 7 1194.36 8 9 1. 83 2390.00 2381 12 2.15E-03 58.4 42 0 1302.02 14 3 4.15 2605.31 2598 13 3.85E-03 37.9 43 0 1378.71 10 11 1. 52 2758.70 2751 11 2.78E-03 71. 6 44 0 1461.25* 324 0 2.25 2923.80 2917 15 8.99E-02 5.6 45 0 1765.07* 32 0 2.89 3531.46 3524 13 8.90E-03 18.6 Flag: "*" = Peak area was modified by background subtraction Page 3599 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:11:59
  • DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 26-NOV-2015 14:25:00 G405235031 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:09:51 139.62 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA32 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 U-235 143.76 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 Page 3600 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 CE-141 145.44 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 CAN 0 01:00:00.58 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460. 82. 10.66* 1.119E+OO 1.398E+Ol 1.398E+Ol, 11.23 OK ZN-65 1115. 54 50.60* 1.397E+OO 1.045E-01 2.534E-01 93.95 OK CD-109 88.03 3.70* 4.556E+00 8.954E-01 1.430E+OO 220.35 OK SN-126 64.28 9.60 2.229E+OO Line Not Found Absent 86.94 8.90 4.556E+OO 3.722E-01 3.722E-01 220.35 OK 87.57 37.00* 4.556E+OO 8.954E-02 8.954E-02 220.35 OK BA-137M 661.66 89.90* 2.104E+OO 1.903E-01 1. 941E-01 33.35 OK CS-137 661.66 85.10* 2.104E+OO 2. OllE-01 2. 051E-01 33.35 OK CE-141 145.44 48.29* 6.092E+OO 5.132E-02 3.958E+Ol 188.15 OK TL-208 277.37 6.60 4.277E+OO Line Not Found Absent 583.19 85.00* 2.325E+OO 2.750E-01 2.750E-01 35.35 OK 860.56 12.50 1.714E+OO Line Not.Found Absent BI-212 727.33 6.67* 1.953E+OO 8.238E-01 8.238E-01 80.37 OK 785.37 1.10 1.839E+OO 3.649E+OO 3.649E+OO 88.65 OK 1620.50 1. 47 1.022E+OO Line Not Found Absent PB-212 74.82 10.28 3.470E+OO 1.154E+OO 1.154E+OO 65.05 OK 77.11 17.10 3.695E+OO 1.759E+OO 1. 759E+OO 28.75 OK 238.63 43.60* 4.787E+00 1.162E+OO 1.162E+OO 12.28 OK 300.09 3.30 4.016E+OO Line Not Found Absent BI-214 609.32 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 OK 1120. 29 14.92 1.392E+OO 1.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 OK PB-214 74.82 5.80 3.423E+00 Line Not Found <<INT Reject 77 .11 9.70 3.695E+OO 3.101E+OO 3.102E+OO 28.75 OK 87.09 3.41 4.545E+OO Line Not Found <<INT Reject 242.00 7.25 4.745E+OO Line Not Found <<INT Reject 295.22 18.42 4.062E+OO 1.254E+OO l.255E+OO 31.06 OK 351. 93 35.60* 3.518E+OO 1.068E+OO 1.069E+OO 23.21 OK RN-222 609.32 45.49* 2.246E+00 9.824E-01 9.827E-01 20. 96 OK 1120. 29 14.92 1.392E+OO 1.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 OK RA-224 240.99 4.10* 4.743E+OO 3.688E-01 3.688E-01 356.75 OK RA-226 609.32 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 OK 1120.29 14.92 1.392E+OO 1.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO 1.121Et00 37.23 OK AC-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.639E+00 l .114E+OO 1.114E+OO 51. 96 OK 794.95 4.25 l.823E+00 Line Not Found Absent 835. 71 1. 61 1. 753E+OO Line Not Found Absent 911.20 25.80* l.638E+OO 8.982E-01 8.982E-01 38.82 OK 968.97 15.80 1.561E+OO 1. 031E+OO 1. 031E+OO 45.21 OK RA-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.639E+OO 1.114E+OO 1. 114E+OO 51. 96 OK 794.95 4.25 1.823E+OO Line Not Found Absent 835.71 1. 61 1.753E+OO Line Not Found Absent 911.20 25.80* l.638E+OO 8.982E-01 8.982E-01 38.82 OK 968. 97 15.80 1.561E+OO 1. 031E+OO 1. 031E+OO 45.21 OK TH-228 74.82 10.28 3.470E+OO 1.154E+OO 1.154E+OO 65.05 OK 77 .11 17.10 3.695E+OO 1. 759E+OO l.759E+OO 28.75 OK Page 3601of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 238.63 43. 60* 4.787E+OO 1.162E+OO 1.162E+OO J_2. 2 8 OK 300.09 3.30 4.016E+OO Line Not Found Absent TH-230 609.32 45.49* 2.246E+OO 9.824E-01 9.824E-01 20. 96 OK 1120.29 14.92 l.392E+OO 1.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO l.121E+OO 37.23 OK TH-232 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.639E+OO 1.114E+OO 1.114E+OO 51. 96 OK 835.71 1. 61 1. 753E+OO Line Not Found Absent 911. 20 25.80* l.638E+OO 8.982E-01 8.982E-01 38.82 OK 968.97 15.80 1. 561E+OO 1.031E+OO 1.031E+00 45.21 OK U-234 609.32 45.49* 2.246E+OO 9.824E-01 9.824E-01 20. 96 OK 1120.29 14.92 1. 392E+OO 1.065E+OO 1.065E+OO 44.24 OK 1764.49 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 OK U-235 89. 96 3.47 4.758E+OO Line Not Found Absent 93.35 5.60 4.976E+OO 1.429E+OO 1.429E+00 81. 61 OK 143.76 10. 96* 6.095E+00 Line Not Found <<INT Reject 163.33 5.08 5.924E+OO Line Not Found Absent 185. 72 57.20 5.605E+OO 1. 411E-01 1. 411E-01 80.25 OK 205.31 5.01 5. 302E+OO . Line Not Found Absent AM-243 43.53 5.90 1.701E-01 Line Not Found Absent 74.66 67.20* 3.470E+OO 1. 765E-01 1. 765E-01 65.05 OK ANH-511 511. 00 100.00* 2.588E+OO l.067E-01 l.067E-01 80.01 OK Flag: "*" = Keyline Page 3602 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:12:00.81 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * . . .
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l * *Acquisition date 3-0CT-2016 09:09:51 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
  • Sample date 26-NOV-2015 14:25:00 Analyst initials: MXRl *
  • Sample ID G405235031 Sample Quantity 1.3962E+02 GRAM *
  • Batch Number 1596249 Wet*weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.398E+Ol l.539E+OO ZN-65 2.534E-01 2.333E-01 CD-109 1.430E+OO 3.089E+OO SN-126 8.954E-02 l.934E-01 BA-137M 1. 941E-01 6.344E-02 CS-137 2. 051E-01 6.702E-02 CE-141 3.958E+Ol 7.297E+Ol TL-208 2.750E-01 9.527E-02 BI-212 8.238E-01 6.489E-01 PB-212 l.162E+OO l.399E-01 BI-214 9.827E-01 2.019E-01 PB-214 1.069E+00 2. 431E-01 RN-222 9.827E-01 2.019E-01 RA-224 3.688E-01 1.289E+OO RA-226 9.827E-01 2.019E-01 AC-228 8.982E-01 3.417E-01 RA-228 8.982E-01 3.417E-01 TH-228 1.162E+OO 1.399E-01 TH-230 9.824E-01 2.018E-01 TH-232 8.982E-01 3.417E-01 U-234 9.824E-01 2.018E-01 U-235 3.792E-01 4.020E-01 AM-243 1. 7 65E-01 l.125E-01 ANH-511 1.067E-01 8.368E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3603 of 5809 Key-Line Activity (pCi/GRAM -4.375E+OO 2.714E-02 O.OOOE+OO -1.733E-02 8.642E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.407E+Ol 4.918E-02 l.129E+41 3.578E-02 3.686E-01 2.266E+04 MDA (pCi/GRAM 7.486E-01 3.281E-01 3.077E+OO 1. 781E-01 5.102E-02 5.390E-02 6.698E+Ol 6.553E-02 7. 965E-01 9.344E-02 1.212E-01 1.382E-01 1.212E-01 1. OOlE+OO l.212E-01 2.730E-01 2.730E-01 9.344E-02 l.211E-01 2.730E-01 1.211E-01 4.136E-01 1.255E-01 5.400E-02 MDA (pCi/GRAM 2.602E+Ol 1. 076E-01 O.OOOE+OO 6.485E-02 7.552E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 6.299E+02 O.OOOE+OO SHORT HLIF MN-54 -2. 251E-02 7.482E-02 1.316E-01 NOT IDENT. C0-56 6.602E-02 5.547E-01 l.073E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 l.209E-02 5.630E-02 l.028E-01 NOT IDENT. C0-58 -2.868E-02 6.680E-01 1.267E+OO NOT IDENT. FE-59 7.864E-01 7.630E+OO 1.584E+Ol NOT IDENT. C0-60 -1.891E-02 3.538E-02 6.479E-02 NOT IDENT. GE-68 -l.027E+OO 2.286E+OO 4.299E+OO NOT IDENT. AS-73 9.986E+OO 1.955E+Ol 3. 783E+Ol NOT IDENT. AS-74 O.OOOE+OO 1. 086E+04 0.000E+OO SHORT HLIF SE-75 3.508E-02 2.303E-01 4.339E-01 NOT IDENT. BR-77 O.OOOE+OO 8.219E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO l.012E+03 O.OOOE+OO SHORT HLIF RB-83 2.436E-01 6.334E-01 1.312E+OO NOT IDENT. KR-85 7.363E+OO 9.00lE+OO 1.690E+Ol NOT IDENT. SR-85 8.803E-01 l.078E+OO 2.024E+OO NOT IDENT. RB-86 O.OOOE+OO 4.289E+04 O.OOOE+OO SHORT HLIF Y-88 1. 089E-01 2.289E-01 5.671E-01 NOT IDENT. Y-91 -2. 296E+02 5.789E+02 1.086E+03 NOT IDENT. NB-94 2. 991E-02 3.730E-02 7.610E-02 NOT IDENT. NB-95 -5.163E-01 l.193E+00 1.806E+OO NOT IDENT. NB-95M -5.773E-01 2.845E+OO 4.843E+OO NOT IDENT. ZR-95 1.562E+OO 1. 743E+OO 3.764E+OO NOT IDENT. NB-97 O.OOOE+OO l.672E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.638E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 406E+41 O.OOOE+OO SHORT HLIF RH-101 8.540E-03 3.671E-02 6.721E-02 NOT IDENT. RH-102 -4.078E-02 6.598E-02 9.701E-02 NOT IDENT. RU-103 -5.023E+00 7.687E+OO 1. 341E+Ol FAIL ABUN RH-106 -6.563E-02 6.005E-01 9. 996E-01 NOT IDENT. RU-106 -6.563E-02 6.005E-01 9. 996E-01 NOT IDENT. AG-108M 1.395E-02 2.864E-02 5.819E-02 NOT IDENT. AG-llOM 9.579E-02 7.959E-02 l.881E-01 FAIL ABUN SN-113 -5.297E-02 2.842E-01 5.306E-01 NOT IDENT. CD-115 O.OOOE+OO 1.186E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.777E+05 O.OOOE+OO SHORT HLIF TE-123M -4.232E-02 l.427E-01 2.739E-01 NOT IDENT. SB-124 3.304E-01 1.813E+OO 4.393E+OO NOT IDENT. SB-125 -8.641E-02 1.115E-01 1.933E-01 FAIL ABUN TE-125M 7. 801E+Ol 3.956E+02 7.207E+02 NOT IDENT. I-126 O.OOOE+OO l.960E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.054E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.015E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.427E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 7.858E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.187E+27 O.OOOE+OO SHORT HLIF BA-133 -2.023E-02 4.523E-02 7.292E-02 NOT IDENT. I-133 O.OOOE+OO 1.376E+41 O.OOOE+OO SHORT HLIF CS-134 3.667E-02 6.464E-02 1.284E-01 FAIL ABUN CS-135 1. 759E-02 l.624E-01 2.845E-01 NOT IDENT. I-135 O.OOOE+OO 1.339E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 7.284E+05 O.OOOE+OO SHORT HLIF CE-139 3.429E-02 1.219E-01 2.428E-01 NOT IDENT. BA-140 O.OOOE+OO 2.846E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 7.893E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -3.216E-01 4.212E-01 6. 965E-01 NOT IDENT. PM-144 1.165E-02 6.301E-02 l.217E-01 NOT IDENT. PR-144 1.018E+OO 5.507E+OO 1. 063E+Ol NOT IDENT. PM-146 3.303E-03 4. 718E-02 9.095E-02 NOT IDENT. ND-147 O.OOOE+OO 6.622E+07 O.OOOE+OO SHORT HLIF PM-147 -4.625E+Ol 9.551E+02 l.705E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 -4*. 213E-03 3.597E-02 4. 801E-02 FAIL ABUN EU-152 -2.159E-04 l.060E-01 2.022E-01 FAIL ABUN GD-153 -5.504E-02 2.355E-01 4.158E-01 NOT IDENT. EU-154 5.825E-02 l.182E-01 2. 571E-01 NOT IDENT. EU-155 -9.052E-03 l.310E-01 2.344E-01 FAIL ABUN TB-160 -7.102E-02 2.371E+OO 3.997E+OO FAIL ABUN H0-166M -3.605E-02 7.798E-02 1.180E-01 NOT IDENT. TM-171 3.902E+OO 4.541E+Ol 8.493E+Ol NOT IDENT. HF-172 -2. 723E-01 2.607E-01 4.192E-Ol NOT IDENT. LU-172 -l.317E-02 7.127E-02 1.412E-01 FAIL ABUN LU-176 -1.385E-02 2.550E-02 4.650E-02 FAIL ABUN HF-181 1.333E+OO 5.734E+OO 1.126E+Ol NOT IDENT. TA-182 l.057E-01 1.024E+OO 2.066E+OO FAIL ABUN Page 3604 of 5809 RE-183 -1.978E+OO 5.353E+OO 9.626E+OO NOT IDENT. RE-184 -5.128E+OO 3.263E+Ol 6.161E+Ol NOT IDENT. W-188 -6.558E+Ol 1.394E+02 2.270E+02 NOT IDENT. IR-192 -3.755E-01 5.903E-01 1.062E+OO FAIL ABUN HG-203 2.157E+OO 3.262E+OO 6.567E+OO NOT IDENT. BI-207 -1.820E-02 5.147E-02 9.798E-02 FAIL ABUN PB-210 3.590E+OO 8.738E+OO 1. 698E+Ol NOT IDENT. BI-211 O.OOOE+OO 3.382E-01 7.893E-01 NOT IDENT. PB-211 l.608E-01 7.550E-01 1. 468E+OO NOT IDENT. RN-219 -l.209E-01 4.508E-01 8.314E-01 FAIL RA-223 6.234E-02 6.689E-01 1.170E+OO FAIL ABUN AC-227 5.266E-02 2.289E-01 4.523E-01 NOT IDENT. TH-227 5.266E-02 2.289E-01 4.523E-01 NOT IDENT. TH-229 8.785E-02 5.032E-01 9.864E-01 FAIL ABUN PA-231 9.055E-02 5.282E-01 9.263E-01 NOT IDENT. TH-231 6.234E-02 6.689E-01 1.170E+OO FAIL ABUN PA-233 -3.171E-03 6.204E-02 l.189E-01 NOT IDENT. PA-234 6.928E-02 2.412E-01 5.230E-01 FAIL ABUN PA-234M -5.147E-01 4.015E+OO 8. 051E+OO NOT IDENT. TH-234 1. 369E-03 l.948E+00 3.628E+OO FAIL ABUN NP-237 -3. l 71E-03 6.204E-02 1.189E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 l.369E-03 1.948E+OO 3.628E+OO FAIL ABUN NP-239 5.605E-02 2.818E-01 5.145E-01 NOT IDENT. PU-239 l.082E+02 3.543E+02 6.482E+02 NOT IDENT. AM-241 -l.804E-01 2.143E-01 3.672E-01 NOT IDENT. CM-243 2.973E-02 l.157E-01 2 .138E-01 NOT IDENT. BK-247 2.027E-02 7.794E-02 1.404E-01 NOT IDENT. CM-247 -6.403E-03 3.984E-02 7.448E-02 NOT IDENT. CF-249 -2.454E-02 3.752E-02 6.666E-02 NOT IDENT. CF-251 7.552E-02 l.234E-01 2.499E-01 NOT IDENT. Page 3605 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:11:58.68 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 310 10.66* 1.119E+OO l.398E+Ol l.398E+Ol 11. 23 ZN-65 1115.54 14 50.60* 1.397E+OO l.045E-01 2.534E-01 93.95 CD-109 88.03 60 3.70* 4.556E+OO 1.929E+OO 3.082E+OO 101.77 SN-126 64.28 ------9.60 2.229E+OO ------Line Not Found ------86.94 60 8.90 4.556E+OO 8.021E-01 8.021E-01 101.77 87.57 60 37.00* 4.556E+OO 1.929E-01 l.929E-01 101.77 BA-137M 661.66 67 89.90* 2.104E+OO 1.903E-01 1. 941E-01 33.35 CS-137 661.66 67 85.10* 2.104E+OO 2.0llE-01 2. 051E-01 33.35 CE-141 145.44 47 48.29* 6.092E+OO 8.607E-02 6.638E+Ol 108.17 TL-208 277.37 ------6.60 4.277E+OO ------Line Not Found ------583.19 101 85.00* 2.325E+OO 2.750E-01 2.750E-01 35.35 860.56 ------12.50 1.714E+OO ------Line Not Found ------BI-212 727.33 20 6.67* 1. 953E+OO 8.238E-01 8.238E-01 80.37 785.37 14 1.10 l.839E+00 3.649E+OO 3.649E+OO 88.65 1620.50 ------1. 47 1.022E+OO ------Line Not Found ------PB-212 74.82 119 10.28 3.470E+OO 1. 787E+OO l.787E+00 41. 48 77 .11 207 17.10 3.695E+OO 1. 759E+OO 1. 759E+OO 28.75 238.63 451 43.60* 4.787E+OO l.162E+00 l.162E+00 12.28 300.09 ------3.30 4.016E+OO ------Line Not Found ------BI-214 609.32 187 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 1120.29 41 14.92 1.392E+OO 1.065E+OO 1.065E+OO 44.24 1764.49 30 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 PB-214 74.82 119 5.80 3.470E+00 3.167E+OO 3.168E+OO 41. 48 77 .11 207 9.70 3.695E+OO 3.101E+OO 3.102E+OO 28.75 87.09 60 3.41 4.556E+OO 2.093E+OO 2.094E+00 101.77 242.00 85 7.25 4.743E+OO 1.330E+OO 1. 331E+OO 53.67 295.22 174 18.42 4.062E+OO l.254E+OO 1.255E+OO 31. 06 351. 93 249 35.60* 3.518E+OO 1.068E+OO l.069E+00 23.21 RN-222 609.32 187 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 1120.29 41 14.92 1.392E+OO 1.065E+OO 1.065E+OO 44.24 1764.49 30 15.30 9.460E-01 l.121E+OO 1.121E+OO 37.23 RA-224 240.99 85 4.10* 4.743E+OO 2.353E+OO 2.353E+OO 53.67 RA-226 609.32 187 45.49* 2.246E+OO 9.824E-01 9.827E-01 20. 96 1120. 29 41 14.92 l.392E+OO 1.065E+OO 1.065E+OO 44.24 1764.49 30 15.30 9.460E-01 l.121E+OO 1.121E+OO 37.23 AC-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 85 11. 27 3.639E+OO l .114E+OO 1.114E+OO 51. 96 794.95 ------4.25 1.823E+OO ------Line Not Found ------835.71 ------1. 61 1. 753E+OO ------Line Not Found ------911.20 71 25.80* 1. 638E+OO 8.982E-01 8.982E-01 38.82 968.97 47 15.80 1.561E+OO 1. 031E+OO 1. 031E+OO 45.21 RA-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 85 11.27 3.639E+OO l.114E+OO 1.114E+OO 51. 96 794.95 ------4.25 1.823E+OO ------Line Not Found ------835.71 ------1. 61 1. 753E+OO ------Line Not Found ------911. 20 71 25.80* 1.638E+OO 8.982E-01 8.982E-01 38.82 968. 97 47 15.80 1. 561E+OO 1. 031E+OO 1. 031E+OO 45.21 Page 3606 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 119 10.28 3.470E+OO 1.787,E+OO 1. 787E+OO 41. 48 77 .11 207 17.10 3.695E+OO 1.759E+OO 1. 759E+OO 28.75 238.63 451 43.60* 4.787E+OO 1.162E+OO 1.162E+OO 12.28 300.09 ------3.30 4.016E+OO ------Line Not Found ------TH-230 609.32 187 45.49* 2.246E+OO 9.824E-01 9.824E-01 20. 96 1120.29 41 14.92 1.392E+OO 1. 065E+OO 1. 065E+OO 44.24 1764.49 30 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 TH-232 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 85 11. 27 3.639E+OO 1.114E+OO 1.114E+OO 51. 96 835.71 ------1. 61 1.753E+OO ------Line Not Found ------911.20 7'1 25.80* 1.638E+OO 8.982E-01 8.982E-01 38.82 968. 97 47 15.80 1.561E+OO 1.031E+OO 1.031E+OO 45.21 U-234 609.32 187 45.49* 2.246E+OO 9.824E-01 9.824E-01 20.96 1120.29 41 14.92 1.392E+OO 1.065E+OO 1.065E+00 44.24 1764.49 30 15.30 9.460E-01 1.121E+OO 1.121E+OO 37.23 U-235 89. 96 ------3.47 4.758E+OO ------Line Not Found ------93.35 74 5.60 4.976E+OO 1.429E+OO 1.429E+00 81. 61 143.76 47 10. 96* 6.092E+OO 3.792E-01 3.792E-01 108.17 163.33 ------5.08 5.924E+OO ------Line Not Found ------185. 72 84 57.20 5.605E+OO 1.411E-01 1.411E-01 80.25 205.31 ------5.01 5.302E+OO ------Line Not Found ------AM-243 43.53 ------5.90 1. 701E-01 ------Line Not Found ------74.66 119 67.20* 3.470E+OO 2.733E-01 2.733E-01 41. 48 ANH-511 511.00 51 100.00* 2.588E+OO l.067E-01 l.067E-01 80.01 Flag: "*" Key line Page 3607 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235031 Acquisition date 3-0CT-2016 09:09:51 Total number of lines in spectrum 45 Number of unidentified lines 13 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Hlife 1. 25E+09Y 244.06D 461. 40D 2.30E+05Y 30.08Y 30.08Y 32.51D l.41E+10Y 1. 41E+10Y 1.41E+l0Y 1600. ODY 1600. OOY 1600. OOY l.41E+l0Y 1600. DOY 1. 41E+10Y 1. 41E+10Y 1.41E+10Y 7.54E+04Y 1. 41E+l0Y 2.45E+05Y 7.04E+08Y 7370.00Y l.OOE+09Y Decay 1. 00 2.42 1. 60 1. 00 1. 02 1. 02 771. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.398E+Ol l.045E-01 1.929E+OO 1. 929E-01 l.903E-01 2. OllE-01 8.607E-02 2.750E-01 8.238E-01 1.162E+OO 9.824E-01 1.068E+OO 9.824E-01 2.353E+OO 9.824E-01 8.982E-01 8.982E-01 1.162E+00 9.824E-01 8.982E-01 9.824E-01 3.792E-01 2.733E-01 1.067E-01 3.189E+Ol 3.189E+Ol Decay Corr pCi/GRAM 1.398E+Ol 2.534E-01 3.082E+OO 1.929E-.Ql 1.941E-01 2. 051E-01 6.638E+Ol 2.750E-01 8.238E-01 1.162E+OO 9.827E-01 1.069E+OO 9.827E-01 2.353E+OO 9.827E-01 8.982E-01 8.982E-01 1.162E+OO 9.824E-01 8.982E-01 9.824E-01 3.792E-01 2.733E-01 1.067E-01 9.950E+Ol 9.950E+Ol 71.11%
  • Decay Corr 2-Sigma Error 0.157E+Ol 2.380E-01 3.137E+OO 1. 964E-01 0.647E-01 0.684E-01 7.180E+Ol 0. 972E-01 6. 621E-01 0.143E+OO 2.060E-01 0.248E+OO 2.060E-01 l.263E+00 2.060E-01 3.487E-01 3.487E-01 0.143E+00 2.059E-01 3.487E-01 2.059E-01 4.102E-01 1.134E-01 0.854E-01 "M" Manually accepted 2-Sigma %Error 11. 23 93.95 101.77 101.77 33.35 33.35 108.17 35.35 80.37 12.28 20. 96 23.21 20.96 53.67 20. 96 38.82 38.82 12.28 20.96 38.82 20. 96 108.17 41. 48 80.01 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3608 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235031 Acquisition date : 3-0CT-2016 09:09:51 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 208.93 50 139 0.93 419.07 413 12 l.24E-02 **** 5.24E+OO 0 271.27 36 119 2.19 543.76 536 13 9.lOE-03 **** 4.35E+OO T 0 328.63 69 62 1. 61 658.48 652 15 1.77E-02 57.3 3.73E+OO T 0 367.02 19 39 2.46 135. 27 730 11 4.95E-03 **** 3.40E+OO T 0 463.71 16 30 0.67 928.65 925 9 4.17E-03 **** 2.80E+OO T 0 563.44 28 12 1. 81 1128 .11 1123 12 7.50E-03 64.2 2.39E+00 T 0 572.16 20 27 1. 44 1145.56 1140 14 5.32E-03 **** 2.36E+OO 0 627.98 17 18 0.82 1257.20 1250 12 4.50E-03 **** 2.19E+OO 1 666.32 18 9 1. 80 1333.89 1317 22 4.76E-03 80.2 2.09E+OO T 0 670.67 9 11 0.67 1342.59 1338 7 2.36E-03 **** 2.08E+OO 0 717.06 13 19 4.54 1435.36 1427 13 3.45E-03 **** 1.98E+OO 0 768. 71 33 23 6.07 1538.68 1531 15 9.03E-03 72.7 1.87E+OO 0 799.40 25 51 4.04 1600.05 1583 29 6.94E-03 **** 1.81E+OO 0 883.49 9 2 1. 23 1768.23 1764 8 2.54E-03 84.8 1.68E+OO T 0 961. 54 11 5 0.81 1924.35 1921 7 2.99E-03 98.9 1.57E+OO T 0 965. 08 14 9 0. 96 1931.43 1927 9 4.0lE-03 96. 9 1.57E+OO T 0 1054.10 6 16 3.99 2109.46 2100 11 l.81E-03 **** 1.46E+OO 0 1175.28 8 7 1.28 2351. 84 2345 9 2.22E-03 **** 1.34E+OO 7 1191. 67 20 10 2.92 2384.61 2381 12 5.64E-03 63.1 1. 33E+OO 7 1194.36 8 9 1. 83 2390.00 2381 12 2.15E-03 **** 1.32E+OO 0 1302.02 13 3 4.15 2605.31 2598 13 3.85E-03 75.8 1. 23E+OO 0 1378. 71 10 11 1. 52 2758.70 2751 11 2.78E-03 **** 1.18E+OO Flags: "T" = Tentatively associated Page 3609 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:12:12.78 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l *
  • Acquisition date 3-0CT-2016 09:09:51 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
  • Sample date 26-NOV-2015 14:25:00 Nuclide Library : SOLID *
  • Sample ID G405235031 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.3962E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 ZN-65 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 3.132E-01 1. 389E-01 1.467E+OO 8.456E-02 2.152E-02 2.273E-02 3.150E+Ol 2.902E-02 3.415E-01 4. 311E-02 5.333E-02 6.314E-02 5.333E-02 4.620E-01 5.333E-02 l.191E-01 1.191E-01 4. 311E-02 5.331E-02 l.191E-01 5.331E-02 1.955E-01 5.939E-02 2.413E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3610 of 5809 Le (pCi/GRAM 1.150E+Ol 4.647E-02 0.000E+OO 2.455E-02 3.194E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3611of5809 5.738E-02 4.669E-01 O.OOOE+OO 4.814E-02 5.461E-01 6.740E+OO 2.563E-02 1. 797E+OO 1.777E+Ol 0. 000.E+OO l.994E-01 O.OOOE+OO O.OOOE+OO 5.766E-01 7.749E+OO 9.281E-01 O.OOOE+OO 2.226E-01 4.571E+02 3.437E-02 7.879E-01 2.238E+OO 1. 672E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.140E-02 4.141E-02 5.944E+OO 4.394E-01 4.394E-01 2. 631E-02 7.971E-02 2.420E-01 O.OOOE+OO O.OOOE+OO 1.277E-01 1.633E+OO 8.627E-02 3. 391E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.280E-02 O.OOOE+OO 5.790E-02 l.316E-01 O.OOOE+OO O.OOOE+OO 1.137E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.243E-01 5.416E-02 4.734E+OO 4. lOlE-02 O.OOOE+OO 7.965E+02 O.OOOE+OO 2.185E-02 9.291E-02 1.955E-01 1.107E-01 l.098E-01 1. 710E+OO 5.210E-02 3.986E+Ol 1.943E-01 5.936E-02 2.122E-02 5.073E+00 8.952E-01 4.479E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3612 of 5809 2.555E+Ol 1.034E+02 4.871E-01 3.060E+OO 4.209E-02 7.947E+OO 3.784E-01 6.709E-01 3.799E-01 5. 3 5 lE-,Cll 2.087E-01 2.087E-01 4.620E-01 4.281E-01 5. 351E-01 5.444E-02 2.230E-01 3.451E+OO 1. 715E+OO 5.444E-02 O.OOOE+OO 1.715E+OO 2.410E-01 3.043E+02 1. 706E-01 1. OOlE-01 6.455E-02 3.395E-02 2.983E-02 l.173E-01 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:12:17.87 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • 4 DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235031.CNF;l * *Acquisition date 3-0CT-2016 09:09:51 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
  • Sample date 26-NOV-2015 14:25:00 Nuclide Library : SOLID *
  • Sample ID G405235031 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : l.3962E+02 GRAM *
  • Quantity Err ( % ) : 1. 4325E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.398E+Ol 1. 703E+OO 1. 703E+OO ZN-65 2.534E-01 2.335E-01 2.335E-01 CD-109 l.430E+OO 3.097E+00 3.097E+OO SN-126 8.950E-02 l.938E-01 l.938E-01 BA-137M l.941E-01 6.399E-02 6.399E-02 CS-137 2.051E-01 6.759E-02 6.759E-02 CE-141 3.958E+Ol 7.302E+Ol 7.302E+Ol TL-208 2.750E-01 9.599E-02 9.599E-02 BI-212 8.238E-01 6.502E-01 6.502E-01 PB-212 l.162E+00 l.530E-01 l.530E-01 BI-214 9.827E-01 2.062E-01 2.062E-01 PB-214 l.069E+OO 2.472E-01 2.472E-01 RN-222 9.827E-01 2.062E-01 2.062E-01 RA-224 3.680E-01 l.295E+OO l.295E+OO RA-226 9.827E-01 2.062E-01 2.062E-01 AC-228 8.982E-01 3.448E-01 3.448E-01 RA-228 8.982E-01 3.448E-01 3.448E-01 TH-228 l.162E+00 l.530E-01 l.530E-01 TH-230 9.824E-01 2.062E-01 2.062E-01 TH-232 8.982E-01 3.448E-01 3.448E-01 U-234 9.824E-01 2.062E-01 2.062E-01 U-235 3.792E-01 4.025E-01 4.025E-01 AM-243 1. 765E-01 l.137E-01 l.137E-01 ANH-511 l.067E-01 8.379E-02 8.379E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -4.375E+OO l.408E-t01 l.421E+Ol NOT IDENT. NA-22 2.714E-02 4.919E-02 5.068E-02 NOT IDENT. NA-24 l.OOOE+41 l.217E+41 O.OOOE+OO SHORT HLIF AL-26 -l.733E-02 3.579E-02 3.664E-02 NOT IDENT. SC-46 8.642E-02 3.686E-01 3.706E-Ol FAIL ABUN V-48 l.544E+04 2.267E+04 2.372E+04 SHORT HLIF Page 3613of5809 CR-51 1.417E+02 6.299E+02 6.332E+02 SHORT HLIF MN-54 -2.251E-02 7.483E-02 7. 551E-02 NOT IDENT. C0-56 6.602E-02 5.547E-01 5.555E-01 NOT IDENT. MN-56 1.000E+41 7.923E+41 0.000E+OO SHORT HLIF C0-57 1.209E-02 5.631E-02 5.657E-02 NOT IDENT. C0-58 -2.868E-02 6.680E-01 6.681E-01 NOT IDENT. FE-59 7.864E-01 7.630E+OO 7.638E+OO NOT IDENT. C0-60 -1.891E-02 3.539E-02 3.640E-02 NOT IDENT. GE-68 -1.027E+OO 2.286E+OO 2.332E+OO NOT IDENT. AS-7] 9.986E+OO 1. 966E+Ol 2 .. Ol 7E+Ol NOT IDENT. AS-74 -l.574E+03 1.086E+04 1.089E+04 SHORT HLIF SE-75 3.508E-02 2.304E-01 2.309E-01 NOT IDENT. BR-77 6.827E+39 6.144E+40 O.OOOE+OO SHORT HLIF SR-82 -4.920E+02 1.013E+03 l.037E+03 SHORT HLIF RB-83 2.436E-01 6.343E-01 6.437E-01 NOT IDENT. KR-85 7.363E+OO 9.006E+OO 9.598E+OO NOT IDENT. SR-85 8.803E-01 1. 079E+OO l.149E+00 NOT IDENT. RB-86 -l.277E+04 4.289E+04 4.328E+04 SHORT HLIF Y-88 1. 089E-01 2.291E-01 2.343E-01 NOT IDENT. Y-91 -2. 296E+02 5.790E+02 5.882E+02 NOT IDENT. NB-94 2. 991E-02 3.732E-02 3. 969E-02 NOT IDENT. NB-95 -5.163E-01 1.193E+OO l.216E+OO NOT IDENT. NB-95M -5.773E-01 2.846E+OO 2.858E+OO NOT IDENT. ZR-95 1. 562E+OO 1. 745E+OO 1.881E+OO NOT IDENT. NB-97 1. 000E+41 1.672E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 1. 37 6E+43 0.000E+OO SHORT HLIF M0-99 -1.495E+33 3.640E+33 O.OOOE+OO SHORT HLIF TC-99M -1. 000E+41' 1. 409E+41 O.OOOE+OO SHORT HLIF RH-101 8.540E-03 3.674E-02 3.694E-02 NOT IDENT. RH-102 -4.078E-02 6.607E-02 6.858E-02 NOT IDENT. RU-103 -5.023E+00 7.691E+OO 8.017E+OO FAIL ABUN RH-106 -6.563E-02 6.005E-01 6.012E-01 NOT IDENT. RU-106 -6.563E-02 6.005E-01 6.012E-01 NOT IDENT. AG-108M l.395E-02 2.864E-02 2.933E-02 NOT IDENT. AG-llOM 9.579E-02 7.974E-02 9.068E-02 FAIL ABUN SN-113 -5.297E-02 2.842E-01 2.852E-01 NOT IDENT. CD-115 6.198E+39 1.186E+41 O.OOOE+OO SHORT HLIF SN-ll 7M 9.306E+03 l.777E+05 l.777E+05 SHORT HLIF TE-123M -4.232E-02 1.427E-01 l.440E-01 NOT IDENT. SB-124 3.304E-01 1.813E+OO l.819E+00 NOT IDENT. SB-125 -8.641E-02 1.115E-01 l .181E-01 FAIL ABUN TE-125M 7.801E+Ol 3.957E+02 3.972E+02 NOT IDENT. I-126 2.494E+06 l.991E+06 2.287E+06 SHORT HLIF SB-126 -1.412E+06 3.066E+06 3 .131E+06 SHORT HLIF SB-127 -1. 142E+22 2.021E+23 O.OOOE+OO SHORT HLIF I-131 9.326E+09 1.427E+l0 1.488E+10 SHORT HLIF I-132 1.000E+41 l.923E+42 O.OOOE+OO SHORT HLIF TE-132 7.335E+26 5.197E+27 O.OOOE+OO SHORT HLIF BA-133 -2.023E-02 4.524E-02 4.615E-02 NOT IDENT. I-133 -1.000E+41 2.331E+41 O.OOOE+OO SHORT HLIF CS-134 3.667E-02 6.466E-02 6.674E-02 FAIL ABUN CS-135 1. 759E-02 l.624E-01 1. 626E-01 NOT IDENT. I-135 1.000E+41 7.171E+41 O.OOOE+OO SHORT HLIF CS-136 2.163E+04 7.284E+05 7.285E+05 SHORT HLIF CE-139 3.429E-02 1.221E-01 l.231E-01 NOT IDENT. BA-140 3.653E+05 2.846E+06 2.851E+06 SHORT HLIF LA-140 -4.757E+05 7.896E+05 8.183E+05 SHORT HLIF CE-143 1.000E+41 2.451E+41 O.OOOE+OO SHORT HLIF CE-144 -3.216E-01 4.216E-01 4.458E-01 NOT IDENT. PM-144 1.165E-02 6.301E-02 6.323E-02 NOT IDENT. PR-144 l.018E+OO 5.508E+OO 5.527E+00 NOT IDENT. PM-146 3.303E-03 4.718E-02 4.720E-02 NOT IDENT. ND-147 -1.085E+07 6.622E+07 6.640E+07 SHORT HLIF PM-147 -4.625E+Ol 9. 551E+o2 9.553E+02 NOT IDENT. PM-149 -1. 000E+41 2.143E+41 O.OOOE+OO SHORT HLIF EU-150 -4. 213'E-03 3.597E-02 3.602E-02 FAIL ABUN EU-152 -2.159E-04 l.060E-01 l.060E-01 FAIL ABUN GD-153 -5.504E-02 2.355E-01 2.368E-01 NOT IDENT. EU-154 5.825E-02 l.182E-01 l.211E-01 NOT IDENT. EU-155 -9.052E-03 1.310E-01 l.310E-01 FAIL ABUN TB-160 -7.102E-02 2. 371E+OO 2.371E+OO FAIL ABUN H0-166M -3.605E-02 7.800E-02 7. 968E-02 NOT IDENT. TM-171 3.902E+OO 4.541E+Ol 4.544E+Ol NOT IDENT. HF-172 -2. 723E-01 2.644E-01 2.915E-01 NOT IDENT. LU-172 -1.317E-02 7.129E-02 7.153E-02 FAIL ABUN LU-176 -l.385E-02 2.550E-02 2.626E-02 FAIL ABUN HF-181 1.333E+OO 5.735E+OO 5.766E+OO NOT IDENT. TA-182 1.057E-01 1.024E+OO 1.025E+OO FAIL ABUN Page 3614of5809 RE-183 -1. 978E+OO 5.363E+OO 5.436E+OO NOT IDENT. RE-184 -5.128E+OO 3.265E+Ol 3.273E+Ol NOT IDENT. W-188 -6.558E+Ol 1. 396E+02 l.427E+02 NOT IDENT. IR-192 -3.755E-01 5.905E-01 6.143E-01 FAIL ABUN HG-203 2.157E+OO 3.264E+OO 3.406E+OO NOT IDENT. BI-207 -l.820E-02 5.147E-02 5.212E-02 FAIL ABUN PB-210 3.590E+OO 8.744E+OO 8.893E+OO NOT IDENT. BI-211 l.660E+OO 3.463E-01 8.244E-01 NOT IDENT. PB-211 1.608E-01 7.550E-01 7.585E-01 NOT IDENT. RN-219 -1.209E-01 4. 511E-01 4.544E-01 FAIL ABUN RA-223 6.234E-02 6.689E-01 6.695E-01 FAIL ABUN AC-227 5.266E-02 2.290E-01 2.302E-01 NOT IDENT. TH-227 5.266E-02 2.290E-01 2.302E-01 NOT IDENT. TH-229 8.785E-02 5.032E-01 5.048E-01 FAIL ABUN PA-231 9.055E-02 5.285E-01 5. 301E-01 NOT IDENT. TH-231 6.234E-02 6.689E-01 6.695E-01 FAIL ABUN PA-233 -3.171E-03 6.204E-02 6.206E-02 NOT IDENT. PA-234 6.928E-02 2.539E-01 2.558E-01 FAIL ABUN PA-234M -5.147E-01 4.015E+OO 4.022E+OO NOT IDENT. TH-234 1.369E-03 1.948E+OO 1.948E+OO FAIL ABUN NP-237 -3.171E-03 6.204E-02 6.206E-02 FAIL ABUN NP-238 1. OOOE+41 3.763E+41 O.OOOE+OO SHORT HLIF U-238 l.369E-03 1.948E+OO 1.948E+OO FAIL ABUN NP-239 5.605E-02 2.818E-01 2.829E-01 NOT IDENT. PU-239 1.082E+02 3.543E+02 3.577E+02 NOT IDENT. AM-241 -l.804E-01 2.147E-01 2.296E-01 NOT IDENT. CM-243 2.973E-02 l.157E-01 1.165E-01 NOT IDENT. BK-247 2.027E-02 7.804E-02 7 .'858E-02 NOT IDENT. CM-247 -6.403E-03 3.985E-02 3.995E-02 NOT IDENT. CF-249 -2.454E-02 3.757E-02 3.916E-02 NOT IDENT. CF-251 7.552E-02 1.237E-01 l.283E-01 NOT IDENT. Page 3615of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 67. 9872 87.09 116.4670 136.47 80.9586 45.60 57.0555 87.57 116.5350 140.51 0.0000 46.54 56.0303 88.03 139.6028 143.76 77.2956 49. 72 0.0000 88.34 139.6547 144.24 77.3293 51. 35 74.5733 88.47 142.8516 145.44 83.3016 51. 87 73.5071 89. 96 124.0261 152.43 64.3407 52.39 75.8340 1093.63 97.8692 153.25 0.0000 52.97 66.8429 91.11 0.0000 323.87 71.2228 53.44 68.0280 92.59 122.0207 156.02 0.0000 54.07 78.3123 93.35 122.1289 158.56 0.0000 57.36 0.0000 94.56 92.7254 159.00 69.8098 57.53 66.1910 94.65 92.7349 162.33 72. 5644 57.98 68.5213 94. 67 92.7372 162.66 0.0000 59.27 68.6579 94.87 92.7585 163.33 73.4793 59.32 76.6738 97.43 89.0211 165.86 65.9259 59.54 77.8445 98.43 97.5526 176.31 68.2073 60.96 73.4236 98.44 97.5539 176.60 0.0000 61.17 70.0040 99.53 74.7626 177.52 64.8148 62.93 87.4475 100 .11 69.9848 181.07 0.0000 63.29 87.4939 102.03 89.4818 181.52 65.0169 63.58 82.9244 103.18 70.2233 184.41 67.7676 64.28 94.5386 103.37 66.6049 143.76 67.8350 66.73 83.3038 105.21 76.4462 193.51 69.1073 67.24 91.4697 105.31 76.4549 197.03 69.2865 125.81 90.3684 106.12 83.8095 198.01 69.3364 67.75 90.3773 106.47 75.3354 201.83 62.4876 69.67 91.7834 109.28 79.2183 203.43 59.4759 70.83 97.7492 111. 00 84.2464 205.31 71. 4666 72. 81 108.9050 111.76 0.0000 210.85 50.4885 72.87 105.8018 114. 06 71. 0419 215.65 47.1023 74.66 104.1074 116. 30 0.0000 222 .11 55.3449 74.82 104.1298 116.74 68.7806 227.09 51.0521 74.97 104.1509 119.76 68.9908 227.38 47.4786 77 .11 104.4463 121.12 69.0848 228.16 0.0000 78.74 101. 9242 121.22 69.0917 228.18 51.0892 79.69 87.9193 121.78 72.8335 116.74 51.0892 80.12 78.5426 122.06 66.6797 235.69 54.0448 80.19 0.0000 122.92 61. 7928 235.96 54.0540 80.57 110. 0230 123.07 61.8019 238.63 47.8307 81. 00 84.9210 265.00 66.7860 238.98 0.0000 81. 07 84.9287 125.81 79.3188 240.99 47.9035 81. 75 113.3364 127.23 62.0529 242.00 47.9342 83.79 80.4859 127.91 73.2708 244.70 54.3591 84.00 71.0353 129.30 70.8812 252.40 0.0000 85.43 105.9518 131. 20 64.7810 252.80 49.1726 86.55 116. 3900 133.02 67.3879 254.15 0.0000 86.79 116.4243 133. 52 79.9043 256.23 43.8020 86.94 116.4460 136.00 72.5805 260.90 0.0000 Page 3616of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 40.7262 355.39 0.0000 584.27 20.1334 264.80 38.5282 356.01 34.7073 595.83 0.0000 265.00 38.5325 364.49 0.0000 427.87 22.3792 268.22 48.2585 366.42 0.0000 602.52 0.0000 269.46 46.9150 372. 51 31. 48 90 604. 72 22.4108 270.03 .46.9305 375.05 30.1650
  • 607.14 17.6232 271.23 46.9637 377.52 33.1229 609.32 18.1711 273.65 0.0000 356.01 28.3368 610.33 18.1773 276.40 58.7464 388.16 34.2687 614.28 17. 6662 277.37 49.9076 388.63 0.0000 618.01 22.5125 277.60 48.9898 391. 69 39.2285 620.36 17 .1660 278.00 46.2270 264.66 30.5282 621. 93 19.3220 279.20 49.0351 401.81 42.3675 630.19 0.0000 279.54 59.2240 402.40 38.4366 631.29 19.3828 279.70 59.2292 404.85 34.5329 633.25 9.6976 280.46 67.5880 410.95 38.5858 634.78 0.0000 283.69 41. 7426 413.71 28.7274 635.95 17.2559 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 50.1405 423. 72 0.0000 645.85 11. 9019 285.90 0.0000 427;09 34.8768 657.76 9.7760 287.50 35.3258 427.87 34.8889 657.90 0.0000 290.67 44.7031 433.94 22.9874 661.66 9.7881 293.27 0.0000 439.40 17.0308 664.57 0.0000 351.93 42.9509 453.88 27.2153 666.33 0.0000 295. 96 42. 9687 463.37 23.2751 666.50 0.0000 879.38 63.1439 468.07 27.3763 667.71 0.0000 299.98 42.1289 473.00 0.0000 677.62 17.4902 300.09 42.1317 475.06 18.3029 685.70 0.0000 300.13 42.1326 476.78 27.4735 695.00 0.0000 301.36 46.3770 477.60 23. 4113 696.49 19.7930 302.85 49.6972 482.18 24.4741 696. 51 19.7930 256.23 39.4186 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.8980 306.78 46.0462 497.08 29.7487 697.49 20.8995 308.46 36.6823 505.52 15.4382 702.65 16.5259 311. 90 40.5207 507.63 0.0000 706.68 28.6798 316.51 52.9022 511. 00 23. 7225 711.68 26.5146 319.41 0.0000 514.00 26.3311 720.70 0.0000 320.08 0.0000 514.00 26.3311 721. 93 0.0000 321.04 46.4011 520.40 13.4570 722.78 11. 6395 323.87 36.9870 520.69 0.0000 722.91 14. 9656 325.23 48.4019 522.65 0.0000 723.31 13.3042 328.76 0.0000 527.90 0.0000 724.19 19. 9614 333.37 37.1711 528.26 13.4972 727.33 12.2103 333.97 37.1822 529.59 17.6585 733.00 6.6714 334.37 31. 4686 529.87 0.0000 735.93 8.9030 338.28 42.9977 531. 02 0.0000 333.97 17.8145 338.32 42.9987 537.26 0.0000 739.50 0.0000 311. 90 45.9160 546.56 0.0000 747.24 6.6997 340.48 45.9160 552.55 34.5724 748.06 12.2859 340.55 0.0000 563.25 18.9309 752.31 12. 3011 344.28 43.1296 569.33 27.4049 753.82 0.0000 345.93 48.3461 946.00 27.4060 756.73 11.1975 351.06 37.5067 569.70 27.4081 756.80 11.1979 351. 93 37.5234 583.19 20.1257 884.68 6.7327 Page 3617 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 21.8931 1274.44 7.1567 1620.50 4.0481 766.42 21. 3356 1001.03 10.7476 1621. 92 6.0736 766.84 21.3379 1002.74 6.2720 1678.03 0.0000 772.60 0.0000 1004.73 12.5499 1690.97 2.0475 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 Q.0000 1025.87 0.0000 17.64. 4 9 2.0714 778.90 12. 3965 1028.54 0.0000 1063.66 9. 3296 783.70 0.0000 1037.84 12.6473 1771. 35 2.0736 785.37 10.1613 1038.76 0.0000 1791.20 0.0000 792.07 16.9678 631. 29 5.7934 1808.65 6.2563 794.95 20.3782 1048.07 0.0000 1810.72 0.0000 795.86 20.3833 1049.04 15.9414 1836.06 2.0941 810.06 15.9169 1050.41 11.5977 810.29 15.9180 1063.66 12.7234 344.28 13.6445 1077.00 0.0000 810.76 13.6455 1077.34 12.7627 815.77 0.0000 1085.87 10.0473 1048.07 0.0000 1093.63 10.9797 832.01 12.5818 1099.45 10.0775 834.85 18.3151 1112. 07 11. 7 594 835.71 14.8847 1112.84 7. 3511 836.80 0.0000 1115. 54 10.2977 846.75 0.0000 1120.29 10.3079 846.77 13.7808 1120.55 10.3086 856.80 0.0000 1221.41 10.3106 860.56 12.6794 1129. 67 11. 0669 871. 09 8.0912 1131.51 0.0000 873.19 9.2523 1147.95 0.0000' 875.33 0.0000 1173.23 7.4473 879.38 12.1633 1177.95 5. 9641 880.51 15.6429 1189.05 4.4833 883.24 8 .1171 1204.77 1.3.1199 884.68 5.2200 1221. 41 13 .1643 889.28 8.1299 1231. 02 11. 3064 894.76 8 .1413 1235.36 0.0000 898.04 16.2969 1238.28 16.9849 900.72 6.9890 1260.41 0.0000 903.28 9.3249 1271.87 14.2502 911.20 15.7676 1274.44 8.5545 912.08 15.7714 1274.54 8.5545 923.98 0.0000 1291.59 10.4911 926.50 7.9146 1298.22 0.0000 929 .11 18.4795 1312 .11 0.0000 937.49 17.6367 1332.49 8.6523 944 .13 0.0000 1362.66 0.0000 946.00 8.8370 1365.19 9.6735 949.00 12.3812 1368.63 0.0000 667.71 0.0000 1384.29 4.8541 962. 31 0.0000 1408.01 6.8257 964. 08 0.0000 1457.56 0.0000 966 .17 10.6575 1460.82 8.8610 911.20 11.3758 1489.16 3.9583 968.97 11. 37 58 1505.03 8.9308 983.53 0.0000 1584.12 8.0474 984.45 0.0000 1596.21 0.0000 Page 3618of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:12:46.63 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM39.CNF;134 Background date : Z-OCT-2016 11:02:13. Sample date : 23-NOV-2015 11:48:00 Acquisition date : 3-0CT-2016 09:10:21. Sample ID : G405235032 Sample quantity : l.46947E+02 GRAM Detector name : GAM39 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:07.00 0.2% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 3 3 0 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 Energy 46.54* 63.44* 74.79* 77.18* 84.33* 86.94 92.93* 185.82* 195.09 210 .13 238.80* 241.85 295.22* 300.60* 327.47 338.81* 352.21* 463.35 511. 57* 583.73* 601.68 609.44* 661.59 694.50 727.35* 785.08 870.59 875.67 911. 48* 969. 95* 1027.79 1095.58 1102. 55 1120. 45 Page 3619of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 79 93 238 305 35 63 83 83 21 46 373 115 119 23 57 65 164 30 37 86 21 153 57 26 39 30 16 8 71 27 7 7 20 28 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 173 303 179 135 167 157 163 83 76 109 65 59 41 57 45 62 79 17 32 42 6 17 41 38 16 15 13 6 13 34 3 12 0 9 2.05 1. 39 1. 55 1. 08 1. 03 0.82 1. 29 1. 33 0.52 2.74 1. 33 1. 90 1. 36 0.93 2.41 1. 34 1. 40 1. 02 2.17 1. 27 1. 81 0.90 1. 51 5.16 1. 72 1. 43 0.75 0.75 0.84 1. 59 1. 06 1. 47 1. 28 0.68 92.93 126.72 149.42 154.20 168.50 173.72 185 .. 71 371. 48 390.02 420 .11 477.45 483.56 590.29 601.04 654.79 677.47 704.28 926.56 1023.02 1167. 35 1203.24 1218.76 1323.08 1388.89 1454.62 1570.07 1741.13 1751.27 1822.90 1939.87 2055.57 2191.17 2205.10 2240.91 87 119 142 142 164 172 182 366 384 415 469 469 584 596 648 672 699 923 1015 1160 1200 1212 1315 1381 1448 1563 1736 1748 1817 1931 2052 2186 2200 2236 12 2.18E-02 14 2.60E-02 16 6.62E-02 16 8.47E-02 8 9.69E-03 7 1.75E-02 9 2.30E-02 10 2.32E-02 8 5.83E-03 12 1.28E-02 21 1.03E-01 21 3.21E-02 11 3.32E-02 9 6.32E-03 12 1. 59E-02 11 1.81E-02 13 4.57E-02 7 8.26E-03 16 1.04E-02 14 2.39E-02 7 5.73E-03 12 4.25E-02 15 1.58E-02 17 7.17E-03 13 1.07E-02 13 8.24E-03 13 4.44E-03 7 2.35E-03 16 1.99E-02 14 7.59E-03 6 2.00E-03 9 2.08E-03 11 5.56E-03 9 7.83E-03 36.2 42.0 13.0 9.1 68.1 35.2 32.5 24.5 75.8 47.9 6.6 21. 0 14.2 64.4 26. 8 27.4 14.0 29.6 47.1 19.8 30.4 10.1 28.0 58.3 28.1 33.3 52.8 56.9 16.9 50.3 52.9 89.1 22.4 26. 9 Fit 3.58E+OO 3.79E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235032 Acquisition date 3-0CT-2016 09:10:21 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1276.45 13 5 1. 55 2552. 96 2547 11 3.64E-03 43.9 36 0 1378.17* 14 8 2.49 2756.43 2750 11 3.89E-03 50.0

  • 37 0 1408.72* 7 3 1. 58 2817.55 2810 11 1. 98E-03 63.9 38 0 1461.03* 271 7 1. 82 2922.19 2915 14 7.52E-02 6.5 39 0 1764.74* 23 0 1. 60 3529.75 3523 12 6.40E-03 21. 9 Flag: "*" = Peak area was modified by background subtraction Page 3620 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:12:48 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 23-NOV-2015 11:48:00 G405235032 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:10:21 146.95 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID. GAMMA39 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3621of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:07.00 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235032 Acquisition date 3-0CT-2016 09:10:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 8. 983E-.Ol l.391E+Ol l.391E+Ol 13.08 " OK CD-109 88.03 3.70* 6.756E+OO 6.225E-01 9.991E-01 186.05 OK SN-126 64.28 9.60 6.928E+OO 9.148E-01 9.148E-01 84.02 OK 86.94 8.90 6.756E+00 2.588E-01 2.588E-01 186.05 OK 87.57 37.00* 6.756E+OO 6.225E-02 6.225E-02 186.05 OK BA-137M 661.66 89.90* 1.758E+OO 1.909E-01 l.947E-01 56.06 OK CS-137 661.66 85.10* 1.758E+OO 2.017E-01 2.057E-01 56.06 OK TL-208 277.37 6.60 3.709E+OO Line Not Found Absent 583.19 85.00* 1. 951E+OO 2.793E-01 2.793E-01 39.69 OK 860.56 12.50 l.416E+00 Line Not Found Absent PB-210 46.54 4.25* 6.818E+OO 1.809E+OO 1.858E+OO 72.39 OK BI-212 727. 33 6.67* l.626E+OO 1.877E+OO 1.877E+OO 56.14 OK 785.37 1.10 1.527E+OO 9.243E+OO 9.243E+OO 66.67 OK 1620.50 1. 47 8.143E-01 Line Not Found Absent PB-212 74.82 10.28 6.812E+OO l.591E+00 1.591E+OO 37.30 OK 77 .11 17.10 6.799E+OO 1.682E+OO 1.682E+OO 18.11 OK 238.63 43.60* 4.209E+OO 1.185E+OO l.185E+00 13.14 OK 300.09 3.30 3.460E+OO l.139E+OO l.139E+00 128.73 OK B!-214 609.32 45.49* 1.882E+OO 9.574E_:.01 9.578E-01 20.12 OK 1120.29 14.92 l.136E+OO 8.399E-01 8.402E-01 53.71 OK 1764.49 15.30 7.484E-01 9.708E-01 9. 711E-01 43.82 OK PB-214 74.82 5.80 6.812E+00 Line Not Found <<INT Reject 77 .11 9.70 6.799E+OO 2. 965E+OO 2. 967E+OO 18 .11 OK 87.09 3.41 6.755E+OO Line Not Found <<INT Reject 242.00 7.25 4.163E+OO Line Not Found <<INT Reject 295.22 18.42 3.514E+OO l.058E+OO l.058E+OO 28.48 OK 351.93 35.60* 3.012E+OO 8.653E-01 8.656E-01 27.98 OK RN-222 609.32 45.49* 1. 882E+OO 9.574E-01 9.578E-01 20.12 OK 1120. 29 14.92 l.136E+OO 8.399E-01 8.402E-01 53.71 OK 1764.49 15.30 7.484E-01 9.708E-01 9. 711E-01 43.82 OK RA-224 240.99 4.10* 4.165E+OO 2.073E+00 2.073E+OO 84.04 OK RA-226 609.32 45.49* 1.882E+OO 9.574E-01 9.578E-01 20.12 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.402E-01 53.71 OK 1764.49 15.30 7.484E-01 9.708E-01 9. 711E-01 43.82 OK AC-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .116E+OO 1. 051E+OO 1. 051E+OO 54.90 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835.71 1. 61 1. 451E+OO Line Not Found Absent 911.20 25.80* 1. 351E+OO 1.058E+OO 1.058E+OO 33.79 OK 968. 97 15.80 l.283E+OO 6.913E-01 6. 913E-01 100.57 OK RA-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .116E+OO 1. 051E+OO 1.051E+OO 54.90 OK 794.95 4.25 l.512E+00 Line Not Found Absent 835.71 1. 61 1. 451E+OO Line Not Found Absent 911. 20 25.80* 1. 351E+OO 1.058E+OO 1.058E+OO 33.79 OK 968. 97 15.80 l.283E+OO 6.913E-01 6.913E-01 100.57 OK TH-228 74.82 10.28 6.812E+OO 1.591E+OO 1.591E+OO 37.30 OK 77 .11 17.10 6.799E+OO 1.682E+OO 1.682E+OO 18 .11 OK 238.63 43.60* 4.209E+00 1.185E+OO 1.185E+OO 13.14 OK Page 3622 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235032 Acquisition date 3-0CT-2016 09:10:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 3.460E+OO 1.139E+OO l.139E+OO 128.73 OK TH-230 609.32 45.49* l.882E+OO 9.574E-01 9.574E-01 20.12 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.399E-01 53.71 OK 1764.49 15.30 7.484E-01 9.708E-01 9.708E-01 43.82 OK PA-231 283.69 1. 70 3.638E+OO Line Not Found Absent 301.36 5.35* 3.460E+OO 7.028E-01 7.028E-01 128.73 OK TH-232 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .116E+OO 1. 051E+OO 1.051E+OO 54.90 OK 835. 71 1. 61 1. 451E+OO Line Not Found Absent 911. 20 25.80* 1. 351E+OO 1.058E+OO 1.058E+OO 33.79 OK 968.97 15.80 1.283E+OO 6.913E-01 6.913E-01 100.57 OK TH-234 63.29 3.70* 6.928E+OO 2.373E+OO 2.373E+00 84.02 OK 92.59 4.23 6. 722E+OO 1.838E+OO 1.838E+OO 65.07 OK U-234 609.32 45.49* 1.882E+OO 9.574E-01 9.574E-01 20.12 OK 1120.29 14.92 l.136E+OO 8.399E-01 8.399E-01 53.71 OK 1764.49 15.30 7.484E-01 9.708E-01 9.708E-01 43.82 OK U-238 63.29 3.70* 6.928E+OO 2.373E+OO 2.373E+OO 84.02 OK 92.59 4.23 6. 722E+OO 1.838E+OO 1.838E+OO 65.07 OK AM-243 43.53 5.90 *6.236E+OO Line Not Found Absent 74.66 67.20* 6.812E+00 2.434E-01 2.434E-01 37.30 OK ANH-511 511. 00 100.00* 2.181E+OO 9.366E-02 9.366E-02 94.28 OK Flag: "*" = Keyline Page 3623 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:12:49.55 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l *
  • Acquisition date 3-0CT-2016 09:10:21 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:07.00 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:48:00 Analyst initials: MXRl *
  • Sample ID G405235032 Sample Quantity 1.4695E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKA100': [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.391E+Ol 1.783E+OO CD-109 9.991E-01 1.822E+OO SN-126 6.225E-02 1.135E-01 BA-137M 1.947E-01 1.070E-01 CS-137 2.057E-01 1.130E-01 TL-208 2.793E-01 1.086E-01 PB-210 l.858E+OO 1.318E+OO BI-212 1.877E+OO l.033E+OO PB-212 1.185E+OO l.527E-01 BI-214 9.578E-01 l.889E-01 PB-214 8.656E-01 2.374E-01 RN-222 9.578E-01 1.889E-01 RA-224 2.073E+OO 1.707E+OO RA-226 9.578E-01 1.889E-01 AC-228 1.058E+OO 3.503E-01 RA-228 1.058E+OO 3.503E-01 TH-228 1.185E+OO 1.527E-01 TH-230 9.574E-01 1. 888E-01 PA-231 7.028E-01 8.866E-01 TH-232 1.058E+OO 3.503E-01 TH-234 2.373E+OO 1.954E+OO U-234 9.574E-01 l.888E-01 U-238 2.373E+00 l.954E+OO AM-243 2.434E-01 8.898E-02 ANH-511 9. 366E-02. 8.653E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3624 of 5809 Key-Line Activity (pCi/GRAM -6.462E+OO -7.868E-03 O.OOOE+OO 3.435E-03 1.055E-01 K.L. Cnt Uncert (1.96-sigma) 1.861E+Ol 7.425E-02 1. 960E+41 3.741E-02 5.506E-01 MDA (pCi/GRAM 7.664E-01 1.959E+OO 1.220E-01 8.901E-02 9.403E-02 7.193E-02 8.477E-01 1.120E+00 9. 966E-02 1.435E-01 1.405E-01 1.435E-01 1.069E+OO 1.435E-01 2.695E-01 2.695E-01 9. 966E-02 1.434E-01 9.121E-01 2.695E-01 l.lOOE+OO 1.434E-01 1.lOOE+OO 5.812E-02 5.689E-02 MDA (pCi/GRAM 3.370E+Ol l.247E-01 0.000E+OO 8.253E-02 1.131E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 3.276E+04 O.OOOE+OO SHORT HLIF CR-51 0.000E+OO 6.835E+02 0.000E+OO SHORT HLIF MN-54 -l.174E-02 8.448E-02 1.652E-01 NOT IDENT. C0-56 3.179E-03 6.325E-01 1.279E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -7.879E-02 5.591E-02 8.788E-02 NOT IDENT. C0-58 3.985E-01 7.408E-01 l.630E+OO NOT IDENT. FE-59 6.214E+OO 1. 021E+Ol l.841E+Ol NOT IDENT. C0-60 6.175E-03 4.475E-02 9.417E-02 NOT IDENT. ZN-65 3.938E-02 2.4.35E-01 4.421E-01 NOT IDENT. GE-68 -5.495E-02 3.006E+OO 5.989E+OO NOT IDENT. AS-73 -2.061E+OO 3.140E+OO 5.570E+OO NOT IDENT. AS-74 O.OOOE+OO 1.278E+04 0.000E+OO SHORT HLIF SE-75 -6.568E-02 2.402E-01 4.567E-01 NOT IDENT. BR-77 O.OOOE+OO 2.221E+39 0.000E+OO SHORT HLIF SR-82 0.000E+OO l.445E+03 0.000E+OO SHORT HLIF RB-83 l.496E-01 8.844E-01 1. 730E+OO NOT IDENT. KR-85 6.786E+OO 8. 496E+OO 1.650E+Ol NOT IDENT. SR-85 8.362E-01 1.051E+OO 2.040E+OO NOT IDENT. RB-86 O.OOOE+OO 5.737E+04 O.OOOE+OO SHORT HLIF Y-88 l.282E-01 1.653E-01 5.428E-01 NOT IDENT. Y-91 -5.732E+02 8.145E+02 l.406E+03 NOT IDENT. NB-94 -l .139E-02 4.232E-02 7. 572E-02 FAIL ABUN NB-95 2.377E-01 l.270E+OO 2.436E+OO NOT IDENT. NB-95M 3.200E-01 3.371E+OO 5.933E+OO NOT IDENT. ZR-95 1.020E+OO 2 .112E+OO 4.292E+00 NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.022E+34 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.577E+41 O.OOOE+OO SHORT HLIF RH-101 -3. 871E-02 3.819E-02 6.240E-02 NOT IDENT. RH-102 -6.147E-03 7.564E-02 1. 414E-01 NOT IDENT. RU-103 -5.187E+OO 8.262E+OO l.445E+Ol FAIL ABUN RH-106 5.840E-01 5.986E-01 1.305E+OO NOT IDENT. RU-106 5.840E-01 5.986E-01 1.305E+OO NOT IDENT. AG-108M -9.803E-03 3.lOlE-02 5.742E-02 NOT IDENT. AG-llOM 8.754E-03 l.377E-01 2. 771E-01 NOT IDENT. SN-113 -3.520E-01 3.081E-01 5. lllE-01 NOT IDENT. CD-115 O.OOOE+OO 1.538E+41 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 2.127E+05 O.OOOE+OO SHORT HLIF TE-123M -4.061E-02 l.430E-01 2.772E-01 NOT IDENT. SB-124 9.029E-01 2.943E+OO 6.773E+OO NOT IDENT. SB-125 -8.656E-02 l.246E-01 2.182E-01 FAIL ABUN TE-125M -2.878E+02 3.106E+02 5.160E+02 NOT IDENT. I-126 O.OOOE+OO 3.079E+06 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 3.433E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 4 .114E+23 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 2.263E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 1.110E+28 O.OOOE+OO SHORT HLIF BA-133 -l.616E-02 5.183E-02 8.539E-02 NOT IDENT. I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 3.412E-04 6.250E-02 1. 251E-01 NOT IDENT. CS-135 -5.162E-02 1.712E-01 3.214E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 8.142E+05 O.OOOE+OO SHORT HLIF CE-139 -l.305E-01 1. 2 62E-01 2.299E-01 NOT IDENT. BA-140 O.OOOE+OO 3.535E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1.380E+06 O.OOOE+OO SHORT HLIF CE-141 -2.275E+Ol 3. 372E+Ol 6.394E+Ol NOT IDENT. CE-143 O.OOOE+OO l.100E+41 O.OOOE+OO SHORT HLIF CE-144 -6.124E-02 3.475E-01 6.852E-01 NOT IDENT. PM-144 7.378E-02 7.863E-02 1.639E-01 NOT IDENT. PR-144 6.445E+OO 6.882E+OO 1.434E+Ol NOT IDENT. PM-146 -4.878E-03 5.283E-02 9.995E-02 NOT IDENT. ND-147 0.000E+OO 1.137E+OB O.OOOE+OO SHORT HLIF PM-147 -4.251E+02 8.860E+02 1. 531E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 4.225E-03 3.281E-02 5.755E-02 FAIL ABUN EU-152 4.650E-02 1.115E-01 2.152E-01 FAIL ABUN GD-153 -1.553E-01 1.940E-01 2.981E-01 NOT IDENT. EU-154 -3.456E-02 1.781E-Ol 2.931E-01 NOT IDENT. EU-155 6.434E-02 1.064E-01 2.031E-01 FAIL ABUN TB-160 4.028E-01 2.971E+OO 5.426E+OO FAIL ABUN H0-166M 2.250E-02 6.452E-02 1.299E-01 FAIL ABUN TM-171 3.074E+OO 5. 872E+OO 1.137E+Ol NOT IDENT. HF-172 -3.020E-01 2.639E-01 4.258E-01 FAIL ABUN LU-172 5.645E-02 9.457E-02 1. 930E-01 FAIL ABUN Page 3625 of 5809 LU-176 1.050E-02 2.740E-02 5. 351E-02 FAIL ABUN HF-181 5.006E+00 6.683E+OO 1.395E+Ol NOT IDENT. TA-182 -4.823E-01 1.278E+OO 2.355E+OO FAIL ABUN RE-183 4.347E-01 1.419E+OO 2.509E+OO NOT IDENT. RE-184 3.156E+Ol 4.974E+Ol 1.085E+02 NOT IDENT. W-188 -4.407E+Ol l.548E+02 2. 596E+02 FAIL ABUN IR-192 1.918E-01 5.619E-01 1.134E+OO FAIL ABUN HG-203 1.718E+OO 3.512E+OO 7.062E+OO NOT IDENT. BI-207 9.375E-03 6.418E-02 1. 294E-01 FAIL ABUN BI-211 O.OOOE+OO 6.539E-01 8.785E-01 FAIL ABUN PB-211 6.792E-01 8.782E-01 1. 794E+OO NOT IDENT. RN-219 -8.680E-02 5.175E-01 9.636E-01 NOT IDENT. RA-223 -4.522E-01 7.949E-01 1. 265E+OO FAIL ABUN AC-227 2. 963E-02 2.816E-01 5.478E-01 FAIL ABUN TH-227 2. 963E-02 2.816E-01 5.478E-01 FAIL ABUN TH-229 1.113E-01 4.786E-01 9.562E-01 FAIL ABUN TH-231 -4.522E-01 7.949E-01 1. 265E+OO FAIL ABUN PA-233 -l.112E-02 6.766E-02 1. 287E-01 FAIL ABUN PA-234 -7.373E-02 3.457E-01 6.699E-01 NOT IDENT. PA-23.4M 1. 24 7E+OO 4.672E+00 9.997E+OO NOT IDENT. U-235 -3.449E-03 1.867E-01 3. 696E-01 FAIL ABUN NP-237 -l.112E-02 6.766E-02 1.287E-01 FAIL ABUN NP-238 O.OOOE+OO 1.535E+41 O.OOOE+OO SHORT HLIF NP-239 9 .117E-03 2.591E-01 4.694E-01 NOT IDENT. PU-239 5.093E+02 3.321E+02 6. 720E+02 NOT IDENT. AM-241 -1.444E-02 6.603E-02 1.108E-01 NOT IDENT. CM-243 -3.460E-03 9.758E-02 1.769E-01 NOT IDENT. BK-247 -5.904E-02 7.827E-02 1. 414E-01 FAIL ABUN CM-247 -1.206E-02 4.764E-02 8.791E-02 NOT IDENT. CF-249 -2.708E-03 4.882E-02 9.238E-02 NOT IDENT. CF-251 -4.573E-02 1.222E-01 2.336E-01 NOT IDENT. Page 3626 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:12:47.43 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 261 10.66* 8.983E-01 1.391E+Ol l.391E+Ol 13.08 CD-109 88.03 78 3.70* 6.756E+OO 1.597E+OO 2.563E+OO 70.40 SN-126 64.28 119 9.60 6.928E+OO 9.148E-01 9.148E-01 84.02 8 6 .. 94 78 8.90 6.756E+OO 6.640E-01 6.640E-01 70.40 87.57 78 37.00* 6.756E+OO l.597E-01 l.597E-01 70.40 BA-137M 661. 66 59 89.90* 1. 758E+OO 1.909E-01 1. 94 7E-01 56.06 CS-137 661. 66 59 85.10* 1. 758E+OO 2.017E-01 2.057E-01 56.06 TL-208 277.37 ------6.60 3.709E+OO ------Line Not Found ------583.19 91 85.00* 1.-951E+OO 2.793E-01 2.793E-01 39.69 860.56 ------12.50 1.416E+OO ------Line Not Found ------PB-210 46.54 103 4.25* 6.818E+00 1.809E+00 1.858E+OO 72.39 BI-211 72. 87 ------1.23 6.824E+OO ------Line Not Found ------351.06 182 12.92* 3.012E+OO 2.384E+OO 2.384E+OO 27.98 BI-212 727.33 40 6.67* -1.626E+OO 1.877E+OO 1.877E+OO 56.14 785.37 30 1.10 1.527E+OO 9.243E+OO 9.243E+OO 66.67 1620.50 ------1. 47 8.143E-01 ------Line Not Found ------PB-212 74.82 300 10.28 6.812E+OO 2.188E+OO 2.188E+OO 25.99 77 .11 383 17.10 6.799E+OO 1.682E+OO 1.682E+OO 18 .11 238.63 426 43.60* 4.209E+OO 1.185E+OO l.185E+OO 13.14 300.09 25 3.30 3.460E+OO 1.139E+OO 1.139E+OO 128.73 BI-214 609.32 160 45.49* 1.882E+OO 9.574E-01 9.578E-01 20.12 1120.29 28 14.92 1.136E+OO 8.399E-01 8.402E-01 53.71 1764.49 22 15.30 7.484E-01 9.708E-01 9.711E-01 43.82 PB-214 74.82 300 5.80 6.812E+OO 3.877E+OO 3.879E+OO 25.99 77 .11 383 9.70 6.799E+OO 2.965E+OO 2.967E+OO 18 .11 87.09 78 3.41 6.756E+OO 1. 733E+OO 1. 734E+OO 70.40 242.00 132 7.25 4.165E+OO 2.230E+OO 2. 231E+OO 42.07 295.22 134 18.42 3.514E+OO 1.058E+OO 1.058E+OO 28.48 351. 93 182 35.60* 3.012E+OO 8.653E-01 8.656E-01 27.98 RN-222 609.32 160 45.49* 1.882E+OO 9.574E-01 9.578E-01 20.12 1120.29 28 14.92 l.136E+00 8.399E-01 8.402E-01 53. 71 1764.49 22 15.30 7.484E-01 9.708E-01 9.711E-01 43.82 RA-224 240.99 132 4.10* 4.165E+OO 3.943E+OO 3.943E+OO 42.07 RA-226 609.32 160 45.49* 1.882E+OO 9.574E-01 9.578E-01 20.12 1120.29 28 14.92 l.136E+00 8.399E-01 8.402E-01 53. 71 1764.49 22 15.30 7.484E-01 9.708E-01 9.711E-01 43.82 AC-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 72 11. 27 3 .116E+OO 1.051E+OO 1. 051E+OO 54.90 794.95 ------4.25 1.512E+OO ------Line Not Found ------835.71 ------1. 61 1. 451E+OO ------Line Not Found ------911.20 72 25.80* 1. 351E+OO 1.058E+OO 1.058E+OO 33.79 968. 97 27 15.80 1.283E+OO 6.913E-01 6.913E-01 100.57 RA-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 72 11. 27 3 .116E+OO 1.051E+OO 1. 051E+OO 54.90 794.95 ------4.25 1.512E+OO ------Line Not Found ------835.71 ------1. 61 1.451E+OO ------Line Not Found ------911. 20 72 25.80* 1.351E+OO 1.058E+OO 1.058E+OO 33.79 Page 3627 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235032 Acquisition date 3-0CT-2016 09:10:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968. 97 27 15.80 1. 283E+OO 6.913E-01 6.9il3E-01 100.57 TH-228 74.82 300 10.28 6.812E+OO 2.188E+OO 2.188E+OO 25.99 77 .11 383 17.10 6.799E+OO l.682E+OO l.682E+OO 18 .11 238.63 426 43.60* 4.209E+OO l.185E+OO l.185E+OO 13 .14 300.09 25 3.30 3.460E+OO l.139E+OO l.139E+OO 128.73 TH-230 609.32 160 45.49* l.882E+OO 9.574E-01 9.574E-01 20.12 1120.29 28 14.92 l.136E+OO 8.399E-01 8.399E-01 53.71 1764.49 22 15.30 7.484E-01 9.708E-01 9.708E-01 43.82 PA-231 283.69 ------1. 70 3.638E+OO ------Line Not Found ------301.36 25 5.35* 3.460E+OO 7.028E-01 7.028E-01 128.73 TH-232 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 72 11. 27 3 .116E+OO l.051E+OO 1. 051E+OO 54.90 835.71 ------1. 61 l.451E+OO ------Line Not Found ------911.20 72 25.80* l.351E+OO l.058E+OO l.058E+OO 33.79 968. 97 27 15.80 1. 283E+OO 6.913E-01 6.913E-01 100.57 TH-234 63.29 119 3.70* 6.928E+OO 2.373E+OO 2.373E+00 84.02 92.59 102 4.23 6.722E+OO l.838E+OO l.838E+OO 65.07 U-234 609.32 160 45.49* 1. 882E+OO 9.574E-01 9.574E-01 20.12 1120.29 28 14.92 8.399E-01 8.399E-01 53.71 1764.49 22 15.30 7.484E-01 9.708E-01 9.708E-01 43.82 U-238 63.29 119 3.70* 6.928E+00 2.373E+OO 2.373E+OO 84.02 92.59 102 4.23 6.722E+OO l.838E+OO l.838E+OO 65.07 AM-243 43.53 ------5.90 6.236E+OO ------Line Not Found ------74.66 300 67.20* 6.812E+OO 3.347E-01 3.347E-01 25.99 ANH-511 511. 00 40 100.00* 2.181E+OO 9.366E-02 9.366E-02 94.28 Flag: "*" Key line Page 3628 of 5809 Summary of Nuclide Activity Sample ID : G405235032 Acquisition date Page : 3 3-0CT-2016 09:10:21 Total number of lines in spectrum 39 Number of unidentified lines 5 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 22.20Y 7.04E+08Y l.41E+l0Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 60 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 391E+Ol 1.597E+OO l.597E-01 l.909E-01 2.017E-01 2.793E-01 1.809E+OO 2.384E+OO 1.877E+OO l.185E+00 9.574E-01 8.653E-01 9.574E-01 3.943E+OO 9.574E-01 1.058E+OO 1.058E+OO 1.185E+OO 9.574E-01 7.028E-01 1.058E+OO 2.373E+OO 9.574E-01 2.373E+OO 3.347E-01 9.366E-02 4.343E+Ol 4.343E+Ol
  • Decay Corr pCi/GRAM 1.391E+Ol 2.563E+OO l.597E-01 1. 947E-01 2.057E-01 2.793E-01 1.858E+OO 2.384E+OO 1.877E+OO 1.185E+OO 9.578E-01 8.656E-01 9.578E-01 3.943E+OO 9.578E-01 1.058E+OO 1.058E+OO 1.185E+OO 9.574E-01 7.028E-01 l.058E+OO 2.373E+OO 9.574E-01 2.373E+OO 3.347E-01 9.366E-02 4.445E+Ol 4.445E+Ol 87.18% Decay Corr 2-Sigma Error 0.182E+Ol 1.805E+OO 1.124E-01 l.092E-01 l.153E-01 l.109E-01 1.345E+OO 0.667E+OO 1.054E+OO 0.156E+OO 1.927E-01 2.422E-01 1.927E-01 1.659E+OO l.927E-01 0.357E+OO 0.357E+OO 0.156E+00 1.927E-01 9.047E-01 0.357E+OO 1.994E+00 l.927E-01 1.994E+OO 0.870E-01 8.830E-02 "M" Manually accepted 2-Sigma %Error 13.08 70.40 70.40 56.06 56.06 39.69 72. 39 27.98 56.14 13.14 20.12 27.98 20.12 42.07 20.12 33.79 33.79 13 .14 20.12 128.73 33.79 84.02 20.12 84.02 25.99 94.28 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3629 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235032 Acquisition date : 3-0CT-2016 09:10:21 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 84.33 43 209 1. 03 168.50 164 8 9.69E-03 **** 6.77E+OO T 0 185.82 97 96 1. 33 371.48 366 10 2.32E-02 49.0 5. llE+OO T 0 195.09 24 88 0.52 390.02 384 8 5.83E-03 **** 4.93E+OO 0
  • 210.13 53 126 2.74 420 .11 12 1.28E-02 95.9 4.66E+OO T 0 327.47 64 50 2.41 654.79 648 12 1.59E-02 53.6 3.21E+OO T 0 463.35 32 19 1. 02 926.56 923 7 8.26E-03 59.2 2.37E+OO T 0 601.68 22 7 1. 81 1203.24 1200 7 5.73E-03 60.8 1. 90E+OO T 0 694.50 27 40 5.16 1388.89 1381 17 7.17E-03 **** 1. 69E+OO T 0 870.59 16 13 0.75 1741.13 1736 13 4.44E-03 **** 1. 40E+OO T 0 875.67 9 6 0.75 1751.27 1748 7 2.35E-03 **** 1. 40E+OO T 0 1027.79 7 3 1. 06 2055.57 2052 6 2.00E-03 **** 1. 22E+00 T 0 1095.58 7 11 1. 47 2191.17 2186 9 2.08E-03 **** 1.16E+OO 0 1102. 55 20 0 1. 28 2205.10 2200 11 5.56E-03 44.7 1.15E+OO 0 1276.45 13 5 1. 55 2552.96 2547 11 3.64E-03 87.8 1.0lE+OO 0 1378.17 14 8 2.49 2756.43 2750 11 3.89E-03 **** 9.48E-01 0 1408.72 7 3 1. 58 2817.55 2810 11 1.98E-03 **** 9.29E-01 T Flags: "T" = Tentatively associated Page 3630 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:13:01.06 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l *
  • Acquisition date 3-0CT-2016 09:10:21 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:07.00 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:48:00 Nuclide Library : SOLID *
  • Sample ID G405235032 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : l.4695E+02 GRAM * *Wet wt corr 1.00000 Wet Weight* 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.107E-01 9.323E-01 5.806E-02 3.995E-02 4.220E-02 3.169E-02 3.974E-01 4.950E-01 4.590E-02 6.348E-02 6.355E-02 6.348E-02 4.924E-01 6.348E-02 1.146E-01 1.146E-01 4.590E-02 6.346E-02 4.171E-01 1.146E-01 5.213E-01 6.346E-02 5.213E-01 2.745E-02 2.519E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3631 of 5809 Le (pCi/GRAM 1.507E+Ol 5. 372E-02 O.OOOE+OO 3.177E-02 4. 966E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 .PM-14 7 PM-149 EU-150 'EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 3632 of 5809 O.OOOE+OO 7.287E-02 5.566E-01 O.OOOE+OO 4.094E-02 7 .117E-01 7.757E+OO 3.910E-02 1.914E-01 2.581E+OO 2. 631E+OO O.OOOE+OO 2.087E-01 O.OOOE+OO O.OOOE+OO 7.729E-01 7. 451E+OO 9.215E-01 O.OOOE+OO l.963E-01 5.984E+02 3.364E-02 1. 081E+OO 2.760E+OO 1.897E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.915E-02 6.258E-02 6.318E+OO 5.832E-01 5.832E-01 2.557E-02 1.218E-01 2.288E-01 O.OOOE+OO O.OOOE+OO 1.290E-01 2.687E+OO 9.742E-02 2.394E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 3.860E-02 O.OOOE+OO 5.528E-02 1.489E-01 O.OOOE+OO O.OOOE+OO l.069E-01 O.OOOE+OO O.OOOE+OO 2.987E+Ol O.OOOE+OO 3 .196E-01 7.426E-02 6.498E+OO 4.492E-02 O.OOOE+OO 7.149E+02 O.OOOE+OO 2.637E-02 9.847E-02 l.397E-01 1.256E-01 9.561E-02 2.370E+OO 5.707E-02 5.381E+OO l.988E-01 8.332E-02 2.450E-02 SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT ,I DENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3633 of 5809 6.313E+OO 1,013E+OO 1.185E+OO 4.783E+Ol 1.183E+02 5.164E-01 3.272E+OO 5.667E-02 4. 211E-01 8.262E-01 4.415E-01 5. 771E-01 2.548E-01 2.548E-01 4.450E-01 5. 771E-01 5.881E-02 2.903E-01 4.331E+OO 1.737E-01 5.881E-02 O.OOOE+OO 2.204E-01 3.175E+02 5.245E-02 8.307E-02 6.448E-02 4.026E-02 4.228E-02 1.088E-01 NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:13:06.62 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235032.CNF;l * *Acquisition date 3-0CT-2016 09:10:21 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:07.00 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:48:00 Nuclide Library : SOLID *
  • Sample ID G405235032 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : l.4695E+02 GRAM *
  • Quantity Err(%) : 1.3610E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-201'6 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1. 391E+Ol 1.925E+OO l.925E+OO CD-109 9. 991E-01 1.834E+OO l.834E+00 SN-126 6.225E-02 1.142E-01 l.142E-01 BA-137M 1. 947E-01 1.073E-01 l.073E-01 CS-137 2.057E-01 1.134E-01 1.134E-01 TL-208 2.793E-01 1.093E-01 l.093E-01 PB-210 1.858E+OO l.328E+OO 1.328E+OO BI-212 1.877E+00 l.037E+00 1.037E+OO PB-212 1.185E+OO 1. 651E-01 l.651E-01 BI-214 9.578E-01 l.933E-01 1.933E-01 PB-214 8.656E-01 2.401E-01 2.401E-01 RN-222 9.578E-01 1.933E-01 1.933E-01 RA-224 2.073E+OO 1. 715E+OO 1. 715E+OO RA-226 9.578E-01 1.933E-01 1.933E-01 AC-228 1.058E+OO 3.544E-01 3.544E-01 RA-228 1.058E+OO 3.544E-01 3.544E-01 TH-228 1.185E+00 1.651E-01 1.651E-01 TH-230 9.574E-01 1.933E-01 1.933E-01 PA-231 7.028E-01 8.992E-01 8.992E-01 TH-232 1.058E+OO 3.544E-01 3.544E-01 TH-234 2.373E+OO 2.024E+OO 2.024E+OO U-234 9.574E-01 l.933E-01 l.933E-01 U-238 2.373E+00 2.024E+OO 2.024E+OO AM-243 2.434E-01 9.096E-02 9. 096E-02 ANH-511 9.366E-02 8.662E-02 8.662E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1 . 96-sigma ) BE-7 -6.462E+00 1. 861E+Ol 1.884E+Ol NOT IDENT. NA-22 -7.868E-03 7.425E-02 7.433E-02 NOT IDENT. NA-24 -l.OOOE+41 4.673E+41 O.OOOE+OO SHORT HLIF AL-26 3.435E-03 3.741E-02 3.744E-02 NOT IDENT. SC-46 1.055E-01 5.507E-01 5.527E-01 FAIL ABUN Page 3634 of 5809 V-48 -4.997E+02 3.276E+04 3.276E+04 SHORT HLIF CR-51 9.148E+Ol 6.835E+02 6.848E+02 SHORT HLIF MN-54 -l.174E-02 8.448E-02 8.464E-02 NOT IDENT. C0-56 3.179E-03 6.325E-01 6.325E-01 NOT IDENT. MN-56 -1.000E+41 3.858E+43 0.000E+OO SHORT HLIF C0-57 -7.879E-02 5.602E-02 6.633E-02 NOT IDENT. C0-58 3.985E-01 7.410E-01 7.624E-01 NOT IDENT. FE-59 6.214E+OO 1.022E+Ol l.060E+Ol NOT IDENT. C0-60 6.175E-03 4.475E-02 4.483E-02 NOT IDENT. ZN:-65 3.938E-02 2.435E-.01 2.441E-01 NOT IDENT. GE-68 -5.495E-02 3.006E+OO 3.006E+OO NOT IDENT. AS-73 -2.061E+OO 3.169E+OO 3.302E+OO NOT IDENT. AS-74 -1.214E+03 1. 278E+04 l.279E+04 SHORT HLIF SE-75 -6.568E-02 2.402E-01 2.420E-01 NOT IDENT. BR-77 1. 724E+40 1. 567E+41 0.000E+OO SHORT HLIF SR-82 8.449E+02 1.445E+03 1.494E+03 SHORT HLIF RB-83 l.496E-Ol 8.846E-01 8.872E-01 NOT IDENT. KR-85 6.786E+OO 8.501E+00 9.034E+OO NOT IDENT. SR-85 8.362E-01 1.052E+OO l.117E+OO NOT IDENT. RB-86 -7.807E+03 5.738E+04 5.748E+04 SHORT HLIF Y-88 1.282E-01 l.655E-01 1. 753E-01 NOT IDENT. Y-91 -5.732E+02 8.147E+02 8.547E+02 NOT IDENT. NB-94 -l.139E-02 4.232E-02 4.263E-02 FAIL ABUN NB-95 2.377E-01 l.270E+OO l.274E+OO NOT IDENT. NB-95M 3.200E-01 ,3. 371E+OO 3.374E+OO NOT IDENT. ZR-95 1.020E+OO 2 .112E+00 2.162E+OO NOT IDENT. NB-97 1.000E+41 1.625E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 7.286E+41 O.OOOE+OO SHORT HLIF M0-99 -6. 571E+32 l.022E+34 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 1.580E+41 O.OOOE+OO SHORT HLIF RH-101 -3. 871E-02 3.883E-02 4.257E-02 NOT IDENT. RH-102 -6.147E-03 7.564E-02 7.569E-02 NOT IDENT. RU-103 -5.187E+OO 8.266E+00 8. 591E+OO FAIL ABUN RH-106 5.840E-01 5.997E-01 6.549E-01 NOT IDENT. RU-106 5.840E-01 5.997E-01 6.549E-01 NOT IDENT. AG-108M -9.803E-03 3.102E-02 3.133E-02 NOT IDENT. AG-llOM 8.754E-03 l.377E-01 l.378E-01 NOT IDENT. SN-113 -3.520E-01 3.084E-01 3.468E-01 NOT IDENT. CD-115 -1.000E+41 l.549E+41 O.OOOE+OO SHORT HLIF SN-ll 7M -9.578E+04 2.130E+05 2.173E+05 SHORT HLIF TE-123M -4.061E-02 l.430E-01 l.442E-01 NOT IDENT. SB-124 9.029E-01 2.944E+OO 2.972E+OO NOT IDENT. SB-125 -8.656E-02 l.246E-01 1.306E-01 FAIL ABUN TE-125M -2.878E+02 3 .111E+02 3. 371E+02 NOT IDENT. I-126 -8.599E+05 3.082E+06 3.106E+06 SHORT HLIF SB-126 -1.382E+06 3.444E+06 3.499E+06 SHORT HLIF SB-127 -2.333E+23 5.316E+23 O.OOOE+OO SHORT HLIF I-131 -2.147E+09 2. 263E+10 2.265E+10 SHORT HLIF I-132 l.000E+41 5.818E+42 O.OOOE+OO SHORT HLIF TE-132 -7.447E+27 l.154E+28 O.OOOE+OO SHORT HLIF BA-133 -l.616E-02 5.183E-02 5.234E-02 NOT IDENT. I-133 -1.000E+41 3.252E+41 O.OOOE+OO SHORT HLIF CS-134 3.412E-04 6.250E-02 6.250E-02 NOT IDENT. CS-135 -5.162E-02 1. 712E-01 1. 728E-01 NOT IDENT. I-135 -1.000E+41 l.021E+42 O.OOOE+OO SHORT HLIF CS-136 -l.013E+05 8.143E+05 8.155E+05 SHORT HLIF CE-139 -l.305E-01 l.289E-01 1. 417E-01 NOT IDENT. BA-140 -1.522E+05 3.535E+06 3.536E+06 SHORT HLIF LA-140 -1. 8 06E+06 l.383E+06 l.605E+06 SHORT HLIF CE-141 -2.275E+Ol 3.374E+Ol 3.526E+Ol NOT IDENT. CE-143 1.000E+41 1.105E+41 O.OOOE+OO SHORT HLIF CE-144 -6.124E-02 3.476E-01 3.487E-01 NOT IDENT. PM-144 7.378E-02 7.877E-02 8.550E-02 NOT IDENT. PR-144 6.445E+OO 6.888E+OO 7.476E+OO NOT IDENT. PM-146 -4.878E-03 5.283E-02 5.287E-02 NOT IDENT. ND-147 -6.719E+07 l.137E+08 l.177E+08 SHORT HLIF PM-147 -4.251E+02 8.862E+02 9.067E+02 NOT IDENT. PM-149 1.000E+41 4.643E+41 O.OOOE+OO SHORT HLIF EU-150 4.225E-03 3.281E-02 3.287E-02 FAIL ABUN EU-152 4.650E-02 l .115E-01 l.135E-01 FAIL ABUN GD-153 -1.553E-01 l.942E-01 2.064E-01 NOT IDENT. EU-154 -3.456E-02 1. 781E-01 1. 788E-01 NOT IDENT. EU-155 6.434E-02 l.065E-01 l.104E-01 FAIL ABUN TB-160 4.028E-01 2. 972E+OO 2.977E+OO FAIL ABUN H0-166M 2.250E-02 6.453E-02 6.532E-02 FAIL ABUN TM-171 3.074E+OO 5.878E+OO 6.039E+OO NOT IDENT. HF-172 -3.020E-01 2.685E-01 3.0lOE-01 FAIL ABUN LU-172 5.645E-02 9.475E-02 9.810E-02 FAIL ABUN Page 3635 of 5809 LU-176 l.050E-02 2.740E-02 2.780E-02 FAIL ABUN HF-181 5.006E+OO 6.686E+OO 7.057E+OO NOT IDENT. TA-182 -4.823E-01 l.278E+OO l.296E+OO FAIL ABUN RE-183 4.347E-01 l.420E+OO l.434E+OO NOT IDENT. RE-184 3.156E+Ol 5.036E+Ol 5.233E+Ol NOT IDENT. W-188 -4.407E+Ol l.549E+02 l.562E+02 FAIL ABUN IR-192 l.918E-01 5.620E-01 5.686E-01 FAIL ABUN HG-203 l.718E+OO 3.513E+OO 3.597E+OO NOT IDENT. BI-207 9.375E-03 6.418E-02 6.432E-02 FAIL ABUN BI-211 2.384E+OO 6. 625E-Ol. l.263E+OO FAIL ABUN PB-211 6.792E-01 8.789E-01 9.307E-01 NOT IDENT. RN-219 -8.680E-02 5.176E-01 5.190E-01 NOT IDENT. RA-223 -4.522E-01 7.953E-01 8.210E-01 FAIL ABUN AC-227 2. 963E-02 2.817E-01 2.820E-01 FAIL ABUN TH-227 2. 963E-02 2.817E-01 2.820E-01 FAIL ABUN TH-229 l .113E-01 4.786E-01 4.812E-01 FAIL ABUN TH-231 -4.522E-01 7.953E-01 8.210E-01 FAIL ABUN PA-233 -l.112E-02 6.766E-02 6.785E-02 FAIL ABUN PA-234 -7.373E-02 3.558E-01 3.574E-01 NOT IDENT. PA-234M l.247E+OO 4. 672E+00 4.706E+OO NOT IDENT. U-235 -3.449E-03 l.867E-01 1. 867E-01 FAIL ABUN NP-237 -l .112E-02 6.766E-02 6.785E-02 FAIL ABUN NP-238 -l.OOOE+41 l.536E+41 O.OOOE+OO SHORT HLIF NP-239 9. ll 7E-03 2.591E-01 2.591E-01 NOT IDENT. PU-239 5.093E+02 3.328E+02 4.044E+02 NOT IDENT. AM-241 -l.444E-02 6.604E-02 6.636E-02 NOT IDENT. CM-243 -3.460E-03 9.759E-02 9.760E-02 NOT IDENT. BK-247 -5.904E-02 7.917E-02 8.352E-02 FAIL ABUN CM-247 -l.206E-02 4.768E-02 4.799E-02 NOT IDENT. CF-249 -2.708E-03 4.882E-02 4.883E-02 NOT IDENT. CF-251 -4.573E-02 l.223E-01 l.240E-01 NOT IDENT. Page 3636 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 96. 7190 87.09 129.2920 136.47 64.3860 45.60 75.0593 87:57 129.3771 140.51 0.0000 46.54 75.2030 88.03 129.4596 143.76 69.0807 49. 72 0.0000 88.34 140.5708 144.24 73.3284 51. 35 90.8022 88.47 140.5953 145.44 70.8853 51.87 83.8145 89. 96 135.3411 152.43 59.4791 52.39 78.3038 1093.63 102.1932 153.25 0.0000 52.97 91. 8274 91.11 0.0000 323.87 83.4133 53.44 105.3581 92.59 106.0352 156.02 0.0000 54.07 96. 5040 93.35 106.1418 158.56 0.0000 57.36 0.0000 94.56 82.8195 159.00 66.6940 57.53 111. 4159 94.65 84.4218 162.33 61. 7563 57.98 87.3956 94.67 84.4245 162.66 0.0000 59.27 111.7584 94.87 84.4466 163.33 49.7942 59.32 111. 7682 97.43 97.5172 165.86 81. 7508 59.54 111. 8111 98.43 90.0393 176.31 68.6243 60. 96 107.9212 98.44 90.0404 176.60 0.0000 61.17 107.9600 99.53 72 .1326 177.52 70.4366 62. 93 108.2840 100 .11 62.5609 181.07 0.0000 63.29 108.3500 102.03 92.8627 181.52 70.6822 63.58 108.4027 103.18 79.7109 184.41 55.9870 64.28 108.5297 103.37 79.7300 143.76 56.0495 66.73 116.2327 105.21 70.2251 193.51 55.5364 67.24 120.9213 105.31 70.2339 197.03 68.9594 125.81 114.8804 106.12 71.5155 198.01 53.0884 67.75 94.9785 106.47 71.5461 201.83 71. 8918 69.67 102.9543 109.28 77.8740 203.43 62.2092 70.83 110. 8396 111. 00 52.4289 205.31 64.0825 72. 81 96.1264 111.76 0.0000 210.85 49.1668 72.87 96.1353 114. 06 67.3025 215.65 52.4913 74.66 96. 3994 116. 30 0.0000 222 .11 57.7109 74.82 96. 4228 116.74 78. 5596 227.09 53.4015 74.97 96.4443 119. 76 72.6719 227.38 57.0341 77 .11 96.7552 121.12 78.9517 228.16 0.0000 78.74 105.9484 121.22 78.9604 228.18 60.6918 79.69 102.9753 121. 78 99.9974 116. 74 60.6918 80.12 74.9380 122.06 100.0289 235.69 57.3847 80.19 0.0000 122.92 55.6248 235. 96 45.5521 80.57 117.1677 123.07 54.3978 238.63 45.6406 81. 00 103.1720 265.00 76.7034 238.98 0.0000 81. 07 106.3088 125.81 96.7246 240.99 45.7179 81. 75 100.1536 127.23 94.3906 242.00 45.7509 83.79 100.4456 127.91 88.2462 244.70 30.2537 84.00 100.4753 129.30 58.5042 252.40 0.0000 85.43 94.3854 131. 2 0 88.5593 252.80 47.9444 86.55 94.5331 133.02 73.7347 254.15 0.0000 86.79 94.5642 133.52 68.3550 256.23 57.3000 86.94 108.7720 136.00 62.6831 260.90 0.0000 Page 3637of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 42.7572 355.39 0.0000 584.27 18.5356 264.80 47.4099 356.01 35.3672 595.83 0.0000 265.00 49.2756 364.49 0.0000 427.87 23.0405 268.22 59.6302 366.42 0.0000 602.52 0.0000 269.46 49.4222 372.51 36.6748 604.72 6.5933 270.03 46.6420 375.05 30.7692 607.14 16.4978 271.23 44.8125 377.52 29.8151 609.32 19. 8135 273.65 0.0000 356.01 25.9259 610.33 28.0805 276.40 54.3325 388.16 39.9748 614.28 21. 5051 277.37 61.8656 388.63 0.0000 618.01 23.1909 277.60 55.3125 391.69 43.0516 620. 36 27.6326 278.00 43.1362 264.66 32.1849 621. 93 12.1655 279.20 44.1084 401.81 43.2738 630.19 0.0000 279.54 60.0755 402.40 44.2936 631.29 21. 0851 279.70 60.0820 404.85 32.2533 633.25 21.1005 280.46 53. 5372 410.95 16.1758 634.78 0.0000 283.69 50.8250 413. 71 27.3340 635.95 17.7858 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 45.2275 423. 72 0.0000 645.85 24.5432 285.90 0.0000 427.09 30.5701 657.76 21.8470 287.50 39.6271 427.87 33.6398 657.90 0.0000 290.67 41.1246 433.94 26.5813 661. 66 25.8039 293.27 0.0000 439.40 21.5255 664.57 0.0000 351. 93 31.2873 453.88 27.8635 666.33 0.0000 295.96 31.3021 463.37 25.9125 666.50 0.0000 879.38 28.5028 468.07 20.7743 667.71 0.0000 299.98 38.5117 473.00 0.0000 677.62 21.4353 300.09 38.5142 475.06 29.1758 685.70 0.0000 300.13 38.5150 476.78 31. 2836 695. oo* 0.0000 301.36 38.5447 477.60 27.1225 696.49 18.1680 302.85 34.2935 482.18 19.8609 696. 51 18.1680 256.23 44.3402 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 27.2598 306.78 31. 5109 497.08 24.1993 697.49 27.2607 308.46 33.4548 505.52 17.4238 702.65 25.0329 311. 90 40.2295 507.63 0.0000 706.68 20.5093 316.51 29.7752 511. 00 20.1106 711. 68 13.6958 319.41 0.0000 514.00 17.4869 720.70 0.0000 320.08 0.0000 514.00 17.4869 721. 93 0.0000 321. 04 23.1138 520.40 21.2533 722.78 15.4649 323.87 47.7517 520.69 0.0000 722.91 15.4655 325.23 39.1001 522.65 0.0000 723.31 15.4677 328.76 0.0000 527.90 0.0000 724.19 10.3147 333.37 32.0104 528.26 24.5217 727. 33 19.5034 333.97 37.8431 529.59 18.1351 733.00 15.5165 334.37 37.8519 529.87 0.0000 735.93 13.8062 338.28 35. 9913 531. 02 0.0000 333.97 17.2662 338.32 35.9920 537.26 0.0000 739.50 0.0000 311.90 42.3663 546.56 0.0000 747.24 12.7017 340.48 42.3663 552.55 23.6892 748.06 11.5503 340.55 0.0000 563.25 27.0355 752.31 16.1926 344.28 31.6235 569.33 28.1847 753.82 0.0000 345.93 42.0088 946.00 27.1016 756.73 13.8989 351.06 30.3718 569.70 27.1037 756.80 13.8994 351. 93 30.3863 583.19 18.5280 884.68 16.2524 Page 3638of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 18.5853 1274.44 5.5834 1620.50 6.3794 766.42 17.4274 1001.03 7.4536 1621. 92 7.4443 766.84 11. 6199 1002.74 7.4570 1678.03 0.0000 772. 60 0.0000 1004.73 15.8545 1690.97 3.2292 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739. 50 0. 0.000 1025.87 0. OOOQ 1764.49 2.1798 778.90 20.9949 1028.54 0.0000 1063.66 5.4550 783.70 0.0000 1037.84 8.4644 1771.35 4.3647 785.37 14.9015 1038.76 0.0000 1791.20 0.0000 792.07 25.4724 631.29 10.3682 1808.65 3.2937 794.95 22.8579 1048.07 0.0000 1810.72 0.0000 795.86 19.3467 1049.04 15.0908 1836.06 0.0000 810.06 11.4817 1050.41 11. 3218 810.29 11. 4825 1063.66 15.1455 344.28 11.4833 1077.00 0.0000 810.76 10.6011 1077.34 13. 2968 815.77 0.0000 1085.87 7.6143 1048.07 0.0000 1093.63 7.6284 832.01 18.6704 1099.45 3. 8196 834.85 20.4661 1112.07 15.3242 835. 71 22.2511 1112. 84 14.3692 836.80 0.0000 1115. 54 12.2695 846.75 0.0000 1120.29 10.5562 846.77 15.1801 1120.55 9.2133 856.80 0.0000 1221.41 10.7509 860.56 12.5516 1129.67 12.5033 871.09 12.9498 1131.51 0.0000 873.19 0.0000 1147.95 0.0000 875.33 0.0000 1173.23 17.4891 879.38 14.4229 1177.95 20.4258 880.51 15.6295 1189.05 9.7510 883.24 20.7553 1204.77 17.6144 884.68 17.1532 1221.41 16.6981 889.28 15.3673 1231. 02 15.7490 894.76 16. 2966 1235.36 0.0000 898.04 12.6866 1238.28 14.7885 900.72 19.9516 1260.41 0.0000 903.28 11. 7979 1271.87 7.9453 911. 20 10.9146 1274.44 14.3095 912.08 10.9171 1274.54 14.3095 923.98 0.0000 1291. 59 6.9812 926.50 12.7875 1298.22 0.0000 92 9. 11 14.6245 1312 .11 0.0000 937.49 17.4066 1332.49 7.0419 944.13 0.0000 1362.66 0.0000 946.00 16.5284 1365.19 6.0765 949.00 11.9471 1368.63 0.0000 667.71 0.0000 1384.29 6.1000 962.31 20.9048 1408.01 3.0646 964.08 16.2400 1457.56 0.0000 966 .17 25 .1124 1460.82 6.1930 911.20 23.0980 1489.16 4 .1511 968. 97 23.0980 1505.03 5.2048 983.53 0.0000 1584.12 8.4502 984.45 0.0000 1596.21 0.0000 Page 3639 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:15:51.19 ********************************************************************************
  • GEL Laboratories LLc" *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM25.CNF;357 Background date : Z-OCT-2016 11:01:25. Sample date 23-NOV-2015 11:53:00 Acquisition date : 3-0CT-2016 09:15:18. Sample ID G405235033 Sample quantity 1.66788E+02 GRAM Detector name : GAM25 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.54 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 2 2 0 0 0 0 0 0 0 0 0 4 4 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3640 of 5809 Energy 46.58* 57.57* 63.27* 74.83* 77.19* 84.07* 88.48 92.91* 128.95 177.16 178.79 185.90* 191.54 210.34 238.76* 241.75 270.37 293.03 295.35* 300.61 338.48* 352.02* 422. 96 463.13 511. 36* 527.08 563.56 583.36* 609.42* 662.06 683.77 704.20 770.18 796.52 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 56 18 32 229 344 63 219 143 19 13 20 100 14 60 408 102 50 25 131 22 59 252 11 26 61 16 16 91 166 19 7 20 6 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 183 141 267 166 126 140 216 169 124 46 75 127 52 76 61 89 62 38 45 68 54 50 25 16 38 15 13 42 36 17 24 32 39 24 0.97 0.98 0.75 0.95 0.87 2.09 3.77 1. 22 0. 96 1. 25 1.10 1. 58 0.90 0.98 1.11 1. 65 2.58 1. 49 1.15 0.99 1.23 1.18 0.63 1. 45 2.79 1. 41 1. 89 0.99 1. 27 2.14 3.26 4.88 0.59 1.17 92. 67 114.63 126.04 149.16 153.88 167. 62 176.45 185.31 257.38 353.79 357.04 371.27 382.54 420.14 476.99 482. 96 540.20 585.52 590.16 600.67 676.42 703.49 845.40 925.75 1022.21 1053.66 1126. 63 1166. 25 1218.37 1323.68 1367.12 1408.00 1539.99 1592.69 89 113 122 143 143 164 171 182 253 351 356 365 379 416 470 470 535 582 582 597 672 698 841 922 1014 1049 1122 1160 1212 1320 1359 1400 1530 1587 9 1.55E-02 47.3 6 5.03E-03107.1 9 8.96E-03 96.2 15 6. 37E-02 11.1 15 9.54E-02 7.5 7 1.76E-02 34.2 11 6.07E-02 14.7 9 3. 96E-02 19. 6 8 5.23E-03105.5 5 3.49E-03 84.9 7 5.64E-03 72.6 11 2.78E-02 24.8 6 3.84E-03 87.0 10 1.66E-02 30.4 19 1.13E-01 6. 0 19 2.83E-02 22.7 9 1. 39E-02 31. 9 16 6.85E-03 50.3 16 3.63E-02 12.6 10 6.llE-03 73.1 10 l.65E-02 27.0 11 6.99E-02 8.4 6 2.98E-03 80.3 8 7.29E-03 33.6 17 l.69E-02 30.6 10 4.44E-03 51.7 10 4.46E-03 48.3 12 2.52E-02 18.0 13 4.61E-02 10.9 8 5.39E-03 43.7 10 2.03E-03132.6 16 5.56E-03 67.1 14 1.77E-03210.2 9 2 .13E-03122 .1 Fit 5.16E-01 1.33E+OO 5.34E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 805.08 15 10 4.41 1609.82 1602 14 4.lOE-03 53.2 36 0 814.59 9 11 0.60 1628.84 1624 8 2.40E-03 76.7 37 0 860.60 26 18, 2.74 1720.91 1715 12 7. llE-03 38.6 38 0 911. 28* 95 6 1. 76 1822.33 1816 15 2.63E-02 12.3 39 0 969. 67* 34 24 1. 56 1939.15 1933 13 9.51E-03 35.9 40 0 981.44 9 4 1. 46 1962.71 1958 9 2.59E-03 51. 7 41 0 1105. 03 31 19 6.14 2210.03 2195 25 8.62E-03 41. 6 42 0 1121.65* 27 57 0.97 2243.29 2234 20 7.59E-03 69.6 43 0 1239. 96 7 30 0.67 2480.08 2471 12 2.05E-03152.7 44 0 1260.11 15 6 1. 61 2520.40 2513 13 4.14E-03 43.5 45 0 1265.43 16 0 1. 39 2531.06 2526 10 4.44E-03 25.0 46 0 1376.80 21 2 2.39 2753.97 2749 11 5.74E-03 26.8 47 0 1389.44 7 2 1. 56 2779.27 2775 8 1.91E-03 52.3 48 0 1460.79* 342 0 2.43 2922.11 2915 16 9.50E-02 5.5 49 0 1764.68* 30 0 2.15 3530.50 3524 13 8.28E-03 19.2 Flag: "*" = Peak area was modified by background subtraction Page 3641of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:15:53 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 23-NOV-2015 11:53:00 G405235033 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-GCT-2016 09:15:18 166.79 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA25 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3642 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 CD-109 TH-229 U-235 AM-243 TH-228 PB-212 BI-211 Line 240.99 87.57 88.03 88.47 89. 96' 74.66 74.82 74.82 351.06 CAN 0 01:00:00.54 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.131E+OO 1.245E+Ol 1.245E+01 10.91 OK CD-109 88.03 3.70* 9.261E+OO 3.116E+OO 5.000E+OO 37.19 OK SN-126 64.28 9.60 9.543E+OO 2.217E-01 2.217E-01 192.38 OK 86.94 8.90 9.280E+OO Line Not Found Absent 87.57 37.00* 9.261E+OO 3 .116E-01 3 .116E-01 37.19 OK BA-137M 661.66 89.90* 2.256E+OO 4.661E-02 4.754E-02 87.40 OK CS-137 661.66 85.10* 2.256E+OO 4.924E-02 5.023E-02 87.40 OK TL-208 277.37 6.60 4;809E+OO Line Not Found Absent 583.19 85.00* 2.510E+OO 2.099E-01 2.099E-01 36.00 OK 860.56 12.50 1.810E+OO 5.330E-01 5.330E-01 77.30 OK PB-210 46.54 4.25* 9.147E+OO 9.292E-01 9.546E-01 94.62 OK BI-211 72.87 1.23 9.424E+OO Line Not Found Absent 351.06 12.92* 3.893E+OO 3.254E-01 3.254E-01 224.40 OK PB-212 74.82 10.28 9.405E+OO 9.975E-01 9.975E-01 34.80 OK 77 .11 17.10 9.382E+OO 1.322E+OO 1.322E+OO 14.98 OK 238.63 43.60* 5.476E+OO 9.371E-01 9.371E-01 11. 95 OK 300.09 3.30 4.479E+OO 7. 962E-01 7.962E-01 146.20 OK BI-214 609.32 45.49* 2.419E+OO 7. 421E-01 7.424E-01 21.77 OK 1120.29 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 OK 1764.49 15.30 . 9.335E-01 8.916E-01 8.919E-01 38.47 OK PB-214 74.82 5.80 9.405E+OO Line Not Found <<INT Reject 77 .11 9.70 9.382E+OO 2. 331E+OO 2.332E+OO 14.98 OK 87.09 3.41 9.279E+OO Line Not Found <<INT Reject 242.00 7.25 5.413E+OO Line Not Found <<INT Reject 295.22 18.42 4.550E+OO 8.355E-01 8.358E-01 25.28 OK 351. 93 35.60* 3.894E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.419E+OO 7. 421E-01 7.424E-01 21.77 OK 1120.29 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 OK 1764.49 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 OK RA-224 240.99 4.10* 5.418E+OO 1.039E+OO 1.039E+OO 115.47 OK RA-226 609.32 45.49* 2.419E+OO 7.421E-01 7.424E-01 21. 77 OK 1120.29 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 OK 1764.49 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 OK AC-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.031E+OO 6.879E-01 6.879E-01 54.05 OK 794.95 4.25 1.935E+OO Line Not Found Absent 835.71 1. 61 1.856E+OO Line Not Found Absent 911.20 25.80* 1. 725E+OO 9.939E-01 9.939E-01 24.61 OK 968.97 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 OK RA-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11.27 4. 031E+OO 6.879E-01 6.879E-01 54.05 OK 794.95 4.25 1. 935E+OO Line Not Found Absent 835.71 1. 61 1.856E+OO Line Not Found Absent 911.20 25.80* 1. 725E+OO 9.939E-01 9.939E-01 24.61 OK 968. 97 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 OK TH-228 74.82 10.28 9.405E+OO 9.975E-01 9.975E-01 34.80 OK 77 .11 17.10 9.382E+OO 1.322E+OO 1.322E+OO 14.98 OK 238.63 43.60* 5.476E+OO 9. 371E-01 9. 371E-01 11. 95 OK 3Q0.09 3.30 4.479E+OO 7. 962E-01 7. 962E-01 146.20 OK Page 3643 of 5809 Nuclide Line Activity Report (continued) Page : 3 ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-229 85.43

  • 14.70 9. 313E+OO 2.827E-01 2.828E-01 468.42 OK 88.47 24.00 9.261E+OO 4.803E-01 4.804E-01 37.19 OK 193.51 4.41* 6.496E+OO Line Not Found Absent 210.85 2.80 6.083E+OO 1.951E+OO 1.951E+OO 60.83 OK TH-230 609.32 45.49* 2.419E+OO 7.421E-01 7. 421E-01 21.77 OK 1120.29 14.92 l.442E+OO 5.778E-01 5.778E-01 139.21 OK 1764.49 15.30 9.335E-01 8.916E-01 8.916E-01 38.47 OK* PA-231 283.69 1. 70 4.715E+OO Line Not Found Absent 301.36 5.35* 4.479E+OO 4. 911E-01 4. 911E-01 146.20 OK TH-232 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.031E+OO 6.879E-01 6.879E-01 54.05 OK 835. 71 1. 61 1.856E+OO Line Not Found Absent 911. 20 25.80* 1.725E+OO 9.939E-01 9.939E-01 24.61 OK 968. 97 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 OK TH-234 63.29 3.70* 9.543E+OO 5.752E-01 5.752E-01 192.38 OK 92.59 4.23 9.200E+OO 2.221E+OO 2.221E+OO 39.28 OK U-234 609.32 45.49* 2.419E+OO 7.421E-01 7.421E-01 21.77 OK 1120.29 14.92 1.442E+OO 5.778E-01 5.778E-01 139.21 OK 1764.49 15.30 9. 335E-01' 8.916E-01 8.916E-01 38.47 OK U-235 89. 96 3.47 9.261E+OO 3.322E+OO 3.322E+OO 37.19 OK 93.35 5.60 9.200E+OO 1.677E+OO l.677E+OO 39.28 OK 143.76 10.96* 7.922E+OO Line Not Found Absent 163.33 5.08 7.333E+OO Line Not Found Absent 185. 72 57.20 6. 696E+00 1.475E-01 1.475E-01 49.63 OK 205.31 5.01 6.202E+OO Line Not Found Absent U-238 63.29 3.70* 9.543E+OO 5.752E-01 5.752E-01 192.38 OK 92.59 4.23 9.200E+OO 2. 221E+OO 2.221E+OO 39.28 OK AM-243 43.53 5.90 8.344E+00 Line Not Found Absent 74.66 67.20* 9.405E+OO l.526E-01 1.526E-01 34.80 OK ANH-511 511. 00 100.00* 2.808E+OO 1. 086E-01 l.086E-01 61.15 OK Flag: "*" = Keyline Page 3644 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:15:54.03 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* ** * *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l * *Acquisition date 3-0CT-2016 09:15:18 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: O 01:00:00.54 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:53:00 Analyst initials: MXRl *
  • Sample ID G405235033 Sample Quantity 1.6679E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.245E+Ol 1.331E+OO CD-109 5.000E+OO 1.823E+OO SN-126 3 .116E-01 1.136E-01 BA-137M 4.754E-02 4.072E-02 CS-137 5.023E-02 4.302E-02 TL-208 2.099E-01 7.404E-02 PB-210 9.546E-01 8.852E-01 BI-211 3.254E-01 7.156E-01 PB-212 9.371E-01 1. 097E-01' BI-214 7.424E-01 1.584E-01 PB-214 9.540E-01 1. 570E-01 RN-222 7.424E-01 l.584E-01 RA-224 1.039E+OO 1.176E+OO RA-226 7.424E-01 1.584E-01 AC-228 9.939E-01 2.397E-01 RA-228 9.939E-01 2.397E-01 TH-228 9. 371E-01 1.097E-01 TH-229 -l.356E-01 3.616E-01 TH-230 7. 421E-01 1.583E-01 PA-231 4.911E-01 7.036E-01 TH-232 9.939E-01 2.397E-01 TH-234 5.752E-01 1.084E+OO U-234 7. 421E-01 1.583E-01 U-235 -6.673E-02 1.223E-01 U-238 5.752E-01 1.084E+OO AM-243 1.526E-01 5.205E-02 ANH-511 1. 08 6E-01 6.509E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3645 of 5809 Key-Line Activity (pCi/GRAM 5.797E+00 7.739E-03 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) l.150E+Ol 4.402E-02 1. 960E+41 MDA (pCi/GRAM 5. lllE-01 9.225E-01 5. 741E-02 6.128E-02 6.473E-02 5.157E-02 5.458E-01 2.390E-01 7.373E-02 1.029E-01 2.740E-01 1. 029E-01 7.916E-01 1.029E-01 1. 898E-01 1. 898E-01 7.373E-02 6.115E-01 l.029E-01 5.767E-01 1.898E-01 7.002E-01 1. 029E-01 2.284E-01 7.002E-01 3.806E-02 3.849E-02 MDA (pCi/GRAM 2.428E+Ol 8.863E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -4.657E-03 2. 551E-02 5.368E-02 NOT IDENT. SC-46 -7.630E-02 3.097E-01 6.142E-01 FAIL ABUN V-48 O.OOOE+OO 2.247E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.591E+02 O.OOOE+OO SHORT HLIF MN-54 2.332E-02 6.353E-02 l.317E-01 NOT IDENT. C0-56 -l.888E-02 4.738E-01 9.496E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1. 701E-02 2.807E-02 5.350E-02 NOT IDENT. C0-58 1. 488E-01 5.994E-01 l.018E+OO NOT IDENT. ,&'E-59 -1. 548E+OO 6.509E+OO .. 1.292E+Ol NOT IDENT. C0-60 -2.902E-02 3.783E-02 6.229E-02 NOT IDENT. ZN-65 6.868E-02 l.823E-01 3.398E-01 NOT IDENT. GE-68 -2.094E-01 2.278E+OO 4.427E+OO NOT IDENT. AS-73 -5.035E-02 1.581E+OO 3.319E+OO NOT IDENT. AS-74 O.OOOE+OO 9.573E+03 O.OOOE+OO SHORT HLIF SE-75 1. 970E-02 l.682E-01 3.197E-01 NOT IDENT. BR-77 0.000E+OO 1. 596E+39 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8. 813E+02 O.OOOE+OO SHORT HLIF RB-83 -3.363E-01 5. lllE-01 9.174E-01 NOT IDENT. KR-85 5.943E+OO 5.607E+OO 1.228E+Ol NOT IDENT. SR-85 7. 311E-01 6.935E-01 1.518E+OO NOT IDENT. RB-86 O.OOOE+OO 4.543E+04 O.OOOE+OO SHORT HLIF Y-88 -8.004E-02 2. 411E-01 4.697E-01 NOT IDENT. Y-91 -4.258E+02 6.690E+02 1.157E+03 NOT IDENT. NB-94 2.705E-02 2.873E-02 6.112E-02 NOT IDENT. NB-95 5.409E-01 7.547E-01 1.530E+OO NOT IDENT. NB-95M 5.313E-01 2.103E+OO 3.768E+OO NOT IDENT. ZR-9$ -1.002E-01 l.520E+OO 2.857E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 5. T57E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 7.546E-04 2 .171E-02 4.029E-02 NOT IDENT. RH-102 2.362E-02 5.353E-02 l.090E-01 NOT IDENT. RU-103 -2.313E+OO 5.470E+OO 9.940E+OO FAIL ABUN RH-106 5.091E-02 4.445E-01 8. 725E-01 NOT IDENT. RU-106 5.091E-02 4.445E-01 8.725E-01 NOT IDENT. AG-108M l.429E-02 2.158E-02 4.623E-02 NOT IDENT. AG-llOM -5.220E-02 8.605E-02 1.581E-01 NOT IDENT. SN-113 -1.333E-01 1.932E-01 3.581E-01 NOT IDENT. CD-115 O.OOOE+OO l.014E+41 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.365E+05 O.OOOE+OO SHORT HLIF TE-123M 2.838E-02 9.220E-02 1.852E-01 NOT IDENT. SB-124 1.014E+OO 2.487E+OO 5.684E+OO NOT IDENT. SB-125 -3.301E-03 8.494E-02 1. 681E-01 FAIL ABUN TE-125M -1.522E+Ol 1. 787E+02 3.591E+02 NOT IDENT. I-126 O.OOOE+OO 2.039E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.894E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.779E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.408E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 7.686E+27 0.000E+OO SHORT HLIF BA-133 1.032E-02 3.173E-02 6.073E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 2.949E-02 7.056E-02 1. 044E-01 FAIL ABUN CS-135 4.657E-02 l.153E-01 2.086E-01 NOT IDENT. I-135 O.OOOE+OO 8.535E+40 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 6.666E+05 O.OOOE+OO SHORT HLIF CE-139 -5.265E-02 8.435E-02 l.548E-01 NOT IDENT. BA-140 O.OOOE+OO 2.373E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 9.283E+05 O.OOOE+OO SHORT HLIF CE-141 -8 .118E+OO 2.186E+Ol 4.142E+Ol NOT IDENT. CE-143 O.OOOE+OO 9.855E+40 0.000E+OO SHORT HLIF CE-144 -l.102E-01 2.362E-01 4.502E-01 NOT IDENT. PM-144 3.034E-02 4.212E-02 9.126E-02 NOT IDENT. PR-144 2.670E+OO 3.690E+OO 7.997E+OO NOT IDENT. PM-146 3.413E-04 2.975E-02 6.018E-02 NOT IDENT. ND-147 O.OOOE+OO 6. 7 60E+07 O.OOOE+OO SHORT HLIF PM-147 1. 649E+02 4.869E+02 l.002E+03 NOT IDENT. PM-149 O.OOOE+OO 1.569E+41 0.000E+OO SHORT HLIF EU-150 3.398E-02 l.919E-02 4.289E-02 FAIL ABUN EU-152 1. 815E-03 6.684E-02 l.362E-01 NOT IDENT. GD-153 -3.060E-02 9. 651E-02 l.895E-01 NOT IDENT. EU-154 2.098E-02 1. 075E-01 2.170E-01 NOT IDENT. EU-155 2.049E-02 6. 031E-02 l.249E-01 NOT IDENT. TB-160 1.399E+OO 1. 713E+OO 3.908E+OO FAIL ABUN H0-166M -2.306E-02 4.847E-02 8.553E-02 FAIL ABUN TM-171 2.265E+OO 2. 968E+00 6.558E+OO NOT IDENT. Page 3646 of 5809 HF-172 1.815E-02 1.438E-01 2.703E-01 FAIL ABUN LU-172 5.152E-02 6.525E-02 1.442E-01 FAIL ABUN LU-176 -5.952E-03 2.034E-02 3.604E-02 FAIL ABUN HF-181 -5.165E-01 4.276E+OO 8.363E+OO FAIL ABUN TA-182 1. 570E-01 8.981E-01 1.797E+OO FAIL ABUN RE-183 7.872E-01 1.652E+OO 1. 672E+OO FAIL ABUN RE-184 -5.474E+OO 3.609E+Ol 7.085E+Ol NOT IDENT. W-188 -7.519E+OO 1.050E+02 1. 775E+02 FAIL ABUN IR-192 -9.633E-02 4.069E-01 8.085E-01 FAIL ABUN HG-203 -1.666E+OO 2.574E+OO 4.423E+OO NOT BI-207 -7.231E-03 4.892E-02 9.341E-02 FAIL ABUN PB-211 -6.909E-02 4.916E-01 9. 714E-01 NOT IDENT. BI-212 5.654E-01 5.254E-01 1.093E+OO NOT IDENT. RN-219 2.788E-02 2. 881E-01 5.832E-01 FAIL ABUN RA-223 -l.224E-01 4.698E-01 9.264E-01 FAIL ABUN AC-227 -2.602E-02 1. 727E-01 3.182E-01 FAIL ABUN TH-227 -2.602E-02 l.727E-01 3.182E-01 FAIL ABUN TH-231 -1.224E-01 4.698E-01 9.264E-01 FAIL ABUN PA-233 -2.878E-02 4.547E-02 8.707E-02 FAIL ABUN PA-234 1.176E-01 2.449E-01 5.230E-01 NOT IDENT. PA-234M -1.218E+OO 3.796E+OO 7.333E+OO NOT IDENT. NP-237 -2.878E-02 4.547E-02 8.707E-02 FAIL ABUN NP-238 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -6. 581E-02 1.366E-01 2.642E-01 NOT IDENT. PU-239 2.092E+02 4.327E+02 4.054E+02 FAIL ABUN AM-241 -2.037E-02 3.827E-02 6.426E-02 NOT IDENT. CM-243 1.669E-02 5.052E-02 l.054E-01 NOT IDENT. BK-247 9.306E-03 5.382E-02 1. 029E-01 FAIL ABUN CM-247 l.127E-02 2.593E-02 5.447E-02 NOT IDENT. CF-249 -2.139E-02 2.847E-02 5.241E-02 NOT IDENT. CF-251 5.937E-02 9.882E-02 1.334E-01 FAIL ABUN Page 3647 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:15:51.91 Nuclide Line Activity Report Nuclide .Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 333 10.66* 1.131E+OO 1.245E+Ol 1.245E+Ol 10.91 CD-109 88.03 296 3.70* 9.261E+OO 3.886E+OO 6.236E+OO 29.40 SN-126 64.28 45 9.60 9.543E+OO 2.217E-01 2.217E-01 192.38 86.94 ------8.90 9.280E+OO ------Line Not Found ------87.57 296 37.00* 9.261E+OO 3.886E-01 3.886E-01 29.40 BA-137M 661.66 21 89.90* 2.256E+OO 4. 661E-02 4.754E-02 87.40 CS-137 661.66 21 85.10* 2.256E+OO 4.924E-02 5.023E-02 87.40 TL-208 277.37 ------6.60 4.809E+OO ------Line Not Found ------583.19 99 85.00* 2.510E+OO 2.099E-01 2.099E-01 36.00 860.56 27 12.50 1.810E+OO 5.330E-01 5.330E-01 77.30 PB-210 46.54 80 4.25* 9.147E+OO 9.292E-01 9.546E-01 94.62 BI-211 72. 87 ------1. 23 9.424E+OO ------Line Not Found ------351.06 294 12.92* 3.893E+00 2.628E+OO 2.628E+OO 16.79 PB-212 74.82 316 10.28 9.405E+OO l.469E+OO 1. 469E+OO 22.20 77 .11 471 17.10 9.382E+OO 1.322E+OO l.322E+00 14.98 238.63 497 43.60* 5.476E+oo* 9.371E-01 9. 371E-01 11. 95 300.09 26 3.30 4.479E+00 7. 962E-01 7.962E-01 146.20 BI-214 609.32 181 45.49* 2.419E+OO 7.421E-01 7.424E-01 21.77 1120.29 28 14.92 l.442E+OO 5.778E-01 5.780E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 PB-214 74.82 316 5.80 9.405E+00 2.604E+OO 2.605E+00 22.20 77 .11 471 9.70 9.382E+OO 2.331E+OO 2.332E+OO 14.98 87.09 296 3.41 9.261E+OO 4.216E+OO 4.218E+OO 29.40 242.00 124 7.25 5.418E+OO 1.423E+OO 1.424E+00 45.30 295.22 156 18.42 4.550E+OO 8.355E-01 8.358E-01 25.28 351. 93 294 35.60* 3.893E+00 9.536E-01 9.540E-01 16.79 RN-222 609.32 181 45.49* 2.419E+OO 7. 421E-01 7.424E-01 21. 77 1120.29 28 14.92 l.442E+OO 5.778E-01 S.780E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 RA-224 240.99 124 4.10* 5.418E+OO 2.516E+OO 2.516E+OO 45.30 RA-226 609.32 181 45.49* 2.419E+OO 7. 421E-01 7.424E-01 21. 77 1120. 29 28 14.92 1.442E+OO 5.778E-01 5.780E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.919E-01 38.47 AC-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 69 11. 27 4. 031E+OO 6.879E-01 6.879E-01 54.05 794.95 ------4.25 1.935E+OO ------Line Not Found ------835.71 ------1. 61 l.856E+OO ------Line Not Found ------911.20 98 25.80* 1. 725E+OO 9.939E-01 9.939E-01 24.61 968. 97 35 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 RA-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 69 11. 27 4.031E+OO 6.879E-01 6.879E-01 54.05 794.95 ------4.25 l.935E+OO ------Line Not Found ------835.71 ------1. 61 1.856E+OO ------Line Not Found ------911.20 98 25.80* 1. 725E+OO 9.939E-01 9.939E-01 24.61 968.97 35 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 TH-228 74.82 316 10.28 9.405E+OO 1.469E+OO 1.469E+OO 22.20 77 .11 471 17.10 9.382E+OO l.322E+00 1.322E+OO 14.98 Page 3648 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 497 43.60* 5.476E+OO 9. 37J.E-01 9.371E-01 11. 95 300.09 26 3.30 4.479E+OO 7. 962E-01 7. 962E-01 146.20 TH-229 85.43 86 14.70 9.313E+OO 2.827E-01 2.828E-01 68.42 88.47 296 24.00 9.261E+OO 5.990E-01 5.991E-01 29.40 193.51 ------4.41* 6. 496E+OO ------Line Not Found ------210.85 74 2.80 6.083E+OO 1. 951E+OO 1.951E+OO 60.83 TH-230 609.32 181 45.49* 2.419E+OO 7. 421E-01 7.421E-01 21.77 1120.29 28 14.92 1.442E+OO 5.778E-01 5.778E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.916E-01 38.47 PA-231 283.69 ------1. 70 4. 715E+OO ------Line Not Found ------301.36 26 5.35* 4.479E+OO 4. 911E-01 4. 911E-01 146.20 TH-232 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 69 11. 27 4.031E+OO 6.879E-01 6.879E-01 54.05 835. 71 ------1. 61 1. 856E+OO ------Line Not Found ------911. 20 98 25.80* 1. 725E+OO 9.939E-01 9.939E-01 24.61 968.97 35 15.80 1.636E+OO 6.143E-01 6.143E-01 71. 84 TH-234 63.29 45 3.70* 9.543E+OO 5.752E-01 5.752E-01 192.38 92.59 192 4.23 9.200E+OO 2.221E+OO 2.221E+OO 39.28 U-234 609.32 181 45.49* 2.419E+OO 7.421E-01 7.421E-01 21.77 1120. 29 28 14.92 l.442E+OO 5.778E-01 5.778E-01 139.21 1764.49 28 15.30 9.335E-01 8.916E-01 8.916E-01 38.47 U-235 89. 96 296 3.47 9.261E+OO 4.143E+00 4.143E+OO 29.40 93.35 192 5.60 9.200E+OO 1. 677E+OO 1.677E+OO 39.28 143.76 ------10.96* . 7. 922E+OO ------Line Not Found ------163.33 ------5.08 7.333E+OO ------Line Not Found ------185.72 125 57.20 6.696E+OO 1.475E-01 1.475E-01 49.63 205.31 ------5.01 6.202E+OO ------Line Not Found ------U-238 63.29 45 3.70* 9.543E+OO 5.752E-01 5.752E-01 192.38 92.59 192 4.23 9.200E+OO 2. 221E+OO 2.221E+OO 39.28 AM-243 43.53 ------5.90 8.344E+OO ------Line Not Found ------74.66 316 67.20* 9.405E+OO 2.247E-01 2.247E-01 22.20 ANH-511 511. 00 68 100.00* 2.808E+OO 1.086E-01 l.086E-01 61.15 Flag: "*" Keyline Page 3649 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235033 Acquisition date 3-0CT-2016 09:15:18 Total number of lines in spectrum 49 Number of unidentified lines 12 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1.41E+l0Y 22.20Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600.00Y l.41E+l0Y 1.41E+10Y l.41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 60 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.245E+Ol 3.886E+OO 3.886E-01 4.661E-02 4.924E-02 2.099E-01 9.292E-01 2.628E+OO 9.371E-01 7. 421E-01 9.536E-01 7. 421E-01 2.516E+OO 7.421E-01 9.939E-01 9.939E-01 9.371E-01 5.990E-01 7. 421E-01 4.911E-01 9.939E-01 5.752E-01 7.421E-01 1.475E-01 5.752E-01 2.247E-01 1. 086E-01 3.534E+Ol 3.534E+Ol Decay Corr pCi/GRAM 1.245E+Ol 6.236E+OO 3.886E-01 4.754E-02 5.023E-02 2.099E-01 9.546E-01 2.628E+OO 9. 371E-01 7.424E-01 9.540E-01 7.424E-01 2.516E+OO 7.424E-01 9.939E-01 9.939E-01 9. 371E-01 5.991E-01 7.421E-01 4. 911E-01 9.939E-01 5.752E-01 7.421E-01 1.475E-01 5.752E-01 2.247E-01 1. 086E-01 3.772E+Ol 3. 772E+Ol 75.51% Decay Corr 2-Sigma Error 0.136E+Ol 1.833E+OO 1.142E-01 4.155E-02 4.390E-02 0.756E-01 9.033E-01 0.441E+OO 1.120E-01 1.616E-01 1.602E-01 1.616E-01 1.140E+00 1.616E-01 2.446E-01 2.446E-01 1.120E-01 l.761E-01 1.616E-01 7.180E-01 2.446E-01 11. 06E-01 l.616E-01 0.732E-01 11. 06E-01 0.499E-01 0.664E-01 "M" Manually accepted 2-Sigma %Error 10.91 29.40 29.40 87.40 87.40 36.00 94.62 16.79 11. 95 21.77 16.79 21. 77 45.30 21.77 24.61 24.61 11. 95 29.40 21. 77 146.20 24.61 192.38 21.77 49.63 192.38 22.20 61.15 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3650 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235033 Acquisition date : 3-0CT-2016 09:15:18 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 57.57 26 199 0.98 114. 63 113 6 5.03E-03 **** 9.63E+OO T 0 128.95 25 162 0. 96 257.38 253 8 5.23E-03 **** 8.36E+OO T 0 177.16 16 58 1. 25 353.79 351 5 3.49E-03 **** 6.93E+OO T 0 178.79 26 94 1.10 .357. 04 356 7 5.64E-03 **** 6.89E+OO 0 191.54 17 65 0.90 382.54 379 6 3.84E-03 **** 6.55E+OO 0 270.37 60 75 2.58 540.20 535 9 l.39E-02 63.9 4.92E+OO T 2 293.03 29 45 1. 49 585.52 582 16 6.85E-03 **** 4.58E+OO T 0 422.96 12 29 0.63 845.40 841 6 2.98E-03 **** 3. 31E+OO T 0 463 .13 30 18 1. 45 925.75 922 8 7.29E-03 67.3 3.06E+OO T 0 527.08 18 17 1. 41 1053.66 1049 10 4.44E-03 **** 2.74E+OO T 0 563.56 18 14 1. 89 1126. 63 1122 10 4.46E-03 96. 6 2.58E+OO T 0 683.77 8 26 3.26 1367.12 1359 10 2.03E-03 **** 2.20E+OO 0 704.20 21 34 4.88 1408.00 1400 16 5.56E-03 **** 2.14E+OO 0 770.18 7 41 0.59 1539.99 1530 14 1.77E-03 **** 1. 99E+OO 0 796.52 8 26 1.17 1592.69 1587 9 2 .13E-03 **** 1.93E+00 T 0 805.08 16 11 4.41 1609.82 1602 14 4.lOE-03 **** 1. 91E+00 0 814.59 9 12 0.60 1628.84 1624 8 2.40E-03 **** 1. 90E+OO T 0 981.44 10 4 1. 46 1962.71 1958 9 2.59E-03 **** 1.62E+OO 0 1105. 03 31 19 6.14 2210.03 2195 25 8.62E-03 83.3 1.46E+OO 0 1239.96 7 30 0.67 2480.08 2471 12 2.05E-03 **** 1.32E+OO 0 12 60 .11 15 6 1. 61 2520.40 2513 13 4.14E-03 87.1 1. 30E+OO T 0 1265.43' 16 0 1. 39 2531.06 2526 10 4.44E-03 50.0 1.29E+OO 0 1376.80 20 2 2.39 2753.97 2749 11 5.74E-03 53.5 1.20E+OO 0 1389.44 7 2 1. 56 2779.27 2775 8 1. 91E-b3 **** 1.19E+OO Flags: "T" = Tentatively associated Page 3651of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:16:06.40 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l *
  • Acquisition date 3-0CT-2016 09:15:18 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.54 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:53:00 Nuclide Library : SOLID *
  • Sample ID G405235033 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.6679E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File . : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.044E-01 4.300E-01 2.676E-02 2.747E-02 2.902E-02 2.282E-02 2.549E-01 1.067E-01 3.415E-02 4.573E-02 l.324E-01 4.573E-02 3.667E-01 4.573E-02 8.086E-02 8.086E-02 3.415E-02 2.830E-01 4.571E-02 2.613E-01 8.086E-02 3.311E-01 4.571E-02 1. 066E-01 3. 311E-01 l.797E-02 l.698E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3652 of 5809 Le (pCi/GRAM 1.090E+Ol 3.827E-02 O.OOOE+OO 2.009E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-ll3 CD-ll5 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3653 of 5809 2.590E-01 O.OOOE+OO O.OOOE+OO 5.906E-02 4.172E-01 O.OOOE+OO 2.473E-02 4.369E-01 5.448E+OO 2.55(1E-02 l.492E-01 l.924E+OO l.556E+OO O.OOOE+OO l.463E-01 O.OOOE+OO 0.000E+OO 3.944E-01 5.584E+OO 6.903E-01 O.OOOE+OO l.815E-01 5.053E+02 2.762E-02 6. 696E-01 1. 741E+OO l.255E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO l.876E-02 4.887E-02 4.338E+OO 3.881E-01 3.881E-01 2.094E-02 6.742E-02 l.605E-01 O.OOOE+OO O.OOOE+OO 8.605E-02 2.347E+OO 7.593E-02 l.672E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.752E-02 O.OOOE+OO 4.714E-02 9.612E-02 O.OOOE+OO O.OOOE+OO 7.188E-02 O.OOOE+OO O.OOOE+OO l.928E+Ol O.OOOE+OO 2. 096E-01 4.029E-02 3.531E+OO 2.658E-02 O.OOOE+OO 4.670E+02 O.OOOE+OO l.978E-02 6.172E-02 8.850E-02 9.379E-02 5.849E-02 l.715E+OO 3. 728E-02 3.075E+OO l.256E-01 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3654 of 5809 6.290E-02 1. 64 6E-02 3.720E+OO 7.831E-01 7. 901E-01 3.093E+Ol 8.078E+Ol 3.692E-01 2.032E+OO 4.109E.-02 4.365E-01 5.014E-01 2.636E-01 4.248E-01 1.459E-01 l.459E-01 4.248E-01 3. 967E-02 2.304E-01 3.201E+OO 3. 967E-02 O.OOOE+OO 1.225E-01 1.902E+02 3.017E-02 4.913E-02 4.712E-02 2.467E-02 2.348E-02 6.124E-02 FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:16:11.91 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * ' DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235033.CNF;l *
  • Acquisition date 3-0CT-2016 09:15:18 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.54 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:53:00 Nuclide Library : SOLID *
  • Sample ID G405235033 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity 1.6679E+02 GRAM *
  • Quantity Err(%) 1.1991E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN. *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.245E+Ol 1.481E+OO CD-109 5.000E+OO 1.874E+OO SN-126 3 .116E-01 1.156E-01 BA-137M 4.754E-02 4.077E-02 CS-137 5.023E-02 4.307E-02 TL-208 2.099E-01 7.4S8E-02 PB-210 9.546E-01 8.888E-01 BI-211 3.254E-01 7.294E-01 PB-212 9.371E-01 1.204E-01 BI-214 7.424E-01 1.616E-01 PB-214 9.540E-01 1.619E-01 RN-222 7.424E-01 1.616E-01 RA-224 1.039E+00 1.181E+OO RA-226 7.424E-01 1.616E-01 AC-228 9.939E-01 2.450E-01 RA-228 9.939E-01 2.450E-01 TH-228 9.371E-01 1.204E-01 TH-229 -1.356E-01 3.616E-01 TH-230 7. 421E-01 1.615E-01 PA-231 4. 911E-01 7 .114E-01 TH-232 9.939E-01 2.450E-01 TH-234 5.752E-01 1.092E+OO U-234 7.421E-01 1.615E-01 U-235 -6.673E-02 1.224E-01 U-238 5.752E-01 1.092E+OO AM-243 1.526E-01 5.366E-02 ANH-511 1. 086E-01 6.524E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3655 of 5809 Key-Line Activity (pCi/GRAM 5.797E+OO 7.739E-03 -1.000E+41 K.L Act error ( 1 . 96-sigma ) 1.151E+Ol 4.402E-02 6.763E+41 TPU ( 1 . 96-sigma ) 1.481E+OO 1. 874E+OO 1.156E-01 4.077E-02 4.307E-02 7.458E-02 8.888E-01 7.294E-01 1. 204E-01 1.616E-01 1.619E-01 1.616E-01 1.181E+OO 1.616E-01 2.450E-01 2.450E-01 1.204E-01 3.616E-01 1.615E-01 7 .114E-01 2.450E-01 1.092E+OO 1.615E-01 1.224E-01 1.092E+OO 5.366E-02 6.524E-02 TPU ( 1. 96-sigma) 1.180E+Ol 4.416E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -4.657E-03 2. 551E-02 2.560E-02 NOT IDENT. SC-46 -7.630E-02 3.097E-01 3 .116E-01 FAIL ABUN V-48 -1.526E+03 2.247E+04 2.248E+04 SHORT HLIF CR-51 -1. 861E+02 4.592E+02 4.668E+02 SHORT HLIF MN-54 2.332E-02 6.354E-02 6.440E-02 NOT IDENT. C0-56 -1.888E-02 4.738E-01 4.739E-01 NOT IDENT. MN-56 -1.000E+41 3.414E+42 O.OOOE+OO SHORT HLIF C0-57 -1. 701E-02 2.808E-02 2. 911E-02 NOT IDENT. C0-58 l.488E-01 5.994E-01 6.032E-01 NOT IDENT. -1.548E+OO 6.510E+OO 6.. 547E+OO NOT IDENT. C0-60 -2.902E-02 3.784E-02 4.004E-02 NOT IDENT. ZN-65 6.868E-02 1.823E-01 1.849E-01 NOT IDENT. GE-68 -2.094E-01 2.278E+OO 2.280E+OO NOT IDENT. AS-73 -5.035E-02 1.581E+OO l.582E+OO NOT IDENT. AS-74 -6 .12 6E+02 9.573E+03 9.577E+03 SHORT HLIF SE-75 l.970E-02 l.682E-01 l.685E-01 NOT IDENT. BR-77 1.363E+40 l.239E+41 O.OOOE+OO SHORT HLIF SR-82 -2.913E+02 8. 814E+02 8. 911E+02 SHORT HLIF RB-83 -3.363E-01 5 .131E-01 5.351E-01 NOT IDENT. KR-85 5.943E+OO 5.612E+OO 6.219E+OO NOT IDENT. SR-85 7. 311E-01 6.941E-01 7.684E-01 NOT IDENT. RB-86 -1.944E+Ol 4.543E+04 4.543E+04 SHORT HLIF Y-88 -8.004E-02 2. 411E-01 2.438E-01 NOT IDENT. Y-91 -4.258E+02 6.692E+02 6. 961E+02 NOT IDENT. NB-94 2.705E-02 2.875E-02 3.123E-02 NOT IDENT. NB-95 5.409E-01 7. 551E-01 7.935E-01 NOT IDENT. NB-95M 5.313E-01 2.103E+OO 2. ll 7E+OO NOT IDENT. ZR-95 -1.002E-01 1.520E+OO 1.521E+OO NOT IDENT. NB-97 l.000E+41 2.735E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 6.038E+41 O.OOOE+OO SHORT HLIF M0-99 -5.458E+32 5.757E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 1. 017E+42 0.000E+OO SHORT HLIF RH-101 7.546E-04 2 .171E-02 2 .171E-02 NOT IDENT. RH-102 2.362E-02 5.357E-02 5.462E-02 NOT IDENT. RU-103 -2. 313E+OO 5.471E+OO 5.569E+OO FAIL ABUN RH-106 5. 091E-02 4.445E-01 4. 451E-01 NOT IDENT. RU-106 5.091E-02 4.445E-01 4.451E-01 NOT IDENT. AG-108M 1. 42 9E-02 2.159E-02 2.253E-02 NOT IDENT. AG-llOM -5.220E-02 8.609E-02 8.925E-02 NOT IDENT. SN-113 -l.333E-01 l.933E-01 2.024E-01 NOT IDENT. CD-115 l.OOOE+41 l.031E+41 O.OOOE+OO SHORT HLIF SN-ll 7M 6. 966E+04 l.368E+05 1.403E+05 SHORT HLIF TE-123M 2.838E-02 9. 221E-02 9.309E-02 NOT IDENT. SB-124 1.014E+OO 2.488E+OO 2.530E+OO NOT IDENT. SB-125 -3.301E-03 8.494E-02 8.496E-02 FAIL ABUN TE-125M -1.522E+Ol l.787E+02 1. 789E+02 NOT IDENT. I-126 8.265E+05 2.043E+06 2.077E+06 SHORT HLIF SB-126 3. 727E+05 1.895E+06 1.903E+06 SHORT HLIF SB-127 2.244E+22 2.797E+23 O.OOOE+OO SHORT HLIF I-131 7.160E+08 l.408E+l0 l.408E+l0 SHORT HLIF I-132 1.000E+41 4.736E+42 O.OOOE+OO SHORT HLIF TE-132 4.058E+27 7.878E+27 O.OOOE+OO SHORT HLIF BA-133 1.032E-02 3.174E-02 3.208E-02 NOT IDENT. I-133 -1.000E+41 8.397E+41 O.OOOE+OO SHORT HLIF CS-134 2.949E-02 7.057E-02 7.181E-02 FAIL ABUN CS-135 4.657E-02 1.154E-01 l.172E-01 NOT IDENT. I-135 l.000E+41 7.166E+41 O.OOOE+OO SHORT HLIF CS-136 -4.422E+05 6.684E+05 6.975E+05 SHORT HLIF CE-139 -5.265E-02 8.502E-02 8.827E-02 NOT IDENT. BA-140 -5.634E+05 2.373E+06 2.386E+06 SHORT HLIF LA-140 -2.105E+05 9.284E+05 9.332E+05 SHORT HLIF CE-141 -8.118E+OO 2.186E+Ol 2.217E+Ol NOT IDENT. CE-143 1.000E+41 9.912E+40 O.OOOE+OO SHORT HLIF CE-144 -l.102E-01 2.363E-01 2.414E-01 NOT IDENT. PM-144 3.034E-02 4.216E-02 4.432E-02 NOT IDENT. PR-144 2.67bE+OO 3.692E+00 3.883E+00 NOT IDENT. PM-146 3.413E-04 2.975E-02 2.975E-02 NOT IDENT. ND-147 -4.752E+05 6.760E+07 6.760E+07 SHORT HLIF PM-147 l.649E+02 4.870E+02 4.926E+02 NOT IDENT. PM-149 -1.000E+41 l.585E+41 0.000E+OO SHORT HLIF EU-150 3.398E-02 1.924E-02 2.460E-02 FAIL ABUN EU-152 1.815E-03 6.684E-02 6.685E-02 NOT IDENT. GD-153 -3.060E-02 9.653E-02 9.751E-02 NOT IDENT. EU-154 2.098E-02 l.075E-01 1.079E-01 NOT IDENT. EU-155 2.049E-02 6.033E-02 6.103E-02 NOT IDENT. TB-160 1.399E+OO 1. 715E+OO 1.827E+OO FAIL ABUN H0-166M -2.306E-02 4.848E-02 4.958E-02 FAIL ABUN TM-171 2.265E+OO 2.974E+OO 3.144E+OO NOT IDENT. Page 3656 of 5809 HF-172 1. 815E-02 1.438E-01 l.440E-01 FAIL ABUN LU-172 5.152E-02 6.546E-02 6.946E-02 FAIL ABUN LU-176 -5.952E-03 2.034E-02 2.052E-02 FAIL ABUN HF-181 -5.165E-01 4.276E+OO 4.282E+OO FAIL ABUN TA-182 l.570E-01 8.981E-01 9.009E-01 FAIL ABUN RE-183 7.872E-01 1.657E+OO 1.694E+OO FAIL ABUN RE-184 -5.474E+00 3. 611E+Ol 3.620E+Ol NOT IDENT. W-188 -7.519E+OO l.050E+02 1.050E+02 FAIL ABUN IR-192 -9.633E-02 4.069E-01 4.092E-01 FAIL ABUN HG-203 -1.666E+OO 2.575E+OO 2.682E+OO NOT IDENT. BI-207 -7.231E-03 4.892E-02 4.903E-02 FAIL ABUN PB-211 -6.909E-02 4.916E-01 4.926E-01 NOT IDENT. BI-212 5.654E-01 5.262E-01 5.846E-01 NOT IDENT. RN-219 2.788E-02 2.881E-01 2.884E-01 FAIL ABUN RA-223 -1.224E-01 4.699E-01 4. 731E-01 FAIL ABUN AC-227 -2.602E-02 l.728E-01 1.732E-01 FAIL ABUN TH-227 -2.602E-02 1. 728E-01 l.732E-01 FAIL ABUN TH-231 -1.224E-01 4.699E-01 4. 731E-01 FAIL ABUN PA-233 -2.878E-02 4.549E-02 4.730E-02 FAIL ABUN PA-234 1.176E-01 2.794E-01 2.844E-01 NOT IDENT. PA-234M -1.218E+OO 3.796E+00 3.835E+OO NOT IDENT. NP-237 -2.878E-02 4.549E-02 4.730E-02 FAIL ABUN NP-238 -l.OOOE+41 9.347E+41 O.OOOE+OO SHORT HLIF NP-239 -6. 581E-02 1.367E-01 l.399E-01 NOT IDENT. PU-239 2.092E+02 4.328E+02 4.430E+02 FAIL ABUN AM-241 -2.037E-02 3.830E-02 3.938E-02 NOT IDENT. CM-243 1.669E-02 5.054E-02 5. llOE-02 NOT IDENT. BK-2'47 9.306E-03 5.386E-02 5.402E-02 FAIL ABUN CM-247 l.127E-02 2.599E-02 2.649E-02 NOT IDENT. CF-249 -2.139E-02 2.852E-02 3. OllE-02 NOT IDENT. CF-251 5.937E-02 9.904E-02 1. 026E-01 FAIL ABUN Page 3657 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 53.3078 87.09 63 .1127 136.47 52.2037 45.60 66. 9659 87.57 63.2048 140.51 0.0000 46.54 67.2744 88.03 63.2928 143.76 68. 7161 49. 72 0.0000 88.34 63.3521 144.24 61.9060 51. 35 77.7822 88.47 63.3770 145.44 59.1028 51.87 68.9688 89. 96 63.6598 152.43 65.9285 52.39 56.3553 1093.63 63.7880 153.25 0.0000 52.97 55.7473 91.11 0.0000 323.87 62.1495 53.44 73.9804 92.59 63.5753 156.02 0.0000 54.07 77. 9694 93.35 63. 7152 158.56 0.0000 57.36 0.0000 94.56 63.9373 159.00 51.5953 57.53 70.6758 94.65 54.6512 162.33 70.2455 57.98 70.8071 94.67 54.6545 162.66 0.0000 59.27 89.7519 94.87 54.6856 163.33 53.0370 59.32 89.7701 97.43 70.3174 165.86 70.7056 59.54 89.8506 98.43 66.9876 176.31 62.6450 60. 9'6 90.3644 98.44 66.9894 176.60 0.0000 61.17 90.4400 99.53 56.5820 177.52 20.9256 62.93 100.4888 100 .11 55.7864 181. 07 0.0000 63.29 100.6294 102.03 65.8696 181.52 61.1037 63.58 100.7422 103.18 55.3583 184.41 58.2281 64.28 101.0137 103.37 55.3867 143.76 58.3561 66.73 80.7121 105,21 64.6342 193.51 60.1853 67.24 87.2493 105.31 64.6512 197.03 52. 9612 125.81 97.5157 106.12 61.18 92 198.01 62.7861 67.75 98.3403 106.47 63.0466 201.83 62.0767 69.67 90.9806 109.28 62.5981 203.43 56.7734 70.83 86.2386 111. 00 70 .1613 205.31 62.4142 72. 81 95.2553 111.76 0.0000 210.85 50.7968 72. 87 95.2749 114. 06 67. 0268 215.65 57.8367 74.66 95.8659 116.30 0.0000 222 .11 46.0362 74.82 95.9176 116.74 64.6957 227.09 56.5437 74.97 95. 9667 119.76 60.5120 227.38 57.6987 77 .11 96. 6630 121.12 56.0371 228.16 0.0000 78.74 79.7424 121.22 56.0504 228.18 45.3052 79.69 91.1005 121. 78 61. 7365 116.74 45.3052 80.12 83.4404 122.06 62. 7133 235.69 44.2570 80.19 0.0000 122.92 49.7089 235. 96 44.2735 80.57 85.2329 123.07 46.9116 238.63 52.8632 81. 00 71.4050 265.00 53.5549 238.98 0.0000 81. 07 71.4212 125.81 55.3921 240.99 53.0331 81. 75 73.8136 127.23 60.6226 242.00 53.1054 83.79 83.2967 127.91 59.7679 244.70 50.9811 84.00 83.3516 129.30 59.9546 252.40 0.0000 85.43 71. 2781 131.20 62.4393 252.80 50.3578 86.55 63.0089 133.02 63.3292 254.15 0.0000 86.79 63.0546 133. 52 71.0834 256.23 43.5237 86.94 63.0839 136.00 55.0483 260.90 0.0000 Page 3658 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 36.8579 355.39 0.0000 584.27 19.9107 264.80 35.6754 356.01 26.2988 595.83 0.0000 265.00 36.8740 364.49 0.0000 427.87 20.1171 2 68. 22 38.2158 366.42 0.0000 602.52 0.0000 269.46 33.4901 372.51 40.9678 604. 72 14.3300 270.03
  • 33.5140 375.05 35.7088
  • 607.14 14.3514 271.23 35.1619 377.52 38.4753 609.32 21. 2907 273.65 0.0000 356.01 33.3009 610.33 21.3037 276.40 39.8069 388.16 36.1426 614.28 17.6179 277.37 48.3069 388.63 0.0000 618.01 20.3336 277.60 48.3203 391.69 35.3517 620. 36 12.8604 278.00 42.3006 264.66 26.4978 621.93 20.3816 279.20 53.2544 401. 81 28.3542 630.19 0.0000 279.54 56.9083 402.40 24.7083 631.29 19.4180 279.70 56.9198 404.85 28.4299 633.25 24.8409 280.46 46.0620 410.95 37.8010 634.78 0.0000 283.69 48.6731 413.71 25.8769 635.95 12.9810 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 53.6492 423. 72 0.0000 645.85 11. 9686 285.90 0.0000 427.09 20.5637 657.76 18.0778 287.50 39. H33 427.87 29.9303 657.90 0.0000 290.67 35.9863 433.94 21. 6210 661. 66 25.2555 293.27 0.0000 439.40 22.6621 664.57 0.0000 351.93 34.5309 453.88 19.1064 666.33 o. oo*oo 295. 96 34.5599 463.37 24.0621 666.50 0.0000 879.38 29.7114 468.07 28.0141 667.71 0.0000 299.98 34.7180 473.00 0.0000 677.62 14.9584 300.09 34. 7223 475.06* 29.1364 685.70 0.0000 300.13 34.7240 476.78 20.4219 695.00 0.0000 301.36 31.4602 477.60 19.4617 696. 49 11.1963 302.85 38.1471 482.18 23.4351 696. 51 11.1967 256.23 43.2021 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 16.8024 306.78 42.4792 497.08 19.7469 697.49 16.8036 308.46 42.5581 505.52 20.8620 702.65 16.8512 311. 90 46.0694 507.63 0.0000 706.68 21. 9542 316.51 41. 2490 511. 00 18.9497 711. 68 21.4492 319.41 0.0000 514.00 18.9900 720.70 0.0000 320.08 0.0000 514.00 18.9907 721. 93 0.0000 321.04 42.2963 520.40 20.0806 722.78 15.8981 323.87 42.4235 520.69 0.0000 722. 91 15.8993 325.23 46.7330 522.65 0.0000 723. 31 17.0386 328.76 0.0000 527.90 0.0000 724.19 29.5473 333.37 31. 8779 528.26 16.6584 727. 33 23.9044 333.97 18.0067 529.59 15.1575 733.00 27.4014 334.37 24.4475 529.87 0.0000 735.93 16.0081 338.28 39.6183 531. 02 0.0000 333.97 14.8768 338.32 39.6192 537.26 0.0000 739.50 0.0000 311. 90 44.0222 546.56 0.0000 747.24 21. 8528 340.48 44.0222 552.55 13.3438 748.06 24.1633 340.55 0.0000 563.25 14.4728 752.31 20.7568 344.28 31.1946 569.33 29.0618 753.82 0.0000 345.93 32.9817 946.00 22.8361 756.73 18.4922 351.06 23.5541 569.70 22.8397 756.80 18.4928 351.93 23.5745 583.19 19.8976 884.68 13.9199 Page 3659 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 8.7079 1274.44 18.3361 1620.50 3. 7 621 766.42 13.9370 1001.03 16. 4371 1621. 92 4.7043 766.84 19.7482 1002.74 14.5129 1678.03 0.0000 772. 60 0.0000 1004.73 10.6512 1690.97 4.7864 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 [).0000 1025.87 0.0000 l:c.764.49 4. 8721 778.90 18.4064 1028.54 0.0000 1063.66 8.7820 783.70 0.0000 1037.84 9.8083 1771. 35 5.8562 785.37 13.1895 1038.76 0.0000 1791.20 0.0000 792.07 16.9383 631.29 18.6985 1808.65 3.9383 794.95 19.7887 1048.07 0.0000 1810.72 0.0000 795.86 15.9088 1049.04 19.7009 1836.06 5.9446 810.06 7 .1191 1050.41 12.8120 810.29 10.6798 1063.66 19.8096 344.28 10.6809 1077.00 0.0000 810.76 9.4954 1077.34 15.9287 815.77 0.0000 1085.87 13. 9821 1048.07 0.0000 1093.63 8.0122 832.01 28.7734 1099.45 9.0330 834.85 20.7083 1112. 07 14.5195 835. 71 18.9153 1112. 84 12.9094 836.80 0.0000 1115. 54 12.9219 846.75 0.0000 1120. 29 14 .1572 846.77 18.1067 1120 .'55 14.1589 856.80 0.0000 1221.41 14.1624 860.56 10.9329 1129.67 19.4813 871.09 17.3927 1131.51 0.0000 873.19 11. 9114 1147.95 0.0000 875.33 0.0000 1173.23 14.4230 879.38 9.1879 1177.95 11. 3505 880.51 10 .1118 1189.05 16. 5723 883.24 15.6465 1204.77 23.9490 884.68 17.4982 1221.41 13. 6118 889.28 11. 9967 1231.02 18.9075 894.76 12.9507 1235.36 0.0000 898.04 12.0431 1238.28 21.0583 900. 72 16.6943 1260.41 0.0000 903.28 17.6414 1271.87 11. 7083 911. 20 11.1801 1274.44 11. 7177 912.08 11.1844 1274.54 11. 7184 923.98 0.0000 1291.59 9.6394 926.50 15.9427 1298.22 0.0000 929 .11 12.2050 1312 .11 0.0000 937.49 28.2651 1332.49 14.1013 944 .13 0.0000 1362. 66 0.0000 946.00 13.2374 1365.19 7.6686 949.00 14.2003 1368.63 0.0000 667.71 0.0000 1384.29 8.8140 962. 31 19.9900 1408.01 3.3283 964.08 15.2417 1457.56 0.0000 966 .17 16.7804 1460.82 5.4064 911.20 18.1355 1489.16 10.8984 968.97 18.1355 1505.03 8.2099 983.53 0.0000 1584.12 6.5218 984.45 0.0000 1596.21 0.0000 Page 3660 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:16:40.80 ********************************************************************************
  • GEL LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : Z-OCT-2016 11:01:35. Sample date 23-NOV-2015 11:20:00 Acquisition date : 3-0CT-2016 09:15:46. Sample ID G405235034 Sample quantity 1.52487E+02 GRAM Detector name : GAM28 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.42 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** ' Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 2 2 2 2 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 3 3 0 0 Energy 60.47 63.24* 75.22* 77.22 87.28 89.87 92.97* 109.97 186.34* 238.92* 242.24 277.86 295.76 301.27 338.61 352.21* 371.44 511. 41
  • 564.49 579.28 583.86* 609.82*

662.78* 729. 51 767.85* 861.59 886.67 911. 97* 969. 38 1002.53* 1014.01 1016.81 1102.17 1121. 77* Page 3661of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT* Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 29 42 141 258 44 41 87 41 82 450 86 31 146 41 78 258 23 46 27 19 120 153 41 37 22 35 9 90 71 13 14 19 11 48 26 114 147 142 133 96 151 94 137 58 65 70 69 78 66 63 34 47 32 22 35 42 53 60 21 16 7 18 39 23 0 0 5 34 1. 08 1. 32 1. 32 1. 35 0.86 1. 33 1. 64 1. 49 1. 80 1. 55 1. 80 1.26 1.32 0.98 0.92 1. 58 1. 52 3.26 2.23 1.34 1. 60 1. 87 1. 69 3.28 0.74 2.06 1.16 1. 79 5.81 0. 71 1. 39 1. 70 1.23 2.03 121. 00 126.54 150.53 154.53 174.66 179.85 186.05 220.08 372.94 478.17 484.82 556.11 591. 93 602.97 677.70 704.91 743.40 1023.57 1129.79 1159.39 1168. 57 1220.53 1326.52 1460.08 1536.82 1724.45 1774.63 1825.28 1940.18 2006.54 2029.50 2035.10 2205.96 2245.18 120 120 143 143 172 178 183 217 368 474 474 551 587 598 674 699 739 1014 1123 1153 1163 1214 1320 1450 1530 1715 1771 1818 1925 1999 2028 2028 2200 2238 19 8.llE-03 19 1.17E-02 21 3.93E-02 21 7.18E-02 6 1.21E-02 5 1.15E-02 8 2.41E-02 8 1.13E-02 12 2.29E-02 25 l.25E-01 25 2.39E-02 10 8.54E-03 10 4.05E-02 11 1.13E-02 9 2.16E-02 12 7.17E-02 9 6.26E-03 17 1.29E-02 14 7.58E-03 9 5.15E-03 12 3.33E-02 14 4.26E-02 12 1.14E-02 26 1. 02E-02 12 6.08E-03 16 9.85E-03 8 2.52E-03 15 2.50E-02 26 1.99E-02 19 3.62E-03 11 3.88E-03 11 5. 25E-03 10 3.llE-03 18 1.33E-02 24.6 3.57E+OO 50.2 18.8 1.93E+OO 10.8 44.7 39.0 28.7 43.8 31. 7 5.7 2.65E+OO 27.6 54.6 13.6 45.2 21. 8 8. 9 52.1 43.2 47.7 51. 6, 13.7 12.4 39.8 59.3 47.9 30.2 58.4 15.1 26. 7 95.9 14.3 9.90E-01 22.4 47.7 31. 4 Peak Search Report (continued) Page : 2 Sample ID : G405235034 Acquisition date 3-0CT-2016 09:15:46 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1157 .11 8 13 1.16 2315.93 2311 9 2.34E-03 85.0 36 0 1189.83 49 0 4. 71 2381.41 2371 18 1.36E-02 14.3 37 0 1345.72 24 0 2.53 2 42 2684 17 6.67E-03 20.4 38 0 1461.78* 369 15 1. 86 2925.71 2919 14 1.03E-01 5.7 39 0 1592.90 5 5 0.48 3188.16 3186 6 l.39E-03 81. 9 40 0 1730.16 16 3 2.30 3462.88 3457 11 4.52E-03 31. 6 41 0 1765.64* 37 0 1. 95 3533.88 3526 15 1.03E-02 17.3 Flag: "*" = Peak area was modified by background subtraction Page 3662 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:16:42 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 23-NOV-2015 11:20:00 G405235034 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:15:46 152.49 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOL IP GAMMA28 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3663 of 5809 PB-214 PB-214 PB-214 PB-214 TL-208 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 277.37 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 HG-203 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 279.20 74.66 74.82 74.82 351.06 CAN 0 01:00:00.42 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235034 Acquisition date 3-0CT-2016 09:15:46 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66*; 1.237E+OO 1.332E+Ol 1.332E+Ol 11. 33 OK CD-109 88.03 3.70* 5.423E+OO 4.194E-01 6. 731E-01 296.78 OK TE-125M 109.28 0.27* 6.445E+OO 1.441E+Ol 6.460E+02 87.60 OK SN-126 64.28 9.60 2.991E+OO 9.454E-01 9.454E-01 100.42 OK 86.94 8.90 5.423E+OO l.744E-01 1.744E-01 296.78 OK 87.57 37.00* 5.423E+OO 4.194E-02 4.194E-02 296.78 OK BA-137M 661. 66 89.90* 2.303E+OO 1.028E-01 l.048E-01 79.68 OK CS-137 661. 66 85.10* 2.303E+OO l.086E-01 l.107E-01 79.68 OK HG-203 70.83 3.69 3.912E+OO Line Not Found Absent 72. 87 6.19 4.138E+OO Line Not Found Absent 279.20 81.56* 4.559E+OO 2.198E-02 2.382E+OO 234.08 OK TL-208 277.37 6.60 4.566E+OO Line Not Found <<INT Reject 583.19 85.00* 2.539E+OO 2.920E-01 2.920E-01 27.44 OK 860.56 12.50 l.886E+OO 7.583E-01 7.583E-01 60.47 OK BI-211 72. 87 1. 23 4.138E+OO Line Not Found Absent 351.06 12.92* 3.783E+OO 1.015E-01 1.015E-01 910.10 OK PB-212 74.82 10.28 4.384E+OO l.417E+OO l.417E+OO 54.14 OK 77 .11 17.10 4.583E+OO 2.090E+OO 2.090E+OO 21. 68 OK 238.63 43.60* 5.lOlE+OO 1.160E'+OO 1.160E+OO 11. 38 OK 300.09 3.30 4.282E+OO 1. 613E+OO 1. 613E+00 90.48 OK BI-214 609.32 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 OK 1120.29 14.92 1.538E+OO 1.025E+OO 1. 025E+OO 62.84 OK 1764.49 15.30 1.044E+OO 1.085E+OO l.086E+00 34.63 OK PB-214 74.82 5.80 4.343E+OO Line Not Found <<INT Reject 77 .11 9.70 4.583E+OO 3.684E+OO 3.685E+OO 21. 68 OK 87.09 3.41 5.409E+OO Line Not Found <<INT Reject 242.00 7.25 5.054E+OO Line Not Found <<INT Reject 295.22 18.42 4.344E+OO 1.022E+00 1.023E+OO 27.12 OK 351.93 35.60* 3.786E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 OK 1120. 29 14.92 1.538E+OO 1.025E+00 l.025E+00 62.84 OK 1764.49 15.30 1.044E+OO 1.085E+OO 1.086E+00 34.63 OK RA-224 240.99 4.10* 5.051E+OO 5.683E-01 5.683E-01 246.02 OK RA-226 609.32 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 OK 1120. 29 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62. 84 OK 1764.49 15.30 1.044E+OO 1.085E+OO 1.086E+OO 34.63 OK AC-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.786E-01 9.786E-01 43.53 OK 794.95 4.25 2.005E+00 Line Not Found Absent 835. 71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* 1. 806E+OO 9.674E-01 9.674E-01 30 .11 OK 968.97 15.80 1. 723E+OO 1.306E+OO l.306E+00 53.35 OK RA-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.786E-01 9.786E-01 43.53 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835.71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 9.674E-01 9.674E-01 30 .11 OK 968.97 15.80 1. 723E+OO 1.306E+OO 1.306E+OO 53.35 OK TH-228 74.82 10.28 4.384E+00 1. 417E+OO 1.417E+OO 54.14 OK Page 3664 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235034 Acquisition date 3-0CT-2016 09:15:46 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77 .11 17.10 4.583E+OO 2.090E+OO .2.. 090E+OO 21. 68 OK 238.63 43.60* 5 .101E+OO 1.160E+OO l.160E+OO 11. 38 OK 300.09 3.30 4.282E+OO 1.613E+OO 1.613E+OO 90.48 OK TH-230 609.32 45.49* 2.455E+OO 7.170E-01 7.170E-01 24.75 OK 1120.29 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 OK 1764.49 15.30 1.044E+OO 1.085E+OO l.085E+OO 34.63 OK PA-231 283.69 1. 70 4.487E+OO Line Not Found Absent 301.36 5.35* 4.282E+OO 9.950E-01 9.950E-01 90.48 OK TH-232 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11.27 3.904E+OO 9.786E-01 9.786E-01 43.53 OK 835. 71 1. 61 l.930E+OO Line Not Found Absent 911. 20 25.80* 1.806E+OO 9.674E-01 9.674E-01 30 .11 OK 968.97 15.80 1.723E+OO 1.306E+OO 1.306E+OO 53.35 OK TH-234 63.29 3.70* 2.991E+OO 2.453E+OO 2.453E+OO 100.42 OK 92.59 4.23 5.783E+OO 2.212E+OO 2.212E+OO 57.47 OK U-234 609.32 45.49* 2.455E+OO 7.170E-01 7.170E-01 24.75 OK 1120.29 14.92 1,538E+OO 1.025E+OO 1.025E+OO 62.84 OK 1764.49 15.30 1.044E+OO 1.085E+OO 1.085E+OO 34.63 OK U-235 89.96 3.47 5.597E+OO 1.330E+OO 1.330E+OO 77.94 OK 93.35 5.60 5.783E+OO 1. 671E+OO 1. 671E+OO 57.47 OK 143.76 10. 96* 6.593E+OO Line Not Found Absent 163.33 5.08 6.352E+OO Line Not Found Absent 185.72 57.20 5.975E+OO 1.413E-01 1.413E-01 63.45 OK 205.31 5.01 5.647E+OO Line Not Found Absent U-238 63.29 3.70* 2.991E+OO 2.453E+OO 2.453E+OO 100.42 OK 92.59 4.23 5.783E+OO 2.212E+OO 2.212E+OO 57.47 OK AM-241 59.54 35.90* 2.628E+OO 2.003E-01 2.006E-01 49.14 OK AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.384E+OO 2.168E-01 2.168E-01 54.14 OK ANH-511 511. 00 100.00* 2.814E+OO 8.764E-02 8.764E-02 86.30 OK Flag: "*" = Keyline Page 3665 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:16:43.69 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;l *
  • Acquisition date 3-0CT-2016 09:15:46 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.42 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:20:00 Analyst initials: MXRl *
  • Sample ID G405235034 Sample Quantity 1.5249E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.332E+Ol 1.478E+OO 6.426E-01 CD-109 6. 731E-01 1.958E+OO 2.032E+OO TE-125M 6.460E+02 5.546E+02 5.213E+02 SN-126 4.194E-02 l.220E-01 1.273E-01 BA-137M 1.048E-01 8.185E-02 7.083E-02 CS-137 1.107E-01 8.646E-02 7.483E-02 HG-203 2.382E+OO 5.463E+OO 4.560E+00 TL-208 2.920E-01 7.852E-02 4.606E-02 BI-211 1.015E-01 9. 051E-01 3.331E-01 PB-212 1.160E+OO 1.293E-01 8.924E-02 BI-214 7.173E-01 1. 739E-01 1. 093E-01 PB-214 1.059E+OO 1.847E-01 3.126E-01 RN-222 7.173E-01 1.739E-01 1.093E-01 RA-224 5.683E-01 1.370E+OO 9.563E-01 RA-226 7.173E-01 1.739E-01 1.093E-01 AC-228 9.674E-01 2.854E-01 1. 962E-01 RA-228 9.674E-01 2.854E-01 1. 962E-01 TH-228 1.160E+OO 1.293E-01 8.924E-02 TH-230 7.170E-01 1.739E-01 1. 093E-01 PA-231 9.950E-01 8.823E-01 6.843E-01 TH-232 9.674E-01 2.854E-01 1.962E-01 TH-234 2.453E+OO 2.414E+OO 2.094E+OO U-234 7.170E-01 1.739E-01 1.092E-01 U-235 -1.439E-03 1.846E-01 3.356E-01 U-238 2. 453E+o*o 2.414E+OO 2.094E+00 AM-241 2.006E-01 9.659E-02 2.451E-01 AM-243 2.168E-01 1.151E-01 8.252E-02 ANH-511 8.764E-02 7.412E-02 4. 272E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM BE-7 8.348E-01 1.271E+Ol 2.481E+Ol NOT IDENT. NA-22 -4.777E-02 4 .131E-02 6.204E-02 NOT IDENT. Page 3666 of 5809 NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 l.547E-02 2.448E-02 6.358E-02 NOT IDENT. SC-46 -2.201E-01 3.903E-01 6.050E-01 FAIL ABUN V-48 O.OOOE+OO 2.604E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.097E+02 O.OOOE+OO SHORT HLIF MN-54 2.235E-02 5.521E-02 1. 17 5E-01 NOT IDENT. C0-56 -1. 782E-01 5. 096E-01 9.679E-01 NOT IDENT. MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 -l.905E-02 4.852E-02 8. 596E-02 NOT IDENT. C0-58 3.946E-02 6.144E-01 l.245E+OO NOT IDENT. FE-59 -5.883E+OO 8.378E+OO l.201E+Ol NOT IDENT. C0-60 l.348E-02 3.622E-02 7.706E-02 NOT IDENT. ZN-65 -8.759E-02 l.973E-01 3.060E-01 NOT IDENT. GE-68 -5.803E-01 2.493E+OO 4.821E+OO NOT IDENT. AS-73 -8.156E+OO 9.830E+OO 1. 737E+Ol NOT IDENT. AS-74 O.OOOE+OO l.183E+04 O.OOOE+OO SHORT HLIF SE-75 l.688E-01 2.081E-01 4.340E-01 NOT IDENT. BR-77 O.OOOE+OO l.894E+39 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 9.634E+02 O.OOOE+OO SHORT HLIF RB-83 -9.954E-02 6.778E-01 l.272E+OO NOT IDENT. KR-85 8.167E+OO 6.956E+OO l.395E+Ol NOT IDENT. SR-85 1. OllE+OO 8.612E-01 1. 727E+OO NOT IDENT. RB-86 O.OOOE+OO 4.938E+04 O.OOOE+OO SHORT HLIF Y-88 3.775E-02 l.239E-01 3.491E-01 NOT IDENT. Y-91 5.339E+02 5.828E+02 1. 290E+03 NOT IDENT. NB-94 1. 04 7E-02 2.836E-02 5.633E-02 NOT IDENT. NB-95 -6.412E-02 9. 401E-01 1. 676E+OO NOT IDENT. NB-95M 5.124E-01 2.638E+OO 4.747E+OO NOT IDENT. ZR-95 4.297E-01 l.518E+00 3.168E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 037E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 9.763E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -6.833E-03 3.482E-02 6.242E-02 NOT IDENT. RH-102 -2.568E-02 5.892E-02 l.040E-01 FAIL ABUN RU-103 2.388E-01 6.790E+OO l.308E+Ol FAIL ABUN RH-106 -3.706E-02 4.378E-01 8.279E-01 NOT IDENT. RU-106 -3.706E-02 4.378E-01 8.279E-01 NOT IDENT. AG-108M 1. 296E-04 2.579E-02 4.959E-02 NOT IDENT. AG-llOM -6.847E-02 l.028E-01 l.550E-01 NOT IDENT. SN-113 -2.662E-02 2.129E-01 4.078E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 2.107E+05 O.OOOE+OO SHORT HLIF TE-123M -5. 996E-02 l.441E-01 2.499E-01 NOT IDENT. SB-124 l.555E-01 2.448E+00 5.061E+OO NOT IDENT. SB-125 -l.639E-03 9.043E-02 1. 746E-01 NOT IDENT. I-126 O.OOOE+OO 2.107E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.542E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.288E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.683E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.823E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.151E+27 O.OOOE+OO SHORT HLIF BA-133 3.794E-03 4.035E-02 7.104E-02 FAIL ABUN I-133 O.OOOE+OO l.207E+41 O.OOOE+OO SHORT HLIF CS-134 4.324E-02 4.652E-02 l.030E-01 FAIL ABUN CS-135 -l.680E-01 l.393E-01 2.434E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 6. 571E+05 O.OOOE+OO SHORT HLIF CE-139 -4. 221E-02 l.lOOE-01 2 .133E-Ol NOT IDENT. BA-140 O.OOOE+OO 2.742E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO l.076E+06 O.OOOE+OO SHORT HLIF CE-141 -8.592E+OO 3.332E+Ol 5.893E+Ol NOT IDENT. CE-143 0.000E+OO 1. 2 92E+4 l O.OOOE+OO SHORT HLIF CE-144 -9.719E-02 3.463E-01 6.169E-01 NOT IDENT. PM-144 -l.774E-02 6.166E-02 l.095E-01 NOT IDENT. PR-144 -l.539E+OO 5.400E+OO 9 .*596E+OO NOT IDENT. PM-146 3.158E-02 4.136E-02 8.603E-02 NOT IDENT. ND-147 O.OOOE+OO 8.050E+07 O.OOOE+OO SHORT HLIF PM-147 -3.560E+02 8.368E+02 1:478E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 8.007E-03 2.395E-02 4.590E-02 FAIL ABUN EU-152 -4.794E-02 9.410E-02 1. 721E-01 NOT IDENT. GD-153 -l.638E-01 l.877E-01 3.242E-01 NOT IDENT. EU-154 -l.140E-01 l.009E-01 l.531E-01 NOT IDENT. EU-155 6.302E-02 l.069E-01 2.070E-01 FAIL ABUN TB-160 6.260E-02 2.053E+OO 4.109E+OO FAIL ABUN H0-166M -5.778E-02 5.685E-02 8.882E-02 NOT IDENT. TM-171 l.286E+Ol l.988E+Ol 4.027E+Ol NOT IDENT. Page 3667 of 5809 HF-172 -1.829E-01 2.340E-01 3.986E-01 FAIL ABUN LU-172 -3.839E-02 6.747E-02 1.212E-01 FAIL ABUN LU-176 -8.265E-03 2.379E-02 4.245E-02 FAIL ABUN HF-181 3.274E+OO 5.054E+OO 1.047E+Ol NOT IDENT. TA-182 -2.729E-01 9.655E-01 1. 790E+OO FAIL ABUN RE-183 -1.981E-01 3.687E+OO 6.503E+OO FAIL ABUN RE-184 -2.086E+OO 3.266E+Ol 6.572E+Ol NOT IDENT. W-188 -l.149E+Ol 1.219E+02 2.131E+02 FAIL ABUN IR-192 2.380E-01 4.900E-01 9.945E-01 FAIL ABUN BI-207 2.278E-02 4.65:tE-02 9.781E-02 FAIL ABUN PB-210 2.036E+OO 3.637E+OO 7.284E+OO NOT IDENT. PB-211 -5.210E-02 6.358E-01 1.208E+OO NOT IDENT. BI-212 l.109E+OO 6.120E-01 1.318E+OO NOT IDENT. RN-219 2.893E-02 3.732E-01 7.197E-01 NOT IDENT. RA-223 -8.507E-03 5.594E-01 1.080E+OO FAIL ABUN AC-227 -2.436E-02 l.927E-01 3.749E-01 FAIL ABUN TH-227 -2.436E-02 1.927E-01 3.749E-01 FAIL ABUN TH-229 -2.682E-01 4. 271E-01 8.053E-01 FAIL ABUN TH-231 -8.507E-03 5.594E-01 1.080E+OO FAIL ABUN PA-233 -1. 896E-02 5.582E-02 1.048E-01 FAIL ABUN PA-234 -l.484E-01 2.345E-01 4. 231E-01 FAIL ABUN PA-234M 3 .134E+OO 3.917E+OO 8.979E+OO FAIL ABUN NP-237 -1. 896E-02 5.582E-02 1.048E-01 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 -1.174E-01 2.442E-01 4. 301E-01 FAIL ABUN PU-239 1.029E+02 3. 251E+02 6.050E+02 NOT IDENT. CM-243 4.367E-02 9.608E-02 1.848E-01 FAIL ABUN BK-247 3.465E-02 6.670E-02 1.359E-01 NOT IDENT. CM-247 1.436E-02 3.556E-02 7.047E-02 FAIL ABUN CF-249 1. 748E-02 3.125E-02 6.464E-02 NOT IDENT. CF-251 8.237E-02 1.084E-01 2.250E-01 NOT IDENT. Page 3668 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:16:41.51 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 357 10.66* l.237E+OO l.332E+Ol 1.332E+Ol 11. 33 CD-109 88.03 55 3.70* 5.423E+OO l.361E+OO 2.185E+OO 89.48 TE-125M 109.28 51 0.27* 6.445E+OO l.441E+Ol 6.460E+02 87.60 SN-126 64.28 55 9.60 2.991E+OO 9.454E-01 9.454E-01 100.42 86.94 55 8.90 5.423E+OO 5.660E-01 5.660E-01 89.48 87.57 55 37.00* 5.423E+OO 1.361E-01 l.361E-01 89.48 BA-137M 661. 66 43 89.90* 2.303E+OO 1.028E-01 1.048E-01 79.68 CS-137 661.66 43 85.10* 2.303E+OO 1. 086E-01 1.107E-01 79.68 HG-203 70.83 ------3.69 3.912E+OO ------Line Not Found ------72.87 ------6.19 4.138E+OO ------Line Not Found ------279.20 35 81. 56* 4.559E+OO 4. 672E-02 5.063E+OO 109.26 TL-208 277.37 35 6.60 4.559E+OO 5.774E-01 5.774E-01 109.26 583.19 128 85.00* 2.539E+OO 2.920E-01 2.920E-01 27.44 860.56 36 12.50 1.886E+OO 7.583E-01 7.583E-01 60.47 BI-211 72.87 ------1. 23 4 .138E+OO ------Line Not Found ------*351. 06 290 12. 92* ' 3.783E+OO 2.918E+OO 2.918E+OO 17.79 PB-212 74.82 183 10.28 4.384E+OO 1.994E+OO 1.994E+OO 37.68 77 .11 333 17.10 4.583E+OO 2.090E+OO 2.090E+OO 21. 68 238.63 524 43.60* 5.101E+OO 1.160E+OO 1.160E+OO 11. 38 300.09 46 3.30 4.282E+OO 1.613E+OO 1.613E+OO 90.48 BI-214 609.32 163 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 1120.29 48 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 1764.49 35 15.30 1.044E+OO 1.085E+OO 1. 086E+OO 34.63 PB-214 74.82 183 5.80 4.384E+OO 3.534E+OO 3.536E+OO 37.68 77.11 333 9.70 4.583E+00 3.684E+OO 3.685E+OO 21. 68 87.09 55 3.41 5.423E+OO 1.477E+OO 1.478E+OO 89.48 242.00 100 7.25 5. 051E+OO 1.344E+OO l.344E+OO 55.12 295.22 166 18.42 4.344E+OO l.022E+OO 1.023E+OO 27.12 351. 93 290 35.60* 3.783E+OO 1.059E+OO 1.059E+OO 17.79 RN-222 609.32 163 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 1120.29 48 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 1764.49 35 15.30 1.044E+OO 1.085E+OO l.086E+00 34.63 RA-224 240.99 100 4.10* 5. 051E+OO 2.376E+OO 2.376E+OO 55.12 RA-226 609.32 163 45.49* 2.455E+OO 7.170E-01 7.173E-01 24.75 1120.29 48 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 1764.49 35 15.30 1.044E+OO 1.085E+OO 1.086E+OO 34.63 AC-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 87 11. 27 3.904E+OO 9.786E-01 9.786E-01 43.53 794.95 ------4.25 2.005E+OO ------Line Not Found ------835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 92 25.80* 1.806E+OO 9.674E-01 9.674E-01 30.11 968. 97 72 15.80 1. 723E+OO l.306E+OO 1.306E+OO 53.35 RA-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 87 11. 27 3.904E+OO 9.786E-01 9.786E-01 43.53 794.95 ------4.25 2.005E+OO ------Line Not Found ------835. 71 ------1. 61 1.930E+OO ------Line Not Found ------911. 20 92 25.80* l.806E+OO 9.674E-01 9.674E-01 30 .11 Page 3669 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235034 Acquisition date 3-0CT-2016 09:15:46 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968.97 72 15.80 1.723E+OO 1.306E+OO 1. .306E+OO 53.35 TH-228 74.82 183 10.28 4.384E+OO 1.994E+OO 1.994E+OO 37.68 77 .11 333 17.10 4.583E+OO 2.090E+OO 2.090E+OO 21. 68 238.63 524 43.60* 5.101E+OO 1.160E+OO 1.160E+OO 11. 38 300.09 46 3.30 4.282E+OO 1.613E+OO 1.613E+OO 90.48 TH-230 609.32 163 45.49* 2.455E+OO 7.170E-01 7.170E-01 24.75 1120.29 48 14.92 1.538E+00 1.025E+OO 1.025E+00 62.84 1764.49 35 15.30 1.044E+OO l.085E+OO 1.085E+OO 34.63 PA-231 283.69 ------1. 70 4.487E+OO ------Line Not Found ------301.36 46 5.35* 4.282E+OO 9.950E-01 9.950E-01 90.48 TH-232 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 87 11. 27 3.904E+OO 9.786E-01 9.786E-01 43.53 835. 71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 92 25.80* 1.806E+OO 9.674E-01 9.674E-01 30.11 968. 97 72 15.80 1.723E+OO l.306E+OO 1.306E+OO 53.35 TH-234 63.29 55 3.70* 2. 991E+OO 2.453E+OO 2.453E+00 100.42 92.59 110 4.23 5.783E+OO 2.212E+OO 2.212E+00 57.47 U-234 609.32 163 45.49* 2.455E+OO 7.170E-01 7.170E-01 24.75 1120.29 48 14.92 1.538E+OO 1.025E+OO 1.025E+OO 62.84 1764.49 35 15.30 1.044E+OO 1.085E+OO 1.085E+OO 34.63 U-235 89. 96 52 3.47 5.597E+00 1.330E+OO 1.330E+OO 77.94 93.35 110 5.60 5.783E+OO 1. 671E+OO 1. 671E+OO 57.47 143.76 ------10.96* 6.593E+OO ------Line Not Found ------163.33 ------5.08 6.352E+OO ------Line Not Found ------185.72 98 57.20 5.975E+OO 1. 413E-01 1.413E-01 63.45 205.31 ------5.01 5.647E+OO ------Line Not Found ------U-238 63.29 55 3.70* 2.991E+OO 2.453E+OO 2.453E+OO 100.42 92.59 110 4.23 5.783E+OO 2.212E+OO 2.212E+OO 57.47 AM-241 59.54 38 35.90* 2.628E+OO 2.003E-01 2.006E-01 49.14 AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 183 67.20* 4.384E+OO 3.050E-01 3. 051E-01 37.68 ANH-511 511. 00 50 100.00* 2.814E+OO 8.764E-02 8.764E-02 86.30 Flag: "*" Key line Page 3670 of 5809 Summary of Nuclide Activity Sample ID : G405235034 Acquisition date Page : 3 3-0CT-2016 09:15:46 Total number of lines in spectrum 41 Number of unidentified lines 10 Number of lines tentatively identified by NID 31 Nuclide Type : Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-241 AM-243 ANH-511 Hlife 1.25E+09Y 461. 40D 57.40D 2.30E+05Y 30.08Y 30.08Y 46.59D 1. 41E+l0Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600. OOY 1600. OOY 1. 41E+10Y 1600.00Y l.41E+l0Y 1. 41E+l0Y 1.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 432.60Y 7370.00Y 1. OOE+09Y Decay 1. 00 1. 60 44.8 1. 00 1. 02 1. 02 108. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 ' 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.332E+Ol 1. 361E+OO 1.441E+Ol 1.361E-01 1. 028E,-01 1. 086E-01 4. 672E-02. 2.920E-01 2.918E+OO 1.160E+OO 7.170E-01 1.059E+OO 7.170E-01 2.376E+OO 7.170E-01 9.674E-01 9.674E-01 1.160E+OO 7.170E-01 9.950E-01 9.674E-01 2.453E+OO 7.170E-01 1.413E-01 2.453E+OO 2.003E-01 3.050E-01 8.764E-02 5.157E+Ol 5.157E+Ol Decay Corr pCi/GRAM l.332E+Ol 2.185E+OO 6.460E+02 l.361E-01 1.048E-01 1.107E-01 5.063E+OO 2.920E-01 2.918E+OO 1.160E+OO 7.173E-01 l.059E+OO 7.173E-01 2.376E+00 7.173E-01 9.674E-01 9.674E-01 1.160E+OO 7.170E-01 9.950E-01 9.674E-01 2.453E+OO 7.170E-01 1.413E-01 2.453E+OO 2.006E-01 3.051E-01 8.764E-02 6.890E+02 6.890E+02 75.61% Decay Corr 2-Sigma Error 0.151E+Ol 1.955E+OO 5.659E+02 1.218E-01 0.835E-01 0.882E-01 5.532E+OO 0. 801E-01 0.519E+OO 0 .132E+OO 1. 775E-01 0.189E+OO 1.775E-01 1.309E+OO 1. 775E-01 2.913E-01' 2.913E-01 0.132E+OO l.774E-01 9.003E-01 2.913E-01 2.463E+OO 1.774E-01 0.897E-01 2.463E+OO 0.986E-01 1.149E-01 7.563E-02 "M" Manually accepted 2-Sigma %Error 11. 33 89.48 87.60 89.48 79.68 79.68 109.26 27.44 17.79 11. 38 24.75 17.79 24.75 55.12 24.75 30.11 30.11 11. 38 24.75 90.48 30 .11 100.42 24.75 63.45 100.42 49.14 37.68 86.30 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3671 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235034 Acquisition date : 3-0CT-2016 09:15:46 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 371.44 25 38 1. 52 743.40 739 9 6.26E-03 **** 3.63E+OO T 0 564.49 29 34 2.23 1129.79 1123 14 7.58E-03 95.4 2. 61E+OO T 0 579.28 20 24 1. 34 1159. 39 1153 9 5.15E-03 **** 2.55E+OO 0' 729. 51 38 63 3.28 1460.08 1450 26 1.02E-02 **** 2.14E+OO 0 767.85 23 22 0.74 1536.82 1530 12 6.08E-03 95.7 2.06E+OO T 0 886.67 9 7 1.16 1774.63 1771 8 2.52E-03 **** 1. 85E+OO 0 1002.53 13 23 0.71 2006.54 1999 19 3.62E-03 **** 1.68E+OO T 3 1014.01 14 0 1. 39 2029.50 2028 11 3.88E-03 28.7 1.66E+OO 3 1016.81 19 0 1. 70 2035.10 2028 11 5.25E-03 44.9 1. 66E+OO 0 1102.17 11 5 1. 23 2205. 96 2200 10 3. llE-03 95.4 1.56E+OO 0 1157 .11 8 12 1.16 2315.93 2311 9 2.34E-03 **** 1.50E+OO 0 1189.83 48 0 4. 71 2381. 41 2371 18 l.36E-02 28.6 1. 47E+OO T 0 1345. 72 23 0 2.53 2693.42 2684 17 6.67E-03 40.8 1.33E+OO 0 1592.90 5 5 0.48 3188.16 3186 6 1.39E-03 **** 1.15E+OO 0 1730.16 15 3 2.30 3462.88 3457 11 4.52E-03 63.3 1.06E+OO Flags: "T" = Tentatively associated Page 3672 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:16:56.33 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;l * *Acquisition date 3-0CT-2016 09:15:46 Sensitivity 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.42 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:20:00 Nuclide Library : SOLID *
  • Sample ID G405235034 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.5249E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]E'FF GAM28 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-241 AM-243 ANH-511 Le (pCi/GRAM 2.705E-01 9.592E-01 2.423E+02 6.0lOE-02 3.206E-02 3.387E-02 2.076E+OO 1.985E-02 1.524E-01 4.148E-02 4.852E-02 l.512E-01 4.852E-02 4.446E-01 4.852E-02 8.353E-02 8.353E-02 4.148E-02 4.850E-02 3 .118E-01 8.353E-02 9.822E-01 4.850E-02 1.580E-01 9.822E-01 l.145E-01 3.879E-02 l.892E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3673 of 5809 Le (pCi/GRAM l.106E+Ol 2.492E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59. C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3674 of 5809 2.524E-02 2.526E-01 O.OOOE+OO O.OOOE+OO 5.165E-02 4.239E-01 O.OOOE+OO 4.019E-02 5.473E-01 4.971E+OO 3.291E-02 l.319E-01 2 .115E+OO 8.050E+OO 0.000E+OO 2.015E-01 O.OOOE+OO O.OOOE+OO 5.666E-01 6.377E+OO 7.895E-01 O.OOOE+OO l.228E-01 5.708E+02 2.506E-02 7.378E-01 2.208E+OO l.402E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.934E-02 4.598E-02 5.859E+OO 3.627E-01 3.627E-01 2.241E-02 6.538E-02 l.835E-01 O.OOOE+OO O.OOOE+OO l.168E-01 2.046E+OO 7.844E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.237E-02 O.OOOE+OO 4.620E-02 l.124E-01 O.OOOE+OO O.OOOE+OO 9.982E-02 O.OOOE+OO O.OOOE+OO 2.763E+Ol O.OOOE+OO 2.878E-01 4.912E-02 4.304E+OO 3.919E-02 O.OOOE+OO 6.916E+02 O.OOOE+OO 2.109E-02 7.897E-02 l.520E-01 6.169E-02 9.744E-02 1. 806E+00 3.862E-02 l.877E+Ol l.863E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOTcIDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3675 of 5809 5.122E-02 1. 946E-02 4.734E+OO 7.783E-01 3.044E+OO 2.820E+Ol 9.759E+Ol 4.580E-01 4.316E-02 3.425E+OO 5.501E-01 6.117E-01 3. 291E-01 4. 968E-01 l.723E-01 l.723E-01 3.754E-01 4. 968E-01 4.806E-02 1.794E-01 4. OllE+OO 4.806E-02 O.OOOE+OO 2.015E-01 2.857E+o2 8.683E-02 6.302E-02 3.242E-02 2.932E-02 1.059E-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:17:01.60 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235034.CNF;l *
  • Acquisition date 3-0CT-2016 09:15:46 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.42 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:20:00 Nuclide Library : SOLID *
  • Sample ID G405235034 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.5249E+02 GRAM *
  • Quantity Err(%) : 1.3116E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.332E+Ol 1.635E+OO CD-109 6.731E-01 1.968E+OO TE-125M 6.460E+02 5.559E+02 SN-126 4.194E-02 1.226E-01 BA-137M 1.048E-01 8.197E-02 CS-137 1.107E-01 8.660E-02 HG-203 2.379E+OO 5.472E+OO TL-208 2.920E-01 7.952E-02 BI-211 1.015E-01 9.217E-01 PB-212 1.160E+OO l.434E-01 BI-214 7.173E-01 l.767E-01 PB-214 1.059E+OO 1.900E-01 RN-222 7.173E-01 l.767E-01 RA-224 5.683E-01 1.376E+OO RA-226 7.173E-01 1. 7 67E-01 AC-228 9.674E-01 2.898E-01 RA-228 9.674E-01 2.898E-01 TH-228 1.160E+OO l.434E-01 TH-230 7.170E-01 1.766E-01 PA-231 9.950E-01 9.075E-01 TH-232 9.674E-01 2.898E-01 TH-234 2.453E+OO 2.474E+OO U-234 7.170E-01 l.766E-01 U-235 -l.439E-03 l.846E-01 U-238 2.453E+00 2.474E+OO AM-241 2.006E-01 9.769E-02 AM-243 2.168E-01 1.164E-01 ANH-511 8.764E-02 7.421E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3676 of 5809 Key-Line Activity (pCi/GRAM 8.348E-01 -4.777E-02 K.L Act error ( 1 . 96-sigma ) 1. 271E+Ol 4 .135E-02 TPU (1.96-sigma) 1.635E+OO 1. 968E+OO 5.559E+02 1.226E-01 8.197E-02 8.660E-02 5.472E+OO 7.952E-02 9.217E-01 1.434E-01 1.767E-01 l.900E-01 1. 767E-01 1.376E+OO 1. 767E-01 2.898E-01 2.898E-01 1.434E-01 1.766E-01 9.075E-01 2.898E-01 2.474E+OO 1.766E-01 1.846E-01 2.474E+OO 9.769E-02 1.164E-01 7.421E-02 TPU (1. 96-sigma) 1.272E+Ol NOT IDENT. 4.662E-02 NOT IDENT.

NA-24 -l.OOOE+41 2.042E+41 O.OOOE+OO SHORT HLIF AL-26 1. 547E-02 2.450E-02 2.547E-02 NOT IDENT. SC-46 -2.201E-01 3.904E-01 4.028E-01 FAIL ABUN V-48 -l.653E+04 2.605E+04 2.710E+04 SHORT HLIF CR-51 3.092E+02 6.099E+02 6.256E+02 SHORT HLIF MN-54 2.235E-02 5.522E-02 5.613E-02 NOT IDENT. C0-56 -1. 782E-01 5.097E-01 5.160E-01 NOT IDENT. MN-56 -l.OOOE+41 2.861E+41 O.OOOE+OO SHORT HLIF C0-57 -1.905E-02 4.853E-02 4.929E-02 NOT IDENT. C0-.58 3.946E-02 6.144E-.01 6.147E:-01 NOT IDENT. FE-59 -5.883E+OO 8.389E+OO 8.798E+OO NOT IDENT. C0-60 1.348E-02 3.622E-02 3.673E-02 NOT IDENT. ZN-65 -8.759E-02 l.973E-01 2.012E-01 NOT IDENT. GE-68 -5.803E-01 2.493E+OO 2.506E+OO NOT IDENT. AS-73 -8.156E+OO 9. 972E+OO 1. 063E+Ol NOT IDENT. AS-74 -l.144E+04 l.187E+04 1. 294E+04 SHORT HLIF SE-75 l.688E-01 2.083E-01 2.217E-01 NOT IDENT. BR-77 l.698E+40 1.544E+41 0.000E+OO SHORT HLIF SR-82 -4.785E+02 9.636E+02 9.875E+02 SHQRT HLIF RB-83 -9.954E-02 6.779E-01 6.794E-01 NOT IDENT. KR-85 8.167E+OO 6. 964E+OO 7.877E+OO NOT IDENT. SR-85 1. OllE+OO 8.622E-01 9.752E-01 NOT IDENT. RB-86 6.148E+03 4.939E+04 4.946E+04 SHORT HLIF Y-88 3.775E-02 1.239E-01 1. 251E-01 NOT IDENT. Y-91 5.339E+02 5.832E+02 6.309E+02 NOT IDENT. NB-94 1. 047E-02 2.837E-02 2.876E-02 NOT IDENT. NB-95 -6.412E-02 9.401E-01 9.405E-01 NOT IDENT. NB-95M 5.124E-01 2.638E+OO 2. 648E+OO' NOT IDENT. ZR-95 4.297E-01 1.518E+OO 1. 531E+OO NOT IDENT. NB-97 1.000E+41 1. 041E+42 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.038E+41 O.OOOE+OO SHORT HLIF M0-99 -6.793E+33 9.776E+33 O.OOOE+OO SHORT HLIF TC-99M -1. OOOE+41 2.389E+42 O.OOOE+OO SHORT HLIF RH-101 -6.833E-03 3.484E-02 3.497E-02 NOT IDENT. RH-102 -2.568E-02 5.896E-02 6.008E-02 FAIL ABUN RU-103 2.388E-01 6.790E+OO 6.791E+OO FAIL ABUN RH-106 -3.706E-02 4.378E-01 4.381E-01 NOT IDENT. RU-106 -3.706E-02 4.378E-01 4.381E-01 NOT IDENT. AG-108M 1. 296E-04 2.579E-02 2.579E-02 NOT IDENT. AG-llOM -6.847E-02 1.029E-01 l.074E-01 NOT IDENT. SN-113 -2.662E-02 2.130E-01 2.133E-01 NOT IDENT. CD-115 6.312E+40 3.113E+41 O.OOOE+OO SHORT HLIF SN-117M -5.127E+04 2.108E+05 2.120E+05 SHORT HLIF TE-123M -5. 996E-02 l.442E-01 l.467E-01 NOT IDENT. SB-124 1.555E-01 2.448E+OO 2.449E+OO NOT IDENT. SB-125 -l.639E-03 9.043E-02 9.043E-02 NOT IDENT. I-126 1.378E+06 2 .116E+06 2.205E+06 SHORT HLIF SB-126 -6.778E+05 2.545E+06 2.564E+06 SHORT HLIF SB-127 1. 364E+23 3.833E+23 O.OOOE+OO SHORT HLIF I-131 -l.753E+l0 1. 685E+10 1.861E+10 SHORT HLIF I-132 -l.000E+41 1.950E+42 O.OOOE+OO SHORT HLIF TE-132 -8.859E+27 9.898E+27 O.OOOE+OO SHORT HLIF BA-133 3.794E-03 4.035E-02 4.039E-02 FAIL ABUN I-133 -l.000E+41 2. 251E+41 O.OOOE+OO SHORT HLIF CS-134 4.324E-02 4.656E-02 5.048E-02 FAIL ABUN CS-135 -1. 680E-01 1. 398E-01 1.590E-01 NOT IDENT. I-135 -1.000E+41 9.394E+41 O.OOOE+OO SHORT HLIF CS-136 -5.567E+05 6. 601E+05 7.062E+05 SHORT HLIF CE-139 -4. 221E-02 1.104E-01 1.120E-01 NOT IDENT. BA-140 -1.147E+06 2.743E+06 2.791E+06 SHORT HLIF LA-140 9.198E+04 l.076E+06 l.077E+06 SHORT HLIF CE-141 -8.592E+OO 3.332E+Ol 3.354E+Ol NOT IDENT. CE-143 1.000E+41 l.297E+41 O.OOOE+OO SHORT HLIF CE-144 -9.719E-02 3.463E-01 3.491E-01 NOT IDENT. PM-144 -1. 774E-02 6.167E-02 6.219E-02 NOT IDENT. PR-144 -1. 539E+OO 5.401E+OO 5.445E+OO NOT IDENT. PM-146 3.158E-02 4.142E-02 4.380E-02 NOT IDENT. ND-147 -4.384E+07 8.053E+07 8.292E+07 SHORT HLIF PM-147 -3.560E+02 8.369E+02 8.522E+02 NOT IDENT. PM-149 1.000E+41 2.522E+41 O.OOOE+OO SHORT HLIF EU-150 8.007E-03 2.395E-02 2.422E-02 FAIL ABUN EU-152 -4.794E-02 9.414E-02 9.659E-02 NOT IDENT. GD-153 -1.638E-01 1.880E-01 2.019E-01 NOT IDENT. EU-154 -1.140E-01 1.0lOE-01 1.134E-01 NOT IDENT. EU-155 6.302E-02 l.070E-01 1.107E-01 FAIL ABUN TB-160 6.260E-02 2.053E+OO 2.053E+OO FAIL ABUN H0-166M -5.778E-02 5.693E-02 6.261E-02 NOT IDENT. TM-171 1.286E+Ol 1. 991E+Ol 2.074E+Ol NOT IDENT. Page 3677 of 5809 HF-172 -1. 829E-01 2.359E-01 2.499E-01 FAIL ABUN LU-172 -3.839E-02 6.758E-02 6.977E-02 FAIL ABUN LU-176 -8.265E-03 2.379E-02 2.408E-02 FAIL ABUN HF-181 3.274E+OO 5.056E+OO 5.267E+OO NOT IDENT. TA-182 -2. 729E-01 9.656E-01 9.734E-01 FAIL ABUN RE-183 -1. 981E-01 3.687E+OO 3.688E+OO FAIL ABUN RE-184 -2.086E+OO 3.267E+Ol 3.268E+Ol NOT IDENT. W-188 -l.149E+Ol 1.219E+02 l.220E+02 FAIL ABUN IR-192 2.380E-01 4.901E-01 5.017E-01 FAIL ABUN '. BI-207 2.278E-02 4.765E-02 FAIL ABUN PB-210 2.036E+OO 3.642E+OO 3.755E+OO NOT IDENT. PB-211 -5.210E-02 6.358E-01 6.362E-01 NOT IDENT. BI-212 l.109E+OO 6.146E-01 7.922E-01 NOT IDENT. RN-219 2.893E-02 3.732E-01 3.735E-01 NOT IDENT. RA-223 -8.507E-03 5.594E-01 5.594E-01 FAIL ABUN AC-227 -2.436E-02 l.928E-01 l.931E-01 FAIL ABUN TH-227 -2.436E-02 l.928E-01 l.931E-01 FAIL ABUN TH-229 -2.682E-01 4.273E-01 4.441E-01 FAIL ABUN TH-231 -8.507E-03 5.594E-01 5.594E-01 FAIL ABUN PA-233 -1. 896E-02 5.582E-02 5.648E-02 FAIL ABUN PA-234 -l.484E-01 2.895E-01 2. 972E-01 FAIL ABUN PA-234M 3.134E+OO 3.919E+OO 4.166E+OO FAIL ABUN NP-237 -1. 896E-02 5.582E-02 5.648E-02 FAIL ABUN NP-238 -1.000E+41 4.811E+41 O.OOOE+OO SHORT HLIF NP-239 -1.174E-01 2.444E-01 2.501E-01 FAIL ABUN PU-239 l.029E+02 3.252E+02 3.285E+02 NOT IDENT. CM-243 4.367E-02 9.617E-02 9.816E-02 FAIL ABUN BK-247 3.465E-02 6.706E-02 6.886E-02 NOT IDENT. CM-247 1. 436E-02 3.564E-02 3.622E-02 FAIL ABUN CF-249 1. 748E-02 3.128E-02 3.226E-02 NOT IDENT. CF-251 8.237E-02 l.088E-01 l.150E-01 NOT IDENT. Page 3678 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 67.7320 87.09 106.0090 136.47 72.9840 45.60 79.5984 87.57 95.4818 140.51 0.0000 46.54 64.0330 88.03 95.5523 143.76 79.7523 49.72 0.0000 88.34 95.6004 144.24 71. 2035 51. 35 59.4449 88.47 95.6202 145.44 82.3668 51. 87 52.0750 89. 96 100.4113 152.43 66.9158 52.39 45.7516 1093.63 82.2431 153.25 0.0000 52.97 53.2681 91.11 0.0000 323.87 62.0819 53.44 69.3204 92.59 80. 9670 156.02 0.0000 54.07 64.0764 93.35 81.0624 158.56 0.0000 57.36 0.0000 94.56 87.3433 159.00 78.6366 57.53 62.4014 94.65 87.3549 162.33 60.9648 57.98 73.2290 94. 67 87.3578 162.66 0.0000 59.27 66.2270 94.87 87.3845 163.33 64.3750 59.32 67.6737 97.43 93.4962 165.86 80.4756 59.54 67.7043 98.43 77.4524 176.31 76.2680 60. 96 75.8466 98.44 77.4534 176.60 0.0000 61.17 75.8789 99.53 60. 2111 177.52 67.0283 62.93 76.1473 100 .11 74.1694 181. 07 0.0000 63.29 76.2016 102.03 84.8384 181. 52 70.2799 63.58 76.2453 103.18 68.6828 184.41 76.8887 64.28 76.3505 103.37 69.8666 143.76 75.2768 66.73 76.7136 105.21 71. 2193 193.51 77.5699 67.24 76.7884 105.31 71. 2293 197.03 51.0212 125.81 76.8530 106.12 73.2601 198.01 57.1270 67.75 76.8626 106.47 67.0589 201.83 65.1489 69.67 83.7535 109.28 57.9307 203.43 61.7653 70.83 77.3070 111. 00 69.4476 205.31 74.9438 72. 81 82.0215 111.76 0.0000 210.85 74.4459 72. 87 82.0300 114. 06 75.6499 215.65 70.3670 74.66 82.2947 116. 30 0.0000 222 .11 61. 0362 74.82 82.3179 116.74 85.4138 227.09 58.6329 74.97 82.3399 119.76 75.0370 227.38 66.6451 77 .11 82.6516 121.12 82.3302 228.16 0.0000 78.74 82.8858 121.22 82.3407 228.18 67.5793 79.69 83.0213 121. 78 84.7897 116.74 67.5793 80.12 83.0823 122.06 78.8473 235.69 55.0331 80.19 0.0000 122.92 56.2112 235. 96 55.0450 80.57 83.1461 123.07 55.0261 238.63 58.3065 81. 00 97.4491 265.00 65.8437 238.98 0.0000 81. 07 97.4610 125.81 88.8320 240.99 58.4196 81. 75 103. 5772 127.23 86.5863 242.00 58.4679 83.79 90.3748 127.91 75.8284 244.70 58.5968 84.00 88.8997 129.30 86.8118 252.40 0.0000 85.43 110.2537 131. 20 83.3925 252.80 50.8121 86.55 110.4550 133.02 62.9878 254.15 0.0000 86.79 110. 4980 133.52 71.5101 256.23 45.4908 86.94 105.9827 136.00 86.3146 260.90 0.0000 Page 3679 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.2106 355.39 0.0000 584.27 13.1577 264.80 43.0470 356.01 33.6451 595.83 0.0000 265.00 44.8858 364.49 0.0000 427.87 41.9583 268.22 74.3802 366.42 0.0000 602.52 0.0000 269.46 65. 2596 372. 51 31.0309 604.72 16.5912 270.03 62.5284 375.05 34.0381 607.14 19.9292 271.23 53.3814 377.52 32.6066 609.32 21. 0557 273.65 0.0000 356.01 33. 7205 610.33 21. 0650 276.40 51.2792 388.16 23.8628 614.28 21. 6550 277.37 40.6833 388.63 0.0000 618.01 17.7956 277.60 40.6896 391. 69 28.8938 620.36 14.4727 278.00 40.7021 264.66 39.0579 621. 93 17.8242 279.20 34. 7198 401. 81 37.0790 630.19 0.0000 279.54 34.7290 402.40 37.0918 631. 2 9 25.7206 279.70 34.7328 404.85 36.1392 633.25 21. 2644 280.46 33.3625 410.95 26.1904 634.78 0.0000 283.69 40.8731 413.71 44.3903 635.95 16.8060 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 38.1339 423. 72 0.0000 645.85 22.4976 285.90 0.0000 427.09 25.4084 657.76 22.0391 287.50 40.9859 427.87 26.4359 657.90 0.0000 290.67 36.4117 433.94 29.5829 661.66 30.5629 293.27 0.0000 439.40 30.6927 664.57 0.0000 351.93 46.3660 453.88 '23.7113 666.33 0.0000 295.96 46.3901 463.37 32 .1157 666.50 0.0000 879.38 33.8005 468.07 18.6929 667.71 0.0000 299.98 35.2440 473.00 0.0000 677.62 22.7799 300.09 35.2463 475.06 18.7592 685.70 0.0000 300 .13 35.2470 476.78 23.9906 695.00 0.0000 301.36 35.2776 477.60 21. 9135 696.49 29.8276 302.85 39.5519 482.18 20.9176 696. 51 29.8276 256.23 32.5269 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.6565 306.78 47.5925 497.08 24.2325 697.49 20.6580 308.46 44.4335 505.52 22.2159 702.65 17.2485 311. 90 47.3806 507.63 0.0000 706.68 23.0322 316.51 37.0735 511. 00 20.1529 711. 68 28.8442 319.41 0.0000 514.00 19 .1191 720.70 0.0000 320.08 0.0000 514.00 19 .1191 721. 93 0.0000 321.04 36.2327 520.40 24.5039 722. 78 27.8047 323.87 44.8992 520.69 0.0000 722.91 27.8057 325.23 57.3694 522.65 0.0000 723.31 20.8572 328.76 0.0000 527.90 0.0000 724.19 10.4319 333.37 52.8706 528.26 17.1094 727. 33 23.2088 333.97 36.9281 529.59 25.6797 733.00 23.2568 334.37 33.1860 529.87 0.0000 735.93 19.2070 338.28 55.9326 531.02 0.0000 333.97 26.2061 338.32 55.9338 537.26 0.0000 739.50 0.0000 311. 90 40.5602 546.56 0.0000 747.24 15.7791 340.48 40.5602 552.55 20.5439 748.06 14.9066 340.55 0.0000 563.25 19.5564 752.31 16.6859 344.28 51. 3071 569.33 29.4126 753.82 0.0000 345.93 36.8249 946.00 27.7806 756.73 16.7120 351.06 38.8892 569.70 27.7838 756.80 16.7126 351.93 38.9103 583.19 13.1519 884.68 9.8766 Page 3680 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 16.9424 1274.44 7.5930 1620.50 5.4907 766.42 21.1824 1001.03 8.5537 1621. 92 4.3938 766.84 21.1853 1002.74 8.5578 1678.03 0.0000 772.60 0.0000 1004.73 8.5627 1690.97 5.5652 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.00QO 1764.49 1.8051 778.90 17.7289 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 12.4835 1771.35 7.2293 785.37 23.0991 1038.76 0.0000 1,791. 20 0.0000 792.07 22.2618 631.29 5.7759 1808.65 1.8194 794.95 14.2617 1048.07 0.0000 1810.72 0.0000 795.86 14.2661 1049.04 21.1917 1836.06 0.9141 810.06 17.0228 1050.41 15.4180 810.29 17.0239 1063.66 13.5394 344.28 17.0245 1077.00 0.0000 810.76 17.0268 1077.34 16.5020 815.77 0.0000 1085.87 15.5674 1048.07 0.0000 1093.63 15.5996 832.01 17.1474 1099.45 15. 62.30 834.85 13.5498 1112. 07 13.7163 835. 71 15.3611 1112.84 15.6787 836.80 0.0000 1115. 54 18.8273 846.75 0.0000 1120.29 13.7454 846.77 20.8578 1120.55 13.7462 856.80 0.0000 1221.41 13.7488 860.56 9.1092 1129. 67 17.3218 871.09 11.8816 1131. 51 0.0000 873.19 12 .. 8041 1147.95 0.0000 875.33 0.0000 1173.23 13.9333 879.38 17.4113 1177.95 20 .. 9244 880.51 11.9173 1189.05 8.9923 883.24 10.2758 1204.77 10.0305 884.68 17.6238 1221. 41 18.1285 889.28 14.7075 1231.02 18.1714 894.76 13.8121 1235.36 0.0000 898.04 12. 9045 1238.28 18.2032 900.72 13.8377 1260.41 0.0000 903.28 12.9255 1271.87 8.1553 911. 20 11.1061 1274.44 16.3203 912.08 11.1090 1274. 54 16.3213 923.98 0.0000 1291.59 8.1929 926.50 12.0875 1298.22 0.0000 929 .11 11.1665 1312 .11 0.0000 937.49 17. 7255 1332.49 8.2705 944 .13 0.0000 1362.66 0.0000 946.00 16.8349 1365.19 5.2072 949.00 14.9780 1368.63 0.0000 667.71 0.0000 1384.29 5.2295 962. 31 19.5482 1408.01 4.2053 964.08 7.5225 1457.56 0.0000 966 .17 7.5271 1460.82 9.5696 911. 20 7.5332 1489.16 2.1392 968. 97 7.5332 1505.03 4.2925 983.53 0.0000 1584.12 8. 7231 984.45 0.0000 1596. 21 0.0000 Page 3681of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:17:30.81 ******************************************************************************** *
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM33.CNF;235 Background date : Z-OCT-2016 11:02:02. Sample date 23-NOV-2015 11:06:00 Acquisition date : 3-0CT-2016 09:16:17. Sample ID G405235035 Sample quantity 1.64073E+02 GRAM Detector name : GAM33 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real 0 01:00:00.73 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 1 1 8 8 8 0 0 0 6 6 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3682 of 5809 Energy 40.90 64.05* 68.49 75.06* 77.06 87.03 89.83 94.27 118. 51 128.82 154.68 163.47* 166.25 186.12* 209.48 224.37 238.59* 241. 74 270.13 295.21 300.05 338.80* 351.99* 424.65 462.97 510.89* 562.17 583.40* 597.97 609.40* 644.53 661.59 705.95 727.69 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 20 13 29 75 157 43 46 59 29 20 20 28 22 44 73 47 353 70 49 129 26 72 181 21 22 25 17 89 15 138 8 9 11 23 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 82 201 70 124 107 192 179 90 67 95 36 84 52 102 82 105 72 59 64 56 46 46 88 13 13 38 7 38 29 48 25 36 14 12 1. 43 1. 23 0.94 1.10 1.11 1. 33 1. 43 1. 25 0.92 0.93 1. 34 2.01 1. 05 1. 06 1. 63 3.68 1.19 1. 44 1.19 0.88 1. 44 1. 05 1. 49 0.87 1. 05 2.74 1. 41 1. 26 0.57 1. 36 2.18 0.60 0.95 2.01 81. 97 128.21 137.07 150.20 154.20 174.11 179.69 188.57 236.98 257.58 309.23 326.79 332.34 372.05 418.71 448.45 476.86 483.14 539.87 589.97 599.64 677.07 703.44 848.63 925.21 1020.98 1123.47 1165. 92 1195. 04 1217.88 1288.12 1322.22 1410.91 1454.37 76 123 135 143 143 169 169 169 234 255 307 323 323 368 414 442 469 469 535 585 596 673 696 845 922 1014 1120 1161 1190 1213 1283 1319 1408 1451 8 5.54E-03 83.0 11 3.50E-03224.5 5 8.00E-03 47.8 16 2.lOE-02 28.5 7.47E-01 16 4.35E-02 14.4 25 l.19E-02 51.6 5.71E+OO 25 l.27E-02 53.8 25 l.65E-02 39.4 7 7. 98E-03 51.1 7 5.55E-03 83.9 5 5. 54E-03 51. 3 12 7.71E-03 60.8 1.98E+OO 12 6.18E-03 58.4 10 1.22E-02 49.8 10 2.02E-02 26.4 13 l.32E-02 46. 7 18 9.79E-02 6.8 1.56E+OO 18 l.95E-02 22.5 10 1.35E-02 34.2 10 3.58E-02 14.1 9 7.28E-03 50.2 10 2.00E-02 22.0 16 5.04E-02 13.8 7 5.80E-03 36.6 7 6.02E-03 35.6 14 6.83E-03 70.3 7 4.70E-03 35.6 10 2.48E-02 17.5 12 4. 08E-03 81. 4 12 3.83E-02 13.4 12 2.31E-03123.0 9 2.50E-03124.7 7 3.06E-03 64.0 8 6.27E-03 35.1 Peak Search Report (continued) Page : 2 Sample ID : G405235035 Acquisition date 3-0CT-2016 09:16:17 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 767.90 25 24 1.14 1534.78 1529 11 6.84E-03 43.9 36 0 786.15 16 8 1. 00 1571.25 1567 10 4.52E-03 40.2 37 0 795.80 8 0 .. 54 1590.56 1585 9 2.18E-03107.6 38 0 806.45 7 12 1.17 1611. 85 1605 9 l.95E-03100.0 39 0 821. 53 18 5 3.01 1642.01 1637 11 4.86E-03 34.8 40 0 860.72 19 11 1. 08 1720.37 1715 11 5.28E-03 40.9 41 0 911. 09* 88 6 1. 57 1821.10 1814 13 2.44E-02 12.5 42 3 965.06 37 7 2.28 1929.05 1921 22 1. 03E-02 22.4 l.49E+OO 43 3 969.50* 40 6 1. 82 1937.94 1921 22 l. lOE-02 20.6 44 0 1121.12* 29 28 0.63 2241. 23 2232 16 7.94E-03 45.9 45 0 1137. 59 7 2 1. 41 2274.18 2271 7 1. 96E-03 49.2 46 0 1378. 42 15 6 1. 62 2756.10 2749 11 4.03E-03 40.9 47 0 1406.85* 10 0 1. 49 2813.00 2806 11 2.75E-03 35.8 48 0 1460.88* 335 3 2.07 2921.16 2913 15 9.30E-02 5.7 49 0 1501.18 7 2 1. 36 3001.84 2998 7 2.04E-03 47.4 50 0 1764.68* 27 0 2.61 3529.43 3522 13 7.45E-03 20.7 Flag: "*" = Peak area was modified by background subtraction Page 3683 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:17:33 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 23-NOV-2015 11:06:00 G405235035 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:16:17 164.07 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA33 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 'PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3684 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.73 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235035 Acquisition date 3-0CT-2016 09:16:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status K-40 1460.a2 10.66* l.134E+OO 1.233E+Ol 1. 233E+O.l 11. 33 OK CD-109 88.03 3.70* 4.887E+OO 5.956E-01 9.559E-01 255.58 OK SN-126 64.28 9.60 2.549E+OO 3.248E-01 3.248E-01 448.91 OK 86.94 8.90 4.887E+OO 2.476E-01 2.476E-01 255.58 OK 87.57 37.00* 4.887E+00 5.956E-02 5.956E-02 255.58 OK BA-137M 661.66 89.90* 2 .115E+OO 2.331E-02 2.378E-02 249.44 OK CS-137 661.66 85.10* 2.115E+OO 2.462E-02 2.512E-02 249.44 OK CE-139 165.86 80.00* 5.922E+OO 2.700E-02 l.319E-01 116.79 OK TL-208 277.37 6.60 4.258E+OO Line Not Found Absent 583.19 85.00* 2.334E+OO 2.253E-01 2.253E-01 35.00 OK 860.56 12.50 1.727E+OO 4.197E-01 4.197E-01 81. 71 OK BI-212 727. 33 6.67* 1. 965E+OO 8.389E-01 8.389E-01 70.29 OK 785.37 1.10 1. 851E+OO 3.852E+OO 3.852E+OO 80.37 OK 1620.50 1. 47 1.036E+OO Line Not Found Absent PB-212 74.82 10.28 3.825E+OO 6.676E-01 6.676E-01 104.28 OK 77 .11 17.10 4.028E+OO 1.410E+OO 1.410E+OO 28.90 OK 238.63 43.60* 4.776E+OO 9.366E-01 9.366E-01 13. 53 OK 300.09 3.30 4.000E+OO 1.071E+OO 1.071E+OO 100.50 OK BI-214 609.32 45.49* 2.255E+OO 6.677E-01 6.679E-01 26.76 OK 1120. 29 14.92 1.407E+OO 6.277E-01 6.279E-01 91. 79 OK 1764.49 15.30 9.591E-01 7.932E-01 7.935E-01 41. 37 OK PB-214 74.82 5.80 3.800E+OO Line Not Found <<INT Reject 77 .11 9.70 4.028E+OO 2.485E+OO 2.486E+OO 28.90 OK 87.09 3.41 4.892E+OO Line Not Found <<INT Reject 242.00 7.25 4.727E+OO Line Not Found <<INT Reject 295.22 18.42 4.052E+OO 9.326E-01 9.330E-01 28.15 OK 351.93 35.60* 3.512E+00 7.685E-01 7.688E-01 27.69 OK RN-222 609.32 45.49* 2.255E+OO 6.677E-01 6.679E-01 26. 76 OK 1120.29 14.92 l.407E+OO 6.277E-01 6.279E-01 91. 79 OK 1764.49 15.30 9. 591E-01 7.932E-01 7.935E-01 41. 37 OK RA-224 240.99 4.10* 4. 731E+OO 3.453E-01 3.453E-01 292. 72 OK RA-226 609.32 45.49* 2.255E+OO 6.677E-01 6.679E-01 26. 76 OK 1120.29 14.92 l.407E+OO 6.277E-01 6.279E-01 91. 79 OK 1764.49 15.30 9.591E-01 7.932E-01 7.935E-01 41. 37 OK AC-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.624E+00 9.380E-01 9.380E-01 44.00 OK 794.95 4.25 1.834E+OO 4.858E-01 4.858E-01 215 .11 OK 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* 1.653E+OO 9.736E-01 9.736E-01 25.07 OK 968. 97 15.80 1. 576E+OO 7.468E-01 7.468E-01 41. 20 OK RA-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.624E+OO 9.380E-01 9.380E-01 44.00 OK 794.95 4.25 1.834E+OO 4.858E-01 4.858E-01 215 .11 OK 835.71 1. 61 1.766E+OO Line Not Found Absent 911.20 25.80* 1.653E+OO 9.736E-01 9.736E-01 25.07 OK 968.97 15.80 1. 576E+OO 7.468E-01 7.468E-01 41. 20 OK TH-228 74.82 10.28 3.825E+OO 6.676E-01 6.676E-01 104.28 OK 77 .11 17.10 4.028E+OO l.410E+OO 1.410E+OO 28.90 OK 238.63 43.60* 4.776E+OO 9.366E-01 9.366E-01 13.53 OK Page 3685 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235035 Acquisition date 3-0CT-2016 09:16:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09. 3.30 4.000E+OO 1.071E+OO 1.071E+OO OK TH-230 609.32 45.49* 2.255E+OO 6.677E-01 6.677E-01 26. 76 OK 1120.29 14.92 1.407E+OO 6.277E-01 6.277E-01 91. 79 OK 1764.49 15.30 9.591E-01 7.932E-01 7.932E-01 41. 37 OK PA-231 283.69 1. 70 4.183E+OO Line Not Found Absent 301.36 5.35* 4.000E+OO 6.604E-01 6.604E-01 100.50 OK TH-232 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.624E+OO 9.380E-01 9.380E-01 44.00 OK 835.71 1. 61 1.766E+OO Line Not Found Absent 911.20 25.80* 1.653E+OO 9.736E-01 9.736E-01 25.07 OK 968.97 15.80 1. 576E+OO 7.468E-01 7.468E-01 41.20 OK U-234 609.32 45.49* 2.255E+OO 6.677E-01 6.677E-01 26.76 OK 1120.29 14.92 1. 407E+OO 6.277E-01 6.277E-01 91.79 OK 1764.49 15.30 9.591E-01 7.932E-01 7.932E-01 41. 37 OK U-235 89. 96 3.47 5.083E+OO 1.587E+00 1.587E+OO 107.70 OK 93.35 5.60 5.355E+OO 1.203E+OO l.203E+OO 78.78 OK 143.76 10.96* 6.181E+OO Line Not Found Absent 163.33 5.08 5. 962E+OO 5.276E-01 5.276E-01 121.65 OK 185.72 57.20 5. 611E+OO 7.762E-02 7.762E-02 99.67 OK 205.31 5.01 5.295E+OO Line Not Found Absent AM-243 43.53 5.90 2.461E-01 Line Not Found Absent 74.66 67.20* 3.825E+00 l.021E-01 1.021E-01 104.28 OK ANH-511 511. 00 100.00* 2.593E+OO 4. 819E-02 4.819E-02 140.62 OK Flag: "*" = Keyline Page 3686 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:17:34.08 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * ' * * . DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l *
  • Acquisition date 3-0CT-2016 09:16:17 Sensitivity : 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:06:00 Analyst initials: MXRl *
  • Sample ID. G405235035 Sample Quantity 1.6407E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 * *Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.233E+01 1.369E+OO CD-109 9.559E-01 2.394E+OO SN-126 5.956E-02 l.492E-01 BA-137M 2.378E-02 5.812E-02 CS-137 2.512E-02 6.140E-02 CE-139 l.319E-01 l.510E-01 TL-208 2.253E-01 7.729E-02 BI-212 8.389E-01 5.778E-01 PB-212 9.366E-01 1.241E-01 BI-214 6.679E-01 1. 752E-01 PB-214 7.688E-01 2.086E-01 RN-222 6.679E-01 l.752E-01 RA-224 3.453E-01 9.906E-01 RA-22 6 6.679E-01 1. 752E-01 AC-228 9.736E-01 2.392E-01 RA-228 9.736E-01 2.392E-01 TH-228 9.366E-01 1. 241E-01 TH-230 6.677E-01 1. 751E-01 PA-231 6.604E-01 6.504E-01 TH-232 9.736E-01 2.392E-01 U-234 6.677E-01 1.751E-01 U-235 4. 831E-02 1.566E-01 AM-243 1. 021E-01 l.044E-01 ANH-511 4.819E-02 6.640E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3687 of 5809 Key-Line Activity (pCi/GRAM 2.251E+OO 1. 208E-02 0.000E+OO -l.033E-02 -8.621E-02 O.OOOE+OO K.L. Cnt Uncert ( 1 . 96-sigma ) 1.393E+Ol 3.855E-02 l.960E+41 1. 972E-02 3.710E-01 2.508E+04 MDA (pCi/GRAM 5.330E-01 1. 911E+OO l.198E-01 6.443E-02 6.806E-02 1.884E-01 6.325E-02 1. 017E+OO 8.057E-02 1.140E-01 1.131E-01 1.140E-01 8.635E-01 1.140E-01 1.926E-01 1.926E-01 8.057E-02 1.139E-01 7.170E-01 1.926E-01 1.139E-01 3. llOE-01 8.539E-02 4.704E-02 MDA (pCi/GRAM 2.804E+Ol 8.363E-02 O.OOOE+OO 3.617E-02 7.030E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 4.792E+02 O.OOOE+OO SHORT HLIF MN-54 3.984E-03 6. 251E-02 1.212E-01 NOT IDENT. C0-56 -1.071E-02 4.907E-01 9.465E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 4.350E-04 4.306E-02 7.707E-02 NOT IDENT. C0-58 7.502E-01 5.416E-01 1. 311E+OO NOT IDENT. FE-59 3.728E+OO 8.452E+OO 1. 799E+Ol NOT IDENT. C0-60 -1.357E-02 3. 719E-02 7.075E-02 NOT IDENT. ZN-65 6.778E-03 1.415E-01 2.661E-01 NOT IDENT. GE-68 2.070E+OO 2.329E+OO 5.264E+OO NOT IDENT. AS-73 -2.675E+OO 1.0lOE+Ol 2.023E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.073E+04 O.OOOE+OO SHORT HLIF SE-75 -8.750E-02 2.047E-01 3.577E-01 NOT IDENT. BR-77 O.OOOE+OO 1.823E+39 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 8. 272E+02 O.OOOE+OO SHORT HLIF RB-83 -7.747E-02 5.927E-01 1.167E+OO NOT IDENT. KR-85 5. 968E+OO 6.150E+OO 1.267E+Ol NOT IDENT. SR-85 7.378E-01 7.613E-01 1.568E+OO NOT IDENT. RB-86 O.OOOE+OO 4.446E+04 O.OOOE+OO SHORT HLIF Y-88 3.215E-02 2.316E-01 5.087E-01 NOT IDENT. Y-91 l.332E+02 5.795E+02 1.202E+03 NOT IDENT. NB-94 2.102E-02 3 .131E-02 6.092E-02 NOT IDENT. NB-95 1.323E-01 9.351E-01 1.693E+OO NOT IDENT. NB-95M 1. 782E+OO 2.459E+OO 4.848E+OO NOT IDENT. ZR-95 -2.318E-01 1.610E+OO 3.050E+OO NOT IDENT. NB-97 O.OOOE+OO 1.382E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 0. OO'OE+OO 7.175E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -9.528E-04 3.162E-02 5.582E-02 NOT IDENT. RH-102 3.375E-03 4.645E-02 9.395E-02 FAIL ABUN RU-103 2.025E-01 6.227E+OO 1.250E+Ol FAIL ABUN RH-106 -3.279E-01 4.390E-01 7.670E-01 NOT IDENT. RU-106 -3.279E-01 4.390E-01 7.670E-01 NOT IDENT. AG-108M -4.500E-03 2.260E-02 4.435E-02 NOT IDENT. AG-llOM 4.260E-02 8.491E-02 l.825E-01 FAIL ABUN SN-113 -2.090E-02 2.126E-01 4.222E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1. 735E+05 O.OOOE+OO SHORT HLIF TE-123M -2.574E-02 1.175E-01 2.185E-01 NOT IDENT. SB-124 l.221E+00 1.653E+OO 4.539E+OO FAIL ABUN SB-125 6.022E-02 1.0lOE-01 1. 967E-01 FAIL ABUN TE-125M 1.209E+02 2.995E+02 5.946E+02 NOT IDENT. I-126 O.OOOE+OO 1.922E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.329E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.768E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.576E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.305E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.843E+27* O.OOOE+OO SHORT HLIF BA-133 -9.869E-03 3.413E-02 5. 972E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3.225E-02 6.798E-02 9.161E-02 FAIL ABUN CS-135 -1.342E-02 l.440E-01 2.388E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.578E+05 O.OOOE+OO SHORT HLIF BA-140 O.OOOE+OO 2.224E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 8.643E+05 O.OOOE+OO SHORT HLIF CE-141 -l.916E+Ol 2.777E+Ol 4.947E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.256E+41 O.OOOE+OO SHORT HLIF CE-144 5.756E-02 2.980E-01 5.831E-01 NOT IDENT. PM-144 -4.602E-02 4.686E-02 7.668E-02 NOT IDENT. PR-144 -4.000E+OO 4.108E+OO 6.735E+00 NOT IDENT. PM-146 1.194E-02 3.579E-02 7.471E-02 NOT IDENT. ND-147 O.OOOE+OO 6.337E+07 O.OOOE+OO SHORT HLIF PM-147 4.642E+01 7 .112E+02 l.284E+03 NOT IDENT. PM-149 'O.OOOE+OO 9.353E+40 O.OOOE+OO SHORT HLIF EU-150 -6. 931E-03 2.125E-02 3.955E-02 FAIL ABUN EU-152 -1.637E-02 7.724E-02 1.458E-01 FAIL ABUN GD-153 . 2.156E-02 l.643E-01 2.997E-01 FAIL ABUN EU-154 3.822E-02 9.576E-02 2. 096E-01 NOT IDENT. EU-155 4.946E-02 1.059E-01 2 .114E-01 FAIL ABUN TB-160 8.292E-01 2.053E+OO 4.211E+OO FAIL ABUN H0-166M 2.036E-02 4.253E-02 9.148E-02 NOT IDENT. TM-171 2.748E-01 2.331E+Ol 4.782E+Ol NOT IDENT. HF:-172 1.131E-01 2.229E-01 4.148E-01 . FAIL ABUN LU-172 3.522E-02 6.618E-02 l.466E-01 FAIL ABUN LU-176 -9.939E-03 1.988E-02 3.838E-02 FAIL ABUN HF-181 -1.409E+OO 4.890E+OO 9.378E+OO NOT IDENT. Page 3688 of 5809 TA-182 -l.830E-03 8.743E-01 1. 762E+OO FAIL ABUN RE-183 -2.048E-01 3.389E+OO 6.845E+OO FAIL ABUN RE-184 -3.690E+OO 3.036E+Ol 5.885E+Ol NOT IDENT. W-188 -8.986E+Ol l.154E+02 l.901E+02 FAIL ABUN IR-192 8.661E-02 4.353E-01 8.989E-01 FAIL ABUN HG-203 -5.679E-01 2.352E+OO 4.686E+OO NOT IDENT. BI-207 1. 311E-02 4.401E-02 9.336E-02 FAIL ABUN PB-210 3.521E-01 4.807.E+OO 9.913E+OO NOT IDENT. BI-211 O.OOOE+OO 5.746E-01 7.122E-01 FAIL ABUN PB-211 2.560E-01 5.632E-01 l.182E+OO NOT RN-219 4.562E-02 2.849E-01 5.887E-01 FAIL ABUN RA-223 1.418E-02 4.697E-01 9.545E-01 FAIL ABUN AC-227 4.818E-02 2.123E-01 3. 996E-01 FAIL ABUN TH-227 4.818E-02 2.123E-01 3.996E-01 FAIL ABUN TH-229 -2.067E-01 4.153E-01 7.369E-01 FAIL ABUN TH-231 1.418E-02 4.697E-01 9.545E-01 FAIL ABUN PA-233 -2.122E-02 4.464E-02 8.664E-02 FAIL ABUN PA-23-4 1.512E-01 2.361E-01 5.108E-01 FAIL ABUN PA-234M 3.563E+OO 4 .139E+OO 9.064E+OO FAIL ABUN TH-234 8.427E-01 3.707E+OO 2.795E+OO FAIL ABUN NP-237 -2.122E-02 4.464E-02 8.664E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 8.427E-01 3.707E+OO 2.795E+OO FAIL ABUN NP-239 -6.923E-03 2. llOE-01 3.769E-01 NOT IDENT. PU-239 2 .. 999E+02 4.929E+02 5.588E+02 FAIL ABUN AM-241 l.337E-02 l.443E-01 2.730E-01 NOT IDENT. CM-243 -l.303E-02 9.263E-02 l.774E-01 NOT IDENT. .BK-247 -8.280E-03 6.511E-02 l.181E-01 FAIL ABUN CM-247 -5.190E-03 2.683E-02 5.300E-02 NOT IDENT. CF-249 -1. 475E-02 3.155E-02 6.008E-02 NOT IDENT. CF-251 -2.099E-02 9.731E-02 l.793E-01 NOT IDENT. Page 3689 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:17:31.58 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 326 10.66* l.134E+OO 1.233E+Ol 1.233E+Ol 11. 33 CD-109 88.03 58 3.70* 4.887E+OO l.455E+OO 2.335E+OO 103.28 SN-126 64.28 17 9.60 2.549E+OO 3.248E-01 3.248E-01 448.91 86.94 58 8.90 4.887E+OO 6.049E-01 6.049E-01 103.28 87.57 58 37.00* 4.887E+OO l.455E-01 l.455E-01 103.28 BA-137M 661. 66 10 89.90* 2 .115E+OO 2.331E-02 2.378E-02 249.44 CS-137 661. 66 10 85.10* 2 .115E+OO 2.462E-02 2.512E-02 249.44 CE-139 165.86 28 80.00* 5.922E+OO 2.700E-02 1.319E-01 116. 79 TL-208 277.37 ------6.60 4.258E+OO ------Line Not Found ------583.19 98 85.00* 2.334E+OO 2.253E-01 2.253E-01 35.00 860.56 20 12.50 1.727E+OO 4.197E-01 4.197E-01 81. 71 BI-211 72.87 ------1. 23 3. 591E+OO ------Line Not Found ------351.06 210 12.92* 3.512E+OO 2 .118E+OO 2 .118E+OO 27.69 BI-212 727. 33 24 6.67* 1. 965E+OO 8.389E-Ol 8.389E-01 70.29 785.37 17 1.10 1. 851E+OO 3.852E+OO 3.852E+OO 80.37 1620.50 ------1. 47 1.036E+00 ------Line Not Found ------PB-212 74.82 103 10.28 3.825E+OO l.194E+OO l.194E+OO 56.98 77 .11 212 17.10 4.028E+OO l.410E+OO l.410E+OO 28.90 238.63 426 43.60* 4.776E+00 9.366E-01 9.366E-01 13.53 300.09 31 3.30 4.000E+OO 1.071E+OO 1. 071E+OO 100.50 BI-214 609.32 150 45.49* 2.255E+OO 6.677E-01 6.679E-01 26.76 1120.29 29 14.92 1. 407E+OO 6.277E-01 6.279E-01 91.79 1764.49 25 15.30 9. 591E-01 7.932E-01 7.935E-01 41. 37 PB-214 74.82 103 5.80 3.825E+OO 2 .116E+OO 2. ll 7E+OO 56.98 77 .11 212 9.70 4.028E+OO 2.485E+OO 2.486E+OO 28.90 87.09 58 3.41 4.887E+OO l.579E+00 l.579E+OO 103.28 242.00 85 7.25 4.731E+OO l.128E+OO l.128E+OO 45.02 295.22 152 18.42 4.052E+00 9.326E-01 9.330E-01 28.15 351. 93 210 35.60* 3.512E+OO 7.685E-01 7.688E-01 27.69 RN-222 609.32 150 45.49* 2.255E+OO 6.677E-01 6.679E-01 26. 76 1120.29 29 14.92 l.407E+OO 6.277E-01 6.279E-01 91. 79 1764.49 25 15.30 9. 591E-01 7.932E-01 7.935E-01 41. 37 RA-224 240.99 85 4.10* 4.731E+OO l.994E+OO l.994E+OO 45.02 RA-22 6 609.32 150 45.49* 2.255E+OO 6.677E-01 6.679E-01 26. 76 1'120.29 29 14.92 l.407E+OO 6.277E-01 6.279E-01 91. 79 1764.49 25 15.30 9.591E-01 7.932E-01 7.935E-01 41. 37 AC-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 84 11. 27 3.624E+OO 9.380E-01 9.380E-01 44.00 794.95 8 4.25 l.834E+OO 4.858E-01 4.858E-01 215 .11 835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 91 25.80* l.653E+OO 9.736E-01 9.736E-01 25.07 968. 97 41 15.80 l.576E+OO 7.468E-01 7.468E-01 41. 20 RA-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 84 11. 27 3.624E+OO 9.380E-01 9.380E-01 44.00 794.95 8 4.25 l.834E+OO 4.858E-01 4.858E-01 215.11 835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 91 25.80* l.653E+OO 9.736E-01 9.736E-01 25.07 Page 3690 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235035 Acquisition date 3-0CT-2016 09:16:17 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968.97 41 15.80 1.576E+OO 7.468E-01 7.468E-01 41. 20 TH-228 74.82 103 10.28 3.825E+OO 1.194E+OO 1.194E+OO 56.98 77 .11 212 17.10 4.028E+OO 1.410E+OO 1.410E+OO 28.90 238.63 426 43.60* 4.776E+OO 9.366E-01 9.366E-01 13.53 300.09 31 3.30 4.000E+OO 1. 071E+OO 1. 071E+OO 100.50 TH-230 609.32 150 45.49* 2.255E+OO 6.677E-01 6.677E-01 26. 76 1120.29 29 14.92 1.407E+OO 6.277E-01 6.277E-01 91. 79 1764.49 25 15.30 9. 591E-01 7.932E-01 7.932E-01 41. 37 PA-231 283.69 ------1. 70 4.183E+OO ------Line Not Found ------301.36 31 5.35* 4.000E+OO 6.604E-01 6.604E-01 100.50 TH-232 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 84 11. 27 3.624E+OO 9.380E-01 9.380E-01 44.00 835. 71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 91 25.80* 1.653E+OO 9.736E-01 9.736E-01 25.07 968. 97 41 15.80 1.576E+OO 7.468E-01 7.468E-01 41.20 U-234 609.32 150 45.49* 2.255E+OO 6.677E-01 6.677E-01 26. 76 1120.29 29 14.92 1.407E+OO 6.277E-01 6.277E-01 91. 79 1764.49 25 15.30 9.591E-01 7.932E-01 7.932E-01 41. 37 U-235 89. 96 61 3.47 5.083E+OO 1.587E+OO 1.587E+OO 107.70 93.35 79 5.60 5.355E+OO 1.203E+OO 1.203E+00 78.78 143.76 ------10. 96* 6.181E+OO ------Line Not Found ------163.33 35 5.08 5.962E+OO 5.276E-01 5.276E-01 121. 65 185. 72 54 57.20 5. 611E+OO 7.762E-02 7.762E-02 99.67 205.31 ------5.01 5.295E+OO ------Line Not Found ------AM-243 43.53 ------5.90 2.461E-01 ------Line Not Found ------74.66 103 67.20* 3.825E+OO 1. 826E-01 1. 826E-01 56.98 ANH-511 511. 00 27 100.00* 2.593E+OO 4.819E-02 4.819E-02 140.62 Flag: "*" Key line Page 3691 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235035 Acquisition date 3-0CT-2016 09:16:17 Total number of lines in spectrum 50 Number of unidentified lines 8 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-139 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Hlife l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 137. 64D l.41E+l0Y 7.04E+08Y 1.41E+l0Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y 1.41E+10Y 1600.00Y l.41E+l0Y l.41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 61 1. 00 1. 02 1. 02 4.88 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.233E+Ol 1.455E+OO l.455E-01 2.331E-02 2.462E-02 2.700E-02 2.253E-01 2 .118E+OO 8.389E-01 9.366E-01 6.677E-01 7.685E-01 6.677E-01 1.994E+OO 6.677E-01 9.736E-01 9.736E-01 9.366E-01 6.677E-01 6.604E-01 9.736E-01 6.677E-01 7.762E-02 1.826E-01 4.819E-02 2.905E+Ol 2.905E+Ol Decay Corr pCi/GRAM 1.233E+Ol 2.335E+OO 1.455E-01 2.378E-02 2.512E-02 1.319E-01 2.253E-01 2 .118E+OO 8.389E-01 9.366E-01 6.679E-01 7.688E-01 6.679E-01 1.994E+OO 6.679E-01 9.736E-01 9.736E-01 9.366E-01 6.677E-01 6.604E-01 9.736E-01 6.677E-01 7.762E-02 1. 826E-01 4.819E-02 3.004E+Ol 3.004E+Ol 84.00% Decay Corr 2-Sigma Error 0.140E+Ol 2.412E+OO 1.503E-01 5.931E-02 6.265E-02 l.540E-01 0.789E-01 0.586E+OO 5.896E-01 1.267E-01 1.787E-01 2.129E-01 1. 787E-01 0.898E+OO 1.787E-01 2.441E-01 2.441E-01 1.267E-01 1.787E-01 6.637E-01 2.441E-01 1.787E-01 7.737E-02 1. 041E-01 6.776E-02 "M" Manually accepted 2-Sigma %Error 11. 33 103.28 103.28 249.44 249.44 116.79 35.00 27.69 70. 29 13.53 26. 76 27.69 26.76 45.02 26. 76 25.07 25.07 13.53 26. 76 100.50 25.07 26.76 99.67 56. 98 140.62 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3692 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235035 Acquisition date : 3-0CT-2016 09:16:17 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 40.90 29 118 1. 43 81. 97 76 8 5.54E-03 **** 1.12E-01 0 68.49 39 96 0.94 137.07 135 5 8.00E-03 95.7 3.09E+OO T 0 118. 51 37 87 0.92 236.98 234 7 7.98E-03 **** 6.14E+OO T 0 128.82 26 123 0.93 255 7 5.55E-03 **** 6.22E+OO T 0 154.68 25 46 1. 34 309.23 307 5 5.54E-03 **** 6.08E+OO T 0 209.48 89 101 1. 63 418.71 414 10 2.02E-02 52.7 5.23E+OO T 0 224.37 58 127 3.68 448.45 442 13 l.32E-02 93.3 4.99E+OO 0 270.13 58 77 1.19 539.87 535 10 1.35E-02 68.3 4.35E+OO T 0 424.65 24 15 0.87 848.63 845 7 5.80E-03 73.3 3. OlE+OO T 0 462.97 24 15 1. 05 925.21 922 7 6.02E-03 71. 2 2.81E+OO T 0 562 .17 19 8 1. 41 1123.47 1120 7 4.70E-03 71. 2 2.40E+OO T 0 597.97 16 32 0.57 1195. 04 1190 12 4.08E-03 **** 2.29E+OO 0 644.53 9 27 2.18 1288.12 1283 12 2. 31E-03 **** 2.16E+OO T 0 705.95 12 15 0.95 1410.91 1408 7 3.06E-03 **** 2. OlE+OO T 0 767.90 26 26 1.14 1534.78 1529 11 6.84E-03 87.8 1. 88E+OO T 0 806.45 7 13 1.17 1611. 85 1605 9 1. 95E-03 **** 1.82E+OO 0 821.53 18 5 3.01 1642.01 1637 11 4.86E-03 69.6 1. 7 9E+OO 3 965' 06 38 7 2.28 1929.05 1921 22 l.03E-02 44.8 1.58E+OO T 0 1137. 59 7 2 1. 41 2274.18 2271 7 1. 96E-03 98.5 1. 39E+OO 0 1378.42 14 5 1. 62 2756.10 2749 11 4.03E-03 81. 7 l.19E+OO 0 1406.85 10 0 1. 49 2813.00 2806 11 2.75E-03 71. 6 1.17E+OO T 0 1501.18 7 2 1. 36 3001.84 2998 7 2.0'4E-03 94.7 1. llE+OO Flags: "T" = Tentatively associated Page 3693 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:17:46.92 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * **
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l *
  • Acquisition date 3-0CT-2016 09:16:17 Sensitivity 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:06:00 Nuclide Library : SOLID *
  • Sample ID G405235035 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.6407E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-139 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 2.148E-01 8. 963E-01 5.620E-02 2.878E-02 3.041E-02 8.734E-02 2.839E-02 4.600E-01 3.713E-02 5.074E-02 5 .135E-02 5.074E-02 3.979E-01 5.074E-02 8.142E-02 8.142E-02 3.713E-02 5.072E-02 3.278E-01 8.142E-02 5. 072E-02 l.457E-01 4.003E-02 2.104E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3694 of 5809 Le (pCi/GRAM 1.265E+Ol 3.559E-02 O.OOOE+OO 1.143E-02 3.005E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-ll3 CD-ll5 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 3695 of 5809 5.335E-02 4. ll9E-01 O.OOOE+OO 3.571E-02 5.784E-01 7.941E+OO 2. 964E-02 l. ll5E-01 2.330E+OO 0.000E+OO l.633E-Ol O.OOOE+OO 0.000E+OO 5.130E-01 5.726E+OO 7.087E-01 O.OOOE+OO 2.019E-01 5.251E+02 2. 729E-02 7.441E-01 2.258E+OO l.339E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.602E-02 4.085E-02 5.553E+OO 3. 3llE-Ol 3. 3llE-01 l.975E-02 7.885E-02 l.904E-01 0.000E+OO O.OOOE+OO l.OlOE-01 l.777E+OO 8.936E-02 2.786E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.667E-02 0.000E+OO 4.039E-02 l.lOOE-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.289E+Ol O.OOOE+OO 2.707E-01 3.257E-02 2.862E+OO 3.347E-02 O.OOOE+OO 5.942E+02 O.OOOE+OO 1. 789E-02 6.575E-02 l.394E-01 8. 968E-02 9.952E-02 1. 851E+OO 3.983E-02 2.207E+Ol l.943E-01 6.369E-02 1. 741E-02 4.180E+OO 7.619E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL AB.UN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3696 of 5809 3.169E+OO 2.465E+Ol 8.598E+Ol 4.098E-01 2.138E+OO 4.081E-02 4.604E+OO 3.419E-01 5.360E-01 *2.631E;-01 4.337E-01 1.846E-01 1.846E-01 3. 411E-01 4.337E-01 3.894E-02 2.226E-01 4.043E+OO 1. 322E+OO 3.894E-02 O.OOOE+OO 1.322E+OO 1. 746E-01 2.624E+02 1.268E-01 8.303E-02 5.409E-02 2.364E-02 2.700E-02 8.297E-02 FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:17:52.20 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235035.CNF;l * *Acquisition date 3-0CT-2016 09:16:17 Sensitivity : 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:06:00 Nuclide Library : SOLID *
  • Sample ID G405235035 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.6407E+02 GRAM *
  • Quantity Err(%) : 1.2190E-03 % * *Wet wt corr 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 1. 233E+Ol 1.512E+OO CD-109 9.559E-01 2.402E+OO SN-126 5.956E-02 1. 496E-01 BA-137M 2.378E-02 5. 813E-02 CS-137 2.512E-02 6 .141E-02 CE-139 l.319E-01 l.533E-01 TL-208 2.253E-01 7.787E-02 BI-212 8.389E-01 5.794E-01 PB-212 9.366E-01 1.336E-01 BI-214 6.679E-01 1.775E-01 PB-214 7.688E-01 2. llOE-01 RN-222 6.679E-01 1.775E-01 RA-224 3.453E-01 9. 966E-01 RA-226 6.679E-01 l.775E-01 AC-228 9.736E-01 2.443E-01 RA-228 9.736E-01 2.443E-01 TH-228 9.366E-01 1. 336E-01 TH-230 6.677E-01 1.774E-01 PA-231 6.604E-01 6.655E-01 TH-232 9.736E-01 2.443E-01 U-234 6.677E-01 1.774E-01 U-235 4. 831E-02 1.566E-01 AM-243 l.021E-01 l.051E-01 ANH-511 4.819E-02 6.643E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3697 of 5809 Key-Line Activity (pCi/GRAM 2.251E+OO 1.208E-02 l.OOOE+41 -1.033E-02 -8.621E-02 -1.048E+04 K.L Act error ( 1 . 96-sigma ) 1.393E+Ol 3.855E-02 7.360E+41 1. 97 3E-02 3.710E-01 2.509E+04 TPU ( 1. 96-sigma) 1. 512E+OO 2.402E+OO l.496E-01 5.813E-02 6.141E-02 1.533E-01 7.787E-02 5.794E-01 1.336E-01 1. 775E-01 2. llOE-01 1. 775E-01 9. 966E-01 1. 775E-01 2.443E-01 2.443E-01 1.336E-01 1.774E-01 6.655E-01 2.443E-01 1.774E-01 1.566E-01 1.051E-01 6.643E-02 TPU ( 1 . 96-sigma) 1. 396E+Ol 3.893E-02 O.OOOE+OO 2.027E-02 3.730E-01 2.553E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -4.693E+02 4.796E+02 5.242E+02 SHORT HLIF MN-54 3.984E-03 6. 251E-02 6.254E-02 NOT IDENT. C0-56 -1. 071E-02 4.907E-01 4.907E-01 NOT IDENT. MN-56 -l.OOOE+41 3.439E+42 O.OOOE+OO SHORT HLIF C0-57 4.350E-04 4.306E-02 4.306E-02 NOT IDENT. C0-58 7.502E-01 5.425E-01 6.393E-01 NOT IDENT. FE-59 3. 728E+OO 8.456E+OO 8.622E+OO NOT IDENT. C0-60 -1.357E-02 3.719E-02 3.769E-02 NOT IDENT. ZN-65 6.778E-03 l.415E-01 l.415E-01 NOT IDENT. GE-.68 2.070E+OO 2.330E+00 :2.510E+OO NOT IDENT. AS-73 -2.675E+OO 1. OllE+Ol l.018E+Ol NOT IDENT. AS-74 2.573E+03 l.073E+04 l.079E+04 SHORT HLIF SE-75 -8.750E-02 2.048E-01 2.086E-01 NOT IDENT. BR-77 l.376E+40 1.251E+41 O.OOOE+OO SHORT HLIF SR-82 l.210E+Ol 8.272E+02 8. 272E+02 SHORT HLIF RB-83 -7.747E-02 5.928E-01 5.938E-01 NOT IDENT. KR-85 5. 968E+OO 6.155E+OO 6.717E+OO NOT IDENT. SR-85 7.378E-01 7.619E-01 8.314E-01 NOT IDENT. RB-86 4.167E+04 4.450E+04 4. 831E+04 SHORT HLIF Y-88 3.215E-02 2.316E-01 2. 321E-01 NOT IDENT. Y-91 l.332E+02 5.795E+02 5.826E+02 NOT IDENT. NB-94 2.102E-02 3.132E-02 3. 272E-02 NOT IDENT. NB-95 1.323E-01 9.351E-01 9.370E-01 NOT IDENT. NB-95M 1.782E+OO 2.463E+OO 2. 591E+OO NOT IDENT. ZR-95 -2.318E-01 1.610E+OO 1.614E+OO NOT IDENT. NB-97 l.OOOE+41 l.383E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 2.944E+42 O.OOOE+OO SHORT HLIF M0-99 -4.416E+33 7.182E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 8.984E+41 O.OOOE+OO SHORT HLIF RH-101 -9.528E-04 3.162E-02 3.162E-02 NOT IDENT. RH-102 3.375E-03 4.645E-02 4.648E-02 FAIL ABUN RU-103 2.025E-01 6.227E+OO 6.227E+00 FAIL ABUN RH-106 -3.279E-01 4.394E-01 4.636E-01 NOT IDENT. RU-106 -3.279E-01 4.394E-01 4.636E-01 NOT IDENT. AG-108M -4.500E-03 2.260E-02 2.269E-02 NOT IDENT. AG-llOM 4.260E-02 8.494E-02 8.708E-02 FAIL ABUN SN-113 -2.090E-02 2.126E-01 2.128E-01 NOT IDENT. CD-115 5.774E+40 2.786E+41 O.OOOE+OO SHORT HLIF SN-ll 7M -6. 967E+04 1. 737E+05 1. 765E+05 SHORT HLIF TE-123M -2.574E-02 1.175E-01 1.181E-01 NOT IDENT. SB-124 1.221E+OO 1.654E+OO 1.743E+OO FAIL ABUN SB-125 6.022E-02 1.0lOE-01 l.046E-01 FAIL ABUN TE-125M 1.209E+02 2. 996E+02 3.045E+02 NOT IDENT. I-126 -1.058E+06 l.927E+06 l.986E+06 SHORT HLIF SB-126 -5.671E+05 2.332E+06 2.346E+06 SHORT HLIF SB-127 8.054E+22 3.002E+23 O.OOOE+OO SHORT HLIF I-131 -7.539E+09 1. 57 6E+10 l.613E+l0 SHORT HLIF I-132 -1.000E+41 1.946E+42 O.OOOE+OO SHORT HLIF TE-132 -3.492E+27 9.955E+27 0.000E+OO SHORT HLIF BA-133 -9.869E-03 3.413E-02 3.442E-02 NOT IDENT. I-133 l.OOOE+41 3.751E+41 O.OOOE+OO SHORT HLIF CS-134 3.225E-02 6.799E-02 6.953E-02 FAIL ABUN CS-135 -l.342E-02 1. 440E-01 1.441E-01 NOT IDENT. I-135 -1.000E+41 2.184E+42 O.OOOE+OO SHORT HLIF CS-136 -3.336E+05 4.593E+05 4.833E+05 SHORT HLIF BA-140 3.406E+05 2.224E+06 2.230E+06 SHORT HLIF LA-140 -1. 7 52E+05 8.643E+05 8.679E+05 SHORT HLIF CE-141 -1.916E+Ol 2.778E+Ol 2.910E+Ol NOT IDENT. CE-143 1.000E+41 1. 2 61E+41 O.OOOE+OO SHORT HLIF CE-144 5.756E-02 2.981E-01 2.992E-01 NOT IDENT. PM-144 -4.602E-02 4.695E-02 5.133E-02 NOT IDENT. PR-144 -4.000E+OO 4. lllE+OO 4.489E+OO NOT IDENT. PM-146 1.194E-02 3.580E-02 3.620E-02 NOT IDENT. ND-147 -2. 038E+o7 6.338E+07 6.404E+07 SHORT HLIF PM-147 4.642E+Ol 7 .113E+02 7 .116E+02 NOT IDENT. PM-149 -1. OOOE+41 9.623E+40 0.000E+OO SHORT HLIF EU-150 -6. 931E-03 2.125E-02 2.148E-02 FAIL ABUN EU-152 -1.637E-02 7. 725E-02 7.760E-02 FAIL ABUN GD-153 2.156E-02 l.643E-01 1. 646E-01 FAIL ABUN EU-154 3.822E-02 9.577E-02 9.731E-02 NOT IDENT. EU-155 4.946E-02 l.060E-01 l.083E-01 FAIL ABUN TB-160 8.292E-01 2.054E+OO 2.087E+OO FAIL ABUN H0-166M 2.036E-02 4.254E-02 4.352E-02 NOT IDENT. TM-171 2.748E-01 2. 331E+Ol 2.331E+Ol NOT IDENT. HF-172 1.131E-01 2.236E-01 2.294E-01 FAIL ABUN LU-172 3.522E-02 6.628E-02 6.816E-02 FAIL ABUN LU-176 -9.939E-03 1. 989E-02 2.039E-02 FAIL ABUN HF-181 -1.409E+00 4.890E+OO 4.931E+OO NOT IDENT. Page 3698 of 5809 TA-182 -l.830E-03 8.743E-01 8.743E-01 FAIL ABUN RE-183 -2.048E-01 3.389E+OO 3.391E+OO FAIL ABUN RE-184 -3.690E+00 3.038E+Ol 3.042E+Ol NOT IDENT. W-188 -8.986E+Ol 1.158E+02 l.227E+02 FAIL ABUN IR-192 8.661E-02 4.353E-01 4.371E-01 FAIL ABUN HG-203 -5.679E-01 2.352E+OO 2.366E+OO NOT IDENT. BI-207 1. 311E-02 4.401E-02 4.441E-02 FAIL ABUN PB-210 3.521E-01 4.807E+OO 4.809E+OO NOT IDENT. BI-211 2 .118E+OO 5.822E-01 l.118E+OO FAIL ABUN PB-211 2.560E-01 5.633E:-Ol 5.750E-01 NOT .IDENT. RN-219 4.562E-02 2.850E-01 2.857E-01 FAIL ABUN RA-223 l.418E-02 4.697E-01 4.697E-01 FAIL ABUN AC-227 4. 818E-02 2.124E-01 2.135E-01 FAIL ABUN TH-227 4.818E-02 2.124E-01 2.135E-01 FAIL ABUN TH-229 -2.067E-01 4.154E-01 4.257E-01 FAIL ABUN TH-231 1.418E-02 4.697E-01 4.697E-01 FAIL ABUN PA-233 -2.122E-02 4.465E-02 4.566E-02 FAIL ABUN PA-234 l.512E-01 2.927E-01 3.005E-01 FAIL ABUN PA-234M 3.563E+OO 4 .141E+OO 4.442E+OO FAIL ABUN TH-234 8.427E-01 3.712E+OO 3.731E+OO *FAIL ABUN NP-237 -2.122E-02 4.465E-02 4.566E-02 FAIL ABUN NP-238 -1.000E+41 4.750E+41 0.000E+OO SHORT HLIF U-238 8.427E-01 3.712E+OO 3. 731E+OO FAIL ABUN NP-239 -6.923E-03 2. llOE-01 2. llOE-01 NOT IDENT. PU-239 2.999E+02 4.931E+02 5 .113E+02 FAIL ABUN AM-241 1.337E-02 1.443E-01 1.444E-01 NOT IDENT. CM-243 -1.303E-02 9.264E-02 9.282E-02 NOT IDENT. BK-247 -8.280E-03 6.513E-02 6.524E-02 FAIL ABUN CM-247 -5.190E-03 2.685E-02 2.695E-02 NOT IDENT. CF-249 -1.475E-02 3.157E-02 3.227E-02 NOT IDENT. CF-251 -2.099E-02 9.734E-02 9.780E-02 NOT IDENT. Page 3699 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 43.6508 87.09 76.6525 136.47 51.5361 45.60 51.7159 87.57 76.7138 140.51 0.0000 46.54 55.6064 88.03 76.7721 143.76 50.8881 49. 72 0.0000 88.34 76.8113 144.24 46.4899 51. 35 45.7623 88.47 76.8276 145.44 66.5085 51.87 46. 7719 89. 96 77.0153 152.43 61.0929 52.39 47.7835 1093.63 77.1000 153.25 0.0000 52.97 46.8899 91.11 0.0000 323.87 45.9129 53.44 45.9820 92.59 77.3426 156.02 0.0000 54.07 45.0879 93.35 77.4359 158.56 0.0000 57.36 0.0000 94.56 77.5846 159.00 55.1691 57.53 49.2998 94.65 77.5955 162.33 57.2567 57.98 53.2179 94.67 77.5978 162.66 0.0000 59.27 55.6287 94.87 77.6224 163.33 54.3025 59.32 55.6346 97.43 54.0332 165.86 54.4526 59.54 55.6604 98.43 58.2794 176.31 51.6193 60. 96 63.6164 98.44 58.2802' 176.60 0.0000 61.17 66.2421 99.53 67.7597 177.52 56.2779 62.93 69.0899 100 .11 67.8193 181.07 0.0000 63.29 69.1408 102.03 71.1553 181.52 62.2760 63.58 69.1815 103.18 74.4218 184.41 55.5190 ,64. 28 69.2794 103.37 74.4430 143.76 50. 9596 66.73 70.9321 105.21 74.6461 193.51 63.0258 67.24 71. 0030 105.31 74.6569 197.03 57.3852 125.81 71.0640 106.12 82 .1148 198.01 64.4733 67.75 71. 0739 106.47 92.6896 201. 83 65.8848 69.67 87.1917 109.28 60.2820 203.43 60.0932 70.83 65.5383 111. 00 71. 0316 205.31 55.0848 72. 81 74.7528 111.76 0.0000 210.85 33.2209 72. 87 74.7614 114. 06 61. 7551 215.65 48.8589 74.66 75.0086 116. 30 0.0000 222 .11 49.1423 74.82 75.0309 116.74 54.1476 227.09 49.7594 74.97 75.0515 119.76 55. 8011 227.38 48.1665 77 .11 75.3433 121.12 44.4360 228.16 0.0000 78.74 64.4800 121. 22 50.1765 228.18 51.4134 79.69 76.6987 121.78 50. 2139 116. 74 51.4134 80.12 79.4499 122.06 53.1032 235.69 46.0872 80.19 0.0000 122.92 63.5810 235.96 46.0980 80.57 63.3403 123.07 63.5936 238.63 46.2023 81. 00 55.2956 265.00 66.8811 238.98 0.0000 81. 07 55.3023 125.81 60.5784 240.99 46.2939 81. 75 85.0773 127.23 63.5801 242.00 46.3334 83.79 93.5070 127.91 67.9749 244.70 24.4406 84.00 93.5400 129.30 61.9384 252.40 0.0000 85.43 76.4402 131.20 56.6433 252.80 44.2864 86.55 76.5839 133.02 42.5801 254.15 0.0000 86.79 76.6142 133.52 52.4392 256.23 44.4089 86.94 76.6336 136.00 63.5605 260.90 0.0000 Page 3700 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 44.7067 355.39 0.0000 584.27 10.4462 264.80 42.2281 356.01 27.8092 595.83 0.0000 265.00 42.2344 364.49 0.0000 427.87 18.0359 268.22 48.1516 366.42 0.0000 602.52 0.0000 269.46 41.1352 372.51 22.2992 604. 72 22.5842 270.03 41.1533 375.05 33.9473 607.14 15. 0720 271.23 41.6077 377.52 27.7355 609.32 22.1262 273.65 0.0000 356.01 34.1290 610.33 22.1352 276.40 45.9497 388.16 33.3167 614.28 16.6296 277.37 47.6554 388.63 0.0000 618.01 17.1605 277.60 47.6635 391.69 29.7773 620. 36 14.1458 278.00 35. 9681 264.66 20.8634 621.93 22.2444 279.20 40.1865 401.81 21.7847 630.19 0.0000 279.54 43.5470 402.40 25.4246 631.29 14.2108 279.70 41.0397 404.85 25.4604 633.25 16.2539 280.46 35.1965 410.95 31.0249 634.78 0.0000 283.69 34.4419 413.71 31.0733 635.95 12.2041 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 36.1684 423.72 0.0000 645.85 12.2534 285.90 0.0000 427.09 24.8621 657.76 15.3906 287.50 25. 2728 427.87 23.4912 657.90 0.0000 290.67 44.3311 433.94 24.9565 661.66 23.6364 293.27 0.0000 439.40 21.3224 664.57 0.0000 351. 93 27.9579 453.88 20.5547 666.33 0.0000 295. 96 27.9727 463.37 16.9017 666.50 0.0000 879.38 20.3823 468.07 22.5908 667. 71 0.0000 299.98 30.6042 473.00 0.0000 677.62 16.5469 300.09 30.6072 475.06 23.6170 685.70 0.0000 300.13 30.6079 476.78 25.5289 695.00 0.0000 301.36 38.2938 477.60 26.4858 696.49 21. 8776 302.85 38.3340 482.18 26.5474 696. 51 21. 8776 256.23 28.1445 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.5896 306.78 40.1497 497.08 21. 0153 697.49 14.5907 308.46 30.7896 505.52 23.0215 702.65 15 .. 6635 311. 90 33.4355 507.63 0.0000 706.68 14 .1191 316.51 32.6825 511. 00 24.0448 711.68 10.4781 319.41 0.0000 514.00 15.8924 720.70 0.0000 320.08 0.0000 514.00 15.8924 721. 93 0.0000 321. 04 30.1963 520.40 19.3229 722.78 26.5156 323.87 32.8480 520.69 0.0000 722. 91 26.5166 325.23 32.8781 522.65 0.0000 723. 31 20.5220 328.76 0.0000 527.90 0.0000 724.19 15.7916 333.37 34.7982 528.26 17.4565 727.33 30.0389 333.97 35.5083 529.59 15.5267 733.00 20.0677 334.37 30.0331 529.87 0.0000 735.93 15.8600 338.28 32.2929 531.02 0.0000 333.97 12.6953 338.32 32.2937 537.26 0.0000 739.50 0.0000 311. 90 26.2213 546.56 0.0000 747.24 15.9259 340.48 26.2213 552.55 10.7892 748.06 7.4344 340.55 0.0000 563.25 19.2191 752.31 24.4646 344.28 31.5439 569.33 19.7664 753.82 0.0000 345.93 30.2619 946.00 19.7681 756.73 19.1770 351. 06 32.5617 569.70 18.7812 756.80 19.1777 351.93 32.5798 583.19 25.8551 884.68 16.0223 Page 3701of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 7 65. 81 14.4300 1274.44 11. 5108 1620.50 3.0031 766.42 22.4509 1001.03 9.2214 1621. 92 8.0103 766.84 22.4543 1002.74 16.1453 1678.03 0.0000 772. 60 0.0000 1004.73 13.8467 1690.97 1. 0148 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 1025.87 0.0000 1764.49 1.0287 778.90 8.5908 1028.54 0.0000 1063.66 7.2089 783.70 0.0000 1037.84 10.4839 1771.35 3.0901 785.37 11. 3011 1038.76 0.0000 1791.20 0.0000 792.07 17.8005 631.29 10.5095 1808.65 3 .1111 794.95 16.1981 1048.07 0.0000 1810.72 0.0000 795.86 8.1018 1049.04 10.5168 1836.06 4.1685 810.06 11. 7237 1050.41 7.8904 810.29 10.4219 1063.66 12.3192 344.28 8.6852 1077.00 0.0000 810.76 5.4289 1077.34 10.5989 815.77 0.0000 1085.87 9.7385 1048.07 0.0000 1093.63 9.7586 832.01 12.0299 1099.45 14.2168 834.85 17.5143 1112. 07 13.3731 835.71 17.5195 1112. 84 14.2676 836.80 0.0000 1115. 54 8.5670 846.75 0.0000 1120.29 15.1894 846.77 15.3860 1120*. 55 15.1904 856.80 0.0000 1221. 41 15.1935 860.56 8.8319 1129. 67 10.7490 871.09 11. 077 5 1131.51 0.0000 873.19 14.4108 1147.95 0.0000 875.33 0.0000 1173.23 7.2471 879.38 13.3286 1177.95 10.8838 880.51 8.8890 1189.05 10.9146 883.24 17.7936 1204.77 13.6972 884.68 8.9007 1221.41 13.7540 889.28 12.2568 1231. 02 18.3826 894.76 13.3940 1235.36 0.0000 898.04 12.2909 1238.28 11.9701 900.72 14.5377 1260.41 0.0000 903.28 10.0726 1271. 87 10. 2111 911.20 10.0975 1274.44 8.3595 912.08 10.1005 1274.54 8.3595 923.98 0.0000 1291.59 6.5283 926.50 6.7637 1298.22 0.0000 929 .11 11. 2821 1312 .11 0.0000 937.49 18.0977 1332. 49 12.2407 944.13 0.0000 1362.66 O.QOOO 946.00 9.0723 1365.19 6.6403 949.00 13.6206 1368.63 0.0000 667.71 0.0000 1384.29 2.8581 962.31 5.1282 1408.01 4.5973 964.08 4.5609 1457.56 0.0000 966 .17 4.5636 1460.82 5.8129 911. 20 4.5674 1489.16 3.8984 968.97 4.5674 1505.03 10.9525 983.53 0.0000 1584.12 7.9507 984.45 0.0000 1596.21 0.0000 Page 3702 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:18:21.50 ********************************************************************************
  • GEL LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : Z-OCT-2016 11:02:08. Sample date 23-NOV-2015 11:12:00 Acquisition date : 3-0CT-2016 09:16:44. Sample ID G405235036 Sample quantity 1.62257E+02 GRAM Detector name : GAM36 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.33 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 *3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 1 1 0 0 0 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 5 0 0 0 0 0 0 0 0 0 0 4 4 0 Energy 74.95* 77.10* 87.19 92.82* 137.93 147.89 186.09* 209.98 238.63* 241. 61 245.61 270.50 295.45* 300.31 305.63 338.51 349.45 351.99* 409.99 464.25 515.57 538.68 543.65 562. 29 583.75* 603.12 609.47* 727.30 900.61 905.40* 911. 55* 966 .14 969 .14 1120.69* Page 3703 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 71 142 70 40 30 22 42 24 256 71 22 26 90 32 10 46 10 137 19 11 16 12 22 8 59 15 106 22 13 10 50 9 15 27 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 98 98 103 128 71 44 106 77 31 38 30 49 58 41 29 66 21 33 22* 35 12 36 7 1 34 8 8 11 0 2 5 7 7 8 0.87 0.93 1. 37 1. 50 1.27 0.75 0.86 1. 49 0.93 1. 78 1.35 0.77 1. 08 0.59 1. 40 1. 85 1.16 1.28 1. 70 1.29 2.21 5.95 2.36 0.71 1.17 1. 84 1. 28 0.77 0.83 2.72 2.04 1. 83 1. 68 2.39 149.88 154.17 174.36 185.62 275.85 295.77 372 .16 419.94 477.25 483.20 491.21 540.98 590.88 600.60 611. 24 677.00 698.88 703.96 819.95 928.46 1031.10 1077.29 1087.24 1124.52 1167. 42 1206.16 1218.86 1454.47 1801. 00 1810.56 1822.86 1932.00 1938.00 2240.98 146 146 172 182 272 293 367 414 472 472 488 536 585 597 606 669 692 700 815 923 1014 1062 1083 1123 1161 1200 1214 1450 1797 1806 1818 1930 1930 2233 12 1.98E-02 23.6 1.27E+OO 12 3.93E-02 14.4 7 1.94E-02 26.7 8 1. llE-02 54. 0 8 8.20E-03 53.0 6 6.02E-03 53.8 10 l.16E-02 50.7 10 6. 72E-03 71. 0 16 7.12E-02 7.4 1.08E+OO 16 1. 96E-02 21. 3 7 6.llE-03 46.4 8 7. llE-03 51. 7 12 2.50E-02 20.3 10 8.89E-03 41.l 9 2.64E-03112.4 14 1.27E-02 40.7 8 2.79E-03 86.2 10 3. 81E-02 11. 6 10 5.20E-03 52.7 12 2.99E-03112.0 22 4.52E-03 57.1 1.07E+OO 18 3. 45E-03116. 7 10 6. 09E-03 31. 5 5 2.13E-03 45.4 13 1.65E-02 24.2 11 4.16E-03 45.1 11 2. 95E-02 11. 5 10 6.19E-03 34.2 8 3.61E-03 27.7 9 2.72E-03 45.1 10 1.39E-02 17.0 12 2.62E-03 42.8 1.71E+OO 12 4.25E-03 44.3 16 7.60E-03 30.5 Peak Search Report (continued) Sample ID : G405235036 Pk It Energy Area Bkgnd 35 0 1280.68* 5 9 36 0 12 91.10 7 2 . 37 0 1461. 09* 164 7 FWHM 0.47 1. 38 06 Acquisition date Channel Left Pw 2560.83 2554 9 2581.65 2578 7 2921.44 2914 13 Page : 2 3-0CT-2016 09:16:44 Cts/Sec %Err Fit 1.52E-03109.5 2.0lE-03 48.1 4.57E-02 8.5 Flag: "*" = Peak area was modified by background subtraction Page 3704of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:18:23 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 23-NOV-2015 11:12:00 G405235036 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:16:44 162.26 GRAM Sample type .: Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3705of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351. 06
  • CAN 0 01:00:00.33 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235036 Acquisition date 3-0CT-2016 09:16:44 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 6.546E-01 1.060E+Ol 1.060E+Ol 17.07 OK CD-109 88.03 3.70* 4.292E+OO l.850E+OO 2.970E+OO 80.29 OK SN-126 64.28 9.60 2.567E+OO Line Not Found Absent 86.94 8.90 4.292E+OO 7.693E-01 7.693E-01 80.29 OK 87.57 37.00* 4.292E+OO l.850E-01 1.850E-01 80.29 OK TL-208 277.37 6.60 3.041E+OO Line Not Found Absent 583.19 85.00* 1.495E+OO 2.349E-01 2.349E-01 48.40 OK 860.56 12.50 1.058E+OO Line Not Found Absent PB-212 74.82 10.28 3.493E+OO 7.135E-01 7 .135E-01 87.15 OK 77 .11 17.10 3.655E+OO 1.410E+OO 1.410E+OO 28.78 OK 238.63 43.60* 3.499E+OO 9.340E-01 9.340E-01 14. 72 OK 300.09 3.30 2.817E+OO 1.868E+OO 1. 868E+OO 82.17 OK BI-214 609.32 45.49* 1.437E+OO 8.142E-01 8.145E-01 22.99 OK 1120. 29 14.92 8.369E-01 l.019E+00 1.019E+OO 60.99 OK 1764.49 15.30 5.419E-01 Line Not Found Absent PB-214 74.82 5.80 3.482E+OO Line Not Found <<INT Reject 77 .11 9.70 3.655E+OO 2.485E+OO 2.486E+OO 28.78 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 3.455E+OO Line Not Found <<INT Reject 295.22 18.42 2.862E+OO 9.287E-01 9.290E-01 40.66 OK 351. 93 35.60* 2.414E+OO 8.501E-01 8.504E-01 23.27 OK RN-222 609.32 45.49* 1.437E+OO 8.142E-01 8.145E-01 22.99 OK 1120. 29 14.92 8.369E-01 l.019E+OO l.019E+00 60.99 OK 1764.49 15.30 5.419E-01 Line Not Found Absent RA-224 240.99 4.10* 3.460E+OO 1.123E+OO 1.123E+OO 120.72 OK RA-226 609.32 45.49* 1.437E+OO 8.142E-01 8.145E-01 22.99 OK 1120.29 14.92 8.369E-01 1.019E+OO 1.019E+OO 60.99 OK 1764.49 15.30 5.419E-01 Line Not Found Absent AC-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.507E+OO 8.644E-01 8.644E-01 81. 42 OK 794.95 4.25 1.134E+OO Line Not Found Absent 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 OK 968.97 15.80 9.524E-01 4.816E-01 4.816E-01 88.69 OK RA-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.507E+OO 8.644E-01 8.644E-01 81. 42 OK 794.95 4.25 l.134E+OO Line Not Found Absent 835.71 1. 61 l.085E+OO Line Not Found Absent 911.20 25.80* 1.005E+00 9.219E-01 9.219E-01 34.07 OK 968.97 15.80 9.524E-01 4.816E-01 4.816E-01 88.69 OK TH-228 74.82 10.28 3.493E+OO 7.135E-01 7.135E-01 87.15 OK 77 .11 17.10 3.655E+OO 1.410E+OO l.410E+00 28.78 OK 238.63 43.60* 3.499E+OO 9.340E-01 9.340E-01 14.72 OK 300.09 3.30 2.817E+OO 1. 868E+OO 1.868E+OO 82.17 OK TH-230 609.32 45.49* l.437E+OO 8.142E-01 8.142E-01 22.99 OK 1120.29 14.92 8.369E-01 1.019E+OO 1.019E+OO 60.99 OK 1764.49 15.30 5.419E-01 Line Not Found Absent PA-231 283.69 1. 70 2.976E+OO Line Not Found Absent 301.36 5.35* 2.817E+OO 1.152E+OO 1.152E+OO 82.17 OK Page 3706 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235036 Acquisition date Nuclide Type: Nuclide Z'H-232 U-234 AM-243 Energy 105.21 338.32 835. 71 911.20 968. 97 609.32 1120.29 1764.49 43.53 74.66 Flag: "*" = Keyline Page 3707 of 5809 %Abn 1.10 11. 27 1. 61 25.80* 15.80 45.49* 14.92 15.30 5.90 67.20* Uncorrected Decay Corr %Eff pCi/GRAM pCi/GRAM 4.933E+OO -----. Line Not Found 2.507E+OO 8.644E-01 8.644E-01 1.085E+OO Line Not Found 1.005E+OO 9.219E-01 9.219E-01 9.524E-01 4.816E-01 4.816E-01 1.437E+OO 8.142E-01 8.142E-01 8.369E-01 1.019E+OO 1.019E+OO 5.419E-01 Line Not Found 5.957E-01 Line Not Found 3.493E+OO l.091E-01 1.092E-01 Page : 3 3-0CT-2016 09:16:44 2-Sigma %Error Status Absent 81. 42 OK Absent 34.07 OK 88.69 OK 22.99 OK 60.99 OK Absent Absent 87-.15 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:18:24.60 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* ** * * ' DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l *
  • Acquisition date 3-0CT-2016 09:16:44 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:12:00 Analyst initials: MXRl *
  • Sample ID G405235036 Sample Quantity l.6226E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File :* DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 l.060E+Ol 1. 773E+OO 7.126E-01 CD-109 2.970E+OO 2.337E+OO 2. 096E+OO SN-126 l.850E-01 l.456E-01 l.313E-01 TL-208 2.349E-01 l .114E-01 5.556E-02 PB-212 9.340E-01 1. 347E-01 9.819E-02 BI-214 8.145E-01 l.835E-01 l.360E-01 PB-214 8.504E-01 l.939E-01 l.167E-01 RN-222 8.145E-01 l.835E-01 l.360E-01 RA-224 l.123E+OO 1. 329E+OO l.054E+OO RA-226 8.145E-01 l.835E-01 l.360E-01 AC-228 9.219E-01 3.078E-01 2.486E-01 RA-228 9.219E-01 3.078E-01 2.486E-01 TH-228 9.340E-01 l.347E-01 9.819E-02 TH-230 8.142E-01 l.835E-01 1. 359E-01' PA-231 l.152E+00 9.281E-01 6.582E-01 TH-232 9.219E-01 3.078E-01 2.486E-01 U-234 8.142E-01 l.835E-01 l.359E-01 AM-243 l.092E-01 9.322E-02 8.170E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -l.064E+Ol l.355E+Ol 2.471E+Ol NOT IDENT. NA-22 3.170E-02 5.942E-02 l.290E-01 NOT IDENT. NA-24 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF AL-26 3.627E-02 4.312E-02 l. l 72E-01 NOT IDENT. SC-46 2.299E-01 4.645E-01 l.052E+OO FAIL ABUN V-48 O.OOOE+OO 3.529E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.254E+02 O.OOOE+OO SHORT HLIF MN-54 l.838E-02 7.036E-02 l.509E-01 NOT IDENT. C0-56 -3.226E-02 5.935E-01 l.195E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 2.380E-02 3.952E-02 8.466E-02 FAIL ABUN C0-58 -l.390E-01 7.991E-01 l.559E+OO NOT IDENT. Page 3708of5809 FE-59 9.008E-01 8.271E+OO 1. 861E+Ol FAIL ABUN C0-60 -2.800E-02 4.645E-02 8.517E-02 NOT IDENT. ZN-65 -5.428E-02 2.233E-01 3.929E-01 NOT IDENT. GE-68 3. 071E+OO 3. llOE+OO 7.350E+OO NOT IDENT. AS-73 -3.276E+OO 7.927E+OO 1. 631E+Ol NOT IDENT. AS-74 O.OOOE+OO l.195E+04 O.OOOE+OO SHORT HLIF SE-75 -l.llOE-01 2.086E-01 3.721E-01 NOT IDENT. BR-77 0.000E+OO l.977E+39 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO l .131E+03 O.OOOE+OO SHORT HLIF RB-83 -l.912E-01 8.405E-01 l.607E+OO NOT I KR-85 6.430E+OO 7.474E+OO l.698E+Ol NOT IDENT. SR-85 7.952E-01 9.253E-01 2.102E+OO NOT IDENT. RB-86 O.OOOE+OO 6.654E+04 O.OOOE+OO SHORT HLIF Y-88 -7.376E-03 2.799E-01 6.479E-01 NOT IDENT. Y-91 4. 011E+02 7.878E+02 l.777E+03 NOT IDENT. NB-94 l.108E-02 3.145E-02 6.887E-02 NOT IDENT. NB-95 -l.178E-01 l.104E+OO 2.183E+OO NOT IDENT. NB-95M 1. 968E+OO 2.817E+00 5.479E+OO NOT IDENT. ZR-95 l.042E+OO l.878E+OO 4.217E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 718E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO l.913E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 9.814E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.598E-02 3.391E-02 6.459E-02 NOT IDENT. RH-102 l.880E-02 7.656E-02 l.591E-01 NOT IDENT. RU-103 -l.082E+OO 6.248E+OO l.296E+Ol FAIL ABUN RH-106 9.562E-02 5. lllE-01 l.109E+OO NOT IDENT. RU-106 9.562E-02 5. lllE-01 *1.109E+OO NOT IDENT. AG-108M -5.279E-03 2.571E-02 5.252E-02 NOT IDENT. AG-llOM 3.206E-02 9. 701E-02 2. 211E-01 NOT IDENT. SN-113 1. 611E-01 2.368E-01 5.396E-01 NOT IDENT. CD-115 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.982E+05 O.OOOE+OO SHORT HLIF TE-123M -7.255E-02 l.257E-01 2.334E-01 NOT IDENT. SB-124 6.176E-01 2.853E+OO 6.988E+OO NOT IDENT. SB-125 1. 210E-01 l.242E-01 2.806E-01 FAIL ABUN TE-125M 1. 274E+02 3. 096E+02 6. 431E+02 NOT IDENT. I-126 O.OOOE+OO 2.122E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.012E+06 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 4.174E+23 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 2.142E+l0 O.OOOE+OO SHORT HLIF I-132 0.000E+OO l.394E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.056E+28 O.OOOE+OO SHORT HLIF BA-133 -3.443E-03 4.624E-02 7.943E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 6.324E-02 5. 968E-02 l.407E-01 FAIL ABUN CS-135 6.958E-02 l.497E-01 2.835E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 6.074E+05 O.OOOE+OO SHORT HLIF BA-137M 1. 080E-02 3.802E-02 8.088E-02 NOT IDENT. CS-137 l.141E-02 4.016E-02 8.544E-02 NOT IDENT. CE-139 -l.998E-02 1. 070E-01 2.065E-01 NOT IDENT. BA-140 O.OOOE+OO l.003E+07 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO l.224E+06 O.OOOE+OO SHORT HLIF CE-141 -6.765E+OO 3.143E+Ol 5.496E+Ol NOT IDENT. CE-143 0.000E+OO l.726E+41 O.OOOE+OO SHORT HLIF CE-144 l.124E-01 3.258E-01 6.706E-01 NOT IDENT. PM-144 2.471E-03 6.715E-02 l.358E-01 NOT IDENT. PR-144 2.396E-01 5.884E+OO l.191E+Ol NOT IDENT. PM-146 1. 672E-02 4.152E-02 9.215E-02 NOT IDENT. ND-147 O.OOOE+OO 1. 051E+08 O.OOOE+OO SHORT HLIF PM-147 3. 096E+02 7. 296E+02 l.523E+03 NOT IDENT. PM-149 O.OOOE+OO l.409E+41 O.OOOE+OO SHORT HLIF EU-150 5.709E-03 3.261E-02 5.769E-02 FAIL ABUN EU-152 -6.003E-02 l.197E-01 1. 872E-01 FAIL ABUN GD-153 -l.144E-01 l.635E-01 3 .115E-01 NOT IDENT. EU-154 6.950E-02 l.426E-01 3.077E-Ol NOT IDENT. EU-155 -1. 761E-02 8. 967E-02 1. 793E-01 FAIL ABUN TB-160 2.992E-01 2. 082E+OO . 4.508E+OO FAIL ABUN H0-166M -l.913E-02 5. 611E-02 l.080E-01 FAIL ABUN TM-171 2.088E+OO l.620E+Ol 3.503E+Ol NOT IDENT. HF-172 l.068E-01 2.175E-01 4.515E-01 NOT IDENT. LU-172 3.250E-02 8.303E-02 l.852E-01 FAIL ABUN LU-176 l.985E-02 4.371E-02 3.638E-02 FAIL ABUN HF-181 -3.044E+OO 5.261E+OO 9.995E+OO NOT IDENT. TA-182 8.676E-01 l. l 77E+OO 2.777E+OO FAIL ABUN RE-183 -5.533E-01 2.781E+OO 5.793E+OO NOT IDENT. RE-184 2.855E+Ol 2.503E+Ol 7.678E+Ol NOT IDENT. Page 3709 of 5809 W-188 7.686E+Ol l.278E+02 2.514E+02 NOT IDENT. IR-192 -4.386E-02 5.485E-01 l.033E+OO FAIL ABUN HG-203 -2.129E+OO 2.928E+OO 5.016E+OO NOT IDENT. BI-207 1.217E-03 5. 013E-02 l.032E-01 FAIL ABUN PB-210 l.423E-Ol 2.128E+OO 4.604E+OO NOT IDENT. BI-211 O.OOOE+OO 5.342E-01 8.095E-01 FAIL ABUN PB-211 3.558E-01 7.958E-01 l.656E+OO NOT IDENT. BI-212 1.336E+OO 8. 951E-01 1.624E+OO FAIL ABUN RN-219 5.605E-02 3.895E-01 8.222E-01 FAIL ABUN RA-223 -3.544E-01 6.451E-01 1.119E+OO . FAIL ABUN AC-227 -3.757E-02 2.338E-01 4.388E-01 FAIL ABUN TH-227 -3.757E-02 2.338E-01 4.388E-01 FAIL ABUN TH-229 -3.053E-01 4. l 71E-01 7.455E-01 FAIL ABUN TH-231 -3.544E-01 6.451E-01 1.119E+OO FAIL ABUN PA-233 1. 871E-02 6.343E-02 1.254E-01 FAIL ABUN PA-234 1.488E-01 2.550E-01 6.124E-01 NOT IDENT. PA-234M 3.609E+OO 4.654E+OO 1.117E+Ol NOT IDENT. TH-234 -l.884E-01 1. 035E+OO 2.145E+OO FAIL ABUN U-235 4. 722E-02 1.592E-01 3.157E-01 FAIL ABUN NP-237 1. 871E-02 6.343E-02 1.254E-01 FAIL ABUN NP-238 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF U-238 -1.884E-01 1.035E+OO 2.145E+OO FAIL ABUN NP-239 -8.077E-02 2.142E-01 4.165E-01 NOT IDENT. PU-239 2.454E+02 2.999E+02 6.329E+02 NOT IDENT. AM-241 2.294E-02 1. 074E-01 2.313E-01 NOT IDENT. CM-243 -2.489E-02 8.694E-02 1.720E-01 NOT IDENT. BK-247 -l.090E-02 6.476E-02 1.227E-01 NOT IDENT. CM-247 -4.952E-03 3.793E-02 7: 696E-02 NOT IDENT. CF-249 8.157E-04 3.414E-02 7.213E-02 NOT IDENT. CF-251 4.614E-03 1.028E-01 2.027E-01 NOT IDENT. ANH-511 -1.687E-02 4.760E-02 l.088E-01 NOT IDENT. Page 3710of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:18:22.26 Nuclide Line Activity Report Nuclide Tywe: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 160 10.66* 6.546E-01 1.060E+Ol 1.060E+Ol 17.07 CD-109 88.03 93 3.70* 4.292E+OO 2.706E+OO 4.344E+OO 53.37 SN-126 64.28 ------9.60 2.567E+OO ------Line Not Found ------86.94 93 8.90 4.292E+OO 1.125E+OO 1.125E+OO 53.37 87.57 93 37.00* 4.292E+OO
  • 2. 706E-01 2.706E-01 53.37 TL-208 277.37 ------6.60 3.041E+OO ------Line Not Found ------583.19 64 85.00* 1.495E+OO 2.349E-01 2.349E-01 48.40 860.56 ------12.50 1.058E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 3.327E+OO ------Line Not Found ------351.06 158 12.92* 2.414E+OO 2.342E+OO 2.342E+OO 23.27 PB-212 74.82 96 10.28 3.493E+OO 1.237E+OO 1.237E+OO 47.20 77 .11 190 17.10 3.655E+OO 1.410E+OO 1. 410E+OO 28.78 238.63 308 43.60* 3.499E+OO 9.340E-01 9.340E-01 14. 72 30.0. 09 38 3.30 2.817E+OO 1.868E+OO 1. 8 68E+OO 82.17 BI-214 609.32 115 45.49* 1.437E+OO 8.142E-01 8.145E-01 22.99 1120.29 27 14.92 8.369E-01 1.019E+00 1.019E+OO ' 60. 99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------PB-214 74.82 96 5.80 3.493E+OO 2.193E+OO 2.194E+OO 47.20 77 .11 190 9.70 3.655E+OO 2.485E+00 2.486E+OO 28.78 87.09 93 3.41 4.292E+OO 2.936E+OO 2.938E+OO 53.37 242.00 85 7.25 3.460E+OO 1.564E+OO 1.564E+OO 42.68 295.22 106 18.42 2.862E+OO 9.287E-01 9.290E-01 40.66 351. 93 158 35.60* 2.414E+00 8. 501E-01 8.504E-01 23.27 RN-222 609.32 115 45.49* 1.437E+OO 8.142E-01 8.145E-01 22.99 1120. 29 27 14.92 8.369E-01 1.019E+00 1.019E+OO 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------RA-224 240.99 85 4.10* 3.460E+OO 2.765E+OO 2.765E+OO 42.68 RA-226 609.32 115 45.49* 1.437E+OO 8.142E-01 8.145E-01 22.99 1120.29 27 14.92 8.369E-01 1.019E+OO l.019E+OO 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------AC-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 53 11.27 2.507E+OO 8.644E-01 8.644E-01 81. 42 794.95 ------4.25 1.134E+OO ------Line Not Found ------835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 52 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 968. 97 16 15.80 9.524E-01 4.816E-01 4.816E-01 88.69 RA-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 53 11.27 2.507E+OO 8.644E-01 8.644E-01 81. 42 794.95 ------4.25 1.134E+OO ------Line Not Found ------835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 52 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 968. 97 16 15.80 9.524E-01 4.816E-01 4.816E-01 88.69 TH-228 74.82 96 10.28 3.493E+OO l.237E+OO 1.237E+OO 47.20 77 .11 190 17.10 3.655E+OO 1.410E+OO 1.410E+OO 28.78 238.63 308 43.60* 3.499E+OO 9.340E-01 9.340E-01 14.72 300.09 38 3.30 2.817E+OO 1.868E+OO 1. 8 68E+OO 82.17 TH-230 609.32 115 45.49* 1.437E+OO 8.142E-01 8.142E-01 22.99 Page 3711of5809 Nuclide Line Activity Report (continued) Sample ID : G405235036 Acquisition date Page : 2 3-0CT-2016 09:16:44 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error H20 .29 27 14.92 8.369E-01 1. 019EHlO 1.019E+OO 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------PA-231 283.69 ------1. 70 2.976E+OO ------Line Not Found ------301.36 38 5.35* 2.817E+OO 1.152E+OO 1.152E+OO 82.17 TH-232 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 53 11.27 2.507E+OO 8.644E-01 8.644E-01 81. 42 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 52 25.80* 1.005E+OO 9.219E-01 9.219E-01 34.07 968. 97 16 15.80 9.524E-01 4.816E-01 4.816E-01 88.69 U-234 609.32 115 45.49* 1.437E+OO 8.142E-01 8.142E-01 22.99 1120.29 27 14.92 8.369E-01 1.019E+OO 1.019E+OO 60.99 1764.49 ------15.30 5.419E-01 ------Line Not Found ------AM-243 43.53 ------5.90 5.957E-01 ------Line Not Found ------74.66 96 67.20* 3.493E+OO l.893E-01 1. 893E-01 47.20 Flag: "*" Key line Page 3712 of 5809 Summary of Nuclide Activity Sample ID : G405235036 Acquisition date Page : 3 3-0CT-2016 09:16:44 Total number of lines in spectrum 37 Number of unidentified lines 6 Number of lines tentatively identified by NID 31 Nuclide Type : Nuclide K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 Hlife 1. 25E+09Y 461.40D 2.30E+05Y 1.41E+10Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600.00Y 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+10Y 1.41E+10Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 2.45E+05Y 7370.00Y Decay 1. 00 1. 61 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity c Uncorrected pCi/GRAM l.060E+Ol 2.706E+00 2.706E-01 2.349E-01 2.342E+00 9.340E-01 8.142E-01 8.501E-01 8.142E-01 2.765E+OO 8.142E-01 9.219E-01 9.219E-01 9.340E-01 8.142E-01 1.152E+OO 9.219E-01 8.142E-01 l.893E-01 2.982E+Ol 2.982E+Ol Decay Corr pCi/GRAM 1.060E+Ol 4.344E+OO 2.706E-01 2.349E-01 2.342E+OO 9.340E-01 8.145E-01 8.504E-01 8.145E-01 2.765E+OO 8.145E-01 9.219E-01 9.219E-01 9.340E-01 8.142E-01 1.152E+OO 9.219E-01 8.142E-01 1. 8 93E-01 3.146E+Ol 3.146E+Ol 83.78% Decay Corr 2-Sigma Error 0.181E+Ol 2.318E+OO 1.444E-01 l.137E-01 0.545E+00 l.375E-01 l.873E-01 l.979E-01 1.873E-01 1.180E+OO 1. 873E-01 3.141E-01 3 .141E-01 1. 37 5E-01 l.872E-01 0.947E+OO 3 .141E-01 l.872E-01 0.894E-01 "M" Manually accepted 2-Sigma %Error 17.07 53.37 53.37 48.40 23.27 14.72 22.99 23.27 22.99 42.68 22.99 34.07 34.07 14.72 22.99 82.17 34.07 22.99 47.20 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3713of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235036 Acquisition date : 3-0CT-2016 09:16:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 92.82 53 169 1. 50 185.62 182 8 1.llE-02 **** 4.56E+OO T 0 137.93 38 91 1. 27 275.85 272 8 8.20E-03 **** 5.02E+00 T 0 147.89 27 56 0.75 295.77 293 6 6.02E-03 **** 4.90E+OO 0 186.09 51 131 0.86 372,.16 367 10 1.16E-02 **** 4.30E+OO T 0 209.98 29 94 1. 49 419.94 414 10 6.72E-03 **** 3. 91E+OO T 0 245.61 26 36 1. 35 491. 21 488 7 6.llE-03 92.8 3.41E+OO T 0 270.50 30 59 0.77 540.98 536 8 7.llE-03 **** 3. llE+OO T 0 305.63 11 33 1. 40 611. 24 606 9 2.64E-03 **** 2.77E+OO T 0 349.45 12 24 1.16 698.88 692 8 2.79E-03 **** 2.43E+OO 0 409.99 21 25 1. 70 819.95 815 10 5.20E-03 **** 2.08E+OO T 0 464.25 12 39 1. 29 928.46 923 12 2.99E-03 **** 1. 85E+OO T 5 515.57 18 14 2.21 1031.10 1014 22 4.52E-03 **** 1.68E+OO 0 538.68 14 39 5.95 1077.29 1062 18 3.45E-03 **** 1. 61E+OO T 0 543.65 24 8 2.36 1087.24 1083 10 6.09E-03 63.0 1.60E+OO 0 562.29 8 1 0. 71 1124. 52 1123 5 2.13E-03 90.8 1.55E+OO T 0 603.12 16 9 1. 84 1206.16 1200 11 4.16E-03 90.3 1. 45E+OO T 0 727.30 24 11 0.77 1454.47 1450 10 6.19E-03 68.4 1. 23E+OO T 0 900.61 13 0 0.83 1801.00 1797 8 3.61E-03 55.5 1.02E+OO T 0 905.40 10 2 2.72 1810.56 1806 9 2. 72E-03 90. 2 1. OlE+OO 4 966 .14 10 7 1. 83 1932.00 1930 12 2.62E-03 85.5 9.55E-01 T 0 1280.68 5 9 0.47 2560.83 2554 9 1.52E-03 **** 7. 41E-01 0 1291.10 7 2 1. 38 2581.65 2578 7 2.0lE-03 96.2 7.36E-01 T Flags: "T" = Tentatively associated Page 3714 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:18:37.96 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO :*[CANBERRA. GAMMA.ARCHIVE. GAMMA] G405235036. CNF; 1 *
  • Acquisition date 3-0CT-2016 09:16:44 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:12:00 Nuclide Library : SOLID *
  • Sample ID G405235036 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.6226E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 Le (pCi/GRAM 2.657E-01 9.797E-01 6.136E-02 2.267E-02 4.474E-02 5.806E-02 5.069E-02 5.806E-02 4.805E-01 5.806E-02 9.958E-02 9.958E-02 4.474E-02 5.804E-02 2.851E-01 9.958E-02 5.804E-02 3. 791E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 Page 3715of5809 Le (pCi/GRAM 1.026E+Ol 5.380E-02 O.OOOE+OO 4.667E-02 4.416E-01 O.OOOE+OO 0.000E+OO 6.354E-02 4. 963E-01 O.OOOE+OO 3.887E-02 6.532E-01 7.515E+OO NOT I DENT .. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-14*9 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 Page 3716of5809 3.264E-02 1.598E-01 3.164E+OO 7.481E+00 0.000E+OO 1. 641E-01 O.OOOE+OO O.OOOE+OO 6.938E-01 7.544E+QO 9.338E-01 O.OOOE+OO 2.295E-01 7.586E+02 2.932E-02 9.250E-01 2. 511E+OO 1. 806E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 996E-02 6.983E-02 5.403E+OO 4. 712E-01 4. 712E-01 2.258E-02 9.003E-02 2.388E-01 O.OOOE+OO O.OOOE+OO 1.062E-01 2.616E+00 1. 2 67E-01 2. 991E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3. 501E-02 O.OOOE+OO 6.150E-02 l.285E-01 O.OOOE+OO O.OOOE+OO 3.494E-02 3.691E-02 9.442E-02 O.OOOE+OO O.OOOE+OO 2.515E+Ol O.OOOE+OO 3.094E-01 5.863E-02 5.141E+00 4.014E-02 O.OOOE+OO 7.029E+02 O.OOOE+OO 2.610E-02 8.312E-02 l.435E-01 l.277E-01 8.223E-02 1.833E+OO 4.445E-02 1.609E+Ol 2. 096E-01 7.634E-02 l.563E-02 4.214E+00 l.184E+OO 2.664E+OO 3.047E+Ol 1.128E+02 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3717 of 5809 4.590E-01 2.217E+OO 4.169E-02 2.106E+OO 3.838E-01 7.459E-01 7.333E-01 3.643E-01 4. 964E-01 1. 981E-01 l.981E-01 3.364E-01 4. 964E-Ol 5.637E-02 2.513E-01 4.763E+OO 9.972E-01 1.455E-01 5.637E-02 O.OOOE+OO 9. 972E-01 1.914E-01 2.954E+02 1.065E-01 7.924E-02 5.437E-02 3.419E-02 3.153E-02 9.264E-02 5.056E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:18:43.38 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235036.CNF;l *
  • Acquisition date 3-0CT-2016 09:16:44 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
  • Sample date 23-NOV-2015 11:12:00 Nuclide Library : SOLID *
  • Sample ID G405235036 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity 1.6226E+02 GRAM *
  • Quantity Err(%) 1.2326E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 CD-109 SN-126 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 1.060E+Ol 2.970E+OO 1.850E-01 2.349E-01 9.340E-01 8.145E-01 8.504E-01 8.145E-01 1.123E+OO 8.145E-01 9.219E-01 9.219E-01 9.340E-01 8.142E-01 1.152E+OO 9.219E-01 8.142E-01 1.092E-01 Act Error ( 1. 96-sigma) 1.858E+OO 2.356E+OO l.464E-01 1.119E-01 l.435E-01 l.869E-01 l.971E-01 1. 869E-01 1.335E+OO 1. 8 69E-01 3.114E-01 3 .114E-01 1.435E-01 1. 868E-01 9. 601E-01 3 .114E-01 1. 868E-01 9.402E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 3718of5809 Key-Line Activity (pCi/GRAM -1.064E+Ol 3.170E-02 1.000E+41 3.627E-02 2.299E-01 -4.571E+04 -3.855E+02 l.838E-02 -3.226E-02 -1. OOOE+41 2.380E-02 -1.390E-01 K.L Act error ( 1. 96-sigma) 1.356E+Ol 5.944E-02 2.638E+41 4.318E-02 4.646E-01 3.533E+04 6.256E+02 7.037E-02 5.935E-01 l.555E+42 3.954E-02 7.991E-01 TPU ( 1. 96-sigma) 1.858E+OO 2.356E+OO 1.464E-01 l .119E-01 l.435E-01 1. 869E-01 l.971E-01 l.869E-01 1.335E+OO 1.869E-01 3 .114E-01 3.114E-01 l.435E-01 1.868E-01 9.601E-01 3.114E-01 1. 868E-01 9.402E-02 TPU (1. 96-sigma) l.438E+Ol 6 .113E-02 O.OOOE+OO 4.618E-02 4.760E-01 4.090E+04 6.493E+02 7.085E-02 5.937E-01 O.OOOE+OO 4.097E-02 8.016E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT.

FE-59 9.008E-01 8.271E+OO 8.281E+OO FAIL ABUN C0-60 -2.800E-02 4.646E-02 4.814E-02 NOT IDENT. ZN-65 -5.428E-02 2.233E-01 2.246E-01 NOT IDENT. GE-68 3.071E+OO 3 .112E+OO 3.406E+OO NOT IDENT. AS-73 -3.276E+OO 7.955E+OO 8. 091E+OO NOT IDENT. AS-74 4.053E+03 1.195E+04 l.209E+04 SHORT HLIF SE-75 -1. llOE-01 2.086E-01 2.145E-01 NOT IDENT. BR-77 1.370E+40 l.246E+41 0.000E+OO SHORT HLIF SR-82 4.368E+02 1.132E+03 l.149E+03 SHORT HLIF RB-83 -1.912E-01 409E-01 8.453E-01 NOT IDENT. KR-85 6.430E+OO 7.479E+OO 8.021E+OO NOT IDENT. SR-85 7.952E-01 9.259E-01 9.928E-01 NOT IDENT. RB-86 3.988E+04 6.656E+04 6.895E+04 SHORT HLIF Y-88 -7.376E-03 2.799E-01 2.799E-01 NOT IDENT. Y-91 4. 011E+02 7.880E+02 8.084E+02 NOT IDENT. NB-94 1.108E-02 3.145E-02 3.185E-02 NOT IDENT. NB-95 -1.178E-01 1.104E+OO 1.105E+OO NOT IDENT. NB-95M 1. 968E+OO 2.821E+OO 2.957E+OO NOT IDENT. ZR-95 1.042E+OO 1.878E+OO 1. 936E+OO NOT IDENT. NB-97 -1.000E+41 1. 719E+41 . O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.914E+41 0.000E+OO SHORT HLIF M0-99 3.797E+33 9.818E+33 0.000E+OO SHORT HLIF TC-99M l.000E+41 6.280E+41 0.000E+OO SHORT HLIF RH-101 -1.598E-02 3.404E-02 3.479E-02 NOT IDENT. RH-102 1. 880E-02 7.657E-02 7.704E-02 NOT IDENT. RU-103 -1.082E+OO 6.248E+OO 6.267E+OO FAIL ABUN RH-106 9.562E-02 5. lllE-01 5.129E-01 NOT IDENT. RU-106 9.562E-02 5. lllE-01 5.129E-01 NOT IDENT. AG-108M -5.279E-03 2.571E-02 2.582E-02 NOT IDENT. AG-llOM 3.206E-02 9.702E-02 9.809E-02 NOT IDENT. SN-113 1.611E-01 2.369E-01 2.478E-01 NOT IDENT. CD-115 -7.985E+39 3.858E+41 O.OOOE+OO SHORT HLIF SN-ll 7M -2.346E+05 2.003E+05 2.265E+05 SHORT HLIF TE-123M -7.255E-02 1.257E-01 l.299E-01 NOT IDENT. SB-124 6.176E-01 2.853E+OO 2. 867E+OO. NOT IDENT. SB-125 l.210E-01 l.243E-01 1.357E-01 FAIL ABUN TE-125M 1.274E+02 3.097E+02 3.150E+02 NOT IDENT. I-126 2.106E+05 2.122E+06 2.124E+06 SHORT HLIF SB-126 -1.624E+06 3.028E+06 3 .115E+06 SHORT HLIF SB-127 2.055E+23 5 .121E+23 O.OOOE+OO SHORT HLIF I-131 -2.268E+10 2.145E+10 2.376E+10 SHORT HLIF I-132 -1.000E+41 1.946E+42 O.OOOE+OO SHORT HLIF TE-132 1.296E+27 1.057E+28 O.OOOE+OO SHORT HLIF BA-133 -3.443E-03 4.624E-02 4.626E-02 NOT IDENT. I-133 -1.000E+41 8.737E+41 O.OOOE+OO SHORT HLIF CS-134 6.324E-02 5.974E-02 6.619E-02 FAIL ABUN CS-135 6.958E-02 1.498E-01 1.530E-01 NOT IDENT. I-135 -1. OOOE+41 7.734E+41 O.OOOE+OO SHORT HLIF CS-136 1.507E+05 6.076E+05 6 .114E+05 SHORT HLIF BA-137M 1. OSOE-02 3.802E-02 3.833E-02 NOT IDENT. CS-137 1.141E-02 4.016E-02 4.049E-02 NOT IDENT. CE-139 -1. 998E-02 1. 070E-01 1. 074E-01 NOT IDENT. BA-140 4.387E+06 1.004E+07 1.023E+07 SHORT HLIF LA-140 -8.774E+05 l.224E+06 l.287E+06 SHORT HLIF CE-141 -6.765E+OO 3.143E+Ol 3.158E+Ol *NOT IDENT. CE-143 1.000E+41 1. 729E+41 O.OOOE+OO SHORT HLIF CE-144 1.124E-01 3.259E-01 3.298E-01 NOT IDENT. PM-144 2.471E-03 6.715E-02 6.716E-02 NOT IDENT. PR-144 2. 396E-01 5.884E+OO 5.885E+OO NOT IDENT. PM-146 l.672E-02 4.154E-02 4.222E-02 NOT IDENT. ND-147 -6.125E+07 1.051E+08 l.087E+08 SHORT HLIF PM-147 3.096E+02 7.297E+02 7.429E+02 NOT IDENT. PM-149 1.000E+41 1.427E+41 O.OOOE+OO SHORT HLIF EU-150 5.709E-03 3 ;261E-02 3.271E-02 FAIL ABUN EU-152 -6.003E-02 1.197E-01 l.227E-01 FAIL ABUN G*D-153 -1.144E-01 1. 636E-01 1. 716E-01 NOT IDENT. EU-154 6.950E-02 l.426E-01 1.460E-01 NOT IDENT. EU-155 -1.761E-02 8. 968E-02 9.003E-02 FAIL ABUN TB-160 2.992E-01 2.082E+OO 2.087E+OO FAIL ABUN H0-166M -1.913E-02 5.612E-02 5.678E-02 FAIL ABUN TM-171 2.088E+OO 1.620E+Ol 1.623E+Ol NOT IDENT. HF-172 1.068E-01 2.182E-01 2.234E-01 NOT IDENT. LU-172 3.250E-02 8.310E-02 8.438E-02 FAIL ABUN LU-176 l.985E-02 4.371E-02 4.462E-02 FAIL ABUN HF-181 -3.044E+OO 5.263E+OO 5.439E+OO NOT IDENT. TA-182 8.676E-01 1.178E+00 1.241E+OO FAIL ABUN RE-183 -5.533E-01 2.782E+OO 2.794E+OO NOT IDENT. RE-184 2.855E+Ol 2.603E+01 2.904E+Ol NOT IDENT. Page 3719of5809 W-188 7.686E+Ol 1. 281E+o2 1.327E+02 NOT IDENT. IR-192 -4.386E-02 5.485E-01 5.488E-01 FAIL ABUN HG-203 -2.129E+OO 2.929E+00 3.083E+OO NOT IDENT. BI-207 1.217E-03 5.013E-02 5.013E-02 FAIL ABUN PB-210 1.423E-01 2.128E+OO 2.129E+OO NOT IDENT. BI-211 2.342E+00 5.443E-01 1.188E+OO FAIL ABUN PB-211 3.558E-01 7. 960E-01 8.120E-01 NOT IDENT. BI-212 1.336E+OO 8.976E-01 1. 081E+OO FAIL ABUN RN-219 5.605E-02 3.895E-01 3.904E-01 FAIL ABUN RA-223 -3.544E-01 6 ..455E-01 6.649E-01 FAIL ABUN AC-227 -3.757E-02 2.339E-01 2.345E-01 FAIL ABUN TH-227 -3.757E-02 2.339E-01 2.345E-01 FAIL ABUN TH-229 -3.053E-01 4.173E-01 4.394E-01 FAIL ABUN TH-231 -3.544E-01 6.455E-01 6.649E-01 FAIL ABUN PA-233 1.871E-02 6.344E-02 6.400E-02 FAIL ABUN PA-234 1. 48 8E-01 3.066E-01 3 .139E-01 NOT IDENT. PA-234M 3.609E+OO 4.657E+OO 4.933E+OO NOT IDENT. TH-234 -1.884E-01 1.036E+OO 1.039E+OO FAIL ABUN U-235 4. 722E-02 1.592E-01 1.606E-01 FAIL ABUN NP-237 1. 871E-02 6.344E-02 6.400E-02 FAIL ABUN NP-238 l.000E+41 1.904E+42 O.OOOE+OO SHORT HLIF U-238 -1.884E-01 1.036E+OO 1.039E+OO FAIL ABUN NP-239 -8.077E-02 2.143E-01 2.174E-01 NOT IDENT. PU-239 2.454E+02 3. 001E+02 3.199E+02 NOT IDENT. AM-241 2.294E-02 1.074E-01 1. 079E-01 NOT IDENT. CM-243 -2.489E-02 8.697E-02 8.769E-02 NOT IDENT. BK-247 -1.090E-02 6.479E-02 6.498E-02 NOT IDENT. CM-247 -4.952E-03 3.794E-02 3.800E-02 NOT IDENT. CF-249 8.157E-04 3.414E-02 3.414E-02 NOT IDENT. CF-251 4.614E-03 1.028E-01 1.028E-01 NOT IDENT. ANH-511 -1.687E-02 4.760E-02 4.821E-02 NOT IDENT. Page 3720of5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 22.6668 87.09 68.7588 136.47 39.9849 45.60 35.4275 87.57 68.8320 140.51 0.0000 46.54 30.8024 88.03 68.9016 143.76 39.1449 49. 72 0.0000 88.34 68.9486 144.24 36.2361 51. 35 44.9328 88.47 83.7051 145.44 41.8639 51. 87 43.3996 89. 96 72.7416 152.43 58.5067 52.39 40.2504 1093.63 58.6345 153.25 0.0000 52.97 47.5817 91.11 0.0000 323.87 48.7189 53.44 48.4589 92.59 74.9381 156.02 0.0000 54.07 32.3686 93.35 75.0592 158.56 0.0000 57.36 0.0000 94.56 48.9728 159.00 44.0557 57.53 31. 8897 94.65 48.9820 162.33 43.2605 57.98 47.4881 94.67 48.9840 162.66 0.0000 59.27 36.1609 94.87 46.6140 163.33 42.3147 59.32 36.1661 97.43 50.4667 165.86 41. 4548 59.54 41.9464 98.43 46.0549 176.31 44.1049 60. 96 43.7685 98.44 46.0561 176.60 0.0000 61.17 55.3630 99.53 52.4935 177.52 36.9849 62.93 51.4845 100 .11 56.1795 181.07 0.0000 63.29 53.1981 102.03 45.4803 181.52 45.4435 63.58 46.5856 103.18 56.5243 184.41 45.6154 64.28 48.3422 103.37 51. 0734 143.76 45.6926 66.73 48.6631 105.21 44.8504 193.51 40.9037 67.24 52.9299 105.31 44.8593 197.03 45.2964 125.81 56.3559 106.12 46.7635 198.01 36.9141 67.75 56.3661 106.47 44. 9603 201.83 32.8481 69.67 53.2682 109.28 50.7375 203.43 33.9736 70.83 61.0593 111. 00 55.5295 205.31 39.7253 72.81 62.5033 111. 76 0.0000 210.85 29.9905 72.87 62.5128 114. 06 44.6766 215.65 26.9272 74.66 55.6565 116. 30 0.0000 222 .11 36.8923 74.82 55.6784 116.74 50.5072 227.09 33.8254 74.97 55.6992 119.76 47.0196 227.38 40.3852 77 .11 55.9903 121.12 46.1902 228.16 0.0000 78.74 58.8038 121. 22 40.5415 228.18 32.7740 79.69 54.3141 121.78 32.0874 116.74 32.7740 80.12 56.6827 122.06 32.1033 235.69 27.9039 80.19 0.0000 122.92 43.4991 235. 96 24.9739 80.57 61. 3745 123.07 43.5103 238.63 35.3589 81. 00 49.5549 265.00 49.2380 238.98 0.0000 81. 07 49.5628 125.81 46.5680 240.99 35.4478 81. 75 60. 9632 127.23 64.7811 242.00 35.4858 83.79 56.0000 127.91 61.9950 244.70 17.7935 84.00 57.1941 129.30 48.7565 252.40 0.0000 85.43 67.9186 131.20 65.2161 252.80 26.9154 86.55 64.5673 133.02 43.2875 254.15 0.0000 86.79 68.7124 133.52 41.3977 256.23 31. 5111 86.94 68.7356 136.00 41.2435 260.90 0.0000 Page 3721of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 26.1038 355.39 0.0000 584.27 6.6440 264.80 26.1073 356.01 19.6787 595.83 0.0000 265.00 22.7063 364.49 0.0000 427.87 12.9238 268.22 24.2969 366.42 0.0000 602.52 0.0000 269.46 34.2096 372. 51 23.6688 604.72 2.8781 270.03 34.2279 375.05 22.4665 6Q7.14 0.0000 271.23 31. 9836 377.52 23.3419 609.32 11. 5396 273.65 0.0000 356.01 16.7517 610.33 11.5454 276.40 26.4035 388.16 15. 9648 614.28 13.0150 277.37 16.0867 388.63 0.0000 618.01 9.6590 277.60 19.5380 391.69 12.6364 620.36 9.6704 278.00 25.2945 264.66 24.5897 621.93 7.7425 279.20 29.9276 401.81 18.6699 630.19 0.0000 279.54 28.7857 402.40 22.9224 631. 29 14.5856 279.70 26.4871 404.85 19.3906 633.25 13.6263 280.46 11. 5244 410.95 13.6663 634.78 0.0000 283.69 21.9630 413. 71 20.5391 635.95 8. 7715 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 18.5249 423.72 0.0000 645.85 6.8556 285.90 0.0000 427.09 15.5475 657.76 9.8507 287.50 18.5610 427.87 16.4201 657.90 0.0000 290.67 17.0644 433.94 14.7522 661.66 10.8559 293.27 0.0000 439.40 12.1933 664.57 0.0000 351. 93 26.4823 453. 88 11. 4308 666.33 0.0000 295. 96 26.4996 463.37 13.2703 666.50 0.0000 879.38 16.4063 468.07 14.6413 667.71 0.0000 299.98 14.0804 473.00 0.0000 677.62 9.9443 300.09 14.0819 475.06 12.4779 685.70 0.0000 300 .13 14.0823 476.78 12.4913 695.00 0.0000 301.36 14.0977 477.60 15.1756 696.49 13.0418 302.85 23.5278 482.18 15.2188 696. 51 13.0418 256.23 29.8452 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.0501 306.78 15.7402 497.08 9.9376 697.49 14.0513 308.46 9.4580 505.52 9.5342 702.65 8.0482 311. 90 22.5306 507.63 0.0000 706.68 8.0632 316.51 22.6205 511. 00 11.8427 711. 68 10.1017 319.41 0.0000 514.00 11.8638 720.70 0.0000 320.08 0.0000 514.00 11.8638 721. 93 0.0000 321. 04 22.7086 520.40 14.2898 722.78 6.0913 323.87 28.7542 520.69 0.0000 722. 91 10.6602 325.23 32.3855 522.65 0.0000 723. 31 12.1855 328.76 0.0000 527.90 0.0000 724.19 9.1428 333.37 25.7630 528.26 13.2510 727.33 8.1383 333.97 27.3870 529.59 11. 0508 733.00 9.1783 334.37 27.3960 529.87 0.0000 735.93 13.2751 338.28 26. 6762 531. 02 0.0000 333.97 10.2185 338.32 26.6769 537.26 0.0000 739.50 0.0000 311.90 29.1533 546.56 0.0000 747.24 9.2358 340.48 29.1533 552.55 13.0612 748.06 9.2391 340.55 0.0000 563.25 12.6689 752.31 12.3413 344.28 29.2434 569.33 13.1820 753.82 0.0000 345.93 22.7751 946.00 13.1831 756.73 7.2131 351.06 14.7015 569.70 14.1260 756.80 6.1826 351. 93 14. 7118 583.19 6.6403 884.68 11. 3697 Page 3722 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 11.3787 1274.44 5.6460 1620.50 1.0057 766.42 12.4165 1001.03 3.3931 1621.92 1.0060 766.84 8.2790 1002.74 11. 3167 1678.03 0.0000 772. 60 0.0000 1004.73 13.5894 1690.97 2.0430 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000. 1764.49 1. 0377 778.90 9.3615 1028.54 0.0000 1063.66 3 .1166 783.70 0.0000 1037.84 6.8706 1771.35 2.0782 785.37 13.5586 1038.76 0.0000 1791.20 0.0000 792.07 9.4131 631.29 8.0385 1808.65 1. 0472 794.95 7.3298 1048.07 0.0000 1810.72 0.0000 795.86 6.2852 1049.04 6.8955 1836.06 2.1061 810.06 10.5363 1050.41 3.4495 810.29 8.4297 1063.66 5.7739 344.28 7.3765 1077.00 0.0000 810.76 10.5391 1077.34 4.6393 815.77 0.0000 1085.87 8.1410 1048.07 0.0000 1093.63 4.6634 832.01 8.5036 1099.45 5.2562 834.85 7.4492 1112. 07 4.3973 835.71 11. 7099 1112. 84 836.80 0.0000 1115. 54 8.4521 846.75 0.0000 1120.29 7.0537 846.77 8:5534 1120. 55 7.0542 856.80 0.0000 1221.41 7.0562 860.56 7.5244 1129. 67 7.0742 871.09 9.7134 1131. 51 0.0000 873.19 9. 7211 1147. 95 0.0000 875.33 0.0000 1173.23 4.4800 879.38 5.4134 1177.95 10.7673 880.51 8.6650 1189.05 6.3015 883.24 3.2528 1204.77 7.2349 884.68 4.3394 1221.41 5.4525 889.28 5.4338 1231.02 8.2013 894.76 7.6229 1235.36 0.0000 898.04 8 .1772 1238.28 10.0446 900. 72 8.1854 1260.41 0.0000 903.28 0.0000 1271.87 8.2958 911.20 5.4781 1274.44 4.4276 912.08 5.4799 1274.54 4.4279 923.98 0.0000 1291.59 7.4146 926.50 7.7124 1298.22 0.0000 929 .11 11. 0282 1312 .11 0.0000 937.49 4.4246 1332.49 7. 4971 944.13 0.0000 1362.66 0.0000 946.00 3.3286 1365.19 3.7810 949.00 14.4393 1368.63 0.0000 667.71 0.0000 1384.29 2.8499 962. 31 5.0219 1408.01 4.7787 964.08 8.3749 1457.56 0.0000 966.17 18.4383 1460.82 2.9055 911. 20 16.7786 1489.16 3.9009 968. 97 16.7786 1505.03 2.9370 983.53 0.0000 1584.12 3.9895 984.45 0.0000 1596.21 0.0000 Page 3723of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:19:12.36 ******************************************************************************** GEL Laborator\es LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM41.CNF;ll9 Background date : Z-OCT-2016 11:02:18. Sample date 30-NOV-2015 11:19:00 Acquisition date : 3-0CT-2016 09:17:13. Sample ID G405235037 Sample quantity 1.78756E+02 GRAM Detector name : GAM41 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:05.72 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3724 of 5809 Energy 46.55* 61.13 63.48* 74.97* 77.27* 87.41 90.02 93.06* 143.25* 186.02* 210.01 230.38 238.99* 242.05 277.81 286.06 296.16 301.08 322.00 329.47* 338.97 352.20* 444.91 462.81* 511. 40* 583.76* 609.85* 620.72 679.71 728.45* 767.97 886.62* 912.01* 965. 51 *BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 39 25 82 179 223 92 62 110 24 101 26 23 275 81 33 22 90 19 19 14 38 187 11 39 31 77 120 19 8 17 37 6 43 25 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 87 121 111 168 109 79 94 130 112 95 83 52 70 44 40 57 62 70 44 52 58 55 18 21 38 32 32 15 18 20 37 4 10 12 0.98 1. 32 1. 04 1.14 0.85 1.12 1.19 1.18 3.86 1.20 0.92 0.87 0.95 1. 50 1. 63 0.89 1. 27 1. 00 1. 82 0.89 0.92 1.14 1. 41 1. 42 1.23 1. 53 1. 68 2.75 0.83 1.12 6.58 0.65 1.13 1. 69 93.39 122.54 127.24 150.21 154.81 175.10 180.30 186.39 286.74 372.24 420.23 460.95 478.17 484.29 555.80 572.28 592.49 602.32 644.16 659.08 678.08 704.55 889.94 925.74 1022.90 1167. 60 1219.79 1241.53 1359.50 1456.98 1536.03 1773.35 1824.14 1931.15 90 120 120 145 145 173 178 183 281 365 415 458 473 482 552 568 584 596 637 653 674 699 886 919 1016 1159 1211 1234 1353 1450 1520 1770 1817 1925 7 1.09E-02 47.4 18 6.90E-03 69.8 18 2.27E-02 25.8 15 4.96E-02 13.8 15 6.19E-02 9.9 5 2.56E-02 17.8 6 1. 72E-02 27. 9 10 3.06E-02 24.4 11 6.73E-03 89.4 14 2.81E-02 23.8 9 7.llE-03 67.3 8 6.36E-03 57.8 9 7.65E-02 8.3 7 2.24E-02 17.8 9 9.03E-03 38.7 10 6.08E-03 68.1 11 2.50E-02 19.6 .12 5.26E-03 90.9 11 5.28E-03 71.4 9 3. 80E-03101. 0 12 l.04E-02 44.3 13 5 .19E-02 11. 0 7 3.05E-03 72.2 12 1.09E-02 29.6 14 8.63E-03 54.5 14 2.15E-02 19.5 14 3.35E-02 13.7 12 5.24E-03 47.1 9 2.22E-03101.9 10 4.70E-03 56.2 24 1.03E-02 45.7 7 1. 55E-03 78. 4 12 1. 20E-02 21. 4 12 7.02E-03 33.8 Fit 1.95E+OO 3.45E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969.88* 38 7 1. 57 1939.89 1936 9 1.05E-02 21. 9 36 0 1053.89 15 0 2.39 2107.93 2103 9 4.17E-03 25.8 37 0 1121.45 15 1. 57 2243.08 2235 12 7.16E-03 3q.0 38 0 1204.21 9 26 5.89 2408.65 2390 21 2.46E-03148.2 39 0 1207.05 15 5 1. 54 2414.33 2410 10 4.17E-03 38.0 40 0 1237.81 22 7 3.75 2475.86 2469 14 6. llE-03 33.2 41 0 1264.29 10 5 0.78 2528.85 2521 13 2.65E-03 63.0 42 0 1461. 78* 275 0 1. 92 2923. 96 2917 14 7.63E-02 6.1 43 0 1766.23 18 3 2.53 3533.15 3527 11 5.05E-03 29.4 Flag: "*" = Peak area was modified by background subtraction Page 3725of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:19:14 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 11:19:00 G405235037 Acquisition date : Sample quantity Sample geometry .. Detector geometry: 3-0CT-2016 09:17:13 178.76 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID
  • GAMMA41 0 01:00:00.00 1. 50 keV No Empirical 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3726of5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 HG-203 '279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:05.72 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 8.926E-01 1.191E+Ol 1+.191E+Ol 12.18 OK Y-91 1204.77 0. 26* 1.058E+OO 1.372E+Ol 5.267E+02 296.36 OK RH-106 621. 93 9.93* 1.938E+OO 4.592E-01 8.153E-01 94.29 OK 1050.41 1. 56 1.196E+OO Line Not Found Absent RU-106 621. 93 9.93* 1. 938E+OO 4.592E-01 8.153E-01 94.29 OK 1050.41 1.56 1.196E+OO Line Not Found Absent CD-109 88.03 3.70* 7.447E+OO 1.367E+OO 2. l 72E+OO 55.08 OK SN-126 64.28 9.60 7.794E+OO 6.753E-01 6.753E-01 51. 53 OK 86.94 8.90 7.447E+OO 5.685E-01 5.685E-01 55.08 OK 87.57 37.00* 7.447E+OO l.367E-Ol l.367E-01 55.08 OK HG-203 70.83 3.69 7.737E+OO Line Not Found Absent 72. 87 6.19 7. 711E+OO Line Not Found Absent 279.20 81.56* 3.902E+OO 3.626E-02 3.541E+00 115. 06 OK TL-208 277.37 6.60 3.907E+OO Line Not Found <<INT Reject 583.19 85.00* 2.050E+OO 2.099E-01 2.099E-01 38.95 OK 860.56 12.50 1. 434E+OO Line Not Found Absent PB-210 46.54 4.25* 7.553E+OO 7.803E-01 8. OllE-01 94.74 OK BI-211 72.87 1.23 7. 711E+OO Line Not Found Absent 351.06 12.92* '3.212E+OO 4.002E-01 4.002E-01 222.31 OK PB-212 74.82 10.28 7.681E+OO 9. 891E-01 9.891E-01 41. 37 OK 77.11 17.10 7.644E+OO 1.032E+OO 1.032E+OO 19.74 OK 238.63 43.60* 4.381E+OO 7.662E-01 7.662E-01 16.56 OK 300.09 3.30 3.659E+OO 8.094E-01 8.094E-01 181. 75 OK BI-214 609.32 45.49* 1.969E+OO 6.315E-01 6.317E-01 27.31 OK 1120.29 14.92 l.127E+OO 6.586E-01 6.589E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent PB-214 74.82 5.80 7.683E+OO Line Not Found <<INT Reject 77 .11 9.70 7.644E+OO 1.819E+OO 1.820E+OO 19.74 OK 87.09 3.41 7.454E+OO Line Not Found <<INT Reject 242.00 7.25 4.340E+OO Line Not Found <<INT Reject 295.22 18.42 3.708E+OO 6.813E-01 6.816E-01 39.20 OK 351. 93 35.60* 3.214E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 OK 1120.29 14.92 1.127E+OO 6.586E-01 6.589E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent RA-224 240.99 4.10* 4.340E+OO 1.197E+OO 1.197E+OO 81. 47 OK RA-226 609.32 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 OK 1120. 29 14.92 1.127E+OO 6.586E-01 6.589E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent AC-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 OK 794.95 4.25 1.543E+OO Line Not Found Absent 835. 71 1. 61 l.473E+OO Line Not Found Absent 911. 20 25.80* 1.360E+OO 5.447E-01 5.447E-01 42.74 OK 968. 97 15.80 1.285E+OO 8.194E-01 8.194E-01 43.89 OK RA-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 OK 794.95 1.543E+OO Line Not Found Absent 835. 71 1. 61 l.473E+OO Line Not Found Absent Page 3727 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status ..911.20 25.80* l.360E+OO 5.447E-01 5.4t\7E-01 42.74 OK 968. 97 15.80 1. 285E+OO 8.194E-01 8.194E-01 43.89 OK TH-228 74.82 10.28 7.681E+OO 9. 891E-01 9. 8 91E-01 41. 37 OK 77 .11 17.10 7.644E+OO l.032E+OO 1.032E+OO 19.74 OK 238.63 43.60* 4.381E+OO 7.662E-01 7.662E-01 16.56 OK 300.09 3.30 3.659E+OO 8.094E-01 8.094E-01 181. 7 5 OK TH-230 609.32 45.49* l.969E+OO 6.315E-01 6.315E-01 27.31 OK 1120.29 14.92 1.127E+OO 6.586E-01 6.586E-01 71.98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent PA-231 283.69 1. 70 3.838E+OO Line Not Found Absent 301.36 5.35* 3.659E+OO 4.993E-01 4.993E-01 181.75 OK TH-232 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 OK 835.71 1. 61 l.473E+OO Line Not Found Absent 911. 20 25.80* 1.360E+OO 5.447E-01 5.447E-01 42.74 OK 968. 97 15.80 1. 285E+OO 8.194E-01 8.194E-01 43.89 OK TH-234 63.29 3.70* 7.794E+OO 1. 752E+OO 1. 752E+OO 51. 53 OK 92.59 4.23 7.320E+OO 2 .112E+OO 2 .112E+OO 48.79 OK U-234 609.32 45.49* l .'969E+OO 6.315E-01 6.315E-01 27.31 OK 1120. 29 14.92 l.127E+OO 6.586E-01 6.586E-01 71. 98 OK 1764.49 15.30 7.620E-01 Line Not Found Absent U-235 89.96 3.47 7.390E+OO 1.435E+OO l.435E+OO 55.85 OK 93.35 5.60 7.320E+OO 1.595E+OO 1.595E+OO 48.79 OK 143.76 10.96* 6.105E+00 2.047E-01 2.047E-01 178.90 OK 163.33 5.08 5.667E+OO Line Not Found Absent 185.72 57.20 5.223E+OO l.858E-01 1.858E-01 47.55 OK 205.31 5.01 4.887E+OO Line Not Found Absent U-238 63.29 3.70* 7.794E+OO 1. 752E+OO 1.752E+OO 51. 53 OK 92.59 4.23 7.320E+OO 2.112E+00 2 .112E+OO 48.79 OK AM-243 43.53 5.90 7.421E+OO Line Not Found Absent 74.66 67.20* 7.681E+OO 1. 513E-01 l.513E-01 41. 37 OK ANH-511 511. 00 100.00* 2.313E+OO 6.463E-02 6.463E-02 108.92 OK Flag: "*" = Keyline Page 3728of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:19:15.40 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l * *Acquisition date 3-0CT-2016 09:17:13 Sensitivity 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:05.72 Half life ratio : ***** *
  • Sample date 30-NOV-2015 11:19:00 Analyst initials: MXRl * *Sample ID G405235037 Sample Quantity 1.7876E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1 . 96-sigma ) K-40 1.191E+Ol 1.422E+OO Y-91 5.267E+02 1.530E+03 RH-106 8.153E-01 7.533E-01 RU-106 8.153E-01 7.533E-01 CD-109 2.172E+OO 1.172E+OO SN-126 l.367E-01 7.381E-02 HG-203 3.541E+OO 3.993E+OO TL-208 2.099E-01 8.012E-02 PB-210 8. OllE-01 7.438E-01 BI-211 4.002E-01 8.719E-01 PB-212 7.662E-01 1.243E-01 BI-214 6.317E-01 1. 691E-01 PB-214 8.269E-01 1. 779E-01 RN-222 6.317E-01 1.691E-01 RA-224 1.197E+OO 9.555E-01 RA-226 6.317E-01 1. 691E-01 AC-228 5.447E-01 2.281E-01 RA-228 5.447E-01 2. 281E-01 TH-228 7.662E-01 l.243E-01 TH-230 6.315E-01 l.690E-01 PA-231 4.993E-01 8.893E-01 TH-232 5.447E-01 2.281E-01 TH-234 1. 752E+OO 8.849E-01 U-234 6.315E-01 1.690E-01 U-235' 2.047E-01 3.589E-01 U-238 1. 752E+OO 8.849E-01 AM-243 1. 513E-01 6.135E-02 ANH-511 6.463E-02 6.899E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 3729of5809 Key-Line Activity (pCi/GRAM 4.951E+OO 2 .148E-02 K.L. Cnt Uncert ( 1. 96-sigma) l.183E+Ol 5.785E-02 MDA (pCi/GRAM 4.971E-01 1.627E+02 9.015E-01 9.015E-01 1.205E+OO 8.663E-02 4.637E+OO 6.035E-02 6. 551E-01 3.181E-01 8.523E-02 1.118E-01 2.782E-01 1.118E-01 8.243E-01 l .118E-01 2.023E-01 2.023E-01 8.523E-02 1.118E-01 6.810E-01 2.023E-01 8.832E-01 1.118E-01 2.927E-01 8.832E-01 4.876E-02 4.164E-02 MDA (pCi/GRAM 2.443E+Ol 1.189E-01 NOT IDENT. NOT IDENT.

NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 -9.950E-03 2. 081E-02 4.180E-02 NOT IDENT. SC-46 1.846E-02 3.663E-01 6.833E-01 FAIL ABUN V-48 O.OOOE+OO 1. 67 5E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 4.474E+02 O.OOOE+OO SHORT HLIF MN-54 -1.910E-02 5.795E-02 l.123E-01 NOT IDENT. C0-56 1.179E-01 5.198E-01 1. 079E+OO FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 9.342E-04 3.829E-02 7.865E-02 NOT IDENT. C0-58 -3.216E-01 5 .118E-01 9.465E-01 NOT IDENT. FE-59 4.637E-01 6.280E+OO 1.318E+Ol NOT IDENT. C0-60 -1.435E-02 3.329E-02 6.186E-02 NOT IDENT. ZN-65 5.808E-02 1.972E-01 3.692E-01 NOT IDENT. GE-68 4.767E-01 2.351E+OO 4.899E+OO NOT IDENT. AS-73 5.366E-01 2.lOOE+OO 4.135E+00 NOT IDENT. AS-74 O.OOOE+OO 6.310E+03 O.OOOE+OO SHORT HLIF SE-75 -5.786E-02 l.594E-01 3.076E-01 NOT IDENT. BR-77 O.OOOE+OO 2.365E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.176E+02 O.OOOE+OO SHORT HLIF RB-83 2.332E-02 5.549E-01 1. lOlE+OO NOT IDENT. KR-85 9.059E+OO 6.785E+OO l.426E+Ol NOT IDENT. SR-85 1. 041E+OO 7.804E-01 1.640E+OO NOT IDENT. RB-86 O.OOOE+OO 3. 723E+04 0.000E+OO SHORT HLIF Y-88 -7.732E-02 1.lOOE-01 1.512E-01 NOT IDENT. NB-94 3.035E-03 3. 221E-02 6.550E-02 NOT IDENT. NB-95 9.359E-01 8.413E-01 1. 948E+OO NOT IDENT. NB-95M -8. 811E-01 2.324E+OO 3.952E+00 NOT IDENT. ZR-95 -3.235E-01 1.504E+OO 2.758E+OO' NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 268E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.423E-02 2.746E-02 5.414E-02 NOT IDENT. RH-102 4.448E-03 4.258E-02 9.179E-02 FAIL ABUN RU-103 6.983E-01 4.765E+OO 9.746E+OO FAIL ABUN AG-108M 9.877E-03 2.190E-02 4.602E-02 NOT IDENT. AG-llOM -1.078E-01 1.126E-01 l.638E-01 FAIL ABUN SN-113 -l.763E-01 2.004E-01 3.466E-01 NOT IDENT. CD-115 O.OOOE+OO 3.426E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1.131E+05 O.OOOE+OO SHORT HLIF TE-123M -8.763E-02 1.073E-01 2.037E-01 NOT IDENT. SB-124 -1.014E+OO 1.570E+OO 2.882E+OO NOT IDENT. SB-125 6. 964E-02 8.785E-02 1.897E-01 FAIL ABUN TE-125M -l.005E+Ol 2.120E+02 4.356E+02 NOT IDENT. I-126 O.OOOE+OO l.283E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.709E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.987E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 8.087E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 2.020E+27 O.OOOE+OO SHORT HLIF BA-133 1. 961E-03 3.948E-02 6.973E-02 FAIL ABUN I-133 O.OOOE+OO 1. 580E+41 0.000E+OO SHORT HLIF CS-134 2.644E-02 4.629E-02 l.015E-01 NOT IDENT. CS-135 5.875E-02 1.113E-01 2.332E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.886E+05 O.OOOE+OO SHORT HLIF BA-137M l.295E-02 3.584E-02 7.557E-02 NOT IDENT. CS-137 l.368E-02 3.786E-02 7.983E-02 NOT IDENT. CE-139 -4.497E-02 9.740E-02 l.898E-01 NOT IDENT. BA-140 O.OOOE+OO 2.103E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.695E+05 0.000E+OO SHORT HLIF CE-141 5. 951E+OO 2.498E+Ol 4.682E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 3.493E-02 2.796E-01 5.776E-01 NOT IDENT. PM-144 2.328E-02 5.124E-02 l.105E-01 NOT IDENT. PR-144 2.387E+00 4.422E+OO 9. 645.E+OO NOT IDENT. PM-146 -3.748E-03 3.535E-02 6.848E-02 NOT IDENT. ND-147 0.000E+OO 5.077E+07 O.OOOE+OO SHORT HLIF PM-147' 3.548E+02 6.434E+02 l.369E+03 NOT IDENT. PM-149 O.OOOE+OO l.335E+41 O.OOOE+OO SHORT HLIF EU-150 2.641E-03 2.134E-02 4.085E-02 FAIL ABUN EU-152 2. 960E-02 8.183E-02 l.533E-01 FAIL ABUN GD-153 -4.303E-02 l.307E-01 2.376E-01 NOT IDENT. EU-154 6.833E-02 l.393E-01 2.917E-01 NOT IDENT. EU-155 6.519E-02 7.019E-02 l.551E-01 FAIL ABUN TB-160 8.906E-01 1. 995E+OO 4.307E+OO FAIL ABUN H0-166M 2.744E-03 5.261E-02 l.080E-01 NOT IDENT. TM-171 6.914E-01 4.234E+OO 8.305E+OO NOT IDENT. Page 3730of5809 HF-172 -6.034E-02 1.846E-01 3.675E-01 FAIL ABUN LU-172 8.908E-03 7.132E-02 l.480E-01 FAIL ABUN LU-176 -3.688E-03 l.887E-02 3.673E-02 FAIL ABUN HF-181 -1.086E+OO 4. lllE+OO 7.737E+OO NOT IDENT. TA-182 8.428E-01 1.028E+OO 2.265E+OO FAIL ABUN RE-183 -3.351E-01 9.872E-01 1.693E+OO NOT IDENT. RE-184 -9.713E+OO 2.597E+Ol 5.073E+Ol NOT IDENT. W-188 -6.489E+Ol 1. 449E+02 l.820E+02 FAIL ABUN IR-192 2.320E-01 4.392E-01 8.425E-01 FAIL ABUN BI-207 5.354E-02 1.030E-01 F4\IL ABUN PB-211 4. 972E-02 5.259E-01 1.051E+OO NOT IDENT. BI-212 6.954E-01 7.661E-01 l.202E+OO FAIL ABUN RN-219 -3.126E-01 3.188E-01 5.408E-01 NOT IDENT. RA-223 -6.418E-01 7.388E-01 7.995E-01 FAIL ABUN AC-227 -4.557E-02 l.756E-01 3.421E-01 FAIL ABUN TH-227 -4.557E-02 l.756E-01 3.421E-01 FAIL ABUN TH-229 -8.083E-02 3.831E-01 7.562E-01 FAIL ABUN TH-231 -6.418E-01 7.388E-01 7.995E-01 FAIL ABUN PA-233 1.631E-02 4.587E-02 9.512E-02 FAIL ABUN PA-234 -2.836E-Ol 2.629E-01 4.289E-01 NOT IDENT. PA-234M 3.633E+OO 4.330E+00 9.626E+OO NOT IDENT. NP-237 1. 631E-02 4.587E-02 9.512E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -4.034E-02 1. 757E-01 3.567E-01 FAIL ABUN PU-239 1. 881E+02 2.415E+02 5.190E+02 .NOT IDENT. AM-241 l.506E-02 4.595E-02 8.377E-02 NOT IDENT. CM-243 -3.773E-02 6.573E-02 1.310E-01 FAIL ABUN BK-247 -4.058E-02 5. 590E'-Q,2 l.029E-01 NOT IDENT. CM-247 -2.013E-02 2.738E-02 4.834E-02 FAIL ABUN CF-249 3.363E-02 3.060E-02 6.815E-02 NOT IDENT. CF-251 2.247E-02 9.675E-02 l.983E-01 FAIL ABUN Page 3731 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:19:13.13 Nuclide Line Activity Report Nuclide Type: . Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 270 10.66* 8.926E-01 l.191E+Ol 1.191E+Ol 12.18 Y-91 1204.77 9 0.26* l.058E+OO 1.372E+Ol 5.267E+02 296.36 RH-106 621.93 21 9.93* 1.938E+OO 4.592E-01 8.153E-01 94.29 1050.41 ------1. 56 l .196E+OO ------Line Not Found ------RU-106 621. 93 21 9.93* 1.938E+OO 4.592E-01 8.153E-01 94.29 1050.41 ------1. 56 l.196E+OO ------Line Not Found ------CD-109 88.03 131 3.70* 7.447E+OO 1.995E+OO 3.169E+OO 35.67 SN-126 64.28 120 9.60 7.794E+OO 6.753E-01 6.753E-01 51. 53 86.94 131 8.90 7.447E+OO 8.295E-01 8.295E-01 35.67 87.57 131 37.00* 7.447E+OO 1.995E-01 l.995E-01 35.67 HG-203 70.83 ------3.69 7.737E+OO ------Line Not Found ------72. 87 ------6.19 7. 711E+OO ------Line Not Found ------279.20 40 81.56* 3.902E+OO 5.325E-02 5.199E+OO 77.37 TL-208 277.37 40 6.60 3.902E+OO 6.580E-01 6.580E-01 77.37 583.19 87 85.00* 2.050E+OO 2.099E-01 2.099E-01 38.95 860.56 ------12.50 1.'434E+OO ------Line Not Found ------PB-210 46.54 60 4.25* 7.553E+OO 7.803E-01 8. OllE-01 94.74 BI-211 72. 87 ------1. 23 7.711E+00 ------Line Not Found ------351.06 225 12.92* 3.212E+OO 2.277E+OO 2.277E+OO 21. 96 PB-212 74.82 258 10.28 7.681E+OO 1.373E+OO 1.373E+OO 27.70 77 .11 321 17.10 7.644E+OO 1.032E+OO 1.032E+OO 19.74 238.63 348 43.60* 4.381E+OO 7.662E-01 7.662E-01 16.56 300.09 23 3.30 3.659E+OO 8.094E-01 8.094E-01 181.75 BI-214 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 1120.29 26 14.92 l.127E+OO 6.586E-01 6.589E-01 71. 98 1764.49 ------15.30 7.620E-01 ------Line Not Found ------PB-214 74.82 258 5.80 7.681E+OO 2.434E+OO 2.435E+OO 27.70 77 .11 321 9.70 7.644E+OO 1.819E+OO l.820E+00 19.74 87.09 131 3.41 7.447E+OO 2.165E+OO 2.166E+00 35. 67 242.00 102 7.25 4.340E+OO 1.358E+OO 1.359E+OO 35.52 295.22 111 18.42 3.708E+OO 6.813E-01 6.816E-01 39.20 351. 93 225 35.60* 3.212E+OO 8.266E-01 8.269E-01 21. 96 RN-222 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 1120.29 26 14.92 l.127E+OO 6.586E-01 6.589E-01 71. 98 1764.49 ------15.30 7.620E-01 ------Line Not Found ------RA-224 240.99 102 4.10* 4.340E+OO 2.402E+OO 2.402E+OO 35.52 RA-226 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.317E-01 27.31 1120.29 26 14.92 l.127E+OO 6.586E-01 6.589E-01 71. 98 1764.49 ------15.30 7.620E-01 ------Line Not Found ------AC-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 45 11. 27 3.317E+OO 5.105E-01 5.105E-01 88.51 794.95 ------4.25 1.543E+OO ------Line Not Found ------835.71 ------1. 61 l.473E+OO ------Line Not Found ------911.20 45 25.80* 1.360E+OO 5.447E-01 5.447E-01 42.74 968. 97 40 15.80 l.285E+OO 8.194E-01 8.194E-01 43.89 RA-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 45 11.27 3.317E+OO 5.105E-01 5.105E-01 88.51 Page 3732 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235037 Acquisition date 3-0CT-2016 09:17:13 Nuclide Type: Nuclide Uncorrected Decay Corr 2-Sigma Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 ------4.25 1. 543E+O,O ------Line Not Found ------835. 71 ------1. 61 1.473E+OO ------Line Not Found ------911. 20 45 25.80* l.360E+OO 5.447E-01 5.447E-01 42.74 968. 97 40 15.80 1.285E+OO 8.194E-01 8.194E-01 43.89 TH-228 74.82 258 10.28 7.681E+OO 1.373E+OO 1.373E+OO 27.70 77 .11 321 17.10 7.644E+OO l.032E+OO 1.032E+OO 19.74 238.63 348 43.60* 4.381E+OO 7.662E-01 7.662E-01 16.56 300.09 23 3.30 3.659E+OO 8.094E-01 8.094E-01 181.75 TH-230 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.315E-01 27.31 1120.29 26 14.92 1.127E+OO 6.586E-01 6.586E-01 71. 98 1764.49 ------15.30 7.620E-01 ------Line Not Found ------PA-231 283.69 ------1. 70 3.838E+OO ------Line Not Found ------301.36 23 5.35* 3.659E+OO 4.993E-01 4.993E-01 181.75 TH-232 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 45 11. 27 3.317E+OO 5.105E-01

  • 5 .105E-01 88.51 835. 71 ------1. 61 1.473E+OO ------Line Not Found ------911.20 45 25.80* 1.360E+OO 5.447E-01 5.447E-01 42.74 968. 97 40 15.80 l.285E+OO 8.194E-01 8.194E-01 43.89 TH-234 63.29 120 3.70* 7.794E+OO 1. 752E+OO 1. 752E+OO 51. 53 92.59 156 4.23 7.320E+OO 2 .112E+OO 2 .112E+OO 48.79 U-234 609.32 135 45.49* 1. 969E+OO 6.315E-01 6.315E-01 27.31 1120.29 26 14.92 l.127E+00 6.586E-01 6.586E-01 71. 98 1764.49 ------15.30 7.620E-01 ------Line Not Found ------U-235 89. 96 88 3.47 7.390E+OO 1.435E+OO 1.435E+OO 55.85 93.35 156 5.60 7.320E+OO 1.595E+OO 1.595E+OO 48.79 143.76 33 10.96* 6.105E+OO 2.047E-01 2.047E-01 178.90 163.33 ------5.08 5.667E+OO ------Line Not Found ------185. 72 132 57.20 5.223E+OO 1.858E-01 1.858E-01 47.55 205.31 ------5.01 4.887E+OO ------Line Not Found ------U-238 63.29 120 3.70* 7.794E+OO 1. 7 52E+OO 1. 7 52E+OO 51. 53 92.59 156 4.23 7.320E+OO 2 .112E+OO 2 .112E+OO 48.79 AM-243 43.53 ------5.90 7.421E+OO ------Line Not Found ------74.66 .258 67.20* 7. 681E+OO 2.lOlE-01 2. lOlE-01 27.70 ANH-511 . 511. 00 36 100.00* 2.313E+OO 6.463E-02 6.463E-02 108.92 Flag: "*" Key line Page 3733 of 5809 Summary of Nuclide Activity Sample ID : G405235037 Acquisition date Page : 3 3-0CT-2016 09:17:13 Total number of lines in spectrum 43 Number of unidentified lines 8 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 Y-91 RH-106 RU-106 CD-109 SN-126 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 58.51D 371.80D 371. 80D 461. 40D 2.30E+05Y 46.59D 1. 41E+l0Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600. OOY 1600. OOY 1. 41E+l0Y 1600. OOY l.41E+l0Y 1. 41E+10Y 1.41E+10Y 7.54E+04Y 7.04E+08Y l.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 38.4 1. 78 1. 78 1. 59 1. 00 97.6 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 i: 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.191E+Ol 1. 372E+Ol 4.592E-01 4.592E-01 1.995E+00 l.995E-01 5.325E-02 2.099E-01 7.803E-01 2.277E+OO 7.662E-01 6.315E-01 8.266E-01 6.315E-01 2.402E+OO 6.315E-01 5.447E-01 5.447E-01 7.662E-01 6.315E-01 4.993E-01 5.447E-01 1. 752E+OO 6.315E-01 2.047E-01 1. 752E+OO 2.lOlE-01 6.463E-02 4.609E+Ol 4.609E+Ol
  • Decay Corr pCi7GRAM l.191E+Ol 5.267E+02 8.153E-01 8.153E-01 3.169E+OO 1.995E-01 5.199E+OO 2.099E-01 8. OllE-01 2.277E+00 7.662E-01 6.317E-01 8.269E-01 6.317E-01 2.402E+OO 6.317E-01 5.447E-01 5.447E-01 7.662E-01 6.315E-01 4.993E-01 5.447E-01 1. 752E+OO 6.315E-01 2.047E-01 1. 7 52E+00 2.lOlE-01 6.463E-02 5.661E+02 5. 661E+02 81. 40% Decay Corr 2-Sigma Error 0.145E+Ol 15.61E+02 7.687E-01 7.687E-01 1.130E+00 0.712E-01 4.023E+OO 0.818E-01 7.590E-01 0.500E+OO l.269E-01 1.725E-01 1. 816E-01 1. 725E-01 0.853E+OO 1.725E-01 2.328E-01 2.328E-01 1. 2 69E-01 l.725E-01 9.074E-01 2.328E-01 0.903E+OO 1.725E-01 3.662E-01 0.903E+00 0.582E-01 7.040E-02 "M" Manually accepted 2-Sigma %Error 12.18 296.36 94.29 94.29 35.67 35.67 77.37 38.95 94.74 21. 96 16.56 27.31 21. 96 27.31 35.52 27.31 42.74 42.74 16.56 27.31 181. 7 5 42.74 51. 53 27.31 178.90 51. 53 27.70 108.92 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3734of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235037 Acquisition date : 3-0CT-2016 09:17:13 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 2 61.13 37 179 1. 32 122.54 120 18 6.90E-03 **** 7.80E+00 T 0 210.01 33 107 0.92 420.23 415 9 7.llE-03 **** 4.81E+OO T 0 230.38 29 66 0.87 460.95 458 8 6.36E-03 **** 4.50E+00 0 286.06 27 71 572.28 568 10 6.08E-03 **** 3.81E_,_00 T 0 322.00 23 54 1. 82 644.16 637 11 5.28E-03 **** 3.46E+OO T 0 329.47 17 63 0.89 659.08 653 9 3.80E-03 **** 3.40E+00 T 0 444.91 13 21 1. 41 889.94 886 7 3.05E-03 **** 2.62E+OO 0 462.81 45 24 1. 42 925.74 919 12 1.09E-02 59.2 2.53E+OO T 0 679. 71 9 20 0.83 1359. 50 1353 9 2.22E-03 **** 1. 78E+OO 0 728. 45 18 22 1.12 1456.98 1450 10 4.70E-03 **** l.67E+OO T 0 767.97 40 40 6.58 1536.03 1520 24 1.03E-02 91.4 1. 59E+OO T 0 8 8 6. 62 6 4 0.65 1773.35 1770 7 1.55E-03 **** 1. 40E+OO 0 965.51 26 12 1. 69 1931.15 1925 12 7.02E-03 67.6 1.29E+OO T 0 1053.89 15 0 2.39 2107.93 2103 9 4.17E-03 51.6 1.19E+OO 0 1207.05 15 5 1. 54 2414.33 2410 10 4.17E-03 76.0 1. 06E+OO 0 1237.81 22 7 3.75 2475.86 2469 14 6.llE-03 66.5 1. 03E+00 T 0 1264.29 10 5 0.78 2528.85 2521 13 2.65E-03 **** 1.0lE+OO 0 1766.23 17 3. 2. 53 3533.15 3527 11 5.05E-03 58.8 7. 61E-01 Flags: "T" = Tentatively associated Page 3735 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:19:27.21 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • 4 DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l * *Acquisition date 3-0CT-2016 09:17:13 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:05.72 Half life ratio : ***** *
  • Sample date 30-NOV-2015 11:19:00 Nuclide Library : SOLID *
  • Sample ID G405235037 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7876E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 Y-91 RH-106 RU-106 CD-109 SN-126 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 u-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.880E-01 O.OOOE+OO 3.958E-01 3.958E-01 5.662E-01 4.102E-02 2 .131E+OO 2. 67 6E-02 3.069E-01 l.445E-01 3.941E-02 4.926E-02 1.339E-01 4. 92 6E-02 3.778E-01 4.926E-02 8.443E-02 8.443E-02 3.941E-02 4.924E-02 3.094E-01 8.443E-02 4.195E-01 4.924E-02 1.371E-01 4.195E-01 2.315E-02 1.823E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 3736of5809 Le (pCi/GRAM 1.093E+Ol 5.224E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 3737 of 5809 1. 321E-02 2.877E-01 O.OOOE+OO O.OOOE+OO 4.823E-02 4.756E-01 O.OOOE+OO 3.690E-02 3.937E-01 5.502E+OO 2.424E-02 1.603E-01 2.109E+OO 1.953E+OO O.OOOE+OO 1. 386E-01 O.OOOE+OO O.OOOE+OO 4.812E-01 6.498E+OO 7.474E-01 O.OOOE+OO 1. 766E-02 2.932E-02 8.702E-01 1.819E+OO l.191E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.538E-02 3.939E-02 4.236E+OO 2.053E-02 6.831E-02 l.530E-01 O.OOOE+OO O.OOOE+OO 9.416E-02 9.109E-01 8.564E-02 2.039E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.163E-02 O.OOOE+OO 4.481E-02 1.071E-01 O.OOOE+OO O.OOOE+OO 3. 411E-02 3.603E-02 8.841E-02 O.OOOE+OO O.OOOE+OO 2.190E+Ol O.OOOE+OO 2.700E-01 4.909E-02 4.287E+OO 3.025E-02 O.OOOE+OO 6.434E+02 O.OOOE+OO l.852E-02 6.938E-02 1.115E-01 l.283E-01 7.274E-02 1. 888E+00 4. 7 62E-02 3.913E+00 1.722E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT I DENT.* NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3738of5809 6.306E-02 1. 656E-02 3.399E+00 9.997E-01 7.960E-01 2.070E+Ol 8.240E+Ol 3.836E-01 4.478E-02 .; 4. 694E-01 5.480E-01 2.385E-01 3.556E-01 l.556E-01 1.556E-01 3.506E-01 3.556E-01 4.312E-02 l.773E-01 4.256E+OO 4.312E-02 O.OOOE+OO 1.666E-01 2.441E+02 3. 960E-02 6.118E-02 4.642E-02 2.124E-02 3.098E-02 9.250E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:19:32.98 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235037.CNF;l * *Acquisition date 3-0CT-2016 09:17:13 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:05.72 Half life ratio : ***** *
  • Sample date 30-NOV-2015 11:19:00 Nuclide Library : SOLID *
  • Sample ID G405235037 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7876E+02 GRAM *
  • Quantity Err(%) : 1.1188E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.191E+Ol 1.747E+OO 1.747E+OO Y-91 5.267E+02 l.530E+03 1.530E+03 RH-106 8.153E-01 7.574E-01 7.574E-01 RU-106 8.153E-01 7.574E-01 7.574E-01 CD-109 2.172E+OO l.203E+OO 1.203E+OO SN-126 1.367E-01 7.540E-02 7.540E-02 HG-203 3. 541E+OO 4.013E+OO 4.013E+OO TL-208 2.099E-01 8.210E-02 8.210E-02 PB-210 8.0llE-01 7.505E-01 7.505E-01 BI-211 4.002E-01 9.023E-01 9.023E-01 PB-212 7.662E-01 l.440E-01 l.440E-01 BI-214 6.317E-01 1.773E-01 1.773E-01 PB-214 8.269E-01 1.914E-01 1.914E-01 RN-222 6.317E-01 1.773E-01 1.773E-01 RA-224 1.197E+OO 9.744E-01 9.744E-01 RA-226 6.317E-01 1.773E-01 1.773E-01 AC-228 5.447E-01 2. 371E-01 2. 371E-01 RA-228 5.447E-01 2. 371E-01 2. 371E-01 TH-228 7.662E-01 1. 440E-01 1.440E-01 TH-230 6.315E-01 1. 772E-01 1. 772E-01 PA-231 4.993E-01 8. 964E-01 8.964E-01 TH-232 5.447E-01 2. 371E-01 2. 371E-01 TH-234 1. 752E+OO 9.852E-01 9.852E-01 U-234 6.315E-01 1. 772E-01 l.772E-01 U-235 2.047E-01 3. 596E-01 3. 596E'-01 U-238 1.752E+OO 9.852E-01 9.852E-01 AM-243 1. 513E-01 6.427E-02 6.427E-02 ANH-511 6.463E-02 6.921E-02 6. 921E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1 . 96-sigma) BE-7 4.951E+OO l.184E+Ol 1.204E+Ol NOT IDENT. NA-22 2.148E-02 5.788E-02 5.868E-02 NOT IDENT. Page 3739of5809 NA-24 1.000E+41 2.350E+41 O.OOOE+OO SHORT HLIF AL-26 -9.950E-03 2.083E-02 2 .131E-02 NOT IDENT. SC-46 l.846E-02 3.663E-01 3.664E-01 FAIL ABUN V-48 2 .110E+03 1.676E+04 l.678E+04 SHORT HLIF CR-51 3.204E+02 4.482E+02 4.709E+02 SHORT HLIF MN-54 -l.910E-02 5.798E-02 5.862E-02 NOT IDENT. C0-56 1.179E-01 5.199E-01 5.226E-01 FAIL ABUN MN-56 1. OOOE+41 4.410E+41 0.000E+OO SHORT HLIF C0-57 9.342E-04 3.829E-02 3.829E-02 NOT IDENT. C0-58 -3.216E-01 5.128E-Ol. 5.329E-01 NOT IDENT. FE-59 4.637E-01 6.280E+OO 6.284E+OO NOT IDENT. C0-60 -1.435E-02 3.331E-02 3.393E-02 NOT IDENT. ZN-65 5.808E-02 1. 975E-01 l.992E-01 NOT IDENT. GE-68 4.767E-01 2.352E+OO 2.362E+OO NOT IDENT. AS-73 5.366E-01 2.104E+OO 2.118E+OO NOT IDENT. AS-74 -2.462E+03 6.315E+03 6.412E+03 SHORT HLIF SE-75 -5.786E-02 1.595E-01 1.616E-01 NOT IDENT. BR-77 1.458E+39 1.296E+40 O.OOOE+OO SHORT HLIF SR-82 -2.573E+Ol 7.176E+02 7.177E+02 SHORT HLIF RB-83 2.332E-02 5.549E-01 5.550E-01 NOT IDENT. KR-85 9.059E+OO 6.829E+OO 7.957E+00 NOT IDENT. SR-85 1.041E+OO 7.855E-01 9.150E-01 NOT IDENT. RB-86 2.215E+04 3.742E+04 3.873E+04 SHORT HLIF Y-88 -7.732E-02 1.102E-01 l.155E-01 NOT IDENT. NB-94 3.035E-03 3.221E-02 3.224E-02 NOT IDENT. NB-95 9.359E-01 8.460E-01 9.453E-01 NOT IDENT. NB-95M -8. 811E-01 2.326E+OO 2.360E+00 NOT IDENT. ZR-95 -3.235E-01 1.505E+OO 1.512E+OO NOT IDENT. NB-97 l.OOOE+41 2.243E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 6.296E+41 O.OOOE+OO SHORT HLIF M0-99 8.364E+32 1.271E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 8.473E+42 O.OOOE+OO SHORT HLIF RH-101 -l.423E-02 2.762E-02 2.836E-02 NOT IDENT. RH-102 4.448E-03 4.258E-02 4.263E-02 FAIL ABUN RU-103 6.983E-01 4.765E+OO 4.776E+OO FAIL ABUN AG-108M 9.877E-03 2.192E-02 2.237E-02 NOT IDENT. AG-llOM -l.078E-01 l.132E-01 1.232E-01 FAIL ABUN SN-113 -1.763E-01 2.009E-01 2.160E-01 NOT IDENT. CD-115 -4.606E+39 3.427E+40 0.000E+OO SHORT HLIF SN-ll 7M 1. 469E+04 1.131E+05 1.133E+05 SHORT HLIF TE-123M -8.763E-02 1. 076E-01 1.146E-01 NOT IDENT. SB-124 -1.014E+OO 1.572E+00 l.637E+00 NOT IDENT. SB-125 6.964E-02 8.804E-02 9.347E-02 I FAIL ABUN TE-125M -1.005E+Ol 2.120E+02 2 .121E+02 NOT IDENT. I-126 6.486E+05 l.287E+06 1.320E+06 SHORT HLIF SB-126 -9.864E+05 1.721E+06 1. 778E+06 SHORT HLIF SB-127 -4.399E+22 9.354E+22 O.OOOE+OO SHORT HLIF I-131 l.201E+09 8.088E+o9 8.106E+09 SHORT HLIF I-132 1. OOOE+41 1.909E+42 0.000E+OO SHORT HLIF TE-132 -7.918E+25 2.021E+27 O.OOOE+OO SHORT HLIF BA-133 1. 961E-03 3.949E-02 3.949E-02 FAIL ABUN I-133 1.000E+41 2.440E+41 O.OOOE+OO SHORT HLIF CS-134 2.644E-02 4.637E-02 4.787E-02 NOT IDENT. CS-135 5.875E-02 1.115E-01 l.146E-01 NOT IDENT. I-135 -1.000E+41 8.129E+41 O.OOOE+OO SHORT HLIF CS-136 2.405E+05 4.907E+05 5.026E+05 SHORT HLIF BA-137M l.295E-02 3.586E-02 3.633E-02 NOT IDENT. CS-137 1.368E-02 3.788E-02 3.838E-02 NOT IDENT. CE-139 -4.497E-02 9.789E-02 9.996E-02 NOT IDENT. BA-140 2.016E+06 2.110E+06 2.298E+06 SHORT HLIF LA-140 -6.821E+05 6. 716E+05 7.386E+05 SHORT HLIF CE-141 5.951E+OO 2.499E+Ol 2.513E+Ol NOT IDENT. CE-143 l.OOOE+41 7.079E+41 O.OOOE+OO SHORT HLIF CE-144 3.493E-02 2.797E-01 2. 801E-01 NOT IDENT. PM-144 2.328E-02 5.129E-02 5.235E-02 NOT IDENT. PR-144 2.387E+OO 4.427E+OO 4. 556E+o*o NOT IDENT. PM-146 -3.748E-03 3.535E-02 3.539E-02 NOT IDENT. ND-147 -1.141E+07 5.079E+07 5.105E+07 SHORT HLIF PM-147 3.548E+02 6.447E+02 6.643E+02 NOT IDENT. PM-149 1.000E+41 1.356E+41 O.OOOE+OO SHORT HLIF EU-150 2. 641E-03 2 .134E-02 2.138E-02 FAIL ABUN EU-152 2. 960E-02 8.188E-02 8.296E-02 FAIL ABUN GD-153 -4.303E-02 1.308E-01 1.322E-01 NOT IDENT. EU-154 6.833E-02 1.394E-01 1.427E-01 NOT IDENT. EU-155 6.519E-02 7.057E-02 7.644E-02 FAIL ABUN TB-160 8.906E-01 1.998E+OO 2.038E+OO FAIL ABUN H0-166M 2.744E-03 5.261E-02 5.262E-02 NOT IDENT. TM-171 6.914E-01 4.235E+OO 4.246E+OO NOT IDENT. Page 3740of5809 HF-172 -6.034E-02 1.850E-01 1. 870E-01 FAIL ABUN LU-172 8.908E-03 7.134E-02 7.146E-02 FAIL ABUN LU-176 -3.688E-03 l.887E-02 l.894E-02 FAIL ABUN HF-181 -1.086E+OO 4 .112E+OO 4.142E+OO NOT IDENT. TA-182 8.428E-01 l.030E+00 l.098E+OO FAIL ABUN RE-183 -3.351E-01 9.894E-01 1. OOlE+OO NOT IDENT. RE-184 -9.713E+OO 2.610E+Ol 2.646E+Ol NOT IDENT. W-188 -6.489E+Ol l.452E+02 1.481E+02 FAIL ABUN IR-192 2.320E-01 4.397E-01 4.520E-01 FAIL ABUN BI-207 5.357E-02 5.374E-02 FAIL ABQN PB-211 4.972E-02 5.259E-01 5.264E-01 NOT IDENT. BI-212 6.954E-01 7.688E-01 8.303E-01 FAIL ABUN RN-219 -3.126E-01 3.220E-01 3.515E-01 NOT IDENT. RA-223 -6.418E-01 7.415E-01 7.959E-01 FAIL ABUN AC-227 -4.557E-02 1. 757E-01 l.769E-01 FAIL ABUN TH-227 -4.557E-02 1. 757E-01 1. 769E-01 FAIL ABUN TH-229 -8.083E-02 3.832E-01 3.849E-01 FAIL ABUN TH-231 -6.418E-01 7.415E-01 7.959E-01 FAIL ABUN PA-233 1.631E-02 4.589E-02 4.648E-02 FAIL ABUN PA-234 -2.836E-01 4.190E-01 4.381E-01 NOT IDENT. PA-234M 3.633E+OO 4.361E+OO 4.659E+OO NOT IDENT. NP-237 1. 631E-02 4.589E-02 4.648E-02 FAIL ABUN NP-238 -1.000E+41 4.469E+41 0.000E+OO SHORT HLIF NP-239 -4.034E-02 1. 7 58E-01 1. 768E-01 FAIL ABUN PU-239 1. 881E+o2 2.425E+02 2.569E+02 NOT IDENT. AM-241 1.506E-02 4.600E-02 4.650E-02 NOT IDENT. CM-243 -3.773E-02 6.589E-02 6.805E-02 FAIL ABUN BK-247 -4.058E-02 5.658E-02 5.947E-02 NOT IDENT. CM-247 -2.013E-02 2.762E-02 2.907E-02 FAIL ABUN CF-249 3.363E-02 3.082E-02 3.435E-02 NOT IDENT. CF-251 2.247E-02 9.680E-02 9.733E-02 FAIL ABUN Page 3741of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 57.4984 87.09 123. 9638 136.47 72 .. 5224 45.60 68.6647 87.57 106.5029 140.51 0.0000 46.54 73.8750 88.03 80.2402 143.76 72 .1645 49.72 0.0000 8ff.34 80.2739 144.24 72 .1991 51. 35 91.1306 88.47 80.2876 145.44 64.2524 51. 87 101.8809 89. 96 98.0457 152.43 77.2665 52.39 78.2630 1093.63 40.2603 153.25 0.0000 52.97 72. 4112 91.11 0.0000 323.87 53.9978 53.44 83.1661 92.59 78.2043 156.02 0.0000 54.07 89.2087 93.35 83.3318 158.56 0.0000 57.36 0.0000 94.56 83.4628 159.00 66.8969 57.53 110 .1053 94.65 83.4723 162.33 52.5938 57.98 92.6242 94.67 83.4743 162.66 0.0000 59.27 89.6297 94.87 72. 1102 163.33 62. 6253 59.32 89.6374 97.43 86.3074 165.86 71.8662 59.54 89.6713 98.43 73.1997 176.31 57.8429 60. 96 119.1815 98.44 73.2006 176.60 0.0000 61.17 119. 2234 99.53 64.4772 177.52 59.7414 62.93 119.5741 100 .11 66.2219 181.07 0.0000 63.29 119.6449 102.03 83.3998 181.52 56.7185 63.58 119. 7023 103.18 73.2904 184.41 42.5274 64.28 119.8396 103.37 79.2743 143.76 42.5742 66.73 120.3141 105.21 56.3847 193.51 58.6844 67.24 120.4123 105.31 56.3918 197.03 61. 6548 125.81 107.1077 106.12 73.5515 198.01 67.3125 67.75 107.1191 106.47 74.4382 201.83 60.0163 69.67 126.9777 109.28 68.6776 203.43 50.7030 70.83 100.2966 111. 00 86.8801 205.31 50.7777 72.81 107. 9610 111.76 0.0000 210.85 43.9140 72.87 124.3303 114.06 72.5126 215.65 43.6014 74.66 118.1038 116. 30 0.0000 222 .11 48.5762 74.82 118.1316 116. 74 72.7339 227.09 40.1513 74.97 118.1580 119.76 72 .1116 227.38 41. 5941 77 .11 118. 5315 121.12 67.8695 228.16 0.0000 78.74 95.7097 121. 22 67.8771 228.18 45.9238 79.69 99.1455 121.78 66.1776 116.74 45.9238 80.12 104.1669 122.06 76.6500 235.69 53.3885 80.19 0.0000 122.92 79.3380 235. 96 53.3987 80.57 102.5790 123.07 83.7109 238.63 50.6084 81. 00 92.7090 265.00 76.7861 238.98 0.0000 81. 07 92.7181 125.81 77.8379 240.99 40.5542 81. 75 132.5814 127.23 87.5910 242.00 40.5833 83.79 97.2274 127.91 74.5071 244.70 30.4951 84.00 94.7623 129.30 65.8379 252.40 0.0000 85.43 123.2671 131.20 86.2016 252.80 35.0468 86.55 135.1343 133.02 67.8583 254.15 0.0000 86.79 135.1780 133.52 66 .1301 256.23 38.0558 86.94 123.9388 136.00 63.6475 260.90 0.0000 Page 3742of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 33.3643 355.39 0.0000 584.27 20.6689 264.80 40.2376 356.01 31.0870 595.83 0.0000 265.00 40.2426 364.49 0.0000 427.87 18.4857 268.22 33.4425 366.42 0.0000 602.52 0.0000 269.46 30.5169 372. 51 19.8620 604.72 26.0358 270 .. 03 39.3913 375.05 28.2623. 607.14 18.5306 271.23 44.3500 377.52 25.1543 609.32 18.5456 273.65 0.0000 356.01 25.2368 610.33 18.5527 276.40 38.5652 388.16 17.9152 614.28 6. 9673 277.37 33.6417 388.63 0.0000 618.01 6.9768 277.60 33.6465 391. 69 31.6718 620.36 12.8020 278.00 33.6555 264.66 24.3912 621. 93 17.4670 279.20 43.0920 401. 81 32.8940 630.19 0.0000 279.54 43.1017 402.40 27. 5964 631. 29 11.3921 279.70 50.5383 404.85 22.3168 633.25 12.2769 280.46 44.6136 410.95 27. 7128 634.78 0.0000 283.69 40.2347 413.71 30.9523 635.95 21.9444 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 36. 7975 423. 72 0.0000 645.85 10.5707 285.90 0.0000 427.09 19.3359 657.76 19.4608 287.50 28.3811 427.87 18.2683 657.90 0.0000 290.67 41.9077 433.94 17.2432 661.66 21.2585 293.27 0.0000 439.40 22.6898 664.57 0.0000 351. 93 30.0183 453.88 20.6664 666.33 0.0000 295. 96 27.0286 463.37 20.7554 666.50 0.0000 879.38 18.0480 468.07 26.2725 667.71 0.0000 299.98 33 .1161 473.00 0.0000 677.62 15.6755 300.09 33 .1182 475.06 21.9617 685.70 0.0000 300 .13 33 .1195 476.78 21. 9784 695.00 0.0000 301.36 33.1437 477.60 18.6882 696. 49 16.1345 302.85 27.1423 482.18 20.9289 696.51 15.2382 256.23 39.2444 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.0355 306.78 31. 2371 497.08 13.3036 697.49 19.7267 308.46 29.2513 505.52 26. 7026 702.65 23. 35.38 311. 90 26.2788 507. 63 0.0000 706.68 20.6865 316.51 25.8434 511. 00 16.7276 711. 68 18.0182 319.41 0.0000 514.00 15.0738 720.70 0.0000 320.08 0.0000 514.00 15.0738 721. 93 0.0000 321. 04 29.4685 520.40 15.6737 722. 78 11. 5734 323.87 42.7485 520.69 0.0000 722.91 15.9146 325.23 24.4468 522.65 0.0000 723.31 18.8106 328.76 0.0000 527.90 0.0000 724.19 20.2631 333.37 31.9287 528.26 19.0939 727. 33 19.0159 333.97 29.4826 529.59 13.4854 733.00 18.1439 334.37 36.8613 529.87 0.0000 735.93 15.4369 338.28 30.7855 531. 02 0.0000 333.97 18.1702 338.32 30.7861 537.26 0.0000 739.50 0.0000 311. 90 30.8234 546.56 0.0000 747.24 9 .1135 340.48 30.8234 552.55 15.8793 748.06 15. 4965 340.55 0.0000 563.25 15.9460 752.31 15.5178 344.28 24.7104 569.33 22.8337 753.82 0.0000 345.93 32.9779 946.00 20.5518 756.73 15.8443 351.06 33.0703 569.70 20.5532 756.80 15.8443 351.93 33.0859 583.19 20.6602 884.68 10.9937 Page 3743 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 11. 0002 1274.44 14.6750 1620.50 7.8122 766.42 11. 0024 1001.03 8.8157 1621. 92 3.3490 766.84 11. 0039 1002.74 13.7193 1678.03 0.0000 772.60 0.0000 1004.73 18.6283 1690.97 3.6152 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.5Q 0.0000 1025.87 0.0000 1764.49 4.5752 778.90 7.3633 1028.54 0.0000 1063.66 1.5264 783.70 0.0000 1037.84 5.9319 1771. 35 1.5268 785.37 11.0669 1038.76 0.0000 1791.20 0.0000 792.07 17.5585 631. 29 10.8986 1808.65 2.7649 794.95 15.7243 1048.07 0.0000 1810.72 0.0000 795.86 12.9528 1049.04 15.8623 1836.06 1.8515 810.06 12.0792 1050.41 14.2813 810.29 12.0800 1063.66 16.9149 344.28 13.0101 1077.00 0.0000 810.76 13.9407 1077.34 10.9812 815.77 0.0000 1085.87 5.0015 1048.07 0.0000 1093.63 10.0220 832.01 10.2877 1099.45 8.0288 834.85 15.9126 1112. 07 11. 0725 835.71 14.9800 1112. 84 12.0813 836.80 0.0000 1115.54 11.2834 846.75 0.0000 1120.29 11. 0940 846.77 15. 9676 1120. 55 11.0947 856.80 0.0000 1221.41 6.4563 860.56 16.0314 1129. 67 11.1182 871. 09 10.4045 1131.51 0.0000 873.19 13.2498 1147.95 0.0000 875.33 0.0000 1173.23 16.3350 879.38 12.3252 1177.95 11. 2424 880.51 9.4836 1189.05 12.2952 883.24 19.7412 1204.77 0.0000 884.68 16. 7111 1221.41 10.3198 889.28 9 .12 69 1231. 02 13.7882 894.76 10.4740 1235.36 0.0000 898.04 10.4834 1238.28 14.5007 900.72 11. 4448 1260.41 0.0000 903.28 9.5441 1271.87 14.6058 911.20 8.6086 1274.44 12.5259 912.08 8.6105 1274.54 13.5705 923.98 0.0000 1291.59 5.2383 92 6. 50 11. 52 61 1298.22 0.0000 929 .11 11. 5342 1312.11 0.0000 937.49 14.4502 1332.49 7. 3961 944.13 0.0000 1362.66 0.0000 946.00 18.3454 1365.19 4.2546 949.00 10.6294 1368.63 0.0000 667.71 0.0000 1384.29 8.5420 962. 31 9.3094 1408.01 2.1455 964.08 3.1046 1457.56 0.0000 966.17 7.7656 1460.82 3.2514 911.20 0.0000 1489.16 1.0897 968. 97 0.0000 1505.03 5.4645 983.53 0.0000 1584.12 4.4353 984.45 0.0000 1596.21 0.0000 Page 3744of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:20:03.75 ********************************************************************************
  • GEi Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM43.CNF;l51 Background date : Z-OCT-2016 11:02:23. Sample date 30-NOV-2015 10:40:00 Acquisition date : 3-0CT-2016 09:17:37. Sample ID G405235038 Sample quantity 1.70192E+02 GRAM Detector name : GAM43 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.65 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 1 1 0 0 0 4 4 0 0 4 4 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3745of5809 Energy 42. 96 51. 69 54.53* 74.69 77.06 88.08 92.78* 111. 81 126.75 12 9 .11 185. 96* 209.35 238.57* 241.64 258.87 266.78 270.05 277.60 295.27* 299.95* 308.04 338.35 351. 67* 389.09 392.32 463.79 490.97 511.12*

583.09* 609.40* 661. 42 720.47 728.72 769.43 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 32 60 29 82 145 101 51 14 17 37 66 30 356 77 27 22 36 24 111 26 7 75 182 10 14 71 26 2 109 112 40 16 61 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 134 85 66 111 123 157 105 88 45 109 117 84 63 94 67 35 67 67 46 39 47 46 54 20 21 24 39 45 15 34 16 16 32 29 2.91 1. 57 1. 03 1. 23 1.11 3.87 1. 51 0.44 1. 21 1. 39 1. 23 1. 34 1.10 1. 71 0.94 1. 56 1. 95 0.98 1. 57 1. 21 0.55 1. 04 1. 38 0.94 1. 32 2.35 6.33 2.79 1. 70 1. 45 1.16 1. 24 2.78 1. 31 85.69 103.16 108.84 149.18 153.92 175.96 185.37 223.43 253.32 258.05 371. 78 418.57 477.03 483.18 517.65 533.46 540.00 555 .11 590.45 599.82 616.00 676.64 703.29 778.14 784.61 927.58 981.95 1022.26 1166. 23 1218.87 1322.93 1441. 05 1457.56 1538.98 81 99 107 144 144 171 182 219 252 252 366 415 469 469 512 531 531 549 586 596 609 673 697 774 780 918 973 1015 1161 1212 1317 1437 1446 1533 9 9.02E-03 66.7 8 1.68E-02 29.7 6 7.93E-03 49.3 15 2.28E-02 25.0 15 4.04E-02 15.0 11 2.81E-02 26.0 7 1.42E-02 38.0 7 3.77E-03120.3 10 4.75E-03 52.2 10 1. 04E-02 51. 4 9 1. 82E-02 33. 2 10 8.40E-03 59.2 20 9.89E-02 6.6 20 2.15E-02 29.0 10 7.41E-03 60.7 14 6.llE-03 42.2 14 9.98E-03 45.9 10 6.55E-03 70.0 10 3.08E-02 15.2 8 7.33E-03 46.1 8 2. OlE-03169. 6 8 2.08E-02 19.5 12 5.06E-02 11.0 6 2.78E-03 78.4 7 3.83E-03 55.9 19 1.98E-02 20.2 19 7.28E-03 59.8 14 4.37E-04***** 10 3.03E-02 12.0 11 3.12E-02 13.9 13 1.lOE-02 26.3 10 4.54E-03 51.0 26 1.71E-02 28.4 14 5.llE-03 65.4 Fit 9.49E-01 4.25E+OO 4.42E-01 1. 95E+00 Peak Search Report (continued) Page : 2 Sample ID : G405235038 Acquisition date 3-0CT-2016 09:17:37 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 796. 61 9 25 3.78 1593.35 1581 14 2.62E-03115.9 36 0 827.72 16 8 2.40 1655.58 1650 11 4.46E-03 42.6 .37 1 854.43 15 16 2.04 1709.00 1703 20 4.28E-03 57.4 7.43E+QO 38 1 856.93 29 15 2.04 1714.00 1703 20 8.14E-03 30.9 39 0 911.28* 69 40 1. 30 1822.73 1815 16 1.92E-02 24.0 40 1 965 .12 20 11 2.34 1930.43 1926 24 5.52E-03 34.1 1.79E+OO 41 1 968.70 45 13 2.34 1937.57 1926 24 1.26E-02 24.4 42 0 1032. 96 9 5 1. 42 2066.10 2062 8 2.58E-03 54.9 43 4 1065.40 16 7 2.20 2131.00 2125 14 4.39E-03 35.8 4.26E-01 44 4 1067.83 8 1 1. 80 2135. 85 2125 14 2.14E-03 53.6 45 0 1120.89 18 25 1. 43 2241.98 2235 15 4.98E-03 63.0 46 0 1177.22 15 13 1. 65 2354.66 2348 14 4.27E-03 57.1 47 0 1244.93 6 9 0.47 2490.08 2484 8 l.69E-03 97.0 48 0 1460.55* 307 3 2.10 2921.34 2913 15 8.52E-02 5.9 49 0 1764.03* 17 0 0. 72 3528.30 3520 15 4.77E-03 26.5 Flag: "*" = Peak area was modified by background subtraction Page 3746 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:20:05 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 10:40:00 G405235038 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 09:17:37 170.19 GRAM Sample type : Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA43 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3747 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.65 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235038 Acquisition date 3-0CT-2016 09:17:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.002E+OO 1.238E+Ol l.238E+Ol J_l.86 OK AS-73 53.44 10.30* 9.178E-01 1.918E+OO 2.738E+Ol 98.59 OK CD-109 88.03 3.70* 4.365E+OO 3.050E+OO 4.845E+OO 64. 96 OK SN-113 391.69 64.94* 3 .112E+OO 3.501E-02 2.237E-01 OK SN-126 64.28 9.60 l.983E+OO Line Not Found Absent 86.94 8.90 4.365E+OO 1.268E+OO 1. 268E+OO 64. 96 OK 87.57 37.00* 4.365E+OO 3.050E-01 3.050E-01 64. 96 OK CS-135 268.22 16.00* 4.342E+OO 1.698E-01 l.698E-01 84.47 OK BA-137M 661.66 89.90* 1.974E+OO 1.071E-01 l.092E-01 52.70 OK CS-137 661.66 85.10* 1.974E+OO l .131E-01 l.154E-01 52.70 OK TM-171 51. 35 0.27 6.497E-01 2.199E+02 2.982E+02 59.33 OK 52.39 0.47* 6.497E-01 1.263E+02 l.713E+02 59.33 OK 66.73 0.14 2.262E+OO Line Not Found Absent TL-208 277.37 6.60 4.202E+00 4.542E-01 4.542E-01 139.97 OK 583.19 85.00* 2.199E+OO 2.845E-01 2.845E-01 23.91 OK 860.56 12.50 1.582E+OO Line Not Found Absent PB-212 74.82 10.28 3.134E+OO l.118E+OO 1.118E+OO 71. 23 OK 77 .11 17.10 3.377E+OO 1.546E+OO 1.546E+OO 30.01 OK 238.63 43.60* 4.739E+OO' 9.370E-01 9.370E-01 13 .13 OK 300.09 3.30 3.937E+OO 1.076E+OO 1.076E+OO 92.17 OK BI-214 609.32 45.49* 2 .117E+OO 5.666E-01 5.668E-01 27.84 OK 1120.29 14.92 1.266E+OO 4.246E-01 4.247E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 OK PB-214 74.82 5.80 3.147E+OO Line Not Found <<INT Reject 77 .11 9.70 3.377E+OO 2.725E+OO 2. 726E+OO 30.01 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 4.688E+OO Line Not Found <<INT Reject 295.22 18.42 3.990E+OO 8.000E-01 8.003E-01 30.31 OK 351.93 35.60* 3.428E+OO 7.757E-01 7.760E-01 22.09 OK RN-222 609.32 45.49* 2 .117E+OO 5.666E-01 5.668E-01 27.84 OK 1120. 29 14.92 l.266E+OO 4.246E-01 4.247E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 OK RA-224 240.99 4.10* 4.694E+00 7.685E-01 7.685E-01 174.16 OK RA-226 609.32 45.49* 2 .117E+00 5.666E-01 5.668E-01 27.84 OK 1120.29 14.92 1.266E+OO 4.246E-01 4.247E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 OK AC-228 105.21 1.10 5. 396E+OO Line Not Found Absent 338.32 11. 27 3.546E+OO 9.761E-01 9 .. 761E-01 39.05 OK 794.95 4.25 1.691E+OO Line Not Found Absent 835.71 1. 61 1.621E+OO Line Not Found Absent 911.20 25.80* 1. 508.E+OO 8.193E-01 8.193E-01 48.07 OK 968. 97 15.80 1.432E+OO 9.129E-01 9.129E-01 48.81 OK RA-228 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.546E+OO 9.761E-01 9. 761E-01 39.05 OK 794.95 4.25 l.691E+00 Line Not Found Absent 835.71 1. 61 1. 621E+OO Line Not Found Absent 911.20 25.80* l.508E+00 8.193E-01 8.193E-01 48.07 OK 968. 97 15.80 l.432E+OO 9.129E-01 9.129E-01 48.81 OK TH-228 74.82 10.28 3.134E+OO 1.118E+OO l .118E+00 71. 23 OK Page 3748of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235038 Acquisition date 3-0CT-2016 09:17:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status ** 77 .11 17.10 3.377E+OO l.546E+OO 30.01 OK 238.63 43.60* 4.739E+OO 9.370E-01 9.370E-01 13.13 OK 300.09 3.30 3.937E+OO l.076E+OO l.076E+00 92.17 OK TH-230 609.32 45.49* 2 .117E+OO 5.666E-01 5.666E-01 27.84 OK 1120.29 14.92 1.266E+OO 4.246E-01 4.246E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.620E-01 52.95 OK PA-231 283.69 1. 70 4.127E+OO Line Not Found Absent 301.36 5.35* 3.937E+OO 6.635E-01 6.635E-01 92.17 OK TH-232 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.546E+OO 9. 761E-01 9.761E-01 39.05 OK 835.71 1. 61 1. 621E+OO Line Not Found Absent 911. 20 25.80* 1.508E+OO 8.193E-01 8.193E-01 48.07 OK 968. 97 15.80 l.432E+OO 9.129E-01 9.129E-01 48.81 OK U-234 609.32 45.49* 2 .117E+OO 5.666E-01 5.666E-01 27.84 OK 1120.29 14.92 l.266E+OO 4.246E-01 4.246E-01 125.97 OK 1764.49 15.30 8.365E-01 5.620E-01 5.620E-01 52.95 OK AM-243 43.53 5.90 1.014E-01 3.532E+Ol 3.532E+Ol 133.45 OK 74.66 67.20* 3.134E+OO 1. 711E-01 1. 711E-01 71. 23 OK CF-249 252.80 2.50 4.533E+OO Line Not Found -----Absent 333.37 14.60 3.593E+OO Line Not Found Absent 388.16 66.00* 3.135E+OO 2.481E-02 2.485E-02 156.84 OK ANH-511 511. 00 100.00* 2.465E+OO 3.170E-03 3.170E-032134.97 OK *Flag: "*" = Keyline Page 3749 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:20:06.82 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l * *Acquisition date 3-0CT-2016 09:17:37 Sensitivity : 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.65 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Analyst initials: MXRl * *Sample ID G405235038 Sample Quantity 1.7019E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File DKA100: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.238E+Ol 1.439E+OO AS-73 2.738E+Ol 2.645E+Ol CD-109 4.845E+OO 3.084E+00 SN-113 2.237E-01 2. 451E-01 SN-126 3.050E-01 1.942E-01 CS-135 1.698E-01 1. 406E-01 BA-137M 1.092E-01 5.640E-02 CS-137 1.154E-01 5.958E-02 TM-171 l.713E+02 9. 960E+Ol TL-208 2.845E-01 6.666E-02 PB-212 9.370E-01 1.206E-01 BI-214 5.668E-01 l.547E-01 PB-214 7.760E-01 1.680E-01 RN-222 5.668E-01 l.547E-01 RA-224 7.685E-01 1.312E+OO RA-226 5.668£-01 1. 54 7E-01 AC-228 8.193£-01 3.860E-01 RA-228 8.193£-01 3.860E-01 TH-228 9.370£-01 1.206E-01 TH-230 5.666£-01 l.546E-01 PA-231 6.635£-01 5.993E-01 TH-232 8.193£-01 3.860E-01 U-234 5.666£-01 1.546E-01 AM-243 1. 711£-01 l.194E-01 CF-249 2.485£-02 3.819E-02 ANH-511 3.170£-03 6.633E-02 Non-Identified Nuclides Nuclide
  • BE-7 NA-22 NA-24 AL-26 Page 3750 of 5809 Key-Line Activity (pCi/GRAM -5.736E+OO -l.412E-02 O.OOOE+OO -1.236£-02 K.L. Cnt Uncert (1.96-sigma) 1.263E+Ol 4.877E-02 1.960E+41 3. lllE-02 MDA (pCi/GRAM 6.582E-01 2.522E+Ol 2.130E+OO 4.203E-01 1.352E-01 2.407E-01 5.907E-02 6.240E-02 5. 971E+Ol 6.132E-02 8.681E-02 1. 317E-01 l.140E-01 1.317E-01 9.308£-01 1.317E-01 2.602E-01 2.602£-01 8.681£-02 1.316E-01 7. 396£-01 2.602£-01 1.316£-01 1.051£-01 3.879£-02 4.723£-02 MDA (pCi/GRAM 2.251E+Ol 9.365£-02 O.OOOE+OO 5.866£-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 2.703E-01 3. 968E-01 8.625E-01 FAIL ABUN V-48 0.000E+OO 2.035E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.353E+02 O.OOOE+OO SHORT HLIF MN-54 2.686E-02 6.304E-02 l.314E-01 NOT IDENT. C0-56 -3. 201E-03 4.586E-01 9.115E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 5.143E-03 4.857E-02 9.125E-02 NOT IDENT. C0-58 1.387E-01 6.086E-01 1.247E+OO NOT IDENT. FE-59 2.372E+OO 8.065E+OO 1. 626E+Ol NOT IDENT. C0-60 l.128E-02 4.240E-02 8.942E-02 NOT I DENT.; ZN-65 0.000E+OO l.607E-01 2.792E-01 NOT IDENT. GE-68 -2. 413E-01 2.007E+OO 3. 901E+OO NOT IDENT. AS-74 O.OOOE+OO 6.439E+03 O.OOOE+OO SHORT HLIF SE-75 3.837E-02 2.005E-01 3.632E-01 NOT IDENT. BR-77 0.000E+OO 2.312E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 1.044E+03 O.OOOE+OO SHORT HLIF RB-83 -2.502E-01 7.342E-01 l.419E+OO NOT IDENT. KR-85 -2.349E+OO 7. 961E+OO 1.253E+Ol NOT IDENT. SR-85 -2. 721E-01 9.159E-01 1.441E+OO NOT IDENT. RB-86 O.OOOE+OO 3.308E+04 O.OOOE+OO SHORT HLIF Y-88 -8.303E-02 l.711E-01 3.177E-01 NOT IDENT. Y-91 -l.197E+02 5.995E+02 1.165E+03 NOT IDENT. NB-94 -1.205E-02 2.924E-02 5.483E-02 NOT IDENT. NB-95 -9.290E-02 9.182E-01 1.570E+OO NOT IDENT. NB-95M -3.887E-01 2.454E+OO 4.255E+00 NOT IDENT. ZR-95 8.792E-01 l.478E+OO 3.183E+OO NOT IDENT. NB-97 O.OOOE+OO 9.864E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.403E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.525E+41 O.OOOE+OO SHORT HLIF RH-101 2.937E-02 3.003E-02 6.382E-02 FAIL ABUN RH-102 1.634E-02 5.397E-02 1.130E-01 NOT IDENT. RU-103 -3.664E+OO 7.344E+OO 1.116E+Ol FAIL ABUN RH-106 -4.074E-02 4.694E-01 9.335E-01 NOT IDENT. RU-106 -4.074E-02 4.694E-01 9.335E-01 NOT IDENT. AG-108M -1.106E-02 2.638E-02 4.762E-02 NOT IDENT. AG-llOM -l.242E-01 l.035E-01 1.604E-01 NOT IDENT. CD-115 O.OOOE+OO 3.462E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.160E+05 O.OOOE+OO SHORT HLIF TE-123M 2.577E-02 l.123E-01 2.318E-01 NOT IDENT. SB-124 l.463E+OO 1. 779E+OO 4.871E+OO NOT IDENT. SB-125 -6.762E-02 9.768E-02 l.697E-01 FAIL ABUN TE-125M 3.479E+Ol 3.382E+02 5.900E+02 NOT IDENT. I-126 0.000E+OO l.433E+06 0.000E+OO SHORT HLIF SB-126 O.OOOE+OO 2.521E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 9.023E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 9.615E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.838E+27 O.OOOE+OO SHORT HLIF BA-133 5.826E-03 3.982E-02 7.036E-02 FAIL ABUN I-133 O.OOOE+OO 9.779E+40 O.OOOE+OO SHORT HLIF CS-134 4.068E-02 9.241E-02 1.113E-01 FAIL ABUN I-135 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 4.898E+05 O.OOOE+OO SHORT HLIF CE-139 -l.039E-01 9.441E-02 1. 748E-01 NOT IDENT. BA-140 O.OOOE+OO 2.035E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.136E+05 O.OOOE+OO SHORT HLIF CE-141 -l.347E+Ol 2. 513E+Ol 4.921E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.415E+41 O.OOOE+OO SHORT HLIF CE-144 -2.379E-01 3.257E-01 6.022E-01 NOT IDENT. PM-144 1.692E-02 5.685E-02 l.160E-01 NOT IDENT. PR-144 1.550E+OO 4.970E+00 1.016E+Ol NOT IDENT. PM-i46 -1.941E-02 4.176E-02 7.563E-02 NOT IDENT. ND-147 O.OOOE+OO 4.899E+07 O.OOOE+OO SHORT HLIF PM-147 3.652E+Ol 8.214E+02 l.537E+03 NOT IDENT. PM-149 O.OOOE+OO 1.410E+41' O.OOOE+OO SHORT HLIF EU-150 -1.836E-02 2.754E:-02 4.297E-02 FAIL ABUN EU-152 -3.342E-02 8. 725E-02 1.613E-01 FAIL ABUN GD-153 -l.124E-01 l.983E-01 3.575E-01 NOT IDENT. EU-154 -4.213E-02 l.217E-01 2.310E-01 NOT IDENT. EU-155 2.382E-02 l.030E-01 l.989E-01 NOT IDENT. TB-160 l.138E+OO 1. 776E+OO 3.923E+OO FAIL ABUN H0-166M -3.298E-02 5.440E-02 9.885E-02 NOT IDENT. HF-172 2.024E-01 2.069E-01 4.546E-01 FAIL ABUN LU-172 -3.067E-02 7.432E-02 l.334E-01 FAIL ABUN LU-176 1.058E-02 3.517E-02 4.423E-02 FAIL ABUN HF-181 2. 507E-Cll 4.386E+00 8.466E+OO NOT IDENT. TA-182 3.567E-01 l.128E+OO 2.303E+OO FAIL ABUN Page3751 of5809 RE-183 2.083E+OO 5.140E+OO 9.809E+OO NOT IDENT. RE-184 -1.787E+Ol 3. 726E+Ol 6.436E+Ol NOT IDENT. W-188 2.622E+Ol l.143E+02 2.062E+02 NOT IDENT. IR-192 3.321E-01 4.274E-01 9.004E-01 FAIL ABUN HG-203 -2.113E-01 2.204E+OO 3.861E+OO NOT IDENT. BI-207 -8.451E-03 5.413E-02 8.826E-02 FAIL ABUN PB-210 -3.340E+OO 9.826E+OO 1. 762E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.626E-01 7.270E-01 FAIL ABUN PB-211 -2.421E-01 6.675E-01 1.217E+OO NOT IDENT. BI-212 O.OOOE+OO 1. 336E+OO 1.339E+OO FAIL ABUN RN-219 1.009E-01 3.491E-01 6.917E-01 FAIL ABUN RA-223 1. 027E-01 5.134E-01 1.019E+OO FAIL ABUN AC-227 -2.400E-02 2.142E-01 3.730E-01 FAIL ABUN TH-227 -2.400E-02 2.142E-01 3.730E-01 FAIL ABUN TH-229 1. 758E-03 3.749E-01 7.516E-01 FAIL ABUN TH-231 l.027E-01 5.134E-01 l.019E+OO FAIL ABUN PA-233 3.351E-02 5.235E-02 1.084E-01 FAIL ABUN PA-234 -9. 969E-02 3. OllE-01 5.528E-01 FAIL ABUN PA-234M -3.021E+OO 3.889E+OO 6.504E+OO NOT IDENT. TH-234 -1.459E-01 1.591E+OO 3 .114E+OO FAIL ABUN U-235 2.090E-01 l.573E-01 3.451E-01 FAIL ABUN NP-237 3.351E-02 5.235E-02 l.084E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 -1.459E-01 1. 591E+OO 3 .114E+OO FAIL ABUN NP-239 1.137E-01 2.239E-01 4.401E-01 FAIL ABUN PU-239 5.759E+02 5.796E+02 6.423E+02 FAIL ABUN AM-241 -1.384E-01 1.909E-01 3.534E-01 NOT IDENT. CM....:243 -4.867E-02 9.784E-02 1. 7 68E-01 FAIL ABUN BK-247 4.107E-03 6. 672E-02 1. 18 8E-01 NOT IDENT. CM-247 l.285E-02 3.248E-02 6.498E-02 FAIL ABUN CF-251 -7.742E-02 9.753E-02 1.842E-01 NOT IDENT. Page 3752of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:20:04.51 Nuclide Line Activity Report Nuclide T}(pe:

  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 300 10.66* 1.002E+OO l.238E+Ol 1.238E+Ol 11. 86 AS-73 53.44 41 10.30* 9.178E-01 l.918E+OO 2.738E+Ol 98.59 CD-109 88.03 139 3.70* 4.365E+OO 3.787E+OO 6.016E+OO 51. 98 SN-113 391.69 16 64.94* 3.112E+OO 3.501E-02 2.237E-01 111. 79 SN-126 64.28 ------9.60 1.983E+OO ------Line Not Found ------86.94 139 8.90 4.365E+OO 1.575E+OO 1. 575E+OO 51. 98 87.57 139 37.00* 4.365E+OO 3.787E-01 3.787E-01 51. 98 CS-135 2 68. 22 27 16.00* 4.342E+OO l.698E-01 1.698E-01 84.47 BA-137M 661. 66 43 89.90* 1. 974E+OO 1. 071E-01 l.092E-01 52.70 CS-137 661. 66 43 85.10* 1.974E+OO 1.131E-01 1.154E-01 52.70 TM-171 51. 35 87 0.27 6.497E-01 2.199E+02 2.982E+02 59.33 52.39 87 0.47* 6.497E-01 1.263E+02 1.713E+02 59.33 66.73 ------0.14 2.262E+OO ------Line Not Found ------TL-208 277.37 29 6.60 4.202E+OO 4.542E-01 4.542E-01 139.97 583.19 121 85.00* 2.199E+OO 2.845E-01 2.845E-01 23.91 860.56 ------'12.50 1.582E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 2. 941E+OO ------Line Not Found ------351.06 215 12.92* 3.428E+OO 2.137E+OO 2 .137E+OO 22.09 PB-212 74.82 115 10.28 3.134E+OO 1.570E+OO 1.570E+OO 49.99 77.11 202 17.10 3.377E+OO 1.546E+OO 1.546E+OO 30.01 238.63 439 43.60* 4.739E+OO 9.370E-01 9.370E-01 13 .13 300.09 32 3.30 3.937E+OO 1.076E+OO 1.076E+OO 92.17 BI-214 609.32 124 45.49* 2 .117E+OO 5.666E-01 5.668E-01 27.84 1120.29 18 14.92 l.266E+OO 4.246E-01 4.247E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 PB-214 74.82 115 5.80 3.134E+OO 2.782E+OO 2.783E+OO 49.99 77 .11 202 9.70 3.377E+OO 2.725E+OO 2.726E+OO 30.01 87.09 139 3.41 4.365E+OO 4.llOE+OO 4. lllE+OO 51. 98 242.00 95 7.25 4.694E+OO 1.235E+OO l.235E+OO 58.08 295.22 133 18.42 3.990E+OO 8.000E-01 8.003E-01 30.31 351. 93 215 35.60* 3.428E+OO 7.757E-01 7.760E-01 22.09 RN-222 609.32 124 45.49* 2 .117E+OO 5.666E-01 5.668E-01 27.84 1120.29 18 14.92 1.266E+OO 4.246E-01 4.247E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 RA-224 240.99 95 4.10* 4.694E+OO 2.183E+OO 2.183E+OO 58.08 RA-226 609.32 124 45.49* 2 .117E+OO 5.666E-01 5.668E-01 27.84 1120.29 18 14.92 1. 266E+OO 4.246E-01 4.247E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.622E-01 52.95 AC-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 88 11. 27 3.546E+OO 9.761E-01 9.761E-01 39.05 794.95 ------4.25 1.691E+OO ------Line Not Found ------835.71 ------1. 61 1.621E+OO ------Line Not Found ------911.20 72 25.80* 1.508E+OO 8.193E-01 8.193E-01 48.07 968. 97 47 15.80 1.432E+OO 9.129E-01 9.129E-01 48.81 RA-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 88 11. 27 3.546E+OO 9.761E-01 9.761E-01 39.05 794.95 ------4.25 1. 691E+OO ------Line Not Found ------Page 3753of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235038 Acquisition date 3-0CT-2016 09:17:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error .835.71 ------1. 61 1. 621E+OO ------* Line Not Found ------911. 20 72 25.80* 1.508E+OO 8.193E-01 8.193E-01 48.07 968.97 47 15.80 l.432E+OO 9.129E-01 9.129E-01 48.81 TH-228 74.82 115 10.28 3.134E+OO 1. 570E+OO 1.570E+OO 49.99 77 .11 202 17.10 3.377E+OO 1. 546E+OO 1.546E+OO 30.01 238.63 439 43.60* 4.739E+00 9.370E-01 9.370E-01 13.13 300.09 32 3.30 3.937E+OO 1.076E+OO 1. 076E+OO 92.17 TH-230 609.32 124 45.49* 2 .117E+OO 5.666E-01 5.666E-01 27.84 1120.29 18 14.92 l.266E+OO 4.246E-01 4.246E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.620E-01 52.95 PA-231 283.69 ------1. 70 4.127E+OO ------Line Not Found ------301.36 32 5.35* 3.937E+OO 6.635E-01 6.635E-01 92.17 TH-232 105.21 ------1.10 5.396E+OO ------Line Not Found ------338.32 88 11.27 3.546E+OO 9.761E-01 9. 761E-01 39.05 835.71 ------1. 61 l.621E+OO ------Line Not Found ------911.20 72 25.80* 1.508E+OO 8.193E-01 8.193E-01 48.07 968. 97 47 15.80 1.432E+OO 9.129E-01 9.129E-01 48.81 U-234 609.32 124 45.49* 2 .117E+OO 5.666E-01 5.666E-01 27.84 1120.29 18 14.92 l.266E+OO 4.246E-01 4.246E-01 125.97 1764.49 16 15.30 8.365E-01 5.620E-01 5.620E-01 52.95 AM-243 43.53 48 5.90 1.014E-01 3.532E+Ol 3.532E+Ol 133. 45 74.66 115 67.20* 3.134E+OO 2.401E-01 2. 401E-01 49.99 CF-249 252.80 ------2.50 4.533E+OO ------Line Not Found ------333.37 ------14.60 3.593E+00 ------Line Not Found ------388.16 12 66.00* 3.135E+OO 2.481E-02 2.485E-02 156.84 ANH-511 511. 00 2 100.00* 2.465E+OO 3.170E-03 3.170E-03 2134.97 Flag: "*" Key line Page 3754 of 5809 Summary of Nuclide Activity Sample ID : G405235038 Acquisition date Page : 3 3-0CT-2016 09:17:37 Total number of lines in spectrum 49 Number of unidentified lines 9 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-113 SN-126 CS-135 BA-137M CS-137 TM-171 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 CF-249 ANH-511 Hlife 1.25E+09Y 80.30D 461. 40D 115. 09D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y 1.92Y 1. 41E+10Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 4IE+l0Y 1600.00Y 1. 41E+l0Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7370.00Y 351.00Y l.OOE+09Y Decay 1. 00 14.3 1. 59 6.39 1. 00 'l. 00 1. 02 1. 02 1. 36 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.238E+Ol 1.918E+OO 3.787E+OO 3.501E-02 3.787E-01 1.698E-01 l.071E-01 1.131E-01 1. 263E+02 2.845E-01 2.137E+OO 9.370E-01 5.666E-01 7.757E-01 5.666E-01 2.183E+OO 5.666E-01 8.193E-01 8.193E-01 9.370E-01 5.666E-01 6.635E-01 8.193E-01 5.666E-01 2.401E-01 2.481E-02 3.170E-03 1.587E+02 l.587E+02 Decay Corr pCi/GRAM l.238E+Ol 2.738E+Ol 6.016E+OO 2.237E-01 3.787E-01 l.698E-01 l.092E-01 1.154E-01 l.713E+02 2.845E-01 2.137E+OO 9.370E-01 5.668E-01 7.760E-01 5.668E-01 2.183E+OO 5.668E-01 8.193E-01 8.193E-01 9.370E-01 5.666E-01 6.635E-01 8.193E-01 5.666E-01 2.401E-01 2.485E-02 3.170E-03 2.315E+02 2.315E+02 81. 63% Decay Corr 2-Sigma Error 0.147E+Ol 2.699E+Ol 3.127E+OO 2.501E-01 1. 969E-01 1.435E-01 0.575E-01 0.608E-01 1. 016E+02 0.680E-01 0.472E+OO l.230E-01 1.578E-01 1.714E-01 1.578E-01 1.268E+OO 1.578E-01 3.939E-01 3.939E-01 1.230E-01 1.578E-01 6 .116E-01 3.939E-01 1. 578E-01 1. 200E-01 3.897E-02 67.68E-03 "M" Manually accepted 2-Sigma %Error 11. 86 98.59 51. 98 111.79 51.98 84.47 52.70 52.70 59.33 23.91 22.09 13.13 27.84 22.09 27.84 58.08 27.84 48.07 48.07 13.13 27.84 92.17 48.07 27.84 49.99 156.84 2134.97 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3755 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235038 Acquisition date : 3-0CT-2016 09:17:37 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 92.78 70 144 1. 51 185.37 182 7 1.42E-02 75.9 4. 71E+OO T 0 111. 81 18 118 0.44 223.43 219 7 3.77E-03 **** 5.64E+OO T 4 126.75 23 59 1. 21 253.32 252 10 4.75E-03 **** 5. 96E+OO T ' 4 129 .11 49 143 1. 39 252 10 1. 04E-02 **** 5.98E+OO T 0 185. 96 83 148 1.23 371. 78 366 9 1. 82E-02 66.4 5.57E+OO T 0 209.35 38 105 1. 34 418.57 415 10 8.40E-03 **** 5.19E+OO 0 258.87 33 82 0.94 517.65 512 10 7.41E.:...03 **** 4.45E+OO 3 270.05 44 81 1. 95 540.00 531 14 9.98E-03 91. 8 4.30E+OO T 0 308.04 9 56 0.55 616.00 609 8 2.0lE-03 **** 3.85E+OO T 0 463.79 81 27 2.35 927.58 918 19 1.98E-02 40.4 2.68E+OO T 0 490.97 30 44 6.33 981. 95 973 19 7.28E-03 **** 2.55E+00 T 0 720.47 18 17 1.24 1441. 05 1437 10 4.54E-03 **** 1. 84E+00 T 0 728. 72 66 34 2.78 1457.56 1446 26 1. 71E-02 56.8 1. 82E+OO T 0 769.43 20 31 1. 31 1538.98 1533 14 5. llE-03 **** 1.74E+OO 0 796. 61 10 26 3.78 1593.35 1581 14 2.62E-03 **** 1. 69E+00 T 0 827. 72 17 8 2.40 1655.58 1650 11 4.46E-03 85.2 1.63E+OO 1 854.43 16 17 2.04 1709.00 1703 20 4.28E-03 **** 1.59E+OO 1 856.93 31 16 2.04 1714.00 1703 20 8.14E-03 61. 8 1.59E+OO T 1 965.12 21 11 2.34 1930.43 1926 24 5.52E-03 68.2 1.44E+OO T 0 1032. 96 10 5 1. 42 2066.10 2062 8 2.58E-03 **** l.36E+OO 4 1065.40 16 7 2.20 2131.00 2125 14 4.39E-03 71. 7 1.32E+OO 4 1067.83 8 1 1. 80 2135.85 2125 14 2.14E-03 **** 1.32E+00 0 1177.22 15 13 1. 65 2354.66 2348 14 4.27E-03 **** 1.21E+OO T 0 1244.93 6 9 0.47 2490.08 2484 8 1.69E-03 **** 1.16E+OO Flags: "T" = Tentatively associated Page 3756of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:20:18.98 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l * *Acquisition date 3-0CT-2016 09:17:37 Sensitivity 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.65 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Nuclide Library : SOLID *
  • Sample ID G405235038 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7019E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA:GAMMA]EFF GAM43 CAN.CNF;?
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-113 SN-126 CS-135 BA-137M CS-137 TM-171 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 CF-249 ANH-511 Le (pCi/GRAM 2.725E-01 1.147E+Ol 1.000E+OO l.903E-01 6.348E-02 l. lllE-01 2.598E-02 2.744E-02 2. 715E+Ol 2.734E-02 4.032E-02 5.938E-02 5.180E-02 5.938E-02 4.323E-01 5.938E-02 1.144E-01 l.144E-01 4.032E-02 5.936E-02 3. 396E-01 1.144E-01 5.936E-02 4.942E-02 1.635E-02 2.108E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3757of5809 Le (pCi/GRAM 9.992E+OO 4.012E-02 O.OOOE+OO 2.196E-02 3.803E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3758of5809 O.OOOE+OO 0.000E+OO 5.818E-02 3.949E-01 O.OOOE+OO 4.280E-02 5.476E-Ol 7.116E+OO 3.849E-02 l 1.632E+OO O.OOOE+OO l.669E-01 O.OOOE+OO O.OOOE+OO 6.414E-01 5.644E+OO 6.491E-01 O.OOOE+OO 1. 031E-01 5.072E+02 2. 411E-02 6.859E-01 l.977E+OO 1. 411E+00 O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 3.000E-02 5.018E-02 4.956E+OO 4.134E-01 4 .134E-01 2 .137E-02 6.734E-02 O.OOOE+OO O.OOOE+OO 1. 081E-01 1.933E+00 7.582E-02 2.771E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.201E-02 O.OOOE+OO 5.002E-02 O.OOOE+OO O.OOOE+OO 8.090E-02 O.OOOE+OO O.OOOE+OO 2.302E+Ol O.OOOE+OO 2.805E-01 5.210E-02 4.562E+OO 3.390E-02 O.OOOE+OO 7.202E+02 O.OOOE+OO 1. 962E-02 7.357E-02 l.678E-01 9. 911E-02 9.297E-02 1.710E+00 4.327E-02 2.141E-01 5.647E-02 2.036E-02 3. 772E+OO 1.028E+OO 4.584E+OO SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN.-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-251 Page 3759 of 5809 2.777E+Ol 9.476E+Ol 4.135E-01 1. 749E+OO 3.784E-02 8.202E+OO 3.494E-01 5.535E-01 6.189E-01 3.146E-01 4.663E-01 1.716E-01 1.716E-01 3.491E-01 4.663E-01 4.989E-02 2.415E-01 2.729E+OO 1.462E+OO l.628E-01 4.989E-02 O.OOOE+OO 1.462E+OO 2.059E-01 3.040E+02 1. 639E-01 8.239E-02 5.455E-02 2.962E-02 8.557E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. , VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:20:24.07 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235038.CNF;l *
  • Acquisition date 3-0CT-2016 09:17:37 Sensitivity : 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.65 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Nuclide Library : SOLID *
  • Sample ID G405235038 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity 1.7019E+02 GRAM *
  • Quantity Err(%) 1.1751E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;?
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.238E+Ol 1.578E+OO AS-73 2.738E+Ol 2.705E+Ol CD-109 4.845E+OO 3 .113E+OO SN-113 2.237E-01 2.453E-01 SN-126 3.050E-01 l.953E-01 CS-135 1.698E-01 1. 411E-01 BA-137M 1.092E-01 5.659E-02 CS-137 l.154E-01 5.978E-02 TM-171 1.713E+02 1.008E+02 TL-208 2.845E-01 6.776E-02 PB-212 9.370E-01 1.306E-01 BI-214 5.668E-01 1.566E-01 PB-214 7.760E-01 1. 711E-01 RN-222 5.668E-01 1.566E-01 RA-224 7.685E-01 1.316E+OO RA-226 5.668E-01 1.566E-01 AC-228 8.193E-01 3.883E-01 RA-228 8.193E-01 3.883E-01 TH-228 9.370E-01 1.306E-01 TH-230 5.666E-01 1.565E-01 PA-231 6.635E-01 6.158E-01 TH-232 8.193E-01 3.883E-01 U-234 5.666E-01 1.565E-01 AM-243 1. 711E-01 1.202E-01 CF-249 2.485E-02 3.825E-02 ANH-511 3.170E-03 6.633E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3760of5809 Key-Line Activity (pCi/GRAM -5.736E+OO -l.412E-02 l.000E+41 -1.236E-02 K.L Act error ( 1. 96-sigma) 1. 264E+Ol 4.878E-02 2.190E+41 3 .112E-02 TPU ( 1. 96-sigma) l.578E+00 2.705E+Ol 3 .113E+OO 2.453E-01 1.953E-01 l.411E-01 5.659E-02 5.978E-02 1.008E+02 6.776E-02 1. 306E-01 1.566E-01 1.711E-01 1.566E-01 1.316E+OO 1.566E-01 3.883E-01 3.883E-01 1. 306E-01 1.565E-01 6.158E-01 3.883E-01 l.565E-01 1.202E-01 3.825E-02 6.633E-02 TPU ( 1. 96-sigma) 1.290E+Ol 4.919E-02 O.OOOE+OO 3.162E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 2.703E-01 3. 969E-01 4.152E-01 FAIL ABUN V-48 -1.199E+04 2.036E+04 2.106E+04 SHORT HLIF CR-51 -6.908E+Ol 4.353E+02 4.364E+02 SHORT HLIF MN-54 2.686E-02 6.305E-02 6.420E-02 NOT IDENT. C0-56 -3. 201E-03 4.586E-01 4.586E-01 NOT IDENT. MN-56 -1.000E+41 3.143E+43 0.000E+OO SHORT HLIF C0-57 5.143E-03 4.857E-02 4.863E-02 NOT IDENT. C0-58 1.387E-01 6.086E-01 6 .119E-01 NOT IDENT. FE-59 2.372E+OO 8.066E+OO 8.137E+OO NOT IDENT. C0-60 l.128E-02

  • 4.240E-02 4.270E-02 NOT IDENT. ZN-65 O.OOOE+OO 1.607E-01 O.OOOE+OO NOT IDENT. GE-68 -2.413E-01 2.007E+OO 2.0lOE+OO NOT IDENT. AS-74 l.938E+03 6.441E+03 6.500E+03 SHORT HLIF SE-75 3.837E-02 2.005E-01 2.013E-01 NOT IDENT. BR-77 1. 797E+39 l.597E+40 0.000E+OO SHORT HLIF SR-82 -7.878E+02 l.044E+03 l.103E+03 SHORT HLIF RB-83 -2.502E-01 7.350E-01 7.436E-01 NOT IDENT. KR-85 -2.349E+OO 7. 962E+OO 8.032E+OO NOT IDENT. SR-85 -2. 721E-01 9.160E-01 9.241E-01 NOT IDENT. RB-86 1.139E+03 3.308E+04 3.308E+04 SHORT HLIF Y-88 -8.303E-02 1. 712E-01 1. 753E-01 NOT IDENT. Y-91 -1.197E+02 5.995E+02 6.020E+02 NOT IDENT. NB-94 -1. 205E-02 2.924E-02 2.974E-02 NOT IDENT. NB-95 -9.290E-02 9.182E-01 9.192E-01 NOT IDENT. NB-95M -3.887E-01 2.455E+OO 2.461E+OO NOT IDENT. ZR-95 8.792E-01 1.478E+OO 1.530E+OO NOT IDENT. NB-97 1. OOOE+41 9.874E+40 O.OOOE+OO SHORT HLIF ZR-97 -l.000E+41 6.661E+41 O.'OOOE+OO SHORT HLIF M0-99 -1.597E+32 1. 403E+33 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 1.528E+41 O.OOOE+OO SHORT HLIF RH-101 2.937E-02 3.049E-02 3.324E-02 FAIL ABUN RH-102 l.634E-02 5.399E-02 5.449E-02 NOT IDENT. RU-103 -3.664E+OO 7.346E+00 7.529E+OO FAIL ABUN RH-106 -4.074E-02 4.694E-01 4.698E-01 NOT IDENT. RU-106 -4.074E-02 4.694E-01 4.698E-01 NOT IDENT. AG-108M -l.106E-02 2.638E-02 2.685E-02 NOT IDENT. AG-llOM -l.242E-01 l.037E-01 l.179E-01 NOT IDENT. CD-115 -4.955E+40 3. 581E+40 O.OOOE+OO SHORT HLIF SN-ll 7M -2.620E+04 l.160E+05 l.166E+05 SHORT HLIF TE-123M 2.577E-02 l.123E-01 l.129E-01 NOT IDENT. SB-124 1.463E+OO 1. 781E+OO 1. 899E+OO NOT IDENT. SB-125 -6.762E-02 9. 772E-02 l.024E-01 FAIL ABUN TE-125M 3.479E+Ol 3.382E+02 3.386E+02 NOT IDENT. I-126 -4.637E+05 1.435E+06 1. 450E+06 SHORT HLIF SB-126 2.522E+06 2.567E+06 2.807E+06 SHORT HLIF SB-127 -2.615E+22 9.749E+22 O.OOOE+OO SHORT HLIF I-131 7.203E+09 9. 621E+09 l.015E+10 SHORT HLIF I-132 1.000E+41 2.054E+42 O.OOOE+OO SHORT HLIF TE-132 -5.779E+26 l.853E+27 O.OOOE+OO SHORT HLIF BA-133 5.826E-03 3.982E-02 3. 991E-02 FAIL ABUN I-133 1.000E+41 2.100E+41 O.OOOE+OO SHORT HLIF CS-134 4.068E-02 9.243E-02 9.423E-02 FAIL ABUN I-135 1.000E+41 1.305E+42 O.OOOE+OO SHORT HLIF CS-136 -1.930E+05 4.903E+05 4.979E+05 SHORT HLIF CE-139 -1.039E-01 9.669E-02 l.074E-01 NOT IDENT. BA-140 -3.555E+05 2.035E+06 2. 041E+06 SHORT HLIF LA-140 -6.638E+05 6.144E+05 6.834E+05 SHORT HLIF CE-141 -l.347E+Ol 2. 513E+Ol 2.586E+Ol NOT IDENT. CE-143 1.000E+41 1. 419E+41 O.OOOE+OO SHORT HLIF CE-144 -2.379E-01 3.260E-01 3.432E-01 NOT IDENT. PM-144 1.692E-02 5.686E-02 5.737E-02 NOT IDENT. PR-144 1.550E+OO 4.970E+OO 5.019E+OO NOT IDENT. PM-146 -1.941E-02 4.179E-02 4.269E-02 NOT IDENT. ND-147 -2.956E+07 4. 901E+07 5.079E+07 SHORT HLIF I PM-147 3.652E+Ol 8.214E+02 8.216E+02 NOT IDENT. i?M-149 l.OOOE+41 l.428E+41 O.OOOE+OO SHORT HLIF EU-150 -1.836E-02 2.755E-02 2.877E-02 FAIL ABUN EU-152 -3.342E-02 8. 727E-02 8.856E-02 FAIL ABUN GD-153 -l.124E-01 1.984E-01 2.047E-01 NOT IDENT. EU-154 -4.213E-02 1. 217E-01 1.232E-01 NOT IDENT. EU-155 2.382E-02 1.030E-01 1.035E-01 NOT IDENT. TB-160 1.138E+OO 1.777E+OO l.850E+OO FAIL ABUN H0-166M -3.298E-02 5.642E-02 NOT IDENT. HF-172 2.024E-01 2.095E-01 2.285E-01 FAIL ABUN LU-172 -3.067E-02 7.438E-02 7.566E-02 FAIL ABUN LU-176 1.058E-02 3.518E-02 3.550E-02 FAIL ABUN HF-181 2.507E-01 4.386E+OO 4.388E+OO NOT IDENT. TA-182 3.567E-01 1.128E+00 l.140E+OO FAIL ABUN Page 3761of5809 RE-183 2.083E+OO 5 .151E+OO 5.236E+OO NOT IDENT. RE-184 -1.787E+Ol 3.752E+Ol 3.837E+Ol NOT IDENT. W-188 2.622E+Ol 1.143E+02 1.150E+02 NOT IDENT. IR-192 3.321E-01 4.276E-01 4.531E-01 FAIL ABUN HG-203 -2 .113E-01 2.204E+OO 2.206E+OO NOT IDENT. BI-207 -8.451E-03 5.413E-02 5.426E-02 FAIL ABUN PB-210 -3.340E+OO 9.832E+OO 9.947E+OO NOT IDENT. BI-211 2.137E+OO 4. 725E-01 1.073E+OO FAIL ABUN PB-211 -2.421E-01 6.676E-Ol 6.764E-01 NOT IDENT. BI,..-212 2.400E+OO 1 *. 342E+OO 1.723E+OO FAIL ABUN
  • RN-219 l.009E-01 3.493E-01 3.522E-01 FAIL ABUN RA-223 1.027E-01 5.134E-01 5.155E-01 FAIL ABUN AC-227 -2.400E-02 2.142E-01 2.145E-01 FAIL ABUN TH-227 -2.400E-02 2.142E-01 2.145E-01 FAIL ABUN TH-229 1.758E-03 3.749E-01 3.749E-01 FAIL ABUN TH-231 1.027E-01 5.134E-01 5.155E-01 FAIL ABUN PA-233 3.351E-02 5.237E-02 5. 451E-02 FAIL ABUN PA-234 -9. 969E-02 3.220E-01 3. 251E-01 FAIL ABUN PA-234M -3.021E+OO 3.892E+OO 4.123E+OO NOT IDENT. TH-234 -l.459E-01 1.592E+OO 1.593E+OO FAIL ABUN U-235 2.090E-01 l.577E-01 1.837E-01 FAIL ABUN NP-237 3. 351E-02 5.237E-02 5. 451E-02 FAIL ABUN NP-238 -1.000E+41 2.624E+41 O.OOOE+OO SHORT HLIF U-238 -1.459E-01 1.592E+OO 1.593E+OO FAIL ABUN NP-239 l.137E-01 2.241E-01 2.299E-01 FAIL ABUN PU-239 5.759E+02 5.802E+02 6.356E+02 FAIL ABUN AM-241 -1.384E-01 l.912E-01 2. OllE-01 NOT IDENT. CM-243. -4.867E-02 9.795E-02 1.004E-01 FAIL ABUN BK-247 4.107E-03 6. 672E-02 6.675E-02 NOT IDENT. CM-247 1.285E-02 3.255E-02 3.306E-02 FAIL ABUN CF-251 -7.742E-02 9.792E-02 1.040E-01 NOT IDENT. Page 3762of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 68.8594 87.09 79.7662 136.47 80.3799 45.60 57.9438 87.57 79.8461 140.51 0.0000 46.54 69.1879 88.03 79.9228 143.76 56.7160 49.72 0.0000 88.34 79.9741 144.24 67.7686 51. 35 50.5560 88.47 79.9953 145.44 83.1620 51. 87 50.6340 89.96 67.1245 152.43 77.1451 52.39 33.8077 1093.63 67.2178 153.25 0.0000 52.97 33.8651 91.11 0.0000 323.87 63.5892 53.44 33. 9114 92.59 80.6692 156.02 0.0000 54.07 33.9731 93.35 74.5771 158.56 0.0000 57.36 0.0000 94.56 74.7563 159.00 59.6878 57.53 55.7471 94.65 74.7695 162.33 65.1733 57.98 58.6783 94.67 74.7725 162.66 0.0000 59.27 74.3243 94.87 79.4774 163.33 42. 6372 59.32 75.4116 97.43 90.4476 165.86 75.0864 59.54 71.1447 98.43 63.5532 176.31 63.7236 60. 96 72.4976 98.44 63.5544 176.60 0.0000 61.17 72.5380 99.53 79.0191 177.52 74.4587 62.93 85. 9262 100 .11 73.2031 181.07 0.0000 63.29 72.9421 102.03 60.4341 181.52 74.8339 63.58 59.9228 103.18 74.8139 184.41 71. 5259 64.28 66.5797 103.37 74.8409 143.76 71. 6414 66.73 87.8613 105.21 63.1757 193.51 56.9508 67.24 81. 37 50 105.31 63.1870 197.03 68.9886 125.81 79.2625 106.12 78.8025 198.01 67.2507 67.75 79.2757 106.47 80.0476 201.83 72.1137 69.67 82.9697 109.28 76.8521 203.43 64.9302 70.83 85.7905 111. 00 71. 0649 205.31 59.1132 72.81 90.6542 111. 76 0.0000 210.85 59.0221 72.87 90.6673 114.06 61.3553 215.65 59.3372 74.66 82.8384 116. 30 0.0000 222 .11 57.8879 74.82 82.8689 116.74 58.3949 227.09 52.5644 74. 97 82.8977 119.76 78.2588 227.38 50.7025 77 .11 83.3053 121.12 72.3087 228.16 0.0000 78.74 84.3652 121. 22 72. 3208 228.18 52.6248 79.69 67.9372 121. 78 73.6148 116.74 52.6248 80.12 66.4910 122.06 73.6491 235.69 61. 0881 80.19 0.0000 122.92 72.5247 235. 96 56.8420 80.57 81.6833 123.07 75.0014 238.63 56.9977 81. 00 83.2749 265.00 85.3331 238.98 0.0000 81. 07 83.2878 125.81 79.0430 240.99 57.1344 81.75 90.9949 127.23 89.1266 242.00 57.1930 83.79 59.4081 127.91 89.2246 244.70 44.4447 84.00 73.1509 129.30 89.4221 252.40 0.0000 85.43 76.4313 131.20 71. 4208 252.80 39.5031 86.55 79.6763 133.02 63. 2962 254.15 0.0000 86.79 79.7160 133.52 79.0154 256.23 46.4016 86.94 79.7414 136.00 75.3021 260.90 0.0000 Page 3763 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 39.4676 355.39 0.0000 584:27 15.9849 264.80 40.9353 356.01 31.5692 595.83 0.0000 265.00 40.9430 364.49 0.0000 427.87 28.3889 268.22 48.8892 366.42 0.0000 602.52 0.0000 269.46 48.9451 372.51 35.1531 604.72 30.8335 270.03 4fL 9716 375.05 33.0832 39.6905 271.23 52.9486 377.52 31.0043 609.32 28.5119 273.65 0.0000 356.01 25.7749 610.33 20.6124 276.40 41.3779 388.16 9.6953 614.28 33.1919 277.37 41. 414 7 388.63 0.0000 618.01 28.6339 277.60 41.4232 391. 69 30.7776 620.36 24.0433 278.00 26.6391 264.66 29.3401 621. 93 21. 2852 279.20 32.5945 401.81 29.3632 630.19 0.0000 279.54 41.4967 402.40 29.3747 631.29 17.6635 279.70 41.5027 404.85 40.3220 633.25 18.6102 280.46 38.5644 410.95 36 .1119 634.78 0.0000 283.69 39.6688 413.71 28.5047 635.95 13.0443 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 39.7298 423.72 0.0000 645.85 14.9775 285.90 0.0000 427.09 32.0769 657.76 7.5308 287.50 51. 7440 427.87 34.3067 657.90 0.0000 290.67 38.9175 433.94 32.2203 661. 66 17.9180 293.27 0.0000 439.40 24.5289 664.57 0.0000 351. 93 39. 0722 453.88 29.2553 666.33 0.0000' 295. 96 39.0976 463.37 16.9775 666.50 0.0000 879.38 24 .1143 468.07 22.1343 667.71 0.0000 299.98 31. 6884 473.00 0.0000 677.62 15.1997 300.09 31. 6916 475.06 20.5181 685.70 0.0000 300.13 31.6923 476.78 21.6804 695.00 0.0000 301.36 42.3008 477.60 27.3994 696.49 22.0349 302.85 39.3293 482.18 21. 7 507 696. 51 22.0349 256.23 40.3947 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 23.0010 306.78 34.9078 497.08 29.4486 697.49 23.0032 308.46 45. 5960 505.52 22.6294 702.65 23.0559 311. 90 33.5338 507.63 0.0000 706.68 19.2474 316.51 29.5817 511. 00 23.2823 711.68 24.1119 319.41 0.0000 514.00 33.2338 720.70 0.0000 320.08 0.0000 514.00 33.2338 721. 93 0.0000 321.04 34.8114 520.40 35.1099 722.78 15.5059 323.87 35.9179 520.69 0.0000 722.91 15.5068 325.23 35.9570 522.65 0.0000 723.31 15.5093 328.76 0.0000 527.90 0.0000 724.19 15.5151 333.37 44.6713 528.26 23.8030 727. 33 21.7506 333.97 51. 2100 529.59 11. 4690 733.00 21.8032 334.37 41.9123 529.87 0.0000 735.93 17.1526 338.28 49.8271 531.02 0.0000 333.97 20.2846 338.32 49.8291 537.26 0.0000 739.50 0.0000 311. 90 45.2337 546.56 0.0000 747.24 15.6680 340.48 45.2337 552.55 16.9729 748.06 19.5917 340.55 0.0000 563.25 22.4602 752.31 16.6825 344.28 42.7601 569.33 18.9265 753.82 0.0000 345.93 37.5930 946.00 19.8294 756.73 13.7637 351.06 33.5475 569.70 20.7328 756.80 13.7642 351. 93 33.5697 583.19 22.6936 884.68 18.9322 Page 3764 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.3680 1274.44 9.6671 1620.50 6.0920 766.42 18.9516 1001.03 17.2129 1621. 92 4.0625 766.84 15.7959 1002.74 7.5349 1678.03 0.0000 772. 60 0.0000 1004.73 10. 7712 1690.97 1.0309 776.52 0.0000 507.63 0.0000 1750.46 0.0000 . 739.50 0.0000 1025.87 0.0000 1764.49 3.1403 778.90 15.8735 1028.54 0.0000 1063.66 14.6720 783.70 0.0000 1037.84 8.7100 1771. 35 5.2412 785.37 12.9310 1038.76 0.0000 1791.20 0.0000 792.07 9.5748 631.29 12.0098 1808.65 5.2808 794.95 18. 9722 1048.07 0.0000 1810.72 0.0000 795.86 23.9729 1049.04 14.2045 1836.06 3.1857 810.06 17.0768 1050.41 8.7451 810.29 18.0829 1063.66 14.0500 344.28 18.0840 1077.00 0.0000 810.76 15.0719 1077.34 9.9212 815.77 0.0000 1085.87 8.8423 1048.07 0.0000 1093.63 14.4028 832.01 19.4514 1099.45 13.3191 834.85 15.2129 1112. 07 10.0272 835.71 13.1888 1112.84 11.1444 836.80 0.0000 1115. 54 8.9224 846.75 0.0000 1120.29 16.7542 846.77 14'.2636 1120. 55 16.7551 856.80 0.0000 1221.41 16.7587 860.56 13.1086 1129. 67 19.0410 871.09 16.4502 1131. 51 0.0000 873.19 14.4050 1147.95 0.0000 875.33 0.0000 1173.23 7.5631 879.38 9.2815 1177.95 10.9055 880.51 11. 3488 1189.05 15.4992 883.24 16.5239 1204.77 17.3997 884.68 22.7318 1221.41 19.3214 889.28 11. 3850 1231. 02 16.6052 894.76 8.2966 1235.36 0.0000 898.04 13.4979 1238.28 17.1668 900. 72 14.5503 1260.41 0.0000 903.28 19.0218 1271.87 8.3962 911.20 17.7346 1274.44 15.8703 912.08 17.7398 1274.54 14.9367 923.98 0.0000 1291.59 9.3784 926.50 17.8306 1298.22 0.0000 929 .11 17.8472 1312.11 0.0000 937.49 22 .1113 1332. 49 10.4274 944 .13 0.0000 1362.66 0.0000 946.00 20.0646 1365.19 5.7357 949.00 20.0849 1368.63 0.0000 667.71 0.0000 1384.29 9.6060 962. 31 16.9912 1408.01 4.8315 964. 08 15.3013 1457.56 0.0000 966 .17 15.9499 1460.82 7.8305 911.20 15. 9654 1489.16 1. 9709 968. 97 15. 9654 1505.03 9. 8911 983.53 0.0000 1584.12 12.0861 984.45 0.0000 1596.21' 0.0000 Page 3765of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:20:52.95 ******************************************************************************** *
  • GEL LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date : Z-OCT-2016 11:02:28. Sample date 30-NOV-2015 10:43:00 Acquisition date : 3-0CT-2016 09:18:06. Sample ID G405235039 Sample quantity 1.75326E+02 GRAM Detector name : GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.74 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 0 0 0 0 0 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 40.61* 75.04 77.09* 87.13 92.79* 178.00 181.98 186.14* 209.28 238.57* 241.92 259.16 272.46 295.31 300.41 338.82 351. 74* 419.10 462.78 510.73* 518.48 583.37* 596.54 609.37* 728. 90 795.09 861.58 911. 87* 969 .18* 1011. 06 1031.91 1104. 71 1120.13 1136.61 Page 3766 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 26 84 141 37 58 32 22 72 49 271 55 32 16 106 34 88 244 19 41 75 13 93 6 158 17 15 26 58 36 11 8 13 34 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 86 131 92 119 128 55 57 103 90 110 48 57 73 63 50 57 28 24 29 22 18 38 20 12 40 22 9 27 8 5 10 4 3 5 1. 05 1.16 1. 05 0.69 0.83 1. 05 0.94 0.80 1. 05 1.19 0.89 1.18 0.63 1. 54 1. 56 1. 67 1. 35 0.99 1. 37 1. 97 0.76 1. 46 0.64 1. 39 1. 37 1. 72 4.22 0.89 2.19 1.16 0.50 1. 29 2.31 0.85 81. 66 150.54 154.65 174.74 186.05 356.55 364.51 372. 82 419.14 477.73 484.44 518.92 545.55 591.25 601.46 678.32 704.17 838.96 926.37 1022.31 1037.82 1167. 68 1194. 03 1219.70 1458.93 1591.39 1724.45 1825 .11 1939.81 2023.64 2065.38 2211. 07 2241.95 2274.93 78 146 146 172 183 353 362 368 414 472 482 514 541 586 586 673 696 835 919 1014 1033 1163 1188 1214 1452 1582 1719 1817 1935 2017 2060 2208 2236 2272 8 7.12E-03 67.4 13 2.33E-02 24.9 13 3.91E-02 14.7 6 1.03E-02 49.8 8 1. 60E-02 37. 7 8 8.78E-03 44.2 7 6.00E-03 62.2 10 2.0lE-02 29.6 10 1. 37E-02 39 .1 10 7.52E-02 9.6 6 1.53E-02 24.8 10 8.84E-03 47.9 10 4.51E-03104.6 25 2.93E-02 16.4 25 9.38E-03 43.7 14 2. 44E-02 21. 0 16 6.77E-02 8.2 8 5.40E-03 50.1 15 1. 13E-02 33. 2 15 2.08E-02 21.6 10 3.68E-03 67.9 13 2.58E-02 17.3 9 1.71E-03137.5 14 4.39E-02 9.3 15 4.59E-03 88.1 12 4.30E-03 64.6 12 7.35E-03 29.8 18 1. 61E-02 25 .1 12 1.00E-02 24.1 9 3.06E-03 46.5 10 2.22E-03 82.0 7 3.62E-03 39.3 11 9.57E-03 19.4 6 2 .14E-03 61. 0 Fit 7.66E-01 2.19E+00 Peak Search Report (continued) : 2 Sample ID : G405235039 Acquisition date 3-0CT-2016 09:18:06 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1156.28 14 6 4.08 2314.30 2308 11 3.75E-03 43.3 36 0 1318.67 10 7 1. 32 2639.37 2631 13 2.64E-03 64.1 37 0 1360.33 7. 2 0.95 2722.75 2718 8 1. 94E-03 SJ_. 5 38 0 1460.76* 347 15 2.26 2923.82 2914 20 9.64E-02 6.1 39 0 1764.36 25 0 0.67 3531.64 3526 10 6.94E-03 20.0 Flag: "*" = Peak area was modified by background subtraction Page 3767 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:20:54 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 10:43:00 G405235039 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:18:06 175.33 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID
  • GAMMA44 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3768 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.74 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235039 Acquisition date 3-0CT-2016 09:18:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 . 1460.82 10.66* l.030E+OO 1.326E+Ol 1.326E+Ol 12.16 OK CD-109 88.03 3.70* 4.450E+OO 6.341E-01 1.007E+OO 214.94 OK SN-126 64.28 9.60 2.161E+OO Line Not Found Absent 86.94 8.90 4.450E+OO 2.636E-01 2.636E-01 214.94 OK 87.57 37.00* 4.450E+OO 6.341E-02 6.341E-02 214.94 OK TL-208 277.37 6.60 4.074E+OO Line Not Found Absent 583.19 85.00* 2.178E+OO 2.398E-01 2.398E-01 34.57 OK 860.56 12.50 1.591E+OO 6.033E-01 6.033E-01 59.55 OK BI-211 72.87 1. 23 3.135E+OO Line Not Found Absent 351.06 12.92* 3.338E+OO 7.570E-01 7.570E-01 111. 45 OK PB-212 74.82 10.28 3.363E+OO 1.044E+OO 1.044E+OO 72 .10 OK 77 .11 17.10 3.570E+OO l.404E+OO 1.404E+OO 29.48 OK 238.63 43.60* 4.587E+OO 7.262E-01 7.262E-01 19.24 OK 300.09 3.30 3.815E+OO 1.398E+OO 1.398E+OO 87.41 OK BI-214 609.32 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 OK 1120.29 14.92 1. 288E+OO 7. 831E-01 7.834E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 OK PB-214 74.82 5.80 3.340E+OO Line Not Found <<INT Reject 77 .11 9.70 . 3.570E+OO 2.476E+OO 2.477E+OO 29.48 OK 87.09 3.41 4.447E+OO Line Not Found <<INT Reject 242.00 7.25 4.538E+OO Line Not Found <<INT Reject 295.22 18.42 3.870E+OO 7.744E-01 7.747E-01 32.77 OK 351. 93 35.60* 3.336E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.102E+00 7.863E-01 7.865E-01 18.53 OK 1120.29 14.92 1. 288E+OO 7. 831E-01 7.834E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 OK RA-224 240.99 4.10* 4.539E+OO 2 .131E-01 2.131E-01 424.31 OK RA-226 609.32 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 OK 1120.29 14.92 l.288E+OO 7. 831E-01 7.834E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 OK AC-228 '105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.446E+OO 1.162E+OO 1.162E+OO 42.03 OK 794.95 4.25 1. 696E+OO 9.848E-01 9.848E-01 129. 26 OK 835.71 1. 61 l.630E+OO Line Not Found Absent 911. 20 25.80* 1.520E+OO 6.656E-01 6.656E-01 50.14 OK 968. 97 15.80 l.448E+OO 7.020E-01 7.020E-01 48.17 OK RA-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11.27 3.446E+OO 1.162E+OO 1.162E+OO 42.03 OK 794.95 4.25 1. 696E+OO 9.848E-01 9.848E-01 129. 26 OK 835. 71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* l.520E+OO 6.656E-01 6.656E-01 50.14 OK 968. 97 15.80 1.448E+OO 7.020E-01 7.020E-01 48.17 OK TH-228 74.82 10.28 3.363E+OO 1.044E+00 1.044E+OO 72 .10 OK 77 .11 17.10 3.570E+OO l.404E+OO 1.404E+OO 29.48 OK 238.63 43.60* 4.587E+OO 7.262E-01 7.262E-01 19.24 OK 300.09 3.30 3.815E+OO 1.398E+OO 1.398E+OO 87.41 OK TH-230 609.32 45.49* 2.102E+OO 7.863E-01 7.863E-01 18.53 OK 1120.29 14.92 1. 288E+OO 7. 831E-01 7.831E-01 38.74 OK 1764.49 15.30 8.674E-01 7.675E-01 7.675E-01 40.00 OK Page 3769of5809 Nuclide Line Activity Report (continued) Sample ID : G405235039 Acquisition date Nuclide Type: Uncorrected Decay Corr Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM PA-231 .283.69 1. 70 4.000E+OO Line Not Found 301.36 5.35* 3.815E+OO 8.623E-01 8.623E-01 TH-232 105.21 1.10 5.460E+OO Line Not Found 338.32 11. 27 3.446E+OO 1.162E+OO 1.162E+OO 835.71 1. 61 l.630E+OO Line Not Found 911.20 25.80* 1.520E+OO 6.656E-01 6.656E-01 968. 97 15.80 1.448E+OO 7.020E-01 7.020E-01 U-234 609.32 45.49* 2.102E+OO 7.863E-01 7.863E-01 1120.29 14.92 1.288E+OO 7.831E-01 7. 831E-01 1764.49 15.30 8.674E-01 7.675E-01 7.675E-01 AM-243 43.53 5.90 1.573E-01 Line Not Found 74.66 67.20* 3.363E+OO 1.597E-01 1.597E-01 ANH-511 511. 00 100.00* 2.432E+OO 1.498E-01 1.498E-01 Flag: "*" = Keyline Page 3770 of 5809 Page : 3 3-0CT-2016 09:18:06 2-Sigma %Error Status Absent 87.41 OK Absent 42.03 OK Absent 50.14 OK 48.17 OK 18.53 OK 38.74 OK 40.00 OK Absent 72.10 OK 43.22 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:20:55.72 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l * *Acquisition date 3-0CT-2016 09:18:06 Sensitivity 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:43:00 Analyst initials: MXRl * *Sample ID G405235039 Sample Quantity 1.7533E+02 GRAM *
  • Batch Number 1596249 Wet Weight ' 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1.96-sigma) K-40 1.326E+Ol 1.580E+OO CD-109 1.007E+OO 2.121E+OO SN-126 6.341E-02 1.336E-01 TL-208 2.398E-01 8.122E-02 BI-211 7.570E-01 8.268E-01 PB-212 7.262E-01 1.369E-01 BI-214 7.865E-01 1.428E-01 PB-214 1.049E+OO 1. 679E-01 RN-222 7.865E-01 1. 428E-01 RA-224 2 .131E-01 8.863E-01 RA-22 6 7.865E-01 l.428E-01 AC-228 6.656E-01 3. 271E-01 RA-228 6.656E-01 3. 271E-01 TH-228 7.262E-01 1.369E-01 TH-230 7.863E-01 l.428E-01 PA-231 8.623E-01 7.387E-01 TH-232 6.656E-01 3. 271E-01 U-234 7.863E-01 l.428E-01 AM-243 1.597E-01 1.128E-01 ANH-511 l.498E-01 6.346E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 Page 3771of5809 Key-Line Activity (pCi/GRAM 5.243E+OO 1.652E-02 O.OOOE+OO 4.463E-03 3.230E-03 O.OOOE+OO O.OOOE+OO 6.097E-02 -3.090E-01 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 9.283E+OO 3.994E-02 1.922E+41 l.791E-02 3.450E-01 1.799E+04 4.103E+02 5.493E-02 5.054E-01 1.666E+41 MDA (pCi/GRAM 6.697E-01 2.206E+OO 1. 451E-01 5.900E-02 2.611E-01 8.133E-02 5.130E-02 2.705E-01 5.130E-02 l.002E+OO 5 .130E-02 2.215E-01 2.215E-01 8 .133E-02 5.128E-02 7.205E-01 2.215E-01 5.128E-02 9.712E-02 4.247E-02 'MDA (pCi/GRAM 2.066E+Ol 8.728E-02 0.000E+OO 4.736E-02 7.165E-01 O.OOOE+OO O.OOOE+OO l.260E-01 8.620E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF C0-57 -7.484E-03 3.959E-02 7.670E-02 NOT IDENT. C0-58 -7.752E-02 5.647E-01 1.070E+OO NOT IDENT. FE-59 -5.222E+OO 7.033E+OO 1.183E+Ol NOT IDENT. C0-60 -8.632E-03 3.585E-02 6.948E-02 NOT IDENT. ZN-65 7.066E-02 1.719E-01 3.344E-01 NOT IDENT. GE-68 1.875E+OO 2.148E+OO 4.931E+OO NOT IDENT. AS-73 2.388E+OO 1.164E+Ol 2.484E+Ol NOT IDENT. AS-74 O.OOOE+OO 1.034E+04 O.OOOE+OO SHORT HLIF SE-75 7.491E-02 1.913E-01 3. 718E-01 NOT IDENT. BR-77 O.OOOE+OO 2. 624.E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.916E+02 O.OOOE+OO SHORT HLIF RB-83 -6.218E-02 5.262E-01 9.413E-01 NOT IDENT. KR-85 3.336E+OO 7.501E+OO 1.191E+Ol NOT IDENT. SR-85 3.821E-01 8.629E-01 1. 370E+OO NOT IDENT. RB-86 0.000E+OO 3.330E+04 O.OOOE+OO SHORT HLIF Y-88 -9.573E-02 1.845E-01 3.575E-01 NOT IDENT. Y-91 l.148E+02 5.506E+02 l.130E+03 NOT IDENT. NB-94 1.948E-02 2.932E-02 6.179E-02 NOT IDENT. NB-95 -9.620E-01 9.766E-01 1. 57 9E+OO NOT IDENT. NB-95M -1.519E+OO 2.407E+OO 3.782E+OO NOT IDENT. ZR-95 4.581E-01 1.437E+OO 2.929E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.759E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO l.106E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -l.440E-02 2.937E-02 5.499E-02 NOT IDENT. RH-102 -7.529E-03 4.589E-02 8.928E-02 NOT IDENT. RU-103 -2.584E+OO 5.040E+00 9.413E+00 FAIL ABUN RH-106 -2.712E-01 4.400E-01 7.843E-01 NOT IDENT. RU-106 -2.712E-01 4.400E-01 7.843E-01 NOT IDENT. AG-108M -1. 626E-03 l.942E-02 3.939E-02 NOT IDENT. AG-110M 3.866E-02 9.659E-02 2. 081E-01 NOT IDENT. SN-113 -7.694E-02 1.833E-01 3.543E-01 NOT IDENT. CD-115 O.OOOE+OO 2.298E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l .196E+05 O.OOOE+OO SHORT HLIF TE-123M -2.888E-02 l.149E-01 2.161E-01 NOT IDENT. SB-124 -9.616E-02 1.738E+OO 3.755E+OO NOT IDENT. SB-125 -4.279E-02 8.552E-02 1.617E-01 FAIL ABUN TE-125M -4.637E+Ol 2. 518E+02 4.920E+02 NOT IDENT. I-126 0.000E+OO 1.212E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.678E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 9 .117E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 7.179E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.688E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. 781E+27 O.OOOE+OO SHORT HLIF BA-133 -2.530E-02 3.716E-02 6.099E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.496E-02 8.228E-02 l.044E-01 FAIL ABUN CS-135 -4.172E-02 1. 274E-01 2.267E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.451E+05 O.OOOE+OO SHORT HLIF BA-137M 3.342E-02 3.149E-02 6.981E-02 NOT IDENT. CS-137 3. 531E-02 3.327E-02 7.375E-02 NOT IDENT. CE-139 3.897E-02 9. 331E-02 l.863E-01 NOT IDENT. BA-140 O.OOOE+OO 1.929E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.378E+05 O.OOOE+OO SHORT HLIF CE-141 -4.003E-02 2.481E+Ol 4.789E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.203E+41 O.OOOE+OO SHORT HLIF CE-144 4.438E-02 3.091E-01 6.095E-01 NOT IDENT. PM-144 2.998E-02 5.585E-02 1.148E-01 NOT IDENT. PR-144 2.630E+OO 4.874E+OO 1.002E+Ol NOT IDENT. PM-146 -1.209E-02 3.848E-02 7.393E-02 NOT IDENT. ND-147 O.OOOE+OO 3. 972E+07 O.OOOE+OO SHORT HLIF PM-147 1. 716E+02 6.675E+02 1. 348E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 911E+41 O.OOOE+OO SHORT HLIF EU-150 l.204E-02 2.187E-02 4.30$E-02 FAIL ABUN EU-152 -l.932E-02 7.201E-02 1. 279E-01 NOT IDENT. GD-153 -l.216E-01 l.455E-01 2.701E-01 NOT IDENT. EU-154 3.807E-02 9.700E-02 2. ll5E-01 NOT IDENT. EU-155 -6.484E-02 9.195E-02 1. 718E-01 FAIL ABUN TB-160 -8.553E-01 1. 696E+OO 3.246E+OO FAIL ABUN H0-166M -4.712E-02 5.402E-02 8.980E-02 NOT IDENT. TM-171 -2.068E+Ol 2.838E+Ol 5.554E+Ol NOT IDENT. HF-172 5.585E-02 l.978E-01 3.963E-01 NOT IDENT. LU-172 -4.625E-02 5.750E-02 l.OOlE-01 FAIL ABUN LU-176 -1.041E-03 2.284E-02 4.166E-02 FAIL ABUN HF-181 l.437E-01 3.402E+OO 7.025E+OO NOT IDENT. TA-182 -2.623E-01 1.024E+OO 1. 930E+OO FAIL ABUN Page 3772 of 5809 RE-183 2.188E+OO 3.788E+OO 8.248E+OO NOT IDENT. RE-184 -3.405E+00 2.920E+Ol 5.957E+Ol NOT IDENT. W-188 l.452E+Ol 1.003E+02 l.895E+02 NOT IDENT. IR-192 2.705E-02 3.866E-01 7.977E-01 FAIL ABUN HG-203 -5.983E-02 2.089E+OO 4.283E+OO NOT IDENT. BI-207 -l.693E-03 4.688E-02 9.373E-02 FAIL ABUN PB-210 5.454E+OO 6.175E+OO l.401E+Ol NOT IDENT. PB-211 l.141E-01 4.985E-01 1.042E+OO NOT IDENT. BI-212 8.082E-01 5.029E-01 l.140E+OO NOT IDENT. RN-219 1. l19E-01 3. ll 7E-01 6.533E-01 &AIL ABUN RA-223 2.153E-01 4.781E-01 1.014E+OO FAIL ABUN AC-227 -1. 229E-01 2.223E-01 3.497E-01 FAIL ABUN TH-227 -1. 229E-01 2.223E-01 3.497E-01 FAIL ABUN TH-229 -6.383E-02 3.761E-01 7.027E-01 FAIL ABUN TH-231 2.153E-01 4.781E-01 1.014E+OO FAIL ABUN PA-233 -2. 411E-03 4.832E-02 9.814E-02 FAIL ABUN PA-234 -1.025E-01 2.354E-01 4.520E-01 NOT IDENT. PA-234M -l.321E-01 3.478E+OO 7.102E+OO NOT IDENT. TH-234 1.396E+OO 1.253E+OO 2.786E+00 FAIL ABUN U-235 6.815E-02 1. 477E-01 2.974E-01 FAIL ABUN NP-237 -2. 411E-03 4.832E-02 9.814E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 1.396E+OO 1. 253E+OO 2.786E+OO FAIL ABUN NP-239 7 . .S75E-03 1. 966E-01 3.902E-01 NOT IDENT. PU-239 6.336E+Ol 2.626E+02 5.225E+02 NOT IDENT. AM-241 3.515E-02 1.553E-01 3.283E-01 NOT IDENT. CM-243 3.830E-02 7.988E-02 l.664E-01 NOT IDENT. BK-247 -1.032E-02 6.550E-02 1.193E-01 NOT IDENT. CM-247 -5.977E-03 2.931E-02 5.761E-02 NOT IDENT. CF-249 -1.810E-03 2.889E-02 5.831E-02 NOT IDENT. CF-251 1.837E-01 l.590E-01 1.899E-01 FAIL ABUN Page 3773 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:20:53.64 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 340 10.66* 1.030E+OO 1. 32 6E+Ol 1. 32 6E+Ol 12.16 CD-109 88.03 52 3.70* 4.450E+OO 1.348E+OO 2.141E+OO 99.62 SN-126 64.28 -------9.60 2.161E+OO ------Line Not Found ------86.94 52 8.90 4.450E+OO 5.603E-01 5.603E-01 99.62 87.57 52 37.00* 4.450E+OO 1.348E-01 l.348E-01 99.62 TL-208 277.37 ------6.60 4.074E+OO ------Line Not Found ------583.19 104 85.00* 2.178E+OO 2.398E-01 2.398E-01 34.57 860.56 28 12.50 1.591E+OO 6.033E-01 6.033E-01 59.55 BI-211 72. 87 ------1. 23 3.135E+OO ------Line Not Found ------351.06 291 12.92* 3.338E+OO 2.891E+OO 2. 891E+OO 16.33 PB-212 74.82 120 10.28 3.363E+OO 1.481E+OO l.481E+OO 49.90 77 .11 200 17.10 3.570E+OO 1.404E+OO l.404E+OO 29.48 238.63 339 43.60* 4.587E+OO 7.262E-01 7.262E-01 19.24 300.09 41 3.30 3.815E+OO 1.398E+OO 1.398E+OO 87.41 BI-214 609.32 176 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 1120.29 35 14.92 1:288E+OO 7. 831E-01 7.834E-01 38.74 1764.49 24 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 PB-214 74.82 120 5.80 3.363E+OO 2.624E+OO 2.625E+OO 49.90 77 .11 200 9.70 3.570E+00 2.476E+OO 2.477E+OO 29.48 87.09 52 3.41 4.450E+OO 1.462E+OO 1.463E+OO 99.62 242.00 69 7.25 4.539E+OO 8.949E-01 8.952E-01 49.62 295.22 129 18.42 3.870E+OO 7.744E-01 7.747E-01 32.77 351. 93 291 35.60* 3.338E+00 1.049E+OO l.049E+OO 16.33 RN-222 609.32 176 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 1120.29 35 14.92 1.288E+OO 7.831E-01 7.834E-01 38.74 1764.49 24 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 RA-224 240.99 69 4.10* 4.539E+OO 1.582E+OO 1.582E+OO 49.62 RA-226 609.32 176 45.49* 2.102E+OO 7.863E-01 7.865E-01 18.53 1120.29 35 14.92 1. 288E+OO 7.831E-01 7.834E-01 38.74 1764.49 24 15.30 8.674E-01 7.675E-01 7.678E-01 40.00 AC-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 105 11. 27 3.446E+OO l.162E+OO 1.162E+OO 42.03 794.95 17 4.25 1. 696E+OO 9.848E-01 9.848E-01 129.26 835. 71 ------1. 61 1.630E+OO ------Line Not Found ------911. 20 61 25.80*. l.520E+OO 6.656E-01 6.656E-01 50.14 968. 97 37 15.80 1.448E+OO 7.020E-01 7.020E-01 48.17 RA-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 105 11. 27 3.446E+OO 1.162E+OO 1.162E+OO 42.03 794.95 17 4.25 1. 696E+OO 9.848E-01 9.848E-01 129. 2 6 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 61 25.80* 1.520E+OO 6.656E-01 6.656E-01 50.14 968. 97 37 15.80 1. 448E+OO 7.020E-01 7.020E-01 48.17 TH-228 74.82 120 10.28 3.363E+OO 1. 481E+OO 1.481E+OO 49.90 77 .11 200 17.10 3.570E+OO 1.404E+OO 1.404E+OO 29.48 238.63 339 43.60* 4.587E+OO 7.262E-01 7.262E-01 19.24 300.09 41 3.30 3.815E+OO 1.398E+OO 1.398E+OO 87.41 TH-230 609.32 176 45.49* 2.102E+OO 7.863E-01 7.863E-01 18.53 Page 3774 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235039 Acquisition date Page : 2 3-0CT-2016 09:18:06 Nuclide Type: Nuclide PA-231 TH-232 U-234 AM-243 ANH-511 Flag: "*" Page 3775of5809 Energy 1120.29 1764.49 283.69 301.36 105.21 338.32 835. 71 911. 20 968. 97 609.32 1120.29 1764.49 43.53 74.66 511. 00 Key line Area %Abn 35 14.92 24 15.30 ------1. 70 41 5.35* ------1.10 105 11. 27 ------1. 61 61 25.80* 37 15.80 176 45.49* 35 14.92 24 15.30 ------5.90 120 67.20* 85 100.00* Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCilGRAM %Error 1. 288E+OO. 7.831E-01 7. 831E-01 38.74 8.674E-01 7.675E-01 7.675E-01 40.00 4.000E+OO ------Line Not Found ------3.815E+OO 8.623E-01 8.623E-01 87.41 5.460E+OO ------Line Not Found ------3.446E+OO 1.162E+OO 1.162E+oo 42.03 1.630E+OO ------Line Not Found ------1. 520E+OO 6.656E-01 6.656E-01 50.14 1.448E+OO 7.020E-01 7.020E-01 48.17 2.102E+OO 7.863E-01 7.863E-01 18.53 1.288E+OO 7. 831E-01 7. 831E-01 38.74 8.674E-01 7.675E-01 7.675E-01 40.00 l.573E-01 ------Line Not Found ------3.363E+OO 2.265E-01 2.265E-01 49.90 2.432E+OO l.498E-01 1.498E-01 43.22 Summary of Nuclide Activity Sample ID : G405235039 Acquisition date Page : 3 3-0CT-2016 09:18:06 Total number of lines in spectrum 39 Number of unidentified lines 13 Number of lines tentatively identified by NID 26 Nuclide Type : Nuclide K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 1. 41E+10Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 59 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity
  • Uncorrected pCi/GRAM l.326E+Ol 1.348E+OO 1.348E-01 2.398E-01 2.891E+OO 7.262E-01 7.863E-01 1. 049E+OO 7.863E-01 1.582E+OO 7.863E-01 6.656E-01 6.656E-01 7.262E-01 7.863E-01 8.623E-01 6.656E-01 7.863E-01 2.265E-01 l.498E-01 2.913E+Ol 2.913E+Ol Decay Corr pCi/GRAM 1.326E+Ol 2.141E+OO l.348E-01 2.398E-01 2. 891E+OO 7.262E-01 7.865E-01 1.049E+OO 7.865E-01 1.582E+OO 7.865E-01 6.656E-01 6.656E-01 7.262E-01 7.863E-01 8.623E-01 6.656E-01 7.863E-01 2.265E-01 1.498E-01 2.992E+Ol 2.992E+Ol 66.67% Decay Corr 2-Sigma Error 0.161E+Ol 2.132E+OO l.343E-01 0.829E-01 0.472E+OO l.397E-01 l.457E-01 0 .171E+OO 1.457E-01 0.785E+OO 1.457E-01 3.337E-01 3.337E-01 1.397E-01 1.457E-01 7.537E-01 3.337E-01 l.457E-01 l .130E-01 0.648E-01 "M" Manually accepted 2-Sigma %Error 12.16 99.62 99.62 34.57 16.33 19.24 18.53 16.33 18.53 49.62 18.53 50.14 50.14 19.24 18.53 87.41 50.14 18.53 49.90 43.22 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3776of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235039 Acquisition date : 3-0CT-2016 09:18:06 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 40.61 39 131 1. 05 81. 66 78 8 7.12E-03 **** 5.88E-02 0 92.79 80 179 0.83 186.05 183 8 l.60E-02 75.5 4.84E+OO T 0 178.00 41 72 1. 05 356.55 353 8 8.78E-03 88.3 5.53E+OO T 0 181.98 ,28 74 0.94 364.51 362 7 6.00E-030**** 5.46E+OO T 0 186.14 93 133 0.80 372.82 368 10 2.0lE-02 59.2 5.40E+OO T 0 209.28 63 114 1. 05 419.14 414 10 1.37E-02 78.3 5.03E+OO 0 259.16 39 71 1.18 518.92 514 10 8.84E-03 95.8 4.30E+OO 0 272.46 20 90 0.63 545.55 541 10 4.51E-03 **** 4.13E+OO T 0 419.10 23 28 0.99 838. 96 835 8 5.40E-03 **** 2.87E+OO 0 462.78 47 34 1. 37 926.37 919 15 1.13E-02 66.4 2.64E+OO T 0 518.48 15 20 0.76 1037.82 1033 10 3.68E-03 **** 2.40E+OO 0 596.54 7 22 0.64 1194. 03 1188 9 1.71E-03 **** 2.14E+OO T 0 728.90 18 44 1. 37 1458.93 1452 15 4.59E-03 **** 1.82E+OO 0 1011.06 11 5 1.16 2023.64 2017 9 3.06E-03 92.9 1.40E+OO 0 1031.91 8 10 0.50 2065.38 2060 10 2.22E-03 **** l.38E+OO 0 1104. 71 13 4 1. 29 2211. 07 2208 7 3.62E-03 78.6 1.30E+OO 0 1136.61 8 5 0.85 2274.93 2272 6 2.14E-03 **** l.27E+OO 0 1156.28 14 6 4.08 2314.30 2308 11 3.75E-03 86.5 1. 25E+OO 0 1318.67 9 6 1. 32 2639.37 2631 13 2.64E-03 **** 1.12E+OO 0 1360.33 7 2 0.95 2722.75 2718 8 l.94E-03 **** 1.lOE+OO Flags: "T" = Tentatively associated' Page 3777 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:21:08.10 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l * *Acquisition date 3-0CT-2016 09:18:06 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:43:00 Nuclide Library : SOLID *
  • Sample ID G405235039 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7533E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3 *' Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Le (pCi/GRAM 2.814E-01 l.042E+OO 6.871E-02 2.623E-02 1.163E-01 3.755E-02 1.931E-02 1.301E-01 1. 931E-02 4.678E-01 1.931E-02 9.554E-02 9.554E-02 3.755E-02 1.930E-02 3.299E-01 9.554E-02 1.930E-02 4.568E-02 1. 873E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 3778of5809 Le (pCi/GRAM 9.075E+OO 3.726E-02 O.OOOE+OO 1.678E-02 3.091E-01 O.OOOE+OO 0.000E+OO 5.573E-02 3. 721E-01 O.OOOE+OO 3.557E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77

  • SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB=--160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3779 of 5809 4.616E-01 4.944E+OO 2.883E-02 l.455E-01 2.161E+OO l.144E+Ol O.OOOE+OO 1. 711E-01 O.OOOE+OO O.OOOE+OO 4.034E-01 5.345E+OO 6.146E-01 O.OOOE+OO 1. 2 67E-01 4.928E+02 2.767E-02 6.929E-01 1.739E+OO l.289E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.561E-02 3.846E-02 4.088E+00 3.398E-01 3.398E-01 1. 727E-02 9.166E-02 1.573E-01 O.OOOE+OO O.OOOE+OO 1.003E-01 l.406E+OO 7.186E-02 2.286E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.732E-02 O.OOOE+OO 4.669E-02 1.041E-01 O.OOOE+OO O.OOOE+OO 3.143E-02 3.320E-02 8.666E-02 O.OOOE+OO O.OOOE+OO 2.237E+Ol O.OOOE+OO 2.844E-01 5.162E-02 4.506E+OO 3.308E-02 O.OOOE+OO 6.263E+02 O.OOOE+OO 1. 966E-02 . 5. 685E-02 l.245E-01 9.017E-02 7. 961E-02 1.380E+OO 3.890E-02 2.547E+Ol 1.851E-01 4.026E-02 l.907E-02 3.056E+OO 8. 472E-01 3.843E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 AA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3780of5809 2.553E+Ol 8.639E+Ol 3.620E-01 1.958E+OO 4.084E-02 6.516E+OO 4.664E-01 5.207E-01 2.955E-01 4.639E-01 l.598E-01 1.598E-01 3.245E-01 4.639E-01 4.473E-02 1.924E-01 3.049E+OO 1.307E+OO l.390E-01 4.473E-02 O.OOOE+OO 1.307E+OO 1.812E-01 2.443E+02 1.528E-01 7.739E-02 5.475E-02 2.595E-02 2.612E-02 8.839E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:21:14.84 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235039.CNF;l * *Acquisition date 3-0CT-2016 09:18:06 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.74 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:43:00 Nuclide Library : SOLID *
  • Sample ID G405235039 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity 1.7533E+02 GRAM *
  • Quantity Err(%) 1.1407E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * * *' Eff. Cal. date 6-SEP-2016 04: 59: 25 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1. 326E+Ol 1.724E+OO 1.724E+OO CD-109 1. 007E+OO 2.128E+OO 2.128E+OO SN-126 6. 341E-02 l.339E-01 l.339E-01 TL-208 2.398E-01 8.186E-02 8.186E-02 BI-211 7.570E-01 8.377E-01 8.377E-01 PB-212 7.262E-01 1.422E-01 l.422E-01 BI-214 7.865E-01 l.467E-01 l.467E-01 PB-214 l.049E+00 l.735E-01 1.735E-01 RN-222 7.865E-01 1.467E-01 1. 467E-01 RA-224 2 .131E-01 8.909E-01 8.909E-01 RA-22 6 7.865E-01 1.467E-01 1. 467E-01 AC-228 6.656E-01 3.288E-01 '3.288E-01 RA-228 6.656E-01 3.288E-01 3.288E-01 TH-228 7.262E-01 1.422E-01 1.422E-01 TH-230 7.863E-01 l.467E-01 1.467E-01 PA-231 8.623E-01 7.613E-01 7. 613E-01 TH-232 6.656E-01 3.288E-01 3.288E-01 U-234 7.863E-01 l.467E-01 l.467E-01 AM-243 1.597E-01 1.136E-01 l.136E-01 ANH-511 1.498E-01 6.375E-02 6.375E-02 Non-Identified Nuclides Key-Line K. L Act error* Activity TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 5.243E+OO 9.285E+OO 9.581E+OO NOT IDENT. NA-22 1.652E-02 3.994E-02 4.063E-02 NOT IDENT. NA-24 -l.000E+41 1.974E+41 O.OOOE+OO SHORT HLIF AL-26 4.463E-03 1. 7 91E-02 l.803E-02 NOT IDENT. SC-46 3.230E-03 3.450E-01 3.450E-01 FAIL ABUN V-48 -8.919E+03 1. 799E+04 1.844E+04 SHORT HLIF CR-51 1.329E+02 4.103E+02 4.147E+02 SHORT HLIF MN-54 6.097E-02 5.499E-02 6.148E-02 NOT IDENT. C0-56 -3.090E-01 5.056E-01 5.244E-01 NOT IDENT. MN-56 -1.000E+41 1. 666E+41 0.000E+OO SHORT HLIF Page 3781of5809 C0-57 -7.484E-03 3.959E-02 3.973E-02 NOT IDENT. C0-58 -7.752E-02 5.647E-01 5.658E-01 NOT IDENT. FE-59 -5.222E+OO 7.043E+OO 7.426E+00 NOT IDENT. C0-60 -8.632E-03 3.585E-02 3.606E-02 NOT IDENT. ZN-65 7.066E-02 1. 719E-01 1. 748E-01 NOT IDENT. GE-68 1.875E+OO 2.149E+OO 2.310E+OO NOT IDENT. AS-73 2.388E+OO 1.165E+Ol 1.170E+Ol NOT IDENT. AS-74 3.836E+03 1.034E+04 1.048E+04 SHORT HLIF SE-75 7.491E-02 1.913E-01 1.943E-01 NOT IDENT. BR-77 , 1.392E+39 1. 237E+40 O.OOOE+OO SHORT HLIF SR-82 5.203E+Ol 7.916E+02 7.920E+02 SHORT HLIF RB-83 -6.218E-02 5.263E-01 5.270E-01 NOT IDENT. KR-85 3.336E+OO 7.502E+OO 7.651E+OO NOT IDENT. SR-85 3. 821E-01 8.631E-01 8.801E-01 NOT IDENT. RB-86 3.786E+04 3.335E+04 3.746E+04 SHORT HLIF Y-88 -9.573E-02 1.847E-01 1. 896E-01 NOT IDENT. Y-91 1.148E+02 5.507E+02 5.531E+02 NOT IDENT. NB-94 1.948E-02 2.933E-02 3.062E-02 NOT IDENT. NB-95 -9.620E-01 9.775E-01 1. 069E+OO NOT IDENT. NB-95M -1.519E+OO 2.410E+OO 2.505E+OO NOT IDENT. ZR-95 4.581E-01 1.437E+OO 1.451E+00 NOT IDENT. NB-97 -1.000E+41 2.180E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1. 760E+41 O.OOOE+OO SHORT HLIF M0-99 -6.006E+32 1.107E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 3.595E+41 O.OOOE+OO SHORT HLIF RH-101 -l.440E-02 2.949E-02 3.020E-02 NOT IDENT. RH-102 -7.529E-03 4.590E-02 4.602E-02 NOT IDENT. RU-103 -2.584E+OO 5.042E+OO 5.174E+OO FAIL ABUN RH-106 -2. 712E-01 4.403E-01 4.570E-01 NOT IDENT. RU-106 -2.712E-01 4.403E-01 4.570E-01 NOT IDENT. AG-108M -1.626E-03 1.942E-02 1.943E-02 NOT IDENT. AG-llOM 3.866E-02 9.661E-02 9.817E-02 NOT IDENT. SN-113 -7.694E-02 1.833E-01 1.866E-01 NOT IDENT. CD-115 1.191E+40 2.308E+40 O.OOOE+OO SHORT HLIF SN-117M 7.387E+04 l.200E+05 1.245E+05 SHORT HLIF TE-123M -2.888E-02 1.149E-01 1.157E-01 NOT IDENT. SB-124 -9.616E-02 1. 738E+OO 1. 739E+OO NOT IDENT. SB-125 -4.279E-02 8.554E-02 8.768E-02 FAIL ABUN TE-125M -4.637E+Ol 2.518E+02 2.527E+02 NOT IDENT. I-126 1. 661E+05 1.212E+06 1.214E+06 SHORT HLIF SB-126 -1.473E+06 1.701E+06 1. 826E+06 SHORT HLIF SB-127 l.312E+23 2.064E+23 O.OOOE+OO SHORT HLIF I-131 -4.759E+09 7.182E+09 7.496E+09 SHORT HLIF I-132 -1.000E+41 l.906E+42 O.OOOE+OO SHORT HLIF TE-132 9.811E+26 1.828E+27 O.OOOE+OO SHORT HLIF BA-133 -2.530E-02 3.718E-02 3.889E-02 NOT IDENT. I-133 1.000E+41 9.506E+41 O.OOOE+OO SHORT HLIF CS-134 6. 496E-02 8.233E-02 8.738E-02 FAIL ABUN CS-135 -4 .172E-02 1.274E-01 1.288E-01 NOT IDENT. I-135 1.000E+41 2.240E+42 O.OOOE+OO SHORT HLIF CS-136 -6.943E+04 3.452E+05 3.466E+05 SHORT HLIF BA-137M 3.342E-02 3.153E-02 3.494E-02 NOT IDENT. CS-137 3.531E-02 3. 331E-02 3.691E-02 NOT IDENT. CE-139 3.897E-02 9.364E-02 9. 527E-02 NOT IDENT. BA-140 9.426E+05 1.930E+06 1. 976E+06 SHORT HLIF LA-140 -1.865E+04 4.378E+05 4.379E+05 SHORT HLIF CE-141 -4.003E-02 2. 481E+Ol 2.481E+Ol NOT IDENT. CE-143 1.000E+41 1.208E+41 O.OOOE+OO SHORT HLIF CE-144 4.438E-02 3.091E-01 3.097E-01 NOT IDENT. PM-144 2.998E-02 5.588E-02 5.749E-02 NOT IDENT. PR-144 2.630E+OO 4.875E+OO 5.017E+OO NOT IDENT. PM-146 -1.209E-02 3.849E-02 3.888E-02 NOT IDENT. ND-147 -1.703E+07 3.973E+07 4.046E+07 SHORT HLIF PM-147 1. 716E+02 6.675E+02 6.720E+02 NOT IDENT. PM-149 -1.000E+41 1.923E+41 O.OOOE+OO SHORT HLIF EU-150 1.204E-02 2.188E-02 2.254E-02 FAIL ABUN EU-152 -1.932E-02 7.202E-02 7.254E-02 NOT IDENT. GD-153 -1.216E-01 1.456E-01 1.556E-01 NOT IDENT. EU-154 3.807E-02 9.701E-02 9.851E-02 NOT IDENT. EU-155 -6.484E-02 9.207E-02 9.660E-02 FAIL ABUN TB-160 -8.553E-01 1. 696E+OO 1. 740E+00 FAIL ABUN H0-166M -4. 712E-02 5.408E-02 5. 811E-02 NOT IDENT. TM-171 -2.068E+Ol 2.844E+Ol 2.993E+Ol NOT IDENT. HF-172 5.585E-02 1.980E-01 1. 996E-01 NOT IDENT. LU-172 -4.625E-02 5.769E-02 6.134E-02 FAIL ABUN LU-176 -1.041E-03 2.284E-02 2.285E-02 FAIL ABUN HF-181 1.437E-01 3.402E+00 3.403E+OO NOT IDENT. TA-182 -2.623E-01 1.024E+OO 1.031E+OO FAIL ABUN Page 3782of5809 RE-183 2.188E+OO 3.804E+OO 3.930E+OO NOT IDENT. RE-184 -3.405E+OO 2.922E+Ol 2.926E+Ol NOT IDENT. W-188 1.452E+Ol 1.003E+02 1.005E+02 NOT IDENT. IR-192 2.705E-02 3.866E-01 3.868E-01 FAIL ABUN HG-203 -5.983E-02 2.089E+OO 2.089E+OO NOT IDENT. BI-207 -l.693E-03 4.688E-02 4.688E-02 FAIL ABUN PB-210 5.454E+OO 6.195E+OO 6.665E+OO NOT IDENT. PB-211 l.141E-01 4.985E-01 5.012E-01 NOT IDENT. BI-212 8.082E-01 5.046E-01 6.223E-01 NOT IDENT. RN-219 l .119E-01 3.120E-01 3 .161Kr01 FAIL ABUN RA-223 2.153E-01 4.783E-01 4.880E-01 FAIL ABUN AC-227 -1.229E-01 2.228E-01 2.296E-01 FAIL ABUN TH-227 -1.229E-01 2.228E-01 2.296E-01 FAIL ABUN TH-229 -6.383E-02 3. 7 61E-01 3.772E-01 FAIL ABUN TH-231 2.153E-01 4.783E-01 4.880E-01 FAIL ABUN PA-233 -2. 411E-03 4.832E-02 4.833E-02 FAIL ABUN PA-234 -l.025E-01 2.630E-01 2.671E-01 NOT IDENT. PA-234M -l.321E-01 3.478E+00 3.479E+00 NOT IDENT. TH-234 l.396E+OO 1.291E+OO 1.436E+OO FAIL ABUN 6.815E-02 l.478E-01 1.509E-01 FAIL ABUN NP-237 -2. 411E-03 4.832E-02 4.833E-02 FAIL ABUN NP-238 l.000E+41 6.595E+41 O.OOOE+OO SHORT HLIF U-238 1.396E+OO 1.291E+OO l.436E+00 FAIL ABUN NP-239 7.875E-03 1. 966E-01 1. 966E-01 NOT IDENT. PU-239 6.336E+Ol 2.626E+02 2.642E+02 NOT IDENT. AM-241 3.515E-02 l.553E-01 1.561E-01 NOT IDENT. CM-243 3.830E-02 7. 996E-02 8.180E-02 NOT IDENT. BK-247 -1.032E-02 6.553E-02 6.570E-02 NOT IDENT. CM-247 -5.977E-03 2.932E-02 2.945E-02 NOT IDENT. CF-249 -l.810E-03 2.889E-02 2.890E-02 NOT IDENT. CF-251 1.837E-01 l.604E-01 1.805E-01 FAIL ABUN Page 3783of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 48.2185 87.09 90.6453 136.47 65.5134 45.60 55.0496 87.57 105.2002 140.51 0.0000 46.54 42.7447 88.03 97.4013 143.76 57.5377 49.72 0.0000 88.34 97.4630 144.24 57.5781 51. 35 45.1748 88.47 97.4886 145.44 67.4719 51. 87 47.0528 89. 96 49.5518 152.43 56.0528 52.39 51.6545 1093.63 82.0372 153.25 0.0000 52.97 44.4788 91.11 0.0000 323.87 59.4959 53.44 39.0847 92.59 63.7588 156.02 0.0000 54.07 45.5284 93.35 63.8540 158.56 0.0000 57.36 0.0000 94.56 54.6708 159.00 60.9955 57.53 56.9976 94.65 54.6804 162.33 50.1286 57.98 50.6236 94.67 54.6825 162.66 0.0000 59.27 59 .1111 94.87 54.7038 163.33 68.0423 59.32 59.1189 97.43 64.3589 165.86 50.3627 59.54 56.3805 98.43 62.4659 176.31 34.7836 60. 96 63.0852 '98. 44 62. 4671 176.60 0.0000 61.17 67.7608 99.53 58.5571 177.52 31.8072 62.93 53.1497 100 .11 64.6846 181.07 0.0000 63.29 46.6652 102.03 68.9727 181.52 36.5313 63.58 57.9075 103.18 49.8056 184.41 36.6602 64.28 71.1091 103.37 49.8232 143.76 35.1888 66.73 57.4230 105.21 69.3738 193.51 52 .1157 67.24 65.0349 105.31 69.3862 197.03 55.8186 125.81 66.9921 106.12 60.2905 198.01 48.8964 67.75 67.0029 106.47 60.3283 201.83 52.6190 69.67 70.1581 109.28 61. 6571 203.43 55. 0573 70.83 72.2525 111. 00 59.7815 205.31 48.5214 72. 81 68.7673 111. 76 0.0000 210.85 47.2461 72. 87 68.7772 114. 06 76.6755 215.65 51. 0566 74.66 83.4476 116. 30 0.0000 222 .11 51. 4109 74.82 83.4781 116.74 56.2070 227.09 45.6712 74.97 83.5066 119. 76 62.7667 227.38 37.2694 77 .11 83.9095 121.12 52.4223 228.16 0.0000 78.74 74.8559 121.22 52. 4311 228.18 43.3169 79.69 67.2518 121. 78 59.8258 116.74 43.3169 80.12 62.1367 122.06 58.8032 235.69 58.2026 80.19 0.0000 122.92 62.0398 235. 96 58.2180 80.57 67.3804 123.07 62.0551 238.63 48.6462 81. 00 69.0646 265.00 63.1691 238.98 0.0000 81. 07 72. 9664 125.81 61. 2723 240.99 65.8273 81.75 76.9700 127.23 73.0567 242.00 35.7943 83.79 84.8067 127.91 69.9558 244.70 19.5764 84.00 82.2338 129.30 63.7344 252.40 0.0000 85.43 85.0983 131.20 64.9893 252.80 35.7632 86.55 90.5450 133.02 64.1025 254.15 0.0000 86.79 90.5892 133.52 62.0135 256.23 49.4910 86.94 90.6180 136.00 57.9543 260.90 0.0000 Page 3784of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 37.4139 355.39 0.0000 584.27 21. 6375 264.80 44.9033 356.01 36.3224 595.83 0.0000 265.00 44. 9110 364.49 0.0000 427.87 16.2049 268.22 48.7988 366.42 0.0000 602.52 0.0000 269.46 50.1074 372.51 28.1398 604. 72 17.1747 270.03 45 .1198 .375.o5. 30.9197 607.14 10.9422 271.23 43.4973 377.52 29.1517 609.32 3.1298 273.65 0.0000 356.01 24.7072 610.33 3.1312 276.40 31.5155 388.16 25.6997 614.28 14.1180 277.37 39.3656 388.63 0.0000 618.01 18.8577 277.60 39.3732 391.69 26.6825 620. 36 17.8301 278.00 37.0310 264.66 24.0698 621.93 19.9432 279.20 38.7563 401.81 25.0148 630.19 0.0000 279.54 42.9814 402.40 30.5864 631. 29 14.7611 279.70 40.4590 404.85 21. 3529 633.25 16.8854 280.46 37.9559 410.95 28.8979 634.78 0.0000 283.69 36.3731 413.71 28.0170 635.95 17.9636 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 33.8867 423.72 0.0000 645.85 15.9241 285.90 0.0000 427.09 8.4791 657.76 17.0794 287.50 27.1595 427.87 28.2776 657.90 0.0000 290.67 33.1919 433.94 17.9791 661. 66 13.9019 293.27 0.0000 439.40 14.2432 664.57 0.0000 351. 93 39.3029 453.88 28.7451 666.33 0.0000 295. 96 39.3282 463.37 16.3837 666.50 0.0000 879.38 39.4161 468.07 14.4974 667. 71 0.0000 299.98 39. 4629 473.00 0.0000 677. 62 8. 6172 300.09 39.4667 475.06 21. 3519 685.70 0.0000 300 .13 39. 4676 476.78 18.4592 695.00 0.0000 301.36 39.5088 477.60 11. 6641 696. 49 19.5513 302.85 39.5584 482.18 14.6198 696. 51 19.5520 256.23 37.4607 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.6452 306.78 40.1208 497.08 20.6454 697.49 28.2534 308.46 38.8806 505.52 20.7449 702.65 16.3367 311.90 36.3920 507.63 0.0000 706.68 17.4564 316.51 31. 3110 511. 00 18.8276 711. 68 25.1478 319.41 0.0000 514.00 17.8667 720. 70 0.0000 320.08 0 .. 0000 514.00 17.8667 721. 93 0.0000 321.04 38.4087 520.40 13.4478 722. 78 13.1836 323.87 31. 4971 520.69 0.0000 722. 91 11. 5361 325.23 42.9179 522.65 0.0000 723. 31 11. 5382 328.76 0.0000 527.90 0.0000 724 .19 14.8403 333.37 25.3875 528.26 7.0031 727. 33 14.3097 333.97 27.7804 529.59 12.0142 733.00 9.9305 334.37 33.0826 529.87 0.0000 735.93 8.8379 338.28 26.5466 531.02 0.0000 333.97 11. 0547 338.32 26.5472 537.26 0.0000 739.50 0.0000 311. 90 26.5918 546.56 0.0000 747.24 21.0897 340.48 26.5918 552.55 20.2718 748.06 16.6553 340.55 0.0000 563.25 28.5400 752.31 13.3477 344.28 25.3358 569.33 20.4500 753.82 0.0000 345.93 18.6920 946.00 20.4517 756.73 14.4864 351.06 22.3389 569.70 20.4541 756.80 14.4869 351. 93 22.3531 583.19 21. 6255 884.68 15.6469 Page 3785of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 31. 3177 1274.44 10.0352 1620.50 4.3054 766.42 24.6121 1001.03 12.7922 1621. 92 2.1534 766.84 24.6166 1002.74 7.3137 1678.03 0.0000 772.60 0.0000 1004.73 16.1009 1690.97 3.2781 776.52 0.0000 507.63 0.0000 1750.46 0.0000 .. 739.50 0.0000 1025.87 0.0000 1764.49 1. 77 50 778.90 15.7415 1028.54 0.0000 1063.66 0.0000 783.70 0.0000 1037.84 14.7939 1771.35 2.2219 785.37 18.0371 1038.76 0.0000 1791.20 0.0000 15.8246 631.29 8.3441 1808.65 1.1193 794.95 20.3687 1048.07 0.0000 1810.72 0.0000 795.86 16.9800 1049.04 6.4950 1836.06 4.5012 810.06 15.9363 1050.41 8.3546 810.29 15.9380 1063.66 15.8462 344.28 14.8001 1077.00 0.0000 810.76 14.8022 1077.34 8.4243 815.77 0.0000 1085.87 10.3232 1048.07 0.0000 1093.63 12.2296 832.01 19.5151 1099.45 16.1551 834.85 .8.0442 1112. 07 17.0277 835.71 16.0941 1112.84 14.1925 836.80 0.0000 1115. 54 10.6060 846.75 0.0000 1120.29 12.3279 846.77 20.7788 1120. 55 10.6217 856.80 0.0000 1221. 41 7.5884 860.56 11.6032 1129. 67 12.3621 871.09 12.8127 1131. 51 0.0000 873.19 16.3197 1147.95 0.0000 875.33 0.0000 1173.23 9.6307 879.38 15.7725 1177.95 11. 5723 880.51 14.9025 1189.05 8.7067 883.24 17.5494 1204.77 13.6035 884.68 14.0469 1221.41 20.5001 889.28 13.1909 1231. 02 18. 5964 894.76 8. 8113 1235.36 0.0000 898.04 11. 4678 1238.28 18.6335 900.72 13.2449 1260.41 0.0000 903.28 13.2568 1271.87 8. 9072 911.20 13.2944 1274.44 7.9229 912.08 13.2985 1274.54 7.9229 923.98 0.0000 1291.59 10.9436 926.50 8.9105 1298.22 0.0000 929 .11 10.7021 1312 .11 0.0000 937.49 9.8388 1332.49 10.0555 944 .13 0.0000 1362.66 0.0000 946.00 15.2501 1365.19 1.3519 949.00 11. 6737 1368.63 0.0000 667. 71 0.0000 1384.29 4.0752 962.31 18.9428 1408.01 8.1982 964. 08 14.4414 1457.56 0.0000 966 .17 18.7872 1460.82 9.3417 911. 20 18.9857 1489.16 4.1797 968.97 18.9857 1505.03 6. 2926 983.53 0.0000 1584.12 4.2712 984.45 0.0000 1596.21 0.0000 Page 3786of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:21:50.63 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM12.CNF;467 Background date : Z-OCT-2016 11:00:40. Sample date 30-NOV-2015 13:23:00 Acquisition date : 3-0CT-2016 09:20:08. Sample ID G405235040 Sample quantity 1.72014E+02 GRAM Detector name : GAM12 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 4 4 0 2 2 0 0 0 0 0 2 2 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 5 5 0 Page 3787of5809 Energy 36.14* 37.58* 59. 26 74.85 77.41* 86.98 93.16* 116. 83 154.17 185.69* 238.54* 241.43 270.09 295.02 299.82 310.07 328.27 338.20* 351.83* 433.68 463.28 510.64* 568.90 583.04* 609.35* 662.07 696.57 711. 78 727.75 786.26 809.27 839.82 842.93 860.90 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 36 14 30 94 132 39 65 22 12 95 360 98 53 119 29 16 22 72 184 14 33 16 45 97 155 51 8 22 21 17 11 10 23 23 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 28 34 88 171 142 148 128 72 103 84 85 68 66 53 57 61 57 66 49 42 49 74 48 32 52 30 33 8 36 18 4 4 7 19 1. 76 1. 21 1. 29 1. 54 1. 29 1. 46 1. 65 0.49 1.17 1. 20 1. 46 1. 75 1. 26 1. 69 2.18 1. 78 1. 37 1.19 1. 27 0.71 1. 84 1. 60 1. 95 1. 52 1. 51 2.69 4.22 0.53 0. 71 2.75 1. 67 1. 36 2.76 2.12 72 .12 75.00 118. 36 149.53 154.66 173.78 186.14 233.50 308.17 371.22 476.93 482.70 540.03 589.89 599.50 620.00 656.40 67 6. 27 703.52 867.27 92 6. 4 7 1021.23 1137. 78 1166. 07 1218.71 1324.19 1393.23 1423.66 1455.61 1572. 70 1618.73 1679.87 1686.08 1722.04 68 68 116 144 144 171 182 230 305 367 470 470 535 585 585 612 649 670 698 859 919 1017 1131 1159 1210 1317 1382 1420 1449 1564 1615 1678 1678 1718 16 1.00E-02 43.6 3.61E+OO 16 3.75E-03109.4 7 8.19E-03 55.7 16 2.62E-02 27.3 5.56E-01 16 3.66E-02 18.5 7 1.07E-02 54.6 9 1.80E-02 37.2 6 6.07E-03 65.4 7 3.27E-03146.6 10 2.65E-02 21.6 22 1.00E-01 7.1 2.19E+OO 22 2.72E-02 25.9 10 1.47E-02 32.2 21 3.32E-02 14.6 2.17E+OO 21 8.17E-03 60.5 11 4.53E-03 95.6 9 6.12E-03 57.5 11 2.0lE-02 25.2 11 5.12E-02 10.6 12 3.97E-03 94.3 13 9.25E-03 46.6 14 4.51E-03126.1 16 1.25E-02 37.5 14 2.69E-02 16.2 15 4. 32E-02 13. 1 12 1. 41E-02 25. 8 15 2.34E-03153.4 10 6. 07E-03 31. 9 11 5.96E-03 58.1 12 4.82E-03 54.4 7 2.92E-03 42.7 14 2.70E-03 38.5 5.98E-01 14 6.43E-03 32.8 9 6.49E-03 38.8 Peak Search Report (continued) Page : 2 Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911.13* 78 7 2.06 1822.57 1817 13 2.15E-02 13.7 36 0 918.40 6 4 0.49 1837.13 1833 6 1.54E-03 73.7 37 0 934 .. 87 23 8 2.45 1870.07 1864 12 6.45E-03.32.8 38 0 954.97 9 6 1. 47 1910.29 1903 11 2.36E-03 63.5 39 0 969. 92 36 33 1. 09 1940.23 1931 12 1. OlE-02 35.5 40 0 1099.51 7 20 4.47 2199.60 2189 12 1.94E-03142.l 41 0 1120.28 42 21 1. 75 2241.15 2234 14 1.17E-02 27. 8 42 0 1185.40 12 6 2.75 2371. 50 2365 12 3.33E-03 50.0 43 0 1238.67 26 6 0.74 2478.13 2474 10 7.35E-03 26.9 44 0 1242.98 7 2 0.62 2486.77 2484 6 2.04E-03 45.7 45 0 1255.12 11 24 3.73 2511. 07 2499 18 3.08E-03112.8 46 0 1321.66 10 2 2 .11 2644.27 2638 10 2.78E-03 42.7 47 0 1325.88 7 0 0.58 2652.71 2650 6 1.94E-03 37.8 48 0 1337 .19 8 2 0.69 2675. 36 2672 6 2.08E-03 44.7 49 0 1340.06 6 3 0.52 2681.10 2678 6 1.60E-03 63.6 50 0 1460.76 350 0 2.12 2922.75 2916 14 9.72E-02 5.3 51 0 1589.14 10 3 3.47 3179.79 3173 13 2.67E-03 50.5 52 0 1764.76 16 9 4.12 3531. 46 3525 12 4.49E-03 44.6 Flag: "*" = Peak area was modified by bac,kground subtraction Page 3788 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:21:52 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 13:23:00 G405235040 Acquisition date : Sample quantity Sample eeometry : 3-0CT-2016 09:20:08 172.01 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : SOLID GAMMA12 0 01:00:00.00 1.50 keV Errors propagated: No Efficiency type : -Linear Abundance limit 75.00 Interference Report Interfering Nuclide Page 3789of5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40

  • 1460.82 10.66* 1.082E+OO 1. 295E+Ol 1 l.295E+Ol 10.69 OK C0-58 810.76 99.45* 1.744E+OO 2.810E-02 5.708E-01 85.45 OK CD-109 88.03 3.70* 4.287E+OO 6.705E-01 l.065E+OO 242.14 OK SN-126 64.28 9.60 2.033E+OO Line Not Found Absent 86.94 8.90 4.287E+OO 2.788E-01 2.788E-01 242.14 OK 87.57 37.00* 4.287E+OO 6.705E-02 6.705E-02 242.14 OK BA-137M 661.66 89.90* 2.040E+OO 1.320E-01 1.345E-01 51. 51 OK CS-137 661.66 85.10* 2.040E+OO l.394E-01 1.421E-01 51. 51 OK PR-144 696. 51 1.34* 1. 960E+OO 1.521E+OO 3.217E+00 306.78 OK 1489.16 0.28 1.064E+OO Line Not Found Absent TL-208 277.37 6.60 4.142E+OO Line Not Found Absent 583.19 85.00* 2.256E+00 2.451E-01 2. 451E-01 32.38 OK 860.56 12.50 1.662E+OO 5.180E-01 5.180E-01 77.70 OK BI-212 727.33 6.67* 1.894E+OO 7.986E-01 7.986E-01 116.26 OK 785.37 1.10 1. 783E+OO 4 .118E+OO 4 .118E+OO 108. 7*9 OK 1620.50 1. 47 9.870E-01 Line Not Found Absent PB-212 74.82 10.28 3.170E+OO l.286E+OO 1.286E+OO 76.32 OK 77 .11 17.10 3.429E+00 1.374E+OO 1.374E+OO 37.08 OK 238.63 43.60* 4.647E+OO 9. 611E-01 9.611E-01 14.14 OK 300.09 3.30 3.891E+OO 1.207E+OO 1.207E+OO 121. 08 OK BI-214 609.32 45.49* 2.179E+OO 7.560E-01 7.563E-01 26.14 OK 1120.29 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 OK 1764.49 15.30 9.120E-01 4. 811E-01 4.813E-01 89.14 OK PB-214 74.82 5.80 3.167E+OO Line Not Found <<INT Reject 77 .11 9.70 3.429E+00 2.422E+OO 2.423E+OO 37.08 OK 87.09 3.41 4.296E+OO Line Not Found <<INT Reject 242.00 7.25 4.599E+OO Line Not Found <<INT Reject 295.22 18.42 3.942E+00 8.680E-01 8.683E-01 29.19 OK 351. 93 35.60* 3.411E+OO 7.832E-01 7.835E-01 21. 24 OK RN-222 609.32 45.49* 2.179E+OO 7.560E-01 7.563E-01 26.14 OK 1120.29 14.92 l.350E+OO 9.249E-01 9.253E-01 55.63 OK 1764.49 15.30 9.120E-01 4. 811E-01 4.813E-01 89.14 OK RA-224 240.99 4.10* 4.607E+OO l.262E+00 1.262E+OO 120.32 OK RA-226 609.32 45.49* 2.179E+OO 7.560E-01 7.563E-01 26 .14 OK 1120.29 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 OK 1764.49 15.30 9.120E-01 4. 811E-01 4. 813E-01 89.14 OK AC-228 105.21 1.10 5.379E+OO Line Not Found Absent 338.32 11. 27 3.525E+OO 9.430E-01 9.430E-01 50.35 OK 794.95 4.25 1.768E+OO Line Not Found Absent 835. 71 1. 61 1. 701E+OO Line Not Found Absent 911.20 25.80* 1.590E+OO 8.631E-01 8. 631E-01 27.35 OK 968. 97 15.80 1.513E+OO 6.904E-01 6.904E-01 71. 06 OK RA-228 105.21 1.10 5.379E+OO Line Not Found Absent 338.32 11. 27 3.525E+OO 9.430E-01 9.430E-01 50.35 OK 794.95 4.25 1. 768E+OO Line Not Found Absent 835.71 1. 61 1. 701E+OO Line Not Found Absent 911.20 25.80* 1.590E+OO 8.631E-01 8. 631E-01 27.35 OK 968. 97 15.80 l.513E+00 6.904E-01 6.904E-01 71. 06 OK TH-228 74.82 10.28 3.170E+OO 1.286E+OO 1.286E+OO 76.32 OK Page 3790 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235040 Acquisition date 3-0CT-2016 09:20:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status .77 .11 17.10 3.449E+OO 1.374E+OO 1.374E+OO 37.08 238.63 43.60* 4.647E+OO 9. 611E-.01 9.611E-01 14.14 OK 300.09 3.30 3.891E+OO l.207E+OO 1.207E+OO 121. 08 OK TH-230 609.32 45.49* 2.179E+OO 7.560E-01 7.560E-01 26.14 OK 1120.29 14.92 1.350E+OO 9.249E-01 9.250E-01 55.63 OK 1764.49 15.30 9.120E-01 4. 811E-01 4.811E-01 89.14 OK TH-232 105.21 1.10 5.379E+OO Line Not Found Absent 338.32 11. 27 3.525E+OO 9.430E-01 9.430E-01 50.35 OK 835.71 1. 61 l.701E+OO Line Not Found Absent 911.20 25.80* 1. 590E+OO 8.631E-01 8.631E-01 27.35 OK 968.97 15.80 1.513E+OO 6.904E-01 6.904E-01 71. 06 OK U-234
  • 609.32 45.49* 2.179E+OO 7.560E-01 7.560E-01 26.14 OK 1120.29 14.92 1.350E+OO 9.249E-01 9.250E-01 55.63 OK 1764.49 15.30 9.120E-01 4.811E-01 4. 811E-01 89.14 OK AM-241 59.54 35.90* 1.495E+OO 3.456E-01 3.461E-01 111. 43 OK AM-243 43.53 5.90 2.347E-01 Line Not Found Absent 74.66 67.20* 3.170E+OO 1. 968E-01 1. 968E-01 76.32 OK ANH-511 511. 00 100.00* 2.510E+OO 3.192E-02 3.192E-02 252.30 OK Flag: "*" = Keyline Page 3791of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:21:54.56 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l * *Acquisition date 3-0CT-2016 09:20:08 Sensitivity : 3.000 *
  • Detector ID GAM12 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:23:00 Analyst initials: MXRl * *Sample ID G405235040 Sample Quantity l.7201E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;13
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM K-40 1. 2 95E+Ol 1.356E+OO 4.622E-01 C0-58 5.708E-01 4.780E-01 1. 071E+OO CD-109 1.065E+OO 2.527E+OO 2.870E+OO SN-126 6.705E-02 1. 591E-01 1.822E-01 BA-137M 1.345E-01 6.791E-02 5.994E-02 CS-137 l.421E-01 7.174E-02 6.332E-02 PR-144 3.217E+00 9.670E+OO 6.447E+00 TL-208 2.451E-01 7.777E-02 5.007E-02 BI-212 7.986E-01 9.099E-01 8.785E-01 PB-212 9. 611E-01 1.332E-01 8.824E-02 BI-214 7.563E-01 1.938E-01 l.300E-01 PB-214 7.835E-01 l.631E-01 l.070E-01 RN-222 7.563E-01 1.938E-01 1.300E-01 RA-224 1.262E+OO 1.488E+OO 9.454E-01 RA-226 7.563E-01 1.938E-01 1.300E-01 AC-228 8.631E-01 2.313E-01 2.020E-01 RA-228 8.631E-01 2.313E-01 2.020E-01 TH-228 9. 611E-01 1.332E-01 8.824E-02 TH-230 7.560E-01 1.937E-01 l.300E-01 TH-232 8.631E-01 2.313E-01 2.020E-01 U-234 7.560E-01 1.937E-01 l.300E-01 AM-241 3.461E-01 3.779E-01 3.665E-01 AM-243 1. 968E-01 l.472E-01 1.090E-01 ANH-511 3.192E-02 7.892E-02 4.917E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -5.510E+OO 1.165E+Ol 2.120E+Ol NOT IDENT. NA-22 -2.605E-02 3.679E-02 6.434E-02 NOT IDENT. NA-24 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF AL-26 3.655E-03 2.971E-02 6.474E-02 NOT IDENT. SC-46 -l.997E-01 3.379E-01 6.293E-01 FAIL ABUN V-48 O.OOOE+OO 1. 728E+04 O.OOOE+OO SHORT HLIF Page 3792 of 5809 CR-51 O.OOOE+OO 4.942E+02 O.OOOE+OO SHORT HLIF MN-54 1.118E-02 5.682E-02 1. 18 6E-01 NOT IDENT. C0-56 1.057E-01 3.900E-01 7.747E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.864E-02 4.421E-02 9.225E-02 NOT IDENT. FE-59 4.862E+OO 1.355E+Ol 1.477E+Ol FAIL ABUN C0-60 -8.745E-03 3.492E-02 5.893E-02 NOT IDENT. ZN-65 2.053E-02 1.586E-01 2.936E-01 NOT IDENT. GE-68 2.099E-01 2.160E+OO 4.428E+OO NOT IDENT. AS-73 -rl.083E+Ol 1.604E+Ol 2.876E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.006E+03 O.OOOE+OO SHORT HLIF SE-75 -1.393E-02 1.958E-01 3.654E-01 NOT IDENT. BR-77 O.OOOE+OO 2.472E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 8.126E+02 O.OOOE+OO SHORT HLIF RB-83 2.144E-02 6.767E-01 l.306E+OO NOT IDENT. KR-85 1.675E+OO 7.881E+OO l.376E+Ol NOT IDENT. SR-85 1.917E-01 9.057E-01 1.582E+OO NOT IDENT. RB-86 O.OOOE+OO 3.628E+04 O.OOOE+OO SHORT HLIF Y-88 1.230E-01 2.291E-01 5.435E-01 NOT IDENT. Y-91 2.977E+02 5.810E+02 1.223E+03 NOT IDENT. NB-94 8.461E-03 2.810E-02 5.607E-02 NOT IDENT. NB-95 -8.984E-02 8.139E-01 l.628E+OO NOT IDENT. NB-95M 2.774E+OO 2.690E+OO 5.176E+OO NOT IDENT. ZR-95 7.492E-02 1.627E+OO 3.085E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 1.047E+41 O.OOOE+OO SHORT HLIF M0-99 0.000E+OO 1.208E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.'960E+41 O.OOOE+OO SHORT HLIF RH-101 2.038E-02 3.455E-02 7.177E-02 NOT IDENT. RH-102 9.662E-03 5. 963E-02 1.160E-01 FAIL ABUN RU-103 6.176E+OO 5.541E+OO 1. 240E+Ol FAIL ABUN RH-106 2.252E-02 4.572E-01 8.870E-01 NOT IDENT. RU-106 2.252E-02 4.572E-01 8.870E-01 NOT IDENT. AG-108M 2.777E-02 5.133E-02 4.782E-02 FAIL ABUN AG-llOM 4.762E-02 8. 962E-02 1. 969E-01 NOT IDENT. SN-113 9.502E-02 2.388E-01 4.793E-01 NOT IDENT. CD-115 O.OOOE+OO 3.192E+40 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.465E+05 O.OOOE+OO SHORT HLIF TE-123M -5.088E-02 l.299E-01 2.518E-01 NOT IDENT. SB-124 -7.465E-01 1.909E+OO 3.633E+OO NOT IDENT. SB-125 -1.222E-01 1.133E-01 1.596E-01 FAIL ABUN TE-125M 2.179E+02 2.902E+02 6.187E+02 NOT IDENT. I-126 O.OOOE+OO 1.308E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.839E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7. 591E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 9.512E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.949E+27 O.OOOE+OO SHORT HLIF BA-133 2.374E-03 3. 724E-02 6.607E-02 NOT IDENT. I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 5. OOlE-02 4.828E-02 l.085E-01 FAIL ABUN CS-135 1.438E-01 1.335E-01 2.646E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.275E+05 O.OOOE+OO SHORT HLIF CE-139 4.305E-02 9.510E-02 l.973E-01 NOT IDENT. BA-140 O.OOOE+OO l.594E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.716E+05 O.OOOE+OO SHORT HLIF CE-141 -1.054E+Ol 2.674E+Ol 5.208E+Ol NOT IDENT. CE-143 O.OOOE+OO 7.831E+40 O.OOOE+OO SHORT HLIF CE-144 -1.168E-01 3.322E-01 6.532E-01 NOT IDENT. PM-144 3.688E-02 1.109E-01 9.315E-02 FAIL ABUN PM-146 4.302E-03 4 .119E-02 8.055E-02 NOT IDENT. ND-147 O.OOOE+OO 4.816E+07 O.OOOE+OO SHORT HLIF PM-147 8.258E+02 7.543E+02 1. 643E+03 NOT IDENT. PM-149 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF EU-150 1.016E-02 2.381E-02 4.419E-02 FAIL ABUN EU-152 -2.983E-02 8.740E-02 1.638E-01 FAIL ABUN GD-153 2.578E-02 l.825E-01 3.424E-01 NOT IDENT. EU-154 -5. 921E-02 9.084E-02 1. 613E-01 NOT IDENT. EU-155 l .112E-02 l.031E-01 2 .119E-01 FAIL ABUN TB-160 1.228E+OO 1.583E+OO 3.665E+OO FAIL ABUN H0-166M 9.904E-02 6.199E-02 l .134E-01 FAIL ABUN TM-171 -3.224E+OO 3.515E+Ol 6.700E+Ol NOT IDENT. HF-172 7.206E-02 2.255E-01 4.634E-01 NOT IDENT. LU-172 -3.215E-03 1.013E-01 1.734E-01 FAIL ABUN LU-176 -6.254E-03 2.198E-02 3.717E-02 FAIL ABUN HF-181 2.035E+OO 4. 611E+OO 9.390E+OO NOT IDENT. TA-182 -4.575E-01 7.802E-01 1.409E+OO FAIL ABUN Page 3793of5809 RE-183 7.625E+OO 8.327E+OO 9.525E+OO FAIL ABUN RE-184 5.040E+OO 3.152E+Ol 6.557E+Ol NOT IDENT. W-188 1.599E+Ol 1.208E+02 2.149E+02 NOT IDENT. IR-192 2.863E-02 4.810E-01 9.154E-01 FAIL ABUN HG-203 1.581E+OO 2.532E+OO 5.203E+OO NOT IDENT. BI-207 1.lOBE-02 3.946E-02 8.433E-02 FAIL ABUN PB-210 4.707E+OO 6.881E+OO 1.394E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.493E-01 7.265E-01 FAIL ABUN PB-21-1 3.784E-01 6.576E-01 1.340E+OO NOT IDENT. RN-219 17 8E-02 3.760E-01 7.153E-01 0 FAIL ABUN RA-223 -l.179E-01 5.697E-01 9. 681E-01 FAIL ABUN AC-227 8.106E-02 2.059E-01 4.180E-01 FAIL ABUN TH-227 8.106E-02 2.059E-01 4.180E-01 FAIL ABUN TH-229 3.593E-01 4.398E-01 9.166E-01 FAIL ABUN PA-231 4.441E-01 4.183E-01 8.293E-01 NOT IDENT. TH-231 -1.179E-01 5.697E-01 9.681E-01 FAIL ABUN PA-233 4.532E-03 5. 972E-02 1.055E-01 FAIL ABUN PA-234 7.769E-02 2.107E-01 4.636E-01 FAIL ABUN PA-234M -9.195E-01 4.037E+OO 7.943E+OO NOT IDENT. TH-234 l.104E+OO 1.816E+OO 3.602E+OO FAIL ABUN U-235 -6.166E-02 l.672E-01 3.288E-01 FAIL ABUN NP-237 4.532E-03 5. 972E-02 1.0SSE-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 1.104E+OO 1.816E+OO 3.602E+OO FAIL ABUN NP-239 2.808E-01 3.602E-01 4.731E-01 FAIL ABUN PU-239 1.204E+Ol 3.104E+02 6.240E+02 NOT IDENT. CM-243 -3.044E-02 9.247E-02 l.849E-01 NOT IDENT. BK-247 l.772E-02 6.728E-02 1.231E-01 NOT IDENT. CM-247 -5.995E-03 3.520E-02 6.644E-02 NOT IDENT. CF-249 9.005E-04 3.234E-02 6. 331E-02 NOT IDENT. CF-251 -l.447E-02 9. 716E-02 1.917E-01 NOT IDENT. Page 3794 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:21:51.43 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 342 10.66* l.082E+OO 1.295E+Ol 1. 295E+Ol 10.69 C0-58 810.76 11 99.45* 1. 744E+OO 2.810E-02 5.708E-01 85.45 CD-109 88.03 53 3.70* 4.287E+OO 1.470E+OO 2.335E+OO 109.26 SN-126 64.28 ------9.60 2.033E+OO ------Line Not Found ------86.94 53 8.90 4.287E+OO 6.113E-01 6 .113E-01 109.26 87.57 53 37.00* 4.287E+OO 1.470E-01 1. 470E-01 109.26 BA-137M 661.66 55 89.90* 2.040E+OO l.320E-01 1.345E-01 51. 51 CS-137 661. 66 55 85.10* 2.040E+OO 1.394E-01 l.421E-01 51. 51 PR-144 696. 51 9 1.34* 1.960E+OO 1.521E+OO 3.217E+OO 306.78 1489.16 ------0.28 l.064E+OO ------Line Not Found ------TL-208 277.37 ------6.60 4.142E+OO ------Line Not Found ------583.19 108 85.00* 2.256E+OO 2. 451E-01 2.451E-01 32.38 860.56 25 12.50 1.662E+OO 5.180E-01 5.180E-01 77.70 BI-211 72.87 ------1. 23 2. 964E+OO ------Line Not Found ------351.06 218 12.92* 3. 411E+OO 2.158E+OO 2.158E+OO 21. 24 BI-212 727.33 23 6.67* 1. 894E+OO 7.986E-01 7.986E-01 116.26 785.37 19 1.10 1. 783E+OO 4 .118E+OO 4 .118E+OO 108.79 1620.50 ------1. 47 9.870E-01 ------Line Not Found ------PB-212 74.82 133 10.28 3.170E+OO 1. 776E+OO 1.776E+OO 54.69 77 .11 185 17.10 3.429E+OO 1. 374E+OO 1.374E+OO 37.08 238.63 446 43.60* 4.647E+OO 9. 611E-01 9. 611E-01 14.14 300.09 35 3.30 3. 891E+OO 1.207E+OO 1.207E+OO 121.08 BI-214 609.32 172 45.49* 2.179E+OO 7.560E-01 7.563E-01 26 .14 1120.29 43 14.92 l.350E+OO 9.249E-01 9.253E-01 55.63 1764.49 15 15.30 9.120E-01 4.811E-01 4.813E-01 89.14 PB-214 74.82 133 5.80 3.170E+OO 3.148E+OO 3.149E+OO 54.69 77 .11 185 9.70 3.429E+OO 2.422E+OO 2.423E+OO 37.08 87.09 53 3.41 4.287E+OO l.596E+OO 1.596E+OO 109.26 242.00 121 7.25 4.607E+00 1.582E+OO 1.582E+OO 51. 87 295.22 144 18.42 3.942E+OO 8.680E-01 8.683E-01 29.19 351. 93 218 35.60* 3. 411E+OO 7.832E-01 7.835E-01 21. 24 RN-222 609.32 172 45.49* 2.179E+OO 7.560E-01 7.563E-01 26.14 1120. 29 43 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 1764.49 15 15.30 9.120E-01 4. 811E-01 4.813E-01 89.14 RA-224 240.99 121 4.10* 4.607E+OO 2.797E+OO 2.797E+OO 51. 87 RA-226 609.32 172 45.49* 2.179E+OO 7.560E-01 7.563E-01 26.14 1120.29 43 14.92 1.350E+OO 9.249E-01 9.253E-01 55.63 1764.49 15 15.30 9.120E-01 4. 811E-01 4.813E-01 89.14 AC-228 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 86 11. 27 3.525E+00 9.430E-01 9.430E-01 50.35 794.95 ------4.25 1. 768E+OO ------Line Not Found ------835.71 ------1. 61 1. 701E+OO ------Line Not Found ------911.20 81 25.80* 1.590E+OO 8.631E-01 8. 631E-01 27.35 968.97 38 15.80 1.513E+OO 6.904E-01 6.904E-01 71. 06 RA-228 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 86 11. 27 3.525E+OO 9.430E-01 9.430E-01 50.35 794.95 ------4.25 1.768E+OO ------Line Not Found ------Page 3795of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID G405235040 Acquisition date 3-0CT-2016 09:20:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 835. 71 ------1. 61 l.701El+OO ------Line Not Found ------911.20 Bl 25.80* 1.590E+OO 8.631E-01 8.631E-01 27.35 968. 97 38 15.80 l.513E+OO 6.904E-01 6.904E-01 71. 06 TH-228 74.82 133 10.28 3.170E+OO 1.776E+OO 1.776E+OO 54.69 77 .11 185 17.10 3.429E+OO 1.374E+OO 1.374E+OO 37.08 238.63 446 43.60* 4.647E+OO 9.611E-01 9. 611E-01 14.14 300.09 35 3.30 3.891E+OO 1.207E+OO 1.207E+OO 121.08 TH-230 609.32 172 45.49* 2.179E+OO 7.560E-01 7.560E-01 26 .14 1120.29 43 14.92 1.350E+OO 9.249E-01 9.250E-01 55.63 1764.49 15 15.30 9.120E-01 4. BllE-01 4.BllE-01 89.14 TH-232 105.21 ------1.10 5.379E+OO ------Line Not Found ------338.32 86 11.27 3.525E+OO 9.430E-01 9.430E-01 50.35 835. 71 ------1. 61 1.701E+OO ------Line Not Found ------911. 20 81 25.80* 1.590E+OO 8. 631E-01 8. 631E-01 27.35 968. 97 38 15.80 1. 513E+OO 6.904E-01 6.904E-01 71. 06 U-234 609.32 172 45.49* 2.179E+OO 7.560E-01 7.560E-01 26.14 1120.29 43 14.92 1.350E+OO 9.249E-01 9.250E-01 55.63 1764.49 15 15.30 9.120E-01 4.BllE-01 4.BllE-01 89.14 AM-241 59. 54' 42 35.90* 1.495E+00 3.456E-01 3:461E-01 111. 43 AM-243 43.53 ------5.90 2.347E-01 ------Line Not Found ------74.66 133 67.20* 3.170E+OO 2.717E-01 2.717E-01 54.69 ANH-511 511. 00 18 100.00* 2.510E+OO 3.192E-02 3.192E-02 252.30 Flag: "*" Key line Page 3796 of 5809 Surrunary of Nuclide Activity Sample ID : G405235040 Acquisition date Page : 3 3-0CT-2016 09:20:08 Total number of lines in spectrum 52 Number of unidentified lines 15 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 PR-144 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 'RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-241 AM-243 ANH-511 Hlif e l.25E+09Y 70.86D 461.40D 2.30E+05Y 30.08Y 30.08Y 284.910 l.41E+l0Y 7.04E+08Y 1. 41E+l0Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y l.41E+10Y 1. 41E+l0Y l.41E+l0Y 7.54E+04Y 1. 41E+10Y 2.45E+05Y 432.60Y 7370.00Y l.OOE+09Y Decay 1. 00 20.3 1. 59 1. 00 1. 02 1. 02 2 .11 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.295E+Ol 2.810E-02 1.470E+OO 1. 470E-01 1.320E-01 1.394E-01 l.521E+OO 2.451E-01 2.158E+OO 7.986E-01 9.611E-01 7.560E-01 7.832E-01 7.560E-01 2.797E+OO 7.560E-01 8.631E-01 8.631E-01 9. 611E-01 7.560E-01 8.631E-01 7.560E-01 3.456E-01 2. 717E-01 3.192E-02 3.211E+Ol 3.211E+Ol Decay Corr pCi/GRAM l.295E+Ol 5.708E-01 2.335E+OO 1. 470E-01 l.345E-01 l.421E-01 3.217E+OO 2,. 451E-01 2.158E+OO 7.986E-01 9.611E-01 7.563E-01 7.835E-01 7.563E-01 2.797E+OO 7. 5'63E-01 8.631E-01 8.631E-01 9. 611E-01 7.560E-01 8.631E-01 7.560E-01 3.461E-01 2.717E-01 3.192E-02 3.522E+Ol 3.522E+Ol 71.15% Decay Corr 2-Sigma Error 0.138E+Ol 4.877E-01 2.551E+OO l.607E-01 0.693E-01 0.732E-01 9.868E+OO 0.794E-01 0.458E+OO 9.285E-01 1.359E-01 l.977E-01 1.664E-01 1.977E-01 1.451E+OO l.977E-01 2.361E-01 2.361E-01 l.359E-01 1.976E-01 2.361E-01 1.976E-01 3.856E-01 1.486E-01 8.053E-02 "M" Manually accepted
  • 2-Sigma %Error 10.69 85.45 109.26 109.26 51. 51 51. 51 306.78 32.38 21.24 116.26 14.14 26.14 21.24 26.14 51. 87 26.14 27.35 27.35 14.14 26.14 27.35 26.14 111. 43 54.69 252.30 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3797 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235040 Acquisition date : 3-0CT-2016 09:20:08 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 36.14 55 42 1. 76 72 .12 68 16 l.OOE-02 87.2 2.66E-02 4 37.58 20 51 1. 21 75.00 68 16 3.75E-03 **** 4.73E-02 0 93.16 89 175 1. 65 186.14 182 9 l.80E-02 74.4 4.74E+OO T 0 116 .. 83 29 9'1 0.49 233.50 230 6 6.07E-03 **** 5.74E+OO T 0 154.17 15 134 1.17 308.17 305 7 3.27E-03 **** 5.86E+OO T 0 185.69 122 107 1.20 371. 22 367 10 2.65E-02 43.2 5.45E+OO T 0 270.09 64 81 1.26 540.03 535 10 l.47E-02 64.3 4.23E+OO T 0 310.07 20 73 1. 78 620.00 61.2 11 4.53E-03 **** 3.79E+OO 0 328.27 26 68 1. 37 656.40 649 9 6.12E-03 **** 3. 61E+OO T 0 433.68 16 48 0.71 8 67. 27 859 12 3.97E-03 **** 2.87E+OO T 0 463.28 38 56 1. 84 926.47 919 13 9.25E-03 93.2 2.72E+OO T 0 568.90 50 53 1. 95 1137.78 1131 16 1. 25E-02 75.0 2.30E+00 T 0 711.78 24 9 0.53 1423.66 1420 10 6.07E-03 63.9 l.93E+OO T 5 839.82 10 4 1. 36 1679.87 1678 14 2.70E-03 76.9 l.69E+OO 5 842.93 24 8 2.76 1686.08 1678 14 6.43E-03 65.7 l.69E+00 0 918.40 6 5 0.49 1837 .13 1833 6 l.54E-03 **** l.58E+OO 0 934.87 24 8 2.45 1870.07 1864 12 6.45E-03 65.6 l.56E+OO 0 954.97 9 6 1. 47 1910.29 1903 11 2.36E-03 **** 1. 53E+00 T 0 1099.51 7 20 4.47 2199.60 2189 12 l.94E-03 **** l.37E+OO T 0 1185. 40 12 6 2.75 2371. 50 2365 12 3.33E-03 **** l.29E+OO 0 1238.67 27 6 0.74 2478.13 2474 10 7.35E-03 53.8 1.24E+OO T 0 1242.98 7 2 0.62 2486.77 24'84 6 2.04E-03 91. 5 l.24E+OO 0 1255.12 11 24 3.73 2511. 07 2499 18 3.08E-03 **** l.23E+OO 0 1321. 66 10 2 2 .11 2644.27 2638 10 2.78E-03 85.4 l.18E+OO 0 1325.88 7 0 0.58 2652. 71 2650 6 l.94E-03 75.6 l.18E+OO 0 1337.19 7 1 0.69 2675. 36 2672 6 2.08E-03 89.4 1. l 7E+OO 0 1340.06 6 3 0.52 2681.10 2678 6 l.60E-03 **** 1. l 7E+OO 0 1589.14 9 3 3.47 3179.79 3173 13 2.67E-03 **** l.OOE+OO Flags: "T" = Tentatively associated Page 3798of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:22:08.76 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l *
  • Acquisition date 3-0CT-2016 09:20:08 Sensitivity 3.000 *
  • Detector ID GAM12 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:23:00 Nuclide Library : SOLID *
  • Sample ID G405235040 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7201E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 22-SEP-2016 11:41:01 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;13
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 PR-144 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-241 AM-243 ANH-511 Le (pCi/GRAM 1. 792E-01 4.640E-01 1. 371E+OO 8.705E-02 2.656E-02 2.806E-02 2.730E+OO 2.182E-02 3.909E-01 4.lOOE-02 5.881E-02 4.833E-02 5.881E-02 4.393E-01 5.881E-02 8.619E-02 8.619E-02 4.lOOE-02 5.878E-02 8.619E-02 5.878E-02 1. 712E-01 5.140E-02 2.212E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 3799 of 5809 Le (pCi/GRAM 9.365E+OO 2.598E-02 O.OOOE+OO 2.569E-02 2.667E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3800 of 5809 5.220E-02 3.300E-01 O.OOOE+OO 4.330E-02 6.444E+OO 2.374E-02 1.257E-01 1.918E+00 l.339E+Ol O.OOOE+OO 1.679E-01 0.000E+OO O.OOOE+OO 5.868E-01 6.280E+OO 7.216E-01 O.OOOE+OO 2.214E-01 5.420E+02 2.489E-02 7.199E-01 2.436E+OO 1.371E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.397E-02 5.193E-02 5.591E+00 3.922E-01 3.922E-01 2 .151E-02 8.636E-02 2.200E-01 O.OOOE+OO O.OOOE+OO 1.180E-01 1.360E+OO 7.090E-02 2.915E+02 0.000E+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.988E-02 O.OOOE+OO 4.890E-02 1.231E-01 O.OOOE+OO O.OOOE+OO 9.208E-02 O.OOOE+OO O.OOOE+OO 2.445E+Ol O.OOOE+OO 3.060E-01 4.092E-02 3.643E-02 O.OOOE+OO 7.730E+02 O.OOOE+OO 2.023E-02 7. 484E-02. l.603E-01 6.553E-02 9.952E-02 1. 596E+OO 5.083E-02 3.121E+Ol 2.185E-01 7. 721E-02 l.683E-02 4.246E+00 5.903E-01 4.465E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3801 of 5809 2.865E+Ol 9.913E+Ol 4.210E-01 2.419E+OO 3.631E-02 6.569E+00 3.492E-01 6.160E-01 3.268E-01 4.410E-01 l.939E-01 1.939E-01 4.313E-01 3.844E-01 4.410E-01 4.842E-02 l.990E-01 3.484E+OO 1.709E+OO 1. 546E-01 4.842E-02 O.OOOE+OO 1. 709E+OO 2.224E-01 2.948E+02 8.650E-02 5.663E-02 3.039E-02 2.865E-02 8.923E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUW FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:22:16.21 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235040.CNF;l *
  • Acquisition date 3-0CT-2016 09:20:08 Sensitivity : 3.000 *
  • Detector ID GAM12 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:23:00 Nuclide Library : SOLID *
  • Sample ID G405235040 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity 1.7201E+02 GRAM *
  • Quantity Err(%) 1.1627E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-SEP-2016 11: 41: 01 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM12 CAN.CNF;l3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 C0-58 CD-109 SN-126 BA-137M CS-137 PR-144 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 AM-241 AM-243 ANH-511 1.295E+Ol 5.708E-01 1.065E+OO 6.705E-02 l.345E-01 1.421E-01 3.217E+OO 2. 451E-01 7.986E-01 9. 611E-01 7.563E-01 7.835E-01 7.563E-01 1.262E+OO 7.563E-01 8. 631E-01 8. 631E-01 9.611E-01 7.560E-01 8.631E-01 7.560E-01 3.461E-01 1. 968E-01 3.192E-02 Act Error ( 1. 96-sigma) 1.517E+OO 4.786E-01 2.533E+OO 1.595E-01 6.816E-02 7.201E-02 9.671E+OO 7.848E-02 9.109E-01 l.429E-01 1. 965E-01 1.665E-01 1. 965E-01 1.493E+OO 1. 965E-01 2.355E-01 2.355E-01 l.429E-01 1.964E-01 2.355E-01 1. 964E-01 3.788E-01 l.480E-01 7.893E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3802 of 5809 Key-Line Activity (pCi/GRAM -5.510E+OO -2.605E-02 l.OOOE+41 3.655E-03 -1.997E-01 -1.061E+04 K.L Act error ( 1. 96-sigma) 1.166E+Ol 3.680E-02 3.840E+41 2. 971E-02 3.380E-01 1. 728E+04 TPU ( 1 . 96-sigma ) 1.517E+OO 4.786E-01 2.533E+OO 1.595E-01 6.816E-02 7.201E-02 9.671E+00 7.848E-02 9.109E-01 1.429E-01 1. 965E-01 l.665E-01 1. 965E-01 l.493E+OO 1. 965E-01 2.355E-01 2.355E-01 1.429E-01 1. 964E-01 2.355E-01 1. 964E-01 3.788E-01 l.480E-01 7.893E-02 TPU ( 1. 96-sigma) l.192E+Ol 3.863E-02 O.OOOE+OO 2.975E-02 3.498E-01 1.793E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -9.408E+Ol 4.942E+02 4. 960E+02 SHORT HLIF MN-54 l .118E-02 5.683E-02 5.705E-02 NOT IDENT. C0-56 1.057E-01 3. 901E-01 3.929E-01 FAIL ABUN MN-56 l.000E+41 3.691E+41 O.OOOE+OO SHORT HLIF C0-57 1. 864E-02 4.422E-02 4. 501E-02 NOT IDENT. FE-59 4.862E+OO 1.355E+Ol 1.373E+Ol FAIL ABUN C0-60 -8.745E-03 3.492E-02 3.514E-02 NOT IDENT. ZN-65 2.053E-02 1.586E-01 1.588E-01 NOT IDENT. GE-68 2.099E-01 2.160E+OO 2.162E+OO NOT IDENT. AS-73 -1. 0,.83E+Ol 1.619E+Ol 1. 691E+Ol NOT, IDENT. AS-74 1.824E+02 7.006E+03 7.006E+03 SHORT HLIF SE-75 -1.393E-02 1.958E-01 1. 959E-01 NOT IDENT. BR-77 1. 784E+39 1.585E+40 O.OOOE+OO SHORT HLIF SR-82 6. 831E+02 8 .132E+02 8.696E+02 SHORT HLIF RB-83 2.144E-02 6.767E-01 6.768E-01 NOT IDENT. KR-85 1.675E+OO 7.881E+OO 7.918E+OO NOT IDENT. SR-85 l.917E-01 9.057E-01 9.099E-Ol NOT IDENT. RB-86 1.561E+03 3.628E+04 3.628E+04 SHORT HLIF Y-88 1.230E-01 2.292E-01 2.359E-01 NOT IDENT. Y-91 2.977E+02 5.811E+02 5. 964E+02 NOT IDENT. NB-94 8.461E-03 2.BlOE-02 2.836E-02 NOT IDENT. NB-95 -8.984E-02 8.139E-01 8.149E-01 NOT IDENT. NB-95M 2.774E+00 2.699E+OO 2.975E+OO NOT IDENT. ZR-95 7.492E-02 l.627E+OO 1.627E+00 NOT IDENT. NB-97 1. OOOE+41 9.049E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 1.048E+41 O.OOOE+OO SHORT HLIF M0-99 6.152E+31 1.208E+33 O.OOOE+OO SHORT HLIF TC-99M -1. OOOE+41 7.838E+41 O.OOOE+OO SHORT HLIF RH-101 2.038E-02 3.475E-02 3.594E-02 NOT IDENT. RH-102 9.662E-03 5. 964E-02 5.980E-02 FAIL ABUN RU-103 6.176E+OO 5.549E+OO 6.208E+00 FAIL ABUN RH-106 2.252E-02 4.572E-01 4.573E-01 NOT IDENT. RU-106 2.252E-02 4. 572E-01 4.573E-01 NOT IDENT. AG-108M 2.777E-02 5.134E-02 5.284E-02 FAIL ABUN AG-llOM 4.762E-02 8. 965E-02 9.218E-02 NOT IDENT. SN-113 9.502E-02 2.388E-01 2.426E-01 NOT IDENT. CD-115 -2.288E+40 3.220E+40 O.OOOE+OO SHORT HLIF SN-117M -9.273E+04 1. 469E+05 1.527E+05 SHORT HLIF TE-123M -5.088E-02 l.299E-01 1.319E-01 NOT IDENT. SB-124 -7.465E-01 1.910E+OO 1.939E+OO NOT IDENT. SB-125 -1.222E-01 1.134E-01 1. 261E-01 FAIL ABUN TE-125M 2.179E+02 2.904E+02 3.066E+02 NOT IDENT. I-126 2.075E+05 1.308E+06 l.311E+06 SHORT HLIF SB-126 -5.838E+05 1.842E+06 1. 861E+06 SHORT HLIF SB-127 6.613E+21 7.648E+22 O.OOOE+OO SHORT HLIF I-131 4. 771E+09 9.515E+09 9.755E+09 SHORT HLIF I-132 1.000E+41 6.859E+42 O.OOOE+OO SHORT HLIF TE-132 l.845E+27 2.095E+27 O.OOOE+OO SHORT HLIF BA-133 2.374E-03 3.724E-02 3. 725E-02 NOT IDENT. I-133 -1.000E+41 8.787E+42 O.OOOE+OO SHORT HLIF CS-134 5.00lE-02 4.833E-02 5.333E-02 FAIL ABUN CS-135 1.438E-01 1. 339E-01 1.487E-01 NOT IDENT. I-135 l.000E+41 1.162E+42 O.OOOE+OO SHORT HLIF CS-136 -9.550E+04 4.277E+05 4.298E+05 SHORT HLIF CE-139 4.305E-02 9.550E-02 9.745E-02 NOT IDENT. BA-140 3.900E+05 l.594E+06 l.603E+06 SHORT HLIF LA-140 1.140E+05 5. 716E+05 5.739E+05 SHORT HLIF CE-141 -1.054E+Ol 2.674E+Ol 2.716E+Ol NOT IDENT. CE-143 l.000E+41 7.901E+40 0.000E+OO SHORT HLIF CE-144 -l.168E-01 3.323E-01 3.364E-01 NOT IDENT. PM-144 3.688E-02 l.109E-01 l.121E-01 FAIL ABUN PM-146 4.302E-03 4. 119E-02 4.124E-02 NOT IDENT. ND-147 -3.261E+06 4. 816E+07 4.819E+o7 SHORT HLIF PM-147 8.258E+02 7.552E+02 8.420E+02 NOT IDENT. PM-149 -1.000E+41 2.688E+41 O.OOOE+OO SHORT HLIF EU-150 1.016E-02 2.425E-02 FAIL ABUN EU-152 -2.983E-02 8. 741E-02 8.844E-02 FAIL ABUN GD-153 2.578E-02 l.825E-01 1.829E-01 NOT IDENT. EU-154 -5.921E-02 9.088E-02 9.471E-02 NOT IDENT. EU-155 1.112E-02 1. 031E-01 l.033E-01 FAIL ABUN TB-160 1. 228E+OO 1.585E+OO 1. 679E+OO FAIL ABUN H0-166M 9.904E-02 6.222E-02 7.658E-02 FAIL ABUN TM-171 -3.224E+OO 3.515E+Ol 3.518E+Ol NOT IDENT. HF-172 7.206E-02 2.258E-01 2.281E-01 NOT IDENT. LU-172 -3.215E-03 l.013E-01 l.013E-01 FAIL ABUN LU-176 -6.254E-03 2.198E-02 2.216E-02 FAIL ABUN HF-181 2.035E+OO 4. 611E+OO 4.702E+OO NOT IDENT. TA-182 -4.575E-01 7.804E-01 8. 072E-01 FAIL ABUN Page 3803 of 5809 RE-183 7.625E+OO 8.414E+OO 9.089E+OO FAIL ABUN RE-184 5.040E+OO 3.154E+Ol 3.162E+Ol NOT IDENT. W-188 l.599E+Ol l.208E+02 l.210E+02 NOT IDENT. IR-192 2.863E-02 4.810E-01 4.811E-01 FAIL ABUN HG-203 l.581E+OO 2.533E+OO 2.632E+OO NOT IDENT. BI-207 1.108E-02 3.946E-02 3.978E-02 FAIL ABUN PB-210 4.707E+OO 6.895E+OO 7.214E+OO NOT IDENT. BI-211 2.158E+OO 4.599E-01 l.076E+00 FAIL ABUN PB-211 3.784E-01 6.579E-01 6.797E-01 NOT IDENT. RN-219 -4 .178.E-02 3.760E-01 3.765E-01 FAIL ABUN RA-223 -l.179E-01 5.698E-01 5.722E-01 FAIL ABUN AC-227 8.106E-02 2.062E-01 2.094E-01 FAIL ABUN TH-227 8.106E-02 2.062E-01 2.094E-01 FAIL ABUN TH-229 3.593E-01 4.401E-01 4.690E-01 FAIL ABUN PA-231 4. 441E-01 4.289E-01 4.733E-01 NOT IDENT. TH-231 -l.179E-01 5.698E-01 5. 722E-01 FAIL ABUN PA-233 4.532E-03 5. 972E-02 5.975E-02 FAIL ABUN PA-234 7.769E-02 2.287E-01 2.314E-01 FAIL ABUN PA-234M -9.195E-01 4.037E+OO 4.059E+OO NOT IDENT. TH-234 1.104E+00 l.833E+OO 1.899E+OO FAIL ABUN U-235 -6.166E-02 l.673E-01 1. 696E-01 FAIL ABUN NP-237 4.532E-03 5.972E-02 5.975E-02 FAIL ABUN NP-238 -l.OOOE+41 2.125E+41 O.OOOE+OO SHORT HLIF U-238 l.104E+OO l.833E+OO l.899E+00 FAIL ABUN NP-239 2.808E-01 3.609E-01 3.825E-01 FAIL ABUN PU-239 l.204E+Ol 3.104E+02 3.105E+02 NOT IDENT. CM-243 -3.044E-02 9. 251E-02 9.352E-02 NOT IDENT. BK-247 1. 772E-02 6.738E-02 6.785E-02 NOT IDENT. CM-247 -5.995E-03 3.521E-02 3. 531E-02 NOT IDENT. CF-249 9.005E-04 3.234E-02 3.234E-02 NOT IDENT. CF-251 -1. 44 7E-02 9.717E-02 9.739E-02 NOT IDENT. Page 3804 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 51.9531 87.09 132.1236 136.47 66.4241 45.60 85.5104 87.57 153.2205 140.51 0.0000 46.54 70.9532 88.03 153.2949 143.76 82.1577 49. 72 0.0000 88.34 142.6056 144.24 70.4471 51. 35 72. 6906 88.47 142.6250 145.44 88.5932 51. 87 73.9776 89. 96 136.8226 152.43 74.9796 52.39 61.6936 1093.63 136.9188 153.25 0.0000 52.97 70.3883 91.11 0.0000 323.87 88.2753 53.44 75.3776 92.59 103.5413 156.02 0.0000 54.07 80.3913 93.35 103.6212 158.56 0.0000 57.36 0.0000 94.56 67.4359 159.00 84.9359 57.53 76.2164 94.65 67.4423 162.33 76.9026 57.98 81.2358 94.67 67.4435 162.66 0.0000 59.27 67.2592 94.87 67.4569 163.33 80.6228 59.32 67. 2 635 97.43 68.9297 165.86 55.9880 59.54 67.2831 98.43 59.8844 176.31 59.1732 60. 96 91.5419 98.44 59.8851 17 6. 60 0.0000 61.17 104.8859 99.53 67.7684 177.52 63.8494 62.93 98.8662 100 .11 79.1075 181. 07 0.0000 63.29 85.1390 102.03 70.5450 181. 52 52.8884 63.58 85.1703 103.18 77.5980 184.41 65.5423 64.28 85.2458 103.37 77.6120 143.76 66.0649 66.73 98.9191 105.21 76.8738 193.51 65.4683 67.24 99.8204 105.31 76.8809 197.03 71. 2415 125.81 105.7492 106.12 83.0598 198.01 59.0926 67.75 105.7581 106.47 76.9646 201.83 62.9972 69.67 83.2896 109.28 71.0274 203.43 64.0025 70.83 89.7234 111. 00 86.9483 205.31 49.0007 72. 81 103.8670 111.76 0.0000 210.85 71.8631 72.87 103.8745 114. 06 68.6947 215.65 57.8490 74.66 92.2432 116. 30 0.0000 222 .11 65.6898 74.82 92.2598 116.74 58.2656 227.09 68.7480 74.97 92.2759 119. 76 74.3532 227.38 66.8498 77 .11 92.5015 121.12 58.4892 228.16 0.0000 78.74 79.0685 121. 22 59.3805 228.18 46.8168 79.69 97.0254 121.78 66.5031 116.74 46.8168 80.12 103.4580 122.06 68.2930 235.69 59.0157 80.19 0.0000 122.92 83.4324 235.96 60.4647 80.57 111.1767 123.07 87.8813 238.63 57.6733 81. 00 111.2298 265.00 90.5916 238.98 0.0000 81. 07 102.2882 125.81 82.7482 240.99 57.7502 81. 75 104.9236 127.23 89.0828 242.00 57.7832 83.79 85.9204 127.91 82.8946 244.70 47.7437 84.00 85.9398 129.30 96.3762 252.40 0.0000 85.43 116. 9034 131. 20 84.9090 252.80 46.5049 86.55 110. 6120 133.02 82.3512 254.15 0.0000 86.79 132.0813 133.52 81.4894 256.23 47.5625 86.94 132 .1025 136.00 61.0156 260.90 0.0000 Page 3805 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 44.4635 355.39 0.0000 584.27 15.5199 264.80 45.6374 356.01 29. 0410 595.83 0.0000 265.00 39.4980 364.49 0.0000 427.87 15.5990 268.22 36.6348 366.42 0.0000 602.52 0.0000 269.46 43.9902 372.51 36.9463 604. 72 26.7754 2?0.03 44.0030 375.05 45.2Q49 607.14 30.1443 271.23 44.0314 377.52 43.1954 609.32 30.1641 273.65 0.0000 . 356. 01 32.9987 610.33 30.1740 276.40 51. 0172 388.16 29.9588 614.28 15.1051 277.37 46.1346 388.63 0.0000 618.01 23.5233 277.60 46.1404 391.69 35.1753 620.36 20.1775 278.00 46.1499 264.66 39.4581 621.93 19.0655 279.20 46.1786 401.81 39.4766 630.19 0.0000 279.54 40.2901 402.40 41. 5641 631. 2 9 22.4927 279.70 40.2935 404.85 33.2845 633.25 22.5065 280.46 52.1072 410.95 35.4513 634.78 0.0000 283.69 56.1326 413.71 34.4468 635.95 30.4080 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 44.3536 423.72 0.0000 645.85 11.2952 285.90 0.0000 427.09 42.4981 657.76 17.0020 287.50 49.3347 427.87 40.9368 657.90 0.0000 290.67 44.4717 433.94 36.2983 661. 66 20.4250 293.27 0.0000 439.40 30.5759 664.57 0.0000 351. 93 38.6295 453.88 28.6232 666.33 0.0000 295. 96 38.6437 463.37 29.7882 666.50 0.0000 879.38 38.6937 468.07 23.9781 667.71 0.0000 299.98 38.7207 473.00 0.0000 677.62 17.0990 300.09 38.7223 475.06 16.0263 685.70 0.0000 300 .13 38.7231 476.78 21.3818 695.00 0.0000 301.36 32.7858 477.60 25.6655 696.49 12.6064 302.85 29.8267 482.18 23.5657 696. 51 10.3143 256.23 29.8511 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.7554 306.78 35.8608 497.08 13.9992 697.49 13.7563 308.46 38.8810 505.52 23.3288 702.65 17.2198 311. 90 40.4431 507.63 0.0000 706.68 15.1701 316.51 41.0325 511. 00 27.0523 711. 68 17.2626 319.41 0.0000 514.00 32. 4963 720. 70 0.0000 320.08 0.0000 514.00 32. 4963 721. 93 0.0000 321. 04 39 .1143 520.40 26.0537 722.78 29.4356 323.87 39.1658 520.69 0.0000 722.91 29.4366 325.23 43.7133 522.65 0.0000 723.31 24.2454 328.76 0.0000 527.90 0.0000 724.19 17.3218 333.37 34.7997 528.26 25.0355 727. 33 21. 9602 333.97 31.7820 529.59 14.1569 733.00 17.3633 334.37 28.7609 529.87 0.0000 735.93 17.3767 338.28 44.4816 531. 02 0.0000 333.97 19.7019 338.32 44.4825 537.26 0.0000 739.50 0.0000 311. 90 42.5024 546.56 0.0000 747.24 13.9438 340.48 42.5024 552.55 15.3621 748.06 15.1090 340.55 0.0000 563.25 24.7751 752.31 15.1259 344.28 43.5888 569.33 24.2720 753.82 0.0000 345.93 36.5200 946.00 24.2738 756.73 20.9678 351.06 29.4862 569.70 24.2756 756.80 20.9685 351. 93 29.4974 583.19 15.5142 884.68 17.5067 Page 3806 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 21. 0183 1274.44 14.8003 1620.50 3.1053 766.42 20.1454 1001.03 16.6679 1621.92 5.1767 766.84 17.5195 1002.74 12.0423 1678.03 0.0000 772. 60 0.0000 1004.73 12.9742 1690.97 5.2304 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 .1025.87 0.0000 1764.49 778.90 17.5751 1028.54 0.0000 1063.66 9.5235 783.70 0.0000 1037.84 11.1995 1771.35 5.2914 785.37 7.0417 1038.76 0.0000 1791.20 0.0000 792.07 17.6343 631.29 9.3500 1808.65 4.2556 794.95 15.0000 1048.07 0.0000 1810. 72 0.0000 795.86 15.0037 1049.04 14.9678 1836.06 3.2040 810.06 14.1719 1050.41 13.1002 810.29 14.1729 1063.66 10.3219 344.28 14.1733 1077.00 0.0000 810.76 14.1743 1077.34 13.1737 815.77 0.0000 1085.87 12.2542 1048.07 0.0000 1093.63 22.6582 832.01 12.4683 1099.45 18.1488 834.85 16.0417 1112. 07 16.1097 835.71 19.0163 1112. 84 20.5798 836.80 0.0000 1115. 54 10.6210 846.75 0.0000 1120.29 13.2882 846.77 8.5808 1120.55 13.2891 856.80 0.0000 1221. 41 13.2916 860.56 23.3173 1129. 67 17.1167 871.09 12. 5871 1131. 51 0.0000 873.19 10.7944 1147.95 0.0000 875.33 0.0000 1173.23 11.5093 879.38 8.1076 1177.95 12.4795 880.51 13.5164 1189.05 7.6958 883.24 17.1318 1204.77 14.4736 884.68 11. 7257 1221.41 14.5184 889.28 16.2532 1231. 02 14.5450 894.76 9.9453 1235.36 0.0000 898.04 15.3819 1238.28 21.7492 900. 72 11. 7697 1260.41 0.0000 903.28 14.4946 1271. 87 11. 7231 911.20 11. 4097 1274.44 11. 72 90 912.08 11. 4120 1274.54 11.7290 923.98 0.0000 1291.59 5.8828 926.50 10.0184 1298.22 0.0000 929 .11 4.3743 1312 .11 0.0000 937.49 13.1480 1332.49 7.9009 944 .13 0.0000 1362.66 0.0000 946.00 9.1483 1365.19 6.9526 949.00 5.8588 1368.63 0.0000 667.71 0.0000 1384.29 3.9861 962. 31 10.2833 1408.01 7.0034 964.08 19.1052 1457.56 0.0000 966 .17 16.1734 1460.82 4.0374 911.20 18.3905 1489.16 2.0281 968. 97 18.3905 1505.03 6.0996 983.53 0.0000 1584.12 8.2349 984.45 0.0000 1596.21 0.0000 Page 3807of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:22:45.84 ******************************************************************************** * ' *GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621354.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM16.CNF;440 Background date : Z-OCT-2016 11:00:50. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 09:20:38. Sample ID G1203621354 Sample quantity : 1.78756E+02 GRAM Detector name : GAM16 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.18 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 92.48* 46 60 1. 41 184.98 178 15 1.29E-02 42.6 2 0 111.49 18 29 1. 43 222.97 218 9 4.91E-03 60.1 3 0 144.01* 17 35 1.23 287.97 283 11 4.76E-03 74.8 4 0 185.87* 6 35 2.03 371.66 368 9 1.57E-03218.9 5 0 199.03* 16 26 1.28 397.97 393 8 4.49E-03 63.9 6 0 273.79 23 68 5.30 547.42 534 21 6. 41E-03 91. 8 7 0 299.66 22 9 0.88 599.14 595 9 6.llE-03 32.5 8 0 383.80 8 22 0.80 767. 34 760 10 2 .15E-03119. 8 9 0 422.80 16 6 2.99 845.31 840 9 4.33E-03 39.1 10 0 511.46* 19 9 2.61 1022.57 1016 16 5.15E-03 70.0 11 0 551.98 7 2 1. 46 1103.57 1100 7 2.07E-03 46.7 12 0 565.28 9 9 1. 58 1130 .16 1126 11 2.62E-03 67.7 13 0 638.92 7 9 0.59 1277.39 1269 11 l.94E-03 97.2 14 0 838.68 7 5 1. 37 1676.81 1672 10 1. 94E-03 70. 7 15 0 849.09 8 0 1. 49 1697.63 1695 6 2.22E-03 35.4 16 0 1461.40* 4 5 0.89 2922.12 2916 10 1.05E-03136.7 Flag: "*" = Peak area was modified by background subtraction Page 3808of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 10:22:47 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621354.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 12-SEP-2016 00:00:00 G1203621354 Acquisition date : Sample quantity Sample geometry. Detector geometry: 3-0CT-2016 09:20:38 178.76 GRAM Sample Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA16 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line U-235 143.76 Page 3809 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line CE-141 145.44 CAN 0 01:00:00.18 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Sample ID : G1203621354 Nuclide Type: Nuclide Energy %Abn %Eff K-40

  • 1460.82 10.66* 1.215E+OO CE-141 145.44 48.29* 6.768E+OO U-235 89.96 3.47 5.608E+OO 93.35 5.60 5.774E+OO 143.76 10. 96* 6.770E+OO 163.33 5.08 6.541E+OO 185. 72 57.20 6.166E+OO 205.31 5.01 5.819E+OO ANH-511 511. 00 100.00* 2.835E+OO Flag: "*" = Keyline Page 3810of5809 Acquisition date Uncorrected Decay Corr pCi/GRAM pCi/GRAM l.203E-01 1.203E-01 2.709E-02 4.277E-02 Line Not Found 8.508E-01 8.508E-01 Line Not Found Line Not Found 8.759E-03 8.759E-03 Line Not Found 3.146E-02 3.146E-02 Page : 2 3-0CT-2016 09:20:38 2-Sigma %Error Status 273.45 OK 166.66 OK Absent 85.24 OK <<INT Reject Absent 437.85 OK Absent 139.98 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:22:48.93 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621354.CNF;l *
  • Acquisition date 3-0CT-2016 09:20:38 Sensitivity 3.000 *
  • Detector ID GAM16 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
  • Sample ID G1203621354 Sample Quantity 1.7876E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
  • Eff. 'File : DKAlOO: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.203E-01 3.224E-01 4.423E-01 CE-141 4.277E-02 6.985E-02 4.733E-02 U-235 1.305E-01 1.913E-01 1.847E-01 ANH-511 3.146E-02 4.315E-02 2.498E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -8 .196E-02 1.605E-01 3.033E-01 NOT IDENT. NA-22 -3.268E-03 l.382E-02 2. 963E-02 NOT IDENT. NA-24 O.OOOE+OO 2.654E+08 O.OOOE+OO SHORT HLIF AL-26 -2 .113E-02 2.232E-02 3.495E-02 NOT IDENT. SC-46 -5.940E-03 1.535E-02 3.152E-02 NOT IDENT. V-48 -3. 725E-03 3. 951E-02 8.527E-02 NOT IDENT. CR-51 -5.904E-02 2. 081E-01 4.194E-01 NOT IDENT. MN-54 -9. 996E-03 2.156E-02 3.567E-02 NOT IDENT. C0-56 8.005E-03 1.918E-02 4.236E-02 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.793E-03 9.920E-03 1.955E-02 NOT IDENT. C0-58 -9.923E-03 l.852E-02 3.614E-02 NOT IDENT. FE-59 -3.439E-02 4.188E-02 7.070E-02 NOT IDENT. co.:.60 3.549E-03 l.450E-02 3.602E-02 NOT IDENT. ZN-65 -1.849E-03 3.450E-02 7.490E-02 NOT IDENT. GE-68 2.389E-01 3.694E-01 1.050E+OO NOT IDENT. AS'-73 -7. 761E-02 4.120E-01 8.695E-01 NOT IDENT. AS-74 2.345E-02 6.759E-02 l.437E-01 NOT IDENT. SE-75 -2.877E-02 2.497E-02 3.829E-02 NOT IDENT. BR-77 -3.293E+Ol 2.741E+Ol 4.947E+Ol NOT IDENT. SR-82 -9.639E-02 l.598E-01 2.756E-01 NOT IDENT. RB-83 3.589E-02 3.236E-02 8.191E-02 FAIL ABUN KR-85 4.513E+OO 3.668E+OO 8.776E+OO NOT IDENT. SR-85 2.544E-02 2.075E-02 4. 962E-02 NOT IDENT. RB-86 1.416E-01 3.250E-01 8.465E-01 NOT IDENT. Y-88 -4.175E-03 1.593E-02 3.664E-02 NOT IDENT. Page 3811of5809 Y-91 -4.335E+OO 7.522E+OO 1.382E+Ol NOT IDENT. NB-94 -3.675E-03 1.843E-02 3.535E-02 NOT IDENT. NB-95 4. 021E-03 1.515E-02 3.523E-02 NOT IDENT. NB-95M -l.822E-02 4.654E-02 8.496E-02 NOT IDENT. ZR-95 -9.992E-03 3.568E-02 6.837E-02 NOT IDENT. NB-97 O.OOOE+OO l.603E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 4.378E+08 O.OOOE+OO SHORT HLIF M0-99 -8.378E+OO 2.729E+Ol 5.212E+Ol NOT IDENT. TC-99M O.OOOE+OO 4.994E+23 O.OOOE+OO SHORT HLIF RH-101 -4.797E-03 1. l;i7E-02 2.266E-02 FAIL ABUN RH-102 5.097E-03 2.416E-02 5.295E-02 NOT IDENT. RU-103 2.0lOE-02 2.270E-02 5.333E-02 NOT IDENT. RH-106 -1.539E-02 l.472E-01 2.988E-01 NOT IDENT. RU-106 -1.539E-02 1.472E-01 2.988E-01 NOT IDENT. AG-108M -5.794E-03 1. 447E-02 2.809E-02 NOT IDENT. CD-109 4.947E-02 2.679E-01 5.464E-01 NOT IDENT. AG-llOM -2.342E-02 2.084E-02 3.214E-02 NOT IDENT. SN-113 -6.025E-03 2.378E-02 4.737E-02 NOT IDENT. CD-115 1.203E+Ol 3.738E+Ol 8. 272E+Ol NOT IDENT. SN-ll 7M 1.659E-02 2.693E-02 5.953E-02 NOT IDENT. TE-123M 5.520E-03 l.104E-02 2.383E-02 NOT IDENT. SB-124 9.344E-03 3.751E-02 9.952E-02 NOT IDENT. SB-125 3.455E-02 3.759E-02 9.238E-02 NOT IDENT. TE-125M -2.689E+OO 3.779E+OO 6.245E+OO NOT IDENT. I-126 -l.158E-01 l.580E-01 2.690E-01 NOT IDENT. SB-126 -4.417E-02 9.452E-02 1.826E-01 NOT IDENT. SN-126 8.352E-03 2.663E-02 5.532E-02 NOT IDENT. SB-127 -l.324E+OO 2.239E+OO 3.945E+'OO NOT IDENT. I-131 4.884E-02 9.468E-02 2.123E-01 NOT IDENT. I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 l.497E-01 1.279E+OO 2.513E+OO FAIL ABUN BA-133 -7.059E-03 1. 841E-02 3.657E-02 FAIL ABUN I-133 O.OOOE+OO 3.624E+05 O.OOOE+OO SHORT HLIF CS-134 7.014E-03 1. 931E-02 4. 271E-02 NOT IDENT. CS-135 4.886E-03 6.127E-02 l.325E-01 NOT IDENT. I-135 O.OOOE+OO 1.707E+22 O.OOOE+OO SHORT HLIF CS-136 -2.788E-02 5.064E-02 9.663E-02 FAIL ABUN BA-137M -1. 475E-02 l.893E-02 3.187E-02 NOT IDENT. CS-137 -1.558E-02 2.000E-02 3.367E-02 NOT IDENT. CE-139 -4.285E-03 l.390E-02 2.624E-02 NOT IDENT. BA-140 -8.493E-02 l.818E-01 3.420E-01 FAIL ABUN LA-140 -9.886E-02 8.816E-02 1.180E-01 NOT IDENT. CE-143 O.OOOE+OO 1.277E+03 O.OOOE+OO SHORT HLIF CE-144 -7.222E-02 7.936E-02 1.390E-01 NOT IDENT. PM-144 -4.886E-03 1.789E-02 3.406E-02 NOT IDENT. PR-144 -3.668E-01 1.343E+OO 2.557E+OO NOT IDENT. PM-146 1.896E-03 1.559E-02 3.467E-02 NOT IDENT. ND-147 -3.394E-01 3.225E-01 4.955E-01 FAIL ABUN PM-147 1.232E+02 2.642E+02 5.862E+02 NOT IDENT. PM-149 9.794E+Ol 2. 886E+o2 6.356E+02 NOT IDENT. EU-150 5.203E-03 1.246E-02 2.751E-02 NOT IDENT. EU-152 -3.694E-02 4.644E-02 8.594E-02 NOT IDENT. GD-153 -1.229E-02 3.678E-02 6.684E-02 NOT IDENT. EU-154 -9.229E-03 3.904E-02 8.369E-02 NOT IDENT. EU-155 -2.888E-02 3. 696E-02 6.782E-02 NOT IDENT. TB-160 -1.756E-02 7.490E-02 l.527E-01 FAIL ABUN H0-166M -2.132E-02 3.657E-02 6.409E-02 FAIL ABUN TM-171 -1.465E+OO 7.523E+OO 1.602E+Ol NOT IDENT. HF-172 -9.223E-03 7.061E-02 1.424E-01 NOT IDENT. LU-172 -3.036E-02 2.993E-02 4.704E-02 NOT IDENT. LU-176 1.223E-03 l.077E-02 2.339E-02 NOT IDENT. HF-181 l.194E-03 2.099E-02 4.488E-02 NOT IDENT. TA-182 -4.403E-03 7.623E-02 1.630E-01 NOT IDENT. RE-183 8.638E-03 8.641E-02 l.905E-01 NOT IDENT. RE-184 -5. 311E-03 3.913E-02 9.157E-02 NOT IDENT. W-188 1.309E+OO 3.508E+OO 7.710E+OO NOT IDENT. IR-192 1.686E-03 1. 791E-02 3.789E-02 NOT IDENT. HG-203 -3.844E-03 2.133E-02 3.927E-02 NOT IDENT. BI-207 -7.275E-03 2.318E-02 4.659E-02 NOT IDENT. TL-208 1.068E-03 1.483E-02 3.336E-02 NOT IDENT. PB-210 -6.798E-02 1.892E+OO 4.125E+OO NOT IDENT. BI-211 l.147E-02 l.074E-01 2.225E-01 NOT IDENT. PB-211 6.915E-02 3.478E-01 7.428E-01 NOT IDENT. BI-212 2.834E-03 2.220E-01 4.607E-01 NOT IDENT. PB-212 -4.025E-02 2.735E-02 4.741E-02 FAIL ABUN BI-214 2.178E-02 4.304E-02 9.221E-02 NOT IDENT. PB-214 2.002E-02 3.820E-02 8.331E-02 NOT IDENT. RN-219 5.933E-03 l.785E-01 3.780E-01 NOT IDENT. Page 3812of5809 RN-222 2.178E-02 4.304E-02 9. 221E-02 NOT IDENT. RA-223 2.099E-01 3.049E-01 6.907E-01 FAIL ABUN RA-224 1.697E-01 2.767E-01 6.183E-01 NOT IDENT. RA-226 2.178E-02 4.304E-02 9. 221E-02 NOT IDENT. AC-227 2.399E-03 1.093E-01 2.330E-01 FAIL ABUN TH-227 2.399E-03 1.093E-01 2.330E-01 FAIL ABUN AC-228 -4.298E-02 6.603E-02 1. 411E-01 NOT IDENT. RA-228 -4.298E-02 6.603E-02 1.411E-01 NOT IDENT. TH-228 -4.025E-02 2.735E-02 4.741E-02 FAIL ABUN TH-229 -1.046E-01 2.207E-01 4.018E-01 IDENT. TH-230 2.178E-02 4.304E-02 9. 221E-02 NOT IDENT. PA-231 2.805E-02 1. 797E-01 3.648E-01 NOT IDENT. TH-231 2.099E-01 3.049E-01 6.907E-01 FAIL ABUN TH-232 -4.298E-02 6.603E-02 1.411E-01 NOT IDENT. PA-233 -1.360E-02 2.509E-02 4.934E-02 FAIL ABUN PA-234 -7.284E-02 l.478E-01 2.846E-01 FAIL ABUN PA-234M -9.380E-01 l.908E+OO 4.369E+OO NOT IDENT. TH-234 -5.147E-01 6.441E-01 1.333E+OO FAIL ABUN U-234 2.178E-02 4.304E-02 9.221E-02 NOT IDENT. NP-237 -1. 360E-02 2.509E-02 4.934E-02 FAIL ABUN NP-238 O.OOOE+OO 6.197E+Ol O.OOOE+OO SHORT HLIF U-238 -5.147E-01 6.441E-01 1.333E+OO FAIL ABUN NP-239 4.052E-02 8.103E-02 1.863E-01 NOT IDENT. PU-239 7.359E+Ol l.306E+02 2.864E+02 NOT IDENT. AM-241 -8 .'443E-03 6.021E-02 1.285E-01 NOT IDENT. AM-243 l.957E-03 1. 791E-02 3.897E-02 NOT IDENT. CM-243 8.762E-03 3.572E-02 7.845E-02 NOT IDENT. BK-247 -5.194E-02 4.312E-02 6.525E-02 NOT IDENT. CM-247 -3.138E-03 1.690E-02 3.438E-02 NOT IDENT. CF-249 l.870E-03 l.873E-02 3.975E-02 NOT IDENT. CF-251 1.446E-02 5.694E-02 1.156E-01 NOT IDENT. Page 3813of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:22:46.72 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 4 10.66* 1.215E+OO 1.203E-01 1.203E-01 273.45 CE-141 145.44 23 48.29* 6.768E+OO 2. 961E-02 4.674E-02 149.62 U-235 89. 96 ------3.47 5.608E+OO ------Line Not Found ------93.35 66 5.60 5.774E+OO 8.508E-01 8.508E-01 85.24 143.76 23 10. 96* 6.768E+OO 1.305E-01 1.305E-01 149.62 163.33 ------5.08 6.541E+OO ------Line Not Found ------185. 72 7 5,7. 20 6.166E+OO 8.759E-03 8.759E-03 437.85 205.31 ------5.01 5.819E+OO ------Line Not Found ------ANH-511 511. 00 21 100.00* 2.835E+OO 3.146E-02 3.146E-02 139.98 Flag: "*" Key line Page 3814of5809

'. Summary of Nuclide Activity Sample ID : Gl203621354 Acquisition date Page : 2 3-0CT-2016 09:20:38 Total number of lines in spectrum 16 Number of unidentified lines 4 Number of lines tentatively identified by NID 12 Nuclide Type : Nuclide K-40 CE-141 U-235 ANH-511 Hlife 1. 25E+09Y 32. 510 7.04E+08Y l.OOE+09Y Decay 1. 00 1. 58 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.203E-01 2.961E-02 l.305E-01 3.146E-02 3 .119E-01 3 .119E-01

  • Decay Corr pCi/GRAM l.203E-01 4.674E-02 l.305E-01 3.146E-02 3.290E-01 3.290E-01 75.00% Decay Corr 2-Sigma Error 3.290E-01 6.994E-02 1.952E-01 4.403E-02 2-Sigma %Error 273.45 149.62 149.62 139.98 Flags: "K" "E" Keyline not found Manually edited "M" "A" Manually accepted Nuclide specific abn. limit Flags Page 3815of5809 Unidentified Energy Lines Page : 3 Sample ID : G1203621354 Acquisition date : 3-0CT-2016 09:20:38 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 111.49 24 41 1. 43 222.97 218 9 4.91E-03 **** 6.58E+OO T 0 199.03 21 33 1. 28 397.97 393 8 4.49E-03 **** 5.93E+OO T 0 273.79 29 84 5.30 547.42 534 21 6.41E-03 **** 4.73E+OO T Q 299.66 27 11 0.88 599.14 9 6. llE-03 65.1 4.40E+OO T 0 383.80 9 27 0.80 767.34 760 10 2.15E-03 **** 3.59E+OO T 0 422.80 18 8 2.99 845.31 840 9 4.33E-03 78.2 3.31E+OO T 0 551. 98 8 2 1. 46 1103.57 1100 7 2.07E-03 93.3 2.66E+OO T 0 565.28 11 10 1. 58 1130 .16 1126 11 2.62E-03 **** 2.61E+OO 0 638.92 8 10 0.59 1277.39 1269 11 1.94E-03 **** 2.37E+OO 0 838.68 7 5 1. 37 1676.81 1672 10 1.94E-03 **** 1. 91E+OO 0 849.09 9 0 1. 49 1697.63 1695 6 2.22E-03 70.7 1.89E+OO Flags: "T" = Tentatively associated Page 3816of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:23:03.47 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621354.CNF;l *
  • Acquisition date 3-0CT-2016 09:20:38 Sensitivity 3.000 *
  • Detector ID GAM16 Energy tolerance: 1.500 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID Gl203621354 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7876E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]'EFF GAM16 CAN.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CE-141 U-235 ANH-511 Le (pCi/GRAM l.767E-01 2.064E-02 8.394E-02 1.038E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 Page 3817 of5809 Le (pCi/GRAM 1. 263E-01 1.050E-02 O.OOOE+OO 1.173E-02 1.192E-02 3.384E-02 1.845E-01 1.462E-02 1.742E-02 O.OOOE+OO 8.629E-03 1.435E-02 2.600E-02 1.357E-02 2.942E-02 4.029E-01 3.864E-01 6.255E-02 l.672E-02 2.213E+Ol 1.032E-01 3.530E-02 3.898E+OO 2.204E-02 3.277E-01 1.158E-02 4.896E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102. RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 PB-210 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 Page 3818of5809 1. 497E-02 1.398E-02 3.658E-02 2.757E-02 O.OOOE+OO O.OOOE+OO 2.094E+Ol O.OOOE+OO 9.956E-03 2.199E-02 2.336E-02 1.236E-01 1.236E-01 1.199E-02 2.408E-01 1.139E-02 2.069E-02 3.520E+Ol 2.652E-02 1.065E-02 3.526E-02 3.994E-02 2.658E+00 1.097E-01 7.433E-02 2. 451E-02 1.633E+OO 9.355E-02 O.OOOE+OO 1.123E+OO 1. 572E-02 O.OOOE+OO 1. 783E-02 5.829E-02 O.OOOE+OO 3.423E-02 1.307E-02 1.380E-02 1.17 9E-02 l.421E-01 4.182E-02 O.OOOE+OO 6.078E-02 l.423E-02 1.068E+OO l.435E-02 l.835E-01 2.599E+02 2.825E+02 1.218E-02 3. 714E-02 2.959E-02 2.965E-02 2.919E-02 6.335E-02 2.702E-02 7.020E+OO 6.283E-02 1. 741E-02 1.019E-02 l.888E-02 6.422E-02 8.459E-02 3.278E-02 3.439E+OO l.681E-02 1. 742E-02 l.835E-02 1.393E-02 1.844E+OO 9. 911E-02 3.249E-01 l.889E-01 2.102E-02 4.0BOE-02 3. 724E-02 l.625E-01 4.0BOE-02 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOO' IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. *FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. RA-223 RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3819of5809 3.085E-01 2.805E-01 4.080E-02 l.035E-01 1.035E-01 5.783E-02 5.783E-02 2.102E-02 1. 776E-01 4.080E-02 1. 564E-01 3.085E-01 5.783E-02 2.095E-02 1.142E-01 1. 766E+OO 6.068E-01 4.080E-02 2.095E-02 O.OOOE+OO 6.068E-01 8.129E-02 1. 2 8 6E+02 5.676E-02 1. 726E-02 3.444E-02 2.842E-02 1. 4 7 6E-02 l.730E-02 5.215E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:23:13.33 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621354.CNF;l * *Acquisition date 3-0CT-2016 09:20:38 Sensitivity : 3.000 *
  • Detector ID GAM16 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.18 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621354 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity 1.7876E+02 GRAM *
  • Quantity Err(%) 1.1188E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 23-SEP-2016 08:25:42 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM16 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma ) K-40 1.203E-01 3.225E-01 3.225E-01 CE-141 4.277E-02 6.987E-02 6.987E-02 U-235 1.305E-01 l.914E-01 1.914E-01 ANH-511 3.146E-02 4.317E-02 4.317E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) BE-7 -8.196E-02 1.605E-01 l.647E-01 NOT IDENT. NA-22 -3.268E-03 l.382E-02 1.390E-02 NOT IDENT. NA-24 1.313E+08 2.654E+08 2.720E+08 SHORT HLIF AL-26 -2 .113E-02 2.236E-02 2. 431E-02 NOT IDENT. SC-46 -5.940E-03 1.535E-02 1.558E-02 NOT IDENT. V-48 -3.725E-03 3. 951E-02 3.955E-02 NOT IDENT. CR-51 -5.904E-02 2.081E-01 2.098E-01 NOT IDENT. MN-54--9. 996E-03 2.157E-02 2.203E-02 NOT IDENT. C0-56 8.005E-03 1.919E-02 1.952E-02 NOT IDENT. MN-56 1.000E+41 2.419E+41 O.OOOE+OO SHORT HLIF C0-57 -2.793E-03 9.921E-03 l.OOOE-02 NOT IDENT. C0-58 -9.923E-03 1.852E-02 1.905E-02 NOT IDENT. FE-59 -3.439E-02 4 .196E-02 4.473E-02 NOT IDENT. C0-60 3.549E-03 l.450E-02 l.459E-02 NOT IDENT. ZN-65 -l.849E-03 3.450E-02 3. 451E-02 NOT IDENT. GE-68 2.389E-01 3.695E-01 3.849E-01 NOT IDENT. AS-73 -7.761E-02 4.123E-01 4.138E-01 NOT -IDENT. AS-74 2.345E-02 6.762E-02 6.844E-02 NOT IDENT. SE-75 -2.877E-02 2.501E-02 2.818E-02 NOT IDENT. BR-77 -3.293E+Ol 3.418E+Ol 3.726E+Ol NOT IDENT. SR-82 -9.639E-02 1.599E-01 1.657E-01 NOT IDENT. RB-83 3.589E-02 3.273E-02 3.651E-02 FAIL ABUN KR-85 4.513E+OO 3.673E+OO 4.199E+OO NOT IDENT. SR-85 2.544E-02 2.077E-02 2.373E-02 NOT IDENT. RB-86 l.416E-01 3. 251E-01 3. 313E-01 NOT IDENT. Y-88 -4.175E-03 l.593E-02 l.604E-02 NOT IDENT. Page 3820 of 5809 Y-91 -4.335E+OO 7.523E+OO 7.773E+OO NOT IDENT. NB-94 -3.675E-03 1.843E-02 1.850E-02 NOT IDENT. NB-95 4.021E-03 1.515E-02 1. 526E-02 NOT IDENT. NB-95M -l.822E-02 4.656E-02 4.728E-02 NOT IDENT. ZR-95 -9.992E-03 3.569E-02 3.597E-02 NOT IDENT. NB-97 l.000E+41 l.604E+41 0.000E+OO SHORT HLIF ZR-97 2.002E+08 4.379E+08 4.471E+08 SHORT HLIF M0-99 -8.378E+OO 2.730E+Ol 2.756E+Ol NOT IDENT. TC-99M -1.787E+23 4.997E+23 O.OOOE+OO SHORT HLIF RH-101 -4.797E-03 l.200E-02 FAIL ABUN RH-102 5.097E-03 2.416E-02 2.427E-02 NOT IDENT. RU-103 2.0lOE-02 2. 272E-02 2.446E-02 NOT IDENT. RH-106 -l.539E-02 1. 472E-01 1. 473E-01 NOT IDENT. RU-106 -1.539E-02 1. 472E-01 1. 473E-01 NOT IDENT. AG-108M -5.794E-03 1. 447E-02 l.471E-02 NOT IDENT. CD-109 4.947E-02 2.680E-01 2.689E-01 NOT IDENT. AG-110M -2.342E-02 2.087E-02 2.339E-02 NOT IDENT. SN-113 -6.025E-03 2.378E-02 2.394E-02 NOT IDENT. CD-115 l.203E+Ol 3. 7'38E+Ol 3.778E+Ol NOT IDENT. SN-117M l.659E-02 2.694E-02 2.796E-02 NOT IDENT. TE-123M 5.520E-03 l.104E-02 l.132E-02 NOT IDENT. SB-124 9.344E-03 3.752E-02 3.775E-02 NOT IDENT. SB-125 3.455E-02 3.762E-02 4.072E-02 NOT IDENT. TE-125M -2.689E+OO 3.782E+OO 3.971E+OO NOT IDENT. I-126 -1.158E-01 1.582E-01 1.666E-01 NOT IDENT. SB-126 -4.417E-02 9.462E-02 9.670E-02 NOT IDENT. SN-126 8.352E-03 2.663E-02 2.690E-02 NOT IDENT. SB-127 -1.324E+OO 2.244E+OO 2. 322E+O'O NOT IDENT. I-131 4.884E-02 9.471E-02 9.723E-02 NOT IDENT. I-132 1.000E+41 7.094E+41 O.OOOE+OO SHORT HLIF TE-132 1.497E-01 1.279E+00 l.281E+OO FAIL ABUN BA-133 -7.059E-03 1.842E-02 1. 8 69E-02 FAIL ABUN I-133 -8.566E+04 3.626E+05 3.646E+05 SHORT HLIF CS-134 7.014E-03 1.931E-02 l.957E-02 NOT IDENT. CS-135 4.886E-03 6.127E-02 6.131E-02 NOT IDENT. I-135 2.219E+22 2.022E+22 O.OOOE+OO SHORT HLIF CS-136 -2.788E-02 5.070E-02 5.223E-02 FAIL ABUN BA-137M -1.475E-02 1.894E-02 2.008E-02 NOT IDENT. CS-137 -1.558E-02 2. OOlE-02 2.121E-02 NOT IDENT. CE-139 -4.285E-03 1.393E-02 1. 406E-02 NOT IDENT. BA-140 -8.493E-02 1.818E-01 l.858E-01 FAIL ABUN LA-140 -9.886E-02 8.829E-02 9.890E-02 NOT IDENT. CE-143 2.193E+02 l.277E+03 1. 281E+03 SHORT HLIF CE-144 -7.222E-02 7.946E-02 8.587E-02 NOT IDENT. PM-144 -4.886E-03 1.789E-02 l.803E-02 NOT IDENT. PR-144 -3.668E-01 1. 344E+OO l.354E+OO NOT IDENT. PM-146 1.896E-03 1. 559E-02 1.561E-02 NOT IDENT. ND-147 -3.394E-01 3.229E-01 3.573E-01 FAIL ABUN PM-147 l.232E+02 2.643E+02 2. 701E+02 NOT IDENT. PM-149 9.794E+Ol 2.889E+02 2.922E+02 NOT IDENT. EU-150 5.203E-03 l.246E-02 l.268E-02 NOT IDENT. EU-152 -3.694E-02 4.649E-02 4.938E-02 NOT IDENT. GD-153 -l.229E-02 3.679E-02 3. 721E-02 NOT IDENT. EU-154 -9.229E-03 3.904E-02 3.926E-02 NOT IDENT. EU-155 -2.888E-02 3.702E-02 3.924E-02 NOT IDENT. TB-160 -1. 7 56E-02 7. 491E-02 7.533E-02 FAIL ABUN H0-166M -2.132E-02 3.659E-02 3.783E-02 FAIL ABUN TM-171 -1. 46SE+OO 7.524E+OO 7.553E+00 NOT IDENT. HF-172 -9.223E-03 7.062E-02 7.074E-02 NOT IDENT. LU-172 -3.036E-02 3.008E-02 3.305E-02 NOT I DENT.-LU-176 1.223E-03 l.077E-02 1.078E-02 NOT IDENT. HF-181 l.194E-03 2.099E-02 2.lOOE-02 NOT IDENT. TA-182 -4.403E-03 7.623E-02 7.626E-02 NOT IDENT. RE-183 8.638E-03 8.641E-02 8.650E-02 NOT IDENT. RE-184 -5. 311E-03 3.913E-02 3.920E-02 NOT IDENT. W-188 1.309E+OO 3. 511E+OO 3.560E+OO NOT IDENT. IR-192 1. 68 6E-03 1. 791E-02 1. 7 93E-02 NOT IDENT. HG-203 -3.844E-03 2.133E-02 2.140E-02 NOT IDENT. BI-207 -7.275E-03 2.318E-02 2.341E-02 NOT IDENT. TL-208 l.068E-03 1.483E-02 1.484E-02 NOT IDENT. PB-210 -6.798E-02 1.892E+OO 1. 8 92E+OO NOT IDENT. BI-211 1.147E-02 1.074E-01 1. 075E-01 NOT IDENT. PB-211 6.915E-02 3.478E-01 3.492E-01 NOT IDENT. BI-212 2.834E-03 2.220E-01 2.220E-01 NOT IDENT. PB-212 -4.025E-02 2.744E-02 3.289E-02 FAIL ABUN BI-214 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. PB-214 2.002E-02 3.821E-02 3.926E-02 NOT IDENT. RN-219 5.933E-03 1.785E-01 1.786E-01 NOT IDENT. Page 3821of5809 RN-222 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. RA-223 2.099E-01 3.052E-01 3.195E-01 FAIL ABUN RA-224 l.697E-01 2.768E-01 2.872E-01 NOT IDENT. RA-226 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. AC-227 2.399E-03 1.093E-01 l.093E-01 FAIL ABUN TH-227 2.399E-03 1.093E-01 l.093E-01 FAIL ABUN AC-228 -4.298E-02 6.606E-02 6.885E-02 NOT IDENT. RA-228 -4.298E-02 6.606E-02 6.885E-02 NOT IDENT. TH-228 -4.025E-02 2.744E-02 3.289E-02 FAIL ABUN TH-229 -1. 046E--,01 2.208E-()1 .2.258E-01 NOT IDENT. TH-230 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. PA-231 2.805E-02 l.798E-01 1.803E-01 NOT IDENT. TH-231 2.099E-01 3.052E-01 3.195E-01 FAIL ABUN TH-232 -4.298E-02 6.606E-02 6.885E-02 NOT IDENT. PA-233 -1. 360E-02 2.SlOE-02 2.584E-02 FAIL ABUN PA-234 -7.284E-02 1.697E-01 l.729E-01 FAIL ABUN PA-234M -9.380E-01 1.908E+OO l.954E+OO NOT IDENT. TH-234 -5.147E-01 6.541E-01 6.940E-01 FAIL ABUN U-234 2.178E-02 4.305E-02 4.415E-02 NOT IDENT. NP-237 -1.360E-02 2.SlOE-02 2.584E-02 FAIL ABUN NP-238 3.348E+Ol 6.199E+Ol 6.380E+Ol SHORT HLIF U-238 -5.147E-01 6.541E-01 6.940E-01 FAIL ABUN NP-239 4.052E-02 8. llOE-02 8.313E-02 NOT IDENT. PU-239 7.359E+Ol 1. 306E+02 1.348E+02 NOT IDENT. AM-241 -8.443E-03 6.021E-02 6.033E-02 NOT IDENT. AM-243 1.957E-03 1. 791E-02 1. 793E-02 NOT IDENT. CM-243 8.762E-03 3.573E-02 3.594E-02 NOT IDENT. BK-247 -5.194E-02 4.438E-02 5.017E-02 NOT IDENT. CM-247 -3.138E-03 1.691E-02 1. 696E-02 NOT IDENT. CF-249 1.870E-03 1.873E-02 1.875E-02 NOT IDENT. CF-251 l.446E-02 5. 696E-02 5.733E-02 NOT IDENT. Page 3822 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 19.1250 87.09 21. 6729 136.47 15.4885 45.60 17.4169 87.57 16.2705 140.51 19.2908 46.54 14.7095 88.03 16.2856 143.76 15.6543 49.72 12.0661 88.34 19.0117 144.24 15.6652 51. 35 16.7863 88.47 19.0167 145.44 15.6921 51. 87 18.6793 89. 96 21. 4574 152.43 24.9014 52.39 14.9656 1093.63 21.4864 153.25 23.7961 52.97 14.9902 91.11 21.5063 323.87 19.2889 53.44 19.7006 92.59 21. 5687 156 .. 02 18.1990 54.07 24.4343 93.35 21.6005 158.56 14.8374 57.36 0.0000 94.56 21.6510 159.00 17.1300 57.53 23.7174 94.65 21.6546 162.33 24.0883 57.98 19.9464 94.67 21. 6555 162.66 20.6559 59.27 20.0145 94.87 21.6638 163.33 21. 8226 59.32 20.9703 97.43 24.8793 165.86 31.1137 59.54 20.9824 98.43 22.8486 176.31 37. 3672 60. 96 28.7179 98.44 22.8491 17 6. 60 30.3719 61.17 28.7335 99.53 10.4070 177.52 24.5591 62.93 20.2036 100 .11 19.7947 181. 07 21.1424 63.29 29.8515 102.03 18.8189 181. 52 27.0300 63.58 29.8731 103.18 9.4291 184.41 18.8694 64.28 31. 8560 103.37 14.6725 143.76 27.1672 66.73 30.1060 105.21 23 .1331 193.51 26.2254 67.24 24.3090 105.31 22.0855 197.03 20.7465 125.81 28.2283 106.12 20.0109 198.01 15.5773 67.75 25.3123 106.47 14.7541 201.83 24.0692 69.67 27.3843 109.28 19.7692 203.43 24 .1122 70.83 21. 5747 111. 00 22.3066 205.31 30.2036 72.81 26.5993 111.76 22.3357 210.85 21. 8795 72.87 26.6031 114. 06 24.2027 215.65 34.2122 74.66 18.7969 116.30 19.2921 222 .11 14.7631 74.82 26.7209 116.74 10.7256 227.09 24.7330 74.97 26.7299 119.76 24.7920 227.38 24.7403 77 .11 24.8680 121.12 16.2044 228.16 22.2841 78.74 28.9498 121.22 15.1265 228.18 22.2847 79.69 22.0072 121. 7 8 23.7918 116.74 22.2847 80.12 25. 0313 122.06 22.7206 235.69 17.4654 80.19 25.0351 122.92 26.0023 235.96 17.4701 80.57 22.0487 123.07 26.0085 238.63 30.8627 81. 00 18.0564 265.00 17.3558 238.98 30.8736 81. 07 18.0592 125.81 20.6798 240.99 23.4105 81. 75 32.1516 127.23 22.9075 242.00 26.7814 83.79 20.1810 127.91 26.2079 244.70 25.1743 84.00 20.1898 129.30 18.6039 252.40 26.2073 85.43 29.3620 131. 20 17.5610 252.80 24.5260 86.55 22.3256 133.02 22.0120 254.15 0.0000 8 6. 7 9 21. 6597 133. 52 28.6375 256.23 21. 2121 86.94 21.6663 136.00 14.3721 260.90 22.1576 Page 3823 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 33.3522 355.39 0.0000 584.27 5.2895 264.80 33.3561 356.01 16.5934 595.83 11.7041 265.00 33.3625 364.49 12.9863 427.87 11. 7314 268.22 17.1594 366.42 19.5068 602.52 0.0000 269.46 17.1790 372.51 14. 9271 604.72 6. 4119 270.03 -17.1879. 375.05 12.1502 607 .14 17.1185 271.23 17.2066 377.52 9.8309 609.32 9.6394 273.65 17.2441 356.01 14.1064 610.33 12.8589 276.40 22.0406 388.16 14.1486 614.28 7.5153 277.37 20.7622 388.63 14.1531 618.01 10.7552 277.60 20.7661 391.69 18.9107 620.36 8.6139 278.00 20.7734 264.66 13.3184 621.93 8.6204 279.20 23.3954 401.81 12.3766 630.19 0.0000 279.54 23.4025 402.40 14.2865 631. 29 6.4941 279.70 24. 9662 404.85 14.3100 633.25 9.7504 280.46 20.8188 410.95 14.3680 634.78 8 .1311 283.69 25.2275 413.71 13.4346 635.95 11.3895 284.31 20. 8896 414.70 12.4829 636.99 10.8525 285.41 16.5535 423.72 8.6929 645.85 9.8079 285.90 17.4320 427.09 4.6463 657.76 4.3830 287.50 19.2021 427.87 5.8108 657.90 0.0000 290.67 18.3793 433.94 15.5553 661.66 14.2695 293.27 0.0000 439.40 13.6579 664.57 0.0000 351. 93 15.8152 453.88 6.8905 666.33 13.2002 295. 96 15.8251 463.37 7.9202 666.50 12 .1011 879.38 10.5735 468.07 6.9497 667.71 0.0000 299.98 9.7038 473.00 8. 9617 677.62 8.8447 300.09 9.7047 475.06 13.9573 685.70 13.3145 300 .13 9.7049 476.78 7.9837 695.00 11.1410 301.36 10.5981 477.60 12.9799 696.49 11.1483 302.85 15.9170 482.18 9.0101 696. 51 11.1483 256.23 11. 68 83 487.02 10.0395 697.00 14.4959 304.85 15.0576 492.35 11. 0774 697.30 16.7279 306.78 14.1947 497.08 8.0781 697.49 16.7297 308.46 13.3258 505.52 16.7410 702.65 12.2958 311. 90 16.0360 507.63 0.0000 706.68 14.5568 316.51 19.6730 511. 00 8.1417 711. 68 15.7101 319.41 17.9264 514.00 8.1553 720.70 6.7588 320.08 21.5229 514.00 8.1553 721.93 0.0000 321.04 25.1295 520.40 4.0921 722. 78 3.3824 323.87 15.2914 520.69 5 .1160 722.91 1.1275 325.23 21.6113 522.65 0.0000 723.31 2.2555 328.76 21.6714 527.90 8.2178 724.19 2.2563 333.37 21.7495 528.26 5.1371 727. 33 5.6482 333.97 15.4128 529.59 8.2253 733.00 7. 92 63 334.37 18.1384 529.87 0.0000 735.93 3.4011 338.28 14.5547 531. 02 10.2897 333.97 9.0755 338.32 14.5550 537.26 12.3892 739.50 7.9479 311.90 20.9575 546.56 0.0000 747.24 2.2781 340.48 20.9575 552.55 4.6837 748.06 3.4183 340.55 22.7809 563.25 4.7098 752.31 3.4243 344.28 22.8455 569.33 11.0242 753.82 4.5685 345.93 13. 7244 946.00 6.3000 756.73 8.0043 351.06 16.5330 569.70 6.3008 756.80 5.7176 351. 93 12.8672 583.19 4.2293 884.68 4.5874 Page 3824 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 3.4431 1274.44 7.4849 1620.50 5.5142 766.42 3.4440 1001.03 2. 8112 1621. 92 4.4126 766.84 6.8892 1002.74 1.8752 1678.03 0.0000 772.60 0.0000 1004.73 6.5674 1690.97 1.1194 776.52 6.9158 507.63 0.0000 1750.46 0.0000 5.7664 1025.87 O.OQOO 1764.49 4.5459 778.90 4.6149 1028.54 0.0000 1063.66 1.8205 783.70 5.7798 1037.84 2.8445 1771. 35 1.8209 785.37 2.3134 1038.76 0.0000 1791.20 0.0000 792.07 8 .1182 631.29 3.8030 1808.65 6.4207 794.95 5.8055 1048.07 4.7559 1810.72 0.0000 795.86 5.8075 1049.04 4.7574 1836.06 1.8443 810.06 11. 3873 1050.41 5.7114 810.29 8.7601 1063.66 6.6907 344.28 8.7607 1077.00 1.9194 810.76 8.7619 1077.34 0.9598 815.77 6.1451 1085.87 5.7740 1048.07 4.3939 1093.63 9.6460 832.01 5.2998 1099.45 7.7305 834.85 11. 3184 1112. 07 1.9398 835.71 9.9070 1112.84 3.8806 836.80 0.0000 1115. 54 4.8547 846.75 0.0000 1120. 29 7.7783 846.77 4.2634 1120.55 6.8065 856.80 6.2406 1221.41 8.7534 860.56 7.1421 1129. 67 1.9500 871. 09 3.5847 1131.51 0.0000 873.19 13.4532 1147. 95 0.0000 875.33 0.0000 1173.23 1. 9747 879.38 9.8878 1177.95 3.9546 880.51 5.3956 1189.05 0.9918 883.24 9.9016 1204.77 4.9808 884.68 9.0060 1221.41 5.0037 889.28 5.4126 1231.02 4.0134 894.76 1.8077 1235.36 4.0183 898.04 3.6196 1238.28 3.0161 900.72 2.7173 1260.41 0.0000 903.28 2.7198 1271.87 3.0434 911. 20 4.5456 1274.44 3.0456 912.08 2.7282 1274.54 3.0456 923.98 0.0000 1291.59 5.0989 926.50 5.4838 1298.22 0.0000 929 .11 3.6592 1312 .11 2.0505 937.49 2.7523 1332.49 2.0613 944 .13 5. 5172 1362.66 0.0000 946.00 9.2010 1365 .19 2.0784 949.00 6.4474 1368.63 0.0000 667.71 0.0000 1384.29 2.0883 962.31 6.4762 1408.01 3.1507 964.08 5.5543 1457.56 0.0000 966.17 8.3372 1460.82 5.3183 911.20 6.4907 1489.16 3.2122 968. 97 6.4907 1505.03 2.1494 983.53 5.5904 1584.12 3.2822 984.45 0.0000 1596.21 9.8729 Page 3825of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:23:48.28 ********************************************************************************
  • 4 GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621355.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM27.CNF;330 Background date : Z-OCT-2016 11:01:30. Sample date 30-NOV-2015 10:40:00 Acquisition date : 3-0CT-2016 09:21:06. Sample ID G1203621355 Sample quantity : 1.70095E+02 GRAM Detector name GAM27 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.94 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 2 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3826 of 5809 Energy 46.85* 63.28* 72.95 75.00* 77.05 87.08 89.88 92.83* 128.35 143.77* 163.65* 186.05* 209.11 225.87 238.68* 241.80 270.69 295.59* 300.50 328.98 338.07* 351.90* 463.97 491. 06 511. 06* 583.46* 609.47* 642.39 663.05* 728. 29 742.43 845.51 860. 2 9 881.21 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 19 36 35 161 284 63 59 45 50 15 7 70 46 20 404 88 42 200 53 15 90 312 20 17 73 155 202 15 17 38 27 8 29 15 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 136 167 212 168 168 227 82 196 106 81 133 106 77 54 161 74 70 74 52 76 57 69 71 20 55 42 53 18 46 41 12 7 12 17 1. 58 1. 00 1. 23 0.95 1. 24 1.15 1. 22 1. 29 2.38 0.75 1. 40 1. 72 0.85 1. 27 1.14 1.22 2.21 1. 08 1.18 1.29 1. 34 1. 28 3.36 1. 56 1. 83 1. 46 1. 46 1. 60 1. 97 1. 82 0.81 1. 23 1. 45 3. 68 93.01 125.87 145.23 149.32 153.43 173.50 179.10 185.01 256.06 286.91 326.69 371.51 417.64 451.18 476.81 483.06 540.85 590.67 600.50 657.49 675.67 703.35 927.58 981. 79 1021.80 1166. 67 1218.71 1284.60 1325.95 1456.48 1484.78 1691. 05 1720.62 1762.50 89 122 142 142 142 171 177 177 252 284 324 367 415 449 471 481 536 586 597 651 669 697 919 979 1016 1159 1212 1279 1320 1448 1480 1687 1715 1754 8 5.25E-03115.3 7 1.0lE-02 63.9 15 9.80E-03 68.3 15 4.47E-02 15.1 15 7.89E-02 10.1 7 1.75E-02 41.5 12 1.65E-02 21.8 12 1. 25E-02 60. 7 8 1.39E-02 38.2 6 4.lOE-03103.6 8 1.98E-03287.1 8 1. 93E-02 30. 4 8 1.29E-02 35.6 6 5.45E-03 63.0 10 1.12E-01 7. 8 6 2.46E-02 19.3 11 1.16E-02 41.7 11 5.56E-02 11.1 8 1.47E-02 27.3 10 4.26E-03108.8 11 2.49E-02 20.1 13 8.67E-02 7.9 13 5.57E-03 89.7 9 4.68E-03 52.2 15 2.02E-02 29.1 16 4.30E-02 12.7 15 5.62E-02 10.7 9 4.26E-03 57.7 15 4.77E-03 93.8 15 1.05E-02 40.3 10 7.42E-03 31.4 6 2.llE-03 67.4 10 7.93E-03 29.8 14 4.12E-03 65.1 Fit 4.62E+OO 9.35E-01 Peak Search Report (continued) Page : 2 Sample ID : Gl203621355 Acquisition date 3-0CT-2016 09:21:06 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 893.41 69 26 15.20 1786.90 1773 33 1.93E-02 24.9 36 0 911. 45* 90 43 1.14 1823.01 1817 13 2.50E-02 18.6 37 0 927.40 23 J.4 4.86 1854.93 1846 15 6.46E-03 41. 5 38 0 969.64* 55 45 1. 46 1939.47 1934 14 1.54E-02 29.4 39 0 1120.31* 66 11 1. 73 2240.99 2235 11 1. 83E-02 16.1 40 0 1126.44 10 6 1. 44 2253.27 2250 8 2. 72E-03 54.1 41 0 1177.68 15 2 0.98 2355.81 2352 8 4.13E-03 30.8 42 0 1180.97 13 2 0.76 2362.41 2359 8 3.72E-03 32.5 43 0 1193.17 10 17 3.36 2386.82 2379 10 2.79E-03 83.6 44 0 1237.59 31 19 0.92 2475.71 2467 15 8.73E-03 34.9 45 0 1279.23 12 1 0.64 2559.04 2556 8 3.22E-03 35.6 46 0 1297.27 6 16 2.86 2595.15 2585 13 l.66E-03144.7 47 0 1364.61 4 6 1. 23 2729.93 2722 9 l .19E-03116. 7 48 0 1376.86 31 0 1. 21 2754.45 2747 14 8. 61E-03 18.0 49 0 1409.66 18 3 3.28 2820.10 2813 14 4.94E-03 32.4 50 0 1460.82* 417 4 2.06 2922.50 2915 16 l.16E-01 5.1 51 0 1765.04* 27 7 2.24 3531.43 3524 13 7.52E-03 29.0 Flag: "*" = Peak area was modified by background subtraction Page 3827 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 10:23:51 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621355.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 10:40:00 G1203621355 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 09:21:06 170.10 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA27 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3828 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.94 10.00 0.00 % 'Peak Energy . . 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G1203621355 Acquisition date 3-0CT-2016 09:21:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 10.66* l.403E+OO 1.202E+Ol 10.14 OK C0-56 846.77 99.94* 2.182E+OO l.621E-02 2.572E-01 134. 83 OK 1037.84 14.17 l.863E+OO Line Not Found Absent 1238.28 66.90 l.617E+OO l.282E-01 2.033E+OO 69.84 OK 1771.35 15.47 l.172E+OO Line Not Found Absent CD-109 88.03 3.70* 7.559E+OO 2.810E-01 4.463E-01 409.78 OK SN-126 64.28 9.60 5.534E+OO 4.297E-01 4.297E-01 127.75 OK 86.94 8.90 7.559E+OO l.168E-01 1.168E-01 409.78 OK 87.57 37.00* 7.559E+OO 2.810E-02 2.810E-02 409.78 OK BA-137M 661.66 89.90* 2.620E+OO 3.503E-02 3. 572E-02 187.70 OK CS-137 661.66 85.10* 2.620E+OO 3.701E-02 3.773E-02 187.70 OK TL-208 277.37 6.60 5.132E+OO Line Not Found Absent 583.19 85.00* 2.885E+OO 3.083E-01 3.083E-01 25.31 OK 860.56 12.50 2.153E+OO 4.920E-01 4.920E-01 59.57 OK PB-210 46.54 4.25* 2.754E+OO 1.042E+OO 1.070E+OO 230.61 OK PB-212 74.82 10.28 6. 772E+OO 7.609E-01 7.609E-01 58.94 OK 77 .11 17.10 6.937E+OO l.470E+OO l.470E+00 20 .11 OK 238.63 43.60* 5.748E+OO 8.762E-01 8.762E-01 15.68 OK 300.09 3. 30 4.823E+OO 1. 763E+OO 1. 763E+OO 54.55 OK BI-214 609.32 45.49* 2.791E+OO 7.732E-01 7.735E-dl 21. 38 OK 1120. 29 14.92 1. 754E+00 1.129E+OO 1.129E+OO 32.27 OK 1764.49 15.30 l.177E+OO 6.303E-01 6.305E-01 58.08 OK PB-214 74.82 5.80 6.757E+OO Line Not Found <<INT Reject 77.11 9.70 6.937E+OO 2.591E+OO 2.592E+OO 20 .11 OK 87.09 3.41 7.559E+OO Line Not Found <<INT Reject 242.00 7.25 5.693E+OO l.163E+00 1.164E+OO 38.53 OK 295.22 18.42 4.885E+OO 1.180E+OO 1.180E+OO 22.14 OK 351. 93 35.60* 4.262E+OO l.069E+OO 1.069E+OO 15.89 OK RN-222 609.32 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 OK 1120. 29 14.92 1.754E+OO l.129E+OO 1.129E+OO 32.27 OK 1764.49 15.30 l.177E+00 6.303E-01 6.305E-01 58.08 OK RA-226 609.32 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 OK 1120.29 14.92 1.754E+OO 1.129E+OO l.129E+OO 32.27 OK 1764.49 15.30 l.177E+OO 6.303E-01 6.305E-01 58.08 OK AC-228 105.21 1.10 8.060E+OO Line Not Found Absent 338.32 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 OK 794.95 4.25 2.286E+OO Line Not Found Absent 835.71 1. 61 2.201E+OO Line Not Found Absent 911. 20 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 OK 968. 97 15.80 1. 964E+OO 8 .137E-01 8.137E-01 58.83 OK 105.21 1.10 8.060E+OO Line Not Found Absent 338.32 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 OK 794.95 4.25 2.286E+OO Line Not Found Absent 835. 71 1. 61 2.201E+OO Line Not Found Absent 911.20 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 OK 968. 97 15.80 l.964E+OO 8 .137E-01 8.137E-01 58.83 OK TH-228 74.82 10.28 6. 772E+OO 7.609E-01 7.609E-01 58.94 OK 77 .11 17.10 6.937E+OO 1.470E+OO l.470E+OO 20 .11 OK 238.63 43.60* 5.748E+OO 8.762E-01 8.762E-01 15.68 OK Page 3829 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G1203621355 Acquisition date 3-0CT-2016 09:21:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 3.30 4.823E+OO 1. 763E+OO 1. 763E+OQ 54.55 OK TH-230 609.32 45.49* 2.791E+OO 7.732E-01 7.732E-01 21. 38 OK 1120.29 14.92 1. 754E+OO 1.129E+OO 1.129E+OO 32.27 OK 1764.49 15.30 1.177E+OO 6.303E-01 6.303E-01 58.08 OK PA-231 283.69 1. 70 5.044E+OO Line Not Found Absent 301.36 5.35* 4.823E+OO 1.087E+OO 1.087E+OO 54.55 OK TH-232 105.21 1.10 8.060E+OO Line Not Found Absent 338.32 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 OK 835. 71 1. 61 2.201E+OO Line Not Found Absent 911. 20 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 OK 968. 97 15.80 1. 964E+OO 8 .137E-01 8.137E-01 58.83 OK TH-234 63.29 3.70* 5.534E+OO 1.115E+OO 1.115E+OO 127.75 OK 92.59 4.23 7.793E+OO 8.209E-01 8.209E-01 121.48 OK U-234 609.32 45.49* 2.791E+OO 7.732E-01 7.732E-01 21. 38 OK 1120.29 14.92 1. 754E+OO 1.129E+OO 1.129E+OO 32.27 OK 1764.49 15.30 1. 177E+OO 6.303E-01 6.303E-01 58.08 OK U-235 89. 96 3.47 7.683E+00 1.346E+OO l.346E+OO 43.58 OK 93.35 5.60 7.793E+OO 6.201E-01 6.201E-01 121. 48 OK 143.76 10.96* 7.743E+OO 1. OOlE-01 1. OOlE-01 207.10 OK 163.33 5.08 7.318E+OO 1. 089E-01 l.089E-01 574.18 OK 185. 72 57.20 6.810E+00 9.991E-02 9. 991E-02 '60. 79 OK 205.31 5.01 6.393E+OO Line Not Found Absent U-238 63.29 3.70* 5.534E+OO 1. 115E+OO 1.115E+OO 127.75 OK 92.59 4.23 7.793E+OO 8.209E-01 8.209E-01 121.48 OK AM-243 43.53 5.90 2.021E+OO Line Not Found Absent 74.66 67.20* 6.772E+OO 1.164E-01 1.164E-01 58.94 OK ANH-511 511.00 100.00* 3 .191E+OO 1.133E-01 l.133E-01 58.16 OK Flag: "*" = Keyline Page 3830of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:23:53.38 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621355.CNF;l *
  • Acquisition date 3-0CT-2016 09:21:06 Sensitivity : 3.000 *
  • Detector ID GAM27 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.94 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Analyst initials: MXRl * *Sample ID G1203621355 Sample Quantity 1.7010E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM27 CAN.'CNF;13
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.202E+Ol 1.195E+OO C0-56 2.572E-01 3.398E-01 CD-109 4.463E-01 1. 7 92E+OO SN-126 2.810E-02 1.129E-01 BA-137M 3.572E-02 6.570E-02 CS-137 3.773E-02 6. TL-208 3.083E-01 7.646E-02 PB-210 1.070E+OO 2.417E+OO PB-212 8.762E-01 1.346E-01 BI-214 7.735E-01 1. 621E-01 PB-214 1.069E+OO 1.665E-01 RN-222 7.735E-01 l.621E-01 RA-226 7.735E-01 1.621E-01 AC-228 7.786E-01 2.839E-01 RA-228 7.786E-01 2.839E-01 TH-228 8.762E-01 1.346E-01 TH-230 7.732E-01 1.620E-01 PA-231 1.087E+OO 5.814E-01 TH-232 7.786E-01 2.839E-01 TH-234 1.115E+OO l.396E+00 U-234 7.732E-01 1.620E-01 U-235 1.00lE-01 2.032E-01 U-238 1.115E+OO 1. 396E+OO AM-243 l.164E-01 6.724E-02 ANH-511 1.133E-01 6.461E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3831of5809 Key-Line Activity (pCi/GRAM 3.678E+OO 2.007E-02 O.OOOE+OO l.348E-03 1. 969E-01 K.L. Cnt Uncert ( 1. 96-sigma) l.018E+Ol 3.275E-02 l.163E+41 2.044E-02 3.186E-01 MDA (pCi/GRAM 4.316E-01 7.009E-01 1.622E+OO l.024E-01 4.983E-02 5.264E-02 4.442E-02 1.808E+OO 8.079E-02 9.914E-02 9.042E-02 9.914E-02 9.914E-02 1.841E-01 1.841E-01 8.079E-02 9.910E-02 5.989E-01 1. 841E-01 1. 2 64E+OO 9.910E-02 2.518E-01 1.264E+OO 5.755E-02 4.140E-02 MDA (pCi/GRAM 2.073E+Ol 6. 7 62E-02 O.OOOE+OO 4.652E-02 6.883E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1.530E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.922E+02 O.OOOE+OO SHORT HLIF MN-54 2.301E-02 4.982E-02 1.054E-01 NOT IDENT. MN-56 O.OOOE+OO 1.321E+41 O.OOOE+OO SHORT HLIF C0-57 -4.736E-03 3.484E-02 6.586E-02 NOT IDENT. C0-58 -1. 976E-01 4.286E-01 8.210E-01 NOT IDENT. FE-59 -3.122E+OO 6.409E+OO 1.170E+Ol NOT IDENT. C0-60 3.445E-03 2.518E-02 5.302E-02 NOT IDENT. ZN-65 4.042E-03 l.320E-01 2.349E-01 NOT IDENT. GE-68 2. 096E+OO 2.037E+OO 4.508E+OO NOT IDENT. AS-73 -1.544E+OO 3.929E+OO 7.706E+OO NOT IDENT. AS-74 O.OOOE+OO 5.787E+03 O.OOOE+OO SHORT HLIF SE-75 -6.294E-02 l.598E-01 3. llOE-01 NOT IDENT. BR-77 O.OOOE+OO 2.583E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 6. 968E+02 O.OOOE+OO SHORT HLIF RB-83 3.257E-02 5.307E-01 l.040E+OO NOT IDENT. KR-85 7.659E-01 6.101E+OO 1.068E+Ol NOT IDENT. SR-85 8.767E-02 7.020E-01 1.229E+OO NOT IDENT. RB-86 O.OOOE+OO 3.195E+04 O.OOOE+OO SHORT HLIF Y-88 2.683E-02 l.421E-01 3.400E-01 NOT IDENT. Y-91 -3.144E+02 4.620E+02 8.069E+02 NOT IDENT. NB-94 -2.081E-02 2.563E-02 4. 271E-02 NOT IDENT. NB-95 -9.650E-01 7.396E-01 1.098E+OO NOT IDENT. NB-95M -4.666E-01 2.107E+00 3.739E+OO NOT IDENT. ZR-95 7.913E-01 1. 365E+OO 2.755E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.139E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 693E+41 O.OOOE+OO SHORT HLIF RH-101 O.OOOE+OO 4.806E-02 4.741E-02 FAIL ABUN RH-102 2.394E-02 4.712E-02 9.612E-02 NOT IDENT. RU-103 l.021E+OO 4.656E+OO 9.393E+OO FAIL ABUN RH-106 7.037E-02 4.641E-01 8.916E-01 NOT IDENT. RU-106 7.037E-02 4.641E-01 8.916E-01 NOT IDENT. AG-108M -l.534E-02 2.186E-02 3.870E-02 NOT IDENT. AG-llOM 3.414E-03 9.427E-02 1.282E-01 NOT IDENT. SN-113 -1.954E-02 1.656E-01 3.248E-01 NOT IDENT. CD-115 O.OOOE+OO 3.293E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.140E+05 O.OOOE+OO SHORT HLIF TE-123M 6.327E-02 l.058E-01 2.078E-01 NOT IDENT. SB-124 6.668E-01 1. 779E+OO 3. 969E+OO NOT IDENT. SB-125 l.810E-02 7.460E-02 l.511E-01 FAIL ABUN TE-125M 1. 07 5E+02 2.210E+02 4.391E+02 NOT IDENT. I-126 O.OOOE+OO 1.049E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 521E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 8.688E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 7.297E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.554E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.819E+27 O.OOOE+OO SHORT HLIF BA-133 -3.907E-02 3.499E-02 5.465E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 l.935E-02 3.801E-02 7.724E-02 FAIL ABUN CS-135 -3.494E-02 l.022E-01 1.784E-01 NOT IDENT. I-135 O.OOOE+OO 1. 742E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.398E+05 O.OOOE+OO SHORT HLIF CE-139 2.436E-02 9.839E-02 l.730E-01 NOT IDENT. BA-140 O.OOOE+OO 1.615E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.438E+05 O.OOOE+OO SHORT HLIF CE-141 -7.203E+OO 2.469E+Ol 4.148E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 6. 42 6E-02 2.633E-01 5.098E-01 NOT IDENT. PM-144 8.028E-03 4. 591E-02 8.860E-02 NOT IDENT. PR-144 -2.579E-01 4.136E+OO 7. 714E+OO NOT IDENT. PM-146 -1. 331E-02 2.789E-02 5.190E-02 NOT IDENT. ND-147 O.OOOE+OO 4 .112E+07 O.OOOE+OO SHORT HLIF PM-147 -1. 748E+02 5.920E+02 1. 105E+03 NOT IDENT. PM-149 O.OOOE+OO 1.313E+41 O.OOOE+OO SHORT HLIF EU-150 6.773E-03 1. 866E-02 3.517E-02 FAIL ABUN EU-152 -2.135E-02 6.860E-02 1.320E-01 NOT IDENT. GD-153 -1.419E-01 l.253E-01 2.217E-01 NOT IDENT. EU-154 3.377E-02 8.418E-02 l.642E-01 NOT IDENT. EU-155 6. 871E-02 7.541E-02 l.551E-01 FAIL ABUN TB-160 -4.399E-01 1.406E+OO 2.733E+OO FAIL ABUN H0-166M l.746E-02 4.678E-02 9.286E-02 NOT IDENT. TM-171 -8.480E-01 7.778E+OO l.566E+Ol NOT IDENT. HF-172 -1.107E-01 1. 765E-01 2.904E-01 FAIL ABUN LU-172 1. 07 6E-02 5.610E-02 1.152E-01 FAIL ABUN LU-176 -1.847E-02 l.786E-02 3.221E-02 FAIL ABUN Page 3832 of 5809 HF-181 1.264E+OO 3.195E+OO 6. 672E+OO NOT IDENT. TA-182 2.691E-01 6.952E-01 1. 447E+OO FAIL ABUN RE-183 1.175E-02 1.620E+OO 3.234E+OO FAIL ABUN RE-184 1.190E+Ol 2.907E+Ol 5.578E+Ol FAIL ABUN W-188 4.785E+Ol 9.976E+Ol 1. 97 6E+02 FAIL ABUN IR-192 7.654E-02 3.865E-01 7.803E-01 FAIL ABUN HG-203 -l.326E-02 2.120E+OO 4.222E+OO FAIL ABUN BI-207 2.323E-02 3. 724E-02 8.0lOE-02 FAIL ABUN BI-211 O.OOOE+OO 4.586E-01 6.803E-01 FAIL ABUN PB-211 -1.684E-01 5.093E-01 9.648E-01 NOT IDE.NT. BI-212 O.OOOE+OO 8.728E-01 1.043E+OO FAIL ABUN RN-219 -6.253E-02 2. 896E-01 5.558E-01 FAIL ABUN RA-223 -2.036E-01 4. 961E-01 8.402E-01 FAIL ABUN RA-224 O.OOOE+OO 7.768E-01 1.223E+OO FAIL ABUN AC-227 3.791E-02 1. 769E-01 3.602E-01 FAIL ABUN TH-227 3.791E-02 1. 769E-01 3.602E-01 FAIL ABUN TH-229 l.694E-01 3.792E-01 7.245E-01 FAIL ABUN TH-231 -2.036E-01 4. 961E-01 8.402E-01 FAIL ABUN PA-233 -3.877E-02 4.164E-02 7.577E-02 FAIL ABUN PA-234 -1. 719E-01 2.017E-01 3.534E-01 FAIL ABUN PA-234M 8.732E-01 3.256E+OO 6.693E+00 NOT IDENT. NP-237 -3.877E-02 4.164E-02 7.577E-02 FAIL ABUN NP-238 O.OOOE+OO l.915E+41 O.OOOE+OO SHORT HLIF NP-239 1. 071E-01 l.685E-01 3.395E-01 NOT IDENT. PU-239 O.OOOE+OO 4.339E+02 4.530E+02 FAIL ABUN AM-241 -1.913E-02 7.794E-02 l.409E-01 NOT IDENT. CM-243 -3.200E-02 6.561E-02 1. 221E-01 NOT IDENT. BK-247 -1. 725E-02 5.235E-02 l.025E-01 NOT IDENT. CM-247 3.584E-03 2.661E-02 5.293E-02 NOT IDENT. CF-249 9.104E-03 2.940E-02 5.940E-02 NOT IDENT. CF-251 -2.734E-02 l.003E-01 l.810E-01 NOT IDENT. Page 3833 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 10:23:49.59 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 407 10.66* l.403E+OO l.202E+Ol l.202E+Ol 10.14 C0-56 846.77 8 99.94* 2.182E+OO 1.621E-02 2.572E-01 134.83 1037.84 ------14.17 1.863E+00 ------Line Not Found ------1238.28 31 66.90 1.617E+OO l.282E-01 2.033E+OO 69.84 1771.35 ------15.47 1.172E+OO ------Line Not Found ------CD-109 88.03 86 3.70* 7.559E+OO 1.364E+OO 2.167E+00 83.01 SN-126 64.28 52 9.60 5.534E+OO 4.297E-01 4.297E-01 127.75 86.94 86 8.90 7.559E+OO 5. 672E-01 5.672E-01 83.01 87.57 86 37.00* 7.559E+00 l.364E-01 1.364E-01 83.01 BA-137M 661. 66 19 89.90* 2.620E+00 3.503E-02 3. 572E-02 187.70 CS-137 661. 66 19 85.10* 2.620E+OO 3.701E-02 3.773E-02 187.70 TL-208 277.37 ------6.60 5.132E+OO ------Line Not Found ------583.19 171 85.00* 2.885E+00 3.083E-01 3.083E-01 25.31 860.56 30 12.50 2.153E+OO 4.920E-01 4.920E-01 59.57 PB-210 46.54 28 4.25* 2.754E+OO l.042E+00 1.070E+OO 230.61 BI-211 72.87 49 1.23 6.592E+OO 2.686E+OO 2.686E+OO 136.52 351. 06 367 12.92* 4.262E+00 2.945E+00 2.945E+OO 15.89 PB-212 74.82 225 10.28 6.772E+OO 1.424E+OO 1.424E+OO 30.20 77 .11 395 17.10 6.937E+OO l.470E+OO 1.470E+OO 20 .11 238.63 497 43.60* 5.748E+00 8.762E-01 8.762E-01 15.68 300.09 64 3.30 4.823E+00 1.763E+OO 1. 763E+OO 54.55 BI-214 609.32 222 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 1120. 29 67 14.92 1. 754E+OO l.129E+OO 1.129E+OO 32.27 1764.49 26 15.30 1.177E+OO 6.303E-01 6.305E-01 58.08 PB-214 74.82 225 5.80 6. 772E+OO 2.524E+00 2.525E+00 30.20 77 .11 395 9.70 6.937E+00 2.591E+OO 2.592E+OO 20 .11 87.09 86 3.41 7.559E+OO l.480E+OO 1.481E+OO 83.01 242.00 109 7.25 5.693E+OO l.163E+00 1.164E+OO 38.53 295.22 241 18.42 4.885E+00 l.180E+OO 1.180E+OO 22.14 351.93 367 35.60* 4.262E+OO 1.069E+OO 1.069E+OO 15.89 RN-222 609.32 222 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 1120. 29 67 14.92 1. 754E+OO l.129E+OO 1.129E+00 32.27 1764.49 26 15.30 l.177E+00 6.303E-01 6.305E-01 58.08 RA-224 240.99 109 4.10* 5.693E+OO 2.057E+OO 2.057E+OO 38.53 RA-226 609.32 222 45.49* 2.791E+OO 7.732E-01 7.735E-01 21. 38 1120.29 67 14.92 1. 754E+OO 1.129E+OO 1.129E+OO 32.27 1764.49 26 15.30 1. l 77E+OO 6.303E-01 6.305E-01 58.08 AC-228 105.21 ------1.10 8.060E+00 ------Line Not Found ------338.32 106 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 794.95 ------4.25 2.286E+OO ------Line Not Found ------835. 71 ------1. 61 2. 201E+OO ------Line Not Found ------911.20 94 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 968. 97 57 15.80 1. 964E+OO 8 .137E-01 8 .137E-01 58.83 RA-228 105.21 ------1.10 8.060E+00 ------Line Not Found ------338.32 106 11. 27 4.399E+00 9.435E-01 9.435E-01 40.20 794.95 ------4.25 2.286E+OO ------Line Not Found ------835. 71 ------1. 61 2.201E+00 ------Line Not Found ------Page 3834 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G1203621355 Acquisition date 3-0CT-2016 09:21:06 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Ef f pCi/GRAM pCi/GRAM %Error 911. 20 94 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 968. 97 57 15.80 1. 964E+OO 8.137E-01 8.137E-01 58.83 TH-228 74.82 225 10.28 6.772E+OO 1.424E+00 1.424E+OO 30.20 77 .11 395 17.10 6.937E+OO 1.470E+OO 1.470E+OO 20 .11 238.63 497 43.60* 5.748E+OO 8.762E-01 8.762E-01 15.68 300.09 64 3.30 4.823E+OO 1. 763E+OO 1. 763E+OO 54.55 TH-230 609.32 222 45.49* 2.791E+OO 7.732E-01 7.732E-01 21. 38 1120.29 67 14.92 1. 754E+OO 1.129E+OO 1.129E+OO 32.27 1764.49 26 15.30 1.177E+OO 6.303E-01 6.303E-01 58.08 PA-231 283.69 ------1. 70 5.044E+OO ------Line Not Found ------301.36 64 5.35* 4.823E+OO 1.087E+OO 1.087E+OO 54.55 TH-232 105.21 ------1.10 8.060E+OO ------Line Not Found ------338.32 106 11. 27 4.399E+OO 9.435E-01 9.435E-01 40.20 835.71 ------1. 61 2.201E+OO ------Line Not Found ------911. 20 94 25.80* 2.060E+OO 7.786E-01 7.786E-01 37.20 968. 97 57 15.80 1.964E+OO 8.137E-01 8.137E-01 58.83 TH-234 63.29 52 3.70* 5.534E+OO 1.115E+OO 1.115E+OO 127.75 92.59 61 4.23 7.793E+OO 8.209E-01 8.209E-01 121. 48 U-234 609.32 222' 45.49* 2.791E+OO 7.732E-01 7. 732E-01' 21. 38 1120.29 67 14.92 1. 754E+OO 1.129E+OO l.129E+OO 32.27 1764.49 26 15.30 1.177E+OO 6.303E-01 6.303E-01 58.08 U-235 89.96 81 3.47 7.683E+00 1.346E+OO 1.346E+OO 43.58 93.35 61 5.60 7.793E+OO 6.201E-01 6.201E-01 121.48 143.76 19 10. 96* 7.743E+OO 1.00lE-01 l.OOlE-01 207.10 163.33 9 5.08 7.318E+OO l.089E-01 1.089E-01 574.18 185. 72 88 57.20 6.810E+OO 9. 991E-02 9.991E-02 60.79 205.31 ------5.01 6.393E+OO ------Line Not Found ------U-238 63.29 52 3.70* 5.534E+OO 1.115E+OO 1.115E+OO 127.75 92.59 61 4.23 7.793E+OO 8.209E-01 8.209E-01 121. 48 AM-243 43.53 ------5.90 2. 021E+OO ------Line Not Found ------74.66 225 67.20* 6. 772E+OO 2.179E-01 2.179E-01 30.20 ANH-511 511. 00 82 100.00* 3.191E+OO l.133E-01 1.133E-01 58.16 Flag: "*" Key line Page 3835 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : Gl203621355 Acquisition date 3-0CT-2016 09:21:06 Total number of lines in spectrum 51 Number of unidentified lines 9 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 C0-56 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 77.23D 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 22.20Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600.00Y 1600. OOY 1. 41E+l0Y 1600. OOY 1.41E+10Y l.41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 15.9 1. 59 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.202E+Ol 1. 621E-02 l.364E+OO l.364E-01 3.503E-02 3. 701E-02 3.083E-01 1.042E+OO 2.945E+OO 8.762E-01 7.732E-01 1.069E+OO 7.732E-01 2.057E+OO 7.732E-01 7'.786E-01 7.786E-01 8.762E-01 7.732E-01 l.087E+OO 7.786E-01 l .115E+OO 7.732E-01 1. OOlE-01 l .115E+OO 2.179E-01 l.133E-01 T. 273E+Ol 3.273E+Ol Decay Corr pCi/GRAM l.202E+Ol 2. 572E-01 2.167E+OO l.364E-01 3. 572E-02 3.773E-02 3.083E-01 1. 070E+OO 2.945E+OO 8.762E-01 7.735E-01 1.069E+OO 7.735E-01 2.057E+OO 7.735E-01 7.786E-01 7.786E-01 8.762E-01 7.732E-01 1.087E+OO 7.786E-01 l .115E+00 7.732E-01 1.00lE-01 1.115E+OO 2.179E-01 1.133E-01 3.381E+Ol 3.381E+Ol 82.35% Decay Corr 2-Sigma Error 0.122E+Ol 3.468E-01 1.799E+OO l.133E-01 6.704E-02 7.082E-02 0.780E-01 2.467E+OO 0.468E+OO l.374E-01 1.654E-01 0.170E+OO 1.654E-01 0.793E+OO l.654E-01 2. 896E-01 2. 896E-01 1.374E-01 1.653E-01 0.593E+OO 2. 896E-01 1.424E+OO 1.653E-01 2.073E-01 1.424E+OO 0.658E-01 0.659E-01 "M" Manually accepted 2-Sigma %Error 10.14 134.83 83.01 83.01 187.70 187.70 25.31 230.61 15.89 15.68 21. 38 15.89 21. 38 38.53 21. 38 37. 20' 37.20 15.68 21. 38 54.55 37.20 127.75 21. 38 207.10 127.75 30.20 58.16 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3836 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : Gl203621355 Acquisition date : 3-0CT-2016 09:21:06 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 128.35 66 140 2.38 256.06 252 8 1.39E-02 76.5 8.00E+OO T 0 209 .11 58 96 0.85 417.64 415 8 1.29E-02 71.1 6. 31E+OO 0 225.87 24 67 1. 27 451.18 449 6 5.45E-03 **** 5.98E+OO T 0 270.69 51 85 2. 21
  • 540.85 536 11 l.16E-02 83.4 5.23E+OO Tc 0 328.98 18 90. 1.29 657.49 651 10 4.26E-03 **** 4.49E+OO T 0 463.97 23 81 3.36 927.58 919 13 5.57E-03 **** 3.44E+OO T 0 491.06 19 23 1. 56 981.79 979 9 4.68E-03 **** 3.29E+OO T 0 642.39 17 19 1. 60 1284.60 1279 9 4.26E-03 **** 2.68E+OO 0 728.29 41 44 1. 82 1456.48 1448 15 1.05E-02 80.6 2.44E+OO T 0 742.43 29 13 0.81 1484.78 1480 10 7.42E-03 62.7 2.41E+OO 0 881.21 16 18 3.68 1762.50 1754 14 4.12E-03 **** 2. llE+OO T 0 893.41 73 27 15.20 1786.90 1773 33 1.93E-02 49.8 2.09E+OO T 0 927.40 24 14 4.86 1854.93 1846 15 6.46E-03 83.0 2.03E+OO T 0 1126.44 10 6 1. 44 2253.27 2250 8 2.72E-03 **** 1. 75E+OO 0 1177.68 15 2 0.98 2355.81 2352 8 4. 13E-03 61. 6 1.68E+OO T 0 1180. 97 13 2 0.76 2362.41 2359 8 3.72E-03 65.1 1.68E+OO 0 1193.17 10 17 3.36 2386.82 2379 10 2.79E-03 **** 1.67E+OO 0 1279.23 12 1 0.64 2559.04 2556 8 3. 22E-03 71. 2 1. 57E+OO 0 1297.27 6 16 2.86 2595.15 2585 13 1.66E-03 **** 1. 55E+OO T 0 1364.61 4 6 1.23 2729.93 2722 9 1.19E-03 **** 1. 49E+00 T 0 1376.86 31 0 1.21 2754.45 2747 14 8.61E-03 35.9 1.48E+OO 0 1409.66 17 3 3.28 2820.10 2813 14 4:94E-03 64.8 1. 45E+OO Flags: "T" = Tentatively associated Page 3837 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:24:13.77 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621355.CNF;l * *Acquisition date 3-0CT-2016 09:21:06 Sensitivity : 3.000 *
  • Detector ID GAM27 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.94 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Nuclide Library : SOLID *
  • Sample ID G1203621355 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity : 1.7010E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM27 'CAN.CNF;13
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-56 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-51'1 Le (pCi/GRAM 1.754E-01 3.057E-01 7.742E-01 4.887E-02 2.224E-02 2.349E-02 1. 967E-02 8.441E-01 3.785E-02 4.468E-02 4.105E-02 4.468E-02 4.468E-02 8.052E-02 8.052E-02 3.785E-02 4.467E-02 2.748E-01 8.052E-02 5.997E-01 4.466E-02 1.183E-01 5.997E-01 2.732E-02 1.874E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 3838 of 5809 Le (pCi/GRAM 9.383E+OO 2.900E-02 O.OOOE+OO 1.802E-02 3.068E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3839 of 5809 O.OOOE+OO 4. 715E-02 O.OOOE+OO 3.086E-02 3.546E-01 5. ll 7E+OO 2.205E-02 l.OlOE-01 2.024E+OO 0.000E+OO l.434E-01 O.OOOE+OO O.OOOE+OO 4.673E-01 4.862E+OO 5.594E-01 O.OOOE+OO l.305E-01 3.492E+02 l.889E-02 4.751E-01 1. 745E+OO l.244E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.228E-02 4.330E-02 4.212E+OO 4.055E-01 4.055E-01 1. 743E-02 5.466E-02 l.466E-01 O.OOOE+OO O.OOOE+OO 9.770E-02 l.627E+OO 6.843E-02 2.073E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.478E-02 O.OOOE+OO 3.444E-02 8.165E-02 O.OOOE+OO O.OOOE+OO 8.129E-02 O.OOOE+OO O.OOOE+OO l.951E+Ol 0.000E+OO 2.393E-01 3.987E-02 3.471E+OO 2.288E-02' O.OOOE+OO 5.173E+02 O.OOOE+OO l.608E-02 6.030E-02 l.039E-01 7.033E-02 7.322E-02 l.182E+OO 4.183E-02 7.333E+OO l.354E-01 5.023E-02 l.468E-02 2.978E+OO SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT 'HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 RA-224 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3840 of 5809 6.345E-01 1.532E+OO 2.467E+Ol 9.201E+Ol 3.604E-01 l.962E+OO 3.550E-02 3.288E-01 4.388E-01 4.83!iiE-01 2.531E-01 3.852E-01 5.843E-01 l.678E-01 1.678E-01 3.404E-01 3.852E-01 3.437E-02 l.512E-01 2. 967E+OO 3.437E-02 O.OOOE+OO 1. 596E-01 2.136E+02 6.676E-02 5.705E-02 4.725E-02 2.419E-02 2. 728E-02 8.517E-02 FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 10:24:20.53 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* ** * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621355.CNF;l *
  • Acquisition date 3-0CT-2016 09:21:06 Sensitivity 3.000 *
  • Detector ID GAM27 Energy tolerance: 1.500 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.94 Half life ratio : ***** *
  • Sample date 30-NOV-2015 10:40:00 Nuclide Library : SOLID *
  • Sample ID G1203621355 Analyst initials: MXRl * *Batch Number 1596249 Sample Quantity 1.7010E+02 GRAM *
  • Quantity Err(%) 1.1758E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 3-0CT-2016 06:09:32 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM27 CAN.CNF;13
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act' Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.202E+01 1.349E+OO C0-56 2. 572E-01 3.400E-01 CD-109 4.465E-01 l.805E+OO SN-126 2. 811E-02 1.136E-01 BA-137M 3. 572E-02 6.572E-02 CS-137 3.773E-02 6.943E-02 TL-208 3.083E-01 7.759E-02 PB-210 l.070E+OO 2.419E+OO PB-212 8.762E-01 1.426E-01 BI-214 7.735E-01 1.655E-01 PB-214 1.069E+OO 1.725E-01 RN-222 7.735E-01 l.655E-01 RA-22 6 7.735E-01 1.655E-01 AC-228 7.786E-01 2.866E-01 RA-228 7.786E-01 2.866E-01 TH-228 8.762E-01 1. 426E-01 TH-230 7.732E-01 1.654E-01 PA-231 1.087E+OO 6.261E-01 TH-232 7.786E-01 2.866E-01 TH-234 1.115E+OO 1.417E+OO U-234 7.732E-01 1.654E-01 U-235 1.00lE-01 2.032E-01 U-238 1.115E+OO 1.417E+OO AM-243 1.164E-01 6.878E-02 ANH-511 l .133E-01 6.477E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3841of5809 Key-Line Activity (pCi/GRAM 3.678E+00 2.007E-02 1. OOOE+41 1.348E-03 1.969E-01 K.L Act error ( 1. 96-sigma) 1.018E+Ol 3.275E-02 l.246E+41 2.044E-02 3.187E-01 TPU ( 1. 96-sigma) 1. 349E+OO 3.400E-01 1. 805E+OO 1.136E-01 6. 572E-02 6.943E-02 7.759E-02 2.419E+OO 1.426E-01 1.655E-01 1.725E-01 1.655E-01 1.655E-01 2.866E-01 2.866E-01 1. 426E-01 1.654E-01 6.261E-01 2.866E-01 1.417E+OO 1.654E-01 2.032E-01 1.417E+OO 6.878E-02 6.477E-02 TPU ( 1. 96-sigma) 1.031E+Ol 3.398E-02 O.OOOE+OO 2.045E-02 3.308E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 -7. 696E+03 1.530E+04 l.569E+04 SHORT HLIF CR-51 -1.543E+Ol 3.922E+02 3.923E+02 SHORT HLIF MN-54 2. 301E-02 4.983E-02 5.090E-02 NOT IDENT. MN-56 l.OOOE+41 1. 322E+41 0.000E+OO SHORT HLIF C0-57 -4.736E-03 3.484E-02 3.490E-02 NOT IDENT. C0-58 -1.976E-01 4.287E-01 4.379E-01 NOT IDENT. FE-59 -3.122E+OO 6.413E+OO 6.566E+OO NOT IDENT. C0-60 3.445E-03 2.518E-02 2.523E-02 NOT IDENT. ZN-65 4.042E-03 1.320E-01 1. 320E-01 NOT IDENT. G&-68 2. 096E+OO 2.039E+OO
  • 2.247E+OO NOT IDENT. AS-73' -1.544E+OO 3.942E+OO 4.003E+OO NOT IDENT. AS-74 5.615E+03 5.806E+03 6.333E+03 SHORT HLIF SE-75 -6.294E-02 l.598E-01 l.623E-01 NOT IDENT. BR-77 1. 681E+39 1.495E+40 O.OOOE+OO SHORT HLIF SR-82 9.295E+02 6.982E+02 8.143E+02 SHORT HLIF RB-83 3.257E-02 5.307E-01 5.309E-01 NOT IDENT. KR-85 7.659E-01 6.101E+OO 6. lllE+OO NOT IDENT. SR-85 8.767E-02 7.020E-01 7.031E-01 NOT IDENT. RB-86 3.506E+04 3.199E+04 3.568E+04 SHORT HLIF Y-88 2.683E-02 1.421E-01 1.426E-01 NOT IDENT. Y-91 -3.144E+02 4.621E+02 4.834E+02 NOT IDENT. NB-94 -2. 081E-02 2.565E-02 2.731E-02 NOT IDENT. NB-95 -9.650E-01 7.407E-01 8.590E-01 NOT IDENT. NB-95M -4.666E-01 2.107E+OO 2 .118E+OO NOT IDENT. ZR-95 7.913E-01 1.365E+OO 1. 411E+OO NOT IDENT. NB-97 1.000E+41 2.440E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 6.698E+41 O.OOOE+OO SHORT HLIF M0-99 5.807E+32 1.140E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 1. 696E+41 O.OOOE+OO SHORT HLIF RH-101 6.413E-02 4.945E-02 5.728E-02 FAIL ABUN RH-102 2.394E-02 4.716E-02 4.838E-02 NOT IDENT. RU-103 1.021E+OO 4.657E+OO 4.679E+OO FAIL ABUN RH-106 7.037E-02 4.641E-01 4.652E-01 NOT IDENT. RU-106 7.037E-02 4.641E-01 4.652E-01 NOT IDENT. AG-108M -1.534E-02 2.186E-02 2.293E-02 NOT IDENT. AG-llOM 3.414E-03 9.427E-02 9.429E-02 NOT IDENT. SN-113 -1.954E-02 1.656E-01 1.659E-01 NOT IDENT. CD-115 -4.280E+39 3.294E+40 O.OOOE+OO SHORT HLIF SN-117M 4.373E+04 1.142E+05 1.158E+05 SHORT HLIF TE-123M 6.327E-02 1.059E-01 1. 096E-01 NOT IDENT. SB-124 6.668E-01 1. 779E+OO 1.804E+OO NOT IDENT. SB-125 1.810E-02 7.460E-02 7.505E-02 FAIL ABUN TE-125M l.075E+02 2. 211E+02 2.263E+02 NOT IDENT. I-126 8.075E+04 1.049E+06 l.050E+06 SHORT HLIF SB-126 -2.045E+05 l.521E+06 1.524E+06 SHORT HLIF SB-127 2.156E+21 8.694E+22 O.OOOE+OO SHORT HLIF I-131 -3.985E+09 7.299E+09 7.517E+09 SHORT HLIF I-132 -l.000E+41 1.905E+42 O.OOOE+OO SHORT HLIF TE-132 9.226E+25 1.819E+27 O.OOOE+OO SHORT HLIF BA-133 -3.907E-02 3.502E-02 3.920E-02 NOT IDENT. I-133 l.000E+41 l.497E+42 O.OOOE+OO SHORT HLIF CS-134 1.935E-02 3. 801E-02 3.900E-02 FAIL ABUN CS-135 -3.494E-02 1.022E-01 1.034E-01 NOT IDENT. I-135 -1.000E+41 7.173E+41 O.OOOE+OO SHORT HLIF CS-136 4.882E+04 3.398E+05 3.406E+05 SHORT HLIF CE-139 2.436E-02 9. 851E-02 9.912E-02 NOT IDENT. BA-140 3.266E+05 1.615E+06 1.621E+06 SHORT HLIF LA-140 -3.715E+05 5. 441E+05 5.693E+05 SHORT HLIF CE-141 -7.203E+OO 2.469E+Ol 2.490E+Ol NOT IDENT. CE-143 -1.000E+41 2 .110E+41 O.OOOE+OO SHORT HLIF CE-144 6.426E-02 2.633E-01 2.649E-01 NOT IDENT. PM-144 8.028E-03 4.591E-02 4.606E-02 NOT IDENT. PR-144 -2.579E-01 4.136E+OO 4.138E+OO NOT IDENT. PM-146 -l.331E-02 2.791E-02 2.854E-02 NOT IDENT. ND-147 -7.226E+06 4 .112E+07 4.125E+07 SHORT HLIF PM-147 -1. 748E+02 5.921E+02 5.973E+02 NOT IDENT. PM-149 -1.000E+41 1. 332E+41 O.OOOE+OO SHORT HLIF EU-150 6.773E-03 1. 866E-02 1.891E-02 FAIL ABUN EU-152 -2 .'135E-02 6.861E-02 6.928E-02 NOT IDENT. GD-153 -1. 419E-01 1. 256E-01 1.410E-01 NOT IDENT. EU-154 3.377E-02 8.419E-02 8.555E-02 NOT IDENT. EU-155 6. 871E-02 7.557E-02 8.167E-02 FAIL ABUN TB-160 -4.399E-01 l.406E+OO 1.420E+OO FAIL ABUN H0-166M 1. 746E-02 4.678E-02 4.744E-02 NOT IDENT. TM-171 -8.480E-01 7.778E+OO 7.787E+00 NOT IDENT. HF-172 -1.107E-01 1.774E-01 1.843E-01 FAIL ABUN LU-172 1. 076E-02 5.611E-02 5.632E-02 FAIL ABUN LU-176 -1. 847E-02 1.788E-02 1. 972E-02 FAIL ABUN Page 3842 of 5809 HF-181 l.264E+OO 3 .196E+OO 3.246E+OO NOT IDENT. TA-182 2.691E-01 6.952E-01 7.057E-01 FAIL ABUN RE-183 1.17 SE-02 1.620E+OO 1.620E+OO FAIL ABUN RE-184 l.190E+Ol 2. 921E+Ol 2.970E+Ol FAIL ABUN W-188 4.785E+Ol 9. 991E+Ol l.022E+02 FAIL ABUN IR-192 7.654E-02 3.865E-01 3.880E-01 FAIL ABUN HG-203 -l.326E-02 2.120E+OO 2.120E+OO FAIL ABUN BI-207 2.323E-02 3.725E-02 3.870E-02 FAIL ABUN BI-211 2.945E+OO 4.775E-01 l.411E+OO FAIL ABUN PB-211 -1.684E-01 5.094E-01 5.lSOE-01 NOT IDENT. BI-212 1.105E+OO 8.746E-01 l.007E+OO FAIL ABUN RN-219 -6.253E-02 2.897E-01 2. 911E-01 FAIL ABUN RA-223 -2.036E-01 4.962E-01 5.047E-01 FAIL ABUN RA-224 2.057E+OO 7.847E-01 1.215E+OO FAIL ABUN AC-227 3.791E-02 1.770E-01 1.778E-01 FAIL ABUN TH-227 3.791E-02 1.770E-01 1.778E-01 FAIL ABUN TH-229 l.694E-01 3.793E-01 3.869E-01 FAIL ABUN TH-231 -2.036E-01 4. 962E-01 5.047E-01 FAIL ABUN PA-233 -3.877E-02 4.169E-02 4.520E-02 FAIL ABUN PA-234 -l.719E-01 2.817E-01 2.922E-01 FAIL ABUN PA-234M 8.732E-01 3.256E+OO 3.280E+OO NOT IDENT. NP-237 -3.877E-02 4.169E-02 4.520E-02 FAIL ABUN NP-238 -l.000E+41 1.916E+41 O.OOOE+OO SHORT HLIF NP-239 l.071E-01 1.687E-01 1. 755E-01 NOT IDENT. PU-239 5.790E+02 4.346E+02 5.070E+02 FAIL ABUN AM-241 -l.913E-02 7.795E-02 7.843E-02 NOT IDENT. CM-243 -3.200E-02 6.568E-02 6. 724E-02 NOT IDENT. BK'--247 -1. 725E-02 5.246E-02 '5.304E-02 NOT IDENT. CM-247 3.584E-03 2.662E-02 2.667E-02 NOT IDENT. CF-249 9.104E-03 2. 941E-02 2.970E-02 NOT IDENT. CF-251 -2.734E-02 l.004E-01 1. OllE-01 NOT IDENT. Page 3843 of 5809
  • GEL taboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 75.5737 87.09 145.1000 136.47 86.1691 45.60 65.5803 87.57 145.2323 140.51 0.0000 46.54 65.7580 88.03 145.3587 143.76 80.1685 49.72 0.0000 88.34 109.0829 144.24 90.1517 51. 35 80.1621 88.47 109.1099 145.44 84.1762 51. 87 78.3396 89. 96 108. 0118 152.43 77.6201 52.39 74.5741 1093.63 108.1489 153.25 0.0000 52.97 86.3281 91.11 0.0000 323.87 73.1543 53.44 94.2045 92. 59 108.5374 156.02 0.0000 54.07 97.2776 93.35 108.6886 158.56 0.0000 57.36 0.0000 94. 56 80.6340 159.00 67.7617 57.53 116. 7861 94.65 80.6468 162.33 79.7767 57.98 107.0919 94.67 80.6497 162.66 0.0000 59.27 116. 9610 94.87 80.6790 163.33 81.0510 59.32 116.9755 97.43 105.5757 165.86 73.8410 59.54 117.0384 98.43 76.9175 176.31 94.2609 60'. 96 113.4834 98.44 76.9191 176.60 0.0000 61.17 114.8610 99.53 74.9251 177.52 93.1999 62.93 114.3490 100 .11 70.7146 181.07 0.0000 63.29 114. 4455 102.03 77.3992 181.52 89.6317 63.58 114.5236 103.18 80.7827 184.41 83.5045 64.28 121. 0283 103.37 80.8084 143.76 91.6706 66.73 120.3735 105.21 71. 3330 193.51 69.3522 67.24 135.5768 105.31 71. 3446 197.03 81.8331 125.81 126.6643 106.12 85.5130 198.01 62.3570 67.75 126.6835 106.47 93.1446 201.83 65.0693 69.67 125.2081 109.28 81.6084 203.43 82.3974 70.83 137.6747 111. 00 80.7455 205.31 59.1482 72.81 116. 9153 111.76 0.0000 210.85 69.4061 72. 87 116. 9302 114.06 71. 2740 63.5212 74.66 117.3768 116. 30 0.0000 222 .11 70.2034 74.82 117.4163 116.74 67.1711 227.09 65.5102 74.97 117.4532 119.76 70.8052 227.38 59.2276 77 .11 117.9778 121.12 75.3872 228.16 0.0000 78.74 126.2642 121. 22 78. 7250 228.18 60.5354 79.69 89.3810 121. 78 81. 0117 116.74 60.5354 80.12 99.0923 122.06 77.7155 235.69 71.1382 80.19 0.0000 122.92 77.8165 235.96 67.3450 80.57 99.1816 123.07 68.9388 238.63 73.8850 81. 00 103.4035 265.00 62.3245 238.98 0.0000 81. 07 98.2471 125.81 80.3870 240.99 102.1375 81. 75 115.9854 127.23 70.4862 242.00 46.0052 83.79 109.5202 127.91 70. 5571 244.70 49.9646 84.00 109.5652 129.30 77.8075 252.40 0.0000 85.43 125.1682 131.20 76.5228 252.80 55.9301 86.55 133.7998 133.02 83.4928 254.15 0.0000 86.79 145.0164 133.52 72.2607 256.23 57.8293 86.94 145.0577 136.00 73.6487 260.90 0.0000 Page 3844 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 54.7853 355.39 0.0000 584.27 20.2463 264.80 53.0523 356.01 43.4348 595.83 0.0000 265.00 53.0623 364.49 0.0000 427.87 26.8483 268.22 45.7965 366.42 0.0000 602.52 0.0000 269.46 47.1555 372.51 30.2337 604. 72 40.3503 270.03 47.1786 375.05 40. 6966 607.14 22.6218 271.23 47.2269 377.52 35.0759 609.32 28.0365 273.65 0.0000 356.01 39.0331 610.33 28.0492 276.40 57.0998 388.16 37.2354 614.28 14.5909 277.37 43.9585 388.63 0.0000 618.01 25.9844 277.60 43. 9677 391.69 30.6230 620.36 23.8441 278.00 51.0190 264.66 42.3520 621.93 31.4544 279.20 58 .1152 401. 81 38.5303 630.19 0.0000 279.54 59.0135 402.40 35.6541 631.29 20.6954 279.70 58.1394 404.85 39.5711 633.25 20.7140 280.46 55.5326 410.95 40.6935 634.78 0.0000 283.69 45.0764 413.71 39.7938 635.95 22.9226 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 52.2228 423.72 0.0000 645.85 13.1567 285.90 0.0000 427.09 38.1677 657.76 21.4924 287.50 47.8795 427.87 27.4155 657.90 0.0000 290.67 51. 2039 433.94 37.3452 661. 66 23.1849 293.27 0.0000 439.40 31.5521 664.57 0.0000 351. 93 45.5049 '453.88 24.8622 666.33 0 .'0000 295. 96 45.5329 463.37 32.9993 666.50 0.0000 879.38 34.8923 468.07 33.0886 667. 71 0.0000 299.98 44.3367 473.00 0.0000 677.62 21.1222 300.09 44.3397 475.06 35.2336 685.70 0.0000 300.13 44.3417 476.78 26.1989 695.00 0.0000 301.36 41.6950 477.60 25.2029 696. 49 24.6542 302.85 43.0908 482.18 18.1930 696. 51 28.0162 256.23 39.1024 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 36.9934 306.78 54.0320 497.08 22.4194 697.49 36.9961 308.46 35.1668 505.52 27. 6411 702.65 31. 4590 311.90 47.9191 507.63 0.0000 706.68 19.1319 316.51 45.3674 511. 00 30.8029 711. 68 20.2991 319.41 0.0000 514.00 32.3947 720.70 0.0000 320.08 0.0000 514.00 32.3947 721.93 0.0000 321. 04 41. 8831 520.40 25.7975 722.78 23.7908 323.87 49.2726 520.69 0.0000 722. 91 23.7916 325.23 28.7718 522.65 0.0000 723.31 18. 6968 328.76 0.0000 527.90 0.0000 724.19 18.7035 333.37 35.8397 528.26 25.9033 727. 33 23.8344 333.97 31. 7184 529.59 23.8479 733.00 17.0636 334.37 40.0042 529.87 0.0000 735.93 26.1951 338.28 43.3473 531. 02 0.0000 333.97 13.6753 338.32 43.3482 537.26 0.0000 739.50 0.0000 311. 90 40.1839 546.56 0.0000 747.24 25.7419 340.48 40.1839 552.55 26.2278 748.06 20.6001 340.55 0.0000 563.25 16.8757 752.31 21. 7809 344.28 42.6103 569.33 31.7371 753.82 0.0000 345.93 34.4996 946.00 31. 7395 756.73 20.6704 351.06 32.5782 569.70 31. 7419 756.80 20. 6711 351.93 32.5989 583.19 20.2362 884.68 19.5774 Page 3845 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 32.2679 1274.44 18.7335 1620.50 3.2950 766.42 27.6650 1001.03 13 .1331 1621. 92 8.7896 766.84 25.3641 1002.74 18.7720 1678.03 0.0000 772.60 0.0000 1004.73 15. 9660 1690.97 4.4578 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 d764.49 3.6189 778.90 25.4823 1028.54 0.0000 1063.66 15.3979 783.70 0.0000 1037.84 26.5662 1771.35 3.3973 785.37 17.4170 1038.76 0.0000 1791.20 0.0000 792.07 18.6257 631. 2 9 23.7839 1808.65 3.6500 794.95 13.9844 1048.07 0.0000 1810.72 0.0000 795.86 16.3208 1049.04 12.3763 1836.06 2.7519 810.06 19.3380 1050.41 19.0491 810.29 19.3393 1063.66 13.3873 344.28 19.3406 1077.00 0.0000 810.76 18.4634 1077.34 13.4412 815.77 0.0000 1085.87 12.5128 1048.07 0.0000 1093.63 13.5061 832.01 26.5833 1099.45 22.2251 834.85 18.6275 1112. 07 10.6683 835.71 23.9571 1112.84 12. 6112 836.80 0.0000 1115. 54 12.4266 846.75 0.0000 1120.29 13.6104 846.77 15.6788 112'0. 55 13. 6112 856.80 0.0000 1221.41 12. 9655 860.56 14.3237 1129. 67 18.7148 871.09 17.0726 1131.51 0.0000 873.19 17.4708 1147.95 0.0000 875.33 0.0000 1173.23 7.8936 879.38 17.1225 1177.95 11. 0653 880.51 17.1289 1189.05 17.4410 883.24 14.4380 1204.77 21. 8939 884.68 10.8340 1221. 41 12.9952 889.28 15.3725 1231.02 22.4492 894.76 15.4016 1235.36 0.0000 898.04 15.4187 1238.28 19.0777 900. 72 15.4332 1260.41 0.0000 903.28 14.5381 1271. 87 11.1423 911.20 16.3993 1274.44 8.1089 912.08 16.4042 1274.54 6.4871 923.98 0.0000 1291.59 14.6602 926.50 21. 9785 1298.22 0.0000 929 .11 17.5980 1312 .11 0.0000 937.49 20.2202 1332.49 7.2000 944 .13 0.0000 1362.66 0.0000 946.00 21.1989 1365.19 3.3180 949.00 15.6838 1368.63 0.0000 667.71 0.0000 1384.29 6.2498 962. 31 21.3119 1408.01 5.2377 964.08 17.8008 1457.56 0.0000 966 .17 26.7196 1460.82 6. 3629 911.20 18. 5718 1489.16 8.5391 968.97 18.5718 1505.03 10.7117 983.53 0.0000 1584.12 9.8091 984.45 0.0000 1596.21 0.0000 Page 3846 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:26:31.23 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621356.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM06.CNF;499 Background date : Z-OCT-2016 11:00:12. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 09:11:02. Sample ID G1203621356 Sample quantity 1.15000E+02 GRAM Detector name : GAM06 Detector geometry: CAN Elapsed live time: 0 00:15:00.00 Elapsed real time: 0 00:15:04.89 0.5% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596249 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 0 9 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 37.09 45.10 46.51* 51. 85 59.50 88.00 122.28 164.58 167. 41 225.90 284.90 385.80 661. 30 739.32 891. 33 996. 25 1086.07 1115. 01 1162. 31 1172.54 1331. 69 1351.56 1398.56 1484.54 1548.58 1585.08 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 94 450 5038 142 14909 2482 298 98 39 80 66 72 11854 61 42 42 81 167 49 7487 6682 22 11 7 15 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 2568 2604 2670 2206 3321 1352 865 639 491 770 474 471 494 264 198 227 406 346 105 330 73 9 10 15 7 6 1. 24 1. 83 0.92 1. 45 0.98 1. 01 1. 02 1. 37 1. 38 1. 51 1. 57 1. 33 1. 46 4.33 0.73 1. 32 6.36 4.31 1. 81 1. 92 2 .13 2.31 0.88 1.16 2.25 0.59 73.94 89.95 92.76 103.43 118. 71 175.67 244.18 328. 71 334.36 451.26 569.18 770.85 1321.61 1477.62 1781.56 1991. 39 2171.03 2228.91 2323.52 2343.98 2662.34 2702.08 2796.11 2968.13 3096.27 3169.29 72 87 87 102 114 171 240 325 333 448 567 767 1316 1472 1779 1987 2164 2221 2321 2334 2653 2696 2791 2960 3087 3160 5 1.04E-01 81.9 10 5.00E-01 17.4 10 5.60E+OO 2.2 5 1. 58E-01 50. 2 11 1.66E+Ol 1.1 10 2.76E+OO 3.4 9 3.31E-01 18.8 8 1.09E-01 46.0 6 4.30E-02 91.6 8 8. 91E-02 61. 0 7 7.33E-02 55.8 8 7.99E-02 53.6 14 1. 32E+Ol 1. 0 11 6.81E-02 53.1 6 4.64E-02 55.6 8 4.62E-02 64.9 17 9.05E-02 57.9 15 1. 85E-01 25. 6 9 5.48E-02 39.6 20 8. 32E+OO 1. 3 18 7. 42E+OO 1. 3 12 2.47E-02 34.2 10 1.19E-02 71. 4 10 7.27E-03123.9 14 1. 67E-02 45. 5 12 7.78E-03 79.5 Flag: "*" = Peak area was modified by background subtraction Page 3847of5809 Fit 1.64E+OO

. VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 09:26:33 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621356.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621356 SOLID GAMMA6 0 00:15:00.00 1. 50 keV No Empirical 75.00 Acquisition date : Sample quantity geometry Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 09:11:02 115. 00 GRAM CAN 0 00:15:04.89 10.00 0.00 % Peak Energy 0.5% No interference correction performed Page 3848 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : G1203621356 Acquisition date 3-0CT-2016 09:11:02 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06

  • 312 85.60* 6.177E+OO 1.540E+OO 1.621E+OO 37.61 136.47 ------10.68 6.083E+OO ------Line Not Found ------C0-60 1173.23 7132 99.85 1.227E+OO 1.520E+02 l.532E+02 2.60 1332.49 6329 99.98* l.092E+OO l.514E+02 l.526E+02 2.52 ZN-65 1115. 54 159 50.60* 1. 285E+OO 6.384E+OO 6.784E+OO 51. 23 CD-109 88.03 2636 3.70* 5.253E+OO 3.541E+02 3.657E+02 6. 86 SN-126 64.28 ------9.60 2.772E+OO ------Line Not Found ------86. 94 2636 8.90 5.253E+OO 1. 472E+02 1. 472E+02 6.86 87.57 2636 37.00* 5.253E+OO 3.541E+Ol 3.541E+Ol 6.86 BA-137M 661.66 11577 89.90* 2.028E+OO 1.658E+02 l.660E+02 2.00 CS-137 661. 66 11577 85.10* 2.028E+OO 1. 751E+02 1. 754E+02 2.00 CE-139 165.86 101 80.00* 5.647E+OO 5.856E-01 6.522E-01 91. 98 PM-147 121. 22 312 0.00* 6.177E+OO 4.626E+04 4.698E+04 37.61 PM-149 285.90 67 3.10* 3.879E+OO 1.450E+Ol l.181E+04 111. 62 TM-171 51. 35 154 0.27 1.156E+OO 1.290E+03 l.318E+03 100.40 52.39 154 0.47* 1.156E+OO 7.413E+02 7. 572E+02 100.40 66.73 ------0.14 3.097E+OO ------Line Not Found ------PB-210 46.54 5485 4.25* 6.176E-01 5.456E+03 5.466E+03 4.39 AM-241 59.54 16078 35.90* 2.126E+OO 5.502E+02 5.503E+02 2.27 Flag: "*" Key line Page 3849 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:26:34.13 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621356.CNF;l * *Acquisition date 3-0CT-2016 09:11:02 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:04.89 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
  • Sample ID G1203621356 Sample Quantity l.1500E+02 GRAM *
  • Batch Number 1596249 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;14 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) C0-57 1. 627E+OO 5. 996E-01 C0-60 1.526E+02 3.766E+OO ZN-65 6.784E+OO 3.406E+OO CD-109 3.657E+02 2.458E+Ol SN-126 3.541E+Ol 2.380E+OO BA-137M 1.660E+02 3.261E+OO CS-137 1. 754E+02 3.445E+OO CE-139 6.522E-01 5.879E-01 PM-147 4.698E+04 1.732E+04 PM-149 1.181E+04 1.292E+04 TM-171 7.572E+02 7.450E+02 PB-210 5.466E+03 2.349E+02 AM-241 5.503E+02 1.222E+Ol Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 Page 3850 of 5809 Key-Line Activity (pCi/GRAM -1.900E+00 1.218E-01 O.OOOE+OO 1. 818E-01 2.569E-01 8.129E-01 -3. 611E-01 7.870E+OO 2.281E-01 -7.242E-01 O.OOOE+OO -3.445E-01 -1.166E+00 2.860E+OO -2.lOOE+Ol -1.482E+OO 4. 911E-01 K.L. Cnt Uncert ( 1 . 96-sigma ) 6.816E+OO 4.037E-01 4. 969E+09 2.534E-01 2.569E-tOO 9.793E-01 l.899E+OO 6.403E+OO 6.938E-01 8.545E-01 1.170E+41 8.146E-01 2.025E+OO 2.610E+Ol 2.669E+Ol 1.940E+OO 6.981E-01 MDA (pCi/GRAM 5.200E-01 7.581E-01 2.990E+00 1. 573E+Ol 1.532E+00 l.030E+00 1.088E+OO 5.730E-01 1. 501E+04 1.770E+04 9. 011E+02 1.949E+02 5.831E+OO MDA (pCi/GRAM 1.190E+Ol 7.655E-01 O.OOOE+OO 5.666E-01 5.087E+OO l.540E+OO 3.376E+OO l.208E+Ol 1.195E+OO 1.385E+OO 0.000E+OO 1.355E+OO 3.508E+OO 4.665E+Ol 4.415E+Ol 3.269E+OO 1.193E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN BR-77 l.824E+02 7.495E+02 l.270E+03 NOT IDENT. SR-82 1.460E-01 6.875E+OO 1.178E+Ol NOT IDENT. RB-83 6.953E-01 1.238E+OO 2. 231E+OO NOT IDENT. KR-85 -4.998E+Ol l.071E+02 1.852E+02 NOT IDENT. SR-85 -2.829E-01 6.060E-01 1.048E+OO NOT IDENT. RB-86 5.068E+OO 2.0lOE+Ol 3.617E+Ol NOT IDENT. Y-88 1.861E-01 3.lOlE-01 6.718E-01 NOT IDENT. Y-91 -l.102E+02 2.525E+02 4.423E+02 NOT IDENT. NB-94 1.422E-02 5.048E-01 8.744E-01 NOT IDENT. NB-9.5 1.5.02E-01 7.252E-01 l .255E+OO NOT IDENT. NB-95M 1. 07 5E+OO 1. 742E+OO 2.986E+OO NOT IDENT. ZR-95 -5.329E-01 1.334E+OO 2.239E+OO NOT IDENT. NB-97 O.OOOE+OO 5.816E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.203E+10 O.OOOE+OO SHORT HLIF M0-99 1.529E+03 1.590E+03 1. 722E+03 FAIL ABUN TC-99M O.OOOE+OO 1. 311E+25 O.OOOE+OO SHORT HLIF RH-101 -5. 671E-02 3.599E-01 6.257E-01 NOT IDENT. RH-102 -5.007E-02 8.620E-01 l.498E+OO NOT IDENT. RU-103 6 .113E-01 7.813E-01 1.418E+OO NOT IDENT. RH-106 -1.772E+OO 5.129E+OO 8.791E+00 NOT IDENT. RU-106 -1. 772E+OO 5.129E+OO 8.791E+OO NOT IDENT. AG-108M 1.015E-01 5. 671E-01 1. OllE+OO NOT IDENT. AG-llOM -2.468E-01 1.090E+OO 1.813E+OO NOT IDENT. SN-113 4.319E-01 7.584E-01 1.384E+OO NOT IDENT. CD-115 4.932E+02 1. 318E+03 2.356E+03 NOT IDENT. SN-ll 7M 6.257E-01 8.749E-01 1. 54 7E+OO NOT IDENT. TE-123M 1.149E-01 3.439E-01 6.00lE-01 NOT IDENT. SB-124 -8.329E-OI 7.390E-01 1.073E+OO NOT IDENT. SB-125 -9.187E-01 1.645E+OO 2. 871E+OO NOT IDENT. TE-125M 6.992E+Ol 1.17 9E+02 2 .118E+02 NOT IDENT. I-126 -3.153E-01 5.416E+OO 8. 351E+OO NOT IDENT. SB-126 1.420E+OO 3.273E+OO 5.766E+OO NOT IDENT. SB-127 -4.207E+Ol 6.444E+Ol l.078E+02 NOT IDENT. I-131 -3.580E-01 3.103E+OO 5.574E+OO FAIL ABUN I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 1.188E+Ol 4.376E+Ol 6.845E+Ol NOT IDENT. BA-133 -l.834E-01 6. 572E-01 1.175E+OO NOT IDENT. I-133 O.OOOE+OO l.446E+07 0.000E+OO SHORT HLIF CS-134 -l.346E-01 7.171E-01 1.212E+OO NOT IDENT. CS-135 3.058E-01 2.324E+OO 3.880E+OO NOT IDENT. I-135 O.OOOE+OO 4.270E+23 O.OOOE+OO SHORT HLIF CS-136 -1.037E-01 3.030E+OO 5.394E+OO NOT IDENT. BA-140 2.364E+OO 6.151E+OO 1.099E+Ol NOT IDENT. LA-140 2.730E-01 9.107E-01 1. 847E+OO NOT IDENT. CE-141 -5.769E-01 8.028E-01 l.357E+OO NOT IDENT. CE-143 0.000E+OO 4.336E+04 O.OOOE+OO SHORT HLIF CE-144 1.140E+OO 2.299E+OO 4.074E+OO NOT IDENT. PM-144 -5.622E-02 5.315E-01 9.145E-01 NOT IDENT. PR-144 -4.644E+OO 3.989E+Ol 6.859E+Ol NOT IDENT. PM-146 -5.729E-01 8.390E-01 1. 451E+OO NOT IDENT. ND-147 -9.134E-01 1. 371E+Ol 2.407E+Ol NOT IDENT. EU-150 -1.768E-01 3.984E-01 7 .119E-01 NOT IDENT. EU-152 -2.253E-01 1.440E+OO 2.593E+OO FAIL ABUN GD-153 -4.815E-01 9.736E-01 1. 700E+OO NOT IDENT. EU-154 3.175E-01 1.137E+OO 2.153E+OO FAIL ABUN EU-155 2.236E-01 l.233E+OO 2.189E+OO FAIL ABUN TB-160 9.867E-01 2.934E+OO 5.021E+OO FAIL ABUN H0-166M 7.945E-01 9.576E-01 1.723E+OO NOT IDENT. HF-172 2.123E+OO 2.339E+OO 3.926E+OO FAIL ABUN LU-172 -3. 481E-01 1. 541E+OO 2.379E+OO FAIL ABUN LU-176 -9.479E-02 3.846E-01 6.956E-01 FAIL ABUN HF-181 -2.714E-01 9.176E-01 1.601E+OO NOT IDENT. TA-182 -1. lOlE+OO 1. 741E+OO 3.0lOE+OO NOT IDENT. RE-183 O.OOOE+OO 5.916E+00 1.229E+Ol FAIL ABUN RE-184 9.017E-01 3.102E+OO 5. 271E+OO NOT IDENT. W-188 -8.10'.3E+Ol 1. l 77E+02 l.888E+02 FAIL ABUN IR-192 -3.332E-01 5.418E-01 9.665E-01 NOT IDENT. HG-203 -l.094E-01 6.467E-01 1.063E+OO NOT IDENT. BI-207 -3.845E-01 l.022E+OO 1. 793E+OO NOT IDENT. TL-208 -1.255E-Ol 5.507E-01 9.552E-01 NOT IDENT. BI-211 2.417E+OO 3.053E+OO 5.656E+OO NOT IDENT. PB-211 2.617E+OO 1.173E+Ol 2.112E+Ol NOT IDENT. BI-212 3.240E+OO 8.152E+OO 1. 431E+Ol NOT IDENT. PB-212 l.849E-01 7.737E-01 1. 311E+OO NOT IDENT. BI-214 -3.655E-01 1.097E+OO 1.887E+OO NOT IDENT. PB-214 8.612E-01 1. lllE+OO 2.057E+OO FAIL ABUN RN-219 -9.777E-01 6.652E+OO 1.184E+Ol NOT IDENT. RN-222 -3.655E-01 1.097E+OO 1.887E+OO NOT IDENT. Page 3851of5809 RA-223 6.770E+OO 9.522E+OO 1. 766E+Ol NOT IDENT. RA-224 -4.861E+OO 8.388E+OO l.374E+Ol NOT IDENT. RA-226 -3.655E-01 l.097E+OO l.887E+00 NOT IDENT. AC-227 2.578E-02 3.693E+OO 6.160E+OO NOT IDENT. TH-227 2.578E-02 3.693E+OO 6.160E+OO NOT IDENT. AC-228 l.598E+00 3.237E+OO 5.530E+OO NOT IDENT. RA-228 l.598E+OO 3.237E+OO 5.530E+OO NOT IDENT. TH-228 l.849E-01 7.737E-01 1. 311E+OO NOT IDENT. TH-229 2.881E-01 6.823E+OO l.161E+Ol FAIL ABUN -3.655E-01 l.097E+OO 1.88.;?E+OO NOT IDENT. PA-231 -l.169E+OO 6.678E+OO l.212E+Ol FAIL ABUN TH-231 6.770E+OO 9.522E+OO 1. 766E+Ol NOT IDENT. TH-232 l.598E+OO 3.237E+OO 5.530E+OO NOT IDENT. PA-233 4.085E-01 9.866E-01 l.816E+OO NOT IDENT. PA-234 -3.750E+OO 7.176E+OO l.260E+Ol NOT IDENT. PA-234M 4.808E+Ol 9.825E+Ol 1. 672E+02 NOT IDENT. TH-234 -3.161E+OO 1.747E+Ol 2.925E+Ol NOT IDENT. U-234 -3.655E-01 l.097E+OO l.887E+OO NOT IDENT. U-235 4.519E-02 2.294E+OO 3.983E+OO FAIL ABUN NP-237 4.085E-01 9.866E-01 l.816E+OO NOT IDENT. NP-238 O.OOOE+OO 3.252E+03 O.OOOE+OO SHORT HLIF U-238 -3.161E+OO 1. 747E+Ol 2.925E+Ol NOT IDENT. NP-239 4.003E+OO 3.145E+OO 5.739E+00 NOT IDENT. PU-239 -7.410E+02 3.782E+03 6.563E+03 NOT IDENT. AM-243 8.737E-02 6.262E-01 l.127E+OO NOT IDENT. CM-243 7.468E-01 1.220E+OO 2.198E+OO NOT IDENT. BK-247 7.513E-01 1.215E+OO 2.069E+OO FAIL ABUN CM-247 -l.226E-01 6.205E-01 l.102E+OO NOT IDENT. CF-249 -5.793E-02 6.933E-01 l .115E+OO NOT IDENT. CF-251 6.516E-01 l.500E+OO 2. 613E+OO FAIL ABUN ANH-511 6.898E-03 4.657E-01 8.338E-01 NOT IDENT. Page 3852 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 09:26:32.25 Nuclide Line Activity Report Nuclide Type:
  • Nuclide Uncorrected Decay Corr 2-Sigrna Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 312 85.60* 6.177E+OO 1.540E+00 1. 627E+OO 37.61 136.47 ------10.68 6.083E+OO ------Line Not Found ------C0-60 1173.23 7132 99.85 1.227E+OO 1.520E+02 1.532E+02 2.60 1332.49 6329 99.98* 1.092E+OO 1.514E+02 1.526E+02 2.52 ZN-65 1115.54 159 50.60* 1.285E+OO 6.384E+OO 6.784E+OO 51. 23 CD-109 88.03 2636 3.70* 5.253E+OO 3.541E+o2 3.657E+02 6. 86 SN-126 64.28 ------9.60 2.772E+OO ------Line Not Found ------86.94 2636 8.90 5.253E+OO 1. 472E+02 1.472E+02 6. 86 87.57 2636 37.00* 5.253E+OO 3.541E+Ol 3.541E+Ol 6.86 BA-137M 661.66 11577 89.90* 2.028E+OO 1.658E+o2 1.660E+02 2.00 CS-137 661.66 11577 85.10* 2.028E+OO 1. 751E+02 1. 754E+02 2.00 CE-139 165.86 101 80.00* 5.647E+OO 5.856E-01 6.522E-01 91. 98 PM-147 121.22 312 0.00* 6.177E+OO 4.626E+04 4.698E+04 37.61 PM-149 285.90 67 3.10* 3.879E+OO 1.450E+Ol 1.181E+04 111. 62 TM-171 51. 35 154 0.27 1.156E+OO 1. 290E+03 1.318E+03 100.40 52.39 154 0.47* 1.156E+OO 7.413E+02 7.572E+02 100.40 66. 73 ------0.14 3.097E+OO ------Line Not Found ------PB-210 46.54 5485 4.25* 6.176E-01 5.456E+03 5.466E+03 4.39 AM-241 59.54 16078 35.90* 2.126E+OO 5.502E+02 5.503E+02 2.27 Flag: "*" Key line .. Page 3853 of 5809 Summary of Nuclide Activity Sample ID : Gl203621356 Acquisition date Page : 2 3-0CT-2016 09:11:02 Total number of lines in spectrum 26 Number of unidentified lines 9 Number of lines tentatively identified by NID 17 Nuclide Type : Nuclide C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M CS-137 CE-139 PM-147 PM-149 TM-171 PB-210 AM-241 Hlife 271. 74D 5.27Y 244.06D 461. 40D 2.30E+05Y 30.08Y 30.08Y 137.64D 2.62Y 53.08H 1.92Y 22.20Y 432.60Y Decay 1. 06 1. 01 1. 06 1. 03 1. 00 1. 00 1. 00 1.11 1. 02 815. 1. 02 1. 00 1. 00 Total Activity Grand Total Activity c Uncorrected Decay Corr pCi/GRAM pCi/GRAM 1.540E+OO 1.627E+OO 1.514E+02 1.526E+02 6.384E+OO 6.784E+OO 3.541E+02 3.657E+02 3. 541E+Ol 3.541E+Ol 1.658E+02 1.660E+02 1. 751E+02 1. 754E+02 5.856E-01 6.522E-01 4.626E+04 4.698E+04 1.450E+Ol l.181E+04 7.413E+02 7. 572E+02 5.456E+03 5.466E+03 5.502E+02 5.503E+02 ------------------5.392E+04 6.648E+04 5.392E+04 6.648E+04 65.38% Decay Corr 2-Sigma 2-Sigma Error %Error 0.612E+OO 37.61 0.038E+02 2.52 3.476E+OO 51. 23 0.251E+02 6.86 0.243E+Ol 6.86 *0.033E+02 2.00 0.035E+02 2.00 5.999E-01 91. 98 1. 767E+04 37.61 1.319E+04 111. 62 7.602E+02 100.40 0.240E+03 4.39 0.125E+02 2.27 Flags: "K" Keyline not found "E" = Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Page 3854of5809 Flags Unidentified Energy Lines Page : 3 Sample ID : Gl203621356 Acquisition date : 3-0CT-2016 09:11:02 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 37.09 103 2821 1.24 73.94 72 5 l.04E-01 **** 1. OlE-01 9 45.10 491 2838 1. 83 89.95 87 10 5.00E-01 34.9 5.04E-01 T 0 167.41 40 508 1. 38 334.36 333 6 4.30E-02 **** 5.60E+OO 0 225.90
  • 82 787 1. 51 451.26 448 8 8.91E-02 **** 4. 61E+OO T 0 385.80 72 471 1. 33 770.85 767 8 7.99E-02 **** 3.08E+OO 0 739.32 60 256 4.33 1477.62 1472 11 6.81E-02 **** 1. 85E+OO T 0 891.33 40 191 0.73 1781.56 1779 6 4.64E-02 **** l.57E+OO 0 996.25 40 218 1. 32 1991.39 1987 8 4.62E-02 **** l.42E+OO T 0 1086.07 78 388 6.36 2171.03 2164 17 9.05E-02 **** l.32E+OO T 0 1162.31 47 100 1. 81 2323.52 2321 9 5.48E-02 79.3 1.24E+OO 0 1351.56 21 8 2.31 2702.08 2696 12 2.47E-02 68.5 l.08E+OO 0 1398.56 10 10 0.88 2796.11 2791 10 l.19E-02 **** 1. 04E+OO 0 1484.54 6 15 1.16 2968.13 2960 10 7.27E-03 **** 9.90E-01 0 1548.58 14 7 2.25 3096.27 3087 14 l.67E-02 90.9 9.55E-01 0 1585.08 7 6 0.59 3169.29 3160 12 7.78E-03 **** 9.36E-01 T Flags: "T" = Tentatively associated Page 3855 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:26:46.69 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621356.CNF;l * *Acquisition date 3-0CT-2016 09:11:02 Sensitivity 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00, Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:04.89 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621356 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.1500E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M CS-137 CE-139 PM-147 PM-149 TM-171 PB-210 AM-241 Le (pCi/GRAM 2.530E-01 3.467E-01 1.438E+OO 7.678E+OO 7.477E-01 4.959E-01 5.239E-01 2.778E-01 7.302E+03 8.612E+03 4.443E+02 9.613E+Ol 2.870E+OO ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 BR-77 Page 3856 of 5809 Le (pCi/GRAM 5.782E+OO 3.514E-01 0.000E+OO 2.417E-01 2.216E+OO 7.435E-01 1.627E+OO 5.869E+OO 5.754E-01 6.668E-01 O.OOOE+OO 6.523E-01 l.688E+OO 2.247E+Ol 2.177E+Ol 1.573E+OO 5.800E-01 6.175E+02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.

SR-82 5.653E+OO NOT IDENT. RB-83 1. 078E+OO NOT IDENT. KR-85 8.933E+Ol NOT IDENT. SR-85 5.056E-01 NOT IDENT. RB-86 1. 741E+Ol NOT IDENT. Y-88 2.873E-01 NOT IDENT. Y-91 2.066E+02 NOT IDENT. NB-94 4.190E-01 NOT IDENT. NB-95 6.029E-01 NOT IDENT. ... NB-95M 1. 453E+OO. NOT IDENT . ZR-95 1. 075E+OO NOT IDENT. NB-97 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO SHORT HLIF M0-99 8.266E+02 FAIL ABUN TC-99M O.OOOE+OO SHORT HLIF RH-101 3.043E-01 NOT IDENT. RH-102 7.191E-01 NOT IDENT. RU-103 6.869E-01 NOT IDENT. RH-106 4.223E+OO NOT IDENT. RU-106 4.223E+OO NOT IDENT. AG-108M 4.921E-01 NOT IDENT. AG-llOM 8.742E-01 NOT IDENT. SN-113 6. 721E-01 NOT IDENT. CD-115 1.137E+03 NOT IDENT. SN-117M 7.525E-01 NOT IDENT. TE-123M 2.918E-01 NOT IDENT. SB-124 4.303E-01 NOT IDENT. SB-125 1.394E+OO NOT IDENT. TE-125M 1. 031E+02 NOT IDENT. I-126 4.009E+OO NOT IDENT. SB-126 2.769E+OO NOT IDENT. SB-127 5.163E+Ol NOT IDENT. I-131 2.702E+OO FAIL ABUN I-132 O.OOOE+OO SHORT HLIF TE-132 3.333E+Ol NOT IDENT. BA-133 5.702E-01 NOT IDENT. I-133 O.OOOE+OO SHORT HLIF CS-134 5.818E-01 NOT IDENT. CS-135 1.886E+OO NOT IDENT. I-135 O.OOOE+OO SHORT HLIF CS-136 2.598E+OO NOT IDENT. BA-140 5.305E+OO NOT IDENT. LA-140 7.970E-01 NOT IDENT. CE-141 6.590E-01 NOT IDENT. CE-143 O.OOOE+OO SHORT HLIF CE-144 l.982E+OO NOT IDENT. PM-144 4.384E-01 NOT IDENT. PR-144 3.288E+Ol NOT IDENT. PM-146 7.056E-01 NOT IDENT. ND-147 1.161E+Ol NOT IDENT. EU-150 3.453E-01 NOT IDENT. EU-152 1.257E+OO FAIL ABUN

  • GD-153 8.274E-01 NOT IDENT. EU-154 9.877E-01 FAIL ABUN EU-155 1. 066E+OO FAIL ABUN TB-160 2. 421E+OO FAIL ABUN H0-166M 8.276E-01 NOT IDENT. HF-172 1. 911E+OO FAIL ABUN LU-172 1.146E+OO FAIL ABUN LU-176 3.376E-01 FAIL ABUN HF-181 7.769E-01 NOT IDENT. TA-182 1.380E+OO NOT IDENT. RE-183 6.083E+OO FAIL ABUN RE-184 2.546E+OO NOT IDENT. W-188 9.159E+Ol FAIL ABUN IR-192 4.687E-01 NOT IDENT. HG-203 5.167E-01 NOT IDENT. BI-207 8.616E-01 NOT IDENT. TL-208 4.592E-01 NOT IDENT. BI-211 2.746E+OO NOT IDENT. PB-211 1.025E+Ol NOT IDENT. BI-212 6.876E+OO NOT IDENT. PB-212 6.374E-01 NOT IDENT. BI-214 9.082E-01 NOT IDENT. PB-214 9.989E-01 FAIL ABUN RN-219 5.744E+OO NOT IDENT. RN-222 9.082E-01 NOT IDENT. RA-223 8.583E+OO NOT I DENT .. Page 3857of5809 RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 .PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 3858 of 5809 6.673E+00 9.082E-01 2.992E+OO 2.992E+OO 2.677E+OO 2.677E+OO 6.374E-01 5.651E+OO 9.082E-01 5.884E+OO 8.583E+OO 2.677E+OO 8.831E-01 6.106E+OO 8.070E+Ol l.426E+Ol 9.082E-01 1.938E+OO 8.831E-01 O.OOOE+OO 1.426E+Ol 2.797E+OO 3.190E+03 5.507E-01 1. 070E+OO 1.006E+OO 5.348E-01 5.404E-01 1. 269E+OO 4.028E-01 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 09:26:52.45 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 , * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621356.CNF;l *
  • Acquisition date 3-0CT-2016 09:11:02 Sensitivity 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:04.89 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID' *
  • Sample ID Gl203621356 Analyst initials: MXRl *
  • Batch Number 1596249 Sample Quantity : 1.1500E+02 GRAM *
  • Quantity Err(%) : 1.7391E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * * '* Eff. Cal. date 8-MAR-2016 07:26:53 E'ff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) C0-57 1.627E+OO 6. llOE-01 6.llOE-01 C0-60 l.526E+02 1. 245E+Ol 1.245E+Ol ZN-65 6.784E+OO 3.615E+OO 3.615E+OO CD-109 3.657E+02 4.352E+Ol 4.352E+Ol SN-126 3.541E+Ol 3.774E+OO 3.774E+00 BA-137M 1. 660E+02 1.409E+Ol 1.409E+Ol CS-137 1. 754E+02 1.488E+Ol 1.488E+Ol CE-139 6.522E-01 6.035E-01 6.035E-01 PM-147 4.698E+04 1. 7 65E+04 1. 765E+04 PM-149 1.181E+04 l.306E+04 1.306E+04 TM-171 7.572E+02 7.483E+02 7.483E+02 PB-210 5.466E+03 5.253E+02 5.253E+02 AM-241 5.503E+02 4.434E+Ol 4.434E+Ol Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.900E+OO 6.818E+OO 6.872E+OO NOT IDENT. NA-22 1. 218E-01 4.038E-01 4.075E-01 NOT IDENT. NA-24 -5.212E+08 4.970E+09 4.975E+09 SHORT HLIF AL-26 1.818E-01 2.538E-01 2.667E-01 NOT IDENT. K-40 2.569E-01 2.569E+OO 2. 572E+OO NOT IDENT. SC-46 8.129E-01 9.843E-01 1.050E+OO NOT IDENT. V-48 -3.611E-01 1.900E+OO 1.907E+OO NOT IDENT. CR-51 7.870E+OO 6.445E+OO 7.357E+OO NOT IDENT. MN-54 2.281E-01 6.943E-01 7.018E-01 NOT IDENT. C0-56 -7.242E-01 8.585E-01 9.185E-01 NOT IDENT. MN-56 -l.OOOE+41 1.175E+41 O.OOOE+OO SHORT HLIF C0-58 -3.445E-01 8.155E-01 8.301E-01 NOT IDENT. FE-59 -l.166E+OO 2.037E+OO 2.103E+OO NOT IDENT. GE-68 2.860E+OO 2.610E+Ol 2.614E+Ol NOT IDENT. AS-73 -2.lOOE+Ol 2.704E+Ol 2.865E+Ol NOT IDENT. AS-74 -1.482E+OO 1. 946E+OO 2.058E+OO NOT IDENT. SE-75 4. 911E-01 6. 996E-01 7.338E-01 FAIL ABUN Page 3859 of 5809 BR-77 1.824E+02 7.581E+o2 7.625E+02 NOT IDENT. SR-82 l.460E-01 6.875E+00 6.876E+OO NOT IDENT. RB-83 6.953E-01 1.243E+00 l.282E+OO NOT IDENT. KR-85 -4.998E+Ol 1. 072E+02 l.095E+02 NOT IDENT. SR-85 -2.829E-01 6.065E-01 6.198E-01 NOT IDENT. RB-86 5.068E+OO 2.012E+Ol 2.025E+Ol NOT IDENT. Y-88 1. 8 61E-01 3.104E-01 3.215E-01 NOT IDENT. Y-91 -1.102E+02 2.527E+02 2.575E+02 NOT IDENT. NB-94 l.422E-02 5.048E-01 5.048E-01 NOT IDENT. NB-95 l.502E-01 7'.254E-01 7.285E-01 NOT IDENT. NB-95M l.075E+OO 1. 745E+OO 1.812E+OO NOT IDENT. ZR-95 -5.329E-01 1.335E+OO l.356E+OO NOT IDENT. NB-97 l.OOOE+41 5.875E+40 O.OOOE+OO SHORT HLIF ZR-97 2.497E+08 1.203E+10 l.203E+10 SHORT HLIF M0-99 l.529E+03 l.598E+03 1. 740E+03 FAIL ABUN TC-99M -8.303E+22 1.311E+25 O.OOOE+OO SHORT HLIF RH-101 -5. 671E-02 3.601E-01 3.610E-01 NOT IDENT. RH-102 -5.007E-02 8.620E-01 8.623E-01 NOT IDENT. RU-103 6 .113E-01 7.832E-01 8.303E-01 NOT IDENT. RH-106 -1.772E+OO 5.132E+OO 5.194E+OO NOT IDENT. RU-106 -1. 772E+OO 5.132E+OO 5.194E+OO NOT IDENT. AG-108M l.015E-01 5. 671E-01 5.690E-01 NOT IDENT. AG-llOM -2.468E-01 1.090E+OO 1. 096E+00 NOT IDENT. SN-113 4.319E-01 7.593E-01 7.838E-01 NOT IDENT. CD-115 4.932E+02 l.319E+03 l.337E+03 NOT IDENT. SN-ll 7M 6.257E-01 8.761E-01 9.203E-01 NOT IDENT. TE-123M l.149E-01 3.440E-01 3.479E-01 NOT IDENT. SB-124 -8.329E-01 7.417E-01 . 8. 314E-01 NOT IDENT. SB-125 -9.187E-01 1.647E+OO 1.698E+OO NOT IDENT. TE-125M 6.992E+Ol l.180E+o2 l.222E+02 NOT IDENT. I-126 -3.153E-01 5.416E+OO 5.418E+OO NOT IDENT. SB-126 l.420E+00 3.278E+OO 3.339E+OO NOT IDENT. SB-127 -4.207E+Ol 6.467E+Ol 6.740E+Ol NOT IDENT. I-131 -3.580E-01 3.104E+OO 3.108E+OO FAIL ABUN I-132 -1.000E+41 5.004E+41 O.OOOE+OO SHORT HLIF TE-132 1.188E+Ol 4.378E+Ol 4.410E+Ol NOT IDENT. BA-133 -l.834E-01 6.574E-01 6.626E-01 NOT IDENT. I-133 5.749E+06 1.449E+07 1. 472E+07 SHORT HLIF CS-134 -l.346E-01 7.173E-01 7.198E-01 NOT IDENT. CS-135 3.058E-01 2.325E+OO 2.329E+OO NOT IDENT. I-135 -l.860E+23 4.368E+23 O.OOOE+OO SHORT HLIF CS-136 -1.037E-01 3.030E+OO 3.030E+OO NOT IDENT. BA-140 2.364E+OO 6.155E+OO 6.246E+00 NOT IDENT. LA-140 2.730E-01 9. llOE-01 9.193E-01 NOT IDENT. CE-141 -5.769E-01 8.038E-01 8.448E-01 NOT IDENT. CE-143 -3 .131E+04 4.346E+04 4.570E+04 SHORT HLIF CE-144 1.140E+OO 2. 301E+OO 2.358E+OO NOT IDENT. PM-144 -5.622E-02 5.316E-01 5.322E-01 NOT IDENT. PR-144 -4.644E+OO 3.989E+Ol 3.995E+Ol NOT IDENT. PM-146 -5. 729E-01 8.412E-01 8.799E-01 NOT IDENT. ND-147 -9.134E-01 1.371E+Ol 1. 372E+Ol NOT IDENT. EU-150 -1.768E-01 3.987E-01 4.066E-01 NOT IDENT. EU-152 -2.253E-01 l.440E+00 1.443E+00 FAIL ABUN GD-153 -4.815E-01 9.743E-01 9.982E-01 NOT IDENT. EU-154 3.175E-01 1.138E+OO 1.146E+OO FAIL ABUN EU-155 2.236E-01 1.233E+OO l.237E+OO FAIL ABUN TB-160 9.867E-01 2.936E+OO 2.970E+OO FAIL ABUN H0-166M 7.945E-01 9.606E-01 1.025E+OO NOT IDENT. HF-172 2.123E+OO 2.367E+OO 2.554E+OO FAIL ABUN LU-172 -3.481E-01 1.542E+OO l.550E+OO FAIL ABUN LU-176 -9.479E-02 3.847E-01 3.870E-01 FAIL ABUN HF-181 -2.714E-01 9.179E-01 9.260E-01 NOT IDENT. TA-182 -1.lOlE+OO 1. 744E+OO l.813E+OO NOT IDENT. RE-183 7. 211E+Ol 9.687E+OO 3.392E+Ol FAIL ABUN RE-184 9.017E-01 3.105E+OO 3. 131E+OO NOT IDENT. W-188 -8.103E+Ol 1.182E+02 l.238E+02 FAIL ABUN IR-192* -3.332E-01 5.427E-01 5.631E-01 NOT IDENT. HG-203 -l.094E-01 6.468E-01 6.487E-01 NOT IDENT. BI-207 -3.845E-01 1.024E+OO 1.038E+OO NOT IDENT. TL-208 -l.255E-01 5.508E-01 5.537E-01 NOT IDENT. BI-211 2.417E+OO 3.061E+OO 3.249E+OO NOT IDENT. PB-211 2.617E+OO 1.173E+Ol 1.179E+Ol NOT IDENT. BI-212 3.240E+OO 8.158E+OO 8.287E+OO NOT IDENT. PB-212 1.849E-01 7.739E-01 7.784E-01 NOT IDENT. BI-214 -3.655E-01 l.098E+OO l. llOE+OO NOT IDENT. PB-214 8.612E-01 1.114E+OO 1.180E+OO FAIL ABUN RN-219 -9.777E-01 6.654E+OO 6.668E+OO NOT IDENT. RN-222 -3.655E-01 1.098E+OO 1. llOE+OO NOT IDENT. Page 3860 of 5809 RA-223 6.770E+OO 9.548E+OO 1.002E+Ol NOT IDENT. RA-224 -4. 861E+OO 8.400E+OO 8.681E+OO NOT IDENT. RA-226 -3.655E-01 1.098E+OO 1. llOE+OO NOT IDENT. AC-227 2.578E-02 3.693E+OO 3.693E+00 NOT IDENT. TH-227 2.578E-02 3.693E+OO 3.693E+00 NOT IDENT. AC-228 1.598E+OO 3.244E+OO 3.323E+00 NOT IDENT. RA-228 l.598E+OO 3.244E+OO 3.323E+00 NOT IDENT. TH-228 1.849E-01 7.739E-01 7.784E-01 NOT IDENT. TH-229 2.881E-01 6.823E+OO 6.824E+OO FAIL ABUN TH-230 -3.655E-01 1.098E+OO 1.11oe+oo NOT IDENT. PA-231 -l.169E+OO 6.684E+OO 6.704E+OO FAIL ABUN TH-231 6.770E+OO 9.548E+OO l.002E+Ol NOT IDENT. TH-232 1.598E+OO 3.244E+OO 3.323E+OO NOT IDENT. PA-233 4.085E-01 9.874E-01 1.004E+OO NOT IDENT. PA-234 -3.750E+OO 8.374E+OO 8.543E+OO NOT IDENT. PA-234M 4.808E+Ol 9.851E+Ol 1.009E+02 NOT IDENT. TH-234 -3.161E+OO 1. 749E+Ol 1. 754E+Ol NOT IDENT. U-234 -3.655E-01 1.098E+OO 1. llOE+OO NOT IDENT. U-235 4.519E-02 2.294E+OO 2.295E+OO FAIL ABUN NP-237 4.085E-01 9.874E-01 1.004E+OO NOT IDENT. NP-238 9.343E+02 3.255E+03 3.282E+03 SHORT HLIF U-238 -3.161E+OO 1. 749E+Ol 1. 754E+Ol NOT IDENT. NP-239 4.003E+OO 3.169E+OO 3.647E+OO NOT IDENT. PU-239 -7.410E+02 3.783E+03 3.798E+03 NOT IDENT. AM-243 8.737E-02 6.263E-01 6.275E-01 NOT IDENT. CM-243 7.468E-01 1.222E+OO 1. 268E+00 NOT IDENT. BK-247 7.513E-01 1.226E+OO 1.272E+OO FAIL ABUN CM-247 -1. 226E-01 6.209E-01 6.233E-01 NOT IDENT. CF-249 -5.793E-02 6.933E-01 6.938E-01 NOT IDENT. CF-251 6.516E-01 1.502E+OO 1.530E+OO FAIL ABUN ANH-511 6.898E-03 4.657E-01 4.657E-01 NOT IDENT. Page 3861of5809
  • GEL Laboratories LLC *
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  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 1841.6368 87.09 540.2142 136.47 460.9942 45.60 1632 .1157 87.57 540.7593 140.51 426.1465 46.54 1637.0526 88.03 541.2784 143.76 420.8557 49.72 1436.5237 88.34 541.6288 144.24 399.0442 51. 35 1549.3970 88.47 541. 77 59 145.44 418.7352 51. 87 1588.1833 89.96 477.9510 152.43 392.0894 52.39 1590.6327 90.64 485.0193 153.25 408.5446 52.97 1670.1371 91.11 459.8628 154.21 377.0555 53.44 1700.5043 92.59 474.0950 156.02 407.9984 54.07 1766.8883 93.35 448.7623 158.56 373.9821 57.36 0.0000 94.56 435.3367 159.00 386.0335 57.53 1896. 7218 94.65 435.4156 162.33 361. 5121 57.98 1234.1639 94.67 435.4328 162.66 377.5258 59.27 1238.5405 94.87 435.6045 163.33 406.7118 59.32 1238.7048 97.43 466.9885 165.86 329.9534 59.54 1239.4467 98.43 431. 8263 176.31 398.3127 60.96 1244.1995 98.44 431. 8365 176.60 375.'3414 61.17 1244.8989 99.53 425.9043 177.52 347 .1316 62.93 483.8324 100 .11 442.0270 181.07 391.8653 63.29 508.3216 102.03 438.7333 181.52 376.5805 63.58 535.1631 103.18 424.9270 184.41 463.5320 64.28 585.5295 103.37 425.0786 185.72 443.1284 66.73 544.6443 105.21 456.1524 193.51 427.1057 67.24 587.2230 105.31 456.2370 197.03 428.8974 67.68 615.2103 106.12 442.0823 198.01 456.5096 67.75 615.3185 106.47 465.1269 201.83 418.8242 69.67 596.2616 109.28 411. 8016 203.43 430.9726 70.83 568.5532 111. 00 414.0692 205.31 412.5306 72. 81 570.3317 111.76 417.6237 210.85 463.2906 72. 87 546.4139 114. 06 432.3581 215.65 448.4814 74.66 573.7481 116. 30 444.1089 222.11 478.3616 74.82 573.9606 116.74 413.2031 227.09 449.7927 74.97 592.7150 119.76 460.5810 227.38 435.9221 77 .11 606.8308 121.12 417.2996 228.16 431. 6065 78.74 575.3989 121.22 417.3686 228.18 431.6178 79.69 593.5003 121. 78 417.7574 235.69 394.5819 80.12 623.1636 122.06 417.9518 235. 96 417.0800 80.19 623.2599 122.92 418.5507 238.63 382.7823 80.57 634.1205 123.07 418.6542 238.98 384.1026 81. 00 641. 3106 123.68 414.6590 240.99 414.4981 81. 07 641.4095 125.81 387.4579 242.00 387.6539 81. 75 637.6574 127.23 422.5348 244.70 400.6040 83.79 614.3232 127.91 446.6158 252.40 389.3047 84.00 598.1945 129.30 410.5677 252.80 377.4751 85.43 627.8812 131.20 412.8418 254.15 0.0000 86.55 539.6000 133. 02 410.9207 256.23 376.3369 86.79 539.8682 133.52 396.7395 260.90 370.7928 86.94 540.0412 136.00 433.6263 264.66 364.8504 Page 3862 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 352.7736 364.49 338.2066 600.60 219.9227 265.00 368.5981 366.42 368.6027 602.52 0.0000 268.22 389.1797 '372.51 332.2588 604.72 214.2797 269.46 405.4677 375.05 345.2649 607.14 216.5708 270.03 393.4985 1093.63 321. 0511 609.32 226.9834 271 .. 23 408.5777 342.1172 610.33 202.6600 273.65 398.4865 388.16 323.0641 614.28 217.3422 276.40 357.8354 388.63 333.8947 618.01 189.1176 277.37 391.2734 391. 69 335.0645 620.36 198.5469 277.60 391.3513 400.66 357.8993 621. 93 212.0116 278.00 417.2699 401. 81 349.1598 630.19 0.0000 279.20 395. 6115 402.40 361. 9377 631.29 191.3735 279.54 376.0659 404.85 341.7550 633.25 201.8459 279.70 376.1219 410.95 396. 7425 634.78 217.4564 280.46 392.3735 413.71 373.8317 635.95 199.0155 283.69 317.4495 414.70 405.0286 636.99 182.6105 284.31 370.2850 423. 72 355.2798 645.85 204.1021 285.41 390.4193 427.09 371. 6702 657.76 221.9183 285.90 425.2024 427.87 392.0595 657.90 0.0000 287.50 364.7453 433.94 410.2072 661.66 219.1858 290.67 381. 0799 439.40 393.1544 664.57 0.0000 293.27 0.0000 453.88 449.0684 666.33 194.5598 295.22 362.6666 463.37 442.3387 666.50 194.5750 295.96 339.2031 468.07 469.9850 667.71 0.0000 298.58 358.7325 473.00 437.3877 677.62 178.7435 299.98 372.0931 475.06 400.0995 685.70 195.2301 300.09 372.1295 476.78 409.9898 695.00 168.4976 300.13 372.1385 477.60 397.8772 696. 49 182.3931 301.36 371. 7025 482.18 366.6733 696. 51 182.3931 302.85 355.4464 487.02 325.8087 697.00 180.3137 304.50 378.5610 492.35 327.7942 697.30 186.6992 304.85 370.3027 497.08 279.8274 697.49 184.5953 306.78 368.3877 505.52 255.1984 702.65 174.3835 308.46 376.4778 507.63 0.0000 706.68 169. 3710 311. 90 380.1000 511. 00 251.1715 711. 68 165. 4696 316.51 373.0986 514.00 265.1476 720.70 176.8399 319.41 331.5927 514.00 265.1476 721. 93 0.0000 320.08 325.8281 520.40 243.7690 722.78 169.4887 321.04 377.0369 520.69 241.8672 722. 91 173.7927 323.87 348.9738 522.65 0.0000 723. 31 183.4757 325.23 362.9910 527.90 238.9488 724 .19 205.0126 328.76 348.6494 528.26 240.9496 727. 33 183.7958 333.37 353.3668 529.59 243.0729 733.00 206.8672 333.97 366.4058 529.87 0.0000 735.93 171. 5254 334.37 359.6604 531. 02 245.2193 737.46 194. 3115 338.28 377.1281 537.26 234.3029 739.50 199.8822 338.32 381.4512 546.56 0.0000 747.24 214.6289 340.48 351.0408 552.55 222.4182 748.06 204.9423 340.55 351.0657 563.25 222.6875 752.31 197.6999 344.28 340.8382 569.33 225.4023 753.82 192.3910 345.93 349.0748 569.50 225.4207 756.73 206.7765 351.06 326.9728 569.70 225.4391 756.80 206.7765 351.93 328.0572 583.19 213.9707 763.94 192 .1133 355.39 0.0000 584.27 206.0427 765.81 190.0718 356.01 368. 3571 595.83 243.6575 766.42 202.1405 Page 3863 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 205.4567 1002.74 241.3669 1678.03 0.0000 772.60 0.0000 1004.73 243.3125 1690.97 16.0611 776.52 190.9143 1021. 30 0.0000 1750.46 0.0000 777.92 216.2703 1025.87 0.0000 1764.49 15.2219 778.90 216.3585 1028.54 0.0000 1770.23 15.2390 783.70 .212. 3738 .1037. 84 216 .1124 "1771.35 9.7993 785.37 213.6242 1038.76 0.0000 1791.20 0.0000 792.07 194.3262 1046.59 215.8037 1808.65 5.4852 794.95 198. 9697 1048.07 229.5129 1810. 72 0.0000 795.86 201.2546 1049.04 236.8499 1836.06 6.6182 801.95 230.5638 1050.41 211.5260 810.06 223.5160 1063.66 216.0687 810.29 212.4191 1077.00 210.5573 810.45 225.7813 1077.34 219.7412 810.76 236.9296 1085.87 214.8047 815.77 212.8777 1093.63 242.9238 818.51 219.7973 1099.45 238.7498 832.01 211. 9790 1112. 07 239.8518 834.85 212.2097 1112.84 210 .1108 835.71 213.4021 1115. 54 210.2770 836.80 0.0000 1120.29 164.7548 846.75 0.0000 1120.55 169.2188 846.77 259.4238 1121.30 175.6973 856.80 232.1015 1129. 67 146.9871 860.56 239.2381 1131.51 0.0000 871.09 252.6948 1147.95 0.0000 873.19 250.6152 1173.23 109.3093 875.33 0.0000 1177.95 78.5078 879.38 227. 2111 1189.05 75.7275 880.51 229.5928 1204.77 77.9711 883.24 226.3916 1221.41 52.5427 884.68 253.9685 1231.02 34.4839 889.28 220.0156 1235.36 43.1570 8 94-. 7 6 254.8989 1238.28 41. 2704 898.04 260.9539 1260.41 0.0000 900. 72 276.1621 1271.87 39 .'7162 903.28 253.3814 1274.44 36.8357 911.20 282.9822 1274.54 36.8357 912.08 283.0719 1291.59 26.2930 923.98 0.0000 1298.22 0.0000 926.50 292.6465 1312 .11 27.4155 929 .11 302.2225 1332.49 38.3906 937.49 314.7693 1362.66 0.0000 944 .13 334.7746 1365.19 12.9048 946.00 349.9043 1368.63 0.0000 949.00 323.9335 1384.29 20.9474 954.55 0.0000 1408.01 9.0313 962. 31 298.0709 1457.56 0.0000 964.08 307.0807 1460.82 13.2142 966 .17 271.0984 1489.16 9.3566 968.97 256.3254 1505.03 17.4628 983.53 240. 7143 1584.12 3.3473 984.45 0.0000 1596.21 10.4889 996.26 259.7588 1620.50 7.3815 1001.03 228.7188 1621. 92 12.6584 Page 3864 of 5809 11 2ij1o. --* . , os-Ocl:-2016 1 '£9 t:,. i f L ... Ys4/./* Dilte; e'oM:(;. oir 100 mq tw GAB. have llllank reuortet:S.iridiidei:!I Of . 11( ME;ll4/ffll)tp,,eo/4r 1s ,tJlao '!r Cif . .. . . :rt greab?I" tftian f,JDC, <en:cr.is 40% or EesS. Ef bef<iw lilei 14\oAi MOC;.. J$:oimv. -,cnst.rument lajthln Clted<Jswt...;*'-'.Method ROii./ Ll.O baS beeiii met. I * * . .* . If . ., . . . .. . , less tlian 5* MON MOC, then RPD is less, tt greater s.:f.toN Mtic; R?o 20% or * * * [f MDiV MDC, th,Ei'Rl>D -Or meets 'the Client's reeiuii-ed.RER acce!itance crltcna *. . vietill {S'.15,-125"/o.. . '(Or contract accei#aii'i:e iJtan'k ttian*.ttie l:i.o. FY6, r.trl """""l'YlfACL S::::Ctl.. ft.ti'"" ' ----Ves. -Lt_ .,._t,*,. ;,/ / ***7 / jr;;(p. ? !i;.Jmple was'ii.tn wlth!n time.* 'AnvJJ: li:amp(Q v.ias comi:ctlv r>resari/Qd lf reauired. ISirtE!ars-:ralcen for Radioactive batches. Method si)ike anci LCS are \Vltiiln (gr meets ct!Wdal. No blarik spaces on*.dat;f forms. 1A11'1ine oirt5'1nitlii1ild anci Ciabii:I. '**..:'transcriiltion' ermr:iare'*aiiii'a'tant_' Aux data* IS *cac-rort; . .c1ient soeCia1 reau1rements ilacie itas been Checked. IRatil Data *and,-or.spcctrum ar<<Jinciuded.anr:i' properiv.statused *. ---*-es ver .. e
  • 1 ****. . '" f--"-..::-L-*_.....:. .. --'c._:...:. ._.,,... ,r..;,;.,. /. / */ *77 .. 7 .,,;;, . **J;4r . ilt'k' -., ..... ._J),;fi. ,, . Batch Data EXce1>tion RaportS '{DER) comliteted,.lf aiJplli:iible; / ...
  • J.tk'71/Jf1li4
  • Jl((.?.::Jtf/. B,*h E)(.ceptlo'.i'! seco)ld rev*evfed. . . . . . * -. . _ ','"'. AllllUot*correctlon *comPll!ted if feoulred. Reyiew hlStorlcal .res1,Jlts ii' available, Cif REMP. results a'bove MDC have been verified bv. hlstorkal results, recount: or r&-analvsls. l ' / ..... ---* ... * .. * ...,_,,.._..........,.o/. of 5809 . IL{"

GEL Laboratories LLC Form GEL-DER .. Mo.Day Yr. 03-0CT-16 Instrument Type: GAMMA SPECTROMETER Batch ID: 1596252 DATA EXCEPTl6N REPORT Division: Quality Criteria: Radiochemistry Specifications Test I Method: Matrix Type: DOE HASL 300, 4.5.2.3/Ga-01-R Solid Sample Numbers: See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

DER Report No.: 1563784 Revision No.: 1 Type: Process Client Code: MJWC Sample received out of holding for sample 405235041, sample Samples were analyzed as soon as possible. Reporting results. 405235042, sample 405235043, sample 405235044, sample'405235045, sample 405235046, sample 405235047, sample 405235048, sample 405235049, sample 405235050, sample 405235051, sample 405235052, sample 405235053, sample 405235054, sample 405235055, sample 405235056, sample 405235057, sample 405235058, sample 405235059, sample 405235060 and DUP 1203621362 Originator's Name: Data Validator/Group Leader: Bryan Williams 03-0CT-16 Spencer Collins 03-0CT-16 Page 1 Page 3866 of 5809 09/16/201() . Analyst:* '!\lX!l-f i:cs:isot(,lpe:*:Mixed Gamma . LCS;:Code: Initials: PbS. :Prep Date:: 'ff;i.{'.tte Ffrst Client.ut1eD'ateil CiJ04t2<ii6. Due .Date: O?f3Dil01 (;: IS.[&,. . '.ExplrationJ)ate: 'Vot: \.o. ':Library: £1.?k\]). Baliuu:e ..... __.:N ..... * *-+/._A _____ _ Hazard. ,Al(:)ot . Sentfngi>nt(!rtl!ne .Sampl,eIO C!ient_!lescriplionJ f ontaincr..fD typ_e .Coile 'Ciicnt Geom'etry (J .. _.:19 lJctector . (lt:Ap(>lk.Rblli) 405235041-1 4,.m;a.t;.t SAMPL!= *MJWCOOI SOIL . (JjJ l'.;J * . *t51.483g: 405235042-l 4.4D.R.2.J: SAMPLE' M.tiVCOOtz SOIL ,. :176;8 g ! g* I 4.-m:it2:4 MJWCl:ioi SOIL 165.'J!1$s Q I '41)5235044"1 'SAl\f:PBE= SOIL 30-1'/0Y*1S,13i;IO:OO* t 128.844,g I .. '3'2... .! *405l3So4s;.1 4.'ID.lt5;2 *SAMPi:E, ,M.J\VCOOi son. 130;599,g l 3"1 405235046.1 4,5;\.it;Jj, SAl\JPLE' so it i0I 156.9:!.llg !* '2t:J *k5A.R.li4 '.SAMPl;E >MJWCOOt SOIL 07*DE<:;*1S10:IO:OO(Lf l:'il.349g 1. "'tS .:f;SB.It:!:J *s;\r.wi.&: 'M.IWCOOl: SOIL 'ft.f-13U77.:g 1. *'Lt:(;* I . 405235049-1 4.5B.R;t:3' SAi\WLE. .M.J\Vc"6011 soiL !3:3Jioo .147.30.lg J l . 405)350511-1

  • 4;5B;JU;"4 iSAMPl.E: L )C: ,405235')51_-1 *t5B:ttl;3_. SAJ\.:U't;t* MJWC::OOt: .SOIL 07*DEC,1513:0l:001 * .i ::_ It1J.0121r "t.\t ,4os2Jsils1-t 4.SBJt:Mi SA:;\;JP!::E0 SOIL .*, * ......... '165;245 g \.\IJ , 40S2350SJ..I *4.!lC.ItS.2 SAl\tpi.Jt M;J\vcoo1* .SOIL w 113.Glll*g ':!>' 4052350,s;t.1 4.SC.R.1.3 SA!\lPLE: *MJW<::OIH *SOIL 146.46lg 40Sl3505S. i "':scn;1 . .t, MJ\V.Clioj: SOlL 142.583.g j \\'. ,4052Jsos(l.1, *4:sc.itfa** *SAl\iPLE, MJw(:bor iSOlL , ** JOl_.481 s r ;J(!523505M 4'5Clt2:3 SAMPLE: MJWCOOl' SOJL t1Ml35g 'Sl. ..io5bsil5S.1 . 4;SCJt2;4 SAi\1PbE MJ\Vcoo1 . so1.L l40;6:22g 405235059-1 5.tA.R.1*2 MJ\VCOOl S(>IL 12:26:0'.\'t : . 154*2,"a: 7 .... *s.11\.R.P' SAMPI.E' MJWCOill '.SOIL .: l52..26Gg \iS 1200621361-1' -MB MB" "QPACCOUl\'T .:son. DUP.* QC-,\CCOUNT* *SOI.L ;i0-NO\li1.5' t.3:2'MPfl.f : 120362J36J.;l LCS LCS QG SOIL* tiJiiliio *ft?. HS-'\. l . *-*GEL .Laboratories ELC, . RUdiocliemistrY:DMslon 01 t VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:57:25.97 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : Z-OCT-2016 11:01:35. Sample date 30-NOV-2015 13:27:00 Acquisition date : 3-0CT-2016 05:54:08. Sample ID G405235041 Sample quantity 1.81483E+02 GRAM Detector name : GAM28 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.41 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 3 3 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 74.82* 77.24 87.41 93.17* 116. 91 186.22* 208.98 238.89* 241. 70 295.86 300.31 338.63 352.28* 448.85 463.26 480.40 511. 83* 523.66 583.75* 601. 53 609.77* 618.45 662.53* 675.73 727.33 816.35 861.08 867.40 912.08* 969. 82 1120.37* 1183. 05 1239.39 1461. 82* Page 3868 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 126 171 39 30 33 71 . 42 340 104 125 34 80 215 16 47 21 56 13 126 28 191 16 17 15 30 15 17 24 67 51 49 13 16 383 198 204 259 155 143 116 91 95 112 89 39 51 72 19 36 30 76 14 51 30 32 39 25 26 23 10 16 18 23 35 26 13 25 7 1. 48 1. 31 1. 54 1. 25 1. 43 1. 21 0.95 1. 24 1. 97 1.11 1. 85 0.97 1. 60 2.29 1. 37 4.87 2 .11 1. 36 1. 51 3.98 1. 75 3.06 1. 48 3.34 1. 44 0.53 1. 30 3.86 1. 35 1. 33 1. 35 5.36 2.13 2.08 149.74 154.57 174.93 186.45 233.97 372. 69 418.24 478.12 483.75 592.13 601. 04 677.73 705.06 898.35 927.19 961. 49 1024.40 1048.08 1168. 34 1203.93 1220.43 1237.79 1326.02 1352.44 1455.73 1633.90 1723.41 1736.07 1825.49 1941. 06 2242.38 2367.85 2480.60 2925.80 142 142 169 183 227 369 414 472 472* 585 597 672 699 894 922 955 1014 1044 1161 1197 1211 1229 1321 1345 1448 1628 1717 1729 1817 1935 2234 2360 2476 2919 19 3.50E-02 19 4.74E-02 11 1.09E-02 8 8.22E-03 10 9.21E-03 10 1. 96E-02 8 1.17E-02 24 9.45E-02 24 2.88E-02 11 3.46E-02 8 9.39E-03 12 2.22E-02 12 5.98E-02 9 4.56E-03 12 1. 31E-02 13 5.97E-03 22 l.57E-02 9 3.47E-03 16 3.50E-02 15 7.78E-03 18 5.29E-02 17 4.41E-03 9 4.66E-03 13 4 .14E-03 13 8.43E-03 11 4.07E-03 12 4.76E-03 17 6.73E-03 15 l.86E-02 14 1.42E-02 16 l.37E-02 13 3.61E-03 9 4.46E-03 13 l.07E-01 23. 2 1. 55E+OO 16.4 81. 4 81.9 70.4 32.4 42.2 7.2 2.49E+OO 29.0 17.1 36.6 21.1 10.6 52.9 27.2 56.3 45.7 60.1 15.1 46.6 10.2 92.8 62.3 75.2 37.1 50.7 54.5 44.1 20.0 28.3 28.0 63.5 61. 2 5.3 Peak Search Report (continued) Sample ID : G405235041 Pk It Energy Area Bkgnd 35 0 1540.81 9 0 36 0 1765.92* 28 8 37 .o 1848.94 13 3 Acquisition date FWHM Channel Left Pw 0. 62 3083.89 3079 10 2.73 3534.45 3526 16 1. 48 3700.61 .3695 10 Page : 2 3-0CT-2016 05:54:08 Cts/Sec %Err Fit 2.50E-03 33.3 7.85E-03 30.2 3.74E-03 35.0 Flag: "*" = Peak area was modified by background subtraction Page 3869of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:57:28 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID Sample.type Detector name : 30-NOV-2015 13:27:00 G405235041 Acquisition date : Sample quantity Sample geGlmetry Detector geometry: 3-0CT-2016 05:54:08 181. 48 GRAM Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA28 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3870 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.41 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235041 Acquisition date 3-0CT-2016 05:54:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.23.JE+OO 1.183E+Ol 1.183E+Ol . 10.64 OK

  • CD-109 88.03 3.70* 5.432E+OO 4.268E-01 6.777E-01 447.68 OK SN-126 64.28 9.60 3.124E+OO Line Not Found Absent 86.94 8.90 5.432E+OO 1. 775E-01 1. 775E-01 447.68 OK 87.57 37.00* 5.432E+OO 4.268E-02 4.268E-02 447.68 OK BA-137M 661. 66 89.90* 2.304E+OO 3.721E-02 3.794E-02 124.68 OK CS-137 661. 66 85.10* 2.304E+OO 3.931E-02 4.008E-02 124.68 OK TL-208 277.37 6.60 4.566E+OO Line Not Found Absent 583.19 85.00* 2.539E+OO 2.731E-01 2.731E-01 30.19 OK 860.56 12.50 l.887E+OO 3.210E-01 3.210E-01 108. 96 OK BI-211 72.87 1. 23 4.138E+OO Line Not Found Absent 351.06 12.92* 3.783E+OO 8.826E-03 8.826E-03******* OK PB-212 74.82 10.28 4.344E+OO 1.256E+OO 1.256E+OO 64.18 OK 77.11 17.10 4.585E+OO 1. 313E+OO 1.313E+OO 32.89 OK 238.63 43.60* 5.101E+OO 8. 071E-01 8. 071E-01 14.30 OK 300.09 3.30 4.293E+OO 1. 224E+OO 1.224E+OO 73.14 OK BI-214 609.32 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 OK 1120.29 14.92 1.539E+OO 9.149E-01 9.152E-01 55.98 OK 1764.49 15.30 1.044E+OO 6.974E-01 6.977E-01 60.31 OK PB-214 74.82 5.80 4.343E+OO Line Not Found <<INT Reject 77.11 9.70 4.585E+OO 2.315E+OO 2.316E+OO 32.89 OK 87.09 3.41 5.409E+OO Line Not Found <<INT Reject 242.00 7.25 5.054E+OO Line Not Found <<INT Rej*ect 295.22 18.42 4.343E+OO 7.994E-01 7.997E-01 34.29 OK 351. 93 35.60* 3.786E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 OK 1120.29 14.92 1.539E+OO 9.149E-01 9.152E-01 55.98 OK 1764.49 15.30 1.044E+OO 6.974E-01 6.977E-01 60.31 OK RA-224 240.99 4.10* 5.059E+OO 1. 221E+OO 1. 221E+OO 131. 43 OK RA-226 609.32 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 OK 1120.29 14.92 1.539E+OO 9.149E-01 9.152E-01 55.98 OK 1764.49 15.30 1.044E+OO 6.974E-01 6.977E-01 60.31 OK AC-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.153E-01 9.153E-01 42.22 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835.71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 OK 968. 97 15.80 1.723E+OO 8.137E-01 8.137E-01 56.63 OK RA-228 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11. 27 3.904E+OO 9.153E-01 9.153E-01 42.22 OK 794.95 4.25 2.005E+OO Line Not Found Absent 835. 71 1. 61 1.930E+OO Line Not Found Absent 911. 20 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 OK 968. 97 15.80 1.723E+OO 8.137E-01 8.137E-01 56.63 OK TH-228 74.82 10.28 4.344E+OO l.256E+OO 1.256E+OO 64.18 OK 77 .11 17.10 4.585E+OO 1.313E+OO 1. 313E+OO 32.89 OK 238.63 43.60* 5 .101E+OO 8. 071E-01 8. 071E-01 14.30 OK 300.09 3.30 4.293E+OO 1.224E+OO 1.224E+OO 73.14 OK TH-230 609.32 45.49* 2.455E+OO 7.939E-01 7.939E-01 20.48 OK Page 3871 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235041 Acquisition date 3-0CT-2016 05:54:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 .l.539E.t-00 9.149E-01 9.149E-01 55.98 OK ** 1764.49 15.30 1.044E+OO 6.974E-01 6.974E-01 60.31 OK PA-231 283.69 1. 70 4.487E+OO Line Not Found Absent 301.36 5.35* 4.293E+OO 7.547E-01 7.547E-01 73.14 OK TH-232 105.21 1.10 6.315E+OO Line Not Found Absent 338.32 11.27 3.904E+OO 9.153E-01 9.153E-01 42.22 OK 835.71 1. 61 1.930E+OO Line Not Found Absent 911. 20 25.80* l.806E+OO 6.291E-01 6.291E-01 39.97 OK 968.97 15.80 1.723E+OO 8.137E-01 8.137E-01 56.63 OK U-234 609.32 45.49* 2.455E+OO 7.939E-01 7.939E-01 20.48 OK 1120.29 14.92 1.539E+OO 9.149E-01 9.149E-01 55.98 OK 1764.49 15.30 l.044E+00 6.974E-01 6.974E-01 60.31 OK AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.344E+OO l.922E-01 l.922E-01 64.18 OK ANH-511 511. 00 100.00* 2.812E+OO 9.561E-02 9.561E-02 91. 39 OK Flag: "*" == Keyline Page 3872 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:57:29.76 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE. DATA * '* * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l * *Acquisition date 3-0CT-2016 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.41 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:27:00 Analyst initials: MXRl *
  • Sample ID G405235041 Sample Quantity l.8148E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.183E+Ol 1.233E+OO CD-109 6.777E-01 2.973E+OO SN-126 4. 2 68E-02 1.873E-01 BA-137M 3.794E-02 4.636E-02 CS-137 4.008E-02 4.898E-02 TL-208 2. 731E-01 8.080E-02 BI-211 8.826E-03 8.712E-01 PB-212 8. 071E-01 l.131E-01 BI-214 7.942E-01 l.594E-01 PB-214 8.029E-01 l.668E-01 RN-222 7.942E-01 1.594E-01 RA-224 1.221E+OO 1.572E+OO RA-226 7.942E-01 l.594E-01 AC-228 6. 291E-01 2.464E-01 RA-228 6.291E-01 2.464E-01 TH-228 8.071E-01 l .131E-01 TH-230 7.939E-01 1.594E-01 PA-231 7.547E-01 5.410E-01 TH-232 6.291E-01 2.464E-01 U-234 7.939E-01 1.594E-01 AM-243 1.922E-01 l.209E-01 ANH-511 9.561E-02 8.563E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-2°6 SC-46 V-48 CR-51 MN-54 Page 3873 of 5809 Key-Line Activity (pCi/GRAM -2.191E-01 -3.133E-03 O.OOOE+OO 9.807E-03 -5.154E-02 O.OOOE+OO O.OOOE+OO -l.507E-02 K.L. Cnt Uncert * ( 1. 96-sigma) 1.151E+Ol 4.147E-02 1.640E+41 1.932E-02 3.074E-01 1.631E+04 4 .114E+02 4.486E-02 MDA (pCi/GRAM 4.280E-01 2.012E+OO l.275E-01 5.412E-02 5. 717E-02 4.938E-02 2.838E-01 7.667E-02 8.436E-02 2.522E-01 8.436E-02 8.215E-01 8.436E-02 2.040E-01 2.040E-01 7.667E-02 8.433E-02 6. 421E-01 2.040E-01 8.433E-02 8.042E-02 4.218E-02 MDA (pCi/GRAM 2.013E+Ol 8.013E-02 0.000E+OO 5. *o27E-02 6.107E-01 O.OOOE+OO O.OOOE+OO 8.755E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 2.359E-01 3.183E-01 7.383E-01 FAIL ABUN MN-56 O.OOOE+OO l.330E+41 O.OOOE+OO SHORT HLIF C0-57 2.007E-02 3.755E-02 7.512E-02 NOT IDENT. C0-58 -5.366E-01 5.507E-01 7.859E-01 NOT IDENT. FE-59 -2.765E+OO 7.132E+OO 1.321E+Ol NOT IDENT. C0-60 l.676E-02 3.302E-02 7.121E-02 NOT IDENT. ZN-65 3.236E-02 l.379E-01 2.582E-01 NOT IDENT. GE-68 3.568E-01 1. 967E+OO 4.llOE+OO NOT IDENT. AS-73 7 .118E-01 7.667E+OO 1.542E+Ol NOT IDENT. AS-74 04000E+OO 6.412E+03 O.OOOE+OO HLIF SE-75 3.921E-02 1.560E-01 3.226E-01 NOT IDENT. BR-77 O.OOOE+OO 2.013E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 6.619E+02 0.000E+OO SHORT HLIF RB-83 -7.956E-02 5.151E-01 8.069E-01 NOT IDENT. KR-85 l.199E+Ol 6.695E+OO 1.484E+Ol NOT IDENT. SR-85 1. 374E+OO 7.680E-01 1.702E+OO NOT IDENT. RB-86 O.OOOE+OO 3.086E+04 O.OOOE+OO SHORT HLIF Y-88 -3.347E-02 l.661E-01 3.512E-01 NOT IDENT. Y-91 -8.323E+Ol 4.945E+02 9.417E+02 NOT IDENT. NB-94 3.764E-03 2.770E-02 5.314E-02 NOT IDENT. NB-95 -2.157E-01 7.525E-01 1.468E+OO NOT IDENT. NB-95M 6.486E-01 2.187E+00 4.070E+OO NOT IDENT. ZR-95 -4.732E-01 1.213E+OO 2.353E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 9.670E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 7.707E-04 2.980E-02 5.632E-02 NOT IDENT. RH-102 7.192E-03 4.975E-02 9.731E-02 NOT IDENT. RU-103 4.882E+OO 4.914E+00 1.085E+Ol FAIL ABUN RH-106 -6.489E-02 4.481E-01 7.483E-01 NOT IDENT. RU-106 -6.489E-02 4.481E-01 7.483E-01 NOT IDENT. AG-108M -l.657E-03 2.181E-02 4.250E-02 NOT IDENT. AG-110M -2.353E-02 6.819E-02 1.333E-01 NOT IDENT. SN-113 -1.516E-01 1.871E-01 3.351E-01 NOT IDENT. CD-115 O.OOOE+OO 2.626E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.185E+05 O.OOOE+OO SHORT HLIF TE-123M 4.146E-02 1.180E-01 2.263E-01 NOT IDENT. SB-124 -5.395E-01 1.225E+OO 2.288E+00 NOT IDENT. SB-125 -5.858E-02 7.809E-02 l.397E-01 FAIL ABUN TE-125M 3.575E+02 2.626E+02 5.525E+02 NOT IDENT. I-126 O.OOOE+OO 1. 294E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.650E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.770E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 8.049E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.684E+27 O.OOOE+OO SHORT HLIF BA-133 5.065E-03 3.547E-02 6.415E-02 NOT IDENT. I-133 O.OOOE+OO l.811E+41 O.OOOE+OO SHORT HLIF CS-134 2.947E-02 3.597E-02 8.122E-02 NOT IDENT. CS-135 -3.974E-02 1.121E-01 2.176E-01 NOT IDENT. I-135 O.OOOE+OO 1.017E+41 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 4.021E+05 O.OOOE+OO SHORT HLIF CE-139 -2.894E-02 8.760E-02 1. 763E-01 NOT IDENT. BA-140 O.OOOE+OO 1.663E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.030E+05 O.OOOE+OO SHORT HLIF CE-141 -4.633E+OO 2.484E+Ol 4.568E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.477E-01 2.927E-01 5.104E-01 NOT IDENT. PM-144 -7.349E-03 4.538E-02 8.436E-02 FAIL ABUN PR-144 -6.410E-01 3.959E+OO 7.358E+OO NOT IDENT. PM-146 4.002E-02 3.280E-02 7.211E-02 NOT IDENT. ND-147 O.OOOE+OO 4 .119E+07 O.OOOE+OO SHORT HLIF PM-147 -2.057E+02 6.735E+02 1.248E+03 NOT IDENT. PM-149 0.000E+OO 1. 960E+41 0.000E+OO SHORT HLIF EU-150 -1.533E-02 1. 960E-02 3. lOlE-02 FAIL ABUN EU-152 -3.274E-02 7.623E-02 1.371E-01 NOT IDENT. GD-153 -2.430E-02 l.542E-01 2.939E-01 NOT IDENT. EU-154 -7.654E-03 *1.013E-01 l.957E-01 NOT IDENT. EU-155 l.440E-01 9.169E-02 1. 967E-01 FAIL ABUN TB-160 -l.598E-01 1.485E+OO 2.989E+OO FAIL ABUN H0-166M 4.164E-02 4.165E-02 9.240E-02 NOT IDENT. TM-171. 3.747E+OO 1.817E+Ol 3.684E+Ol NOT IDENT. HF-172 1.520E-01 l.927E-01 3. 88.7E-01 NOT IDENT. LU-172 -1.882E-02 5.670E-02 1.080E-01 FAIL ABUN LU-176 -l.850E-04 2.079E-02 4 .115E-02 FAIL ABUN HF-181 -l.030E+OO 4.586E+OO 7.676E+OO NOT IDENT. TA-182 8.049E-02 8.034E-01 1. 591E+OO FAIL ABUN Page 3874 of 5809 RE-183 7.150E-01 2.591E+OO 5.320E+00 NOT IDENT. RE-184 -9.123E+OO 2.949E+Ol 5.672E+Ol NOT IDENT. W-188 -7.636E+Ol l .150E+o2 l.905E+02 NOT IDENT. IR-192 -l.241E-01 4.075E-01 7.863E-01 FAIL ABUN HG-203 l.115E+OO 2.026E+OO 4.255E+00 NOT IDENT. BI-207 -5.187E-03 3. 713E-02 7.285E-02 FAIL ABUN PB-210 2. 871E-01 2. 941E+OO 5. 962E+00 NOT IDENT. PB-211 l.675E-01 5.050E-01 l.033E+OO NOT IDENT. BI-212 9. 611E-01 6.997E-01 9.733E-01 FAIL ABUN 4 . RN-219 9.597E-02 . 2. 962E-01 4 6.035E-01 NOT IDENT. RA-223 l.121E-01 4.307E-01 8.828E-01 FAIL ABUN AC-227 3.136E-02 l.768E-01 3.607E-01 FAIL ABUN TH-227 3.136E-02 l.768E-01 3.607E-01 FAIL ABUN TH-229 -l.910E-01 3.872E-01 7.594E-01 FAIL ABUN TH-231 l.121E-01 4.307E-01 8.828E-01 FAIL ABUN PA-233 -l.434E-02 4.449E-02 8.618E-02 FAIL ABUN PA-234 6.026E-03 2.016E-01 4.124E-01 NOT IDENT. PA-234M -2.242E+OO 3.002E+OO 5.820E+OO NOT IDENT. TH-234 1. 378E-01 l.031E+OO 2.078E+OO FAIL ABUN U-235 8.410E-02 l.545E-01 3.035E-01 FAIL ABUN NP-237 -1.434E-02 4.449E-02 8.618E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 1. 378E-01 1.031E+OO 2.078E+OO FAIL ABUN NP-239 3.654E-01 5.044E-Ol 4.283E-01 FAIL ABUN PU-239 l.305E+02 2. 816E+02 5.474E+02 NOT IDENT. AM-241 5.439E-02 1.190E-01 2.450E-01 NOT IDENT. CM-243 -l.148E-01 8.637E-02 1.472E-01 NOT IDENT. BK-247 -3 .'643E-03 5.211E-02 l.047E-01 NOT IDENT. CM-247 7.164E-03 2.740E-02 5.541E-02 NOT IDENT. CF-249 1. 758E-02 2.798E-02 5.915E-02 NOT IDENT. CF-251 -2.456E-03 8.975E-02 1.833E-01 NOT IDENT. Page 3875 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:57:26.91 Nuclide Line Activity Report Nuclide T.ype: . Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 377 10.66* 1.237E+OO 1.183E+Ol 1.183E+Ol 10.64 CD-109 88.03 57 3.70* 5.432E+OO 1.164E+OO 1.847E+OO 162.79 SN-126 64.28 ------9.60 3.124E+OO ------Line Not Found ------86.94 57 8.90 5.432E+OO 4.837E-01 4.837E-01 162.79 87.57 57 37.00* 5.432E+OO 1.164E-01 1.164E-01 162.79 BA-137M 661.66 19 89.90* 2.304E+OO 3.721E-02 3.794E-02 124.68 CS-137 661.66 19 85.10* 2.304E+OO 3. 931E-02 4.008E-02 124.68 TL-208 277.37 ------6.60 4.566E+OO ------Line Not Found ------583.19 142 85.00* 2.539E+OO 2. 731E-01 2. 731E-01 30.19 860.56 18 12.50 1. 887E+OO 3.210E-01 3.210E-01 108. 96 BI-211 72.87 ------1. 23 4.138E+OO ------Line Not Found ------351.06 261 12.92* 3.783E+OO 2. 211E+OO 2. 211E+OO 21. 20 PB-212 74.82 184 10.28 4.344E+OO 1.707E+OO 1. 707E+OO 46.35 77 .11 249 17.10 4.585E+00 1.313E+OO 1.313E+OO 32.89 238.63 434 43.60* 5.101E+00 8. 071E-01 8. 071E-01 14.30 300.09 42 3.30 4.293E+OO l.224E+OO 1.224E+OO 73.14 BI-214 609.32 214 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 1120.29 51 14.92 1.539E+OO 9.149E-01 9.152E-01 55.98 1764.49 27 15.30 1.044E+00 6.974E-01 6.977E-01 60.31 PB-214 74.82 184 5.80 4.344E+OO 3.026E+OO 3.027E+OO 46.35 77 .11 249 9.70 4.585E+OO 2.315E+OO 2.316E+OO 32.89 87.09 57 3.41 5.432E+OO 1. 263E+OO 1.263E+00 162.79 242.00 132 7.25 5.059E+OO 1. 490E+OO 1.490E+OO 58.06 295.22 155 18.42 4.343E+OO 7.994E-01 7.997E-01 34.29 351. 93 261 35.60* 3.783E+OO 8.026E-01 8.029E-01 21. 20 RN-222 609.32 214 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 1120.29 51 14.92 1.539E+OO 9.149E-01 9.152E-01 55.98 1764.49 27 15.30 1.044E+OO 6.974E-01 6.977E-01 60.31 RA-224 240.99 132 4.10* 5.059E+OO 2.634E+OO 2.634E+OO 58.06 RA-226 609.32 214 45.49* 2.455E+OO 7.939E-01 7.942E-01 20.48 1120. 29 51 14.92 1.539E+OO 9.149E-01 9.152E-01 55.98 1764.49 27 15.30 1.044E+00 6.974E-01 6.977E-01 60.31 AC-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 97 11. 27 3.904E+OO 9.153E-01 9.153E-01 42.22 794.95 ------4.25 2.005E+00 ------Line Not Found ------835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 71 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 968. 97 54 15.80 1.723E+OO 8.137E-01 8.137E-01 56.63 RA-228 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 97 11.27 3.904E+00 9.153E-01 9.153E-01 .42. 22 794.95 ------4.25 2.005E+OO ------Line Not Found ------835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 71 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 968. 97 54 15.80 1.723E+OO 8.137E-01 8.137E-01 56.63 TH-228 74.82 184 10.28 4.344E+OO 1.707E+OO 1.707E+00 46.35 77 .11 249 17.10 4.585E+OO 1. 313E+OO 1. 313E+OO 32.89 238.63 434 43.60* 5.101E+OO 8. 071E-01 8.071E-01 14.30 Page 3876of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235041 Acquisition date 3-0CT-2016 05:54:08 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 30.0. 09 42 3.30 4.293E+OO 1. 224E+oo. 1.224E+OO 73.14 TH-230 609.32 214 45.49* 2.455E+OO 7.939E-01 7.939E-01 20.48 1120.29 51 14.92 1.539E+OO 9.149E-01 9.149E-01 55.98 1764.49 27 15.30 1.044E+OO 6.974E-01 6.974E-01 60.31 PA-231 283.69 ------1. 70 4.487E+OO ------Line Not Found ------301.36 42 5.35* 4.293E+OO 7.547E-01 7.547E-01 73.14 TH-232 105.21 ------1.10 6.315E+OO ------Line Not Found ------338.32 97 11.27 3.904E+OO 9.153E-01 9.153E-01 42.22 835.71 ------1. 61 1.930E+OO ------Line Not Found ------911.20 71 25.80* 1.806E+OO 6.291E-01 6.291E-01 39.97 968. 97 54 15.80 1. 723E+OO 8.137E-01 8.137E-01 56.63 U-234 609.32 214 45.49* 2.455E+OO 7.939E-01 7.939E-01 20.48 1120.29 51 14.92 1.539E+OO 9.149E-01 9.149E-01 55.98 1764.49 27 15.30 1.044E+OO 6.974E-01 6.974E-01 60.31 AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 184 67.20* 4.344E+OO 2.612E-01 2.612E-01 46.35 ANH-511 511.00 65 100.00* 2.812E+OO 9.561E-02 9.561E-02 91. 39 Flag: "*" Keyline Page 3877 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235041 Acquisition date 3-0CT-2016 05:54:08 Total number of lines in spectrum 37 Number of unidentified lines 8 Number of lines tentatively identified by NID 29 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Hlife l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1.41E+10Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1. 41E+l0Y 1.41E+l0Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 59 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.183E+Ol 1.164E+OO l.164E-01 3.721E-02 3.931E-02 2. 731E-01 2. 211E+OO 8.071E-01 7.939E-01 8.026E-01 7.939E-01 2.634E+OO 7.939E-01 6.291E-01 6.291E-01 8.071E-01 7.939E-01 7.547E-01 6.291E-01 7.939E-01 2.612E-01 9.561E-02 2.769E+Ol 2.769E+Ol Decay Corr pCi7GRAM 1.183E+Ol 1.847E+OO 1.164E-01 3.794E-02 4.008E-02 2.731E-01 2. 211E+OO 8. 071E-01 7.942E-01 8.029E-01 7.942E-01 2.634E+OO 7.942E-01 6.291E-01 6.291E-01 8.071E-01 7.939E-01 7.547E-01 6.291E-01 7.939E-01 2.612E-01 9.561E-02 2.837E+Ol 2.837E+Ol 78.38% Decay Corr 2-Sigma Error 0.126E+Ol 3.007E+OO 1.894E-01 4.731E-02 4.998E-02 0.824E-01 0.469E+OO 1.154E-01 1.627E-01 l.702E-01 l.627E-01 1.530E+OO 1.627E-01 2.514E-01 2.514E-01 1.154E-01 1.626E-01 5.520E-01 2.514E-01 1. 62 6E-01 1.210E-01 8.738E-02 "M" Manually accepted 2-Sigma %Error 10.64 162.79 162.79 124.68 124.68 30.19 21. 20 14.30 20.48 21. 20 20.48 58.06 20.48 39.97 39.97 14.30 20.48 73.14 39.97 20.48 46.35 91. 39 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3878 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235041 Acquisition date : 3-0CT-2016 05:54:08 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 93.17 42 222 1.25 186.45 183 8 8.22E-03 **** 5.79E+OO T 0 116. 91 46 199 1. 43 233.97 227 10 9.21E-03 **** 6.57E+OO T 0 186.22 93 152 1.21 372. 69 369 10 1. 96E-02 64.7 5.98E+OO T .o 208.98 55 118 0.95 418. 2.4 414 8. 1.17E-02 84.4 5.58E+OO. 0 448.85 19 22 2.29 898.35 894 9 4.56E-03 **** 3.12E+OO 0 463.26 55 42 1. 37 927.19 922 12 1.31E-02 54.5 3.04E+OO T 0 480.40 25 34 4.87 961.49 955 13 5.97E-03 **** 2. 96E+OO 0 523.66 14 16 1. 36 1048.08 1044 9 3.47E-03 **** 2.76E+OO T 0 601.53 32 34 3.98 1203.93 1197 15 7.78E-03 93.3 2.48E+OO T 0 618.45 18 44 3.06 1237.79 1229 17 4. 41E-03 **** 2.43E+OO T 0 675.73 16 29 3.34 1352.44 1345 13 4.14E-03 **** 2.27E+OO 0 727. 33 33 25 1. 44 1455.73 1448 13 8.43E-03 74.3 2.15E+OO T 0 816.35 16 11 0.53 1633.90 1628 11 4.07E-03 **** 1. 97E+OO T 0 867.40 26 19 3.86 1736.07 1729 17 6.73E-03 88.3 1. 88E+OO 0 1183. 05 13 13 5.36 2367.85 2360 13 3.61E-03 **** 1.47E+OO 0 1239.39 16 25 2.13 2480.60 2476 9 4.46E-03 **** 1. 42E+OO T 0 1540.81 9 0 0.62 3083.89 3079 10 2.50E-03 66.7 1.18E+OO 0 1848.94 13 2 1. 48 3700.61 3695 10 3.74E-03 70.0 9.99E-01 Flags: "T" = Tentatively associated Page 3879of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:57:46.05 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l * *Acquisition date 3-0CT-2016 05:54:08 Sensitivity 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.41 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:27:00 Nuclide Library : SOLID *
  • Sample ID G405235041 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. ----.Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 *RA-228 TH-228 TH-230 PA-231 TH-232 U-234 AM-243 ANH-511 Le (pCi/GRAM l.709E-01 9. 572E-01 6.063E-02 2.419E-02 2.555E-02 2.197E-02 1.297E-01 3.562E-02 3.693E-02 1.217E-01 3.693E-02 3.817E-01 3.693E-02 8. 962E-02 8. 962E-02 3.562E-02 3. 691E-02 2.948E-01 8. 962E-02 3. 691E-02 3.805E-02 1.899E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 3880 of 5809 Le (pCi/GRAM 9.013E+OO 3.492E-02 0.000E+OO 1. 960E-02 2.653E-01 O.OOOE+OO 0.000E+OO 3.782E-02 3.211E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 Page 3881of5809 O.OOOE+OO 3.517E-02 3.330E-01 5.822E+OO 3.085E-02 1.115E-01 1. 808E+OO 7.186E+OO O.OOOE+OO l.485E-01. O.OOOE+OO O.OOOE+OO 3.473E-01 6.908E+OO 7.923E-01 O.OOOE+OO 1.339E-01 4.129E+02 2.392E-02 6. 551E-01 1.903E+OO 1.033E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.653E-02 4.354E-02 4.907E+OO 3.308E-01 3.308E-01 1.920E-02 5.654E-02 1.507E-01 O.OOOE+OO O.OOOE+OO 1. 063E-01 7.659E-01 6.222E-02 2.616E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.936E-02 O.OOOE+OO 3.612E-02 1.007E-01 O.OOOE+OO O.OOOE+OO 8.243E-02 O.OOOE+OO O.OOOE+OO 2.148E+Ol O.OOOE+OO 2.375E-01 3.742E-02 3.264E+OO 3.278E-02 O.OOOE+OO 5.832E+02 O.OOOE+OO 1.390E-02 6.245E-02 1.383E-01 8.526E-02 9.310E-02 1.296E+OO 4.126E-02 1. 723E+Ol 1.831E-01 4.605E-02 1.906E-02 3.456E+OO 7.004E-01 2.491E+OO SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3882of5809 2.491E+:Ol 8.802E+Ol 3.615E-01 1.970E+OO 3.154E-02 2.790E+OO 4.700E-01 4.460E-01 2.753E-01 4.043E-01 1.672E-01 1. 672E-01 3.561E-01 4.043E-01 3.935E-02 1. 788E-01 2.502E+OO 9.821E-01 1.433E-01 3.935E-02 O.OOOE+OO 9.821E-01 2.023E-01 2.590E+02 1.155E-01 6.873E-02 4.808E-02 2.528E-02 2.700E-02 8.589E-02 NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. fAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:57:52.29 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235041.CNF;l *
  • Acquisition date 3-0CT-2016 05:54:08 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.41 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:27:00 Nuclide Library : SOLID *
  • Sample ID G405235041 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM *
  • Quantity Err(%) : 1.1020E-03 % *
  • Wet wt corr 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 1-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1.183E+Ol 1. 380E+OO 1.380E+OO CD-109 6.777E-01 2.977E+OO 2.977E+OO SN-126 4.268E-02 1.875E-01 1. 875E-:-Ol BA-137M 3.794E-02 4.639E-02 4.639E-02 CS-137 4.008E-02 4. 901E-02 4. 901E-02 TL-208 2.731E-01 8.164E-02 8.164E-02 BI-211 8.826E-03 8.817E-01 8.817E-01 PB-212 8. 071E-01 l.211E-01 l.211E-01 BI-214 7.942E-01 l.631E-01 l.631E-01 PB-214 8.029E-01 l.702E-01 l.702E-01 RN-222 7.942E-01 1. 631E-01 1.631E-01 RA-224 1. 221E+OO 1.577E+OO 1.577E+OO RA-226 7.942E-01 1. 631E-01 l.631E-01 AC-228 6.291E-01 2.485E-01 2.485E-01 RA-228 6.291E-01 2.485E-01 2.485E-01 TH-228 8. 071E-01 l.211E-01 1.211E-01 TH-230 7.939E-01 1.630E-01 1.630E-01 PA-231 7.547E-01 5.645E-01 5.645E-01 TH-232 6.291E-01 2.485E-01 2.485E-01 U-234 7.939E-01 1.630E-01 l.630E-01 AM-243 1.922E-01 l.218E-01 l.218E-01 ANH-511 9.561E-02 8.572E-02 8.572E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) BE-7 -2.191E-01 1.151E+Ol 1.151E+Ol NOT IDENT. NA-22 -3.133E-03 4.147E-02 4.149E-02 NOT IDENT. NA-24 l.OOOE+41 1. 700E+41 O.OOOE+OO SHORT HLIF AL-26 9.807E-03 l.933E-02 1.983E-02 NOT IDENT. SC-46 -5.154E-02 3.074E-01 3.082E-01 FAIL ABUN V-48 2.863E+03 1.631E+04 1.636E+04 SHORT HLIF CR-51 -l.913E+02 4 .115E+02 4.204E+02 SHORT HLIF MN-54 -l.507E-02 4.487E-02 4.538E-02 NOT IDENT. Page 3883 of 5809 C0-56 2.359E-01 3.184E-01 3.357E-01 FAIL ABUN MN-56 l.000E+41 1.330E+41 O.OOOE+OO SHORT HLIF C0-57 2.007E-02 3.756E-02 3.864E-02 NOT IDENT. C0-58 -5.366E-01 5.512E-01 6.020E-01 NOT IDENT. FE-59 -2.765E+OO 7.135E+OO 7.243E+OO NOT IDENT. C0-60 l.676E-02 3.302E-02 3.387E-02 NOT IDENT. ZN-65 3.236E-02 1.379E-01 1. 38 6E-01 NOT IDENT. GE-68 3.568E-Ol 1. 967E+OO 1.974E+OO NOT IDENT. AS-73 7 .118E-01 7.668E+OO 7.675E+OO NOT IDENT. AS-74 -7.144E+02 6.412E+03 6.420&+03 SHORT HLIF SE-75 3.921E-02 l.560E-01 1.570E-01 NOT IDENT. BR-77 l.436E+39 1.275E+40 O.OOOE+OO SHORT HLIF SR-82 -1. 409E+02 6.620E+02 6.650E+02 SHORT HLIF RB-83 -7.956E-02 5.153E-01 5.165E-01 NOT IDENT. KR-85 l.199E+Ol 6.713E+OO 8.619E+OO NOT IDENT. SR-85 l.374E+OO 7.701E-01 9.882E-01 NOT IDENT. RB-86 -1. 011E+03 3.086E+04 3.086E+04 SHORT HLIF Y-88 -3.347E-02 l.661E-01 l.668E-01 NOT IDENT. Y-91 -8.323E+Ol 4.945E+02 4.959E+02 NOT IDENT. NB-94 3.764E-03 2.770E-02 2.775E-02 NOT IDENT. NB-95 -2.157E-01 7.525E-01 7.588E-01 NOT IDENT. NB-95M 6.486E-01 2.188E+OO 2.207E+OO NOT IDENT. ZR-95 -4.732E-01 1.214E+OO l.232E+OO NOT IDENT. NB-97 1.000E+41 2 .113E+41 O.OOOE+OO SHORT HLIF ZR-97 1. 000E+41 2.218E+41 O.OOOE+OO SHORT HLIF M0-99 -6.514E+32 9.682E+32 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 2.065E+41 O.OOOE+OO SHORT HLIF RH-101 7.707E-04 2.980E-02 2.980E-02 NOT IDENT. RH-102 7.192E-03 4.975E-02 4.986E-02 NOT IDENT. RU-103 4.882E+OO 4.920E+OO 5.390E+OO FAIL ABUN RH-106 -6.489E-02 4.481E-01 4.490E-01 NOT IDENT. RU-106 -6.489E-02 4.481E-01 4.490E-01 NOT IDENT. AG-108M -l.657E-03 2.181E-02 2.183E-02 NOT IDENT. AG-llOM -2.353E-02 6.820E-02 6.902E-02 NOT IDENT. SN-113 -1.516E-01 1. 872E-01 1.992E-01 NOT IDENT. CD-115 l.503E+40 2.640E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 6. 715E+04 1.187E+05 l.225E+05 SHORT HLIF TE-123M 4.146E-02 1.181E-01 l.195E-01 NOT IDENT. SB-124 -5.395E-01 1.225E+OO l.249E+OO NOT IDENT. SB-125 -5.858E-02 7.813E-02 8.247E-02 FAIL ABUN TE-125M 3.575E+02 2.634E+02 3.088E+02 NOT IDENT. I-126 6.654E+04 1.294E+06 l.294E+06 SHORT HLIF SB-126 9.420E+05 l.660E+06 l.713E+06 SHORT HLIF SB-127 -3.575E+22 9.264E+22 O.OOOE+OO SHORT HLIF I-131 -5.677E+09 8.053E+09 8.450E+09 SHORT HLIF I-132 -1. OOOE+41 1.909E+42 O.OOOE+OO SHORT HLIF TE-132 4.747E+26 1.695E+27 O.OOOE+OO SHORT HLIF BA-133 5.065E-03 3.547E-02 3.554E-02 NOT IDENT. I-133 -1. OOOE+41 2.594E+41 0.000E+OO SHORT HLIF CS-134 2.947E-02 3.599E-02 3.836E-02 NOT IDENT. CS-135 -3.974E-02 1.121E-01 l.135E-01 NOT IDENT. I-135 1.000E+41 7.026E+41 O.OOOE+OO SHORT HLIF CS-136 -4.347E+04 4.022E+05 4.026E+05 SHORT HLIF CE-139 -2.894E-02 8.780E-02 8.876E-02 NOT IDENT. BA-140 -8.930E+05 l.664E+06 1.712E+06 SHORT HLIF LA-140 -7.616E+04 6.030E+05 6.040E+05 SHORT HLIF CE-141 -4.633E+OO 2.484E+Ol 2.493E+Ol NOT IDENT. CE-143 -l.000E+41 3.231E+41 0.000E+OO SHORT HLIF CE-144 -2.477E-01 2.931E-01 3.136E-01 NOT IDENT. PM-144 -7.349E-03 4.539E-02 4. 551E-02 FAIL ABUN PR-144 -6.410E-01 3.959E+OO 3. 969E+OO NOT IDENT. PM-146 4.002E-02 3.292E-02 3.754E-02 NOT IDENT. ND-147 -2.792E+07 4.122E+07 4.309E+07 SHORT HLIF PM-147 -2.057E+02 6.736E+02 6.799E+02 NOT IDENT. PM-149 6.814E+40 4.470E+41 O.OOOE+OO SHORT HLIF EU-150 -l.533E-02 1. 961E-02 2.080E-02 FAIL ABUN EU-152 -3.274E-02 7.625E-02 7.766E-02 NOT IDENT. GD-153 -2.430E-02 l.542E-01 l.546E-01 NOT IDENT. EU-154 -7.654E-03 l.013E-01 l.013E-01 NOT IDENT. EU-155 l.440E-01 9.226E-02 l.128E-01 FAIL ABUN TB-160 -l.598E-01 1.485E+OO l.487E+OO FAIL ABUN H0-166M 4.164E-02 4. l 72E-02 4.574E-02 NOT IDENT. TM-171 3.747E+OO 1. 817E+Ol 1.825E+Ol NOT IDENT. HF-172 1. 520E-01 l.943E-01 2.060E-01 NOT IDENT. LU-172 -1. 882E-02 5.674E-02 5.737E-02 FAIL ABUN LU-176 -1.850E-04 2.079E-02 2.079E-02 FAIL ABUN HF-181 -l.030E+00 4.586E+OO 4.610E+OO NOT IDENT. TA-182 8.049E-02 8.034E-01 8.043E-01 FAIL ABUN Page 3884 of 5809 RE-183 7.150E-01 2.594E+OO 2.614E+OO NOT IDENT. RE-184 -9.123E+OO 2.957E+Ol 2.986E+Ol NOT IDENT. W-188 -7.636E+Ol l.153E+02 1. 203E+02 NOT IDENT. IR-192 -1. 241E-01 4.075E-01 4 .113E-01 FAIL ABUN HG-203 1.115E+OO 2.027E+OO 2.088E+00 NOT IDENT. BI-207 -5.187E-03 3. 713E-02 3.720E-02 FAIL ABUN PB-210 2.871E-01 2. 941E+OO 2.944E+00 NOT IDENT. PB-211 1. 67 5E-01 5. 051E-01 5.107E-01 NOT IDENT. BI-212 9. 611E-01 7.014E-01 8.244E-01 FAIL ABUN RN-219 9.597E-02 2. 996E-01 NOT IDENT. RA-223 1.121E-01 4.308E-01 4.337E-01 FAIL ABUN AC-227 3.136E-02 1.768E-01 1.774E-01 FAIL ABUN TH-227 3.136E-02 1. 768E-01 l.774E-01 FAIL ABUN TH-229 -l.910E-01 3.873E-01 3. 967E-01 FAIL ABUN TH-231 1.121E-01 4.308E-01 4.337E-01 FAIL ABUN PA-233 -1.434E-02 4.450E-02 4.497E-02 FAIL ABUN PA-234 6.026E-03 2.017E-01 2.018E-01 NOT IDENT. PA-234M -2.242E+OO 3.003E+OO 3.169E+OO NOT IDENT. TH-234 1. 378E-01 1.032E+OO l.033E+00 FAIL ABUN U-235 8.410E-02 l.545E-01 1.591E-01 FAIL ABUN NP-237 -l.434E-02 4.450E-02 4.497E-02 FAIL ABUN NP-238 -l.000E+41 7.561E+41 O.OOOE+OO SHORT HLIF U-238 1. 378E-01 1.032E+OO l.033E+00 FAIL ABUN NP-239 3.654E-01 5.053E-01 5.315E-01 FAIL ABUN PU-239 1.305E+02 2.816E+02 2.877E+02 NOT IDENT. AM-241 5.439E-02 l.190E-01 l.215E-01 NOT IDENT. CM-243 -1.148E-01 8.702E-02 l.012E-01 NOT IDENT. BK-247 -3.643E-03 5.212E-02 5.215E:....02 NOT IDENT. CM-247 7.164E-03 2.742E-02 2.761E-02 NOT IDENT. CF-249 1. 758E-02 2. 801E-02 2. 911E-02 NOT IDENT. CF-251 -2.456E-03 8.975E-02 8.976E-02 NOT IDENT. Page 3885 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 63.5639 87.09 127. 2108 136.47 87.5808 45.60 77.5038 87.57 127.3091 140.51 0.0000 46.54 64.0330 88.03 127.4031 143.76 72.3906 49. 72 0.0000 88.34 127.4672 144.24 74.8864 51. 35 57.3219 88.47 127.4937 145.44 87.2842 51. 87 53.1378 89. 96 95.8471 152.43 86.7427 52.39 61. 7115 1093.63 125.6492 153.25 0.0000 52.97 57.5295 91.11 0.0000 323.87 78.2232 53.44 57.5892 92.59 116.8675 156.02 0.0000 54.07 61.9405 93.35 117.0052 158.56 0.0000 57.36 0.0000 94.56 87.3433 159.00 72. 3956 57.53 73.1602 94.65 87.3549 162.33 70.9864 57.98 65.6907 94.67 87.3578 162.66 0.0000 59.27 68.0267 94.87 87.3845 163.33 62.7029 59.32 77.7527 97.43 84.2620 165.86 77.1224 59.54 77.7879 98.43 85.5444 176.31 67.7938 60. 96 93.1830 98.44 85.5456 176.60 0.0000 61.17 102.9785 99.53 86.8429 177.52 74.6645 62.93 76.1473 100 .11 64.8983 181.07 0.0000 63.29 81.6446 102.03 84.8384 *181.52 74.6245 63.58 72.9776 103.18 93.1293 184.41 64.0739 64.28 74.1690 103.37 102.4711 143.76 76.9876 66.73 75.6177 105.21 63.0466 193.51 87.9125 67.24 82.2733 105.31 63.0555 197.03 80.4233 125.81 79.0488 106.12 86.5093 198.01 78.7660 67.75 79.0587 106.47 97.0795 201.83 63.4116 69.67 95.5084 109.28 69.2820 203.43 73.9444 70.83 89.8233 111. 00 108.2912 205.31 58.8222 72.81 103.0811 111.76 0.0000 210.85 57.8051 72. 87 103.0917 114. 06 85.1061 215.65 62.4507 74.66 103.4245 116. 30 0.0000 222 .11 59.2670 74.82 103.4536 116.74 87.7864 227.09 65.7399 74.97 103.4812 119.76 65 .1114 227.38 57.7590 77 .11 103.8729 121.12 75.1711 228.16 0.0000 78.74 104.1674 121.22 75.1807 228.18 59.5765 79.69 124.1581 121. 78 64.4880 116.74 59.5765 80.12 110. 7764 122.06 59.7328 235.69 61. 7444 80.19 0.0000 122.92 71.7590 235. 96 61. 7578 80.57 110.8615 123.07 72. 9694 238.63 57.4095 81. 00 107.9436 265.00 83. 8011 238.98 0.0000 81. 07 107.9568 125.81 68.4246 240.99 57.5208 81. 75 106.5794 127.23 87.7889 242.00 57.5684 83.79 112.9684 127.91 104.7154 244.70 57.6953 84.00 99.4471 129.30 90.4289 252.40 0.0000 85.43 126.8673 131.20 73.7238 252.80 47.1827 86.55 127.0989 133.02 78.7347 254.15 0.0000 86.79 127.1484 133.52 81. 2064 256.23 50.9497 86.94 127.1792 136.00 79.0204 260.90 0.0000 Page 3886 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 40.2948 355.39 0.0000 584.27 21. 9295 264.80 39.3834 356.01 36.5707 595.83 0.0000 265.00 43. 9697 364.49 0.0000 427.87 23.1875 2 68. 22 59.6878 366.42 0.0000 602.52 0.0000 269.46 50.5532 372. 51 30.5383 604. 72 0.0000 270.03 45. 68 375.05 39.4645 607.,.14 16.6077 271. 23 57.0629 377.52 29.6423 609.32 16.6229 273.65 0.0000 356.01 31. 7370 610.33 16.6302 276.40 51. 7412 388.16 26.8456 614.28 9.9946 277.37 50.8542 388.63 0.0000 618.01 16.6833 277.60 50.8620 391.69 39.8535 620.36 16.6992 278.00 49.9526 264.66 34.0505 621.93 21.7233 279.20 41.6638 401.81 31. 0662 630.19 0.0000 279.54 44.4531 402.40 32.0794 631.29 22.3657 279.70 46.3104 404.85 29.1121 633.25 21. 2644 280.46 52.8240 410.95 33.2417 634.78 0.0000 283.69 50.1625 413.71 29.2572 635.95 25.7692 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 46.5047 423.72 0.0000 645*. 85 22.4976 285.90 0.0000 427.09 30.4901 657.76 11.8672 287.50 48.4379 427.87 33.5532 657.90 0.0000 290.67 60.2194 433.94 30.6030 661. 66 23. 7711 293.27 0.0000 439.40 22.5080 664.57 0.0000 351. 93 44.9609 453.88. 16.0824 666.33 0.0000 295. 96 44.9844 463.37 24.8638 666.50 0.0000 879.38 33.8005 468.07 23.3661 667. 71 0.0000 299.98 26.7854 473.00 0.0000 677.62 18.7935 300.09 26.7872 475.06 21.8857 685.70 0.0000 300.13 26.7878 476.78 20.3399 695.00 0.0000 301.36 42.3331 477.60 25.0439 696. 49 22.9443 302.85 45.2021 482.18 31.3763 696.51 22.9443 256.23 47.5176 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 27.5420 306.78 52.8805 497.08 16.8574 697.49 27.5439 308.46 34.0342 505.52 23.8028 702.65 25.2979 311. 90 42.6425 507.63 0.0000 706.68 13.8193 316.51 49.4313 511. 00 27.5777 711.68 11. 5377 319.41 0.0000 514.00 27.6165 720.70 0.0000 320.08 0.0000 514.00 27.6165 721. 93 0.0000 321.04 49.5815 520.40 14.9154 722. 78 19 .1157 323.87 35.3462 520.69 0.0000 722. 91 19 .1164 325.23 53.5448 522.65 0.0000 723. 31 22.5953 328.76 0.0000 527.90 0.0000 724.19 24.3411 333.37 33.1643 528.26 17.6440 727.33 19.7275 333.97 38.9476 529.59 18.1898 733.00 23.2568 334.37 36.0718 529.87 0.0000 735.93 8.1484 338.28 27. 9663 531.02 0.0000 333.97 11. 6471 338.32 27. 9669 537.26 0.0000 739.50 0.0000 311. 90 34.7659 546.56 0.0000 747.24 15.7791 340.48 34.7659 552.55 30.2752 748.06 10.5223 340.55 0.0000 563.25 27.1617 752.31 22.8333 344.28 42.9818 569.33 20.6978 753.82 0.0000 345.93 34.8867 946.00 16.3416 756.73 21. 9894 351.06 37.9169 569.70 16.3434 756.80 21.9902 351. 93 37.9376 583.19 21. 9198 884.68 20.2822 Page 3887 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 24.7076 1274.44 10.4404 1620.50 6.5889 766.42 22.0650 1001.03 14.2561 1621. 92 3.2953 766.84 16.7717 1002.74 11. 4104 1678.03 0.0000 772. 60 0.0000 1004.73 18.0769 1690.97 3.3391 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.000.0 1025.87 0.0000 1764.48 4.5127 778.90 10.6373 1028.54 0.0000 1063.66 4.5173 783.70 0.0000 1037.84 13.4437 1771. 35 1.5061 785.37 11.5496 1038.76 0.0000 1791.20 0.0000 792.07 12.4666 631. 29 14.4397 1808.65 1.8194 794.95 13.3704 1048.07 0.0000 1810.72 0.0000 795.86 12.4828 1049.04 17.3386 1836.06 4.5706 810.06 21.5024 1050.41 15.4180 810.29 21. 5039 1063.66 15.4736 344.28 22.9383 1077.00 0.0000 810.76 22.9414 1077.34 12.6191 815.77 0.0000 1085.87 12.6485 1048.07 0.0000 1093.63 14.6246 832.01 11.7325 1099.45 23.4346 834.85 17.1631 1112. 07 11.1970 835.71 21. 6863 1112. 84 11. 7590 836.80 0.0000 1115. 54 10.9826 846.75 0.0000 1120.29 11.7817 846.77 8.1617 1120.55 11.7825 856.80 0.0000 1221.41 11.7847 860.56 14.5747 1129. 67 6.8893 871.09 11.6988 1131. 51 0.0000 873.19 16.0966 1147.95 0.0000 875.33 0.0000 1173.23 12.9381 879.38 15.5785 1177.95 12.7539 880.51 13.7508 1189.05 19.4120 883.24 13.7622 1204.77 19.0580 884.68 13.7686 1221.41 17.1214 889.28 16.5460 1231.02 12 .1143 894.76 12.8913 1235.36 0.0000 898.04 17.5133 1238.28 16.1807 900. 72 13.8377 1260.41 0.0000 903.28 21. 234 7 1271.87 17.3300 911. 20 17.5846 1274.44 16.3203 912.08 17.5893 1274.54 16.3213 923.98 0.0000 1291.59 16.3857 926.50 12.0875 1298.22 0.0000 929 .11 13.0276 1312 .11 0.0000 937.49 20.5243 1332.49 9.3043 944.13 0.0000 1362.66 0.0000 946.00 14.0291 1365.19 3.1243 949.00 14.0419 1368. 63 0.0000 667. 71 0.0000 1384.29 5.2295 962. 31 19.7362 1408.01 12.6160 964.08 10.5314 1457.56 0.0000 966 .17 19.5705 1460.82 5.3165 911.20 24.4829 1489.16 6.4175 968. 97 24.4829 1505.03 6.4387 983.53 0.0000 1584.12 7.6328 984.45 0.0000 1596. 21 0.0000 Page 3888 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:57:48.10 ******************************************************************************** GEL LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM08.CNF;320 Background date : Z-OCT-2016 11:00:23. Sample date 30-NOV-2015 13:53:00 Acquisition date : 3-0CT-2016 06:55:55. Sample ID G405235042 Sample quantity 1.76800E+02 GRAM Detector name : GAMOB Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.67 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 3 3 0 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 62.99* 74.79* 76.94* 92.73* 94.82 144.04* 185.86* 213.01 238.59* 241. 76 270. 96 295.37* 300.25 307.48 339.27* 352.15* 370.31 463.41 511. 28* 583.44* 609.45* 661. 7 4 728.09* 733.46 794.49 861. 60* 911. 20* 924.29 971.14* 1001.34* 1028.25 1120.48* 1155. 72 1163.80 Page 3889 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 19 105 124 66 23 5 47 94 234 56 27 101 21 13 66 170 33 30 47 110 121 Bl 34 9 16 14 66 9 23 17 8 24 18 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 93 121 120 150 83 87 92 223 119 49 71 39 44 62 63 83 57 29 22 15 49 29 18 8 8 23 11 2 41 3 19 7 8 9 1. 39 1.18 1.18 1. 48 1. 08 0.88 1. 29 8.20 1. 00 1. 65 0.73 1. 55 1. 55 4.45 1. 39 1. 43 7.15 2.78 2.42 1. 59 1. 46 1. 57 1. 63 1. 77 1. 29 0.73 1.11 0.53 1. 02 0.62 1. 42 1. 57 1. 59 1. 26 126.24 149.84 154.13 185.74 189.91 288.40 372. 09 426.41 477.59 483.93 542.35 591.20 600.95 615.43 679.03 704.81 741.13 927.42 1023.18 1167.56 1219.61 1324.21 1456. 96 1467.71 1589.80 1724.07 1823.30 1849.49 1943.22 2003.65 2057.47 2241.99 2312.49 2328.65 123 144 144 170 170 285 368 412 473 482 537 586 586 607 672 699 733 922 1017 1162 1214 1319 1449 1463 1583 1714 1816 1845 1933 1997 2051 2237 2305 2322 7 5.23E-03 92.6 16 2.91E-02 20.2 1.23E+OO 16 3.45E-02 17.6 23 1.84E-02 39.3 3.36E+OO 23 6.40E-03 75.5 6 l.45E-03298.l 9 1. 31E-02 42. 6 27 2.61E-02 46.0 9 6.50E-02 10.9 6 1. 55E-02 24. 4 10 7.56E-03 61.4 19 2.BlE-02 15.6 1.13E+OO 19 5.85E-03 61.0 12 3.66E-03123.5 14 1.82E-02 29.5 14 4.72E-02 14.1 18 9.30E-03 56.2 12 8.28E-03 40.9 19 1. 31E-02 35. 4 14 3.07E-02 12.2 14 3.37E-02 15.5 11 2.24E-02 17.2 15 9.58E-03 33.5 7 2.43E-03 65.1 11 4.36E-03 43.5 19 3.97E-03 87.4 15 1.82E-02 17.1 7 2. 51E-03 41. 5 16 6.49E-03 67.1 13 4.76E-03 35.7 10 2.12E-03115.0 10 6.79E-03 30.3 17 4.94E-03 44.4 12 2.63E-03 70.8 Peak Search Report (continued) Page : 2 Sample ID : G405235042 Acquisition date 3-0CT-2016 06:55:55 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1168. 05 10 7 1. 08 2337.17 2333 9 2.76E-03 57.1 36 0 1261.90 12 7 1. 33 2524.91 2519 11 3.41E-03 52.5 0 1301.59 13 0 0.83 2604.31. 2599 10 3. 61E-03 27.7 38 0 1460.69 305 4 2.03 2922.58 2915 15 8.48E-02 5.9 39 0 1764.43* 18 0 1.18 3530.17 3523 13 4.88E-03 28.1 Flag: "*" = Peak area was modified by background subtraction Page 3890 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:57:50 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 13:53:00 G405235042 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 06:55:55 176.80 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAS 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3891of5809 PB-214 U-235 PB-214 PB-214 PB-214 PB-214 Line 242.00 143.76 74.82 74.82 74.82 351.93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 CE-141 AM-243 TH-228 PB-212 BI-211 Line 240.99 145.44 74.66 74.82 74.82 351.06 CAN 0 01:00:00.67 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235042 Acquisition date 3-0CT-2016 06:55:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40

  • 1460.82 10.66* 9. 6;72E-01 1.233E+Ol 1.233E+Ol 11. 78 BA-137M 661.66 89.90* 1.815E+OO 2. 313E-01 2.358E-01 34.47 OK CS-137 661.66 85.10* 1. 815E+OO 2.443E-01 2.491E-01 34.47 OK TL-208 277.37 6.60 3.710E+OO Line Not Found Absent 583.19 85.00* 2.006E+OO 3.083E-01 3.083E-01 24.40 OK 860.56 12.50 1.477E+OO 3.489E-01 3.489E-01 174.76 OK PB-212 74.82 10.28 3.316E+OO l.414E+OO 1.414E+OO 54.34 OK 77 .11 17.10 3.509E+OO l.258E+00 1.258E+OO 35.22 OK 238.63 43.60* 4.174E+OO 6.871E-01 6. 871E-01 21. 74 OK 300.09 3.30 3.477E+OO 9.534E-01 9.534E-01 121.97 OK BI-214 609.32 45.49* l.937E+OO 6.508E-01 6. 511E-01 30.99 OK 1120.29 14.92 l.202E+OO 5. 911E-01 5. 913E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 OK PB-214 74.82 5.80 3.318E+OO Line Not Found <<INT Reject 77 .11 9.70 3.509E+OO 2.218E+OO 2.218E+OO 35.22 OK 87.09 3.41 4.288E+OO Line Not Found Absent 242.00 7.25 4.130E+OO Line Not Found <<INT Reject 295.22 18.42 3.525E+OO 8. llOE-01 8 .113E-01 31.12 OK 351.93 35.60* 3.044E+00 7.984E-01 7.987E-01 28.20 OK RN-222 609.32 45.49* 1.937E+OO 6.508E-01 6. 511E-01 30.99 OK 1120.29 14.92 1. 202E+OO 5. 911E-01 5. 913E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 OK RA-224 240.99 4.10* 4.133E+OO 3.237E-01 3.237E-01 298.89 OK RA-226 609.32 45.49* 1.937E+OO 6.508E-01 6. 511E-01 30.99 OK 1120.29 14.92 1.202E+OO 5. 911E-01 5.913E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 OK TH-228 74.82 10.28 3.316E+OO l.414E+OO l.414E+00 54.34 OK 77 .11 17.10 3.509E+OO 1.258E+OO 1.258E+OO 35.22 OK 238.63 43.60* 4.174E+OO 6.871E-01 6. 871E-01 21.74 OK 300.09 3.30 3.477E+OO 9.534E-01 9.534E-01 121.97 OK TH-230 609.32 45.49* 1.937E+OO 6.508E-01 6.508E-01 30.99 OK 1120.29 14.92 1. 202E+OO 5. 911E-01 5. 911E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.677E-01 56.10 OK PA-231 283.69 1. 70 3.643E+00 Line Not Found Absent 301.36 5.35* 3.477E+OO 5.881E-01 5. 881E-01 121. 97 OK TH-234 63 .29 3.70* 2.108E+OO 1.498E+OO 1.498E+OO 185.14 OK 92.59 4.23 4.622E+OO 2.017E+OO 2.017E+OO 78.54 OK U-234 609.32 45.49* l.937E+OO 6.508E-01 6.508E-01 30.99 OK 1120.29 14.92 1. 202E+OO 5. 911E-01 5. 911E-01 60.69 OK 1764.49 15.30 8.180E-01 5.677E-01 5.677E-01 56.10 OK U-235 89. 96 3.47 4.467E+00 Line Not Found Absent 93.35 5.60 4.622E+OO 1.523E+OO 1.523E+OO 78.54 OK 143.76 10. 96* 5.442E+OO 4.947E-02 4.947E-02 596 .16 OK 163.33 5.08 5.246E+OO Line Not Found Absent 185. 72 57.20 4.930E+00 9.198E-02 9.198E-02 85 .11 OK 205.31 5.01 4.641E+OO Line Not Found Absent U-238 63.29 3.70* 2.108E+OO 1.498E+OO 1.498E+00 185.14 OK 92.59 4.23 4.622E+OO 2.017E+OO 2.017E+OO 78.54 OK AM-243 43.53 5.90 2.327E-01 Line Not Found Absent Page 3892 of 5809 Nuclide Line Activity Report (continued) Page : 3 3-0CT-2016 06:55:55 Sample ID : G405235042 Acquisition date Nuclide Type: Nuclide ANH-511 Energy 7.4. 66 511. 00 %Abn 67.20* 100.00* Flag: "*" = Keyline Page 3893 of 5809 %Eff 3.316E+OO 2.232E+OO Uncorrected Decay Corr 2-Sigma pCi/GRAM pCi/GRAM %Error 2.163E-01 2.163$-01 54.34 1.023E-01 1.023E-01 70.85 Status OK OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:57:51.10 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l *
  • Acquisition date 3-0CT-2016 06:55:55 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.67 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:53:00 Analyst initials: MXRl * *Sample ID G405235042 Sample Quantity l.7680E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1. 96-sigma) K-40 l.233E+Ol 1.423E+00 BA-137M 2.358E-01 7. 965E-02 CS-137 2. 491E-01 8.415E-02 TL-208 3.083E-01 7.372E-02 PB-212 6.871E-01 1.464E-01 BI-214 6.511E-01 l.977E-01 PB-214 7.987E-01 2.207E-01 RN-222 6. 511E-01 1.977E-01 RA-224 3.237E-01 9.481E-01 RA-226 6. 511E-01 1.977E-01 TH-228 6. 871E-01 l.464E-01 TH-230 6.508E-01 1. 976E-01 PA-231 5.881E-01 7.029E-01 TH-234 1.498E+OO 2. 718E+OO U-234 6.508E-01 1. 976E-01 U-235 4.947E-02 2.890E-01 U-238 1.498E+OO 2.718E+OO AM-243 2.163E-01 l.152E-01 ANH-511 l.023E-01 7.103E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 3894 of 5809 Key-Line Activity (pCi/GRAM 1.495E+Ol -1.235E-02 O.OOOE+OO 8.641E-03 7.510E-02 O.OOOE+OO 0.000E+OO 3.215E-02 -2.901E-01 O.OOOE+OO 1. 767E-02 K.L. Cnt Uncert * ( 1. 9 6-sigma) 1.265E+Ol 3.734E-02 1. 960E+41 1. 952E-02 4.817E-01 1. 689E+04 4.524E+02 4.896E-02 4.658E-01 l.617E+41 4.884E-02 MDA (pCi/GRAM 6.159E-01 6.643E-02 7.018E-02 6.311E-02 1.0lOE-01 1.309E-01 1.220E-01 l.309E-01 1.062E+OO 1.309E-01 1.0lOE-01 1.309E-01 6.746E-01 2.540E+OO 1.309E-01 3.150E-01 2.540E+OO 9.787E-02 4.036E-02 MDA (pCi/GRAM 2.850E+Ol 7.060E-02 O.OOOE+OO 5.458E-02 9.700E-01 O.OOOE+OO O.OOOE+OO l .131E-01 8.545E-01 O.OOOE+OO 9.585E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 -4.666E-01 5.904E-01 1.055E+OO NOT IDENT. FE-59 -5.049E+OO 7.984E+OO 1.408E+Ol NOT IDENT. C0-60 5.863E-03 3.677E-02 7.723E-02 NOT IDENT. ZN-65 3.864E-02 l.443E-01 2.827E-01 NOT IDENT. GE-68 -1.369E+OO 2.448E+OO 4.398E+OO NOT IDENT. AS-73 -1.025E+Ol l.199E+Ol 2.243E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.929E+03 O.OOOE+OO SHORT HLIF SE-75 5.548E-02 2.054E-01 4.219E-01 NOT IDENT. BR-77 O.OOOE+OO 2.623E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.896E+02 O.OOOE+OO SHORT HLIF RB-83 -9.802E-02 5.823E-01 1.069E+OO NOT IDENT. KR-85 6.097E+OO 5.934E+OO l.322E+Ol NOT IDENT. SR-85 6.954E-01 6.805E-01 l.515E+OO NOT IDENT. RB-86 O.OOOE+OO 3.924E+04 O.OOOE+OO SHORT HLIF Y-88 3.127E-02 6.945E-02 2.753E-01 NOT IDENT. Y-91 -5.682E+Ol 5.592E+02 1.082E+03 NOT IDENT. NB-94 -1.328E-02 2.623E-02 5.022E-02 NOT IDENT. NB-95 -2.528E-01 8.902E-01 l.730E+00 NOT IDENT. NB-95M -4.655E-01 2.690E+00 4.769E+OO NOT IDENT. ZR-95 4.518E-01 1.375E+OO 2. 967E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.331E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.027E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.838E+41 O.OOOE+OO SHORT HLIF RH-101 9.922E-03 3.491E-02 6.760E-02 NOT IDENT. RH-102 -8.216E-03 4.404E-02 8.467E-02 NOT IDENT. RU-103 2.616E+OO 5.933E+OO l.239E+Ol FAIL ABUN RH-106 '-3 .17 5E-01 4.677E-01 7. 996E-01 NOT IDENT. RU-106 -3.175E-01 4.677E-01 7. 996E-01 NOT IDENT. AG-108M -6. 2 66E-03 2.733E-02 5.201E-02 NOT IDENT. CD-109 8.134E-02 l.168E+00 2.260E+OO NOT IDENT. AG-llOM -1.853E-02 9.769E-02 1.924E-01 NOT IDENT. SN-113 -4.937E-02 2.262E-01 4.350E-01 NOT IDENT. CD-115 O.OOOE+OO 3.202E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.378E+05 O.OOOE+OO SHORT HLIF TE-123M 2.142E-02 l.354E-01 2.566E-01 NOT IDENT. SB-124 1.157E-02 l.920E+OO 4.303E+OO NOT IDENT. SB-125 8.939E-02 1.008E-01 2.176E-01 FAIL ABUN TE-125M -1.322E+02 3.099E+02 5.665E+02 NOT IDENT. I-126 O.OOOE+OO 1.659E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1. 785E+06 O.OOOE+OO SHORT HLIF SN-126 3.738E-02 7.618E-02 1.516E-01 FAIL ABUN SB-127 O.OOOE+OO 8.020E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.060E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.057E+27 0.000E+OO SHORT HLIF BA-133 1.310E-02 3.859E-02 7. 271E-02 NOT IDENT. I-133 O.OOOE+OO l.241E+41 O.OOOE+OO SHORT HLIF CS-134 7.066E-02 6.025E-02 9.993E-02 FAIL ABUN CS-135 7.375E-04 1.330E-01 2. 411E-01 NOT IDENT. I-135 O.OOOE+OO l.030E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.564E+05 O.OOOE+OO SHORT HLIF CE-139 -7.099E-02 1. 12 6E-01 1. 968E-01 NOT IDENT. BA-140 O.OOOE+OO l.762E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.662E+05 O.OOOE+OO SHORT HLIF CE-141 7.939E+OO 4.638E+Ol 5.258E+Ol FAIL ABUN CE-143 O.OOOE+OO 1.507E+41 O.OOOE+OO SHORT HLIF CE-144 -3.430E-02 3.694E-01 6.850E-01 NOT IDENT. PM-144 -l.214E-03 4. 960E-02 l.016E-01 NOT IDENT. PR-144 -5.977E-02 4.334E+OO 8.886E+OO NOT IDENT. PM-146 4.624E-03 4.204E-02 8.344E-02 NOT IDENT. ND-147 O.OOOE+OO 4.802E+07 O.OOOE+OO SHORT HLIF PM-147 2.994E+02 8. 013E+02 1.581E+03 .NOT IDENT. PM-149 O.OOOE+OO 1. 792E+41 O.OOOE+OO SHORT HLIF EU-150 9.557E-03 2.385E-02 4.526E-02 FAIL ABUN EU-152 -3.597E-03 8.187E-02 l.468E_.:01 NOT IDENT. GD-153 1.846E-01 1. 7 94E-Ol* 3.565E-01 NOT IDENT. EU-154 -3.016E-02 9 .116E-02 l.724E-01 NOT IDENT. EU-155 3.030E-02 1.114E-01 2.189E.:.01 NOT IDENT. TB-160 -3.385E-01 2.036E+OO 4.000E+OO NOT IDENT. H0-166M -3.375E-02 5. 772E-02 1.082E-01 FAIL ABUN TM-171 1.165E+Ol 2.787E+Ol 5.840E+Ol NOT IDENT. HF-172 -5.657E-02 2.454E-01 .4.555E-01 FAIL ABUN LU-172 -8. 596E-02 7.803E-02 1.271E-01 FAIL ABUN LU-176 2.135E-02 5.166E-02 3.864E-02 FAIL ABUN HF-181 2.002E+OO 4.765E+OO 9.808E+OO NOT IDENT. TA-182 2.198E-01 9.055E-01 1.857E+OO FAIL ABUN RE-183 -4.373E-02 3.753E+OO 7.573E+OO NOT IDENT. Page 3895 of 5809 RE-184 -1.125E+OO 3.339E+Ol 6. 727E+Ol NOT IDENT. W-188 1.987E+Ol 1.196E+02 2.197E+02 FAIL ABUN IR-192 -4.992E-01 4.595E-01 8.093E-01 FAIL ABUN HG-203 -3.595E+OO 2.484E+OO 4.248E+OO NOT IDENT. BI-207 6.315E-03 3.790E-02 8.061E-02 FAIL ABUN PB-210 -3.347E+OO 5.445E+OO 1.058E+Ol NOT IDENT. BI-211 O.OOOE+OO 6.079E-01 7.644E-01 FAIL ABUN PB-211 5.547E-02 6.223E-01 1.238E+OO NOT IDENT. BI-212 0.000E+OO 9.296E-01 1.302E+OO FAIL ABUN RN-219 -1.052E-01 6.507E-01 FAIL ABUN RA-223 4 .151E-02 5.534E-01 1.082E+OO FAIL ABUN AC-227 -6.853E-02 1.989E-01 3.892E-01 FAIL ABUN TH-227 -6.853E-02 l.989E-01 3.892E-01 FAIL ABUN AC-228 O.OOOE+OO 2.700E-01 5.024E-01 FAIL ABUN RA-228 O.OOOE+OO 2.700E-01 5.024E-01 FAIL ABUN TH-229 -4.067E-02 4 .114E-01 8.342E-01 NOT IDENT. TH-231 4.151E-02 5.534E-01 1.082E+OO FAIL ABUN TH-232 O.OOOE+OO 2.700E-01 5.024E-01 FAIL ABUN PA-233 -l.259E-02 6.296E-02 l.165E-01 FAIL ABUN PA-234 -l.738E-01 2.461E-01 4.376E-01 FAIL ABUN PA-234M 6. 851E+OO 4.793E+OO 8.846E+OO FAIL ABUN NP-237 -l.259E-02 6.296E-02 l.165E-01 FAIL ABUN NP-238 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF NP-239 4.936E-02 2.323E-01 4.536E-01 NOT IDENT. PU-239 9. 967E+Ol 3 .116E+02 6.049E+02 NOT IDENT. AM-241 1.412E-01 l.644E-01 3.327E-01 NOT IDENT. CM-243 -5.309E-02 1.008E-01 l.857E-01 NOT IDENT. BK-247 2'.102E-02 6. 631E-02 1.371E-01 . NOT IDENT. CM-247 3.517E-03 3.081E-02 6.187E-02 NOT IDENT. CF-249 6.041E-03 3.398E-02 6.864E-02 NOT IDENT. CF-251 2.810E-02 1.029E-01 2.153E-01 NOT IDENT. Page 3896 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:57:49.01 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 299 10.66* 9. 672E-01 l.233E+Ol l.233E+Ol 11.78 BA-137M 661.66 89 89.90* 1. 815E+OO 2.313E-01 2.358E-01 34.47 CS-137 661.66 89 85.10* 1. 815E+OO 2.443E-01 2.491E-01 34.47 CE-141 145.44 7 48.29* 5.442E+OO l.123E-02 7.939E+OO 596.16 TL-208 277.37 ------6.60 3.710E+OO ------Line Not Found ------583.19 124 85.00* 2.006E+OO 3.083E-01 3.083E-01 24.40 860.56 15 12.50 1.477E+OO 3.489E-01 3.489E-01 174.76 BI-211 72.87 ------1. 23 3.135E+OO ------Line Not Found ------351.06 204 12.92* 3.044E+OO 2.200E+OO 2.200E+OO 28.20 PB-212 74.82 150 10.28 3.316E+OO 1. 871E+OO 1. 871E+OO 40.34 77 .11 178 17.10 3.509E+OO l.258E+OO 1.258E+OO 35.22 238.63 295 43.60* 4.174E+OO 6.871E-01 6. 871E-01 21. 74 300.09 26 . 3.30 3.477E+OO 9.534E-01 9.534E-01 121. 97 BI-214 609.32 135 45.49* 1.937E+OO 6.508E-01 6.511E-01 30.99 1120.29 25 14.92 1.202E+OO 5. 911E-01 5. 913E-01 60.69 1764.49 17 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 PB-214 74.82 150 5.80 3.316E+OO 3.317E+OO 3.318E+OO 40.34 77 .11 178 9.70 3.509E+OO 2.218E+OO 2.218E+OO 35.22 87.09 ------3.41 4.288E+OO ------Line Not Found ------242.00 70 7.25 4.133E+OO 9.941E-01 9.945E-01 48.83 295.22 124 18.42 3.525E+OO 8. llOE-01 8 .113E-01 31.12 351. 93 204 35.60* 3.044E+OO 7.984E-01 7.987E-01 28.20 RN-222 609.32 135 45.49* 1.937E+OO 6.508E-01 6. 511E-01 30.99 1120.29 25 14.92 1.202E+OO 5. 911E-01 5.913E-01 60.69 1764.49 17 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 RA-224 240.99 70 4.10* 4.133E+OO 1. 758E+OO 1. 758E+OO 48.83 RA-226 609.32 135 45.49* 1.937E+OO 6.508E-01 6. 511E-01 30.99 1120.29 25 14.92 1.202E+OO 5. 911E-01 5.913E-01 60.69 1764.49 17 15.30 8.180E-01 5.677E-01 5.679E-01 56.10 TH-228 74.82 150 10.28 3.316E+OO 1.871E+OO 1.871E+OO 40.34 77 .11 178 17.10 3.509E+OO l.258E+OO l.258E+OO 35.22 238.63 295 43.60* 4.174E+OO 6.871E-01 6.871E-01 21.74 300.09 26 3.30 3.477E+OO 9.534E-01 9.534E-01 121. 97 TH-230 609.32 135 45.49* 1.937E+OO 6.508E-01 6.508E-01 30.99 1120.29 25 14.92 l.202E+OO 5. 911E-01 5. 911E-01 60.69 1764.49 17 15.30 8.180E-01 5.677E-01 5.677E-01 56.10 PA-231 283.69 ------1. 70 3.643E+00 ------Line Not Found ------301.36 26 5.35* 3.477E+OO 5.881E-01 5.881E-01 121.97 TH-234 63.29 28 3.70* 2.108E+OO 1.498E+OO l.498E+00 185.14 92.59 93 4.23 4.622E+OO 2.017E+00 2.017E+OO 78.54 U-234 609.32 135 45.49* 1.937E+OO 6.508E-01 6.508E-01 30.99 1120.29 25 14.92 1.202E+OO 5. 911E-01 5. 911E-01 60.69 1764.49 17 15.30 8.180E-01 5.677E-01 5.677E-01 56.10 U-235 89. 96 ------3.47 4.467E+OO ------Line Not Found ------93.35 93 5.60 4.622E+OO l.523E+OO 1.523E+OO 78.54 143.76 7 10. 96* 5.442E+OO 4.947E-02 4.947E-02 596 .16 163.33 ------5.08 5.246E+OO ------Line Not Found ------Page 3897of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235042 Acquisition date 3-0CT-2016 06:55:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 185. 72 ..61 57.20 4.930E+OO 9.198E-02 85 .11 205.31 ------5.01 4.641E+OO ------Line Not Found ------U-238 63.29 28 3.70* 2.108E+OO 1.498E+OO 1. 498E+OO 185.14 92.59 93 4.23 4.622E+OO 2.017E+OO 2.017E+OO 78.54 AM-243 43.53 ------5.90 2.327E-01 ------Line Not Found ------74.66 150 67.20* 3.316E+OO 2.863E-01 2.863E-01 40.34 ANH-511 511. 00 54 100.00* 2.232E+OO l.023E-01 l.023E-01 70.85 Flag: "*" Key line Page 3898 of 5809 Summary of Nuclide Activity Sample ID : G405235042 Acquisition date Page : 3 3-0CT-2016 06:55:55 Total number of lines in spectrum 39 Number of unidentified lines 7 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 BA-137M CS-137 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 30.08Y 30.08Y 32. 51D l.41E+10Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600. OOY 1.41E+l0Y 7.54E+04Y 7.04E+08Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 02 1. 02 707. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.233E+Ol 2. 313E-Ol 2.443E-01 l.123E-02 3.083E-Ol 2.200E+OO 6. 871E-01 6.508E-01 7.984E-01 6.508E-Ol 1.758E+OO 6.508E-01 6.871E-01 6.508E-01 5.881E-01 1.498E+OO 6.508E-01 4.947E-02 1.498E+OO 2.863E-01 1.023E-01 2.653E+Ol 2.653E+Ol c Decay Corr pCi/GRAM l.233E+Ol 2.358E-01 2.491E-01 7.939E+OO 3.083E-01 2.200E+OO 6. 871E-01 6. 511E-01 7.987E-01 6. 511E-Ol 1.758E+OO 6. 511E-01 6. 871E-01 6.508E-01 5.881E-01 l.498E+OO 6.508E-01 4.947E-02 1.498E+OO 2.863E-01 1.023E-01 3.447E+Ol 3.447E+Ol 82.05% Decay Corr 2-Sigma Error 0.145E+Ol 0.813E-01 0.859E-01 47.33E+OO 0.752E-01 0.620E+OO 1.494E-01 2.017E-01 2.252E-01 2.017E-01 0.858E+00 2.017E-01 l.494E-01 2.017E-01 7.173E-01 2.773E+OO 2.017E-01 29.49E-02 2.773E+OO l.155E-01 0.725E-01 2-Sigma %Error 11. 78 34.47 34.47 .596 .16 24.40 28.20 21. 74 30.99 28.20 30.99 48.83 30.99 21. 74 30.99 121. 97 185.14 30.99 596 .16 185.14 40.34 70.85 Flags: "K" Keyline not found "E" Manually edited "M" Manually accepted "A" = Nuclide specific abn. limit Page 3899 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235042 Acquisition date : 3-0CT-2016 06:55:55 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 94.82 32 116 1. 08 189.91 170 23 6.40E-03 **** 4.73E+OO T 0 213.01 120 284 8.20 426.41 412 27 2.61E-02 92.0 4.53E+OO 0 270. 96 34 88 0.73 542.35 537 10 7.56E-03 **** 3.78E+OO T 0 304.48 16 75 4.45 615.43 607 12 d. 66E-03 **** 3.41E+OO T 0 339.27 79 76 1. 39 679.03 672 14 1.82E-02 58.9 3.14E+00 T 0 370.31 40 67 7.15 741.13 733 18 9.30E-03 **** 2.92E+OO 0 463.41 34 34 2.78 927.42 922 12 8.28E-03 81. 9 2.42E+00 T 0 728. 09 37 19 1. 63 1456. 96 1449 15 9.58E-03 66.9 1.68E+OO T 0 733.46 9 9 1. 77 1467.71 1463 7 2.43E-03 **** 1.67E+OO T 0 794.49 17 9 1.29 1589.80 1583 11 4.36E-03 87.0 1.57E+OO T 0 911.20 69 12 1.11 1823.30 1816 15 1. 82E-02 34.2 1.41E+OO T 0 924.29 10 2 0.53 1849.49 1845 7 2. 51E-03 82.9 1.40E+OO T 0 971.14 24 43 1. 02 1943.22 1933 16 6.49E-03 **** 1.35E+OO 0 1001.34 18 3 0.62 2003.65 1997 13 4.76E-03 71. 4 1.31E+OO T 0 1028.25 8 20 1. 42 2057.47 2051 10 2.12E-03 **** 1.29E+OO T 0 1155. 72 18 8 1. 59 2312.49 2305 17 4.94E-03 88.7 1.17E+OO 0 1163.80 10 9 1. 26 2328.65 2322 12 2.63E-03 **** 1.17E+OO 0 1168. 05 10 7 1. 08 2337.17 2333 9 2.76E-03 **** 1.16E+OO 0 1261.90 12 7 1. 33 2524.91 2519 11 3.41E-03 **** 1.09E+OO T 0 1301. 59 13 0 0.83 2604.31 2599 10 3. 61E-03 55.5 1.07E+OO Flags: "T" = Tentatively associated Page 3900 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:03.38 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * *******************************************************************************
  • 1 *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l *
  • Acquisition date 3-0CT-2016 06:55:55 Sensitivity 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.67 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:53:00 Nuclide Library : SOLID *
  • Sample ID G405235042 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity: 1.7680E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. 'File : DKA100: [CANBERRA. GAMMA] EFF GAM08 CAN. CNF; 14 * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. *Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.514E-01 2.948E-02 3.114E-02 2.803E-02 4. 711E-02 5.866E-02 5.534E-02 5.866E-02 4.945E-01 5.866E-02 4. 711E-02 5.864E-02 3.042E-01 1.189E+OO 5.864E-02 1.470E-01 1.189E+OO 4.605E-02 1.747E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page3901 of5809 Le (pCi/GRAM 1. 290E+Ol 2.853E-02 O.OOOE+OO 2.004E-02 4.326E-01 O.OOOE+OO O.OOOE+OO 4.876E-02 3.644E-01 O.OOOE+OO 4.496E-02 4.491E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-1$3 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 3902 of 5809 6. 011E+OO 3.236E-02 l.183E-01 1. 875E+OO 1.037E+Ol O.OOOE+OO l.948E-01 O.OOOE+OO O.OOOE+OO 4. 621E-01 5.947E+OO 6.816E-01 O.OOOE+OO 8.295E-02 4.649E+02 2.165E-02 7.619E-01 2.219E+OO l.296E+00 O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 3.178E-02 3.569E-02 5.532E+OO 3.435E-01 3.435E-01 2.337E-02 1.067E+OO 8.297E-02 1. 960E-01 O.OOOE+OO O.OOOE+OO 1.199E-01 1. 656E+OO 9.908E-02 2.649E+02 O.OOOE+OO O.OOOE+OO 7.182E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.290E-02 O.OOOE+OO 4.409E-02 l.105E-01 O.OOOE+OO O.OOOE+OO 9.133E-02 O.OOOE+OO O.OOOE+OO 2.460E+Ol O.OOOE+OO 3.206E-01 4.458E-02 3.902E+OO 3.751E-02 O.OOOE+OO 7.399E+02 O.OOOE+OO 2.059E-02 6.568E-02 1.673E-01 6.967E-02 1.029E-01 1.741E+OO 4.766E-02 2.725E+Ol 2.138E-01 5. 311E-02 1. 740E-02 4.412E+OO 8.038E-01 3.531E+00 2.912E+Ol NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF .NOT NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 AC-228 RA-228 TH-229 TH-231 TH-232 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3903 of 5809 1.007E+02 3.646E-01 l.925E+OO 3.389E-02 4.926E+OO 3.668E-01 5. 596E-01 5.980E-01 2.915E-01 4,. 941E-01 1. 782E-Ol 1. 782E-01 2.350E-01 2.350E-01 3.878E-01 4.941E-01 2.350E-01 5.352E-02 l.829E-01 3.889E+OO 5.352E-02 O.OOOE+OO 2.120E-01 2.843E+02 l.559E-01 8.673E-02 6.321E-02 2.783E-02 3.103E-02 1.00SE-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:08.87 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235042.CNF;l *
  • Acquisition date 3-0CT-2016 06:55:55 Sensitivity : 3.000 *
  • Detector ID GAM08 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.67 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:53:00 Nuclide Library : SOLID *
  • Sample ID G405235042 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity : 1.7680E+02 GRAM *
  • Quantity Err(%) : 1.1312E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 21-JUL-2016 06:09:19 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM08 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma ) K-40 1.233E+Ol 1.562E+OO 1. 562E+OO BA-137M 2.358E-01 8.030E-02 8.030E-02 CS-137 2.491E-01 8.482E-02 8.482E-02 TL-208 3.083E-01 7.488E-02 7.488E-02 PB-212 6.871E-01 1.509E-01 1.509E-01 BI-214 6. 511E-01 1.997E-01 1.997E-01 PB-214 7.987E-01 2.232E-01 2.232E-01 RN-222 6.511E-01 l.997E-01 l.997E-01 RA-224 3.237E-01 9.529E-01 9.529E-01 RA-226 6. 511E-01 1.997E-01 1. 997E-01 TH-228 6. 871E-01 1.509E-01 1. 509E-01 TH-230 6.508E-01 1. 996E-01 1. 996E-01 PA-231 5.881E-01 7.140E-01 7.140E-01 TH-234 1.498E+OO 2.738E+OO 2.738E+OO U-234 6.508E-01 1. 996E-01 1. 996E-01 U-235 4.947E-02 2.890E-01 2.890E-01 U-238 1.498E+OO 2.738E+OO 2.738E+OO AM-243 2.163E-01 l.163E-01 l.163E-01 ANH-511 1.023E-01 7.116E-02 7 .116E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (l'.96-sigma) ( 1. 96-sigma) BE-7 l.495E+Ol 1. 2 67E+Ol 1.435E+Ol NOT IDENT. NA-22 -1.235E-02 3.734E-02 3.775E-02 NOT IDENT. NA-24 1.000E+41 4.268E+41 O.OOOE+OO SHORT HLIF AL-26 8.641E-03 l.953E-02 1. 991E-02 NOT IDENT. SC-46 7.510E-02 4.817E-01 4.829E-01 FAIL ABUN V-48 l.342E+04 l.690E+04 1. 795E+04 SHORT HLIF CR-51 8.273E+Ol 4.525E+02 4.540E+02 SHORT HLIF MN-54 3.215E-02 4.898E-02 5.107E-02 NOT IDENT. C0-56 -2. 901E-01 4.660E-01 4.840E-Ol NOT IDENT. MN-56 -l.OOOE+41 l.618E+41 O.OOOE+OO SHORT HLIF C0-57 l.767E-02 4.884E-02 4.949E-02 NOT IDENT. Page 3904 of 5809 C0-58 -4.666E-01 5.908E-01 6.271E-01 NOT IDENT. FE-59 -5.049E+OO 7.992E+OO 8.310E+OO NOT IDENT. C0-60 5.863E-03 3.677E-02 3.687E-02 NOT IDENT. ZN-65 3.864E-02 1.443E-01 l.453E-01 NOT IDENT. GE-68 -1.369E+OO 2.449E+OO 2.525E+OO NOT IDENT. AS-73 -1.025E+Ol 1.218E+Ol 1.303E+Ol NOT IDENT. AS-74 -3.921E+03 7.936E+03 8.130E+03 SHORT HLIF SE-75 5.548E-02 2.054E-01 2.069E-01 NOT IDENT. BR-77 1. 231E+39 l.094E+40 O.OOOE+OO SHORT HLIF SR-82 -2.936E+Ol 7. 896E+02 7.897E+02 SHORT HLIF RB-83 -9.802E-02 5.824E-01 5. 841E-01 NOT IDENT. KR-85 6.097E+OO 5.939E+OO 6.544E+OO NOT IDENT. SR-85 6.954E-01 6. 811E-01 7.497E-01 NOT IDENT. RB-86 -1. 880E+04 3.925E+04 4.015E+04 SHORT HLIF Y-88 3.127E-02 6.948E-02 7.090E-02 NOT IDENT. Y-91 -5.682E+Ol 5.592E+02 5.598E+02 NOT IDENT. NB-94 -l.328E-02 2.624E-02 2. 691E-02 NOT IDENT. NB-95 -2.528E-01 8.902E-01 8.975E-01 NOT IDENT. NB-95M -4.655E-01 2.690E+OO 2.698E+OO NOT IDENT. ZR-95 4.518E-01 l.375E+OO 1.390E+OO NOT IDENT. NB-97 1.000E+41 2.204E+41 0.000E+OO SHORT HLIF ZR-97 l.OOOE+41 1.332E+41 O.OOOE+OO SHORT HLIF M0-99 7.632E+31 1. 027E+33 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.840E+41 O.OOOE+OO SHORT HLIF RH-101 9.922E-03 3.495E-02 3.524E-02 NOT IDENT. RH-102 -8.216E-03 4.404E-02 4.420E-02 NOT IDENT. RU-103 2.616E+OO 5.935E+OO 6.051E+OO FAIL ABUN RH-106 -3.175E-01 4.681E-01 4.895E-01 NOT IDENT. RU-106 -3.175E-01 4.681E-01 4.895E-01 NOT IDENT. AG-108M -6.266E-03 2.733E-02 2.747E-02 NOT IDENT. CD-109 8.134E-02 l.168E+OO 1.168E+OO NOT IDENT. AG-llOM -1.853E-02 9.769E-02 9.805E-02 NOT IDENT. SN-113 -4.937E-02 2.262E-01 2.273E-01 NOT IDENT. CD-115 3.469E+40 3.266E+40 O.OOOE+OO SHORT HLIF SN-117M 5.137E+04 1.380E+05 l.399E+05 SHORT HLIF TE-123M 2.142E-02 1.354E-01 1.357E-01 NOT IDENT. SB-124 1.157E-02 1.920E+OO 1.920E+OO NOT IDENT. SB-125 8.939E-02 1.008E-01 l.086E-01 FAIL ABUN TE-125M -1.322E+02 3.100E+02 3.157E+02 NOT IDENT. I-126 -1.299E+05 1.659E+06 1.660E+06 SHORT HLIF SB-126 -8.927E+05 l.794E+06 l.838E+06 SHORT HLIF SN-126 3.738E-02 7.622E-02 7.806E-02 FAIL ABUN SB-127 3. 571E+22 9. 471E+22 O.OOOE+OO SHORT HLIF I-131 -l.329E+09 l.060E+l0 l.062E+l0 SHORT HLIF I-132 l.000E+41 l.932E+42 O.OOOE+OO SHORT HLIF TE-132 4.759E+26 2.066E+27 O.OOOE+OO SHORT HLIF BA-133 l.310E-02 3.859E-02 3.904E-02 NOT IDENT. I-133 -1.000E+41 2.233E+41 O.OOOE+OO SHORT HLIF CS-134 7.066E-02 6.032E-02 6.822E-02 FAIL ABUN CS-135 7.375E-04 1.330E-01 1.330E-01 NOT IDENT. I-135 1.000E+41 7.029E+41 O.OOOE+OO SHORT HLIF CS-136 -2.869E+05 3.578E+05 3.805E+05 SHORT HLIF CE-139 -7.099E-02 1.135E-01 l.179E-01 NOT IDENT. BA-140 2.571E+05 1. 762E+06 1.766E+06 SHORT HLIF LA-140 -1.908E+05 6.663E+05 6.718E+05 SHORT HLIF CE-141 7.939E+OO 4.639E+Ol 4.652E+Ol FAIL ABUN CE-143 1.000E+41 1. 511E+41 O.OOOE+OO SHORT HLIF CE-144 -3.430E-02 3.694E-01 3.698E-01 NOT IDENT. PM-144 -1.214E-03 4. 960E-02 4. 960E-02 NOT IDENT. PR-144 -5.977E-02 4.334E+OO 4.334E+OO NOT IDENT. PM-146 4.624E-03 4.204E-02 4.209E-02 NOT IDENT. ND-147 -5.879E+07 4.813E+07 5.495E+07 SHORT HLIF PM-147 2.994E+02 8.014E+02 8.127E+02 NOT IDENT. PM-149 -l.OOOE+41 1.806E+41 O.OOOE+OO SHORT HLIF EU-150 9.557E-03 2.385E-02 2.424E-02 FAIL ABUN EU-152 -3.597E-03 8.187E-02 8.188E-02. NOT IDENT. GD-153 1.846E-01 1. 798E-01 1.981E-01 NOT IDENT. EU-154 -3.016E-02 9. ll 7E-02 9.218E-02 NOT IDENT. EU-155 3.030E-02 1.115E-01 1.123E-01. NOT IDENT. TB-160 -3.385E-01 2.036E+OO 2. 041E+OO NOT IDENT. H0-166M -3.375E-02 5.775E-02 5.972E-02 FAIL ABUN TM-171 1.165E+Ol 2.788E+Ol 2.837E+Ol NOT IDENT. HF-172 -5.657E-02 2.455E-01 2.468E-01 FAIL ABUN LU-172 -8.596E-02 7. 851E-02 8.756E-02 FAIL ABUN LU-176 2.135E-02 5.167E-02 5.255E-02 FAIL ABUN HF-181 2.002E+OO 4.766E+OO 4.850E+OO NOT IDENT. TA-182 2.198E-01 9.056E-01 9. llOE-01 FAIL ABUN RE-183 -4.373E-02 3.753E+OO 3.753E+OO NOT IDENT. Page 3905 of 5809 RE-184 -1.125E+OO 3.339E+Ol 3.339E+Ol NOT IDENT. W-188 1.987E+Ol 1.196E+02 l.199E+02 FAIL ABUN IR-192 -4.992E-01 4.600E-01 5 .121E-01 FAIL ABUN HG-203 -3.595E+OO 2.489E+OO 2.970E+OO NOT IDENT. BI-207 6.315E-03 3.790E-02 3.800E-02 FAIL ABUN PB-210 -3.347E+OO 5.454E+00 5.659E+OO NOT IDENT. BI-211 2.200E+OO 6.158E-01 l.167E+OO FAIL ABUN PB-211 5.547E-02 6.223E-01 6.228E-01 NOT IDENT. BI-212 1. 417E+OO 9.324E-01 l.130E+OO FAIL ABUN RN-219 -1.052E-01 3.424E-01 3.456E-01 FAIL ABUN RA-223 4.151E-02 5.534E-01 5.537E-01 FAIL ABUN AC-227 -6.853E-02 l.991E-01 2.0lSE-01 FAIL ABUN TH-227 -6.853E-02 1. 991E-01 2.0lSE-01 FAIL ABUN AC-228 8.044E-01 2.731E-01 4.539E-01 FAIL ABUN RA-228 8.044E-01 2. 731E-01 4.539E-01 FAIL ABUN TH-229 -4.067E-02 4 .114E-01 4 .118E-01 NOT IDENT. TH-231 4.151E-02 5.534E-01 5.537E-01 FAIL ABUN TH-232 8.044E-01 2. 731E-01 4.539E-01 FAIL ABUN PA-233 -1.259E-02 6.296E-02 6.321E-02 FAIL ABUN PA-234 -1.738E-01 3.164E-01 3.260E-01 FAIL ABUN PA-234M 6.851E+OO 4.803E+00 5.710E+OO FAIL ABUN NP-237 -l.259E-02 6.296E-02 6. 321E-02 FAIL ABUN NP-238 1.000E+41 3.207E+41 O.OOOE+OO SHORT HLIF NP-239 4.936E-02 2.323E-01 2.334E-01 NOT IDENT. PU-239 9. 967E+Ol 3 .116E+02 3.148E+02 NOT IDENT. AM-241 1.412E-01 l.647E-01 1.766E-01 NOT IDENT. CM-243 -5.309E-02 l.009E-01 1.037E-01 NOT IDENT. BK-247 2.102E-02 6.644E-02 6. 711E-02 NOT IDENT. CM-247 3.517E-03 3.081E-02 3.085E-02 NOT IDENT. CF-249 6.041E-03 3.398E-02 3.409E-02 NOT IDENT. CF-251 2.810E-02 1.030E-01 l.037E-01 NOT IDENT. Page 3906 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 72.6218 87.09 91.4164 136.47 82.3165 45.60 65.0560 87.57 91.4993 140.51 0.0000 46.54 75.2672 88.03 91. 57 91 143.76 65.0701 49.72 0.0000 88.34 91.6323 144.24 70.7391 51. 35 51.8652 88.47 91.6545 145.44 66.0219 51. 87 48.8820 89. 96 91. 9097 152.43 71.9144 52.39 50.9890 1093.63 92.0256 153.25 0.0000 52.97 59.2375 91.11 0.0000 323.87 64.7490 53.44 64.4232 92.59 92.3549 156.02 0.0000 54.07 65.5530 93.35 92.4828 158.56 0.0000 57.36 0.0000 94.56 92.6848 159.00 63.9153 57.53 59.9313 94.65 92.6993 162.33 70.3533 57.98 64.1359 94.67 92.7031 162.66 0.0000 59.27 53. 9620 94.87 92.7361 163.33 55.6107 59.32 53. 9688 97.43 52.3782 165.86 70.6594 59.54 53.9975 98.43 79.8295 176.31 61. 9234 60. 96 66.6868 98.44 79.8311 176.60 0.0000 61.17 68 .1102 99.53 70.9706 177.52 60.3347 62.93 71.1865 100 .11 68.7865 181.07 0.0000 63.29 71. 2465 102.03 73.5391 181. 52 61.8773 63.58 69.8967 103.18 85.0182 184.41 72.2172 64.28 64.4097 103.37 80.5099 143.76 62. 5963 66.73 79.2046 105.21 76.2097 193.51 60.5801 67.24 88.8110 105.31 73.9472 197.03 58.2431 125.81 89.9571 106.12 69.4902 198.01 54.0176 67.75 85.7368 106.47 76.3697 201.83 57.6824 69.67 79.3709 109.28 73.2876 203.43 46.5694 70.83 99.4650 111. 00 82.6782 205.31 53.1425 72. 81 84.5493 111.76 0.0000 210.85 58.2290 72.87 84.5601 114. 06 66.9280 215.65 58.5153 74.66 84.8814 116. 30 0.0000 222 .11 59.7746 74.82 84.9097 116.74 63.7335 227.09 65.3680 74.97 84.9362 119. 76 72 .1809 227.38 60.0852 77 .11 85.3141 121.12 61.8308 228.16 0.0000 78.74 75.1245 121. 22 61.8405 228.18 56.5944 79.69 68.0315 121.78 64.2282 116.74 56.5944 80.12 75.3335 122.06 67.7603 235.69 64.1301 80.19 0.0000 122.92 73.6974 235. 96 72.1653 80.57 66.7015 123.07 67.8634 238.63 64.3088 81. 00 66.7586 265.00 80.8083 238.98 0.0000 81. 07 69.6709 125.81 84.5892 240.99 61. 7 662 81. 75 83.9356 127.23 75.3472 242.00 38.9763 83.79 86.0963 127.91 84.8507 244.70 37.7267 84.00 86.1317 129.30 73.2135 252.40 0.0000 85.43 98.0805 131. 20 81. 7038 252.80 42.5316 86.55 91.3227 133.02 72.4189 254.15 0.0000 86.79 91.3638 133. 52 71. 2830 256.23 45.3857 86.94 91.3904 136.00 67.9563 260.90 0.0000 Page 3907 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 43.8965 355.39 0.0000 584.27 21.2776 264.80 43.9014 356.01 25.0424 595.83 0.0000 265.00 41.1649 364.49 0.0000 427.87 22.5716 268.22 39.9042 366.42 0.0000 602.52 0.0000 269.46 36.7326 372. 51 29.7986 604. 72 13.5693 270.03 36.7513
  • 375.05 31.3430 607.14 1.6. 98 0 6 271.23 36.7887 377.52 25 .1159 609.32 24.9299 273.65 0.0000 356.01 23.0201 610.33 24.9425 276.40 35.1039 388.16 27.1005 614.28 17.0367 277.37 39.7552 388.63 0.0000 618.01 19.3415 277.60 41. 6125 391. 69 31.1873 620.36 14.8070 278.00 36.0761 264.66 24.2856 621.93 20.5166 279.20 49.0761 401.81 29.3670 630.19 0.0000 279.54 51. 8688 402.40 25.3255 631.29 11.4465 279.70 52.8020 404.85 28.4090 633.25 10. 3110 280.46 44.4932 410.95 28.5190 634.78 0.0000 283.69 35.3188 413.71 28.5685 635.95 20.6470 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 52.1229 423. 72 0.0000 645.85 19.5864 285.90 0.0000 427.09 27.7773 657.76 17.3730 287.50 42.8892 427.87 21.6148 657.90 0.0000 290.67 37.8592 433.94 29.9594 661.66 20.8835 293.27 0.0000 439.40 26.9479 664.57 0.0000 351. 93 39.4066 453.88 25.0889 666.33 0.0000 295. 96 39.4297 463.37 21.0225 666.50 0.0000 879.38 39.5126 468.07 22.1331 667. 71 0.0000 299.98 39.5570 473.00 0.0000 677.62 16.6465 300.09 39.5604 475.06 30.6862 685.70 0.0000 300 .13 39.5613 476.78 18.0058 695.00 0.0000 301.36 28.2861 477.60 14.8351 696.49 17.6630 302.85 45.3105 482.18 21.2472 696.51 17.6636 256.23 39.6989 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.3194 306.78 39.7698 497.08 16.0666 697.49 20.3208 308.46 42.6663 505.52 12.9121 702.65 18.5942 311. 90 46. 7736 507.63 0.0000 706.68 14.1904 316.51 45.7949 511. 00 14.0292 711.68 25.7733 319.41 0.0000 514.00 14.0516 720.70 0.0000 320.08 0.0000 514.00 14.0516 721. 93 0.0000 321.04 40.2090 520.40 15.6176 722.78 12.8558 323.87 33.5794 520.69 0.0000 722. 91 12.8566 325.23 37.4551 522.65 0.0000 723.31 11. 4301 328.76 0.0000 527.90 0.0000 724.19 15.7217 333.37 42.0304 528.26 14.1569 727. 33 20.0348 333.97 27.5491 529.59 18.5260 733.00 17.2119 334.37 34.8091 529.87 0.0000 735.93 10.0522 338.28 30.0609 531.02 0.0000 333.97 16.7640 338.32 30.0615 537.26 0.0000 739.50 0.0000 311. 90 30.1088 546.56 0.0000 747.24 19.8348 340.48 30.1088 552.55 16.5387 748.06 11. 7241 340.55 0.0000 563.25 17.7357 752.31 22.5845 344.28 24.8349 569.33 14.4531 753.82 0.0000 345.93 31.2025 946.00 14.4547 756.73 12.6691 351.06 32.2950 569.70 12.2318 756.80 12.6696 351. 93 32.3152 583.19 21.2668 884.68 16.3350 Page 3908 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:58:38.72 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM09.CNF;335 Background date : Z-OCT-2016 11:00:29. Sample date 30-NOV-2015 13:59:00 Acquisition date : 3-0CT-2016 06:56:18. Sample ID G405235043 Sample quantity 1.65795E+02 GRAM Detector name : GAM09 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.51 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 1 1 0 0 2 2 7 7 0 0 2 2 1 1 0 0 0 0 0 0 0 0 0 3 3 0 0 0 0 0 0 Page 3910 of 5809 Energy 63.36* 74.99 77.16 87.24 90.12 92.99* 143.38* 185.90* 188.10 238.69* 241.63 270.56 277.63 295.16* 300.32 338.43* 343.92 352.00* 369.64 462.19 510.73* 532.02 558.91* 583.04* 608.93* 630.75 656.18 661.39 727. 56 7 67. 05 785.17 796.66 910.81* 935.55 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 40 98 145 64 47 61 17 84 21 369 96 33 34 156 33 92 18 212 69 55 23 19 6 121 149 16 13 26 45 31 22 17 63 16 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 126 122 101 110 84 119 102 73 84 60 60 76 61 36 48 27 24 55 51 15 70 17 11 24 14 12 18 15 12 11 8 20 12 22 1. 26 1. 03 0.90 0. 96 0.93 1. 25 0.94 1.16 1. 25 1.10 2.14 1. 21 1.13 1. 27 1. 41 1. 32 1. 33 1. 04 8.98 0.92 1. 41 1. 04 1. 21 1. 44 1. 39 1. 71 1. 94 1. 95 2 .11 2.94 1. 49 0.85 1. 56 0.58 126.39 149.66 154.00 174.17 179.93 185.68 286.49 371.57 375.98 477.20 483.08 540.97 555.12 590.18 600.51 676.76 687.76 703.92 739.21 924.39 1021.52 1064 .11 1117.92 1166.20 1218.01 12 61. 66 1312.56 1322.97 1455.38 1534.38 1570.66 1593.64 1822.04 1871.55 123 145 145 170 170 182 284 365 365 473 473 534 550 583 583 672 672 699 728 918 1014 1061 1114 1160 1210 1258 1308 1308 1449 1528 1564 1588 1816 1864 9 1. llE-02 54. 6 14 2.73E-02 20.3 3.15E+OO 14 4.02E-02 13.2 13 1.78E-02 27.8 2.34E+OO 13 1.30E-02 35.8 8 1. 71E-02 35. 8 8 4.80E-03105.4 14 2.34E-02 21.5 5.47E+OO 14 5.83E-03 78.3 16 1.02E-01 6.2 2.73E+OO . 16 2.67E-02 23.8 11 9.06E-03 54.9 10 9.42E-03 46.7 24 4.32E-02 10.8 l.85E+OO 24 9.27E-03 38.0 21 2.55E-02 14.5 1.43E+OO 21 4.89E-03 57.0 11 5.90E-02 9.7 23 1.91E-02 29.7 12 1.53E-02 19.5 14 6.35E-03 90.2 9 5.30E-03 44.3 7 1.79E-03107.0 12 3.37E-02 12.3 12 4.14E-02 9.8 7 4.42E-03 44.1 27 3.53E-03 58.5 1.86E+OO 27 7.lOE-03 39.3 12 1. 25E-02 21. 4 11 8.64E-03 27.3 10 6.14E-03 31.6 13 4.58E-03 60.4 12 1.76E-02 17.3 17 4.46E-03 70.6 Peak Search Report (continued) Page : 2 Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 968.97 39 20 1. 06 1938.44 1934 9 1. 08E-02 26. 2 36 0 1001.21* 6 12 1. 57 2002.94 1995 10 1. 71E-03122. 6 37 0 1008.00 6 .10 0. ;70 2016.53 2011 7 1.77E-03 92.0 38 0 1086.29 11 10 1. 94 2173.18 2168 10 3.06E-03 61. 7 39 0 1119. 57 42 6 2.99 2239.77 2234 11 1.15E-02 19.0 40 0 1175.33 16 11 3.35 2351. 36 2346 12 4.53E-03 48.7 41 0 1200.56 29 3 5.17 2401. 84 . 2396 14 8. llE-03 22.8 42 0 1238.33 13 16 0.69 2477.42 2472 9 3.64E-03 61. 3 43 0 1271. 23 16 0 0.98 2543.25 2537 12 4.44E-03 25.0 44 0 1377.36 7 3 1. 05 2755.63 2752 6 1. 97E-03 53.6 45 0 1450.18* 5 0 0. 96 2901. 33 2898 6 1. 42E-03 48.7 46 0 1460.09* 377 4 2.13 2921.16 2911 18 1.05E-01 5.4 47 0 1607.01 7 2 0.94 3215.17 3212 6 1. 81E-03 49.3 48 0 1763.59* 31 0 1. 32 3528.50 3522 13 8.49E-03 19.4 Flag: "*" = Peak area was modified by background subtraction Page 3911 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:58:40 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 13:59:00 G405235043 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:56:18 165.79 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA9 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3912 of 5809 PB-214 PA-234M PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 766.42 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 NB-95 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 765.81 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.51 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 J.0.66* 1.146E+OO 1. 361E+Ol 1.361E+01 lCJ.. 73 OK NB-95 765.81 99.81* l.922E+OO 7.079E-02 l.980E+00 64.76 OK CD-109 88.03 3.70* 4. 861E+OO 1.169E+OO 1.856E+OO 105.33 OK SN-126 64.28 9.60 2.275E+OO 1.153E+OO 1.153E+OO 109.24 OK 86.94 8.90 4.861E+OO 4.860E-01 4.860E-01 105.33 OK 87.57 37.00* 4.861E+OO 1.169E-01 l.169E-01 105.33 OK BA-137M 661. 66 89.90* 2.157E+OO 6.441E-02 6.567E-02 78.66 OK CS-137 661. 66 85.10* 2.157E+OO 6.804E-02 6.938E-02 78.66 OK TL-208 277.37 6.60 4.349E+OO 6.397E-01 6.397E-01 93.46 OK 583.19 85.00* 2.382E+OO 2.978E-Ol 2.978E-01 24.69 OK 860.56 12.50 1. 758E+OO Line Not Found Absent BI-212 727.33 6.67* 2.003E+OO -1. 627E+OO l.627E+00 42.86 OK 785.37 1.10 1.888E+OO 5.097E+OO 5.097E+OO 63.14 OK 1620.50 1. 47 1.045E+OO Line Not Found Absent PB-212 74.82 10.28 3.688E+OO 9.898E-01 9.898E-01 67.41 OK 77 .11 17.10 3.924E+OO l.334E+OO 1. 334E+OO 26.50 OK 238.63 43.60* 4.882E+OO 9.538E-01 9.538E-01 12.38 OK 300.09 3.30 4.084E+OO 1.329E+OO 1.329E+OO 76.02 OK BI-214 609.32 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 OK 1120.29 14.92 l.430E+OO 8.894E-01 8.898E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 OK PB-214 74.82 5.80 3.669E+OO Line Not Found <<INT Reject 77 .11 9.70 3.924E+OO 2. 351E+OO 2.352E+OO 26.50 OK 87.09 3.41 4.849E+OO Line Not Found <<INT Reject 242.00 7.25 4.832E+OO Line Not Found <<INT Reject 295.22 18.42 4.142E+OO 1. 096E+OO 1.097E+OO 21. 60 OK 351. 93 35.60* 3.588E+OO 8.760E-01 8.763E-01 19.50 OK RN-222 609.32 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 OK 1120.29 14.92 l.430E+00 8.894E-01 8.898E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 OK RA-224 240.99 4.10* 4.838E+OO 7.219E-01 7.219E-01 185.06 OK RA-226 609.32 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 OK 1120.29 14.92 1.430E+OO 8.894E-01 8.898E-01 37.99 OK 1764.49 15.30 9.661E-01 8. 891E-01 8.894E-01 38.85 OK AC-228 105.21 1.10 5. 896E+OO Line Not Found Absent 338.32 11. 27 3.705E+OO 1.164E+OO 1.164E+OO 29.06 OK 794.95 4.25 1.870E+OO Line Not Found Absent 835.71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 6.848E-01 6.848E-01 34.51 OK 968. 97 15.80 1.603E+OO 7.182E-01 7.182E-01 52.38 OK RA-228 105.21 1.10 5. 896E+OO Line Not Found Absent 338.32 11.27 3.705E+OO 1.164E+00 1.164E+OO 29.06 OK 794.95 4.25 l.870E+00 Line Not Found Absent 835.71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 6.848E-01 6.848E-01 34.51 OK 968.97 15.80 l.603E+OO 7.182E-01 7.182E-01 52.38 OK TH-228 74.82 10.28 3.688E+OO 9.898E-01 9.898E-01 67.41 OK 77 .11 17.10 3.924E+OO 1.334E+OO 1.334E+OO 26.50 OK 238.63 43.60* 4.882E+OO 9.538E-01 9.538E-01 12.38 OK Page 3913 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300 .*09 3 .. 30 4.084E+OO 1.329E+OO 1.329E+OO 76.0i.2 OK TH-230 609.32 45.49* 2.302E+OO 7.025E-01 7.025E-01 19.58 OK 1120.29 14.92 1.430E+OO 8.894E-01 8.894E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8.891E-01 38.85 OK PA-231 283.69 1. 70 4.275E+OO Line Not Found Absent 301.36 5.35* 4.084E+OO 8 .196E-01 8 .196E-01 76.02 OK TH-232 105.21 1.10 5.896E+00 Line Not Found Absent 338.32 11.27 3.705E+OO l.164E+OO 1.164E+OO 29.06 OK 835. 71 1. 61 1. 799E+OO Line Not Found Absent 911.20 25.80* 1.682E+OO 6.848E-01 6.848E-01 34.51 OK 968. 97 15.80 1.603E+OO 7.182E-01 7.182E-01 52.38 OK PA-234M 766.42 0.32 l.924E+00 Line Not Found <<INT Reject 1001.03 0.84* l.562E+00 2 .181E+OO 2 .181E+OO 245 .11 OK TH-234 63.29 3.70* 2.275E+OO 2.992E+OO 2.992E+OO 109.24 OK 92.59 4.23 5.276E+OO l.671E+OO 1.671E+OO 71. 54 OK U-234 609.32 45.49* 2.302E+OO 7.025E-01 7.025E-01 19.58 OK 1120.29 14.92 1.430E+OO 8.894E-01 8.894E-01 37.99 OK 1764.49 15.30 9.661E-01 8.891E-01 8.891E-01 38.85 OK U-235 89. 96 3.47 5.079E+OO 1.616E+OO 1. 616E+OO 71. 57 OK 93.35 5.60 5.276E+OO 1.262E+OO 1.262E+OO 71.54 OK 143.76 10.96* 6.313E+00 1.450E-01 1.450E-01 210.79 OK 163.33 5.08 6. 096E+OO Line Not Found Absent 185.72 57.20 5.741E+OO l.453E-01 l.453E-01 42.94 OK 205.31 5.01 5.415E+OO Line Not Found Absent U-238 63.29 3.70* 2.275E+OO 2.992E+OO 2.992E+00 109.24 OK 92.59 4.23 5.276E+OO 1. 671E+OO 1.671E+OO 71. 54 OK AM-243 43.53 5.90 1. 969E-01 Line Not Found Absent 74.66 67.20* 3.688E+OO l.514E-01 l.514E-01 67.41 OK ANH-511 511. 00 100.00* 2.647E+00 4.355E-02 4.355E-02 180.49 OK Flag: "*" = Keyline Page 3914of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:41.93 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l *
  • Acquisition date 3-0CT-2016 06:56:18 Sensitivity : 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.51 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:59:00 Analyst initials: MXRl *
  • Sample ID G405235043 Sample Quantity l.6579E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;16'
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-s,igma) (pCi/GRAM K-40 1.361E+Ol l.432E+OO 4.430E-01 NB-95 1.980E+OO l.257E+OO 1.295E+OO CD-109 1.856E+OO 1.916E+OO 1. 782E+OO SN-126 1.169E-01 1. 207E-01 1.130E-01 BA-137M 6.567E-02 5.063E-02 4.764E-02 CS-137 6.938E-02 5.348E-02 5.033E-02 TL-208 2.978E-01 7.204E-02 4.698E-02 BI-212 1.627E+OO 6.836E-01 7.695E-01 PB-212 9.538E-01 1.157E-01 7. 710E-02 BI-214 7.028E-01 1.349E-01 8. 726E-02 PB-214 8.763E-01 l.674E-01 9.397E-02 RN-222 7.028E-01 1.349E-01 8.726E-02 RA-224 7.219E-01 1.309E+OO 8.266E-01 RA-226 7.028E-01 f.349E-01 8.726E-02 AC-228 6.848E-01 2.316E-01 2.162E-01 RA-228 6.848E-01 2.316E-01 2.162E-01 TH-228 9.538E-01 1.157E-01 7. 710E-02 TH-230 7.025E-01 1.348E-01 8. 723E-02 PA-231 8 .196E-01 6.106E-01 5.796E-01 TH-232 6.848E-01 2.316E-01 2.162E-01 PA-234M 2.181E+OO 5.238E+OO 6.979E+OO TH-234 2.992E+OO 3.203E+OO 2.269E+OO U-234 7.025E-01 1.348E-01 8. 723E-02 U-235 1.450E-01 2.995E-01 2.542E-01 U-238 2.992E+OO 3.203E+OO 2.269E+OO AM-243 l.514E-01 l.OOOE-01 8.182E-02 ANH-511 4.355E-02 7.703E-02 4.957E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -5.083E+OO l.049E+Ol 2.008E+Ol NOT IDENT. NA-22 -3.298E-02 4.607E-02 6.771E-02 NOT IDENT. NA-24 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF Page 3915of5809 AL-26 -1.929E-02 1. 8 98E-02 l.310E-02 NOT IDENT. SC-46 -6.499E-04 2.958E-01 5.945E-01 FAIL ABUN V-48 0.000E+OO l.674E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.952E+02 O.OOOE+OO SHORT HLIF MN-54 -2.346E-02 6.064E-02 1.105E-01 NOT IDENT. C0-56 -7.088E-02 4.541E-01 8.636E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.012E-02 3.674E-02 7.207E-02 NOT IDENT. C0-58 -6.584E-02 5.251E-01 l.017E+OO NOT IDENT. FE-58 -1.864E+OO 7.402E+OO NOT IDENT. C0-60 1.303E-02 2.081E-02 5.449E-02 NOT IDENT. ZN-65 4.lOlE-02 1. 211E-01 2.417E-01 NOT IDENT. GE-68 -9.442E-01 2.044E+OO 3.711E+OO NOT IDENT. AS-73 6.689E-01 9.848E+OO 2.137E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.697E+03 O.OOOE+OO SHORT HLIF SE-75 l.556E-01 1. 574E-01 3.378E-01 NOT IDENT. BR-77 O.OOOE+OO 2. 072E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 5.913E+02 O.OOOE+OO SHORT HLIF RB-83 4.079E-02 5.848E-01 1.190E+OO NOT IDENT. KR-85 2.432E+OO 7.155E+OO 1.334E+Ol NOT IDENT. SR-85 2.780E-01 8.211E-01 1. 531E+OO NOT IDENT. RB-86 O.OOOE+OO 3.324E+04 O.OOOE+OO SHORT HLIF Y-88 -l.493E-03 l.027E-01 2.683E-01 NOT IDENT. Y-91 1. 700E+Ol 4.088E+02 7.785E+02 NOT IDENT. NB-94 2.445E-02 2.626E-02 5.825E-02 NOT IDENT. NB-95M 8.954E-01 2 .118E+OO 3.928E+OO NOT IDENT. ZR-95 7.360E-01 1.261E+OO 2.736E+OO NOT IDENT. NB-97 0. OOOE+OO' l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 726E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.060E+33 O.OOOE+OO SHORT HLIF TC-99M 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 272E-02 2.820E-02 5.405E-02 NOT IDENT. RH-102 7.303E-02 6.318E-02 l.150E-01 FAIL ABUN RU-103 -1.355E+OO 4.568E+OO 9.041E+OO FAIL ABUN RH-106 -1.012E-01 3.653E-01 7. ll 7E-01 NOT IDENT. RU-106 -l.012E-01 3.653E-01 7. ll 7E-01 NOT IDENT. AG-108M l.481E-02 2.037E-02 4.547E-02 NOT IDENT. AG-llOM -6.400E-03 9.520E-02 1.830E-01 NOT IDENT. SN-113 6.763E-02 1.714E-01 3.709E-01 NOT IDENT. CD-115 O.OOOE+OO 3.341E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1.103E+05 O.OOOE+OO SHORT HLIF TE-123M 2.882E-02 1.070E-01 2.150E-01 NOT IDENT. SB-124 -9.836E-03 1.580E+OO 3.550E+00 NOT IDENT. SB-125 3.695E-02 8.420E-02 1. 7 97E-01 FAIL ABUN TE-125M 6.063E+Ol 2.445E+02 5.020E+02 NOT IDENT. I-126 O.OOOE+OO l.057E+06 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 1.368E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.099E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 8.207E+09 O.OOOE+OO SHORT HLIF I-132 0.000E+OO l.522E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.630E+27 O.OOOE+OO SHORT HLIF BA-133 -2.088E-02 3.135E-02 4.720E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6. 551E-02 7.757E-02 9.008E-02 FAIL ABUN CS-135 -1.554E-02 9.616E-02 1.812E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.927E+05 0.000E+OO SHORT HLIF CE-139 -5.700E-02 8.154E-02 1. 496E-01 NOT IDENT. BA-140 O.OOOE+OO l.548E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.165E+05 O.OOOE+OO SHORT HLIF CE-141 -2.573E+OO 2.420E+Ol 4.376E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.305E+41 O.OOOE+OO SHORT HLIF CE-144 l.490E-01 2.697E-01 5.630E-01 NOT IDENT. PM-144 -1.161E-02 4.815E-02 9.171E-02 NOT IDENT. PR-144 -l.012E+OO 4.200E+OO 7.999E+00 NOT IDENT. PM-146 -2.84BE-02 3.418E-02 6.265E-02 NOT IDENT. ND-147 O.OOOE+OO 6.773E+07 0.000E+OO SHORT HLIF PM-147 -3.271E+02 6.308E+02 l.212E+03 NOT IDENT. PM-149 O.OOOE+OO 1.636E+41 O.OOOE+OO SHORT HLIF EU-150 l.443E-02 2.087E-02 4.023E-02 FAIL ABUN EU-152 9.991E-02 l. ll 7E-01 l.407E-01 FAIL ABUN GD-153 -7.806E-02 1. 391E-01 2.692E-01 NOT IDENT. EU-154 -7.594E-02 l.133E-01 l.693E-01 NOT IDENT. EU-155 5.660E-02 8.148E-02 l.747E-01 FAIL ABUN TB-160 8.732E-01 1.486E+OO 3.303E+OO FAIL ABUN H0-166M -1.685E-02 3.937E-02 7.378E-02 FAIL ABUN TM-171 -6.819E+OO 2.278E+Ol 4.796E+Ol NOT IDENT. HF-172 -2.022E-02 l.833E-01 3.626E-01 FAIL ABUN Page 3916of5809 LU-172 1. 477E-03 6.615E-02 1. 284E-01 FAIL ABUN LU-176 1. 063E-02 2.043E-02 4.075E-02 FAIL ABUN HF-181 2.753E+00 3. 720E+OO 8.291E+OO NOT IDENT. TA-182 -4.634E-01 8.979E-01 1.665E+OO NOT IDENT. RE-183 -5.402E-01 3.429E+OO 7.173E+OO NOT IDENT. RE-184 5.587E-01 3.089E+Ol 6.047E+Ol NOT IDENT. W-188 -8.200E+00 9.014E+Ol 1.569E+02 FAIL ABUN IR-192 -7.425E-02 4.095E-01 7.529E-01 FAIL ABUN HG-203 -4.247E-02 2 .137E+OO 3.752E+OO NOT IDENT. BI-207 -l.958E-02 3. 944E-02 7.065E-02 FAIL ABUN PB-210 -7. 391E-01 5.468E+OO 1.150E+Ol NOT IDENT. BI-211 0.000E+OO 4.612E-01 7.057E-01 FAIL ABUN PB-211 l.140E-01 4.836E-01 1.024E+OO NOT IDENT. RN-219 -5.026E-02 2.822E-01 5.695E-01 FAIL ABUN RA-223 2.867E-01 4.449E-01 9.125E-01 FAIL ABUN AC-227 -8.344E-02 l.874E-01 3.388E-01 FAIL ABUN TH-227 -8.344E-02 1.874E-01 3.388E-01 FAIL ABUN TH-229 -3.259E-01 3.564E-01 6.281E-01 FAIL ABUN TH-231 2.867E-01 4.449E-01 9.125E-01 FAIL ABUN PA-233 1.935E-02 4. 971E-02 9.780E-02 FAIL ABUN PA-234 4.847E-02 2. 372E-01 4.792E-01 NOT IDENT. NP-237 1.935E-02 4. 971E-02 9.780E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -4.255E-02 1. 709E-01 3.385E-01 FAIL ABUN PU-239 4.167E+Ol 2.540E+02 5.099E+02 NOT IDENT. AM-241 5.728E-02 1. 417E-01 3.076E-01 NOT IDENT. CM-243 3. 221E-03 7.276E-02 1.489E-01 FAIL ABUN BK-247 3.348E-02 5.776E-02 1.107E-01 NOT IDENT. CM-247 2.355E-03 2.560E-02 5.329E-02 FAIL ABUN CF-249 3.848E-02 2.778E-02 6.265E-02 NOT IDENT. CF-251 -3.990E-02 8.458E-02 1. 579E-01 NOT IDENT. Page 3917 of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:58:39.67 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 367 10.66* 1.146E+OO 1.361E+Ol 1. 361E+Ol 10.73 NB-95 765.81 33 99.81* 1.922E+OO 7.778E-02 2.176E+OO 54. 67 CD-109 88.03 87 3.70* 4.861E+OO 2.179E+OO 3.460E+OO 55.60 SN-126 64.28 56 9.60 2.275E+OO l.153E+OO 1.153E+OO 109.24 86.94 87 8.90 4.861E+OO 9.061E-01 9.061E-01 55.60 87.57 87 37.00* 4.861E+OO 2.179E-01 2.179E-01 55.60 BA-137M 661.66 28 89.90* 2.157E+OO 6.441E-02 6.567E-02 78.66 CS-137 661. 66 28 85.10* 2.157E+OO 6.804E-02 6.938E-02 78.66 TL-208 277.37 41 6.60 4.349E+OO 6.397E-01 6.397E-01 93.46 583.19 133 85.00* 2.382E+OO 2.978E-01 2.978E-01 24.69 860.56 ------12.50 1. 758E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 3.448E+OO ------Line Not Found ------351.06 247 12.92* 3.588E+00 2.414E+OO 2.414E+OO 19.50 BI-212 727.33 48 6.67* 2.003E+OO 1.627E+OO 1.627E+OO 42.86 785.37 23 1.10 1.888E+OO 5.097E+OO 5.097E+OO 63.14 1620.50 ------1. 47 1.045E+OO ------Line Not Found ------PB-212 74.82 135 10.28 3.688E+OO l.608E+OO 1.608E+OO 40.64 77 .11 198 17.10 3.924E+OO 1.334E+OO 1.334E+OO 26.50 238.63 448 43.60* 4.882E+00 9.538E-01 9.538E-01 12.38 300.09 40 3.30 4.084E+OO l.329E+OO 1.329E+OO 76.02 BI-214 609.32 162 45.49* 2.302E+OO 7.025E-Ol 7.028E-01 19.58 1120.29 42 14.92 l.430E+OO 8.894E-01 8.898E-01 37.99 1764.49 29 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 PB-214 74.82 135 5.80 3.688E+OO 2.851E+OO 2.852E+OO 40.64 77 .11 198 9.70 3.924E+OO 2.351E+OO 2.352E+OO 26.50 87.09 87 3.41 4.861E+OO 2.365E+OO 2.366E+OO 55.60 242.00 117 7.25 4.838E+OO 1. 505E+OO l.505E+00 47.68 295.22 185 18.42 4.142E+OO l.096E+00 1.097E+OO 21. 60 351. 93 247 35.60* 3.588E+OO 8.760E-01 8.763E-01 19.50 RN-222 609.32 162 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 1120.29 42 14.92 1.430E+OO 8.894E-01 8.898E-01 37.99 1764.49 29 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 RA-224 240.99 117 4.10* 4.838E+OO 2. 661E+OO 2.661E+OO 47.68 RA-226 609.32 162 45.49* 2.302E+OO 7.025E-01 7.028E-01 19.58 1120. 29 42 14.92 1.430E+00 8.894E-01 8.898E-01 37.99 1764.49 29 15.30 9.661E-01 8.891E-01 8.894E-01 38.85 AC-228 105.21 ------1.10 5. 896E+OO ------Line Not Found ------338.32 107 11. 27 3.705E+OO l.164E+OO 1.164E+OO 29.06 794.95 ------4.25 1.870E+OO ------Line Not Found ------835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 66 25.80* 1. 682E+OO 6.848E-01 6.848E-01 34.51 968.97 40 15.80 1. 603E+OO 7.182E-01 7.182E-01 52.38 RA-228 105.21 ------1.10 5.896E+OO ------Line Not Found ------338.32 107 11. 27 3.705E+00 l.164E+OO 1.164E+OO 29.06 794.95 ------4.25 1. 870E+OO ------Line Not Found ------835.71 ------1. 61 1. 799E+OO ------Line Not Found ------911.20 66 25.80* 1.682E+OO 6.848E-01 6.848E-01 34.51 Page 3918of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error %8.97 40 15.80 l.603E+OO 7.182E-01 52.38 TH-228 74.82 135 10.28 3.688E+OO l.608E+OO l.608E+OO 40.64 77 .11 198 17.10 3.924E+OO 1.334E+OO 1.334E+OO 26.50 238.63 448 43.60* 4.882E+OO 9.538E-01 9.538E-01 12.38 300.09 40 3.30 4.084E+OO l.329E+00 1.329E+OO 76.02 TH-230 609.32 162 45.49* 2.302E+OO 7.025E-01 7.025E-01 19.58 1120.29 42 14.92 1.430E+OO 8.894E-01 8.894E-01 37.99 1764.49 29 15.30 9.661E-01 8.891E-01 8. 891E-01 38.85 PA-231 283.69 ------1. 70 4.275E+OO ------Line Not Found ------301.36 40 5.35* 4.084E+OO 8 .196E-01 8.196E-01 76.02 TH-232 105.21 ------1.10 5.896E+OO ------Line Not Found ------338.32 107 11. 27 3.705E+OO 1.164E+OO 1.164E+OO 29.06 835. 71 ------1. 61 1. 799E+OO ------Line Not Found ------911. 20 66 25.80* 1. 682E+OO 6.848E-01 6.848E-01 34.51 968. 97 40 15.80 1. 603E+OO 7.182E-01 7.182E-01 52.38 PA-234M 766.42 33 0.32 1.922E+OO 2.426E+Ol 2.426E+Ol 54.67 1001.03 6 0.84* 1.562E+OO 2.181E+OO 2.181E+OO 245 .11 TH-234 63.29 56 3.70* 2.275E+OO 2.992E+OO 2.992E+OO 109.24 92.59 82 4.23 5.276E+OO 1. 671E+OO 1. 671E+OO 71. 54 U-234 609.32 162 45.49* 2.302E+OO 7.025E-01 7.025E-01 19.58 1120.29 42 14.92 1.430E+OO 8.894E-01 8.894E-01 37.99 1764.49 2.9 15.30 9.661E-01 8. 891E-01 8.891E-01 38.85 U-235 89.96 63 3.47 5.079E+OO l.616E+00 1.616E+OO 71. 57 93.35 82 5.60 5.276E+OO 1.262E+00 1.262E+OO 71. 54 143.76 22 10.96* 6.313E+OO l.450E-01 l.450E-01 210.79 163.33 ------5.08 6.096E+OO ------Line Not Found ------185. 72 105 57.20 5. 741E+OO 1.453E-01 l.453E-01 42.94 205.31 ------5.01 5.415E+OO ------Line Not Found ------U-238 63.29 56 3.70* 2.275E+OO 2.992E+OO 2.992E+OO 109.24 92.59 82 4.23 5.276E+OO 1. 671E+OO 1.671E+OO 71. 54 AM-243 43.53 ------5.90 1. 969E-01 ------Line Not Found ------74.66 135 67.20* 3.688E+OO 2.460E-01 2.461E-01 40.64 ANH-511 511. 00 25 100.00* 2.647E+OO 4.355E-02 4.355E-02 180.49 Flag: "*" Key line Page 3919of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235043 Acquisition date 3-0CT-2016 06:56:18 Total number of lines in spectrum 48 Number of unidentified lines 11 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 NB-95 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 PA-234M TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 64.030 461.40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1. 41E+10Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600.00Y l.41E+10Y 1600.00Y l.41E+l0Y 1. 41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 28.0 1. 59 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.361E+Ol 7.778E-02 2.179E+OO 2.179E-01 6.441E-02 6.804E-02 2.978E-01 2.414E+OO 1.627E+OO 9.538E-01 7.025E-01 8.760E-01 7.025E-01 2.661E+OO 7.025E-01 6.848E-01 6.848E-01 9.538E-01 7.025E-01 8.196E-01 6.848E-01 2 .181E+OO 2.992E+OO 7.025E-01 1.450E-01 2.992E+OO 2.460E-01 4.355E-02 4.099E+Ol 4.099E+Ol Decay Corr pCi/GRAM 1. 361E+Ol 2.176E+OO 3.460E+OO 2.179E-01 6.567E-02 6.938E-02 2.978E-01 2.414E+OO l.627E+OO 9.538E-01 7.028E-01 8.763E-01 7.028E-01 2.661E+OO 7.028E-01 6.848E-01 6.848E-01 9.538E-01 7.025E-01 8 .196E-01 6.848E-01 2.181E+OO 2.992E+OO 7.025E-01 l.450E-01 2.992E+OO 2.461E-01 4.355E-02 4.437E+Ol 4.437E+Ol 77.08%
  • Decay Corr 2-Sigma Error 0.146E+Ol 1.190E+OO 1. 924E+OO 1. 212E-01 5.166E-02 5.457E-02 0.735E-01 0.471E+OO 0.698E+00 1.181E-01 1.376E-01 1.709E-01 1. 376E-01 1.269E+OO l.376E-01 2.363E-01 2.363E-01 1.181E-01 1. 37 6E-01 6. 231E-01 2.363E-01 5.345E+00 3.268E+OO 1.376E-01 3.056E-01 3.268E+OO l.OOOE-01 7.860E-02 Flags: "M" Manually accepted 2-Sigma %Error 10.73 54.67 55.60 55.60 78.66 78.66 24.69 19.50 42.86 12.38 19.58 19.50 19.58 47.68 19.58 34.51 34.51 12.38 19.58 76. 02 34.51 245 .11 109.24 19.58 210.79 109.24 40.64 180.49 "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3920 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235043 Acquisition date : 3-0CT-2016 06: 56': 18 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 2 188.10 26 105 1. 25 375.98 365 14 5.83E-03 **** 5.70E+OO 0 270.56 39 92 1. 21 540.97 534 11 9.06E-03 **** 4.44E+OO T 1 343.92 21 29 1. 33 687.76 672 21 4.89E-03 **** 3.66E+OO T 0 369.64 80 5.9 8.98 739 .. 21 728 23 1. 91E-02 59.4 3.45E+OO 0 462.19 62 17 0.92 924.39 918 12 l.53E-02 39.0 2.87E+OO T 0 532.02 21 19 1. 04 1064.11 1061 9 5.30E-03 88.6 2.56E+OO T 0 558.91 7 12 1.21 1117.92 1114 7 1. 7 9E-03 **** 2.46E+OO 0 630.75 17 13 1. 71 12 61. 66 1258 7 4.42E-03 88.3 2.24E+00 T 3 656.18 14 20 1. 94 1312.56 1308 27 3.53E-03 **** 2.17E+OO 0 796. 66 17 21 0.85 1593.64 1588 13 4.58E-03 **** 1.87E+OO T 0 935.55 17 23 0.58 1871. 55 1864 17 4.46E-03 **** 1. 65E+OO 0 1008.00 7 10 0.70 2016.53 2011 7 1.77E-03 **** 1.55E+OO 0 1086.29 11 10 1. 94 2173.18 2168 10 3.06E-03 **** 1.46E+OO T 0 1175.33 16 11 3.35 2351.36 2346 12 4.53E-03 97.4 1.37E+OO 0 1200.56 29 3 5.17 2401. 84 2396 14 8. llE-03 45.6 1.35E+OO 0 1238.33 13 16 0.69 2477.42 2472 9 3.64E-03 **** l.32E+OO T 0 1271. 23 16 0 0.98 2543.25 2537 12 4.44E-03 50.0 1.29E+OO T 0 1377.36 7 3 1. 05 2755.63 2752 6 l.97E-03 **** 1.21E+OO 0 1450.18 5 0 0.96 2901.33 2898 6 1. 42E-03 97.4 l.15E+OO 0 1607.01 6 1 0.94 3215.17 3212 6 1. 81E-03 98.5 1. 05E+OO Flags: "T" = Tentatively associated Page 3921 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:53.48 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l *
  • Acquisition date 3-0CT-2016 06:56:18 Sensitivity 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.51 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:59:00 Nuclide Library : SOLID *
  • Sample ID G405235043 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.6579E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;l6
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 NB-95 CD-109 SN-126 BA-137M CS-137 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 PA-234M TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM l.708E-01 5.553E-01 8.325E-01 5.280E-02 2.049E-02 2.164E-02 2.035E-02 3.374E-01 3.549E-02 3.755E-02 4.193E-02 3.755E-02 3.805E-01 3.755E-02 9.363E-02 9.363E-02 3.549E-02 3.754E-02 2.600E-01 9.363E-02 3.012E+OO 1.054E+OO 3.754E-02 1. 17 5E-01 1.054E+OO 3.817E-02 2.237E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 3922 of 5809 Le (pCi/GRAM 8.834E+OO 2.780E-02 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3923 of 5809 2.505E-01 O.OOOE+OO O.OOOE+OO 4.830E-02 3.758E-01 0.000E+OO 3.333E-02 4.387E-01 5.795E+OO l.002E-01 1.566E+OO 9.783E+OO O.OOOE+OO l.544E-01 O.OOOE+OO O.OOOE+OO 5.305E-01 6.080E+OO 6.976E-01 O.OOOE+OO 8.480E-02 3.212E+02 2.604E-02 1. 815E+OO 1.201E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.519E-02 5.160E-02 3.926E+OO 3.057E-01 3.057E-01 2.038E-02 7. 968E-02 l.662E-01 O.OOOE+OO O.OOOE+OO 9.984E-02 1.329E+OO 8 .112E-02 2.342E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.050E-02 O.OOOE+OO 3. 981E-02 8.150E-02 O.OOOE+OO O.OOOE+OO 6.840E-02 O.OOOE+OO O.OOOE+OO 2.034E+Ol O.OOOE+OO 2.616E-01 4.033E-02 3.518E+OO 2.756E-02 O.OOOE+OO 5.593E+02 O.OOOE+OO l.829E-02 6.342E-02 l.245E-01 6.989E-02 8.128E-02 1. 421E+OO 3 .114E-02 2.187E+Ol l.686E-01 5.492E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF *NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3924 of 5809 1.865E-02 3.706E+OO 7.209E-01 3.324E+OO 2.621E+Ol 7.025E+Ol 3.405E-01 1.697E+OO 2. 960E-02 5.325E+OO 3.391E-01 4.586E-01 2.545E-01 4.140E-01 1.546E-01 1. 54 6E-01 2.875E-01 4.140E-01 4.465E-02 2.076E-01 4.465E-02 O.OOOE+OO 1.558E-01 2.384E+02 l.432E-01 6.888E-02 5.055E-02 2.386E-02 2.838E-02 7.248E-02 FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:58:58.62 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235043.CNF;l * *Acquisition date 3-0CT-2016 06:56:18 Sensitivity 3.000 *
  • Detector ID GAM09 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.51 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:59:00 Nuclide Library : SOLID *
  • Sample ID G405235043 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity : 1.6579E+02 GRAM *
  • Quantity Err(%) : 1.2063E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 3-JUN-2016 07:32:22 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM09 CAN.CNF;l6
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 l.361E+Ol 1.598E+OO 1.598E+OO NB-95 1.980E+OO 1. 2 60E+OO 1. 2 60E+OO CD-109 1.856E+OO 1.932E+OO 1.932E+OO SN-126 1.169E-01 1.215E-01 1.215E-01 BA-137M 6.567E-02 5. 071E-02 5.071E-02 CS-137 6.938E-02 5.356E-02 5.356E-02 TL-208 2.978E-01 7.314E-02 7.314E-02 BI-212 1.627E+OO 6.885E-01 6.885E-01 PB-212 9.538E-01 1.262E-01 l.262E-01 BI-214 7.028E-01 l.382E-01 l.382E-01 PB-214 8.763E-01 1.713E-01 1. 713E-01 RN-222 7.028E-01 l.382E-01 1.382E-01 RA-224 7.219E-01 l.316E+OO 1.316E+OO RA-226 7.028E-01 1.382E-01 1.382E-01 AC-228 6.848E-01 2.342E-01 2.342E-01 RA-228 6.848E-01 2.342E-01 2.342E-01 TH-228 9.538E-01 1.262E-01 l.262E-01 TH-230 7.025E-01 1. 381E-01 1. 381E-01 PA-231 8 .196E-01 6.352E-01 6.352E-01 TH-232 6.848E-01 2.342E-01 2.342E-01 PA-234M 2 .181E+OO 5.239E+OO 5.239E+OO TH-234 2.992E+OO 3.271E+OO 3. 271E+OO U-234 7.025E-01 1.381E-01 1. 381E-01 U-235 l.450E-01 2. 996E-01 2. 996E-01 U-238 2.992E+OO 3.271E+OO 3. 271E+OO AM-243 1.514E-01 l.012E-01 l.012E-01 ANH-511 4.355E-02 7.705E-02 7.705E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) BE-7 -5.083E+OO 1.050E+Ol 1. 074E+Ol NOT IDENT. NA-22 -3.298E-02 4.608E-02 4.842E-02 NOT IDENT. NA-24 1.000E+41 2.714E+41 O.OOOE+OO SHORT HLIF Page 3925 of 5809 AL-26 -1. 929E-02 l.902E-02 2. 091E-02 NOT IDENT. SC-46 -6.499E-04 2.958E-01 2.958E-01 FAIL ABUN V-48 6.456E+03 1.675E+04 1.700E+04 SHORT HLIF CR-51 8.305E+Ol 3.952E+02 3.970E+02 SHORT HLIF MN-54 -2.346E-02 6.064E-02 6.156E-02 NOT IDENT. C0-56 -7.088E-02 4.541E-01 4.552E-01 FAIL ABUN MN-56 -l.OOOE+41 6.120E+41 O.OOOE+OO SHORT HLIF C0-57 -1.012E-02 3.674E-02 3.702E-02 NOT IDENT. C0-58 -6.584E-02 5.251E-01 5.260E-01 NOT IDENT. FE-59 -1.864E+OO 7.403E+OO 7. 451E+OO NOT IDENT. C0-60 1.303E-02 2.081E-02 2.162E-02 NOT IDENT. ZN-65 4.lOlE-02 1. 211E-01 l.225E-01 NOT IDENT. GE-68 -9.442E-01 2.044E+OO 2.088E+OO NOT IDENT. AS-73 6.689E-01 9.849E+OO 9.853E+OO NOT IDENT. AS-74 3.681E+Ol 5.697E+03 5.697E+03 SHORT HLIF SE-75 l.556E-01 1.576E-01 1. 725E-01 NOT IDENT. BR-77 1.707E+39 l.516E+40 O.OOOE+OO SHORT HLIF SR-82 -2.042E+02 5.914E+02 5.985E+02 SHORT HLIF RB-83 4.079E-02 5.848E-01 5. 851E-01 NOT IDENT. KR-85 2.432E+00 7.156E+OO 7.239E+00 NOT IDENT. SR-85 2.780E-01 8.212E-01 8.307E-01 NOT IDENT. RB-86 -l.835E+04 3.325E+04 3.426E+04 SHORT HLIF Y-88 -l.493E-03 l.027E-01 l.027E-01 NOT IDENT. Y-91 1. 700E+Ol 4.088E+02 4.088E+02 NOT IDENT. NB-94 2.445E-02 2.628E-02 2.850E-02 NOT IDENT. NB-95M 8.954E-01 2.120E+OO 2.158E+00 NOT IDENT. ZR-95 7.360E-01 1.261E+OO 1.304E+OO NOT IDENT. NB-97 l.OOOE+41 7.501E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 l.727E+41 O.OOOE+OO SHORT HLIF M0-99 -2.204E+32 1. 060E+33 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 3.088E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 272E-02 2.829E-02 2.887E-02 NOT IDENT. RH-102 7.303E-02 6.346E-02 7.150E-02 FAIL ABUN RU-103 -l.355E+00 4.569E+00 4.609E+OO FAIL ABUN RH-106 -1.012E-01 3.653E-01 3.682E-01 NOT IDENT. RU-106 -1.012E-01 3.653E-01 3.682E-01 NOT IDENT. AG-108M 1.481E-02 2.038E-02 2.145E-02 NOT IDENT. AG-llOM -6.400E-03 9.520E-02 9.524E-02 NOT IDENT. SN-113 6.763E-02 1. 715E-01 1.742E-01 NOT IDENT. CD-115 6.029E+39 3.343E+40 0.000E+OO SHORT HLIF SN-117M 3.007E+04 l.104E+05 l .112E+05 SHORT HLIF TE-123M 2.882E-02 1.070E-01 l.078E-01 NOT IDENT. SB-124 -9.836E-03 1.580E+OO 1.580E+OO NOT IDENT. SB-125 3.695E-02 8.422E-02 8.585E-02 FAIL ABUN TE-125M 6.063E+Ol 2.445E+02 2. 461E+02 NOT IDENT. I-126 3.889E+05 l.059E+06 l.073E+06 SHORT HLIF SB-126 2.324E+05 1. 369E+06 1. 373E+06 SHORT HLIF SB-127 -5.464E+22 1.048E+23 O.OOOE+OO SHORT HLIF I-131 -l.029E+09 8.207E+09 8.220E+09 SHORT HLIF I-132 -1.000E+41 l.903E+42 O.OOOE+OO SHORT HLIF TE-132 7.295E+25 l.630E+27 O.OOOE+OO SHORT HLIF BA-133 -2.088E-02 3 .136E-02 3.275E-02 FAIL ABUN I-133 l.000E+41 8. 721E+42 O.OOOE+OO SHORT HLIF CS-134 6. 551E-02 7.763E-02 8.305E-02 FAIL ABUN CS-135 -l.554E-02 9.616E-02 9.642E-02 NOT IDENT. I-135 -1.000E+41 l.188E+42 O.OOOE+OO SHORT HLIF CS-136 -2.153E+04 3.927E+05 3.929E+05 SHORT HLIF CE-139 -5.700E-02 8.235E-02 8.626E-02 NOT IDENT. BA-140 l.218E+06 l.548E+06 1. 643E+06 SHORT HLIF LA-140 5.954E+04 4.165E+05 4.173E+05 SHORT HLIF CE-141 -2.573E+OO 2.420E+Ol 2.423E+Ol NOT IDENT. CE-143 l.OOOE+41 1. 309E+41 O.OOOE+OO SHORT HLIF CE-144 1.490E-01 2.698E-01 2.780E-01 NOT IDENT. PM-144 -l.161E-02 4.815E-02 4.844E-02 NOT IDENT. PR-144 -1.012E+OO 4.200E+OO 4.225E+00 NOT *IDENT. PM-146 -2.848E-02 3.424E-02 3.657E-02 NOT IDENT. ND-147 7.802E+07 6.787E+07 7.644E+07 SHORT HLIF PM-147 -3. 271E+02 6.310E+02 6.480E+02 NOT IDENT. PM-149 1.000E+4l 1.651E+41 O.OOOE+OO SHORT HLIF EU-150 l.443E-02 2.088E-02 2.187E-02 FAIL ABUN EU-152 9.991E-02 l .118E-01 l.206E-01 FAIL ABUN GD-153 -7.806E-02 1.392E-01 1. 436E-01 NOT IDENT. EU-154 -7.594E-02 l.134E-01 l.184E-01 NOT IDENT. EU-155 5.660E-02 8.158E-02 8.548E-02 FAIL ABUN TB-160 8.732E-01 1.487E+OO 1.538E+OO FAIL ABUN H0-166M -1.685E-02 3.938E-02 4. OllE-02 FAIL ABUN TM-171 -6. 819E+OO 2.279E+Ol 2.299E+Ol NOT IDENT. HF-172 -2.022E-02 l.834E-01 l.836E-01 FAIL ABUN Page 3926 of 5809 LU-172 1. 4 77E-03 6.615E-02 6.616E-02 FAIL ABUN LU-176 1. 063E-02 2.043E-02 2.099E-02 FAIL ABUN HF-181 2.753E+OO 3. 721E+OO 3.923E+OO NOT IDENT. TA-182 -4.634E-01 8. 981E-01 9.220E-01 NOT IDENT. RE-183 -5.402E-01 3.430E+OO 3.438E+OO NOT IDENT. RE-184 5.587E-01 3.089E+Ol 3.089E+Ol NOT IDENT. W-188 -8.200E+OO 9.014E+Ol 9.022E+Ol FAIL ABUN IR-192 -7.425E-02 4.095E-01 4.108E-01 FAIL ABUN HG-203 -4.247E-02 2.137E+OO 2.137E+OO NOT IDENT. BI-207 -l.958E-02 3. 9.44E-02 4.042E-02 FAIL ABUN PB-210 -7. 391E-01 5.468E+OO 5.478E+OO NOT IDENT. BI-211 2.414E+OO 4.735E-01 l.187E+OO FAIL ABUN PB-211 l.140E-01 4.837E-01 4.864E-Ol NOT IDENT. RN-219 -5.026E-02 2.823E-01 2.832E-01 FAIL ABUN RA-223 2.867E-01 4.452E-01 4.636E-01 FAIL ABUN AC-227 -8.344E-02 1.878E-01 l.915E-01 FAIL ABUN TH-227 -8.344E-02 1.878E-01 l.915E-01 FAIL ABUN TH-229 -3.259E-01 3.567E-01 3.858E-01 FAIL ABUN TH-231 2.867E-01 4.452E-01 4.636E-01 FAIL ABUN PA-233 1.935E-02 4.971E-02 5.047E-02 FAIL ABUN PA-234 4.847E-02 2.436E-01 2.445E-01 NOT IDENT. NP-237 1.935E-02 4.971E-02 5.047E-02 FAIL ABUN NP-238 -l.000E+41 2.896E+41 O.OOOE+OO SHORT HLIF NP-239 -4.255E-02 1.709E-01 1. 720E-01 FAIL ABUN PU-239 4.167E+Ol 2.540E+02 2.547E+02 NOT IDENT. AM-241 5.728E-02 l.418E-01 1.441E-01 NOT IDENT. CM-243 3.221E-03 7.276E-02 7.277E-02 FAIL ABUN BK-247 3.348E-02 5.816E-02 6.008E-02 NOT IDENT. CM-247 2.355E-03 2.560E-02 2.562E-02 FAIL ABUN CF-249 3.848E-02 2.795E-02 3.290E-02 NOT IDENT. CF-251 -3.990E-02 8.470E-02 8.659E-02 NOT IDENT. Page 3927 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 41. 9090 87.09 67. 6372 136.47 52.7609 45.60 52.3724 87.57 67.7092 140.51 0.0000 46.54 45.4820 88.03 67.7770 143.76 50.4599 49. 72 0.0000 88.34 67.8230 144.24 50.4972 51. 35 43.8109 88.47 67.8425 145.44 60.9684 51. 87 40.6912 89. 96 68.0626 152.43 54.0777 52.39 40.7574 1093.63 31.7307 153.25 0.0000 52.97 44.8339 91.11 0.0000 323.87 55.2053 53.44 38.4847 92.59 49.5644 156.02 0.0000 54.07 46.5922 93.35 49.6439 158.56 0.0000 57. 36 0.0000 94.56 53.3249 159.00 51. 6207 57.53 55.1932 94.65 53.3345 162.33 40.8949 57.98 56.8908 94.67 53.3368 162.66 0.0000 59.27 53.0245 94.87 53.3592 163.33 47.9451 59.32 53.0322 97.43 57.2173 165.86 51.1230 59.54 53.0654 98.43 54.6465 176.31 47.7896 60. 96 59.0175 98.44 54.6474 176.60 0.0000 61.17 59.0523 99.53 52.9723 177.52 50.9224 62.93 56.8698 100 .11 58.4272 181.07 0.0000 63.29 56.9261 102.03 46.9207 181.52 40.9528 63.58 56.9712 103.18 52.4532 184.41 55.4939 64.28 57.0801 103.37 49.7586 143.76 55.5878 66.73 51. 0724 105.21 49.0294 193.51 57.1778 67.24 50.0294 105.31 46.3145 197.03 57. 4271 125.81 63.4443 106.12 51. 8441 198.01 52.2697 67.75 64.2902 106.47 53.6992 201.83 46.2115 69.67 57.0601 109.28 59.4770 203.43 46.3008 70.83 68.4506 111. 00 71.6028 205.31 43.2409 72. 81 72.1764 111.76 0.0000 210.85 49.8938 72.87 72.1875 114.06 56.3140 215.65 38.4296 74.66 64.5773 116. 30 0.0000 222 .11 51.6174 74.82 64.6028 116.74 49.1667 227.09 42.1724 74.97 64.6266 119.76 42.9032 227.38 31. 3692 77 .11 64.9623 121.12 58.8996 228.16 0.0000 78.74 61.7827 121.22 58.9097 228.18 40.0583 79.69 74.5347 121. 78 48.6714 116. 74 40.0583 80.12 68.8708 122.06 56.1868 235.69 40.7507 80.19 0.0000 122.92 48.7681 235. 96 49.4976 80.57 67.7938 123.07 47.8425 238.63 44.8938 81. 00 70.1620 265.00 61.0402 238.98 0.0000 81. 07 73.6250 125.81 61.2633 240.99 45.0064 81. 75 65.6755 127.23 72.7485 242.00 45.0546 83.79 74.0853 127.91 63.3738 244.70 27.9175 84.00 74.1204 129.30 65.4171 252.40 0.0000 85.43 73.1975 131. 20 64.6735 252.80 31.1155 86.55 67.5563 133.02 57.2360 254.15 0.0000 86.79 67.5923 133.52 46.7809 256.23 44.6057 86.94 67.6147 136.00 55.5968 260.90 0.0000 Page 3928 of 5809
  • ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 22.4908 355.39 0.0000 584.27 14.0930 264.80 20.9943 356.01 24.3646 595.83 0.0000 265.00 26.9978 364.49 0.0000 427.87 24.6374 268.22 29.3405 366.42 0.0000 602.52 0.0000 269.46 29.3762 372.51 17.2731 604.72 14.2444 270.03 375.05 29.6682 601.14 12.3605 271.23 36.2168 377.52 19.8154 609.32 12.8502 273.65 0.0000 356.01 14.9315 610.33 18.5709 276.40 31. 8478 388.16 12.4826 614.28 13.3597 277.37 31.8768 388.63 0.0000 618.01 12.4292 277.60 31. 8837 391.69 20.0239 620.36 16. 2723 278.00 31. 8956 264.66 25.1923 621. 93 15.3275 279.20 30. 4118 401.81 26.0528 630.19 0.0000 279.54 30.4215 402.40 23.5418 631.29 24.5423 279.70 31. 9469 404.85 21.8984 633.25 23.1211 280.46 31.9700 410.95 26.2218 634.78 0.0000 283.69 37.7937 413.71 28.8148 635.95 19.2936 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 20.6477 423. 72 0.0000 645 .*85 12.6017 285.90 0.0000 427.09 23.0944 657.76 12.6747 287.50 33.3304 427.87 23.1064 657.90 0.0000 290.67 26.1274 433.94 16.3270 661.66 12.6985 293.27 0.0000 439.40 21.5612 664.57 0.0000 351.93 25.4644 453.88' 28.7320 666.33 0.0000 295.96 25.4811 463.37 18.3959 666.50 0.0000 879.38 25.5416 468.07 26.3580 667.71 0.0000 299.98 25.5738 473.00 0.0000 677.62 12.7948 300.09 25.5758 475.06 18.5322 685.70 0.0000 300.13 25.5771 476.78 21.2021 695.00 0.0000 301.36 25.6053 477.60 22.0968 696.49 20.8505 302.85 29.5236 482.18 15.0687 696. 51 20.8505 256.23 37.3477 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.8784 306.78 30.4061 497.08 17.8894 697.49 17.8799 308.46 40.9921 505.52 20.2277 702.65 12.9434 311. 90 30.5425 507.63 0.0000 706.68 15. 9596 316.51 33.0236 511.00 28.8613 711. 68 13. 9966 319.41 0.0000 514.00 29.8163 720.70 0.0000 320.08 0.0000 514.00 29.8163 721. 93 0.0000 321. 04 34.3348 520.40 21. 7656 722.78 15.0708 323.87 22.5492 520.69 0.0000 722.91 15.0714 325.23 45.1505 522.65 0.0000 723. 31 13.5670 328.76 0.0000 527.90 0.0000 724 .19 19.6039 333.37 23.9252 528.26 15.0317 727. 33 17.1148 333.97 22.3410 529.59 17.7782 733.00 9.6891 334.37 20.7521 529.87 0.0000 735.93 14.1481 338.28 20.4184 531.02 0.0000 333.97 12.1348 338.32 20.4189 537.26 0.0000 739.50 0.0000 311. 90 20.4547 546.56 0.0000 747.24 20.3109 340.48 20.4547 552.55 22.1660 748.06 18.2864 340.55 0.0000 563.25 19.5089 752.31 13.2312 344.28 20.5180 569.33 21. 4380 753.82 0.0000 345.93 22.5592 946.00 21.4399 756.73 11. 2166 351.06 23.0559 569.70 19.5773 756.80 11. 2171 351. 93 23.0722 583.19 14.0851 884.68 10.7401 Page 3929 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 12.2837 1274.44 11. 7296 1620.50 2.9833 7 66. 42 12.2871 1001.03 13. 4272 1621. 92 1.9895 766.84 12.2891 1002.74 13.4351 1678.03 0.0000 772. 60 0.0000 1004.73 11.2032 1690.97 3.0300 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 O.OOQO 1025.87 0.0000 1764.49 2.0519 778.90 7. 4112 1028.54 0.0000 1063.66 4.1089 783.70 0.0000 1037.84 7.9297 1771.35 4 .1096 785.37 9.2889 1038.76 0.0000 1791.20 0.0000 792.07 15.5243 631. 29 11.3607 1808.65 2.0708 794.95 9. 3256 1048.07 0.0000 1810.72 0.0000 795.86 9.3292 1049.04 11. 3696 1836.06 1. 0411 810.06 15.6390 1050.41 19.3367 810.29 13.5549 1063.66 11. 4233 344.28 13.5559 1077.00 0.0000 810.76 14.6004 1077.34 12. 6212 815.77 0.0000 1085.87 4.6019 1048.07 0.0000 1093.63 11. 5332 832.01 12.6216 1099.45 16.1761 834.85 21.0596 1112. 07 15.0799 835.71 14.7468 1112. 84 11. 6024 836.80 0.0000 1115. 54 5.2255 846.75 0.0000 1120.29 10.4663 846.77 16.9264 1120.55 10.4670 856.80 0.0000 1221.41 6.9795 860.56 17.0176 1129. 67 9.3301 871.09 7.4751 1131.51 0.0000 873.19 5.3436 1147.95 0.0000 875.33 0.0000 1173.23 15.5987 879.38 7.4987 1177.95 9.9401 880.51 18.2188 1189.05 16.0280 883.24 9.6552 1204.77 7.1563 884.68 16 .1011 1221.41 19.7737 889.28 9.6771 1231. 02 14.4209 894.76 16.1615 1235.36 0.0000 898.04 11.8665 1238.28 18.7853 900. 72 20.5168 1260.41 0.0000 903.28 14. 0511 1271. 87 2.7350 911.20 14.0923 1274.44 14.5977 912.08 21.1456 1274.54 14.5977 923.98 0.0000 1291.59 6.4168 926.50 10.9009 1298.22 0.0000 929 .11 8.1833 1312 .11 0.0000 937.49 12.0384 1332.49 1.8536 944.13 0.0000 1362.66 0.0000 946.00 12.0751 1365.19 7.4790 949.00 14.2859 1368.63 0.0000 667.71 0.0000 1384.29 11.2742 962. 31 15. 4572 1408.01 3.7808 964.08 18.2288 1457.56 0.0000 966 .17 28.1926 1460.82 3. 8311 911.20 18.8130 1489.16 4.8221 968. 97 18.8130 1505.03 5.8088 983.53 0.0000 1584.12 12.8215 984.45 0.0000 1596.21 0.0000 Page 3930 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:59:26.88 ******************************************************************************** GEL LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM32.CNF;277 Background date : Z-OCT-2016 11:01:57. Sample date 30-NOV-2015 13:50:00 Acquisition date : 3-0CT-2016 06:56:59. Sample ID G405235044 Sample quantity l.28844E+02 GRAM Detector name : GAM32 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.59 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 4 4 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0 0 0 0 0 0 0 0 0 0 0 Energy 54.86 75.44 77.42 89.77 93.17* 186.38* 210.19 239.04* 242 .11 271.41 295.65* 299.84 339.15 352.37* 391.59 466.45 511.13* 583.63* 609.82* 662.31 729.12* 774.90 795.25 835.57 841.13 860.36 911. 98* 969. 82 993.29 1028.32 1038.30 1120.99* 1157. 37 1171. 94 Page 3931 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 38 130 151 51 51 115 53 388 97 25 146 34 63 232 21 20 71 107 181 93 26 9 13 20 22 40 80 71 20 10 8 40 16 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 83 180 126 263 125 148 121 58 44 68 52 43 103 59 44 59 41 35 36 43 48 31 18 6 6 10 31 11 6 5 8 24 5 6 1.11 1. 59 1.15 3.52 1.15 1. 59 2.38 1. 26 1. 49 1. 42 1. 43 1. 58 1. 30 1. 31 2.32 5.18 2.83 1.27 1. 60 1. 22 0.74 4.60 1. 03 4.54 1. 58 2.46 1. 59 1. 47 1. 51 2.60 0.66 1. 68 2.46 1. 87 110. 93 152.10 156.04 180.75 187.55 373.98 421.60 479.30 485.45 544.04 592.53 600.89 679.52 705.97 784.40 934.13 1023.49 1168. 50 1220.89 1325.87 1459.49 1551.05 1591.76 1672.40 1683.51 1721. 97 1825.21 1940.90 1987.85 2057.90 2077.88 2243.25 2316.02 2345.15 107 147 147 172 184 368 415 472 472 538 587 598 672 701 780 925 1015 1162 1215 1321 1451 1544 1586 1666 1678 1715 1820 1935 1981 2051 2073 2238 2312 2341 8 1. 05E-02 44. 8 14 3.62E-02 22.5 1.51E+OO 14 4.19E-02 15.1 12 1.42E-02 65.4 8 1.41E-02 43.2 15 3.20E-02 25.3 11 1.46E-02 43.3 17 l.08E-01 6.2 2.43E+OO 17 2.70E-02 15.9 9 6.81E-03 63.7 10 4.06E-02 12.6 8 9.45E-03 37.3 15 1.75E-02 37.1 12 6.43E-02 9.5 10 5.85E-03 63.3 15 5.61E-03 86.4 14 1.96E-02 26.3 12 2.97E-02 15.0 10 5.04E-02 9.8 12 2.59E-02 17.4 17 7.21E-03 64.3 14 2.57E-03132.5 10 3.58E-03 67.2 12 5.56E-03 33.2 11 5.97E-03 30.2 13 1.12E-02 22.3 12 2.23E-02 18.4 12 l.97E-02 15.3 14 5.53E-03 35.7 10 2.72E-03 53.5 8 2.22E-03 70.7 13 l.12E-02 29.4 9 4.38E-03 38.1 8 3.40E-03 44.8 Peak Search Report (continued) Page : 2 Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1322.39 7 8 3.09 2646.06 2639 11 1. 97E-03 86.5 36 0 1377.89 22 7 1.35 2757.07 2749 14 6. llE-03 33.2 0 1461.23* 330 0 2 .11 2 923. 7 5. 2918 13 9.16E-02 5.6 38 5 1492.06 7 1 1. 39 2985.42 2984 11 1. 83E-03 27.3 6.33E-01 39 5 1494.77* 10 2 1. 92 2990.84 2984 11 2.68E-03 46.7 40 0 1765.20* 34 3 2.54 3531. 71 3526 11 9.53E-03 20.2 Flag: "*" = Peak area was modified by background subtraction Page 3932 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:59:28 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 30-NOV-2015 13:50:00 G405235044 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:56:59 128.84 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA32 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3933 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.59 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1. l19E+OO 1.532E+Ol 1.532E+Ol 11.13 OK MN-54 834.85 99.98* 1.753E+OO 6.575E-02 l.302E-01 66.33 OK AS-73 53.44 10.30* 1.124E+OO 2.236E+OO 3.186E+Ol 89.65 OK SN-113 391.69 64.94* 3.225E+OO 6.089E-02 3.886E-01 126.61 OK BA-137M 661.66 89.90* 2.104E+OO 2.882E-01 2.939E-01 34.77 OK CS-137 661.66 85.10* 2.104E+OO 3.045E-01 3.105E-01 34.77 OK TL-208 277.37 6.60 4.277E+OO Line Not Found Absent 583.19 85.00* 2.326E+OO 3.194E-01 3.194E-01 29. 96 OK 860.56 12.50 1. 714E+OO 1.087E+OO 1.087E+OO 44.65 OK PB-212 74.82 10.28 3.488E+OO 1. 754E+OO l.754E+OO 63.15 OK 77 .11 17.10 3.688E+OO 1.602E+OO l.602E+OO 30.19 OK 238.63 43.60* 4.787E+OO 1.161E+OO 1.161E+OO 12.49 OK 300.09 3.30 4.019E+00 1.581E+OO 1. 581E+OO 74.58 OK BI-214 609.32 45.49* 2.246E+OO 1.044E+OO 1.045E+OO 19.61 OK 1120.29 14.92 l.392E+OO 1.099E+OO 1.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1. 296E+00 1. 297E+00 40.46 OK PB-214 74.82 5.80 3.423E+OO Line Not Found <<INT Reject 77 .11 9.70 3.688E+OO 2.824E+OO 2.825E+OO 30.19 OK 87.09 3.41 4.545E+OO Line Not Found Absent 242.00 7.25 4.745E+OO Line Not Found <<INT Reject 295.22 18.42 4.065E+00 l.204E+OO 1.204E+OO 25.26 OK 351. 93 35.60* 3.520E+OO l.127E+00 1.128E+OO 18.92 OK RN-222 609.32 45.49* 2.246E+OO 1.044E+OO l.045E+OO 19.61 OK 1120.29 14.92 1.392E+OO 1.099E+OO 1.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1.296E+OO 1.297E+OO 40.46 OK RA-224 240.99 4.10* 4.743E+OO 9.949E-01 9.949E-01 113. 31 OK RA-226 609.32 45.49* 2.246E+OO l.044E+OO l.045E+00 19.61 OK 1120.29 14.92 1.392E+00 1.099E+OO 1.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1.296E+OO 1.297E+OO 40.46 OK AC-228 105.21 1.10 5.586E+OO Line Not Found Absent 338.32 11. 27 3.634E+OO 9.413E-01 9.413E-01 74.12 OK 794.95 4.25 l.822E+00 9.610E-01 9.610E-01 134.35 OK 835.71 1. 61 1. 753E+OO 4.083E+OO 4.083E+OO 66.33 OK 911.20 25.80* 1. 638E+OO 1. 089E+OO 1. 089E+OO 36.74 OK 968. 97 15.80 1.561E+OO 1.644E+OO l.644E+OO 30.57 OK RA-228 105.21 1.10 5.586E+00 Line Not Found Absent 338.32 11. 27 3.634E+OO 9.413E-01 9.413E-01 74.12 OK 794.95 4.25 1.822E+OO 9.610E-01 9.610E-01 134.35 OK 835.71 1. 61 1. 753E+OO 4.083E+OO 4.083E+OO 66.33 OK 911.20 25.80* 1.638E+OO 1.089E+OO 1.089E+OO 36. 74 OK 968. 97 15.80 1. 561E+OO 1.644E+OO l.644E+OO 30.57 OK TH-228 74.82 10.28 3.488E+OO 1. 754E+OO 1.754E+OO 63.15 OK 77 .11 17.10 3.688E+OO l.602E+OO 1.602E+OO 30.19 OK 238.63 43.60* 4.787E+OO 1.161E+OO 1.161E+OO 12.49 OK 300.09 3.30 4.019E+OO 1. 581E+OO 1. 581E+OO 74.58 OK TH-230 609.32 45.49* 2.246E+00 l.044E+00 1.044E+OO 19.61 OK 1120.29 14.92 1.392E+OO 1. 099E+OO l.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1.296E+OO 1.296E+OO 40.46 OK TH-232 105.21 1.10 5.586E+OO Line Not Found Absent Page 3934 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 3.38. 32 11. 27 3.634E+OO 9.413E-01 9. 4UE-01 74.12 OK 835.71 1. 61 1. 753E+OO 4.083E+OO 4.083E+OO 66.33 OK 911. 20 25.80* 1.638E+OO 1. 089E+OO 1.089E+OO 36.74 OK 968.97 15.80 1.561E+00 1.644E+OO l.644E+OO 30.57 OK U-234 609.32 45.49* 2.246E+OO 1.044E+OO 1.044E+OO 19.61 OK 1120. 29 14.92 1.392E+OO 1.099E+OO l.099E+OO 58.70 OK 1764.49 15.30 9.460E-01 1.296E+OO 1.296E+OO 40.46 OK U-235 89. 96 3.47 4.745E+OO 2.057E+OO 2.057E+OO 130.83 OK 93.35 5.60 4.974E+OO 1.206E+OO 1.206E+OO 86.31 OK 143.76 10. 96* 6.095E+00 Line Not Found Absent 163.33 5.08 5.924E+00 Line Not Found Absent 185. 72 57.20 5.599E+OO 2.286E-01 2.286E-01 50.50 OK 205.31 5.01 5.302E+OO Line Not Found Absent AM-243 43.53 5.90 l.701E-01 Line Not Found Absent 74.66 67.20* 3.488E+OO 2.684E-01 2.684E-01 63.15 OK ANH-511 511. 00 100.00* 2.589E+OO 1.623E-01 1.623E-01 52.51 OK Flag: "*" = Keyline Page 3935 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:59:29.62 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l *
  • Acquisition date 3-0CT-2016 06:56:59 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:50:00 Analyst initials: MXRl *
  • Sample ID G405235044 Sample Quantity 1.2884E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.532E+Ol 1.671E+OO MN-54 l.302E-01 8.467E-02 AS-73 3.186E+Ol 2.799E+Ol SN-113 3.886E-01 4.821E-01 BA-137M 2.939E-01 l.OOlE-01 CS-137 3.105E-01 l.058E-01 TL-208 3.194E-01 9.377E-02 PB-212 l.161E+00 l.422E-01 BI-214 1.045E+OO 2.008E-01 PB-214 l.128E+OO 2.091E-01 RN-222 l.045E+OO 2.008E-01 RA-224 9.949E-01 l.105E+OO RA-226 1.045E+OO 2.008E-01 AC-228 l.089E+OO 3. 921E-01 RA-228 l.089E+OO 3. 921E-01 TH-228 l .161E+OO l.422E-01 TH-230 l.044E+OO 2.008E-01 TH-232 l.089E+OO 3. 921E-01 U-234 l.044E+OO 2.007E-01 U-235 5.108E-02 1.911E-01 AM-243 2.684E-01 l.661E-01 ANH-511 1.623E-01 8.350E-02 Non-Identified Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 C0-56 Page 3936 of 5809 Key-Line Activity (pCi/GRAM 2.506E+OO -8. 921E-03 O.OOOE+OO 6.046E-03 4.123E-02 O.OOOE+OO O.OOOE+OO 5.512E-01 K.L. Cnt Uncert ( 1. 96-sigma) 1. 54 7E+Ol 5.188E-02 9.800E+40 2.175E-02 4.229E-01 2.167E+04 6.341E+02 5.713E-01 MDA (pCi/GRAM 4. 511E-01 1.251E-01 3.319E+Ol 5.433E-01 7.404E-02 7.822E-02 7.671E-02 l.OOlE-01 l.519E-01 l.500E-01 l.519E-01 1. 072E+OO l.519E-01 2.638E-01 2.638E-01 1. OOlE-01 l.518E-01 2.638E-01 l.518E-01 3.779E-01 l.194E-01 5.915E-02 MDA (pCi/GRAM 3.00lE+Ol 1.0lOE-01 O.OOOE+OO 5.847E-02 8.253E-01 O.OOOE+OO O.OOOE+OO l.223E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN MN-56 O.OOOE+OO l.040E+41 O.OOOE+OO SHORT HLIF C0-57 3.406E-02 5.823E-02 1. 08 6E-01 NOT IDENT. C0-58 -1.143E-01 7.650E-01 1.399E+OO NOT IDENT. FE-59 -4.330E+OO 7.303E+OO l.328E+Ol NOT IDENT. C0-60 -1.343E-02 4.507E-02 8.589E-02 FAIL ABUN ZN-65 4.067E-02 1. 891E-01 3.581E-01 NOT IDENT. GE-68 -5.810E-01 2.754E+OO 5.325E+OO NOT IDENT. AS-74 0.000E+OO 9.203E+03 0.000E+OO SHORT HLIF SE-75 2.311E-02 2.574E-01 4.937E-01 NOT IDENT. BR--;-77 0.000E+OO O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.952E+02 O.OOOE+OO SHORT HLIF RB-83 1.167E-01 7.457E-01 l.459E+OO NOT IDENT. KR-85 6.281E+OO 9.799E+00 1. 784E+Ol NOT IDENT. SR-85 7.154E-01 1.124E+OO 2.045E+OO NOT IDENT. RB-86 O.OOOE+OO 4.291E+04 O.OOOE+OO SHORT HLIF Y-88 -4.482E-03 1. 911E-01 4.407E-01 NOT IDENT. Y-91 -3.384E+02 7.146E+02 1. 301E+03 NOT IDENT. NB-94 1. 416E-02 4.069E-02 7.803E-02 NOT IDENT. NB-95 -1.161E+OO l.098E+OO 1.683E+OO NOT IDENT. NB-95M -1. 288E+OO 3.004E+OO 4.916E+OO NOT IDENT. ZR-95 -2 .196E-01 l.750E+OO 3.245E+00 NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.025E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.442E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 262E-02 4.516E-02 7.724E-02 NOT IDENT. RH-102 -2.012E-02 6. 996E-02 l.264E-01 NOT IDENT. RU-103 2.299E+OO 7.164E+OO 1.426E+Ol FAIL ABUN RH-106 -4.744E-01 5.920E-01 9.785E-01 NOT IDENT. RU-106 -4.744E-01 5.920E-01 9.785E-01 NOT IDENT. AG-108M 2.176E-02 3.465E-02 6. 963E-02 NOT IDENT. CD-109 2.428E+00 1.849E+OO 3.319E+00 NOT IDENT. AG-llOM 3.685E-02 1.118E-01 2.257E-01 NOT IDENT. CD-115 O.OOOE+OO 4.189E+40 0.000E+OO SHORT HLIF SN-117M O.OOOE+OO 1.595E+05 O.OOOE+OO SHORT HLIF TE-123M 5.386E-02 1.461E-01 2.907E-01 NOT IDENT. SB-124 -9.120E-01 2.422E+OO 4.624E+OO NOT IDENT. SB-125 8.443E-02 l.266E-01 2.561E-01 NOT IDENT. TE-125M 5.334E+02 3.889E+02 7.665E+02 NOT IDENT. I-126 O.OOOE+OO 1.684E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.052E+06 O.OOOE+OO SHORT HLIF SN-126 l.573E-01 l.174E-01 2 .112E-01 NOT IDENT. SB-127 O.OOOE+OO l .116E+23 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 1.133E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.453E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.439E+27 O.OOOE+OO SHORT HLIF BA-133 l.622E-02 4.874E-02 8.748E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.337E-02 8.343E-02 1.326E-01 FAIL ABUN CS-135 1. 792E-02 1. 576E-01 2. 7 61E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.740E+05 O.OOOE+OO SHORT HLIF CE-139 9.947E-03 1.365E-01 2.636E-01 NOT IDENT. BA-140 O.OOOE+OO 2.122E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 7.184E+05 O.OOOE+OO SHORT HLIF CE-141 -6.399E+OO 3.227E+Ol 6.163E+Ol NOT IDENT. CE-143 O.OOOE+OO l.187E+41 O.OOOE+OO SHORT HLIF CE-144 9.855E-02 4;739E-01 8.445E-01 NOT IDENT. PM-144 3.148E-02 6.516E-02 1.308E-01 NOT IDENT. PR-144 2. 710E+OO 5.678E+OO 1.139E+Ol NOT IDENT. PM-146 3.352E-03 5.285E-02 1.005E-01 NOT IDENT. ND-147 0.000E+OO 6.956E+07 O.OOOE+OO SHORT HLIF PM-147 -1.808E+02 1.058E+03 1.838E+03 NOT IDENT. PM-149 O.OOOE+OO l.233E+41 O.OOOE+OO SHORT HLIF EU-150 6.617E-03 3.070E-02 5.401E-02 FAIL ABUN EU-152 -5.155E-02 1.185E-01 1.897E:....01 NOT IDENT. GD-153 -l.069E-01 2.415E-01 4.129E-01 NOT IDENT. EU-154 2.369E-03 l.204E-01 2.444E-01 NOT IDENT. EU-155 l.676E-01 1.345E-01 2.648E-01 NOT IDENT. TB-160 5. 871E-01 1.933E+OO 3.981E+OO FAIL ABUN H0-166M -4.417E-02 6.777E-02 l.138E-01 NOT IDENT. TM-171 7.814E-01 4.477E+Ol 7.632E+Ol NOT IDENT. HF-172 3. 331E-01 2. 772E-01 5.414E-01 FAIL ABUN LU-172 -3.785E-03 7.576E-02 1.534E-01 FAIL ABUN LU-176 4.00lE-03 2.484E-02 4.856E-02 FAIL ABUN HF-181 3.763E+OO 5.799E+OO 1.183E+Ol NOT IDENT. TA-182 -6.339E-01 l.090E+OO 1.950E+OO FAIL ABUN RE-183 -8.362E-01 6.026E+OO 9.996E+OO NOT IDENT. Page 3937 of 5809 RE-184 -2.181E+Ol 4.265E+Ol 7.224E+Ol NOT IDENT. W-188 -1.266E+02 l.539E+02 2.354E+02 NOT IDENT. IR-192 -:-9.195E-02 5.634E-01 1.057E+OO FAIL ABUN HG-203 6.113E-01 3.203E+OO 6.174E+OO NOT IDENT. BI-207 -4.214E-02 4.513E-02 7.618E-02 FAIL ABUN PB-210 1. 356E+OO 1.040E+Ol l.925E+Ol NOT IDENT. BI-211 O.OOOE+OO 5.759E-01 8.395E-01 FAIL ABUN PB-211 -1. 771E-01 7.765E-01 l.433E+OO NOT IDENT. BI-212 1.169E+OO 7.675E-01 1.618E+OO NOT IDENT. .. RN-219 l.888E-02 4.558E-01i 8.647E-01 FAIL ABUN RA-223 -3.368E-01 7.014E-01 1.268E+OO FAIL ABUN AC-227 -3.623E-02 2.456E-01 4.646E-01 FAIL ABUN TH-227 -3.623E-02 2.456E-01 4.646E-01 FAIL ABUN TH-229 3.743E-02 5.301E-01 1.021E+OO FAIL ABUN PA-231 5.779E-01 4. 931E-01 9.741E-01 NOT IDENT. TH-231 -3.368E-01 7.014E-01 l.268E+00 FAIL ABUN PA-233 4.165E-02 6.750E-02 l.359E-01 FAIL ABUN PA-234 .-l.260E-01 2.940E-01 5.549E-01 FAIL ABUN PA-234M 1.419E+OO 4.281E+OO 9.168E+OO NOT IDENT. TH-234 -2.028E+OO 2.086E+OO 3.544E+OO FAIL ABUN NP-237 4.165E-02 6.750E-02 1. 359E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 -2.028E+OO 2.086E+OO 3.544E+OO FAIL ABUN NP-239 2.873E-02 3.333E-01 5.902E-01 NOT IDENT. PU-239 3.179E+02 4.286E+02 7.909E+02 NOT IDENT. AM-241 -2.473E-02 2.382E-01 4.294E-01 NOT IDENT. CM-243 -1.356E-01 l.305E-01 2.098E-01 NOT IDENT. BK-247 2.219E-03 8. 321E-02 1. 591E-01 NOT IDENT. CM-247 2.447E-02 3.973E-02 8.037E-02 NOT IDENT. CF-249 -2.829E-02 4.991E-02 7.748E-02 NOT IDENT. CF-251 -2.551E-03 1.168.E-01 2.259E-01 NOT IDENT. Page 3938 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:59:27.56 Nuclide Line Activity Report Nuclide Type: .; Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 314 10.66* l .119E+OO 1.532E+Ol 1.532E+Ol 11.13 MN-54 834.85 20 99.98* 1. 753E+OO 6.575E-02 1.302E-01 66.33 AS-73 53.44 44 10.30* l.124E+OO 2.236E+OO 3.186E+Ol 89.65 SN-113 391.69 22 64.94* 3.225E+OO 6.089E-02 3.886E-01 126.61 BA-137M 661. 66 94 89.90* 2.104E+OO 2.882E-01 2.939E-01 34.77 CS-137 661. 66 94 85.10* 2.104E+OO 3.045E-01 3.105E-01 34.77 TL-208 277.37 ------6.60 4.277E+OO ------Line Not Found ------583.19 108 85.00* 2.326E+OO 3.194E-01 3.194E-01 29. 96 860.56 40 12.50 1.714E+OO l.087E+OO 1.087E+OO 44.65 BI-211 72.87 ------1.23 3.214E+OO ------Line Not Found ------351.06 242 12.92* 3.520E+OO 3.106E+OO 3.106E+OO 18.92 PB-212 74.82 150 10.28 3.488E+OO 2.434E+OO 2.434E+OO 44.97 77 .11 173 17.10 3.688E+OO 1.602E+OO 1.602E+OO 30.19 238.63 416 43.60* 4.787E+OO 1.161E+OO 1.161E+OO 12.49 300.09 36 3.30 4.019E+OO 1.581E+OO 1.581E+OO 74.58 BI-214 609.32 183 45.49* 2.2'46E+OO 1.044E+OO 1.045E+OO 19.61 1120.29 39 14.92 1.392E+OO 1.099E+OO l.099E+OO 58.70 1764.49 32 15.30 9.460E-01 1.296E+OO 1.297E+OO 40.46 PB-214 74.82 150 5.80 3.488E+OO 4.314E+OO 4.315E+OO 44.97 77 .11 173 9.70 3.688E+OO 2.824E+OO 2.825E+OO 30.19 87.09 ------3.41 4.545E+OO ------Line Not Found ------242.00 104 7.25 4.743E+OO 1. 766E+OO 1. 767E+OO 31.72 295.22 155 18.42 4.065E+OO 1.204E+OO 1.204E+OO 25.26 351.93 242 35.60* 3.520E+OO 1.127E+OO l.128E+OO 18.92 RN-222 609.32 183 45.49* 2.246E+OO 1.044E+OO 1.045E+OO 19.61 1120.29 39 14.92 1.392E+OO 1.099E+OO 1.099E+OO 58.70 1764.49 32 15.30 9.460E-01 1. 2 96E+OO l.297E+OO 40.46 RA-224 240.99 104 4.10* 4.743E+OO 3.124E+OO 3.124E+OO 31.72 RA-226 609.32 183 45.49* 2.246E+OO 1.044E+OO 1.045E+OO 19.61 1120.29 39 14.92 1.392E+OO l.099E+OO 1.099E+OO 58.70 1764.49 32 15.30 9.460E-01 l.296E+OO 1.297E+00 40.46 AC-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 66 11. 27 3.634E+OO 9.413E-01 9. 413E-01 74.12 794.95 13 4.25 1.822E+OO 9.610E-01 9.610E-01 134.35 835.71 20 1. 61 1. 753E+OO 4.083E+OO 4.083E+00 66.33 911.20 79 25.80* 1.638E+OO 1.089E+OO 1.089E+OO 36.74 968. 97 70 15.80 1.561E+OO 1.644E+OO 1.644E+OO 30.57 RA-228 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 66 11. 27 3.634E+OO 9.413E-01 9.413E-01 74.12 794.95 13 4.25 1.822E+OO 9.610E-01 9.610E-01 134.35 835.71 20 1. 61 1.753E+OO 4.083E+OO 4.083E+OO 66.33 911.20 79 25.80* 1.638E+OO 1.089E+OO 1.089E+OO 36.74 968.97 70 15.80 1.561E+OO 1.644E+OO 1.644E+OO 30.57 TH-228 74.82 150 10.28 3.488E+OO 2.434E+OO 2.434E+OO 44.97 77 .11 173 17 .10 3.688E+OO 1.602E+OO l.602E+OO 30.19 238.63 416 43.60* 4.787E+OO 1.161E+OO 1.161E+OO 12.49 300.09 36 3.30 4.019E+OO 1.581E+OO 1.581E+OO 74.58 Page 3939 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235044 Acquisition date 3-0CT-2016 06:56:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-230 609.32 l.83 45.49* 2.246E+OO l.044E+00 l.044E-t00 19.61 1120.29 39 14.92 l.392E+OO l.099E+OO l.099E+OO 58.70 1764.49 32 15.30 9.460E-01 l.296E+OO l.296E+OO 40.46 TH-232 105.21 ------1.10 5.586E+OO ------Line Not Found ------338.32 66 11. 27 3.634E+OO 9.413E-01 9.413E-01 74.12 835. 71 20 1. 61 1. 753E+OO 4.083E+OO 4.083E+OO 66.33 911.20 79 25.80* l.638E+OO l.089E+OO l.089E+OO 36.74 968.97 70 15.80 l.561E+OO 1. 644E+OO l.644E+00 30.57 U-234 609.32 183 45.49* 2.246E+OO l.044E+OO l.044E+00 19.61 1120.29 39 14.92 l.392E+00 l.099E+OO l.099E+00 58.70 1764.49 32 15.30 9.460E-01 l.296E+OO l.296E+OO 40.46 U-235 89. 96 58 3.47 4.745E+OO 2.057E+00 2.057E+OO 130.83 93.35 58 5.60 4.974E+OO l.206E+OO 1. 206E+OO 86.31 143.76 ------10. 96* 6.095E+OO ------Line Not Found ------163.33 ------5.08 5.924E+OO ------Line Not Found ------185.72 126 57.20 5.599E+OO 2.286E-01 2.286E-01 50.50 205.31 ------5.01 5.302E+OO ------Line Not Found ------AM-243 43.53 ------5.90 1.701E-01 ------Line Not Found ------74.66 150 67.20* 3.488E+OO 3.723E-01 3. 723E-01 44.97 ANH-511 511. 00 72 100.00* 2.589E+OO l.623E-01 l.623E-01 52.51 Flag: "*" Key line Page 3940 of 5809 Summary of Nuclide Activity Sample ID : G405235044 Acquisition date Page : 3 3-0CT-2016 06:56:59 Total number of lines in spectrum 40 Number of unidentified lines 10 Number of lines tentatively identified by NID 30 Nuclide Type : Nuclide K-40 MN-54 AS-73 SN-113 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Hlife 1.25E+09Y 312.05D 80.30D 115. 09D 30.08Y 30.08Y l.41E+10Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600. OOY l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+10Y l.41E+l0Y 7.54E+04Y 1.41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 98 14.2 6.38 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.532E+Ol 6.575E-02 2.236E+OO 6.089E-02 2.882E-01 3.045E-01 3.194E-01 3.106E+OO 1.161E+OO 1.044E+OO 1.127E+OO 1.044E+OO 3.124E+OO 1.044E+OO 1.089E+OO 1.089E+OO 1.161E+OO 1.044E+OO 1. 089E+OO 1.044E+OO 2.286E-01 3. 723E-01 l.623E-01 3.753E+Ol 3.753E+Ol
  • Decay Corr pCi/GRAM 1.532E+Ol 1.302E-01 3.186E+Ol 3.886E-01 2.939E-01 3.105E-01 3.194E-01 3.106E+OO 1.161E+OO 1.045E+OO 1.128E+OO 1.045E+OO 3.124E+OO 1.045E+OO 1. 089E+OO 1.089E+OO 1.161E+OO 1.044E+OO 1.089E+OO 1.044E+OO 2.286E-01 3. 723E-01 1.623E-01 6.756E+Ol 6.756E+Ol 75.00% Decay Corr 2-Sigma Error 0.171E+Ol 0.864E-01 2.856E+Ol 4.919E-01 l.022E-01 1.079E-01 0.957E-01 0.588E+OO 0.145E+OO 0.205E+OO 0.213E+OO 0.205E+OO 0. 991E+OO 0.205E+OO 0.400E+OO 0.400E+OO 0.145E+OO 0.205E+OO 0.400E+00 0.205E+OO 1.155E-01 1.675E-01 0.852E-01 "M" Manually accepted 2-Sigma %Error 11.13 66.33 89.65 126.61 34.77 34.77 29. 96 18.92 12.49 19.61 18.92 19.61 31.72 19.61 36.74 36.74 12.49 19.61 36.74 19.61 50.50 44.97 52.51 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3941of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235044 Acquisition date : 3-0CT-2016 06:56:59 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 210.19 57 131 2.38 421. 60 415 11 1.46E-02 86.7 5.22E+OO T 0 271.41 26 72 1. 42 544.04 538 9 6.81E-03 **** 4.35E+OO T 0 466.45 21 60 5.18 934.13 925 15 5.61E-03 **** 2.79E+OO 0 72...9.12 26 48 0.74 1459.49 1451 17. 7. 21E-03 **** 1.95E+OO 0 774.90 9 31 4.60 1551. 05 1544 14 2.57E-03 **** 1.86E+OO 0 841.13 21 5 1. 58 1683.51 1678 11 5.97E-03 60.4 l.74E+OO 0 993.29 19 6 1. 51 1987.85 1981 14 5.53E-03 71. 3 1.53E+OO 0 1028.32 10 5 2.60 2057.90 2051 10 2. 72E-03 **** 1.49E+OO T 0 1038.30 8 8 0.66 2077.88 2073 8 2.22E-03 **** 1.48E+OO T 0 1157. 37 15 5 2.46 2316.02 2312 9 4.38E-03 76.2 1.36E+OO 0 1171.94 12 6 1. 87 2345.15 2341 8 3.40E-03 89.6 1.34E+OO T 0 1322.39 7 8 3.09 2646.06 2639 11 1.97E-03 **** 1.22E+OO 0 1377.89 *21 7 1. 35 2757.07 2749 14 6. llE-03 66.5 1.18E+00 5 1492.06 6 1 1. 39 2985.42 2984 11 1. 83E-03 54.6 1.lOE+OO 5 1494.77 9 2 1. 92 2990.84 2984 11 2.68E-03 93.3 1. lOE+OO Flags: "T" = Tentatively associated Page 3942 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:59:41.13 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l *
  • Acquisition date 3-0CT-2016 06:56:59 Sensitivity 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:50:00 Nuclide Library : SOLID *
  • Sample ID G405235044 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.2884E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN *
  • Eff.' File : DKAlOO: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 AS-73 SN-113 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 1.595E-01 5.356E-02 1.542E+Ol 2.472E-01 3.273E-02 3.458E-02 3.433E-02 4.617E-02 6.814E-02 6.861E-02 6.814E-02 4.948E-01 6.814E-02 1.132E-01 1.132E-01 4.617E-02 6.812E-02 1.132E-01 6.812E-02 1. 768E-01 5.614E-02 2.649E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 C0-56 MN-56 Page 3943 of 5809 Le (pCi/GRAM 1. 346E+Ol 4.261E-02 O.OOOE+OO 2.071E-02 3.521E-01 O.OOOE+OO O.OOOE+OO 5.390E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-110M CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-l53 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 3944 of 5809 5.083E-02 6.092E-01 5.444E+OO 3.566E-02 1.523E-01 2.287E+OO O.OOOE+OO 2.285E-01 O.OOOE+OO O.OOOE+OO 6.466E-01 8.165E+OO 9.362E-01 O.OOOE+OO 1. 562E-01 5.618E+02 3.505E-02 7.227E-01 2.270E+00 1.407E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.627E-02 5.558E-02 6.369E+OO 4.248E-01 4.248E-01 3.183E-02 l.584E+00 9.756E-02 O.OOOE+OO O.OOOE+OO 1.357E-01 1. 731E+OO 1.170E-01 3.616E+02 O.OOOE+OO O.OOOE+OO 1.008E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.982E-02 O.OOOE+OO 5.953E-02 1. 266E-01 O.OOOE+OO O.OOOE+OO 1.237E-01 O.OOOE+OO O.OOOE+OO 2.886E+Ol O.OOOE+OO 3.969E-01 5.828E-02 5.074E+OO 4.548E-02 O.OOOE+OO 8.597E+02 O.OOOE+OO 2.469E-02 8.606E-02 1.933E-01 l.030E-01 l.246E-01 1.692E+OO 4. 951E-02 3.540E+Ol 2.545E-01 6.462E-02 2.210E-02 5.354E+OO 8. 296E-01 4.656E+OO 3.090E+Ol NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HL.IF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3945 of 5809 1.073E+02 4.829E-01 2.861E+OO 3.065E-02 9.049E+OO 4.023E-01 6.490E-01 7.481E-01 3.939E-01 fi.808E-01 2.136E-01 2 .136E-01 4.771E-01 4.495E-01 5.808E-01 6.260E-02 2.360E-01 3. 965E+OO 1.667E+OO 6.260E-02 O.OOOE+OO 1.667E+OO 2.778E-01 3.743E+02 2.009E-01 9.768E-02 7.347E-02 3.665E-02 3.499E-02 1.048E-01 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:59:46.46 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235044.CNF;l *
  • Acquisition date 3-0CT-2016 06:56:59 Sensitivity : 3.000 *
  • Detector ID GAM32 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:50:00 Nuclide Library : SOLID *
  • Sample ID G405235044 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity 1.2884E+02 GRAM *
  • Quantity Err(%) 1.5523E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 23-AUG-2016 07:56:33 Eff. Geometry : CAN '*
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM32 CAN.CNF;ll
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.532E+Ol 1.853E+OO 1.853E+OO MN-54 l.302E-01 8.485E-02 8.485E-02 AS-73 3.186E+01 2.875E+Ol 2.875E+Ol SN-113 3.886E-01 4.824E-01 4.824E-01 BA-137M 2.939E-01 l.009E-01 l.009E-01 CS-137 3.105E-01 l.066E-01 1.066E-01 TL-208 3.194E-01 9.475E-02 9.475E-02 PB-212 1.161E+OO 1.550E-01 1.550E-01 BI-214 l.045E+00 2.058E-01 2.058E-01 PB-214 1.128E+OO 2.143E-01 2.143E-01 RN-222 1.045E+OO 2.058E-01 2.058E-01 RA-224 9.949E-01 1.115E+OO 1.115E+OO RA-226 1.045E+OO 2.058E-01 2.058E-01 AC-228 1.089E+OO 3. 960E-01 3. 960E-01 RA-228 1. 089E+OO 3.960E-01 3. 960E-01 TH-228 1.161E+OO l.550E-01 1.550E-01 TH-230 1.044E+OO 2.057E-01 2.057E-01 TH-232 1. 089E+OO 3. 960E-01 3. 960E-01 U-234 1.044E+OO 2.057E-01 2.057E-01 U-235 5.108E-02 1. 911E-01 1. 911E-01 AM-243 2.684E-01 l.675E-01 1.675E-01 ANH-511 1.623E-01 8.376E-02 8.376E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 2.506E+OO 1. 54 7E+Ol 1.551E+Ol NOT IDENT. NA-22 -8.921E-03 5.188E-02 5.203E-02 NOT IDENT. NA-24 1.000E+41 1.077E+41 O.OOOE+OO SHORT HLIF AL-26 6.046E-03 2.176E-02 2.193E-02 NOT IDENT. SC-46 4.123E-02 4.229E-01 4.234E-01 FAIL ABUN V-48 -1.319E+04 2.167E+04 2.248E+04 SHORT HLIF CR-51 -1.960E+02 6. 341E+02 6.403E+02 SHORT HLIF C0-56 5.512E-01 5.717E-01 6.234E-01 FAIL ABUN Page 3946 of 5809 MN-56 1.000E+41 l.040E+41 O.OOOE+OO SHORT HLIF C0-57 3.406E-02 5.825E-02 6.024E-02 NOT IDENT. C0-58 -1.143E-01 7.650E-01 7.667E-01 NOT IDENT. FE-59 -4.330E+OO 7.310E+OO 7.566E+00 NOT IDENT. C0-60 -1.343E-02 4.507E-02 4.547E-02 FAIL ABUN ZN-65 4.067E-02 1. 891E-01 l.900E-01 NOT IDENT. GE-68 -5.810E-01 2.755E+OO 2.767E+00 NOT IDENT. AS-74 3.403E+03 9.208E+03 9.335E+03 SHORT HLIF SE-75 2.311E-02 2.574E-01 2.576E-01 NOT IDENT. .. BR-77 2. 083E+39. l.850E+40
  • O.OOOE+OO SHORT HLIF SR-82 9.421E+02 8. 963E+02 9.918E+02 SHORT HLIF RB-83 1.167E-01 7.459E-01 7.478E-Ol NOT IDENT. KR-85 6.281E+OO 9.802E+OO 1.020E+Ol NOT IDENT. SR-85 7.154E-01 1.125E+OO 1.170E+OO NOT IDENT. RB-86 -1.259E+04 4.291E+04 4.328E+04 SHORT HLIF Y-88 -4.482E-03 1. 911E-01 1. 911E-01 NOT IDENT. Y-91 -3.384E+02 7.147E+02 7.308E+02 NOT IDENT. NB-94 1. 416E-02 4.069E-02 4 .119E-02 NOT IDENT. NB-95 -l.161E+OO 1.099E+OO l.218E+OO NOT IDENT. NB-95M -1. 288E+OO 3.005E+OO 3.061E+OO NOT IDENT. ZR-95 -2 .196E-01 1. 750E+00 1. 753E+00 NOT IDENT. NB-97 l.000E+41 2.404E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 l.026E+41 O.OOOE+OO SHORT HLIF M0-99 -1. 064E+32 1.442E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 3.275E+41 0.000E+OO SHORT HLIF RH-101 -1. 262E-02 4.522E-02 4.558E-02 NOT IDENT. RH-102 -2.012E-02 6.998E-02 7.056E-02 NOT IDENT. RU-103 2.299E+OO 7.164E+OO 7.239E+OO FAIL ABUN RH-106 -4.744E-01 5.927E-01 6. 301E-01 NOT IDENT. RU-106 -4.744E-01 5.927E-01 6.301E-01 NOT IDENT. AG-108M 2.176E-02 3.466E-02 3.602E-02 NOT IDENT. CD-109 2.428E+OO 1.859E+OO 2.157E+OO NOT IDENT. AG-llOM 3.685E-02 1.119E-01 1.131E-01 NOT IDENT. CD-115 2.749E+39 4.189E+40 O.OOOE+OO SHORT HLIF SN-ll 7M -4.939E+04 1. 596E+05 l.612E+05 SHORT HLIF TE-123M 5.386E-02 l.461E-01 1.481E-01 NOT IDENT. SB-124 -9.120E-01 2.422E+OO 2.457E+OO NOT IDENT. SB-125 8.443E-02 1.267E-01 l.323E-01 NOT IDENT. TE-125M 5.334E+02 3. 901E+02 4.583E+02 NOT IDENT. I-126 l.239E+05 1.684E+06 1. 685E+06 SHORT HLIF SB-126 -1.046E+06 2.062E+06 2 .115E+06 SHORT HLIF SN-126 1.573E-01 1.179E-01 1. 375E-01 NOT IDENT. SB-127 5.625E+22 1.369E+23 O.OOOE+OO SHORT HLIF I-131 l.357E+09 l.133E+l0 l .135E+10 SHORT HLIF I-132 -1.000E+41 1.902E+42 O.OOOE+OO SHORT HLIF TE-132 -7.437E+26 2.459E+27 O.OOOE+OO SHORT HLIF BA-133 1. 622E-02 4.874E-02 4.929E-02 NOT IDENT. I-133 -l.000E+41 l.905E+42 O.OOOE+OO SHORT HLIF CS-134 6.337E-02 8.347E-02 8.822E-02 FAIL ABUN CS-135 1. 792E-02 1.576E-01 1.578E-01 NOT IDENT. I-135 -l.000E+41 5. 696E+42 O.OOOE+OO SHORT HLIF CS-136 -3.287E+05 4.753E+05 4.979E+05 SHORT HLIF CE-139 9.947E-03 l.365E-01 1. 366E-01 NOT IDENT. BA-140 1.717E+06 2.123E+06 2.259E+06 SHORT HLIF LA-140 -5.228E+05 7.189E+05 7.565E+05 SHORT HLIF CE-141 -6.399E+OO 3.227E+Ol 3.240E+Ol NOT IDENT. CE-143 l.000E+41 1.191E+41 O.OOOE+OO SHORT HLIF CE-144 9.855E-02 4.739E-01 4.760E-01 NOT IDENT. PM-144 3.148E-02 6.519E-02 6.672E-02 NOT IDENT. PR-144 2.710E+OO 5.679E+OO 5.809E+OO NOT IDENT. PM-146 3.352E-03 5.285E-02 5.287E-02 NOT IDENT. ND-147 3.136E+06 6.956E+07 6.957E+07 SHORT HLIF PM-147 -1.808E+02 l.058E+03 l.062E+03 NOT IDENT. PM-149 -1.000E+41 1.253E+41 0.000E+OO SHORT HLIF EU-150 6.617E-03 3.070E-02 3.084E-02 FAIL ABUN EU-152 -5.155E-02 1.186E-01 1. 208E-01' NOT IDENT. GD-153 -1.069E-01 2.416E-01 2.463E-01 NOT IDENT. EU-154 2.369E-03 l.204E-01 l.204E-01 NOT IDENT. EU-155 1. 676E-01 l.350E-01 1. 54 7E-01 NOT IDENT. TB-160 5.871E-01 1.933E+OO 1. 951E+OO FAIL ABUN H0-166M -4.417E-02 6.781E-02 7.067E-02 NOT IDENT. TM-171 7.814E-01 4.477E+Ol 4.477E+Ol NOT IDENT. HF-172 3.331E-01 2.825E-01 3.199E-01 FAIL ABUN LU-172 -3.785E-03 7.576E-02 7.578E-02 FAIL ABUN LU-176 4.00lE-03 2.484E-02 2.491E-02 FAIL ABUN HF-181 3.763E+OO 5.801E+OO 6.044E+OO NOT IDENT. TA-182 -6.339E-01 l.090E+OO 1.127E+OO FAIL ABUN RE-183 -8.362E-01 6.027E+OO 6.039E+OO NOT IDENT. Page 3947 of 5809 RE-184 -2.181E+Ol 4.298E+Ol 4.409E+Ol NOT IDENT. W-188 -1.266E+02 1.546E+02 l.648E+02 NOT IDENT. IR-192 -9.195E-02 5.635E-01 5.650E-01 FAIL ABUN HG-203 6.113E-01 3.203E+OO 3.215E+OO NOT IDENT. BI-207 -4.214E-02 4.516E-02 4.900E-02 FAIL ABUN PB-210 l.356E+OO l.040E+Ol 1.042E+Ol NOT IDENT. BI-211 3.106E+OO 5.925E-01 1.521E+OO FAIL ABUN PB-211 -1. 771E-01 7.766E-01 7.807E-01 NOT IDENT. BI-212 1.169E+OO 7.697E-01 9.328E-01 NOT IDENT. l.888E-02 4.558E-01 4.559E-01 FAIL ABUN RA-223 -3.368E-01 7.017E-01 7.179E-01 FAIL ABUN AC-227 -3.623E-02 2.457E-01 2.462E-01 FAIL ABUN TH-227 -3.623E-02 2.457E-01 2.462E-01 FAIL ABUN TH-229 3.743E-02 5.301E-01 5.304E-01 FAIL ABUN PA-231 5.779E-01 5.082E-01 5.711E-01 NOT IDENT. TH-231 -3.368E-01 7.017E-01 7.179E-01 FAIL ABUN PA-233 4.165E-02 6.753E-02 7.009E-02 FAIL ABUN PA-234 -1.260E-01 3.274E-01 3.323E-01 FAIL ABUN PA-234M l.419E+OO 4.282E+OO 4.329E+OO NOT IDENT. TH-234 -2.028E+OO 2.134E+OO 2.321E+OO FAIL ABUN NP-237 4.165E-02 6.753E-02 7.009E-02 FAIL ABUN NP-238 -l.OOOE+41 3.908E+41 O.OOOE+OO SHORT HLIF U-238 -2.028E+OO 2.134E+OO 2. 321E+OO FAIL ABUN NP-239 2.873E-02 3.333E-01 3.335E-01 NOT IDENT. PU-239 3.179E+02 4.289E+02 4.522E+02 NOT IDENT. AM-241 -2.473E-02 2.382E-01 2.384E-01 NOT IDENT. CM-243 -1.356E-01 1. 311E-01 1. 447E-01 NOT IDENT. BK-247 2.219E-03 8.321E-02 8. 321E-02 NOT IDENT. CM-247 2.447E-02 3.995E-02 4.144E-02 NOT IDENT. CF-249 -2.829E-02 4. 996E-02 5.156E-02 NOT IDENT. CF-251 -2. 551E-03 1.168E-01 l.168E-01 NOT IDENT. Page 3948 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 81.3617 87.09 99.8288 136.47 73.4470 45.60 69.3616 87.57 99.8871 140.51 0.0000 46.54 72.8394 88.03 99.9429 143.76 64.6930 49. 72 0.0000 88.34 99.9801 144.24 67.2428 51. 35 54.2351 88.47 99. 9961 145. 4"4 77. 4116 51.87 52.7743 89. 96 81. 0940 152.43 66.0339 52.39 54.3289 1093.63 81.1599 153.25 0.0000 52.97 55.8913 91.11 0.0000 323.87 62.7439 53.44 57.4459 92.59 94.1075 156.02 0.0000 54.07 56.7480 93.35 94.1909 158.56 0.0000 57.36 0.0000 94.56 62.3499 159.00 57.8910 57.53 63.9085 94.65 62. 3562 162.33 70.0033 57.98 65.4759 94. 67 62.3578 162.66 0.0000 59.27 74.3794 94.87 62. 3721 163.33 81.1690 59.32 83.5401 97.43 84.2091 165.86 76.2001 59.54 73.2654 98.43 65.0351 176.31 69"*. 0706 60. 96 74.5708 98.44 65'. 0359 176.60 0.0000 61.17 78.0372 99.53 81.9977 177.52 55.3086 62.93 90.8994 100 .11 80.8445 181. 07 0.0000 63.29 97.8550 102.03 66.5067 181.52 52.0135 63.58 85.2279 103.18 93.2275 184.41 57.3418 64.28 72. 6333 103.37 87.1919 143.76 61. 7473 66.73 80.9898 105.21 54.6045 193.51 66.4830 67.24 99.5746 105.31 54.6106 197.03 81. 5652 125.81 90.3684 106.12 72.8778 198.01 63.1926 67.75 90.3773 106.47 76.5505 201.83 75.6892 69.67 101. 0780 109.28 58.4996 203.43 67.8465 70.83 96.1976 111. 00 84.2464 205.31 74 .1135 72.81 71. 5662 111.76 0.0000 210.85 65.1035 72.87 85.5750 114. 06 78.3911 215.65 72.8753 74.66 81. 8822 116. 30 0.0000 222 .11 61.5935 74.82 81. 8999 116.74 83.5193 227.09 53.7390 74.97 81.9164 119.76 72.6868 227.38 54.6452 77 .11 82.1487 121.12 74.0195 228.16 0.0000 78.74 87. 8116 121.22 74.0268 228.18 60.9485 79.69 87.9193 121. 78 59.2544 116.74 60.9485 80.12 84.8260 122.06 58.0361 235.69 58.0982 80.19 0.0000 122.92 85.2740 235. 96 58.1080 80.57 103.7360 123.07 85.2866 238.63 47.8307 81. 00 89.6389 265.00 66.7860 238.98 0.0000 81. 07 89.6470 125.81 53.2924 240.99 47.9035 81. 75 80.2800 127.23 86.8741 242.00 47.9342 83.79 104.1583 127.91 99.3503 244.70 54.3591 84.00 102.6066 129.30 83.3165 252. 4.0 0.0000 85.43 98.0449 131.20 83.4678 252.80 43.7090 86.55 99.7628 133. 02 81.1151 254.15 0.0000 86.79 99.7923 133.52 76.1588 256.23 46.5396 86.94 99.8109 136.00 72.5805 260.90 0.0000 Page 3949 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 50.4491 355.39 0.0000 584.27 24.3720 264.80 48.6189 356.01 28.9227 595.83 0.0000 265.00 48.6243 364.49 0.0000 427.87 15.9851 268.22 38.6068 366.42 0.0000 602.52 0.0000 269.46 40.0157 372. 51 36.9316 604. 72 30.4146 270.03 42.3295 375.05 29.1919 607.14 24.0317 271.23 42.3595 377.52 36.0455 609.32 25.6533 273.65 0.0000
  • 356.01 34 .1996 610.33 22.4543 276.40 43.4132 388.16 39.6538 614.28 19.2722 277.37 54.5287 388.63 0.0000 618.01 17.1523 277.60 52.6872 391.69 34.3250 620. 36 7.5101 278.00 49.9252 264.66 36.4369 621. 93 24.6892 279.20 49. 9603 401. 81 34.4852 630.19 0.0000 279.54 59.2240 402.40 26.6100 631. 29 21.5365 279.70 59.2292 404.85 34.5329 633.25 19.3953 280.46 61.1069 410.95 29.6814 634.78 0.0000 283.69 38.9597 413.71 29.7180 635.95 18.3344 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 48.2834 423.72 0.0000 645.85 23.8038 285.90 0.0000 427.09 31. 8874 657.76 14.6640 287.50 31. 6073 427.87 26.9143 657.90 0.0000 290.67 53.0850 433.94 27.9846 661. 66 19.5762 293.27 0.0000 439.40 29.0525 664.57 0.0000 351. 93 46.2189 453.88 29.2313 666.33 0.0000 295. 96 46.2381 463.37 29.3469 666.50 0.0000 879.38 33.6768 468. 07 27.3763 667.71 0.0000 299.98 39.3203 473.00 0.0000 677.62 14. 2108 300.09 39.3229 475.06 23.3870 685.70 0.0000 300.13 39.3237 476.78 24.4209 695.00 0.0000 301.36 26.7019 477.60 23.4113 696.49 16.4941 302.85 40.7892 482.18 21. 4149 696. 51 16.4941 256.23 30.9717 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.8980 306.78 31.9504 497.08 19.4905 697.49 24.1995 308.46 43.2663 505.52 30.8765 702.65 19. 8311 311. 90 34.8667 507.63 0.0000 706.68 25.3706 316.51 40.6213 511. 00 24.7539 711. 68 23.2003 319.41 0.0000 514.00 27.8800 720.70 0.0000 320.08 0.0000 514.00 27.8800 721. 93 0.0000 321.04 40.7193 520.40 18.6328 722.78 9.9767 323.87 48.3676 520.69 0.0000 722. 91 16.6284 325.23 48.4019 522.65 0.0000 723. 31 16.6302 328.76 0.0000 527.90 0.0000 724 .19 18.2980 333.37 22.8745 528.26 19.7267 727. 33 21. 0905 333.97 34.3220 529.59 21. 8135 733.00 16.6785 334.37 38.6205 529.87 0.0000 735.93 13.3545 338.28 34.3982 531. 02 0.0000 333.97 14.4742 338.32 34.3989 537.26 0.0000 739.50 0.0000 311. 90 34.4370 546.56 0.0000 747.24 20.0991 340.48 34.4370 552.55 25.1436 748.06 14.5197 340.55 0.0000 563.25 17.8792 752.31 10.0646 344.28 40.2543 569.33 15.8105 753.82 0.0000 345.93 36.4515 946.00 15. 8112 756.73 15.6765 351.06 41.8344 569. 70 20.0290 756.80 15. 6771 351. 93 38.4855 583.19 24.3626 884.68 15.7096 Page 3950 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 25.8226 1274.44 4.2940 1620.50 2.0240 766.42 26.9502 1001.03 8.0607 1621. 92 1. 0123 766.84 21. 3379 1002.74 8.0640 1678.03 0.0000 772.60 0.0000 1004.73 11. 6535 1690.97 5 .1187 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50' 0.0000 1025.87 0.0000 1764.49 2.0714 778.90 11. 8330 1028.54 0.0000 1063.66 5.1831 783.70 0.0000 1037.84 11.7440 1771. 35 2.0736 785.37 9.0322 1038.76 0.0000 1791.20 0.0000 792.07 10.1807 631.29 10.8625 1808.65 1.0427 794.95 16.9818 1048.07 0.0000 1810.72 0.0000 795.86 16.9861 1049.04 10.8691 1836.06 2.0941 810.06 17.0538 1050.41 9. 9667 810.29 17.0551 1063.66 9. 9969 344.28 17.0557 1077.00 0.0000 810.76 17.0569 1077.34 14.5859 815.77 0.0000 1085.87 13.7009 1048.07 0.0000 1093.63 10.0648 832.01 13.7256 1099.45 11. 9098 834.85 12.0193 1112. 07 12.8618 835.71 12.0223 1112.84 13.7833 836.80 0.0000 1115.54 8.8266 846.75 0.0000 1120. 29 11. 9645 846.77 8.2685 1120. 55 11. 9653 856.80 0.0000 1221.41 11. 9677 860.56 13.8320 1129. 67 7.3779 871.09 13.8706 1131. 51 0.0000 873.19 13.8784 1147.95 0.0000 875.33 0.0000 1173.23 19.3629 879.38 8.1088 1177.95 17.7058 880.51 16.2222 1189.05 11. 2083 883.24 6.9575 1204.77 18.7427 884.68 10.4399 1221.41 16.9255 889.28 10.4528 1231.02 19.7862 894.76 8.1413 1235.36 0.0000 898.04 13.9688 1238.28 18.8721 900.72 3.4945 1260.41 0.0000 903.28 17.4841 1271. 87 4.7501 911. 20 12.2637 1274.44 9.5050 912.08 12.2667 1274.54 11. 4060 923.98 0.0000 1291.59 7.6299 926.50 7.9146 1298.22 0.0000 929 .11 14. 9596 1312 .11 0.0000 937.49 15.8730 1332.49 10.5750 944 .13 0.0000 1362.66 0.0000 946.00 15.0229 1365.19 5.8041 949.00 12.3812 1368.63 0.0000 667.71 0.0000 1384.29 4.4381 962. 31 17.7454 1408.01 3.9004 964.08 12.7824 1457.56 0.0000 966 .17 19.8939 1460.82 1. 9691 911.20 24.8845 1489.16 3.1666 968.97 24.8845 1505.03 5.9539 983.53 0.0000 1584.12 8.0474 984.45 0.0000 1596.21 0.0000 Page 3951of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:00:16.02 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM39.CNF;l34 Background date : Z-OCT-2016 11:02:13. Sample date 30-NOV-2015 14:15:00 Acquisition date : 3-0CT-2016 06:57:26. Sample ID G405235045 Sample quantity 1.30599E+02 GRAM Detector name : GAM39 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.96 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 2 2 2 0 0 1 1 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3952 of 5809 Energy 46.69* 63.24* 74.84* 77.22* 87.36 89.78 92.73* 98.29 129.50 185.71* 188.58 238.76* 241. 52 253.81 270.62* 295.68* 328.16 338.56* 352.21* 402.02 405.46 511. 00* 518.51 550.08 583.56* 609.72* 62 6. 25 634.04 653.39 661.71 731.13 801.05 911.52* 949.47 BACKGROUND*CORRECTED SAMPLE PEAK REPORT Area 45 94 212 319 77 71 92 33 60 58 36 293 110 31 38 129 28 53 205 23 18 27 19 43 119 104 14 13 8 223 78 6 63 13 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 126 265 189 173 167 172 132 128 137 59 57 102 107 144 124 111 49 65 83 34 8 60 35 29 44 67 30 18 27 45 48 23 31 7 0.82 1.19 1. 41 1. 27 1. 42 1. 28 1. 20 0.63 1. 58 1. 44 1. 32 1. 27 1. 92 3.13 2.47 1. 70 0.91 1. 51 1. 41 1. 43 0. 72 1. 44 4.84 7.41 1. 97 1. 67 0.54 1. 26 0.93 1. 27 11. 48 3.85 1. 45 2.86 93.22 126.33 149.51 154.29 174.55 179.41 185.29 196. 43 258.85 371. 26 377.00 477.36 482.89 507.47 541.09 591. 20 656.17 676.97 704.28 803.90 810.79 1021.86 1036.89 1100. 04 1167. 01 1219.33 1252.38 1267. 96 1306.68 1323.32 1462.16 1602.02 1822.98 1898.90 90 121 143 143 171 171 171 193 253 365 365 473 473 496 538 585 652 671 696 798 808 1015 1031 1090 1158 1212 1246 1262 1299 1316 1446 1593 1815 1893 8 l.25E-02 47.8 12 2.62E-02 37.2 18 5.89E-02 13.3 2.59E+OO 18 8.87E-02 9.7 20 2.14E-02 28.8 2.92E+OO 20 1.97E-02 33.6 20 2.54E-02 26.3 8 9.03E-03 62.8 13 1. 65E-02 42. 5 19 1.62E-02 32.2 3.39E+OO 19 9.93E-03 43.3 15 8.14E-02 8.7 1.57E+OO 15 3.06E-02 26.5 19 8.58E-03 94.5 13 l.04E-02 63.2 13 3.59E-02 19.2 9 7.87E-03 48.4 11 l.47E-02 33.3 16 5.70E-02 12.4 11 6.37E-03 54.3 6 5.llE-03 33.2 15 7.63E-03 73.8 14 5.28E-03 69.9 23 1.19E-02 36 .1 19 3.31E-02 16.9 15 2.90E-02 20.0 13 3.93E-03 83.3 8 3.63E-03 64.5 12 2.12E-03141.4 14 6.19E-02 9.3 40 2.16E-02 32.2 12 1. 80E-03161. 8 16 l.75E-02 24.4 10 3.49E-03 49.6 Peak Search Report (continued) Page : 2 Sample ID : G405235045 Acquisition date 3-0CT-2016 06:57:26 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 1 965.08 24 21 2.03 1930 .11 1921 23 6.77E-03 37.6 8.95E-01 36 1 969.68* 25 13 2.03 1939.31 1921 23 6.86E-03 37.1 37 0 1120.38 26 11 2240.76 2236 10 7.08E-03 30.6 38 0 1219.97 9 8 1. 03 2439.98 2435 8 2.58E-03 61. 8 39 0 1351.60 7 2 0.80 2703.30 2697 10 l.82E-03 59.6 40 0 1461.00* 218 3 1. 69 2922.13 2916 15 6.05E-02 7.2 41 0 1764.89* 25 6 2.03 3530.06 3522 12 6.96E-03 28.6 Flag: "*" = Peak area was modified by background subtraction Page 3953 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 08:00:17 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 14:15:00 G405235045 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:57:26 130.60 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA39 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page :)954 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:06.96 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235045 Acquisition date 3-0CT-2016 06:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 J_0.66* 8.983E-01 1.246E+Ol 1.246E+Ol U.40 OK CD-109 88.03 3.70* 6.753E+00 9 .131E-01 l.450E+OO 137.17 OK SN-126 64.28 9.60 6. 931E+OO 9.550E-01 9.550E-01 74.43 OK 86.94 8.90 6.753E+OO 3.796E-01 3.796E-01 137.17 OK 87.57 37.00* 6.753E+OO 9.131E-02 9.131E-02 137.17 OK BA-137M 661.66 89.90* 1. 758E+OO 8.171E-01 8. 331E-01 18.55 OK CS-137 661.66 85.10* 1.758E+OO 8.632E-01 8. 801E-01 18.55 OK TL-208 277.37 6.60 3.709E+OO Line Not Found Absent 583.19 85.00* l.952E+OO 4.201E-01 4.201E-01 33.77 OK 860.56 12.50 1.416E+OO Line Not Found Absent PB-210 46.54 4.25* 6.835E+OO l.060E+OO 1. 088E+OO 95.59 OK PB-212 74.82 10.28 6.812E+OO 1.330E+OO 1.330E+OO 44.93 OK 77 .11 17.10 6.799E+OO 1.830E+OO 1.830E+OO 19.49 OK 238.63 43.60* 4.209E+OO 9.906E-01 9.906E-01 17.39 OK 300.09 3.30 3.465E+OO Line Not Found Absent BI-214 609.32 45.49* 1. 882E+OO 7 .116E-01 7 .119E-01 40.00 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.402E-01 61. 26 OK 1764.49 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 OK PB-214 74.82 5.80 6.812E+OO Line Not Found <<INT Reject 77 .11 9.70 6.799E+OO 3.226E+OO 3.227E+OO 19.49 OK 87.09 3.41 6.755E+OO Line Not Found <<INT Reject 242.00 7.25 4.163E+OO Line Not Found <<INT Reject 295.22 18.42 3.510E+00 1.225E+OO 1.226E+OO 38.30 OK 351. 93 35.60* 3.012E+OO 1.158E+OO 1.159E+OO 24.76 OK RN-219 271.23 10.80 3.788E+OO 5.644E-01 5.644E-01 126.49 OK 401.81 6.60* 2.683E+OO 7. 771E-01 7. 771E-01 108.62 OK RN-222 609.32 45.49* 1.882E+OO 7 .116E-01 7 .119E-01 40.00 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.402E-01 61. 26 OK 1764.49 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 OK RA-224 240.99 4.10* 4.170E+OO 1.830E+OO 1.830E+OO 124.19 OK RA-226 609.32 45.49* l.882E+00 7 .116E-01 7 .119E-01 40.00 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.402E-01 61. 26 OK 1764.49 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 OK AC-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11.27 3 .118E+OO 9.148E-01 9.148E-01 66.59 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835.71 1. 61 1. 451E+OO Line Not Found Absent 911. 20 25.80* 1.351E+OO 1.024E+OO 1.024E+OO 48.76 OK 968. 97 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 OK RA-228 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .118E+OO 9.148E-01 9.148E-01 66.59 OK 794.95 4.25 1.512E+OO Line Not Found Absent 835. 71 1. 61 1.451E+OO Line Not Found Absent 911. 20 25.80* 1.351E+OO 1.024E+OO 1.024E+OO 48.76 OK 968.97 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 OK TH-228 74.82 10.28 6.812E+OO 1.330E+OO 1.330E+OO 44.93 OK 77 .11 17.10 6.799E+OO l.830E+00 1.830E+OO 19.49 OK 238.63 43.60* 4.209E+OO 9.906E-01 9.906E-01 17.39 OK 300.09 3.30 3.465E+00 Line Not Found Absent Page 3955 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235045 Acquisition date 3-0CT-2016 06:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45 *. 4 9* l.882E+OO 7 .116E-01 7 .116E-01 40.()0 OK 1120.29 14.92 l.136E+OO 8.399E-01 8.399E-01 61. 26 OK 1764.49 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 OK TH-232 105.21 1.10 6.612E+OO Line Not Found Absent 338.32 11. 27 3 .118E+OO 9.148E-01 9.148E-01 66.59 OK 835.71 1. 61 l.451E+00 Line Not Found Absent 911.20 25.80* l.351E+00 1.024E+OO 1.024E+OO 48.76 OK 968. 97 15.80 l.283E+OO 6.878E-01 6.878E-01 74.10 OK TH-234 63.29 3.70* 6. 931E+OO 2.478E+OO 2.478E+OO 74.43 OK 92.59 4.23 6.723E+OO 2.120E+OO 2.120E+00 52.64 OK U-234 609.32 45.49* 1. 882E+OO 7 .116E-01 7 .116E-01 40.00 OK 1120.29 14.92 1.136E+OO 8.399E-01 8.399E-01 61.26 OK 1764.49 15.30 7.483E-01 1.182E+OO l.182E+OO 57.30 OK U-235 89. 96 3.47 6.741E+OO 2.003E+OO 2.003E+OO 67.29 OK 93.35 5.60 6.723E+OO 1.602E+OO 1.602E+OO 52.64 OK 143.76 10. 96* 5.959E+OO Line Not Found Absent 163.33 5.08 5.556E+OO Line Not Found Absent 185. 72 57.20 5.108E+OO l.256E-01 1.256E-01 64.32 OK 205.31 5.01 4.746E+OO Line Not Found Absent U-238 63.29 3.70* 6.931E+OO 2.478E+00 2.478E+00 74.43 OK 92.59 4.23 6.723E+OO 2.120E+OO 2.120E+OO 52.64 OK AM-243 43.53 5.90 6.236E+OO Line Not Found Absent 74.66 67.20* 6.812E+00 2.035E-01 2.035E-01 44.93 OK CM-247 278.00 3.40 3.702E+00 Line Not Found Absent 287.50 2.00 3. 596E+OO Line Not Found Absent 402.40 72. 00* 2.683E+OO 7.124E-02 7.124E-02 108.62 OK ANH-511 511. 00 100.00* 2.183E+OO 7.425E-02 7.425E-02 147.59 OK Flag: "*" = Keyline Page 3956 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:00:19.09 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l *
  • Acquisition date 3-0CT-2016 06:57:26 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.96 Half life ratio : ***** *
  • Sample date 30-NOV-2015 14:15:00 Analyst initials: MXRl *
  • Sample ID G405235045 Sample Quantity l.3060E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date : 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File :' DKAlOO: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4'
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1. 246E+Ol 1.759E+OO 9.655E-01 CD-109 l.450E+OO 1.949E+OO 2. OllE+OO SN-126 9 .131E-02 l.227E-01 1. 266E-01 BA-137M 8. 331E-01 1.515E-01 8.879E-02 CS-137 8.801E-01 1.600E-01 9.379E-02 TL-208 4.201E-01 l.390E-01 8. 596E-02 PB-210 1.088E+OO 1.019E+OO 1.013E+OO PB-212 9.906E-01 1.688E-01 1.370E-01 BI-214 7 .119E-01 2. 7 91E-01 1.914E-01 PB-214 1.159E+OO 2. 811E-01 l.463E-01 RN-219 7.771E-01 8.272E-01 8.942E-01 RN-222 7 .119E-01 2. 7 91E-01 1.914E-01 RA-224 1,830E+OO 2.228E+OO l.470E+OO RA-226 7 .119E-01 2. 7 91E-01 1.914E-01 AC-228 1. 024E+OO 4.895E-01 3. 7 51E-Ol RA-228 1. 024E+OO 4.895E-01 3.751E-01 TH-228 9.906E-01 l.688E-01 1.370E-01 TH-230 7 .116E-01 2.790E-01 1.913E-01 TH-232 1.024E+OO 4.895E-01 3. 7 51E-01 TH-234 2.478E+OO l.807E+OO 1.248E+OO U-234 7.116E-01 2.790E-01 1.913E-01 U-235 -1.990E-Ol 1. 996E-01 3.622E-01 U-238 2.478E+OO 1. 807E+OO 1.248E+OO AM-243 2.035E-01 8. 962E-02 6.731E-02 CM-247 7 .*124E-02 7.583E-02 8.208E-02 ANH-511 7.425E-02 1.074E-01 6.394E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 1. 751E+OO 2.149E+Ol 4.017E+Ol NOT IDENT. NA-22 4.445E-02 5.918E-02 l.349E-01 NOT IDENT. NA-24 O.OOOE+OO 1.432E+41 0.000E+OO SHORT HLIF AL-26 -8.668E-03 1.699E-02 2.134E-02 NOT IDENT. Page 3957 of 5809 SC-46 -5.846E-02 5.860E-01 1.146E+OO FAIL ABUN V-48 O.OOOE+OO 3.139E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6.613E+02 O.OOOE+OO SHORT HLIF MN-54 1.545E-02 8.954E-02 l.816E-01 NOT IDENT. C0-56 4.078E-01 6.426E-01 l.407E+OO NOT IDENT. MN-56 O.OOOE+OO 1.576E+41 0.000E+OO SHORT HLIF C0-57 -3.654E-03 5.449E-02 9.604E-02 NOT IDENT. C0-58 -4.402E-01 7.885E-01 1.456E+OO NOT IDENT. FE-59 2.037E+OO 9.875E+OO 2.042E+Ol NOT IDENT. CO-QO 3.264E-02 5.325E-02 1 .. 195E-01 NOT IDENT. ZN-65 l.253E-01 2.324E-01 4.662E-01 NOT IDENT. GE-68 6.924E-01 2.970E+OO 6.224E+OO NOT IDENT. AS-73 -4.170E-01 3 .118E+OO 5.609E+OO NOT IDENT. AS-74 O.OOOE+OO 1.086E+04 O.OOOE+OO SHORT HLIF SE-75 -2.095E-01 2.733E-01 4.849E-01 FAIL ABUN BR-77 O.OOOE+OO 3.012E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 1.209E+03 O.OOOE+OO SHORT HLIF RB-83 -3.386E-01 1.046E+OO 1.656E+OO NOT IDENT. KR-85 l.421E+Ol 1.096E+Ol 1.978E+Ol NOT IDENT. SR-85 1.628E+OO 1.257E+OO 2.269E+OO NOT IDENT. RB-86 O.OOOE+OO 4. 581E+o4 O.OOOE+OO SHORT HLIF Y-88 -1.176E-01 2.608E-01 4.803E-01 NOT IDENT. Y-91 6.397E+02 8.695E+02 l.859E+03 NOT IDENT. NB-94 -l.941E-02 4.900E-02 8. 496E-02 NOT IDENT. NB-95 7.626E-02 1. 446E+OO 2.664E+OO NOT IDENT. NB-95M 1.422E+OO 3.906E+OO 6.866E+OO NOT IDENT. ZR-95 -2.056E-01 l.979E+OO 3.678E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.815E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -4.958E-03 4 .141E-02 6.638E-02 NOT IDENT. RH-102 7.185E-02 1.172E-01 1.808E-01 NOT IDENT. RU-103 2.587E+OO 9.471E+OO l.836E+Ol FAIL ABUN RH-106 l.318E-01 7.418E-01 l.294E+00 NOT IDENT. RU-106 1.318E-01 7.418E-01 1.294E+OO NOT IDENT. AG-108M -6.352E-03 3. 896E-02 7.200E-02 NOT IDENT. AG-llOM -5.919E-03 l.410E-01 2.799E-01 NOT IDENT. SN-113 6.530E-02 3.406E-01 6.542E-01 NOT IDENT. CD-115 O.OOOE+OO 5.024E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1. 651E+05 O.OOOE+OO SHORT HLIF TE-123M 3.697E-02 1.543E-01 3.045E-01 NOT IDENT. SB-124 1.262E+OO 3.157E+OO 7.318E+OO NOT IDENT. SB-125 2.918E-02 1.279E-01 2. 511E-01 NOT IDENT. TE-125M 1.444E+02 3.487E+02 6.389E+02 NOT IDENT. I-126 O.OOOE+OO 2.273E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.068E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.232E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.435E+10 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.922E+27 O.OOOE+OO SHORT HLIF BA-133 1. 791E-03 5.375E-02 9.266E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 8.342E-02 9.081E-02 1.777E-01 FAIL ABUN CS-135 l.249E-02 2.037E-01 3.500E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 6.216E+05 O.OOOE+OO SHORT HLIF CE-139 -5.362E-02 1. 317E-01 2.472E-01 NOT IDENT. BA-140 O.OOOE+OO 3.037E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1.052E+06 O.OOOE+OO SHORT HLIF CE-141 -2.619E+Ol 3.200E+Ol 5.883E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.346E+41 O.OOOE+OO SHORT HLIF CE-144 -l.957E-01 4.220E-01 7 .114E-01 NOT IDENT. PM-144 -2. 872E-03 8.994E-02 1.642E-01 NOT IDENT. PR-144 3.310E-01 7.749E+OO 1. 431E+Ol NOT IDENT. PM-146 9. 02'4E-03 6.539E-02 l.242E-01 FA.IL ABUN ND-147 O.OOOE+OO 8.100E+07 O.OOOE+OO SHORT HLIF PM-147 -9.931E+Ol 9.089E+02 l.598E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 -l.350E-02 4.044E-02 6.529E-02 FAIL ABUN EU-152 7.796E-02 1.224E-01 2.469E-01 FAIL ABUN GD-153 2.676E-01 3.293E-01 3.699E-01 FAIL ABUN EU-154 l.120E-01 1.453E-01 3.316E-01 NOT IDENT. EU-155 1.119E-01 1.167E-01 2.243E-01 FAIL ABUN TB-160 3.131E-01 2.750E+OO 5.584E+OO FAIL ABUN H0-166M -5.493E-02 8.688E-02 l.449E-01 FAIL ABUN TM-171 -4.845E+OO 6.447E+OO 1.105E+Ol NOT IDENT. HF-172 -9.526E-02 2.935E-01 4.588E-01 FAIL ABUN Page 3958 of 5809 LU-172 8.858E-02 1. 092E-01 2.413E-01 FAIL ABUN LU-176 -l.185E-03 3.308E-02 6.085E-02 FAIL ABUN HF-181 -2.819E+OO 6.867E+OO 1.225E+Ol NOT IDENT. TA-182 1.167E+OO l.413E+00 2.752E+OO FAIL ABUN RE-183 -2.629E-Ol 1.463E+00 2.617E+OO NOT IDENT. RE-184 -1.577E+Ol 4.880E+Ol 9.253E+Ol . NOT IDENT. W-188 -9.552E+Ol 2.001E+02 3.197E+02 FAIL ABUN IR-192 l.602E-01 6.201E-01 l.215E+OO FAIL ABUN HG-203 -6.154E-01 3.619E+OO 6.762E+OO NOT IDENT. BI-207 1. 393E-02
  • 6.840E-02 1.392E-01 FAIL ABUN BI-211 O.OOOE+OO 7.743E-01 1.056E+OO FAIL ABUN PB-211 1. 095E+OO 7.122E-01 1.517E+OO FAIL ABUN BI-212 6.161E-01 8.263E-01 1.649E+OO NOT IDENT. RA-223 1. 374E-01 8.338E-01 1.453E+OO FAIL ABUN AC-227 -1. 511E-01 3.262E-01 5.279E-01 NOT IDENT. TH-227 -1. 511E-01 3.262E-01 5.279E-01 NOT IDENT. TH-229 1. 256E-01 6.026E-01 1. 067E+OO FAIL ABUN PA-231 7.262E-01 6.223E-01 1.248E+OO NOT IDENT. TH-231 1. 374E-01 8.338E-01 1.453E+OO FAIL ABUN PA-233 -l.932E-02 7.146E-02 1.329E-01 NOT IDENT. PA-234 -3.674E-01 4.776E-01 6.938E-01 FAIL ABUN PA-234M -2.144E+OO 6.396E+OO 1. 208E+Ol NOT IDENT. NP-237 -l.932E-02 7.146E-02 l.329E-01 FAIL ABUN NP-238 0.000E+OO 1. 960E+41 0.000E+OO SHORT HLIF NP-239 -5.772E-02 2.933E-01 5.093E-01 FAIL ABUN PU-239 O.OOOE+OO 8.128E+02 7.298E+02 FAIL ABUN AM-241 3.412E-03 7.181E-02 l.204E-01 NOT IDENT. CM-243 -3.753E-02 1.064E-01 1.'836E-01 FAIL ABUN BK-247 -5.036E-02 9.351E-02 1. 696E-01 NOT IDENT. CF-249 -7.312E-03 4.930E-02 9.183E-02 FAIL ABUN CF-251 -6.946E-03 l.387E-01 2. 661E-01 NOT IDENT. Page 3959 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:00:16.70 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 208 10.66* 8.983E-01 l.246E+Ol l.246E+Ol 14.40 CD-109 88.03 89 3.70* 6.753E+OO 2.042E+OO 3.242E+OO 57.56 SN-126 64.28 111 9.60 6.931E+OO 9.550E-01 9.550E-01 74.43 86.94 89 8.90 6.753E+OO 8.490E-01 8.490E-01 57.56 87.57 89 37.00* 6.753E+OO 2.042E-01 2.042E-01 57.56 BA-137M 661. 66 225 89.90* 1. 7 58E+OO 8.171E-01 8.331E-01 18.55 CS-137 661. 66 225 85.10* 1. 758E+OO 8.632E-01 8.801E-01 18.55 TL-208 277.37 ------6.60 3.709E+OO ------Line Not Found ------583.19 121 85.00* 1.952E+OO 4.201E-01 4.201E-01 33.77 860.56 ------12.50 1.416E+OO ------Line Not Found ------PB-210 46.54 54 4.25* 6.835E+OO l.060E+00 1.088E+OO 95.59 BI-211 72. 87 ------1. 23 6.824E+OO ------Line Not Found ------351.06 216 12.92* 3.012E+OO 3. 191E+OO 3. 191E+OO 24.76 PB-212 74.82 246 10.28 6.812E+OO 2.022E+OO 2.022E+00 26.51 77 .11 370 17.10 6.799E+OO 1.830E+OO 1.830E+OO 19.49 238.63 316 43.60* 4.209E+OO 9.906E-01 9.906E-01 17.39 300.09 ------3.30 3.465E+OO ------Line Not Found ------BI-214 609.32 106 45.49* 1.882E+OO 7 .116E-01 7 .119E-01 40.00 1120.29 25 14.92 l.136E+OO 8.399E-01 8.402E-01 61. 26 1764.49 24 15.30 7.483E-01 l.182E+OO 1.182E+00 57.30 PB-214 74.82 246 5.80 6.812E+OO 3.583E+OO 3.584E+00 26.51 77 .11 370 9.70 6.799E+OO 3.226E+OO 3.227E+OO 19.49 87.09 89 3.41 6.753E+OO 2.216E+OO 2.217E+OO 57.56 242.00 119 7.25 4.170E+OO 2.260E+OO 2.261E+OO 52.95 295.22 138 18.42 3.510E+OO l.225E+00 1.226E+00 38.30 351.93 216 35.60* 3.012E+OO l.158E+OO 1.159E+OO 24.76 RN-219 271.23 40 10.80 3.788E+OO 5.644E-01 5.644E-01 126.49 401.81 24 6.60* 2.683E+OO 7. 771E-01 7. 771E-01 108.62 RN-222 609.32 106 45.49* 1.882E+OO 7 .116E-01 7 .119E-01 40.00 1120. 29 25 14.92 l.136E+00 8.399E-01 8.402E-01 61. 26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 RA-224 240.99 119 4.10* 4.170E+OO 3.997E+OO 3.997E+OO 52.95 RA-226 609.32 106 45.49* 1.882E+00 7 .116E-01 7 .119E-01 40.00 1120.29 25 14.92 1.136E+OO 8.399E-01 8.402E-01 61. 26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+00 57.30 AC-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 56 11. 27 3 .118E+00 9.148E-01 9.148E-01 66.59 794.95 ------4.25 1.512E+OO ------Line Not Found ------835.71 ------1. 61 l.451E+00 ------Line Not Found ------911.20 62 25.80* 1. 351E+OO l.024E+OO 1.024E+OO 48.76 968. 97 24 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 RA-228 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 56 11. 27 3 .118E+OO 9.148E-01 9.148E-01 66.59 794.95 ------4.25 1.512E+OO ------Line Not Found ------835. 71 ------1. 61 1.451E+00 ------Line Not Found ------911. 20 62 25.80* 1.351E+OO 1.024E+OO 1.024E+OO 48.76 968. 97 24 15.80 1.283E+OO 6.878E-01 6.878E-01 74.10 Page 3960 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235045 Acquisition date 3-0CT-2016 06:57:26 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 .74.82 246 10.28 6.812E+OO 2. 022E+0..0 2.022E+OO 26.51 77 .11 370 17.10 6.799E+OO 1.830E+OO l.830E+OO 19.49 238.63 316 43.60* 4.209E+OO 9.906E-01 9.906E-01 17.39 300.09 ------3.30 3.465E+OO ------Line Not Found ------TH-230 609.32 106 45.49* 1.882E+OO 7 .116E-01 7 .116E-01 40.00 1120. 29 25 14.92 1.136E+OO 8.399E-01 8.399E-01 61.26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 TH-232 105.21 ------1.10 6.612E+OO ------Line Not Found ------338.32 56 11. 27 3.118E+OO 9.148E-01 9.148E-01 66.59 835. 71 ------1. 61 1. 451E+OO ------Line Not Found ------911.20 62 25.80* 1. 351E+OO 1.024E+OO 1.024E+OO 48.76 968. 97 24 15.80 l.283E+OO 6.878E-01 6.878E-01 74.10 TH-234 63.29 111 3.70* 6. 931E+OO 2.478E+OO 2.478E+OO 74.43 92.59 105 4.23 6.723E+OO 2.120E+OO 2.120E+OO 52.64 U-234 609.32 106 45.49* 1.882E+OO 7 .116E-01 7 .116E-01 40.00 1120.29 25 14.92 1.136E+OO 8.399E-01 8.399E-01 61.26 1764.49 24 15.30 7.483E-01 1.182E+OO 1.182E+OO 57.30 U-235 89.96 81 3.47 6.741E+OO 2.003E+OO 2.003E+OO 67.29 93.35 105 5:60 6. 723E+OO 1.602E+OO 1.602E+OO 52.64 143.76 ------10. 96* 5.959E+OO ------Line Not Found ------163.33 ------5.08 5.556E+OO ------Line Not Found ------185.72 64 57.20 5.108E+OO l.256E-01 l.256E-01 64.32 205.31 ------5.01 4.746E+OO ------Line Not Found ------U-238 63.29 111 3.70* 6. 931E+OO 2.478E+OO 2.478E+OO 74.43 92.59 105 4.23 6. 723E+OO 2.120E+OO 2.120E+OO 52.64 AM-243 43.53 ------5.90 6.236E+OO ------Line Not Found ------74.66 246 67.20* 6.812E+OO 3.093E_.:01 3.093E-01 26.51 CM-247 278.00 ------3.40 3.702E+OO ------Line Not Found ------287.50 ------2.00 3.596E+OO ------Line Not Found ------402.40 24 72. 00* 2.683E+OO 7.124E-02 7.124E-02 108.62 ANH-511 511. 00 28 100.00* 2.183E+OO 7.425E-02 7.425E-02 147.59 Flag: "*" Key line Page 3961 of 5809 Summary of Nuclide Activity Sample ID : G405235045 Acquisition date Page : 3 3-0CT-2016 06:57:26 Total number of lines in spectrum 41 Number of unidentified lines 7 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Hlife l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y l.41E+10Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 7.04E+08Y 1600.00Y 1. 41E+l0Y 1600. OOY 1. 41E+10Y 1.41E+l0Y l.41E+l0Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.56E+07Y 1.00E+09Y Decay 1. 00 1. 59 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.246E+Ol 2.042E+OO 2.042E-01 8.171E-01 8.632E-01 4.201E-01 1.060E+OO 3.191E+OO 9.906E-01 7 .116E-01 1.158E+OO 7. 771E-01 7 .116E-01 3.997E+OO 7 .116E-01 1.024E+OO l.024E+OO 9.906E-01 7 .116E-01 l.024E+OO 2.478E+OO 7 .116E-01 1.256E-01 2.478E+OO 3.093E-01 7.124E-02 7.425E-02 4 .114E+Ol 4 .114E+Ol Decay Corr pCi/GRAM 1.246E+Ol 3.242E+OO 2.042E-01 8.331E-01 8.801E-01 4.201E-01 1.088E+OO 3.191E+OO 9.906E-01 7 .119E-01 1.159E+OO 7. 771E-01 7 .119E-01 3.997E+OO 7 .119E-01 1.024E+OO 1.024E+OO 9.906E-01 7 .116E-01 1.024E+00 2.478E+OO 7 .116E-01 1.256E-01 2.478E+OO 3.093E-01 7.124E-02 7.425E-02 4.240E+Ol 4.240E+Ol 82.93% Decay Corr 2-Sigma Error 0.179E+Ol 1.866E+OO l.175E-01 1.546E-01 l.633E-01 l.419E-01 1.040E+OO 0.790E+OO 1. 723E-01 2.848E-01 0.287E+OO 8. 441E-01 2.848E-01 2 .116E+OO 2.848E-01 0.499E+OO 0.499E+OO l.723E-01 2.847E-01 0.499E+OO 1.844E+OO 2.847E-01 0.808E-01 1.844E+OO 0.820E-01 7.738E-02 10. 96E-02 Flags: "M" Manually accepted 2-Sigma %Error 14.40 57.56 57.56 18.55 18.55 33.77 95.59 24.76 17.39 40.00 24.76 108.62 40.00 52.95 40.00 48.76 48.76 17.39 40.00 48.76 74.43 40.00 64.32 74.43 26.51 108.62 147.59 "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3962 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235045 Acquisition date : 3-0CT-2016 06:57:26 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 98.29 37 147 0.63 196.43 193 8 9.03E-03 **** 6.68E+OO T 0 129.50 67 153 1. 58 258.85 253 13 1.65E-02 85.0 6.24E+OO T 1 188.58 39 62 1. 32 377.00 365 19 9.93E-03 86. 7 5.05E+OO o. 253.81 33 155 3.13 507.47 496 19 8.58E-03 **** 4.00E+OO T 0 328.16 30 51 0.91 656.17 652 9 7.87E-03 96. 9 3.20E+OO T 0 405.46 19 8 0.72 810.79 808 6 5. llE-03 66.4 2.66E+OO T 0 518.51 19 36 4.84 1036.89 1031 14 5.28E-03 **** 2.16E+OO 0 550.08 44 30 7.41 1100. 04 1090 23 1.19E-02 72 .2 2.05E+OO 0 62 6. 25 14 30 0.54 1252.38 1246 13 3.93E-03 **** 1.84E+OO 0 634.04 13 18 1. 26 1267. 96 1262 8 3.63E-03 **** 1. 82E+OO T 0 653.39 8 28 0.93 1306.68 1299 12 2.12E-03 **** 1.78E+OO 0 731.13 78 48 11. 48 1462.16 1446 40 2.16E-02 64.5 1.62E+OO 0 801.05 6 22 3.85 1602.02 1593 12 1.80E-03 **** 1.50E+OO T 0 949.47 12 7 2.86 1898.90 1893 10 3.49E-03 99.2 1.31E+OO T 1 965.08 24 21 2.03 1930 .11 1921 23 6.77E-03 75.2 1.29E+OO T 0 1219.97 9 7 1. 03 2439.98 2435 8 2.58E-03 **** 1. 06E+OO T 0 1351. 60 6 2 0.80 2703.30 2697 10 1.82E-03 **** 9.64E-01 Flags: "T" = Tentatively associated Page 3963 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:00:31.38 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l *
  • Acquisition date 3-0CT-2016 06:57:26 Sensitivity 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.96 Half life ratio : ***** *
  • Sample date 30-NOV-2015 14:15:00 Nuclide Library : SOLID *
  • Sample ID G405235045 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.3060E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 4.016E-01 9.544E-01 6.008E-02 3.932E-02 4.154E-02 3.823E-02 4.774E-01. 6.418E-02 8.649E-02 6.573E-02 4.024E-01 8.649E-02 6.886E-01 8.649E-02 1.651E-01 1. 651E-01 6.418E-02 8.646E-02 1. 651E-01 5.923E-01 8.646E-02 1.688E-01 5.923E-01 3.189E-02 3 .'694E-02 2.835E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 3964 of 5809 Le (pCi/GRAM 1.828E+Ol 5.784E-02 O.OOOE+OO O.OOOE+OO 5.007E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 3965 of 5809 O.OOOE+OO O.OOOE+OO 8.0lOE-02 6 .172E-01 O.OOOE+OO 4.478E-02 6.206E-01 8.768E+OO 5.086E-02 2. 007E-OJ. 2.659E+OO 2.646E+OO O.OOOE+OO 2.217E-01 O.OOOE+OO O.OOOE+OO 7.310E-01 9.005E+OO 1.033E+OO O.OOOE+OO l.597E-01 8.218E+02 3.778E-02 1.191E+OO 3.222E+OO 1.582E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.094E-02 8.143E-02 8.293E+OO 5.710E-01 5. 710E-01 3. 251E-02 1.216E-01 2.988E-01 O.OOOE+OO O.OOOE+OO 1.421E-01 2.937E+OO 1.12 6E-01 3.008E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 4.180E-02 O.OOOE+OO 8.080E-02 1. 620E-01 0.000E+OO O.OOOE+OO 1.150E-01 O.OOOE+OO O.OOOE+OO 2.743E+Ol O.OOOE+OO 3.308E-01 7.367E-02 6.419E+OO 5.651E-02 O.OOOE+OO 7.439E+02 O.OOOE+OO 2.998E-02 l.133E-01 1.749E-01 1.424E-01 1. 056E-01 2.434E+OO 6.366E-02 5.196E+OO 2.140E-01 1. 061E-01 SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 'BK-247 CF-249 CF-251 Page 3966 of 5809 2.793E-02 5.468E+OO 1.200E+OO 1.238E+OO 4.00lE+Ol 1.480E+02 5.550E-01 3.123E+OO 6. 061E-02 5.080E-01 6.800E-01 7.520E-01 6.649E-01 2.428E-01 2.428E-01 4. 967E-01 5. 811E-01 6.649E-01 6.028E-02 2. 971E-01 5.297E+OO 6.028E-02 O.OOOE+OO 2.389E-01 3.445E+02 5.694E-02 8.584E-02 7.793E-02 4.157E-02 l.243E-01 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN *FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:00:36.69 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235045.CNF;l * *Acquisition date 3-0CT-2016 06:57:26 Sensitivity : 3.000 *
  • Detector ID GAM39 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.96 Half life ratio : ***** *
  • Sample date 30-NOV-2015 14:15:00 Nuclide Library : SOLID *
  • Sample ID G405235045 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.3060E+02 GRAM *
  • Quantity Err ( % ) : 1. 5314E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 27-JUL-2016 13:04:01 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM39 CAN.CNF;4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1 . 96-sigma) K-40 1.246E+Ol 1.876E+OO CD-109 1.450E+OO 1.96SE+OO SN-126 9 .131E-02 l.237E-01 BA-137M 8.331E-01 1.557E-01 CS-137 8.801E-01 l.644E-01 TL-208 4.201E-01 l.402E-01 PB-210 1.088E+OO 1.023E+OO PB-212 9.906E-01 1.768E-01 BI-214 7. 119E-01 2.807E-01 PB-214 1.159E+OO 2.852E-01 RN-219 7. 771E-01 8.329E-01 RN-222 7 .119E-01 2.807E-01 RA-224 1.830E+OO 2.234E+OO RA-226 7 .119E-01 2.807E-01 AC-228 1.024E+OO 4.923E-01 RA-228 1.024E+OO 4.923E-01 TH-228 9.906E-01 1. 768E-01 TH-230 7 .116E-01 2.806E-01 TH-232 1.024E+OO 4.923E-01 TH-234 2.478E+OO l.889E+OO U-234 7 .116E-01 2.806E-01 U-235 -1.990E-01 1.999E-01 U-238 2.478E+OO l.889E+OO AM-243 2.035E-01 9.148E-02 CM-247 7 .124E'-02 7.677E-02 ANH-511 7.425E-02 1.074E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 I AL-26 Page 3967 of 5809 Key-Line Activity (pCi/GRAM 1. 7 51E+OO 4.445E-02 -1.000E+41 -8.668E-03 K.L Act error ( 1. 96-sigma) 2.149E+Ol 5.920E-02 1.500E+41 1. 700E-02 TPU ( 1. 96-sigma) 1. 876E+OO 1. 965E+OO l.237E-01 1.557E-01 1.644E-01 1.402E-01 1.023E+OO 1.768E-01 2.807E-01 2.852E-01 8.329E-01 2.807E-01 2.234E+OO 2.807E-01 4.923E-01 4.923E-01 1.768E-01 2.806E-01 4.923E-01 1.889E+OO 2.806E-01 1.999E-01 1.889E+OO 9.148E-02 7.677E-02 1.074E-01 TPU (1.96-sigma) 2.150E+Ol 6.250E-02 0.000E+OO 1. 744E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 -5.846E-02 5.860E-01 5.866E-01 FAIL ABUN V-48 2.548E+03 3 .139E+04 3.141E+04 SHORT HLIF CR-51 -2. 672E+02 6.614E+02 6.723E+02 SHORT HLIF MN-54 1.545E-02 8.955E-02 8.982E-02 NOT IDENT. C0-56 4.078E-01 6.429E-01 6.686E-01 NOT IDENT. MN-56 1.000E+41 1.576E+41 O.OOOE+OO SHORT HLIF C0-57 -3.654E-03 5.449E-02 5.451E-02 NOT IDENT. C0-58 -4.402E-01 7.887E-01 8.133E-01 NOT IDENT. FE-59 2.037E+OO 9.876E+OO 9.919E+00 NOT IDENT. C0-60 3.264E-02 5.327E-02 5.526E-02 NOT IDENT. ZN-65 l.253E-01 2.325E-01 2.392E-01 NOT IDENT. GE-68 6.924E-01 2.970E+OO 2.987E+OO NOT IDENT. AS-73 -4.170E-01 3.119E+OO 3.125E+OO NOT IDENT. AS-74 -4.862E+03 1. 086E+04 l.108E+04 SHORT HLIF SE-75 -2.095E-01 2.735E-01 2.894E-01 FAIL ABUN BR-77 1. 768E+39 l.570E+40 O.OOOE+OO SHORT HLIF SR-82 -2.467E+02 l.210E+03 l.215E+03 SHORT HLIF RB-83 -3.386E-01 1.048E+OO 1.059E+OO NOT IDENT. KR-85 l.421E+Ol 1.097E+Ol 1. 270E+Ol NOT IDENT. SR-85 l.628E+OO 1.259E+OO 1.457E+OO NOT IDENT. RB-86 5.743E+03 4.581E+04 4.589E+04 SHORT HLIF Y-88 -1.176E-01 2.609E-01 2.662E-01 NOT IDENT. Y-91 6.397E+02 8.698E+02 9.164E+02 NOT IDENT. NB-94 -l.941E-02 4.901E-02 4.979E-02 NOT IDENT. NB-95 7.626E-02 l.446E+00 1.446E+00 NOT IDENT. NB-95M 1.422E+OO 3.907E+OO 3.959E+OO NOT IDENT. ZR-95 -2.056E-01 1.979E+OO 1.982E+OO NOT IDENT. NB-97 -1.000E+41 3.808E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 2.985E+42 O.OOOE+OO SHORT HLIF M0-99 -8. 621E+32 l.816E+33 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 2.893E+41 0.000E+OO SHORT HLIF RH-101 -4.958E-03 4.142E-02 4.148E-02 NOT IDENT. RH-102 7.185E-02 l.174E-01 1.218E-01 NOT IDENT. RU-103 2.587E+OO 9.472E+OO 9.544E+OO FAIL ABUN RH-106 1.318E-01 7.419E-01 7.443E-01 NOT IDENT. RU-106 l.318E-01 7.419E-01 7.443E-01 NOT IDENT. AG-108M -6.352E-03 3.896E-02 3.907E-02 NOT IDENT. AG-llOM -5.919E-03 1.410E-01 1.411E-01 NOT IDENT. SN-113 6.530E-02 3.406E-01 3.419E-01 NOT IDENT. CD-115 -4.432E+40 5.090E+40 O.OOOE+OO SHORT HLIF SN-117M 6.192E+04 l.653E+05 1.676E+05 SHORT HLIF TE-123M 3.697E-02 1.543E-01 1.552E-01 NOT IDENT. SB-124 1.262E+OO 3.157E+OO 3.208E+OO NOT IDENT. SB-125 2.918E-02 1. 27 9E-01 1.286E-01 NOT IDENT. TE-125M 1.444E+02 3.488E+02 3.548E+02 NOT IDENT. I-126 -2.537E+04 2.273E+06 2.273E+06 SHORT HLIF SB-126 -6.603E+05 3.070E+06 3.085E+06 SHORT HLIF SB-127 -6. 841E+22 l.565E+23 O.OOOE+OO SHORT HLIF I-131 7.795E+09 1.435E+l0 1.478E+10 SHORT HLIF I-132 l.000E+41 2.206E+42 0.000E+OO SHORT HLIF TE-132 -2.439E+27 3.094E+27 O.OOOE+OO SHORT HLIF BA-133 1. 791E-03 5.375E-02 5.375E-02 NOT IDENT. I-133 1.000E+41 6.330E+41 O.OOOE+OO SHORT HLIF CS-134 8.342E-02 9.088E-02 9.835E-02 FAIL ABUN CS-135 1.249E-02 2.037E-01 2.038E-01 NOT IDENT. I-135 -1.000E+41 8.207E+41 O.OOOE+OO SHORT HLIF CS-136 -2.253E+05 6.221E+05 6.304E+05 SHORT HLIF CE-139 -5.362E-02 1.321E-01 1.343E-01 NOT IDENT. BA-140 -2.679E+06 3.039E+06 3.270E+06 SHORT HLIF LA-140 -1.973E+05 1.052E+06 1.056E+06 SHORT HLIF CE-141 -2.619E+Ol 3.202E+Ol 3.413E+Ol NOT IDENT. CE-143 1.000E+41 1.350E+41 O.OOOE+OO SHORT HLIF CE-144 -l.957E-01 4.221E-01 4.313E-01 NOT IDENT. PM-144 -2. 872E-03 8.994E-02 8.995E-02 NOT IDENT. PR-144 3.310E-01 7.749E+OO 7.750E+OO NOT IDENT. PM-146 9. 024E-0'3 6.539E-02 6.552E-02 FAIL ABU'N ND-147 6.312E+07 8.107E+07 8.592E+07 SHORT HLIF PM-147 -9. 931E+Ol 9.089E+02 9.100E+02 NOT IDENT. PM-149 -1.000E+41 2.673E+41 O.OOOE+OO SHORT HLIF EU-150 -1.350E-02 4.044E-02 4.090E-02 FAIL ABUN EU-152 7. 796E-02 l.225E-01 1. 274E-01 FAIL ABUN GD-153 2.676E-01 3.297E-01 3.511E-01 FAIL ABUN EU-154 l.120E-Ol l.454E-01 l.539E-01 NOT IDENT. EU-155 l .119E-01 1.170E-01 1. 274E-01 FAIL ABUN TB-160 3.131E-01 2.751E+OO 2.754E+OO FAIL ABUN H0-166M -5.493E-02 8.694E-02 9.039E-02 FAIL ABUN TM-171 -4.845E+OO 6.461E+OO 6.820E+OO NOT IDENT. HF-172 -9.526E-02 2.939E-01 2.970E-01 FAIL ABUN Page 3968 of 5809 LU-172 8.858E-02 1. 096E-01 1.166E-01 FAIL ABUN LU-176 -1.185E-03 3.308E-02 3.308E-02 FAIL ABUN HF-181 -2.819E+OO 6.868E+OO 6.985E+OO NOT IDENT. TA-182 l.167E+OO 1.414E+OO 1.509E+OO FAIL ABUN RE-183 -2.629E-01 1. 464E+OO 1.468E+OO NOT IDENT. RE-184 -1.577E+Ol 4.895E+Ol 4.947E+Ol NOT IDENT. W-188 -9.552E+Ol 2.004E+02 2.049E+02 FAIL ABUN IR-192 1.602E-01 6.201E-01 6.243E-01 FAIL ABUN HG-203 -6.154E-01 3.619E+OO 3.630E+OO NOT IDENT. BI-207 1.393E-02 6.(l 4 OE-02 6.869E-02 FAIL ABUN BI-211 3.191E+OO 7.874E-01 1. 640E+OO FAIL ABUN PB-211 1.095E+OO 7.144E-01 8.682E-01 FAIL ABUN BI-212 6.161E-01 8.269E-01 8. 723E-01 NOT IDENT. RA-223 1. 374E-01 8.338E-01 8.361E-Ol FAIL ABUN AC-227 -1. SllE-01 3.268E-01 3.338E-01 NOT IDENT. TH-227 -1. SllE-01 3.268E-01 3.338E-01 NOT IDENT. TH-229 l.256E-01 6.026E-01 6.053E-01 FAIL ABUN PA-231 7.262E-01 6.414E-01 7. 201E-01 NOT IDENT. TH-231 1. 374E-01 8.338E-01 8.361E-01 FAIL ABUN PA-233 -l.932E-02 7.147E-02 7.200E-02 NOT IDENT. PA-234 -3.674E-01 6.362E-01 6.574E-01 FAIL ABUN PA-234M -2.144E+OO 6.397E+OO 6.469E+OO NOT IDENT. NP-237 -1.932E-02 7.147E-02 7.200E-02 FAIL ABUN NP-238 1. 000E+41 5.675E+41 O.OOOE+OO SHORT HLIF NP-239 -5.772E-02 2.933E-01 2.945E-01 FAIL ABUN PU-239 9.757E+02 8.140E+02 9.252E+02 FAIL ABUN AM-241 3.412E-03 7.181E-02 7.183E-02 NOT IDENT. CM-243 -3.753E-02 1.064E-01 1.078'E-01 FAIL ABUN BK-247 -5.036E-02 9.406E-02 9.676E-02 NOT IDENT. CF-249 -7.312E-03 4. 931E-02 4.942E-02 FAIL ABUN CF-251 -6.946E-03 l.387E-01 1.387E-01 NOT IDENT. Page 3969 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 77.6683 87.09 114.7072 136.47 61.8774 45.60 86.8333 87.57 114.7827 140.51 0.0000 46.54 90.6860 88.03 114.8560 143.76 73.2930 49.72 0.0000 88.34 114. 9048 144.24 77.5426 51. 35 101.5943 88.47 114.9248 145.44 70.0414 51. 87 97.2249 89. 96 115.1586 152.43 80.7216 52.39 91.7273 1093.63 115.2645 153.25 0.0000 52.97 90.7076 91.11 0.0000 323.87 68.0924 53.44 85.1831 92.59 115. 5664 156.02 0.0000 54.07 78.5497 93.35 115.6826 158.56 0.0000 57.36 0.0000 94.56 95.5609 159.00 60.7087 57.53 100.5002 94.65 78.8468 162.33 63.4718 57.98 106.2309 94.67 78.8493 162.66 0.0000 59.27 111. 7584 94.87 78.8700 163.33 61.8135 59.32 111.7682 97.43 95.9186 165.86 68.8428 59.54 101.2344 98.43 88.8387 176.31 59.0690 60. 96 87.8517 98.44 88.8399 176.60 0.0000 61.17 104.5508 99.53 73.7355 177.52 67.8279 62.93 116.2628 100 .11 96.2476 181.07 0.0000 63.29 116.3336 102.03 57.8884 181. 52 64.1375 63.58 116.3903 103.18 78.5032 184.41 58. 6114 64.28 116.5266 103.37 '78.5220 143.76 58.6768 66.73 133.0559 105.21 62. 9604 193.51 56.8587 67.24 134. 6972 105.31 62. 9684 197.03 61.0025 125.81 119.4756 106.12 83.6368 198.01 60.1668 67.75 121.0210 106.47 83.6726 201.83 67.4540 69.67 129.0770 109.28 75.4405 203.43 78.2058 70.83 132.3917 111. 00 86.5686 205.31 69.4227 72. 81 107.7079 111.76 0.0000 210.85 62.5759 72.87 107.7179 114. 06 75.8683 215.65 48.4536 74.66 108.0137 116.30 0.0000 222 .11 60.4161 74.82 108.0400 116.74 82.2421 227.09 65.1680 74.97 108.0641 119.76 64.0498 227.38 68.8031 77 .11 108.4125 121.12 62.9146 228.16 0.0000 78.74 108.6750 121. 22 62.9216 228.18 76.0912 79.69 88.9332 121.78 65.4304 116.74 76.0912 80.12 88.9889 122.06 65.4510 235.69 68.3151 80.19 0.0000 122.92 69.2220 235. 96 65.5950 80.57 93.7341 123.07 64.2883 238.63 73.0249 81. 00 104.7352 265.00 61.8576 238.98 0.0000 81. 07 104.7454 125.81 72.7501 240.99 73.1486 81. 75 125.1921 127.23 66.2390 242.00 73.2015 83.79 98.8762 127.91 67.1169 244.70 39.8799 84.00 98.9053 129.30 67.2176 252.40 0.0000 85.43 117.9817 131. 20 67.3550 252.80 43.3343 86.55 114.6214 133.02 61.6539 254.15 0.0000 86.79 114. 6591 133.52 70.0222 256.23 54.0654 86.94 114. 6835 136.00 61.8473 260.90 0.0000 Page 3970 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 52.0522 355.39 0.0000 584.27 21. 8066 264.80 49.2691 356.01 27.9990 595.83 0.0000 265.00 52.9945 364.49 0.0000 427.87 34.0122 268.22 50. 3130 366.42 0.0000 602.52 0.0000 269.46 47.557.3 372. 51 32.7100 604. 72 28.0214 270 .p3 53.1719 375.05 607.14 34.6454 271.23 56.9492 377.52 35.7781 609.32 29.7202 273.65 0.0000 356.01 34.9003 610.33 29.7323 276.40 63.2318 388.16 32.9792 614.28 21.5051 277.37 54.8354 388.63 0.0000 618.01 23.1909 277.60 49.2188 391.69 34.0408 620.36 14.9216 278.00 48.3876 264.66 27.1560 621.93 16.5894 279.20 52.5547 401.81 27.1719 630.19 0.0000 279.54 54.4434 402.40 27.1802 631. 29 16.6461 279.70 54.4493 404.85 22.6781 633.25 9.9950 280.46 46.0232 410.95 31.3406 634.78 0.0000 283.69 41. 4129 413.71 38.4701 635.95 20.0090 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 50.8810 423. 72 0.0000 645.85 16.7340 285.90 0.0000 427.09 34.6461 657.76 23.5276 287.50 53.7796 427.87 22.4266 657.90 0.0000 290.67 63.8141 433.94 31.6931 661.66 20.1943 293.27 0.0000 439.40 27.6757 664.57 0.0000 351. 93 51.1974 453.88 31.9915 666.33 0.0000 295. 96 51.2216 463.37 25.9125 666.50 0.0000 879.38 54.1553 468.07 24.9292 667.71 0.0000 299.98 49.9226 473.00 0.0000 677.62 18.0508 300.09 49.9258 475.06 29.1758 685.70 0.0000 300.13 49.9269 476.78 20.8557 695.00 0.0000 301.36 37.6882 477.60 31.2952 696.49 26.1165 302.85 58.1084 482.18 29.2686 696. 51 24.9810 256.23 47.6776 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 26.1239 306.78 41.0596 497.08 25.2515 697.49 26.1249 308.46 33.4548 505.52 26.9277 702.65 27.3086 311. 90 36.3981 507.63 0.0000 706.68 12.5334 316.51 33.6171 511. 00 20.6398 711. 68 26.2503 319.41 0.0000 514.00 12.7178 720.70 0.0000 320.08 0.0000 514.00 12.7178 721.93 0.0000 321. 04 34.6707 520.40 23.9099 722.78 10.3099 323.87 36.1755 520.69 0.0000 722. 91 10.3103 325.23 34.7556 522.65 0.0000 723. 31 15.4677 328.76 0.0000 527.90 0.0000 724.19 22.3485 333.37 53.8356 528.26 24.5217 727.33 19.5034 333.97 49.4872 529.59 21. 3354 733.00 19.5393 334.37 39.3077 529.87 0.0000 735.93 19.5587 338.28 38.9095 531. 02 0.0000 333.97 19.5684 338.32 38.9103 537.26 0.0000 739.50 0.0000 311. 90 39.4445 546.56 0.0000 747.24 19.6300 340.48 39.4445 552.55 12.9214 748.06 13.8604 340.55 0.0000 563.25 24.8727 752.31 15.0360 344.28 31.2331 569.33 14.0923 753.82 0.0000 345.93 41.0319 946.00 14.0929 756.73 13.8989 351.06 26.4529 569.70 15.1781 756.80 13.8994 351.93 26.4655 583.19 21. 7977 884.68 27.8613 Page 3971 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 23.2316 1274.44 10.2363 1620.50 4.2529 766.42 16.2655 1001.03 16.7706 1621. 92 6.3809 766.84 17.4298 1002.74 8.3892 1678.03 0.0000 772. 60 0.0000 1004.73 16.7871 1690.97 3.2292 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739. 0.0000 1025.87 0.0000 1764.49 6.9754 778.90 12.8302 1028.54 0.0000 1063.66 5.4550 783.70 0.0000 1037.84 15.0479 1771.35 3.2736 785.37 12.2718 1038.76 0.0000 1791.20 0.0000 792. 07 20.2022 631.29 10.3682 1808.65 1.0979 794.95 15.4730 1048.07 0.0000 1810.72 0.0000 795.86 19.6984 1049.04 14.1476 1836.06 3.3083 810.06 14.1313 1050.41 12.2653 810.29 14.1323 1063.66 13.2523 344.28 14.1333 1077.00 0.0000 810.76 16.7850 1077.34 9.4977 815.77 0.0000 1085.87 12.3732 1048.07 0.0000 1093.63 9.5355 832.01 15 .1142 1099.45 10.5038 834.85 16.9068 1112. 07 13.4087 835.71 13.3507 1112. 84 9.5795 836.80 0.0000 1115.54 7.6685 846.75 0.0000 1120.29 14.3948 846.77 10.7153 1120.55 14.3958 856.80 0.0000 1221.41 18.4301 860.56 12.5516 1129. 67 11.5415 871.09 15.2880 1131.51 0.0000 873.19 15.2973 1147.95 0.0000 875.33 0.0000 1173.23 8.7446 879.38 14.4229 1177.95 17.5078 880.51 16.2307 1189.05 17.5518 883.24 14.4385 1204.77 10.7643 884.68 15.3476 1221.41 7.8579 889.28 17.1753 1231. 02 16.7333 894.76 17.2019 1235.36 0.0000 898,04 10.8743 1238.28 10.8449 900. 72 15.4171 1260.41 0.0000 903.28 17.2431 1271.87 10.9248 911. 20 18.1909 1274.44 5.9623 912.08 18.1952 1274.54 5. 9623 923.98 0.0000 1291.59 7.9785 926.50 18.2678 1298.22 0.0000 92 9 .11 19.1947 1312 .11 0.0000 937.49 25.6519 1332. 49 6.0359 944 .13 0.0000 1362.66 0.0000 946.00 22.0378 1365.19 7.0893 949.00 10.1091 1368.63 0.0000 667.71 0.0000 1384.29 8.1333 962.31 14.7563 1408.01 3.0646 964.08 14.7637 1457.56 0.0000 966.17 14.7720 1460.82 8.2573 911. 20 14.7827 1489.16 2.0756 968.97 14.7827 1505.03 6.2457 983.53 0.0000 1584.12 6.3376 984.45 0.0000 1596. 21 0.0000 Page 3972 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 OB:Ol:06.36 ********************************************************************************
  • GEI1 Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date : Z-OCT-2016 11:01:13. Sample date 7-DEC-2015 10:02:00. Acquisition date : 3-0CT-2016 06:57:53. Sample ID G405235046 Sample quantity l.5692BE+02 GRAM Detector name : GAM20 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:14.BB 0.4% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 B 9 10 11 12 13 14 15 16 17 lB 19 20 21 22 23 24 25 26 27 2B 29 30 31 32 33 34 6 6 0 0 0 2 2 0 0 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3973 of 5809 Energy 27.05* 2B.79* 32.30* 36.95* 63.44* 74.90 77.25 B7.3B 93.51* 99.39* 131.15 lB0.90 1B5.56* 20B.31 23B.5B* 241. 74 295.01* 300.35 32B.73 33B.4B* 351. B 9* 445 .11 510.66* 54B.49 5B3.27* 609.3B* 661.42* 727. 53 736.94 76B.7B 7B6.2B BB2.9B BB7.BO 911. 36* BACKGROUND CORRECTED SAMPLE PEAK*REPORT Area 50 29 16 32 47 l 7B 310 120 52 37 41 42 107 17 437 114 166 41 61 61 251 9 29 B 121 207 66 32 2B 30 29 10 16 112 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 13 45 90 150 194 197 160 133 2BO 114 194 99 126 113 62 74 90 B4 77 56 51 30 6B 17 4B 22 24 16 21 37 17 16 7 17 1. 29 1.13 1. 75 2.BO O.B5 1. 36 1.11 1. 05 1. 50 1. 9B 3.B9 1. 44 1. Bl 0.72 1.13 1. 54 1. 34 0.79 4.B7 1.13 1.17 O.BO 2.09 0.7B 1. 74 1. 60 1. 54 2.lB 4.54 1. 30 0.79 1. 01 1.20 1. 73 54.31 57.79 64.BO 74.10 127.03 149.93 154.64 174.B7 1B7.13 19B.B9 262.37 361. Bl 371.12 416.59 477.11 4B3.43 5B9.92 600.60 657.34 676.B5 703.64 B90.05 1021.16 1096.B2 1166. 3B 121B.60 1322. 72 1454.97 1473.BO 1537.51 1572.53 1766.01 1775.67 1B22.B2 51 51 63 72 124 145 145 172 lBl 195 254 357 366 414 471 471 5B2 596 650 671 69B BB4 1013 10B9 1160 1213 1315 1450 1466 1531 156B 1757 1770 1Bl6 12 l.3BE-02 24.7 2.07E+OO 12 7.95E-03 54.7 6 4.37E-03103.0 11 B.93E-03 77.4 B 1. 31E-02 54. 5 14 4.95E-02 15.B 2.15E+00 14 B.60E-02 9.1 6 3.32E-02 17.9 10 l.44E-02 65.1 B 1. 04E-02 53. 0 13 1. 14E-02 72. 5 9 1. lBE-02 45 .1 12 2.9BE-02 23.9 B 4.B4E-0310B.O 19 l.21E-01 5.7 l.05E+OO 19 3.16E-02 17.5 15 4.62E-02 14.7 13 1.15E-02 47.B 15 l.69E-02 34.3 9 1.69E-02 26.0 10 6.9BE-02 B.3 B 2.46E-03114.7 14 B.llE-03 70.9 9 2.llE-03106.5 16 3.37E-02 15.5 13 5.74E-02 B.6 14 1. B2E-02 20. 5 11 B.B7E-03 31.5 14 7.7BE-03 39.5 13 B.30E-03 46.6 11 7.92E-03 33.4 12 2.69E-03 92.3 10 4.32E-03 41.5 14 3.llE-02 12.5 Peak Search Report (continued) Page : 2 Sample ID : G405235046 Acquisition date 3-0CT-2016 06:57:53 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 964.70 13 25 2.59 1929.58 1923 12 3.63E-03 80.4 36 0 969. 38 63 5 1. 49 1938.94 1934 10 1.76E-02 14.2 .37 0 989.92 9 4 :i.. 42 1980.05 1977 6 2.43E-03 50.9 38 0 1010.46 18 12 1. 45 2021.17 2016 12 5.00E-03 45.1 39 0 1080.88 27 8 2.47 2162.12 2153 16 7.54E-03 30.2 40 2 1117.13 14 0 1. 60 2234.70 2233 26 3.77E-03 26. 5 5.65E-01 41 2 1120.44 58 6 2.22 2241.33 2233 26 1. 60E-02 17.2 42 0 1174.53 18 14 3.77 2349.61 2342 14 5.00E-03 50.0 43 0 1214.72 16 10 1. 04 2430.08 2423 11 4.32E-03 48.3 44 0 1238.62 36 13 1. 06 2477.94 2471 13 1. OlE-02 26.3 45 0 1263. 96 12 3 0.62 2528.68 2525 7 3.28E-03 39.0 46 0 1377.92 23 4 2.06 2756.91 2750 14 6.25E-03 27.5 47 0 1460.87* 383 4 1. 84 2923.06 2917 15 l.06E-01 5.3 48 0 1509.50 16 4 3.13 3020.48 3012 14 4.53E-03 34.8 49 0 1764.35 38 0 1. 91 3531.11 3525 12 1. 06E-02 16.2 Flag: "*" = Peak area was modified by background subtraction Page 3974 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:01:08 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample. date Sample ID 7-DEC-2015 10:02:00 G405235046 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 06:57:53 156.93 GRAM Sample type : Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA20 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 3975 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06
  • CAN 0 01:00:14.88 10.00 0.00 % Peak Energy 0.4%

Nuclide Line Activity Report Page : 2 Sample ID : G405235046 Acquisition date 3-0CT-2016 06:57:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 l.312E+OO 1.269E+Ol 1.269E+Ol 10.54 OK SC-46 889.28 99.98* 1. 963E+OO 3.897E-02 4.696E-01 83.02 OK 1120.55 99.99 1.635E+OO 1.683E-01 2.028E+OO 34.44 OK CD-109 88.03 3.70* 6.851E+OO 1.952E+OO 3.068E+OO 55.60 OK SN-126 64.28 9.60 4.805E+OO 6.542E-01 6.542E-01 108.99 OK 86.94 8.90 6. 851E+OO 8 .116E-01 8 .116E-01 55.60 OK 87.57 37.00* 6. 851E+OO l.952E-01 1.952E-01 55.60 OK BA-137M 661. 66 89.90* 2.465E+OO l.506E-01 l.535E-01 40.91 OK CS-137 661. 66 85.10* 2.465E+OO 1.591E-01 1. 621E-01 40.91 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.719E+OO 2.705E-01 2.705E-01 30.91 OK 860.56 12.50 2. OllE+OO Line Not Found Absent BI-212 727.33 6.67* 2.289E+00 1.051E+OO 1.051E+OO 62. 94 OK 785.37 1.10 2.156E+OO 5.987E+OO 5.987E+00 66.71 OK 1620.50 1. 47 l.197E+OO Line Not Found Absent PB-212 74.82 10.28 6.003E+OO 1. 220E+OO 1. 220E+OO 49.27 OK 77 .11 17.10 6.195E+OO 1.837E+OO 1.837E+OO 18.29 OK 238.63 43.60* 5.553E+00 1.020E+OO 1.020E+OO 11. 49 OK 300.09 3.30 4.643E+OO 1.487E+OO 1. 487E+OO 95.58 OK BI-214 609.32 45.49* 2.627E+00 8.865E-01 8.868E-01 17 .11 OK 1120.29 14.92 1.635E+OO 1.128E+OO l.128E+00 34.44 OK 1764.49 15.30 l.106E+OO 1. 017E+OO 1. 017E+OO 32.44 OK PB-214 74.82 5.80 5. 996E+OO Line Not Found <<INT Reject 77 .11 9.70 6.195E+OO 3.239E+00 3.240E+OO 18.29 OK 87.09 3.41 6.836E+00 Line Not Found <<INT Reject 242.00 7.25 5.495E+OO Line Not Found <<INT Reject 295.22 18.42 4.711E+OO 1.061E+OO 1.062E+OO 29.44 OK 351.93 35.60* 4.084E+OO 9.393E-01 9. 396E-01 16.64 OK RN-222 609.32 45.49* 2.627E+00 8.865E-01 8.868E-01 17 .11 OK 1120.29 14.92 1. 635E+OO l.128E+00 1.128E+OO 34.44 OK 1764.49 15.30 l.106E+OO 1.017E+OO 1. 017E+OO 32.44 OK RA-224 240.99 4.10* 5.499E+OO 9.734E-01 9.734E-01 117.17 OK RA-226 609.32 45.49* 2.627E+OO 8.865E-01 8.868E-01 17 .11 OK 1120.29 14.92 1.635E+OO 1.128E+OO 1.128E+00 34.44 OK 1764.49 15.30 l.106E+OO l.017E+00 1. 017E+OO 32.44 OK AC-228 105.21 1.10 7.453E+00 Line Not Found Absent 338.32 11.27 4.215E+OO 6.986E-01 6.986E-01 51. 98 OK 794.95 4.25 2.138E+OO Line Not Found Absent 835.71 1. 61 2.057E+OO Line Not Found Absent 911.20 25.80* 1.923E+OO 1.105E+OO 1.105E+00 24.93 OK 968. 97 15.80 1.833E+OO 1.062E+OO 1.062E+OO 28.37 OK RA-228 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11. 27 4.215E+00 6.986E-01 6.986E-01 51. 98 OK 794.95 4.25 2 .138E+OO Line Not Found Absent 835.71 1. 61 2.057E+OO Line Not Found Absent 911.20 25.80* 1.923E+OO 1.105E+OO 1.105E+OO 24.93 OK 968. 97 15.80 l.833E+OO 1.062E+OO 1.062E+OO 28.37 OK TH-228 74.82 10.28 6.003E+OO 1.220E+OO 1.220E+OO 49.27 OK 77 .11 17.10 6.195E+OO 1.837E+OO 1.837E+OO 18.29 OK Page 3976 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235046 Acquisition date 3-0CT-2016 06:57:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status ' 238.63 43.60* 5.553E+OO 1. 020.E+OO 1.020E+OO 11. 49 OK 300.09 3.30 4.643E+OO 1.487E+OO l.487E+OO 95.58 OK TH-230 609.32 45.49* 2.627E+OO 8.865E-01 8.865E-01 17 .11 OK 1120.29 14.92 l.635E+OO l.128E+OO 1.128E+OO 34.44 OK 1764.49 15.30 1.106E+OO 1.017E+OO 1.017E+OO* 32.44 OK PA-231 283.69 1. 70 4.860E+OO Line Not Found Absent 301.36 5.35* 4.643E+OO 9.175E-01 9.175E-01 95.58 OK TH-232 105.21 1.10 7.453E+OO Line Not Found Absent 338.32 11.27 4.215E+OO 6.986E-01 6.986E-01 51. 98 OK 835.71 1. 61 2.057E+OO Line Not Found Absent 911.20 25.80* 1.923E+OO 1.105E+OO 1.105E+OO 24.93 OK 968. 97 15.80 1.833E+OO 1.062E+OO 1.062E+OO 28.37 OK TH-234 63.29 3.70* 4.805E+OO 1.697E+OO 1.697E+OO 108.99 OK 92.59 4.23 7.128E+OO 1.062E+OO 1.062E+OO 130 .16 OK U-234 609.32 45.49* 2.627E+OO 8.865E-01 8.865E-01 17 .11 OK 1120.29 14.92 1.635E+OO 1.128E+OO l.128E+OO 34.44 OK 1764.49 15.30 1.106E+OO 1.017E+OO 1. 017E+OO 32.44 OK U-238 63.29 3.70* 4.805E+OO 1.697E+OO 1.697E+OO 108.99 OK 92.59 4.23 7.128E+OO 1.062E+OO 1.062E+OO 130.16 OK AM-243 43.53 5.90 1.315E+OO Line Not Found Absent 74.66 67.20* 6.003E+OO 1. 866E-01 l.866E-01 49.27 OK ANH-511 511. 00 100.00* 3.021E+OO 5.052E-02 5.052E-02 141.86 OK Flag: "*" = Keyline Page 3977 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:01:09.75 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l * *Acquisition date 3-0CT-2016 06:57:53 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.88 Half life ratio : ***** *
  • Sample date 7-DEC-2015 10:02:00 Analyst initials: MXRl *
  • Sample ID G405235046 Sample Quantity l.5693E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.269E+Ol 1. 311E+OO SC-46 4.696E-01 3.821E-01 CD-109 3.068E+OO l.672E+OO SN-126 l.952E-01 l.064E-01 BA-137M l.535E-01 6.152E-02 CS-137 l.621E-01 6.499E-02 TL-208 2.705E-01 8.194E-02 BI-212 l.051E+OO 6.481E-01 PB-212 1. 020E+00 l.149E-01 BI-214 8.868E-01 l.487E-01 PB-214 9.396E-01 l.532E-01 RN-222 8.868E-01 l.487E-01 RA-224 9.734E-01 l.118E+OO RA-226 8.868E-01 l.487E-01 AC-228 l.105E+OO 2. 701E-01 RA-228 l.105E+OO 2. 701E-01 TH-228 1. 020E+OO l.149E-01 TH-230 8.865E-01 1. 486E-01 PA-231 9.175E-01 8.594E-01 TH-232 l.105E+OO 2. 701E-01 TH-234 l.697E+OO l.813E+OO U-234 8.865E-01 1. 486E-01 U-238 l.697E+OO l.813E+OO AM-243 1. 866E-01 9.009E-02 ANH-511 5*. 052E-02 7.024E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 Page 3978 of 5809 Key-Line Activity (pCi/GRAM -5 .115E+OO -l.917E-02 O.OOOE+OO l.086E-02 O.OOOE+OO K.L. Cnt Uncert (1.96-sigma) l.107E+Ol 4.237E-02 1. 960E+41 2.590E-02 l.139E+04 MDA (pCi/GRAM 5.147E-01 6.020E-01 l.930E+OO l.232E-01 5.128E-02 5.417E-02 5.019E-02 6.314E-01 7.929E-02 8.519E-02 l.067E-01 8.519E-02 8.498E-01 8.519E-02 l.828E-01 l.828E-01 7.929E-02 8.516E-02 6.520E-01 l.828E-01 l.671E+00 8.516E-02 l.671E+OO 7.188E-02 4.670E-02 MDA (pCi/GRAM 2.023E+Ol 7.807E-02 O.OOOE+OO 6.097E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF CR-51 O.OOOE+OO 3.656E+02 O.OOOE+OO SHORT HLIF MN-54 -4.845E-02 5.460E-02 8.750E-02 NOT IDENT. C0-56 l.518E-01 4.115E-01 8.268E-01 FAIL ABUN MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 -3.777E-02 3.927E-02 6.622E-02 NOT IDENT. C0-58 5.550E-03 4.930E-01 9.453E-01 NOT IDENT. FE-59 -1.985E+OO 5.718E+OO 1.090E+Ol NOT IDENT. C0-60 1.430E-02 3.034E-02 6.764E-02 FAIL ABUN ZN-65 3. 964E-02 1.497E-01 2.823E-01 NOT IDENT. GE-68 -l.014E+OO 1. 792E+OO 2.779E+OO NOT IDENT-1 AS-73 1.646E+OO 4.739E+OO 9.386E+OO NOT IDENT. AS-74 O.OOOE+OO 4.220E+03 O.OOOE+OO SHORT HLIF SE-75 3.793E-03 1. 565E-01 3 .119E-01 NOT IDENT. BR-77 O.OOOE+OO 2.802E+37 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 6.008E+02 0.000E+OO SHORT HLIF RB-83 3.339E-02 5.459E-01 1.068E+OO NOT IDENT. KR-85 5.665E-01 7.039E+OO l.215E+Ol NOT IDENT. SR-85 5.953E-02 7.518E-01 1.298E+OO NOT IDENT. RB-86 O.OOOE+OO 2.212E+04 O.OOOE+OO SHORT HLIF Y-88 1. 568E-02 l.020E-01 2.722E-01 NOT IDENT. Y-91 -2.924E+02 5.226E+02 9.439E+02 NOT IDENT. NB-94 2. 041E-02 2. 513E-02 5.369E-02 NOT IDENT. NB-95 3.249E-02 9.390E-01 1.569E+OO NOT IDENT. NB-95M -6.130E-01 2.090E+OO 3.604E+OO NOT IDENT. ZR-95 1. 472E-01 1.330E+00 2.561E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.267E+41 0.000E+OO SHORT HLIF M0-9-9 O.OOOE+OO 2.104E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 9.llBE-03 3. 061E-02 5.340E-02 NOT IDENT. RH-102 1.775E-02 4.669E-02 9.560E-02 NOT IDENT. RU-103 1. 059E+OO 4.673E+OO 9.369E+OO FAIL ABUN RH-106 -l.928E-01 4.256E-01 7.655E-01 NOT IDENT. RU-106 -l.928E-01 4.256E-01 7.655E-01 NOT IDENT. AG-108M 8.832E-03 2 .139E-02 4.404E-02 NOT IDENT. AG-llOM 2.149E-03 8. 411E-02 1.197E-01 NOT IDENT. SN-113 -9 .181E-02 l.833E-01 3.389E-01 NOT IDENT. CD-115 O.OOOE+OO 3.586E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 9.641E+04 0.000E+OO SHORT HLIF TE-123M 3.681E-02 l.211E-01 2.248E-01 NOT IDENT. SB-124 -3.225E-01 1. 841E+OO 3.677E+OO NOT IDENT. SB-125 -5.840E-03 8.387E-02 l.625E-01 NOT IDENT. TE-125M l.597E+02 2.287E+02 4.481E+02 NOT IDENT. I-126 O.OOOE+OO 8.697E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.073E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.244E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4. 461E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 712E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 3.775E+26 0.000E+OO SHORT HLIF BA-133 2.859E-03 3.448E-02 6.442E-02 NOT IDENT. I-133 O.OOOE+OO l.850E+41 O.OOOE+OO SHORT HLIF CS-134 2.659E-02 4. 811E-02 9.665E-02 NOT IDENT. CS-135 -7.178E-02 l.210E-01 2.261E-01 NOT IDENT. I-135 O.OOOE+OO 1.632E+41 O.OOOE+OO SHORT HLIF CS-136 0.000E+OO 2. 761E+05 O.OOOE+OO SHORT HLIF CE-139 -5.926E-02 1.0lOE-01 1.731E-01 NOT IDENT. BA-140 O.OOOE+OO 8.619E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.160E+05 O.OOOE+OO SHORT HLIF CE-141 3.271E+OO 2.081E+Ol 3.867E+Ol NOT IDENT. CE-143 O.OOOE+OO 7.946E+40 O.OOOE+OO SHORT HLIF CE-144 -1.112E-01 3.246E-01 5.279E-01 NOT IDENT. PM-144 -6.332E-03 4.154E-02 7.840E-02 NOT IDENT. PR-144 -5.377E-01 3.612E+OO 6.822E+OO NOT IDENT. PM-146 8.016E-03 2.997E-02 6.164E-02 FAIL ABUN ND-147 O.OOOE+OO 2.688E+07 O.OOOE+OO SHORT HLIF PM-147 -2.573E+Ol 6.262E+02 l.160E+03 NOT IDENT. PM-149 0.000E+OO 4.503E+40 O.OOOE+OO SHORT HLIF EU-150 2.957E-02 2.439E-02 4.329E-02 FAIL ABUN EU-152 -2.624E-02 7.325E-02. 1.387E-01 FAIL ABUN GD-153 -6. 2.98E-02 1.605E-01 2.662E-01 .NOT IDENT. EU-154 -6.036E-02 1.047E-01 1.886E-01 NOT IDENT. EU-155 3.293E-02 9.435E-02 1. 793E-01 FAIL ABUN TB-160 l.519E-01 1.752E+OO 3.037E+OO FAIL ABUN H0-166M 2.843E-02 4.399E-02 9.315E-02 FAIL ABUN TM-171 -3.299E+OO 1.153E+Ol 2.173E+Ol NOT IDENT. HF-172 -l.727E-01 2.236E-01 3.476E-01 FAIL ABUN LU-172 -3. 901E-04 7.317E-02 1. 44 7E-01 FAIL ABUN LU-176 4.360E-03 l.993E-02 3.845E-02 FAIL ABUN Page 3979 of 5809 HF-181 -l.825E+OO 3.746E+OO 6.828E+OO NOT IDENT. TA-182 -7.189E-02 7.464E-01 1. 466E+OO FAIL ABUN RE-183 8.555E-02 l.801E+00 3.461E+OO NOT IDENT. RE-184 1.310E+Ol 2. 741E+Ol 5.575E+Ol NOT IDENT. W-188 -3.759E+Ol 9.494E+Ol l.602E+02 FAIL ABUN IR-192 1.964E-01 3. 964E-01 8.104E-01 FAIL ABUN HG-203 2.030E-01 2.051E+OO 4.059E+OO NOT IDENT. BI-207 1.858E-02 3.790E-02 8.239E-02 FAIL ABUN PB-210 1. 886E+OO l.478E+OO 3.170E+OO NOT IDENT. BI-211 O.OOOE+OO 4.220E-01 7.389E-01 FAIL ABUN PB-211 2.369E-01 5.108E-01 l.054E+OO NOT IDENT. RN-219 -9.674E-03 3.102E-01 6.031E-01 NOT IDENT. RA-223 2.368E-01 4.959E-01 9.336E-01 FAIL ABUN AC-227 1. 446E-01 2.003E-01 4.146E-01 FAIL ABUN TH-227 l.446E-01 2.003E-01 4.146E-01 FAIL ABUN TH-229 2.438E-02 3.644E-01 7.304E-01 FAIL ABUN TH-231 2.368E-01 4.959E-01 9.336E-01 FAIL ABUN PA-233 -6.129E-04 4.304E-02 8.536E-02 FAIL ABUN PA-234 6. lllE-02 2.261E-01 4.758E-01 FAIL ABUN PA-234M -3.214E-01 3.541E+OO 7.209E+00 NOT IDENT. U-235 -2.878E-02 l.651E-01 2.979E-01 FAIL ABUN NP-237 -6.129E-04 4.304E-02 8.536E-02 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 1. 38 6E-01 2.049E-01 3.993E-01 FAIL ABUN PU-239 l.953E+02 2.743E+02 5.298E+02 NOT IDENT. AM-241 -6. 961E-02 8.839E-02 l.588E-01 NOT IDENT. CM-243 -3.105E-02 8.490E-02 l.530E-01 FAIL ABUN BK-'247 2.122E-02 5.382E-02 l'.108E-01 NOT IDENT. CM-247 -7.907E-03 2.716E-02 5.145E-02 NOT IDENT. CF-249 -3.610E-03 2.972E-02 5.744E-02 NOT IDENT. CF-251 -2.636E-02 9.359E-02 1. 651E-01 NOT IDENT. Page 3980 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:01:07.19 Nuclide Line Activity Report Nuclide Type: .. Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 371 10.66* l.312E+OO 1. 2 69E+Ol 1.269E+Ol 10.54 SC-46 889.28 16 99.98* 1. 963E+OO 3.897E-02 4. 696E-01 83.02 1120. 55 58 99.99 1.635E+OO 1.683E-01 2.028E+OO 34.44 CD-109 88.03 155 3.70* 6. 851E+OO 2.930E+OO 4.605E+OO 35.71 SN-126 64.28 63 9.60 4.805E+OO 6.542E-01 6.542E-01 108.99 86.94 155 8.90 6.851E+OO 1.218E+OO 1.218E+OO 35. 71 87.57 155 37.00* 6.851E+OO 2.930E-01 2.930E-01 35.71 BA-137M 661. 66 70 89.90* 2.465E+OO l.506E-01 1.535E-01 40.91 CS-137 661. 66 70 85.10* 2.465E+OO l.591E-01 1. 621E-01 40.91 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 131 85.00* 2. 719E+OO 2.705E-01 2.705E-01 30.91 860.56 ------12.50 2. OllE+OO ------Line Not Found ------BI-211 72.87 ------1. 23 5.823E+OO ------Line Not Found ------351.06 285 12.92* 4.084E+OO 2.588E+OO 2.588E+OO 16.64 BI-212 727. 33 34 6.67* 2.289E+OO 1. 051E+OO 1. 051E+OO 62.94 785.37 30 1.10 2.156E+OO 5.987E+OO 5.987E+OO 66.71 1620.50 ------1. 47 1.197E+OO ------Line Not Found ------PB-212 74.82 235 10.28 6.003E+OO 1.818E+OO 1.818E+OO 31.. 59 77 .11 407 17.10 6.195E+OO l.837E+OO l.837E+OO 18.29 238.63 516 43.60* 5.553E+OO 1.020E+OO 1. 020E+OO 11. 49 300.09 48 3.30 4.643E+OO 1.487E+OO 1.487E+OO 95.58 BI-214 609.32 221 45.49* 2.627E+OO 8.865E-01 8.868E-01 17.11 1120.29 58 14.92 1.635E+OO 1.128E+OO 1.128E+OO 34.44 1764.49 36 15.30 1.106E+OO 1.017E+OO 1.017E+OO 32.44 PB-214 74.82 235 5.80 6.003E+OO 3.223E+OO 3.224E+OO 31. 59 77 .11 407 9.70 6.195E+OO 3.239E+OO 3.240E+OO 18.29 87.09 155 3.41 6. 851E+OO 3.180E+OO 3.181E+OO 35.71 242.00 134 7.25 5.499E+OO 1.612E+OO 1.612E+OO 35.01 295.22 192 18.42 4.711E+OO 1. 061E+OO 1. 062E+OO 29.44 351. 93 285 35.60* 4.084E+OO 9.393E-01 9.396E-01 16.64 RN-222 609.32 221 45.49* 2.627E+OO 8.865E-01 8.868E-01 17 .11 1120.29 58 14.92 1.635E+OO 1.128E+OO l.128E+OO 34.44 1764.49 36 15.30 1.106E+OO 1.017E+OO 1.017E+OO 32.44 RA-224 240.99 134 4.10* 5.499E+OO 2.850E+OO 2.850E+OO 35.01 RA-226 609.32 221 45.49* 2.627E+OO 8.865E-01 8.868E-01 17 .11 1120.29 58 14.92 1.635E+OO l.128E+OO 1.128E+OO 34.44 1764.49 36 15.30 1.106E+OO 1.017E+OO l.017E+00 32.44 AC-228 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 69 11. 27 4.215E+OO 6.986E-01 6.986E-01 51. 98 794.95 ------4.25 2.138E+OO ------Line Not Found ------835.71 ------1. 61 2.057E+OO ------Line Not Found ------911.20 115 25.80* 1.923E+OO 1.105E+OO 1.105E+OO 24.93 968.97 64 15.80 1.833E+OO l.062E+OO 1.062E+OO 28.37 RA-228 105.21 ------1.10 7.453E+OO ------Line Not Found ------338.32 69 11. 27 4.215E+00 6.986E-01 6.986E-01 51. 98 794.95 ------4.25 2 .138E+OO ------Line Not Found ------835.71 ------1. 61 2.057E+OO ------Line Not Found ------Page 3981of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235046 Acquisition date 3-0CT-2016 06:57:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error .911.20 115 25.80* 1. 923E+OO l.105E+.00 1.105E+OO 24.93 968. 97 64 15.80 1.833E+OO 1.062E+OO 1.062E+OO 28.37 TH-228 74.82 235 10.28 6.003E+OO 1.818E+OO 1.818E+OO 31. 59 77 .11 407 17.10 6.195E+OO 1.837E+OO 1.837E+OO 18.29 238.63 516 43.60* 5.553E+OO 1.020E+OO l.020E+OO 11. 49 300.09 48 3.30 4.643E+OO 1.487E+OO 1.487E+OO 95.58 TH-230 609.32 221 45.49* 2.627E+OO 8.865E-01 8.865E-01 17 .11 1120.29 58 14.92 1.635E+OO l.128E+OO 1.128E+OO 34.44 1764.49 36 15.30 1.106E+OO 1.017E+OO 1.017E+OO 32.44 PA-231 283.69 ------1. 70 4.860E+OO ------Line Not Found ------301.36 48 5.35* 4.643E+OO 9.175E-01 9.175E-01 95.58 TH-232 105.21 ------1.10 7.453E+00 ------Line Not Found ------338.32 69 11. 27 4.215E+OO 6.986E-01 6.986E-01 51. 98 835. 71 ------1. 61 2.057E+OO ------Line Not Found ------911. 20 115 25.80* 1.923E+OO l.105E+OO 1.105E+OO 24.93 968. 97 64 15.80 1.833E+OO 1. 062E+00 1. 062E+00 28.37 TH-234 63.29 63 3.70* 4.805E+OO 1.697E+OO 1.697E+OO 108.99 92.59 67 4.23 7.128E+00 1.062E+OO 1.062E+OO 130.16 U-234 609.32 221 45.49* 2.627E+OO 8.865E-01 8.865E-01 1'7.11 1120.29 58 14.92 1.635E+OO l.128E+OO 1.128E+OO 34.44 1764.49 36 15.30 l.106E+OO 1.017E+OO 1.017E+OO 32.44 U-238 63.29 63 3.70* 4.805E+OO 1.697E+OO 1.697E+OO 108.99 92.59 67 4.23 7.128E+OO 1.062E+OO 1.062E+00 130 .16 AM-243 43.53 ------5.90 1.315E+OO ------Line Not Found ------74.66 235 67.20* 6.003E+OO 2.782E-01 2.782E-01 31. 59 ANH-511 511. 00 32 100.00* 3. 021E+OO 5.052E-02 5.052E-02 141.86 Flag: "*" Key line Page 3982 of 5809 Summary of Nuclide Activity Sample ID : G405235046 Acquisition date Page : 3 3-0CT-2016 06:57:53 Total number of lines in spectrum 49 Number of unidentified lines 16 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 83.79D 461. 40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 7.04E+08Y l.41E+10Y l.41E+l0Y 1600. DOY 1600. O'OY 1600.00Y 1. 41E+10Y 1600. ODY l.41E+l0Y 1. 41E+l0Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 12.1 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity .. Uncorrected pCi/GRAM 1. 269E+Ol 3.897E-02 2.930E+OO 2.930E-01 1. 506E-01 1.591E-01 2.705E-01 2.588E+OO 1. 051E+OO 1.020E+OO 8.865E-01 9.393E-01 8.865E-01 2.850E+OO 8.865E-01 1.105E+OO 1.105E+OO 1. 020E+OO 8.865E-01 9.175E-01 1.105E+OO 1.697E+OO 8.865E-01 1.697E+OO 2.782E-01 5.052E-02 3.839E+Ol 3.839E+Ol Decay Corr pCi/GRAM 1.269E+Ol 4. 696E-01 4.605E+OO 2.930E-01 1.535E-01 1. 621E-01 2.705E-01 2.588E+OO 1.051E+OO 1.020E+OO 8.868E-01 9.396E-01 8.868E-01 2.850E+OO 8.868E-01 1.105E+OO 1.105E+OO 1.020E+OO 8.865E-01 9.175E-01 1.105E+OO 1.697E+OO 8.865E-01 1.697E+OO 2.782E-01 5.052E-02 4.050E+Ol 4.050E+Ol 67.35% Decay Corr 2-Sigma Error 0.134E+Ol 3.899E-01 1.645E+OO 1.047E-01 0.628E-01 0.663E-01 0.836E-01 0.431E+OO 0.661E+OO 0 .117E+OO 1.517E-01 l.563E-01 l.517E-01 0.998E+OO l.517E-01 0.276E+OO 0.276E+OO 0 .117E+OO l.516E-01 8.769E-01 0.276E+OO 1.850E+OO l.516E-01 1.850E+OO 0.879E-01 7.167E-02 "M" Manually accepted 2-Sigma %Error 10.54 83.02 35. 71 35. 71 40.91 40.91 30.91 16.64 62.94 11. 49 17 .11 16.64 17 .11 35.01 17 .11 24.93 24.93 11. 49 17 .11 95.58 24.93 108.99 17 .11 108.99 31. 59 f41. 8 6 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 3983 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235046 Acquisition date : 3-0CT-2016 06:57:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 6 27.05 71 19 1. 29 54.31 51 12 1.38E-02 49.4 4.65E-07 6 28.79 41 65 1.13 57.79 51 12 7.95E-03 **** 4.59E-05 0 32.30 22 128 1. 75 64.80 63 6 4.37E-03 **** 9.28E-03 . 0 36.95 45 210 2.80 72 11 8.93E-03 **** 2.24E-01 0 99.39 48 146 1. 98 198.89 195 8 1.04E-02 **** 7.32E+OO T 0 131.15 51 243 3.89 2 62. 37 254 13 1.14E-02 **** 7.52E+OO T 0 180.90 51 120 1. 44 361. 81 357 9 1.18E-02 90.2 6.67E+OO T 0 185.56 130 153 1. 81 371.12 366 12 2.98E-02 47.9 6.57E+OO T 0 208.31 21 135 0. 72 416.59 414 8 4.84E-03 **** 6. llE+OO 0 328.73 69 88 4.87 657.34 650 15 1.69E-02 68.5 4.32E+OO T 0 445 .11 10 33 0.80 890.05 884 8 2.46E-03 **** 3.37E+OO 0 548.49 8 19 0.78 1096. 82 1089 9 2. llE-03 **** 2.85E+00 0 736.94 29 22 4.54 1473.80 1466 14 7.78E-03 79.1 2.27E+OO T 0 768.78 31 39 1. 30 1537.51 1531 13 8.30E-03 93.1 2.19E+OO 0 882.98 10 17 1. 01 1766.01 1757 12 2.69E-03 **** 1. 97E+OO T 0 964.70 13 25 2.59 1929.58 1923 12 3.63E-03 **** 1.84E+OO T 0 989.92 9 4 1. 42 1980.05 1977 6 2.43E-03 **** 1. 80E+00 0 1010.46 18 12 1. 45 2021.17 2016 12 5.00E-03 90.3 l.77E+00 0 1080.88 27 8 2.47 2162.12 2153 16 7.54E-03 60.3 1. 68E+OO 2 1117.13 14 0 1. 60 2234.70 2233 26 3.77E-03 53.1 1. 64E+OO 0 1174.53 18 14 3.77 2349.61 2342 14 5.00E-03 **** 1.57E+OO T 0 1214.72 15 10 1. 04 2430.08 2423 11 4.32E-03 96.5 l.53E+OO 0 1238.62 36 13 1. 06 2477.94 2471 13 1. OlE-02 52.6 1.51E+OO T 0 1263. 96 12 3 0.62 2528.68 2525 7 3.28E-03 77.9 1. 48E+OO 0 1377.92 22 3 2.06 2756.91 2750 14 6.25E-03 55.0 1.38E+OO 0 1509.50 16 4 3 .13 3020.48 3012 14 4.53E-03 69.7 l.28E+00 Flags: "T" = Tentatively associated Page 3984 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:01:25.66 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l *
  • Acquisition date 3-0CT-2016 06:57:53 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.88 Half life ratio : ***** *
  • Sample date 7-DEC-2015 10:02:00 Nuclide Library : SOLID *
  • Sample ID G405235046 Analyst initials: MXRl *
  • Batch Number 1.596252 Sample Quantity : 1.5693E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 TL-208 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 *U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.107E-01 2.604E-01 9.221E-01 5.887E-02 2.257E-02 2.385E-02 2.220E-02 2. 722E-01 3.683E-02 3.700E-02 4.870E-02 3.700E-02 3.947E-01 3.700E-02 7.807E-02 7.807E-02 3.683E-02 3.699E-02 2.986E-01 7.807E-02 7.959E-01 3.699E-02 7.959E-01 3.420E-02 2 .113E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 Page 3985 of 5809 Le (pCi/GRAM 9.099E+OO 3.350E-02 O.OOOE+OO 2.447E-02 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 3986 of 5809 3.747E-02 3.650E-01 O.OOOE+OO 3. 081E-02 4.126E-01 4.690E+OO 2.869E-02 1. 226E-01 1.128E+OO O.OOOE+OO 1.431E-01 O.OOOE+OO O.OOOE+OO 4.779E-01 5.535E+OO 5. 911E-01 O.OOOE+OO 9.266E-02 4.143E+02 2.401E-02 7.061E-01 1.674E+OO 1.138E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.510E-02 4.237E-02 4.200E+OO 3. 372E-01 3. 372E-01 1. 986E-02 4.917E-02 1.524E-01 O.OOOE+OO 0.000E+OO 1. 058E-01 1.459E+OO 7.327E-02 2 .111E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 2.937E-02 O.OOOE+OO 4.355E-02 1. 047E-01 O.OOOE+OO O.OOOE+OO 8.093E-02 O.OOOE+OO O.OOOE+OO l.815E+01 O.OOOE+OO 2.467E-01 3.419E-02 2.975E+00 2.736E-02 O.OOOE+OO 5.399E+02 O.OOOE+OO 1.997E-02 6.296E-02 l.252E-01 8.073E-02 8.469E-02 1.320E+OO 4 .130E-02 1.022E+Ol 1. 628E-01 6.387E-02 1. 7 64E-02 3.053E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-.211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 3987 of 5809 6.346E-01 1. 631E+OO 2.464E+Ol 7.305E+Ol 3. 741E-01 1. 881E+OO 3.593E-02 l.498E+OO 3.568E-01 4.779E-01 2.737E-01 4.279E-01 1.937E-01 1.937E-01 3.409E-01 4.279E-01 3.876E-02 2.085E-01 3.166E+OO 1.404E-01 3.876E-02 O.OOOE+OO 1.881E-01 2.504E+02 7.483E-02 7.192E-02 5.099E-02 2.317E-02 2.600E-02 7.666E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:01:31.39 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235046.CNF;l * *Acquisition date 3-0CT-2016 06:57:53 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.88 Half life ratio : ***** *
  • Sample date 7-DEC-2015 10:02:00 Nuclide Library : SOLID *
  • Sample ID G405235046 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity 1.5693E+02 GRAM *
  • Quantity Err(%) 1.2745E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.269E+Ol 1.468E+OO SC-46 4. 696E-01 3.826E-01 CD-109 3.068E+OO 1.701E+OO SN-126 1.952E-01 l.078E-01 BA-137M l.535E-01 6.187E-02 CS-137 1. 621E-01 6.536E-02 TL-208 2.705E-01 8.274E-02 BI-212 1. 051E+OO 6.503E-01 PB-212 1.020E+OO 1. 2 69E-01 BI-214 8.868E-01 l.534E-01 PB-214 9. 396E-01 1. 581E-01 RN-222 8.868E-01 l.534E-01 RA-224 9.734E-01 1.126E+OO RA-226 8.868E-01 l.534E-01 AC-228 l.105E+00 2.759E-01 RA-228 l.105E+00 2.759E-01 TH-228 1. 020E+OO l.269E-01 TH-230 8.865E-01 1.534E-01 PA-231 9.175E-01 8.814E-01 TH-232 1.105E+OO 2.759E-01 TH-234 1.697E+OO 1.852E+OO U-234 8.865E-01 1.534E-01 U-238 1.697E+OO 1.852E+OO AM-243 1. 866E-01 9.155E-02 ANH-511 5.052'E-02 7.027E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 Page 3988 of 5809 Key-Line Activity (pCi/GRAM -5.115E+OO -l.917E-02 -1.000E+41 1. 086E-02 -5.929E+03 K.L Act error ( 1. 96-sigma) 1.108E+Ol 4.237E-02 6.259E+41 2. 591E-02 1.139E+04 TPU ( 1. 96-sigma) 1.468E+OO 3.826E-01 1.701E+OO l.078E-01 6.187E-02 6.536E-02 8.274E-02 6.503E-01 1. 2 69E-01 l.534E-01 1.581E-01 l.534E-01 l.126E+OO l.534E-01 2.759E-01 2.759E-01 l.269E-01 1.534E-01 8.814E-01 2.759E-01 1.852E+OO 1.534E-01 1.852E+OO 9.155E-02 7.027E-02 TPU ( 1 . 96-sigma ) l.131E+Ol 4.324E-02 O.OOOE+OO 2.637E-02 l.170E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF CR-51 l.126E+02 3.656E+02 3.691E+02 SHORT HLIF MN-54 -4.845E-02 5.464E-02 5.885E-02 NOT IDENT. C0-56 1.518E-01 4 .115E-01 4 .172E-01 FAIL ABUN MN-56 1.000E+41 2.735E+41 O.OOOE+OO SHORT HLIF C0-57 -3.777E-02 3.930E-02 4.283E-02 NOT IDENT. C0-58 5.550E-03 4.930E-01 4.930E-01 NOT IDENT. FE-59 -i.985E+OO 5.720E+OO 5.790E+00 NOT IDENT. C0-60 1.430E-02 3.034E-02 3.102E-02 FAIL ABUN ZN-65 3. 964E-02 1.497E-01 1.507E-01 NOT IDENT. GE-68 -l.014E+OO 792E+OO 1.850E+OO NOT IDENT. AS-73 1.646E+OO 4.751E+OO 4.809E+OO NOT IDENT. AS-74 -l.713E+OO 4.220E+03 4.220E+03 SHORT HLIF SE-75 3.793E-03 1.565E-01 1.565E-01 NOT IDENT. BR-77 2.488E+38 2.161E+39 O.OOOE+OO SHORT HLIF SR-82 1.806E+02 6.009E+02 6.063E+02 SHORT HLIF RB-83 3.339E-02 5.459E-01 5.461E-01 NOT IDENT. KR-85 5.665E-01 7.039E+OO 7.043E+OO NOT IDENT. SR-85 5.953E-02 7.518E-01 7.523E-01 NOT IDENT. RB-86 -1. 38 6E+04 2.213E+04 2.299E+04 SHORT HLIF Y-88 l.568E-02 1. 021E-01 l.023E-01 NOT IDENT. Y-91 -2.924E+02 5.227E+02 5.391E+02 NOT IDENT. NB-94 2.041E-02 2.515E-02 2.678E-02 NOT IDENT. NB-95 3.249E-02 9.390E-01 9.391E-01 NOT IDENT. NB-95M -6.130E-01 2.090E+OO 2.108E+OO NOT IDENT. ZR-95 1.472E-01 1.330E+OO l.331E+OO NOT IDENT. NB-97 l.000E+41 3.004E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 l.268E+41 O.OOOE+OO SHORT HLIF M0-99 7.318E+31 2.104E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 4.564E+41 O.OOOE+OO SHORT HLIF RH-101 9 .118E-03 3.066E-02 3.093E-02 NOT IDENT. RH-102 1. 775E-02 4.671E-02 4.739E-02 NOT IDENT. RU-103 1.059E+OO 4.673E+OO 4.697E+OO FAIL ABUN RH-106 -l.928E-01 4.258E-01 4.345E-01 NOT IDENT. RU-106 -1. 928E-01 4.258E-01 4.345E-01 NOT IDENT. AG-108M 8.832E-03 2.139E-02 2.176E-02 NOT IDENT. AG-llOM 2.149E-03 8. 411E-02 8. 411E-02 NOT IDENT. SN-113 -9.181E-02 1.834E-01 l.880E-01 NOT IDENT. CD-115 3.850E+39 3.654E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -1.833E+04 9.643E+04 9.679E+04 SHORT HLIF TE-123M 3.681E-02 1.211E-01 l.222E-01 NOT IDENT. SB-124 -3.225E-01 1. 841E+OO l.847E+OO NOT IDENT. SB-125 -5.840E-03 8.387E-02 8. 391E-02 NOT IDENT. TE-125M l.597E+02 2.289E+02 2.399E+02 NOT IDENT. I-126 -5.194E+05 8.726E+05 9.035E+05 SHORT HLIF SB-126 -2.742E+04 1.073E+06 l.073E+06 SHORT HLIF SB-127 -l.038E+22 2.662E+22 O.OOOE+OO SHORT HLIF I-131 -3.345E+08 4.461E+09 4.463E+09 SHORT HLIF I-132 -1.000E+41 1. 8 62E+42 O.OOOE+OO SHORT HLIF TE-132 -6. 031E+25 3.783E+26 0.000E+OO SHORT HLIF BA-133 2.859E-03 3.448E-02 3.450E-02 NOT IDENT. I-133 -l.000E+41 2.592E+41 O.OOOE+OO SHORT HLIF CS-134 2.659E-02 4.812E-02 4.959E-02 NOT IDENT. CS-135 -7.178E-02 1. 211E-01 l.254E-01 NOT IDENT. I-135 -l.000E+41 6.992E+41 O.OOOE+OO SHORT HLIF CS-136 -2 .112E+04 2.761E+05 2.763E+05 SHORT HLIF CE-139 -5.926E-02 1.017E-01 1. 051E-01 NOT IDENT. BA-140 4.661E+05 8.621E+05 8.873E+05 SHORT HLIF LA-140 -2. 072E+05 4.161E+05 4.265E+05 SHORT HLIF CE-141 3. 271E+OO 2.081E+Ol 2.086E+Ol NOT IDENT. CE-143 1.000E+41 8. 011E+40 O.OOOE+OO SHORT HLIF CE-144 -l.112E-01 3.246E-01 3.285E-01 NOT IDENT. PM-144 -6.332E-03 4.154E-02 4.164E-02 NOT IDENT. PR-144 -5.377E-01 3.612E+OO 3. 621E+OO NOT IDENT. PM-146 8.016E-03 2.997E-02 3.019E-02 FAIL ABUN ND-147 -l.122E+07 2.689E+07 2.736E+07 SHORT HLIF PM-147 -2.573E+Ol 6. 2 62E+02 6.263E+02 NOT IDENT. PM-149 -4.003E+40 4.588E+40 0.000E+OO SHORT HLIF EU-150 2.957E-02 2.442E-02 2.782E-02 FAIL ABUN EU-152 -2.624E-02 7.327E-02 7.422E-02 FAIL ABUN GD-153 -6.298E-02 l.606E-01 l.631E-01 NOT IDENT. EU-154 -6.036E-02 1.047E-01 1.082E-01 NOT IDENT. EU-155 3.293E-02 9.438E-02 9.554E-02 FAIL ABUN TB-160 l.519E-01 1. 752E+OO 1. 753E+OO FAIL ABUN H0-166M 2.843E-02 4.402E-02 4.584E-02 FAIL ABUN TM-171 -3.299E+OO 1.154E+Ol l.163E+Ol NOT IDENT. HF-172 -1.727E-Ol 2.253E-01 2.384E-01 FAIL ABUN LU-172 -3.901E-04 7.317E-02 7.317E-02 FAIL ABUN LU-176 4.360E-03 1.993E-02 2.003E-02 FAIL ABUN Page 3989 of 5809 HF-181 -1.825E+OO 3.747E+OO 3.836E+OO NOT IDENT. TA-182 -7.189E-02 7.464E-01 7. 471E-01 FAIL ABUN RE-183 8.555E-02 1. 801E+OO l.802E+OO NOT IDENT. RE-184 1.310E+Ol 2.759E+Ol 2.822E+Ol NOT IDENT. W-188 -3.759E+Ol 9.503E+Ol 9.653E+Ol FAIL ABUN IR-192 l.964E-01 3. 965E-01 4.062E-01 FAIL ABUN HG-203 2.030E-01 2.051E+OO 2.053E+OO NOT IDENT. BI-207 l.858E-02 3.791E-02 3.882E-02 FAIL ABUN PB-210 1.886E+OO 1.487E+OO 1. 713E+OO NOT IDENT. BI-211 2.588E+OO 4 .i37 5E-01 1. 246E+OO FAIL ABUN PB-211 2.369E-01 5.109E-01 5.220E-01 NOT IDENT. RN-219 -9.674E-03 3.102E-01 3.102E-01 NOT IDENT. RA-223 2.368E-01 4. 961E-01 5.074E-01 FAIL ABUN AC-227 1.446E-01 2.013E-01 2 .115E-01 FAIL ABUN TH-227 1.446E-01 2.013E-01 2.115E-01 FAIL ABUN TH-229 2.438E-02 3.644E-01 3.645E-01 FAIL ABUN TH-231 2.368E-01 4. 961E-01 5.074E-01 FAIL ABUN PA-233 -6.129E-04 4.304E-02 4.304E-02 FAIL ABUN PA-234 6. lllE-02 2.366E-01 2.382E-01 FAIL ABUN PA-234M -3.214E-01 3.541E+OO 3.544E+OO NOT IDENT. U-235 -2.878E-02 l.651E-01 1.656E-01 FAIL ABUN NP-237 -6.129E-04 4.304E-02 4.304E-02 FAIL ABUN NP-238 4.781E+40 5.270E+41 O.OOOE+OO SHORT HLIF NP-239 l.386E-01 2.052E-01 2.145E-01 FAIL ABUN PU-239 1.953E+02 2.744E+02 2.882E+02 NOT IDENT. AM-241 -6.961E-02 8.853E-02 9.393E-02 NOT IDENT. CM-243 -3.105E-02 8.495E-02 8.609E-02 FAIL ABUN BK-247 2.122E-02 5.399E-02 5.483E-02 NOT IDENT. CM-247 -7.907E-03 2.719E-02 2.743E-02 NOT IDENT. CF-249 -3.610E-03 2.972E-02 2.977E-02 NOT IDENT. CF-251 -2.636E-02 9.364E-02 9.439E-02 NOT IDENT. Page 3990 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 82.9146 87.09 128.9682 136.47 78.5592 45.60 91.8005 87.57 152. 2725 140.51 0.0000 46.54 54.5410 88.03 152.3671 143.76 88.8718 49. 72 0.0000 88.34 155.4788 144.24 73.0792 51. 35 83.1043 88.47 155.5053 145.44 69.5070 51. 87 95.0677 89.96 153.5216 152.43 72.4293 52.39 89.7516 1093.63 155.9520 153.25 0.0000 52. 97 82.2692 91.11 0.0000 323.87 88.5366 53.44 74.7554 92.59 136.8048 156.02 0.0000 54.07 78.0941 93.35 136.9392 158.56 0.0000 57.36 0.0000 94.56 89.1293 159.00 72.8749 57.53 79.6633 94.65 89.1400 162.33 75.5742 57.98 87.3697 94.67 89.1423 162.66 0.0000 59.27 110.5481 94.87 89.1647 163.33 70.6829 59.32 110.5574 97.43 90. 9961 165.86 84.5154 59.54 110.5986 98.43 79.9144 176.31 62.7151 60.96 96.5938 98.44 79.9155 176.60 0.0000 61.17 96.6277 99.53 80.0234 177. 52 62.7808 62.93 133.2498 100 .11 83.5626 181.07 0.0000 63.29 133.3285 102.03 65.1465 181.52 52.9153 63.58 133.3915 103.18 94.7497 184.41 56.8323 64.28 133.5432 103.37 92.0526 143.76 56.8948 66.73 125.5735 105.21 86.4173 193.51 64.4698 67.24 103.4961 105.31 86.4274 197.03 85.9195 125.81 109.4862 106.12 79.4966 198.01 66.4052 67.75 109.4982 106.47 86.5471 201.83 77.7079 69.67 125.7801 109.28 70.4057 203.43 66.6901 70.83 107.0471 111. 00 96. 4134 205.31 62.9353 72. 81 137.1933 111.76 0.0000 210.85 74.8134 72. 87 137.2054 114. 06 100.2916 215.65 60.4147 74.66 127.8517 116. 30 0.0000 222 .11 66.7766 74.82 127.8821 116.74 71.0088 227.09 54.8353 74.97 127.9099 119. 76 45.1233 227.38 54.8469 77 .11 128.3109 121.12 61.8397 228.16 0.0000 78.74 114.3224 121. 22 61.8464 228.18 55.7500 79.69 114.4770 121.78 78.5457 116.74 55.7500 80.12 108.5178 122.06 83. 3311 235.69 64.3716 80.19 0.0000 122. 92' 51. 2370 235. 96 64.3835 80.57 81.4400 123.07 54.8208 238.63 57.0456 81. 00 98.0891 265.00 50.0868 238.98 0.0000 81. 07 107.1544 125.81 95.6219 240.99 57.1401 81. 75 120. 0967 127.23 73.4206 242.00 57.1805 83.79 118 .1648 127.91 84.6545 244.70 46.2708 84.00 112.1374 129.30 79.1797 252.40 0.0000 85.43 130.5773 131.20 79.3368 252.80 53.1750 86.55 133.8163 133.02 75.4723 254.15 0.0000 86.79 133.8593 133.52 77 .1182 256.23 52. 4100 86.94 128.9424 136.00 70.0653 260.90 0.0000 Page 3991of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.0913 355.39 0.0000 584.27 19. 8396 264.80 41. 0951 356.01 25.4592 595.83 0.0000 265.00 37.5267 364.49 0.0000 427.87 16.8092 268.22 64.4663 366.42 0.0000 602.52 0.0000 269.46 38.5322 372.51 33.2910 604. 72 9.4695 270.03 7534 375.05 40.9546 6fJ7.14 15.7965 271.23 59.2096 377.52 33.3779 609.32 14.7554 273.65 0.0000 356.01 34.4429 610.33 14.7611 276.40 52.2061 388.16 32.6006 614.28 22.1732 277.37 53.1386 388.63 0.0000 618.01 23.2604 277.60 42.3375 391. 69 34.5798 620. 36 19.0481 278.00 38.7439 264.66 26.0508 621.93 24.3523 279.20 51.3976 401. 81 32.8234 630.19 0.0000 279.54 54 .1138 402.40 31.8674 631.29 15.9357 279.70 54 .1199 404.85 25.1378 633.25 17.0098 280.46 49.6334 410.95 36.8496 634.78 0.0000 283.69 35.2660 413.71 29.1309 635.95 14.8978 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 41.6407 423.72 0.0000 645.85 17.0859 285.90 0.0000 427.09 27.3631 657.76 12.8682 287.50 32.6309 427.87 29.3280 657.90 0.0000 290.67 43.5938 433.94 22.5494 661.66 18.2541 293.27 0.0000 439.40 30. 9610 664.57 0.0000 351. 93 40.9827 453.88 17.8099 666.33 0.0000 295.96 41. 0019 463.37 27.8228 666.50 0.0000 879.38 21. 9023 468.07 29.8724 667.71 0.0000 299.98 39.7316 473.00 0.0000 677.62 23.7528 300.09 39.7343 475.06 28. 9658 685.70 0.0000 300 .13 39.7352 476.78 19.9915 695.00 0.0000 301.36 39.7644 477.60 33.9972 696.49 17.3848 302.85 39.7998 482.18 31.0593 696. 51 17.3848 256.23 41.2134 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 9.7815 306.78 37.4174 497.08 22.1835 697.49 8.6953 308.46 41.3104 505.52 19.7329 702.65 14.1537 311.90 33 .1157 507.63 0.0000 706.68 15.2629 316.51 39.6616 511. 00 30.4279 711. 68 13.1040 319.41 0.0000 514.00 33.5129 720.70 0.0000 320.08 0.0000 514.00 33.5129 721.93 0.0000 321. 04 43.4649 520.40 23.4193 722. 78 18.0831 323.87 31. 9570 520.69 0.0000 722.91 18.0838 325.23 43.1056 522.65 0.0000 723. 31 31.2403 328.76 0.0000 527.90 0.0000 724 .19 24.6707 333.37 41.9073 528.26 15.3223 727.33 13.1709 333.97 22.3584 529.59 25. 5513 733.00 8.7965 334.37 41. 9312 529.87 0.0000 735.93 14.3081 338.28 52.2949 531. 02 0.0000 333.97 14.3150 338.32 52. 2961 537.26 0.0000 739.50 0.0000 311. 90 36.4641 546.56 0.0000 747.24 16.5686 340.48 36.4641 552.55 17.5347 748.06 18.7826 340.55 0.0000 563.25 21. 7520 752.31 17.7012 344.28 38.4141 569.33 24.9180 753.82 0.0000 345.93 31. 5096 946.00 22.8424 756.73 19.9417 351. 06 36.6760 569.70 22.8442 756.80 19.9424 351. 93 36.6934 583.19 19. 8311 884.68 26.6494 Page 3992 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 26.6641 1274.44 8.0008 1620.50 5.0671 766.42 28.3368 1001.03 15.1308 1621.92 6.0820 766.84 25.0058 1002.74 11.5757 1678.03 0.0000 772.60 0.0000 1004.73 14.2539 1690.97 6.1549 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3 .1154 778.90 32.3501 1028.54 0.0000 1063.66 6.2366 783.70 0.0000 1037.84 14.3730 1771.35 4.1587 785.37 25.1486 1038.76 0.0000 1791.20 0.0000 792.07 30.9119 631.29 15.3046 1808.65 3.1379 794.95 11.2097 1048.07 0.0000 1810.72 0.0000 795.86 20.1833 1049.04 18.9159 1836.06 1.0505 810.06 15.7648 1050.41 10.8127 810.29 15.7660 1063.66 10.8479 344.28 15.7665 1077.00 0.0000 810.76 15.7682 1077.34 11. 6094 815.77 0.0000 1085.87 8.7252 1048.07 0.0000 1093.63 19.1210 832.01 13.6006 1099.45 16.4125 834.85 22.6864 1112. 07 10.0594 835.71 12.4806 1112.84 12.1956 836.80 0.0000 1115. 54 -11.7156 846.75 0.0000 1120.29 9. 162 6 846.77 14'. 7969 1120.55 9.1632 856.80 0.0000 1221.41 9.1650 860.56 17 .1411 1129. 67 13.2231 871.09 8.0231 1131.51 0.0000 873.19 11. 4685 1147.95 0.0000 875.33 0.0000 1173.23 11.1299 879.38 13.7861 1177.95 16.3410 880.51 13.7905 1189.05 13.0310 883.24 6.9004 1204.77 24.2845 884.68 6.9033 1221.41 14.9990 889.28 13.8242 1231.02 13.1515 894.76 13.8452 1235.36 0.0000 898.04 15.0127 1238.28 11. 2903 900.72 16.1795 1260.41 0.0000 903.28 13.8779 1271.87 12.3200 911. 20 11. 5898 1274.44 18.0154 912.08 11. 5926 1274.54 17.0673 923.98 0.0000 1291.59 12.3708 926.50 16.2935 1298.22 0.0000 929 .11 12.8110 1312 .11 0.0000 937.49 17.5085 1332.49 6.7180 944.13 0.0000 1362.66 0.0000 946.00 14.0386 1365.19 4.8303 949.00 18.4404 1368.63 0.0000 667.71 0.0000 1384.29 9.0508 962.31 11.2793 1408.01 4.8715 964. 08 19.7477 1457.56 0.0000 966.17 0.0000 1460.82 6.8898 911.20 15.5359 1489.16 5.9374 968. 97 15.5359 1505.03 6.3520 983.53 0.0000 1584.12 9.0621 984.45 0.0000 1596.21 0.0000 Page 3993 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:03:01.04 ******************************************************************************** 4* GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM25.CNF;357 Background date : Z-OCT-2016 11:01:25. Sample date 7-DEC-2015 10:10:00. Acquisition date : 3-0CT-2016 07:00:30. Sample ID G405235047 Sample quantity 1.51349E+02 GRAM Detector name : GAM25 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.56 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 2 2 0 0 0 0 0 0 3 3 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 3994 of 5809 Energy 46.64* 53.35* 63.13* 74.85* 77.15* 83.83* 88.17 92.83* 129.09 186.02* 209.42 238.77* 241.67 270.41 276.52 277.89* 295.19* 300.34 328.32 338.88* 352.09* 447.74 464.79 482.67 511.26* 556.69 583.58* 588.90 609.55* 62 6. 45 690.83 694.35 727 .11 797.89 , BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 68 38 55 165 430 32 244 126 23 86 37 449 110 44 17 25 169 43 41 96 268 22 14 19 8 15 108 8 185 36 17 10 37 30 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 221 110 241 227 177 143 264 159 138 134 106 80 104 83 12 44 64 53 58 66 74 11 49 23 62 21 42 19 54 45 18 13 7 28 1. 04 1.16 0. 72 0.76 0.79 1.14 3.47 1. 39 0.78 1.12 0.99 1. 03 1. 54 0.79 0.83 1. 33 1.19 0.90 2.39 1. 56 1. 08 2.19 0.90 1. 77 1.24 0.64 1. 32 1.25 1. 40 7.10 2.00 1. 38 1. 72 5.52 92.79 106.19 125.75 149.19 153.79 167.14 175.83 185.15 257.66 371.50 418.30 477.00 482.79 540.29 552.49 555.24 589.83 600.13 656 .11 677.21 703.63 894.95 929.06 964. 83 1022.01 1112.89 1166. 69 1177.33 1218.63 1252.45 1381.24 1388.28 1453.82 1595.43 88 104 122 146 146 165 170 182 254 368 414 470 470 535 551 551 583 596 651 671 698 892 922 962 1015 1105 1162 1174 1212 1238 1372 1385 1449 1586 10 1. 88E-02 44. 2 6 l.06E-02 47.4 8 1.54E-02 52.4 16 4.59E-02 14.8 4.09E+OO 16 l.20E-01 6.8 6 8.93E-03 62.3 12 6.78E-02 14.9 8 3.51E-02 20.8 8 6. 33E-03 91. 8 9 2.40E-02 27.7 9 l.OlE-02 53.4 17 l.25E-01 5.7 1.25E+00 17 3.07E-02 22.3 10 l.22E-02 41.4 9 4.79E-03 36.9 3.14E+OO 9 6.92E-03 53.1 12 4.69E-02 12.4 9 l.20E-02 34.1 10 1.13E-02 38.3 15 2.66E-02 21.6 11 7.45E-02 8.8 7 5.97E-03 33.0 11 3.80E-03101.3 8 5.14E-03 50.1 13 2.17E-03241.l 11 4.lOE-03 66.5 13 3.00E-02 15.6 7 2.36E-03 89.5 15 5. 13E-02 11. 4 21 1. OlE-02 50 .1 12 4.61E-03 56.8 6 2.71E-03 67.5 10 1. 02E-02 21. 6 18 8.39E-03 46.8 Peak Search Report (continued) Page : 2 Sample ID : G405235047 Acquisition date 3-0CT-2016 07:00:30 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 877.76 4 17 1. 25 1755.24 1749 8 1.17E-03179 .1 36 0 911.59* 78 28 1. 93 1822.94 1816 14 2.17E-02 18.5 37 0 922.94 5 1. 72 1845.64 1841 7 2.16E-03 6Q.6 38 0 964. 31 21 6 1. 90 1928.42 1922 11 5.92E-03 30.5 39 0 969.34* 61 0 2.33 1938.49 1933 13 l.69E-02 13. 8 40 0 1009.53 5 10 0.67 2018.92 2013 8 l.35E-03128.3 41 0 1120.86* 39 18 1. 60 2241. 72 2233 14 1.08E-02 28.2 42 0 1154 .11 9 19 0.42 2308.26 2297 13 2.51E-03105.8 43 0 1178.35 18 13 4.77 2356.78 2351 13 5.00E-03 47.5 44 0 1258.31 16 18 1. 86 2516.80 2509 17 4.57E-03 62.7 45 0 1338. 77 5 9 4.35 2677.86 2668 11 l.39E-03133.0 46 0 1460.65* 402 0 1. 98 2921. 82 2913 18 1.12E-01 5.0 47 0 1764.66* 42 4 2.63 3530.46 3523 14 1.1 7E-02 18.5 Flag: "*" '."" Peak area was modified by background subtraction Page 3995 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:03:03 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 10:10:00 G405235047 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:00:30 151.35 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report GAMMA25 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 3996 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.56 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235047 Acquisition date 3-0CT-2016 07:00:30 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. l31E+OO 1.597E+Ol 1. 597E+Ol 10.05 OK AS-73 53.44 10.30* 9.638E+OO 2.507E-01 3.366E+OO 94.70 OK CD-109 88.03 3.70* 9.265E+OO 3.424E+OO 5.381E+OO 39.59 OK SN-126 64.28 9.60 9.545E+OO 3.905E-01 3.905E-01 104.75 OK 86.94 8.90 9.265E+OO 1.423E+OO 1.423E+OO 39.59 OK 87.57 37.00* 9.265E+OO 3.424E-01 3.424E-01 39.59 OK HG-203 70.83 3.69 9.445E+OO Line Not Found Absent 72.87 6.19 9.424E+OO Line Not Found Absent 279.20 81.56* 4. 801E+OO 1.447E-02 1.272E+OO 268.94 OK TL-208 277.37 6.60 4.809E+OO Line Not Found <<INT Reject 583.19 85.00* 2.509E+OO 2.673E-01 2.673E-01 31. 22 OK 860.56 12.50 1. 810E+OO. Line Not Found Absent PB-210 46.54 4.25* 9.157E+OO 1.149E+OO 1.179E+OO 88.41 OK PB-212 74.82 10.28 9.404E+OO 4.478E-01 4.478E-01 80.06 OK 77 .11 17.10 9.382E+OO 1. 704E+OO 1.704E+OO 13.54 OK 238.63 43.60* 5.476E+OO 1.083E+OO 1.083E+OO 11. 42 OK 300.09 3.30 4.483E+OO 1.645E+OO 1.645E+OO 68. 26 OK BI-214 609.32 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 OK 1120.29 14. 92 . 1.443E+OO 8.896E-01 8.899E-01 56.43 OK 1764.49 15.30 9.335E-01 1.386E+OO 1.387E+OO 37.02 OK PB-214 74.82 5.80 9.405E+OO Line Not Found <<INT Reject 77 .11 9.70 9.382E+OO 3. 005E+OO -3.006E+OO 13.54 OK 87.09 3.41 9.279E+OO Line Not Found <<INT Reject 242.00 7.25 5.413E+OO Line Not Found <<INT Reject 295.22 18.42 4.552E+OO 1.135E+OO 1.136E+OO 24.72 OK 351.93 35.60* 3.893E+OO 1.074E+OO 1.074E+OO 17.57 OK RN-222 609.32 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 OK 1120.29 14.92 l.443E+OO 8.896E-01 8.899E-01 56.43 OK 1764.49 15.30 9.335E-01 1.386E+OO 1.387E+OO 37.02 OK RA-224 240.99 4.10* 5.420E+OO 8.483E-01 8.483E-01 161.11 OK RA-226 609.32 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 OK 1120.29 14.92 1.443E+OO 8. 896E-01 8.899E-01 56.43 OK 1764.49 15.30 9.335E-01 1. 386E+OO 1.387E+OO 37.02 OK AC-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.027E+OO 1.17 6E+OO 1.176E+OO 43.10 OK 794.95 4.25 1.935E+OO Line Not Found Absent 835. 71 1. 61 1.856E+OO Line Not Found Absent 911. 20 25.80* 1.724E+OO 8.859E-01 8.859E-01 37.10 OK 968.97 15.80 1.637E+OO 1.177E+OO 1.177E+OO 27.51 OK RA-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.027E+OO 1. l 76E+OO l.176E+OO 43.10 OK 794.95 4.25 1.935E+OO Line Not Found Absent 835. 71 1. 61 l.856E+OO Line Not Found Absent 911. 20 25.80* 1.724E+OO 8.859E-01 8.859E-01 37.10 OK 968. 97 15.80 1.637E+OO 1.177E+OO l.177E+OO 27.51 OK TH-228 74.82 10.28 9.404E+OO 4.478E-01 4.478E-01 80.06 OK 77 .11 17.10 9.382E+OO 1. 704E+OO 1.704E+OO 13. 54 OK 238.63 43.60* 5.476E+OO 1.083E+OO 1.083E+OO 11. 42 OK 300.09 3.30 4.483E+OO 1.645E+OO 1.645E+OO 68.26 OK Page 3997 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235047 Acquisition date 3-0CT-2016 07:00:30 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230

  • 609.32 45.49* 2.418E+OO 8.813E-01 8,..813E-01 22.84 OK 1120.29 14.92 1.443E+OO 8.896E-01 8.896E-01 56.43 OK 1764.49 15.30 9.335E-01 1.386E+OO 1.386E+OO 37.02 OK PA-231 283.69 1. 70 4. 715E+OO Line Not Found Absent 301.36 5.35* 4.483E+OO 1.014E+OO 1.014E+00 68.26 OK TH-232 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.027E+OO 1.176E+OO 1.176E+OO 43.10 OK 835.71 1. 61 l.856E+OO Line Not Found Absent 911.20 25.80* 1.724E+OO 8.859E-01 8.859E-01 37.10 OK 968. 97 15.80 1.637E+00 l.177E+OO 1.177E+OO 27.51 OK TH-234 63.29 3.70* 9.545E+00 1.013E+OO 1. 013E+00 104.75 OK 92.59 4.23 9.202E+OO 2.029E+OO 2.029E+OO 41. 59 OK U-234 609.32 45.49* 2.418E+00 8.813E-01 8. 813E-01 22.84 OK 1120.29 14.92 1.443E+OO 8.896E-01 8.896E-01 56.43 OK 1764.49 15.30 9.335E-01 l.386E+OO 1.386E+OO 37.02 OK U-238 63.29 3.70* 9.545E+OO 1. 013E+OO 1. 013E+OO 104.75 OK 92.59 4.23 9.202E+OO 2.029E+OO 2.029E+00 41. 59 OK AM-243 43.53 5.90 8.344E+OO Line Not Found Absent 74.66 67.20* *9. 404E+OO 6.851E-02 6.851E-02 80.06 OK ANH-511 511. 00 100.00* 2.809E+OO l.484E-02 1. 484E-02 482.27 OK Flag: "*" = Keyline r I Page 3998 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:03:05.02 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l *
  • Acquisition date 3-0CT-2016 07:00:30 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 7-DEC-2015 10:10:00 Analyst initials: MXRl *
  • Sample ID G405235047 Sample Quantity 1.5135E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
  • Combined Activity-MDA Report NO.TE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM -K-40 1.597E+Ol 1.573E+OO 4.293E-01 AS-73 3.366E+OO 3.124E+OO 2.878E+OO CD-109 5.381E+OO 2.088E+OO 1.045E+OO SN-126 3.424E-01 l.329E-01 6.644E-02 HG-203 1.272E+OO 3.352E+OO 3.925E+OO TL-208 2.673E-01 8.178E-02 6.899E-02 PB-210 1.179E+OO 1.022E+OO 6.320E-01 PB-212 1.083E+OO 1.212E-01 9.189E-02 BI-214 8.816E-01 l.974E-01 l.195E-01 PB-214 1.074E+OO 1. 849E-01 1.203E-01 RN-222 8.816E-01 l.974E-01 1.195E-01 RA-224 8.483E-01 1.339E+OO 9.866E-01 RA-22 6 8.816E-01 l.974E-01 1.195E-01 AC-228 8.859E-01 3. 221E-01 2.472E-01 RA-228 8.859E-01 3.221E-01 2.472E-01 TH-228 l.083E+OO l.212E-01 9.189E-02 TH-230 8.813E-01 1.973E-01 1.194E-01 PA-231 1.014E+OO 6.786E-01 6.694E-01 TH-232 8.859E-01 3. 221E-01 2.472E-01 TH-234 1.013E+OO 1.040E+OO 7.514E-01 U-234 8.813E-01 l.973E-01 1.194E-01 U-238 l.013E+OO 1.040E+OO 7.514E-01 AM-243 6. 851E-02 5.375E-02 4.420E-02 ANH-511 l.484E-02 7.016E-02 4.474E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -1.498E+OO l.024E+Ol l.979E+Ol NOT IDENT. NA-22 1. 8 92E-02 4.591E-02 9.629E-02 NOT IDENT. NA-24 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF AL-26 1. 641E-02 1.857E-02 5.896E-02 NOT IDENT. SC-46 2.375E-01 3 .-539E-01 7.786E-01 FAIL ABUN I V-48 0. OOOE+OO"-l.554E+04 O.OOOE+OO SHORT HLIF Page 3999 of 5809 COA 405235 CR-51 O.OOOE+OO 3.623E+02 O.OOOE+OO SHORT HLIF MN-54 3 .114E-02 6.194E-02 1. 311E-01 NOT IDENT. C0-56 l.064E-02 4.034E-01 8.232E-01 NOT IDENT. MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 l.562E-02 3.077E-02 6.282E-02 NOT IDENT. C0-58 5. 071E-01 5.222E-01 1.195E+00 NOT IDENT. FE-59 3.160E-01 7.548E+OO 1.493E+Ol NOT IDENT. C0-60 3.414E-02 4.531E-02 9.255E-02 NOT IDENT. ZN-65 1.009E-01 2.076E-01 3.865E-01 NOT IDENT. GE-68 1.277E+OO 2. 743E+OO 5.617E+OO NOT IDENT. AS-74 O.OOOE+OO 5.628E+03 O.OOOE+OO SHORT HLIF SE-75 l.437E-01 1.597E-01 3.281E-01 NOT IDENT. BR-77 O.OOOE+OO 2.953E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.800E+02 O.OOOE+OO SHORT HLIF RB-83 3.605E-01 5.972E-01 1.248E+OO NOT IDENT. KR-85 4.580E-01 6.606E+OO 1.160E+Ol NOT IDENT. SR-85 4.702E-02 7.055E-01 1.238E+OO NOT IDENT. RB-86 O.OOOE+OO 3.500E+04 O.OOOE+OO SHORT HLIF Y-88 6.973E-02 1.498E-01 4.127E-01 NOT IDENT. Y-91 7.802E+Ol 6.323E+02 1.220E+03 NOT IDENT. NB-94 -9.474E-03 3.525E-02 6.307E-02 NOT IDENT. NB-95 1.140E-01 8.681E-01 1. 646E+OO NOT IDENT. NB-95M 3.327E-01 2.338E+OO 4. OllE+OO NOT IDENT. ZR-95 9.346E-01 1.592E+OO 3.205E+OO NOT IDENT. NB-97 O.OOOE+OO 1.808E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.920E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF RH-101 -1.326E-02 2.612E-02 4.489E-02 NOT IDENT. RH-102 -3.004E-02 5.983E-02 9.153E-02 NOT IDENT. RU-103 -5.389E-01 5.149E+OO 9.684E+OO FAIL ABUN RH-106 2.099E-01 4.636E-01 9.457E-01 NOT IDENT. RU-106 2.099E-01 4.636E-01 9.457E-01 NOT IDENT. AG-108M 8.297E-03 2.274E-02 4.695E-02 NOT IDENT. AG-llOM -4.504E-02 9. 872E-02 1.840E-01 NOT IDENT. SN-113 9.424E-03 2.025E-01 4.016E-01 NOT IDENT. CD-115 O.OOOE+OO 4.158E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 7.316E+04 O.OOOE+OO SHORT HLIF TE-123M 4.133E-02 9.566E-02 1.902E-01 NOT IDENT. SB-124 -l.156E+OO 1.636E+OO 2.812E+OO NOT IDENT. SB-125 -1.212E-03 8.542E-02 1.687E-01 FAIL ABUN TE-125M 1.087E+02 1.724E+02 3.564E+02 NOT IDENT. I-126 O.OOOE+OO 8.372E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.319E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.848E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.385E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4.264E+26 O.OOOE+OO SHORT HLIF BA-133 4.513E-02 3.874E-02 7.902E-02 FAIL ABUN I-133 O.OOOE+OO 1.076E+41 O.OOOE+OO SHORT HLIF CS-134 6.562E-02 5.098E-02 1.153E-01 NOT IDENT. CS-135 9.733E-02 1.108E-01 2.139E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.344E+05 O.OOOE+OO SHORT HLIF BA-137M 5.086E-02 3. 696E-02 8.035E-02 NOT IDENT. CS-137 5.372E-02 3.904E-02 8.488E-02 NOT IDENT. CE-139 3.480E-02 9.004E-02 1. 761E-01 NOT IDENT. BA-140 O.OOOE+OO 1.194E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.190E+05 O.OOOE+OO SHORT HLIF CE-141 -1.922E+Ol 1.915E+Ol 3.371E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 696E+41 O.OOOE+OO SHORT HLIF CE-144 -2.232E-02 2.469E-01 4.765E-01 NOT IDENT. PM-144 -4.633E-02 6.018E-02 8.427E-02 NOT IDENT. PR-144 -4. 041E+OO 5.229E+OO 7.316E+OO NOT IDENT. PM-146 1.016E-02 3.492E-02 7.165E-02 NOT IDENT. ND-147 O.OOOE+OO 3.219E+07 o. o*ooE+oo SHORT HLIF PM-147 3.208E+02 5.398E+02 1.108E+03 NOT IDENT. PM-149 O.OOOE+OO 4.846E+40 0.000E+OO SHORT HLIF EU-150 8.107E-03 2.252E-02 4.244E-02 FAIL ABUN EU-152 4.306E-03 8.512E-02 1. 540E-01 FAIL ABUN GD-153 -4.498E-02 9.529E-02 1.812E-01 NOT IDENT. EU-154 4.277E-02 1.118E-01 2.336E-01 NOT IDENT. EU-155 5.468E-02 7.004E-02 1.454E-01 NOT IDENT. TB-160 1.515E-01 1. 780E+OO 3.262E+OO FAIL ABUN H0-166M 2.706E-03 5.909E-02 1.113E-01 NOT IDENT. TM-171 O.OOOE+OO 6.866E+OO 6.828E+OO FAIL ABUN HF-172 1.406E-01 1.631E-01 3.198E-01 FAIL ABUN LU-172 5.697E-02 8.025E-02 1.724E-01 FAIL ABUN Page 4000 of 5809 LU-176 -4.754E-03 2.189E-02 3.866E-02 FAIL ABUN HF-181 5.741E+OO 5.637E+OO 8.816E+OO FAIL ABUN TA-182 6.906E-02 1.102E+OO 2.lOOE+OO FAIL ABUN RE-183 -3.469E-02 6.934E-01 l.427E+00 NOT IDENT. RE-184 1.807E+Ol 2.820E+Ol 6.177E+Ol NOT IDENT. W-188 -5.588E+Ol 1.114E+02 1.726E+02 FAIL ABUN IR-192 1.113E-01 3.827E-01 7.877E-01 FAIL ABUN BI-207 -l.804E-02 4.080E-02 7.525E-02 FAIL ABUN BI-211 O.OOOE+OO 5.094E-01 7.673E-01 FAIL ABUN PB-211 5.806E-01 1.240E+OO 4NOT IDENT. BI-212 O.OOOE+OO 5.759E-01 1.156E+OO FAIL ABUN RN-219 6.834E-02 3.174E-01 6.423E-01 FAIL ABUN RA-223 l.866E-02 5.773E-01 1.045E+OO FAIL ABUN AC-227 l.689E-01 l.997E-01 3.983E-01 FAIL ABUN TH-227 1.689E-01 l.997E-01 3.983E-01 FAIL ABUN TH-229 2.414E-01 3.557E-01 7 .116E-01 FAIL ABUN TH-231 1. 8 66E-02 5.773E-01 l.045E+OO FAIL ABUN PA-233 6.112E-03 4. 972E-02 l.007E-01 FAIL ABUN PA-234 2.434E-01 2.739E-01 6.077E-01 NOT IDENT. PA-234M 2. 972E+OO 4.197E+OO 9.205E+OO NOT IDENT. U-235 6.915E-02 1.391E-01 2.752E-01 FAIL ABUN NP-237 6 .112E-03 4. 972E-02 1.007E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 1.134E-01 1.602E-01 3.308E-01 FAIL ABUN PU-239 2.625E+02 4. 723E+02 4.801E+02 FAIL ABUN AM-241 -2.899E-02 3.793E-02 6.903E-02 NOT IDENT. CM-243 -l.313E-03 5.876E-02 1.166E-01 FAIL ABUN BK-247 4.518E-02 5. 65'4E-02 l.144E-01 FAIL ABUN CM-247 5.547E-03 3.083E-02 6.176E-02 FAIL ABUN CF-249 8.787E-03 3.316E-02 6.707E-02 NOT IDENT. CF-251 -4.824E-02 9.093E-02 1. 641E-01 NOT IDENT. Page 4001 of 5 809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:03:02.14 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 388 10.66* 1.131E+OO 1.597E+Ol 1.597E+Ol 10.05 AS-73 53.44 50 10.30* 9.638E+OO 2.507E-01 3.366E+OO 94.70 CD-109 88.03 309 3.70* 9.265E+OO 4.470E+OO 7.025E+OO 29.77 SN-126 64.28 72 9.60 9.545E+OO 3.905E-01 3.905E-01 104.75 86.94 309 8.90 9.265E+00 1.858E+OO l.858E+OO 29.77 87.57 309 37.00* 9.265E+00 4.470E-01 4.470E-01 29.77 HG-203 70.83 ------3.69 9.445E+OO ------Line Not Found ------72. 87 ------6.19 9.424E+OO ------Line Not Found ------279.20 28 81.56* 4. 801E+OO 3.609E-02 3.174E+OO 106.15 TL-208 277.37 28 6.60 4. 801E+OO 4.460E-01 4.460E-01 106.15 583.19 115 85.00* 2.509E+00 2.673E-01 2.673E-01 31. 22 860.56 ------12.50 1.810E+OO ------Line Not Found ------PB-210 46.54 90 4.25* 9.157E+OO l.149E+OO 1.179E+OO 88.41 BI-211 72.87 ------1.23 9.424E+OO ------Line Not Found ------351. 06 300 12.92* 3.893E+OO 2.959E+OO 2.959E+OO 17.57 PB-212 74.82 212 10.28 '9. 404E+OO 1.088E+OO 1. 088E+00 29.55 77 .11 551 17.10 9.382E+00 1.704E+OO 1.704E+OO 13.54 238.63 521 43.60* 5.476E+OO 1.083E+OO 1.083E+OO 11. 42 300.09 49 3.30 4.483E+OO l.645E+00 1.645E+OO 68.26 BI-214 609.32 195 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 1120. 29 39 14.92 l.443E+OO 8. 896E-01 8.899E-01 56.43 1764.49 40 15.30 9.335E-01 l.386E+OO 1.387E+OO 37.02 PB-214 74.82 212 5.80 9.404E+OO 1.929E+OO 1.930E+OO 29.55 77 .11 551 9.70 9.382E+OO 3.005E+OO 3.006E+OO 13.54 87.09 309 3.41 9.265E+OO 4.850E+OO 4.852E+00 29.77 242.00 128 7.25 5.420E+OO 1.615E+OO 1.616E+OO 44.59 295.22 192 18.42 4.552E+OO l.135E+OO l.136E+00 24. 72 351. 93 300 35.60* 3.893E+OO l.074E+OO 1.074E+OO 17.57 RN-222 609.32 195 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 1120.29 39 14.92 l.443E+OO 8. 896E-01 8.899E-01 56.43 1764.49 40 15.30 9.335E-01 1.386E+OO 1.387E+OO 37.02 RA-224 240.99 128 4.10* 5.420E+00 2.856E+OO 2.856E+OO 44.59 RA-226 609.32 195 45.49* 2.418E+OO 8.813E-01 8.816E-01 22.84 1120.29 39 14.92 l.443E+OO 8. 896E-01 8.899E-01 56.43 1764.49 40 15.30 9.335E-01 1.386E+OO 1.387E+OO 37.02 AC-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 108 11. 27 4.027E+OO 1.176E+OO 1.176E+00 43.10 794.95 ------4.25 1.935E+OO ------Line Not Found ------835.71 ------1. 61 1.856E+OO ------Line Not Found ------911.20 79 25.80* 1. 724E+OO 8.859E-01 8.859E-01 37.10 968.97 61 15.80 1.637E+OO l.177E+OO 1.177E+OO 27.51 RA-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 108 11. 27 4.027E+OO l.176E+OO 1.176E+OO 43.10 794.95 ------4.25 1.935E+OO ------Line Not Found ------835. 71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 79 25.80* 1. 724E+OO 8.859E-01 8.859E-01 37.10 968.97 61 15.80 1.637E+OO l.177E+OO 1. l 77E+00 27.51 Page 4002 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235047 Acquisition date 3-0CT-2016 07:00:30 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error .TH-228 74. 82 212 10.28 9. 404E,+00 1.088E+OO 1.088E+OO 29.55 77 .11 551 17.10 9.382E+OO 1.704E+OO 1. 704E+OO 13.54 238.63 521 43.60* 5.476E+OO 1.083E+OO 1.083E+OO 11. 42 300.09 49 3.30 4.483E+OO 1.645E+OO 1.645E+OO 68.26 TH-230 609.32 195 45.49* 2.418E+OO 8. 813E-01 8. 813E-01 22.84 1120.29 39 14.92 l.443E+OO 8. 896E-01 8.896E-01 56.43 1764.49 40 15.30 9.335E-01 1.386E+OO 1.386E+OO 37.02 PA-231 283.69 ------1. 70 4.715E+OO ------Line Not Found ------301.36 49 5.35* 4.483E+OO 1.014E+OO 1.014E+OO 68.26 TH-232 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 108 11. 27 4.027E+OO 1.176E+OO 1.176E+OO 43.10 835.71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 79 25.80* 1. 724E+OO 8.859E-01 8.859E-01 37.10 968.97 61 15.80 1.637E+OO 1. l 77E+OO 1.177E+OO 27.51 TH-234 63.29 72 3.70* 9.545E+OO 1.013E+OO 1. 013E+OO 104.75 92.59 159 4.23 9.202E+OO 2.029E+OO 2.029E+OO 41. 59 U-234 609.32 195 45.49* 2.418E+OO 8.813E-01 8.813E-01 22.84 1120. 29 39 14.92 1.443E+OO 8. 896E-01 8. 896E-01 56.43 1764.49. 40 15.30 9.335E-01 1.386E+OO 1;386E+OO 37.02 U-238 63.29 72 3.70* 9.545E+OO 1.013E+OO 1. 013E+OO 104.75 92.59 159 4.23 9.202E+OO 2.029E+OO 2.029E+OO 41. 59 AM-243 43.53 ------5.90 8.344E+OO ------Line Not Found ------74.66 . 212 67.20* 9.404E+OO 1.665E-01 1.665E-01 29.55 ANH-511 511. 00 8 100.00* 2.809E+OO 1.484E-02 l.484E-02 482.27 Flag: "*" Key line Page 4003 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235047 Acquisition date 3-0CT-2016 07:00:30 Total number of lines in spectrum 47 Number of unidentified lines 11 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-126 HG-203 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 80.300 461.40D 2.30E+05Y 46.590 1. 41E+l0Y 22.20Y 7.04E+08Y 1.41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+10Y 1.41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 13.4 1. 57 1. 00 87.9 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 '1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.597E+Ol 2.507E-01 4.470E+OO 4.470E-01 3.609E-02 2.673E-01 1.149E+OO 2.959E+OO 1.083E+OO 8. 813E-01 l.074E+00 8.813E-01 2.856E+OO 8.813E-01 8.859E-01 8.859E-01 1.083E+OO 8.813E-01 1.014E+OO 8.859E-01 1.013E+OO 8.813E-01 1. 013E+OO 1.665E-01 1.484E-02 4.193E+01 4.193E+Ol Decay Corr pCi/GRAM 1.597E+Ol 3.366E+OO 7.025E+OO 4.470E-01 3.174E+OO 2.673E-01 1.179E+OO 2.959E+OO 1.083E+OO 8.816E-01 1.074E+OO 8.816E-01 2.856E+OO 8.816E-01 8.859E-01 8.859E-01 1.083E+OO 8.813E-01 1.014E+00 8.859E-01 1.013E+OO 8.813E-01 1.013E+OO 1.665E-01 l.484E-02 5.077E+Ol 5.077E+Ol 76.60% Decay Corr 2-Sigma Error 0.160E+Ol 3.188E+OO 2.091E+00 1.331E-01 3.369E+OO 0.834E-01 1.043E+OO 0.520E+OO 0.124E+OO 2.014E-01 0.189E+00 2.014E-01 1.273E+OO 2.014E-01 3.286E-01 3.286E-01 0.124E+00 2.013E-01 0.692E+OO 3.286E-01 1. 061E+OO 2.013E-01 1.061E+OO 0.492E-01 7.159E-02 "M" Manually accepted 2-Sigma %Error 10.05 94.70 29.77 29.77 106.15 31. 22 88.41 17.57 11. 42 22.84 17.57 22.84 44.59 22.84 37.10 37.10 11. 42 22.84 68.26 37.10 104.75 22.84 104.75 29.55 482.27 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4004 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235047 Acquisition date : 3-0CT-2016 07:00:30 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 83.83 41 181 1.14 167.14 165 6 8.93E-03 **** 9.32E+OO T 0 129.09 28 169 0.78 257.66 254 8 6.33E-03 **** 8.36E+OO T 0 186.02 103 159 1.12 371.50 368 9 2.40E-02 55.3 6.69E+OO T 0 209.42 43 0.99 418.30 414 9 l.OlE-02 **** 6.lQE+OO T 0 270.41 50 95 0.79 540.29 535 10 1.22E-02 82.9 4.92E+OO T 4 276.52 20 14 0.83 552.49 551 9 4.79E-03 73.7 4.82E+OO T 0 328.32 46 66 2.39 656 .11 651 10 1.13E-02 76.5 4.14E+OO T 0 447.74 23 11 2.19 894.95 892 7 5.97E-03 66.0 3.15E+OO 0 464.79 15 54 0.90 929.06 922 11 3.80E-03 **** 3.05E+OO T 0 482.67 20 25 1. 77 964. 83 962 8 5.14E-03 **** 2.95E+OO T 0 556.69 16 23 0.64 1112.89 1105 11 4.lOE-03 **** 2.61E+OO 0 588.90 9 20 1. 25 1177.33 1174 7 2.36E-03 **** 2.49E+OO 0 626.45 38 47 7.10 1252.45 1238 21 l.OlE-02 **** 2.36E+OO 0 690.83 17 19 2.00 1381.24 1372 12 4.61E-03 **** 2.18E+OO 0 694.35 10 14 1. 38 1388. 28 1385 6 2.71E-03 **** 2.17E+OO T 0 727 .11 38 8 1. 72 1453.82 1449 10 l.02E-02 43.l 2.09E+OO T 0 797.89 31 29 5.52 1595.43 1586 18 8.39E-03 93.6 1.93E+OO 0 877.76 4 17 1. 25 1755.24 1749 8 l.17E-03 **** 1.78E+OO 0 922.94 8 5 1. 72 1845.64 1841 7 2.16E-03 **** 1.71E+OO T 0 964.31 22 6 1. 90 1928.42 1922 11 5.92E-03 61.0 1. 64E+OO T 0 1009.53 5 10 0.67 2018.92 2013 8 l.35E-03 **** 1. 58E+OO 0 1154 .11 9 19 0.42 2308.26 2297 13 2.51E-03 **** 1. 41E+OO 0 1178.35 18 13 4.77 2356.78 2351 13 5.00E-03 95.1 1.38E+OO T 0 1258.31 16 17 1. 86 2516.80 2509 17 4.57E-03 **** 1.30E+OO 0 1338. 77 5 9 4.35 2677.86 2668 11 1.39E-03 **** 1. 23E+OO Flags: "T" = Tentatively associated Page 4005of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:03:19.19 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • 4 DETECTOR AND SAMPLE DATA * * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l *
  • Acquisition date 3-0CT-2016 07:00:30 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 7-DEC-2015 10:10:00 Nuclide Library : SOLID *
  • Sample ID G405235047 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.5135E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;15
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-126 HG-203 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 1. 58 6E-01 1.341E+OO 4.897E-01 3 .112E-02 1.804E+OO 3.126E-02 2. 967E-01 4.300E-02 5.348E-02 5.512E-02 5.348E-02 4.618E-01 5.348E-02 1.083E-01 1.083E-01 4.300E-02 5.346E-02 3.054E-01 1.083E-01 3.552E-01 5.346E-02 3.552E-01 2.096E-02 1.991E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4006 of 5809 Le (pCi/GRAM 8. 772E+OO 4.158E-02 O.OOOE+OO 2.207E-02 3.426E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-ll3 CD-l15 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 4007 of 5809 5.836E-02 3.561E-Ol O.OOOE+OO 2.931E-02 5.290E-01 6.575E+OO 4.017E-02 l.715E-01 2.504E+OO O.OOOE+OO l.505E-01 O.OOOE+OO O.OOOE+OO 5.613E-01 5.199E+OO 5.549E-01 O.OOOE+OO 1. 528E-01 5.420E+02 2.833E-02 7.335E-01 l.873E+OO l.440E+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 2. 096E-02 3. 966E-02 4.306E+OO 4.217E-01 4.217E-01 2. llOE-02 7.976E-02 l.823E-01 O.OOOE+OO O.OOOE+OO 8.857E-02 9.427E-01 7.561E-02 l.669E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.643E-02 O.OOOE+OO 5.220E-02 9.808E-02 O.OOOE+OO O.OOOE+OO 3.673E-02 3.880E-02 8.247E-02 O.OOOE+OO O.OOOE+OO l.571E+Ol O.OOOE+OO 2.220E-01 3.646E-02 3.164E+00 3.202E-02 O.OOOE+OO 5.177E+02' O.OOOE+OO l.941E-02 7. 013E-02' 8.412E-02 l.007E-01 6.846E-02 l.403E+OO 4. 969E-02 3.197E+OO l.498E-01 7.630E-02 l.763E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4008 of 5809 4.009E+OO 9.341E-01 6.703E-01 2.715E+Ol 7.878E+Ol 3.605E-01 3.148E-02 3.700E-01 5.664E-01 5.288E-01 2.907E-01 4.807E-01 1.848E-01 1.848E-01 3. 311E-01 4.807E-01 4.615E-02 2.699E-01 4.094E+OO 1.294E-01 4.615E-02 O.OOOE+OO 1. 551E-01 2.265E+02 3.240E-02 5.442E-02 5.254E-02 2.809E-02 3.058E-02 7.613E-02 FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL 'ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:03:24.87 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * **
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235047.CNF;l *
  • Acquisition date 3-0CT-2016 07:00:30 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.56 Half life ratio : ***** *
  • Sample date 7-DEC-2015 10:10:00 Nuclide Library : SOLID *
  • Sample ID G405235047 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : l.5135E+02 GRAM *
  • Quantity Err(%) : 1.3214E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal.'date l-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 1.597E+Ol 1. 780E+OO AS-73 3.366E+OO 3.200E+OO CD-109 5.381E+OO 2.143E+OO SN-126 3.424E-01 l.352E-01 HG-203 1. 272E+OO 3.359E+OO TL-208 2.673E-01 8.256E-02 PB-210 1.179E+OO 1.026E+OO PB-212 1.083E+OO 1. 341E-01 BI-214 8.816E-01 2.0lOE-01 PB-214 1.074E+OO l.902E-01 RN-222 8.816E-01 2.0lOE-01 RA-224 8.483E-01 1.347E+OO RA-226 8.816E-01 2.0lOE-01 AC-228 8.859E-01 3.252E-01 RA-228 8.859E-01 3.252E-01 TH-228 1.083E+OO 1.341E-01 TH-230 8.813E-01 2.009E-01 PA-231 1.014E+OO 7.123E-01 TH-232 8.859E-01 3.252E-01 TH-234 1.013E+00 1.064E+OO U-234 8. 813E-01 2.009E-01 U-238 1. 013E+00 1.064E+OO AM-243 6.851E-02 5.532E-02 ANH-511 1.484E-02 7.016E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4009 of 5809 Key-Line Activity (pCi/GRAM -l.498E+OO l.892E-02 -l.000E+41 l.641E-02 2.375E-01 5.650E+03 K.L Act error (l.96-sigma) 1.024E+Ol 4.592E-02 2. 491E+41 1. 8 60E-02 3.540E-01 1.554E+04 TPU ( 1. 96-sigma) 1. 780E+OO 3.200E+OO 2.143E+OO l.352E-01 3.359E+OO 8.256E-02 1. 02 6E+OO 1. 341E-01 2.0lOE-01 l.902E-01 2.0lOE-01 1. 34 7E+OO 2.0lOE-01 3.252E-01 3.252E-01 1.341E-01 2.009E-01 7.123E-01 3.252E-01 l.064E+00 2.009E-01 1.064E+OO 5.532E-02 7.016E-02 TPU (1.96-sigma) 1.026E+Ol 4. 671E-02 O.OOOE+OO 2.00lE-02 3.699E-01 1. 57 5E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -3.670E+02 3.627E+02 3.986E+02 SHORT HLIF MN-54 3 .114E-02 6 .196E-02 6.353E-02 NOT IDENT. C0-56 1.064E-02 4.034E-01 4.035E-01 NOT IDENT. MN-56 l.OOOE+41 4.464E+42 O.OOOE+OO SHORT HLIF C0-57 l.562E-02 3.077E-02 3.157E-02 NOT IDENT. C0-58 5. 071E-01 5.227E-01 5.705E-01 NOT IDENT. FE-59 3.160E-01 7.548E+OO 7.550E+OO NOT IDENT. C0-60 3.414E-02 4.533E-02 4.787E-02 NOT IDENT. ZN-65 1.009E-01 2.076E-01 2.126E-01 NOT IDENT. ' GE-68 1.277E+OO 2. 743E+c:W 2.803E+OO NOT IDENT. AS-74 1. 744E+03 5.630E+03 5.684E+03 SHORT HLIF SE-75 l.437E-01 l.598E-01 l.725E-01 NOT IDENT. BR-77 2.638E+38 2.291E+39 O.OOOE+OO SHORT HLIF SR-82 2.920E+02 6.801E+02 6.927E+02 SHORT HLIF RB-83 3.605E-01 5.992E-01 6.209E-01 NOT IDENT. KR-85 4.580E-01 6.606E+OO 6.609E+OO NOT IDENT. SR-85 4.702E-02 7.055E-01 7.058E-01 NOT IDENT. RB-86 1.543E+04 3.501E+04 3.569E+04 SHORT HLIF Y-88 6.973E-02 l.498E-01 1.531E-01 NOT IDENT. Y-91 7.802E+Ol 6.323E+02 6.333E+02 NOT IDENT. NB-94 -9.474E-03 3.525E-02 3. 551E-02 NOT IDENT. NB-95 l.140E-01 8.681E-01 8. 696E-01 NOT IDENT. NB-95M 3.327E-01 2.339E+OO 2.343E+OO NOT IDENT. ZR-95 9.346E-01 1.593E+OO 1.648E+OO NOT IDENT. NB-97 -1.000E+41 1.809E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 2.320E+41 O.OOOE+OO SHORT HLIF M0-99 l.127E+32 1.921E+32 O.OOOE+OO SHORT HLIF TC-99M '1.000E+41 3.386E+41 O.OOOE+OO SHORT HLIF RH-101 -l.326E-02 2.623E-02 2.691E-02 NOT IDENT. RH-102 -3.004E-02 5.988E-02 6.139E-02 NOT IDENT. RU-103 -5.389E-01 5.149E+OO 5.155E+OO FAIL ABUN RH-106 2.099E-01 4.638E-01 4.733E-01 NOT IDENT. RU-106 2.099E-01 4.638E-01 4.733E-01 NOT IDENT. AG-108M 8.297E-03 2.274E-02 2.305E-02 NOT IDENT. AG-llOM -4.504E-02 9.874E-02 1.008E-01 NOT IDENT. SN-113 9.424E-03 2.025E-01 2.025E-01 NOT IDENT. CD-115 3.397E+37 4.158E+39 O.OOOE+OO SHORT HLIF SN-117M 2.569E+04 7.323E+04 7.414E+04 SHORT HLIF TE-123M 4 .133E-02 9.568E-02 9.747E-02 NOT IDENT. SB-124 -1.156E+00 1.637E+OO 1. 718E+OO NOT IDENT. SB-125 -1.212E-03 8.542E-02 8.542E-02 FAIL ABUN TE-125M 1. 087E+02 1.725E+02 1.793E+02 NOT IDENT. I-126 3.238E+05 8.383E+05 8.510E+05 SHORT HLIF SB-126 -3.794E+04 1.319E+06 1.319E+06 SHORT HLIF SB-127 -8.473E+21 3.079E+22 O.OOOE+OO SHORT HLIF I-131 1.985E+09 4.386E+09 4.477E+09 SHORT HLIF I-132 -1.000E+41 2.025E+42 O.OOOE+OO SHORT HLIF TE-132 1. 425E+2 6 4.303E+26 O.OOOE+OO SHORT HLIF BA-133 4. 513E-02 3.879E-02 4.380E-02 FAIL ABUN I-133 1.000E+41 2.110E+41 O.OOOE+OO SHORT HLIF CS-134 6.562E-02 5.105E-02 5. 901E-02 NOT IDENT. CS-135 9.733E-02 1. llOE-01 1.194E-01 NOT IDENT. I-135 1.000E+41 8.825E+41 O.OOOE+OO SHORT HLIF CS-136 9.445E+04 3.345E+05 3. 372E+05 SHORT HLIF BA-137M 5.086E-02 3.702E-02 4.354E-02 NOT IDENT. CS-137 5. 372E-02 3. 911E-02 4.600E-02 NOT IDENT. CE-139 3.480E-02 9. 031E-02 9.167E-02 NOT IDENT. BA-140 -6.689E+04 1.194E+06 1.194E+06 SHORT HLIF LA-140 -3.217E+05 4.193E+05 4.436E+05 SHORT HLIF CE-141 -1.922E+Ol 1.917E+Ol 2.103E+Ol NOT IDENT. CE-143 1.000E+41 1.699E+41 O.OOOE+OO SHORT HLIF CE-144 -2.232E-02 2.469E-01 2.471E-01 NOT IDENT. PM-144 -4.633E-02 6.025E-02 6.377E-02 NOT IDENT. PR-144 -4.041E+OO 5.232E+OO 5.540E+OO NOT IDENT. PM-146 1.016E-02 3.493E-02 3.523E-02 NOT IDENT. ND-147 -1. 229E+06 3.219E+07 3.219E'.t-07 SHORT HLIF PM-147 3.208E+02 5.400E+02 5.590E+02 NOT IDENT. PM-149 -1.762E+40 4.862E+40 O.OOOE+OO SHORT HLIF EU-150 8.107E-03 2.253E-02 2.282E-02 FAIL ABUN EU-152 4.306E-03 8.512E-02 8.514E-02 FAIL ABUN GD-153 -4.498E-02 9.532E-02 9.746E-02 NOT IDENT. EU-154 4.277E-02 1.118E-01 1.134E-01 NOT IDENT. EU-155 5.468E-02 7.015E-02 7.435E-02 NOT IDENT. TB-160 l.515E-01 1. 780E+OO 1. 781E+OO FAIL ABUN H0-166M 2.706E-03 5.909E-02 5.910E-02 NOT IDENT. TM-171 7.398E+OO 6.896E+OO 7.660E+OO FAIL ABUN HF-172 1. 406E-01 l.647E-01 l.764E-01 FAIL ABUN LU-172 5.697E-02 8.045E-02 8.445E-02 FAIL ABUN Page 4010of5809 LU-176 -4.754E-03 2.190E-02 2.200E-02 FAIL ABUN HF-181 5. 741E+OO 5.643E+OO 6.208E+OO FAIL ABUN TA-182 6.906E-02 1.102E+OO l.102E+OO FAIL ABUN RE-183 -3.469E-02 6.934E-01 6.936E-01 NOT IDENT. RE-184 1.807E+Ol 2.853E+Ol 2. 967E+Ol NOT IDENT. W-188 -5.588E+Ol 1.116E+02 l.144E+02 FAIL ABUN IR-192 l.113E-01 3.827E-01 3.860E-01 FAIL ABUN BI-207 -l.804E-02 4.081E-02 4.161E-02 FAIL ABUN BI-211 2.959E+OO 5.262E-01 1.434E+OO FAIL ABUN PB-211 5.811E-01 6.217E-01 NOT I!VENT. BI-212 1.362E+OO 5.800E-01 8.448E-01 FAIL ABUN RN-219 6.834E-02 3.175E-01 3.190E-01 FAIL ABUN RA-223 1.866E-02 5.773E-01 5.774E-01 FAIL ABUN AC-227 l.689E-01 2.0lOE-01 2.149E-01 FAIL ABUN TH-227 l.689E-01 2.0lOE-01 2.149E-01 FAIL ABUN TH-229 2.414E-01 3.559E-01 3.722E-01 FAIL ABUN TH-231 1.866E-02 5.773E-01 5.774E-01 FAIL ABUN PA-233 6 .112E-03 4.973E-02 4.980E-02 FAIL ABUN PA-234 2.434E-01 3.906E-01 4.057E-01 NOT IDENT. PA-234M 2.972E+OO 4.199E+OO 4.407E+OO NOT IDENT. U-235 6.915E-02 1.392E-01 l.426E-01 FAIL ABUN NP-237 6 .112E-03 4.973E-02 4.980E-02 FAIL ABUN NP-238 -1.000E+41 2 .115E+41 O.OOOE+OO SHORT HLIF NP-239 l.134E-01 l.605E-01 l.684E-01 FAIL ABUN PU-239 2.625E+02 4. 724E+02 4.870E+02 FAIL ABUN AM-241 -2.899E-02 3.799E-02 4.018E-02 NOT IDENT. CM-243 -l.313E-03 5.876E-02 5.876E-02 FAIL ABUN BK-247 4.518E-02 5. 727E-0'2 6.078E-02 FAIL ABUN CM-247 5.547E-03 3.085E-02 3.095E-02 FAIL ABUN CF-249 8.787E-03 3.316E-02 3.340E-02 NOT IDENT. CF-251 -4.824E-02 9.109E-02 9.365E-02 NOT IDENT. Page 4011of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 80.6820 87.09 73.3472 136.47 50.2703 45.60 78.6121 87.57 73.4542 140.51 0.0000 46.54 78.9743 88.03 73.5565 143.76 60.8629 49.72 0.0000 88.34 73.6254 144.24 63.8713 51. 35 58.3366 88.47 73.6543 145.44 76.8336 51. 87 76.4654 89.96 73.9830 152.43 72.9209 52.39 74.1385 1093.63 60.3400 153.25 0.0000 52.97 61. 7740 91.11 0.0000 323.87 71.1712 53.44 61.9020 92.59 69.3549 156.02 0.0000 54.07 62. 0727 93.35 69.5074 158.56 0.0000 57.36 0.0000 94.56 68.5873 159.00 52.6070 57.53 80.6626 94.65 67.4419 162.33 53.9567 57.98 76.1945 94.67 67.4460 162.66 0.0000 59.27 93.8785 94.87 67.4844 163.33 63.2365 59.32 93.8974 97.43 62.4067 165.86 64.5573 59.54 93.9817 98.43 67.8691 176.31 54.2923 60. 96 93.4804 98.44 67.8708 176.60 0.0000 61.17 93.5587 99.53 49.5093 177.52 66.9619 62.93 99.7037 100 .11 61.0994 181.07 0.0000 63.29 99.8432 102.03 63.1992 181.52 66.3713 63.58 99.9551 103.18 66.0728 184.41 79.0491 64.28 113.6404 103.37 66.1067 143.76 67.9053 66.73 108.3242 105.21 67.3273 193.51 46.2137 67.24 101.3475 105.31 67.3450 197.03 59.4463 125.81 101.5122 106.12 69.2878 198.01 58.4561 67.75 99.1398 106.47 70.2519 201.83 55.5423 69.67 89.3703 109.28 58. 9692 203.43 57.8652 70.83 112.3797 111. 00 76.5396 205.31 58.3993 72.81 117.2373 111. 76 0.0000 210.85 54.4777 72.87 130.2905 114.06 73.4540 215.65 55.6122 74.66 112.2532 116. 30 0.0000 222 .11 64.0015 74.82 112. 3138 116.74 59.1504 227.09 47.4967 74.97 112.3713 119.76 68.8906 227.38 50.9106 77 .11 113.1866 121.12 55.1032 228.16 0.0000 78.74 113. 7991 121. 22 55 .1162 228.18 52.1010 79.69 114 .1534 121.78 57.9949 116.74 52.1010 80.12 114. 3133 122.06 54.2892 235.69 62.5702 80.19 0.0000 122.92 64.7154 235. 96 62.5936 80.57 80.2192 123.07 65. 67 63 238.63 71.2504 81. 00 87.0248 265.00 75.1648 238.98 0.0000 81. 07 87.0446 125.81 52.8743 240.99 71.4794 81. 75 87.2343 127.23 79.5671 242.00 71.5768 83.79 77.6685 127.91 70.8360 244.70 50.9811 84.00 77.7198 129.30 71. 3745 252.40 0.0000 85.43 95.0375 131. 20 67.5364 252.80 40.9889 86.55 73.2265 133.02 60.4506 254.15 0.0000 86.79 73.2796 133.52 64.3593 256.23 38.8184 86.94 73.3138 136.00 53 .1168 260.90 0.0000 Page 4012 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 26.1572 355.39 0.0000 584.27 31. 4380 264.80 32.1078 356.01 26.2988 595.83 0.0000 265.00 28.5476 364.49 0.0000 427.87 25. 4111 268.22 25.4772 366.42 0.0000 602.52 0.0000 269.46 26.3137 372. 51 32.0618 604.72 19.1067 27.;0. 03 26.3325 375.05 34 .. 81.61 607.14 27.1083 271.23 26.3714 377.52 28.6328 609.32 24.4843 273.65 0.0000 356.01 39. 6011 610.33 24.4993 276.40 36.9922 388.16 31.6248 614.28 24.0244 277.37 41. 0609 388.63 0.0000 618.01 25.6846 277.60 41. 0723 391.69 31.7259 620.36 17.6830 278.00 41.0920 264.66 25.5841 621.93 17.1634 279.20 43. 5718 401.81 27.4396 630.19 0.0000 279.54 35.5173 402.40 31.1141 631. 29 21. 0361 279.70 35.5244 404.85 24.7615 633.25 24.8409 280.46 40.4053 410.95 31. 3472 634.78 0.0000 283.69 31.6375 413. 71 28.6494 635.95 24.8802 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 26.8246 423. 72 0.0000 645.85 19.5850 285.90 0.0000 427.09 28.9761 657.76 27.3905 287.50 34.2241 427.87 25.2537 657.90 0.0000 290.67 47.4365 433.94 21.6210 661.66 17.5690 293.27 0.0000 439.40 25.4949 664.57 0.0000 351. 93 36.1752 453.88 20.0618 666.33 0.0000 295. 96 36.2057 463.37 15.3997 666.50 0.0000 879.38 19.8076 468.07 20.2861 667.71 0.0000 299.98 28.1051 473.00 0.0000 677.62 19.9446 300.09 28.1085 475.06 24.2803 *685.70 0.0000 300.13 28.1099 476.78 17.5045 695.00 0.0000 301.36 36.4277 477.60 22.3809 696. 49 25.1917 302.85 31.5128 482.18 20.5057 696. 51 25.1926 256.23 23.2627 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 21.8431 306.78 39.9805 497.08 21. 7216 697.49 21. 844 7 308.46 33.3789 505.52 23.8423 702.65 30.3322 311. 90 38.5308 507.63 0.0000 706.68 21.3912 316.51 34.5145 511. 00 21. 9418 711. 68 22.5781 319.41 0.0000 514.00 23.9873 720. 70 0.0000 320.08 0.0000 514.00 23.9883 721. 93 0.0000 321. 04 39.7586 520.40 19.0765 722.78 20.4404 323.87 40.7266 520.69 0.0000 722.91 20.4419 325.23 43.3342 522.65 0.0000 723. 31 15.3347 328.76 0.0000 527.90 0.0000 724 .19 17.0465 333.37 29.5642 528.26 27.2593 727.33 19.3512 333.97 32.1548 529.59 17.1785 733.00 14.8424 334.37 28.3077 529.87 0.0000 735.93 14.8646 338.28 34.4507 531. 02 0.0000 ,333. 97 13.7324 338.32 34.4515 537.26 0.0000 739.50 0.0000 311.90 34. 5272 546.56 0.0000 747.24 19.5525 340.48 34.5272 552.55 16.9364 748.06 16.1089 340.55 0.0000 563.25 16.5404 752.31 24.2163 344.28 33.7941 569.33 29.0618 753.82 0.0000 345.93 32. 9817 946.00 30.1021 756.73 18.4922 351.06 40.1293 569.70 32.1832 756.80 18.4928 351. 93 40.1639 583.19 31. 4172 884.68 28.9998 Page 4013of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.8989 1274.44 13.5108 1620.50 4.7026 766.42 23.2284 1001.03 10.6358 1621. 92 6.5861 766.84 20.9099 1002.74 17.6920 1678.03 0.0000 772. 60 0.0000 1004.73 23.2390 1690.97 4.7864 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739 .* so 0.0000 1025.87 0. 0000. 1764.49 1.9488 778.90 20.1594 1028.54 0.0000 1063.66 17.5641 783.70 0.0000 1037.84 12.7509 1771. 35 1. 9521 785.37 19.3447 1038.76 0.0000 1791.20 0.0000 792.07 15.5268 631.29 15.7461 1808.65 0.0000 794.95 14.1348 1048.07 0.0000 1810.72 0.0000 795.86 14.1411 1049.04 9.8505 1836.06 0.9908 810.06 14.2383 1050.41 10.8409 810.29 12.4598 1063.66 12. 8762 344.28 12.4611 1077.00 0.0000 810.76 9.7922 1077.34 16.9243 815.77 0.0000 1085.87 9. 9872 1048.07 0.0000 1093.63 12.0183 832.01 19.7817 1099.45 15.0549 834.85 16.2065 1112. 07 18.1494 835.71 16.2131 1112. 84 28.2393 836.80 0.0000 1115. 54 14. 5371 846.75 0.0000 1120.29 15.1685 846.77 13.5800 1120.55 15.1703 856.80 0.0000 1221. 41 9. 7113 860.56 13.6661 1129.67 7.1025 871.09 17.0876 1131.51 0.0000 873.19 11. 7281 1147.95 0.0000 875.33 0.0000 1173.23 11. 5384 879.38 11. 7 605 1177.95 18.5735 880.51 13. 2372 1189.05 15.5365 883.24 14.7261 1204.77 19.7839 884.68 19.3401 1221. 41 20.9412 889.28 11. 0739 1231.02 16.8066 894.76 13.8757 1235.36 0.0000 898.04 16.6750 1238.28 17.8996 900.72 21.3316 1260.41 0.0000 903.28 11.1420 1271.87 11.7083 911. 20 16.7701 1274.44 9. 5872 912.08 16.7767 1274.54 9.5878 923.98 0.0000 1291. 59 9.6394 926.50 10.5034 1298.22 0.0000 929 .11 17.8380 1312 .11 0.0000 937.49 16.9590 1332.49 6.9422 944.13 0.0000 1362.66 0.0000 946.00 11.3463 1365.19 7.6686 949.00 21. 7738 1368.63 0.0000 667. 71 0.0000 1384.29 6.6105 962.31 16.7535 1408.01 5.5472 964.08 9.1450 1457.56 0.0000 966 .17 0.0000 1460.82 2.7032 911. 20 3.0544 1489.16 5.4492 968.97 3.0544 1505.03 10.0343 983.53 0.0000 1584.12 9.3169 984.45 0.0000 1596.21 0.0000 Page 4014of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:03:55.47 ********************************************************************************
  • Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM28.CNF;265 Background date : Z-OCT-2016 11:01:35. Sample date 7-DEC-2015 13:28:00. Acquisition date : 3-0CT-2016 07:00:55. Sample ID G405235048 Sample quantity 1.31577E+02 GRAM Detector name : GAM28 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.46 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 2 0 2 2 0 0 0 0 0 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4015of5809 Energy 63.54* 75.02* 77.22 79.44 87.82 92. 89* 95.17 105.77 115 .15 128.10 140.47* 144.18*

185.94* 238.97* 241.98 271.68 295.65 338.88 352.49* 428.57 496.82 510.95* 583.58* 599.58 609.81* 653.27 662.11* 679.99* 727.75 783.28 795.70 8 61. 65 912.02* 955.13 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 30 110 231 52 69 58 25 18 30 15 18 18 65 416 118 35 148 84 304 23 14 71 136 32 187 17 508 16 28 13 35 12 88 17 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 134 164 123 121 247 171 122 100 139 128 134 86 174 83 66 97 110 78 60 50 24 59 19 34 39 9 49 17 16 22 9 18 32 22 1. 88 1. 35 1. 22 1. 36 3.04 1. 25 1.12 1. 24 0.65 1. 28 1. 82 1. 36 1. 59 1. 39 1. 57 2.26 1. 50 0.97 1. 56 4.00 1. 08 1. 78 1. 65 3.31 1. 98 1. 37 1. 84 0.80 2.07 1. 73 3.72 0.58 1. 56 2.23 127.16 150 .13 154.53 158.97 175.75 185.90 190.46 211. 67 230.46 256.36 281.13 288.55 372 .14 478.27 484.30 543.75 591. 71 678.25 705.49 857.75 994.35 1022.64 1168. 00 1200.03 1220.52 1307. 50 1325.18 1360. 96 1456.57 1567.70 1592.56 1724.56 1825.38 1911. 65 124 145 145 145 172 181 181 208 227 254 275 286 367 474 474 536 586 672 698 851 990 1014 1163 1192 1215 1303 1318 1357 1452 1562 1587 1721 1820 1902 7 8.42E-03 67.7 19 3.06E-02 22.6 1.09E+OO 19 6.41E-02 10.8 19 1. 44E-02 47 .1 10 l.91E-02 44.3 13 l.62E-02 41.8 7.13E-01 13 6.89E-03 86.9 6 5.13E-03 88.7 10 8.20E-03 77.7 8 4.25E-03129.8 9 4.97E-03120.5 6 5.03E-03 87.4 11 1.81E-02 42.4 17 1.15E-01 6.3 4.18E-01 17 3.28E-02 17.7 12 9.61E-03 59.2 11 4.12E-02 16.0 10 2.34E-02 22.3 16 8.44E-02 8.3 12 6.45E-03 64.7 8 3.81E-03 69.2 16 l.98E-02 30.7 11 3. 77E-02 10. 8 14 8.93E-03 42.7 12 5.21E-02 10.1 8 4. 59E-03 41.1 15 1.41E-01 5.4 8 4.47E-03 52.7 10 7.85E-03 31.9 10 3.58E-03 74.1 12 9.81E-03 23.9 9 3.32E-03 72.7 14 2.45E-02 17.4 15 4.66E-03 66.2 Peak Search Report (continued) Page : 2 Sample ID : G405235048 Acquisition date : 3-0CT-2016 07:00:55 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969. 93 49 23 2. 70 1941. 28 1936 11 1.37E-02 24.0 36 0 1000.35* 23 0 2.62 2002.17 1996 12 6.37E-03 23.9 37 0 1120.64* 64 15. 2.10 2242.92 2235 15 1.78E-02 18.4 38 0 1461.76* 397 3 2.14 2925.67 2919 13 l.lOE-01 5.1 39 0 1510.25 9 4 1.43 3022. 72 3018 8 2.50E-03 50.9 40 0 1517.03 5 5 0.72 3036.30 3030 10 1. 39E-03 94. 9 41 0 1631.84 12 0 0.62 3266.08 3261 10 3.33E-03 28.9 42 0 1766.05* 36 7 1.49 3534.71 3527 12 1.0lE-02 22.3 Flag: "*" = Peak area was modified by background subtraction Page 4016of5809

  • VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:03:57 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 13:28:00 G405235048 Acquisition date : Sample quantity Sample geometry + Detector geometry: 3-0CT-2016 07:00:55 131. 58 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA28 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 U-235 143.76 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 4017 of 5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86.94 SN-126 87.57 CD-109 88.03 RA-224 240.99 CE-141 145.44 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.46 10.00 0.00 % Peak Energy 0.0%

I Nuclide Line Activity Report Page : 2 Sample ID : G405235048 Acquisition date 3-0CT-2016 07:00:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460. 10.66* 1.237E+OO 1.636E+Ol 1. 10.27 OK RU-103 497.08 91.00* 2.878E+OO 3.079E-02 6.229E+OO 138.39 OK 610.33 5.76 2.455E+OO 7.687E+OO l.555E+03 20.25 OK CD-109 88.03 3.70* 5.460E+OO 1.205E+OO 1.893E+OO 167.38 OK SN-126 64.28 9.60 3.030E+OO 7.008E-01 7.008E-01 135.48 OK 86.94 8.90 5.460E+OO 5.008E-01 5.008E-01 167.38 OK 87.57 37.00* 5.460E+OO 1.205E-01 1. 205E-01 167.38 OK BA-137M 661.66 89.90* 2.305E+OO 1.413E+OO 1.440E+OO 10.79 OK CS-137 661.66 85.10* 2.305E+OO 1.493E+00 1.522E+OO 10.79 OK CE-141 145.44 48.29* 6.589E+OO 9.228E-03 5.623E+OO 733.36 OK EU-155 86.55 30.70 5.460E+OO 1.452E-01 1.637E-01 167.38 OK 105.31 21.10* 6.332E+OO 9.0lOE-02 l.016E-01 177.47 OK TL-208 277.37 6.60 4.566E+OO Line Not Found Absent 583.19 85.00* 2.539E+OO 3.661E-01 3.661E-01 21. 63 OK 860.56 12.50 1.886E+OO 2.867E-01 2.867E-01 145.48 OK BI-211 72. 87 1. 23 4.138E+OO Line Not Found Absent 351.06 12.92* 3.781E+OO 6.364E-01 6.364E-01 184.21 OK PB-212 74.82 10.28 4.364E+OO 9.956E-01 9.956E-01 77.00 OK 77 .11 17.10 4.583E+OO 1.957E+OO l.957E+00 21. 68 OK 238.63 43.60* 5.lOOE+OO 1.156E+OO 1.156E+OO 12.51 OK 300.09 3.30 4.295E+OO Line Not Found Absent BI-214 609.32 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 OK 1120.29 14.92 1.539E+00 1. 546E+OO 1.546E+OO 36. 87 OK 1764.49 15.30 1.045E+OO Line Not Found Absent PB-214 74.82 5.80 4.343E+00 Line Not Found <<INT Reject 77 .11 9.70 4.583E+OO 3.450E+OO 3. 451E+OO 21. 68 OK 87.09 3.41 5.409E+OO Line Not Found <<INT Reject 242.00 7.25 5.054E+OO Line Not Found <<INT Reject 295.22 18.42 4.345E+OO 1.128E+OO 1.129E+OO 31. 95 OK 351. 93 35.60* 3.786E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 OK 1120.29 14.92 1.539E+OO 1.546E+OO 1.546E+OO 36.87 OK 1764.49 15.30 1.045E+00 Line Not Found Absent RA-224 240.99 4.10* 5.054E+OO 1.526E+OO 1. 52 6E+OO 91. 57 OK RA-226 609.32 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 OK 1120.29 14.92 1.539E+OO 1.546E+OO 1. 54 6E+OO 36.87 OK 1764.49 15.30 1.045E+OO Line Not Found Absent AC-228 105.21 1.10 6.332E+OO l.728E+00 1.728E+OO 177.47 OK 338.32 11. 27 3. 901E+OO 1.159E+OO l.159E+00 44.69 OK 794.95 4.25 2.004E+OO 2.358E+OO 2.358E+OO 47.73 OK 835.71 1. 61 l.930E+OO Line Not Found Absent 911. 20 25.80* 1. 806E+OO 1.067E+OO 1.067E+OO 34.78 OK 968. 97 15.80 1.723E+OO l.018E+OO 1.018E+OO 47.91 OK RA-228 105.21 1.10 6.332E+OO 1. 728E+OO 1.728E+OO 177.47 OK 338.32 11. 27 3.901E+OO 1.159E+OO 1.159E+OO 44.69 OK 794.95 4.25 2.004E+OO 2.358E+OO 2.358E+OO 47.73 OK 835.71 1. 61 1.930E+OO Line Not Found Absent 911.20 25.80* 1.806E+OO 1.067E+OO 1.067E+OO 34.78 OK 968.97 15.80 1.723E+OO 1.018E+OO 1.018E+OO 47.91 OK Page 4018of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235048 Acquisition date 3-0CT-2016 07:00:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 4.364E+00 9.956E-01 9.956E-01 77.00 OK 77 .11 17.10 4.583E+OO l.957E+OO l.957E+OO 21.68 OK 238.63 43.60* 5.lOOE+OO l.156E+OO l.156E+OO 12.51 OK 300.09 3.30 4.295E+OO Line Not Found Absent TH-230 609.32 45.49* 2.455E+OO 9.734E-01 9.734E-01 20.25 OK 1120. 29 14.92 l.539E+OO *1. 546E+OO l.546E+OO 36.87 OK 1764.49 15.30 l.045E+OO Line Not Found Absent TH-232 105.21 1.10 6.332E+OO 1. 728E+OO l.728E+OO 177.47 OK 338.32 11.27 3.901E+OO l.159E+OO l.159E+OO 44.69 OK 835.71 1. 61 l.930E+OO Line Not Found Absent 911.20 25.80* l.806E+00 l.067E+OO l.067E+OO 34.78 OK 968. 97 15.80 1. 723E+OO l.018E+OO l.018E+OO 47.91 OK TH-234 63.29 3.70* 3.030E+OO l.818E+OO l.818E+OO 135.48 OK 92.59 4.23 5.779E+OO l.570E+OO l.570E+OO 83.57 OK U-234 609.32 45.49* 2.455E+OO 9.734E-01 9.734E-01 20.25 OK 1120.29 14.92 l.539E+OO l.546E+OO 1. 546E+OO 36.87 OK 1764.49 15.30 l.045E+OO Line Not Found Absent U-235 89. 96 3.47 5.602E+OO Line Not Found Absent 93.35 5.60 5.779E+OO l.186E+OO l.186E+OO' 83.57 OK 143.76 10.96* 6.593E+OO Line Not Found <<INT Reject 163.33 5.08 6.352E+OO 'Line Not Found Absent 185.72 57.20 5.981E+OO 1.197E-01 1.197E-01 84.89 OK 205.31 5.01 5.647E+OO Line Not Found Absent U-238 63.29 3.70* 3.030E+OO 1.818E+OO 1.818E+OO 135.48 OK 92.59 4.23 5.779E+OO 1.570E+OO 1.570E+OO 83.57 OK AM-243 43.53 5.90 4.883E-01 Line Not Found Absent 74.66 67.20* 4.364E+OO 1.523E-01 1.523E-01 77.00 OK ANH-511 511. 00 100.00* 2.816E+OO 1.484E-01 1.484E-01 61.42 OK Flag: "*" = Keyline Page 4019of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:03:58.74 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l *
  • Acquisition date 3-0CT-2016 07:00:55 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.46 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:28:00 Analyst initials: MXRl *
  • Sample ID G405235048 Sample Quantity 1.3158E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.636E+Ol 1.647E+OO RU-103 6.229E+00 8.448E+OO CD-109 1.893E+OO 3.105E+OO SN-126 1.205E-01 1. 97 6E-01 BA-137M l.440E+OO 1.523E-01 CS-137 1.522E+OO 1.609E-01 CE-141 5.623E+OO 4. 041E+Ol EU-155 l.016E-01 1. 767E-01 TL-208 3.661E-01 7.763E-02 BI-211 6.364E-01 1.149E+OO PB-212 1.156E+OO 1.417E-01 BI-214 9.737E-01 1.932E-01 PB-214 1.360E+OO 2. 215E-01 RN-222 9.737E-01 l.932E-01 RA-224 1.526E+OO 1.370E+OO RA-226 9.737E-01 1.932E-01 AC-228 1.067E+OO 3.635E-01 RA-228 1.067E+OO 3 .. 635E-01 TH-228 1.156E+OO 1.417E-01 TH-230 9.734E-01 l.932E-01 TH-232 l.067E+00 3.635E-01 TH-234 1. 818E+OO 2.414E+OO U-234 9.734E-01 1. 932E-01 U-235 1.603E-01 2.747E-01 U-238 1.818E+OO 2.414E+OO AM-243 1.523E-01 1.149E-01 ANH-511. l.484E-01 8.936E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4020 of 5809 Key-Line Activity (pCi/GRAM -l.122E+OO 3.668E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigrna) 1.683E+Ol 4.882E-02 1. 960E+41 MDA (pCi/GRAM 6.664E-01 1.105E+Ol 2.489E+OO 1.593E-01 6.579E-02 6.950E-02 5.007E+Ol 2.334E-01 7.269E-02 3.563E-01 1.140E-01 1. 38 6E-01 3.598E-01 1. 386E-01 1. 222E+OO 1. 38 6E-01 2.743E-01 2.743E-01 1.140E-01 l.385E-01 2.743E-01 2.644E,+00 1.385E-01 4. 061E-01 2.644E+OO 9.726E-02 5.887E-02 MDA (pCi/GRAM 3.086E+Ol 1. 075E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 6.615E-03 2.369E-02 6.016E-02 NOT IDENT. SC-46 7.763E-02 4.141E-01 8.393E-01 FAIL ABUN V-48 O.OOOE+OO 1. 755E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4. 886E+o2 O.OOOE+OO SHORT HLIF MN-54 2. 311E-02 6.839E-02 1.404E-01 NOT IDENT. C0-56 4.028E-Ol 5 .151E-01 l .116E+OO NOT IDENT. MN-56 O.OOOE+OO l.284E+41 O.OOOE+OO SHORT HLIF C0-57 -4.445E-03 5.719E-02 1. OllE-01 NOT IDENT. C0-58 5.473E-02 5.371E-01 l.103E+OO NOT IDENT. FE-59 -2. 6.836E+OO 1.254E+Ol NOT IDEWT. C0-60 1.241E-02 3.878E-02 8.247E-02 NOT IDENT. ZN-65 7. lllE-02 1.912E-01 3.588E-01 NOT IDENT. GE-68 -2.365E+OO 2.651E+OO 4. 572E+OO NOT IDENT. AS-73 -3.549E+OO 1.079E+Ol l.932E+Ol NOT IDENT. AS-74 0.000E+OO 8.245E+03 O.OOOE+OO SHORT HLIF SE-75 -7.304E-02 2. l 72E-01 4.040E-01 NOT IDENT. BR-77 0.000E+OO 3.316E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.583E+o2 0.000E+OO SHORT HLIF RB-83 4.221E-01 7.417E-01 l.486E+00 NOT IDENT. KR-85 8.618E+OO 9.504E+OO 1. 757E+Ol NOT IDENT. SR-85 9.158E-01 1.013E+OO 1. 873E+OO NOT IDENT. RB-86 O.OOOE+OO 3.268E+04 O.OOOE+OO SHORT HLIF Y-88 -2.699E-02 2.250E-01 4.790E-01 NOT IDENT. Y-91 -2.762E+02 5.997E+02 1. 072E+03 NOT IDENT. NB-94 3.432E-02 3.332E-02 7.074E-02 NOT IDENT. NB-95 -1.003E+OO 1.043E+OO 1. 810E+OO NOT IDENT. NB-95M -3.520E-01 3. l 72E+OO 5.348E+OO NOT IDENT. ZR-95 5.605E-01 l.458E+00 3.059E+OO NOT IDENT. NB-97 O.OOOE+OO l.195E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 8.485E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.715E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 2.590E-02 6.588E-02 7. lllE-02 FAIL ABUN RH-102 4.350E-02 6.814E-02 1. 372E-01 NOT IDENT. RH-106 5.829E-01 4.841E-01 1. 079E+OO NOT IDENT. RU-106 5.829E-01 4.841E-01 1.079E+OO NOT IDENT. AG-108M 5.930E-03 3.257E-02 5.977E-02 NOT IDENT. AG-llOM -3 .118E-02 l.085E-01 2.057E-01 NOT IDENT. SN-113 6. 313E-02 2.706E-01 5.199E-01 NOT IDENT. CD-115 O.OOOE+OO 4.428E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO l.246E+05 O.OOOE+OO SHORT HLIF TE-123M -3.515E-02 l.623E-01 2.787E-01 NOT IDENT. SB-124 -2.351E+OO 1.881E+OO 9.527E-01 NOT IDENT. SB-125 1. 761E-01 2.234E-01 2.451E-01 FAIL ABUN TE-125M 9.495E+Ol 3.277E+02 5.999E+02 NOT IDENT. I-126 O.OOOE+OO l.031E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.348E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.857E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 6.345E+09 0.000E+OO SHORT HLIF I-132 O.OOOE+OO 1. 781E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4. 963E+26 O.OOOE+OO SHORT HLIF BA-133 -9.114E-03 4.620E-02 7.656E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 7.228E-02 1.316E-01 FAIL ABUN CS-135 -3.619E-02 1.493E-01 2.500E-01 NOT IDENT. I-135 O.OOOE+OO 8.777E+40 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.365E+05 O.OOOE+OO SHORT HLIF CE-139 -3.694E-03 1.241E-01 2.395E-01 NOT IDENT. BA-140 0.000E+OO 1.464E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.043E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 5.094E-01 3.990E-01 7.839E-01 FAIL ABUN PM-144 1.300E-02 6.183E-02 l.176E-Ol NOT IDENT. PR-144 1.113E+OO 5.371E+OO 1.021E+Ol NOT IDENT. PM-146 -l.524E-02 5. 696E-02 1.027E-01 NOT IDENT. ND-147 O.OOOE+OO 3.747E+07 O.OOOE+OO SHORT HLIF PM-147 -5.018E+o2 9.528E+02 1.622E+03 NOT IDENT. PM-149 O.OOOE+OO 7.246E+40 O.OOOE+OO SHORT HLIF. EU-150 l.114E-04 3.134E-02 5.312E-02 FAIL ABUN EU-152 1.540E-02 l.126E-01 2.141E-01 NOT IDENT. GD-153 6.185E-02 2.184E-01 3.750E-Ol NOT IDENT. EU-154 8.987E-02 1.196E-01 2.634E-01 NOT IDENT. TB-160 -1.076E+OO 1. 991E+OO 3.630E+OO FAIL ABUN H0-166M l.626E-03 5.814E-02 l.091E-01 FAIL ABUN TM-171 -9.139E+OO 2.562E+Ol 4.581E+Ol NOT IDENT. HF-172 -3.073E-03 3.026E-01 4.930E-01 FAIL ABUN LU-172 3.354E-02 8.580E-02 1. 765E-01 FAIL ABUN LU-176 -l.213E-02 2.829E-02 5.151E-02 FAIL ABUN Page 4021 of 5809 HF-.181 -1.503E+OO 5. 321E+OO 9.594E+00 NOT IDENT. TA-182 8.899E-02 8.587E-01 l.722E+00 FAIL ABUN RE-183 4.972E-01 3.302E+OO 6.224E+OO NOT IDENT. RE-184 1. 600E+Ol 3.386E+Ol 7.076E+Ol NOT IDENT. W-188 -7.076E+Ol 1.374E+02 2.214E+02 FAIL ABUN IR-192 3.741E-01 5.436E-01 1.087E+OO FAIL ABUN HG-203 -l.814E-02 2.738E+OO 5.194E+OO NOT IDENT. BI-207 -1. 596E-02 4. 596E-02 8.598E-02 FAIL ABUN PB-210 1.340E+OO 4.413E+OO 8.351E+OO NOT IDENT. PB-211 8.252E-01 7.860E-01 1.619E+OO FAIL ABUN. BI-212 1.132E+OO 7.082E-01 l.288E+OO FAIL ABUN RN-219 3.568E-02 4.606E-01 8.673E-01 FAIL ABUN RA-223 1.968E-01 6.763E-01 1.309E+OO FAIL ABUN AC-227 -2.699E-02 2.495E-01 4.721E-01 FAIL ABUN TH-227 -2.699E-02 2.495E-01 4. 721E-01 FAIL ABUN TH-229 9.613E-02 5.592E-01 1.081E+OO FAIL ABUN PA-231 l.950E-01 5. 331E-01 1.031E+OO NOT IDENT. TH-231 1. 968E-01 6.763E-01 1.309E+OO FAIL ABUN PA-233 -3.749E-02 6.581E-02 1.183E-01 NOT IDENT. PA-234 3.449E-02 2.443E-01 5.059E-01 FAIL ABUN PA-234M 9.084E+OO 4.260E+OO 1.009E+Ol FAIL ABUN NP-237 -3.749E-02 6.581E-02 1.183E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 3.553E-02 2.635E-01 4. 781E-01 FAIL ABUN PU-239 2.347E+02 5. 972E+02 6.686E+02 FAIL ABUN AM-241 -5.943E-02 1.515E-01 2. 721E-01 NOT IDENT. CM-243 -7.438E-02 1.250E-01 l.942E-01 NOT IDENT. EK-247 -3.949E-02 7.927E-02 1.377E-01 FAIL ABUN CM-247 -1. lllE-02 4.322E-02 7.862E-02 NOT IDENT. CF-249 -4.551E-03 4.584E-02 8.491E-02 NOT IDENT. CF-251 3.599E-02 l.250E-01 2.459E-01 NOT IDENT. Page 4022 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:03:56.57 Nuclide Line Activity Report Nuclide .Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 378 10.66* 1.237E+OO 1.636E+Ol l.636E+Ol 10.27 RU-103 497.08 14 91.00* 2.878E+OO 3.079E-02 6.229E+OO 138.39 610.33 191 5.76 2.455E+OO 7.687E+OO 1.555E+03 20.25 CD-109 88.03 79 3.70* 5.460E+OO 2.245E+OO 3.527E+OO 88.60 SN-126 64.28 36 9.60 3.030E+OO 7.008E-01 7.008E-01 135.48 86.94 79 8.90 5.460E+OO 9.332E-01 9.332E-01 88.60 87.57 79 37.00* 5.460E+OO 2.245E-01 2.245E-01 88.60 BA-137M 661.66 513 89.90* 2.305E+OO 1.413E+OO 1.440E+OO 10.79 CS-137 661.66 513 85.10* 2.305E+OO l.493E+OO 1.522E+OO 10.79 CE-141 145.44 20 48.29* 6.589E+OO 3.639E-02 2.217E+Ol 174.83 EU-155 86.55 79 30.70 5.460E+OO 2.705E-01 3. 051E-01 88.60 105.31 21 21.10* 6.332E+OO 9.0lOE-02 1.016E-01 177.47 TL-208 277.37 ------6.60 4.566E+OO ------Line Not Found ------583.19 139 85.00* 2.539E+OO 3. 661E-01 3.661E-01 21. 63 860.56 12 12.50 1.886E+OO 2.867E-01 2.867E-01 145.48 BI-211 72.87 ------1. 23 4 .138E+OO ------Line Not Found ------351.06 321 12.92* 3.781E+OO 3.746E+OO 3.746E+OO 16.62 PB-212 74.82 128 10.28 4.364E+OO 1.632E+OO l.632E+OO 45.28 77 .11 269 17.10 4.583E+OO l.957E+OO 1.957E+OO 21. 68 238.63 450 43.60* 5.lOOE+OO 1.156E+OO 1.156E+00 12.51 300.09 ------3.30 4.295E+OO ------Line Not Found ------BI-214 609.32 191 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 1120.29 62 14.92 1.539E+OO 1.546E+OO 1. 546E+OO 36.87 1764.49 ------15.30 1.045E+OO ------Line Not Found ------PB-214 74.82 128 5.80 4.364E+OO 2.893E+OO 2.894E+OO 45.28 77 .11 269 9.70 4.583E+OO 3.450E+OO 3. 451E+OO 21.68 87.09 79 3.41 5.460E+OO 2.436E+OO 2.436E+OO 88.60 242.00 128 7.25 5.054E+OO 1.992E+OO 1.992E+OO 35.32 295.22 158 18.42 4.345E+oo 1.128E+OO 1.129E+OO 31. 95 351. 93 321 35.60* 3.781E+OO 1.359E+OO 1.360E+OO 16.62 RN-222 609.32 191 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 1120.29 62 14.92 1.539E+OO 1.546E+OO 1.546E+OO 36.87 1764.49 ------15.30 1.045E+OO ------Line Not Found ------RA-224 240.99 128 4.10* 5.054E+OO 3.522E+OO 3.522E+OO 35.32 RA-226 609.32 191 45.49* 2.455E+OO 9.734E-01 9.737E-01 20.25 1120.29 62 14.92 1.539E+OO 1.546E+OO 1. 546E+OO 36.87 1764.49 ------15.30 1.045E+OO ------Line Not Found ------AC-228 105.21 21 1.10 6.332E+OO 1. 728E+OO 1.728E+OO 177.47 338.32 89 11. 27 3.901E+00 l.159E+OO 1.159E+OO 44.69 794.95 35 4.25 2.004E+OO 2.358E+OO 2.358E+OO 47.73 835.71 ------1. 61 1.930E+OO ------Line Not Found ------911. 20 87 25.80* 1.806E+OO l.067E+OO 1.067E+OO 34.78 968.97 49 15.80 1. 723E+OO 1.018E+OO 1.018E+OO 47.91 RA-228 105.21 21 1.10 6.332E+OO 1. 728E+OO 1. 728E+OO 177.47 338.32 89 11. 27 3. 901E+OO 1.159E+OO 1.159E+OO 44.69 794.95 35 4.25 2.004E+OO 2.358E+OO 2.358E+OO 47.73 835. 71 ------1. 61 1.930E+OO ------Line Not Found ------Page 4023 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235048 Acquisition date 3-0CT-2016 07:00:55 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911.20 87 25.80* l.806E+OO 1. 067£+00 l.067E+OO 34.78 968. 97 49 15.80 l.723E+OO l.018E+OO l.018E+OO 47.91 TH-228 74.82 128 10.28 4.364E+OO l.632E+OO l.632E+OO 45.28 77 .11 269 17.10 4.583E+OO l.957E+OO l.957E+OO 21. 68 238.63 450 43.60* 5.lOOE+OO l.156E+OO l.156E+OO 12.51 300.09 ------3.30 4.295E+OO ------Line Not Found ------TH-230 609.32 191 45.49* 2.455E+OO 9.734E-01 9.734E-01 20.25 1120.29 62 14.92 l.539E+OO l.546E+OO l.546E+OO 36.87 1764.49 ------15.30 l.045E+OO ------Line Not Found ------TH-232 105.21 21 1.10 6.332E+OO l.728E+OO l.728E+OO 177.47 338.32 89 11. 27 3.901E+OO l.159E+OO l.159E+00 44.69 835. 71 ------1. 61 1. 930E+00 ------Line Not Found ------911. 20 87 25.80* 1. 806E+OO l.067E+OO l.067E+OO 34.78 968.97 49 15.80 l.723E+OO l.018E+OO l.018E+00 47.91 TH-234 63.29 36 3.70* 3.030E+00 l.818E+00 l.818E+OO 135.48 92.59 67 4.23 5.779E+OO 1. 570E+OO l.570E+OO 83.57 U-234 609.32 191 45.49* 2.455E+OO 9.734E-01 9.734E-01 20.25 1120.29 62 14.92 1.539E+OO l.546E+OO l.546E+OO 36.87 1764.49 ------'15.30 1.045E+OO ------Line Not Found ------U-235 89. 96 ------3.47 5.602E+OO ------Line Not Found ------93.35 67 5.60 5.779E+OO l.186E+OO 1.186E+OO 83.57 143.76 20 10. 96* 6.589E+OO l.603E-01 l.603E-01 174.83 163.33 ------5.08 6.352E+OO ------Line Not Found ------185. 72 72 57.20 5.981E+OO l.197E-01 l.197E-01 84.89 205.31 ------5.01 5.647E+OO ------Line Not Found ------U-238 63.29 36 3.70* 3.030E+OO l.818E+OO l.818E+OO 135.48 92.59 67 4.23 5.779E+OO l.570E+OO l.570E+OO 83.57 AM-243 43.53 ------5.90 4.883E-01 ------Line Not Found ------74.66 128 67.20* 4.364E+00 2.497E-01 2.497E-01 45.28 ANH-511 511. 00 73 100.00* 2.816E+OO l.484E-01 l.484E-01 61. 42 Flag: "*" Key line Page 4024 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235048 Acquisition date 3-0CT-2016 07:00:55 Total number of lines in spectrum 42 Number of unidentified lines 6 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 RU-103 CD-109 SN-126 BA-137M CS-137 CE-lL.11 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 39.26D 461. 40D 2.30E+05Y 30.08Y 30.08Y 32. 51D 4.75Y 1. 41E+l0Y 7.04E+08Y 1.41E+10Y 1600. OOY 1600. OOY 1600. OOY l.41E+10Y 1'600.00Y l.41E+l0Y 1.41E+l0Y 1. 41E+10Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 202. 1. 57 1. 00 1. 02 1. 02 609. 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity
  • Uncorrected pCi/GRAM 1.636E+Ol 3.079E-02 2.245E+OO 2.245E-01 l.413E+OO 1.493E+OO 3.639E-02 9.0lOE-02 3.661E-01 3.746E+OO 1.156E+OO 9.734E-01 1.359E+OO 9.734E-01 3.522E+OO 9.734E-01 1.067E+OO 1.067E+OO l.156E+OO 9.734E-01 1.067E+OO 1. 818E+OO 9.734E-01 1. 603E-01 1.818E+OO 2.497E-01 l.484E-01 4.546E+Ol 4.546E+Ol Decay Corr pCi/GRAM l.636E+Ol 6.229E+OO 3.527E+OO 2.245E-01 l.440E+OO 1.522E+OO 2.217E+Ol 1.016E-01 3.661E-01 3.746E+OO 1.156E+OO 9.737E-01 l.360E+OO 9.737E-01 3.522E+OO 9.737E-01 1.067E+00 1.067E+OO l.156E+OO 9.734E-01 1.067E+OO 1.818E+OO 9.734E-01 1.603E-01 1.818E+OO 2.497E-01 1.484E-01 7.515E+Ol 7.515E+Ol 85. 71% Decay Corr 2-Sigma Error 0.168E+Ol 8.620E+OO 3.125E+00 1. 989E-01 0.155E+00 0.164E+00 3.877E+Ol l.803E-01 0.792E-01 0.622E+OO 0.145E+OO l.972E-01 0.226E+OO 1.972E-01 1.244E+OO 1. 972E-01 0.371E+OO 0. 371E+OO 0.145E+00 1. 971E-01 0. 371E+OO 2.464E+OO 1. 971E-01 2.803E-01 2.464E+OO l.131E-01 0.912E-01 "M" Manually accepted 2-Sigma %Error 10.27 138. 39 88.60 88.60 10.79 10.79 174.83 177.47 21. 63 16.62 12.51 20.25 16.62 20.25 35.32 20.25 34.78 34.78 12.51 20.25 34.78 135.48 20.25 174.83 135.48 45.28 61. 42 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4025 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235048 Acquisition date : 3-0CT-2016 07:00:55 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 2 79.44 60 141 1. 36 158.97 145 19 1'. 44E-02 94.1 4.79E+OO T 2 95.17 29 140 1.12 190.46 181 13 6.89E-03 **** 5.90E+OO T 0 115 .15 34 158 0.65 230.46 227 10 8.20E-03 **** 6.55E+OO T 0 128.10 17 .144 1. 28 256.36 254 8 4.25E-03 **** 6.65E+OO T 0 140.47 20 150 1. 82 281.13 275 9 4.97E-03 **** 6.62E+OO T 0 271.68 37 105 2.26 543.75 536 12 9.61E-03 **** 4.64E+00 T 0 428.57 24 52 4.00 857.75 851 12 6.45E-03 **** 3.23E+OO T 0 599.58 33 34 3.31 1200.03 1192 14 8.93E-03 85.4 2.49E+OO T 0 653.27 17 10 1. 37 1307.50 1303 8 4.59E-03 82.1 2.33E+OO 0 679.99 16 17 0.80 1360. 96 1357 8 4.47E-03 **** 2.26E+OO 0 727.75 28 16 2.07 1456.57 1452 10 7.85E-03 63.9 2.14E+OO T 0 783 .. 28 13 22 1. 73 1567.70 1562 10 3.58E-03 **** 2.03E+OO T 0 955.13 16 22 2.23 1911. 65 1902 15 4.66E-03 **** 1. 74E+OO T 0 1000.35 22 0 2. 62 2002.17 1996 12 6.37E-03 47.8 1.68E+OO T 0 1510.25 9 4 1. 43 3022.72 3018 8 2.50E-03 **** l.20E+00 0 1517. 03 5 5 0.72 3036.30 3030 10 1. 39E-03 **** l.20E+OO 0 1631.84 11 0 0.62 3266.08 3261 10 3.33E-03 57.7 l.12E+OO 0 1766.05 34 7 1. 49 3534.71 3527 12 1. OlE-02 44.6 1. 04E+OO Flags: "T" Tentatively associated Page 4026 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:04:10.39 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l *
  • Acquisition date 3-0CT-2016 07:00:55 Sensitivity 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.46 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:28:00 Nuclide Library : SOLID *
  • Sample ID G405235048 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : l.3158E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 RU-103 CD-109 SN-126 BA-137M CS-137 CE-141 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.747E-01 4.920E+00 l.182E+OO 7.567E-02 2.905E-02 3.069E-02 2. 351E+Ol l.099E-01 3. 272E-02 l.621E-01 5.344E-02 6.229E-02 1. 741E-01 6.229E-02 5.728E-01 6.229E-02 l.205E-01 l.205E-01 5.344E-02 6.226E-02 1. 205E-01 l.249E+OO 6.226E-02 l.920E-01 l.249E+OO 4.586E-02 2.665E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4027 of 5809 Le (pCi/GRAM l.416E+Ol 4.681E-02 O.OOOE+OO 2.252E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. --

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 zN...:65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4028 of 5809 3.688E-01 O.OOOE+OO O.OOOE+OO 6.235E-02 4. 972E-01 O.OOOE+OO 4.750E-02 4.766E-01 5.318E+OO 3.480£-02 1. 56i°E-01 1.959E+OO 9.032E+OO O.OOOE+OO 1.858E-01 O.OOOE+OO O.OOOE+OO 6.726E-01 8.107E+OO 8.641E-01 0.000E+OO 1.850E-01 4.637E+02 3.182E-02 8.068E-01 2. 513E+OO 1.351E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.346E-02 6.183E-02 4.823E-01 4.823E-01 2. 717E-02 8.952E-02 2.386E-01 O.OOOE+OO O.OOOE+OO 1.309E-01 O.OOOE+OO l.125E-01 2.825E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.470E-02 O.OOOE+OO 5.981E-02 1.144E-01 O.OOOE+OO O.OOOE+OO 1.126E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.695E-01 5.250E-02 4.559E+00 4.702E-02 O.OOOE+OO 7.581E+02 O.OOOE+OO 2.444E-02 9.906E-02 1. 765E-01 1.147E-01 1.566E+OO 4. 791E-02 2.140E+Ol 2.321E-01 7.764E-02 2.376E-02 4.345E+OO FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 IH-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4029 of 5809 7.377E-Ol 2.910E+OO 3.133E+Ol l.018E+02 5.047E-Ol 2.410E+OO 3.639E-02 3.932E+OO 7.479E-01 5.897E--:Ol 3.987E-01 6.059E-01 2.189E-01 2.189E-01 5.095E-01 4.813E-01 6.059E-01 5. 421E-02 2.161E-01 4.498E+OO 5. 421E-02 O.OOOE+OO 2.237E-01 3.153E+02 l.270E-01 9.082E-02 6.325E-02 3.610E-02 3.905E-02 1.154E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:04:15.77 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235048.CNF;l * *Acquisition date 3-0CT-2016 07:00:55 Sensitivity : 3.000 *
  • Detector ID GAM28 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.46 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:28:00 Nuclide Library : SOLID *
  • Sample ID G405235048 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.3158E+02 GRAM *
  • Quantity Err(%) : 1.5200E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date . l-AUG-2016 10:02:35 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM28 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.636E+Ol 1.857E+OO RU-103 6.229E+OO 8.453E+OO CD-109 1.893E+OO 3 .115E+OO SN-126 1.205E-01 l.982E-01 BA-137M 1. 440E+OO 1.646E-01 CS-137 1.522E+OO 1.739E-01 CE-141 5.623E+00 4.043E+Ol EU-155 1.016E-01 l.769E-01 TL-208 3.661E-01 7.920E-02 BI-211 6.364E-01 1.165E+OO PB-212 1.156E+OO l.545E-01 BI-214 9.737E-01 l.978E-01 PB-214 1.360E+OO 2.287E-01 RN-222 9.737E-01 1.978E-01 RA-224 1. 526E+OO 1.379E+OO RA-226 9.737E-01 1.978E-01 AC-228 1. 067E+OO 3.677E-01 RA-228 1.067E+OO 3.677E-01 TH-228 1.156E+OO 1.545E-01 TH-230 9.734E-01 l.977E-01 TH-232 1.067E+OO 3.677E-01 TH-234 1.818E+00 2.448E+OO U-234 9.734E-01 1.977E-01 U-235 1.603E-01 2.748E-01 U-238 1. 8'18E+00 2.448E+OO AM-243 1.523E-01 1.160E-01 ANH-511 l.484E-01 8.956E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4030 of 5809 Key-Line Activity (pCi/GRAM -1.122E+OO 3.668E-02 -1. OOOE+41 K.L Act error ( 1. 96-sigma) 1.683E+Ol 4.884E-02 4.768E+41 TPU (1.96-sigma) l.857E+00 8.453E+OO 3 .115E+OO l.982E-01 l.646E-01 l.739E-01 4.043E+Ol l.769E-01 7.920E-02 1.165E+OO 1.545E-01 1.978E-01 2.287E-01 l.978E-01 1.379E+OO l.978E-01 3.677E-01 3.677E-01 1.545E-01 1.977E-01 3.677E-01 2.448E+OO 1.977E-01 2.748E-01 2.448E+00 1.160E-01 8.956E-02 TPU ( 1. 96-sigma) 1.684E+Ol 5.156E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 6.615E-03 2.370E-02 2.389E-02 NOT IDENT. SC-46 7.763E-02 4 .141E-01 4.156E-01 FAIL ABUN V-48 -4.998E+02 1. 755E+04 l.755E+04 SHORT HLIF CR-51 -5.934E+Ol 4. 8 87E+o2 4.894E+02 SHORT HLIF MN-54 2. 311E-02 6.840E-02 6.919E-02 NOT IDENT. C0-56 4.028E-01 5.154E-01 5.464E-01 NOT IDENT. MN-56 1.000E+41 l.284E+41 O.OOOE+OO SHORT HLIF C0-57 -4.445E-03 5.719E-02 5.723E-02 NOT IDENT. C0-58 5.473E-02 5. 371E-01 5.377E-01 NOT IDENT. FE-59 -2. 871E+OO 6.840E+OO 6. 961E+OO NOT IDENT. C0-60 l.241E-02 3.878E-02 3.919E-02 NOT IDENT. ZN-65 7. lllE-02 l.912E-01 1.939E-01 NOT IDENT. GE-68 -2.365E+OO 2.652E+00 2.858E+OO NOT IDENT. AS-73 -3.549E+OO 1.081E+Ol 1.093E+Ol NOT IDENT. AS-74 -3.353E+03 8.250E+03 8.387E+03 SHORT HLIF SE-75 -7.304E-02 2.173E-01 2.198E-01 NOT IDENT. BR-77 2.705E+38 2.348E+39 O.OOOE+OO SHORT HLIF SR-82 -4.613E+02 8. 585E+o2 8.834E+02 SHORT HLIF RB-83 4. 221E-01 7.440E-01 7.679E-01 NOT IDENT. KR-85 8.618E+OO 9. 511E+OO 1.027E+Ol NOT IDENT. SR-85 9.158E-01 l.014E+OO 1.095E+OO NOT IDENT. RB-86 -3.646E+04 3. 272E+04 3.662E+04 SHORT HLIF Y-88 -2.699E-02 2.250E-01 2.253E-01 NOT IDENT. Y-91 -2.762E+02 5.998E+02 6.126E+02 NOT IDENT. NB-94 3.432E-02 3.335E-02 3.676E-02 NOT IDENT. NB-95 -1.003E+OO l.044E+OO 1.138E+OO NOT IDENT. NB-95M -3.520E-01 3. l 72E+OO 3.176E+OO NOT IDENT. zR...:95 5.605E-01 1.459E+00 1.480E+OO NOT IDENT. NB-97 1.000E+41 l.196E+41 0.000E+OO SHORT HLIF ZR-97 1.000E+41 8.495E+40 O.OOOE+OO SHORT HLIF M0-99 1.190E+31 2.715E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 2.364E+41 O.OOOE+OO SHORT HLIF RH-101 2.590E-02 6.605E-02 6.707E-02 FAIL ABUN RH-102 4.350E-02 6.824E-02 7.lOOE-02 NOT IDENT. RH-106 5.829E-01 4.855E-01 5.520E-01 NOT IDENT. RU-106 5.829E-01 4.855E-01 5.520E-01 NOT IDENT. AG-108M 5.930E-03 3.257E-02 3.268E-02 NOT IDENT. AG-llOM -3 .118E-02 l.085E-01 l.094E-01 NOT IDENT. SN-113 6. 313E-02 2.706E-01 2. 721E-01 NOT IDENT. CD-115 -2.381E+39 4.449E+39 O.OOOE+OO SHORT HLIF SN-117M l.417E+04 1. 246E+05 l.247E+05 SHORT HLIF TE-123M -3.515E-02 l.623E-01 1. 631E-01 NOT IDENT. SB-124 -2. 351E+OO 1.886E+OO 2.163E+OO NOT IDENT. SB-125 1. 761E-01 2.235E-01 2. 372E-01 FAIL ABUN TE-125M 9.495E+Ol 3.278E+02 3.305E+02 NOT IDENT. I-126 -7.382E+04 l.031E+06 l.032E+06 SHORT HLIF SB-126 -7.545E+05 1.355E+06 1.397E+06 SHORT HLIF SB-127 -4.602E+20 2.858E+22 O.OOOE+OO SHORT HLIF I-131 1. 481E+09 6.346E+09 6.381E+09 SHORT HLIF I-132 -l.OOOE+41 1. 8 62E+42 0.000E+OO SHORT HLIF TE-132 -4.221E+26 5.253E+26 O.OOOE+OO SHORT HLIF BA-133 -9.114E-03 4.620E-02 4.638E-02 NOT IDENT. I-133 -1.000E+41 1.273E+42 O.OOOE+OO SHORT HLIF CS-134 l.545E-01 7.259E-02 1.006E-01 FAIL ABUN CS-135 -3.619E-02 1.493E-01 l.502E-01 NOT IDENT. I-135 -1. OOOE+41 6.852E+41 O.OOOE+OO SHORT HLIF CS-136 -3.752E+05 3.390E+05 3.788E+05 SHORT HLIF CE-139 -3.694E-03 l.241E-01 1.241E-01 NOT IDENT. BA-140 7.368E+04 1.464E+06 l.465E+06 SHORT HLIF LA-140 -1.070E+05 4.044E+05 4. 072E+05 SHORT HLIF CE-143 1. OOOE+41 2.514E+41 O.OOOE+OO SHORT HLIF CE-144 5.094E-01 4.000E-01 4.612E-01 FAIL ABUN PM-144 1.300E-02 6.183E-02 6.211E-02 NOT IDENT. PR-144 1.113E+OO 5.371E+OO 5.394E+OO NOT IDENT. PM-146 -l.524E-02 5.697E-02 5.739E-02 NOT IDENT. ND-147 -6.558E+06 3.747E+07 3.759E+07 SHORT HLIF PM-147 -5.018E+02 9. 531E+02 9. 796E+02 NOT IDENT. PM-149 3.943E+40 7.298E+40 0.000E+OO SHORT HLIF EU-150 l .114E-04 3.134E-02 3.134E-02 FAIL ABUN EU-152 l.540E-02 l.126E-01 l.129E-01 NOT IDENT. GD-153 6.185E-02 2.184E-01 2.202E-01 NOT IDENT. EU-154 8.987E-02 1.197E-01 1.263E-01 NOT IDENT. TB-160 -1. 07 6E+00 1.992E+OO 2.050E+OO FAIL ABUN H0-166M 1.626E-03 5.815E-02 5.815E-02 FAIL ABUN TM-171 -9.139E+00 2.563E+Ol 2. 596E+Ol NOT IDENT. HF-172 -3.073E-03 3.026E-01 3.026E-01 FAIL ABUN LU-172 3.354E-02 8.587E-02 8. 719E-02 FAIL ABUN LU-176 -1.213E-02 2.830E-02 2.882E-02 FAIL ABUN Page 4031 of 5809 HF-181 -1.503E+OO 5.322E+OO 5.365E+OO NOT IDENT. TA-182 8.899E-02 8.587E-01 8.597E-01 FAIL ABUN RE-183 4. 972E-01 3.303E+OO 3.310E+OO NOT IDENT. RE-184 1.600E+Ol 3.408E+Ol 3.483E+Ol NOT IDENT. W-188 -7.076E+Ol l.377E+02 1.413E+02 FAIL ABUN IR-192 3.741E-01 5.438E-01 5.694E-01 FAIL ABUN HG-203 -1.814E-02 2.738E+OO 2.738E+OO NOT IDENT. BI-207 -1. 596E-02 4. 596E-02 4.652E-02 FAIL ABUN PB-210 l.340E+OO 4.414E+OO 4.455E+OO NOT IDENT. PB-211 8.252E-01 7. 871E-01 8.706E-01 FAIL ABUN BI-212 1.132E+OO 7.106E-01 8.747E-01 FAIL ABUN RN-219 3.568E-02 4.606E-01 4.609E-01 FAIL ABUN RA-223 1. 968E-01 6.764E-01 6.822E-01 FAIL ABUN AC-227 -2.699E-02 2.495E-01 2.498E-01 FAIL ABUN TH-227 -2.699E-02 2.495E-01 2.498E-01 FAIL ABUN TH-229 9.613E-02 5.592E-01 5.609E-01 FAIL ABUN PA-231 1.950E-01 5.347E-01 5.419E-01 NOT IDENT. TH-231 1. 968E-01 6.764E-01 6.822E-01 FAIL ABUN PA-233 -3.749E-02 6.584E-02 6.797E-02 NOT IDENT. PA-234 3.449E-02 2.474E-01 2.479E-01 FAIL ABUN PA-234M 9.084E+OO 4.278E+OO 5.922E+OO FAIL ABUN NP-237 -3.749E--'02 6.584E-02 6.797E-02 FAIL ABUN NP-238 -1.000E+41 2.414E+41 O.OOOE+OO SHORT HLIF NP-239 3.553E-02 2.635E-01 2.640E-01 FAIL ABUN PU-239 2.347E+02 5.973E+02 6.066E+02 FAIL ABUN AM-241 -5.943E-02 1.515E-01 1.539E-01 NOT IDENT. CM-243 -7.438E-02 l.252E-01 l.296E-01 NOT IDENT. BK-247 -3.949E-02 7.967E-02 8 .'164E-02 FAIL ABUN CM-247 -l.lllE-02 4.326E-02 4.355E-02 NOT IDENT. CF-249 -4.551E-03 4.584E-02 4.588E-02 NOT IDENT. CF-251 3.599E-02 1.250E-01 l.261E-01 NOT IDENT. Page 4032 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 59.3957 87.09 119. 6387 136.47 76.2277 45.60 79.5984 87.57 119.7312 140.51 0.0000 46.54 74.5302 88.03 119.8196 143.76 83.4332 49.72 0.0000 88.34 119.8798 144.24 73.6588 51. 35 60.5064 88.47 119.9047 145.44 78.6787 51. 87 60.5771 89. 96 109. 5396 152.43 89.2211 52.39 72. 3514 1093.63 109.6575 153.25 0.0000 52.97 72.4445 91.11 0.0000 323.87 79.4648 53.44 73.5862 92.59 117.6313 156.02 0.0000 54.07 74.7558 93.35 117.7700 158.56 0.0000 57.36 0.0000 94.56 117.9901 159.00 84.8776 57.53 74.2361 94.65 118.0057 162.33 78.5026 57.98 65.6907 94.67 118. 0096 162.66 0.0000 59.27 78.8245 94.87 118.0457 163.33 82.7679 59.32 75.5929 97.43 73.8735 165.86 82.9904 59.54 75.6271 98.43 66.2777 176.31 83.8948 60.96 72.2348 '98.44 66.2785 176.60 0.0000 61.17 72.2656 99.53 83.3692 177.52 72 .1191 62.93 97.9036 100 .11 78.8050 181.07 0.0000 63.29 97.9735 102.03 60.4329 181.52 66.4465 63.58 98.0296 103.18 79.1599 184.41 78.5974 64.28 103.2549 103.37 86.9451 143.76 78.6984 66.73 100.8236 105.21 87.5648 193.51 87.0507 67.24 92.1461 105.31 87.5771 197.03 84.7471 125.81 111. 9858 106.12 85.7299 198.01 79.6315 67.75 111. 9998 106.47 85.7730 201.83 80.7847 69.67 102.4879 109.28 79.8504 203.43 64.3751 70.83 86.8783 111. 00 77.6872 205.31 97.6012 72.81 103.4505 111. 76 0.0000 210.85 94.5901 72.87 96.0711 114. 06 63.0416 215.65 72 .1262 74.66 91.1915 116. 30 0.0000 222 .11 75.1895 74.82 91. 2171 116.74 67.6192 227.09 71. 0701 74.97 91.2415 119.76 63.5234 227.38 73.7539 77.11 91. 58 69 121.12 82.3302 228.16 0.0000 78.74 91. 8465 121.22 82.3407 228.18 67.5793 79.69 91.9966 121. 78 85.9839 116.74 67.5793 80.12 92.0642 122.06 83.6259 235.69 84.5630 80.19 0.0000 122.92 96.8747 235. 96 65.7854 80.57 92.1349 123.07 83.7354 238.63 75.3500 81. 00 97.4491 265.00 77.8153 238.98 0.0000 81. 07 97.4610 125.81 86.4311 240.99 75.4961 81. 75 91. 5683 127.23 86.5863 242.00 75.5585 83.79 88.1154 127.91 81.8465 244.70 62.2028 84.00 94.9268 129.30 81. 9889 252.40 0.0000 85.43 105. 7228 131.20 101.5214 252.80 53.5342 86.55 128.6120 133.02 70.2556 254.15 0.0000 86.79 128.6621 133. 52 58.1777 256.23 56.4086 86.94 119. 6090 136. 00 81. 0465 260.90 0.0000 Page 4033 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 50.3686 355.39 0.0000 584.27 27.4119 264.80 48.3592 356.01 35.1079 595.83 0.0000 265.00 52.7637 364.49 0.0000 427.87 23.1875 268.22 44.0771 366.42 0.0000 602.52 0.0000 269.46 56.9872 372.51 43.3447 604. 72 13.2729 270.03 0112 375.05 45.3842 607 .14 28.2330 271.23 57.0629 377.52 44.4635 609.32 26. 5967 273.65 0.0000 356.01 39. 6712 610.33 26.6084 276.40 60.9807 388.16 45.7370 614.28 23.3208 277.37 51. 7788 388.63 0.0000 618.01 26.6934 277.60 48.0877 391. 69 37.8608 620.36 23.3789 278.00 53.6528 264.66 49.0728 621.93 10.0261 279.20 55.5518 401.81 42.0897 630.19 0.0000 279.54 61.1230 402.40 47.1167 631.29 19.0109 279.70 61.1298 404.85 31.1198 633.25 27.9795 280.46 58.3845 410.95 34.2490 634.78 0.0000 283.69 57.5940 413. 71 47.4169 635.95 25.7692 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 52.0853 423.72 0.0000 645.85 21. 3727 285.90 0.0000 427.09 33.5391 657.76 11. 3021 287.50 48.4379 427.87 33.5532 657.90 0.0000 290.67 50.4163 433.94 30.6030 661.66 19.2433 293.27 0.0000 439.40 33.7620 664.57 0.0000 351.93 59.0112 453.88 44.3298 666.33 0.0000 295. 96 59.0420 463.37 44.5476 666.50 0.0000 879.38 70.4178 468.07 39.4627 667.71 0.0000 299.98 54.9806 473.00 0.0000 677.62 22.2104 300.09 54.9842 475.06 45.8557 685.70 0.0000 300.13 45.1162 476.78 43.8090 695.00 0.0000 301.36 57.3848 477.60 42.7834 696.49 20.6499 302.85 68.7449 482.18 35.5599 696. 51 20.6499 256.23 49.9689 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.9517 306.78 55.7134 497.08 22.1254 697.49 20.6580 308.46 45.3789 505.52 25.3896 702.65 13.7988 311. 90 51.1710 507.63 0.0000 706.68 23.0322 316.51 42.7771 511. 00 30.7597 711. 68 17.3065 319.41 0.0000 514.00 30.2720 720.70 0.0000 320.08 0.0000 514.00 30.2720 721. 93 0.0000 321.04 41.0001 520.40 22.3732 722.78 10.4268 323.87 45.8545 520.69 0.0000 722.91 10.4271 325.23 45.8955 522.65 0.0000 723. 31 6.9524 328.76 0.0000 527.90 0.0000 724.19 10.4319 333.37 50.4674 528.26 18.1787 727. 33 18.5671 333.97 44.7177 529.59 19.2598 733.00 16.7449 334.37 50.5005 529.87 0.0000 735.93 18.6250 338.28 47.2534 531.02 0.0000 333.97 15.1413 338.32 47.2544 537.26 0.0000 739.50 0.0000 311. 90 52.1488 546.56 0.0000 747.24 14.9025 340.48 52.1488 552.55 24.8689 748.06 14.9066 340.55 0.0000 563.25 21.7293 752.31 21.0769 344.28 48.4029 569.33 22.8765 753.82 'o.0000 345.93 43.0270 946.00 19.6099 756.73 14.9528 351.06 34.0280 569.70 19.6121 756.80 14.9533 351.93 34.0465 583.19 27.3997 884.68 23.8096 Page 4034 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 34.4142 1274.44 9 .1116 1620. 50 4.3926 766.42 34.4214 1001.03 7.6033 1621. 92 7.6891 766.84 30.0125 1002.74 12.1711 1678.03 0.0000 772.60 0.0000 1004.73 7. 6113 1690.97 6.6782 776.52 0.0000 507.63 0.0000 1750.46 0.0000 7,39.50 0.0000 1025 .. 87 0.0000 1764.49 5.4152 778.90 14.1831 1028.54 0.0000 1063.66 30.7179 783.70 0.0000 1037.84 16.3245 1771. 35 12. 6513 785.37 17.0578 1038.76 0.0000 1791.20 0.0000 792.07 8.5485 631. 29 9.6265 1808.65 1.8194 794.95 15.1531 1048.07 0.0000 1810.72 0.0000 795.86 15.1577 1049.04 14.4489 1836.06 4.5706 810.06 16.1268 1050.41 11. 5635 810.29 16.1279 1063.66 13.5394 344.28 12.5444 1077.00 0.0000 810.76 12.5461 1077.34 18.4434 815.77 0.0000 1085.87 16.5403 1048.07 0.0000 1093.63 13.6497 832.01 18.0499 1099.45 14.6466 834.85 17.1631 1112. 07 12.7366 835.71 12.6503 1112.84 11.1991 836.80 0.0000 1115. 54 10.9826 846.75 0.0000 1120.29 15.7090 846.77 13.6029 1120. 55 15. 7100 856.80 0.0000 1221. 41 15.7129 860.56 7.2874 1129. 67 18. 6996 871.09 13.7096 1131.51 0.0000 873.19 20.1208 1147 .. 95 0.0000 875.33 0.0000 1173.23 14.9286 879.38 19.2440 1177.95 21.9208 880.51 16.5009 1189.05 7.9932 883.24 14.6797 1204.77 19.0580 884.68 18.3582 1221.41 11. 0786 889.28 15.6267 1231. 02 20.1904 894.76 15.6537 1235.36 0.0000 898.04 15.6698 1238.28 16.1807 900.72 17.5278 1260.41 0.0000 903.28 14.7720 1271.87 15.2911 911.20 17.5846 1274.44 8.1602 912.08 17.5893 1274.54 8.1606 923.98 0.0000 1291.59 10.2411 926.50 16.7366 1298.22 0.0000 929 .11 13.0276 1312 .11 0.0000 937.49 22.3901 1332.49 7.2367 944.13 0.0000 1362.66 0.0000 946.00 10.2880 1365.19 5.2072 949.00 13.4802 1368.63 0.0000 667.71 0.0000 1384.29 5.2295 962. 31 30.0742 1408.01 6.3080 964.08 23.8211 1457.56 0.0000 966 .17 24.0867 1460.82 7.4431 911. 2*0 25.4246 1489.16 4.2783 968. 97 25.4246 1505.03 0.0000 983.53 0.0000 1584.12 8.7231 984.45 0.0000 1596.21 0.0000 Page 4035 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:04:44.51 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * *******************************'************************************************* Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM33.CNF;235 Background date : Z-OCT-2016 11:02:02. Sample date 7-DEC-2015 13:33:00. Acquisition date : 3-0CT-2016 07:01:16. Sample ID G405235049 Sample quantity : 1.47303E+02 GRAM Detector name : GAM33 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.77 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 0 2 10 3 10 4 10 5 0 6 0 7 0 8 0 9 3 10 3 11 3 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 5 27 5 28 3 29 3 30 0 31 0 32 0 33 0 34 0 Page 4036 of 5809 Energy 63.19* 73.22 74.90* 77.17 87.63 92.73* 185.77* 207.99 238.66* 241.51 245.47 270.40 274.70 277.39 295.34 300.67 328.12* 338.02* 351.99* 432.80 471. 21 511.13* 576.91 583.28* 609.36* 661.65 665.34 727 .15 731.15 743.62 768.25 794.57 809.82 860.63 BACKGROUND CORRECTED SAMPLE PEAK REPORT
  • Area 48 33 93 205 86 78 31 32 380 87 41 23 19 25 121 46 23 93 202 20 30 36 15 119 212 160 20 35 16 20 16 21 14 24 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 120 1.13 112 2.59 169 1.47 153 1. 40 227 4.11 215 1.71 162 1.16 157 0.62 69 1. 17 71 1. 62 47 1. 63 77 0.53 51 1.37 58 0.70 7 5 1.13 66 0.74 72 1. 58 48 0.88 62 1. 39 32 1. 01 139 11. 76 39 2.65 15 0.59 34 1.14 23 1. 45 20 1.79 6 2.13 17 2.11 1 2.09 18 3.75 41 2.55 28 4.48 3 .0. 74 15 0.82 12 6. 50 146.53 149.88 154.41 175.31 185.50 371.33 415.73 477.00 482.69 490.60 540.40 549.00 554.37 590.25 600.90 655.74 675.52 703.44 864.90 941.67 1021.45 1152. 93 1165. 67 1217.81 1322. 34 1329. 71 1453.29 1461. 28 1486.23 1535.47 1588.09 1618.59 1720.19 122 144 144 144 171 182 367 410 470 470 470 536 545 552 586 596 647 671 698 861 921 1016 1149 1161 1211 1317 1317 1447 1447 1477 1523 1576 1615 1714 9 1.35E-02 44.7 18 9.05E-03 57.1 18 2.58E-02 29.0 18 5. 71E-02 12. 9 11 2.38E-02 35.7 13 2.16E-02 42.7 10 8.61E-03 83.1 13 8.90E-03 82.3 25 1. 05E-01 6. 4 25 2.41E-02 26.6 25 1.14E-02 37.3 9 6.35E-03 72.1 7 5.30E-03 66.7 8 7.06E-03 55.0 10 3.37E-02 16.0 11 1.27E-02 38.3 12 6.29E-03 79.0 10 2.59E-02 17.6 .9 5.61E-02 10.0 8 5.47E-03 54.7 28 8.35E-03115.1 12 1.0lE-02 47.2 7 4.14E-03 50.9 12 3.31E-02 13.6 13 5.89E-02 8.4 17 4.44E-02 9.6 17 5.52E-03 42.2 18 9.70E-03 30.6 18 4.38E-03 33.1 18 5.65E-03 53.6 17 4.41E-03 97.0 16 5.77E-03 61.0 7 3.84E-03 34.8 12 6.71E-03 37.9 E,:it 2.73E+OO 1. 83E+00 1.53E+OO 8.28E-01 Peak* search Report (continued) Page : 2 Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911. 23* 87 14 1. 32 1821. 40 1816 13 2. 41E-02 14.1 36 0 969.41* 51 37 1. 57 1937.74 1929 15 l.42E-02 29.9 37 0 1015.67 .. 7 8 1. 41 2030.29 2026 8 l.94E-03" 79.5 38 0 1021.36 10 2 1. 90 2041.66 2039 6 2.86E-03 36.7 39 0 1063.75* 10 12 0.74 2126.45 2119 12 2.82E-03 76.1 40 0 1097.44 9 12 0.49 2193.86 ,2184 12 2.54E-03 82.6 41 0 1121.55* 24 28 0.93 2242.10 2233 14 6.56E-03 52.3 42 0 1216.62 14 11 2.12 2432.32 2427 9 3.86E-03 51. 0 43 0 1267.42 7 6 0.88 2533.97 2528 8 2.04E-03 68.1 44 0 1290.36 10 13 0.61 2579.88 2571 14 2.73E-03 86. 4 45 0 1338.05 5 4 0.97 2675.30 2670 8 l.39E-03 82.5 46 0 1367. 85 6 5 1.10 2734.94 2731 7 l.55E-03 80.4 47 0 1460.94* 322 4 1. 71 2921. 28 2915 15 8.94E-02 5.8 48 0 1589.47 10 4 0.60 3178.58 3175 7 2.64E-03 46.0 49 0 1764.74* 31 0 2.92 3529.56. 3521 15 8.56E-03 19.1 Flag: "*" = Peak area was modified by background subtraction Page 4037of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 08:04:46 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 7-DEC-2015 13:33:00 G405235049 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:01:16 147.30 GRAM Sample Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLIDi GAMMA33 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4038of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.77 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page 2 Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.133E+OO 1.307E+Ol l.307E+Ol 11. 59 OK C0-58 810.76 99.45* 1.810E+OO 4.00lE-02 7.582E-01 69.57 OK CD-109 88.03 3.70* 4.931E+OO 2.128E+OO 3.343E+OO 101.05 OK SN-126 64.28 9.60 2.441E+OO 1.346E+OO 1. 346E+OO 89.42 OK 86.94 8.90 4.931E+OO 8.846E-01 8.846E-01 101.05 OK 87.57 37.00* 4.931E+OO 2.128E-01 2.128E-01 101.05 OK BA-137M 661. 66 89.90* 2 .115E+OO 4.469E-01 4.554E-01 19.25 OK CS-137 661. 66 85.10* 2 .115E+OO 4.721E-01 4. 811E-01 19.25 OK TL-208 277.37 6.60 4.258E+OO 5.203E-01 5.203E-01 109.91 OK 583.19 85.00* 2.334E+OO 3.231E-01 3.231E-01 27.18 OK 860.56 12.50 1. 727E+OO 5.793E-01 5.793E-01 75.89 OK PB-212 74.82 10.28 3.808E+OO 1.002E+OO 1.002E+OO 89.84 OK 77 .11 17.10 4.039E+OO 1.906E+OO 1.906E+OO 25.78 OK 238.63 43.60* 4.775E+OO 1.064E+OO 1.064E+OO 12.85 OK 300.09 3.30 3.993E+OO 1. 988E+OO 1.988E+OO 76.62 OK BI-214 609.32 45.49* 2.255E+OO l.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 OK 1764.49 15.30 9. 591E-01 1.0lOE+OO 1. OllE+OO 38.27 OK PB-214 74.82 5. 80' 3.800E+OO Line Not Found <<INT Reject 77 .11 9.70 4.039E+00 3.359E+OO 3.361E+OO 25.78 OK 87.09 3.41 4.892E+OO Line Not Found <<INT Reject 242.00 7.25 4. 727E+OO Line Not Found <<INT Reject 295.22 18.42 4. 051E+OO 9.297E-01 9.300E-01 32.05 OK 351. 93 35.60* 3.512E+OO 9.108E-01 9. lllE-01 20.02 OK RN-222 609.32 45.49* 2.255E+OO 1.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 l.406E+OO 5.678E-01 5.680E-01 104.69 OK 1764.49 15.30 9.591E-01 1.0lOE+OO 1. OllE+OO 38.27 OK RA-224 240.99 4.10* 4.734E+OO 9.609E-01 9.609E-01 154.07 OK RA-226 609.32 45.49* 2 .. 255E+OO 1.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 OK 1764.49 15.30 9. 591E-01 1.0lOE+OO 1. OllE+OO 38.27 OK AC-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.630E+OO l.288E+OO 1.288E+OO 35.17 OK 794.95 4.25 1.836E+OO l.390E+OO 1.390E+OO 122.09 OK 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* 1.653E+OO 1. 047E+OO 1.047E+OO 28.16 OK 968. 97 15.80 l.576E+OO 1.052E+OO 1.052E+OO 59.76 OK RA-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.630E+00 l.288E+OO 1.288E+OO 35.17 OK 794.95 4.25 1. 836E+OO 1.390E+OO l.390E+OO 122.09 OK 835.71 1. 61 1. 766E+OO Line Not Found Absent 911. 20 25.80* 1.653E+OO 1. 047E+OO l.047E+OO 28.16 OK 968.97 15.80 1.576E+OO 1.052E+OO 1. 052E+OO 59.76 OK TH-228 74.82 10.28 3.808E+OO l.002E+OO 1.002E+OO 89.84 OK 77 .11 17.10 4.039E+OO 1.906E+OO 1. 906E+OO 25.78 OK 238.63 43.60* 4.775E+OO 1.064E+OO 1.064E+OO 12.85 OK 300.09 3.30 3.993E+OO 1.988E+OO 1. 988E+OO 76.62 OK TH-230 609.32 45.49* 2.255E+OO 1.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 1.406E+OO 5.678E-01 5.678E-01 104.69 OK Page 4039 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1764.49 15.30 9.591E-01 1.0lOE+OO ], . OllE+OO 38.27 OK PA-231 283.69 1. 70 4.183E+OO Line Not Found Absent 301.36 5.35* 3.993E+OO 1.227E+OO 1.227E+OO 76.62 OK TH-232 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.630E+OO 1.288E+OO l.288E+OO 35.17 OK 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* 1.653E+00 1.047E+OO 1.047E+OO 28.16 OK 968. 97 15.80 1.576E+OO 1.052E+OO 1.052E+OO 59.76 OK TH-234 63.29 3.70* 2.441E+OO 3.492E+OO 3.492E+OO 89.42 OK 92.59 4.23 5.266E+OO 2.207E+OO 2.207E+OO 85.46 OK U-234 609.32 45.49* 2.255E+OO 1.106E+OO 1.106E+OO 16.85 OK 1120.29 14.92 1.406E+OO 5.678E-01 5.678E-01 104.69 OK 1764.49 15.30 9.591E-01 1.0lOE+OO 1.0lOE+OO 38.27 OK U-238 63.29 3.70* 2. 441E+OO 3.492E+OO 3.492E+OO 89.42 OK 92. 59 4.23 5.266E+OO 2.207E+OO 2.207E+OO 85.46 OK AM-243 43.53 5.90 2.461E-01 Line Not Found Absent 74.66 67.20* 3.808E+OO 1.533E-01 1.533E-01 89.84 OK ANH-511 511. 00 100.00* 2.592E+00 7.630E-02 7.630E-02 94.30 OK Flag: "*" = Keyline Page 4040 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:04:47.40 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * 'I DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l * *Acquisition date 3-0CT-2016 07:01:16 Sensitivity : 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:33:00 Analyst initials: MXRl *
  • Sample ID G405235049 Sample Quantity 1.4730E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. 'File : DKA100: [CANBERRA. GAMMA] EFF GAM33 CAN. CNF; 8 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma ) K-40 1.307E+Ol 1.484E+OO C0-58 7.582E-01 5.170E-01 CD-109 3.343E+OO 3.310E+OO SN-126 2.128E-01 2.107E-01 BA-137M 4.554E-01 8.590E-02 CS-137 4.811E-01 9.075E-02 TL-208 3.231E-01 8.606E-02 PB-212 1.064E+OO l.340E-01 BI-214 1.106E+OO 1.826E-01 PB-214 9. lllE-01 1. 788E-01 RN-222 l.106E+00 1. 826E-01 RA-224 9.609E-01 1. 451E+OO RA-226 1.106E+OO 1.826E-01 AC-228 1.047E+OO 2.889E-01 RA-228 1. 047E+OO 2.889E-01 TH-228 1.064E+OO 1.340E-01 TH-230 l.106E+00 1.826E-01 PA-231 1.227E+OO 9.209E-01 TH-232 1.047E+OO 2.889E-01 TH-234 3.492E+OO 3.061E+OO U-234 1.106E+OO 1.825E-01 U-238 3.492E+OO 3.061E+OO AM-243 1.533E-01 l.350E-01 ANH-511 7.630E-02 7.052E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4041 of 5 809 Key-Line Activity (pCi/GRAM -1.221E+Ol 2.539E-02 O.OOOE+OO 7.665E-03 -l.930E-01 O.OOOE+OO K.L. Cnt Uncert (1.96-sigma) 1.055E+Ol 4.514E-02 1. 575E+41 2.004E-02 3.950E-01 1.631E+04 MDA (pCi/GRAM 5.034E-01 7.993E-01 2.225E+OO l.425E-01 6.954E-02 7.346E-02 6.056E-02 1. OOlE-01 l.091E-01 l.315E-01 l.091E-01 1. 073E+OO 1.091E-01 2.024E-01 2.024E-01 1.00lE-01 1.090E-01 6.541E-01 2.024E-01 2.449E+OO l.090E-01 2.449E+OO 9.399E-02 5.863E-02 MDA (pCi/GRAM 1. 738E+Ol 9.975E-02 0.000E+OO 5.442E-02 7.000E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.940E+02 O.OOOE+OO SHORT HLIF MN-54 -4.259E-03 6.172E-02 l.173E-01 NOT IDENT. C0-56 -3.144E-02 4. 413E-01 8.455E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -7.400E-03 4.603E-02 8.555E-02 NOT IDENT. FE-59 1. 27 8E+OO 5.854E+OO l.153E+Ol FAIL ABUN C0-60 6.073E-05 3.063E-02 5.900E-02 NOT IDENT. ZN-65 -7.186E-02 1. 911E-01 3.126E-01 NOT IDENT. GE-68 -l.254E-01 2.033E+OO 4.166E+OO NOT IDENT. AS-73 2.037E+OO l. l,71E+Ol 2.348E+Ol NOT IDENT. AS-74 O.OOOE+OO 6. l 71E+03 O.OOOE+OO SHORT HLIF SE-75 -7.025E-02 2. 272E-01 3.949E-01 NOT IDENT. BR-77 O.OOOE+OO 3.132E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.490E+02 O.OOOE+OO SHORT HLIF RB-83 1. 911E-01 6.309E-01 l.288E+OO NOT IDENT. KR-85 5.945E+OO 7.189E+OO l.421E+Ol NOT IDENT. SR-85 6.302E-01 7.663E-01 l.514E+OO NOT IDENT. RB-86 O.OOOE+OO 2.525E+04 O.OOOE+OO SHORT HLIF Y-88 -l.244E-01 1. 779E-01 2. 891E-01 NOT IDENT. Y-91 l.748E+02 5.545E+02 l.153E+03 NOT IDENT. NB-94 -3.501E-02 3. ll 7E-02 4. 921E-02 NOT IDENT. NB-95 5.625E-01 9.123E-01 l.882E+OO NOT IDENT. NB-95M l.092E-01 2.721E+OO 4.528E+OO NOT IDENT. ZR-95 3.557E-01 l.129E+OO 2.392E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 601E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 929E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.782E+32 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 l.786E-02 3.229E-02 6.345E-02 NOT IDENT. RH-102 2. 911E-04 5.074E-02 l.006E-01 FAIL ABUN RU-103 2.516E+OO 5.743E+OO l.184E+Ol FAIL ABUN RH-106 -2.765E-01 4.620E-01 8.209E-01 NOT IDENT. RU-106 -2.765E-01 4.620E-01 8.209E-01 NOT IDENT. AG-108M 4.062E-02 4.355E-02 6.170E-02 FAIL ABUN AG-llOM 2.267E-02 9.083E-02 l.856E-01 NOT IDENT. SN-113 l.497E-01 2.129E-01 4.533E-01 NOT IDENT. CD-115 O.OOOE+OO 4.184E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 1. 046E+05 O.OOOE+OO SHORT HLIF TE-123M 3.333E-02 l.283E-01 2.434E-01 NOT IDENT. SB-124 2.304E+OO l.989E+OO 5.375E+00 NOT IDENT. SB-125 l.073E-03 9.645E-02 l.834E-01 NOT IDENT. TE-125M l.209E+02 2.879E+02 5.587E+02 NOT IDENT. I-126 O.OOOE+OO l.266E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.276E+06 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 2.428E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 5.319E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF TE-132 O.OOOE+OO 5.054E+26 O.OOOE+OO SHORT HLIF BA-133 8.003E-03 4.236E-02 8.152E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 9.106E-02 l.090E-01 l.082E-01 FAIL ABUN CS-135 -2.384E-03 1. 58 6E-01 2.617E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.902E+05 O.OOOE+OO SHORT HLIF CE-139 -2.357E-02 l.125E-01 2.036E-01 NOT IDENT. BA-140 O.OOOE+OO l.265E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.844E+05 O.OOOE+OO SHORT HLIF CE-141 -l.131E+Ol 2.447E+Ol 4.363E+Ol NOT IDENT. CE-143 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CE-144 l.190E-01 3. 591E-01 6.890E-01 NOT IDENT. PM-144 l.731E-03 5.304E-02 l.031E-01 NOT IDENT. PR-144 l.972E-01 4.617E+OO 8.987E+OO NOT IDENT. PM-146 -9.144E-03 4.275E-02 8.190E-02 NOT IDENT. ND-147 O.OOOE+OO 3 .196E+07 O.OOOE+OO SHORT HLIF PM-147 1. 7 61E+02 7.686E+02 l.483E+03 NOT IDENT. PM-149 O.OOOE+OO 5. 964E+40 O.OOOE+OO SHORT HLIF EU-150 -7.554E-03 2.361E-02 4.062E-02 FAIL ABUN EU-152 -1. 92 6E-02 7.680E-02 l.499E-01 FAIL ABUN GD-153 -5.941E-02 l.948E-01 3.'JOlE-01 NOT IDENT. EU-154 6.468E-02 l. lllE-01 2.460E-01 NOT IDENT. EU-155 -2.088E-02 l.098E-01 2.047E-01 FAIL ABUN TB-160 l.574E+OO l.755E+OO 3.931E+OO FAIL ABUN H0-166M -2.492E-02 5.337E-02 9.579E-02 FAIL ABUN TM-171 -1. 740E+Ol 2.827E+Ol 5.313E+Ol NOT IDENT. HF-172 -7.752E-02 2.060E-01 3.754E-01 FAIL ABUN LU-172 -4.987E-02 8.386E-02 l.298E-01 FAIL ABUN LU-176 l.997E-02 2.346E-02 4.998E-02 FAIL ABUN HF-181 -9.543E-01 3.924E+OO 7.531E+OO NOT IDENT. Page 4042 of 5809 TA-182 9.744E-03 9.093E-01 l.709E+OO FAIL ABUN RE-183 -2.148E+OO 3.507E+OO 6.554E+OO NOT IDENT. RE-184 l.519E+OO 3.528E+Ol 6.697E+Ol NOT IDENT. W-188 3.457E+Ol l.054E+02 2.084E+02 FAIL ABUN IR-192 -3.428E-01 4.034E-01 7.359E-01 FAIL ABUN HG-203 -4.527E-Ol 2.589E+OO 4.554E+OO FAIL ABUN BI-207 4.788E-02 7.142E-02 l.033E-01 FAIL ABUN PB-210 2.201E+OO 5.293E+OO l.093E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.925E-01 8.068E-01 FAIL ABUN PB-211 -Q.557E-02 6.164E-01 l.198E+OO NOT IDENT. BI-212 O.OOOE+OO 8.393E-01 l.354E+OO FAIL ABUN RN-219 7.810E-02 3.837E-01 7.681E-01 FAIL ABUN RA-223 -3.259E-02 5.823E-01 l.039E+OO FAIL ABUN AC-227 6.674E-02 2.077E-01 3.940E-01 FAIL ABUN TH-227 6.674E-02 2.077E-01 3.940E-01 FAIL ABUN TH-229 -9 .114E-03 4.860E-01 8.849E-01 FAIL ABUN TH-231 -3.259E-02 5.823E-01 l.039E+OO FAIL ABUN PA-233 -2.429E-02 4. 963E-02 9.468E-02 FAIL ABUN PA-234 l.804E-01 2.888E-01 6.058E-01 NOT IDENT. PA-234M -2.468E+OO 4.834E+OO 8.513E+OO NOT IDENT. U-235 -8. 013E-02 1. 749E-01 3.193E-01 FAIL ABUN NP-237 -2.429E-02 4. 963E-02 9.468E-02 FAIL ABUN NP-238 O.OOOE+OO l.228E+41 O.OOOE+OO SHORT HLIF NP-239 -2.527E-01 2.467E-01 4.238E-01 FAIL ABUN PU-239 8. OllE+Ol 3.009E+02 5.759E+02 NOT IDENT. AM-241 9.052E-02 l.635E-01 3.147E-01 NOT IDENT. CM-243 -2.619E-03 9.952E-02 l.885E-01 FAIL ABUN BK-247 -4.551E-02 7. 7 41E-02 1. 301E-01 NOT IDENT. CM-247 l.137E-02 3.279E-02 6.713E-02 FAIL ABUN CF-249 3.025E-02 3.318E-02 7.239E-02 NOT IDENT. CF-251 7.615E-04 l.213E-01 2.223E-01 NOT IDENT. Page 4043 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:04:45.25 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 310 10.66* 1.133E+OO 1.307E+Ol 1.307E+Ol 11. 59 C0-58 810.76 14 99.45* l.810E+OO 4.00lE-02 7.582E-01 69.57 CD-109 88.03 107 3.70* 4.931E+OO 2.985E+OO 4.689E+OO 71. 45 SN-126 64.28 62 9.60 2.441E+OO 1.346E+OO l.346E+OO 89.42 86.94 107 8.90 4.931E+OO 1.241E+OO 1.241E+OO 71. 45 87.57 107 37.00* 4. 931E+OO 2.985E-01 2.985E-01 71. 45 BA-137M 661. 66 167 89.90* 2 .115E+OO 4.469E-01 4.554E-01 19.25 CS-137 661.66 167 85.10* 2 .115E+OO 4.721E-01 4. 811E-01 19.25 TL-208 277.37 29 6.60 4.258E+OO 5.203E-01 5.203E-01 109.91 583.19 126 85.00* 2.334E+OO 3. 231E-01 3.231E-01 27.18 860.56 25 12.50 1.727E+OO 5.793E-01 5.793E-01 75.89 BI-211 72.87 41 1.23 3.629E+OO 4.698E+OO 4.698E+OO 114.29 351. 06 223 12.92* 3.512E+OO 2.510E+00 2.510E+OO 20.02 PB-212 74.82 117 10.28 3.808E+OO 1. 527E+OO 1.527E+OO 57.94 77 .11 258 17.10 4.039E+00 1.906E+OO 1.906E+OO 25.78 238.63 434 43.60* '4.775E+OO l.064E+OO 1.064E+OO 12.85 300.09 51 3.30 3.993E+OO 1.988E+OO 1.988E+OO 76. 62 BI-214 609.32 223 45.49* 2.255E+OO l.106E+OO 1.106E+OO 16.85 1120. 29 23 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 1764.49 29 15.30 9.591E-01 1.0lOE+OO 1. OllE+OO 38.27 PB-214 74.82 117 5.80 3.808E+OO 2.706E+00 2.707E+OO 57.94 77 .11 258 9.70 4.039E+OO 3.359E+OO 3.361E+OO 25.78 87.09 107 3.41 4.931E+OO 3.238E+OO 3.240E+OO 71. 45 242.00 99 7.25 4.734E+00 1.473E+OO 1.474E+OO 53 .11 295.22 136 18.42 4.051E+OO 9.297E-01 9.300E-01 32.05 351.93 223 35.60* 3.512E+OO 9.108E-01 9. lllE-01 20.02 RN-222 609.32 223 45.49* 2.255E+00 l.106E+OO 1.106E+OO 16.85 1120.29 23 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 1764.49 29 15.30 9.591E-01 1.0lOE+OO 1. OllE+OO 38.27 RA-224 240.99 99 4.10* 4.734E+OO 2.605E+00 2.605E+OO 53 .11 RA-226 609.32 223 45.49* 2.255E+OO l.106E+00 1.106E+OO 16.85 1120.29 23 14.92 1.406E+OO 5.678E-01 5.680E-01 104.69 1764.49 29 15.30 9.591E-01 1.0lOE+OO 1.0llE+OO 38.27 AC-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 103 11. 27 3.630E+OO 1.288E+OO 1.288E+OO 35.17 794.95 21 4.25 1.836E+OO 1.390E+OO 1.390E+00 122.09 835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 88 25.80* 1.653E+OO 1. 047E+OO 1. 047E+OO 28.16 968. 97 51 15.80 1.576E+OO 1.052E+OO 1.052E+OO 59.76 RA-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 103 11. 27 3.630E+OO l.288E+OO 1.288E+OO 35.17 794.95 21 4.25 1.836E+OO 1.390E+OO l.390E+00 122.09 835.71 ------1. 61 1.766E+OO ------Line Not Found ------911. 20 88 25.80* 1.653E+OO 1.047E+OO 1. 047E+00 28.16 968. 97 51 15.80 1.576E+OO 1.052E+OO 1.052E+OO 59. 76 TH-228 74.82 117 10.28 3.808E+OO 1.527E+OO 1.527E+OO 57.94 77 .11 258 17 .10 4.039E+OO 1.906E+OO l.906E+OO 25.78 ' Page 4044 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235049 Acquisition date 3-0CT-2016 07:01:16 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 434 43.60* 1.064E+OO 1.064E+OO 12.85 300.09 51 3.30 3.993E+OO 1. 988E+OO 1.988E+OO 76.62 TH-230 609.32 223 45.49* 2.255E+OO 1.106E+OO 1.106E+OO 16.85 1120.29 23 14.92 1.406E+OO 5.678E-01 5.678E-01 104.69 1764.49 29 15.30 9.591E-01 l.OlOE+OO 1. OllE+OO 38.27 PA-231 283.69 ------1. 70 4.183E+OO ------Line Not Found ------301.36 51 5.35* 3.993E+OO 1.227E+OO 1.227E+OO 76. 62 TH-232 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 103 11. 27 3.630E+OO 1.288E+OO 1.288E+OO 35 .17 835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 88 25.80* 1.653E+OO 1.047E+OO 1.047E+OO 28.16 968. 97 51 15.80 1. 57 6E+OO 1. 052E+OO 1.052E+OO 59.76 TH-234 63.29 62 3.70* 2. 441E+OO 3.492E+OO 3.492E+OO 89.42 92.59 96 4.23 5.266E+00 2.207E+OO 2.207E+OO 85.46 U-234 609.32 223 45.49* 2.255E+OO l.106E+OO l.106E+OO 16.85 1120.29 23 14.92 1.406E+OO 5.678E-01 5.678E-01 104.69 1764.49 29 15.30 9.591E-01 1.0lOE+OO 1.0lOE+OO 38.27 U-238 63.29 62 3.70* 2.441E+00 3.492E+00 3.492E+00 89.42 92. 59' 96 4.23 5.266E+OO 2.207E+OO 2.207E+OO 85.46 AM-243 43.53 ------5.90 2.461E-01 ------Line Not Found ------74.66 117 67.20* 3.808E+OO 2.336E-01 2.336E-01 57.94 ANH-511 511. 00 39 100.00* 2.592E+OO 7.630E-02 7.630E-02 94.30 Flag: "*" Key line Page 4045 of 5809 Summary of Nuclide Activity Sample ID : G405235049 Acquisition date Page : 3 3-0CT-2016 07:01:16 Total number of lines in spectrum 49 Number of unidentified lines 11 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 70.86D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600. OOY 1. 41E+l0Y l.41E+l0Y l.41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 19.0 1. 57 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.307E+Ol 4.00lE-02 2.985E+OO 2.985E-01 4.469E-01 4.721E-01 3.231E-01 2.510E+OO l.064E+OO l.106E+OO 9.108E-01 l.106E+OO 2.605E+OO l.106E+OO 1. 047E+OO 1.047E+OO l.064E+OO l.106E+00 l.227E+OO 1. 047E+OO 3.492E+OO l.106E+OO 3.492E+OO 2.336E-01 7.630E-02 4.297E+Ol 4.297E+Ol
  • Decay Corr pCi/GRAM l.307E+Ol 7.582E-01 4.689E+OO 2.985E-01 4.554E-01 4.811E-01 3.231E-01 2.510E+00 l.064E+OO l.106E+00 9. lllE-01 l.106E+OO 2.605E+OO l.106E+00 l.047E+OO l.047E+OO l.064E+OO l.106E+00 1. 227E+OO l.047E+OO 3.492E+OO l.106E+OO 3.492E+00 2.336E-01 7.630E-02 4.542E+Ol 4.542E+Ol 77.55% Decay Corr 2-Sigma Error 0.151E+Ol 5.275E-01 3.350E+00 2.132E-01 0.877E-01 0.926E-01 0.878E-01 0.503E+00 0 .137E+OO 0.186E+OO l.824E-01 0.186E+OO l.384E+OO 0.186E+OO 0.295E+OO 0.295E+OO 0.137E+OO 0.186E+OO 0.940E+OO 0.295E+OO 3.123E+OO 0.186E+OO 3.123E+OO l.353E-01 7 .196E-02 "M" Manually accepted 2-Sigma %Error 11. 59 69.57 71. 45 71. 45 19.25 19.25 27.18 20.02 12.85 16.85 20.02 16.85 53 .11 16.85 28.16 28.16 12.85 16.85 76.62 28.16 89.42 16.85 89.42 57.94 94.30 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4046 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235049 Acquisition date : 3-0CT-2016 07:01:16 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 185.77 36 189 1.16 371.33 367 10 8.61E-03 **** 5.62E+OO T 0 207.99 37 182 0.62 415.73 410 13 8.90E-03 **** 5.25E+OO 3 245.47 47 54 1. 63 490.60 470 25 1.14E-02 74.5 4.68E+OO T 0 270.40 26 8.7 0.53 540.40 536 9 6.35E-03 **** 4.3AE+OO T 0 274.70 22 58 1. 37 549.00 545 7 5.30E-03 **** 4.29E+OO T 0 328.12 25 80 1. 58 655.74 647 12 6.29E-03 **** 3. 72E+OO T 0 432.80 21 35 1. 01 864.90 861 8 5.47E-03 **** 2. 96E+OO T 0 471.21 32 150 11. 76 941. 67 921 28 8.35E-03 **** 2.77E+OO 0 576.91 16 16 0.59 1152. 93 1149 7 4.14E-03 **** 2.35E+OO 5 665.34 21 6 2.13 1329.71 1317 17 5.52E-03 84.4 2. llE+OO T 3 727 .15 36 17 2 .11 1453.29 1447 18 9.70E-03 61.1 1.97E+OO T 3 731.15 16 1 2.09 1461. 28 1447 18 4.38E-03 66.3 1. 96E+OO 0 743.62 21 18 3.75 1486.23 1477 18 5.65E-03 **** 1. 93E+OO 0 768.25 16 42 2.55 1535.47 1523 17 4. 41E-03 **** 1. 88E+OO T 0 1015.67 7 8 1. 41 2030.29 2026 8 1.94E-03 **** 1. 52E+OO 0 1021.36 10 2 1. 90 2041. 66 2039 6 2.86E-03 73.4 1. 51E+OO T 0 1063.75 10 12 0.74 2126.45 2119 12 2.82E-03 **** 1. 4 7E+OO T 0 1097.44 9 12 0.49 2193.86 2184 12 2.54E-03 **** 1. 43E+OO 0 1216.62 14 11 2.12 2432.32 2427 9 3.86E-03 **** 1.32E+OO 0 1267.42 7 6 0.88 2533.97 2528 8 2.04E-03 **** 1.28E+OO 0 1290.36 10 13 0.61 2579.88 2571 14 2.73E-03 **** l.26E+00 T 0 1338.05 5 4 0.97 2675.30 2670 8 l.39E-03 **** 1.22E+OO 0 1367.85 5 5 1.10 2734.94 2731 7 1.55E-03 **** 1. 20E+OO T 0 1589.47 9 3 0.60 3178.58 3175 7 2.64E-03 92.1 1.05E+00 Flags: "T" = Tentatively associated Page 4047of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:04:59.82 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * .. *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l *
  • Acquisition date 3-0CT-2016 07:01:16 Sensitivity 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:33:00 Nuclide Library : SOLID *
  • Sample ID G405235049 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.4730E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-58 CD-109 SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.943E-01 3.255E-01 1.050E+OO 6.725E-02 3.099E-02 3.274E-02 2. 672E-02 4.661E-02 4.765E-02 6.003E-02 4.765E-02 4.997E-01 4.765E-02 8.478E-02 8.478E-02 4.661E-02 4.764E-02 2.934E-01 8.478E-02 1.143E+OO 4.764E-02 1.143E+OO 4.409E-02 2.658E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4048 of 5809 Le (pCi/GRAM 7.438E+OO 4.306E-02 O.OOOE+OO l.983E-02 2.999E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4049 of 5809 5.093E-02 3. 631E-01 O.OOOE+OO 3.980E-02 4.828E+OO 2.318E-02 1.334E-01 1. 761E+OO 1.094E+Ol O.OOOE+OO 1.817E-01 O.OOOE+OO O.OOOE+OO 5.747E-01 6.435E+OO 6.856E-01 O.OOOE+OO 9.138E-02 5.053E+02 2. lllE-02 8.443E-01 2.108E+OO 1.020E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 968E-02 4.360E-02 5.325E+OO 3.543E-01 3.543E-01 2.819E-02 7. 966E-02 2.058E-01 O.OOOE+OO O.OOOE+OO l.135E-01 2.223E+OO 8.188E-02 2.622E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.727E-02 O.OOOE+OO 4. 821E-02 1.206E-01 O.OOOE+OO O.OOOE+OO 9.485E-02 O.OOOE+OO O.OOOE+OO 2.033E+Ol O.OOOE+OO 3.226E-01 4.537E-02 3.956E+OO 3.670E-02 0.000E+OO 6.898E+02 O.OOOE+OO 6.713E-02 1.542E-01 1. 063E-01 9.568E-02 1. 721E+OO 4.138E-02 2.460E+Ol 1. 736E-01 5.440E-02 2.305E-02 3.321E+OO 7.333E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M
  • U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4050 of 5809 3.037E+OO 2.950E+Ol 9.555E+Ol 3.299E-01 2.095E+OO 4.516E-02 5.083E+OO 3.878E-01 5.388E-01 6.233E-01 3.498E-01 4.717E-01 1.803E-01 l.803E-01 4.126E-01 4. 717E-01 4.254E-02 2.666E-01 3. 715E+00 l.489E-01 4.254E-02 O.OOOE+OO 1. 968E-01 2.694E+02 1.469E-01 8.807E-02 5. 962E-02 3.042E-02 3.286E-02 l.039E-01 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL' ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:05:05.52 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235049.CNF;l *
  • Acquisition date 3-0CT-2016 07:01:16 Sensitivity : 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:33:00 Nuclide Library : SOLID *
  • Sample ID G405235049 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.4730E+02 GRAM *
  • Quantity Err(%) : 1.3577E-03 %* *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal.* date 10-JUN-2016 07: 00: 49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM * ) ( 1. 96-sigma) K-40 1.307E+Ol 1.632E+OO C0-58 7.582E-01 5.180E-01 CD-109 3.343E+OO 3.326E+OO SN-126 2.128E-01 2 .114E-01 BA-137M 4.554E-01 8.810E-02 CS-137 4.811E-01 9.306E-02 TL-208 3.231E-01 8.714E-02 PB-212 1.064E+OO 1.452E-01 BI-214 1.106E+OO l.887E-01 PB-214 9. lllE-01 l.827E-01 RN-222 1.106E+OO l.887E-01 RA-224 9.609E-01 1.456E+OO RA-226 1.106E+OO l.887E-01 AC-228 1. 047E+OO 2.938E-01 RA-228 1.047E+OO 2.938E-01 TH-228 1.064E+OO 1.452E-01 TH-230 1.106E+OO 1. 886E-01 PA-231 l.227E+00 9.574E-01 TH-232 1. 047E+OO 2.938E-01 TH-234 3.492E+OO 3.157E+OO U-234 l.106E+OO l.886E-01 U-238 3.492E+OO 3.157E+OO AM-243 l.533E-01 l.357E-01 ANH-511 7. 630E-0.2 7.058E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4051 of 5809 Key-Line Activity (pCi/GRAM -1.221E+Ol 2.539E-02 1.000E+41 7.665E-03 -l.930E-01 l.153E+04 K.L Act error (1.96-sigma) 1.056E+Ol 4.515E-02 1. 635E+41 2.004E-02 3.950E-01 1.632E+04 TPU ( 1. 96-sigma) 1.632E+OO 5.180E-01 3.326E+OO 2 .114E-01 8.810E-02 9.306E-02 8. 714E-02 1.452E-01 1. 887E-01 1.827E-01 l.887E-Ql 1.456E+OO 1.887E-01 2.938E-01 2.938E-01 1.452E-01 1.886E-01 9.574E-01 2.938E-01 3.157E+OO 1.886E-01 3.157E+OO l.357E-01 7.058E-02 TPU ( 1. 96-sigma) 1.191E+Ol 4.658E-02 0.000E+OO 2.034E-02 4.045E-01 l.713E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 2.755E+02 3. 941E+02 4.133E+02 SHORT HLIF MN-54 -4.259E-03 6.172E-02 6.175E-02 NOT IDENT. C0-56 -3.144E-02 4.413E-01 4.415E-01 NOT IDENT. MN-56 -l.000E+41 1.329E+42 0.000E+OO SHORT HLIF C0-57 -7.400E-03 4.604E-02 4.616E-02 NOT IDENT. FE-59 l.278E+OO 5.854E+OO 5.883E+OO FAIL ABUN C0-60 6.073E-05 3.063E-02 3.063E-02 NOT IDENT. ZN-65 -7.186E-02 1. 911E-01 1.938E-01 NOT IDENT. GE-68 -l.254E-01 2.033E+OO 2.034E+OO NOT IDENT. AS-73 2.037E+OO l.172E+.01 1.176E+Ol NOT IDENT. AS-74 2.445E+03 6.174E+03 6.271E+03 SHORT HLIF SE-75 -7.025E-02 2.273E-01 2.294E-01 NOT IDENT. BR-77 2.487E+38 2.159E+39 O.OOOE+OO SHORT HLIF SR-82 -8.216E+Ol 7.490E+02 7.499E+02 SHORT HLIF RB-83 1. 911E-01 6.315E-01 6.373E-01 NOT IDENT. KR-85 5.945E+OO 7.193E+OO 7.676E+OO NOT IDENT. SR-85 6.302E-01 7.667E-01 8.177E-01 NOT IDENT. RB-86 -l.557E+03 2.525E+04 2.526E+04 SHORT HLIF Y-88 -l.244E-01 1. 781E-01 1. 8 67E-01 NOT IDENT. Y-91 l.748E+02 5.546E+02 5.601E+o2 NOT IDENT. NB-94 -3.501E-02 3.121E-02 3.497E-02 NOT IDENT. NB-95 5.625E-01 9.126E-01 9.472E-01 NOT IDENT. NB-95M 1.092E-01 2. 721E+OO 2.722E+OO NOT IDENT. ZR-95 3.557E-01 l.129E+OO l.140E+OO NOT IDENT. NB-97 l.OOOE+41 l.601E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.929E+41 O.OOOE+OO SHORT HLIF M0-99 -1.303E+32 1.785E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.025E+42 0. OOOE+OO . SHORT HLIF RH-101 1. 786E-02 3.245E-02 3.343E-02 NOT IDENT. RH-102 2. 911E-04 5.074E-02 5.074E-02 FAIL ABUN RU-103 2.516E+OO 5.744E+OO 5.855E+OO FAIL ABUN RH-106 -2.765E-01 4.623E-01 4.788E-01 NOT IDENT. RU-106 -2.765E-01 4.623E-01 4.788E-01 NOT IDENT. AG-108M 4.062E-02 4.358E-02 4.727E-02 FAIL ABUN AG-llOM 2.267E-02 9.083E-02 9.141E-02 NOT IDENT. SN-113 l.497E-01 2 .130E-01 2.234E-01 NOT IDENT. CD-115 -l.335E+39 4.191E+39 O.OOOE+OO SHORT HLIF SN-117M -8.136E+04 1.050E+05 l .113E+05 SHORT HLIF TE-123M 3.333E-02 l.283E-01 l.292E-01 NOT IDENT. SB-124 2.304E+OO 1.993E+OO 2.247E+OO NOT IDENT. SB-125 l.073E-03 9.645E-02 9.646E-02 NOT IDENT. TE-125M l.209E+02 2.880E+02 2.931E+02 NOT IDENT. I-126 l.530E+06 1.283E+06 1.457E+06 SHORT HLIF SB-126 -2.492E+05 l.277E+06 l.282E+06 SHORT HLIF SB-127 8.943E+21 2.723E+22 O.OOOE+OO SHORT HLIF I-131 -1. 745E+09 5.320E+09 5.377E+09 SHORT HLIF I-132 -1.000E+41 1.906E+42 O.OOOE+OO SHORT HLIF TE-132 -3.481E+26 5.249E+26 O.OOOE+OO SHORT HLIF BA-133 8.003E-03 4.237E-02 4.252E-02 FAIL ABUN I-133 1.000E+41 5.820E+42 O.OOOE+OO SHORT HLIF CS-134 9.106E-02 1.090E-01 1.165E-01 FAIL ABUN CS-135 -2.384E-03 1. 58 6E-01 1.586E-01 NOT IDENT. I-135 -l.000E+41 7.400E+41 0.000E+OO SHORT HLIF CS-136 1.383E+05 2.906E+05 2. 972E+05 SHORT HLIF CE-139 -2.357E-02 l.126E-01 1.131E-01 NOT IDENT. BA-140 -l.282E+05 1. 265E+06 l.267E+06 SHORT HLIF LA-140 -5.470E+04 2.844E+05 2.855E+05 SHORT HLIF CE-141 -1.131E+Ol 2.447E+Ol 2.500E+Ol NOT IDENT. CE-143 l.000E+41 1. 787E+42 O.OOOE+OO SHORT HLIF CE-144 1.190E-01 3.591E-01 3. 631E-01 NOT IDENT. PM-144 1. 731E-03 5.304E-02 5.305E-02 NOT IDENT. PR-144 1.972E-01 4.617E+OO 4.618E+00 NOT IDENT. PM-146 -9.144E-03 4.276E-02 4. 296E-02 NOT IDENT. ND-147 9.035E+06 3 .196E+07 3.222E+07 SHORT HLIF PM-147 1.761E+02 7.686E+02 7. 727E+02 NOT IDENT. PM-149 8.219E+39 5.966E+40 O.OOOE+OO SHORT HLIF EU-150 -7.554E-03 2. 361E-02 2.386E-02 FAIL ABUN EU-152 -1. 926E-02 7.680E-02 7. 729E-02 FAIL ABUN GD-153 -5.941E-02 1.948E-01 1. 967E-01 NOT IDENT. EU-154 6.468E-02 l .112E-01 l.149E-01 NOT IDENT. EU-155 -2.088E-02 1.098E-01 l.102E-01 FAIL ABUN TB-160 1.574E+OO 1. 757E+OO 1.895E+OO FAIL ABUN H0-166M -2.492E-02 5.338E-02 5.455E-02 FAIL ABUN TM-171 -1.740E+Ol 2. 831E+Ol 2.938E+Ol NOT IDENT. HF-172 -7.752E-02 2.063E-01 2.093E-01 FAIL ABUN LU-172 -4.987E-02 8.401E-02 8.697E-02 FAIL ABUN LU-176 1.997E-02 2.348E-02 2.515E-02 FAIL ABUN HF-181 -9.543E-01 3.925E+OO 3.948E+OO NOT IDENT. Page 4052 of 5809 TA-182 9.744E-03 9.093E-01 9.093E-01 FAIL ABUN RE-183 -2.148E+OO 3.523E+00 3.654E+OO NOT IDENT. RE-184 1.519E+OO 3.528E+Ol 3.529E+Ol NOT IDENT. W-188 3.457E+Ol 1.055E+02 l.067E+02 FAIL ABUN IR-192 -3.428E-01 4.036E-01 4.322E-01 FAIL ABUN HG-203 -4.527E-01 2.589E+OO 2.597E+OO FAIL ABUN BI-207 4.788E-02 7.144E-02 7.463E-02 FAIL ABUN PB-210 2.201E+OO 5.297E+OO 5.389E+OO NOT IDENT. BI-211 2.510E+OO 5.050E-01 1.239E+OO FAIL ABUN PB-211 -9.551E-02 6.164E-01 6.180E-01 NOT LDENT. BI-212 1.401E+OO 8.423E-01 1.053E+OO FAIL ABUN RN-219 7.810E-02 3.838E-01 3.855E-01 FAIL ABUN RA-223 -3.259E-02 5.823E-01 5.825E-01 FAIL ABUN AC-227 6.674E-02 2.079E-01 2.lOlE-01 FAIL ABUN TH-227 6.674E-02 2.079E-01 2. lOlE-01 FAIL ABUN TH-229 -9 .114E-03 4.860E-01 4.860E-01 FAIL ABUN TH-231 -3.259E-02 5.823E-01 5.825E-01 FAIL ABUN PA-233 -2.429E-02 4. 965E-02 5.084E-02 FAIL ABUN PA-234 1.804E-01 3.549E-01 3.641E-01 NOT IDENT. PA-234M -2.468E+00 4.836E+OO 4. 962E+OO NOT IDENT. U-235 -8.013E-02 1. 750E-01 1.787E-01 FAIL ABUN NP-237 -2.429E-02 4.965E-02 5.084E-02 FAIL ABUN NP-238 1. OOOE+41 l.229E+41 O.OOOE+OO SHORT HLIF NP-239 -2.527E-01 2.476E-01 2.726E-01 FAIL ABUN PU-239 8. OllE+Ol 3.009E+02 3.031E+02 NOT IDENT. AM-241 9.052E-02 l.637E-01 1.687E-01 NOT IDENT. CM-243 -2.619E-03 9.952E-02 9.953E-02 FAIL ABUN BK-247 -4.551E-02 7.795E-02 8.061E-02 NOT IDENT. CM-247 1.137E-02 3.284E-02 3.324E-02 FAIL ABUN CF-249 3.025E-02 3.327E-02 3.596E-02 NOT IDENT. CF-251 7.615E-04 1.213E-01 1. 213E-01 NOT IDENT. Page 4053 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 52.3810 87.09 92.6644 136.47 71.2733 45.60 55.4770 87.57 92.7384 140.51 0.0000 46.54 50.8940 88.03 92.8090 143.76 59.7382 49.72 0.0000 88.34 92.8563 144.24 70.8418 51. 35 61. 0164 88.47 92.8761 145.44 73.1593 51. 87 58.2263 89.96 82.1497 152.43 68.1708 52.39 64.9855 1093.63 82.2400 153.25 0.0000 52.97 56.4592 91.11 0.0000 323.87 71.6689 53.44 58.4355 92.59 82.4988 156.02 0.0000 54.07 59.4776 93.35 82.5983 158.56 0.0000 57.36 0.0000 94.56 82.7570 159.00 57.4209 57.53 69.5998 94.65 82.7686 162.33 77.9745 57.98 66.7643 94.67 82.7710 162.66 0.0000 59.27 53.0413 94.87 82.7972 163.33 46.3834 59.32 53.0470 97.43 72. 0443 165.86 66.9314 59.54 53. 0716 98.43 63.8298 176.31 65.3844 60. 96 63.6164 98.44 63.8307 176.60 0.0000 61.17 66.2421 99.53 80.2692 177.52 67.7632 62.93 65.5051 100 .11 78.2530 181. 07 0.0000 63.29 65.5533 102.03 79.5266 181. 52 70.7332 63.58 65.5919 103.18 79.6628 184.41 78.6520 64.28 66.6651 103.37 68.1520 143.76 66.0158 66.73 73.5592 105.21 59.9271 193.51 64.1930 67.24 71. 0030 105.31 72.5539 197.03 60.8986 125.81 71. 0640 106.12 68.4290 198.01 72.6790 67.75 74.0353 106.47 68.4639 201.83 72.9438 69.67 83.2284 109.28 63.4547 203.43 56.5583 70.83 75.4683 111. 00 72. 0918 205.31 64.5280 72. 81 76.7462 111. 76 0.0000 210.85 49.0404 72. 87 76.7550 114. 06 69.2083 215.65 50.0506 74.66 77.0088 116. 30 0.0000 222 .11 70.7170 74.82 77.0317 116.74 81.2214 227.09 56.5813 74.97 77.0529 119.76 57.9473 227.38 63.8206 77 .11 77.3525 121.12 61.2787 228.16 0.0000 78.74 77.5775 121. 22 54.8357 228.18 63.8651 79.69 77.7079 121.78 60.2567 116.74 63.8651 80.12 7 6. 7 567 122.06 63.5085 235.69 59.8326 80.19 0.0000 122.92 45.2611 235. 96 59.8465 80.57 76.8170 123.07 45.2700 238.63 60.7925 81. 00 66.0850 265.00 48.5427 238.98 0.0000 81. 07 66.0930 125.81 58.4149 240.99 60.9131 81.75 95.8808 127.23 57.4388 242.00 60.9650 83.79 81.3104 127.91 60.7435 244.70 61.1015 84.00 81.3391 129.30 64.1117 252.40 0.0000 85.43 97.8435 131.20 72.9827 252.80 33.2148 86.55 92.5814 133.02 68.7832 254.15 0.0000 86.79 92.6180 133.52 64.4565 256.23 33.3067 86.94 92.6416 136.00 70.1357 260.90 0.0000 Page 4054 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 50.9159 355.39 0.0000 584.27 18.9026 264.80 52.1642 356.01 34. 9602 595.83 0.0000 265.00 52.1719 364.49 0.0000 427.87 19.0379 268.22 46.4912 366.42 0.0000 602.52 0.0000 269.46 44.8748 372.51 33.8948 604. 72 15.0562 2'J0.03 44.8945 375.05 607.14 19.5936 271.23 44.9363 377.52 32.2090 609.32 16.0918 273.65 0.0000 356.01 30.5365 610.33 16.0983 276.40 30.0762 388.16 19.8099 614.28 22.6767 277.37 41. 3849 388.63 0.0000 618.01 18.1699 277.60 41.3920 391.69 22.5586 620.36 22.2292 278.00 41.4051 264.66 29.0273 621. 93 20.2222 279.20 47.7215 401.81 31.7693 630.19 0.0000 279.54 47.7343 402.40 26.3326 631. 29 14.2108 279.70 42. 7148 404.85 29.0977 633.25 16.2539 280.46 45.2527 410.95 31.0249 634.78 0.0000 283.69 42.8424 413.71 39.2986 635.95 19.3232 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 44.5797 423.72 0.0000 645.85 10.2112 285.90 0.0000 427.09 18.4163 657.76 16.9297 287.50 41. 27 90 427.87 23.2148 657.90 0.0000 290.67 35.4648 433.94 19.4106 661. 66 22.6087 293.27 0.0000 439.40 27. 8119 664.57 0.0000 351.93 44.4785. 453.88 28.0292 666.33 0.0000 295. 96 44.5020 463.37 27.2306 666.50 0.0000 879.38 45.8602 468.07 27.2972 667. 71 0.0000 299.98 25.5035 473.00 0.0000 677. 62 18.6152 300.09 25.5060 475.06 11.3362 685.70 0.0000 300.13 25.5066 476.78 25.5289 695.00 0.0000 301.36 25.5292 477.60 25.5399 696. 49 17.7104 302.85 37.0562 482.18 21.8068 696. 51 17.7104 256.23 39.6582 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.5475 306.78 32.4614 497.08 21. 0153 697.49 14.5907 308.46 37.6317 505.52 26.4747 702.65 26.1058 311. 90 33.4355 507.63 0.0000 706.68 16.7337 316.51 37.8429 511. 00 31.7391 711. 68 18.8606 319.41 0.0000 514.00 18.7819 720.70 0.0000 320.08 0.0000 514.00 18.7819 721. 93 0.0000 321.04 37.2709 520.40 19.3229 722. 78 17.3614 323.87 33.7124 520.69 0.0000 722.91 12.6270 325.23 35.4738 522.65 0.0000 723.31 12.6289 328.76 0.0000 527.90 0.0000 724 .19 15.7916 333.37 28.7085 528.26 24.2452 727. 33 13.7019 333.97 31.3308 529.59 21.3492 733.00 11. 0900 334.37 32.6447 529.87 0.0000 735.93 6.3440 338.28 24.4379 531.02 0.0000 333.97 12.6953 338.32 24.4385 537.26 0.0000 739.50 0.0000 311. 90 31.4656 546.56 0.0000 747.24 12.7407 340.48 31.4656 552.55 16.6742 748.06 7. 9654 340.55 0.0000 563.25 17.7407 752.31 13.8278 344.28 28.0391 569.33 13.8365 753.82 0.0000 345.93 35.0863 946.00 13.8376 756.73 8.5231 351.06 36. 9619 569.70 14.8273 756.80 8.5234 351. 93 36.9824 583.19 18.8941 884.68 16.0223 Page 4055 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 16.0333 1274.44 18.4173 1620.50 4.0042 766.42 16.0364 1001.03 18.4427 1621. 92 5.0064 766.84 16.0388 1002.74 16.1453 1678.03 0.0000 772. 60 0.0000 1004.73 9.2311 1690.97 1.0148 776.52 0.0000 507.63 0.0000 1750.46 0. 0,000 739 .. 50 0.0000 1025.87 0.000() 1764.49 5.1437 778.90 12.8862 1028.54 0.0000 1063.66 8.2388 783.70 0.0000 1037.84 6.9893 1771. 35 4.1201 785.37 14.2071 1038.76 0.0000 1791.20 0.0000 792.07 19.4187 631.29 10.5095 1808.65 1. 0370 794.95 17.8179 1048.07 0.0000 1810.72 0.0000 795.86 9.7222 1049.04 9.6404 1836.06 4.1685 810.06 11. 3981 1050.41 14.9041 810.29 13.0273 1063.66 7.9195 344.28 13.0278 1077.00 0.0000 810.76 6.5146 1077.34 10.5989 815.77 0.0000 1085.87 9.7385 1048.07 0.0000 1093.63 15. 6138 832.01 15.3108 1099.45 7.1084 834.85 15.3250 1112. 07 9.8069 835. 71 10.9497 1112.84 11. 5924 836.80 0.0000 1115.54 15.7062 846.75 0.0000 1120. 29 12.5089 846.77 13.1880 1120. 55 12.5098 856.80 0.0000 1221.41 12. 5123. 860.56 6.6239 1129. 67 2.6873 871.09 12.1852 1131.51 0.0000 873.19 7.7596 1147.95 0.0000 875.33 0.0000 1173.23 17.2118 879.38 7.7750 1177.95 18 .1396 880.51 12.2224 1189.05 20.0100 883.24 13.3452 1204.77 13. 6972 884.68 10.0133 1221. 41 12.2257 889.28 15. 5996 1231.02 11.0295 894.76 13.3940 1235.36 0.0000 898.04 10.0562 1238.28 16.5740 900. 72 10.0646 1260.41 0.0000 903.28 17.9069 1271. 87 12.7307 911.20 8.9756 1274.44 8.3595 912.08 8.9782 1274.54 8.3595 923.98 0.0000 1291.59 11.9375 926.50 18.0365 1298.22 0.0000 929 .11 16.9232 1312 .11 0.0000 937.49 20.3599 1332.49 4. 5196 944 .13 0.0000 1362.66 0.0000 946.00 11. 3403 1365.19 7.5889 949.00 19.2959 1368. 63 0.0000 667. 71 0.0000 1384.29 6.6689 962.31 13.6753 1408.01 6.7043 964.08 20.5239 1457.56 0.0000 966 .17 22.2477 1460.82 3.8752 911. 20 23.9788 1489.16 2.9238 968. 97 23.9788 1505.03 6.8453 983.53 0.0000 1584.12 5.3005 984.45 0.0000 1596.21 0.0000 Page 4056 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:05:34.85 ******************************************************************************** * "GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : Z-OCT-2016 11:02:08. Sample date 7-DEC-2015 13:42:00. Acquisition date : 3-0CT-2016 07:01:40. Sample ID G405235050 Sample quantity 1.71604E+02 GRAM Detector name : GAM36 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.33 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 2 0 2 2 0 0 0 0 0 0 0 0 0 9 9 0 0 2 2 0 0 0 0 0 0 0 0

0 0 0 Page 4057 of 5809 Energy 46.21* 63.24* 74.87* 77.13* 80.83 87.28 89.70 92.70* 186.15* 227.19 238.61* 262. 50 270.55 295.36* 303.06 327.54* 338.76 350.03 351. 88* 426. 49 511. 05* 583.18* 587.54 601.50 609.43* 635 .18 662.20 700.74 727.85 763.74 768.42 794.70 897.43 910.82* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 18 37 100 135 18 79 36 61 63 25 226 28 23 59 39 33 34 10 158 25 20 61 12 12 98 5 16 8 18 9 15 31 7 60 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 81 126 73 66 69 98 25 83 71 51 101 99 30 54 99 35 40 6 28 24 27 14 17 27 14 13 14 14 8 14 3 7 8 7 1. 02 1.19 0.87 0.92 1. 05 1. 29 0.97 1. 08 1. 24 1. 71 1. 06 6.92 1. 43 0.97 7.57 0.88 0.84 1. 76 1. 35 6.53 2.74 1. 72 1. 43 4.23 1. 40 0.51 1. 29 0.96 1. 27 4.41 1. 48 0.66 0.68 2.02 92.38 126.44 149. 72 154.22 161. 63 174.52 179.37 185.37 372.29 454.36 477.20 524.99 541. 09 590.71 606.11 655.06 677.51 700.05 703.75 852.94 1022.06 1166.29 1175.00 1202.92 1218.78 1270.27 1324.30 1401. 36 1455.57 1527.33 1536.69 1589.24 1794.64 1821. 41 90 122 144 144 144 171 178 178 368 451 471 513 538 586 596 650 673 699 699 845 1016 1158 1158 1192 1212 1265 1320 1395 1451 1519 1533 1581 1789 1813 8 4.90E-03 93.3 9 1. 03E-02 57. 9 21 2.79E-02 16.4 1.39E+OO 21 3.74E-02 12.8 21 4.90E-03 84.7 7 2.19E-02 23.7 14 1.0lE-02 19.8 2.77E+OO 14 1.68E-02 28.7 10 1.75E-02 29.5 8 7.05E-03 52.8 10 6.27E-02 10.9 19 7.87E-03 86.6 6 6.30E-03 43.7 10 1.64E-02 26.8 20 1.08E-02 66.2 10 9.lOE-03 38.7 10 9.51E-03 37.8 12 2.73E-03 47.6 7.59E+OO 12 4.39E-02 9.9 16 6.94E-03 48.2 11 5.45E-03 69.2 22 l.68E-02 19.1 9.52E-01 22 3.41E-03 62.2 17 3. 25E-03110. 0 14 2.73E-02 13.4 8 1. 45E-03124 .1 9 4.55E-03 47.5 10 2.17E-03 98.7 9 4.89E-03 38.6 14 2.50E-03 94.3 7 4.09E-03 33.4 15 8.51E-03 26.5 9 1. 86E-03 88. 6 14 1.66E-02 16.5 Peak Search Report (continued) Page : 2 Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 955.36 13 0 1. 50 1910.46 1905 10 3. 61E-03 27.7 36 0 965.48 13 8 1.11 1930.69 1925 10 3.47E-03 49.8 37 . 0 969. 05 35 2.. 1. 95 1937.84 1934 9 9.76E-03 18.5 38 0 1019.06 16 0 4.53 2037.81 2031 13 4.44E-03 25.0 39 0 1120.22* 16 10 0.83 2240.05 2235 10 4.58E-03 44.4 40 0 1239.25 8 11 1. 27 2478.00 2471 11 2.22E-03 87.7 41 0 1305.01 8 5 0.96 2609.47 2605 9 2.08E-03 62.7 42 0 1461.06* 205 0 2.09 2921.39 2915 13 5.69E-02 7.1 43 0 1764.65* 9 5 0. 71 3528.17 3522 11 2.43E-03 66.3 Flag: "*" = Peak area was modified by background subtraction Page 4058 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:05:36 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 13:42:00 G405235050 Acquisition date : Sample quantity : 3-0CT-2016 07:01:40 171.60 GRAM Sample type

  • Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4059 of 5809 Sample geometry 1: Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.33 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 6.546E-01 1.255E+Ol 1.255E+Ol 14.12 OK CD-109 88.03 3.70* 4.297E+OO 2.459E+OO 3.863E+OO 59.22 OK SB-125 176.31 6.89 4.460E+OO Line Not Found Absent 321. 04 0.42 2.640E+OO Line Not Found Absent 427.87 29.80* 2.005E+OO 2 .114E-01 2.599E-01 96. 33 OK 463.37 10.56 1.852E+OO Line Not Found Absent 600.60 17.77 1.455E+OO 2.187E-01 2.689E-01 220.01 OK 635.95 11. 29 1.385E+OO 1.604E-01 1. 972E-01 248.20 OK SN-126 64.28 9.60 2.468E+OO 9.790E-01 9.790E-01 115. 79 OK 86.94 8.90 4.297E+OO 1.022E+00 1.022E+00 59.22 OK 87.57 37.00* 4.297E+OO 2.459E-01 2.459E-01 59.22 OK BA-137M 661. 66 89.90* 1.334E+OO 6.517E-02 6.642E-02 94.95 OK CS-137 661. 66 85.10* 1.334E+OO 6.884E-02 7.016E-02 94.95 OK TL-208 277.37 6.60 3.041E+OO Line Not Found Absent 583.19 85.00* 1. 496E+OO 2.315E-01 2.315E-01 38 .11 OK 860.56 12.50 1.058E+OO Line Not Found Absent PB-210 46.54 4.25* 8.252E-01 3.242E+OO 3.326E+OO 186.69 OK BI-211 72. 87 1. 23 3.327E+OO Line Not Found Absent 351.06 12.92* 2. 415E+'OO 9.855E-01 9.855E-01 103.12 OK PB-212 74.82 10.28 3.486E+OO 1.385E+00 1.385E+OO 42.80 OK 77 .11 17.10 3.657E+00 1.319E+OO 1.319E+OO 25.66 OK 238.63 43.60* 3.500E+OO 8.007E-01 8.007E-01 21. 88 OK 300.09 3.30 2.819E+OO Line Not Found Absent BI-214 609.32 45.49* 1.437E+OO 7.244E-01 7.246E-01 26.85 OK 1120.29 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 OK PB-214 74.82 5.80 3 .,482E+OO Line Not Found <<INT Reject 77 .11 9.70 3.657E+OO 2.325E+OO 2.326E+OO 25.66 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 3.455E+00 Line Not Found Absent 295.22 18.42 2.863E+00 5.924E-01 5.926E-01 53.64 OK 351.93 35.60* 2.414E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1.437E+OO 7.244E-01 7.246E-01 26.85 OK 1120.29 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 OK RA-226 609.32 45.49* 1.437E+OO 7.244E-01 7.246E-01 26.85 OK 1120.29 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 OK AC-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.506E+00 6.299E-01 6.299E-01 75.66 OK 794.95 4.25 1.134E+OO 2. 961E+OO 2. 961E+OO 53.09 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.006E+OO 1.053E+OO 1.053E+OO 32.94 OK 968.97 15.80 9.525E-01 1.059E+OO 1.059E+OO 36.92 OK RA-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.506E+OO 6.299E-01 6.299E-01 75.66 OK 794.95 4.25 1.134E+OO 2. 961E+OO 2. 961E+OO 53.09 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911. 20 25.80* 1.006E+OO 1.053E+OO 1.053E+OO 32.94 OK Page 4060 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 968. 97 15.80 .9.525E-01 1.J)59E+OO 1.059E+OO 36.92 OK TH-228 74.82 10.28 3.486E+OO l.385E+00 1.385E+OO 42.80 OK 77 .11 17.10 3.657E+OO 1.319E+OO l.319E+00 25.66 OK 238.63 43.60* 3.500E+OO 8.007E-01 8.007E-01 21. 88 OK 300.09 3.30 2.819E+OO Line Not Found Absent TH-230 609.32 45.49* 1.437E+OO 7.244E-01 7.244E-01 26.85 OK 1120. 29 14.92 8.373E-01 5.866E-01 5.866E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.384E-01 132.56 OK TH-232 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11.27 2.506E+OO 6.299E-01 6.299E-01 75.66 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911. 20 25.80* 1.006E+OO 1.053E+OO 1.053E+OO 32.94 OK 968. 97 15.80 9.525E-Ol 1.059E+OO 1.059E+OO 36.92 OK TH-234 63.29 3.70* 2.468E+OO 2.540E+OO 2.540E+OO 115. 79 OK 92.59 4.23 4.552E+OO 1.892E+OO 1.892E+OO 57.46 OK U-234 609.32 45.49* 1.437E+OO 7.244E-01 7.244E-01 26. 85 OK 1120.29 14.92 8.373E-01 5.866E-01 5.866E-01 88.76 OK 1764.49 15.30 5.418E-01 4.384E-01 4.384E-01 132.56 OK U-235 89. 96 3.47 4.418E+OO 1.428E+OO l.428E+OO 39.64 OK 93.35 5.60 4.552E+OO 1.429E+00 1.429E+OO 57.46 OK 143.76 10.96* 4.954E+OO Line Not Found Absent 163.33 5.08 4.674E+OO Line Not Found Absent 185. 72 57.20 4.296E+OO 1.429E-01 l.429E-01 59.00 OK 205.31 5.01 3.984E+OO Line Not Found Absent U-238 63.29 3.70* 2.468E+OO 2.540E+OO 2.540E+OO 115.79 OK 92.59 4.23 4.552E+OO 1.892E+OO 1. 892E+OO 57.46 OK AM-243 43.53 5.90 5.957E-01 Line Not Found Absent 74.66 67.20* 3.486E+OO 2 .119E-01 2.120E-01 42.80 OK ANH-511 511. 00 100.00* 1.690E+OO 5.738E-02 5.738E-02 138. 38 OK Flag: "*" = Keyline Page 4061 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:05:37.83 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l *
  • Acquisition date 3-0CT-2016 07:01:40 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:42:00 Analyst initials: MXRl * *Sample ID G405235050 Sample Quantity 1.7160E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.255E+Ol 1.737E+OO CD-109 3.863E+OO 2.242E+OO SB-125 2.599E-01 2.454E-01 SN-126 2.459E-01 1.427E-01 BA-137M 6.642E-02 6.180E-02 CS-137 7.016E-02 6.529E-02 TL-208 2.315E-01 8.647E-02 PB-210 3. 32 6E+OO 6.086E+OO BI-211 9.855E-01 9.959E-01 PB-212 8.007E-01 1. 717E-01 BI-214 7.246E-01 l.907E-01 PB-214 9.503E-01 1.835E-01 RN-222 7.246E-01 1.907E-01 RA-226 7.246E-01 1.907E-01 AC-228 1.053E+OO 3.398E-01 RA-228 1.053E+OO 3.398E-01 TH-228 8.007E-01 1. 717E-01 TH-230 7.244E-01 1.906E-01 TH-232 1.053E+OO 3.398E-01 TH-234 2.540E+OO 2.882E+OO U-234 7.244E-01 1.906E-01 U-235 7.049E-02 1. 766E-01 U-238 2.540E+OO 2.882E+OO AM-243 2.120E-01 8. 8 91E-02 ANH-511 5.738E-02 7.781E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 4062 of 5809 Key-Line Activity (pCi/GRAM 5.186E-01 8.759E-04 O.OOOE+OO -2.649E-02 -1.420E-01 K.L. Cnt Uncert (1.96-sigma) l.085E+Ol 5.428E-02 1. 960E+41 3.778E-02 3.637E-01 MDA (pCi/GRAM 8.223E-01 1.569E+OO 2.009E-01 1.124E-01 8.421E-02 8.896E-02 6.129E-02 4.500E+00 3.467E-01 l.140E-01 1.197E-01 3.357E-01 1.197E-01 1.197E-01 2.708E-01 2.708E-01 l.140E-01 1.197E-01 2.708E-01 l.919E+00 1.197E-01 3.540E-01 l.919E+OO 7.184E-02 6.892E-02 MDA (pCi/GRAM 2. 321E+Ol l.152E-01 O.OOOE+OO 6.149E-02 6.838E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 O.OOOE+OO 1.680E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3. 971E+02 O.OOOE+OO SHORT HLIF MN-54 -2.864E-02 7.340E-02 l.361E-01 NOT IDENT. C0-56 -5.145E-02 5.192E-01 l.033E+OO FAIL ABUN MN-56 0.000E+OO 1. 960E+41 0.000E+OO SHORT HLIF C0-57 -6.166E-03 3.951E-02 7.917E-02 NOT IDENT. C0-58 1.804E-01 4.878E-01 1.136E+00 NOT IDENT. FE-59 6.390E-01 7.582E+OO l.642E+Ol NOT IDENT. C0-60 -1.833E-02 3.382E-02 6.445E-02 NOT IDENT. ZN-65 4.087E-02 1. 851E-01 3.782E-01 NOT IDENT. GE-68 -3.244E-01 2.487E+OO 4.885E+OO NOT IDENT. AS-73 -4.126E+OO 6.353E+OO 1.300E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.176E+03 O.OOOE+OO SHORT HLIF SE-75 -6.605E-03 2.268E-01 4.012E-01 NOT IDENT. BR-77 0.000E+OO 4.008E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.294E+02 O.OOOE+OO SHORT HLIF RB-83 1.325E-01 5.587E-01 l.250E+OO NOT IDENT. KR-85 3.824E+OO 7.365E+OO 1.505E+Ol NOT IDENT. SR-85 4.066E-01 7.853E-01 1.605E+OO NOT IDENT. RB-86 0.000E+OO 3.046E+04 O.OOOE+OO SHORT HLIF Y-88 -6. 631E-02 2.108E-01 4.436E-01 FAIL ABUN Y-91 l.459E+02 6.492E+02 1.399E+03 NOT IDENT. NB-94 5. 731E-03 3.353E-02 6.457E-02 NOT IDENT. NB-95 5.050E-01 1.053E+OO 1.852E+OO NOT IDENT. NB-95M -1.150E-01 2.496E+00 4.409E+OO NOT IDENT. ZR-95 3.079E-01 1.687E+OO 3.393E+OO NOT IDENT. NB-97 0.000E+OO 1. 816E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.077E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.673E-02 2.826E-02 5.204E-02 NOT IDENT. RH-102 -2.757E-02 6.786E-02 1.131E-01 NOT IDENT. RU-103 3.330E+OO 4.878E+OO 1.155E+Ol FAIL ABUN RH-106 -1. 784E-02 5.749E-01 1. l 72E+OO NOT IDENT. RU-106 -1. 784E-02 5.749E-01 1. l 72E+OO NOT IDENT. AG-108M -1.800E-02 2. 331E-02 4. 351E-02 NOT IDENT. AG-llOM 5.908E-03 1.134E-01 2.321E-01 FAIL ABUN SN-113 -1. 2 67E-01 2.203E-01 4.284E-01 NOT IDENT. CD-115 O.OOOE+OO 4. ll 7E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.980E+04 O.OOOE+OO SHORT HLIF TE-123M -8.092E-02 l.130E-01 2.087E-01 NOT IDENT. SB-124 -1.059E+OO 1.467E+OO 1.416E+OO NOT IDENT. TE-125M 2.075E+02 2.485E+02 5.384E+02 NOT IDENT. I-126 0.000E+OO 1.167E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.261E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.050E+22 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 5.900E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 911E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.708E+26 O.OOOE+OO SHORT HLIF BA-133 -l.023E-02 4.627E-02 7.735E-02 FAIL ABUN I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 1.009E-01 l.519E-01 FAIL ABUN CS-135 -3. 451E-02 1.415E-01 2.420E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.636E+05 O.OOOE+OO SHORT HLIF CE-139 -5.049E-02 8.923E-02 1.673E-01 NOT IDENT. BA-140 O.OOOE+OO 1.290E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.995E+05 O.OOOE+OO SHORT HLIF CE-141 -l.165E+Ol 2.362E+Ol 4.384E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.669E+41 O.OOOE+OO SHORT HLIF CE-144 -1.069E-01 3.257E-01 6.342E-01 FAIL ABUN PM-144 -9.170E-04 5.191E-02 9.768E-02 NOT IDENT. PR-144 -5.838E-02 4.516E+OO 8.508E+OO NOT IDENT. PM-146 -2.352E-02 4.604E-02 8.884E-02 NOT IDENT. ND-147 O.OOOE+OO 3.648E+07 O.OOOE+OO SHORT HLIF PM-147 4.273E+02 6.682E+02 1. 441E+03 NOT IDENT. PM-149 0.000E+OO 6.313E+40 O.OOOE+OO SHORT HLIF EU-150 l.233E-02 2.643E-02 5.344E-02 FAIL ABUN EU-152 -1.903E-02 9.506E-02 l.756E-01 FAIL ABUN GD-153 -2.205E-01 1. 651E-01 2.727E-01 NOT IDENT. EU-154 -l.454E-03 1.321E-01 2.790E-01 NOT IDENT. EU-155 l.191E-01 9.630E-02 2.150E-01 FAIL ABUN TB-160 -1.134E+OO 2.083E+OO 3. 713E+OO FAIL ABUN H0-166M 1.215E-02 6.496E-02 l.352E-01 FAIL ABUN TM-171 3.224E+OO l.481E+Ol 3.277E+Ol NOT IDENT. HF-172 3.257E-02 1. 921E-01 3.950E-01 FAIL ABUN LU-172 -1.693E-03 7.624E-02 1.555E-01 FAIL ABUN LU-176 -1. 7 61E-03 2.815E-02 4.885E-02 FAIL ABUN Page 4063 of 5809 HF-181 -8. 911E-01 4.476E+OO 9.045E+OO NOT IDENT. TA-182 2.495E-01 8.907E-01 2.025E+OO FAIL ABUN RE-183 1.068E+OO 2.222E+OO 4. 968E+OO NOT IDENT. RE-184 2.926E+Ol 2.914E+Ol 7.270E+Ol NOT IDENT. W-188 1. 966E+Ol 1.146E+02 2. 096E+02 FAIL ABUN IR-192 -1.459E-01 3.695E-01 6.746E-01 FAIL ABUN HG-203 -4.548E-01 2.344E+OO 4.397E+OO NOT IDENT. BI-207 -4.601E-03 6.561E-02 1.258E-01 FAIL ABUN PB-211 8.667E-02 6.513E-01 1.387E+OO FAIL ABUN BI-212 1.016E+OO
  • 7.686E-01 1.418E+OO FAIL ABUN RN-219 -1.212E-01 3.718E-01 7. 451E-01 FAIL ABUN RA-223 6.744E-02 6.119E-01 1.103E+OO FAIL ABUN RA-224 5.292E-01 7.537E-01 1.408E+OO NOT IDENT. AC-227 -1.323E-01 2.415E-01 3.925E-01 FAIL ABUN TH-227 -1.323E-01 2.415E-01 3.925E-01 FAIL ABUN TH-229 -8. 710E-03 4.030E-01 7.918E-01 FAIL ABUN PA-231 2.909E-01 5.052E-01 9.602E-01 NOT IDENT. TH-231 6.744E-02 6 .119E-01 1.103E+OO FAIL ABUN PA-233 -4.939E-02 5.971E-02 9.985E-02 NOT IDENT. PA-234 4.934E-02 3.090E-01 6.449E-01 NOT IDENT. PA-234M 1.565E+OO 4.278E+OO 9.702E+OO NOT IDENT. NP-237 -4.939E-02 5.971E-02 9.985E-02 NOT IDENT. NP-238 O.OOOE+OO 1.454E+41 O.OOOE+OO SHORT HLIF NP-239 -9.777E-02 2.083E-01 4.058E-01 FAIL ABUN PU-239 2.082E+02 2.717E+02 5.808E+02 NOT IDENT. AM-241 -4.695E-02 1. 066E-01 2.036E-01 NOT IDENT. CM-243 -3.837E-02 8.216E-02 1.618E-01 FAIL ABUN BK-247 9. 963E-04 7.866E-02 1. 399E-01 NOT IDENT. CM-247 -1.347E-02 3.376E-02 6.705E-02 NOT IDENT. CF-249 1.280E-02 3.812E-02 8.234E-02 NOT IDENT. CF-251 2.427E-02 1.020E-01 2.063E-01 FAIL ABUN Page 4064 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:05:35.56 Nuclide Line Activity Report Nuclide.Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 200 10.66* 6.546E-01 l.255E+Ol 1.255E+Ol 14.12 CD-109 88.03 109 3.70* 4.297E+OO 3.005E+OO 4. 721E+OO 47.47 SB-125 176.31 ------6.89 4.460E+OO ------Line Not Found ------321.04 ------0.42 2.640E+OO ------Line Not Found ------427.87 29 29.80* 2.005E+OO 2 .114E-01 2.599E-01 96. 33 463.37 ------10.56 1.852E+OO ------Line Not Found ------600.60 13 17.77 l.455E+00 2.187E-01 2.689E-01 220.01 635.95 6 11. 29 1.385E+OO l.604E-01 1. 972E-01 248.20 SN-126 64.28 53 9.60 2.468E+OO 9.790E-01 9.790E-01 115. 79 86.94 109 8.90 4.297E+00 l.249E+OO 1.249E+OO 47.47 87.57 109 37.00* 4.297E+OO 3.005E-01 3.005E-01 47.47 BA-137M 661. 66 18 89.90* 1.334E+OO 6.517E-02 6.642E-02 94.95 CS-137 661. 66 18 85.10* l.334E+00 6.884E-02 7.016E-02 94.95 TL-208 277.37 ------6.60 3.041E+OO ------Line Not Found ------583.19 67 85.00* 1.496E+OO 2.315E-01 2.315E-01 38 .11 860.56 ------12.50 1.058E+OO ------Line Not Found ------PB-210 46.54 26 4.25* 8.252E-01 3.242E+OO 3.326E+OO 186.69 BI-211 72.87 ------1. 23 3.327E+OO ------Line Not Found ------351.06 187 12.92* 2.415E+OO 2.618E+OO 2.618E+OO 19.71 PB-212 74.82 141 10.28 3.486E+OO 1.720E+OO 1.720E+OO 32.87 77 .11 189 17.10 3.657E+OO 1.319E+OO 1.319E+OO 25.66 238.63 279 43.60* 3.500E+OO 8.007E-01 8.007E-01 21.88 300.09 ------3.30 2.819E+OO ------Line Not Found ------BI-214 609.32 108 45.49* 1.437E+OO 7.244E-01 7.246E-01 26.85 1120.29 17 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 1764.49 8 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 PB-214 74.82 141 5.80 3.486E+OO 3.048E+OO 3.049E+00 32.87 77 .11 189 9.70 3.657E+OO 2.325E+00 2.326E+OO 25.66 87.09 109 3.41 4.297E+OO 3.260E+OO 3.262E+OO 47.47 242.00 ------7.25 3.455E+OO ------Line Not Found ------295.22 71 18.42 2.863E+OO 5.924E-01 5.926E-01 53.64 351. 93 187 35.60* 2.415E+OO 9.500E-01 9.503E-01 19. 71 RN-222 609.32 108 45.49* 1.437E+OO 7.244E-01 7.246E-01 26.85 1120.29 17 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 1764.49 8 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 RA-226 609.32 108 45.49* 1.437E+OO 7.244E-01 7.246E-01 26. 85 1120.29 17 14.92 8.373E-01 5.866E-01 5.868E-01 88.76 1764.49 8 15.30 5.418E-01 4.384E-01 4.386E-01 132.56 AC-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 41 11.27 2.506E+OO 6.299E-01 6.299E-01 75.66 794.95 33 4.25 1.134E+OO 2. 961E+OO 2. 961E+OO 53.09 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 62 25.80* 1.006E+OO 1.053E+OO 1.053E+OO 32.94 968. 97 36 15.80 9.525E-01 1.059E+OO 1.059E+OO 36.92 RA-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 41 11. 27 2.506E+OO 6.299E-01 6.299E-01 75.66 794.95 33 4.25 1.134E+OO 2. 961E+OO 2.961E+OO 53.09 Page 4065 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 835.71 ------1. 61 1.085E+OO ----.--Line Not Found ------911.20 62 25.80* 1. 006E+OO 1.053E+OO 1.053E+OO 32.94 968. 97 36 15.80 9.525E-01 1.059E+OO 1.059E+OO 36.92 TH-228 74.82 141 10.28 3.486E+OO 1. 720E+OO 1.720E+00 32.87 77 .11 189 17.10 3.657E+OO 1.319E+OO 1.319E+OO 25.66 238.63 279 43.60* 3.500E+OO 8.007E-01 8.007E-01 21. 88 300.09 ------3.30 2.819E+OO ------Line Not Found ------TH-230 609.32 108 45.49* 1.437E+OO 7.244E-01 7.244E-01 26.85 1120.29 17 14.92 8.373E-01 5.866E-01 5.866E-01 88.76 1764.49 8 15.30 5.418E-01 4.384E-01 4. 384E-01* 132.56 TH-232 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 41 11.27 2.506E+00 6.299E-01 6.299E-01 75.66 835. 71 ------1. 61 1.085E+OO ------Line Not Found ------911. 20 62 25.80* 1.006E+OO l.053E+OO 1.053E+00 32.94 968.97 36 15.80 9.525E-01 l.059E+00 l.059E+00 36.92 TH-234 63.29 53 3.70* 2.468E+OO 2.540E+OO 2.540E+OO 115. 79 92.59 83 4.23 4.552E+OO 1.892E+OO l.892E+00 57.46 U-234 609.32 108 45.49* 1.437E+OO 7.244E-01 7.244E-01 26.85 1120. 29 17 14.92 8.373E-01 5.866E-01 5.866E-01 88.76 1764.49 8 15.30 5.418E-01 4.384E-01 4.384E-01 132. 56 U-235 89. 96 50 3.47 4.418E+OO l.428E+00 1.428E+OO 39.64 93.35 83 5.60 4.552E+00 1.429E+OO 1.429E+OO 57.46 143.76 ------10. 96* 4.954E+OO ------Line Not Found ------163.33 ------5.08 4.674E+00 ------Line Not Found ------185. 72 80 57.20 4.296E+OO L 429E-01 l.429E-01 59.00 205.31 ------5.01 3.984E+OO ------Line Not Found ------U-238 63.29 53 3.70* 2.468E+OO 2.540E+OO 2.540E+OO 115. 79 92.59 83 4.23 4.552E+00 1.892E+OO 1.892E+OO 57.46 AM-243 43.53 ------5.90 5.957E-01 ------Line Not Found ------74.66 141 67.20* 3.486E+OO 2.631E-01 2.631E-01 32.87 ANH-511 511. 00 22 100.00* 1.690E+OO 5.738E-02 5.738E-02 138.38 Flag: "*" Key line Page 4066 of 5809
    • Page : 3 Summary of Nuclide Activity Sample ID : G405235050 Acquisition date 3-0CT-2016 07:01:40 Total number of lines in spectrum 43 Number of unidentified lines 7 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 CD-109 SB-125 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 461.40D 2.76Y 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 22.20Y 7.04E+08Y 1.41E+10Y 1600. DOY 1600.00Y 1600. ODY 1600. DOY 1.41E+10Y 1.41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1. 00E+09Y Decay 1. 00 1. 57 1.23 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity . Uncorrected pCi/GRAM l.255E+Ol 3.005E+OO 2 .114E-01 3.005E-01 6.517E-02 6.884E-02 2.315E-01 3.242E+OO 2.618E+OO 8.007E-01 7.244E-01 9. 5.00E-01 7.244E-01 7.244E-01 1.053E+OO 1.053E+OO 8.007E-01 7.244E-01 1.053E+OO 2.540E+OO 7.244E-01 1.429E-01 2.540E+00 2. 631E-01 5.738E-02 3.717E+Ol 3.717E+Ol Decay Corr pCi/GRAM 1.255E+Ol 4. 721E+OO 2.599E-01 3.005E-01 6.642E-02 7.016E-02 2.315E-01 3.326E+OO 2.618E+OO 8.007E-01 7.246E-01 9.503E-01 7.246E-01 7.246E-01 l.053E+OO 1.053E+OO 8.007E-01 7.244E-01 1.053E+OO 2.540E+OO 7.244E-01 1.429E-01 2.540E+OO 2. 631E-01 5.738E-02 3.902E+Ol 3.902E+Ol 83. 72% Decay Corr 2-Sigma Error 0.177E+Ol 2.241E+OO 2.504E-01 l.427E-01 6.306E-02 6.662E-02 0.882E-01 6.210E+OO 0.516E+OO 1. 7 52E-01 1.945E-01 1. 873E-01 1.945E-01 1.945E-01 0.347E+OO 0.347E+OO 1. 7 52E-01 1.945E-01 0.347E+OO 2. 941E+OO 1.945E-01 0.843E-01 2. 941E+OO 0.865E-01 7.940E-02 "M" Manually accepted 2-Sigma %Error 14:12 47.47 96.33 47.47 94.95 94.95 38 .11 186.69 19. 71 21. 88 26.85 19. 71 26. 85 26. 85 32.94 32.94 21. 88 26. 85 32.94 115. 79 26. 85 59.00 115.79 32.87 138.38 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4067 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235050 Acquisition date : 3-0CT-2016 07:01:40 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 2 80.83 25 96 1. 05 161.63 144 21 4.90E-03 **** 3.91E+OO T 0 227.19 32 63 1. 71 454.36 451 8 7.05E-03 **** 3.66E+OO T 0 262.50 35 121 6.92 524.99 513 19 7.87E-03 **** 3.20E+OO 0 270.55 28 37 1. 43 .541. 09 538 6 6.30E-03 87.3 3. llE+OO T
  • 0 303.06 47 119 7.57 606.11 596 20 1.08E-02 **** 2.79E+OO T 0 327.54 39 42 0.88 655.06 650 10 9.lOE-03 77.3 2.59E+OO T 9 350.03 12 8 1. 76 700.05 699 12 2.73E-03 95.1 2.43E+OO 2 587.54 14 19 1. 43 1175.00 1158 22 3.41E-03 **** 1. 49E+OO 0 700.74 8 15 0. 96 1401. 36 1395 10 2.17E-03 **** 1.27E+OO 0 727.85 19 9 1. 27 1455.57 1451 9 4.89E-03 77.2 1. 23E+OO T 0 763.74 10 15 4.41 1527.33 1519 14 2.50E-03 **** 1.17E+OO T 0 768.42 16 4 1. 48 1536.69 1533 7 4.09E-03 66.7 1.17E+00 0 897.43 7 9 0.68 1794.64 1789 9 1. 8 6E-03 **** 1.02E+OO T 0 955.36 14 0 1. 50 1910.46 1905 10 3. 61E-03 55.5 9.65E-01 T 0 965. 4 8 13 8 1.11 1930.69 1925 10 3.47E-03 99.6 9.56E-01 T 0 1019.06 16 0 4.53 2037.81 2031 13 4.44E-03 50.0 9. llE-01 0 1239.25 8 11 1. 27 2478.00 2471 11 2.22E-03 **** 7.64E-01 T 0 1305.01 7 4 0. 96 2609.47 2605 9 2.08E-03 **** 7.28E-01 Flags: "T" Tentatively associated Page 4068 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:05:49.60 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l *
  • Acquisition date 3-0CT-2016 07:01:40 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:42:00 Nuclide Library : SOLID *
  • Sample ID G405235050 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity : 1.7160E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 * * , Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SB-125 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.252E-01 7.204E-01 8.759E-02 5.210E-02 3.688E-02 3.896E-02 2.578E-02 2.062E+OO l.533E-01 5.285E-02 5.042E-02 1.606E-01 5.042E-02 5.042E-02 1.119E-01 l .119E-01 5.285E-02 5. 041E-02 l .119E-01 8.876E-01 5. 041E-02 1. 651E-01 8.876E-01 3. 311E-02 3.079E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4069 of 5809 Le (pCi/GRAM 9.944E+00 4.750E-02 O.OOOE+OO l.943E-02 2.704E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4070 of 5809 O.OOOE+OO 5.707E-02 4.319E-01 O.OOOE+OO 3.639E-02 4.634E-01 6.849E+OO 2.283E-02 l.557E-01 l.97'1E+OO 5.925E+OO O.OOOE+OO 1.813E-01 O.OOOE+OO O.OOOE+OO 5.320E-01 6.629E+OO 7.066E-01 O.OOOE+OO 1.402E-01 5.951E+02 2.742E-02 7. 901E-01 2.017E+00 1.450E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.380E-02 4.735E-02 4.978E+OO 5.088E-01 5.088E-01 l.825E-02 9.733E-02 1. 871E-01 O.OOOE+OO 0.000E+OO 9.507E-02 O.OOOE+OO 2.511E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.421E-02 O.OOOE+OO 6.764E-02 1.084E-01 O.OOOE+OO O.OOOE+OO 7.575E-02 O.OOOE+OO O.OOOE+OO 2.028E+Ol 0.000E+OO 2.932E-01 4.023E-02 3.506E+OO 3.880E-02 O.OOOE+OO 6.649E+02 O.OOOE+OO 2. 411E-02 7.780E-02 l.251E-01 1.148E-01 1.005E-01 1.508E+OO 5.851E-02 1.504E+Ol l.823E-01 6.250E-02 2.199E-02 3. 931E+OO SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 .RN-219 RA-223 RA-224 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4071 of 5809 8.341E-01 2.291E+OO 3.066E+Ol 9.408E+Ol 2.894E-01 l.974E+OO 5.349E-02 6.151E-01 6.340E-01 3.280E-01 4.915E-01 6.596E-Ol 1. 759E-01 1. 759E-01 3.612E-01 4.382E-01 4.915E-01 4.390E-02 2.703E-01 4.070E+OO 4.390E-02 O.OOOE+OO 1.868E-01 2.703E+02 9.303E-02 7.444E-02 6.333E-02 2.943E-02 3.684E-02 9.480E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:05:54.96 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235050.CNF;l *
  • Acquisition date 3-0CT-2016 07:01:40 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.33 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:42:00 Nuclide Library : SOLID *
  • Sample ID G405235050 Analyst initials: MXRl * *Batch Number 1596252 Sample Quantity : 1.7160E+02 GRAM *
  • Quantity Err(%) : 1.1655E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date : 1-JUN-2016 09:39:12 Eff. Geometry : CAN' *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.255E+Ol 1.856E+OO l.856E+OO CD-109 3.863E+00 2.267E+OO 2.267E+OO SB-125 2.599E-01 2.456E-01 2.456E-01 SN-126 2.459E-01 1.437E-01 1.437E-01 BA-137M 6.642E-02 6.187E-02 6.187E-02 CS-137 7.016E-02 6.536E-02 6.536E-02 TL-208 2.315E-01 8.703E-02 8.703E-02 PB-210 3.326E+00 6.093E+OO 6.093E+OO BI-211 9.855E-01 l.002E+00 1.002E+OO PB-212 8.007E-01 1. 7 68E-01 l.768E-01 BI-214 7.246E-01 1.932E-01 l.932E-01 PB-214 9.503E-01 1.877E-01 l.877E-01 RN-222 7.246E-01 l.932E-01 l.932E-01 RA-226 7.246E-01 1.932E-01 1.932E-01 AC-228 1.053E+OO 3.441E-01 3.441E-01 RA-228 1.053E+OO 3.441E-01 3.441E-01 TH-228 8.007E-01 1.768E-01 1.768E-01 TH-230 7.244E-01 1. 931E-01 1. 931E-01 TH-232 1.053E+00 3.441E-01 3.441E-01 TH-234 2.540E+00 2.937E+OO 2.937E+OO U-234 7.244E-01 1. 931E-01 1.931E-01 U-235 7.049E-02 1. 766E-01 l.766E-01 U-238 2.540E+OO 2.937E+OO 2.937E+OO AM-243 2.120E-01 9.009E-02 9.009E-02 ANH-511 5.738E-02 7.785E-02 7.785E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1 . 96-sigma ) BE-7 5.186E-01 l.085E+Ol 1.085E+Ol NOT IDENT. NA-22 8.759E-04 5.428E-02 5.428E-02 NOT IDENT. NA-24 l.OOOE+41 6.064E+41 O.OOOE+OO SHORT HLIF AL-26 -2.649E-02 3.782E-02 3. 966E-02 NOT IDENT. SC-46 -1.420E-01 3.637E-01 3.693E-01 FAIL ABUN Page 4072 of 5809 V-48 2. 724E+03 1.680E+04 l.685E+04 SHORT HLIF CR-51 2.742E+02 3.973E+02 4.161E+02 SHORT HLIF MN-54 -2.864E-02 7.341E-02 7.454E-02 NOT IDENT. C0-56 -5.145E-02 5.192E-01 5.198E-01 FAIL ABUN MN-56 -1.000E+41 1.060E+42 0.000E+OO SHORT HLIF C0-57 -6.166E-03 3. 951E-02 3. 961E-02 NOT IDENT. C0-58 1.804E-01 4.879E-01 4.946E-01 NOT IDENT. FE-59 6.390E-01 7.582E+OO 7.588E+00 NOT IDENT. C0-60 -1.833E-02 3.383E-02 3.482E-02 NOT IDENT. ZN-65 _ 4. 087E-02 1.851E-01 l.860E-01 NOT IDENT. GE-68 -3.244E-01 2.487E+OO 2.491E+OO NOT IDENT. AS-73 -4.126E+OO 6.409E+OO 6.673E+OO NOT IDENT. AS-74 -5.756E+02 7.176E+03 7.181E+03 SHORT HLIF SE-75 -6.605E-03 2.268E-01 2.268E-01 NOT IDENT. BR-77 1.869E+38 l.623E+39 O.OOOE+OO SHORT HLIF SR-82 -6.093E+Ol 8.295E+02 8.299E+02 SHORT HLIF RB-83 1.325E-01 5.590E-01 5.622E-01 NOT IDENT. KR-85 3.824E+OO 7.366E+OO 7.565E+00 NOT IDENT. SR-85 4.066E-01 7.855E-01 8.066E-01 NOT IDENT. RB-86 -5. 591E+03 3.046E+04 3.057E+04 SHORT HLIF Y-88 -6. 631E-02 2.108E-01 2.129E-01 FAIL ABUN Y-91 1.459E+02 6.492E+02 6.525E+02 NOT IDENT. NB-94 5. 731E-03 3.353E-02 3.363E-02 NOT IDENT. NB-95 5.050E-01 l.053E+OO 1. 078E+OO NOT IDENT. NB-95M -l.150E-01 2. 496E+OO 2. 496E+OO NOT IDENT. ZR-95 3.079E-01 1.687E+OO 1.693E+OO NOT IDENT. NB-97 l.000E+41 l.816E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 3.256E+42 . 0: OOOE+OO SHORT HLIF M0-99 2.561E+32 2.085E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 2.569E+41 O.OOOE+OO SHORT HLIF RH-101 -2.673E-02 2.867E-02 3. llOE-02 NOT IDENT. RH-102 -2.757E-02 6.789E-02 6.902E-02 NOT IDENT. RU-103 3.330E+00 4.881E+OO 5.107E+OO FAIL ABUN RH-106 -1. 784E-02 5.749E-01 5.750E-01 NOT IDENT. RU-106 -1. 784E-02 5.749E-01 5.750E-01 NOT IDENT. AG-108M -1. 800E-02 2.332E-02 2.469E-02 NOT IDENT. AG-llOM 5.908E-03 l .134E-01 l.134E-01 FAIL ABUN SN-113 -1.267E-01 2.204E-01 NOT IDENT. CD-115 -9.636E+38 4.121E+39 O.OOOE+OO SHORT HLIF SN-ll 7M -3 .114E+04 8.987E+04 9.096E+04 SHORT HLIF TE-123M -8.092E-02 l.130E-01 l.188E-01 NOT IDENT. SB-124 -1.059E+OO 1. 468.E+OO 1.544E+OO NOT IDENT. TE-125M 2.075E+02 2.488E+02 2.658E+02 NOT IDENT. I-126 1. 293E+06 1.180E+06 l.316E+06 SHORT HLIF SB-126 -5.115E+05 l.264E+06 1. 285E+06 SHORT HLIF SB-127 -2.163E+22 4.266E+22 O.OOOE+OO SHORT HLIF I-131 1. 759E+09 5.900E+09 5.953E+09 SHORT HLIF I-132 -l.000E+41 1.863E+42 0.000E+OO SHORT HLIF TE-132 8.409E+26 9.358E+26 O.OOOE+OO SHORT HLIF BA-133 -1.023E-02 4.627E-02 4.650E-02 FAIL ABUN I-133 1.000E+41 2.748E+41 O.OOOE+OO SHORT HLIF CS-134 1. 940E-01 1.013E-01 1.338E-01 FAIL ABUN CS-135 -3.451E-02 l.415E-01 l.424E-01 NOT IDENT. I-135 -1. OOOE+41 7.670E+41 O.OOOE+OO SHORT HLIF CS-136 -1.827E+05 3. 641E+05 3.733E+05 SHORT HLIF CE-139 -5.049E-02 8.980E-02 9. 2 64E-02 NOT IDENT. BA-140 -6.535E+05 l.290E+06 l.324E+06 SHORT HLIF LA-140 -2.890E+05 4.997E+05 5.164E+05 SHORT HLIF CE-141 -1.165E+Ol 2.'362E+Ol 2.420E+Ol NOT IDENT. CE-143 1.000E+41 1. 673E+41 O.OOOE+OO SHORT HLIF CE-144 -l.069E-01 3.258E-01 3.293E-01 FAIL ABUN PM-144 -9.170E-04 5.191E-02 5 .191E-02 NOT IDENT. PR-144 -5.838E-02 4.516E+OO 4.516E+OO NOT IDENT. PM-146 -2.352E-02 4.607E-02 4. 727E-02 NOT IDENT. ND-147 1.322E+07 3.649E+07 3.697E+07 SHORT HLIF PM-147 4.273E+02 6.685E+02 6.957E+02 NOT IDENT. PM-149 -2.438E+40 6.335E+40 0.000E+OO SHORT HLIF EU-150 l.233E-02 2.643E-02 2. 701E-02 FAIL ABUN EU-152 -1.903E-02 9.507E-02 9.545E-02 FAIL ABUN GD-153 -2.205E-01 l.656E-01 l.931E-01 NOT IDENT. EU-154 -1.454E-03 1.321E-01 l.321E-01 NOT IDENT. EU-155 1.191E-01 9.667E-02 l.106E-01 FAIL ABUN TB-160 -1.134E+OO 2.084E+OO 2.146E+OO FAIL ABUN H0-166M 1.215E-02 6.496E-02 6.519E-02 FAIL ABUN TM-171 3.224E+OO 1.481E+Ol l.488E+Ol NOT IDENT. HF-172 3.257E-02 l.922E-01 l.928E-01 FAIL ABUN LU-172 -1.693E-03 7.624E-02 7.624E-02 FAIL ABUN LU-176 -1. 761E-03 2.815E-02 2.816E-02 FAIL ABUN Page 4073 of 5809 HF-181 -8. 911E-01 4.477E+OO 4.495E+OO NOT IDENT. TA-182 2.495E-01 8.908E-01 8.979E-01 FAIL ABUN RE-183 l.068E+OO 2.228E+OO 2.279E+OO NOT IDENT. RE-184 2.926E+Ol 2.997E+Ol 3.275E+Ol NOT IDENT. W-188 1. 966E+Ol l.146E+02 l.150E+02 FAIL ABUN IR-192 -l.459E-01 3.696E-01 3.754E-01 FAIL ABUN HG-203 -4.548E-01 2.344E+OO 2.353E+OO NOT IDENT. BI-207 -4.601E-03 6.561E-02 6.565E-02 FAIL ABUN PB-211 8.667E-02 6.513E-01 6.525E-01 FAIL ABUN BI-212 l.016E+OO
  • 7.703E-01 8. 961E-01 FAIL ABUN RN-219 -1. 212E-01 3.721E-01 3. 761E-01 FAIL ABUN RA-223 6.744E-02 6 .119E-01 6.126E-01 FAIL ABUN RA-224 5.292E-01 7.542E-01 7.910E-01 NOT IDENT. AC-227 -l.323E-01 2.421E-01 2.493E-01 FAIL ABUN TH-227 -l.323E-01 2.421E-01 2.493E-01 FAIL ABUN TH-229 -8.710E-03 4.030E-01 4.030E-01 FAIL ABUN PA-231 2.909E-01 5.090E-01 5.257E-01 NOT IDENT. TH-231 6.744E-02 6.119E-01 6.126E-01 FAIL ABUN PA-233 -4.939E-02 5.976E-02 6.377E-02 NOT IDENT. PA-234 4.934E-02 3.141E-01 3.149E-01 NOT IDENT. PA-234M 1. 565E+OO 4.279E+OO 4.336E+OO NOT IDENT. NP-237 -4.939E-02 5.976E-02 6.377E-02 NOT IDENT. NP-238 l.OOOE+41 l.455E+41 O.OOOE+OO SHORT HLIF NP-239 -9.777E-02 2.085E-01 2 .131E-Ol FAIL ABUN PU-239 2.082E+02 2.719E+02 2.876E+02 NOT IDENT. AM-241 -4.695E-02 l.067E-01 l.087E-01 NOT IDENT. CM-243 -3.837E-02 8.224E-02 8.404E-02 FAIL ABUN BK-2'47 9.963E-04 7. 8 66E-02 7'. 866E-02 NOT IDENT. CM-247 -l.347E-02 3.384E-02 3.438E-02 NOT IDENT. CF-249 l.280E-02 3.813E-02 3.857E-02 NOT IDENT. CF-251 2.427E-02 1. 021E-01 l.026E-01 FAIL ABUN Page 4074 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 6.2529 87.09 54.0667 136.47 43.5320 45.60 40 .1511 87.57 54.1243 140.51 0.0000 46.54 40.2801 88.03 42.4010 143.76 54.8029 49.72 0.0000 88.34 42.4299 144.24 52.8852 51. 35 32.8973 88.47 42.4420 145.44 59.8523 51. 87 38.5774 89. 96 49.6772 152.43 58.5067 52.39 37.8354 1093.63 49.7505 153.25 0.0000 52.97 43.5493 91.11 0.0000 323.87 47.7246 53.44 46.8436 92.59 49.9587 156.02 0.0000 54.07 41. 2700 93.35 50.0395 158.56 0.0000 57.36 0.0000 94.56 50.1672 159.00 48.0608 57.53 40.0665 94.65 50.1766 162.33 46.2787 57.98 38.4817 94. 67 50.1788 162.66 0.0000 59.27 58.0766 94.87 49.0045 163.33 44.3297 59.32 58.0849 97.43 61. 2810 165.86 40.4437 59.54 46.0588 98.43 46.9580 176.31 46.1563 60. 96 48.4482 98.44 46.9592 176.60 0.0000 61.17 46.2735 99.53 41. 6328 177.52 39. 0396 62.93 50.6541 100 .11 41. 6815 181.07 0.0000 63.29 50.7045 102.03 48.2092 181.52 38. 2138 63.58 50.7451 103.18 59.2593 184.41 41. 4685 64.28 50.8427 103.37 52.8975 143.76 34.2694 66.73 58.1720 105.21 43.0197 193.51 36.7085 67.24 57.1306 105.31 43.0284 197.03 45.2964 125.81 51.3091 106.12 53.1820 198.01 33.7500 67.75 51.3184 106.47 69.7343 201.83 50.8616 69.67 56.6504 109.28 47.0475 203.43 39.2820 70.83 56.5364 111. 00 60.1569 205.31 46.8192 72.81 46.0252 111.76 0.0000 210.85 55. 6967 72.87 46.0322 114. 06 55.8458 215.65 29.0814 74.66 46.2377 116. 30 0.0000 222 .11 37.9774 74.82 46.2559 116.74 54.2484 227.09 34.9165 74.97 46.2732 119.76 43.2580 227.38 34.9277 77 .11 46.5150 121.12 43.3622 228.16 0.0000 78.74 46.6971 121.22 36.7702 228.18 30.5891 79.69 46.8026 121.78 42.4687 116.74 30.5891 80.12 46.8500 122.06 46.2665 235.69 39.6530 80.19 0.0000 122.92 51.0642 235. 96 36.7264 80.57 46.8994 123.07 51.0774 238.63 54.1433 81. 00 46.9468 265.00 55.8662 238.98 0.0000 81. 07 46.9542 125.81 44.6672 240.99 56.1256 81. 75 55.7378 127.23 56.2071 242.00 45.8359 83.79 61.2500 127.91 47.6885 244.70 33.3627 84.00 42.0201 129.30 44.9324 252.40 0.0000 85.43 81.9707 131.20 46.9940 252.80 25.7939 86.55 54.0017 133.02 50.0211 254.15 0.0000 86.79 54.0303 133.52 56.8015 256.23 34.5122 86.94 54.0485 136.00 43.4990 260.90 0.0000 Page 4075 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 30.2653 355.39 0.0000 584.27 9.4914 264. 80 30.2694 356.01 22.9585 595.83 0.0000 265.00 30.2751 364.49 0.0000 427.87 9.5732 .268.22 28.8525 366.42 0.0000 602.52 0.0000 269.46 27.3677 372. 51 21.1774 604.72 8.6342 270.0;3 30.8051 375.05 23. 7146. 607.14 5.7632 271.23 41.1218 377.52 12.5046 609.32 9.6163 273. 65 0.0000 356.01 21. 7772 610.33 9. 6212 276.40 30.9955 388.16 20.1660 614.28 5.7844 277.37 32.1733 388.63 0.0000 618.01 20.2839 277.60 31.0309 391.69 22.7455 620.36 12. 5715 278.00 26.4442 264.66 21.1980 621.93 13.5494 279.20 28.7766 401.81 22.0645 630.19 0.0000 279.54 32.2400 402.40 22.0734 631.29 13 .1270 279.70 28.7903 404.85 17.0093 633.25 8.7598 280.46 26.5060 410.95 14.5205 634.78 0.0000 283.69 15.0273 413.71 14.5485 635.95 11. 6953 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 28.9452 423. 72 0.0000 645.85 7.8350 285.90 0.0000 427.09 15.5475 657.76 8.8656 287.50 20.8812 427.87 15.5559 657.90 0.0000 290.67 23.2697 433.94 16.4878 661. 66 16.7773 293.27 0.0000 439.40 21.7738 664.57 0.0000 351. 93 29.5978 453.88 21.9823 666.33 0.0000 295.96 29.6171 463.37 19.4631 666.50 0.0000 879.38 *32.8125 468.07 12.4229 667.71 0.0000 299.98 26. 5964 473.00 0.0000 677.62 11. 9331 300.09 26.5992 475.06 11. 58 66' 685.70 0.0000 300.13 26.5999 476.78 11. 5990 695.00 0.0000 301.36 26.6289 477.60 11. 6048 696.49 7.5241 302.85 26.6649 482.18 17.0092 696. 51 7.5241 256.23 26.7036 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 7.5269 306.78 28.3323 497.08 7.2274 697.49 9.0330 308.46 31.5267 505.52 19.0684 702.65 9.0542 311. 90 29.6455 507.63 0.0000 706.68 12.0947 316.51 16.6677 511. 00 23.6855 711. 68 12.1221 319.41 0.0000 514.00 12.3201 720.70 0.0000 320.08 0.0000 514.00 12.3201 721. 93 0.0000 321. 04 25.0990 520.40 7.3281 722.78 9.7461 323.87 20.7669 520.69 0.0000 722.91 13.7060 325.23 23.9893 522.65 0.0000 723.31 12.1855 328.76 0.0000 527.90 0.0000 724 .19 7.6190 333.37 21.7375 528.26 13.8031 727.33 8.1383 333.97 21.7485 529.59 11. 0508 733.00 6.1189 334.37 25.7845 529.87 0.0000 735.93 15.3174 338.28 20.6134 531.02 0.0000 333.97 8.1748 338.32 20.6140 537.26 0.0000 739.50 0.0000 311. 90 30.7729 546.56 0.0000 747.24 9.2358 340.48 30.7729 552.55 15.8600 748.06 11.2923 340.55 0.0000 563.25 15.0150 752.31 14.3982 344.28 23.1510 569.33 6.5910 753.82 0.0000 345.93 19.5215 946.00 5.6499 756.73 9.8922 351.06 19.6021 569.70 5.6504 7 56. 8*0 7.7283 351.93 19.6157 583.19 9.4861 884.68 10.8529 Page 4076 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 6.2065 1274.44 11. 2919 1620.50 3.0170 766.42 6.2083 1001.03 4.5241 1621. 92 3.0179 766.84 6.2092 1002.74 7.9217 1678.03 0.0000 772.60 0.0000 1004.73 6.7947 1690.97 2.0430 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0 .. 0000 1oa5.87 0.0000 1764.49 5. 18.83 778.90 7.2811 1028.54 0.0000 1063.66 6.2333 783.70 0.0000 1037.84 5. 7255 1771.35 3.1174 785.37 11.4727 1038.76 0.0000 1791.20 0.0000 792.07 6.2754 631.29 6.8901 1808.65 4.1887 794.95 6.2827 1048.07 0.0000 1810.72 0.0000 795.86 6.2852 1049.04 4.5970 1836.06 2.1061 810.06 3.1609 1050.41 4.5993 810.29 4.2148 1063.66 11.5479 344.28 4.2152 1077.00 0.0000 810.76 4.2157 1077.34 6.9590 815.77 0.0000 1085.87 6.9780 1048.07 0.0000 1093.63 5.8293 832.01 8.5036 1099.45 7.8843 834.85 12.7700 1112. 07 6.1562 835.71 12.7744 1112. 84 7.0376 836.80 0.0000 1115. 54 5.6348 846.75 0.0000 1120.29 7.9354 846.77 9.6226 1120.55 7.9360 856.80 0.0000 1221.41 11. 2898 860.56 12.8989 1129. 67 11. 4956 871.09 14.0304 1131. 51 0.0000 873.19 8.6410 1147.95 0.0000 875.33 0.0000 1173.23 8. 9600 879.38 10.8268 1177.95 12.5619 880.51 7.5819 1189.05 15.3035 883.24 7.5899 1204.77 9.0436 884.68 8.6787 1221.41 5.4525 889.28 7.6073 1231. 02 5.4675 894.76 8.1674 1235.36 0.0000 898.04 4.9063 1238.28 7.3052 900. 72 9.8225 1260.41 0.0000 903.28 2.6219 1271.87 6.4523 911.20 7.6694 1274.44 7.3794 912.08 6.5759 1274.54 7.3799 923.98 0.0000 1291.59 4.6341 926.50 6.6106 1298.22 0.0000 929 .11 12 .1311 1312.11 0.0000 937.49 6.6370 1332.49 4.6857 944.13 0.0000 1362.66 0.0000 946.00 7.7668 1365.19 4.7263 949.00 7.7750 1368. 63 0.0000 667. 71 0.0000 1384.29 3.7998 962. 31 8.3698 1408.01 2. 8672 964.08 8.3749 1457.56 0.0000 966 .17 0.0000 1460.82 4.8425 911. 20 8.3893 1489.16 3.9009 968. 97 8.3893 1505.03 4.8950 983.53 0.0000 1584.12 3.9895 984.45 0.0000 1596.21 0.0000 Page 4077 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:06:24.63 ********************************************************************************
  • GEL.Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM41.CNF;119 Background date : Z-OCT-2016 11:02:18. Sample date 7-DEC-2015 13:02:00. Acquisition date : 3-0CT-2016 07:04:39. Sample ID G405235051 Sample quantity l.53012E+02 GRAM Detector name : GAM41 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:05.93 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 6 6 2 2 2 2 0 0 0 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4078 of 5809 Energy 46.53* 63.22* 74.93* 77.27* 84.44* 87.37 89.91 92.78* 156.62 186.12* 238.79* 241. 96 260 .11 271. 39 277.18 280.70 295.61 300.46 328.52* 338.49 352.28* 458.10 494.31 512.04* 543.77 548.25 583.75* 609.86* 662.29* 728.27* 735.71 786.96 853.65 860.64 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 22 50 232 289 58 128 76 107 39 65 304 76 19 65 48 19 109 19 24 61 198 10 14 24 11 12 112 142 41 39 27 10 13 33 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 188 256 180 113 115 124 103 95 94 118 100 65 50 64 15 31 58 41 65 54 38 19 20 55 12 30 13 42 27 16 12 10 12 3 1. 04 0.73 1. 26 0.78 1. 51 1. 32 1.16 1.19 4.03 1. 02 0.89 1. 22 0.86 3.61 2.39 1. 98 1. 44 0.90 2.29 1.19 1. 06 1. 05 1.18 2.31 1. 00 0.60 1. 33 1. 34 1. 49 1. 54 3.28 0.70 0.97 3.12 93.36 126. 73 150.14 154.82 169.16 175.00 180.08 185.83 313.48 372.45 477.78 484.10 520.41 542. 96 554.54 561.57 591. 39 601.08 657.20 677.12 704.71 916.32 988.71 1024.17 1087.64 1096.59 1167. 58 1219.80 1324. 66 1456.62 1471. 51 1574.02 1707.39 1721. 38 88 122 145 145 166 166 166 166 307 368 473 482 515 535 550 550 587 597 651 672 700 910 982 1015 1081 1090 1163 1214 1318 1450 1464 1570 1698 1715 10 6.24E-03121.4 10 1.39E-02 64.6 14 6. 46E-02 11. 9 14 8.03E-02 8.2 26 1.61E-02 33.6 26 3.56E-02 17.3 26 2.llE-02 25.0 26 2.97E-02 21.6 11 1.07E-02 51.7 10 1.80E-02 35.8 9 8.43E-02 8.4 7 2 .12E-02 21. 5 9 5.14E-03 72.4 15 1.80E-02 30.7 19 1. 33E-02 21. 2 19 5.40E-03 66.1 10 3.03E-02 16.1 8 5.29E-03 63.0 12 6.74E-03 71.0 12 1.70E-02 26.8 10 5.51E-02 9.3 8 2.76E-03 85.9 10 3.89E-03 65.5 22 6. 73E-03 91. 7 9 3.02E-03 67.2 16 3.31E-03104.1 13 3.lOE-02 11.8 14 3.96E-02 12.9 13 1.14E-02 30. 6 14 1. 08E-02 28. 0 16 7.46E-03 34.7 7 2.81E-03 61.3 12 3.61E-03 60.1 13 9.09E-03 20.9 Fit l.87E+00 1. 7 5E+OO l.41E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 900. 96 10 18 3.43 1802.03 1794 13 2.65E-03100.2 36 0 911. 87* 61 23 1. 48 1823.85 1817 15 1. 70E-02 21. 5 37 0 970.76i' 23 43 1.28 1941.66 1931 15 6.27E-03 68.4 38 0 1028.71 13 4 0.99 2057.58 2054 8 3.61E-03 38.5 39 0 1048.47 8 11 1. 45 2097.10 2090 9 2.35E-03 78.6 40 0 1121.13 38 11 1. 56 2242.45 2234 16 1.05E-02 26.0 41 0 1134.76 9 14 4.57 2269.70 2259 18 2.54E-03100.0 42 0 1205.40 7 12 1. 52 2411. 03 2405 11 2.00E-03 97.7 43 0 1238.36 28 7 3.28 2476.97 2471 13 7.82E-03 26.6 44 0 1342.79 10 2 1. 34 2685.89 2680 10 2.65E-03 44.8 45 0 1461.79* 261 8 1. 95 2923.97 2916 15 7.25E-02 6.7 46 0 1765.78 31 0 2.15 3532.26 3525 13 8.61E-03 18.0 Flag: "*" = Peak area was modified by background subtraction Page 4079 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:06:27 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 7-DEC-2015 13:02:00 G405235051 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:04:39 153.01 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA41 0 01:00:00.00 1.50 keV No Empirical 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74 .. 82 PB-214 74.82 PB-214 351. 93 Page 4080 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 .. CAN 0 01:00:05.93 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status ** K-40 1460.82 10. 66.* 8.926E-01 1. 30.0E+Ol 1.300E+Ol 13.33 OK Y-91 1204.77 0.26* 1.057E+OO l.267E+Ol 4.470E+02 195.37 OK CD-109 88.03 3.70* 7.448E+OO 2.086E+OO 3.278E+OO 49.90 OK SN-126 64.28 9.60 7.794E+OO 4.293E-01 4.293E-01 129.22 OK 86.94 8.90 7.448E+OO 8.674E-01 8.674E-01 49.90 OK 87.57 37.00* 7.448E+OO 2.086E-01 2.086E-01 49.90 OK BA-137M .661. 66 89.90* 1. 826E+OO l.288E-01 l.313E-01 61. 28 OK CS-137 661.66 85.10* 1.826E+OO 1.361E-01 1.387E-01 61. 28 OK TL-208 277.37 6.60 3.909E+OO 1.048E+OO 1.048E+OO 42.35 OK 583.19 85.00* 2.050E+OO 3.357E-01 3.357E-01 23.63 OK 860.56 12.50 1.434E+OO 9.175E-01 9.175E-01 41. 72 OK PB-210 46.54 4.25* 7.553E+OO 4.626E-01 4.746E-01 242.82 OK BI-211 72. 87 1.23 7. 711E+OO Line Not Found Absent 351.06 12.92* 3.211E+OO 1. 678E-01 1.678E-01 557.00 OK PB-212 74.82 10.28 7.682E+OO 1.364E+OO 1.364E+OO 34.74 OK 77 .11 17.10 7.644E+OO l.400E+OO 1.400E+OO 16.44 OK 238.63 43.60* 4.384E+OO 9.086E-01 9.086E-01 16.78 OK 300.09 3.30 3.665E+OO 8.817E-01 8.817E-01 125.98 OK BI-214 609.32 45.49* 1. 969E+OO 8.289E-01 8.292E-01 25.86 OK 1120. 29 14.92 1.127E+OO 1.101E+OO 1.102E+OO 51. 95 OK 1764.49 15.30 7.616E-01 1.234E+OO l.235E+OO 35.92 OK PB-214 74.82 5.80 7.683E+OO Line Not Found <<INT Reject 77 .11 9.70 7.644E+OO 2.469E+OO 2.470E+OO 16.44 OK 87.09 3.41 7.454E+OO Line Not Found <<INT Reject 242.00 7.25 4.340E+OO Line Not Found <<INT Reject 295.22 18.42 3.713E+OO 8.949E-01 8.952E-01 32.29 OK 351. 93 35.60* 3.214E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1. 969E+OO 8.289E-01 8.292E-Ol 25.86 OK 1120.29 14.92 1.127E+OO 1.101E+OO 1.102E+OO 51. 95 OK 1764.49 15.30 7.616E-01 l.234E+OO 1.235E+OO 35.92 OK RA-224 240.99 4.10* 4.341E+OO 8.710E-01 8. 710E-01 134. 52 OK RA-226 609.32 45.49* 1.969E+OO 8.289E-01 8.292E-01 25.86 OK 1120.29 14.92 1.127E+OO 1.101E+OO 1.102E+OO 51. 95 OK 1764.49 15.30 7.616E-01 l.234E+OO 1.235E+OO 35.92 OK TH-228 74.82 10.28 7.682E+OO 1.364E+OO 1. 364E+OO 34.74 OK 77 .11 17.10 7.644E+OO l.400E+OO l.400E+OO 16.44 OK 238.63 43.60* 4.384E+OO 9.086E-01 9.086E-01 16.78 OK 300.09 3.30 3.665E+OO 8.817E-01 8.817E-01 125.98 OK TH-229 85.43 14.70 7.510E+OO 3.303E-01 3.303E-01 67.29 OK 88.47 24.00 7.448E+OO 3.217E-01 3.217E-01 49.90 OK 193.51 4.41* 5.088E+OO Line Not Found Absent 210.85 2.80 4.797E+OO Line Not Found Absent TH-230 609.32 45.49* 1. 969E+OO 8.289E-01 8.289E-01 25.86 OK 1120.29 14.92 1.127E+OO 1.101E+OO 1.101E+OO 51. 95 OK 1764.49 15.30 7.616E-01 l.234E+OO 1.234E+OO 35.92 OK PA-231 283.69 1. 70 3.838E+OO Line Not Found Absent 301.36 5.35* 3.665E+OO 5.438E-01 5.438E-01 125.98 OK TH-234 63.29 3.70* 7.794E+OO l .114E+OO 1.114E+OO 129.22 OK 92.59 4.23 7.327E+OO 2.152E+OO 2.152E+OO 43.13 OK Page 4081 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status U-234 609.32 45.49* 1. 969E+OO 8.289E-01 8.289E-01 25.86 OK 1120.29 14.92 1.127E+OO 1.101E+OO l. lOlE+OO 51. 95 OK 1764.49 15.30 7.616E-01 1.234E+OO 1.234E+OO 35.92 OK U-235 89. 96 3.47 7.392E+OO 1. 853E+OO 1.853E+OO 50.01 OK 93.35 5.60 7.327E+OO 1.626E+OO l.626E+00 43.13 OK 143.76 10.96* 6.093E+OO Line Not Found Absent 163.33 5.08 5.667E+OO Line Not Found Absent 185.72 57.20 5.221E+OO 1.270E-01 1.270E-01 71. 51 OK 205.31 5.01 4.887E+OO Line Not Found Absent U-238 63.29 3.70* 7.794E+OO 1.114E+OO 1.114E+OO 129.22 OK 92.59 4.23 7.327E+OO 2.152E+OO 2.152E+OO 43.13 OK AM-243 43.53 5.90 7.421E+OO Line Not Found Absent 74.66 67.20* 7.682E+00 2.087E-01 2.087E-01 34.74 OK ANH-511 511. 00 100.00* 2.310E+OO 5.569E-02 5.569E-02 183.43 OK Flag: "*" = Keyline Page 4082 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:06:28.18 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l *
  • Acquisition date 3-0CT-2016 07:04:39 Sensitivity 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:05.93 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:02:00 Analyst initials: MXRl *
  • Sample ID G405235051 Sample Quantity 1.5301E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN * '* Eff. File : DKA100: [CANBERRA.GAMMA']EFF GAM41 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.300E+Ol 1.698E+OO 5.762E-01 Y-91 4.470E+02 8.558E+02 1.170E+03 CD-109 3.278E+OO 1.603E+OO 1. 471E+00 SN-126 2.086E-01 1.020E-01 9.347E-02 BA-137M l.313E-01 7.883E-02 7.425E-02 CS-137 1.387E-01 8.328E-02 7.844E-02 TL-208 3.357E-01 7.773E-02 6.576E-02 PB-210 4.746E-01 l.130E+OO 7.877E-01 BI-211 l.678E-01 9.159E-01 3.364E-01 PB-212 9.086E-01 1.494E-01 1. l 77E-01 BI-214 8.292E-01 2. lOlE-01 1.538E-01 PB-214 9.561E-01 1. 742E-01 3.267E-01 RN-222 8.292E-01 2. lOlE-01 1.538E-01 RA-224 8. 710E-01 1.148E+OO 1.294E+OO RA-226 8.292E-01 2. lOlE-01 l.538E-01 TH-228 9.086E-01 1.494E-01 l.177E-01 TH-229 -2.973E-01 4.543E-01 8.385E-01 TH-230 8.289E-01 2. lOlE-01 1.537E-01 PA-231 5.438E-01 6. 714E-01 8.080E-01 TH-234 l .114E+OO 1. 411E+OO 9.795E-01 U-234 8.289E-01 2.lOlE-01 1.537E-01 U-235 4.726E-02 1. 889E-01 3.814E-01 U-238 1.114E+OO l.411E+OO 9.795E-01 AM-243 2.087E-01 7.104E-02 5.273E-02 ANH-511 5.569E-02 1. OOlE-01 4.910E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM BE-7 -9.905E+OO 1. 2 64E+Ol 2.128E+Ol NOT IDENT. NA-22 -3.849E-02 6.037E-02 l.040E-01 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 1.664E-03 1.836E-02 5 .113E-02 NOT IDENT. SC-46 2.488E-01 4.412E-01 9.554E-01 FAIL ABUN Page 4083 of 5809 V-48 O.OOOE+OO 1.406E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.986E+02 O.OOOE+OO SHORT HLIF MN-54 3.448E-03 6.698E-02 1.359E-01 NOT IDENT. C0-56 -l.502E-01 5 .118E-01 8.557E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 l.592E-02 4.512E-02 9.149E-02 NOT IDENT. C0-58 -4.077E-01 5.687E-01 1.016E+OO NOT IDENT. FE-59 4.668E-01 8. 611E+OO 1.706E+Ol NOT IDENT. C0-60 1.536E-02 4.084E-02 9.061E-02 NOT IDENT. ZN-65 6.570E-02 1.945E-01 3.750E-01 NOT I DENT .* GE-68 4.490E-01 2.176E+OO 4. 672E+OO NOT IDENT. AS-73 2.039E+OO 2.404E+OO 4.729E+OO NOT IDENT. AS-74 O.OOOE+OO 6.889E+03 O.OOOE+OO SHORT HLIF SE-75 -l.930E-01 2.066E-01 3.385E-01 FAIL ABUN BR-77 O.OOOE+OO 3.519E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.857E+02 O.OOOE+OO SHORT HLIF RB-83 3.740E-01 7.598E-01 1.413E+OO NOT IDENT. KR-85 6.826E+OO 7.254E+OO 1.537E+Ol NOT IDENT. SR-85 7.262E-01 7.737E-01 1. 639E+OO NOT IDENT. RB-86 O.OOOE+OO 2.824E+04 O.OOOE+OO SHORT HLIF Y-88 7.026E-02 l.131E-01 3.972E-01 NOT IDENT. NB-94 -1.570E-02 3.316E-02 6.234E-02 NOT IDENT. NB-95 1.098E-01 9.230E-01 1. 873E+OO NOT IDENT. NB-95M -3.960E-01 2.489E+OO 4. 241E+OO NOT IDENT. ZR-95 l.370E-01 1.662E+OO 3.362E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.544E+32 'O. OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 241E+41 O.OOOE+OO SHORT HLIF RH-101 -1.179E-02 3.198E-02 6.172E-02 NOT IDENT. RH-102 2.537E-02 6.707E-02 l.406E-01 NOT IDENT. RU-103 -2.731E+OO 7.0lOE+OO 1. 096E+Ol FAIL ABUN RH-106 4.272E-02 5.094E-01 9.857E-01 NOT IDENT. RU-106 4. 272E-02 5.094E-01 9.857E-01 NOT IDENT. AG-108M 5.362E-03 3.040E-02 5.904E-02 NOT IDENT. AG-llOM -5.692E-02 1.085E-01 2.067E-01 NOT IDENT. SN-113 -8.789E-03 2.399E-01 4.566E-01 NOT IDENT. CD-115 O.OOOE+OO 4.233E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1. 069E+05 O.OOOE+OO SHORT HLIF TE-123M -2.612E-02 1. 380E-01 2. 396E-01 NOT IDENT. SB-124 -5.218E-01 1. 617E+OO 3.487E+OO NOT IDENT. SB-125 -2.784E-02 l.162E-01 2 .139E-01 NOT IDENT. TE-125M -1. 67 5E+Ol 2.421E+02 4.789E+02 NOT IDENT. I-126 O.OOOE+OO l.258E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.222E+06 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 2.780E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 6.007E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.214E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4.475E+26 O.OOOE+OO SHORT HLIF BA-133 -6. ll 7E-03 4.514E-02 7.584E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF GS-134 4.308E-02 4.045E-02 9. 921E-02 NOT IDENT. CS-135 5.576E-02 1.594E-01 2.868E-01 NOT IDENT. I-135 O.OOOE+OO 8.234E+40 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 5.085E+05 O.OOOE+OO SHORT HLIF CE-139 l.499E-03 l .113E-01 2.182E-01 NOT IDENT. BA-140 O.OOOE+OO l.592E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.103E+05 O.OOOE+OO SHORT HLIF CE-141 -5.610E+OO 2.576E+Ol 4.975E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.612E-01 3.344E-01 6.250E-01 NOT IDENT. PM-144 -1. 271E-02 5.816E-02 l.136E-01 NOT IDENT. PR-144 -1.122E+OO 5.052E+OO 9.862E+OO NOT IDENT. PM-146 1.233E-02 4. 551E-02 8.241E-02 FAIL ABUN ND-147 O.OOOE+OO 3.647E+07 O.OOOE+OO s*HORT HLIF PM-147 5.635E+02 7.602E+02 l.583E+03 NOT IDENT. PM-149 O.OOOE+OO 6.451E+40 O.OOOE+OO SHORT HLIF EU-150 2.322E-02 2.665E-02 4.924E-02 FAIL ABUN EU-152 -4.215E-02 l.073E-01 l.855E-01 NOT IDENT. GD-153 -5.847E-03 l.593E-01 2.862E-01 NOT IDENT. EU-154 -6.285E-02 1.416E-01 2.551E-01 NOT IDENT. EU-155 7.073E-02 8.831E-02 1.856E-01 FAIL ABUN TB-160 3.949E-01 1.749E+OO 3.755E+OO FAIL ABUN H0-166M 2.629E-03 6.136E-02 1.240E-01 FAIL ABUN TM-171 -4.548E+OO 5.503E+OO 9.567E+OO NOT IDENT. HF-172 7.144E-05 2.174E-01 4.284E-01 FAIL ABUN LU-172 4.815E-02 9.393E-02 1.999E-01 FAIL ABUN LU-176 3.198E-03 2.297E-02 4.520E-02 FAIL ABUN Page 4084 of 5809 HF-181 3.504E-02 3.953E+00 7.685E+OO NOT IDENT. TA-182 3.794E-Ol 1.170E+OO 2.381E+OO FAIL ABUN RE-183 4.452E-Ol 1. 069E+OO 2.036E+OO NOT IDENT. RE-184 -2.397E+OO 4.090E+Ol 7.080E+Ol NOT IDENT. W-188 3. 965E+Ol 1.145E+02 2.194E+02 FAIL ABUN IR-192 1.141E-01 4.360E-01 8.704E-01 FAIL ABUN HG-203 2.914E+OO 2.444E+OO 4.930E+OO NOT IDENT. BI-207 -3.388E-02 6. 251E-02 1.118E-01 FAIL ABUN PB-211 1. 721E-01 7.210E-01 1.408E+OO NOT IDENT. BI-212
  • O.OOOE+OO 9.842E-01 1. 501Ect-00 FAIL ABUN RN-219 2.931E-01 3.618E-01 7.664E-01 FAIL ABUN RA-223 1.282E-01 6.579E-01 l.162E+OO FAIL ABUN AC-227 1.819E-03 2.360E-01 4.121E-01 FAIL ABUN TH-227 l.819E-03 2.360E-01 4.121E-01 FAIL ABUN AC-228 O.OOOE+OO 3.673E-01 5.974E-01 FAIL ABUN RA-228 O.OOOE+OO 3.673E-01 5.974E-01 FAIL ABUN TH-231 1.282E-01 6.579E-01 1.162E+OO FAIL ABUN TH-232 O.OOOE+OO 3.673E-01 5.974E-01 FAIL ABUN PA-233 5.092E-02 6.0lOE-02 1.256E-01 FAIL ABUN PA-234 2.470E-02 2.577E-01 5.399E-01 NOT IDENT. PA-234M l.659E-01 5.139E+OO 1.0llE+Ol NOT IDENT. NP-237 5.092E-02 6.0lOE-02 l.256E-01 FAIL ABUN NP-238 O.OOOE+OO l.144E+41 O.OOOE+OO SHORT HLIF NP-239 2.606E-02 2.200E-01 4.407E-01 FAIL ABUN PU-239 -9.135E+Ol 2.876E+02 5.568E+02 NOT IDENT. AM-241 3.959E-02 5.594E-02 1.0lOE-01 NOT IDENT. CM-243 -1.313E-02 8.149E-02 l.613E-01 FAIL ABUN BK-247 -6.742E-02 7.765E-02 1.180E-01 FAIL ABUN CM-247 -3.867E-04 3.580E-02 6. 831E-02 FAIL ABUN CF-249 4.362E-03 3.545E-02 6.945E-02 NOT IDENT. CF-251 -7.098E-02 l.159E-01 2.158E-01 NOT IDENT. Page 4085 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:06:25.44 Nuclide Line Activity Report Nuclide Typ.e: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 252 10.66* 8.926E-01 1.300E+Ol 1.300E+Ol 13.33 Y-91 1204.77 7 0.26* 1.057E+OO 1.267E+Ol 4.470E+02 195.37 CD-109 88.03 164 3.70* 7.448E+OO 2. 911E+OO 4.574E+OO 34.58 SN-126 64.28 65 9.60 7.794E+OO 4.293E-01 4.293E-01 129.22 86.94 164 8.90 7.448E+OO 1.210E+OO 1.210E+OO 34.58 87.57 164 37.00* 7.448E+OO 2. 911E-01 2. 911E-01 34.58 BA-137M 661. 66 43 89.90* 1.826E+OO 1.288E-01 1.313E-01 61. 28 CS-137 661.66 43 85.10* 1.826E+OO 1.361E-01 1.387E-01 61. 28 TL-208 277.37 55 6.60 3.909E+00 1.048E+OO 1.048E+00 42.35 583.19 119 85.00* 2.050E+OO 3.357E-01 3.357E-01 23.63 860.56 34 12.50 1.434E+OO 9.175E-01 9.175E-01 41. 72 PB-210 46.54 30 4.25* 7.553E+OO 4.626E-01 4.746E-01 242.82 BI-211 72. 87 ------1.23 7.711E+OO ------Line Not Found ------351.06 223 12.92* 3.211E+OO 2.633E+OO 2.633E+OO 18.59 PB-212 74.82 301 10.28 7.682E+OO 1.869E+00 1.869E+OO 23.80 77 .11 373 17.10 7.644E+OO 1.400E+OO 1.400E+OO '16. 44 238.63 354 43.60* 4.384E+OO 9.086E-01 9.086E-01 16.78 300'. 09 22 3.30 3.665E+OO 8.817E-01 8.817E-01 125.98 BI-214 609.32 151 45.49* 1. 969E+00 8.289E-01 8.292E-01 25.86 1120.29 38 14.92 1.127E+OO l.101E+OO 1.102E+OO 51.95 1764.49 29 15.30 7.616E-01 l.234E+OO 1.235E+OO 35.92 PB-214 74.82 301 5.80 7.682E+OO 3.312E+OO 3.314E+00 23.80 77 .11 373 9.70 7.644E+OO 2.469E+OO 2.470E+OO 16.44 87.09 164 3.41 7.448E+OO 3.159E+OO 3.160E+OO 34.58 242.00 89 7.25 4.341E+OO 1.387E+OO 1.388E+OO 42.98 295.22 125 18.42 3. 713E+OO 8.949E-01 8.952E-01 32.29 351. 93 223 35.60* 3.211E+OO 9.557E-01 9.561E-01 18.59 RN-222 609.32 151 45.49* 1.969E+OO 8.289E-01 8.292E-01 25.86 1120.29 38 14.92 1.127E+OO l .101E+OO 1.102E+00 51. 95 1764.49 29 15.30 7.616E-01 l.234E+OO 1.235E+00 35.92 RA-224 240.99 89 4.10* 4.341E+OO 2.453E+OO 2.453E+OO. 42.98 RA-226 609.32 151 45.49* 1. 969E+OO 8.289E-01 8.292E-01 25.86 1120.29 38 14.92 1.127E+00 l.101E+OO 1.102E+OO 51. 95 1764.49 29 15.30 7.616E-01 l.234E+OO 1.235E+OO 35.92 TH-228 74.82 301 10.28 7.682E+OO 1.869E+OO 1. 869E+OO 23.80 77 .11 373 17.10 7.644E+OO 1.400E+00 1.400E+OO 16.44 238.63 354 43.60* 4.384E+OO 9.086E-01 9.086E-01 16.78 300.09 22 3.30 3.665E+OO 8.817E-01 8.817E-01 125.98 TH-229 85.43 74 14.70 7.510E+00 3.303E-01 3.303E-01 67.29 88.47 164 24.00 7.448E+OO 4.488E-01 4.488E-01 34.58 193.51 ------4.41* 5.088E+OO ------Line Not Found ------210.85 ------2.80 4.797E+OO ------Line Not Found ------TH-230 609.32 151 45.49* 1.969E+OO 8.289E-01 8.289E-01 25.86 1120. 29 38 14.92 1.127E+OO 1.101E+00 1.101E+OO 51. 95 1764.49 29 15.30 7.616E-01 l.234E+OO 1.234E+OO 35.92 PA-231 283.69 ------1. 70 3.838E+OO ------Line Not Found ------301.36 22 5.35* 3.665E+OO 5.438E-01 5.438E-01 125.98 Page 4086 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error TH-234 63.29 65 3.70*. 7.794E+OO 1.114E+OO 1.114E+OO 92.59 136 4.23 7.327E+OO 2.152E+OO 2.152E+OO 43.13 U-234 609.32 151 45.49* 1. 969E+OO 8.289E-01 8.289E-01 25.86 1120. 29 38 14.92 1.127E+OO 1.lOlE+OO l.101E+OO 51. 95 1764.49 29 15.30 7.616E-01 1.234E+OO 1.234E+OO 35.92 U-235 89. 96 97 3.47 7.392E+OO 1. 853E+OO 1.853E+OO 50.01 93.35 136 5.60 7.327E+OO 1.626E+OO 1.626E+OO 43 .13 143.76 ------10.96* 6.093E+OO ------Line Not Found ------163.33 ------5.08 5.667E+OO ------Line Not Found ------185.72 77 57.20 5.221E+OO 1. 270E-01 1.270E-Ol 71. 51 205.31 ------5.01 4.887E+OO ------Line Not Found ------U-238 63.29 65 3.70* 7.794E+OO 1.114E+OO 1.114E+OO 129.22 92.59 136 4.23 7.327E+OO 2.152E+OO 2.152E+OO 43.13 AM-243 43.53 ------5.90 7. 421E+OO ------Line Not Found ------74.66 301 67.20* 7.682E+OO 2.859E-01 .2. 859E-01 23.80 ANH-511 511. 00 26 100.00* 2.310E+OO 5.569E-02 5.569E-02 183.43 Flag: "*" Key line Page 4087 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235051 Acquisition date 3-0CT-2016 07:04:39 Total number of lines in spectrum 46 Number of unidentified lines 9 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 Y-91 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-229 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 58.51D 461.40D 2.30E+05Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1. 41Ei-10Y 7340.00Y 7.54E+04Y 7.04E+08Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 35.3 1. 57 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.300E+Ol 1.267E+Ol 2. 911E+OO 2. 911E-01 l.288E-01 1. 361E-01 3.357E-01 4.626E-01 2.633E+OO 9.086E-01 8.289E-01 9.557E-01 8.289E-01 2.453E+OO 8.289E-01 9.086E-01 4.488E-01 8.289E-01 5.438E-01 1.114E+OO 8.289E-01 l.270E-01 1.114E+OO 2.859E-01 5.569E-02 4.563E+Ol 4.563E+Ol
  • Decay Corr pCi/GRAM 1.300E+Ol 4.470E+02 4.574E+OO 2. 911E-01 1. 313E-01 1.387E-01 3.357E-01 4.746E-01 2.633E+OO 9.086E-01 8.292E-01 9.561E-01 8.292E-01 2.453E+OO 8.292E-01 9.086E-01 4.488E-01 8.289E-01 5.438E-01 1.114E+OO 8.289E-01 l.270E-01 1.114E+OO 2.859E-01 5.569E-02 4. 816E+02 4.816E+02 80.43% Decay Corr 2-Sigma Error 0.173E+Ol 8.732E+02 1.582E+OO 1.007E-01 0.804E-01 0.850E-01 0.793E-01 11. 53E-01 0.489E+00 1.525E-01 2.144E-01 1.777E-01 2.144E-01 1.054E+OO 2.144E-01 1.525E-01 l.552E-01 2.144E-01 6. 851E-01 l.439E+00 2.144E-01 0.908E-01 1.439E+OO 0. 681E-01 10.21E-02 "M" Manually accepted 2-Sigma %Error 13.33 195.37 34.58 34.58 61. 28 61. 28 23.63 242.82 18.59 16.78 25.86 18.59 25.86 42.98 25.86 16.78 34.58 25.86 125.98 129.22 25.86 71. 51 129.22 23.80 183.43 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4088 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235051 Acquisition date : 3-0CT-2016 07:04:39 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 156. 62 47 114 4.03 313. 48 307 11 l.07E-02 **** 5.81E+OO T 0 2 60 .11 21 57 0. 86 520.41 515 9 5.14E-03 **** 4. llE+OO T 0 271.39 75 74 3.61 542.96 535 15 1.80E-02 61. 5 3.97E+OO T 5 280.70 22. 36 1. 98 561. 57 550 19 5.40E-03 **** 3.87E+OO T 0 328.52 27 74 2.29 657.20 651 12 6.74E-03 **** 3.41E+OO T 0 338.49 69 61 1.19 677.12 672 12 1.70E-02 53.5 3.32E+OO T 0 458.10 11 21 1. 05 916.32 910 8 2.76E-03 **** 2.55E+OO 0 494.31 15 22 1.18 988.71 982 10 3.89E-03 **** 2.38E+OO 0 543.77 12 13 1. 00 1087.64 1081 9 3.02E-03 **** 2.19E+OO 0 548.25 13 32 0.60 1096.59 1090 16 3. 31E-03 **** 2.17E+OO 0 728. 27 41 17 1. 54 1456.62 1450 14 1. 08E-02 56 .1 1. 67E+OO T 0 735.71 28 13 3.28 1471.51 1464 16 7.46E-03 69.4 1.66E+OO T 0 786.96 10 10 0.70 1574.02 1570 7 2.81E-03 **** 1. 56E+OO 0 853.65 13 12 0.97 1707.39 1698 12 3. 61E-03 **** 1. 44E+OO 0 900. 96 10 19 3.43 1802.03 1794 13 2.65E-03 **** 1. 37E+OO T 0 911. 87 62 23 1. 48 1823.85 1817 15 l.70E-02 43.0 1.36E+OO T 0 970.76 23 44 1. 28 1941.66 1931 15 6.27E-03 **** l.28E+OO 0 1028.71 13 4 0.99 2057.58 2054 8 3.61E-03 76.9 1.22E+OO T 0 1048.47 8 11 1. 45 2097.10 2090 9 2.35E-03 **** 1.20E+OO T 0 1134.76 9 14 4.57 2269.70 2259 18 2.54E-03 **** 1.12E+OO 0 1238.36 28 7 3.28 2476.97 2471 13 7.82E-03 53.2 1. 03E+OO T 0 1342.79 9 2 1. 34 2685.89 2680 10 2.65E-03 89.5 9. 61E-01 Flags: "T" = Tentatively associated Page 4089 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:06:43.28 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l *
  • Acquisition date 3-0CT-2016 07:04:39 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:05.93 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:02:00 Nuclide Library : SOLID *
  • Sample ID G405235051 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.5301E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 Y-91 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-229 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.179E-01 4.991E+02 6.947E-01 4.415E-02 3.290E-02 3.476E-02 2.896E-02 3.707E-01 1.516E-01 5.519E-02 6.928E-02 1.574E-01 6.928E-02 6.081E-01 6.928E-02 5.519E-02 3.880E-01 6.926E-02 3.685E-01 4.649E;-Ol 6. 92 6E-02 1. 801E-01 4.649E-01 2.498E-02 2.159E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4090 of 5809 Le (pCi/GRAM 9.296E+OO 4.368E-02 O.OOOE+OO 1.664E-02 4.192E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GF.:-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4091 of 5809 O.OOOE+OO 5.897E-02 3.586E-01 O.OOOE+OO 4.305E-02 4.228E-01 7.405E+OO 3.759E-02 1. 599E-01 1.949E+OO 2.243E+OO O.OOOE+OO l.526E-01 O.OOOE+OO O.OOOE+OO 6.315E-01 6. 960E+00 7. 421E-01 O.OOOE+OO 1.344E-01 2.723E-02 8.259E-01 1.956E+OO 1. 481E+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.896E-02 6.285E-02 4.837E+OO 4.306E-01 4.306E-01 2.668E-02 8.801E-02 2.061E-01 O.OOOE+OO O.OOOE+OO l.114E-01 1.177E+OO 9.649E-02 2.251E+02 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.422E-02 O.OOOE+OO 4.282E-02 l.325E-01 O.OOOE+OO O.OOOE+OO 1. 020E-01 0.000E+OO O.OOOE+OO 2.341E+Ol O.OOOE+OO 2.916E-01 4.983E-02 4.325E+OO 3.665E-02 0.000E+OO 7.448E+02 0 .'OOOE+OO 2.244E-02 8.445E-02 1:350E-01 1.072E-01 8.742E-02 1.592E+OO 5.461E-02 4.516E+OO 2.012E-01 8.739E-02 2.054E-02 3.364E+OO SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT .. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RA-223 AC-227 TH-227 AC-228 RA-228 TH-231 TH-232 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4092 of 5809 1.043E+OO 9.650E-01 3.073E+Ol 1.006E+02 3.950E-01 2.273E+OO 4.812E-02 6.399E-01 6.899E-01 3.468E-01 5.307E-01 1.884E-01 l.884E-01 2.795E-01 2.795E-01 5.307E-01 2.795E-01 5.773E-02 2. 271E-01 4.410E+OO 5.773E-02 O.OOOE+OO 2.071E-01 2.610E+02 4.792E-02 7.576E-02 5.329E-02 3.081E-02 3 .118E-02 1.004E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN *FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:06:48.82 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235051.CNF;l *
  • Acquisition date 3-0CT-2016 07:04:39 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:05.93 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:02:00 Nuclide Library : SOLID *
  • Sample ID G405235051 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.5301E+02 GRAM *
  • Quantity Err(%) : 1.3071E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.300E+Ol 2.028E+OO Y-91 4.470E+02 8.566E+02 CD-109 3.278E+OO 1.650E+OO SN-126 2.086E-01 1.044E-01 BA-137M 1.313E-01 7.956E-02 CS-137 l.387E-01 8.405E-02 TL-208 3.357E-01 8.285E-02 PB-210 4.746E-01 1.131E+OO BI-211 1.678E-01 9.645E-01 PB-212 9.086E-01 1. 725E-01 BI-214 8.292E-01 2.215E-01 PB-214 9.561E-01 l.923E-01 RN-222 8.292E-01 2.215E-01 RA-224 8.710E-01 1.169E+OO RA-226 8.292E-01 2.215E-01 TH-228 9.086E-01 1.725E-01 TH-229 -2.973E-01 4.551E-01 TH-230 8.289E-Ol 2.215E-01 PA-231 5.438E-01 6.826E-01 TH-234 l .114E+OO l.437E+OO U-234 8.289E-01 2.215E-01 U-235 4.726E-02 l.890E-01 U-238 l .114E+OO l.437E+OO AM-243 2.087E-01 7.567E-02 ANH-511 5. 5 69E.-02 1.002E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Page 4093 of 5809 Key-Line Activity (pCi/GRAM -9.905E+OO -3.849E-02 -l.000E+41 l.664E-03 2.488E-01 K.L Act error ( 1. 96-sigma) l.267E+Ol 6.045E-02 4.876E+41 l.836E-02 4. 421E-01 TPU (1.96-sigma) 2.028E+00 8.566E+02 1.650E+OO 1.044E-01 7.956E-02 8.405E-02 8.285E-02 1.131E+OO 9.645E-01 1.725E-01 2.215E-01 l.923E-01 2.215E-01 1.169E+OO 2.215E-01 1.725E-01 4.551E-01 2.215E-01 6.826E-01 l.437E+OO 2.215E-01 l.890E-01 l.437E+OO 7.567E-02 l.002E-01 TPU ( 1. 96-sigma) l.343E+Ol 6.289E-02 O.OOOE+OO l.838E-02 4.561E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 -1.673E+04 1.425E+04 1.612E+04 SHORT HLIF CR-51 -4.343E+02 4.004E+02 4.457E+02 SHORT HLIF MN-54 3.448E-03 6.698E-02 6.700E-02 NOT IDENT. C0-56 -l.502E-01 5.120E-01 5.165E-01 FAIL ABUN MN-56 -1.000E+41 3.409E+41 O.OOOE+OO SHORT HLIF C0-57 l.592E-02 4.516E-02 4.573E-02 NOT IDENT. C0-58 -4.077E-01 5.701E-01 5.990E-01 NOT IDENT. FE-59 4.668E-01 8.611E+OO 8.614E+OO NOT IDENT. C0-60 l.536E-02 4.086E-02 4.144E-02 NOT IDENT. ZN-65 6.570E-02 ;I_.948E-01 1.970E-01 NOT IDENT. GE-68 4.490E-01 2.178E+OO 2.187E+OO NOT IDENT. AS-73 2.039E+OO 2.449E+OO 2.616E+OO NOT IDENT. AS-74 -l.552E+03 6.891E+03 6.927E+03 SHORT HLIF SE-75 -1.930E-01 2.073E-01 2.248E-01 FAIL ABUN BR-77 2 .139E+38 1.858E+39 O.OOOE+OO SHORT HLIF SR-82 7.499E+02 8.887E+02 9.508E+02 SHORT HLIF RB-83 3.740E-01 7.620E-01 7.805E-01 NOT IDENT. KR-85 6.826E+OO 7.278E+OO 7.901E+OO NOT IDENT. SR-85 7.262E-01 7.762E-01 8.424E-01 NOT IDENT. RB-86 l.049E+04 2.829E+04 2.869E+04 SHORT HLIF Y-88 7.026E-02 l.132E-01 l.175E-01 NOT IDENT. NB-94 -1.570E-02 3.319E-02 3.394E-02 NOT IDENT. NB-95 1.098E-01 9.231E-01 9.244E-01 NOT IDENT. NB-95M -3. 960E-01 2.490E+OO 2.496E+OO NOT IDENT. ZR-95 1.370E-01 1:662E+OO 1.663E+OO NOT IDENT. NB-97 -l.OOOE+41 3.611E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 4.071E+41 O.OOOE+OO SHORT HLIF M0-99 . 5.418E+31 2.545E+32 0. O'OOE+OO SHORT HLIF TC-99M -l.OOOE+41 1.249E+41 O.OOOE+OO SHORT HLIF RH-101 -1.179E-02 3.208E-02 3.252E-02 NOT IDENT. RH-102 2.537E-02 6.712E-02 6.809E-02 NOT IDENT. RU-103 -2.731E+OO 7.015E+OO 7.122E+OO FAIL ABUN RH-106 4.272E-02 5.094E-01 5.097E-01 NOT IDENT. RU-106 4. 272E-02 5.094E-01 5.097E-01 NOT IDENT. AG-108M 5.362E-03 3.041E-02 3.050E-02 NOT IDENT. AG-llOM -5.692E-02 1.087E-01 l .117E-01 NOT IDENT. SN-113 -8.789E-03 2.399E-01 2.399E-01 NOT IDENT. CD-115 6.370E+38 4.235E+39 O.OOOE+OO SHORT HLIF SN-117M -9.312E+04 1.077E+05 l.156E+05 SHORT HLIF TE-123M -2.612E-02 1. 380E-01 1.385E-01 NOT IDENT. SB-124 -5.218E-01 1.617E+OO l.634E+OO NOT IDENT. SB-125 -2.784E-02 l.163E-01 1.169E-01 NOT IDENT. TE-125M -1. 675E+Ol 2.421E+02 2.422E+02 NOT IDENT. I-126 -1.208E+05 l.258E+06 l.259E+06 SHORT HLIF SB-126 9.679E+05 1.238E+06 1.313E+06 SHORT HLIF SB-127 -2.878E+21 2.808E+22 O.OOOE+OO SHORT HLIF I-131 1.067E+09 6.007E+09 6.027E+09 SHORT HLIF I-132 l.000E+41 l.858E+42 O.OOOE+OO SHORT HLIF TE-132 2.030E+26 4.553E+26 O.OOOE+OO SHORT HLIF BA-133 -6 .117E-03 4.514E-02 4.523E-02 FAIL ABUN I-133 1.000E+41 1.213E+42 O.OOOE+OO SHORT HLIF CS-134 4.308E-02 4.068E-02 4.507E-02 NOT IDENT. CS-135 5.576E-02 1.595E-01 l.615E-01 NOT IDENT. I-135 l.000E+41 6.846E+41 O.OOOE+OO SHORT HLIF CS-136 3.302E+05 5.122E+05 5.334E+05 SHORT HLIF CE-139 l.499E-03 l .113E-01 l .113E-01 NOT IDENT. BA-140 2.603E+05 l.592E+06 l.596E+06 SHORT HLIF LA-140 -2.351E+05 6.106E+05 6.197E+05 SHORT HLIF CE-141 -5.610E+OO 2.577E+Ol 2.589E+Ol NOT IDENT. CE-143 -l.000E+41 2. 461E+41 O.OOOE+OO SHORT HLIF CE-144 -2.612E-01 3.358E-01 3.558E-01 NOT IDENT. PM-144 -1.271E-02 5.818E-02 5.846E-02 NOT IDENT. PR-144 -1.122E+OO 5.053E+OO 5.078E+OO NOT IDENT. PM-146 1.233E-02 4.553E-02 4.587E-02 FAIL ABUN ND-147 1.143E+07 3.648E+07 3.685E+07 SHORT HLIF PM-147 5.635E+02 7. 631E+02 8.042E+02 NOT IDENT. PM-149 -2.023E+40 6.468E+40 O.OOOE+OO SHORT HLIF EU-150 2.322E-02 2.673E-02 2.870E-02 FAIL ABUN EU-152 -4.215E-02 l.073E-01 l.090E-01 NOT IDENT. GD-153 -5.847E-03 1.593E-01 l.593E-01 NOT IDENT. EU-154 -6.285E-02 l.417E-01 1.445E-01 NOT IDENT. EU-155 7.073E-02 8.866E-02 9.422E-02 FAIL ABUN TB-160 3.949E-01 1. 749E+OO 1.758E+OO FAIL ABUN H0-166M 2.629E-03 6.136E-02 6.137E-02 FAIL ABUN TM-171 -4.548E+00 5.537E+OO 5.905E+OO NOT IDENT. HF-172 7.144E-05 2.174E-01 2.174E-01 FAIL ABUN LU-172 4.815E-02 9.440E-02 9.686E-02 FAIL ABUN LU-176 3.198E-03 2.298E-02 2.302E-02 FAIL ABUN Page 4094 of 5809 HF-181 3.504E-02 3.953E+OO 3.953E+OO NOT IDENT. TA-182 3.794E-01 1.171E+OO 1.183E+OO FAIL ABUN RE-183 4.452E-01 1. 072E+OO 1.091E+OO NOT IDENT. RE-184 -2.397E+OO 4. 091E+Ol 4.092E+Ol NOT IDENT. W-188 3. 965E+Ol 1.14 6E+02 l.160E+02 FAIL ABUN IR-192 1.141E-01 4.361E-01 4.391E-01 FAIL ABUN HG-203 2.914E+OO 2.457E+OO 2.786E+OO NOT IDENT. BI-207 -3.388E-02 6.275E-02 6.458E-02 FAIL ABUN PB-211 l.721E-01 7.212E-01 7.253E-01 NOT IDENT. BI-212 1. 791E+OO 9.983E-01 l.284E+oo. FAIL ABUN RN-219 2.931E-01 3.642E-01 3.875E-01 FAIL ABUN RA-223 l.282E-01 6.580E-01 6.605E-01 FAIL ABUN AC-227 1.819E-03 2.360E-01 2.360E-01 FAIL ABUN TH-227 l.819E-03 2.360E-01 2.360E-01 FAIL ABUN AC-228 8. 719E-01 3.817E-01 5.479E-01 FAIL ABUN RA-228 8.719E-01 3.817E-01 5.479E-01 FAIL ABUN TH-231 1.282E-01 6.580E-01 6.605E-01 FAIL ABUN TH-232 8. 719E-01 3.817E-01 5.479E-01 FAIL ABUN PA-233 5.092E-02 6.027E-02 6.449E-02 FAIL ABUN PA-234 2.470E-02 2.592E-01 2.595E-01 NOT IDENT. PA-234M 1.659E-01 5 .139E+OO 5.140E+OO NOT IDENT. NP-237 5.092E-02 6.027E-02 6.449E-02 FAIL ABUN NP-238 -1.000E+41 1.152E+41 0.000E+OO SHORT HLIF NP-239 2.606E-02 2.200E-01 2.203E-01 FAIL ABUN PU-239 -9.135E+Ol 2.878E+02 2.907E+02 NOT IDENT. AM-241 3.959E-02 5.620E-02 5.896E-02 NOT IDENT. CM-243 -1.313E-02 8.150E-02 8 .1 72E-02 FAIL ABUN BK-247 -6.742E-02 7.900E-02 8.464E-02 FAIL ABUN CM-247 -3.867E-04 3.580E-02 3.580E-02 FAIL ABUN CF-249 4.362E-03 3.546E-02 3.551E-02 NOT IDENT. CF-251 -7.098E-02 1.164E-01 l.207E-01 NOT IDENT. Page 4095 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 79.2546 87.09 96. 8336 136.47 82.2510 45.60 85.4408 87.57 96.8968 140.51 0.0000 46.54 85.6012 88.03 96.9570 143.76 74.8373 49. 72 0.0000 88.34 96. 9977 144.24 73.9818 51. 35 104.1492 88.47 97.0142 145.44 90.1319 51. 87 130.3128 89. 96 97.2077 152.43 67.3836 52.39 113.8370 1093.63 97.2956 153.25 0.0000 52.97 87.8431 91.11 0.0000 323.87 66.1473 53.44 83.1661 92.59 97.5452 156.02 0.0000 54.07 88.0192 93.35 97.6414 158.56 0.0000 57. 36 0.0000 94.56 69.5523 159.00 63.7328 57.53 113.6957 94.65 69.5603 162.33 68.0092 57.98 98.2136 94.67 69.5620 162.66 0.0000 59.27 99.2329 94.87 83.4960 163.33 78.0547 59.32 105.6440 97.43 93.9227 165.86 68.2274 59.54 92.8738 98.43 76.2497 176.31 58.7611 60.96 107.5443 98:44 76.2506 176.60 0.0000 61.17 107.5821 99.53 79.7481 177.52 72. 6087 62.93 115.9506 100 .11 83.2019 181.07 0.0000 63.29 116. 0193 102.03 98.7181 181.52 58.1018 63.58 116.0750 103.18 88.6302 184.41 55.4706 64.28 116.2081 103.37 83.5364 143.76 62.0103 66.73 140.9741 105.21 68.3451 193.51 65.2049 67.24 129.7371 105.31 68.3537 197.03 59.7865 125.81 116.8447 106.12 76.1172 198.01 71. 0521 67.75 116. 8572 106.47 90 .. 6948 201.83 65.6428 69.67 122.0940 109.28 78.9792 203.43 58.2146 70.83 122.3129 111. 00 89.4607 205.31 55.4793 72.81 135.7691 111.76 0.0000 210.85 62.3295 72. 87 117.7866 114. 06 77.6921 215.65 62.5585 74.66 108.2618 116. 30 0.0000 222 .11 45.7188 74.82 108.2873 116.74 78.7951 227.09 44.9312 74.97 108.3115 119.76 84.2751 227.38 50.6779 77 .11 108.6539 121.12 67.8695 228.16 0.0000 78.74 117.1618 121.22 67. 8771 228.18 41.1401 79.69 127.2367 121.78 74.8852 116.74 41.1401 80.12 119.047-9 122.06 76.6500 235.69 50.5026 80.19 0.0000 122.92 82.8254 235. 96 50.5122 80.57 96.7883 123.07 78.4790 238.63 76.6355 81. 00 99.3311 265.00 79.4038 238.98 0.0000 81. 07 99.3408 125.81 76.0887 240.99 81.1084 81. 75 102.7506 127.23 85.8392 242.00 52.1785 83.79 118. 0025 127.91 84.1492 244.70 49.3730 84.00 91. 0217 129.30 82.5168 252.40 0.0000 85.43 91. 2010 131. 20 70.3687 252.80 45.7555 86. 55 96.7628 133. 02 89.0089 254.15 0.0000 8 6. 7 9 96. 7941 133. 52 82.8830 256.23 38.0558 86.94 96.8142 136. 00 74.2554 260.90 0.0000 Page 4096 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 44.7474 355.39 0.0000 584.27 18.3724 2 64. 80 45.6353 356.01 31.0870 595.83 0.0000 265.00 45.6410 364.49 0.0000 427.87 20.7964 268.22 42.7867 366.42 0.0000 602.52 0.0000 269.46 36.9156 372. 51 38.6787 604. 72 13.8857 270.03 36.9293 375.05 30.3558 607.14 20.8469 271.23 36.9583 377.52 36.6833 609.32 27.8184 273.65 0.0000 356.01 23.1337 610.33 27.8291 276.40 25.2157 388.16 24.2382 614.28 12.1927 277.37 25.2313 388.63 0.0000 618.01 27. 9072 277.60 25.2349 391.69 29.5603 620.36 10.4744 278.00 25.2416 264.66 24.3912 621. 93 15.1381 279.20 25.2608 401.81 19.0997 630.19 0.0000 279.54 25.2665 402.40 28.6578 631. 29 19.2789 279.70 25.2691 404.85 29.7557 633.25 24.5538 280.46 25.2811 410.95 33.0422 634.78 0.0000 283.69 22.3526 413. 71 24.5484 635.95 11. 4111 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 26.8522 423. 72 0.0000 645.85 11. 4516 285.90 0.0000 427.09 32.2266 657.76 18.3993 287.50 33.8582 427.87 32.2382 657.90 0.0000 290.67 34.7235 433.94 26.9424 661.66 20.3728 293.27 0.0000 439.40 28.0921 664.57 0.0000 351. 93 31.5192 453.88 17.9472 666.33 0.0000 295.96 31.5333 463.37 27.3097 666.50 0.0000 879.38 36.0959 468.07 19.7043 667. 71 0.0000 299.98 28.6003 473.00 0.0000 677.62 20.4851 300.09 28.6021 475.06 18.6674 685.70 0.0000 300 .13 28.6032 476.78 15.3848 695.00 0.0000 301.36 36.1567 477.60 26.3833 696. 49 19. 7200 302.85 24.1265 482.18 16.5228 696. 51 19.7200 256.23 37.7350 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.6219 306.78 31.2371 497.08 24.9442 697.49 17.9333 308.46 34.2947 505.52 18.3581 702.65 21. 5574 311. 90 29.3109 507.63 0.0000 706.68 18.8877 316.51 28. 3771 511. 00 17.8428 711. 68 18.0182 319.41 0.0000 514.00 17.8652 720. 70 0.0000 320.08 0.0000 514.00 17.8652 721. 93 0.0000 321. 04 29.4685 520.40 16.7932 722. 78 17.3602 323.87 33.5881 520.69 0.0000 722.91 17.3613 325.23 42.7819 522.65 0.0000 723. 31 20.2576 328.76 0.0000 527.90 0.0000 724 .19 17.3684 333.37 27.6306 528.26 16.8475 727. 33 13.0395 333.97 20.4740 529.59 19.1042 733.00 3.6288 334.37 33.7896 529.87 0.0000 735.93 11. 6230 338.28 31.8117 531.02 0.0000 333.97 11.6289 338.32 31.8123 537.26 0.0000 739.50 0.0000 311. 90 32.3645 546.56 0.0000 747.24 17.3156 340.48 32.3645 552.55 23.8190 748.06 18.2312 340.55 0.0000 563.25 14.8070 752.31 19.1690 344.28 42.0078 569.33 20.5503 753.82 0.0000 345.93 36.0695 946.00 23. 9771 756.73 17.3678 351.06 27.9031 569.70 23.9788 756.80 17.3678 351. 93 24.8145 583.19 18.3646 884.68 17. 4066 Page 4097 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.4171 1274.44 12. 7183 1620.50 3.3481 766.42 16.5037 1001.03 13.7133 1621. 92 4.4653 766.84 16.5059 1002.74 11. 7594 1678.03 0.0000 772.60 0.0000 1004.73 9.8044 1690.97 2. 7114 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4.5752 778.90 19.3286 1028.54 0.0000 1063.66 3.0529 783.70 0.0000 1037.84 10.8751 1771. 35 10.0767 785.37 17.7070 1038.76 0.0000 1791.20 0.0000 792.07 15. 7103 631.29 12.6820 1808.65 0.9216 794.95 9.2496 1048.07 0.0000 1810.72 0.0000 795.86 4.6260 1049.04 12.6898 1836.06 0.0000 810.06 19.5125 1050.41 12.6945 810.29 19. 5138 1063.66 18.9049 344.28 17.6565 1077.00 0.0000 810.76 14.8701 1077.34 6.9880 815.77 0.0000 1085.87 12.0037 1048.07 0.0000 1093.63 11. 0242 832.01 18.7048 1099.45 14.0504 834.85 14.0405 1112. 07 7.0461 835.71 14.9800 1112.84 9.2048 836.80 0.0000 1115. 54 8. 0596 846.75 0.0000 1120.29 8.0684 846.77 12. '0227 1120. 55 8.0688 856.80 0.0000 1221.41 8.0703 860.56 7.5442 1129. 67 8.0859 871.09 17.9714 1131. 51 0.0000 873.19 15.1426 1147.95 0.0000 875.33 0.0000 1173.23 13. 2722 879.38 8.5328 1177.95 15.3305 880.51 16.1222 1189.05 6.1476 883.24 8.5419 1204.77 11. 3102 884.68 13.2929 1221.41 13.4158 889.28 11. 408 6 1231. 02 11. 3753 894.76 7.6174 1235.36 0.0000 898.04 16.7734 1238.28 8.2861 900. 72 15.2598 1260.41 0.0000 903.28 15.2705 1271.87 4.1731 911. 20 13.3912 1274.44 13.5697 912.08 13.3942 1274.54 15.6583 923.98 0.0000 1291.59 8.3813 926 .'50 9.6051 1298.22 0.0000 929 .11 20.1848 1312 .11 0.0000 937.49 18.3036 1332.49 5.2829 944.13 0.0000 1362.66 0.0000 946.00 8.6899 1365.19 2.1273 949.00 11. 5957 1368.63 0.0000 667.71 0.0000 1384.29 4.2710 962. 31 15.5156 1408.01 5.3638 964.08 13.9707 1457.56 0.0000 966 .17 23.2969 1460.82 3.2514 911.20 21. 3716 1489.16 6.5380 968. 97 21.3716 1505.03 6.5574 983.53 0.0000 1584.12 3.3265 984.45 0.0000 1596.21 0.0000 Page 4098of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:07:20.79 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date : Z-OCT-2016 11:02:28. Sample date 7-DEC-2015 13:11:00. Acquisition date : 3-0CT-2016 07:04:59. Sample ID G405235052 Sample quantity 1.65245E+02 GRAM Detector name : GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.77 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 1 1 0 2 2 0 6 6 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 4 4 0 Energy 74.84 77.17* 87.28 89.95 92.79* 143.99 183.84* 185.83* 227.79 238.68* 241.86 255.61 270.60 295.22 300.90 328.45 339.15 351.95* 372.61 511. 08* .517.16 583.31* 609.48* 661. 81 676 .17 728.23 755.54 760.26 768.70 873.29 911. 29* 964. 8 8 969.04* 1033.95 Page 4099 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 80 136 49 44 63 28 13 38 17 329 87 10 32 125 17 48 88 231 25 38 24 74 134 50 10 15 16 15 22 17 71 27 36 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 118 109 140 78 116 88 47 74 78 79 80 66 40 55 42 51 84 97 49 43 22 51 40 19 25 39 13 9 6 21 18 8 11 14 0.93 1. 06 1. 47 1. 04 1.21 1. 00 1. 51 1. 39 1. 51 1. 20 1. 54 1.29 1. 30 1. 20 0.98 1.10 1.24 1.33 4.02 2.59 1. 39 1. 26 1. 82 1. 00 0.53 0.67 0.86 0.52 2.08 4.16 1. 68 2. 64 1. 77 0.82 150.13 154.81 175.02 180.38 186.05 288.49 368.22 372.21 456.15 477.95 484.31 511. 82 541.82 591.09 602.44 657.58 678.98 704.59 745.94 1023.01 1035.19 1167.56 1219.93 1324.65 1353.40 1457.57 1512.22 1521. 68 1538.58 1747.89 1823.94 1931.20 1939.53 2069.46 143 143 172 178 178 285 366 366 451 473 473 507 539 585 599 653 673 697 739 1015 1030 1162 1214 1321 1346 1449 1505 1516 1535 1737 1819 1925 1925 2062 18 2.23E-02 23.8 8.91E-01 18 3.78E-02 15.2 7 1. 35E-02 43. 0 15 1.22E-02 30.6 1.63E+OO 15 1.76E-02 33.0 7 7.76E-03 59.l 17 3.67E-03 85.7 1.34E+OO 17 1.06E-02 47.0 8 4.68E-03 94.9 28 9.14E-02 7.1 9.25E-01 28 2.42E-02 22.9 8 2.87E-03139.5 6 8.93E-03 35.8 11 3.47E-02 14.6 7 4.81E-03 68.8 11 1. 34E-02 32. 3 13 2.45E-02 24.5 16 6.41E-02 11.7 14 6.94E-03 62.7 16 1.06E-02 47.9 9 6. 55E-03 41. 7 13 2.04E-02 23.3 11 3.72E-02 12.2 8 1. 38E-02 21. l 13 2.75E-03110.4 12 4.26E-03 85.3 11 4.36E-03 52.l 12 4.09E-03 48.6 8 6.03E-03 29.1 18 4.71E-03 69.6 10 1.97E-02 16.5 19 7.36E-03 31.6 6.84E-01 19 9.96E-03 23.4 11 2.57E-03 84.4 Peak Search Report (continued) Page : 2 Sample ID : G405235052 Acquisition date 3-0CT-2016 07:04:59 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1120.27 57 8 1. 45 2242.23 2235 15 l.57E-02 17.0 36 0 1238.15 40 0 0.82 2478.18 2471 16 1. llE-02 15.8 37 0 1277.10 11
  • 1 0.84 2556.16 2553 6 2.93E-03 35 ... 8 38 0 1308. 72 11 4 1. 33 2619.44 2614 9 2. 96E-03 47.0 39 0 1343. 50 13 0 1. 00 2689.08 2683 12 3.61E-03 27.7 40 0 1460.79* 351 7 2.14 2923.88 2917 14 9.76E-02 5.6 41 0 1765.23 19 7 0.91 3533.38 3525 12 5. 31E-03 34.7 Flag: "*" = Peak area was modified by background subtraction Page 4100 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:07:22 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID Sample.type Detector name : 7-DEC-2015 13:11:00 G405235052 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:04:59 165.24 GRAM Elapsed live time: Energy tolerance : Errors propagated: Efficiency type : Abundance limit Interference Report SOLID GAMMA44 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 U-235 143.76 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4101 of 5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 CE-141 145.44 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.77 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235052 Acquisition date 3-0CT-2016 07:04:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 .1460.82 10.66* 1.030E+OO 1.416E+Ol l ..;416E+Ol 11. 24 OK CD-109 88.03 3.70* 4.461E+OO 9.321E-01 1. 465E+OO 168.44 OK SN-126 64.28 9.60 2.161E+00 Line Not Found Absent 86.94 8.90 4.461E+OO 3.875E-01 3.875E-01 168.44 OK 87.57 37.00* 4.461E+OO 9.321E-02 9.321E-02 168.44 OK BA-137M 661.66 89.90* 1. 965E+OO l.373E-01 l.399E-01 42.18 OK CS-137 661.66 85.10* 1. 965E+OO l.450E-01 1. 478E-01 42.18 OK CE-141 145.44 48.29* 5.917E+OO 3.792E-02 2. 311E+Ol 181.44 OK TL-208 277.37 6.60 4.074E+00 Line Not Found Absent 583.19 85.00* 2.178E+00 l.978E-01 l.978E-01 46.53 OK 860.56 12.50 1.592E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.135E+OO Line Not Found Absent 351.06 12.92* 3.336E+OO 2.268E-01 2.268E-01 442.79 OK PB-212 74.82 10.28 3.342E+00 9.186E-01 9.186E-01 77.05 OK 77.11 17.10 3.578E+OO 1.376E+OO 1.376E+OO 30.45 OK 238.63 43.60* 4.585E+OO 9. 072E-01 9.072E-01 14.24 OK 300.09 3.30 3.810E+OO 7.400E-01 7.400E-01 137.50 OK BI-214 609.32 45.49* 2.lOlE+OO 6.925E-01 6.928E-01 24.32 OK 1120.29 14.92 1.288E+OO 1.348E+OO l.348E+OO 33.98 'OK 1764.49 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 OK PB-214 74.82 5.80 3.340E+OO Line Not Found <<INT Reject 77 .11 9.70 3.578E+OO 2.426E+OO 2.427E+OO 30.45 OK 87.09 3.41 4.447E+00 Line Not Found <<INT Reject 242.00 7.25 4.538E+OO Line Not Found <<INT Reject 295.22 18.42 3.870E+OO 9.441E-01 9.444E-01 29.12 OK 351. 93 35.60* 3.336E+00 Line Not Found <<INT Reject RN-222 609.32 45.49* 2. lOlE+OO 6.925E-01 6.928E-01 24.32 OK 1120.29 14.92 l.288E+OO 1.348E+OO 1.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 OK RA-224 240.99 4.10* 4.540E+OO 9.091E-01 9.091E-01 140.33 OK RA-226 609.32 45.49* 2. lOlE+OO 6.925E-01 6.928E-01 24.32 OK 1120.29 14.92 1.288E+OO 1.348E+OO 1.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6.211E-01 6.214E-01 69.40 OK AC-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.443E+OO 1.207E+OO 1.207E+00 48.95 OK 794.95 4.25 1. 696E+OO Line Not Found Absent 835.71 1. 61 1.630E+OO Line Not Found Absent 911. 20 25.80* l.521E+OO 8.518E-01 8.518E-01 33.07 OK 968.97 15.80 l.448E+00 7.324E-01 7.324E-01 46.79 OK RA-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.443E+OO 1.207E+OO 1.207E+00 48.95 OK 794.95 4.25 1. 696E+OO Line Not Found Absent 835.71 1. 61 l.630E+OO Line Not Found Absent 911.20 25.80* 1.521E+OO 8.518E-01 8.518E-01 33.07 OK 968. 97 15.80 1.448E+OO 7.324E-01 7.324E-01 46.79 OK TH-228 74.82 10.28 3.342E+OO 9.186E-01 9.186E-01 77.05 OK 77 .11 17.10 3.578E+OO 1.376E+OO 1.376E+OO 30.45 OK 238.63 43.60* 4.585E+OO 9. 072E-01 9.072E-01 14.24 OK 300.09 3.30 3.810E+OO 7.400E-01 7.400E-01 137.50 OK Page 4102 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235052 Acquisition date 3-0CT-2016 07:04:59 Nuclide Type: 2-Sigma Uncorrected Decay Corr Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 2.101Et00 6.925E-01 6.925E-01 24.32 OK 1120.29 14.92 l.288E+OO 1.348E+OO 1.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6.211E-01 6.211E-01 69.40 OK PA-231 283.69 1. 70 4.000E+OO Line Not Found Absent 301.36 5.35* 3.810E+OO 4.565E-01 4.565E-01 137. 50 OK TH-232 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11.27 3.443E+OO 1.207E+OO 1.207E+OO 48.95 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911. 20 25.80* 1.521E+OO 8.518E-01 8.518E-01 33.07 OK 968. 97 15.80 l.448E+OO 7.324E-01 7.324E-01 46.79 OK U-234 609.32 45.49* 2.101E+OO 6.925E-01 6.925E-01 24.32 OK 1120.29 14.92 1.288E+OO 1.348E+OO 1.348E+OO 33.98 OK 1764.49 15.30 8.670E-01 6.211E-01 6.211E-01 69.40 OK U-235 89.96 3.47 4.655E+OO 1.664E+OO 1.664E+OO 61. 21 OK 93.35 5.60 4.842E+OO 1.422E+OO 1.422E+OO 66.02 OK 143.76 10. 96* 5.918E+OO Line Not Found <<INT Reject 163.33 5.08 5.731E+OO Line Not Found Absent 185. 72 57.20 5.405E+OO 7.020E-02 7.020E-02 94.05 OK 205.31 5.01 5.095E+OO Line Not Found Absent AM-243 43.53 5.90 1.573E-01 Line Not Found Absent 74.66 67.20* 3.342E+OO l.405E-01 l.405E-01 77.05 OK ANH-511 511. 00 100.00* 2.430E+OO 7.973E-02 7.973E-02 95.89 OK Flag: "*" = Keyline Page 4103 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:07:24.32 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * .. DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l *
  • Acquisition date 3-0CT-2016 07:04:59 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:11:00 Analyst initials: MXRl *
  • Sample ID G405235052 Sample Quantity 1.6524E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM44' CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.416E+Ol l.560E+00 CD-109 1.465E+OO 2.418E+OO SN-126 9.321E-02 1.539E-01 BA-137M 1. 399E-01 5.784E-02 CS-137 1.478E-01 6. llOE-02 CE-141 2. 311E+Ol 4. llOE+Ol TL-208 1.978E-01 9.018E-02 BI-211 2.268E-01 9.842E-01 PB-212 9. 072E-01 1.266E-01 BI-214 6.928E-01 1.651E-01 PB-214 1.027E+OO 2.346E-01 RN-222 6.928E-01 1. 651E-01 RA-224 9. 091E-01 l.250E+OO RA-226 6.928E-01 1. 651E-01 AC-228 8.518E-01 2. 761E-01 RA-228 8.518E-01 2. 761E-01 TH-228 9. 072E-01 1.266E-01 TH-230 6.925E-01 1. 651E-01 PA-231 4.565E-01 6.151E-01 TH-232 8.518E-01 2.761E-01 U-234 6.925E-01 1. 651E-01 U-235 2.505E-01 2.900E-01 AM-243 l.405E-01 1. 061E-01 ANH-511 7.973E-02 7.492E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4104 of 5809 Key-Line Activity (pCi/GRAM 5.078E+OO -4.709E-04 O.OOOE+OO 2.565E-03 -l.242E-01 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.179E+Ol 4.743E-02 1.960E+41 3.326E-02 3.861E-01 l.297E+04 MDA (pCi/GRAM 5.992E-01 1. 864E+OO 1.417E-01 5. 965E-02 6. 301E-02 4.062E+Ol 6.347E-02 3.315E-01 8.443E-02 1.308E-01 3.187E-01 1.308E-01 9.052E-01 1.308E-01 2.468E-01 2.468E-01 8.443E-02 l.307E-01 6.774E-01 2.468E-01 l.307E-01 3.374E-01 9.419E-02 4.6?5E-02 MDA (pCi/GRAM 2.446E+Ol 8.435E-02 O.OOOE+OO 7.052E-02 7.500E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.780E+02 O.OOOE+OO SHORT HLIF MN-54 -1.868E-02 6.175E-02 1.118E-01 NOT IDENT. C0-56 -2.089E-01 4. 671E-01 8.216E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 2.319E-02 4.537E-02 9.129E-02 NOT IDENT. C0-58 -6.565E-02 6.036E-01 l.133E+OO NOT IDENT. FE-59 -1.102E+OO 6.391E+OO 1.258E+Ol NOT IDENT. C0-60 6.926E-03 3.033E-02 6.734E-02 NOT IDENT. ZN-65 -1.140E-01 l.891E-01 2.862E-01 NOT IDENT. GE-68 -l .* 309E-02 2.177E+OO 4.422E+OO .NOT IDENT. AS-73 -1. 359E+OO 1. 371E+Ol 2.782E+Ol NOT IDENT. AS-74 0.000E+OO 5.435E+03 O.OOOE+OO SHORT HLIF SE-75 -2. 272E-02 1.935E-01 3.516E-01 NOT IDENT. BR-77 0.000E+OO 2.976E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.557E+02 O.OOOE+OO SHORT HLIF RB-83 -5.029E-01 6.740E-01 1.019E+OO NOT IDENT. KR-85 8. 711E+OO 5.855E+OO l.240E+Ol NOT IDENT. SR-85 9.287E-01 6.245E-01 l.323E+OO NOT IDENT. RB-86 O.OOOE+OO 2.684E+04 O.OOOE+OO SHORT HLIF Y-88 3.866E-03 l.022E-01 2.863E-01 NOT IDENT. Y-91 -2.922E+Ol 5.285E+02 1.040E+03 NOT IDENT. NB-94 9.007E-03 3.567E-02 6.959E-02 NOT IDENT. NB-95 7.526E-01 6. 721E-01 1.424E+OO NOT IDENT. NB-95M -5.399E-01 2.510E+OO 4.127E+OO NOT IDENT. ZR-95 2.042E+00 2.086E+OO 2.693E+OO FAIL ABUN NB-97 O.OOOE+OO 1.736E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.173E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF RH-101 -2.063E-02 3.034E-02 5.514E-02 NOT IDENT. RH-102 -6.334E-03 4.881E-02 9.485E-02 NOT IDENT. RU-103 2.050E+OO 5.283E+OO 1.098E+Ol FAIL ABUN RH-106 -2. 491E-01 4.662E-01 8.376E-01 NOT IDENT. RU-106 -2.491E-01 4.662E-01 8.376E-01 NOT IDENT. AG-108M 1.034E-05 2.625E-02 5.205E-02 NOT IDENT. AG-llOM -7.645E-02 9.590E-02 1. 727E-01 FAIL ABUN SN-113 2.238E-01 2.040E-01 4.546E-01 NOT IDENT. CD-115 O.OOOE+OO 3.639E+39 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.785E+04 O.OOOE+OO SHORT HLIF TE-123M -4.514E-02 1. 313E-01 2.409E-01 NOT IDENT. SB-124 -6.261E-02 l.386E+OO 3.156E+OO NOT IDENT. SB-125 -3.326E-02 9.688E-02 1. 847E-01 NOT IDENT. TE-125M 2.643E+Ol 2.573E+02 5.068E+02 NOT IDENT. I-126 O.OOOE+OO 9.732E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.238E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2.248E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 4.380E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.165E+26 O.OOOE+OO SHORT HLIF BA-133 l.889E-02 3.694E-02 7.206E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.979E-03 4.658E-02 9.184E-02 NOT IDENT. CS-135 8.429E-03 l.271E-01 2.356E-01 NOT IDENT. I-135 O.OOOE+OO l.494E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.098E+05 O.OOOE+OO SHORT HLIF CE-139 -3.729E-03 1. 039E-01 1.957E-01 NOT IDENT. BA-140 O.OOOE+OO 1.322E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.814E+05 0.000E+OO SHORT HLIF CE-143 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -8.229E-02 3.166E-01 5.963E-01 NOT IDENT. PM-144 -2.043E-02 5.660E-02 l.027E-01 NOT IDENT. PR-144 -1. 746E+OO 4.924E+OO 8. 941E+OO NOT IDENT. PM-146 -9.611E-03 3.967E-02 7.647E-02 NOT IDENT. ND-147 O.OOOE+OO 3.374E+07 O.OOOE+OO SHORT HLIF PM-147 3.370E+02 7.818E+02 1.566E+03 NOT IDENT. PM-149 O.OOOE+OO 5.844E+40 0.000E+OO SHORT HLIF EU-150 -l.239E-02 2.869E-02 4.416E-02 FAIL ABUN EU-152 -2.530E-02 8.774E-02 l.527E-01 FAIL ABUN GD-153 5.218E-02 1.667E-01 3 .151E-01 NOT IDENT. EU-154 -3.556E-03 l.157E-01 2.048E-01 FAIL ABUN EU-155 5.619E-02 l.017E-01 2.077E-01 FAIL ABUN TB-160 6.498E-01 2 .117E+OO 4.179E+OO FAIL ABUN H0-166M -2.757E-03 5.332E-02 1.024E-01 FAIL ABUN TM-171 -2.908E+OO 3.255E+Ol 6.632E+Ol NOT IDENT. HF-172 l.615E-01 2.086E-01 4.286E-01 NOT IDENT. LU-172 -3.505E-02 6.371E-02 l.177E-01 FAIL ABUN LU-176 1.238E-02 2.034E-02 4.360E-02 FAIL ABUN HF-181 -5.949E-01 3.582E+OO 7.025E+OO NOT IDENT. Page 4105of5809 TA-182 -9.336E-01 1.067E+OO 1.808E+OO FAIL ABUN RE-183 -9.267E-01 3.633E+OO 7.315E+OO NOT IDENT. RE-184 1.339E+Ol 3.00SE+Ol 6.483E+Ol NOT IDENT. W-188 -1.392E+02 1.004E+02 l.479E+02 FAIL ABUN IR-192 -1. 7 63E-01 3.991E-01 7. 722E-01 FAIL ABUN HG-203 4.00BE-01 2.127E+OO 4.375E+OO NOT IDENT. BI-207 -4.335E-02 4.SOSE-02 7.599E-02 FAIL ABUN PB-210 l.292E+OO 6. 720E+OO 1.422E+Ol NOT IDENT. PB-211 -4.806E-01 6.684E-01 1.221E+OO NOT IDENT. BI-212 6.lJ.SE-01 1.023E+OO 1.225E+OO FAIL ABUN RN-219 2.462E-01 3.367E-01 7.241E-01 FAIL ABUN RA-223 -5.160E-02 5.894E-01 1.054E+OO FAIL ABUN AC-227 l.368E-01 3.743E-01 3.983E-01 FAIL ABUN TH-227 1.368E-01 3.743E-01 3.983E-01 FAIL ABUN TH-229 1.215E-01 3.985E-01 7. 721E-01 FAIL ABUN TH-231 -5.160E-02 5.894E-01 1.054E+00 FAIL ABUN PA-233 2.694E-02 5.046E-02 l.073E-01 FAIL ABUN PA-234 -l.333E-01 2.619E-01 4.925E-01 NOT IDENT. PA-234M 2.979E+OO 3.777E+OO 8.571E+OO NOT IDENT. TH-234 2.685E-01 l.471E+OO 3.000E+OO FAIL ABUN NP-237 2.694E-02 5.046E-02 1.073E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF U-238 2.685E-01 1. 471E+OO 3.000E+OO FAIL ABUN NP-239 -1.431E-02 2.103E-01 4.082E-01 FAIL ABUN PU-239 2 .114E+02 2.728E+02 5.600E+02 NOT IDENT. AM-241 6.lSOE-02 l.657E-01 3.4ff8E-01 NOT IDENT. CM-243 -4.899E-02 9.466E-02 1.777E-01 FAIL ABUN BK-247 -3.478E-02 6.913E_.:_02 l.195E-01 NOT IDENT. CM-247 1.793E-02 3.227E-02 6.780E-02 NOT IDENT. CF-249 -6. 726E-03 3.109E-02 6.lOlE-02 NOT IDENT. CF-251 -1.197E-02 1.045E-01 l.949E-01 FAIL ABUN Page 4106of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:07:21.56 Nuclide Line Activity Report Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 342 10.66* 1.030E+OO 1. 416E+Ol 1. 416E+Ol 11. 24 CD-109 88.03 65 3.70* 4.461E+OO 1.802E+OO 2.832E+OO 85.98 SN-126 64.28 ------9.60 2.161E+OO ------Line Not Found ------86.94 65 8.90 4.461E+OO 7.492E-01 7.492E-01 85.98 87.57 65 37.00* 4. 461E+OO 1.802E-01 1.802E-01 85.98 BA-137M 661.66 53 89.90* 1. 965E+OO 1.373E-01 1.399E-01 42.18 CS-137 661. 66 53 85.10* 1. 965E+OO l.450E-01 1. 478E-01 42.18 CE-141 145.44 36 48.29* 5.917E+OO 5.686E-02 3.466E+Ol 118 .12 TL-208 277.37 ------6.60 4.074E+OO ------Line Not Found ------583.19 81 85.00* 2.178E+OO 1.978E-01 1.978E-01 46.53 860.56 ------12.50 1.592E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 3.135E+OO ------Line Not Found ------351.06 268 12.92* 3.336E+OO 2.828E+OO 2.828E+OO 23.31 PB-212 74.82 110 10.28 3.342E+OO 1.451E+OO 1.451E+OO 47.59 77 .11 185 17.10 3.578E+OO 1.376E+OO 1. 37 6E+OO 30.45 238.63 399 43.60* 4.585E+OO 9. 072E-01 9.072E-01 14.24 300.09 20 3.30 3.810E+OO 7.400E-01 7.400E-01 137.50 BI-214 609.32 146 45.49* 2.101E+OO 6.925E-01 6.928E-01 24.32 lliO. 29 57 14.92 l.288E+OO 1.348E+OO 1.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6.211E-01 6.214E-01 69.40 PB-214 74.82 110 5.80 3.342E+OO 2. 572E+OO 2.573E+OO 47.59 77 .11 185 9.70 3.578E+OO 2.426E+OO 2.427E+OO 30.45 87.09 65 3.41 4. 461E+OO 1.956E+OO 1. 956E+OO 85.98 242.00 106 7.25 4.540E+OO 1.458E+OO 1.459E+OO 45.74 295.22 148 18.42 3.870E+OO 9.441E-01 9.444E-01 29.12 351.93 268 35.60* 3.336E+OO 1.026E+OO 1.027E+OO 23.31 RN-222 609.32 146 45.49* 2 .101E+OO 6.925E-01 6.928E-01 24.32 1120.29 57 14.92 1.288E+OO 1.348E+OO 1.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 RA-224 240.99 106 4.10* 4.540E+OO 2.579E+OO 2.579E+OO 45.74 RA-226 609.32 146 45.49* 2.101E+OO 6.925E-01 6.928E-01 24.32 1120.29 57 14.92 1.288E+OO 1.348E+OO 1.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6. 211E-01 6.214E-01 69.40 AC-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 103 11. 27 3.443E+OO 1.207E+OO 1.207E+OO 48.95 794.95 ------4.25 1. 696E+OO ------Line Not Found ------835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 74 25.80* 1.521E+OO 8. 518E.,-01 8.518E-01 33.07 968. 97 37 15.80 1.448E+OO 7.324E-01 7.324E-01 46.79 RA-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 103 11. 27 3.443E+OO 1.207E+OO 1.207E+OO 48.95 794.95 ------4.25 1. 696E+OO ------Line Not Found ------835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 74 25.80* 1.521E+OO 8.518E-01 8.518E-01 33.07 968. 97 37 15.80 1.448E+OO 7.324E-01 7.324E-01 46.79 TH-228 74.82 110 10.28 3.342E+OO 1. 451E+OO 1. 451E+OO 47.59 77 .11 185 17.10 3.578E+OO 1.376E+OO 1.376E+OO 30.45 Page 4107 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235052 Acquisition date 3-0CT-2016 07:04:59 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 399 43.60* 4.585E+OO 9.072E-01 9. 072E-01 14.24 300.09 20 3.30 3.810E+OO 7.400E-01 7.400E-01 137.50 TH-230 609.32 146 45.49* 2.101E+OO 6.925E-01 6.925E-01 24.32 1120.29 57 14.92 l.288E+OO 1. 348E+OO 1.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6.211E-01 6. 211E-01 69.40 PA-231 283.69 ------1. 70 4.000E+OO ------Line Not Found ------301.36 20 5.35* 3.810E+00 4.565E-01 4.565E-01 137.50 TH-232 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 103 11. 27 3.443E+OO l.207E+OO 1. 207E+OO 48.95 835.71 ------1. 61 1.630E+OO ------* Line Not Found ------911.20 74 25.80* 1.521E+OO 8.518E-01 8.518E-01 33.07 968. 97 37 15.80 1.448E+OO 7.324E-01 7.324E-01 46.79 U-234 609.32 146 45.49* 2.101E+OO 6.925E-01 6.925E-01 24.32 1120.29 57 14.92 l.288E+OO 1.348E+OO 1.348E+OO 33.98 1764.49 18 15.30 8.670E-01 6.211E-01 6. 211E-01 69.40 U-235 89. 96 59 3.47 4.655E+OO 1.664E+OO 1.664E+OO 61. 21 93.35 85 5.60 4.842E+00 1.422E+OO l.422E+OO 66.02 143.76 36 10.96* 5.917E+00 2.505E-01 2.505E-01 118 .12 163.33 ------5.08 5.731E+OO ------Line Not' Found ------185.72 48 57.20 5.405E+OO 7.020E-02 7.020E-02 94.05 205.31 ------5.01 5.095E+OO ------Line Not Found ------AM-243 43.53 ------5.90 1. 573E-01 ------Line Not Found ------74.66 110 67.20* 3.342E+OO 2.220E-01 2.220E-01 47.59 ANH-511 511. 00 43 100.00* 2.430E+OO 7.973E-02 7.973E-02 95.89 Flag: "*" Key line Page 4108of5809 Summary of Nuclide Activity Sample ID : G405235052 Acquisition date Page : 3 3-0CT-2016 07:04:59 Total number of lines in spectrum 41 Number of unidentified lines 7 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA...:.228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 32. 510 1. 41E+l0Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600.00Y 1.41E+10Y 1. 41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 2.45E+05Y 7.04E+08Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 57 1. 00 1. 02 1. 02 610. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity . Uncorrected pCi/GRAM 1.416E+Ol l.802E+OO l.802E-01 l.373E-01 l.450E-01 5.686E-02 1.978E-01 2.828E+OO 9. 072E-01 6.925E-01 1.026E+OO 6.925E-01 2.579E+OO 6.925E-01 8.518E-01 8.518E-01 9.072E-01 6.925E-01 4.565E-01 8.518E-01 6.925E-01 2.505E-01 2.220E-01 7.973E-02 3.195E+Ol 3.195E+Ol Decay Corr pCi/GRAM 1.416E+Ol 2.832E+OO l.802E-01 l.399E-01 1.478E-01 3.466E+Ol l.978E-01 2.828E+OO 9. 072E-01 6.928E-01 l.027E+OO 6.928E-01 2.579E+OO 6.928E-01 8.518E-01 8.518E-01 9.072E-01 6.925E-01 4.565E-01 8.518E-01 6.925E-01 2.505E-01 2.220E-01 7.973E-02 6.759E+Ol 6.759E+Ol 82.93% Decay Corr 2-Sigma Error 0.159E+01 2.435E+OO 1.550E-01 0.590E-01 0.623E-01 4.094E+Ol 0.920E-01 0.659E+OO 1.292E-01 1.685E-01 0.239E+OO 1.685E-01 1.179E+OO 1.685E-01 2.817E-01 2.817E-01 l.292E-01 1.684E-01 6.276E-01 2.817E-01 1. 684E-01 2.959E-01 l.057E-01 7.645E-02 "M" Manually accepted
  • 2-Sigma %Error 11. 24 85.98 85.98 42.18 42.18 118 .12 46.53 23.31 14.24 24.32 23.31 24.32 45.74 24.32 33.07 33.07 14.24 24.32 137.50 33.07 24.32 118 .12 47.59 95.89 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4109 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235052 Acquisition date : 3-0CT-2016 07:04:59 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 6 183.84 17 59 1. 51 368.22 366 17 3.67E-03 **** 5.44E+OO T 0 227.79 21 95 1. 51 456.15 451 8 4.68E-03 **** 4.75E+OO T 0 255.61 12 79 1.29 511. 82 507 8 2.87E-03 **** 4.35E+OO T 0 270.60 38 48 J_. 30 541.82 539 6 8.93E-03 71. 7 4.16E+.00 T 0 328.45 56 59 1.10 657.58 653 11 1. 34E-02 64.6 3.54E+OO T 0 372. 61 29 57 4.02 745.94 739 14 6.94E-03 **** 3.18E+OO T 0 517.16 26 25 1. 39 1035.19 1030 9 6.55E-03 83.4 2.41E+OO 0 676.17 11 27 0.53 1353.40 1346 13 2.75E-03 **** 1. 93E+OO T 0 728.23 16 41 0.67 1457.57 1449 12 4.26E-03 **** 1. 82E+OO T 0 755.54 17 14 0.86 1512.22 1505 11 4.36E-03 **** 1.77E+OO T 0 760. 26 16 10 0.52 1521.68 1516 12 4.09E-03 97.1 1. 76E+OO 0 768.70 23 7 2.08 1538.58 1535 8 6.03E-03 58.3 1.74E+OO 0 873.29 18 22 4.16 1747. 89 1737 18 4.71E-03 **** l.57E+OO T 4 964.88 27 9 2. 64 1931.20 1925 19 7.36E-03 63.1 1. 45E+OO T 0 1033.95 9 14 0.82 2069.46 2062 11 2.57E-03 **** 1.37E+OO 0 1238.15 40 0 0.82 2478.18 2471 16 l. llE-02 31. 6 1.19E+OO T 0 1277.10 10 1 0.84 2556.16 2553 6 2.93E-03 71. 6 1.16E+OO 0 1308.72 11 4 1.33 2619.44 2614 9 2. 96E-03 94.0 l.13E+OO 0 1343.50 13 0 1. 00 2689.08 2683 12 3.61E-03 55.5 1.llE+OO Flags: "T" = Tentatively associated Page 4110 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:07:39.57 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l * *Acquisition date 3-0CT-2016 07:04:59 Sensitivity 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:11:00 Nuclide Library : SOLID *
  • Sample ID G405235052 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : l.6524E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: '[CANBERRA. GAMMA] EFF GAM44 CAN. CNF; 3
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 2.430E-01 8.690E-01 6.680E-02 2.616E-02 2.763E-02 1. 890E+Ol 2.829E-02 1.508E-01 3.894E-02 5.873E-02 l.540E-01 5.873E-02 4.176E-01 5.873E-02 l.074E-01 1. 074E-01 3.894E-02 5.871E-02 3.068E-01 1.074E-01 5.871E-02 1.585E-01 4.408E-02 2.074E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4111 of 5809 Le (pCi/GRAM 1.103E+Ol 3.546E-02 O.OOOE+OO 2.796E-02 3.261E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4112 of 5809 4.837E-02 3.526E-01 O.OOOE+OO 4.279E-02 4.946E-01 5.373E+OO 2.744E-02 1.206E-01 1. 895E+OO 1.295E+Ol O.OOOE+OO 1.609E-01 O.OOOE+OO O.OOOE+OO 4.426E-01 5.558E+OO 5.928E-01 O.OOOE+OO 9.051E-02 4.502E+02 3.140E-02 6.180E-01 l.916E+OO l.175E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.561E-02 4.093E-02 4.916E+OO 3.644E-01 3.644E-01 2.347E-02 7.350E-02 2.074E-01 O.OOOE+OO O.OOOE+OO 1.126E-01 1.118E+OO 8.296E-02 2.367E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.270E-02 O.OOOE+OO 4.017E-02 1. 081E-01 O.OOOE+OO O.OOOE+OO 9.125E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.772E-01 4.534E-02 3.948E+OO 3.415E-02 O.OOOE+OO 7.332E+02 O.OOOE+OO 2. 011E-02 6.889E-02 1.468E-01 8.597E-02 9.729E-02 1.850E+OO 4.485E-02 3.077E+Ol 2.008E-01 4.856E-02 l.995E-02 3.085E+OO 7. 851E-01 NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-.219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4113 of 5809 3.384E+OO 2.852E+Ol 6.577E+Ol 3.499E-01 2.015E+OO 3.162E-02 6. 601E+OO 5.528E-01 5.603E-01 3.293E-01 4.819E-01 1.833E-01 l.833E-01 3.578E-01 4.819E-01 4.908E-02 2.107E-01 3.756E+OO 1. 411E+00 4.908E-02 O.OOOE+OO 1. 411E+OO 1. 895E-01 2.622E+02 1.626E-01 8.278E-02 5.460E-02 3.089E-02 2.731E-02 9.055E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:07:45.84 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA *
  • *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235052.CNF;l *
  • Acquisition date 3-0CT-2016 07:04:59 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.77 Half life ratio : ***** *
  • Sample date 7-DEC-2015 13:11:00 Nuclide Library : SOLID *
  • Sample ID G405235052 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : l.6524E+02 GRAM *
  • Quantity Err(%) : l.2103E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04: 59: 25 Eff. Geometry ' : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 CD-109 SN-126 BA-137M CS-137 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 ANH-511 l.416E+Ol l.465E+OO 9.321E-02 l.399E-01 l.478E-01 2.313E+Ol l.978E-01 2.268E-01 9.072E-01 6.928E-01 l.027E+OO 6.928E-01 9.091E-01 6.928E-01 8.518E-01 8.518E-01 9. 072E-01 6.925E-01 4.565E-01 8.518E-01 6.925E-01 2.505E-01 l.405E-01 7.973E-02 Act Error ( 1. 96-sigma) l.726E+OO 2.426E+OO l.544E-01 5.815E-02 6.143E-02 4. lllE+Ol 9.057E-02 9.970E-01 l.354E-01 l.678E-01 2.384E-01 l.678E-01 l.256E+OO l.678E-01 2.795E-01 2.795E-01 l.354E-01 l.677E-01 6.228E-01 2.795E-01 l.677E-01 2.903E-01 l.070E-01 7.499E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4114of5809 Key-Line Activity (pCi/GRAM 5.078E+OO -4.709E-04 l.OOOE+41 2.565E-03 -l.242E-01 -6.508E+03 K.L Act error ( 1. 96-sigma) 1.179E+Ol 4.743E-02 7.082E+41 3.326E-02 3.861E-01 l.297E+04 TPU ( 1 . 96-sigma ) 1. 726E+OO 2.426E+OO l.544E-01 5.815E-02 6.143E-02 4. lllE+Ol 9.057E-02 9.970E-01 l.354E-01 l.678E-01 2.384E-01 l.678E-01 l.256E+OO l.678E-01 2.795E-01 2.795E-01 l.354E-01 l.677E-01 6.228E-01 2.795E-01 l.677E-01 2.903E-01 l.070E-01 7.499E-02 TPU ( 1. 96-sigma) l.201E+Ol 4.743E-02 O.OOOE+OO 3.328E-02 3.901E-01 l.330E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 1. 591E+02 3.780E+02 3.848E+02 SHORT HLIF MN-54 -1.868E-02 6.175E-02 6.232E-02 NOT IDENT. C0-56 -2.089E-01 4.672E-01 4.766E-01 FAIL ABUN MN-56 -l.OOOE+41 2.199E+41 O.OOOE+OO SHORT HLIF C0-57 2.319E-02 4.538E-02 4.657E-02 NOT IDENT. C0-58 -6.565E-02 6.036E-01 6.044E-01 NOT IDENT. FE-59 -1.102E+OO 6. 391E+OO 6. 411E+OO NOT IDENT. C0-60 6.926E-03 3.033E-02 3.049E-02 NOT IDENT. ZN-65 -1.140E-01 1. 892E-01 1. 960E-01 NOT IDENT. GE-68 -1.309E-02 2.177E+OO 2.177E+OO NOT AS-73 -1.359E+OO l.372E+Ol l.373E+Ol NOT IDENT. AS-74 l .111E+03 5.436E+03 5.459E+03 SHORT HLIF SE-75 -2. 272E-02 1.935E-01 1.938E-Ol NOT IDENT. BR-77 2.132E+38 1. 851E+39 O.OOOE+OO SHORT HLIF SR-82 4.813E+02 6.561E+02 6. 911E+02 SHORT HLIF RB-83 -5.029E-01 6.775E-01 7.145E-01 NOT IDENT. KR-85 8.711E+OO 5.865E+OO 7.058E+OO NOT IDENT. SR-85 9.287E-01 6.257E-01 7.528E-01 NOT IDENT. RB-86 -l.209E+03 2.684E+04 2.684E+04 SHORT HLIF Y-88 3.866E-03 l.022E-01 1.022E-01 NOT IDENT. Y-91 -2.922E+Ol 5.285E+02 5.286E+02 NOT IDENT. NB-94 9.007E-03 3.567E-02 3.590E-02 NOT IDENT. NB-95 7.526E-01 6.729E-01 7.536E-01 NOT IDENT. NB-95M -5.399E-01 2.510E+OO 2.522E+OO NOT IDENT. ZR-95 2.042E+OO 2.087E+OO 2.281E+OO FAIL ABUN NB-97 l.000E+41 l.736E+41 0.000E+OO SHORT HLIF ZR-97 -l.000E+41 3.070E+41 0.000E+OO SHORT HLIF M0-99 4.542E+31 2.173E+32 O.OOOE+OO SHORT HLIF TC-99M -1. OOOE+41 6.857E+41 O.OOOE+OO SHORT HLIF RH-101 -2.063E-02 3.057E-02 3.195E-02 NOT IDENT. RH-102 -6.334E-03 4.881E-02 4.890E-02 NOT IDENT. RU-103 2.050E+OO 5.284E+OO 5.364E+OO FAIL ABUN RH-106 -2.491E-01 4.665E-01 4.798E-01 NOT IDENT. RU-106 -2.491E-01 4.665E-01 4.798E-01 NOT IDENT. AG-108M 1.034E-05 2.625E-02 2.625E-02 NOT IDENT. AG-llOM -7.645E-02 9.598E-02 1.020E-01 FAIL ABUN SN-113 2.238E-01 2.042E-01 2.278E-01 NOT IDENT. CD-115 9.063E+35 3.639E+39 0.000E+OO SHORT HLIF SN-117M -3.524E+03 9.785E+04 9.786E+04 SHORT HLIF TE-123M -4.514E-02 1.313E-01 1. 329E-01 NOT IDENT. SB-124 -6.261E-02 1. 38 6E+OO 1.387E+OO NOT IDENT. SB-125 -3.326E-02 9.689E-02 9.805E-02 NOT IDENT. TE-125M 2.643E+Ol 2.573E+02 2.576E+02 NOT IDENT. I-126 4.940E+05 9.756E+05 1. 001E+06 SHORT HLIF SB-126 4.295E+05 1. 241E+06 1. 256E+06 SHORT HLIF SB-127 -5.030E+21 2.353E+22 O.OOOE+OO SHORT HLIF I-131 -1.318E+09 4.381E+09 4.421E+09 SHORT HLIF I-132 1.000E+41 1. 875E+42 O.OOOE+OO SHORT HLIF TE-132 4.391E+26 8.359E+26 O.OOOE+OO SHORT HLIF BA-133 l.889E-02 3.694E-02 3.791E-02 NOT IDENT. I-133 1.000E+41 6.820E+41 O.OOOE+OO SHORT HLIF CS-134 6.979E-03 4.658E-02 4.669E-02 NOT IDENT. CS-135 8.429E-03 1. 271E-01 1. 271E-01 NOT IDENT. I-135 l.000E+41 6.958E+41 O.OOOE+OO SHORT HLIF CS-136 -4.572E+03 3.098E+05 3.098E+05 SHORT HLIF CE-139 -3. 729E-03 1. 039E-01 1.039E-01 NOT IDENT. BA-140 -7.780E+05 1.322E+06 l.368E+06 SHORT HLIF LA-140 -l.006E+05 3.814E+05 3. 841E+05 SHORT HLIF CE-143 1.000E+41 l.074E+42 0.000E+OO SHORT HLIF CE-144 -8.229E-02 3.167E-01 3.188E-01 NOT IDENT. PM-144 -2.043E-02 5.662E-02 5.736E-02 NOT IDENT. PR-144 -1. 746E+OO 4.924E+OO 4.987E+OO NOT IDENT. PM-146 -9.611E-03 3. 968E-02 3.992E-02 NOT IDENT. ND-147 4.848E+06 3.374E+07 3.381E+o7 SHORT HLIF PM-147 3.370E+02 7.819E+02 7. 965E+02 NOT IDENT. PM-149 l.357E+40 5.85'1E+40 O.OOOE+OO SHORT HLIF EU-150 -l.239E-02 2.869E-02 2.923E-02 FAIL ABUN EU-152 -2.530E-02 8.775E-02 8.849E-02 FAIL ABUN GD-153 5.218E-02 l.667E-01 l.683E-01 NOT IDENT. EU-154 -3.556E-03 l.157E-01 1.157E-01 FAIL ABUN EU-155 5.619E-02 l.018E-01 1.049E-01 FAIL ABUN TB-160 6.498E-01 2 .117E+OO 2 .138E+OO FAIL ABUN H0-166M -2.757E-03 5.332E-02 5.334E-02 FAIL ABUN TM-171 -2.908E+OO 3.255E+Ol 3.257E+Ol NOT IDENT. HF-172 1.615E-01 2.102E-Ol 2.225E-01 NOT IDENT. LU-172 -3.505E-02 6.381E-02 6.574E-02 FAIL ABUN LU-176 1.238E-02 2.034E-02 2. llOE-02 FAIL ABUN HF-181 -5.949E-01 3.582E+OO 3.592E+OO NOT IDENT. Page 4115 of 5809 TA-182 -9.336E-01 l.068E+OO l.148E+OO FAIL ABUN RE-183 -9.267E-01 3.636E+OO 3.660E+OO NOT IDENT. RE-184 l.339E+Ol 3.022E+Ol 3.082E+Ol NOT IDENT. W-188 -l.392E+02 1. 016E+02 l.194E+02 FAIL ABUN IR-192 -1. 7 63E-01 3.992E-01 4.070E-01 FAIL ABUN HG-203 4.008E-01 2.127E+OO 2.135E+OO NOT IDENT. BI-207 -4.335E-02 4.508E-02 4.914E-02 FAIL ABUN PB-210 l.292E+OO 6. 721E+OO 6.746E+OO NOT IDENT. PB-211 -4.806E-01 6.688E-01 7.030E-01 NOT IDENT. BI-212 6. 115E-Ql l.023E+OO l.060E+00 FAIL ABUN RN-219 2.462E-01 3.381E-01 3.559E-01 FAIL ABUN RA-223 -5.160E-02 5.894E-01 5.898E-01 FAIL ABUN AC-227 l.368E-01 3.747E-01 3.797E-01 FAIL ABUN TH-227 l.368E-01 3.747E-01 3.797E-01 FAIL ABUN TH-229 l.215E-01 3.985E-01 4.023E-01 FAIL ABUN TH-231 -5.160E-02 5.894E-01 5.898E-01 FAIL ABUN PA-233 2.694E-02 5.048E-02 5.192E-02 FAIL ABUN PA-234 -l.333E-01 3.030E-01 3.089E-01 NOT IDENT. PA-234M 2.979E+OO 3.779E+OO 4. OllE+OO NOT IDENT. TH-234 2.685E-01 l.472E+OO l.477E+OO FAIL ABUN NP-237 2.694E-02 5.048E-02 5.192E-02 FAIL ABUN NP-238 -l.OOOE+41 3.151E+41 O.OOOE+OO SHORT HLIF U-238 2.685E-01 l.472E+OO l.477E+00 FAIL ABUN NP-239 -l.431E-02 2.103E-01 2.104E-01 FAIL ABUN PU-239 2 .114E+02 2.730E+02 2.892E+02 NOT IDENT. AM-241 6.150E-02 l.658E-01 l.681E-01 NOT IDENT. CM-243 -4.899E-02 9.477E-02 9.731E-02 FAIL ABUN BK-247 -3.478E-02 6.948E-02 7.123E-02 NOT IDENT. CM-247 1. 793E-02 3.241E-02 3.340E-02 NOT IDENT. CF-249 -6. 726E-03 3.109E-02 3.124E-02 NOT IDENT. CF-251 -l.197E-02 l.045E-01 1. 047E-01 FAIL ABUN Page 4116 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 56.4509 87.09 90.6453 136.47 56.9215 45.60 50.6102 87.57 90.7352 140.51 0.0000 46.54 52.5403 88.03 63.1792 143.76 59.7089 49.72 0.0000 88.34 63.2192 144.24 59.7509 51. 35 60.5342 88.47 63.2358 145.44 59.4914 51.87 68.7695 89. 96 72.6759 152.43 62.6473 52.39 54.3732 1093.63 72.7750 153.25 0.0000 52.97 50.8329 91.11 0.0000 323.87 82.6332 53.44 59.9905 92.59 73.0569 156.02 0.0000 54.07 52.8130 93.35 73.1660 158.56 0.0000 57.36 0.0000 94.56 73.3389 159.00 77.6306 57.53 59.7555 94.65 73.3518 162.33 64.6101 57.98 56.1462 94.67 73.3546 162.66 0.0000 59.27 53.5694 94.87 73.3831 163.33 82.5432 59.32 53.5765 97.43 54.9732 165.86 64.9119 59.54 55.4562 98.43 62.4659 176.31 45.3699 60.96 65.8683 98.44 62.4671 176.60 0.0000 61.17 76.1149 99.53 72. 6916 177.52 60.2065 62.93 65.2716 100 .11 66.7060 181.07 0.0000 63.29 71. 8644 102.03 64.9155 181.52 56.3190 63.58 73.7854 103.18 74.2002 184.41 51.5533 64.28 77.6586 103.37 74.2264 143.76 51.6357 66.73 71.5434 105.21 61. 2122 193.51 47.4832 67.24 91.4259 105.31 61.2231 197.03 61.6330 125.81 91.5244 106.12 76.6405 198.01 58.2100 67.75 91.5392 106.47 76.6886 201.83 58.4656 69.67 77 .1107 109.28 64.7400 203.43 58.5716 70.83 93.8015 111. 00 70.0887 205.31 58.6952 72.81 70.6775 111.76 0.0000 210.85 62. 6011 72.87 70.6876 114. 06 67.3501 215.65 51.0566 74.66 70.9784 116. 30 0.0000 222 .11 41. 8461 74.82 71. 0044 116.74 58.2888 227.09 46.8731 74.97 71. 0286 119. 76 70.0895 227.38 46.8874 77 .11 71.3713 121.12 62. 9068 228.16 0.0000 78.74 71.6293 121. 22 62.9173 228.18 43.3169 79.69 72.4250 121.78 70.3216 116.74 43.3169 80.12 71.1983 122.06 63.0034 235.69 61.4361 80.19 0.0000 122.92 75.7095 235. 96 61.4524 80.57 63.4930 123.07 83.0907 238.63 47.4301 81. 00 68.7403 265.00 77.9086 238.98 0.0000 81.07 64.8590 125.81 55.9902 240.99 47.5420 81. 75 72.7480 127.23 71.9979 242.00 47.5902 83.79 84.8067 127.91 68.8959 244.70 47.7175 84.00 77.0126 129.30 55.2365 252.40 0.0000 85.43 86.4075 131.20 68.1855 252.80 36.1743 86.55 90.5450 133.02 63.0341 254.15 0:0000 86.79 90.5892 133.52 64.1519 256.23 46.1916 86.94 90.6180 136.00 56.8810 260.90 0.0000 Page 4117 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.1553 355.39 0.0000 584.27 22.6678 264.80 47.3979 356.01 24.2150 595.83 0.0000 265.00 47.4061 364.49 0.0000 427.87 24.9307 268.22 40.0400 366.42 0.0000 602.52 0.0000 269.46 41. 3386 372.51 30.8630 604. 72 12.4907 270.03 45 .1198 375.05 28.6462. 607.14 21. 8844 271.23 45.1703 377.52 24.5967 609.32 26.0813 273.65 0.0000 356.01 33.8579 610.33 31.3123 276.40 44.5419 388.16 27.5354 614.28 20.3926 277.37 43.7396 388.63 0.0000 618.01 9.4288 277.60 43.7480 391.69 20.2419 620.36 10.4883 278.00 43.7639 264.66 34.2532 621. 93 19.9432 279.20 42.1265 401.81 23.1618 630.19 0.0000 279.54 48.0381 402.40 26.8789 631. 29 14.7611 279.70 52.2595 404.85 42.7057 633.25 14.7747 280.46 47.2340 410.95 31.6945 634.78 0.0000 283.69 38.0649 413.71 25.2153 635.95 12.6802 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 42.3584 423.72 0.0000 645.85 15.9241 285.90 0.0000 427.09 31. 08 99 657.76 14.4108 287.50 37.3443 427.87 31.1053 657.90 0.0000 290.67 45.9580 433.94 28.3881 661. 66 17.1100 293.27 0.0000 439.40 30.3854 664.57 0.0000 351.93 37.5941 453.88 . 26.8288 666.33 0.0000 295.96 37.6182 463.37 25.0574 666.50 0.0000 879.38 48.8417 468.07 25.1288 667.71 0.0000 299.98 49.7576 473.00 0.0000 677.62 17.7729 300.09 49.7623 475.06 29.1162 685.70 0.0000 300 .13 49.7635 476.78 24.2884 695.00 0.0000 301.36 30.9199 477.60 22.3561 696.49 23.8960 302.85 29.6688 482.18 19.4930 696. 51 23.8969 256.23 24.5432 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.3854 306.78 29.3357 497.08 19.6623 697.49 16.3000 308.46 34.5605 505.52 16.2996 702.65 25. 0496 311. 90 30.3266 507.63 0.0000 706.68 22. 9115 316.51 38.2690 511. 00 20.8094 711. 68 17.4941 319.41 0.0000 514.00 5.9556 720.70 0.0000 320.08 0.0000 514.00 5.9556 721. 93 0.0000 321.04 37.5358 520.40 25.4014 722.78 18.1274 323.87 39.3713 520.69 0.0000 722. 91 19.7761 325.23 31.5315 522.65 0.0000 723.31 19.7798 328.76 0.0000 527.90 0.0000 724.19 23.0850 333.37 35.2604 528.26 18.0081 727. 33 20.9142 333.97 44.0959 529.59 25.0295 733.00 20.9645 334.37 38.3758 529.87 0.0000 735.93 17.6758 338.28 36.2804 531. 02 0.0000 333.97 23.2148 338.32 36.2812 537.26 0.0000 739.50 0.0000 311. 90 . 36.3421 546.56 0.0000 747.24 13.3198 340.48 36.3421 552.55 13.1767 748.06 14.4346 340.55 0.0000 563.25 21.4050 752.31 18.3530 344.28 33.3366 569.33 24.5400 753.82 0.0000 345.93 28.0380 946.00 24.5420 756.73 3.3430 351. 06 33.9551 569.70 24.5449 756.80 3.3431 351.93 33.9767 583.19 22.6553 884.68 8. 9411 Page 4118 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 3.3555 1274.44 17.3336 1620.50 7.5345 766.42 8.3905 1001.03 9.1373 1621. 92 8.6138 766.84 8.3920 1002.74 15.5417 1678.03 0.0000 772.60 0.0000 1004.73 15.5520 1690.97 2.1854 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 10.25. 8.7 0.0000 1764.49 l .1D94 778.90 13.4927 1028.54 0.0000 1063.66 3.3322 783.70 0.0000 1037.84 7.3970 1771. 35 1.1110 785.37 7.8912 1038.76 0.0000 1791.20 0.0000 792.07 14.6943 631.29 10.1984 1808.65 4.4771 794.95 12.4475 1048.07 0.0000 1810.72 0.0000 795.86 14.7160 1049.04 7.4229 1836.06 0.9002 810.06 18.2129 1050.41 13.9243 810.29 18.2148 1063.66 17.7104 344.28 17.0770 1077.00 0.0000 810.76 17.0795 1077.34 12.1685 815.77 0.0000 1085.87 8.4463 1048.07 0.0000 1093.63 12.2296 832.01 12.6274 1099.45 13.1934 834.85 17.2375 1112. 07 12.2978 835. 71 13.7949 1112.84 14.0573 836.80 0.0000 1115. 54 16.6665 846.75 0.0000 1120. 29 7.5864 846.77 17.3157 1120.55 7.5869' 856.80 0.0000 1221.41 7.5884 860.56 4. 6413 1129. 67 2.8528 871.09 15.1423 1131. 51 0.0000 873.19 15.1540 1147.95 0.0000 875.33 0.0000 1173.23 13.4830 879.38 16.3567 1177.95 17.3584 880.51 9.6428 1189.05 14. 5111 883.24 19.3044 1204.77 14.5752 884.68 19.3145 1221.41 25.3811 889.28 18.4673 1231.02 16. 9652 894.76 16.7415 1235.36 0.0000 898.04 14. 9964 1238.28 7.8457 900.72 15.0109 1260.41 0.0000 903.28 13.2568 1271. 87 9.2371 911. 20 15.0670 1274.44 9.5074 912.08 15.6036 1274.54 9.5074 923.98 0.0000 1291.59 8.9539 926.50 14.2568 1298.22 0.0000 92 9. 11 16.0532 1312 .11 0.0000 937.49 18.7832 1332.49 5.0278 944 .13 0.0000 1362.66 0.0000 946.00 17. 0442 1365.19 8 .1113 949.00 14.3677 1368.63 0.0000 667.71 0.0000 1384.29 7.1316 962. 31 i2.9894 1408.01 4.0991 964. 08 12.6362 1457.56 0.0000 966 .17 12.6452 1460.82 6.2278 911. 20 12.6572 1489.16 4.1797 968. 97 12. 6572 1505.03 9.4389 983.53 0.0000 1584.12 5.3391 984.45 0.0000 1596.21 0.0000 Page 4119 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:08:16.27 ********************************************************************************
  • Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA] EKG GAM31.CNF;306 Background date : Z-OCT-2016 11:01:52. Sample date 1-DEC-2015 14:24:00. Acquisition date : 3-0CT-2016 07:06:55. Sample ID G405235053 Sample quantity 1.13628E+02 GRAM Detector name : GAM31 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.45 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 0 3 3 3 3 3 0 0 0 0 0 6 6 6 0 0 0 0-0 0 0 0 0 0 0 0 0 0 0 0 4 Page 4120of5809 Energy 34.92 46.45* 52.85* 63.32* 74.89 77.09* 87.25* 89.89 92.79* 129.83 186.17* 192.13 209.30 213.16 237.07* 238.66* 241.75* 253.16 295.61* 301.10 317.48 338.66* 352.12* 393.88 417.46 463.71 583.40* 609.81* 662 .11 679.68 706.37 727.99 771.11 785.68 BACKGROUND CORRECTED SAMPLE PEAK*REPORT Area 33 48 10 33 160 250 84 77 104 63 90 19 29 6 9 323 93 24 90 19 11 60 203 15 32 19 63 137 45 18 9 31 28 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 156 257 207 247 203 111 82 123 115 54 77 37 38 61 15 45 81 27 75 51 20 59 57 14 41 55 32 33 32 31 21 12 17 14 0.67 1. 31 1. 27 0.92 1. 09 0.87 0.91 1. 28 1. 29 2.25 1. 30 0.95 0.92 0.75 1. 45 1. 29 2 .13 1. 27 1. 21 1. 74 1.17 1.19 1. 20 1. 55 0.77 1. 02 1. 73 1. 29 1. 47 3.97 3.43 4.14 5.25 1. 70 69.51 92.54 105.34 126.25 149.38 153.78 174.08 179.36 185.16 259.17 371. 79 383.69 418.00 425. 72 473.50 476.68 482.85 505.66 590.50 601.48 634.21 676.54 703.44 786.91 834.03 92 6. 4 8 1165.69 1218.48 1323.01 1358 .14 1411. 4 7 1454.68 1540.88 1570.00 68 88 104 123 146 146 170 170 170 255 366 381 415 422 472 472 472 503 585 596 631 672 698 784 827 920 1159 1214 1316 1347 1404 1448 1534 1566 6 9. 25E-03 61.1 8 1. 34E-02 61. 2 6 2.77E-03235.6 7 9.07E-03 87.3 12 4.43E-02 16.1 12 6.95E-02 9.4 21 2.33E-02 19.7 21 2.15E-02 27.7 21 2.89E-02 22.5 8 l.76E-02 23.8 11 2.50E-02 22.7 5 5.14E-03 54.1 6 8.05E-03 38.6 7 1.61E-03225.0 17 2.58E-03 76.1 17 8.96E-02 6.8 17 2.58E-02 28.7 7 6.63E-03 41.2 12 2.50E-02 22.5 9 5.25E-03 72.3 6 3.15E-03 72.1 12 1.67E-02 28.8 12*5.64E-02 10.5 6 4.26E-03 45.7 14 8.89E-03 46.4 12 5.39E-03 79.2 15 l.76E-02 23.4 10 3.82E-02 12.0 12 l.25E-02 29.6 18 5.12E-03 74.9 12 2. 41E-03111. 3 13 8.49E-03 30.2 14 7.83E-03 38.6 12 3.30E-03 56.4 Fit l.26E+00 l.59E+00 4.83E+OO l.63E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235053 Acquisition date 3-0CT-2016 07:06:55 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 4 788.17 13 4 1. 43 1574.97 1566 12 3.49E-03 40.1 36 0 795.74 13 7 1. 73 1590.11 1585 10 3.56E-03 48.5 37 0 804.5S* 17 19 4.07 1607.78 1601 15 4. 71E-03 62.0 38 0 842.05 18 8 1.27 1682.66 1676 10 5.06E-03 36.7 39 0 861.42 11 20 0.85 1721. 38 1712 13 2.92E-03 92.0 40 0 866.61 16 2 2.09 1731.76 1727 9 4.38E-03 30.4 41 0 873.71 15 3 1. 95 1745.95 1740 10 4.24E-03 32.2 42 0 911. 70* 57 8 1. 63 1821. 88 1817 10 1. 59E-02 16.6 43 0 935.55 5 17 2.41 1869.56 1860 11 1.25E-03181.0 44 0 964.65 24 8 1. 57 1927.71 1921 11 6.68E-03 30.8 45 0 969.69 20 19 0.69 1937.80 1933 10 5.55E-03 47.2 46 0 1093.35 11 2 1. 54 2184.98 2181 8 3.llE-03 36.8 47 0 1121.84 18 21 1. 49 2241.92 2235 11 4.88E-03 56.8 48 0 1151. 31 6 12 0.61 2300.83 2290 12 l.67E-03122.5 49 0 1174.94 14 11 1. 53 2348.06 2342 12 3.86E-03 60.2 50 0 1239.26 47 4 0.68 2476.62 2468 18 1.30E-02 18.0 51 0 1305. 66 10 2 0.90 2609.36 2605 9 2.79E-03 41.1 52 0 1461. 40* 222 3 2 .11 2920.68 2913 14 6.16E-02 7.0 53 0 1580.37 8 0 0.83 3158.50 3155 8 2.22E-03 35.4 54 0 1765.49* 21 0 1. 97 3528.57 3523 10 5.81E-03 23.4 Flag: "*" == Peak area was modified by background subtraction Page 4121of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 08:08:18 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID l-DEC-2015 14:24:00 G405235053 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:06:55 113.63 GRAM Sample type .: Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA31 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4122 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06
  • CAN 0 01:00:06.45 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235053 Acquisition date 3-0CT-2016 07:06:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66*. 6.945E-01 1.8ti5E+Ol 1.865E+Ol 14.10 OK AS-73 53.44 10.30* 5.707E+OO 1.204E-01 l.699E+00 471.25 OK NB-95M 235.69 24.80* 3.221E+OO 7.798E-02 2.158E+OO 152.26 OK CD-109 88.03 3.70* 5.391E+OO 1. 807E+OO 2.865E+OO 69. 72 OK SN-126 64.28 9.60 5.587E+OO 4.291E-01 4.291E-01 174.69 OK 86.94 8.90 5.391E+OO 7.513E-01 7. 513E-01 69.72 OK 87.57 37.00* 5.391E+OO 1.807E-01 1.807E-01 69. 72 OK BA-137M 661.66 89.90* 1. 340E+OO 2.395E-01 2.442E-01 59.17 OK CS-137 661.66 85.10* 1.340E+OO 2.530E-01 2.580E-01 59.17 OK TL-208 277.37 6.60 2.816E+OO Line Not Found Absent 583.19 85.00* 1. 486E+OO 3.237E-01 3.237E-01 46.76 OK 860.56 12.50 1.083E+OO 4.936E-01 4.936E-01 184. 06 OK PB-210 46.54 4.25* 5.476E+OO 1.482E+OO 1. 521E+OO 122.39 OK BI-211 72.87 1. 23 5.491E+OO Line Not Found Absent 351.06 12.92* 2.285E+OO 1.179E+OO 1.179E+OO 151. 34 OK BI-212 727.33 6.67* 1.241E+OO 2.367E+OO 2.367E+OO 60.41 OK 785.37 1.10 1.167E+OO 5.920E+OO 5.920E+OO 112. 83 OK 1620.50 1. 47 6.312E-01 Line Not Found Absent PB-212 74. 82 ' 10.28 5.476E+OO 1.299E+OO 1. 299E+OO . 54. 73 OK 77 .11 17.10 5.460E+OO 1.877E+OO 1.877E+OO 18.80 OK 238.63 43.60* 3.203E+OO 1.549E+OO 1.549E+OO 13.65 OK 300.09 3.30 2.621E+OO 1. 451E+OO 1. 451E+OO 144.54 OK BI-214 609.32 45.49* 1.433E+OO 1.361E+OO 1. 361E+OO 23. 96 OK 1120.29 14.92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 OK PB-214 74.82 5.80 5.476E+OO Line Not Found <<INT Reject 77 .11 9.70 5.460E+OO 3.308E+OO 3.309E+OO 18.80 OK 87.09 3.41 5.392E+OO Line Not Found <<INT Reject 242.00 7.25 3.165E+OO Line Not Found <<INT Reject 295.22 18.42 2.664E+OO l.218E+OO 1.219E+OO 44.95 OK 351.93 35.60* 2.286E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1.433E+OO 1.361E+OO 1.361E+OO 23. 96 OK 1120.29 14.92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 OK RA-224 240.99 4.10* 3.168E+OO 2.630E+OO 2.630E+OO 110.71 OK RA-226 609.32 45.49* 1.433E+OO 1.361E+OO 1.361E+OO 23. 96 OK 1120.29 14.92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 OK AC-228 105.21 1.10 5.2l5E+OO Line Not Found Absent 338.32 11. 27 2.364E+OO 1.495E+OO 1.495E+OO 57.51 OK 794.95 4.25 1.155E+OO 1.669E+OO 1.669E+OO 97.08 OK 835.71 1. 61 1. llOE+OO Line Not Found Absent 911.20 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 OK 968. 97 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 OK RA-228 105.21 1.10 5.215E+OO Line Not Found Absent 338.32 11. 27 2.364E+OO 1.495E+OO 1.495E+OO 57.51 OK 794.95 4.25 1.155E+OO 1.669E+OO 1.669E+OO 97.08 OK 835. 71 1. 61 1. llOE+OO Line Not Found Absent 911.20 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 OK Page 4123 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235053 Acquisition date 3-0CT-2016 07:06:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status

  • 968. 97 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 OK TH-228 74.82 10.28 5.476E+OO 1.299E+OO 1.299E+OO 54.73 OK 77 .11 17.10 5.460E+OO 1.877E+OO 1.877E+OO 18.80 OK 238.63 43.60* 3.203E+OO 1.549E+OO 1.549E+OO 13.65 OK 300.09 3.30 2.621E+00 1.451E+OO 1. 451E+OO 144.54 OK TH-230 609.32 45.49* 1.433E+OO l.361E+OO 1.361E+OO 23. 96 OK 1120.29 14.92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 1.453E+00 1.453E+OO 46.87. OK PA-231 283.69 1. 70 2.761E+OO Line Not Found Absent 301.36 5.35* 2. 621E+OO 8.948E-01 8.948E-01 144.54 OK TH-232 105.21 1.10 5.215E+OO Line Not Found Absent 338.32 11.27 2.364E+OO 1.495E+OO 1.495E+OO 57.51 OK 835.71 1. 61 1.llOE+OO Line Not Found Absent 911.20 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 OK 968. 97 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 OK TH-234 63. 29 3.70* 5.587E+OO 1.113E+OO 1.113E+00 174.69 OK 92.59 4.23 5.346E+OO 3.199E+OO 3.199E+OO 45.04 OK U-234 609.32 45.49* 1.433E+OO 1.361E+OO 1.361E+OO 23. 96 OK 1120.29 '14. 92 8.740E-01 Line Not Found Absent 1764.49 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 OK U-235 89. 96 3.47 5.370E+OO 2.885E+00 2.885E+OO 55.41 OK 93.35 5.60 5.346E+00 2.416E+OO 2.416E+OO 45.04 OK 143.76 10. 96* 4. 611E+OO Line Not Found Absent 163.33 5.08 4.273E+00 Line Not Found Absent 185.72 57.20 3.902E+OO 2.725E-01 2. 725E-01 45.34 OK 205.31 5.01 3. 621E+OO Line Not Found Absent U-238 63.29 3.70* 5.587E+OO 1.113E+OO 1.113E+OO 174.69 OK 92.59 4.23 5.346E+OO 3.199E+OO 3.199E+OO 45.04 OK AM-243 43.53 5.90 5.049E+OO Line Not Found Absent 74.66 67.20* 5.476E+OO 1.987E-01 1.987E-01 54.73 OK Flag: "*" = Keyline Page 4124of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:08:19.65 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l *
  • Acquisition date 3-0CT-2016 07:06:55 Sensitivity : 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.45 Half life ratio : ***** *
  • Sample date 1-DEC-2015 14:24:00 Analyst initials: MXRl *
  • Sample ID G4052350.53 Sample Quantity 1.1363E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN * .
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM K-40 l.865E+Ol 2.577E+OO 9.734E-01 AS-73 1.699E+OO 7.848E+OO 9.571E+OO NB-95M 2.158E+OO 3.220E+OO 7 .112E+OO CD-109 2.865E+OO 1.957E+OO 2. 331E+OO SN-126 1.807E-01 l.235E-01 l.469E-01 BA-137M 2.442E-01 l.416E-01 l .196E-01 CS-137 2.580E-01 1. 496E-01 1.263E-01 TL-208 3.237E-01 1.483E-01 1.132E-01 PB-210 1. 521E+OO 1.825E+OO 1.575E+OO BI-211 1.179E+OO 1. 749E+OO 6.353E-01 BI-212 2.367E+OO l.401E+OO 1.623E+OO PB-212 1.549E+OO 2.072E-01 1.508E-01 BI-214 1.361E+OO 3 .196E-01 2.487E-01 PB-214 1.647E+OO 3.387E-01 6.060E-01 RN-222 1.361E+OO 3 .196E-01 2.487E-01 RA-224 2.630E+OO 2.853E+OO 1.619E+OO RA-226 1.361E+OO 3.196E-01 2.487E-01 AC-228 1.359E+OO 4.425E-01 4.269E-01 RA-228 1.359E+OO 4.425E-01 4.269E-01 TH-228 1.549E+OO 2.072E-01 1.508E-01 TH-230 1.361E+OO 3.195E-01 2.486E-01 PA-231 8.948E-01 1.268E+OO 1.247E+OO TH-232 l.359E+OO 4.425E-01 4.269E-01 TH-234 l.113E+OO 1.906E+OO 1.934E+OO U-234 l.361E+OO 3.195E-0'1 2.486E-01 U-235 1.112E-01 2.856E-01 5.214E-01 U-238 1.113E+OO 1.906E+OO l.934E+OO AM-243 l.987E-01 1.066E-01 9.914E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM BE-7 -1.162E+Ol 2.455E+Ol 4.373E+Ol NOT IDENT. NA-22 -4.217E-02 9.695E-02 1. 752E-01 NOT IDENT. Page 4125of5809 NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 -8.769E-03 5.684E-02 l.230E-01 NOT IDENT. SC-46 8.840E-02 6.221E-01 1.323E+OO FAIL ABUN V-48 O.OOOE+OO 3.685E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 8.926E+02 O.OOOE+OO SHORT HLIF MN-54 -2. 729E-02 1.379E-01 2.479E-01 NOT IDENT. C0-56 6.006E-01 1.077E+OO 2.176E+OO FAIL ABUN MN-56 O.OOOE+OO 1.814E+41 O.OOOE+OO SHORT HLIF C0-57 3.881E-02 6.601E-02 l.278E-01 NOT IDENT. C0-58 6.132E-02 1.226E+OO 2 .113E+OO NOT I DENT .* FE-59 3.195E+OO l.567E+Ol 3.178E+Ol NOT IDENT. C0-60 -4.484E-03 8.580E-02 l.676E-01 NOT IDENT. ZN-65 1.647E-01 3.409E-01 6.743E-01 NOT IDENT. GE-68 -2.607E-01 3.669E+OO 7.472E+OO NOT IDENT. AS-74 0.000E+OO l.473E+04 O.OOOE+OO SHORT HLIF SE-75 -1.205E-01 4.214E-01 7.135E-01 NOT IDENT. BR-77 O.OOOE+OO 2.762E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 1. 813E+03 O.OOOE+OO SHORT HLIF RB-83 1.675E+OO 1. 272E+OO 2.846E+OO NOT IDENT. KR-85 -3.053E+Ol 1.857E+Ol 2.840E+Ol NOT IDENT. SR-85 -3.468E+OO 2.109E+OO 3.225E+OO NOT IDENT. RB-86 O.OOOE+OO 5.854E+04 O.OOOE+OO SHORT HLIF Y-88 1.564E-01 3.224E-01 9.000E-01 NOT IDENT. Y-91 l.363E+02 1.088E+03 2 .191E+03 NOT IDENT. NB-94 -7.107E-03 6.854E-02 l.112E-01 NOT IDENT. NB-95 3.041E-03 2.217E+OO 3.635E+OO NOT IDENT. ZR-95 2.419E-01 3.079E+OO 5.864E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 929E+41 *o.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.549E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.084E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.143E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 496E-02 5 .119E-02 8.373E-02 NOT IDENT. RH-102 -9.265E-04 9.445E-02 l.834E-01 NOT IDENT. RU-103 -1.245E+OO 9.576E+OO 1.845E+Ol FAIL ABUN RH-106 2.162E-01 8. 727E-01 1.746E+OO NOT IDENT. RU-106 2.162E-01 8.727E-01 l.746E+OO NOT IDENT. AG-108M 7.238E-03 5.566E-02 l.074E-01 NOT IDENT. AG-llOM 2.637E-03 1. 349E-01 2.888E-01 FAIL ABUN SN-113 -1.369E-01 4.188E-01 6.919E-01 NOT IDENT. CD-115 O.OOOE+OO 4.224E+40 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 2 .118E+05 0.000E+OO SHORT HLIF TE-123M -2.899E-02 2.079E-01 3.712E-01 NOT IDENT. SB-124 -1.536E-01 5 .196E+OO 1.048E+Ol NOT IDENT. SB-125 3. 211E-02 1.991E-01 3.874E-01 FAIL ABUN TE-125M 3.297E+Ol 4.267E+02 7.870E+02 NOT IDENT. I-126 O.OOOE+OO 2.091E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.884E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO l.488E+23 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.572E+10 0.000E+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.806E+27 O.OOOE+OO SHORT HLIF BA-133 6.087E-03 8.316E-02 1.453E-01 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 1.099E-01 l.046E-01 1.998E-01 FAIL ABUN CS-135 1.598E-02 2.682E-01 4. 724E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 7.328E+05 O.OOOE+OO SHORT HLIF CE-139 1. 094E-01 1.869E-01 3.541E-01 NOT IDENT. BA-140 O.OOOE+OO 3.403E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO l.283E+06 O.OOOE+OO SHORT HLIF CE-141 -1.163E+Ol 4.342E+Ol 7.463E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 3.845E-01 5.588E-01 1.016E+OO NOT IDENT. PM-144 -4.117E-03 9.409E-02 l.787E-01 NOT IDENT. PR-144 -2. 133E+00 8.554E+OO 1. 556E+Ol NOT IDENT. PM-146 6.430E-02 7.829E-02 l.655E-01 NOT IDENT. ND-147 O.OOOE+OO 6.963E+07 O.OOOE+OO SHORT HLIF PM-147 -1.987E+02 1.102E+03 l.995E+03 NOT IDENT. PM-149 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF EU-150 3.877E-03 4.925E-02 8.644E-02 FAIL ABUN EU-152 8.353E-02 l.595E-01 3.032E-01 FAIL ABUN GD-153 -2. 851E-02 2.426E-01 4.105E-01 NOT IDENT. EU-154 -l.030E-01 2.368E-01 4.280E-01 FAIL ABUN EU-155 -4.819E-02 l.468E-01 2.627E-01 FAIL ABUN TB-160 -3.728E-01 3.322E+OO 6.676E+OO FAIL ABUN H0-166M -5.595E-02 l.134E-01 l.843E-01 NOT IDENT. TM-171 3. 572E+OO l.649E+Ol 1.971E+Ol FAIL ABUN HF-172 l.564E-01 3.590E-01 6.356E-01 FAIL ABUN Page 4126of5809 LU-172 1.714E-01 1.238E-01 3.016E-01 FAIL ABUN LU-176 -2.145E-02 3.821E-02 7.012E-02 FAIL ABUN HF-181 4.405E-03 8.388E+00 l.619E+Ol NOT IDENT. TA-182 6.625E-01 1.889E+OO 3.902E+OO FAIL ABUN RE-183 -4.310E-01 2.217E+OO 4.075E+OO NOT IDENT. RE-184 -3.087E+Ol 6.468E+Ol l.200E+02 NOT IDENT. W-188 -5.636E+Ol 2.052E+02 3.482E+02 FAIL ABUN IR-192 6.475E-01 9.149E-01 l.773E+OO FAIL ABUN HG-203 -3.671E+OO 5. 096E+00 8.102E+OO NOT IDENT. BI-207 . -7.355E-02 9.382E-02 l.605E-01 FAIL ABUN PB-211 -4.319E-01 1.037E+OO l.910E+OO NOT IDENT. RN-219 -2.174E-01 6.073E-01 l.126E+OO NOT IDENT. RA-223 2.570E-01 1.012E+OO 2.007E+OO FAIL ABUN AC-227 1.942E-01 3.963E-01 6.999E-01 FAIL ABUN TH-227 1.942E-01 3.963E-01 6.999E-01 FAIL ABUN TH-229 7.441E-01 7.895E-01 l.383E+OO FAIL ABUN TH-231 2.570E-01 l.012E+OO 2.007E+OO FAIL ABUN PA-233 2.688E-02 l.023E-01 2.033E-01 FAIL ABUN PA-234 1.555E-01 5.005E-01 l.059E+00 FAIL ABUN PA-234M 4.413E-01 7.927E+OO 1. 580E+Ol NOT IDENT. NP-237 2.688E-02 l.023E-01 2.033E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 1.391E-01 3.487E-01 6.601E-01 NOT IDENT. PU-239 O.OOOE+OO 6. 651E+o2 9.589E+02 FAIL ABUN AM-241 -l.079E-02 1. 060E-01 l.953E-01 NOT IDENT. CM-243 1. 828E-02 1.318E-01 2.457E-01 NOT IDENT. BK-247 1.855E-02 1. 380E-01 2.460E-01 NOT IDENT. CM-247 -1.538E-02 5.768E-02 1.080E-01 NOT I DENT., CF-249 -8.217E-03 5.797E-02 1.112E-01 FAIL ABUN CF-251 -7.304E-02 2.008E-01 3.460E-01 NOT IDENT. ANH-511 -8.832E-02 9.035E-02 1.794E-01 NOT IDENT. Page 4127of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:08:17.30 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 209 10.66* 6.945E-01 1.865E+Ol l.865E+Ol 14.10 AS-73 53.44 11 10.30* 5.707E+OO 1.204E-01 l.699E+OO 471.25 NB-95M 235.69 9 24.80* 3.221E+OO 7.798E-02 2.158E+OO 152.26 CD-109 88.03 88 3.70* 5.391E+OO 2.930E+OO 4.645E+OO 39.40 SN-126 64.28 35 9.60 5.587E+OO 4.291E-01 4.291E-01 174.69 86.94 88 8.90 5.391E+OO 1.218E+OO 1. 218E+OO 39.40 87.57 88 37.00* 5.391E+OO 2.930E-01 2.930E-01 39.40 BA-137M 661.66 44 89.90* l.340E+OO 2.395E-01 2.442E-01 59.17 CS-137 661.66 44 85.10* 1.340E+OO 2.530E-01 2.580E-01 59.17 TL-208 277.37 ------6.60 2.816E+00 ------Line Not Found ------583.19 62 85.00* 1. 486E+OO 3.237E-01 3.237E-01 46.76 860.56 10 12.50 1.083E+OO 4.936E-01 4.936E-01 184.06 PB-210 46.54 52 4.25* 5.476E+OO 1.482E+OO l.521E+00 122.39 BI-211 72.87 ------1. 23 5.491E+OO ------Line Not Found ------351.06 203 12.92* 2.285E+OO 4.536E+OO 4.536E+OO 20.99 BI-212 727.33 30 6.67* 1.241E+OO 2.367E+OO 2.367E+OO 60.41 785.37 11 1.10 1.167E+OO 5.920E+00 5.920E+OO 112. 83 1620.50 ------1. 47 6.312E-01 ------Line Not Found ------PB-212 74.82 169 10.28 5.476E+OO 1. 986E+OO l.986E+00 32.23 77 .11 265 17.10 5.460E+00 l.877E+00 1.877E+OO 18.80 238.63 327 43.60* 3.203E+OO 1.549E+OO 1.549E+OO 13. 65 300.09 19 3.30 2. 621E+OO 1. 451E+OO 1.451E+OO 144.54 BI-214 609.32 134 45.49* 1.433E+OO 1. 361E+OO l.361E+OO 23. 96 1120. 29 ------14.92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 1.453E+OO l.453E+00 46.87 PB-214 74.82 169 5.80 5.476E+OO 3.521E+OO 3.522E+OO 32.23 77.11 265 9.70 5.460E+OO 3.308E+OO 3.309E+OO 18.80 87.09 88 3.41 5.391E+OO 3.179E+OO 3.180E+OO 39.40 242.00 94 7.25 3.168E+OO 2.705E+OO 2.706E+OO 57.39 295.22 90 18.42 2.664E+OO 1.218E+OO 1. 219E+OO 44.95 351. 93 203 35.60* 2.285E+OO 1. 646E+OO 1.647E+OO 20.99 RN-222 609.32 134 45.49* l.433E+00 1. 361E+OO 1.361E+OO 23. 96 1120.29 ------14.92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 l.453E+00 1.453E+OO 46.87 RA-224 240.99 94 4.10* 3.168E+OO 4.784E+00 4.784E+OO 57.39 RA-226 609.32 134 45.49* 1.433E+OO 1. 361E+OO 1.361E+OO 23. 96 1120.29 ------14.92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 l.453E+OO l.453E+00 46.87 AC-228 105.21 ------1.10 5.215E+OO ------Line Not Found ------338.32 60 11. 27 2.364E+OO 1.495E+OO 1.495E+OO 57.51 794.95 12 4.25 1.155E+OO 1.669E+OO 1.669E+OO 97.08 835.71 ------1. 61 1. llOE+OO ------Line Not Found ------911. 20 55 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 968. 97 19 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 RA-228 105.21 ------1.10 5.215E+OO ------Line Not Found ------338.32 60 11. 27 2.364E+OO 1.495E+OO 1.495E+OO 57.51 794.95 12 4.25 1.155E+OO l.669E+OO 1.669E+OO 97.08 Page 4128of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235053 Acquisition date 3-0CT-2016 07:06:55 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 835. 71 ------1. 61
  • 1. llOE+OO ------Line Not Found ------. 911. 20 55 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 968. 97 19 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 TH-228 74.82 169 10.28 5.476E+OO 1. 98 6E+OO 1. 986E+OO 32.23 77 .11 265 17.10 5.460E+OO 1.877E+OO 1.877E+OO 18.80 238.63 327 43.60* 3.203E+OO 1.549E+OO 1. 549E+OO 13. 65 300.09 19 3.30 2.621E+OO 1. 451E+OO 1. 451E+OO 144.54 TH-230 609.32 134 45.49* 1.433E+OO 1.361E+OO l.361E+OO 23. 96 1120.29 ------14.92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 PA-231 283.69 ------1. 70 2.761E+OO ------Line Not Found ------301.36 19 5.35* 2. 621E+OO 8.948E-01 8.948E-01 144.54 TH-232 105.21 ------1.10 5.215E+OO ------Line Not Found ------338.32 60 11. 27 2.364E+OO 1.495E+OO 1.495E+OO 57.51 835. 71 ------1. 61 1. llOE+OO ------Line Not Found ------911.20 55 25.80* 1.035E+OO 1.359E+OO 1.359E+OO 33.22 968.97 19 15.80 9.842E-01 8.136E-01 8.136E-01 94.46 TH-234 63.29 35 3.70* 5.587E+OO 1.113E+OO 1.113E+OO 174.69 92.59 109 4.23 5.346E+OO 3.199E+OO 3.199E+OO 45.04 U-234 609.32 134 45.49* 1.433E+OO 1. 361E+OO 1.361E+OO 23.96 1120.29 ------14.92 8.740E-01 ------Line Not Found ------1764.49 20 15.30 5.810E-01 1.453E+OO 1.453E+OO 46.87 U-235 89. 96 81 3.47 5.370E+OO 2.885E+OO 2.885E+OO 55.41 93.35 109 5.60 5.346E+OO 2.416E+OO 2.416E+OO 45.04 143.76 ------10. 96* 4.611E+OO ------Line Not Found ------163.33 ------5.08 4.273E+OO ------Line Not Found ------185. 72 92 57.20 3.902E+OO 2. 725E-01 2.725E-01 45.34 205.31 ------5.01 3.621E+OO ------Line Not Found ------U-238 63.29 35 3.70* 5.587E+OO 1.113E+OO 1.113E+OO 174.69 92.59 109 4.23 5.346E+OO 3.199E+OO 3.199E+OO 45.04 AM-243 43.53 ------5.90 5.049E+OO ------Line Not Found ------74.66 169 67.20* 5.476E+OO 3.039E-01 3.039E-01 32.23 Flag: "*" Key line Page 4129of5809 Summary of Nuclide Activity Sample ID : G405235053 Acquisition date Page : 3 3-0CT-2016 07:06:55 Total number of lines in spectrum 54 Number of unidentified lines 15 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 AS-73 NB-95M CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 Hlife l.25E+09Y 80.30D 64.030 461.40D 2.30E+05Y 30.08Y 30.08Y 1.41E+10Y 22.20Y 7.04E+08Y 1. 41E+10Y l.41E+l0Y 1600.00Y 1600.00Y 1600. OOY 1.41E+10Y 1600.00Y 1.41E+10Y l.41E+l0Y l.41E+10Y 7.54E+04Y 7.04E+08Y l.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y Decay 1. 00 14.1 27.7 1. 59 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity ' Uncorrected pCi/GRAM 1.865E+Ol 1.204E-01 7.798E-02 2.930E+OO 2.930E-01 2.395E-01 2.530E-01 3.237E-01 1.482E+OO 4.536E+OO 2.367E+OO 1.549E+OO 1.361E+OO l.646E+00 1. 361E+OO 4.784E+OO 1.361E+OO 1.359E+00 1.359E+OO 1.549E+OO 1. 361E+OO 8.948E-01 1.359E+OO l .113E+OO 1.361E+OO 2.725E-01 l .113E+00 3.039E-01 5.538E+Ol 5.538E+Ol Decay Corr pCi/GRAM l.865E+Ol 1.699E+OO 2.158E+OO 4.645E+OO 2.930E-01 2.442E-01 2.580E-01 3.237E-01 1. 521E+OO 4.536E+OO 2.367E+OO 1.549E+OO 1. 361E+OO 1.647E+OO 1. 361E+OO 4.784E+OO 1.361E+OO 1.359E+OO 1.359E+OO 1.549E+00 1.361E+OO 8.948E-01 1.359E+OO 1.113E+OO 1.361E+OO 2.725E-01 1.113E+OO 3.039E-01 6. 081E+Ol 6. 081E+Ol 72. 22% Decay Corr 2-Sigma Error 0.263E+Ol 8.008E+OO 3.285E+OO 1.830E+OO l.154E-01 l.445E-01 1.526E-01 1. 513E-01 1.862E+OO 0.952E+OO 1.430E+OO 0. 211E+OO 0.326E+OO 0.346E+00 0.326E+OO 2.745E+OO 0.326E+OO 0. 451E+OO 0. 451E+OO 0.211E+OO 0.326E+OO 12.93E-01 0. 451E+OO 1.945E+OO 0.326E+OO 1. 236E-01 1.945E+OO 0.980E-01 "M" Manually accepted 2-Sigma %Error 14.10 471.25 152.26 39.40 39.40 59.17 59.17 46.76 122.39 20.99 60.41 13.65 23. 96 20.99 23. 96 57.39 23. 96 33.22 33.22 13.65 23. 96 144.54 33.22 174.69 23. 96 45.34 174.69 32.23 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4130 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235053 Acquisition date : 3-0CT-2016 07:06:55 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 34.92 36 170 0.67 69.51 68 6 9.25E-03 **** 1. 44E+OO 0 129.83 66 56 2.25 259.17 255 8 l.76E-02 47.7 4.85E+OO T 0 192.13 19 37 0.95 383.69 381 5 5.14E-03 **** 3. 81E+OO T 0 209.30 30 39 0.92 418.00 415 6 8.05E-03 71.3 3.57E+OO 0 213.16 6 62 0.75 425.72 422 7 1. 61E-03 **** 3.51E+OO 0 253.16 24 27 1. 27 505.66 503 7 6.63E-03 82.5 3.05E+OO T 0 317.48 11 20 1.17 634. 21 631 6 3.15E-03 **** 2.50E+OO T 0 393.88 15 14 1. 55 786.91 784 6 4.26E-03 91. 5 2.07E+OO 0 417.46 32 41 0.77 834.03 827 14 8.89E-03 92.7 l.97E+OO 0 463. 71 19 54 1. 02 926.48 920 12 5.39E-03 **** l.80E+OO T 0 679.68 18 30 3.97 1358.14 1347 18 5.12E-03 **** 1. 31E+OO 0 706.37 8 21 3.43 1411.47 1404 12 2.41E-03 **** l.27E+OO T 0 771.11 27 16 5.25 1540.88 1534 14 7.83E-03 77.2 l.18E+OO T 4 788.17 12 4 1. 43 1574.97 1566 12 3.49E-03 80.2 l.16E+OO 0 804.59 16 19 4.07 1607.78 1601 15 4. 71E-03 **** 1.14E+OO 0 842.05 18 8 1.27 1682.66 1676 10 5.06E-03 73.5 1.lOE+OO 0 866.61 15 2 2.09 1731.76 1727 9 4.38E-03 60.9 1.08E+OO 0 873. 71 15 3 1. 95 1745.95 1740 10 4.24E-03 64.5 1.07E+OO T 0 935.55 4 16 2.41 1869.56 1860 11 1.25E-03 **** 1.0lE+OO 0 964. 65 23 8 1. 57 1927.71 1921 11 6.68E-03 61. 5 9.88E-01 T 0 1093.35 11 2 1. 54 2184.98 2181 8 3. llE-03 73.7 8.92E-01 T 0 1121.84 17 20 1. 49 2241.92 2235 11 4.88E-03 **** 8.73E-01 T 0 1151.31 6 11 0.61 2300.83 2290 12 1. 67E-03 **** 8.54E-01 0 1174.94 13 11 1. 53 2348.06 2342 12 3.86E-03 **** 8.40E-01 0 1239.26 44 4 0.68 2476.62 2468 18 1.30E-02 36.0 8.03E-01 T 0 1305. 66 10 2 0.90 2609.36 2605 9 2.79E-03 82.3 7.67E-01 0 1580.37 8 0 0.83 3158.50 3155 8 2.22E-03 70.7 6.46E-01 Flags: "T" = Tentatively associated Page 4131 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:08:31.28 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l * *Acquisition date 3-0CT-2016 07:06:55 Sensitivity 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.45 Half life ratio : ***** *
  • Sample date 1-DEC-2015 14:24:00 Nuclide Library : SOLID *
  • Sample ID G405235053 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.1363E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 NB-95M CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 Le (pCi/GRAM 3.666E-01 4.568E+OO 3.246E+OO 1.093E+OO 6.890E-02 5.222E-02 5.517E-02 4.953E-02 7.476E-01 2.873E-01 7.039E-01 6.897E-02 1.107E-01 2.921E-01 1.107E-01 7.404E-01 1.107E-01 1. 801E-01 1. 801E-01 6.897E-02 1.106E-01 5.592E-01 1. 801E-01 9.232E-01 1.106E-01 2.428E-01 9.232E-01 4. 711E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4132 of 5809 Le (pCi/GRAM 1.921E+Ol 7.339E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 F.,E-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88. Y-91 NB-94 NB-95 ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page4133 of5809 4.579E-02 5.544E-01 O.OOOE+OO O.OOOE+OO 1. 081E-01 9.605E-01 O.OOOE+OO 5.928E-02 8.979E-01 1.378E+Ol 7.065E-02 2.892E-01 3.064E+OO O.OOOE+OO 3.261E-01 O.OOOE+OO O.OOOE+OO 1. 280E+OO 1. 288E+Ol 1. 463E+OO 0.000E+OO 3.324E-01 9.379E+02 4.860E-02 1.610E+OO 2.554E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.862E-02 7. 831E-02 7.920E+OO 7.599E-01 7.599E-01 4.850E-02 1.173E-01 3.038E-01 O.OOOE+OO O.OOOE+OO 1.709E-01 4.185E+OO 1.744E-01 3. 671E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 6.588E-02 O.OOOE+OO 8.793E-02 2.168E-01 O.OOOE+OO O.OOOE+OO 1.646E-01 O.OOOE+OO O.OOOE+OO 3.449E+Ol O.OOOE+OO 4. 722E-01 7.678E-02 6.688E+OO 7.439E-02 o*. OOOE+OO 9.180E+02 O.OOOE+OO 3.925E-02 1.365E-01 1.910E-01 1.793E-01 1.220E-01 2.811E+OO 7.909E-02 9.400E+OO 2.956E-01 1.292E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-..211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 4134of5809 3 .133E-02 7.132E+OO 1.691E+OO 1.940E+00 5. 091E+Ol 1.567E+02 8.093E-01 3.673E+OO 6.693E-02 8.376E-01 4. 964E-01 9 .119E-01 3.185E-01 3.185E-01 6.377E-01 9.ll9E-01 9.245E-02 4.553E-01 6.794E+OO 9.245E-02 O.OOOE+OO 3.075E-01 4.500E+02 9.318E-02 1.144E-01 1.128E-01 4.788E-02 4. 911E-02 1. 601E-01 8. 431E-02 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN, SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:08:37.00 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235053.CNF;l *
  • Acquisition date 3-0CT-2016 07:06:55 Sensitivity 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.45 Half life ratio : ***** *
  • Sample date 1-DEC-2015 14:24:00 Nuclide Library : SOLID *
  • Sample ID G405235053 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.1363E+02 GRAM *
  • Quantity Err(%) : 1.7601E-03 % *
  • Wet wt corr 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff.'Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) K-40 1.865E+Ol 2.755E+OO 2.755E+OO AS-73 1.699E+OO 7.856E+OO 7.856E+OO NB-95M 2.158E+OO 3.224E+OO 3.224E+OO CD-109 2.865E+OO 1.984E+OO 1.984E+OO SN-126 1. 807E-01 1. 248E-01 1.248E-01 BA-137M 2.442E-01 1. 420E-01 1.420E-01 CS-137 2.580E-01 1.500E-01 1.500E-01 TL-208 3.237E-01 1. 489E-01 1. 489E-01 PB-210 1. 521E+OO 1.830E+OO 1.830E+OO BI-211 1.179E+OO 1. 761E+OO 1. 761E+OO BI-212 2.367E+OO 1.407E+OO 1.407E+OO PB-212 1.549E+OO 2.228E-01 2.228E-01 BI-214 1.361E+OO 3.249E-01 3.249E-01 PB-214 1.647E+OO 3.456E-01 3.456E-01 RN-222 1.361E+OO 3.249E-01 3.249E-01 RA-224 2.630E+OO 2.860E+OO 2.860E+OO RA-226 1.361E+OO 3.249E-01 3.249E-01 AC-228 1.359E+OO 4.479E-01 4.479E-01 RA-228 l.359E+OO 4.479E-01 4.479E-01 TH-228 1.549E+OO 2.228E-01 2.228E-01 TH-230 1. 361E+OO 3.248E-01 3.248E-01 PA-231 8.948E-01 1. 282E+OO 1.282E+OO TH-232 1.359E+OO 4.479E-01 4.479E-01 TH-234 1.113E+OO 1.922E+OO 1.922E+OO U-234 1. 361E+OO 3.248E-01 3.248E-01 U-235 1.112E-01 2.857E-01 2.857E-01 U-238 1.113E+OO 1.922E+OO 1.922E+OO AM-243 l.987E-01 l.081E-01 1.081E-01 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.162E+Ol 2.455E+01 2.510E+Ol NOT IDENT. NA-22 -4.217E-02 9.697E-02 9.881E-02 NOT IDENT. Page 4135of5809 NA-24 -1.000E+41 2.992E+41 O.OOOE+OO SHORT HLIF AL-26 -8.769E-03 5.685E-02 5.698E-02 NOT IDENT. SC-46 8.840E-02 6.221E-01 6.234E-01 FAIL ABUN V-48 1.428E+04 3.686E+04 3.741E+04 SHORT HLIF CR-51 -2.080E+Ol 8.926E+02 8.926E+02 SHORT HLIF MN-54 -2. 729E-02 1.379E-01 1.384E-01 NOT IDENT. C0-56 6.006E-01 1.077E+OO 1. lllE+OO FAIL ABUN MN-56 l.OOOE+41 1.814E+41 O.OOOE+OO SHORT HLIF C0-57 3.881E-02 6.603E-02 6. 831E-02 NOT IDENT. C0-58 6 .132E-02 .1. 226E+OO 1.226E+OO NOT IDENT. FE-59 3.195E+OO 1.567E+Ol 1.573E+Ol NOT IDENT. C0-60 -4.484E-03 8.580E-02 8.582E-02 NOT IDENT. ZN-65 1.647E-01 3.409E-01 3.489E-01 NOT IDENT. GE-68 -2.607E-01 3.669E+OO 3. 671E+OO NOT IDENT. AS-74 -6.317E+03 1.474E+04 1. 501E+o4 SHORT HLIF SE-75 -l.205E-01 4.215E-01 4.249E-01 NOT IDENT. BR-77 2.065E+39 l.828E+40 O.OOOE+OO SHORT HLIF SR-82 5.037E+Ol 1.813E+03 1. 813E+o3 SHORT HLIF RB-83 1. 675E+OO 1.292E+OO 1.497E+OO NOT IDENT. KR-85 -3.053E+Ol 1. 861E+Ol 2.315E+Ol NOT IDENT. SR-85 -3.468E+OO 2 .114E+OO 2.629E+OO NOT IDENT. RB-86 -2.194E+04 5.854E+04 5.937E+04 SHORT HLIF Y-88 l.564E-01 3.226E-01 3.302E-01 NOT IDENT. Y-91 l.363E+02 l.088E+03 1. 089E+03 NOT IDENT. NB-94 -7.107E-03 6.854E-02 6.861E-02 NOT IDENT. NB-95 3.041E-03 2.217E+00 2.217E+OO NOT IDENT. ZR-95 2.419E-01 3.079E+OO 3. 081E+OO NOT IDENT. NB-97' 1.000E+41 l.929E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 1.550E+41 O.OOOE+OO SHORT HLIF M0-99 2.120E+33 2.090E+33 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 l.147E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 496E-02 5.126E-02 5 .171E-02 NOT IDENT. RH-102 -9.265E-04 9.445E-02 9.445E-02 NOT IDENT. RU-103 -1.245E+OO 9.576E+OO 9.592E+OO FAIL ABUN RH-106 2.162E-01 8.728E-01 8.782E-01 NOT IDENT. RU-106 2.162E-01 8.728E-01 8.782E-01 NOT IDENT. AG-108M 7.238E-03 5.566E-02 5.576E-02 NOT IDENT. AG-llOM 2.637E-03 1.349E-01 l.349E-01 FAIL ABUN SN-113 -l.369E-01 4.188E-01 4.233E-01 NOT IDENT. CD-115 -6.488E+39 4.226E+40 O.OOOE+OO SHORT HLIF SN-ll 7M -6. 911E+04 2.120E+05 2.143E+05 SHORT HLIF TE-123M -2.899E-02 2.079E-01 2.083E-01 NOT IDENT. SB-124 -l.536E-01 5 .196E+OO 5 .196E+OO NOT IDENT. SB-125 3. 211E-02 l.991E-01 1.997E-01 FAIL ABUN TE-125M 3.297E+Ol 4.267E+02 4.269E+02 NOT IDENT. I-126 1.095E+06 2.097E+06 2.154E+06 SHORT HLIF SB-126 1. 263E+06 2.894E+06 2.949E+06 SHORT HLIF SB-127 4.091E+22 1.595E+23 O.OOOE+OO SHORT HLIF I-131 7.012E+09 1. 572E+l0 1. 604E+10 SHORT HLIF I-132 -1.000E+41 1. 920E+42 O.OOOE+OO SHORT HLIF TE-132 1.453E+27 2.870E+27 0.000E+OO SHORT HLIF BA-133 6.087E-03 8.316E-02 8. 321E-02 NOT IDENT. I-133 -1.000E+41 3.567E+41 O.OOOE+OO SHORT HLIF CS-134 l.099E-01 1. 047E-01 l.158E-01 FAIL ABUN CS-135 1.598E-02 2.682E-01 2.683E-01 NOT IDENT. I-135 -1.000E+41 7.508E+41 O.OOOE+OO SHORT HLIF CS-136 -8.042E+02 7.328E+05 7.328E+05 SHORT HLIF CE-139 1.094E-01 1. 882E-01 1.945E-01 NOT IDENT. BA-140 -1. 774E+06 3.404E+06 3.497E+06 SHORT HLIF LA-140 -2.828E+05 1.283E+06 l.290E+06 SHORT HLIF CE-141 -1.163E+Ol 4.342E+Ol 4.374E+Ol NOT IDENT. CE-143 1.000E+41 4.432E+41 O.OOOE+OO SHORT HLIF CE-144 3.845E-01 5.592E-01 5.854E-01 NOT IDENT. PM-144 -4. ll 7E-03 9.409E-02 9.411E-02 NOT IDENT. PR-144 -2.133E+OO 8.554E+OO 8.608E+OO NOT IDENT. PM-146 6.430E-02 7.843E-02 8.362E-02 NOT IDENT. ND-147 2.814E+07 6.964E+07 7.079E+07 SHORT HLIF PM-147 -l.987E+02 1.102E+03 1.105E+03 NOT IDENT. PM-149 7.516E+40 6.692E+41 O.OOOE+OO SHORT HLIF EU-150 3.877E-03 4.925E-02 4.928E-02 FAIL ABUN EU-152 8.353E-02 1. 596E-01 1.640E-01 FAIL ABUN GD-153 -2.851E-02 2.426E-01 2.430E-01 NOT IDENT. EU-154 -1.030E-01 2.369E-01 2.414E-01 FAIL ABUN EU-155 -4.819E-02 1.468E-01 l.484E-01 FAIL ABUN TB-160 -3. 728E-01 3.322E+OO 3.326E+OO FAIL ABUN H0-166M -5.595E-02 1.134E-01 l.162E-01 NOT IDENT. TM-171 3. 572E+OO 1.650E+Ol l.658E+Ol FAIL ABUN HF-172 1.564E-01 3.599E-01 3.667E-01 FAIL ABUN Page 4136 of 5809 LU-172 1.714E-01 1.250E-01 1. 469E-01 FAIL ABUN LU-176 -2.145E-02 3.822E-02 3.942E-02 FAIL ABUN HF-181 4.405E-03 8.388E+OO 8.388E+OO NOT IDENT. TA-182 6.625E-01 1.889E+OO 1.912E+OO FAIL ABUN RE-183 -4.310E-01 2.218E+OO 2.227E+OO NOT IDENT. RE-184 -3.087E+Ol 6.512E+Ol 6.659E+Ol NOT IDENT. W-188 -5.636E+Ol 2.053E+02 2.069E+02 FAIL ABUN IR-192 6.475E-Ol 9.153E-01 9.607E-01 FAIL ABUN HG-203 -3.671E+OO 5.099E+OO 5.361E+OO NOT IDENT. BI-207 -7.355E-02 9.386E-02 9.955E-02 FAIL ABUN PB-211 -4.319E-01 1.037E+OO 1.056E+OO NOT IDENT. RN-219 -2.174E-01 6.079E-01 6.158E-01 NOT IDENT. RA-223 2.570E-01 1.012E+OO 1.019E+OO FAIL ABUN AC-227 1.942E-01 3.972E-01 4.067E-01 FAIL ABUN TH-227 l.942E-01 3.972E-01 4.067E-01 FAIL ABUN TH-229 7.441E-01 7.903E-01 8.586E-01 FAIL ABUN TH-231 2.570E-01 1. 012E+OO 1.019E+OO FAIL ABUN PA-233 2.688E-02 1.023E-01 l.030E-01 FAIL ABUN PA-234 1.555E-01 5.312E-01 5.358E-01 FAIL ABUN PA-234M 4.413E-01 7.927E+OO 7.930E+OO NOT IDENT. NP-237 2.688E-02 1.023E-01 1.030E-01 FAIL ABUN NP-238 1.000E+41 3.104E+41 0.000E+OO SHORT HLIF NP-239 1. 391E-01 3.488E-01 3.544E-01 NOT IDENT. PU-239 l.423E+03 6.681E+02 9.263E+02 FAIL ABUN AM-241 -1.079E-02 1.060E-01 l.062E-01 NOT IDENT. CM-243 1.828E-02 1.318E-01 1.321E-01 NOT IDENT. BK-247 l.855E-02 1.381E-01 1.383E-01 NOT IDENT. CM-247 -l.538E-02 5.773E-02 5.815E-02 NOT IDENT. CF-249 -8.217E-03 5.798E-02 5.809E-02 FAIL ABUN CF-251 -7.304E-02 2.0lOE-01 2.037E-01 NOT IDENT. ANH-511 -8.832E-02 9.043E-02 9.880E-02 NOT IDENT. Page 4137 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 100.7624 87.09 76.5680 136.47 61.9439 45.60 115.4579 87.57 76.6492 140.51 0.0000 46.54 115.8266 88.03 76.7267 143.76 49.9167 49. 72 0.0000 88.34 76.7792 144.24 45.7026 51. 35 110.3970 88.47 76.8005 145.44 52.1761 51. 87 122.2180 89. 96 77.0502 152.43 44.1212 52.39 136.4078 1093.63 77.1631 153.25 0.0000 52.97 145.4134 91.11 0.0000 323.87 58.2641 53.44 145.6249 92.59 77.4847 156.02 0.0000 54.07 140.6323 93.35 77.6093 158.56 0.0000 57.36 0.0000 94.56 59.6516 159.00 47.8068 57.53 137.6566 94.65 59.6628 162.33 44.7599 57.98 137. 8370 94.67 59.6651 162.66 0.0000 59.27 152.6341 94.87 59.6904 163.33 53.5698 59.32 152.6557 97.43 62.6152 165.86 46.0804 59.54 146.4992 98.43 57.8414 176.31 51.1948 60. 96 148.2875 98.44 57.8423 176.60 0.000'0 61.17 148.3752 99.53 59.9352 177.52 59.0799 62.93 147.0000 100 .11 55.0865 181.07 0.0000 63.29 147.1464 102.03 57. 2725 181.52 52.2956 63.58 147.2633 103.18 58.3923 184.41 42.7436 64.28 125.5188 103.37 58.4144 143.76 42.8161 66.73 134.8522 105.21 64.5859 193.51 57.6541 67.24 134.1216 105.31 64.5983 197.03 57.1442 125.81 117.8353 106.12 54.7457 198.01 50.3473 67.75 117.8560 106.47 65.7392 201.83 41.3855 69.67 117.5293 109.28 63.0875 203.43 42.6170 70.83 147.3474 111. 00 60.2774 205.31 38.0953 72.81 119.7028 111.76 0.0000 210.85 32.5356 72.87 119.7206 114. 06 59.6090 215.65 40.5076 74.66 121. 8031 116. 30 0.0000 222 .11 35.3133 74.82 121. 8500 116.74 53.8079 227.09 42.6121 74.97 121.8950 119.76 58.1816 227.38 39.0732 77 .11 122.5297 121.12 48.0894 228.16 0.0000 78.74 83.8829 121. 22 48.0976 228.18 31. 9974 79.69 90.3457 121.78 45. 0719 116.74 31. 9974 80.12 67.8274 122.06 43.0440 235.69 36.6413 80.19 0.0000 122.92 50.2935 235. 96 36.6520 80.57 76.7005 123.07 55.4399 238.63 38.3550 81. 00 83.0707 265.00 59.6094 238.98 0.0000 81. 07 84. 9724 125.81 49.5125 240.99 38.4512 81. 75 83.2150 127.23 53.7680 242.00 38.4922 83.79 69.6704 127.91 51. 0696 244.70 35.3848 84.00 65.9019 129.30 50.8430 252.40 0.0000 85.43 94.0861 131.20 38.8600 252.80 26.7618 86.55 76.4764 133.02 41. 7 609 254.15 0.0000 86.79 76.5167 133. 52 43.1882 256.23 26.0413 86.94 76.5430 136.00 56.6516 260.90 0.0000 Page 4138of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 43.0856 355.39 0.0000 584.27 16. 4596 264.80 43.0910 356.01 30.6746 595.83 0.0000 265.00 38.1739 364.49 0.0000 427.87 25.9389 268.22 40.7656 366.42 0.0000 602.52 0.0000 269.46 27.2100 372.51 18.9103 604. 72 18.7156 270.03 32.1747 375.05 24.3600 607.14 26.5469 271. 23 43.3623 377.52 22.5978 609.32 21. 8870 273.65 0.0000 356.01 25.4285 610.33 21. 8981 276.40 26.1468 388.16 20.9542 614.28 12.5386 277.37 27.4174 388.63 0.0000 618.01 15.7025 277.60 27.4235 391. 69 21.9219 620.36 14.6733 278.00 14. 9641 264.66 22.0645 621.93 12.5869 279.20 44.9429 401. 81 23.0026 630.19 0.0000 279.54 46.2060 402.40 23.9328 631.29 11.5922 279.70 46.2127 404.85 22.1304 633.25 8.4388 280.46 29.9978 410.95 21.1143 634.78 0.0000 283.69 31. 7602 413.71 30.6193 635.95 12.6753 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 30.9741 423. 72 0.0000 645.85 10.6144 285.90 0.0000 427.09 21.5382 657.76 12.8110 287.50 31. 8731 427.87 25.2977 657.90 0.0000 290.67 31.5460 433.94 27.2831 661. 66 16.0437 293.27 0.0000 439.40 19.8289 664.57 0.0000 351. 93 29.1431 453.88 16.2052 666.33 0.0000 295.96 29.1627 463.37 22.0590 666.50 0.0000 879.38 20.3350 468.07 25.9728 667. 71 0.0000 299.98 29.2680 473.00 0.0000 677.62 12.9321 300.09 29.2708 475.06 19.3237 685.70 0.0000 300 .13 29.2722 476.78 20.3117 695.00 0.0000 301.36 25.4822 477.60 22.2574 696.49 13.0459 302.85 33.1705 482.18 18.4391 696. 51 15.2202 256.23 25.5533 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 14.1383 306.78 31.5793 497.08 13.7106 697.49 14.1394 308.46 29.9165 505.52 29.5288 702.65 16.3531 311. 90 30.0062 507.63 0.0000 706.68 14.1992 316.51 29.6955 511. 00 33.5746 711.68 16.4203 319.41 0.0000 514.00 63.3125 720.70 0.0000 320.08 0.0000 514.00 63.3125 721. 93 0.0000 321.04 27. 9967 520.40 10.9226 722.78 13.2017 323.87 29.4498 520.69 0.0000 722. 91 13.2026 325.23 39.0216 522.65 0.0000 723. 31 14.8557 328.76 0.0000 527.90 0.0000 724 .19 14.8612 333.37 28.2874 528.26 13. 9647 727.33 14.3309 333.97 31.4458 529.59 13.9749 733.00 3.3154 334.37 28.8347 529.87 0.0000 735.93 16.5985 338.28 21. 9147 531.02 0.0000 333.97 21.0387 338.32 21. 9152 537.26 0.0000 739.50 0.0000 311. 90 21.9538 546.56 0.0000 747.24 11.1202 340.48 21.9538 552.55 17.1909 748.06 12.2367 340.55 0.0000 563.25 19.3263 752.31 12.2591 344.28 19.8193 569.33 24.4932 753.82 0.0000 345.93 27.3432 946.00 24.4951 756.73 14.5155 351.06 30. 1118 569.70 24.4980 756.80 14.5160 351. 93 30 .1325 583.19 16.4505 884.68 17.9206 Page 4139 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.1768 1274.44 12.8452 1620.50 2.1782 766.42 25.2274 1001.03 11. 0277 1621. 92 2.1790 766.84 26.9141 1002.74 12.8734 1678.03 0.0000 772. 60 0.0000 1004.73 7. 3611 1690.97 5.5310 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87
  • 0.0000 1764.49 0.0000 778.90 14.6525 1028.54 0.0000 1063.66 9.9000 783.70 0.0000 1037.84 8.3732 1771.35 3.6010 785.37 14.6922 1038.76 0.0000 1791.20 0.0000 792.07 6.7998 631.29 6.5313 1808.65 3.6287 794.95 6.8079 1048.07 0.0000 1810.72 0.0000 795.86 6.8105 1049.04 11. 2053 1836.06 0.9123 810.06 10.2751 1050.41 13.0789 810.29 6.8506 1063.66 15.9500 344.28 6.8511 1077.00 0.0000 810.76 10.2781 1077.34 7.5391 815.77 0.0000 1085.87 4.7247 1048.07 0.0000 1093.63 4.5469 832.01 10.3656 1099.45 12.3367 834.85 14.9895 1112. 07 12.3851 835. 71 12. 4572 1112. 84 13. 3412 836.80 0.0000 1115.54 7.6299 846.75 0.0000 1120.29 11.4617 846.77 1120. 55 11. 4631 856.80 0.0000 1221.41 11.4653 860.56 6.9880 1129. 67 6.7056 871.09 3.5082 1131.51 0.0000 873 .'19 8.7775 1147.95 0.0000 875.33 0.0000 1173.23 13.9764 879.38 10.5575 1177. 95 6.2203 880.51 11. 4424 1189.05 13. 6522 883.24 9.6918 1204.77 10.7758 884.68 6.1709 1221.41 10.8275 889.28 7.9478 1231.02 11. 2807 894.76 9.7338 1235.36 0.0000 898.04 10.6318 1238.28 12.8580 900. 72 8.8687 1260.41 0.0000 903.28 15.0908 1271.87 15.9756 911.20 9.7932 1274.44 12.9889 912.08 9. 7965 1274.54 12.9897 923.98 0.0000 1291.59 13.0508 926.50 7.1624 1298.22 0.0000 929 .11 7.1689 1312 .11 0.0000 937.49 8.6288 1332.49 10.1501 944.13 0.0000 1362.66 0.0000 946.00 9.9174 1365.19 4.0952 949.00 9.0253 1368.63 0.0000 667.71 0.0000 1384.29 4 .1157 962. 31 4.3526 1408.01 6.2109 964.08 10.1623 1457.56 0.0000 966 .17 14.5283 1460.82 3.1469 911.20 14.5425 1489.16 1. 0562 968. 97 14.5425 1505.03 5.3015 983.53 0.0000 1584.12 8. 6411 984.45 0.0000 1596.21 0.0000 Page 4140of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:09:08.68 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM43.CNF;l51 Background date : Z-OCT-2016 11:02:23. Sample date 2-DEC-2015 14:51:00. Acquisition date : 3-0CT-2016 07:07:21. Sample ID G405235054 Sample quantity : 1.46461E+02 GRAM Detector name GAM43 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.68 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID : 1596252 Detector SN# : Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 1 0 5 5 0 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4141of5809 Energy 59.35 74.65 76.99 80.99 86.94 89.52 92.80* 114.29 129.76 143.95* 185.66* 208.40 219.04 238.49* 241.58 295.04* 320.25 338.38 351.85* 382.39 409.10 441.72 464°.44 511. 23* 566.62 582.95* 609.22* 722. 93 726.85 767.75 774.19 833.02 884.64 888.09 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 33 136 191 35 50 43 102 31 28 13 107 52 41 425 122 142 25 86 240 38 36 21 19 16 7 117 150 12 44 27 19 6 15 4 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 103 132 110 89 103 64 165 107 109 116 102 122 128 42 70 50 45 70 49 84 21 18 55 83 30 21 44 7 9 13 11 9 5 4 1. 50 1. 23 1.12 1. 25 1. 04 1. 06 1. 76 2.27 1. 28 1. 38 1. 54 0.68 6.21 1. 03 1. 68 1. 24 0.65 1. 26 1.19 7.31 3.19 1.10 3.37 1. 42 1. 47 1. 55 1. 71 1. 22 2.06 1. 88 1. 77 0.72 0.85 0.58 118. 49 149.08 153.77 161.77 173.69 178.85 185.41 228.39 259.36 287.74 371.19 416.67 437.95 476.87 483.05 590.00 640.43 676. 71 703.65 764.75 818.17 883.43 928.88 1022.49 1133. 29 1165. 95 1218.50 1445. 96 1453.81 1535.63 1548.50 1666.18 1769.43 1776.34 115 141 141 141 171 177 177 225 253 283 365 412 429 469 469 585 634 670 698 748 813 880 920 1014 1126 1161 1210 1443 1449 1530 1543 1660 1765 1773 8 9.17E-03 55.9 24 3.77E-02 15.8 3.07E+OO 24 5.30E-02 12.2 24 9.67E-03 52.0 6 1.39E-02 35.0 16 1.20E-02 29.9 1.03E+OO 16 2.83E-02 27.3 9 8.52E-03 63.6 9 7.80E-03 70.3 9 3.63E-03153.0 12 2.96E-02 21.9 11 1.44E-02 43.5 15 l.12E-02 62.8 20 1.18E-01 5.5 1.31E+OO 20 3.40E-02 17.7 9 3.93E-02 12.4 12 7.0lE-03 56.8 14 2.40E-02 23.2 11 6.66E-02 8.7 21 1.05E-02 62.6 10 l.OOE-02 29.5 8 5. 77E-03 41. 7 13 5.18E-03 85.3 14 4.47E-03134.7 10 l.94E-03151.2 13 3.25E-02 12.4 19 4.16E-02 13.4 6 3.23E-03 50.7 11 1.23E-02 19.6 10 7.62E-03 30.8 10 5.37E-03 40.5 8 l.58E-03103.8 9 4.03E-03 40.8 7 l.OlE-03103.7 Peak Search Report (continued) Page : 2 Sample ID : G405235054 Acquisition date 3-0CT-2016 07:07:21 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 890.84 9 1 0.95 1781.84 1779 6 2.42E-03 40.2 36 0 902.44 10 15 4.10 1805.04 1797 12 2.75E-03 84.5 37 0 910.91 98. 4 1.-79 1821.99 1814 17 2. 71E-02 11. 2 38 0 922.79 19 17 4 .11 1845.74 1836 17 5.41E-03 53.4 39 0 969. 69 39 41 0.72 1939.57 1929 17 1. 09E-02 42.6 40 0 1042.99 8 8 1.24 2086.17 2080 10 2.26E-03 78.8 41 0 1120.95 39 26 1.27 2242 .11 2235 20 1. 08E-02 35.4 42 0 1215.78 19 6 3.78 2431.79 2425 13 5.34E-03 35.3 43 0 1314.44 4 4 0.94 2629.13 2623 8 1.llE-03100.0 44 0 1341.47 10 3 0. 96 2683.18 2676 11 2.79E-03 45.2 45 0 1353.06 6 2 0.75 2706.35 2702 8 l.63E-03 59.0 46 0 1460.66* 336 0 1. 99 2921.57 2914 18 9.33E-02 5.5 47 0 1764.57* 29 0 2.08 3529.38 3522 14 8.lOE-03 19.6 48 0 1847.26 12 0 2.31 3694.75 3690 10 3.33E-03 28.9 Flag: "*" = Peak area was modified by background subtraction Page 4142of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:09:10 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 14:51:00 G405235054 Acquisition date : Sample quantity Sample geDmetry Detector geometry: 3-0CT-2016 07:07:21 146.46 GRAM Sample. type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA43 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 U-235 143.76 PB-214 87.09 PB-214 87.09 PB-214 87:09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 4143 of 5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 CE-141 145.44 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.68 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235054 Acquisition date 3-0CT-2016 07:07:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40

  • 1460. 82 10.66* 1.00lE+OO l.552E+Ol 1 *. 552E+Ol 11. 02 OK SC-46 889.28 99.98* 1. 541E+OO l.220E-02 1.530E-01 207.36 OK 1120.55 99.99 1.265E+OO l.561E-01 1.957E+OO 70.74 OK CD-109 88.03 3.70* 4.275E+OO 9.991E-01 l.581E+OO 143.54 OK SN-126 64.28 9.60 1.983E+OO Line Not Found Absent 86.94 8.90 4.275E+OO 4.153E-01 4.153E-01 143.54 OK 87.57 37.00* 4.275E+OO 9.991E-02 9.991E-02 143.54 OK TL-208 277.37 6.60 4.205E+OO Line Not Found Absent 583.19 85.00* 2.199E+00 3.376E-01 3.376E-01 24.76 OK 860.56 12.50 1.582E+OO Line Not Found Absent BI-211 72. 87 1. 23 2.941E+OO Line Not Found Absent 351. 06 12.92* 3.426E+OO 1.521E-02 1. 521E-026072 .10 OK PB-212 74.82 10.28 3.129E+OO 2.088E+OO 2.088E+OO 41. 68 OK 77 .11 17.10 3.370E+OO 2.127E+OO 2.127E+00 24.49 OK 238.63 43.60* 4.741E+OO l.202E+OO 1.202E+OO 11. 04 OK 300.09 3.30 3.935E+OO Line Not Found Absent BI-214 609.32 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26.88 OK 1120.29 14.92 l.265E+OO 1.046E+OO l.046E+00 70.74 OK 1764.49 15.30 '8.362E-01 1.103E+OO 1.103E+OO 39.19 OK PB-214 74.82 5.80 3.147E+OO Line Not Found <<INT Reject 77 .11 9.70 3.370E+00 3.749E+OO 3.750E+OO 24.49 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 4.688E+OO Line Not Found <<INT Reject 295.22 18.42 3.992E+OO 1.106E+OO 1.106E+OO 24.81 OK 351. 93 35.60* 3.426E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.118E+00 8.347E-01 8.350E-01 26. 88 OK 1120.29 14.92 1.265E+OO 1.046E+OO 1.046E+OO 70.74 OK 1764.49 15.30 8.362E-01 1.103E+OO 1.103E+OO 39.19 OK RA-224 240.99 4.10* 4.695E+OO 1. 7 61E+OO 1. 761E+OO 79.67 OK RA-226 609.32 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26.88 OK 1120. 29 14.92 1. 2 65E+OO l.046E+OO 1.046E+OO 70.74 OK 1764.49 15.30 8.362E-01 1.103E+00 1.103E+OO 39.19 OK AC-228 105.21 1.10 5. 396E+OO Line Not Found Absent 338.32 11. 27 3.546E+OO 1.225E+OO 1.225E+OO 46.39 OK 794.95 4.25 1.691E+OO Line Not Found Absent 835. 71 1. 61 1. 621E+OO Line Not Found Absent 911. 20 25.80* 1.508E+OO 1.296E+OO 1.296E+OO 22.47 OK 968.97 15.80 l.431E+OO 8.914E-01 8.914E-01 85.15 OK RA-228 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.546E+OO 1.225E+OO 1.225E+OO 46.39 OK 794.95 4.25 1.691E+OO Line Not Found Absent 835.71 1. 61 1. 621E+OO Line Not Found Absent 911.20 25.80* 1.508E+OO 1.296E+OO l.296E+00 22.47 OK 968. 97 15.80 1.431E+OO 8.914E-01 8.914E-01 85.15 OK TH-228 74.82 10.28 3.129E+OO 2.088E+OO 2.088E+OO 41. 68 OK 77 .11 17.10 3.370E+OO 2.127E+OO 2.127E+OO 24.49 OK 238.63 43.60* 4.741E+OO 1.202E+OO 1.202E+OO 11. 04 OK 300.09 3.30 3.935E+OO Line Not Found Absent TH-230 609.32 45.49* 2 .118E+00 8.347E-01 8.347E-01 26.88 OK Page 4144of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235054 Acquisition date 3-0CT-2016 07:07:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1120.29 14.92 1. 265!HOO l.046E+OO 1.046E+OO 70.74 OK 1764.49 15.30 8.362E-01 1.103E+OO 1.103E+OO 39.19 OK TH-232 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11.27 3.546E+OO 1.225E+OO 1.225E+OO 46.39 OK 835. 71 1. 61 l.621E+OO Line Not Found Absent 911.20 25.80* 1.508E+OO 1.296E+OO 1.296E+OO 22.47 OK 968.97 15.80 1. 431E+OO 8.914E-01 8.914E-01 85.15 OK U-234 609.32 45.49* 2 .118E+OO 8.347E-01 8.347E-01 26.88 OK 1120.29 14.92 1.265E+OO 1.046E+OO l.046E+OO 70.74 OK 1764.49 15.30 8.362E-01 l.103E+OO 1.103E+OO 39.19 OK U-235 89. 96 3.47 4.476E+OO 1.770E+OO 1. 770E+OO 59.83 OK 93.35 5.60 4.711E+OO 2.441E+OO 2.441E+OO 54.61 OK 143.76 10.96* 6.023E+OO 1.209E-01 1.209E-01 306.07 OK 163.33 5.08 5.876E+OO Line Not Found Absent 185.72 57.20 5.570E+OO l.999E-01 1.999E-01 43. 72 OK 205.31 5.01 5.260E+OO Line Not Found Absent AM-241 59.54 35.90* 1.428E+OO 4.218E-01 4.223E-01 111.73 OK AM-243 43.53 5.90 1.216E-01 Line Not Found Absent 74.66 67.20* 3.129E+OO 3.195E-01 3 '.195E-01 41. 68 OK ANH-511 511. 00 100.00* 2.464E+OO 3.567E-02 3.567E-02 269.31 OK Flag: "*" = Keyline Page4145 of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:09:11.62 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l *
  • Acquisition date 3-0CT-2016 07:07:21 Sensitivity : 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:51:00 Analyst initials: MXRl *
  • Sample ID G405235054 Sample Quantity 1.4646E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.552E+Ol 1.677E+OO SC-46 1.530E-01 3.108E-01 CD-109 1.581E+OO 2.224E+OO SN-126 9. 991E-02 1.405E-01 TL-208 3.376E-01 8.191E-02 BI-211 1.521E-02 9.053E-01 PB-212 1.202E+OO 1.300E-01 BI-214 8.350E-01 2.200E-01 PB-214 1.112E+OO l.888E-01 RN-222 8.350E-01 2.200E-01 RA-224 1. 761E+OO 1.375E+OO RA-226 8.350E-01 2.200E-01 AC-228 1.296E+OO 2.854E-01 RA-228 1.296E+OO 2.854E-01 TH-228 l.202E+OO l.300E-01 TH-230 8.347E-01 2.199E-01 TH-232 1. 296E+OO 2.854E-01 U-234 8.347E-01 2.199E-01 U-235 1. 209E-01 3.628E-01 AM-241 4.223E-01 4.624E-01 AM-243 3.195E-01 l.305E-01 ANH-511 3.567E-02 9.414E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 Page 4146 of 5809 Key-Line Activity (pCi/GRAM -4.0lOE+OO 1. 351E-02 O.OOOE+OO -7.073E-04 0.000E+OO O.OOOE+OO -5.347E-02 5.346E-02 K.L. Cnt Uncert ( 1. 96-sigma) 1.522E+Ol 4.553E-02 1. 960E+41 2.539E-02 1.636E+04 9.109E+02 8.349E-02 4.945E-01 MDA (pCi/GRAM 5.157E-01 l.152E-01 2.332E+OO 1.485E-01 7. 719E-02 3.806E-01 9. 611E-02 1. 211E-01 3.461E-01 1. 211E-01 1.031E+OO 1. 211E-01 2.273E-01 2.273E-01 9. 611E-02 1.210E-01 2.273E-01 l.210E-01 3.434E-01 4.211E-01 l.225E-01 6.666E-02 MDA (pCi/GRAM 2.731E+Ol 9.890E-02 O.OOOE+OO 5.852E-02 O.OOOE+OO O.OOOE+OO l.217E-Ol 9. 964E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 1.423E-02 5.200E-02 9.678E-02 NOT IDENT. C0-58 -3.193E-01 6.514E-01 l.179E+OO NOT IDENT. FE-59 -6.345E-01 9.474E+OO 1. 774E+Ol NOT IDENT. C0-60 9.919E-03 3. 967E-02 8.633E-02 NOT IDENT. ZN-65 -l.844E-01 2. 496E-01 3.338E-01 NOT IDENT. GE-68 1. 968E+OO 2.654E+OO 5.774E+OO NOT IDENT. AS-73 5. 872E+OO 1.930E+Ol 3.759E+Ol NOT IDENT. AS-74 O.OOOE+OO 6.773E+03 O.OOOE+OO SHORT HLIF SE-75 -1 .. 202E-01 2.122E-01 3.855E-01 I DENT. BR-77 O.OOOE+OO 1.288E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 1. 04 7E+03 O.OOOE+OO SHORT HLIF RB-83 4.129E-01 7.755E-01 1.622E+OO NOT IDENT. KR-85 6.607E+OO 9.456E+OO 1.703E+Ol NOT IDENT. SR-85 7.420E-01 1.062E+OO l.914E+OO NOT IDENT. RB-86 O.OOOE+OO 3.808E+04 O.OOOE+OO SHORT HLIF Y-88 l.067E-01 2.734E-01 6.370E-01 NOT IDENT. Y-91 -1.996E+02 5.378E+02 l.028E+03 NOT IDENT. NB-94 4.359E-02 3.490E-02 7.821E-02 NOT IDENT. NB-95 3.122E-01 l.190E+OO 2 .113E+OO NOT I'DENT. NB-95M -7. 960E-01 2.917E+OO 4.860E+OO NOT IDENT. ZR-95 -5.800E-01 l.550E+OO 2.888E+OO FAIL ABUN NB-97 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 7.257E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF RH-101 -2.173E-02 4.177E-02 6. 511E-02 NOT IDENT. RH-102 3.239E-02 6.329E-02 1.334E-01 FAIL ABUN RU-103 8.324E-01 6.924E+OO 1.314E+Ol FAIL ABUN RH-106 3.598E-02 5.063E-01 1.020E+OO NOT IDENT. RU-106 3.598E-02 5.063E-01 1.020E+OO NOT IDENT. AG-108M 1.463E-03 2.826E-02 5.371E-02 FAIL ABUN AG-llOM 1.566E-01 l.253E-01 2.549E-01 FAIL ABUN SN-113 4.918E-02 2.585E-01 4. 966E-01 NOT IDENT. CD-115 O.OOOE+OO 2.199E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.400E+05 0.000E+OO SHORT HLIF TE-123M 2.600E-02 l.429E-01 2.836E-01 NOT IDENT. SB-124 9.314E-03 2.371E+OO 5.094E+OO FAIL ABUN SB-125 l.178E-01 1.121E-01 2.364E-01 FAIL ABUN TE-125M -6.842E+Ol 3.182E+02 5.709E+02 NOT IDENT. I-126 0.000E+OO l.380E+06 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 2.031E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.976E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 7.918E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF TE-132 0.000E+OO l.444E+27 O.OOOE+OO SHORT HLIF BA-133 -1. 789E-02 4. 913E-02 7. 821E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 3.433E-02 5.312E-02 1.134E-01 NOT IDENT. CS-135 -2.465E-02 l.432E-01 2. 696E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 5.068E+05 O.OOOE+OO SHORT HLIF BA-137M -4.439E-03 4.073E-02 7.821E-02 NOT IDENT. CS-137 -4.689E-03 4.303E-02 8.262E-02 NOT IDENT. CE-139 5.433E-02 l.184E-01 2.388E-01 NOT IDENT. BA-140 0.000E+OO 1.973E+06 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 6.045E+05 O.OOOE+OO SHORT HLIF CE-141 1.859E+Ol 5.575E+Ol 5.063E+Ol FAIL ABUN CE-143 O.OOOE+OO 6.699E+40 O.OOOE+OO SHORT HLIF CE-144 -8.299E-02 3.789E-01 7.097E-01 FAIL ABUN PM-144 2.420E-02 5.510E-02 1.158E-01 NOT IDENT. PR-144 2.108E+OO 4.801E+OO 1.009E+Ol NOT IDENT. PM-146 4.022E-02 4.464E-02 9.503E-02 NOT IDENT. ND-147 O.OOOE+OO 5.542E+07 O.OOOE+OO SHORT HLIF PM-147 6.992E+02 8.977E+02 1. 744E+03 NOT IDENT. PM-149 O.OOOE+OO '1.102E+41 0.000E+OO SHORT HLIF EU-150 3.134E-04 2. 641E-02 4.519E-02 FAIL ABUN EU-152 -5.728E-02 1.164E-01 l.821E-01 NOT IDENT. GD-153 -l.661E-01 2.432E-01 3.825E-01 NOT IDENT. EU-154 3.504E-02 l .118E-01 2.432E-01 FAIL ABUN EU-155 1.012E-01 1.353E-01 2.607E-01 FAIL ABUN TB-160 5. 072E-01 2.464E+OO 4.417E+OO FAIL ABUN H0-166M 3.067E-02 6.914E-02 1.410E-01 FAIL ABUN TM-171 -3.926E+Ol 4.874E+Ol 8.606E+Ol NOT IDENT. HF-172 6.398E-02 2.869E-01 4.864E-01 FAIL ABUN LU-172 -1.178E-01 9.316E-02 l.330E-01 FAIL ABUN LU-176 7.663E-03 2.368E-02 4.686E-02 FAIL ABUN HF-181 -1.270E-01 5.104E+OO 9.522E+OO NOT IDENT. Page 4147 of 5809 TA-182 6.423E-01 l.097E+OO 2.182E+OO FAIL ABUN RE-183 9. llOE+OO 9.974E+OO 1.0lOE+Ol FAIL ABUN RE-184 3.519E+Ol 5.828E+Ol 8.691E+Ol FAIL ABUN W-188 2.453E+Ol 1.430E+02 2.479E+02 NOT IDENT. IR-192 -4.296E-01 6.059E-01 9.246E-01 FAIL ABUN HG-203 -2.098E+OO 2.797E+OO 4.952E+OO NOT IDENT. BI-207 -2.219E-02 5.014E-02 8. 911E-02 FAIL ABUN PB-210 2.532E+OO 1.049E+Ol 2. 072E+Ol NOT IDENT. PB-211 -1.013E+OO 7.892E-01 1.006E+OO FAIL ABUN BI-212 0. ODOE+OO 7.412E-01 1.514E+OO F.AIL ABUN RN-219 2.876E-01 3.762E-01 7.780E-01 NOT IDENT. RA-223 -1.866E-01 6.284E-01 1.025E+OO FAIL ABUN AC-227 -5.008E-02 2.225E-01 *4 .193E-01 FAIL ABUN TH-227 -5.008E-02 2.225E-01 4.193E-01 FAIL ABUN TH-229 l.847E-01 4.558E-01 9 .137E-01 FAIL ABUN PA-231 3.344E-01 4.556E-01 9.238E-01 NOT IDENT. TH-231 -1. 866E-01 6.284E-01 1. 025E+OO FAIL ABUN PA-233 -1.938E-02 6.151E-02 l.132E-01 NOT IDENT. PA-234 -1.068E-01 3.195E-01 5.832E-01 FAIL ABUN PA-234M -3.132E+OO 4.935E+OO 8.429E+OO FAIL ABUN TH-234 1.355E+OO 1. 928E+OO 3.641E+OO FAIL ABUN NP-237 -l.938E-02 6.151E-02 1.132E-01 NOT IDENT. NP-238 O.OOOE+OO 7.173E+40 O.OOOE+OO SHORT HLIF U-238 1.355E+OO 1.928E+OO 3.641E+00 FAIL ABUN NP-239 -1. 463E-01 2.923E-01 4.606E-01 NOT IDENT. PU-239 4.577E+02 6.308E+02 6.731E+02 FAIL ABUN CM-243 8.128E-03 1.140E-01 2.102E-01 NOT IDENT. BK-247 -3.669E-02 6.994E-02 l.277E-01 NOT IDENT. CM-247 2.675E-02 3.317E-02 6.940E-02 NOT IDENT. CF-249 1. 211E-02 4 .119E-02 7.985E-02 NOT IDENT. CF-251 -3.552E-02 1.151E-01 2.197E-01 NOT IDENT. Page 4148of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:09:09.44 Nuclide Line Activity Report .* Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 323 10.66* 1. OOlE+OO l.552E+Ol 1.552E+Ol 11. 02 SC-46 889.28 4 99.98* 1. 541E+OO l.220E-02 l.530E-01 207.36 1120.55 39 99.99 1. 265E+OO 1.561E-01 1.957E+OO 70.74 CD-109 88.03 62 3.70* 4.275E+OO 2.018E+OO 3.195E+OO 69.94 SN-126 64.28 ------9.60 1.983E+OO ------Line Not Found ------86.94 62 8.90 4.275E+OO 8.390E-01 8.390E-01 69.94 87.57 62 37.00* 4.275E+OO 2.018E-01 2.018E-01 69.94 CE-141 145.44 16 48.29* 6.023E+OO 2.745E-02 1.859E+Ol 306.07 TL-208 277.37 ------6.60 4.205E+OO ------Line Not Found ------583.19 123 85.00* 2.199E+OO 3.376E-01 3.376E-Oi 24.76 860.56 ------12.50 1.582E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 2.941E+OO ------Line Not Found ------351. 06 264 12.92* 3.426E+OO 3.062E+OO 3.062E+OO 17.33 PB-212 74.82 170 10.28 3.129E+OO 2. 712E+OO 2.712E+OO 31. 58 77 .11 239 17.10 3.370E+OO 2.127E+OO 2.127E+OO 24.49 238.63' 485 43.60* 4.741E+OO 1.202E+OO 1:202E+OO 11. 04 300.09 ------3.30 3.935E+OO ------Line Not Found ------BI-214 609.32 157 45.49* 2.118E+OO 8.347E-01 8.350E-01 26. 88 1120.29 39 14.92 1.265E+OO 1.046E+OO 1.046E+OO 70.74 1764.49 28 15.30 8.362E-01 1.103E+OO 1.103E+OO 39.19 PB-214 74.82 170 5.80 3.129E+OO 4.807E+OO 4.809E+OO 31. 58 77 .11 239 9.70 3.370E+OO 3.749E+OO 3.750E+OO 24.49 87.09 62 3.41 4.275E+OO 2.190E+OO 2.191E+OO 69.94 242.00 140 7.25 4.695E+OO 2 .101E+OO 2.102E+OO 35.42 295.22 159 18.42 3.992E+OO 1.106E+OO l.106E+00 24.81 351.93 264 35.60* 3.426E+OO 1. lllE+OO 1.112E+OO 17.33 RN-222 609.32 157 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26.88 1120.29 39 14.92 1.265E+OO 1.046E+OO 1.046E+OO 70.74 1764.49 28 15.30 8.362E-01 1.103E+OO 1.103E+OO 39.19 RA-224 240.99 140 4.10* 4.695E+OO 3. 716E+OO 3.716E+OO 35.42 RA-226 609.32 157 45.49* 2 .118E+OO 8.347E-01 8.350E-01 26. 88 1120.29 39 14.92 1. 265E+OO 1.046E+OO 1. 046E+OO 70.74 1764.49 28 15.30 8.362E-01 1.103E+OO 1.103E+OO 39.19 AC-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 96 11. 27 3.546E+OO 1.225E+OO 1. 225E+OO 46.39 794.95 ------4.25 1. 691E+OO ------Line Not Found ------835.71 ------1. 61 1.621E+OO ------Line Not Found ------911.20 98 25.80* 1.508E+OO l.296E+OO 1. 296E+OO 22.47 968. 97 39 15.80 1.431E+OO 8.914E-01 8.914E-01 85.15 RA-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 96 11. 27 3.546E+OO 1.225E+OO 1.225E+OO 46.39 794.95 ------4.25 l.691E+00 ------Line Not Found ------835.71 ------1. 61 1. 621E+OO ------Line Not Found ------911. 20 98 25.80* 1.508E+OO l.296E+OO l.296E+OO 22.47 968.97 39 15.80 1. 431E+OO 8.914E-01 8.914E-01 85.15 TH-228 74.82 170 10.28 3.129E+OO 2. 712E+OO 2.712E+OO 31. 58 77 .11 239 17.10 3.370E+OO 2.127E+OO 2.127E+OO 24.49 Page 4149 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235054 Acquisition date 3-0CT-2016 07:07:21 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 485 43.60* 4.741E+C!O l.202E+OO 1.202E+OO 11. 04 300.09 ------3.30 3.935E+OO ------Line Not Found ------TH-230 609.32 157 45.49* 2 .118E+OO 8.347E-01 8.347E-01 26.88 1120.29 39 14.92 l.265E+OO 1.046E+OO 1. 046E+OO 70.74 1764.49 28 15.30 8.362E-01 1.103E+OO 1.103E+00 39.19 TH-232 105.21 ------1.10 5.396E+OO ------Line Not Found ------338.32 96 11. 27 3.546E+OO 1.225E+OO 1.225E+00 46.39 835.71 ------1. 61 1.621E+OO ------Line Not Found ------911. 20 98 25.80* 1.508E+OO 1. 296E+OO 1. 296E+OO 22.47 968. 97 39 15.80 1.431E+OO 8.914E-01 8.914E-01 85.15 U-234 609.32 157 45.49* 2 .118E+OO 8.347E-01 8.347E-01 26.88 1120.29 39 14.92 1.265E+OO 1.046E+OO 1.046E+OO 70.74 1764.49 28 15.30 8.362E-01 1.103E+OO 1.103E+00 39.19 U-235 89. 96 54 3.47 4.476E+OO 1. 770E+OO 1.770E+OO 59.83 93.35 126 5.60 4. 711E+OO 2.441E+OO 2.441E+OO 54.61 143.76 16 10. 96* 6.023E+OO l.209E-01 1.209E-01 306.07 163.33 ------5.08 5.876E+OO ------Line Not Found ------185.72 124 57.20 5.570E+OO 1.999E-01 1.999E-01 43. 72 205.31 ------5.01 5.260E+OO ------Line Not Found ------AM-241 59.54 42 35.90* 1.428E+OO 4.218E-01 4.223E-01 111. 73 AM-243 43.53 ------5.90 1.216E-01 ------Line Not Found ------74.66 170 67.20* 3.129E+OO 4.149E-01 4.149E-01 31. 58 ANH-511 511. 00 17 100.00* 2.464E+OO 3.567E-02 3.567E-02 269.31 Flag: "*" Key line Page 4150of5809 Page : 3 Sununary of Nuclide Activity Sample ID : G405235054 Acquisition date 3-0CT-2016 07:07:21 Total number of lines in spectrum 48 Number of unidentified lines 13 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 SC-46 CD-109 SN-126 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-241 AM-243 ANH-511 Hlife 1. 25E+09Y 83.79D 461. 40D 2.30E+05Y 32.51D 1. 41E+l0Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600. OOY l.41E+l0Y 1600. OOY 1. 41E+l0Y l.41E+l0Y l.41E+l0Y 7.54E+04Y l.41E+l0Y 2.45E+05Y 7.04E+08Y 432.60Y 7370.00Y l.OOE+09Y Decay 1. 00 12.5 1. 58 1. 00 677. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity ( Uncorrected pCi/GRAM l.552E+Ol l.220E-02 2.018E+OO 2.018E-01 2.745E-02 3.376E-01 3.062E+OO l.202E+OO 8.347E-01 l. lllE+OO 8.347E-01 3.716E+OO 8.347E-01 l.296E+OO 1. 296E+OO l.202E+OO 8.347E-01 l.296E+OO 8.347E-01 l.209E-01 4.218E-01 4.149E-01 3.567E-02 3.747E+Ol 3.747E+Ol Decay Corr pCi/GRAM 1.552E+Ol l.530E-Ol 3.195E+OO 2.018E-01 1.859E+Ol 3.376E-01 3.062E+OO l.202E+OO 8.350E-01 l .112E+OO 8.350E-01 3. 716E+OO 8.350E-01 l.296E+OO l.296E+OO l.202E+OO 8.347E-01 l.296E+OO 8.347E-01 l.209E-01 4.223E-01 4.149E-01 3.567E-02 5.735E+Ol 5.735E+Ol 72.92% Decay Corr 2-Sigma Error 0 .171E+Ol 3. l 72E-01 2.234E+OO l.412E-01 5.689E+Ol 0.836E-01 0.531E+OO 0.133E+OO 2.245E-01 0.193E+OO 2.245E-01 l.316E+OO 2.245E-01 0.291E+OO 0.291E+OO 0.133E+OO 2.244E-01 0.291E+OO 2.244E-01 3.702E-01 4.719E-01 l.310E-01 9.606E-02 "M" Manually accepted

  • 2-Sigma %Error 11. 02 207.36 69.94 69.94 306.07 24.76 17.33 11. 04 26.88 17.33 26.88 35.42 26.88 22.47 22.47 11. 04 26. 88 22.47 26. 88 306.07 111.73 31. 58 269.31 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4151of5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235054 Acquisition date : 3-0CT-2016 07:07:21 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 1 80.99 43 111 1. 25 161.77 141 24 9.67E-03 **** 3.76E+OO T 0 114.29 37 130 2.27 228.39 225 9 8.52E-:-03 **** 5.72E+OO T 0 129.76 34 131 1. 28 259.36 253 9 7.80E-03 **** 5.99E+OO T 0 208.40 60 141 .0.68 416.67 412 11 l.44E-02 87.0 5. 21Et00 0 219.04 47 147 6.21 437.95 429 15 l.12E-02 **** 5.04E+OO 0 320.25 28 50 0.65 640.43 634 12 7.0lE-03 **** 3.72E+OO T 0 382.39 41 92 7.31 764.75 748 21 1. 05E-02 **** 3.18E+OO T 0 409.10 39 23 3.19 818.17 813 10 1. OOE-02 58.9 3.00E+OO 0 441. 72 22 20 1.10 883.43 880 8 5.77E-03 83.4 2.80E+OO 0 464.44 20 60 3.37 928.88 920 13 5.18E-03 **** 2.68E+OO T 0 566.62 7 32 1. 47 1133.29 1126 10 l.94E-03 **** 2.25E+OO 0 722.93 12 8 1. 22 1445.96 1443 6 3.23E-03 **** 1.83E+OO T 0 726.85 46 9 2.06 1453.81 1449 11 l.23E-02 39.3 1.82E+OO T 0 767.75 28 13 1. 88 1535.63 1530 10 7.62E-03 61. 5 1. 74E+OO T 0 774.19 20 11 1. 77 1548.50 1543 10 5.37E-03 81. 0 1.73E+00 0 833.02 6 9 0. 72 1666.18 1660 8 l.58E-03 **** 1. 63E+OO T 0 884.64 15 6 0.85 1769.43 1765 9 4.03E-03 81. 7 l.55E+OO T 0 890.84 9 1 0.95 1781. 84 1779 6 2.42E-03 80.5 1.54E+OO 0 902.44 10 15 4.10 1805.04 1797 12 2.75E-03 **** 1.52E+OO T 0 922.79 20 17 4 .11 1845.74 1836 17 5.41E-03 **** 1.49E+OO T 0 1042.99 8 8 1. 24 2086.17 2080 10 2.26E-03 **** 1. 35E+OO 0 1215.78 19 6 3.78 2431. 79 2425' 13 5.34E-03 70.6 1.18E+OO 0 1314.44 4 4 0.94 2629.13 2623 8 l. llE-03 **** 1.lOE+OO 0 1341.47 10 3 0. 96 2683.18 2676 11 2.79E-03 90.3 1.08E+OO 0 1353. 06 6 2 0.75 2706.35 2702 8 1.63E-03 **** 1.07E+OO 0 1847.26 11 0 2.31 3694.75 3690 10 3.33E-03 57.7 7.99E-01 Flags: "T" = Tentatively associated Page 4152 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:09:23.50 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l *
  • Acquisition date 3-0CT-2016 07:07:21 Sensitivity 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:51:00 Nuclide Library : SOLID *
  • Sample ID G405235054 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.4646E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA. GAMMA] EFF GAM43 CAN. CNF; 7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-241 AM-243 ANH-511 Le (pCi/GRAM 1.925E-01 0.000E+OO 1.094E+OO 6. 965E-02 3.480E-02 1.741E-01 4.456E-02 5.316E-02 1. 672E-01 5.316E-02 4.778E-01 5.316E-02 9.553E-02 9.553E-02 4.456E-02 5.314E-02 9.553E-02 5.314E-02 1. 606E-01 1. 962E-01 5. 772E-02 3.044E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 V-48 CR-51 MN-54 C0-56 MN-56 Page 4153 of 5809 Le (pCi/GRAM 1.225E+Ol 4.173E-02 O.OOOE+OO 2.073E-02 O.OOOE+OO O.OOOE+OO 5.226E-02 4.298E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4154 of 5809 4.522E-02 5.047E-01 7.741E+OO 3.600E-02 l.409E-01 2.523E+OO 1. 755E+Ol O.OOOE+OO 1. 763E-01 O.OOOE+OO O.OOOE+OO 7.349E-01 7.810E+OO 8.775E-01 O.OOOE+OO 2.551E-01 4.295E+02 3.533E-02 9.455E-01 2.263E+OO 1.242E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 3.040E-02 5. 951E-02 5.885E+OO 4.49.3E-01 4.493E-01 2.408E-02 1.128E-01 2.260E-01 O.OOOE+OO O:OOOE+OO 1. 331E-01 1.981E+OO 1. 079E-01 2.658E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.550E-02 O.OOOE+OO 5.025E-02 1.244E-01 O.OOOE+OO O.OOOE+OO 3.504E-02 3.701E-02 1.122E-01 O.OOOE+OO O.OOOE+OO 2.361E+Ol O.OOOE+OO 3.318E-01 5 .116E-02 4.458E+OO 4.306E-02 O.OOOE+OO 8.176E+02 O.OOOE+OO 2.047E-02 8. 296E-02 l.790E-01 l.028E-01 l.231E-01 1.926E+OO 6.344E-02 4.00lE+Ol 2.283E-01 5.476E-02 2.144E-02 4.254E+OO 9.505E-01 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL.ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-2.19 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4155 of 5809 4.697E+OO 3.862E+Ol l.147E+02 4.215E-01 2.276E+OO 3.732E-02 9.681E+OO 4.405E-01 6. 991E-01 3.534E-01 4.633E-01 1.927E-01 1.927E-01 4.266E-01 4.276E-01 4.633E-01 5.170E-02 2.515E-01 3.614E+00 1.713E+00 5.170E-02 O.OOOE+OO 1. 713E+OO 2.143E-01 3.172E+02 9.835E-02 5.832E-02 3.143E-02 3.646E-02 1.025E-01 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT .IDENT.
  • FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:09:28.85 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235054.CNF;l * *Acquisition date 3-0CT-2016 07:07:21 Sensitivity : 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.68 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:51:00 Nuclide Library : SOLID *
  • Sample ID G405235054 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity 1.4646E+02 GRAM *
  • Quantity Err(%) 1.3656E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.552E+Ol 1.863E+OO 1.863E+OO SC-46 1.530E-01 3.109E-01 3.109E-01 CD-109 1.581E+OO 2.237E+OO 2.237E+OO SN-126 9.991E-02 1. 412E-01 l.412E-01 TL-208 3.376E-01 8.317E-02 8.317E-02 BI-211 1.521E-02 9.247E-01 9.247E-01 PB-212 1.202E+00 l.450E-01 l.450E-01 BI-214 8.350E-01 2.229E-01 2.229E-01 PB-214 1.112E+OO l.945E-01 1.945E-01 RN-222 8.350E-01 2.229E-01 2.229E-01 RA-224 1. 761E+OO 1.384E+OO l.384E+OO RA-226 8.350E-01 2.229E-01 2.229E-01 AC-228 1.296E+OO 2.930E-01 2.930E-01 RA-228 1. 296E+OO 2.930E-01 2.930E-01 TH-228 l.202E+OO l.450E-01 l.450E-01 TH-230 8.347E-01 2.228E-01 2.228E-01 TH-232 1.296E+OO 2.930E-01 2.930E-01 U-234 8.347E-01 2.228E-01 2.228E-01 U-235 1.209E-01 3.628E-01 3.628E-01 AM-241 4.223E-01 4.635E-01 4.635E-01 AM-243 3.195E-01 1.326E-01 l.326E-01 ANH-511 3.567E-02 9.415E-02 9.415E-02 Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -4.0lOE+OO 1.522E+Ol l.533E+Ol NOT IDENT. NA-22 l.351E-02 4.553E-02 4.594E-02 NOT IDENT. NA-24 -1.000E+41 2.080E+41 O.OOOE+OO SHORT HLIF AL-26 -7.073E-04 2.539E-02 2.539E-02 NOT IDENT. V-48 -8.580E+03 1.636E+04 1. 681E+o4 SHORT HLIF CR-51 8.187E+02 9 .116E+02 9.835E+02 SHORT HLIF MN-54 -5.347E-02 8.352E-02 8.693E-02 NOT IDENT. C0-56 5.346E-02 4.945E-01 4.951E-01 NOT IDENT. Page 4156 of 5809 MN-56 1.000E+41 9.252E+41 O.OOOE+OO. SHORT HLIF C0-57 1.423E-02 5.200E-02 5.239E-02 NOT IDENT. C0-58 -3.193E-01 6.516E-01 *6.673E-01 NOT IDENT. FE-59 -6.345E-01 9.474E+00 9.478E+OO NOT IDENT. C0-60 9.919E-03 3. 968E-02 3.993E-02 NOT IDENT. ZN-65 -1.844E-01 2.497E-01 2.632E-01 NOT IDENT. GE-68 1. 968E+OO 2.655E+OO 2.799E+OO NOT IDENT. AS-73 5. 872E+OO 1.934E+Ol l.952E+Ol NOT IDENT. AS-74 l.610E+03 6.774E+03 6.813E+03 SHORT HLIF SE-75 -1.202E-01 2.123E-01 2.191E-01 NOT IDENT. BR-77 1.190E+39 l.050E+40 O.OOOE+OO SHORT HLIF SR-82 5.027E+Ol 1. 04 7E+03 1. 04 7E+03 SHORT HLIF RB-83 4.129E-01 7.775E-01 7.995E-01 NOT IDENT. KR-85 6.607E+OO 9.460E+OO 9.918E+OO NOT IDENT. SR-85 7.420E-01 1.063E+OO 1.114E+OO NOT IDENT. RB-86 2.367E+04 3.809E+o4 3.956E+04 SHORT HLIF Y-88 1.067E-01 2.735E-01 2.777E-01 NOT IDENT. Y-91 -1. 996E+02 5.379E+02 5.453E+02 NOT IDENT. NB-94 4.359E-02 3.495E-02 4.009E-02 NOT IDENT. NB-95 3.122E-01 l.190E+OO 1.198E+OO NOT IDENT. NB-95M -7. 960E-01 2.918E+OO 2.940E+OO NOT IDENT. ZR-95 -5.800E-01 l.550E+00 1. 572E+OO FAIL ABUN NB-97 l.000E+41 3.737E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 2.783E+41 O.OOOE+OO SHORT HLIF M0-99 3.133E+32 7.261E+32 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 1.492E+42 O.OOOE+OO SHORT HLIF RH-101 -2.173E-02 4 .196E-02 4.309E-02 NOT IDENT. RH-102 3.239E-02 6.335E-02 6. 501E-02 FAIL ABUN RU-103 8.324E-01 6.925E+OO 6.935E+OO FAIL ABUN RH-106 3.598E-02 5.063E-01 5.066E-01 NOT IDENT. RU-106 3.598E-02 5.063E-01 5.066E-01 NOT IDENT. AG-108M l.463E-03 2.826E-02 2.826E-02 FAIL ABUN AG-llOM l.566E-01 l.256E-01 1. 441E-01 FAIL ABUN SN-113 4.918E-02 2.585E-01 2.594E-01 NOT IDENT. CD-115 4.496E+39 2. 201E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 5.210E+04 1. 401E+05 1. 421E+05 SHORT HLIF TE-123M 2.600E-02 l.429E-01 1.434E-01 NOT IDENT. SB-124 9.314E-03 2. 371E+OO 2.371E+OO FAIL ABUN SB-125 1.178E-01 1.122E-01 l.241E-01 FAIL ABUN TE-125M -6.842E+Ol 3 .182E+02 3.197E+02 NOT IDENT. I-126 -3.929E+05 l.381E+06 1.393E+06 SHORT HLIF SB-126 l.523E+06 2.051E+06 2.163E+06 SHORT HLIF SB-127 3.402E+22 8.449E+22 O.OOOE+OO SHORT HLIF I-131 -2.282E+09 7.919E+09 7.986E+09 SHORT HLIF I-132 -l.000E+41 6 .113E+42 O.OOOE+OO SHORT HLIF TE-132 -5.877E+26 1. 464E+27 O.OOOE+OO SHORT HLIF BA-133 -1. 789E-02 4.913E-02 4.979E-02 FAIL ABUN I-133 -1.000E+41 6.871E+41 O.OOOE+OO SHORT HLIF CS-134 3.433E-02 5.314E-02 5.535E-02 NOT IDENT. CS-135 -2.465E-02 l.433E-01 1.437E-01 NOT IDENT. I-135 -l.000E+41 1.157E+42 O.OOOE+OO SHORT HLIF CS-136 7.616E+04 5.069E+05 5.080E+05 SHORT HLIF BA-137M -4.439E-03 4.073E-02 4.078E-02 NOT IDENT. CS-137 -4.689E-03 4.303E-02 4.308E-02 NOT IDENT. CE-139 5.433E-02 l.189E-01 1.214E-01 NOT IDENT. BA-140 -7.218E+05 1.973E+06 2.000E+06 SHORT HLIF LA-140 4.028E+05 6.048E+05 6.314E+05 SHORT HLIF CE-141 1.859E+Ol 5.576E+Ol 5.638E+Ol FAIL ABUN CE-143 1.000E+41 6.779E+40 O.OOOE+OO SHORT HLIF CE-144 -8.299E-02 3.789E-01 3.808E-01 FAIL ABUN PM-144 2.420E-02 5.512E-02 5.619E-02 NOT IDENT. PR-144 2.108E+OO 4.802E+OO 4.895E+OO NOT IDENT. PM-146 4.022E-02 4.474E-02 4.827E-02 NOT IDENT. ND-147 -5. 996E+07 5.552E+07 6.175E+07 SHORT HLIF PM-147 6.992E+02 8.982E+02 9.519E+02 NOT IDENT. PM-149 l.000E+41 l.124E+41 O.OOOE+OO SHORT HLIF EU-150 3 .134E-04 2.641E-02 2. 641E-02 FAIL ABUN EU-152 -5.728E-02 1.165E-01 1.193E-01 NOT IDENT. GD-153 -l.661E-01 2.4'34E-01 2.546E-01 NOT IDENT. EU-154 3.504E-02 1.118E-01 1.129E-01 FAIL ABUN EU-155 l.012E-01 1.355E-01 1.430E-01 FAIL ABUN TB-160 5.072E-01 2.464E+OO 2.475E+OO FAIL ABUN H0-166M 3.067E-02 6.916E-02 7.053E-02 FAIL ABUN TM-171 -3.926E+Ol 4.887E+Ol 5.198E+Ol NOT IDENT. HF-172 6.398E-02 2. 871E-01 2.885E-01 FAIL ABUN LU-172 -l.178E-01 9.392E-02 1. 079E-01 FAIL ABUN LU-176 7.663E-03 2.368E-02 2.393E-02 FAIL ABUN HF-181 -1.270E-01 5.104E+OO 5.105E+OO NOT IDENT. Page 4157 of 5809 TA-182 6.423E-01 1. 097E+OO l.135E+OO FAIL ABUN RE-183 9. llOE+OO 1.008E+Ol 1.088E+Ol FAIL ABUN RE-184 3.519E+Ol 5.891E+Ol 6.101E+Ol FAIL ABUN W-188 2.453E+Ol l.430E+02 1.435E+02 NOT IDENT. IR-192 -4.296E-01 6.061E-01 6.363E-01 FAIL ABUN HG-203 -2.098E+00 2.798E+OO 2.954E+OO NOT IDENT. BI-207 -2.219E-02 5.014E-02 5 .113E-02 FAIL ABUN PB-210 2.532E+OO 1.050E+Ol 1.056E+Ol NOT IDENT. PB-211 -1.013E+OO 7.909E-01 9.134E-01 FAIL ABUN BI-212 l.926E+.00 7.476E-01 l.146E+OO FAIL ABUN RN-219 2.876E-01 3.779E-01 3. 996E-01 NOT IDENT. RA-223 -1.866E-01 6.285E-01 6.341E-01 FAIL ABUN AC-227 -5.008E-02 2.226E-01 2.237E-01 FAIL ABUN TH-227 -5.008E-02 2.226E-01 2.237E-01 FAIL ABUN TH-229 1.847E-01 4.559E-01 4.635E-01 FAIL ABUN PA-231 3.344E-01 4.612E-01 4.852E-01 NOT IDENT. TH-231 -1.866E-01 6.285E-01 6.341E-01 FAIL ABUN PA-233 -1.938E-02 6.152E-02 6.213E-02 NOT IDENT. PA-234 -1.068E-01 3.420E-01 3.454E-01 FAIL ABUN PA-234M -3.132E+OO 4.937E+OO 5.135E+OO FAIL ABUN TH-234 l.355E+00 l.951E+00 2.045E+00 FAIL ABUN NP-237 -1.938E-02 6.152E-02 6.213E-02 NOT IDENT. NP-238 -1.000E+41 7.184E+40 O.OOOE+OO SHORT HLIF U-238 1.355E+OO 1. 951E+OO 2.045E+OO FAIL ABUN NP-239 -1. 4 63E-01 2.926E-01 2.999E-01 NOT IDENT. PU-239 4.577E+02 6. 311E+02 6.640E+02 FAIL ABUN CM-243 8.128E-03 1.140E-01 l.140E-01 NOT IDENT. BK-247 -3.669E-02 7. 033E-02 , 7.225E-02 NOT IDENT. CM-247 2.675E-02 3.348E-02 3.558E-02 NOT IDENT. CF-249 1. 211E-02 4.121E-02 4.157E-02 NOT IDENT. CF-251 -3.552E-02 1.151E-01 l.162E-01 NOT IDENT. Page 4158of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 56.5264 87.09 88.9700 136.47 69.4951 45.60 58.9785 87.57 76.0074 140.51 0.0000 46.54 62.2691 88.03 76.0804 143.76 70.2601 49.72 0.0000 88.34 76 .1292 144.24 70.3099 51. 35 71.6210 88.47 76.1494 145.44 64.9173 51. 87 64.3473 89. 96 69.4391 152.43 78.0023 52.39 75.0109 1093.63 69.5357 153.25 0.0000 52.97 62.4388 91.11 0.0000 323.87 71.3231 53.44 56.1657 92.59 69.8099 156.02 0.0000 54.07 66.8845 93.35 69.9161 158.56 0.0000 57.36 0.0000 94.56 70.0841 159.00 74.3935 57.53 55.7471 94.65 70.0964 162.33 76.4701 57.98 62. 9718 94.67 70.0992 162.66 0.0000 59.27 62.4755 94.87 70.1271 163.33 81. 7939 59.32 62.4839 97.43 87.7068 165.86 68.9747 59.54 62.5211 98.43 67.4762 176.31 71.6891 60. 96 77.9079 98.44 67.4775 176. 60 0.0000 61.17 77.9513 99.53 56.6107 177.52 70.9131 62. 93 62.3599 100 .11 60.2154 181.07 0.0000 63.29 59.5149 102.03 73.4689 181.52 58.7980 63.58 65.3704 103.18 68.8763 184.41 61.6911 64.28 86.2262 103.37 68. 9011 143.76 61. 7 907 66.73 70.2891 105.21 75.0956 193.51 57.8548 67.24 67.0794 105.31 75.1091 197.03 66.2654 125.81 84.7669 106.12 84.7724 198.01 63.6155 67.75 84.7810 106.47 83.6318 201. 83 67.5495 69.67 76.7009 109.28 66.0447 203.43 47.1887 70.83 84.3113 111. 00 57.8156 205.31 50.8648 72. 81 89.1681 111.76 0.0000 210.85 71. 9332 72.87 89.1809 114. 06 70.2357 215.65 62.5822 74.66 89.5551 116.30 0.0000 222 .11 50.4185 74.82 89.5880 116.74 72.9936 227.09 59.1349 74.97 89.6191 119.76 67.2536 227.38 66.6643 77 .11 90.0598 121.12 56.3763 228.16 0.0000 78.74 90.3912 121.22 56.3857 228.18 64.8412 79.69 90.5829 121.78 61.3457 116.74 64.8412 80.12 90. 6696 122.06 61.3743 235.69 68.1914 80.19 0.0000 122.92 79.9001 235. 96 53.9999 80.57 90.7593 123.07 71.3128 238.63 54.1478 81. 00 90.8453 265.00 78.7690 238.98 0.0000 81. 07 90.8594 125.81 72.4561 240.99 54.2777 81.75 78.8622 127.23 80.8741 242.00 54.3333 83.79 61. 6930 127.91 71. 8754 244.70 41.5773 84.00 75.4368 129.30 72. 0345 252.40 0.0000 85.43 87.1317 131.20 63 .1161 252.80 37.5761 86.55 88.8697 133.02 59. 9648 254.15 0.0000 86.79 88.9140 133.52 74.0145 256.23 47.3683 86.94 88.9423 136.00 72.7921 260.90 0.0000 Page 4159 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 48.7254 355.39 0.0000 584.27 28.1552 264.80 48.7325 356.01 39.4615 595.83 0.0000 265.00 46.7920 364.49 0.0000 427.87 12.8208 268.22 50.8447 366.42 0.0000 602.52 0.0000 269.46 47.9662 372. 51 35.1531 604. 72 19.0874 46.0333 375.05 22. 607.14 17.4565 271. 23 43.1433 377.52 22.4514 609.32 17.4750 273.65 0.0000 356.01 35.4405 610.33 17.4837 276.40 39.4076 388.16 32.3175 614.28 16.2271 277.37 53.2474 388.63 0.0000 618.01 21.1126 277.60 53.2584 391.69 31.'317 5 620.36 14.7959 278.00 51. 3049 264.66 22.8201 621.93 17.5835 279.20 58.2750 401.81 21.7505 630.19 0.0000 279.54 64.2211 402.40 19.5831 631.29 16.7338 279.70 64.2303 404.85 39.2322 633.25 26.0543 280.46 37.5756 410.95 37.7533 634.78 0.0000 283.69 53.5529 413.71 18.0895 635.95 14.9077 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 41. 7163 423.72 0.0000 645.85 20.5941 285.90 0.0000 427.09 28.7586 657.76 21. 6509 287.50 53.7341 427.87 21.0267 657.90 0.0000 290.67 47.8984 433.94 24.4430 661. 66 26.4055 293.27 0.0000 439.40 25.0864 664.57 0.0000 351.93 46.0852 453.88 15.7528 666.33 0.0000 295.96 37.5938 463.37 29.4277 666.50 0.0000 879.38 46.7214 468.07 25.5396 667.71 0.0000 299.98 36.2153 473.00 0.0000 677.62 20.8996 300.09 36.2190 475.06 27.3574 685.70 0.0000 300.13 36.2197 476.78 23. 9625 695.00 0.0000 301.36 38.2721 477.60 29.6827 696.49 14.3706 302.85 58.4897 482.18 24.0403 696. 51 14.3706 256.23 40.3947 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 18.2091 306.78 33.3901 497.08 23. 0969 697.49 18.2108 308.46 36.4768 505.52 34.8145 702.65 13.4493 311. 90 42.6793 507.63 0.0000 706.68 26.9464 316.51 50.4930 511. 00 37.2516 711.68 21. 2185 319.41 0.0000 514.00 27.9863 720.70 0.0000 320.08 0.0000 514.00 27.9863 721. 93 0.0000 321.04 32.7637 520.40 23.6992 722.78 23.2588 323.87 35.4048 520.69 0.0000 722.91 23.2603 325.23 52.3945 522.65 0.0000 723. 31 20.1621 328.76 0.0000 527.90 0.0000 724 .19 0.0000 333.37 31.0217 528.26 24.6846 727.33 7.7681 333.97 31. 0364 529.59 22.9380 733.00 9.0847 334.37 27.9415 529.87 0.0000 735.93 18.5170 338.28 28.0278 531. 02 0.0000 333.97 21. 4548 338.32 28.0289 537.26 0.0000 739.50 0.0000 311. 90 38.9946 546.56 0.0000 747.24 17.6265 340.48 38.9946 552.55 22.3328 748.06 24.4896 340.55 0.0000 563.25 20.1243 752.31 16.6825 344.28 45.3674 569.33 31.7244 753.82 0.0000 345.93 38.8461 946.00 25.9585 756.73 16.7131 351.06 38.7893 569.70 20.1920 756.80 16.7136 351. 93 38.8149 583.19 28.1401 884.68 22.0876 Page 4160of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 20.5258 1274.44 11. 8154 1620.50 2.0307 766.42 14.2137 1001.03 19.3645 1621. 92 3.0469 766.84 12. 4111 1002.74 13.9934 1678.03 0.0000 772.60 0.0000 1004.73 15.0797 1690.97 4.1234 776.52 0.0000 507. 63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 2.0936 778.90 7.9368 1028.54 0.0000 1063.66 1. 7467 783.70 0.00.00 1037.84 10.4520 1771. 35 2.9950 785.37 15.9150 1038.76 0.0000 1791.20 0.0000 792.07 23.9370 631.29 5.2406 1808.65 2 .1123 794.95 11.9824 1048.07 0.0000 1810.72 0.0000 795.86 12.9853 1049.04 14.2045 1836.06 3.1857 810.06 10.0452 1050.41 14.2108 810.29 12.0553 1063.66 13.1719 344.28 12.0560 1077.00 0.0000 810.76 17. 0815 1077.34 8.8188 815.77 0.0000 1085.87 14.3687 1048.07 0.0000 1093.63 21.0503 832.01 10.1309 1099.45 16.6489 834.85 21.0952 1112. 07 8.9131 835.71 17.8557 1112.84 11.1444 836.80 0.0000 1115. 54 19.6292 846.75 0.0000 1120.29 15. 6372 846.77 12.2260 1120. 55 15.6381' 856.80 0.0000 1221.41 15.6415 860.56 19.4581 1129. 67 19.7130 871.09 21. 5909 1131.51 0.0000 873.19 10.2893 1147.95 0.0000 875.33 0.0000 1173.23 14.5211 879.38 13.2004 1177.95 9.9967 880.51 16.5073 1189.05 10.0289 883.24 18.1763 1204.77 11. 9050 884.68 14.8790 1221.41 9.2007 889.28 0.0000 1231.02 15.6827 894.76 8. 2966 1235.36 0.0000 898.04 19.9354 1238.28 15.7142 900. 72 16.6289 1260.41 0.0000 903.28 11. 0960 1271.87 15.8595 911.20 9.3889 1274.44 7.4684 912.08 9.3917 1274.54 7.4684 923.98 0.0000 1291.59 7.5027 926.50 11.7472 1298.22 0.0000 929.11 20.1568 1312 .11 0.0000 937.49 14.7408 1332.49 6.6356 944 .13 0.0000 1362.66 0.0000 946.00 16.8965 1365.19 2.8679 949.00 15.8565 1368.63 0.0000 667.71 0.0000 1384.29 8.6454 962. 31 11.8938 1408.01 9.6631 964.08 15.3013 1457.56 0.0000 966 .17 25.5198 1460.82 2.9364 911. 20 20.2229 1489.16 5.9127 968. 97 20.2229 1505.03 5.9347 983.53 0.0000 1584.12 4.0287 984.45 0.0000 1596.21 0.0000 Page 4161of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:19:11.60 ********************************************************************************
  • GEL Laboratories LLC ; *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235055.CNF;l Background file : DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM11.CNF;517 Background date : Z-OCT-2016 11:00:34. Sample date : 2-DEC-2015 14:59:00. Acquisition date : 3-0CT-2016 07:18:44. Sample ID : G405235055 Sample quantity : 1.42583E+02 GRAM Detector name : GAMll Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.58 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 1 5 5 5 5 0 0 0 6 6 0 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4162of5809 Energy 63.34* 73.12* 74.95* 77.09* 87.10 88.77 90.10 92.62* 186.16* 209.16 216.23 238.58* 241. 80 270.53 277.21 280.00* 295.32* 299.81 328.23 338.39* 352.03* 409.52 463.24 466.55 511.15* 546.28 583.16* 609.52* 724. 04 727. 29* 795.61 806.09 835.33 861.31 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 14 22 158 247 125 45 90 112 95 55 10 444 115 29 35 15 132 21 43 102 260 26 31 15 55 12 138 163 16 21 20 25 22 21 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 132 130 127 122 155 148 110 128 138 101 77 50 87 74 48 48 84 75 50 47 82 41 32 25 39 9 22 46 11 24 15 27 17 24 0.86 1. 00 1. 01 1. 01 1. 45 1. 52 1.12 1. 53 1. 39 1.29 1.18 0. 96 1. 97 0.75 1. 28 1. 61 1. 02 0.72 2. 96 1. 07 1. 29 0.78 0.97 0.61 1. 68 1. 33 1. 47 1. 38 2.30 1. 41 0.98 5.27 1. 88 3.79 126.58 146.16 149.82 154 .11 174.14 177.48 180.13 185.18 372.40 418.42 432.57 477.29 483.74 541.23 554.60 560.20 590.85 599.83 656.71 677.03 704.33 819.37 926.88 933.50 1022.75 1093.04 1166. 82 1219.56 1448. 71 1455.21 1591.89 1612.85 1671.35 1723.33 124 143 143 143 165 165 165 165 368 413 429 471 471 538 551 551 586 599 652 673 697 815 924 930 1015 1090 1161 1214 1445 1452 1586 1597 1665 1717 7 3.93E-03142.8 17 6.03E-03 88.0 17 4.38E-02 14.2 17 6.87E-02 9.8 29 3.48E-02 19.9 29 l.24E-02 58.2 29 2.50E-02 23.2 29 3.12E-02 23.3 11 2.63E-02 27.8 10 l.54E-02 36.6 7 2.67E-03154.9 20 l.23E-01 5.5 20 3.20E-02 22.6 9 8.08E-03 57.0 13 9.71E-03 38.4 13 4.03E-03 89.8 10 3.68E-02 15.7 7 5.90E-03 71.0 10 l.19E-02 34.6 10 2.84E-02 16.4 13 7.23E-02 9.6 9 7.08E-03 49.2 6 8.49E-03 33.3 8 4.26E-03 62.5 16 l.54E-02 33.8 6 3.44E-03 47.4 12 3.83E-02 11.3 11 4. 52E-02 11. 5 7 4.31E-03 43.0 9 5.95E-03 47.0 12 5.45E-03 48.1 21 7.00E-03 54.7 11 5.97E-03 42.5 16 5.83E-03 56.5 Fit 4.65E+00 5 .13E+OO l.70E+OO l.99E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235055 Acquisition date : 3-0CT-2016 07:18:44 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 902.13 24 17 3.44 1804.99 1796 17 6.64E-03 44.5 36 0 911. 50* 85 20 1. 66 1823. 73 1818 15 2.35E-02 16.0 37 0 968.9,7* 54 11 1.04 1938.70 1934 9 J..49E-02 18.2 38 0 992.16 6 7 0.59 1985.10 1982 8 1. 78E-03 77. 8 39 0 1004.93 15 3 1.99 2010.65 2007 8 4.lOE-03 34.5 40 0 1011. 06 6 8 0.74 2022.90 2017 8 1.73E-03 88.1 41 0 1120.75* 41 30 2.17 2242.33 2235 12 1.14E-02 31. 5 42 0 1218.96 10 16 0.54 2438.77 2431 12 2.80E-03 88.8 43 0 1238.47 24 11 0.87 2477.79 2472 11 6.67E-03 33.7 44 0 1307.89 8 4 0.65 2616.65 2613 7 2.15E-03 59.4 45 0 1311. 09 6 2 0.98 2623.04 2620 7 1. 67E-03 55. 4 46 0 1378.42 18 3 1.37 2757.71 2751 14 4.98E-03 32.2 47 0 1460.98* 409 12 1.83 2922.82 2915 16 l.14E-01 5.3 48 0 1510.64 6 3 1.33 3022.13 3018 8 1. 67E-03 68. 7 49 0 1765.50* 9 18 1. 53 3531. 7 9 3524 10 2.49E-03 97.1 Flag: "*" = Peak area was modified by background subtraction Page 4163 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:19:13 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235055.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 14:59:00 G405235055 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:18:44 142.58 GRAM Sample type .; : Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAll 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4164 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 74.82 74.82 74.82 351. 93 87.09 87.09 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 AM-243 TH-228 PB-212 BI-211 SN-126 SN-126 Line 240.99 74.66 74.82 74.82 351.06 86.94 87.57 CAN 0 01:00:00.58 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10. 66* ' l.238E+OO l.566E+Ol 10.65 OK MN-54 834.85 99.98* 1. 951E+OO 5.867E-02 1.157E-01 84.94 OK CD-109 88.03 3.70* 6.347E+OO 1.222E+OO l.934E+00 116. 41 OK SN-126 64.28 9.60 3.887E+OO 2.492E-01 2.492E-01 285.54 OK 86.94 8.90 6.243E+OO 1.089E+OO 1. 089E+OO 53.79 OK 87.57 37.00* 6.243E+OO 2.620E-01 2.620E-01 53.79 OK HG-203 70.83 3.69 4.810E+OO Line Not Found Absent 72.87 6.19 5.060E+OO 4.502E-01 4.252E+Ol 176.05 OK 279.20 81.56* 4.679E+OO 2.224E-02 2 .101E+OO 17 9. 62 OK TL-208 277.37 6.60 4.717E+OO 6.579E-01 6.579E-01 76.73 OK 583.19 85.00* 2.582E+OO 3. 451E-01 3.451E-01 22.59 OK 860.56 12.50 1.906E+OO 4. 681E-01 4. 681E-01 113. 09 OK BI-211 72. 87 1. 23 5.060E+OO 2.266E+OO 2.266E+00 176.05 OK 351.06 12.92* 3.883E+OO 4. 031E-01 4. 031E-01 245.18 OK PB-212 74.82 10.28 5.247E+OO 1.369E+OO 1.369E+OO 41.15 OK 77 .11 17.10 5.454E+OO 1. 718E+OO 1.718E+OO 19.51 OK 238.63 43.60* 5. 301E+OO 1.140E+OO 1.140E+OO 10.96 OK 300.09 3.30 4.428E+OO 8.462E-01 8.462E-01 142.02 OK BI-214 609.32' 45.49* 2.494E+OO 7.851E-01 7. 853E-01' 22.91 OK 1120.29 14.92 1.547E+OO 9.205E-01 9.209E-01 62.91 OK 1764.49 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 OK PB-214 74.82 5.80 5.234E+OO Line Not Found <<INT Reject 77 .11 9.70 5.454E+OO 3.028E+OO 3.029E+OO 19.51 OK 87.09 3.41 6.242E+OO Line Not Found <<INT Reject 242.00 7.25 5.244E+OO Line Not Found <<INT Reject 295.22 18.42 4.482E+OO 9.343E-01 9.346E-01 31. 36 OK 351. 93 35.60* 3.884E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.494E+OO 7. 851E-01 7.853E-01 22.91 OK 1120.29 14.92 1. 547E+OO 9.205E-01 9.209E-01 62. 91 OK 1764.49 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 OK RA-224 240.99 4.10* 5.247E+OO 1.519E+OO 1.519E+OO 100.40 OK RA-226 609.32 45.49* 2.494E+OO 7.851E-01 7.853E-01 22.91 OK 1120.29 14.92 1.547E+OO 9.205E-01 9.209E-01 62.91 OK 1764.49 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 OK AC-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11.27 4. OllE+OO 1.305E+OO 1.305E+OO 32.77 OK 794.95 4.25 2.027E+OO 1.219E+OO l.219E+00 96.12 OK 835.71 1. 61 1. 951E+OO 3.643E+OO 3.643E+OO 84.94 OK 911.20 25.80* l.823E+OO 9.506E-01 9.506E-01 32.02 OK 968. 97 15.80 1.738E+OO 1.028E+OO 1.028E+OO 36.48 OK RA-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4. OllE+OO 1.305E+00 1.305E+OO 32.77 OK 794.95 4.25 2.027E+OO 1.219E+OO 1.219E+OO 96.12 OK 835. 71 1. 61 1.951E+OO 3.643E+OO 3.643E+OO 84.94 OK 911. 20 25.80* 1.823E+OO 9.506E-01 9.506E-01 32.02 OK 968. 97 15.80 1.738E+OO 1.028E+OO 1.028E+OO 36.48 OK TH-228 74.82 10.28 5.247E+OO 1.369E+OO 1.369E+OO 41.15 OK 77 .11 17.10 5.454E+OO 1. 718E+OO 1. 718E+OO 19.51 OK 238.63 43.60* 5. 301E+OO l.140E+00 1.140E+OO 10. 96 OK Page 4165of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 300.09 3.30 4.428E+OO 8.462E-01 8.462E-01 142.02 OK TH-230 609.32 45.49* 2.494E+OO 7.851E-01 7.851E-01 22.91 OK 1120. 29 14.92 1.547E+OO 9.205E-01 9.206E-01 62.91 OK 1764.49 15.30 1.039E+OO 2.798E-01 2.798E-01 194.22 OK TH-232 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4. OllE+OO l.305E+OO 1.305E+OO 32.77 OK 835.71 1. 61 1.951E+OO 3.643E+OO 3.643E+OO 84.94 OK 911.20 25.80* 1.823E+OO 9.506E-01 9.506E-01 32.02 OK 968. 97 15.80 1.738E+00 1.028E+OO 1. 028E+OO 36. 48 OK TH-234 63.29 3.70* 3.887E+OO 6.466E-01 6.466E-01 285.54 OK 92.59 4.23 6.560E+OO 2.586E+OO 2.586E+OO 46.65 OK U-234 609.32 45.49* 2.494E+OO 7. 851E-01 7.851E-01 22.91 OK 1120.29 14.92 1. 547E+OO 9.205E-01 9.205E-01 62.91 OK 1764.49 15.30 1.039E+OO 2.798E-01 2.798E-01 194.22 OK U-235 89.96 3.47 6.425E+OO 2.578E+OO 2.578E+OO 46.33 OK 93.35 5.60 6.560E+OO 1.953E+OO 1.953E+OO 46.65 OK 143.76 10.96* 7.059E+OO Line Not Found Absent 163.33 5.08 6. 731E+OO Line Not Found Absent 185. 72 57.20 6.280E+OO 1.592E-01 1.592E-01 55.51 OK 205.31 5.01 5.902E+00 Line Not Found Absent U-238 63. 29 3.70* 3.887E+OO 6.466E-01 6.466E-01 285.54 OK 92.59 4.23 6.560E+OO 2.586E+OO 2.586E+00 46.65 OK AM-243 43.53 5.90 9.310E-01 Line Not Found Absent 74.66 67.20* 5.247E+OO 2.095E-01 2.095E-01 41.15 OK -ANH-511 511. 00 100.00* 2.867E+OO 1.076E-01 1.076E-01 67.65 OK Flag: "*" = Keyline Page 4166 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:19:14.50 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235055.CNF;l * *Acquisition date 3-0CT-2016 07:18:44 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:59:00 Analyst initials: MXRl *
  • Sample ID G405235055 Sample Quantity 1.4258E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.566E+Ol 1.635E+OO MN-54 1.157E-01 9. 631E-02 CD-109 1.934E+OO 2.207E+OO SN-126 2.620E-01 1.381E-01 HG-203 2.101E+OO 3.698E+OO TL-208 3. 451E-01 7.639E-02 BI-211 4.031E-01 9.685E-01 PB-212 1.140E+OO l.224E-01 BI-214 7.853E-01 1. 764E-01 PB-214 1.081E+OO 2.029E-01 RN-222 7.853E-01 1. 764E-01 RA-224 1.519E+OO 1.495E+OO RA-226 7.853E-01 1. 764E-01 AC-228 9.506E-01 2.983E-01 RA-228 9.506E-01 2.983E-01 TH-228 1.140E+OO 1.224E-01 TH-230 7. 851E-01 1. 763E-01 TH-232 9.506E-01 2.983E-01 TH-234 6.466E-01 1.809E+OO U-234 7. 851E-01 1. 763E-01 U-235 l.054E-01 1.839E-01 U-238 6.466E-01 1.809E+OO AM-243 2.095E-01 8.449E-02 ANH-511 1.076E-01 7 .132E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4167of5809 Key-Line Activity (pCi/GRAM 2.135E+00 -7.539E-03 O.OOOE+OO -2.270E-02 -l.034E-01 O.OOOE+OO K.L. Cnt Uncert (1. 96-sigma) 1.313E+Ol 3.370E-02 1.960E+41 2.650E-02 3.186E-Ol l.852E+04 MDA (pCi/GRAM 7.527E-01 1. 061E-01 1.583E+OO l.004E-01 4.402E+OO 6.780E-02 3.207E-01 8.561E-02 l. ll 7E-01 3.276E-01 l.117E-01 9.180E-01 1. ll 7E-01 l.994E-01 1.994E-01 8.561E-02 1.116E-01 l.994E-01 1. 744E+OO 1.116E-01 3.559E-01 1. 744E+OO 7.061E-02 4.428E-02 MDA (pCi/GRAM 2.602E+Ol 6. 721E-02 O.OOOE+OO 3.826E-02 5.819E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.940E+02 O.OOOE+OO SHORT HLIF C0-56 -9.827E-02 4.747E-01 8.743E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.965E-02 4.152E-02 7.600E-02 NOT IDENT. C0-58 5.349E-01 5.409E-01 1.165E+OO NOT IDENT. FE-59 -2.997E+OO 6.039E+OO l.130E+Ol NOT IDENT. C0-60 5.845E-03 3.957E-02 8.222E-02 NOT IDENT. ZN-65 -5.151E-02 1. 780E-01 2.958E-01 NOT IDENT. GE-68 8.335E-01 2.155E+OO 4.619E+OO NOT IDENT. AS-73 2.915E-01 6.694E+OO 1. 341E+Ol NOT I DENT .. AS-74 O.OOOE+OO 6.458E+03 O.OOOE+OO SHORT HLIF SE-75 1.280E-01 2.108E-01 4.065E-01 FAIL ABUN BR-77 O.OOOE+OO 1.213E+38 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 5.781E+02 O.OOOE+OO SHORT HLIF RB-83 1.943E-01 5.513E-01 1.149E+OO NOT IDENT. KR-85 4.389E+OO 7.099E+OO 1.350E+Ol NOT IDENT. SR-85 4.913E-01 7.974E-01 1.516E+OO NOT IDENT. RB-86 O.OOOE+OO 3.281E+04 O.OOOE+OO SHORT HLIF Y-88 5 .113E-02 l.433E-01 3.836E-01 NOT IDENT. Y-91 5.437E+Ol 4. 841E+o2 9.935E+02 NOT IDENT. NB-94 2.015E-03 2. 978E-02* 5.755E-02 NOT IDENT. NB-95 -7.864E-01 9.864E-01 1.645E+OO NOT IDENT. NB-95M 7.041E-01 2.337E+OO 4.087E+OO NOT IDENT. ZR-95 1. 273E+OO 1.398E+OO 3.065E+00 FAIL ABUN NB-97 O.OOOE+OO l.777E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 451E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 7.218E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 -8.904E-03 3.026E-02 5.594E-02 NOT IDENT. RH-102 2.331E-02 5.997E-02 l.209E-01 NOT IDENT. RU-103 -1.254E+OO 5.342E+OO 1. 024E+Ol FAIL ABUN RH-106 -3.852E-01 4.630E-01 7.868E-01 NOT IDENT. RU-106 -3.852E-01 4.630E-01 7.868E-01 NOT IDENT. AG-108M -1. 872E-02 2.145E-02 3.788E-02 FAIL ABUN AG-llOM 7.178E-02 l.OOOE-01 2.123E-01 NOT IDENT. SN-113 -1.212E-01 2.078E-01 3.857E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 703E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1. l 70E+05 O.OOOE+OO SHORT HLIF TE-123M -2. 961E-02 1.236E-01 2.261E-01 NOT IDENT. SB-124 -7.729E-01 1. 971E+OO 3.721E+00 FAIL ABUN SB-125 3.077E-03 1.046E-01 2.047E-01 FAIL ABUN TE-125M 4.238E+Ol 2.603E+02 5.035E+02 NOT IDENT. I-126 O.OOOE+OO 1.091E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.564E+06 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 5.586E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 6.899E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF TE-132 O.OOOE+OO l.256E+27 O.OOOE+OO SHORT HLIF BA-133 -7.207E-03 3.586E-02 6.292E-02 FAIL ABUN I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 8.021E-02 7.556E-02 1.061E-01 FAIL ABUN CS-135 -8.247E-02 l.558E-01 2.408E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.942E+05 O.OOOE+OO SHORT HLIF BA-137M -1.994E-03 2.939E-02 6.125E-02 NOT IDENT. CS-137 -2.107E-03 3.105E-02 6.470E-02 NOT IDENT. CE-139 6.543E-02 l.032E-01 2.023E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 696E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.159E+05 O.OOOE+OO SHORT HLIF CE-141 -2.425E+Ol 2.762E+Ol 4.810E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 7.253E-02 3.338E-01 6.393E-01 NOT IDENT. PM-144 2.415E-02 5.483E-02 1.108E-01 NOT IDENT. PR-144 2.030E+00 4.767E+OO 9.618E+OO NOT IDENT. PM-146 -4.580E-04 3.984E-02 7.823E-02 NOT IDENT. ND-147 O.OOOE+OO 4.655E+07. O.OOOE+OO SHORT HLIF PM-147 -5.363E+Ol 6.984E+02 l.324E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 -6.984E-03 2.588E-02 4.469E-02 FAIL ABUN EU-152 -5.224E-03 7.306E-02 1.457E-01 NOT IDENT. GD-153 -9.376E-02 1. 649E-01 2.789E-01 NOT IDENT. EU-154 -1.843E-02 8.236E-02 1.643E-01 FAIL ABUN EU-155 4.286E-02 9.480E-02 l.876E-01 FAIL ABUN TB-160 -6.734E-02 1.655E+00 3.197E+OO FAIL ABUN H0-166M -5.234E-03 5.855E-02 1.099E-01 FAIL ABUN TM-171 -7.729E-01 1.458E+Ol 2. 911E+Ol NOT IDENT. HF-172 -3.845E-02 2. lllE-01 3.938E-01 FAIL ABUN LU-172 4.600E-02 6.608E-02 l.490E-01 FAIL ABUN Page 4168 of 5809 LU-176 -1.423E-02 2.274E-02 3. 781E-02 FAIL ABUN HF-181 -3.849E+OO 4.018E+OO 6.906E+OO NOT IDENT. TA-182 5. 096E-02 8.lOlE-01 l.486E+OO FAIL ABUN RE-183 -1.584E-01 2.217E+OO 4.397E+00 NOT IDENT. RE-184 O.OOOE+OO 6.264E+Ol 6.706E+Ol FAIL ABUN W-188 4.864E+Ol l .191E+02 2. 096E+02 FAIL ABUN IR-192 -9.828E-02 4.658E-01 8.178E-01 FAIL ABUN BI-207 2.538E-02 4.149E-02 9. 231E-02 FAIL ABUN PB-210 -1.565E-01 2.157E+OO 4.309E+OO NOT IDENT. PB-211* 4.857E-01 7. 072E-01 NOT IDENT. BI-212 7.973E-01 7.343E-01 l.204E+OO FAIL ABUN RN-219 -2.008E-01 3.705E-01 6.866E-01 FAIL ABUN RA-223 3. 371E-03 5.541E-01 9.988E-01 FAIL ABUN AC-227 -4.685E-02 2.038E-01 3.629E-01 FAIL ABUN TH-227 -4.685E-02 2.038E-01 3.629E-01 FAIL ABUN TH-229 2.503E-01 4.606E-01 8.830E-01 FAIL ABUN PA-231 4.614E-01 4.617E-01 9.078E-01 NOT IDENT. TH-231 3. 371E-03 5.541E-01 9.988E-01 FAIL ABUN PA-233 -4.883E-03 5.664E-02 1. OllE-01 FAIL ABUN PA-234 -7.978E-02 2.245E-01 4.036E-01 NOT IDENT. PA-234M 2.193E-01 4.447E+OO 7.990E+OO NOT IDENT. NP-237 -4.883E-03 5.664E-02 1. OllE-01 FAIL ABUN NP-238 0.000E+OO 1. 960E+41 0.000E+OO SHORT HLIF NP-239 -l.615E-01 2.036E-01 3.634E-01 FAIL ABUN PU-239 8.953E+Ol 2.788E+02 5.389E+02 NOT IDENT. AM-241 2.645E-02 1.014E-01 2.048E-01 NOT IDENT. CM-243 -7.247E-02 8.916E-02 1.604E-01 FAIL ABUN BK-247 4.946E-02 7.313E-02 1.413E-01 NOT IDENT: CM-247 -3.300E-02 3.395E-02 5.992E-02 FAIL ABUN CF-249 8.827E-03 3.478E-02 7.019E-02 NOT IDENT. CF-251 1.028E-01 9.801E-02 1.997E-01 NOT IDENT. Page 4169 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:19:12.30 Nuclide Line Activity Report Nuclide Type: .. Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 393 10.66* 1.238E+OO l.566E+Ol 1.566E+Ol 10.65 MN-54 834.85 22 99.98* 1. 951E+OO 5.867E-02 1.157E-01 84.94 CD-109 88.03 55 3.70* 6.347E+OO 1.222E+OO 1.934E+OO 116. 41 SN-126 64.28 18 9.60 3.887E+OO 2.492E-01 2.492E-01 285.54 86.94 153 8.90 6.243E+OO 1. 447E+OO 1. 44 7E+OO 39.73 87.57 153 37.00* 6.243E+OO 3.481E-01 3.481E-01 39.73 HG-203 70.83 ------3.69 4.810E+OO ------Line Not Found ------72. 87 27 6.19 5.060E+OO 4.502E-01 4.252E+Ol 176.05 279.20 16 81.56* 4.679E+OO 2.224E-02 2.101E+OO 179.62 TL-208 277.37 39 6.60 4.717E+OO 6.579E-01 6.579E-01 76.73 583.19 144 85.00* 2.582E+OO 3.451E-01 3.451E-01 22.59 860.56 21 12.50 l.906E+OO 4. 681E-01 4.681E-01 113. 09 BI-211 72.87 27 1. 23 5.060E+OO 2.266E+OO 2.266E+OO 176.05 351.06 284 12.92* 3.883E+OO 2.977E+OO 2.977E+OO 19.15 PB-212 74.82 194 10.28 5.247E+OO 1. 897E+OO l.897E+OO 28.41 77 .11 304 . 17 .10 5.454E+00 1.718E+OO 1.718E+OO 19.51 238.63 500 43.60* 5. 301E+OO 1.140E+OO 1.140E+OO 10. 96 300.09 23 3.30 4.428E+OO 8.462E-01 8.462E-01 142.02 BI-214 609.32 169 45.49* 2.494E+00 7. 851E-01 7.853E-01 22.91 1120.29 40 14.92 1.547E+OO 9.205E-01 9.209E-01 62. 91 1764.49 8 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 PB-214 74.82 194 5.80 5.247E+OO 3.361E+00 3.363E+OO 28.41 77 .11 304 9.70 5.454E+OO 3.028E+OO 3.029E+OO 19.51 87.09 153 3.41 6.243E+OO 3.777E+OO 3.778E+OO 39.73 242.00 130 7.25 5.247E+00 1. 793E+OO 1.794E+OO 45.24 295.22 147 18.42 4.482E+OO 9.343E-01 9.346E-01 31. 36 351. 93 284 35.60* 3.883E+OO 1.081E+OO 1.081E+OO 19.15 RN-222 609.32 169 45.49* 2.494E+OO 7.851E-01 7.853E-01 22.91 1120.29 40 14.92 1. 547E+OO 9.205E-01 9.209E-01 62.91 1764.49 8 15.30 1. 039E+OO 2.798E-01 2.799E-01 194.22 RA-224 240.99 130 4.10* 5.247E+OO 3.171E+OO 3.171E+OO 45.24 RA-226 609.32 169 45.49* 2.494E+OO 7.851E-01 7.853E-01 22.91 1120.29 40 14.92 1. 547E+OO 9.205E-01 9.209E-01 62.91 1764.49 8 15.30 1.039E+OO 2.798E-01 2.799E-01 194.22 AC-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 112 11. 27 4.0llE+OO 1.305E+OO 1.305E+OO 32.77 794.95 20 4.25 2.027E+OO 1.219E+OO 1.219E+OO 96.12 835. 71 22 1. 61 1.951E+00 3.643E+OO 3.643E+OO 84.94 911.20 85 25.80* 1.823E+OO 9.506E-01 9.506E-01 32.02 968. 97 54 15.80 1. 738E+OO 1.028E+OO l.028E+OO 36.48 RA-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 112 11. 27 4. OllE+OO 1.305E+OO 1.305E+OO 32.77 794.95 20 4.25 2.027E+OO 1.219E+OO 1.219E+OO 96.12 835.71 22 1. 61 1. 951E+OO 3.643E+OO 3.643E+OO 84.94 911.20 85 25.80* 1.823E+OO 9.506E-01 9.506E-01 32.02 968. 97 54 15.80 1.738E+OO 1.028E+OO 1.028E+OO 36.48 TH-228 74.82 194 10.28 5.247E+OO 1.897E+OO 1.897E+OO 28.41 Page 4170 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 304 17.10. 5.454E+OO 1.718E+OO 1. 718E+OO 19.5i 238.63 500 43.60* 5.301E+OO 1.140E+OO 1.140E+OO 10. 96 300.09 23 3.30 4.428E+OO 8.462E-01 8.462E-01 142.02 TH-230 609.32 169 45.49* 2.494E+OO 7.851E-01 7. 851E-01 22.91 1120. 29 40 14.92 1. 547E+00 9.205E-01 9.206E-Ol 62.91 1764.49 8 15.30 1.039E+OO 2.798E-01 2.798E-Ol 194.22 TH-232 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 112 11. 27 4. OllE+OO 1.305E+OO 1.305E+OO 32.77 835. 71 22 1. 61 1.951E+OO 3.643E+OO 3.643E+OO 84.94 911. 20 85 25.80* 1.823E+OO 9.506E-01 9.506E-Ol 32.02 968. 97 54 15.80 1.738E+OO 1.028E+OO 1.028E+OO 36.48 TH-234 63.29 18 3.70* 3.887E+00 6.466E-01 6.466E-01 285.54 92.59 136 4.23 6.560E+OO 2.586E+OO 2.586E+OO 46.65 U-234 609.32 169 45.49* 2.494E+OO 7.851E-01 7.851E-01 22.91 1120.29 40 14.92 1. 547E+OO 9.205E-01 9.205E-01 62.91 1764.49 8 15.30 I 1.039E+OO 2.798E-01 2.798E-01 194.22 U-235 89.96 109 3.47 6.425E+OO 2.578E+OO 2.578E+OO 46.33 93.35 136 5.60 6.560E+OO 1.953E+OO 1.953E+OO 46.65 143.76 ------10.96* 7.059E+OO ------Line Not Found ------163.33 ------5.08 6. 731E+OO ------Line Not Found ------185.72 109 57.20 6.280E+OO l.592E-01 1.592E-01 55.51 205.31 ------5.01 5.902E+OO ------Line Not Found ------U-238 63.29 18 3.70* 3.887E+OO 6.466E-01 6.466E-01 285.54 92.59 136 4.23 6.560E+OO 2.586E+OO 2.586E+OO 46.65 AM-243 43.53 ------5.90 9.310E-01 ------Line Not Found ------74.66 194 67.20* 5.247E+OO 2. 901E-01 2.901E-01 28.41 ANH-511 511. 00 59 100.00* 2.867E+OO l.076E-01 1. 076E-01 67. 65 Flag: "*" Key line Page4171 of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235055 Acquisition date 3-0CT-2016 07:18:44 Total number of lines in spectrum 49 Number of unidentified lines 9 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide K-40 MN-54 CD-109 SN-126 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 312.05D 461. 40D 2.30E+05Y 46.59D 1. 41E+l0Y 7.04E+08Y l.41E+10Y 1600. OOY 1600.00Y 1600. OOY 1. 41E+10Y 1600.00Y l.41E+l0Y 1. 41E+l0Y l.41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 97 1. 58 1. 00 94.5 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity
  • Uncorrected pCi/GRAM l.566E+Ol 5.867E-02 1.222E+OO 3.481E-01 2.224E-02 3.451E-01 2.977E+OO l.140E+OO 7. 851E-01 1. 081E+OO 7.851E-01 3.171E+OO 7. 851E-01 9.506E-01 9.506E-01 1.140.E+OO 7.851E-01 9.506E-01 6.466E-01 7.851E-01 l.592E-01 6.466E-01 2.901E-01 1. 076E-01 3.580E+Ol 3.580E+Ol Decay Corr pCi7GRAM 1. 566E+Ol l.157E-01 1.934E+OO 3.481E-01 2. lOlE+OO 3. 451E-01 2.977E+OO 1.140E+OO 7.853E-01 1.081E+OO 7.853E-01 3.171E+OO 7.853E-01 9.506E-01 9.506E-01 1.140E+OO 7. 851E-01 9.506E-01 6.466E-01 7. 851E-01 l.592E-01 6.466E-01 2.901E-01 1.076E-01 3.865E+Ol 3.865E+Ol 81. 63% Decay Corr 2-Sigma Error 0.167E+Ol 0.983E-01 2.252E+OO l.383E-01 3.774E+OO 0.780E-01 0.570E+00 0.125E+OO 1. 800E-01 0.207E+OO 1.800E-01 1.435E+OO l.800E-01 3.044E-01 3.044E-01 0.125E+OO 1. 799E-01 3.044E-01 18.46E-01 1.799E-01 0.884E-01 18.46E-01 0.824E-01 0.728E-01 "M" Manually accepted 2-Sigma %Error Flags 10.65 84.94 116. 41 39.73 179.62 22.59 19.15 10. 96 22.91 19.15 22.91 45.24 22.91 32.02 32.02 10. 96 22.91 32.02 285.54 22.91 55.51 K 285.54 28.41 67. 65 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4172 of 5809 Unidentified Energy Lines Page : 4 Sample ID : G405235055 Acquisition date : 3-0CT-2016 07:18:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.16 63 114 1. 29 418.42 413 10 l.54E-02 73.2 5.83E+OO 0 216.23 11 88 1.18 432.57 429 7 2.67E-03 **** 5.70E+OO T 0 270.53 32 82 0.75 541.23 538 9 8.08E-03 **** 4.81E+OO T 0 328.23 4, 7 55 2. 96 656. 71 652 10 l.19E-02 6.9. 2 4. llE+OO T 0 409.52 27 44 0.78 819.37 815 9 7.08E-03 98.3 3.43E+OO T 0 463.24 33 35 0.97 926.88 924 6 8.49E-03 66.6 3.lOE+OO T 0 466.55 16 26 0.61 933.50 930 8 4.26E-03 **** 3.09E+OO 0 546.28 13 9 1. 33 1093.04 1090 6 3.44E-03 94.9 2. 72E+OO T 0 724.04 16 11 2.30 1448.71 1445 7 4.31E-03 86.0 2.18E+OO T 0 727.29 22 25 1. 41 1455.21 1452 9 5.95E-03 94.0 2.17E+OO T 0 806.09 26 27 5.27 1612.85 1597 21 7.00E-03 **** 2. OlE+OO 0 902 .13 24 17 3.44 1804.99 1796 17 6.64E-03 89.0 l.84E+OO T 0 992.16 6 7 0.59 1985.10 1982 8 1. 78E-03 **** 1. 71E+OO 0 1004.93 15 3 1. 99 2010.65 2007 8 4.lOE-03 69.0 1. 69E+OO T 0 1011. 06 6 8 0.74 2022.90 2017 8 1. 7 3E-03 **** l.68E+OO 0 1218.96 10 16 0.54 2438.77 2431 12 2.80E-03 **** 1. 44E+OO 0 1238.47 23 11 0.87 2477.79 2472 11 6.67E-03 67.3 1.43E+OO T 0 1307.89 8 4 0.65 2616.65 2613 7 2.lSE-03 **** 1.36E+OO 0 1311. 09 6 2 0.98 2623.04 2620 7 1. 67E-03 **** 1.36E+OO T 0 1378.42 17 3 1. 37 2757.71 2751 14 4.98E-03 64.3 1. 30E+OO 0 1510.64 6 3 1. 33 3022 .13 3018 8 l.67E-03 **** 1. 20E+OO Flags: "T" = Tentatively associated Page 4173 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:19:26.49 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA].G405235055.CNF;l * *Acquisition date 3-0CT-2016 07:18:44 Sensitivity 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:59:00 Nuclide Library : SOLID *
  • Sample ID G405235055 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : l.4258E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA:GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 CD-109 SN-126 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 3.222E-01 4.574E-02 7.401E-01 4. 696E-02 2.019E+OO 3.059E-02 1. 457E-.Ol 3. 960E-02 4.942E-02 l.585E-01 4.942E-02 4.247E-01 4.942E-02 8.436E-02 8.436E-02 3. 960E-02 4.940E-02 8.436E-02 8.192E-01 4.940E-02 1.683E-01 8.192E-01 3.315E-02 1. 960E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4174 of 5809 Le (pCi/GRAM 1.177E+Ol 2. 716E-02 O.OOOE+OO 1.209E-02 2.422E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 l\S-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-.141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 4175of5809 3.790E-01 O.OOOE+OO 3.535E-02 5.lOOE-01 4.705E+00 3.515E-02 1. 2 61E-01 2.004E+00 6.282E+OO O.OOOE+OO 1.882E-01 O.OOOE+OO O.OOOE+OO 5.076E-01 6.128E+OO 6.882E-01 O.OOOE+OO 1.394E-01 4.260E+02 2.552E-02 7.275E-01 1. 891E+OO 1. 360E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.615E-02 5.423E-02 4.517E+OO 3.407E-01 3.407E-01 l.646E-02 9.371E-02 1.728E-01 O.OOOE+OO O.OOOE+OO l.054E-01 1.393E+OO 9.321E-02 2.361E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.821E-02 O.OOOE+OO 4.754E-02 l.109E-01 O.OOOE+OO O.OOOE+OO 2.710E-02 2.863E-02 9.467E-02 O.OOOE+OO O.OOOE+OO 2.256E+Ol O.OOOE+OO 2.999E-01 4.958E-02 4.302E+OO 3.515E-02 0.000E+OO 6.166E+02 O.OOOE+OO 2.043E-02 6.554E-02 1.302E-01 6.639E-02 8.808E-02 1.359E+OO 4.890E-02 1.359E+Ol l.844E-01 6.465E-02 l.709E-02 FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 PB-210 PB-211 BI.-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4176of5809 3.005E+OO 6.254E-01 2.053E+OO 2.943E+Ol 9.638E+Ol 3.718E-01 4.008E-02 2.020E+OO 6.221E-01 5.519E-01 3 .114E-01 4.550E-01 1.659E-01 1.659E-01 4.141E-01 4.227E-01 4.550E-01 4.609E-02 l.678E-01 3.489E+OO 4.609E-02 O.OOOE+OO 1.685E-01 2.530E+02 9.609E-02 7.493E-02 6.559E-02 2. 703E-'02 3.199E-02 9.317E-02 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:19:32.42 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235055.CNF;l * *Acquisition date 3-0CT-2016 07:18:44 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.58 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:59:00 Nuclide Library : SOLID *
  • Sample ID G405235055 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.4258E+02 GRAM *
  • Quantity Err(%) : 1.4027E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10: 31: 39 Eff.' Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.566E+Ol 1.828E+OO l.828E+OO MN-54 l.157E-01 9.643E-02 9.643E-02 CD-109 1.934E+OO 2.212E+OO 2.212E+OO SN-126 2.620E-01 l.395E-01 1.395E-01 HG-203 2.101E+OO 3.700E+OO 3.700E+OO TL-208 3.451E-01 7.779E-02 7.779E-02 BI-211 4.031E-01 9.814E-01 9.814E-01 PB-212 1.140E+OO l.365E-01 l.365E-01 BI-214 7.853E-01 1.795E-01 1. 795E-01 PB-214 1.081E+OO 2.078E-01 2.078E-01 RN-222 7.853E-01 1.795E-01 1. 795E-01 RA-224 1.519E+OO 1.501E+OO 1.501E+OO RA-226 7.853E-01 1. 795E-01 1.795E-01 AC-228 9.506E-01 3.023E-01 3.023E-01 RA-228 9.506E-01 3.023E-01 3.023E-01 TH-228 1.140E+OO 1.365E-01 1.365E-01 TH-230 7.851E-01 1.795E-01 1. 795E-01 TH-232 9.506E-01 3.023E-01 3.023E-01 TH-234 6.466E-01 1.815E+OO 1.815E+OO U-234 7.851E-01 1. 795E-01 1.795E-01 U-235 1.054E-01 l.840E-01 1.840E-01 U-238 6.466E-01 1.815E+OO 1.815E+OO AM-243 2.095E-01 8.608E-02 8.608E-02 ANH-511 1.076E-01 7.145E-02 7.145E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 2.135E+OO 1.313E+Ol 1.316E+Ol NOT IDENT. NA-22 . -7. 539E-03 3.370E-02 3.387E-02 NOT IDENT. NA-24 1.000E+41 2.584E+41 O.OOOE+OO SHORT HLIF AL-26 -2.270E-02 2.654E-02 2.844E-02 NOT IDENT. SC-46 -1.034E-01 3.187E-01 3.221E-01 FAIL ABUN V-48 5.826E+03 l.852E+04 1.870E+04 SHORT HLIF Page 4177 of 5809 CR-51 -2.688E+02 3.941E+02 4.123E+02 SHORT HLIF C0-56 -9.827E-02 4.747E-01 4.768E-01 FAIL ABUN MN-56 -l.OOOE+41 4.830E+41 0.000E+OO SHORT HLIF C0-57 -l.965E-02 4.153E-02 4.247E-02 NOT IDENT. C0-58 5.349E-01 5.414E-01 5.927E-01 NOT IDENT. FE-59 -2.997E+OO 6.043E+OO 6.192E+OO NOT IDENT. C0-60 5.845E-03 3.957E-02 3. 966E-02 NOT IDENT. ZN-65 -5.151E-02 1.780E-01 1. 795E-01 NOT IDENT. GE-68 8.335E-01 2.155E+OO 2.188E+OO NOT IDENT. AS-73 2.915E-01 6. 695E+OO 6.696E+OO NOT IDENT. AS-74 6.843E+03 6.483E+03 7.180E+03 SHORT HLIF SE-75 1.280E-01 2.109E-01 2.187E-01 FAIL ABUN BR-77 l.130E+39 9. 968E+39 O.OOOE+OO SHORT HLIF SR-82 -8.309E+Ol 5.781E+02 5.793E+02 SHORT HLIF RB-83 1.943E-01 5.519E-01 5.588E-01 NOT IDENT. KR-85 4.389E+OO 7 .101E+OO 7. 372E+OO NOT IDENT. SR-85 4.913E-01 7.977E-01 8.279E-01 NOT IDENT. RB-86 -1.047E+04 3.281E+04 3.315E+04 SHORT HLIF Y-88 5 .113E-02 l.433E-01 1.452E-01 NOT IDENT. Y-91 5.437E+Ol 4.841E+02 4.847E+02 NOT IDENT. NB-94 2.015E-03 2.978E-02 2.980E-02 NOT IDENT. NB-95 -7.864E-01 9.870E-01 1.049E+OO NOT IDENT. NB-95M 7.041E-01 2.338E+OO 2.359E+OO NOT IDENT. ZR-95 1.273E+OO 1.399E+OO l.512E+00 FAIL ABUN NB-97 1.000E+41 l.777E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1. 451E+41 0.000E+OO SHORT HLIF M0-99 8.174E+31 7.219E+32 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 7.433E+41 O.'OOOE+OO SHORT HLIF RH-101 -8.904E-03 3. 031E-02 3.057E-02 NOT IDENT. RH-102 2.331E-02 6.000E-02 6.091E-02 NOT IDENT. RU-103 -l.254E+OO 5.342E+OO 5. 372E+OO FAIL ABUN RH-106 -3.852E-01 4.636E-01 4. 951E-01 NOT IDENT. RU-106 -3.852E-01 4.636E-01 4.951E-01 NOT IDENT. AG-108M -1.872E-02 2.147E-02 2.307E-02 FAIL ABUN AG-llOM 7.178E-02 1. OOlE-01 1.052E-01 NOT IDENT. SN-113 -l.212E-01 2.079E-01 2.149E-01 NOT IDENT. CD-115 6.075E+38 l.703E+40 O.OOOE+OO SHORT HLIF SN-117M -3.391E+04 l.171E+05 l .181E+05 SHORT HLIF TE-123M -2. 961E-02 1.236E-01 l.243E-01 NOT IDENT. SB-124 -7. 72 9E-01 1. 972E+OO 2.002E+00 FAIL ABUN SB-125 3.077E-03 l.046E-01 l.046E-01 FAIL ABUN TE-125M 4.238E+Ol 2.604E+02 2. 611E+02 NOT IDENT. I-126 1.381E+06 l.108E+06 l.271E+06 SHORT HLIF SB-126 -9.968E+04 l.564E+06 1.565E+06 SHORT HLIF SB-127 -7.840E+21 5.693E+22 O.OOOE+OO SHORT HLIF I-131 6.016E+09 6.905E+09 7.418E+09 SHORT HLIF I-132 -1.000E+41 2.068E+42 O.OOOE+OO SHORT HLIF TE-132 3.828E+26 1. 266E+27 O.OOOE+OO SHORT HLIF BA-133 -7.207E-03 3.587E-02 3.601E-02 FAIL ABUN I-133 l.000E+41 2.903E+41 O.OOOE+OO SHORT HLIF CS-134 8.021E-02 7.564E-02 8.384E-02 FAIL ABUN CS-135 -8.247E-02 1.559E-01 1.603E-01 NOT IDENT. I-135 1.000E+41 7.480E+41 O.OOOE+OO SHORT HLIF CS-136 -4. 421E+04 3.943E+05 3.948E+05 SHORT HLIF BA-137M -1.994E-03 2.939E-02 2.940E-02 NOT IDENT. CS-137 -2.107E-03 3.105E-02 3.106E-02 NOT IDENT. CE-139 6.543E-02 l.040E-01 1.081E-01 NOT IDENT. BA-140 l.882E+06 1.698E+06 l.898E+06 SHORT HLIF LA-140 -4.197E+05 6.162E+05 6.446E+05 SHORT HLIF CE-141 -2.425E+Ol 2.764E+Ol 2.973E+Ol NOT IDENT. CE-143 1.000E+41 2.204E+42 O.OOOE+OO SHORT HLIF CE-144 7.253E-02 3.338E-01 3.354E-01 NOT IDENT. PM-144 2.415E-02 5.485E-02 5.592E-02 NOT IDENT. PR-144 2.030E+OO 4.768E+OO 4.855E+OO NOT IDENT. PM-146 -4.580E-04 3.984E-02 3.984E-02 NOT IDENT. ND-147 -7.527E+06 4.655E+07 4.667E+07 SHORT HLIF PM-147 -5.363E+Ol 6.984E+02 6.988E+02 NOT IDENT. PM-149 2. 313E+39 2.510E+41 O.OOOE+OO SHORT HLIF EU-150 -6.984E-03 2.588E-02 2.608E-02 FAIL ABUN EU-152 -5.224E-03 7.306E-02 7.310E-02 NOT IDENT. GD-153 -9.376E-02 1.650E-01 1.704E-01 NOT IDENT. EU-154 -1.843E-02 8.237E-02 8.279E-02 FAIL ABUN EU-155 4.286E-02 9.485E-02 9.680E-02 FAIL ABUN TB-160 -6.734E-02 1.655E+OO 1.656E+OO FAIL ABUN H0-166M -5.234E-03 5.855E-02 5.860E-02 FAIL ABUN TM-171 -7. 729E-01 1.458E+Ol 1.458E+Ol NOT IDENT. HF-172 -3.845E-02 2 .112E-01 2 .119E-01 FAIL ABUN LU-172 4.600E-02 6.625E-02 6.942E-02 FAIL ABUN Page 4178 of 5809 LU-176 -1.423E-02 2.275E-02 2.364E-02 FAIL ABUN HF-181 -3.849E+00 4. 021E+OO 4.379E+OO NOT IDENT. TA-182 5. 096E-02 8.lOlE-01 8.104E-01 FAIL ABUN RE-183, -1.584E-01 2.217E+OO 2.218E+OO NOT IDENT. RE-184 7.182E+Ol 6.503E+Ol 7.265E+Ol FAIL ABUN W-188 4.864E+Ol l.192E+02 1.212E+02 FAIL ABUN IR-192 -9.828E-02 4.658E-01 4.679E-01 FAIL ABUN BI-207 2.538E-02 4.150E-02 4.305E-02 FAIL ABUN PB-210 -l.565E-01 2.157E+OO 2.158E+OO NOT IDENT. PB-211 4.857E-01 7.076E-01 7.407E-Ql NOT IDENT. BI-212 7.973E-01 7.354E-Ol 8.185E-01 FAIL ABUN RN-219 -2.008E-01 3.714E-01 3.822E-01 FAIL ABUN RA-223 3.371E-03 5.541E-01 5.541E-01 FAIL ABUN AC-227 -4.685E-02 2.039E-01 2.050E-01 FAIL ABUN TH-227 -4.685E-02 2.039E-01 2.050E-01 FAIL ABUN TH-229 2.503E-01 4.607E-01 4.744E-01 FAIL ABUN PA-231 4.614E-01 4. 721E-01 5.159E-01 NOT IDENT. TH-231 3. 371E-03 5.541E-01 5.541E-01 FAIL ABUN PA-233 -4.883E-03 5.664E-02 5.668E-02 FAIL ABUN PA-234 -7.978E-02 2.423E-01 2.450E-01 NOT IDENT. PA-234M 2.193E-01 4.447E+OO 4.448E+OO NOT IDENT. NP-237 -4.883E-03 5.664E-02 5.668E-02 FAIL ABUN NP-238 1.000E+41 4.420E+41 O.OOOE+OO SHORT HLIF NP-239 -l.615E-01 2.040E-01 2.166E-01 FAIL ABUN PU-239 8.953E+Ol 2.788E+02 2.817E+02 NOT IDENT. AM-241 2.645E-02 l.015E-01 1.022E-01 NOT IDENT. CM-243 -7.247E-02 8. 941E-02 9.519E-02 FAIL ABUN BK-247 4.946E-02 , 7. 381E-02 7.710E-02 NOT IDENT. CM-247 -3.300E-02 3.440E-02 3.748E-02 FAIL ABUN CF-249 8.827E-03 3.478E-02 3.501E-02 NOT IDENT. CF-251 1.028E-01 9.869E-02 1.090E-01 NOT IDENT. Page 4179 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 55.4826 87.09 69.5624 136.47 58.4507 45.60 62.6247 87.57 69.6319 140.51 0.0000 46.54 66.2062 88.03 69.6979 143.76 76.7111 49.72 0.0000 88.34 69.7420 144.24 68.4663 51. 35 63.7357 88.47 69.7606 145.44 99.7617 51.87 62.9705 89. 96 69.9729 152.43 72. 4218 52.39 68.2495 1093.63 70.0689 153.25 0.0000 52.97 56.2492 91.11 0.0000 323.87 53.6622 53.44 72.7896 92.59 70.3432 156.02 0.0000 54.07 83.3379 93.35 70.4488 158.56 0.0000 57.36 0.0000 94.56 70.6171 159.00 67.7861 57.53 83.2703 94.65 70.6295 162.33 67.0279 57.98 67.5750 94.67 70.6323 162.66 0.0000 59.27 81.9015 94.87 70.6600 163.33 71. 3787 59.32 81.9125 97.43 80.6072 165.86 56.6538 59.54 71.3851 98.43 64. 0961 176.31 72. 5922 60. 96 76.6674 98.44 64.0976 176.60 0.0000 61.17 76.7098 99.53 86.7110 177.52 43.4045 62.93 80.0254 100 .11 91.6283 181.07 0.0000 63.29 80.0996 102.03 72.5985 181.52 59.9800 63.58 80.1590 103.18 91.1837 184.41 67.1245 64.28 80.3023 103.37 87.3344 143.76 66.8667 66.73 76.6081 105.21 68.1559 193.51 63.0683 67.24 88.9891 105.31 68.1682 197.03 47.7746 125.81 87.2861 106.12 69.2439 198.01 67.8506 67.75 89.1009 106.47 79.0466 201.83 53.6257 69.67 63.8988 109.28 71.5982 203.43 66.0356 70.83 91. 8828 111. 00 76.7348 205.31 68.7941 72.81 78.3443 111.76 0.0000 210.85 51.1639 72.87 78.3555 114.06 70.2205 215.65 53.3261 74.66 78.6809 116. 30 0.0000 222 .11 65.1243 74.82 78.7098 116.74 72.5294 227.09 39.0515 74.97 78.7373 119.76 61.9134 227.38 37.9146 77 .11 79.1205 121.12 63.0538 228.16 0.0000 78.74 79.4092 121. 22 63.0639 228.18 45.9955 79.69 86.3614 121. 7 8 70.1357 116.74 45.9955 80.12 81. 5037 122.06 70.1682 235.69 44.8086 80.19 0.0000 122.92 64.2441 235. 96 52.5488 80.57 74.1675 123.07 64.2598 238.63 51.1422 81. 00 70.5252 265.00 64.3237 238.98 0.0000 81. 07 70.5356 125.81 76.6477 240.99 51. 2637 81. 75 79.3151 127.23 75.8108 242.00 51. 3154 83.79 69.0826 127.91 75.8932 244.70 38.9806 84.00 69 .1130 129.30 70.9891 252.40 0.0000 85.43 69.3219 131.20 73.2360 252.80 43. 6134 86.55 69.4845 133.02 57.1228 254.15 0.0000 86.79 69.5190 133.52 71. 4580 256.23 42.5753 86.94 69.5410 136.00 62.5079 260.90 0.0000 Page 4180of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 40.5327 355.39 0.0000 584.27 28.6023 264.80 40.5379 356.01 28.3063 595.83 0.0000 265.00 42.9313 364.49 0.0000 427.87 20.8821 268.22 57.4131 366.42 0.0000 602.52 0.0000 269.46 39.9160 372. 51 27.7839 604.72 23.9141 270.03 33.5474 375.05 35.6631 607.14 19.4540 271.23 33.5841 377.52 38.3407 609.32 19.9740 273.65 0.0000 356.01 34.1369 610.33 19.9837 276.40 40.9737 388.16 31.6069 614.28 19.5222 277.37 41.0100 388.63 0.0000 618.01 14.0410 277.60 41.0183 391.69 33.4448 620.36 11. 0452 278.00 41. 0339 264.66 30.1097 621. 93 24 .1162 279.20 41. 0775 401.81 40.7694 630.19 0.0000 279.54 41.0909 402.40 44.3319 631.29 20.1880 279.70 41. 0961 404.85 29.3080 633.25 31.3204 280.46 37.0924 410.95 20.0652 634.78 0.0000 283.69 33. 9652 413.71 25.4628 635.95 23.2677 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.0919 423. 72 0.0000 645.85 18.2944 285.90 0.0000 427.09 32.4478 657.76 16.3522 287.50 36.5140 427.87 34.2682 657.90 0.0000 290.67 35.8019 433.94 25.3494 661.66 12.2861 293.27 0.0000 439.40 34.5225 664.57 0.0000 351. 93 '35.5349 453.88 26.5869 666.33 0.0000 295. 96 35.5579 463.37 16.5989 666.50 0.0000 879.38 44.2408 468.07 16.6465 667.71 0.0000 299.98 42.6531 473.00 0.0000 677.62 14.4386 300.09 42.6563 475.06 26.0039 685.70 0.0000 300.13 42.6584 476.78 32.5384 695.00 0.0000 301.36 40.6498 477.60 27.9034 696.49 18.7207 302.85 42.7568 482.18 27.0471 696. 51 18.7214 256.23 37.8766 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.9707 306.78 40.8361 497.08 21. 6388 697.49 23.9321 308.46 42.1327 505.52 18.4348 702.65 19.8149 311. 90 37.2830 507.63 0.0000 706.68 21.9391 316.51 37.4240 511. 00 19.9146 711. 68 23.0339 319.41 0.0000 514.00 22.7979 720. 70 0.0000 320.08 0.0000 514.00 22.7979 721. 93 0.0000 321. 04 28.3811 520.40 15.2533 722. 78 17.3580 323.87 35.1384 520.69 0.0000 722. 91 17.3594 325.23 37.6895 522.65 0.0000 723. 31 11. 0486 328.76 0.0000 527.90 0.0000 724 .19 9.4739 333.37 34.1406 528.26 19.1496 727.33 22.1356 333.97 43.0126 529.59 18.2060 733.00 21. 5546 334.37 41. 7606 529.87 0.0000 735.93 20.1001 338.28 40.6191 531.02 0.0000 333.97 17.9961 338.32 40.6201 537.26 0.0000 739.50 0.0000 311. 90 25.4303 546.56 0.0000 747.24 17.0072 340.48 25.4303 552.55 18.4325 748.06 19 .1396 340.55 0.0000 563.25 22.4394 752.31 19.1733 344.28 28.0552 569.33 21. 5318 753.82 0.0000 345.93 26.8140 946.00 20.5557 756.73 10. 6714 351. 06 33.3284 569.70 17.6206 756.80 10. 6718 351.93 33.3506 583.19 28.5858 884.68 21. 4063 Page 4181of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 31. 0627 1274.44 6.9924 1620.50 6.1919 766.42 31.0709 1001.03 15.4075 1621. 92 7.2264 766.84 22.5031 1002.74 11.2117 1678.03 0.0000 772. 60 0.0000 1004.73 12.8548 1690.97 5.2386 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 J.025.87 0.0000 1764.49 6 .,8 08 6 778.90 10.7682 1028.54 0.0000 1063.66 3.1952 783.70 0.0000 1037.84 15.0597 1771. 35 3.1959 785.37 8.6370 1038.76 0.0000 1791.20 0.0000 792.07 9.7427 631.29 13.3255 1808.65 5.3665 794.95 11. 37 97 1048.07 0.0000 1810.72 0.0000 795.86 11. 3835 1049.04 17.7808 1836.06 1. 0792 810.06 4.9059 1050.41 12.4517 810.29 3. 2710 1063.66 8.9313 344.28 3.2711 1077.00 0.0000 810.76 6.5432 1077.34 10.7629 815.77 0.0000 1085.87 16.1873 1048.07 0.0000 1093.63 8 .112 9 832.01 18.1415 1099.45 12.6422 834.85 . 13.2085 1112. 07 11. 7844 835. 71 13.2129 1112. 84 13.6002 836.80 0.0000 1115. 54 14.5186 846.75 0.0000 1120.29 12.7217 846'.77 16.5851 1120.55 12.7225 856.80 0.0000 1221.41 10.1808 860.56 13.3369 1129. 67 16.4026 871.09 15.6201 1131.51 0.0000 873.19 16.7487 1147.95 0.0000 875.33 0.0000 1173.23 19.3812 879.38 11.1914 1177.95 10.1655 880.51 12.3155 1189.05 12.9797 883.24 15. 6896 1204.77 11.1746 884.68 11.2130 1221. 41 8.9813 889.28 11. 2317 1231. 02 15.0088 894.76 8.4402 1235.36 0.0000 898.04 13.5205 1238.28 15.0391 900. 72 15.7893 1260.41 0.0000 903.28 15.8035 1271.87 9.4855 911.20 10.1880 1274.44 7.5938 912.08 10.1913 1274.54 7.5938 923.98 0.0000 1291.59 11.4426 926.50 12. 5196 1298.22 0.0000 929.11 15.9482 1312 .11 0.0000 937.49 14.8525 1332.49 8.6743 944 .13 0.0000 1362.66 0.0000 946.00 11. 4583 1365.19 4. 8596 949.00 14. 9112 1368.63 0.0000 667.71 0.0000 1384.29 3.1250 962. 31 19.5885 1408.01 7.8589 964. 08 19.0237 1457.56 0.0000 966 .17 15.5759 1460.82 11. 9407 911.20 15.0127 1489.16 2.0034 968. 97 15.0127 1505.03 9.3840 983.53 0.0000 1584.12 3.0712 984.45 0.0000 1596.21 0.0000 Page 4182 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:51:13.42 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM01.CNF;402 Background date : Z-OCT-2016 10:59:55. Sample date 2-DEC-2015 14:50:00. Acquisition date : 3-0CT-2016 07:50:44. Sample ID G405235056 Sample quantity 1.01481E+02 GRAM Detector name : GAMOl Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.36 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 4 4 4 4 0 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4183 of 5809 Energy 63.24* 74.92 77.27* 84.19* 87.35 89.92 92.69* 118. 8 9 129.46 185.72* 209.81 238.68* 241.62* 270.14 277.36 295.66* 301.88 329.38 338.46*

352.05* 402.08 435.49 463.09 510.91* 565.33* 583.25* 609.44* 661.77 719. 57 770.32 786.97 795.19 879.40 883.43 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 29 119 187 37 99 67 115 25 46 105 34 358 99 34 32 115 25 16 66 246 50 11 23 39 50 89 193 51 23 30 8 13 9 4 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 118 129 109 167 142 131 96 73 109 107 104 58 93 63 43 98 73 72 65 60 95 33 19 46 27 24 19 24 9 30 16 15 4 9 1.18 1. 09 1.17 1. 77 1. 64 1. 63 1. 25 0.89 1. 07 1. 62 0. 96 1. 03 2 .17 1.11 0.69 1.19 3.81 1. 44 1. 04 1. 38 8.98 1. 25 1. 49 2.44 5.07 1. 47 1. 39 1. 07 2.59 4.46 0.88 1. 42 0.96 0.53 127.18 150.53 155.24 169.08 175.39 180.54 186.07 238.46 259.61 372 .12 420.28 478.02 483.90 540.93 555.37 591. 97 604.41 659.39 677.55 704.73 804.77 871.57 926.77 1022.39 1131.21 1167. 05 1219.40 1324.04 1439.62 1541.09 1574.38 1590.81 1759.18 1767.23 124 147 147 164 164 164 164 235 256 365 415 474 474 535 552 585 598 651 672 700 790 865 922 1014 1122 1160 1215 1321 1435 1530 1568 1585 1756 1762 8 8.09E-03 70.2 15 3.30E-02 18.0 15 5.20E-02 12.3 31 1.02E-02 68.8 31 2.76E-02 24.7 31 l.87E-02 37.0 31 3.20E-02 19.9 7 6. 90E-03 61. 0 10 1.28E-02 44.8 13 2.91E-02 23.7 10 9.49E-03 59.0 19 9.95E-02 6.3 19 2. 74E-02 31. 0 10 9.46E-03 46.7 8 8.81E-03 40.2 13 3.20E-02 20.2 12 6.95E-03 71.8 12 4.33E-03111.9 11 1.82E-02 27.5 12 6.82E-02 9.2 26 1.40E-02 55.5 10 2.92E-03106.2 8 6.31E-03 39.9 17 1.07E-02 49.4 18 1.40E-02 28.9 14 2.48E-02 16.2 12 5.36E-02 8.7 9 1. 41E-02 22. 5 11 6.47E-03 31. 7 21 8.25E-03 50.5 8 2.22E-03 93.5 10 3.61E-03 62.3 7 2.36E-03 50.1 7 1.12E-03131.8 Fit 6.86E-01 1.36E+OO 6.39E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235056 Acquisition date 3-0CT-2016 07:50:44 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911. 67* 63 20 1. 42 1823.70. 1819 13 1.76E-02 20.9 36 0 920.31 9 13 0.94 1840.98 1833 11 2.37E-03 90.5 37. 0 9 12 1. 26 1847.74 1843 83.7 38 0 969 .18 37 12 1.19 1938.68 1935 10 l.03E-02 24.1 39 0 1043.52 9 5 1. 47 2087.31 2081 10 2.58E-03 55.4 40 0 1109.70 18 3 3.67 2219.61 2214 11 5.08E-03 29.2 41 0 1120.23* 28 18 1. 84 2240.67 2236 10 7.86E-03 33.8 42 0 1225.45 6 12 0.50 2451. 03 2447 8 l.59E-03113.3 43 0 1266.62 6 4 0.89 2533.33 2530 6 1. 78E-03 63.9 44 0 1275.23 5 7 1. 39 2550.54 2543 10 1. 2 6E-03122 .1 45 0 1378.12 16 5 0.54 2756.24 2751 10 4.55E-03 35.3 46 0 1460.75* 288 0 1. 63 2921. 40 2914 14 7.99E-02 6.0 47 0 1589.26 8 1 1. 39 3178.30 3175 6 2.lOE-03 44.4 48 0 1764.50* 30 7 1. 53 3528.60 3522 10 8.19E-03 26.0 49 0 1799.81 6 0 0.99 3599.17 3596 6 1.67E-03 40.8 Flag: "*" == Peak area was modified by background subtraction Page 4184of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:51:15 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 14:50:00 Acquisition date : 3-0CT-2016 07:50:44 G405235056 Sample quantity 101.48 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID Sample geometry GAMMAl Detector geometry: 0 01:00:00.00 Elapsed real time: 1.50 keV Half life ratio No Linear 75.00 Systematic Error Efficiencies at Interfering Interfered ------------------------------------Nuclide Line Nuclide Line PB-214 242.00 RA-224 240.99 PB-214 87.09 SN-126 86.94 PB-214 87.09 SN-126 87.57 PB-214 87.09 CD-109 88.03 PB-214 87.09 TH-229 88.47 PB-214 74.82 AM-243 74.66 PB-214 74.82 TH-228 74.82 PB-214 74.82 PB-212 74.82 PB-214 351.93 BI-211 351.06 Page 4185 of 5809 CAN 0 01:00:00.36 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235056 Acquisition date 3-0CT-2016 07:50:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status NA-22 1274.54 99.94* 1.095E+OO 2 .* 878E-02 3. 596E-02 244.20 OK K-40 1460.82 10.66* 9.709E-01 1.922E+Ol 1. 922E+Ol 11. 93 OK CD-109 88.03 3.70* 4.590E+OO 3.160E+OO 5.003E+OO 67.98 OK SN-126 64.28 9.60 2.294E+OO 9.696E-01 9.696E-01 140.35 OK 86.94 8.90 4.590E+OO 1.314E+OO 1.314E+OO 67.98 OK 87.57 37.00* 4.590E+OO 3.160E-01 3.160E-01 67.98 OK BA-137M 661.66 89.90* 1.883E+OO 2 .112E-01 2.154E-01 44.91 OK CS-137 661.66 85.10* 1.883E+OO 2.232E-01 2.275E-01 44.91 OK TL-208 277.37 6.60 3.944E+OO 8.703E-01 8.703E-01 80.47 OK 583.19 85.00* 2.090E+OO 3.536E-01 3.536E-01 32.35 OK 860.56 12.50 1. 520E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.328E+OO Line Not Found Absent 351.06 12.92* 3.215E+OO 9.152E-01 9.152E-01 167.70 OK PB-212 74.82 10.28 3.532E+OO 1.722E+OO 1.722E+OO 52.62 OK 77 .11 17.10 3.757E+OO 2 .130E+OO 2 .130E+OO 24.57 OK 238.63 43.60* 4.454E+OO l.321E+00 l.321E+00 12.53 OK 300.09 3.30 3.690E+OO Line Not Found Absent BI-214 609.32 45.49* 2.015E+OO l.479E+00 1.480E+OO 17.43 OK 1120.29 14.92 l.223E+00 1.078E+OO 1.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+OO 1.638E+OO 52.01 OK PB-214 74.82 5.80 3.522E+OO Line Not Found <<INT Reject 77 .11 9.70 3.757E+00 3.755E+OO 3.757E+OO 24.57 OK 87.09 3.41 4. 572E+OO Line Not Found <<INT Reject 242.00 7.25 4.406E+00 Line Not Found <<INT Reject 295.22 18.42 3.737E+OO 1.193E+OO 1.193E+OO 40.38 OK 351.93 35.60* 3.216E+OO Line Not Found <<INT Reject RN-219 271.23 10.80 4. 031E+OO 5.586E-01 5.586E-01 93.47 OK 401.81 6.60* 2.865E+OO 1.886E+OO 1.886E+OO 110. 94 OK RN-222 609.32 45.49* 2.015E+00 1.479E+OO 1. 480E+OO 17.43 OK 1120.29 14.92 1.223E+OO 1.078E+00 1.078E+OO 67.61 OK 1764.49 15.30 8.116E-01 1.637E+OO 1.638E+OO 52.01 OK RA-224 240.99 4.10* 4. 411E+00 1.794E+OO 1. 794E+OO 143 .11 OK RA-226 609.32 45.49* 2.015E+00 1.479E+OO 1.480E+OO 17.43 OK 1120.29 14.92 1.223E+OO 1.078E+OO 1.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+OO 1.638E+OO 52.01 OK AC-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.327E+00 1.243E+OO 1.243E+00 54.91 OK 794.95 4.25 1. 621E+OO 1. 321E+OO 1.321E+OO 124.51 OK 835. 71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1.450E+OO 1.181E+OO 1.181E+OO 41. 80 OK 968.97 15.80 1.379E+OO 1.190E+OO 1.190E+00 48.16 OK RA-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11.27 3.327E+OO 1.243E+OO 1.243E+OO 54.91 OK 794.95 4.25 1.621E+OO 1. 321E+OO 1.321E+OO 124.51 OK 835.71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1.450E+OO 1.181E+OO 1.181E+OO 41. 80 OK 968. 97 15.80 1. 379E+OO 1.190E+00 1.190E+OO 48.16 OK TH-228 74.82 10.28 3.532E+OO 1.722E+OO 1.722E+OO 52.62 OK 77 .11 17.10 3.757E+OO 2.130E+OO 2.130E+OO 24.57 OK Page 4186 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235056 Acquisition date 3-0CT-2016 07:50:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 238.63 43.60* 4.454E+OO 1.321E+OO l.321E+OO OK 300.09 3.30 3.690E+OO Line Not Found Absent TH-229 85.43 14.70 4.354E+OO 4.200E-01 4.200E-01 137.59 OK 88.47 24.00 4.590E+OO 4. 872E-01 4.873E-01 67.98 OK 193.51 4.41* 5.168E+OO Line Not Found Absent 210.85 2.80 4.899E+OO 1. 787E+OO 1.787E+OO 118. 06 OK TH-230 609.32 45.49* 2.015E+OO 1.479E+OO l.480E+OO 17.43 OK 1120.29 14.92 1.223E+OO 1.078E+OO 1.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+OO 1.637E+OO 52.01 OK PA-231 283.69 1. 70 3.870E+OO Line Not Found Absent 301.36 5.35* 3. 671E+OO 9.078E-01 9.078E-01 143.69 OK TH-232 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.327E+OO 1.243E+OO 1.243E+OO 54.91 OK 835. 71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1.450E+OO 1.181E+OO l.181E+OO 41. 80 OK 968. 97 15.80 1. 379E+OO 1.190E+OO 1.190E+OO 48.16 OK TH-234 63.29 3.70* 2.294E+OO 2.516E+OO 2.516E+OO 140.35 OK 92.59 4.23 4.940E+OO 4.012E+OO 4.012E+OO 39.80 OK U-234 609.32 45.49* 2.015E+OO 1.479E+OO 1.479E+OO 17. 43 OK 1120.29 14.92 1.223E+OO 1.078E+OO 1.078E+OO 67.61 OK 1764.49 15.30 8 .116E-01 1.637E+OO 1.637E+00 52.01 OK U-235 89. 96 3.47 4.767E+OO 2. 967E+OO 2.967E+OO 73.97 OK 93.35 5.60 4.940E+OO 3.031E+OO 3. 031E+OO 39.80 OK 143.76 10. 96* 5.868E+OO Line Not Found Absent 163.33 5.08 5.647E+OO Line Not Found Absent 185. 72 57.20 5.297E+OO 2.485E-01 2.485E-01 47.46 OK 205.31 5.01 4.973E+OO Line Not Found Absent U-238 63. 29 3.70* 2.294E+OO 2.516E+OO 2.516E+OO 140.35 OK 92.59 4.23 4.940E+OO 4.012E+OO 4.012E+OO 39.80 OK AM-243 43.53 5.90 3.822E-01 Line Not Found Absent 74.66 67.20* 3.532E+OO 2.634E-01 2.634E-01 52.62 OK CM-247 278.00 3.40 3.944E+OO l.689E+OO 1.689E+OO 80.47 OK 287.50 2.00 3.826E+OO Line Not Found Absent 402.40 72.00* 2.865E+OO l.729E-01 1. 729E-01 110. 94 OK ANH-511 511. 00 100.00* 2.335E+OO 1.168E-01 l.168E-01 98.90 OK Flag: "*" = Keyline Page 4187of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:51:16.73 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l * *Acquisition date 3-0CT-2016 07:50:44 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.36 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:50:00 Analyst initials: MXRl *
  • Sample ID G405235056 Sample Quantity 1.0148E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) NA-22 3. 596E-02 8.607E-02 K-40 1.922E+Ol 2.247E+OO CD-109 5.003E+OO 3.333E+00 SN-126 3.160E-01 2.105E-01 BA-137M 2.154E-01 9.478E-02 CS-137 2.275E-01 l.OOlE-01 TL-208 3.536E-01 1.121E-01 BI-211 9.152E-01 l.504E+OO PB-212 l.321E+OO l.622E-01 BI-214 1.480E+OO 2.528E-01 PB-214 1.526E+OO 2.742E-01 RN-219 1.886E+OO 2.050E+OO RN-222 l.480E+OO 2.528E-01 RA-224 1.794E+OO 2.516E+OO RA-226 1.480E+OO 2.528E-01 AC-228 1.181E+OO 4.839E-01 RA-228 1.181E+OO 4.839E-01 TH-228 1.321E+OO l.622E-01 TH-229 -7.270E-01 7.080E-01 TH-230 1.480E+OO 2.527E-01 PA-231 9.078E-01 1.278E+OO TH-232 1.181E+OO 4.839E-01 TH-234 2.516E+OO 3.460E+OO U-234 1.479E+OO 2.527E-01 U-235 l.323E-03 2.863E_.:01 U-238 2.516E+OO 3.460E+OO AM-243 2.634E-01 l.358E-01 CM-247 l.729E-01 l.879E:..._01 ANH-511 l.168E-01 l.132E-01 Non-Identified Nuclides Nuclide BE-7 Page 4188 of 5809 Key-Line Activity (pCi/GRAM -8.317E+OO K.L. Cnt Uncert ( 1. 96-sigma) 1. 757E+Ol MDA (pCi/GRAM l.623E-01 9.665E-01 2.829E+OO 1. 799E-01 8.188E-02 8.650E-02 8.415E-02 5.541E-01 l.463E-01 l.585E-01 5.099E-01 1.157E+OO l.585E-01 1.569E+OO l.585E-01 4.780E-01 4.780E-01 l.463E-01 1.211E+OO l.584E-01 1.149E+OO 4.780E-01 4.004E+OO 1.584E-01 5.332E-01 4.004E+OO l.527E-01 1.062E-01 7.738E-02 MDA (pCi/GRAM 3.114E+Ol NOT IDENT.

NA-24 O.OOOE+OO 1.638E+41 0.000E+OO SHORT HLIF AL-26 -8.408E-03 4.021E-02 8.619E-02 NOT IDENT. SC-46 -2.005E-01 4.825E-01 8.570E-01 FAIL ABUN V-48 O.OOOE+OO 2. 715E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 7.276E+02 O.OOOE+OO SHORT HLIF MN-54 2.357E-02 9.243E-02 l.838E-01 NOT IDENT. C0-56 -1.269E-01 7.765E-01 1.424E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 5.378E-02 7.240E-02 1.319E-01 NOT IDENT. C0-5.8 -5.712E-01 9.971E-01 1 . .685E+OO NOT IDENT. FE-59 -3.805E+00 1.249E+Ol 2.198E+Ol NOT IDENT. C0-60 4. 963E-02 6.260E-02 l.449E-01 NOT IDENT. ZN-65 -2.445E-01 3.013E-01 3.769E-01 NOT IDENT. GE-68 -l.554E+00 3.948E+OO 6.833E+OO NOT IDENT. AS-73 1.065E+OO l.931E+Ol 3.355E+Ol NOT IDENT. AS-74 O.OOOE+OO l.161E+04 O.OOOE+OO SHORT HLIF SE-75 4.107E-01 3.104E-01 6.141E-01 FAIL ABUN BR-77 O.OOOE+OO 1. 621E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 1.439E+03 O.OOOE+OO SHORT HLIF RB-83 2.602E-01 9.162E-01 1.828E+OO NOT IDENT. KR-85 3.894E+OO 1.076E+Ol 1.932E+Ol NOT IDENT. SR-85 4.377E-01 l.210E+OO 2.172E+OO NOT IDENT. RB-86 O.OOOE+OO 5.748E+04 O.OOOE+OO SHORT HLIF Y-88 -6. 096E-02 3.556E-01 7.446E-01 NOT IDENT. Y-91 -7.074E+02 8.861E+02 l.537E+03 NOT IDENT. NB-94 5.150E-03 4.562E-02 8.771E-02 NOT IDENT. NB-95 -8.782E-01 1. 565E+OO 2.279E+OO NOT IDENT. NB-95M -l.423E+OO 4.446E+OO 7.129E+OO NOT IDENT. ZR-95 4.433E-01 2.447E+OO 4. 714E+OO NOT IDENT. NB-97 O.OOOE+OO l.436E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.223E+33 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.657E+41 O.OOOE+OO SHORT HLIF RH-101 -2.685E-02 5.212E-02 8.382E-02 NOT IDENT. RH-102 -2.462E-02 9.129E-02 l.650E-01 NOT IDENT. RU-103 -1.435E-01 9.725E+OO l.824E+Ol FAIL ABUN RH-106 8.675E-02 7.708E-01 1. 479E+OO NOT IDENT. RU-106 8.675E-02 7.708E-01 1. 479E+OO NOT IDENT. AG-108M 3.834E-02 4.025E-02 8.450E-02 NOT IDENT. AG-110M 6.092E-02 1. 573E-01 3 .112E-01 FAIL ABUN SN-113 7.437E-02 3.723E-01 6.830E-01 NOT IDENT. CD-115 O.OOOE+OO 2.779E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 1.803E+05 O.OOOE+OO SHORT HLIF TE-123M 6.262E-02 1.880E-01 3.603E-01 NOT IDENT. SB-124 2.949E+OO 2.653E+OO 7.907E+OO NOT IDENT. SB-125 7.366E-02 1. 513E-01 3.017E-01 FAIL ABUN TE-125M 2.398E+02 5.144E+02 9.023E+02 NOT IDENT. I-126 O.OOOE+OO 2.205E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 3.043E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 9.620E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.308E+l0 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.284E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.104E+27 O.OOOE+OO SHORT HLIF BA-133 -2.190E-02 7.246E-02 l.157E-01 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 8.693E-02 1. 061E-01 1.698E-01 FAIL ABUN CS-135 2.504E-02 2.262E-01 3.838E-01 NOT IDENT. I-135 O.OOOE+OO 8.597E+40 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.883E+05 O.OOOE+OO SHORT HLIF CE-139 -4.365E-03 1.647E-01 3.064E-01 NOT IDENT. BA-140 O.OOOE+OO 2.606E+06 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 8.560E+05 O.OOOE+OO SHORT HLIF CE-141 5.775E+00 4.223E+Ol 7.912E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -2.250E-01 5.813E-01 9.450E-01 NOT IDENT. PM-144 -l.405E-02 9.562E-02 l.735E-01 NOT IDENT. PR-144 -l.173E+OO 8.339E+OO l.515E+Ol NOT IDENT. PM-146 -5.622E-02 7.224E-02 l.217E-01 NOT IDENT. ND-147 O.OOOE+OO 7.615E+07 O.OOOE+OO SHORT HLIF PM-147 6. 631E+02 1.236E+03 2.213E+03 NOT IDENT. PM-149 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 l.302E-02 4.168E-02 7.271E-02 FAIL ABUN EU-152 -4.123E-02 1.359E-01 2.460E-01 NOT IDENT. GD-153 -3.395E-02 3.lOlE-01 4.791E-01 NOT IDENT. EU-154 8.791E-02 2.104E-01 3.576E-01 FAIL ABUN EU-155 8.291E-02 1.812E-01 3.193E-01 FAIL ABUN TB-160 2.476E+00 2.431E+OO 5.699E+OO FAIL ABUN H0-166M -1.346E-02 8.706E-02 1.598E-01 FAIL ABUN Page 4189 of 5809 TM-171 -2.061E+OO 4.545E+Ol 7.822E+Ol NOT IDENT. HF-172 2.944E-01 3.454E-01 6.337E-01 FAIL ABUN LU-172 -2.267E-02 1.069E-01 . 1. 962E-01 FAIL ABUN LU-176 -1. 540E-02 3.814E-02 6.0SOE-02 FAIL ABUN HF-181 3.098E+OO 6.816E+00 1.368E+Ol NOT IDENT. TA-182 -4.430E-01 1.488E+OO 2.471E+OO FAIL ABUN RE-183 -4.553E-01 6.173E+OO 1.058E+Ol NOT IDENT. RE-184 8.850E+OO 4.939E+Ol 9.761E+Ol NOT IDENT. W-188 -5.362E+Ol l.982E+02 3.199E+02 FAIL ABUN IR-192. 2.829E-01 7.398E-01 1.43.1._E+OO FAIL ABUN HG-203 -3.501E+OO 4.243E+OO 6.329E+OO NOT IDENT. BI-207 1. 941E-02 8.051E-02 1.573E-01 FAIL ABUN PB-210 -2.426E+OO 7.363E+OO l.260E+Ol NOT IDENT. PB-211 -6.006E-01 1.022E+OO 1. 778E+OO NOT IDENT. BI-212 1.071E+OO 8.800E-01 1.856E+OO NOT IDENT. RA-223 -l.870E-01 8.835E-01 l.445E+OO FAIL ABUN AC-227 -8.628E-02 3.606E-01 6.548E-01 NOT IDENT. TH-227 -8.628E-02 3.606E-01 6.548E-01 NOT IDENT. TH-231 -1.870E-01 8.835E-01 l.445E+00 FAIL ABUN PA-233 -2.617E-02 9.190E-02 l.663E-01 NOT IDENT. PA-234 -4.521E-01 4. SllE-01 6.750E-01 FAIL ABUN PA-234M 1. lllE-01 8.053E+OO 1.541E+Ol NOT IDENT. NP-237 -2.617E-02 9 .190E-02 1.663E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 -8.382E-03 4.284E-01 6.651E-01 FAIL ABUN PU-239 8.918E+02 7.830E+02 9.430E+02 FAIL ABUN AM-241 -8.625E-02 2.930E-01 4.494E-01 NOT IDENT. CM-243 -5.985E-02 l.650E-01 2.708E-01 FAIL ABUN BK-247 8.175E-02 1.086E-01 2.007E-01 FAIL ABUN CF-249 l.794E-02 5.157E-02 1.014E-01 NOT IDENT. CF-251 1.485E-01 l.675E-01 3. 313E-01 NOT IDENT. Page 4190of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:51:14.24 Nuclide Line Activity Report Nuclide Type:

  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error NA-22 1274.54 4 99.94* 1.095E+OO 2.878E-02 3. 596E-02 244.20 K-40 1460.82 269 10.66* 9.709E-01 1.922E+Ol 1.922E+Ol 11. 93 CD-109 88.03 98 3.70* 4.590E+OO 4.260E+OO 6.743E+OO 49.35 SN-126 64.28 29 9.60 2.294E+OO 9. 696E-01 9.696E-01 140.35 86.94 98 8.90 4.590E+OO 1.771E+OO 1. 771E+OO 49.35 87.57 98 37.00* 4.590E+OO 4.260E-01 4.260E-01 49.35 BA-137M 661. 66 48 89.90* 1.883E+OO 2.112E-01 2.154E-01 44.91 CS-137 661. 66 48 85.10* l.883E+OO 2.232E-01 2.275E-01 44.91 TL-208 277.37 31 6.60 3.944E+OO 8.703E-01 8.703E-01 80.47 583.19 85 85.00* 2.090E+OO 3.536E-01 3.536E-01 32.35 860.56 ------12.50 1. 520E+OO ------Line Not Found ------BI-211 72. 87 ------1.23 3.328E+OO ------Line. Not Found ------351. 06 236 12.92* 3.215E+OO 4.202E+OO 4.202E+OO 18.34 PB-212 74.82 118 10.28 3.532E+OO 2.395E+OO 2.395E+OO 36.09 77 .11 185 17.10 3.757E+OO 2.130E+OO 2.130E+OO 24.57 238.63 347 43.60* 4.454E+OO 1. 321E+OO 1.321E+OO 12.53 300.09 ------3.30 3.690E+OO ------Line Not Found ------BI-214 609.32 183 45.49* 2.015E+OO l.479E+OO 1.480E+OO 17.43 1120.29 27 14.92 l.223E+OO 1.078E+OO 1.078E+OO 67.61 1764.49 27 15.30 8 .116E-01 1.637E+OO 1.638E+OO 52.01 PB-214 74.82 118 5.80 3.532E+OO 4.244E+OO 4.246E+OO 36.09 77 .11 185 9. 70 3.757E+OO 3.755E+OO 3.757E+OO 24.57 87.09 98 3.41 4.590E+OO 4.622E+OO 4.624E+OO 49.35 242.00 95 7.25 4.411E+OO 2.207E+OO 2.208E+00 62.04 295.22 111 18.42 3.737E+OO 1.193E+OO 1.193E+OO 40.38 351. 93 236 35.60* 3.215E+OO 1.525E+OO 1.526E+OO 18.34 RN-219 271.23 33 10.80 4. 031E+OO 5.586E-01 5.586E-01 93.47 401.81 48 6.60* 2.865E+OO 1.886E+OO 1.886E+OO 110. 94 RN-222 609.32 183 45.49* 2.015E+OO 1.479E+OO l.480E+OO 17.43 1120.29 27 14.92 1.223E+OO 1.078E+OO 1.078E+OO 67.61 1764.49 27 15.30 8 .116E-01 1.637E+OO 1.638E+OO 52.01 RA-224 240.99 95 4.10* 4. 411E+OO 3.903E+OO 3.903E+OO 62.04 RA-226 609.32 183 45.49* 2.015E+OO 1.479E+OO 1.480E+OO 17.43 1120.29 27 14.92 1.223E+OO 1.078E+OO 1.078E+OO 67.61 1764.49 27 15.30 8 .116E-01 1.637E+OO 1.638E+OO 52.01 AC-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.327E+OO l.243E+OO l.243E+OO 54.91 794.95 12 4.25 1. 621E+OO 1.321E+OO 1.321E+OO 124.51 835. 71 ------1. 61 l.557E+OO ------Line Not Found ------911. 20 60 25.80* 1.450E+OO 1.181E+OO 1.181E+OO 41. 80 968.97 35 15.80 1. 379E+OO 1.190E+OO 1.190E+OO 48.16 RA-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.327E+OO 1.243E+OO 1.243E+OO 54.91 794.95 12 4.25 1.621E+OO 1.321E+OO 1. 321E+OO 124.51 835.71 ------1. 61 1.557E+OO ------Line Not Found ------911.20 60 25.80* 1.450E+OO 1.181E+OO 1.181E+OO 41. 80 968. 97 35 15.80 1.379E+OO 1.190E+OO 1.190E+OO 48.16 Page 4191of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235056 Acquisition date 3-0CT-2016 07:50:44 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-228 74.82 118 10 .2a 3.532E+OO 2.395E+00 2.395E+OO 36.Q9 77.11 185 17.10 3.757E+OO 2.130E+OO 2.130E+OO 24.57 238.63 347 43.60* 4.454E+OO l.321E+OO l.321E+OO 12.53 300.09 ------3.30 3.690E+OO ------Line Not F°ound ------TH-229 85.43 36 14.70 4.354E+OO 4.200E-01 4.200E-01 137.59 88.47 98 24.00 4.590E+OO 6.567E-01 6.568E-01 49.35 193.51 ------4.41* 5.168E+OO ------Line Not Found ------210.85 33 2.80 4.899E+OO l.787E+OO 1. 787E+OO 118. 06 TH-230 609.32 183 45.49* 2.015E+OO l.479E+OO l.480E+OO 17.43 1120. 29 27 14.92 l.223E+OO l.078E+OO l.078E+OO 67.61 1764.49 27 15.30 8 .116E-01 l.637E+OO l.637E+OO 52.01 PA-231 283.69 ------1. 70 3.870E+OO ------Line Not Found ------301.36 24 5.35* 3.671E+00 9.078E-01 9.078E-01 143.69 TH-232 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 63 11. 27 3.327E+OO l.243E+OO l.243E+OO 54.91 835. 71 ------1. 61 l.557E+00 ------Line Not Found ------911.20 60 25.80* 1.450E+OO l.181E+OO 1.181E+OO 41. 80 968. 97 35 15.80 l.379E+OO l.190E+OO 1.190E+OO 48.16 TH-234 63.29 29 3.70* 2.294E+OO 2.516E+OO 2.516E+OO 140.35 92.59 113 4.23 4.940E+00 4.012E+OO 4.012E+00 39.80 U-234 609.32 183 45.49* 2.015E+OO 1. 479E+OO l.479E+OO 17.43 1120.29 27 14.92 1.223E+OO 1.078E+OO l.078E+OO 67.61 1764.49 27 15.30 8 .116E-01 1.637E+OO 1.637E+OO 52.01 U-235 89. 96 66 3.47 4.767E+OO 2. 967E+00 2. 967E+00 73.97 93.35 113 5.60 4.940E+00 3. 031E+OO 3. 031E+OO 39.80 143.76 ------10. 96* 5.868E+OO ------Line Not Found ------163.33 ------5.08 5.647E+OO ------Line Not Found ------185. 72 102 57.20 5.297E+OO 2.485E-01 2.485E-01 47.46 205.31 ------5.01 4.973E+OO ------Line Not Found ------U-238 63.29 29 3.70* 2.294E+OO 2.516E+OO 2.516E+OO 140.35 92.59 113 4.23 4.940E+OO 4.012E+OO 4.012E+OO 39.80 AM-243 43.53 ------5.90 3.822E-01 ------Line Not Found ------74.66 118 67.20* 3.532E+OO 3.663E-01 3.663E-01 36.09 CM-247 278.00 31 3.40 3.944E+00 1. 689E+OO 1.689E+OO 80.47 287.50 ------2.00 3.826E+00 ------Line Not Found ------402.40 48 72. 00* 2.865E+OO 1. 729E-01 1.729E-01 110.94 ANH-511 511. 00 37 100.00* 2.335E+OO l.168E-01 1.168E-01 98.90 Flag: "*" Key line Page 4192of5809 Summary of Nuclide Activity Sample ID : G405235056 Acquisition date Page : 3 3-0CT-2016 07:50:44 Total number of lines in spectrum 49 Number of unidentified lines 12 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide NA-22 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Hlife 2.60Y l.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600. OOY 7.04E+08Y 1600. DOY l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+l0Y 1.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1. 56E+07Y l.00E+09Y Decay 1.25 1. 00 1. 58 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 2.878E-02 l.922E+Ol 4.260E+OO 4.260E-01 2 .112E-01 2.232E-01 3.536E-Ol 4.202E+OO 1. 321E+OO 1. 479E+OO 1.525E+OO 1.886E+OO 1.479E+OO 3.903E+OO 1. 479E+OO 1.181E+OO l.181E+OO 1. 321E+OO 6.567E-01 1.479E+OO 9.078E-01 1.181E+OO 2.516E+OO 1.479E+00 2.485E-01 2.516E+OO 3.663E-01 l.729E-01 l.168E-01 5.732E+Ol 5.732E+Ol Decay Corr pCi/GRAM 3. 596E-02 1.922E+Ol 6.743E+OO 4.260E-01 2.154E-01 2.275E-01 3.536E-01 4.202E+OO 1.321E+OO 1.480E+OO 1. 52 6E+OO 1.886E+00 l.480E+OO 3.903E+OO 1.480E+OO 1.181E+OO 1.181E+OO 1.321E+OO 6.568E-01 1.480E+OO 9.078E-01 1.181E+OO 2.516E+OO 1. 4 7 9E+OO 2.485E-01 2.516E+OO 3.663E-01 1.729E-01 l.168E-01 5.982E+Ol 5.982E+Ol 75.51%
  • Decay Corr 2-Sigma Error 8.782E-02 0.229E+Ol 3.327E+OO 2.102E-01 0. 967E-01 1.022E-01 1.144E-01 0.771E+OO 0.166E+OO 0.258E+OO 0.280E+OO 2.092E+00 0.258E+OO 2.422E+OO 0.258E+OO 0.494E+OO 0.494E+OO 0.166E+OO 3.241E-01 0.258E+OO 13.04E-01 0.494E+OO 3.531E+00 0.258E+OO 1.179E-01 3.531E+OO 1.322E-01 l.918E-01 l.155E-01 "M" Manually accepted 2-Sigma %Error 244.20 11. 93 49.35 49.35 44.91 44.91 32.35 18.34 12.53 17.43 18.34 110. 94 17.43 62.04 17.43 41. 80 41. 80 12.53 49.35 17.43 143.69 41. 80 140.35 17.43 47.46 140.35 36.09 110. 94 98.90 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4193 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235056 Acquisition date : 3-0CT-2016 07:50:44 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 118. 8 9 24 72 0.89 238.46 235 7 6.90E-03 **** 5.83E+OO T 0 129. 4 6 45 107 1. 07 259.61 256 10 1.28E-02 89.6 5. 91E+OO T 0 329.38 15 70 1. 44 659.39 651 12 4.33E-'-03 **** 3.41E+OO T 0 435.49 J.O 31 1.25 871.57 865 10 2.92E-03 t*** 2.67E+OO 0 463.09 22 18 1. 49 926.77 922 8 6.31E-03 79.7 2.54E+OO T 0 565.33 48 26 5.07 1131.21 1122 18 1.40E-02 57.7 2.14E+OO 0 719. 57 22 8 2.59 1439.62 1435 11 6.47E-03 63.5 1. 76E+OO T 0 770.32 28 29 4.46 1541. 09 1530 21 8.25E-03 **** 1.66E+OO 0 786.97 8 15 0.88 1574.38 1568 8 2.22E-03 **** 1.63E+OO 0 879.40 8 3 0. 96 1759.18 1756 7 2.36E-03 **** 1. 49E+OO T 0 883.43 4 8 0.53 1767.23 1762 7 l.12E-03 **** 1. 49E+OO T 0 920. 31 8 13 0.94 1840.98 1833 11 2.37E-03 **** 1. 44E+00 0 923.70 9 11 1. 26 1847.74 1843 10 2.54E-03 **** 1.43E+OO T 0 1043.52 9 4 1. 47 2087.31 2081 10 2.58E-03 **** 1.30E+OO 0 1109. 70 17 3 3.67 2219.61 2214 11 5.08E-03 58.5 1.23E+OO 0 1225.45 5 12 0.50 2451.03 2447 8 1. 59E-03 **** 1.13E+OO 0 1266.62 6 3 0.89 2533.33 2530 6 1.78E-03 **** 1. lOE+OO 0 1378.12 15 4 0.54 2756.24 2751 10 4.55E-03 70.7 1.02E+OO 0 1589.26 7 1 1. 39 3178.30 3175 6 2.lOE-03 88.8 8.98E-01 0 1799.81 6 0 0.99 3599.17 3596 6 1.67E-03 81. 6 7. 96E-01 Flags: "T" = Tentatively associated
  • Page 4194of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:51:28.87 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * *******************************************************************************
  • iC *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l *
  • Acquisition date 3-0CT-2016 07:50:44 Sensitivity 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.36 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:50:00 Nuclide Library : SOLID *
  • Sample ID G405235056 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.0148E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide NA-22 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 6.986E-02 3.874E-01 1.323E+OO 8. 413E-02 3.496E-02 3.693E-02 3.648E-02 2.532E-01 6.806E-02 6.839E-02 2.464E-01 5.262E-01 6.839E-02 7.297E-01 6.839E-02 "2 .125E-01 2.125E-01 6.806E-02 5.620E-01 6.836E-02 5. 241E-01 2.125E-01 l.885E+OO 6.836E-02 2.512E-01 1. 885E+OO 7.211E-02 4.830E-02 3.443E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-24 Page 4195 of 5809 Le (pCi/GRAM l.350E+Ol NOT IDENT. O.OOOE+OO SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58
  • FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 Page 4196 of 5809 3.054E-02 3.443E-01 O.OOOE+OO O.OOOE+OO 7.935E-02 6 .115E-01 O.OOOE+OO 6.163E-02 7.182E-01 9.336E+OO 6.197E-02 1.504E-01 2.883E+00 1.568E+Ol O.OOOE+OO 2.829E-01 O.OOOE+OO O.OOOE+OO 8.018E-01 8.619E+OO 9.688E-01 O.OOOE+OO 2.788E-01 6.447E+02 3.831E-02 9.765E-01 3.321E+OO 2.061E+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 3.896E-02 7.191E-02 8 .113E+OO 6.501E-01 6.501E-01 3.815E-02 1.342E-01 3.086E-01 O.OOOE+OO O.OOOE+OO 1.679E-01 3.121E+OO 1.357E-01 4.250E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 5.254E-02 O.OOOE+OO 7.540E-02 1.766E-01 O.OOOE+OO O.OOOE+OO 1.429E-01 O.OOOE+OO O.OOOE+OO 3.718E+Ol O.OOOE+OO 4.406E-01 7.687E-02 '6. 711E+00 5.426E-02 O.OOOE+OO 1. 032E+03 O.OOOE+OO 3.323E-02 1. lllE-01 2.236E-01 1. 511E-01 1.500E-01 2.436E+00 6.956E-02 3.657E+Ol NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT . NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 'BK-247 CF-249 CF-251 Page 4197of5809 2. 965E-01 8.087E-02 2.732E-02 6. 096E+OO 1.030E+OO 4.942E+OO 4.171E+01 1.464E+02 6.554E-01 2.871E+OO 6.806E-02 5.898E+00 7. 966E-01 8.428E-01 6.507E-01 3.026E-01 3.026E-01 6.507E-01 7.591E-02 2.787E-01 6.829E+OO 7.591E-02 O.OOOE+OO 3. llOE-01 4.449E+02 2.099E-01 1.265E-01 9.228E-02 4.558E-02 1. 551E-01 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN .NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:51:34.75 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235056.CNF;l * *Acquisition date 3-0CT-2016 07:50:44 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.36 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:50:00 Nuclide Library : SOLID *
  • Sample ID G405235056 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity 1.0148E+02 GRAM *
  • Quantity Err(%) 1.9708E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * * * 'Eff. Cal. date 20-JUL-2016 07: 03: 55 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1. 96-sigma) NA-22 3.596E-02 8.608E-02 K-40 1.922E+01 2.460E+OO CD-109 5.003E+00 3.365E+00 SN-126 3.160E-01 2 .119E-01 BA-137M 2.154E-01 9.523E-02 CS-137 2.275E-01 l.006E-01 TL-208 3.536E-01 1.131E-01 BI-211 9.152E-01 1.518E+OO PB-212 1.321E+OO 1. 766E-01 BI-214 1.480E+00 2.607E-01 PB-214 1.526E+OO 2.815E-01 RN-219 1.886E+00 2.064E+OO RN-222 1.480E+OO 2.607E-01 RA-224 1. 794E+00 2. 521E+OO RA-226 1.480E+OO 2.607E-01 AC-228 1.181E+OO 4.876E-01 RA-228 l.181E+00 4.876E-01 TH-228 1.321E+OO 1. 766E-01 TH-229 -7.270E-01 7.088E-01 TH-230 l.480E+00 2.606E-01 PA-231 9.078E-01 1.293E+OO TH-232 1.181E+00 4.876E-01 TH-234 2.516E+00 3.505E+OO U-234 1. 479E+00 2.606E-01 U-235 l.323E-03 2.863E-01 U-238 2.516E+00 3.505E+00 AM-243 2.634E-01 l.374E-01 CM-247 1.729E-01 1.902E-01 ANH-511 1.168E-01 1.133E-01 Non-Identified Nuclides Nuclide BE-7 Page 4198of5809 Key-Line Activity (pCi/GRAM -8.317E+OO K.L Act error ( 1. 96-sigma) 1.757E+Ol TPU ( 1. 96-sigma) 8.608E-02 2.460E+OO 3.365E+OO 2.119E-01 9.523E-02 1.006E-01 1.131E-01 l.518E+00 1.766E-01 2.607E-01 2.815E-01 2.064E+00 2.607E-01 2.521E+OO 2.607E-01 4.876E-01 4.876E-01 1.766E-01 7.088E-01 2.606E-01 1.293E+00 4.876E-01 3.505E+00 2.606E-01 2.863E-01 3.505E+OO 1.374E-01 1.902E-01 1.133E-01 TPU ( 1. 96-sigma) l.796E+Ol NOT IDENT.

NA-24 l.OOOE+41 l.698E+41 O.OOOE+OO SHORT HLIF AL-26 -8.408E-03 4.022E-02 4.039E-02 NOT IDENT. SC-46 -2.005E-01 4.826E-01 4.910E-01 FAIL ABUN V-48 2.328E+04 2.716E+04 2.912E+04 SHORT HLIF CR-51 7.961E+Ol 7.276E+02 7.285E+02 SHORT HLIF MN-54 2.357E-02 9.243E-02 9.304E-02 NOT IDENT. C0-56 -1.269E-01 7.766E-01 7.787E-01 NOT IDENT. MN-56 -1.000E+41 6.597E+41 O.OOOE+OO SHORT HLIF C0-57 5.378E-02 7.244E-02 7.639E-02 NOT IDENT. C0-58 -5.712E-01 9.974E-01 1. 030.E+OO NOT IDENT. FE-59 -3.805E+00 l.249E+Ol 1.261E+Ol NOT IDENT. C0-60 4. 963E-02 6.263E-02 6.651E-02 NOT IDENT. ZN-65 -2.445E-01 3.014E-01 3.209E-01 NOT IDENT. GE-68 -1.554E+OO 3.948E+OO 4.0lOE+OO NOT IDENT. AS-73 1.065E+00 l.931E+Ol 1. 931E+Ol NOT IDENT. AS-74 -8.097E.+03 l.163E+04 1. 218E+04 SHORT HLIF SE-75 4.107E-01 3. lllE-01 3.620E-01 FAIL ABUN BR-77 1. 320E+39 l.165E+40 O.OOOE+OO SHORT HLIF SR-82 -1.120E+03 1.440E+03 l.526E+03 SHORT HLIF RB-83 2.602E-01 9.169E-01 9.243E-01 NOT IDENT. KR-85 3.894E+OO 1. 07 6E+Ol 1. 091E+Ol NOT IDENT. SR-85 4.377E-01 1.210E+OO 1.226E+OO NOT IDENT. RB-86 -2.691E+04 5.749E+04 5.876E+04 SHORT HLIF Y-88 -6.096E-02 3.557E-01 3.567E-01 NOT IDENT. Y-91 -7.074E+02 8.865E+02 9.421E+02 NOT IDENT. NB-94 5.150E-03 4.563E-02 4.568E-02 NOT IDENT. NB-95 -8.782E-01 1.565E+OO 1.615E+OO NOT IDENT. NB-95M -1.423E+OO 4.448E+OO 4.494E+OO NOT IDENT. ZR-95 4.433E-01 2.448E+OO 2.456E+OO NOT IDENT. NB-97 -1. OOOE+41 1.437E+41 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 2.376E+41 O.OOOE+OO SHORT HLIF M0-99 -1.177E+33 l.226E+33 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 1.659E+41 O.OOOE+OO SHORT HLIF RH-101 -2.685E-02 5.235E-02 5.373E-02 NOT IDENT. RH-102 -2.462E-02 9 .131E-02 9.199E-02 NOT IDENT. RU-103 -l.435E-01 9. 725E+OO 9. 725E+OO FAIL ABUN RH-106 8.675E-02 7.708E-01 7.718E-01 NOT IDENT. RU-106 8.675E-02 7.708E-01 7.718E-01 NOT IDENT. AG-108M 3.834E-02 4.028E-02 4.383E-02 NOT IDENT. AG-llOM 6.092E-02 1.573E-01 1.597E-01 FAIL ABUN SN-113 7.437E-02 3.723E-01 3.738E-01 NOT IDENT. CD-115 2.222E+40 2.809E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 8.576E+04 l.806E+05 1.847E+05 SHORT HLIF TE-123M 6.262E-02 l.880E-01 l.901E-01 NOT IDENT. SB-124 2.949E+OO 2.657E+OO 2.971E+OO NOT IDENT. SB-125 7.366E-02 1.514E-01 1.550E-01 FAIL ABUN TE-125M 2.398E+02 5.146E+02 5.258E+02 NOT IDENT. I-126 -2.409E+05 2.205E+06 2.208E+06 SHORT HLIF SB-126 4.891E+06 3.182E+06 3.871E+06 SHORT HLIF SB-127 -3.246E+22 1.064E+23 O.OOOE+OO SHORT HLIF I-131 -8.032E+09 1. 309E+10 1.358E+10 SHORT HLIF I-132 1.000E+41 1.889E+42 O.OOOE+OO SHORT HLIF TE-132 4.936E+26 2 .114E+27 O.OOOE+OO SHORT HLIF BA-133 -2.190E-02 7.247E-02 7.314E-02 FAIL ABUN I-133 -1.000E+41 9. 507E+41. O.OOOE+OO SHORT HLIF CS-134 8.693E-02 l.061E-01 1.131E-01 FAIL ABUN CS-135 2.504E-02 2.262E-01 2.265E-01 NOT IDENT. I-135 -1.000E+41 6. 961E+41 O.OOOE+OO SHORT HLIF CS-136 -3.382E+04 4.883E+05 4.886E+05 SHORT HLIF CE-139 -4.365E-03 l.647E-01 1. 647E-01 NOT IDENT. BA-140 -1.651E+06 2.607E+06 2.711E+06 SHORT HLIF LA-140 -2.335E+05 8.560E+05 8.625E+05 SHORT HLIF CE-141 5.775E+OO 4.223E+Ol 4.231E+Ol NOT IDENT. CE-143 1.000E+41 2.275E+41 O.OOOE+OO SHORT HLIF CE-144 -2.250E-01 5.814E-01 5.902E-01 NOT IDENT. PM-144 -l.405E-02 9.562E-02 9.583E-02 NOT IDENT. PR-144 -1. l 73E+OO 8.339E+OO 8.356E+OO NOT IDENT. PM-146 -5.622E-02 7.235E-02 7.666E-02 NOT IDENT. ND-147 7.175E+06 7.615E+07 7.622E+07 SHORT HLIF PM-147 6.631E+02 1.236E+03 1. 272E+03 NOT IDENT. PM-149 l.OOOE+41 4.117E+41 O.OOOE+OO SHORT HLIF EU-150 l.302E-02 4.168E-02 4.209E-02 FAIL ABUN EU-152 -4.123E-02 1.359E-01 1.371E-01 NOT IDENT. GD-153 -3.395E-02 3.lOlE-01 3.105E-01 NOT IDENT. 8.791E-02 2.104E-01 2.141E-01 FAIL ABUN EU-155 8.291E-02 1.813E-01 1. 851E-01 FAIL ABUN TB-160 2.476E+OO 2.435E+OO 2.679E+OO FAIL ABUN H0-166M -l.346E-02 8.707E-02 8.728E-02 FAIL ABUN Page 4199of5809 TM-171 -2.061E+OO 4.545E+Ol 4.546E+Ol NOT IDENT. HF-172 2.944E-01 3.487E-01 3. 731E-01 FAIL ABUN LU-172 -2.267E-02 1.069E-01 1.074E-01 FAIL ABUN LU-176 -1.540E-02 3.814E-02 3.877E-02 FAIL ABUN HF-181 3.098E+OO 6.818E+OO 6.959E+OO NOT IDENT. TA-182 -4.430E-01 1.488E+OO 1.502E+OO FAIL ABUN RE-183 -4.553E-01 6.173E+OO 6.176E+OO NOT IDENT. RE-184 8.850E+OO 4.944E+Ol 4. 960E+Ol NOT IDENT. W-188 -5.362E+Ol 1.983E+02 'l.998E+02 FAIL ABUN IR-192 2.829E-01 7.399E-01 7. 508E-..()1 FAIL ABUN HG-203 -3.501E+OO 4.246E+OO 4.530E+OO NOT IDENT. BI-207 1.941E-02 8. OSlE-02 8.099E-02 FAIL ABUN PB-210 -2.426E+OO 7.366E+OO 7.447E+OO NOT IDENT. PB-211 -6.006E-01 1.023E+OO 1.058E+OO NOT IDENT. BI-212 1. 071E+OO 8.816E-01 1.00SE+OO NOT IDENT. RA-223 -l.870E-01 8.835E-01 8.875E-01 FAIL ABUN AC-227 -8.628E-02 3.608E-01 3.629E-01 NOT IDENT. TH-227 -8.628E-02 3.608E-01 3.629E-01 NOT IDENT. TH-231 -1. 870E-01 8.835E-01 8.875E-01 FAIL ABUN PA-233 -2.617E-02 9.190E-02 9.266E-02 NOT IDENT. PA-234 -4. 521E-01 6.863E-01 7.160E-01 FAIL ABUN PA-234M l. lllE-01 8.053E+OO 8.053E+OO NOT IDENT. NP-237 -2.617E-02 9.190E-02 9.266E-02 NOT IDENT. NP-238 1.000E+41 3.683E+41 O.OOOE+OO SHORT HLIF NP-239 -8.382E-03 4.284E-01 4.284E-01 FAIL ABUN PU-239 8.918E+02 7.840E+02 8. 811E+02 FAIL ABUN AM-241 -8.625E-02 2.930E-01 2.956E-01 NOT IDENT. CM-243 -5.985E-02 1.651E-01 1. 673E-01 FAIL ABUN BK-247 8.175E-02 l.098E-01 1.158E-01 FAIL ABUN CF-249 l.794E-02 5.159E-02 5.222E-02 NOT IDENT. CF-251 1.485E-01 1.683E-01 1. 811E-01 NOT IDENT. Page 4200 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 80.8814 879.38 69.2091 482.18 68.1542 45.60 59.0989 87.57 69.2191 133.52 73.2301 46.54 70.7781 87.09 69.2291 264.66 61.5581 49.72 0.0000 87.57 69.2607 122.06 61.5789 51. 35 67.7282 88.03 69.2909 140.51 0.0000 51. 87 73.6162 88.34 69.3113 143.76 78.0153 52.39 70.1573 193.51 69. 3196 144.24 72. 9518 52.97 60.8478 89.96 69.4170 145.44 78.1079 53.44 66.7384 90.64 69.4609 152.43 73.3682 125.81 72.6501 91.11 0.0000 153.25 0.0000 57.36 0.0000 63. 29 69.5866 154.21 55.5202 57.53 70.6071 143.76 69.6349 156.02 0.0000 57.98 68.2905 94.56 69. 7118 158.56 0.0000 1093.63 75.4714 94.65 69.7175 159.00 55.6994 57.98 75.4761 94.67 69.7188 162.33 66.1280 59.54 75.4958 94.87 69.7314 162.66 0.0000 60.96 56. 7167 97.43 65.3963 163.33 53. 2813 61.17 69.3375 311. 90 65.4545 165.86 64.5592 62.93 86.4541 946.00 65.4553 176.31 71.9234 63.29 86.4899 99.53 61.4235 1048.07 0.0000 63.58 86.5186 1221.41 62.6839 177.52 52.8991 64.28 94.8906 2 65. 00 72.6382 739.50 0.0000 66.73 74.5357 103.18 76.4078 181.52 70.4177 67.24 79.3386 103.37 76.4206 711. 68 65.3168 67.68 86.9181 116.74 76.4206 185.72 65.3687 67.75 95.2594 105.21 69.1340 193.51 77.9338 69.67 95.4602 105.31 69.1400 197.03 61.4230 70.83 79.6499 106.12 71.6584 127.23 65.8485 72.81 90.9928 106.47 77.8589 306.78 57.1950 279.20 90.9986 109.28 75.5659 203.43 56.3672 72.87 90.9986 111. 00 88.0794 205.31 68.7713 74.66 97.1676 228.16 0.0000 210.85 51. 7403 74.82 97.1837 114. 06 78.3511 215.65 68.2852 1063.66 97.1988 116. 30 0.0000 222 .11 48.0580 238.63 97.4136 116.74 69.7966 290.67 55.3260 351.93 97.4136 119.76 73. 2962 177.52 58.9048 78.74 97.5755 121.12 56.2816 228.16 0.0000 79.69 81. 9936 121.22 52.5336 228.18 52.6795 80.12 67.5532 121. 78 51.3054 235.69 69.9210 80.19 0.0000 122.06 51.3166 256.23 65.8968 80.57 82.0657 122.92 68.1341 238.63 59.2552 81. 00 82.1010 123.07 68.1419 238.98 0.0000 81. 07 82.1067 123.68 76.8632 240.99 59.3278 81.75 74.9126 125.81 51.4658 242.00 59.3586 323.87 69.0091 127.23 70.3711 344.28 43.2295 84.00 69.0234 127.91 75.4367 252.40 0.0000 85.43 69 .1191 129.30 63.7694 252.80 61. 4936 86.55 69.1935 131. 20 64.2807 254.15 0.0000 Page 4201of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 256.23 54.3518 351. 93 37.8206 583.19 14.3241 260.90 0.0000 507.63 0.0000 584.27 14.3287 264.66 23.1955 356.01 38.3568 595.83 0.0000 264.80 30.0197 364.49 0.0000 600.60 21.5947 265.00 30.0224 366.42 0.0000 602.52 0.0000 268.22 42.3705 372. 51 . 22.8794 604.72 24.7090 269.46 37.3815 129.30 37.2163 607.14 24.7256 270.03 37.3915 377.52 23.8795 609.32 13.4015 271.23 50.6447 383.85 33.5132 497.08 13.4052 273.65 0.0000 388.16 22.0590 433.94 7.7423 356.01 57.6308 388.63 0.0000 696.49 23.7684 277.37 40.2680 391.69 26.5067 620.36 18.6138 277.60 40.2725 400.66 33.7268 621. 93 16.5527 278.00 40.2805 401. 81 33.7418 667. 71 0.0000 279.20 48.0887 402.40 33.7489 631. 29 18.6702 279.54 48. 0962 404.85 33.7795 453.88 14.5292 27'9. 7 0 48.1004 410.95 34.8230 595.83 0.0000 280.46 39.8688 413.71 24.2071 635.95 18.6943 283.69 40.3879 414.70 0.0000 636.99 0.0000 364.49 0.0000 423.72 0.0000 645.85 18.7449 285.41 42.2574 404.85 28.2165 884.68 18.8057 285.90 0.0000 427.87 20.4386 657.90 0.0000 402.40 44.1377 433.94 16.5812 661. 66 11. 5044 290.67 '44.2021 333.97 20.5223 664.57 0.0000 293.27 0.0000 453.88 34.3762 666.33 0.0000 295.22 38.7572 463.37 22.1709 720.70 0.0000 295.96 38.7700 468.07 27.6343 667.71 0.0000 298.58 41. 5887 685.70 ,0.0000 677.62 16.8047 299.98 36.0666 475.06 22.7529 685.70 0.0000 300.09 36.0682 476.78 18.8067 695.00 0.0000 300.13 36.0690 477.60 19.8018 696. 49 22.1647 301.36 36.0888 482.18 16.8575 696. 51 22.1647 302.85 36.1126 1596.21 0.0000 697.00 0.0000 304.50 29.1897 527.90 0.0000 697.30 14.7799 537.26 0.0000 497.08 21.9221 697.49 14.7804 306.78 36.1761 505.52 23.9800 702.65 14.7998 316.51 37.1313 507.63 0.0000 706.68 20.1063 311. 90 41. 8359 511. 00 22.0204 711. 68 16.9538 316.51 33.5361 514.00 18.0337 720.70 0.0000 531.02 0.0000 514.00 18.0337 721.93 0.0000 320.08 0.0000 520.40 14.0547 1690.97 12.7510 427.87 27.0683 238.98 0.0000 722.91 12.7515 323.87 30.8395 522.65 0.0000 1274.44 19.1287 325.23 28.0518 527.90 0.0000 724.19 27.1052 328.76 0.0000 528.26 17.1086 727.33 15.9570 388.16 39.4083 520.40 22.1495 733.00 12.7837 333.97 32.3795 529.87 0.0000 735.93 11. 7269 334.37 29.5691 531. 02 0.0000 737.46 11.7314 338.28 36.6688 537.26 0.0000 739.50 0.0000 911.20 36.6696 546.56 0.0000 747.24 12.8291 340.48 36.7021 552.55 18.2505 748.06 8.5544 340.55 0.0000 563.25 18.3091 752.31 9.6335 344.28 33.9324 795.86 22.9276 753.82 0.0000 345.93 30.1829 569.50 21.3999 756.73 12.8589 351. 06 37.8076 569.70 21. 4016 756.80 12.8589 Page 4202 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 763.94 8.0508 984.45 0.0000 1596.21 0.0000 765.81 19.3308 996.26 13.5601 1620.50 3.7656 766.42 8.5928 1001.03 14.7038 1621. 92 5.6495 766.84 8.5938 1002.74 12.4462 1678.03 0.0000 772.60 0.0000 1004.73 14.7149 1690.97 0.0000 776.52 0. 00.DO 1021.30 0.0000 0.0000 777.92 0.0000 1025.87 0.0000 1764.49 7.6826 778.90 9.6962 1028.54 0.0000 1770. 23 6.7274 783.70 0.0000 846.77 6.8364 1771.35 0. 9612 727. 33 17.2643 1038.76 0.0000 1791.20 0.0000 792.07 16.2109 1046.59 1. 7120 1808.65 2.8978 794.95 10.8146 1048.07 0.0000 846.75 0.0000 795.86 11. 3579 1049.04 7.9929 1836.06 3.8777 801.95 21.6650 621. 93 6.8530 810. 06 14.1087 1063.66 11. 4510 810.29 19.5366 1077.00 0.0000 810.45 18.4519 1077.34 13.7773 810.76 17.3678 1085.87 16.0998 815.77 0.0000 1093.63 9.2135 818.51 0.0000 1099.45 13.8359 832.01 10.9082 1112. 07 5.2006 834.85 10.9151 1112. 84 6.9351 835.71 13 .1011 1115. 54 13.8770 1260.41 0.0000 609.32 11.5747 846.75 0.0000 889.28 11. 57 55 846.77 14.2283 1121.30 13.8926 856.80 0.0000 1129. 67 15.0736 860.56 9. 8811 1131. 51 0.0000 702.65 8.8037 1147.95 0.0000 873.19 13.2119 1173.23 12.2714 529.87 0.0000 1177.95 12.2825 879.38 9.9225 1189.05 14.9435 880.51 0.0000 1204.77 16.7479 883.24 16.5515 1221.41 11.3164 884.68 14.9008 1231.02 8.8556 889.28 8.8392 1235.36 0.0000 903.28 3.3186 1238.28 15.9598 898.04 8.8558 1260.41 0.0000 900.72 8.8610 1271.87 7.1343 903.28 9.9741 1274.44 12.8470 911.20 21.6479 1274.54 12.8479 912.08 21. 6519 1099.45 6.2634 923.98 0.0000 1298.22 0.0000 926.50 11. 6946 1312 .11 0.0000 929 .11 6.6863 1332.49 5.4053 937.49 11.1637 1362.66 0.0000 944 .13 0.0000 1365.19 7.2456 946.00 17.8939 1368.63 0.0000 949.00 7.8334 1384.29 3.6338 954.55 0.0000 1408.01 7.2949 962. 31 20.1995 1457.56 0.0000 964.08 16.1654 1460.82 5.5166 966 .17 11. 7 924 696.51 5.5404 968. 97 10 .1133 1505.03 3.7024 983.53 0.0000 1584.12 3.7461 Page 4203 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:52:04.97 ******************************************************************************** * " GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;477 Background date : Z-OCT-2016 11:00:07. Sample date 2-DEC-2015 14:55:00. Acquisition date : 3-0CT-2016 07:51:32. Sample ID G405235057 Sample quantity 1.15835E+02 GRAM Detector name : GAM05 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.59 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 1 1 1 5 5 5 5 0 3 3 0 0 0 0 3 3 3 3 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4204 of 5809 Energy 31. 49 46.20* 62.83* 72.69 74.52* 76.70* 83.62* 86.72* 89.64 92.39* 117. 65 128.93 130. 85 143.91* 185.50* 209.04 231.76 238.36* 241.38 269.63 276.86 284.39 287.37 294.89* 299.82 310.55 327.51 338.09* 351.68* 373.77 463 .11 510.47* 583.14* 609.27* BACKGROUND CORRECTED *SAMPLE PEAK REPORT Area 24 37 129 36 241 384 56 141 120 133 33 45 36 12 93 35 20 424 130 40 18 15 41 169 29 26 29 119 259 19 34 44 115 205 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 93 164 200 136 137 139 118 150 107 118 73 77 59 135 101 88 69 59 58 39 66 64 31 57 67 47 35 45 68 33 26 67 42 27 0.53 0.70 0.90 0.93 0.94 0.94 0. 96 1. 41 1. 03 1.15 1. 66 1. 28 1.17 1. 40 0.87 '1. 04 1. 82 0. 96 1. 50 1. 55 1. 56 4.54 2.31 1. 09 1.12 3.44 1. 59 1.11 1. 05 1. 57 1.17 1. 39 1. 27 1. 24 64.83 94.21 127.46 147 .17 150. 83 155.17 169.01 175.21 181.04 186.54 237.01 259.56 263.40 289.50 372. 62 419.68 465.07 478.27 484.31 540.77 555.22 570.27 576.23 591.26 601.10 622.55 656.45 677.59 704.76 748.92 927.48 1022.12 1167.37 1219.59 63 91 123 144 144 144 166 166 166 166 234 256 256 284 368 416 462 471 471 537 537 562 572 586 597 616 653 672 700 746 924 1014 1160 1213 6 6.56E-03 67.5 8 1.03E-02 66.2 9 3.57E-02 22.4 18 9.90E-03 55.4 2.04E+OO 18 6.69E-02 10.4 18 1. 07E-01 7. 3 27 l.55E-02 33.4 8.49E-01 27 3.92E-02 17.4 27 3.34E-02 16.5 27 3.70E-02 17.7 7 9.18E-03 46.4 13 1.26E-02 37.2 2.80E+00 13 9.96E-03 43.2 9 3.37E-03176.9 9 2.60E-02 23.0 8 9.61E-03 50.0 7 5.69E-03 70.5 17 1.18E-01 5.7 1.06E+OO 17 3.62E-02 13.6 25 1.lOE-02 33.2 1.16E+OO 25 5. OlE-03 81. 6 11 4. llE-03110. 7 10 1.14E-02 29.6 10 4.70E-02 11.5 10 7.99E-03 55.9 11 7.28E-03 54.2 7 7.95E-03 39.1 13 3.29E-02 15.1 11 7.20E-02 8.8 7 5.27E-03 54.6 8 9. 36E-03 31. 4 16 1.21E-02 49.8 14 3.18E-02 15.4 14 5.70E-02 9.0 Peak Search Report (continued) Page : 2 Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 661. 41 72 22 1. 45 1323.81 1316 13 1. 99E-02 18.1 36 0 665.98 21 15 1. 75 1332. 95 1329 11 5.90E-03 42.5 31 0 727.39 31 15 2.33 1455.68, 1451 10 8.61E-03 29.5 38 0 802.80* 18 7 0.66 1606.41 1601 9 5.03E-03 38.l 39 0 806.83 19 6 0.95 1614.45 1611 8 5.28E-03 33.7 40 0 842.74 22 11 2.80 1686.23 1681 11 6. llE-03 36.1 41 0 904.18 14 6 0.91 1809.04 1805 8 3.95E-03 39.8 42 0 911.32* 112 18 1. 67 1823. 31' 1817 12 3.12E-02 12.2 43 0 957.80 11 7 0.95 1916.20 1913 8 3.12E-03 52.0 44 0 964.81 14 6 1. 01 1930.22 1927 7 3.82E-03 41. 3 45 0 969.02 69 6 1.29 1938.64 1934 12 1.92E-02 14.0 46 0 1000.86* 10 . 17 0.67 2002.27 1992 14 2.66E-03100.5 47 0 1006.36 7 3 1.10 2013.27 2010 6 2.06E-03 51.5 48 0 1021.14* 8 14 1. 42 2042.80 2039 9 2.19E-03 93.2 49 0 1045.66 9 5 0.62 2091.82 2087 8 2.43E-03 58.3 50 0 1120. 83* 29 23 1. 55 2242.07 2233 18 8.06E-03 43.1 51 0 1239.14 23 26 1. 40 2478.53 2473 14 6.47E-03 49.8 52 0 1279.37 5 12 4.20 2558.95 2549 12 1.39E-03145.6 53 0 1285.23 6 2 0.64 2570.67 2567 7 1. 74E-03 53. 2 54 0 . 1337.51 7 8 1. 34 2675.16 2668 11 l.85E-03 92.l 55 0 1396. 44 8 2 0.70 2792.94 2788 9 2.19E-03 49.1 56 0 1408.26 12 0 1. 74 2816.58 2812 10 3.33E-03 28.9 57 0 1461. 08* 321 19 2.41 2922.16 2914 15 8.93E-02 6.3 58 0 1764.58 41 0 1. 07 3528.80 3523 13 1. 14E-02 15.6 Flag: "*" = Peak area was modified by background subtraction Page 4205 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:52:07 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 2-DEC-2015 14:55:00 G405235057 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:51:32 115. 83 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAS 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4206 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 TH-229 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 85.43 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.59 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page 2 Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.244E+OO 1.482E+Ol l.482E+Ol 12.70 CD-109 88.03 3.70* 8. 914E+OO 1. 772E+OO 2.806E+OO 60.17 OK SN-126 64.28 9.60 9.124E+OO 1.029E+OO 1.029E+OO 44.76 OK 86.94 8.90 8. 914E+OO 7.368E-01 7.368E-01 60.17 OK 87.57 37.00* 8.914E+OO 1. 772E-01 l.772E-01 60.17 OK CS-135 268.22 16.00* 5.038E+OO 3.243E-01 3.243E-01 66.49 OK BA-137M 661. 66 89.90* 2.417E+OO 2.089E-01 2.129E-01 36.21 OK CS-137 661. 66 85.10* 2.417E+OO 2.207E-01 2.250E-01 36.21 OK TL-208 277.37 6.60 4.930E+OO 3.652E-01 3.652E-01 163.20 OK 583.19 85.00* 2.673E+OO 3.217E-01 3.217E-01 30.77 OK 860.56 12.50 1.959E+OO Line Not Found Absent PB-210 46.54 4.25* 9.666E+OO 6.380E-01 6.549E-01 132. 41 OK PB-212 74.82 10.28 8.979E+OO 1.087E+OO 1.087E+OO 37.83 OK 77 .11 17.10 8. 967E+OO 1.741E+OO 1. 741E+OO 14.56 OK 238.63 43.60* 5.564E+OO 1.160E+OO 1.160E+OO 11. 42 OK 300.09 3.30 4.617E+OO 1.239E+OO 1.239E+OO 111. 85 OK BI-214 609.32 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 OK 1120.29 14.92 1.575E+OO 7.645E-01 7.648E-01 86.25 OK 1764.49 15.30 1.032E+OO 1.574E+OO 1.574E+OO 31. 23 OK PB-214 74.82 5.80 8.977E+OO Line Not Found <<INT Reject 77 .11 9.70 8. 967E+OO 3.070E+OO 3. 071E+OO 14.56 OK 87.09 3.41 8.912E+OO Line Not Found <<INT Reject 242.00 7.25 5.497E+OO Line Not Found <<INT Reject 295.22 18.42 4.681E+00 1. 290E+OO 1.290E+OO 23.00 OK 351. 93 35.60* 4.043E+OO 1.173E+OO 1.174E+OO 17.65 OK RN-222 609.32 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 OK 1120. 29 14.92 1.575E+OO 7.645E-01 7.648E-01 86.25 OK 1764.49 15.30 1.032E+OO 1.574E+OO 1.574E+OO 31. 23 OK RA-224 240.99 4.10* 5.508E+OO l.542E+OO 1.542E+OO 75.39 OK RA-226 609.32 45.49* 2.581E+OO l .112E+00 1.112E+OO 18. 02 OK 1120. 29 14.92 1.575E+OO 7.645E-01 7.648E-01 86.25 OK 1764.49 15.30 1.032E+OO 1.574E+OO 1.574E+OO 31. 23 OK AC-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO 1.645E+OO 1.645E+OO 30.14 OK 794.95 4.25 2.087E+OO Line Not Found Absent 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.870E+OO l.457E+OO 1.457E+OO 24.31 OK 968.97 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 OK RA-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO 1.645E+OO 1.645E+OO 30.14 OK 794.95 4.25 2.087E+OO Line *Not Found Absent 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.870E+OO 1.457E+OO 1.457E+OO 24.31 OK 968. 97 15.80 l.779E+OO 1.530E+OO 1.530E+OO 27.95 OK TH-228 74.82 10.28 8.979E+OO 1.087E+OO 1.087E+OO 37.83 OK 77 .11 17.10 8. 967E+OO 1. 741E+OO 1. 741E+OO 14.56 OK 238.63 43.60* 5.564E+OO 1.160E+OO l.160E+OO 11. 42 OK 300.09 3.30 4.617E+OO 1.239E+OO l.239E+OO 111. 85 OK TH-229 85.43 14.70 8.914E+OO 4.461E-01 4.461E-01 60.17 OK Page 4207 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Nuclide Type: Nuclide Energy %Abn %Eff Uncorrected Decay Corr 2-Sigrna pCi/GRAM pCi7GRAM %Error Status 88.47 24.00 8.89JE+OO 3.886E-01 3.886E-01 33.02 OK 193.51 4.41* 6. 511E+OO Line Not Found Absent 210.85 2.80 6 .116E+OO Line Not Found Absent TH-230 609.32 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 OK 1120.29 14.92 l.575E+OO 7.645E-01 7.645E-01 86.25 OK 1764.49 15.30 1.032E+OO l.574E+OO l.574E+OO 31.23 OK TH-232 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.178E+OO 1.645E+OO 1.645E+00 30.14 OK 835. 71 1. 61 2.005E+OO Line Not Found Absent 911. 20 25.80* 1.870E+OO l.457E+OO 1.457E+OO 24.31 OK 968. 97 15.80 1.779E+OO l.530E+OO 1.530E+OO 27.95 OK PA-233 300.13 6.63 .4. 617E+OO 6.166E-01 6.166E-01 111. 85 OK 311. 90 38.50* 4.484E+OO 9.945E-02 9.945E-02 108.41 OK 340.48 4.45 4.154E+OO Line Not Found Absent TH-234 63.29 3.70* 9.124E+OO 2.669E+OO 2.669E+OO 44.76 OK 92.59 4.23 8.869E+00 2.447E+OO 2.447E+OO 35.39 OK U-234 609.32 45.49* 2.581E+OO 1.112E+OO l .112E+00 18.02 OK 1120.29 14.92 1.575E+OO 7.645E-01 7.645E-01 86.25 OK 1764.49 15.30 1.032E+00 1.574E+OO 1.574E+OO 31.23 OK U-235 89. 96 3.47 8.893E+OO 2.688E+OO 2.688E+OO 33.02 OK 93.35 5.60 8.869E+OO 1.849E+00 1.849E+OO 35.39 OK 143.76 10. 96* 7.805E+OO 9.619E-02 9.619E-02 353. 72 OK 163.33 5.08 7.279E+OO Line Not Found Absent 185. 72 57.20 6.705E+OO 1.634E-01 1.634E-01 45.99 OK 205.31 5.01 6.238E+OO Line Not Found Absent U-238 63.29 3.70* 9.124E+OO 2.669E+OO 2.669E+OO 44.76 OK 92.59 4.23 8.869E+OO 2.447E+00 2.447E+OO 35.39 OK PU-239 129.30 0.01* 8.197E+OO 5.946E+02 5.946E+02 74.31 OK 375.05 0.00 3.844E+OO 2.064E+03 2.064E+03 109.17 OK 413. 71 0.00 3.534E+OO Line Not Found Absent AM-243 43.53 5.90 9.491E+OO Line Not Found Absent 74.66 67.20* 8.979E+OO l.663E-01 l.663E-01 37.83 OK ANH-511 511. 00 100.00* 2.976E+OO 9.425E-02 9.425E-02 99.66 OK Flag: "*" = Keyline Page 4208 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:52:08.13 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  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l *
  • Acquisition date 3-0CT-2016 07:51:32 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:55:00 Analyst initials: MXRl *
  • Sample ID G405235057 Sample Quantity 1.1583E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 l.482E+Ol 1.845E+OO 6.930E-01 CD-109 2.806E+OO 1.654E+OO l.283E+OO SN-126 1. 772E-01 l.045E-01 8.lOOE-02 CS-135 3.243E-01 2 .113E-01 2.661E-01 BA-137M 2.129E-01 7.556E-02 7.185E-02 CS-137 2.250E-01 7.982E-02 7.590E-02 TL-208 3.217E-01 9. 701E-02 6.547E-02 PB-210 6.549E-01 8.498E-01 6. 972E-01 PB-212 l.160E+OO l.298E-01 9. 511E-02 BI-214 1.112E+OO 1. 964E-01 1.275E-01 PB-214 1.174E+OO 2.030E-01 1.304E-01 RN-222 1.112E+OO 1.964E-01 1. 27 5E-01 RA-224 1.542E+OO l.139E+OO 1. 020E+OO RA-226 1.112E+OO l.964E-01 1. 27 5E-01 AC-228 1.457E+OO 3.470E-01 2.959E-01 RA-228 1.457E+OO 3.470E-01 2.959E-01 TH-228 1.160E+OO 1.298E-01 9. 511E-02 TH-229 -l.705E-01 4.424E-01 7.744E-01 TH-230 1.112E+OO 1. 964E-01 1. 27 5E-01 TH-232 l.457E+00 3.470E-01 2.959E-01 PA-233 9.945E-02 l.057E-01 9.168E-02 TH-234 2.669E+OO 1.171E+OO 8.652E-01 U-234 1.112E+OO 1. 964E-01 l.275E-01 U-235 9.619E-02 3.334E-01 2.876E-01 U-238 2.669E+OO l.171E+OO 8.652E-01 PU-239 5.946E+02 4.330E+02 4.347E+02 AM-243 1.663E-01 6.167E-02 5.094E-02 ANH-511 9.425E-02 9.205E-02 5.649E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -4.080E-01 1.560E+Ol 2.970E+Ol NOT IDENT. NA-22 l.150E-02 5.274E-02 9.900E-02 NOT IDENT. Page 4209 of 5809 NA-24 O.OOOE+OO 1.887E+41 O.OOOE+OO SHORT HLIF AL-26 -2.923E-03 4.248E-02 8. 481E-02 NOT IDENT. SC-46 3.292E-01 4.356E-01 9.297E-01 FAIL ABUN V-48 O.OOOE+OO 2.219E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 6. 096E+02 O.OOOE+OO SHORT HLIF MN-54 -l.825E-02 8.935E-02 1.588E-01 NOT IDENT. C0-56 -1.867E-01 6.254E-01 1.032E+00 FAIL ABUN MN-56 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.356E-02 4.248E-02 7.717E-02 NOT IDENT. C0-58 .,5 .131E-01 8.645E-01 1.246E+OO NOT IDENT. FE-59 -2.163E+OO 7.424E+OO 1.420E+Ol NOT IDENT. C0-60 -6.648E-03 4.244E-02 7.341E-02 NOT IDENT. ZN-65 -3.291E-02 1.991E-01 3.378E-01 NOT IDENT. GE-68 1.482E+OO 2.539E+OO 5.533E+OO NOT IDENT. AS-73 l.372E+00 2.258E+OO 4.518E+OO NOT IDENT. AS-74 O.OOOE+OO 8.017E+03 O.OOOE+OO SHORT HLIF SE-75 -1. 731E-02 2.457E-01 4.334E-01 NOT IDENT. BR-77 O.OOOE+OO 1.296E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 9.019E+02 O.OOOE+OO SHORT HLIF RB-83 5.226E-01 6.834E-01 1.456E+OO NOT IDENT. KR-85 -2.533E+OO 9.981E+00 1. 621E+Ol NOT IDENT. SR-85 -2.890E-01 1.121E+OO 1.820E+OO NOT IDENT. RB-86 O.OOOE+OO 3.750E+04 O.OOOE+OO SHORT HLIF Y-88 2.007E-01 2.412E-01 6. 413E-01 NOT IDENT. Y-91 -4.706E+02 5.827E+02 9.852E+02 NOT IDENT. NB-94 2.358E-02 3.520E-02 7.225E-02 NOT IDENT. NB-95 -6.240E-01 1.155E+OO 1. 971E+00 NOT IDENT. NB-95M -1.684E-01 2. 511E+00 4.468E+OO NOT IDENT. ZR-95 -4.362E-01 1. 798E+OO 3. 251E+OO NOT IDENT. NB-97 O.OOOE+OO 1.642E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 9.557E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 8.332E+40 0.000E+OO SHORT HLIF RH-101 -2.473E-02 2.979E-02 4.689E-02 NOT IDENT. RH-102 5.794E-03 7.128E-02 l.363E-01 FAIL ABUN RU-103 -2.458E+OO 6.735E+OO 1.238E+Ol FAIL ABUN RH-106 -1.378E-01 5.142E-01 9.486E-01 NOT IDENT. RU-106 -1. 378E-01 5.142E-01 9.486E-01 NOT IDENT. AG-108M l.293E-02 2.933E-02 5.944E-02 NOT IDENT. AG-llOM 1.235E-02 l.124E-01 2.164E-01 NOT IDENT. SN-113 -2.551E-02 2.405E-01 4.626E-01 NOT IDENT. CD-115 O.OOOE+OO 2.162E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 0.000E+OO l.254E+05 0.000E+OO SHORT HLIF TE-123M l.236E-02 1.313E-01 2.427E-01 NOT IDENT. SB-124 8.533E-01 2.134E+OO 5.179E+OO NOT IDENT. SB-125 2.586E-03 9. 572E-02 1.885E-01 FAIL ABUN TE-125M 7.125E+Ol 2.584E+02 4.920E+02 NOT IDENT. I-126 O.OOOE+OO 1. 858E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO l.868E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.977E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 9.673E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.470E+27 O.OOOE+OO SHORT HLIF BA-133 3 .118E-.02 4.185E-02 8.175E-02 FAIL ABUN I-133 O.OOOE+OO 1.054E+41 O.OOOE+OO SHORT HLIF CS-134 8.lOOE-02 6.282E-02 1.359E-01 FAIL ABUN I-135 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 4.575E+05 O.OOOE+OO SHORT HLIF CE-139 2.891E-02 l.040E-01 1.959E-01 NOT IDENT. BA-140 O.OOOE+OO 1.950E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.868E+05 O.OOOE+OO SHORT HLIF CE-141 -6.913E+OO 2.633E+Ol 4.381E+Ol NOT IDENT. CE-143 O.OOOE+OO l.002E+41 O.OOOE+OO SHORT HLIF CE-144 6.266E-03 2. 721E-01 4.785E-01 NOT IDENT. PM-144 4.109E-02 6.091E-02 l.259E-01 NOT IDENT. PR-144 3.545E+OO 5.302E+OO 1.095E+Ol NOT IDENT. PM-146 5.332E-02 4.458E-02 9.779E-02 NOT IDENT. ND-147 O.OOOE+OO 4.966E+07 0.000E+OO SHORT HLIF PM-147 -l.960E+02 7.428E+02 l.255E+03 NOT IDENT. PM-149 O.OOOE+OO 5.800E+40 O.OOOE+OO SHORT HLIF EU-150 l.283E-02 3.042E-02 5.234E-02 FAIL ABUN EU-152 9.310E-02 9.925E-02 2. 031E-01 FAIL ABUN GD-153 -5.012E-03 l.443E-01 2.694E-01 NOT IDENT. EU-154 2.812E-02 l.289E-01 2.420E-01 NOT IDENT. EU-155 3.631E-02 8.797E-02 1. 702E-01 FAIL ABUN TB-160 -4.829E-01 2.026E+00 3.683E+OO FAIL ABUN H0-166M -7.540E-03 6.419E-02 1.198E-01 FAIL ABUN TM-171 1.374E-01 4.592E+00 8.916E+OO NOT IDENT. Page 4210 of 5809 HF-172 -2 .133E-02 2.188E-01 3.740E-01 FAIL ABUN LU-172 -4.430E-02 7.225E-02 l.299E-01 FAIL ABUN LU-176 -8.702E-03 2.509E-02 3.893E-02 FAIL ABUN HF-181 -2.728E+00 4.912E+OO 8.827E+OO NOT IDENT. TA-182 -8.829E-01 l.139E+OO 1.940E+OO FAIL ABUN RE-183 2.162E-01 1.000E+OO 1.957E+OO NOT IDENT. RE-184 4.936E+Ol 3.847E+Ol 8.300E+Ol FAIL ABUN W-188 2.368E-01 1.422E+02 2.053E+02 FAIL ABUN IR-192 -2.643E-02 5.317E-01 9.364E-01 FAIL ABUN HG-203 -2.678E-01 3.354E+OQ 4.749E+OO FAIL ABUN BI-207 9.534E-03 5.008E-02 1.035E-01 FAIL ABUN BI-211 O.OOOE+OO 5. 591E-01 1.000E+OO FAIL ABUN PB-211 -1.130E-02 6.654E-01 l.291E+OO NOT IDENT. BI-212 1.310E+OO 7.566E-01 1.425E+OO FAIL ABUN RN-219 -1.032E-01 3.581E-01 6.770E-01 NOT IDENT. RA-223 -2.873E-01 6.702E-01 l.015E+OO FAIL ABUN AC-227 -1.220E-02 2.177E-01 3.902E-01 FAIL ABUN TH-227 -l.220E-02 2.177E-01 3.902E-01 FAIL ABUN PA-231 3.039E-02 5.201E-01 8.531E-01 FAIL ABUN TH-231 -2.873E-01 6.702E-01 1. 015E+OO FAIL ABUN PA-234 4.694E-02 3.417E-01 6.469E-01 FAIL ABUN PA-234M 4.103E+OO 8.086E+OO 1.091E+Ol FAIL ABUN NP-237 9.945E-02 1.057E-01 1.119E-01 FAIL ABUN NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 3.358E-01 3.052E-01 3.731E-01 FAIL ABUN AM-241 2.664E-03 5.058E-02 9.129E-02 NOT IDENT. CM-243 -3.432E-02 7.706E-02 l.402E-01 FAIL ABUN BK-247 '4.861E-02 7.488E-02 1.437E-01 FAIL ABUN CM-247 -1.586E-02 3.372E-02 6.222E-02 FAIL ABUN CF-249 3.662E-02 4.189E-02 8.713E-02 NOT IDENT. CF-251 -9.189E-03 1. 07 6E-01 1.952E-01 FAIL ABUN Page 4211 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:52:05.87 Nuclide Line Activity Report
  • Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 303 10.66* 1.244E+OO 1.482E+Ol 1.482E+Ol 12.70 CD-109 88.03 151 3.70* 8.914E+OO 2. 961E+OO 4.687E+OO 34.81 SN-126 64.28 139 9.60 9.124E+OO 1.029E+OO 1.029E+OO 44.76 86.94 151 8.90 8.914E+OO l.231E+OO l.231E+OO 34.81 87.57 151 37.00* 8.914E+OO 2. 961E-01 2. 961E-01 34.81 CS-135 2 68. 22 40 16.00* 5.038E+OO 3.243E-01 3.243E-01 66.49 BA-137M 661. 66 70 89.90* 2.417E+OO 2.089E-01 2.129E-01 36.21 CS-137 661.66 70 85.10* 2.417E+OO 2.207E-01 2.250E-01 36.21 TL-208 277.37 18 6.60 4.930E+OO 3.652E-01 3.652E-01 163.20 583.19 113 85.00* 2.673E+OO 3.217E-01 3.217E-01 30.77 860.56 ------12.50 1.959E+OO ------Line Not Found ------PB-210 46.54 40 4.25* 9.666E+OO 6.380E-01 6.549E-01 132.41 BI-211 72.87 38 1.23 8.991E+00 2.246E+OO 2.246E+OO 110.80 351.06 261 12.92* 4.043E+OO 3.233E+OO 3.233E+OO 17.65 PB-212 74.82 258 10.28 8.979E+OO 1.815E+OO 1.815E+OO 20.70 77. ll 412 17.10 8.967E+OO 1.741E+OO 1. 741E+OO 14.56 238.63 434 43.60* 5.564E+OO l.160E+OO l.160E+00 11. 42 300.09 29 3.30 4.617E+OO l.239E+OO l.239E+OO 111. 85 BI-214 609.32 201 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 1120.29 28 14.92 1.575E+00 7.645E-01 7.648E-01 86.25 1764.49 38 15.30 1.032E+OO 1.574E+OO 1.574E+OO 31. 23 PB-214 74.82 258 5.80 8.979E+00 3.217E+OO 3.218E+OO 20.70 77 .11 412 9.70 8. 967E+OO 3.070E+OO 3.071E+OO 14.56 87.09 151 3.41 8.914E+OO 3.213E+OO 3.214E+OO 34.81 242.00 133 7.25 5.508E+OO 2.162E+OO 2.162E+OO 27.13 295.22 172 18.42 4.681E+OO 1. 290E+OO 1. 290E+00 23.00 351.93 261 35.60* 4.043E+OO l.173E+OO 1.174E+OO 17.65 RN-222 609.32 201 45.49* 2.581E+OO 1.112E+OO 1.112E+OO 18.02 1120.29 28 14.92 1. 575E+OO 7.645E-01 7.648E-01 86.25 1764.49 38 15.30 1.032E+OO 1. 574E+00 l.574E+00 . 31. 23 RA-224 240.99 133 4.10* 5.508E+OO 3.822E+00 3.822E+OO 27.13 RA-226 609.32 201 45.49* 2.581E+OO l .112E+OO 1.112E+OO 18.02 1120.29 28 14.92 1. 575E+OO 7.645E-01 7.648E-01 86.25 1764.49 38 15.30 1.032E+OO 1.574E+OO 1.574E+OO 31. 23 AC-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 120 11. 27 4.178E+OO 1.645E+OO 1.645E+OO 30.14 794.95 ------4.25 2.087E+OO ------Line Not Found ------835. 71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 108 25.80* 1.870E+OO l.457E+00 1.457E+OO 24.31 968.97 66 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 RA-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 120 11. 27 4.178E+00 1.645E+OO 1.645E+OO 30.14 794.95 ------4.25 2.087E+OO ------Line Not Found ------835.71 ------1. 61 2.005E+00 ------Line Not Found ------911. 20 108 25.80* 1.870E+OO 1.457E+OO 1.457E+OO 24.31 968. 97 66 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 TH-228 74.82 258 10.28 8.979E+OO 1. 815E+OO 1.815E+OO 20.70 Page 4212 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 77 .11 ..412 17.10 8. 967E+OO 1. 741E+OO l.741E;;J-00 14.56 238.63 434 43.60* 5.564E+OO 1.160E+OO 1.160E+OO 11. 42 300.09 29 3.30 4.617E+OO l.239E+00 l.239E+OO 111. 85 TH-229 85.43 151 14.70 8.914E+OO 7.453E-01 7.454E-01 34.81 88.47 128 24.00 8.893E+OO 3.886E-01 3.886E-01 33.02 193.51 ------4.41* 6. 511E+OO ------Line Not Found ------210.85 ------2.80 6 .116E+OO ------Line Not Found ------TH-230 609.32 201 45.49* 2.581E+OO l .112E+00 1.112E+OO 18.02 1120.29 28 14.92 1.575E+OO 7.645E-01 7.645E-01 86.25 1764.49 38 15.30 1.032E+OO l.574E+OO 1.574E+OO 31. 23 TH-232 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 120 11.27 4.178E+OO l.645E+00 1.645E+OO 30.14 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 108 25.80* 1.870E+OO 1.457E+OO 1.457E+OO 24.31 968. 97 66 15.80 1. 779E+OO 1.530E+OO 1.530E+OO 27.95 PA-233 300.13 29 6.63 4.617E+OO 6.166E-01 6.166E-01 111. 85 311. 90 26 38.50* 4.484E+OO 9.945E-02 9.945E-02 108.41 340.48 ------4.45 4.154E+OO ------Line Not Found ------TH-234 63.29 139 3.70* 9.124E+OO 2.669E+OO 2.669E+OO 44.76 92.59 142 4.23 8.869E+OO 2.447E+OO 2.447E+OO 35.39 U-234 609.32 201 45.49* 2.581E+OO l .112E+00 1.112E+OO 18. 02 1120.29 28 14.92 1.575E+OO 7.645E-01 7.645E-01 86.25 1764.49 38 15.30 1.032E+OO 1.574E+OO l.574E+OO 31.23 U-235 89. 96 128 3.47 8.893E+OO 2.688E+OO 2.688E+OO 33.02 93.35 142 5.60 8.869E+OO 1.849E+OO 1.849E+OO 35.39 143.76 13 10. 96* 7.805E+OO 9.619E-02 9.619E-02 353.72 163.33 ------5.08 7.279E+OO ------Line Not Found ------185. 72 97 57.20 6.705E+OO 1.634E-01 l.634E-01 45.99 205.31 ------5.01 6.238E+OO ------Line Not Found ------U-238 63.29 139 3.70* 9.124E+OO 2.669E+OO 2.669E+OO 44.76 92.59 142 4.23 8.869E+OO 2.447E+OO 2.447E+OO 35.39 PU-239 129.30 47 0.01* 8.197E+OO 5.946E+02 5.946E+02 74.31 375.05 19 0.00 3.844E+OO 2.064E+03 2.064E+03 109.17 413.71 ------0.00 3.534E+OO ------Line Not Found ------AM-243 43.53 ------5.90 9.491E+00 ------Line Not Found ------74.66 258 67.20* 8.979E+OO 2.776E-01 2.777E-01 20.70 ANH-511 511. 00 43 100.00* 2.976E+OO 9.425E-02 9.425E-02 99.66 Flag: "*" Key line Page 4213of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235057 Acquisition date 3-0CT-2016 07:51:32 Total number of lines in spectrum 58 Number of unidentified lines 11 Number of lines tentatively identified by NID 47 Nuclide Type : Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 PA-233 TH-234 U-234 U-235 U-238 PU-239 AM-243 ANH-511 Hlif e l.25E+09Y 461. 40D 2.30E+05Y 2.30E+06Y 30.08Y 30.08Y l.41E+l0Y 22.20Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600.00Y l.41E+10Y 1600.00Y 1. 41E+l0Y 1.41E+10Y 1. 41E+10Y 7340.00Y 7.54E+04Y 1. 41E+l0Y 2.14E+06Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 24110. OOY 7370.00Y l.OOE+09Y Decay 1. 00 1. 58 1. 00 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1.00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.482E+Ol 2. 961E+OO 2. 961E-01 3.243E-01 2.089E-01 2.207E-01 3.217E-01 6.380E-01 3.233E+OO l.160E+OO l .112E+OO l.173E+OO 1.112E+OO 3.822E+OO l .112E+00 l.457E+OO l.457E+00 l.160E+OO 3.886E-01 1.112E+OO 1.457E+OO 9.945E-02 2.669E+00 l.112E+OO 9.619E-02 2.669E+OO 5.946E+02 2.776E-01 9.425E-02 6.412E+02 6.412E+02 Decay Corr pCi7GRAM 1.482E+Ol 4.687E+OO 2. 961E-01 3.243E-01 2.129E-01 2.250E-01 3.217E-01 6.549E-01 3.233E+OO l.160E+OO l .112E+00 1.174E+OO 1.112E+00 3.822E+OO 1.112E+OO 1.457E+OO 1.457E+OO 1.160E+OO 3.886E-01 1.112E+OO 1.457E+OO 9.945E-02 2.669E+OO 1.112E+OO 9.619E-02 2.669E+OO 5.946E+02 2.777E-01 9.425E-02 6.429E+02 6.429E+02 81.03% Decay Corr 2-Sigma Error 0.188E+Ol 1.632E+OO 1.031E-01 2.156E-01 0.771E-01 0.814E-01 0.990E-01 8. 672E-01 0. 571E+OO 0.132E+OO 0.200E+OO 0.207E+OO 0.200E+OO 1.037E+OO 0.200E+OO 0.354E+OO 0.354E+OO 0.132E+OO l.283E-01 0.200E+OO 0.354E+OO 10.78E-02 1.194E+OO 0.200E+OO 34.02E-02 1.194E+OO 4.418E+02 0.575E-01 9.393E-02 "M" Manually accepted
  • 2-Sigma %Error 12.70 34.81 34.81 66.49 36.21 36.21 30.77 132. 41 17.65 11. 42 18.02 17.65 18.02 27.13 18.02 24.31 24.31 11. 42 33.02 18.02 24.31 108.41 44.76 18. 02 353.72 44.76 74.31 20.70 99.66 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4214 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235057 Acquisition date : 3-0CT-2016 07:51:32 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 31. 49 26 104 0.53 64.83 63 6 6.56E-03 **** 1. 49E+OO 5 83.62 60 126 0. 96 169.01 166 27 1.55E-02 66.8 8.93E+OO T 0 117. 65 35 77 1. 66 237.01 234 7 9.18E-03 92.7 8.46E+OO T 3 U0.85 38 61 1.17 263.40 256 13. 9. 96E-03 86.3 8.15E+OO T 0 209.04 36 91 1. 04 419.68 416 8 9.61E-03 99.9 6.15E+OO 0 231. 76 21 70 1. 82 465.07 462 7 5.69E-03 **** 5.69E+OO 0 284.39 15 65 4.54 570.27 562 11 4. llE-03 **** 4.82E+OO T 0 287.37 42 31 2.31 576.23 572 10 1.14E-02 59.2 4.78E+OO T 0 327.51 29 36 1. 59 656.45 653 7 7.95E-03 78.2 4.29E+OO T 0 463 .11 33 26 1.17 927.48 924 8 9.36E-03 62.8 3.22E+OO T 0 665.98 21 14 1. 75 1332.95 1329 11 5.90E-03 85.0 2.40E+OO T 0 727.39 30 15 2.33 1455.68 1451 10 8. 61E-03 59.0 2.24E+OO T 0 802.80 18 7 0.66 1606.41 1601 9 5.03E-03 76.2 2.07E+OO T 0 806.83 18 6 0.95 1614.45 1611 8 5.28E-03 67.4 2.06E+OO 0 842.74 21 11 2.80 1686.23 1681 11 6.llE-03 72.3 1. 99E+OO 0 904.18 14 6 0.91 1809.04 1805 8 3.95E-03 79.5 1.88E+OO T 0 957.80 11 7 0.95 1916.20 1913 8 3.12E-03 **** 1.80E+OO 0 964.81 13 6 1. 01 1930.22 1927 7 3.82E-03 82.6 l.78E+OO T 0 1000.86 9 17 0.67 2002.27 1992 14 2.66E-03 **** 1.73E+OO T 0 1006.36 7 2 1.10 2013.27 2010 6 2.06E-03 **** 1. 72E+OO 0 1021.14 8 14 1. 42 2042.80 2039 9 2.19E-03 **** 1.70E+OO T 0 1045.66 8 '5 0.62 2091.82 2087 8 2.43E-03 **** 1. 67E+OO T 0 1239.14 22 24 1. 40 2478.53 2473 14 6.47E-03 99.6 1. 44E+OO T 0 1279.37 5 11 4.20 2558.95 2549 12 l.39E-03 **** 1. 40E+OO 0 1285.23 6 2 0.64 2570.67 2567 7 l.74E-03 **** 1. 40E+OO 0 1337.51 6 8 1. 34 2675.16 2668 11 1.85E-03 **** 1. 35E+OO 0 1396. 44 7 2 0.70 2792.94 2788 9 2.19E-03 98.3 1.30E+OO 0 1408.26 11 0 1. 74 2816.58 2812 10 3.33E-03 57.7 1.29E+OO T Flags: "T" = Tentatively associated Page 4215 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:52:20.43 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l *
  • Acquisition date 3-0CT-2016 07:51:32 Sensitivity 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:55:00 Nuclide Library : SOLID *
  • Sample ID G405235057 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.1583E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 PA-233 TH-234 U-234 U-235 U-238 PU-239 AM-243 ANH-511 Le (pCi/GRAM 2.807E-01 5.988E-01 3.779E-02 l.221E-01 3.180E-02 3.360E-02 2.887E-02 3.262E-01 4.390E-02 5.627E-02 5.906E-02 5.627E-02 4. 711E-01 5.627E-02 l.298E-01 1.298E-01 4.390E-02 3.563E-01 5.625E-02 1.298E-01 4.070E-02 4.061E-01 5.625E-02 l.334E-01 4. 061E-0'1 2.001E+02 2.399E-02 2.529E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4216 of 5809 Le (pCi/GRAM 1.341E+Ol 4.175E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 4217 of 5809 3.373E-02 4.073E-01 O.OOOE+OO 0.000E+OO 7.079E-02 4.475E-01 O.OOOE+OO 3.588E-02 5.376E-01 5. 971E+OO 2.950E-02 1. 429E-01 2.402E+OO 2.130E+00 O.OOOE+OO 1.995E-01 O.OOOE+OO 0.000E+OO 6.498E-01 7.381E+OO 8.288E-01 O.OOOE+OO 2.560E-01 4.076E+02 3. 231E-02 8.736E-01 2.060E+OO 1.422E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.155E-02 6.084E-02 5.488E+OO 4.127E-01 4.127E-01 2.685E-02 9. 351E-02 2.082E-01 O.OOOE+OO O.OOOE+OO 1.129E-01 2.016E+OO 8.363E-02 2.307E+02 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.712E-02 O.OOOE+OO 6.144E-02 O.OOOE+OO 0.000E+OO 9.077E-02 O.OOOE+OO O.OOOE+OO 2.030E+Ol O.OOOE+OO 2.183E-01 5. 613E-02 4.882E+OO 4.430E-02 O.OOOE+OO 5.810E+02 0.000E+OO 2.396E-02 9.314E-02 1.263E-01 1.020E-01 7. 963E-02 1.558E+OO 5. 281E-02 4.187E+OO 1. 740E-01 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 , BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 PA-231 TH-231 PA-234 PA-234M NP-237 NP-238 NP-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4218of5809 5.316E-02 1. 738E-02 3.893E+OO 8.289E-01 9.206E-01 3.664E+Ol 9.300E+Ol 4.255E-01 2.165E+OO 4.450E-02_ 4.835E-01 5.806E-01 6.538E-01 3.016E-01 4.564E-01 1. 773E-01 1. 773E-01 3.907E-01 4.564E-01 2.832E-01 4.853E+00 5.080E-02 O.OOOE+OO 1.733E-01 4.294E-02 6.512E-02 6.610E-02 2. 772E-02 3.998E-02 9.015E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN* FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:52:26.17 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235057.CNF;l * *Acquisition date 3-0CT-2016 07:51:32 Sensitivity 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 2-DEC-2015 14:55:00 Nuclide Library : SOLID *
  • Sample ID G405235057 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.1583E+02 GRAM *
  • Quantity Err(%) : 1.7266E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN '*
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) K-40 1. 482E+Ol 2.00lE+OO 2.00lE+OO CD-109 2.806E+OO 1.687E+OO 1.687E+OO SN-126 1. 772E-01 1. 061E-01 1.061E-01 CS-135 3.243E-01 2.124E-01 2.124E-01 BA-137M 2.129E-01 7. 611E-02 7. 611E-02 CS-137 2.250E-01 8.040E-02 8.040E-02 TL-208 3.217E-01 9.798E-02 9.798E-02 PB-210 6.549E-01 8.519E-01 8.519E-01 PB-212 1.160E+OO 1.437E-01 1.437E-01 BI-214 1.112E+OO 2.021E-01 2. 021E-01 PB-214 1.174E+OO 2.088E-01 2.088E-01 RN-222 l .112E+OO 2. 021E-01 2.021E-01 RA-224 1. 542E+OO 1.152E+OO 1.152E+00 RA-226 1.112E+OO 2.021E-01 2.021E-01 AC-228 1. 457E+OO 3.549E-01 3.549E-01 RA-228 1.457E+OO 3.549E-01 3.549E-01 TH-228 1.160E+OO 1.437E-01 1.437E-01 TH-229 -1.705E-01 4.425E-01 4.425E-01 TH-230 1.112E+OO 2. 021E-01 2. 021E-01 TH-232 1.457E+OO 3.549E-01 3.549E-01 PA-233 9.945E-02 1.058E-01 1.058E-01 TH-234 2.669E+OO 1.311E+OO 1. 311E+00 U-234 1.112E+OO 2. 021E-01 2. 021E-01 U-235 9.619E-02 3.335E-01 3.335E-01 U-238 2.669E+OO 1. 311E+OO 1. 311E+00 PU-239 5.946E+02 4.338E+02 4.338E+02 AM-243 1.663E-01 6.408E-02 6.408E-02 ANH-511 9.425E-02 9.213E-02 9.213E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) BE-7 -4.080E-01 1.560E+Ol 1.560E+Ol NOT IDENT. NA-22 1.150E-02 5.274E-02 5.300E-02 NOT IDENT. Page 4219of5809 NA-24 1.000E+41 l.939E+41 0.000E+OO SHORT HLIF AL-26 -2.923E-03 4.248E-02 4.250E-02 NOT IDENT. SC-46 3.292E-01 4.358E-01 4.604E-01 FAIL ABUN V-48 -7.745E+03 2.219E+04 2.246E+04 SHORT HLIF CR-51 -4.315E+02 6.099E+02 6.401E+02 SHORT HLIF MN-54 -1.825E-02 8.935E-02 8.973E-02 NOT IDENT. C0-56 -l.867E-01 6.254E-01 6.311E-01 FAIL ABUN MN-56 -1.000E+41 3.275E+41 O.OOOE+OO SHORT HLIF C0-57 -l.356E-02 4.248E-02 4.292E-02 NOT IDENT. C0-58 -5.13c1E-01 8.648E-01 8.952E-01 NOT JDENT. FE-59 -2.163E+OO 7.425E+OO 7.489E+OO NOT IDENT. C0-60 -6.648E-03 4.244E-02 4.254E-02 NOT IDENT. ZN-65 -3.291E-02 1. 991E-01 1. 996E-01 NOT IDENT. GE-68 1.482E+OO 2.539E+OO 2.626E+OO NOT IDENT. AS-73 1. 372E+OO 2.275E+OO 2.358E+OO NOT IDENT. AS-74 l.536E+03 8.018E+03 8.048E+03 SHORT HLIF SE-75 -1.731E-02 2.457E-01 2.458E-01 NOT IDENT. BR-77 1.158E+39 l.022E+40 O.OOOE+OO SHORT HLIF SR-82 5.007E+02 9.022E+02 9.300E+02 SHORT HLIF RB-83 5.226E-01 6. 872E-01 7.264E-01 NOT IDENT. KR-85 -2.533E+OO 9. 981E+OO 1.005E+Ol NOT IDENT. SR-85 -2.890E-01 1.121E+OO l.129E+OO NOT IDENT. RB-86 l.513E+04 3.751E+04 3.812E+04 SHORT HLIF Y-88 2.007E-01 2.416E-01 2.580E-01 NOT IDENT. Y-91 -4.706E+02 5.830E+02 6.204E+02 NOT IDENT. NB-94 2.358E-02 3.522E-02 3.679E-02 NOT IDENT. NB-95 -6.240E-01 1.156E+OO l.189E+OO NOT IDENT. NB-95M -l.684E-01 2. 511E+OO 2.512E+00 NOT IDENT. ZR-95 -4.362E-01 1. 798E+OO 1.809E+OO NOT IDENT. NB-97 l.OOOE+41 l.642E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 2.092E+41 O.OOOE+OO SHORT HLIF M0-99 -4.577E+31 9.557E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 8.390E+40 O.OOOE+OO SHORT HLIF RH-101 -2.473E-02 3.013E-02 3.212E-02 NOT IDENT. RH-102 5.794E-03 7.128E-02 7.133E-02 FAIL ABUN RU-103 -2.458E+00 6.736E+OO 6.826E+OO FAIL ABUN RH-106 -l.378E-01 5.143E-01 5.180E-01 NOT IDENT. RU-106 -1.378E-01 5.143E-01 5.180E-01 NOT IDENT. AG-108M l.293E-02 2.933E-02 2.991E-02 NOT IDENT. AG-llOM l.235E-02 l.124E-01 1.125E-01 NOT IDENT. SN-113 -2. 551E-02 2.405E-01 2.407E-01 NOT IDENT. CD-115 1. 871E+40 2.190E+40 O.OOOE+OO SHORT HLIF SN-ll 7M -5. 451E+04 l.256E+05 l.280E+05 SHORT HLIF TE-123M 1.236E-02 1. 313E-01 1.315E-01 NOT IDENT. SB-124 8.533E-01 2.134E+00 2.169E+00 NOT IDENT. SB-125 2.586E-03 9. 572E-02 9.573E-02 FAIL ABUN TE-125M 7.125E+Ol 2.584E+02 2.604E+02 NOT IDENT. I-126 2.231E+06 1.884E+06 2.135E+06 SHORT HLIF SB-126 -1.558E+06 l.891E+06 2.017E+06 SHORT HLIF SB-127 -3.139E+22 9 .110E+22 O.OOOE+OO SHORT HLIF I-131 2.122E+08 9.673E+09 9.674E+09 SHORT HLIF I-132 l.000E+41 1.939E+42 O.OOOE+OO SHORT HLIF TE-132 5.883E+26 l.490E+27 O.OOOE+OO SHORT HLIF BA-133 3 .118E-02 4.187E-02 4.417E-02 FAIL ABUN I-133 1.000E+41 2.124E+41 O.OOOE+OO SHORT HLIF CS-134 8.lOOE-02 6.291E-02 7.274E-02 FAIL ABUN I-135 . 1.000E+41 1.132E+42 O.OOOE+OO SHORT HLIF CS-136 -2.198E+05 4.581E+05 4.687E+05 SHORT HLIF CE-139 2. 891E-02 l.042E-01 1.050E-01 NOT IDENT. BA-140 -7.912E+05 1.950E+06 1.982E+06 SHORT HLIF LA-140 -3.570E+04 6.868E+05 6.870E+05 SHORT HLIF CE-141 -6.913E+OO 2.634E+Ol 2.652E+Ol NOT IDENT. CE-143 1.000E+41 1.007E+41 O.OOOE+OO SHORT HLIF CE-144 6.266E-03 2.721E-01 2. 721E-01 NOT IDENT. PM-144 4.109E-02 6.096E-02 6.371E-02 NOT IDENT. PR-144 3.545E+OO 5.j04E+OO 5.539E+OO NOT IDENT. PM-146 5.332E-02 4.475E-02 5.079E-02 NOT IDENT. ND-147 -3.013E+07 4. 969E+07 5 .151E+07 SHORT HLIF PM-147 -1. 960E+02 7.429E+02 7. 481E+02 NOT IDENT. PM-149 1.000E+41 6. 211E+40 O.OOOE+OO SHORT HLIF EU-150 l.283E-02 3.042E-02 3.097E-02 FAIL ABUN EU-152 9.310E-02 9.938E-02 l.079E-01 FAIL ABUN GD-153 -5.012E-03 1.443E-01 1.443E-01 NOT IDENT. EU-154 2.812E-02 1.289E-01 l.295E-01 NOT IDENT. EU-155 3. 631E-02 8.801E-02 8.952E-02 FAIL ABUN TB-160 -4.829E-01 2.026E+00 2.038E+OO FAIL ABUN H0-166M -7.540E-03 6.419E-02 6.428E-02 FAIL ABUN TM-171 l.374E-01 4.592E+00 4.593E+OO NOT IDENT. Page 4220 of 5809 HF-172 -2.133E-02 2.188E-01 2.190E-01 FAIL ABUN LU-172 -4.430E-02 7.239E-02 7.510E-02 FAIL ABUN LU-176 -8.702E-03 2.509E-02 2.540E-02 FAIL ABUN HF-181 -2. 728E+OO 4.914E+00 5.065E+OO NOT IDENT. TA-182 -8.829E-01 1.140E+OO l.207E+OO FAIL ABUN RE-183 2.162E-01 1.00lE+OO 1.006E+OO NOT IDENT. RE-184 4.936E+Ol 4. 031E+Ol 4.604E+Ol FAIL ABUN W-188 2.368E-01 l.422E+02 1.422E+02 FAIL ABUN IR-192 -2.643E-02 5.317E-01 5.319E-01 FAIL ABUN .HG-203 -2.678E-01 3.354E+OO 3.356E+OO FAIL ABUN BI-207 9.534E-03 5.008E-02 5.027E-02 FAIL ABUN BI-211 3.233E+OO 5.776E-01 l.568E+00 FAIL ABUN PB-211 -l.130E-02 6.654E-01 6.654E-01 NOT IDENT. BI-212 1.310E+OO 7.595E-01 9.619E-01 FAIL ABUN RN-219 -l.032E-01 3.583E-01 3.613E-01 NOT IDENT. RA-223 -2.873E-01 6.705E-01 6.829E-01 FAIL ABUN AC-227 -1. 220E-02 2.177E-01 2.177E-01 FAIL ABUN TH-227 -1. 220E-02 2.177E-01 2.177E-01 FAIL ABUN PA-231 3.039E-02 5.201E-01 5.203E-01 FAIL ABUN TH-231 -2.873E-01 6.705E-01 6.829E-01 FAIL ABUN PA-234 4.694E-02 3.459E-01 3.466E-01 FAIL ABUN PA-234M 4.103E+OO 8.088E+OO 8.296E+00 FAIL ABUN NP-237 9.945E-02 1.058E-01 1.149E-01 FAIL ABUN NP-238 -1.000E+41 2.483E+41 O.OOOE+OO SHORT HLIF NP-239 3.358E-01 3.064E-01 3.418E-01 FAIL ABUN AM-241 2.664E-03 5.058E-02 5.060E-02 NOT IDENT. CM-243 -3.432E-02 7.712E-02 7.866E-02 FAIL ABUN BK-247 4.861E-02 7. 551E-02 7.863E-02 FAIL' ABUN CM-247 -l.586E-02 3.382E-02 3.457E-02 FAIL ABUN CF-249 3.662E-02 4.199E-02 4.512E-02 NOT IDENT. CF-251 -9.189E-03 1.076E-01 1.076E-01 FAIL ABUN Page 4221of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 63.4503 87.09 64.9837 136.47 47.6878 45.60 70.4172 87.57 65. 0611 140.51 0.0000 46.54 70.6720 88.03 65.1345 143.76 55.1985 49.72 0.0000 88.34 65.1836 144.24 55.2438 51.35 79.8433 88.47 65.2045 145.44 59.3106 51. 87 76.8232 89. 96 65.4405 152.43 59.0054 52.39 69.0301 1093.63 65.5477 153.25 0.0000 52.97 68.3754 91.11 0.0000 323.87 52.1555 53.44 66.8949 92.59 65.8526 156.02 0.0000 54.07 59.8580 93.35 65.9706 158.56 0.0000 57.36 0.0000 94. 56 60.7934 159.00 57.6123 57.53 72.6732 94.65 60.8063 162.33 46.7384 57.98 78.4414 94.67 60.8089 162.66 0.0000 59.27 77.9597 94.87 60.8369 163.33 45.7938 59.32 77.9725 97.43 71.0959 165.86 48.0169 59.54 82.3627 98.43 80.2770 176.31 52.9276 60. 96 83.8263' 98.44 80.2787 176.60 0.0000 61.17 77.6180 99.53 56.0621 177.52 50.9417 62.93 78.0475 100 .11 66.9998 181.07 0.0000 63.29 78.1346 102.03 59.1021 181.52 43.2210 63.58 78.2046 103.18 61. 0745 184.41 49.3494 64.28 86.8973 103.37 66. 5712 143.76 49.4412 66.73 89.7589 105.21 57.6816 193.51 52.1059 67.24 99.0508 105.31 61.3572 197.03 49.1501 125.81 91.6787 106.12 67.8857 198.01 72.7522 67.75 86.6955 106.47 79.8712 201.83 69.8976 69.67 86.0665 109.28 69.2648 203.43 56.0363 70.83 77.3814 111. 00 58.3915 205.31 56.1752 72. 81 87.1200 111.76 0.0000 210.85 53.6776 72. 87 87.1349 114. 06 49.7428 215.65 38.3149 74.66 87.5687 116. 30 0.0000 222 .11 39. 7271 74.82 87. 6072 116.74 62.5153 227.09 48.8514 74.97 87.6434 119.76 44.0227 227.38 51.0895 77 .11 88.1549 121.12 58.0124 228.16 0.0000 78.74 88.5400 121. 22 58.0236 228.18 38.5398 79.69 83.8790 121.78 57.7706 116.74 38.5398 80.12 86.2740 122.06 65.3829 235.69 48.2326 80.19 0.0000 122.92 51.2541 235. 96 48.2484 80.57 82.9204 123.07 51.2689 238.63 48.3986 81. 00 67.4484 265.00 64.6361 238.98 0.0000 81. 07 67.4609 125.81 62.3536 240.99 48.5312 81. 75 94.7266 127.23 61.2439 242.00 45.1984 83.79 64.4496 127.91 45.0335 244.70 40.8043 84.00 64.4841 129.30 45.1497 252.40 0.0000 85.43 64.7167 131. 20 45.3082 252.80 41.1784 86.55 64.8974 133.02 41.2676 254.15 0.0000 86.79 64.9357 133.52 36.1416 256.23 34.4458 86.94 64. 9600 136.00 48.6206 260.90 0.0000 Page 4222 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 46.3501 355.39 0.0000 584.27 18.7271 264.80 46.3574 356.01 21.4866 595.83 0.0000 265.00 32.4570 364.49 0.0000 427.87 28.8466 268.22 41. 8744 366.42 0.0000 602.52 0.0000 269.46 35.7176 372. 51 30.7537 604. 72 26.9176 270.03 35.7391 375.05 34.6704 607.14 J.7.9692 271.23 35.7840 377.52 36.0262 609.32 18.9900 273.65 0.0000 356.01 38.7964 610.33 19.0008 276.40 35.9777 388.16 27.6829 614.28 13.5297 277.37 36.0142 388.63 0.0000 618.01 15.0629 277.60 36.0227 391.69 28.6279 620.36 20.1099 278.00 36.0376 264.66 23. 5871 621. 93 18 .1143 279.20 37.6514 401. 81 26.2311 630.19 0.0000 279.54 37.6641 402.40 28.8669 631.29 20.2271 279.70 37.6699 404.85 27.1685 633.25 21. 2606 280.46 37.6997 410.95 45.7846 634.78 0.0000 283.69 30.7322 413.71 30.8806 635.95 17.2359 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 4.7363 423.72 0.0000 645.85 23.4399 285.90 0.0000 427.09 16.0400 657.76 10.7670 287.50 26.8952 427.87 20.5073 657.90 0.0000 290.67 30.9488 433.94 23.2848 661.66 20.0356 293.27 0.0000 439.40 17.9818 664.57 0.0000 351.93 31. 8856 453.88 15.4415 666.33 0.0000 295.96 21.5387 463.37 23.7720 666.50 0.0000 879.38 23.9929 468.07 30.2688 667. 71 0.0000 299.98 35.2380 473.00 0.0000 677.62 14. 5013 300.09 35.2415 475.06 28.5687 685.70 0.0000 300.13 35.2433 476.78 24.9115 695.00 0.0000 301.36 38.4932 477.60 29.5404 696.49 14.6369 302.85 40.1550 482.18 25.9270 696. 51 14.6375 256.23 38.6094 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.9188 306.78 29.0208 497.08 25.2460 697.49 23.0125 308.46 29.0669 505.52 22.5630 702.65 15.7300 311. 90 21. 0615 507.63 0.0000 706.68 22.0647 316.51 34.1694 511. 00 24.5284 711. 68 17.9048 319.41 0.0000 514.00 39.6980 720. 70 0.0000 320.08 0.0000 514.00 39.6980 721.93 0.0000 321. 04 20.8329 520.40 14.2346 722.78 15.8820 323.87 34.4027 520.69 0.0000 722.91 12.7065 325.23 18.0428 522.65 0.0000 723.31 14.2976 328.76 0.0000 527.90 0.0000 724.19 9.5358 333.37 38.0039 528.26 13.3506 727.33 14.8551 333.97 31. 4115 529.59 13.3614 733.00 14.8949 334.37 28.1147 529.87 0.0000 735.93 17.0462 338.28 23.6491 531.02 0.0000 333.97 13.8596 338.32 23.6497 537.26 0.0000 739.50 0.0000 311. 90 24.9420 546.56 0.0000 747.24 13.9225 340.48 24.9420 552.55 19.3538 748.06 18.2133 340.55 0.0000 563.25 25.3187 752.31 20.3962 344.28 26.0260 569.33 17.5906 753.82 0.0000 345.93 36.7562 946.00 17.5928 756.73 19.3616 351.06 31. 0456 569.70 15.6393 756.80 19.3623 351.93 31. 0689 583.19 18. 7163 884.68 18.3461 Page 4223 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 28.0820 1274.44 8.5321 1620.50 2.1292 766.42 25.9287 1001.03 12.4641 1621. 92 6.3896 766.84 20.5308 1002.74 14.2534 1678.03 0.0000 772.60 0.0000 1004.73 3.5658 1690.97 2.1642 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 J.025.87 0.0000 1764.49 4 .. 3999 778.90 10.8643 1028.54 0.0000 1063.66 4.4053 783.70 0.0000 1037.84 9.0192 1771. 35 3.3049 785.37 25.0599 1038.76 0.0000 1791.20 0.0000 792.07 21. 8555 631.29 10.1322 1808.65 5.5527 794.95 18.6007 1048.07 0.0000 1810.72 0.0000 795.86 13.1353 1049.04 17.3848 1836.06 1.1170 810.06 16.5204 1050.41 18.6353 810.29 19.8259 1063.66 10.9197 344.28 19.8274 1077.00 0.0000 810.76 21. 4828 1077.34 9.1425 815.77 0.0000 1085.87 17.4205 1048.07 0.0000 1093.63 11. 9503 832.01 15.5632 1099.45 11. 9733 834.85 25.5989 1112. 07 11. 0984 835. 71 24.4949 1112. 84 12.3340 836.80 0.0000 1115. 54 11. 8516 846.75 o. ooo*o 1120.29 12.0550 846.77 13.4224 1120.55 12.0566 856.80 0.0000 1221.41 12.0590 860.56 19.1236 1129. 67 17.6733 871.09 12.4269 1131.51 0.0000 873.19 6.7842 1147.95 0.0000 875.33 0.0000 1173.23 16.9761 879.38 12.4685 1177.95 9.4452 880.51 15.8765 1189.05 12.3216 883.24 13.6230 1204.77 15.2383 884.68 12.4950 1221.41 20.1015 889.28 9.1042 1231.02 18.2404 9.1237 1235.36 0.0000 898.04 15.9875 1238.28 12.5073 900. 72 12.0031 1260.41 0.0000 903.28 17.1643 1271.87 3.1094 911.20 17.2180 1274.44 7.7793 912.08 17.2235 1274.54 7.7793 923.98 0.0000 1291.59 8.7951 926.50 17.3199 1298.22 0.0000 929 .11 15.0254 1312 .11 0.0000 937.49 18.5521 1332.49 6.3273 944 .13 0.0000 1362.66 0.0000 946.00 15.1222 1365.19 5.9861 949.00 13.9746 1368. 63 0.0000 667.71 0.0000 1384.29 2.0057 962. 31 10.5333 1408.01 6.0557 964. 08 12.6483 1457.56 0.0000 966 .17 3.5161 1460.82 6.1403 911.20 8.4475 1489.16 10.3088 968. 97 8.4475 1505.03 6.2102 983.53 0.0000 1584.12 9.4982 984.45 0.0000 1596.21 0.0000 Page 4224 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:52:57.76 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA. GAMMA.ARCHIVE. GAMMA] G405235058. CNF; '1 Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM06.CNF;499 Background date : Z-OCT-2016 11:00:12. Sample date 2-DEC-2015 15:00:00. Acquisition date : 3-0CT-2016 07:51:57. Sample ID G405235058 Sample quantity 1.40622E+02 GRAM Detector name GAM06 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.66 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 4 4 4 0 3 3 0 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 63.38* 74.89* 77.17 79.22 87.15 89.98 92.87* 102.61 129.51 153.61 177.33 185.74* 209.36 238.57*

241.97* 289.24 295.20* 314.64 338.31 351.91 358.65 401.80 408.85 463.77 546.34 583.42* 609.15* 614.41 637.75 782.94 860.04* 911. 12* 967.76 1070.72 Page 4225 of 5809 BACKGROUND* CORRECTED SAMPLE PEAK REPORT Area 25 124 202 51 60 65 76 24 27 30 25 66 52 359 100 42 129 8 71 239 20 39 33 32 10 73 160 8 20 9 15 43 89 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 133 128 88 87 120 94 129 88 161 81 64 127 96 46 62 55 58 52 70 57 45 73 56 33 12 48 35 11 13 11 8 35 19 8 1. 24 1. 36 1.14 1. 37 1. 49 1.13 1. 28 1. 23 0. 96 0.86 0.86 1. 23 1.19 1.18 1. 70 2.13 1. 27 0.69 1.18 1. 06 1. 42 6.83 3.49 1. 61 1. 41 0.82 1. 32 1. 72 0.92 1.11 1. 25 1. 63 4.91 1. 02 126.47 149.48 154.03 158.13 173.97 179.63 185.40 204.88 258.63 306.80 354.20 370.99 418.21 476.59 483.37 577.85 589.77 628.63 675.94 703.12 716.60 802.84 816.93 926. 71 1091. 7 9 1165. 92 1217.36 1227.87 1274.53 1564.83 1719.00 1821.14 1934.42 2140.32 123 143 143 143 171 177 177 200 253 304 349 365 412 469 469 573 585 622 670 697 712 788 810 921 1088 1157 1212 1224 1269 1558 1715 1814 1924 2132 8 7.03E-03 83.l 19 3.43E-02 18.8 l.73E+OO 19 5. 60E-02 11. l 19 1.41E-02 44.5 6 1.67E-02 31.6 14 l.80E-02 24.7 2.15E+00 14 2.12E-02 30.3 8 6.65E-03 71.4 12 7.57E-03 95.3 7 8.19E-03 53.7 8 7.06E-03 58.5 11 1.84E-02 35.9 10 1. 44E-02 38 .1 24 9.97E-02 6.3 l.28E+OO 24 2.79E-02 19.8 13 1.18E-02 39.3 10 3.58E-02 14.4 8 2.22E-03160.l 13 l.99E-02 26.7 12 6.64E-02 9.0 9 5.56E-03 64.5 22 1. 08E-02 59. 4 18 9.03E-03 56.0 12 9.00E-03 40.6 8 2. 65E-03 71. l 16 2.04E-02 24.4 13 4.46E-02 11.4 8 2.17E-03 79.9 13 5.45E-03 44.2 9 2.43E-03 76.9 8 4.03E-03 44.7 14 l.19E-02 33. 2 20 2.47E-02 16.2 11 2.66E-03 66.6 Peak Search Report (continued) Page : 2 Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1074.01 7 4 1.12 2146.91 2144 6 1.89E-03 61. 8 36 0 1119. 38 47 0 1. 63 2237.66 2232 11 1.31E-02 14.6 37 0 1184.25 16 8 3.85 2367.40 2361 12 4.46E-03 44.5 38 0 1211.50 10 19 4.02 2421.91 2411 13 2.76E-03 96. 8 39 0 1238.54* 13 20 0.96 2476.01 2466 14 3.63E-03 79.6 40 0 1274.57 13 8 0.59 2548.08 2541 15 3.68E-03 52.9 41 0 1280.43 13 4 2.12 2559.80 2555 9 3.58E-03 40.4 42 0 1291.47 8 0 1*. 35 2581. 88 2579 6 2.22E-03 35.4 43 0 1459.92* 268 5 2.15 2918.87 2911 18 7.43E-02 6.5 44 0 1558.82 8 0 0.88 3116.75 3111 11 2.22E-03 35.4 45 0 1764.00 29 6 2.40 3527.33 3522 11 7.92E-03 24.6 Flag: "*" = Peak area was modified by background subtraction Page 4226 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:53:00 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 2-DEC-2015 15:00:00 G405235058 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 07:51:57 140.62 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA6 0 01:00:00.00 1.50 keV No Empirical 75.00 Interference Report Interfering Nuclide Page 4227 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.66 10.00 0.00 % Peak Energy 0.0% Nuclide Line Activity Report Page : 2 Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status NA-22 1274.54 99.94* 1.136E+OO 6 .. 042E-02 7.552E-02 105.89 OK K-40 1460.82 10.66* 1.005E+OO 1.278E+Ol 1.278E+Ol 12. 92 OK CD-109 88.03 3.70* 5.194E+OO 1.008E+OO 1. 596E+OO 129.43 OK SN-126 64.28 9.60 2.650E+OO 6.557E-01 6.557E-01 166.19 OK 86.94 8.90 5.194E+OO 4.192E-01 4.192E-01 129.43 OK 87.57 37.00* 5.194E+OO 1.008E-01 1.008E-01 129.43 OK TL-208 277.37 6.60 3.958E+OO Line Not Found Absent 583.19 85.00* 2.242E+OO 2.136E-01 2 .136E-01 48.76 OK 860.56 12.50 1.625E+OO 3.833E-01 3.833E-01 89.41 OK BI-211 72. 87 1. 23 3.859E+OO Line Not Found Absent 351. 06 12.92* 3.304E+OO 2.400E-01 2.400E-01 435.46 OK PB-212 74.82 10.28 4.088E+OO 1.302E+OO 1.302E+OO 56.98 OK 77 .11 17.10 4.331E+OO 1.770E+OO 1. 770E+00 22.26 OK 238.63 43.60* 4.430E+OO 1. llOE+OO 1.llOE+OO 12.54 OK 300.09 3.30 3. 729E+OO Line Not Found Absent BI-214 609.32 45.49* 2.167E+OO 8.998E-01 9.00lE-01 22.81 OK 1120.29 14.92 1. 281E+OO 1.290E+OO 1.290E+OO 29.17 OK 1764.49 15.30 8.593E-01 1.090E+OO 1. 091E+OO 49.19 OK PB-214 74.82 5.80 4.080E+OO Line Not Found <<INT Reject 77 .11 9.70 4.331E+OO 3.121E+00 3.122E+00 22.26 OK 87.09 3.41 5.190E+OO Line Not Found <<INT Reject 242.00 7.25 4.384E+OO Line Not Found <<INT Reject 295.22 18.42 3.776E+OO 1.089E+00 1.090E+00 28.83 OK 351. 93 35.60* 3.304E+00 Line Not Found <<INT Reject RN-222 609.32 45.49* 2.167E+00 8.998E-01 9.00lE-01 22.81 OK 1120.29 14.92 1.281E+OO 1.290E+00 1.290E+OO 29.17 OK 1764.49 15.30 8.593E-01 1.090E+OO 1.091E+OO 49.19 OK RA-224 240.99 4.10* 4.384E+OO 1.403E+OO 1.403E+OO 102.14 OK RA-226 609.32 45.49* 2.167E+OO 8.998E-01 9.00lE-01 22.81 OK 1120.29 14.92 1.281E+OO 1.290E+OO 1.290E+OO 29.17 OK 1764.49 15.30 8.593E-01 1.090E+OO 1. 091E+OO 49.19 OK AC-228 105.21 1.10 6.007E+OO Line Not Found Absent 338.32 11. 27 3.404E+OO 1.082E+OO 1.082E+00 53.31 OK 794.95 4.25 1.739E+00 Line Not Found Absent 835.71 1. 61 1.666E+00 Line Not Found Absent 911.20 25.80* 1.544E+OO 5.761E-01 5.761E-01 66.46 OK 968. 97 15.80 1. 463E+OO 2.045E+OO 2.045E+00 32.42 OK RA-228 105.21 1.10 6.007E+OO Line Not Found Absent 338.32 11. 27 3.404E+OO 1.082E+00 1.082E+OO 53.31 OK 794.95 4.25 1. 739E+OO Line Not Found Absent 835.71 1. 61 l.666E+00 Line Not Found Absent 911.20 25.80* 1.544E+OO 5.761E-01 5.761E-01 66.46 OK 968. 97 15.80 1.463E+OO 2.045E+OO 2.045E+OO 32.42 OK TH-228 74.82 10.28 4.088E+OO 1.302E+OO 1.302E+OO 56.98 OK 77 .11 17.10 4.331E+00 1.770E+OO 1.770E+OO 22.26 OK 238.63 43.60* 4.430E+OO 1. llOE+OO 1. llOE+OO 12.54 OK 300.09 3.30 3.729E+OO Line Not Found Absent TH-230 609.32 45.49* 2.167E+OO 8.998E-01 8.998E-01 22.81 OK 1120.29 14.92 1. 281E+OO 1.290E+00 1.290E+OO 29.17 OK Page 4228 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1764.49 8.593E-Ol l.090E+OO l.090E+OO 49 .,19 OK TH-232 105.21 1.10 6.007E+OO Line Not Found Absent 338.32 11.27 3.404E+OO l.082E+OO l.082E+OO 53.31 OK 835.71 1. 61 l.666E+OO Line Not Found Absent 911.20 25.80* l.544E+OO 5.761E-01 5.761E-01 66.46 OK 968. 97 15.80 l.463E+OO 2.045E+OO 2.045E+OO 32.42 OK TH-234 63. 29 3.70* 2.650E+OO l.701E+OO 1. 701E+OO 166.19 OK 92.59 4.23 5.546E+OO 2.088E+OO 2.088E+OO 60.51 OK U-234 609.32 45.49* 2.167E+OO 8.998E-01 8.998E-01 22.81 OK 1120.29 14.92 l.281E+OO l.290E+OO l.290E+OO 29.17 OK 1764.49 15.30 8.593E-Ol l.090E+OO l.090E+OO 49.19 OK U-235 89. 96 3.47 5. 381E+OO 2.237E+OO 2.237E+OO 49.44 OK 93.35 5.60 5.546E+OO l.577E+OO l.577E+OO 60.51 OK 143.76 10. 96* 5.990E+OO Line Not Found Absent 163.33 5.08 5.669E+OO Line Not Found Absent 185.72 57.20 5.267E+OO l.340E-01 l.340E-01 71. 82 OK 205.31 5.01 4. 931E+OO Line Not Found Absent U-238 63.29 3.70* 2.650E+OO l.701E+OO 1. 701E+OO 166.19 OK 92.59 4.23 5.546E+OO 2:088E+OO 2.088E+OO 60.51 OK AM-243 43.53 5.90 3.924E-01 Line Not Found Absent 74.66 67.20* 4.088E+OO 1.992E-01 l.992E-01 56.98 OK CM-247 278.00 3.40 3. 951E+OO Line Not Found Absent 287.50 2.00 3.852E+OO Line Not Found Absent 402.40 72. 00* 2.988E+OO l.037E-01 1.037E-01 118.78 OK Flag: "*" = Keyline Page 4229 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:53:01.63 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l *
  • Acquisition date 3-0CT-2016 07:51:57 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.66 Half life ratio : ***** *
  • Sample date 2-DEC-2015 15:00:00 Analyst initials: MXRl *
  • Sample ID G405235058 Sample Quantity l.4062E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;14 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) NA-22 7.552E-02 7.836E-02 K-40 1. 27 8E+Ol 1.618E+OO CD-109 1.596E+OO 2.025E+OO SN-126 1.008E-01 1.279E-Ol. TL-208 2.136E-01 1.020E-01 BI-211 2.400E-01 1.024E+OO PB-212 1. llOE+OO 1.364E-01 BI-214 9. OOlE-01 2.012E-01 PB-214 1. l 77E+00 2.085E-01 RN-222 9.00lE-01 2.012E-01 RA-224 1.403E+OO 1.404E+OO RA-226 9.00lE-01 2.012E-01 AC-228 5.761E-01 3.752E-01 RA-228 5.761E-01 3.752E-01 TH-228 1. llOE+OO 1.364E-01 TH-230 8.998E-01 2.012E-01 TH-232 5.761E-01 3.752E-01 TH-234 1. 701E+OO 2. 771E+OO U-234 8.998E-01 2.012E-01 U-235 -1. 530E-01 1. 872E-01 U-238 1.701E+OO 2.771E+OO AM-243 l.992E-01 l .112E-01 CM-247 1.037E-01 1.207E-01 Non-Identified Nuclides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4230 of 5809 Key-Line Activity (pCi/GRAM -4.102E+OO O.OOOE+OO 1. 2 69E-02 -l.707E-01 O.OOOE+OO O.OOOE+OO l.705E-03 K.L. Cnt Uricert ( 1. 96-sigma) 1. 362E+Ol 1. 960E+41 1. 758E-02 4.398E-01 1. 713E+04 5.082E+02 6.077E-02 MDA (pCi/GRAM 9. 996E-02 7.994E-01 2.003E+OO 1. 272E-01 6.600E-02 3.567E-01 9.399E-02 l.463E-01 3.626E-01 1.463E-01 1.008E+OO l.463E-01 2.910E-01 2.910E-01 9.399E-02 1.463E-01 2.910E-01 2.380E+OO l.463E-01 3.260E-01 2.380E+OO 8.266E-02 6.739E-02 MDA (pCi/GRAM 2.569E+Ol O.OOOE+OO 5.887E-02 7.772E-01 O.OOOE+OO 0.000E+OO 1.186E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1.384E-01 4.630E-01 9.559E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -2.0l6E-02 4.351E-02 7.949E-02 NOT IDENT. C0-58 1. 792E-01 6.560E-01 1.320E+OO NOT IDENT. FE-59 -1. 94 7E+OO 7.246E+OO 1.413E+Ol FAIL ABUN C0-60 -2.169E-02 4.225E-02 7.685E-02 NOT IDENT. ZN-65 8.983E-02 1.839E-01 3.719E-01 NOT IDENT. GE-68 2.020E+OO 2.047E+OO 4.873E+OO NOT IDENT. AS-73 7.549E+OO 1.039E+Ol 2.208E+Ol NOT IDENT. AS-')4 O.OOOE+OO 7.044E+03 o.oooE+oo SHORT HLIF SE-75 -2.326E-02 2.292E-01 4. ll 7E-01 FAIL ABUN BR-77 O.OOOE+OO 1. 361E+38 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 8.291E+02 O.OOOE+OO SHORT HLIF RB-83 -3.538E-01 6.272E-01 1.136E+OO NOT IDENT. KR-85 -1.858E+Ol 9.356E+OO 1. 38 9E+Ol NOT IDENT. SR-85 -2.090E+OO 1. 051E+OO 1.560E+OO NOT IDENT. RB-86 O.OOOE+OO 3.208E+04 0.000E+OO SHORT HLIF Y-88 6.817E-02 l.llOE-01 3.905E-01 NOT IDENT. Y-91 -2.083E+02 7.454E+02 l.216E+03 NOT IDENT. NB-94 -1. 263E-02 3.108E-02 5.598E-02 NOT IDENT. NB-95 5.774E-01 9.991E-01 2.050E+OO NOT IDENT. NB-95M 1.957E-01 2.765E+OO 4.683E+OO NOT IDENT. ZR-95 -2.882E-01 1. 759E+OO 3.263E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.022E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 7.855E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -2.229E-0'2 3.652E-02 5. 969E-02 NOT IDENT. RH-102 6.837E-02 6.025E-02 1.357E-01 NOT IDENT. RU-103 -2.835E+OO 5.818E+OO 1. 072E+Ol FAIL ABUN RH-106 2.237E-02 4.221E-01 8.509E-01 NOT IDENT. RU-106 2.237E-02 4.221E-01 8.509E-01 NOT IDENT. AG-108M -3.215E-02 2.698E-02 4.484E-02 FAIL ABUN AG-llOM 5.421E-02 8.817E-02 l.971E-01 NOT IDENT. SN-113 -7.223E-02 2.496E-01 4.541E-01 NOT IDENT. CD-115 O.OOOE+OO 2.009E+40 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO l.359E+05 O.OOOE+OO SHORT HLIF TE-123M -3.504E-02 l.363E-01 2.485E-01 NOT IDENT. SB-124 7. 596E-02 3.073E+OO 6.265E+OO NOT IDENT. SB-125 -2.627E-02 l.070E-01 2.044E-01 FAIL ABUN TE-125M 9.559E+Ol 2. 871E+02 5.625E+02 NOT IDENT. I-126 O.OOOE+OO l.303E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.648E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.412E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 9.269E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 869E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. 592E+27 O.OOOE+OO SHORT HLIF BA-133 4.894E-03 5.346E-02 7.836E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5.284E-02 5.281E-02 l.164E-01 NOT IDENT. CS-135 3.380E-02 1. 620E-01 2.983E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.683E+05 O.OOOE+OO SHORT HLIF BA-137M 4.642E-02 3.850E-02 8.476E-02 NOT IDENT. CS-137 4.904E-02 4.067E-02 8.954E-02 NOT IDENT. CE-139 -8.686E-02 l .131E-01 l.949E-01 NOT IDENT. BA-140 O.OOOE+OO 1.662E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 6.663E+05 O.OOOE+OO SHORT HLIF CE-141 2.817E+Ol 2.646E+Ol 5.419E+Ol NOT IDENT. CE-143 O.OOOE+OO 6.984E+40 O.OOOE+OO SHORT HLIF CE-144 -7.366E-02 3. 891E-01 6.645E-01 FAIL ABUN PM-144 1. 324E-02 5.214E-02 1.058E-01 NOT IDENT. PR-144 1.189E+OO 4.549E+OO 9.238E+OO NOT IDENT. PM-146 1.308E-02 4.512E-02 9.156E-02 NOT IDENT. ND-147 0.000E+OO 5.207E+07 O.OOOE+OO SHORT HLIF PM-147 -3.347E+Ol 7.316E+02 l.394E+03 NOT IDENT. PM-149 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF EU-150 -1.835E-02 2.882E-02 4.702E-02 FAIL ABUN EU-152 1.166E-03 9. 081E-02 1. 739E-01 NOT IDENT. GD-153 -5.349E-02 1.574E-01 2.953E-01 FAIL ABUN EU-154 l.846E-01 l.916E-01 2.716E-01 FAIL ABUN EU-155 2.398E-02 1.112E-01 2.016E-01 FAIL ABUN TB-160 1. 937E+OO 1.786E+OO 4.239E+OO FAIL ABUN H0-166M 7.871E-03 5.148E-02 1.036E-01 FAIL ABUN TM-171 -2.742E+Ol 2.468E+Ol 4.497E+Ol NOT IDENT. HF-172 4.928E-02 2.480E-01 4.426E-01 FAIL ABUN LU-172 5.876E-02 9.137E-02 l.987E-01 FAIL ABUN LU-176 -1.208E-02 2.141E-02 4.057E-02 FAIL ABUN Page 4231 of 5809 HF-181 8. 071E-01 4.529E+OO 9.173E+OO NOT IDENT. TA-182 -l.536E-02 l.066E+OO 2.109E+00 FAIL ABUN RE-183 l.327E+OO 3.440E+OO 7.050E+OO NOT IDENT. RE-184 1. 813E+Ol 3.674E+Ol 7.623E+Ol NOT IDENT. W-188 O.OOOE+OO 2.591E+02 2.156E+02 FAIL ABUN IR-192 -7.938E-03 5. l 72E-01 9.318E-01 FAIL ABUN HG-203 -3.093E+OO 3.173E+OO 5.047E+OO NOT IDENT. BI-207 -l.544E-02 5.957E-02 l.003E-01 FAIL ABUN PB-210 2.381E+00 4.614E+OO 9.569E+OO NOT IDENT. PB-2ll 5.370E-01 6.003E-01 1. U8E+OO NOT IDENT. BI-212 1. 783E-01 5.427E-01 1. 076E+OO NOT IDENT. RN-219 O.OOOE+OO l.317E+OO 7.759E-01 FAIL ABUN RA-223 5. 720E-01 5.498E-01 1. 211E+OO FAIL ABUN AC-227 4.106E-02 2.457E-01 4.551E-01 FAIL ABUN TH-227 4.106E-02 2.457E-01 4.551E-01 FAIL ABUN TH-229 3.130E-02 4.717E-01 8.765E-01 FAIL ABUN PA-231 -4.929E-02 4. 551E-01 8.940E-01 NOT IDENT. TH-231 5.720E-01 5.498E-01 1. 211E+OO FAIL ABUN PA-233 2.051E-02 6.940E-02 1. 28 6E-01 NOT IDENT. PA-234 -l.490E-01 2.800E-01 5.238E-01 NOT IDENT. PA-234M 2.711E+OO 5.044E+OO l.066E+Ol NOT IDENT. NP-237 2.051E-02 6.940E-02 1.286E-01 NOT IDENT. NP-238 O.OOOE+OO 8.269E+40 O.OOOE+OO SHORT HLIF NP-239 -6.698E-02 2.234E-01 4.153E-01 FAIL ABUN PU-239 4.395E+02 8. 211E+02 6.694E+02 FAIL ABUN AM-241 -2.189E-02 1. 57 5E-01 2.870E-01 NOT IDENT. CM-243 l.252E-01 1. 753E-01 1. 629E-01 FAIL ABUN BK-247 -l.648E-02 7.841E-02 l.388E-01 FAIL ABUN CF-249 3.881E-03 3.619E-02 7.266E-02 NOT IDENT. CF-251 l.658E-01 1.901E-01 2.156E-01 FAIL ABUN ANH-511 -7.462E-03 5.064E-02 l.081E-01 NOT IDENT. Page 4232 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:52:59.18 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error NA-22 1274.54 13 99.94* 1.136E+OO 6.042E-02 7.552E-02 105.89 K-40 1460.82 257 10.66* 1.005E+OO 1.278E+Ol 1.278E+Ol 12.92 CD-109 88.03 72 3.70* 5.194E+OO 2.012E+OO 3.185E+OO 63.25 SN-126 64.28 31 9.60 2.650E+OO 6.557E-01 6.557E-01 166.19 86.94 72 8.90 5.194E+OO 8.365E-01 8.365E-01 63.25 87.57 72 37.00* 5.194E+OO 2.012E-01 2.012E-01 63.25 TL-208 277.37 ------6.60 3.958E+OO ------Line Not Found ------583.19 76 85.00* 2.242E+OO 2.136E-01 2.136E-01 48.76 860.56 15 12.50 1.625E+OO 3.833E-01 3.833E-01 89.41 BI-211 72. 87 ------1. 23 3.859E+OO ------Line Not Found ------351.06 259 12.92* 3.304E+OO 3.241E+OO 3.241E+OO 18.08 PB-212 74.82 151 10.28 4.088E+00 1.917E+OO 1.917E+OO 37.59 77 .11 246 17.10 4.331E+OO 1. 770E+OO 1.770E+OO 22.26 238.63 402 43.60* 4.430E+OO 1. llOE+OO 1. llOE+OO 12.54 300.09 ------3.30 3.729E+OO ------Line Not Found ------BI-214' 609.32 166 45.49* 2.167E+OO 8.'998E-01 9.00lE-01 22.81 1120.29 46 14.92 1.281E+OO 1.290E+OO 1.290E+OO 29.17 1764.49 27 15.30 8.593E-01 1.090E+OO 1.091E+OO 49.19 PB-214 74.82 151 5.80 4.088E+OO 3.397E+OO 3.398E+OO 37.59 77 .11 246 9.70 4.331E+00 3 .121E+OO 3.122E+OO 22.26 87.09 72 3.41 5.194E+OO 2.183E+OO 2.184E+OO 63.25 242.00 112 7.25 4.384E+OO 1.883E+OO 1.883E+OO 39.68 295.22 142 18.42 3.776E+OO 1.089E+OO 1.090E+OO 28.83 351. 93 259 35.60* 3.304E+OO 1.176E+OO 1.177E+OO 1,8. 08 RN-222 609.32 166 45.49* 2.167E+OO 8.998E-01 9.00lE-01 22.81 1120.29 46 14.92 1.281E+OO 1.290E+OO 1.290E+OO 29.17 1764.49 27 15.30 8.593E-01 1.090E+OO 1. 091E+OO 49.19 RA-224 240.99 112 4.10* 4.384E+OO 3.329E+OO 3.329E+OO 39.68 RA-226 609.32 166 45.49* 2.167E+OO 8.998E-01 9.00lE-01 22.81 1120.29 46 14.92 1.281E+OO 1.290E+OO 1.290E+OO 29.17 1764.49 27 15.30 8.593E-01 1.090E+OO 1. 091E+OO 49.19 AC-228 105.21 ------1.10 6.007E+00 ------Line Not Found ------338.32 78 11. 27 3.404E+OO 1.082E+OO 1.082E+OO 53.31 794.95 ------4.25 1.739E+OO ------Line Not Found ------835.71 ------1. 61 1.666E+00 ------Line Not Found ------911.20 43 25.80* 1.544E+OO 5. 761E-01 5.761E-01 66.46 968. 97 89 15.80 1.463E+OO 2.045E+OO 2.045E+OO 32.42 RA-228 105.21 ------1.10 6.007E+OO ------Line Not Found ------338.32 78 11. 27 3.404E+OO 1.082E+OO 1.082E+OO 53.31 794.95 ------4.25 1.739E+OO ------Line Not Found ------835. 71 ------1. 61 1.666E+OO ------Line Not Found ------911.20 43 25.80* 1.544E+OO 5.761E-01 5.761E-01 66.46 968. 97 89 15.80 1.463E+OO 2.045E+OO 2.045E+OO 32.42 TH-228 74.82 151 10.28 4.088E+OO 1.917E+OO 1.917E+OO 37.59 77.11 246 17.10 4. 331E+OO 1.770E+OO 1. 770E+OO 22.26 238.63 402 43.60* 4.430E+OO 1.llOE+OO 1. llOE+OO 12.54 300.09 ------3.30 3.729E+OO ------Line Not Found ------Page 4233 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH.-230 609.32 166 45. 4.9* 2.167E+OO 8.998E-01 8.998E-01 22 . .81 1120.29 46 14.92 1. 281E+OO 1. 290E+OO 1. 290E+OO 29.17 1764.49 27 15.30 8.593E-01 1.090E+OO 1.090E+OO 49.19 TH-232 105.21 ------1.10 6.007E+OO ------Line Not Found ------338.32 78 11. 27 3.404E+OO 1.082E+OO 1.082E+OO 53.31 835. 71 ------1. 61 l.666E+OO ------Line Not Found ------911.20 43 25.80* 1.544E+OO 5. 761E-01 5. 761E-01 66.46 968. 97 89 15.80 1.463E+00 2.045E+OO 2.045E+OO 32.42 TH-234 63.29 31 3.70* 2.650E+00 1. 701E+OO 1. 701E+OO 166.19 92.59 92 4.23 5.546E+OO 2.088E+00 2.088E+OO 60.51 U-234 609.32 166 45.49* 2.167E+OO 8.998E-01 8.998E-01 22.81 1120.29 46 14.92 1.281E+OO 1.290E+OO 1.290E+OO 29.17 1764.49 27 15.30 8.593E-01 l.090E+00 1.090E+OO 49.19 U-235 89. 96 78 3.47 5. 381E+OO 2.237E+OO 2.237E+OO 49.44 93.35 92 5.60 5.546E+OO l.577E+OO 1.577E+OO 60.51 143.76 ------10.96* 5.990E+OO ------Line Not Found ------163.33 ------5.08 5.669E+OO ------Line Not Found ------185.72 76 57.20 5.267E+00 l.340E-01 l.340E-01 71. 82 205.31 ------5.01 4.931E+OO ------Line Not Found ------U-238 63.29 31 3.70* 2.650E+OO 1. 701E+OO 1. 701E+OO 166.19 92.59 92 4.23 5.546E+00 2.088E+OO 2.088E+OO 60.51 AM-243 43.53 ------5.90 3.924E-01 ------Line Not Found ------74.66 151 67.20* 4.088E+OO 2.932E-01 2.932E-01 37.59 CM-247 278.00 ------3.40 3. 951E+OO ------Line Not Found ------287.50 ------2.00 3.852E+OO ------Line Not Found ------402.40 42 72.00* 2.988E+OO l.037E-01 1.037E-01 118.78 Flag: "*" Key line Page 4234 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235058 Acquisition date 3-0CT-2016 07:51:57 Total number of lines in spectrum 45 Number of unidentified lines 9 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide NA-22 K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 Hlife 2.60Y 1.25E+09Y 461. 40D 2.30E+05Y 1.41E+10Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600.00Y 1600.00Y 1.41E+10Y 1600.00Y 1. 41E+10Y 1.41E+10Y 1.41E+10Y 7.54E+04Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.56E+07Y Decay 1.25 1. 00 1. 58 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 6.042E-02 1.278E+Ol 2.012E+OO 2.012E-01 2.136E-Ol 3.241E+OO 1. llOE+OO 8.998E-01 1. 17 6E+OO 8.998E-Ol 3.329E+OO 8.998E-01 5.761E-'01 5. 761E-01 1. llOE+OO 8.998E:..01 5. 761E-01 1. 701E+OO 8.998E-01 1. 340E-01 1. 701E+OO 2.932E-01 1.037E-01 3.540E+Ol 3.540E+Ol Decay Corr pCi/GRAM 7.552E-02 1.278E+Ol 3.185E+OO 2.012E-01 2.136E-01 3. 241E+OO 1.llOE+OO 9. OOlE-01 1.177E+OO 9. OOlE-01 3.329E+OO 9.00lE-01 5. 761E-01 5.761E-01 1. llOE+OO 8.998E-01 5. 761E-01 1. 701E+OO 8.998E-01 1.340E-01 1. 701E+OO 2.932E-01 1.037E-01 3.659E+Ol 3.659E+Ol 80.00% Decay Corr 2-Sigma Error 7. 996E-02 0.165E+Ol 2.014E+OO l.273E-01 1.041E-01 0.586E+OO 0.139E+OO 2.053E-01 0.213E+OO 2.053E-01 1.321E+OO 2.053E-01 3.829E-01 3.829E-01 0.139E+OO 2.053E-01 3.829E-01 2.827E+OO 2.053E-01 0. 962E-01 2.827E+OO 1.102E-01 1.232E-01 "M" Manually accepted 2-Sigma %Error 105.89 12.92 63.25 63.25 48.76 18.08 12.54 22.81 18.08 22.81 39.68 22.81 66.46 66.46 12.54 22.81 66.46 166.19 22.81 71. 82 166.19 37.59 118. 78 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4235 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235058 Acquisition date : 3-0CT-2016 07:51:57 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 79.22 62 106 1. 37 158.13 143 19 1. 41E-02 88.9 4.54E+OO T 0 102.61 29 105 1.23 204.88 200 8 6.65E-03 **** 5.94E+OO T 0 129.51 32 188 0. 96 258.63 253 12 7.57E-03 **** 6.15E+OO T 0 153.61 .34 93 0.86 306.80 304 7 8.19E-03.**** 5.84E+OO T 0 177.33 29 73 0.86 354.20 349 8 7.06E-03 **** 5.42E+OO T 0 209.36 59 108 1.19 418.21 412 10 1. 44E-02 76.1 4.86E+OO T 0 289.24 47 60 2.13 577.85 573 13 1.18E-02 78.5 3.83E+OO T 0 314.64 9 57 0.69 628.63 622 8 2.22E-03 **** 3.60E+OO 0 358.65 22 49 1. 42 716. 60 712 9 5.56E-03 **** 3.26E+OO 0 408.85 35 59 3.49 816.93 810 18 9.03E-03 **** 2.95E+00 0 463.77 34 35 1. 61 926. 71 921 12 9.00E-03 81. 2 2.68E+OO T 0 546.34 10 13 1. 41 1091. 7 9 1088 8 2.65E-03 **** 2.36E+OO T 0 614.41 8 12 1. 72 1227.87 1224 8 2.17E-03 **** 2.15E+OO T 0 637.75 20 14 0.92 1274.53 1269 13 5.45E-03 88.4 2.09E+OO T 0 782.94 9 11 1.11 1564.83 1558 9 2.43E-03 **** 1. 76E+OO T 0 1070.72 9 8 1. 02 2140.32 2132 11 2.66E-03 **** 1.33E+OO 0 1074.01 7 4 1.12 2146.91 2144 6 1. 89E-03 **** 1. 33E+OO 0 1184.25 16 8 3.85 2367.40 2361 12 4.46E-03 88.9 1. 22E+OO 0 1211.50 10 19 4.02 2421. 91 2411 13 2.76E-03 **** 1.19E+OO 0 1238.54 13 19 0. 96 2476.01 2466 14 3.63E-03 **** 1.17E+OO T 0 1280.43 13 4 2.12 2559.80 2555 9 3.58E-03 80.9 1.13E+00 0 1291.47 8 0 1. 35 2581. 88 2579 6 2.22E-03 70.7 1.12E+OO T 0 1558.82 8 0 0.88 3116.75 3111 11 2.22E-03 70.7 9.49E-01 Flags: "T" = Tentatively associated Page 4236 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:53:15.84 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l *
  • Acquisition date 3-0CT-2016 07:51:57 Sensitivity 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.66 Half life ratio : ***** *
  • Sample date 2-DEC-2015 15:00:00 Nuclide Library : SOLID *
  • Sample ID G405235058 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.4062E+02 GRAM *
  • Wet wt corr : 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide NA-22 K-40 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 Le (pCi/GRAM 4.199E-02 3.321E-01 9.394E-01 5. 968E-02 2.913E-02 l.609E-01 4. 311E-02 6.569E-02 1. 750E-01 6.569E-02 4.623E-01 6.569E-02 1. 272E-01 1. 272E-01 4. 311E-02 6.566E-02 1.272E-01 1.112E+OO 6.566E-02 l.515E-01 1.112E+OO 3.853E-02 3.024E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4237 of 5809 Le (pCi/GRAM l.139E+Ol O.OOOE+OO 2.086E-02 3.305E-01 O.OOOE+OO O.OOOE+OO 5.062E-02 4.088E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 . SE-7 5 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4238 of 5809 0.000E+OO 3. 661E-02 5.741E-01 5.907E+OO 3.lOOE-02 l.592E-01 2.064E+OO 1.026E+Ol O.OOOE+OO 1.877E-01 O.OOOE+OO O.OOOE+OO 4.898E-01 6.218E+OO 6.984E-01 O.OOOE+OO l.316E-01 5.207E+02 2.418E-02 9.133E-01 2.156E+OO 1.428E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.769E-02 6.057E-02 4.652E+00 3.639E-01 3.639E-01 1.951E-02 8.370E-02 2.034E-01 O.OOOE+OO O.OOOE+OO 1.150E-01 2.555E+OO 9.143E-02 2.627E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3. 531E-02 O.OOOE+OO 5.166E-02 1. 37 6E-01 0.000E+OO O.OOOE+OO 3.827E-02 4.043E-02 8. 965E-02 O.OOOE+OO O.OOOE+OO 2.532E+Ol O.OOOE+OO 3.088E-01 4.608E-02 4.026E+OO 4 .113E-02 O.OOOE+OO 6.433E+02 O.OOOE+OO 2.122E-02 7.826E-02 l.366E-01 1.163E-01 9.402E-02 1.834E+OO 4.466E-02 2.066E+01 2.065E-01 8.732E-02 1.811E-02 4.062E+00 SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 . CF-249 CF-251 ANH-511 Page 4239 of 5809 9.093E-01 3.284E+00 3.321E+Ol 9.768E+01 4.215E-01 2.304E+00 4.276E-02 4.484E+OO 5.029E-01 4.794E-01. 3.503E-01 5.524E-01 2.088E-01 2.088E-01 4.050E-01 4.095E-01 5.524E-01 5.897E-02 2.211E-01 4.717E+OO 5.897E-02 O.OOOE+OO 1.922E-01 3.152E+02 l.334E-01 7.521E-02 6.330E-02 3.266E-02 9.973E-02 5. lllE-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:53:21.62 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235058.CNF;l *
  • Acquisition date 3-0CT-2016 07:51:57 Sensitivity : 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.66 Half life ratio : ***** *
  • Sample date 2-DEC-2015 15:00:00 Nuclide Library : SOLID *
  • Sample ID G405235058 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.4062E+02 GRAM *
  • Quantity Err ( % ) : 1. 4223E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * * *' Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) NA-22 7.552E-02 7.862E-02 K-40 1. 27 8E+Ol 1.950E+OO CD-109 1. 596E+OO 2.046E+OO SN-126 1.008E-01 l.292E-01 TL-208 2.136E-01 1.037E-01 BI-211 2.400E-01 1. 097E+OO PB-212 l. llOE+OO 1. 691E-01 BI-214 9.00lE-01 2.153E-01 PB-214 1.177E+OO 2.337E-01 RN-222 9. OOlE-01 2.153E-01 RA-224 1.403E+OO 1.432E+OO RA-226 9.00lE-01 2.153E-01 AC-228 5.761E-01 3.827E-01 RA-228 5.761E-01 3.827E-01 TH-228 1. llOE+OO 1.691E-01 TH-230 8.998E-01 2.152E-01 TH-232 5.761E-01 3.827E-01 TH-234 1.701E+OO 2.797E+OO U-234 8.998E-01 2.152E-01 U-235 -l.530E-01 1. 875E-01 U-238 1.701E+OO 2.797E+OO AM-243 1.992E-01 l.132E-01 CM-247 1.037E-01 l.222E-01 Non-Identified Nuclides Nuclide BE-7 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4240 of 5809 Key-Line Activity (pCi/GRAM -4.102E+OO 1.000E+41 1. 2 69E-02 -l.707E-01 3.213E+03 3.086E+02 1. 705E-03 K.L Act error ( 1. 96-sigma) -1. 362E+01 1.630E+43 1. 761E-02 4.403E-01 1.713E+04 5.090E+02 6.077E-02 TPU ( 1. 96-sigma) 7.862E-02 1.950E+OO 2.046E+OO 1. 2 92E-01 1.037E-01 1.097E+OO 1.691E-01 2.153E-01 2.337E-01 2.153E-01 1.432E+OO 2.153E-01 3.827E-01 3.827E-01 1. 691E-01 2.152E-01 3.827E-01 2.797E+OO 2.152E-01 1. 875E-01 2.797E+OO l.132E-01 l.222E-01 TPU ( 1. 96-sigma) 1.375E+Ol O.OOOE+OO 1.851E-02 4.470E-01 1. 720E+04 5.277E+02 6.078E-02 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1.384E-01 4.633E-01 4.675E-01 FAIL ABUN MN-56 l.OOOE+41 3.348E+41 O.OOOE+OO SHORT HLIF C0-57 -2.0l6E-02 4.353E-02 4.447E-02 NOT IDENT. C0-58 1. 792E-01 6.563E-01 6.612E-01 NOT IDENT. FE-59 -1. 94 7E+OO 7.255E+OO 7.308E+OO FAIL ABUN C0-60 -2.169E-02 4.229E-02 4.340E-02 NOT IDENT. ZN-65 8.983E-02 1.846E-01 1. 890E-01 NOT IDENT. GE-68 2.020E+OO 2.075E+OO 2.266E+OO NOT IDENT. AS-73 7.549E+OO 1.051E+Ol 1.105E+Ol NOT IDENT. AS-74 -3.527E+03 7.054E+03 7. 23lE+03 SHORT HLIF SE-75 -2.326E-02 2.292E-01 2.294E-01 FAIL ABUN BR-77 1.107E+39 9.771E+39 O.OOOE+OO SHORT HLIF SR-82 2.146E+Ol 8.291E+02 8.291E+02 SHORT HLIF RB-83 -3.538E-01 6.297E-01 6.496E-01 NOT IDENT. KR-85 -1.858E+Ol 9.492E+OO 1.266E+Ol NOT IDENT. SR-85 -2.090E+OO 1.067E+OO l.423E+OO NOT IDENT. RB-86 2.281E+04 3.231E+04 3.391E+04 SHORT HLIF Y-88 6.817E-02 l. lllE-01 l.153E-01 NOT IDENT. Y-91 -2.083E+02 7.456E+02 7.515E+02 NOT IDENT. NB-94 -1.263E-02 3. lllE-02 3.162E-02 NOT IDENT. NB-95 5.774E-01 1. OOlE+OO 1.034E+OO NOT IDENT. NB-95M 1.957E-01 2.765E+OO 2.767E+OO NOT IDENT. ZR-95 -2.882E-01 1.759E+OO 1. 764E+OO NOT IDENT. NB-97 -l.000E+41 4.274E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 l.026E+41 O.OOOE+OO SHORT HLIF M0-99 3.047E+32 7.863E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 2.984E+41 O.OOOE+OO SHORT HLIF RH-101 -2.229E-02 3.677E-02 3.812E-02 NOT IDENT. RH-102 6.837E-02 6.071E-02 6.809E-02 NOT IDENT. RU-103 -2.835E+OO 5.823E+OO 5. 962E+OO FAIL ABUN RH-106 2.237E-02 4.221E-01 4.222E-01 NOT IDENT. RU-106 2.237E-02 4.221E-01 4.222E-01 NOT IDENT. AG-108M -3.215E-02 2.712E-02 3.075E-02 FAIL ABUN AG-llOM 5. 421E-02 8.843E-02 9.175E-02 NOT IDENT. SN-113 -7.223E-02 2. 496E-01 2.517E-01 NOT IDENT. CD-115 -3.768E+39 2.010E+40 O.OOOE+OO SHORT HLIF SN-117M -7.517E+04 l.363E+05 l.404E+05 SHORT HLIF TE-123M -3.504E-02 l.363E-01 l.373E-01 NOT IDENT. SB-124 7. 596E-02 3.073E+OO 3.074E+OO NOT IDENT. SB-125 -2.627E-02 1.070E-01 1.076E-01 FAIL ABUN TE-125M 9.559E+Ol 2.872E+02 2.904E+02 NOT IDENT. I-126 -l.044E+05 l.303E+06 l.304E+06 SHORT HLIF SB-126 -1.950E+05 1. 649E+06 l.651E+06 SHORT HLIF SB-127 -2.415E+22 7.253E+22 O.OOOE+OO SHORT HLIF I-131 -5.715E+09 9.284E+09 9.634E+09 SHORT HLIF I-132 -l.OOOE+41 1. 8 94E+42 O.OOOE+OO SHORT HLIF TE-132 3.407E+26 l.599E+27 O.OOOE+OO SHORT HLIF BA-133 4.894E-03 5.346E-02 5. 351E-02 NOT IDENT. I-133 -1.000E+41 5.326E+41 O.OOOE+OO SHORT HLIF CS-134 5.284E-02 5.310E-02 5.820E-02 NOT IDENT. CS-135 3.380E-02 1. 621E-01 1.628E-01 NOT IDENT. I-135 l.OOOE+41 8.141E+41 O.OOOE+OO SHORT HLIF CS-136 2.296E+05 3.709E+05 3.850E+05 SHORT HLIF BA-137M 4.642E-02 3.869E-02 4.399E-02 NOT IDENT. CS-137 4.904E-02 4.087E-02 4.647E-02 NOT IDENT. CE-139 -8.686E-02 l.145E-01 1.211E-01 NOT IDENT. BA-140 6.440E+05 l.663E+06 1.688E+06 SHORT HLIF LA-140 -3.322E+05 6.668E+05 6.834E+05 SHORT HLIF CE-141 2.817E+Ol 2.654E+Ol 2.942E+Ol NOT IDENT. CE-143 l.OOOE+41 7.109E+40 O.OOOE+OO SHORT HLIF CE-144 -7.366E-02 3. 891E-01 3.905E-01 FAIL ABUN PM-144 1.324E-02 5.216E-02 5.250E-02 NOT IDENT. PR-144 1.189E+OO 4.551E+OO 4.582E+OO NOT IDENT. PM-146 l.308E-02 4.514E-02 4.553E-02 NOT IDENT. ND-147 -7.103E+06 5.208E+07 5.217E+07 SHORT HLIF PM-147 -3.347E+Ol 7.317E+02 7.318E+02 NOT IDENT. PM-149 -3.033E+40 3.220E+41 O.OOOE+OO SHORT HLIF EU-150 -1.835E-02 2.887E-02 3.004E-02 FAIL ABUN EU-152 1.166E-03 9. 081E-02 9.081E-02 NOT IDENT. GD-153 -5.349E-02 l.574E-01 l.593E-01 FAIL ABUN EU-154 1.846E-01 1.922E-01 2.094E-01 FAIL ABUN EU-155 2.398E-02 1.113E-01 1.118E-01 FAIL ABUN TB-160 1.937E+OO 1. 803E+OO 2.004E+OO FAIL ABUN H0-166M 7. 871E-03 5.148E-02 5.160E-02 FAIL ABUN TM-171 -2.742E+Ol 2. 481E+Ol 2.771E+Ol NOT IDENT. HF-172 4.928E-02 2. 481E-01 2.491E-01 FAIL ABUN LU-172 5.876E-02 9.209E-02 9.583E-02 FAIL ABUN LU-176 -l.208E-02 2.144E-02 2.212E-02 FAIL ABUN Page 4241of5809 HF-181 8.071E-01 4.529E+OO 4.544E+00 NOT IDENT. TA-182 -1.536E-02 1.066E+OO 1.066E+OO FAIL ABUN RE-183 l.327E+OO 3.446E+OO 3.498E+00 NOT IDENT. RE-184 1.813E+Ol 3.707E+Ol 3. 796E+Ol NOT IDENT. W-188 3.367E+02 2.634E+02 3.040E+02 FAIL ABUN IR-192 -7.938E-03 5 .172E-01 5. l 72E-01 FAIL ABUN HG-203 -3.093E+OO 3.186E+OO 3.478E+OO NOT IDENT. BI-207 -1.544E-02 5.963E-02 6.003E-02 FAIL ABUN PB-210 2.381E+OO 4.618E+OO 4.742E+OO NOT IDENT. PB-211 5.370E-01 6.022E-01 6.491E.-01 NOT IDENT. BI-212 1.783E-01 5.430E-01 5.489E-01 NOT I DENT*. RN-219 1.131E+OO 1.327E+OO 1.422E+OO FAIL ABUN RA-223 5.720E-01 5.530E-01 6.lOlE-01 FAIL ABUN AC-227 4.106E-02 2.457E-01 2.464E-01 FAIL ABUN TH-227 4.106E-02 2.457E-01 2.464E-01 FAIL ABUN TH-229 3.130E-02 4.717E-01 4.719E-01 FAIL ABUN PA-231 -4.929E-02 4.553E-01 4.558E-01 NOT IDENT. TH-231 5.720E-01 5.530E-01 6.lOlE-01 FAIL ABUN PA-233 2.051E-02 6.943E-02 7.004E-02 NOT IDENT. PA-234 -1. 490E-01 3.284E-01 3.352E-01 NOT IDENT. PA-234M 2.711E+OO 5. 061E+OO 5.206E+OO NOT IDENT. NP-237 2.051E-02 6.943E-02 7.004E-02 NOT IDENT. NP-238 -1. OOOE+41 8.394E+40 O.OOOE+OO SHORT HLIF NP-239 -6.698E-02 2.235E-01 2.255E-01 FAIL ABUN PU-239 4.395E+02 8.217E+02 8.453E+02 FAIL ABUN AM-241 -2.189E-02 1. 57 5E-01 1. 578E-01 NOT IDENT. CM-243 1.252E-01 1.758E-01 l.846E-01 FAIL ABUN BK-247 -1.648E-02 7.849E-02 7.884E-02 FAIL ABUN CF-249 3.881E-03 3.619E-02 3.624E-02 NOT IDENT. CF-251 1.658E-01 l.913E-01 2.053E-01 FAIL ABUN ANH-511 -7.462E-03 5.065E-02 5.076E-02 NOT IDENT. Page 4242 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 62.9377 879.38 77.4414 482.18 66.2441 45.60 71.0732 87.57 77.4662 133.52 62.1524 46.54 56.6870 87.09 77.4911 264.66 54.0733 49.72 0.0000 87.57 76.2976 122.06 58.2747 51. 35 44.4594 88.03 76.3708 140.51 0.0000 51. 87 60.2444 88.34 76.4203 143.76 72.5976 52.39 64.7096 193.51 76.4410 144.24 63.1732 52.97 54.3087 89. 96 72.8428 145.44 45.3542 53.44 43.8576 90.64 72.9449 152.43 53.9833 125.81 43.9379 91.11 0.0000 153.25 0.0000 57.36 0.0000 63.29 73.2342 154.21 58.7480 57.53 56.7952 143.76 73.3461 156.02 0.0000 57.98 54.2001 94.56 65.7842 158.56 0.0000 1093.63 59.7424 94.65 65. 7961 159.00 56.9910 57.98 62.4257 94.67 65.7987 162.33 62.6525 59.54 61.8682 94.87 65.8247 162.66 0.0000 60. 96 56.1338 97.43 58.3736 163.33 53.0023 61.17 56.1653 311. 90 46.7893 165.86 59.6955 62.93 66.6320 946.00 46.7904 176.31 41. 8118 63.29 66.6947 99.53 53.4008 1048.07 0.0000 63.58 66.7451 1221. 41 46.9409 177.52 42.6109 64.28 66.8660 265.00 41.2233 739.50 0.0000 66.73 67.8911 103.18 49.8371 181.52 59.0714 67.24 86.1867 103.37 49.8549 711. 68 60.0257 67. 68 90.2309 116. 74 49.8549 185. 72 60.1230 67.75 90.2467 105.21 59.2406 193.51 48.3304 69.67 72.0521 105.31 59.2516 197.03 55.3052 70.83 97.9736 106.12 45.4939 127.23 49.7189 72. 81 62.7549 106.47 70.2638 306.78 48.8061 279.20 62.7638 109.28 59.6814 203.43 57.9937 72.87 62.7638 111. 00 52.8811 205.31 51. 6613 74.66 63.0289 228.16 0.0000 210.85 48.9284 74.82 63.0522 114. 06 55.1733 215.65 46.1163 1063.66 63.0745 116. 30 0.0000 222 .11 55.7314 238.63 63.3863 116. 74 57.4453 290.67 39.6876 351. 93 63.3863 119.76 43.5593 177.52 46.7059 78.74 63.6213 121.12 48.7357 228.16 0.0000 79.69 63.7567 121. 22 48.7438 228.18 50.2515 80.12 51. 3046 121. 78 45.7399 235.69 43.9733 80.19 0.0000 122.06 54.9134 256.23 41.2367 80.57 53.8611 122.92 54.9921 238.63 41. 3499 81. 00 50.1514 123.07 49.9125 238.98 0.0000 81. 07 50.1591 123.68 57.1006 240.99 41.4498 81. 75 65.3042 125.81 60.0287 242.00 41. 4920 323.87 64.3336 127.23 69.7388 344.28 41.6058 84.00 64.3627 127.91 63.6556 252.40 0.0000 85.43 92.4099 129.30 63.7975 252.80 39.5450 86.55 77.4029 131.20 63.9905 254.15 0.0000 Page 4243 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 256.23 38.4753 351. 93 28.7159 583.19 19.0866 260.90 0.0000 507.63 0.0000 584.27 19. 0966 264.66 37.5760 356.01 26.1865 595.83 0.0000 264.80 35.1561 364.49 0.0000 600.60 18.2424 265.00 40.0123 366.42 0.0000 602.52 0.0000 2 68. 22 43.7827 372. 51 . 28.2773 604. 72 16.7565 269.46 42.6167 129.30 19.4765 607.14 30.5029 270.03 34 .1113 377.52 22.1720 609.32 25.9555 271.23 51. 224 7 383.85 26. 7279 497.08 25. 9690 273.65 0.0000 388.16 25.0229 433.94 16.8364 356.01 41.6658 388.63 0.0000 696. 49 9.2003 277.37 39.2500 391.69 29.0270 620.36 12.2813 277.60 39.2578 400.66 25.6930 621.93 11.2663 278.00 41. 7270 401.81 25.7133 667. 71 0.0000 279.20 56.5159 402.40 . 25. 7238 631. 29 10.2889 279.54 54.0748 404.85 8.1370 453.88 16.9921 279.70 54.0829 410.95 20. 4272 595.83 0.0000 280.46 44.2804 413.71 31. 3800 635.95 6.1870 283.69 40.7092 414.70 0.0000 636.99 0.0000 364.49 0.0000 423. 72 0.0000 645.85 13.4687 285.41 39.5361 404.85 24.7780 884.68 18.7537 285.90 0.0000 427.87 27.5452 657.90 0.0000 402.40 33.0086 433.94 30.4199 661.66 13.5686 290.67 29.7913 333.97 31.4524 664.57 0.0000 293.27 0.0000 453.88 22.4067 666.33 0.0000 295.22 29.9106 463.37 19.7221 720.70 0.0000 295.96 29.9297 468.07 16.9534 667.71 0.0000 298.58 43.3312 685.70 0.0000 677.62 9.4629 299.98 39.0448 475.06 15.1338 685.70 0.0000 300.09 39.0486 476.78 27.4589 695.00 0.0000 300.13 39.0495 477.60 24.6305 696. 49 12. 7251 301. 36 41. 7 643 482.18 18.0487 696. 51 12.7251 302.85 32.6174 1596.21 0.0000 697.00 0.0000 304.50 30.9884 527.90 0.0000 697.30 15. 9119 537.26 0.0000 497.08 20.1246 697.49 13.7916 306.78 31.0486 505.52 26.0013 702.65 18.0763 316.51 27.2274 507.63 0.0000 706.68 18.1088 311. 90 35.3973 511. 00 35.7436 711. 68 11.7430 316.51 30.4570 514.00 59. 9969 720.70 0.0000 531.02 0.0000 514.00 59. 9969 721. 93 0.0000 320.08 0.0000 520.40 19.4238 1690.97 18.2361 427.87 38.2132 238.98 0.0000 722.91 15.0191 323.87 21.2789 522.65 0.0000 1274.44 17.1673 325.23 35.7878 527.90 0.0000 724 .19 20.3939 328.76 0.0000 528.26 17.5591 727.33 18.2721 388.16 33.4498 520.40 18.5477 733.00 12.9292 333.97 39.9013 529.87 0.0000 735.93 21.5755 334.37 39.9146 531.02 0.0000 737.46 10.7951 338.28 32.7189 537.26 0.0000 739.50 0.0000 911.20 32.7204 546.56 0.0000 747.24 10.8398 340.48 25.8752 552.55 17.7935 748.06 7.5905 340.55 0.0000 563.25 17.8945 752.31 16.2939 344.28 26.9902 795.86 17.9524 753.82 0.0000 345.93 22.8674 569.50 17.9539 756.73 18. 5011 351. 06 28.6971 569.70 17.9553 756.80 18. 5011 Page 4244 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 763.94 15.2817 984.45 0.0000 1596.21 0.0000 765.81 15.2931 996.26 15.1645 1620.50 6.3270 766.42 14.2045 1001.03 13.4015 1621. 92 7.3841 766.84 16.3928 1002.74 12.5153 1678.03 0.0000 772.60 0.0000 1004.73 16.1016 1690.97 6.4244 776.52 0.0CJOO 1021. 30 0.0000 1750.46 0.0000 777.92 0.0000 1025.87 0.0000 1764.49 1.7396 778.90 6.5896 1028.54 0.0000 1770.23 6.5310 783.70 0.0000 846.77 8.1381 1771.35 2.1776 727. 33 9.9104 1038.76 0.0000 1791.20 0.0000 792.07 20.9784 1046.59 11.7876 1808.65 0.0000 794.95 7.7377 1048.07 0.0000 846.75 0.0000 795.86 9.9521 1049.04 7.2598 1836.06 0.0000 801.95 15.5187 621. 93 6.3549 810.06 14.4563 1063.66 13.1282 810.29 13. 3457 1077.00 0.0000 810.45 12.2345 1077.34 2.9299 810.76 12.2358 1085.87 8.2617 815.77 0.0000 1093.63 11. 0420 818.51 0.0000 1099.45 11.0618 832.01 12.3374 1112. 07 13.8803 834.85 11. 2280 1112.84 10.5783 835. 71 12.3549 1115. 54 7.4106 1260.41 0.0000 609.32 8.9057 846.75 0.0000 889.28 8.9063 846.77 9.0234 1121.30 5.9391 856.80 0.0000 1129. 67 12.0939 860.56 5.1022 1131. 51 0.0000 702.65 4.5531 1147. 95 0.0000 873.19 9 .1133 1173.23 15.0771 529.87 0.0000 1177.95 9.0586 879.38 4.5671 1189.05 9.0873 880.51 11. 4225 1204.77 15.2139 883.24 10.2905 1221. 41 13.3745 884.68 5.7200 1231.02 18.3914 889.28 14.8969 1235.36 0.0000 903.28 18. 3711 1238.28 12.4771 898.04 11. 4958 1260.41 0.0000 900.72 17.2601 1271.87 3.0998 903.28 10.3656 1274.44 9.3059 911.20 16.1704 1274.54 9.3059 912.08 16.1755 1099.45 9.7382 923.98 0.0000 1298.22 0.0000 926.50 8.1291 1312 .11 0.0000 929 .11 9.2992 1332. 49 9.8438 937.49 11. 6581 1362.66 0.0000 944.13 0.0000 1365 .19 3.9707 946.00 14.9082 1368.63 0.0000 949.00 6.1451 1384.29 2.9925 954.55 0.0000 1408.01 3.0104 962.31 16.9318 1457.56 0.0000 964.08 14 .1187 1460.82 8.1318 966 .17 14.1289 696. 51 5 .1169 968.97 14.1421 1505.03 5.1361 983.53 0.0000 1584.12 8.3682 Page 4245 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:53:53.65 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM07.CNF;484 Background date : Z-OCT-2016 11:00:17. Sample date 16-DEC-2015 12:26:00 Acquisition date : 3-0CT-2016 07:52:25. Sample ID G405235059 Sample quantity 1.54222E+02 GRAM Detector name : GAM07 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.48 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 2 2 2 0 0 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 2 2 2 2 0 0 0 0 0 0 0 0 0 Page 4246 of 5809 Energy 63.60* 72. 79 74.78* 77.22 87.32 92.80* 134.52 148.88 179.99 186.25* 209.57 238.62* 241. 92 278.61 295.23* 338.34* 352.03* 382.20 399.15 452. 96 463.12 510.65* 513.20 583.03* 588.34* 598.02 609.32* 657.01 661. 62 670.17 727 .18* 769.31 860.05 911. 05* BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 15 29 152 184 66 71 38 16 17 68 49 351 99 26 138 71 198 12 20 23 32 15 19 110 19 10 159 24 25 7 34 35 17 44 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 144 97 115 113 157 121 90 49 99 108 102 53 65 46 53 51 60 21 35 44 27 22 20 17 18 30 58 18 10 32 28 23 9 15 1. 36 1. 24 1. 08 1. 07 1. 23 1. 62 0.71 0.66 0.62 0.79 1. 94 1.15 1. 87 1. 41 1. 33 1. 08 1. 24 0.78 1. 03 1. 83 1.23 1. 85 1. 69 1. 92 1. 93 0.50 1. 63 2.79 1. 98 4.30 1. 59 6'.17 0.78 0. 96 127.70 146.07 150.05 154.93 175.11 186.09 269.50 298.21 360.41 372. 93 419.57 477.65 484.24 557.62 590.84 677.05 704.43 764.75 798.65 906.24 926.56 1021. 59 1026.69 1166. 33 1176.94 1196. 30 1218.89 1314. 27 1323.48 1340.57 1454.57 1538.83 1720.29 1822.26 124 143 143 143 171 183 266 296 359 368 415 471 471 553 586 673 698 762 794 896 921 1016 1016 1159 1159 1187 1210 1305 1319 1328 1448 1528 1715 1815 7 4.04E-03144.1 17 8.04E-03 54.1 17 4.23E-02 13.8 17 5.llE-02 11.8 8 1.83E-02 35.2 7 1. 98E-02 30. 0 8 1.06E-02 46.7 5 4.52E-03 69.4 8 4.86E-03100.4 10 1. 90E-02 32. 1 11 l.36E-02 42.5 28 9.75E-02 6.5 28 2.76E-02 21.5 10 7.15E-03 52.7 11 3.84E-02 13.6 10 1.98E-02 22.8 12 5.51E-02 10.7 7 3.33E-03 69.6 11 5.52E-03 62.4 16 6.46E-03 67.0 11 8.87E-03 36.4 16 4.28E-03 93.3 16 5.37E-03 62.8 27 3.06E-02 12.6 27 5.36E-03 49.1 12 2.78E-03114.0 18 4.42E-02 13.9 15 6.58E-03 44.8 10 6.94E-03 31.0 16 1.94E-03184.6 14 9.39E-03 38.0 19 9.72E-03 37.3 10 4.60E-03 43.1 13 1. 23E-02 25. 0 Fit 1. 91E+OO 1.45E+OO 9.12E-01 2.47E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 963. 99 14 8 0.63 1928.14 1922 9 3.79E-03 47.7 36 0 968.61* 50 18 1. 51 1937.38 1932 11 1.39E-02 22.5 3.7 0 1121. 69 29 36 2.37 2243.4.9 2232 18 8.19E-03 51.1 38 0 1236.82 39 10 4.95 2473.72 2464 20 1. 08E-02 25.5 39 0 1244.12 14 3 1. 57 2488.33 2485 8 3.89E-03 35.7 40 0 1250 .13 21 0 1. 06 2500.33 2494 13 5.83E-03 21. 8 41 0 1460.43* 277 9 2.49 2920.91 2914 16 7.69E-02 6.5 42 0 1763.79* 32 0 1. 67 3527.61 3521 13 8.98E-03 19.1 Flag: "*" = Peak area was modified by background subtraction Page 4247of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 08:53:56 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 16-DEC-2015 12:26:00 G405235059 Acquisition date : Sample quantity Sample qeometry : 3-0CT-2016 07:52:25 154.22 GRAM SampJ.e type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA7 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4248 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.48 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.122E+OO 1.089E+Ol 1.089E+Ol 13.08 OK KR-85 514.00 0.43* 2.624E+OO 8.956E+OO 9.438E+OO 125.53 OK SR-85 514.00 96.00* 2.624E+OO 4.049E-02 9.167E-01 125.53 OK CD-109 88.03 3.70* 5.750E+OO 1.0lOE+OO l.566E+OO 137.29 OK SN-126 64.28 9.60 3.539E+OO 2.749E-01 2.749E-01 288.28 OK 86.94 8.90 5.750E+OO 4.201E-01 4.201E-01 137. 29 OK 87.57 37.00* 5.750E+OO 1.0lOE-01 1.0lOE-01 137.29 OK BA-137M 661.66 89.90* 2.138E+OO 6.687E-02 6. 811E-02 61. 97 OK CS-137 661. 66 85.10* 2.138E+OO 7.064E-02 7.195E-02 61.97 OK CE-144 80.12 1. 36 5.243E+OO Line Not Found Absent 133.52 11. 09* 6.655E+OO 3.103E-01 6.312E-01 93.36 OK HG-203 70.83 3.69 4.380E+OO Line Not Found Absent 72.87 6.19 4.582E+OO 6.482E-01 4.981E+Ol 108.28 OK 279.20 81.56* 4.361E+OO l.716E-02 1.319E+OO 252.06 OK TL-208 277.37 6.60 4.377E+OO Line Not Found <<INT Reject 583.19 85.00* 2.366E+OO 2.859E-01 2.859E-01 25 .13 OK 860.56 12.50 1. 737E+OO 3.815E-01 3.815E-01 86.16 OK PB-212 74.82 10.28 4.777E+OO 1.398E+OO 1.398E+OO 40.28 OK 77 .11 17.10 5.000E+OO 1.359E+OO' 1.359E+OO 23.60 OK 238.63 43.60* 4.930E+OO 9.310E-01 9.310E-01 12.94 OK 300.09 3.30 4.103E+OO Line Not Found Absent BI-214 609.32 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 OK 1120. 29 14.92 1. 404E+OO. 6.828E-01 6.831E-01 102.23 OK 1764.49 15.30 9.426E-01 1.032E+00 l.032E+OO 38.16 OK PB-214 74.82 5.80 4.781E+OO Line Not Found <<INT Reject 77 .11 9.70 5.000E+OO 2.395E+OO 2. 396E+OO 23.60 OK 87.09 3.41 5.736E+OO Line Not Found <<INT Reject 242.00 7.25 4.877E+OO Line Not Found <<INT Reject 295.22 18.42 4.159E+OO 1.006E+OO 1.007E+OO 27.17 OK 351.93 35.60* 3.591E+OO 8.509E-01 8.512E-01 21. 49 OK RN-222 609.32 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 OK 1120.29 14.92 1.404E+OO 6.828E-01 6. 831E-01 102.23 OK 1764.49 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 OK RA-224 240.99 4.10* 4.879E+OO 1.048E+OO 1.048E+OO 124.88 OK RA-226 609.32 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 OK 1120.29 14.92 l.404E+OO 6.828E-01 6.831E-01 102.23 OK 1764.49 15.30 9.426E-01 l.032E+OO 1.032E+OO 38.16 OK AC-228 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.713E+OO 9.407E-01 9.407E-01 45.57 OK 794.95 4.25 1.849E+OO Line Not Found Absent 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.660E+OO 5.125E-01 5.125E-01 50.05 OK 968. 97 15.80 1.581E+OO 9.879E-01 9.879E-01 45.02 OK RA-228 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.713E+OO 9.407E-01 9.407E-01 45.57 OK 794.95 4.25 1.849E+OO Line Not Found Absent 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* l.660E+OO 5.125E-01 5.125E-01 50.05 OK 968. 97 15.80 1. 581E+OO 9.879E-01 9.879E-01 45.02 OK Page 4249 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 4.717E+OO l.398E+OO 1.398E+OO 40.28 OK,. 77 .11 17.10 5.000E+OO 1.359E+OO 1.359E+OO 23.60 OK 238.63 43.60* 4.930E+OO 9.310E-01 9.310E-01 12.94 OK 300.09 3.30 4.103E+OO Line Not Found Absent TH-230 609.32 45.49* 2.284E+OO 7.943E-01 7.943E-01 27.84 OK 1120.29 14.92 1.404E+OO 6.828E-01 6.828E-01 102.23 OK 1764.49 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 OK TH-232 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.713E+OO 9.407E-01 9.407E-01 45.57 OK 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.660E+OO 5.125E-01 5.125E-01 50.05 OK 968.97 15.80 1.581E+OO 9.879E-01 9.879E-01 45.02 OK TH-234 63.29 3.70* 3.539E+00 7.133E-01 7.133E-01 288.28 OK 92.59 4.23 6.049E+OO 1.730E+OO 1. 7 30E+OO 60.04 OK U-234 609.32 45.49* 2.284E+OO 7.943E-01 7.943E-01 27.84 OK 1120. 29 14.92 1.404E+OO 6.828E-01 6.828E-01 102.23 OK 1764.49 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 OK U-238 63.29 3.70* 3.539E+OO 7 .133E-01 7.133E-01 288.28 OK 92.59 4.23 6.049E+OO 1. 730E+00 '1.730E+OO 60.04 OK AM-243 43.53 5.90 6.933E-01 Line Not Found Absent 74.66 67.20* 4.777E+OO 2.139E-01 2.139E-01 40.28 OK ANH-511 511. 00 100.00* 2.635E+OO 3.091E-02 3. 091E-02 186.67 OK Flag: "*" = Keyline Page 4250 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:53:57.55 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l *
  • Acquisition date 3-0CT-2016 07:52:25 Sensitivity : 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:26:00 Analyst initials: MXRl *
  • Sample ID G405235059 Sample Quantity 1.5422E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1.96-sigma) K-40 1.089E+Ol 1. 396E+OO KR-85 9.438E+OO 1.161E+Ol SR-85 9.167E-01 l.128E+OO CD-109 1.566E+OO 2.108E+OO SN-126 l.OlOE-01 l.360E-01 BA-137M 6.811E-02 4.136E-02 CS-137 7.195E-02 4.370E-02 CE-144 6.312E-01 5.775E-01 HG-203 1.319E+OO 3.257E+OO TL-208 2.859E-01 7.039E-02 PB-212 9.310E-01 l.181E-01 BI-214 7.946E-01 2.168E-01 PB-214 8.512E-01 1. 793E-01 RN-222 7.946E-01 2.168E-01 RA-224 1.048E+OO l.283E+OO RA-226 7.946E-01 2.168E-01 AC-228 5.125E-01 2.514E-01 RA-228 5.125E-01 2.514E-01 TH-228 9.310E-01 l.181E-01 TH-230 7. 943E:....01 2.167E-01 TH-232 5.125E-01 2.514E-01 TH-234 7 .133E-01 2.015E+OO U-234 7.943E-01 2.167E-01 U-238 7.133E-01 2.015E+OO AM-243 2.139E-01 8.445E-02 ANH-511 3.091E-02 5.655E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4251 of 5809 Key-Line Activity (pCi/GRAM 7.517E+OO -l.128E-02 O.OOOE+OO l.592E-02 K.L. Cnt Uncert ( 1. 96-sigma) l.102E+Ol 3.941E-02 1.022E+41 l.801E-02 MDA (pCi/GRAM 5.482E-01 1.007E+Ol 9.777E-01 2.042E+OO l.235E-01 5.203E-02 5.497E-02 6.368E-01 3.283E+OO 5.315E-02 8.188E-02 1.003E-01 l .119E-01 1.003E-01 8.779E-01 1.003E-01 1.938E-01 1.938E-01 8.188E-02 1.002E-01 1.938E-01 1.894E+OO l.002E-01 1.894E+OO 7.012E-02 4.124E-02 MDA (pCi/GRAM 2.294E+Ol 7.530E-02 O.OOOE+OO 5. 723E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 4.706E-02 2.583E-01 5.613E-01 FAIL ABUN V-48 O.OOOE+OO 8.489E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.034E+02 O.OOOE+OO SHORT HLIF MN-54 1. 713E-02 5.108E-02 1.lOlE-01 NOT IDENT. C0-56 1.229E-01 3.322E-01 7.339E-01 FAIL ABUN MN-56 0.000E+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 9.700E-04 4.375E-02 8.216E-02 NOT IDENT. C0-58 -4.837E-01 5.007E-01 7.692E-01 NOT IDENT. FE-59 -l.555E-01 4.542E+OO 9.330E+OO NOT IDENT. C0-60 ..-3.350E-02 3.385E-02 5.224E-02 NOT IDENT. ZN-65 -9.375E-02 l.761E-01 2.691E-01 NOT IDENT. GE-68 l.547E-01 2.376E+OO 4.753E+OO NOT IDENT. AS-73 l.536E+OO 6.234E+OO l.259E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.219E+03 O.OOOE+OO SHORT HLIF SE-75 3.439E-02 1.517E-01 3.126E-01 FAIL ABUN BR-77 O.OOOE+OO 2.049E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.713E+02 O.OOOE+OO SHORT HLIF RB-83 6.140E-02 5.735E-01 1.129E+OO NOT IDENT. RB-86 O.OOOE+OO 2.103E+04 O.OOOE+OO SHORT HLIF Y-88 1. 011E-02 1.654E-01 3.892E-01 NOT IDENT. Y-91 1.307E+02 4.997E+02 l.013E+03 NOT IDENT. NB-94 3.563E-03 3.026E-02 5.843E-02 NOT IDENT. NB-95 1.723E-01 6. 969E-01 1.380E+OO NOT IDENT. NB-95M -6.126E-01 2.043E+OO 3.555E+OO NOT IDENT. ZR-95 1.402E+OO 1. 311E+OO 2.880E+OO NOT IDENT. NB-97 O.OOOE+OO 8. 772E+40 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l .'858E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF RH-101 -2.778E-03 3.109E-02 5.766E-02 NOT IDENT. RH-102 l.395E-02 6.030E-02 1.186E-01 NOT IDENT. RU-103 -7. 381E-01 3.839E+OO 7.400E+00 FAIL ABUN RH-106 2.025E-01 4.601E-01 9.427E-01 NOT IDENT. RU-106 2.025E-01 4.601E-01 9.427E-01 NOT IDENT. AG-108M -1.490E-03 2.210E-02 4.348E-02 NOT IDENT. AG-110M -2. 896E-02 8.181E-02 1.588E-01 FAIL ABUN SN-113 l.070E-01 1.674E-01 3.605E-01 NOT IDENT. CD-115 O.OOOE+OO 2.577E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 5.855E+04 O.OOOE+OO SHORT HLIF TE-123M -l.493E-02 l.121E-01 2.048E-01 NOT IDENT. SB-124 5.087E-01 1. 730E+OO 3.951E+OO NOT IDENT. SB-125 -8.908E-04 9.241E-02 1.808E-01 FAIL ABUN TE-125M -2.700E+Ol 2.166E+02 4.046E+02 NOT IDENT. I-126 O.OOOE+OO 5.751E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6.989E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 4.437E+21 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 2. 211E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5. 996E+25 O.OOOE+OO SHORT HLIF BA-133 2. 962E-02 3.615E-02 7.228E-02 NOT IDENT. I-133 O.OOOE+OO 1.747E+41 0.000E+OO SHORT HLIF CS-134 4.534E-02 4.753E-02 1.030E-01 NOT IDENT. CS-135 -7. 331E-02 1.201E-01 2.259E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.051E+05 O.OOOE+OO SHORT HLIF CE-139 4.492E-02 1.00lE-01 l.912E-01 NOT IDENT. BA-140 O.OOOE+OO 7.700E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1.968E+05 O.OOOE+OO SHORT HLIF CE-141 -7.395E+OO 2.023E+Ol 3.319E+Ol NOT IDENT. CE-143 O.OOOE+OO l.585E+41 O.OOOE+OO SHORT HLIF PM-144 -7.689E-03 5.624E-02 1. 040E-01 NOT IDENT. PR-144 -7.228E-01 4.857E+OO 8. 963E+OO NOT IDENT. PM-146 7.277E-02 9.556E-02 7.303E-02 FAIL ABUN ND-147 O.OOOE+OO 1.914E+07 O.OOOE+OO SHORT HLIF PM-147 -1. 964E+02 7.712E+02 1.416E+03 NOT IDENT. PM-149 O.OOOE+OO 3.386E+39 O.OOOE+OO SHORT HLIF EU-150 1.155E-02 2.408E-02 4.548E-02 FAIL ABUN EU-152 7.353E-02 8.385E-02 l.790E-01 FAIL ABUN GD-153 -2.923E-02 l.502E-01 2.806E-01 NOT IDENT. EU-154 -3.012E-02 9.645E-02 l.833E-01 NOT IDENT. EU-155 1.494E-02 9.463E-02 l.818E-01 FAIL ABUN TB-160 1.505E-01 1.227E+OO 2.650E+OO FAIL ABUN H0-166M 2.305E-02 5.073E-02 1.044E-01 NOT IDENT. TM-171 1.147E+Ol 1.577E+Ol 3.302E+Ol NOT IDENT. HF-172 -4.844E-02 1. 948E-01 3.582E-01 FAIL ABUN LU-172 3.773E-02 6.077E-02 1.381E-01 FAIL ABUN LU-176 1.260E-02 2.082E-02 4.372E-02 FAIL ABUN HF-181 7.512E-01 3.840E+00 7.579E+OO FAIL ABUN Page 4252 of 5809 TA-182 5.890E-01 7.914E-01 1. 752E+OO FAIL ABUN RE-183 1.356E+00 2.158E+OO 4.444E+OO NOT IDENT. RE-184 1.928E+Ol 2.132E+01 4.980E+Ol NOT IDENT. W-188 2.429E+01 9. 271E+Ol 1. 721E+02 FAIL ABUN IR-192 -4.843E-02 4.043E-01 7.776E-01 FAIL ABUN BI-207 4.790E-02 4.467E-02 l.037E-01 FAIL ABUN PB-210 1. llOE+OO 2.483E+OO 5.099E+OO NOT IDENT. BI-211 O.OOOE+OO 4.938E-Ol 7.661E-01 FAIL ABUN PB-211 -1.553E-01 6.407E-01 l.158E+00 NOT IDENT. BI-212 O.OOOE+OO 9. 695E-CU 1.263E+OO FAIL ABUN RN-219 -l.461E-01 3.692E-01 6.090E-01 NOT IDENT. RA-223 -4.198E-01 5.266E-01 9.556E-01 FAIL ABUN AC-227 9.510E-03 l.800E-01 3.635E-01 NOT IDENT. TH-227 9.510E-03 1. 800E-01 3.635E-01 NOT IDENT. TH-229 -3.598E-01 4.533E-01 7.603E-01 FAIL ABUN PA-231 4.705E-02 3.484E-01 6.817E-01 NOT IDENT. TH-231 -4.198E-01 5.266E-01 9.556E-01 FAIL ABUN PA-233 1.272E-02 5.619E-02 1.128E-01 NOT IDENT. PA-234 1.094E-01 2.485E-01 5. 372E-01 NOT IDENT. PA-234M -2.999E+OO 3.997E+OO 7.239E+OO NOT IDENT. U-235 -4.179E-02 1.642E-01 2. 964E-01 FAIL ABUN NP-237 1. 272E-02 5.619E-02 l.128E-01 NOT IDENT. NP-238 O.OOOE+OO 2.881E+40 O.OOOE+OO SHORT HLIF NP-239 3.381E-03 2 .131E-01 4.026E-01 FAIL ABUN PU-239 -2.255E+Ol 2.991E+02 5. 531E+02 NOT IDENT. AM-241 -4.930E-02 1.177E-01 2.055E-01 NOT IDENT. CM-243 -l.268E-02 8.494E-02 1. 596E-01 FAIL ABUN BK-247 *1.355E-02 5.526E-02 l.140E-01 NOT IDENT. CM-247 -2.023E-02 3.396E-02 5.398E-02 FAIL ABUN CF-249 -2.376E-04 3.370E-02 6.606E-02 NOT IDENT. CF-251 5.777E-02 1.120E-01 2.005E-01 NOT IDENT. Page 4253of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:53:54.48 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 268 10.66* 1.122E+OO 1. 089E+Ol 1.089E+Ol 13.08 KR-85 514.00 21 0.43* 2.624E+OO 8.956E+OO 9.438E+OO 125.53 SR-85 514.00 21 96.00* 2.624E+OO 4.049E-02 9.167E-01 125.53 CD-109 88.03 85 3.70* 5.750E+OO l.938E+OO 3.004E+OO 70.39 SN-126 64.28 19 9.60 3.539E+OO 2.749E-01 2.749E-01 288.28 86.94 85 8.90 5.750E+OO 8.057E-01 8.057E-01 70.39 87.57 85 37.00* 5.750E+OO 1.938E-01 l.938E-01 70.39 BA-137M 661. 66 26 89.90* 2.138E+OO 6.687E-02 6. 811E-02 61. 97 CS-137 661. 66 26 85.10* 2.138E+OO 7.064E-02 7.195E-02 61. 97 CE-144 80.12 ------1. 36 5.243E+00 ------Line Not Found ------133.52 47 11. 09* 6.655E+OO 3.103E-01 6.312E-01 93.36 HG-203 70.83 ------3.69 4.380E+OO ------Line Not Found ------72.87 38 6.19 4.582E+00 6.482E-01 4. 981E+Ol 108.28 279.20 30 81. 56* 4.361E+OO 4.065E-02 3.123E+OO 105.50 TL-208 277.37 30 6.60 4.361E+OO 5.023E-01 5.023E-01 105.50 583.19 118 85.00* 2.366E+OO 2.859E-01 '2.859E-01 25.13 860.56 17 12.50 l.737E+00 3.815E-01 3.815E-01 86.16 BI-211 72. 87 38 1. 23 4.582E+OO 3.262E+OO 3.262E+OO 108.28 351.06 223 12.92* 3.591E+OO 2.345E+00 2.345E+OO 21. 49 PB-212 74.82 198 10.28 4.777E+00 1. 966E+OO 1. 966E+00 27.55 77 .11 239 17.10 5.000E+OO 1.359E+OO 1.359E+OO 23.60 238.63 411 43.60* 4.930E+00 9.310E-01 9.310E-01 12.94 300.09 ------3.30 4.103E+OO ------Line Not Found ------BI-214 609.32 170 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 1120.29 29 14.92 l.404E+OO 6.828E-01 6. 831E-01 102.23 1764.49 31 15.30 9.426E-01 1. 032E+OO 1. 032E+OO 38.16 PB-214 74.82 198 5.80 4.777E+OO 3.485E+OO 3.486E+00 27.55 77 .11 239 9.70 5.000E+OO 2.395E+OO 2. 396E+00 23.60 87.09 85 3.41 5.750E+OO 2.103E+00 2.104E+OO 70.39 242.00 116 7.25 4.879E+OO 1.599E+OO 1.600E+OO 43.01 295.22 158 18.42 4.159E+OO 1. 006E+OO 1.007E+OO 27.17 351. 93 223 35.60* 3. 591E+OO 8.509E-01 8.512E-01 21. 49 RN-222 609.32 170 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 1120.29 29 14.92 1.404E+OO 6.828E-01 6.831E-01 102.23 1764.49 31 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 RA-224 240.99 116 4.10* 4.879E+OO 2.828E+OO 2.828E+OO 43.01 RA-226 609.32 170 45.49* 2.284E+OO 7.943E-01 7.946E-01 27.84 1120.29 29 14.92 l.404E+00 6.828E-01 6.831E-01 102.23 1764.49 31 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 AC-228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 81 11. 27 3.713E+OO 9.407E-01 9.407E-01 45.57 794.95 ------4.25 l.849E+00 ------Line Not Found ------835. 71 ------1. 61 1.777E+OO ------Line Not Found ------911.20 45 25.80* 1.660E+00 5.125E-01 5.125E-01 50.05 968. 97 51 15.80 1. 581E+OO 9.879E-01 9.879E-01 45.02 RA-228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 81 11. 27 3. 713E+OO 9.407E-01 9.407E-01 45.57 Page 4254 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 ------4.25 1.849E+OO ------Line Not Found ------835. 71 ------1. 61 1.777E+OO ------Line Not Found ------911.20 45 25.80* 1.660E+OO 5.125E-01 5.125E-01 50.05 968. 97 51 15.80 1. 581E+OO 9.879E-01 9.879E-01 45.02 TH-228 74.82 198 10.28 4.777E+OO 1. 966E+OO 1. 966E+OO 27.55 77 .11 239 17.10 5.000E+OO 1.359E+OO 1.359E+OO 23.60 238.63 411 43.60* 4.930E+OO 9.310E-01 9.310E-01 12.94 300.09 ------3.30 4.103E+OO ------Line Not Found ------TH-230 609.32 170 45.49* 2.284E+OO 7.943E-01 7.943E-01 27.84 1120.29 29 14.92 l.404E+OO 6.828E-01 6.828E-01 102.23 1764.49 31 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 TH-232 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 81 11.27 3. 713E+OO 9.407E-01 9.407E-01 45.57 835.71 ------1. 61 1.777E+OO ------Line Not Found ------911.20 45 25.80* 1.660E+OO 5.125E-01 5.125E-01 50.05 968. 97 51 15.80 1.581E+OO 9.879E-01 9.879E-01 45.02 TH-234 63.29 19 3.70* 3.539E+OO 7 .133E-01 7 .133E-01 288.28 92.59 91 4.23 6.049E+OO 1.730E+OO 1. 730E+OO 60.04 U-234 609.32 170 45.49* 2.28'4E+OO 7.943E-01 7.943E-01 27.84 1120.29 29 14.92 1.404E+OO 6.828E-01 6.828E-01 102.23 1764.49 31 15.30 9.426E-01 1.032E+OO 1.032E+OO 38.16 U-238 63.29 19 3.70* 3.539E+OO 7.133E-01 7.133E-01 288.28 92.59 91 4.23 6.049E+OO 1.730E+OO 1.730E+OO 60.04 AM-243 43.53 ------5.90 6.933E-01 ------Line Not Found ------74.66 198 67.20* 4.777E+OO 3.008E-01 3.008E-01 27.55 ANH-511 511. 00 17 100.00* 2.635E+OO 3.091E-02 3.091E-02 186.67 Flag: "*" Key line Page 4255 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235059 Acquisition date 3-0CT-2016 07:52:25 Total number of lines in spectrum 42 Number of unidentified lines 9 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-40 KR-85 SR-85 CD-109 SN-126 BA-137M CS-137 CE-144 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 'RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 10.56Y 64.84D 461. 40D 2.30E+05Y 30.08Y 30.08Y 284.91D 46.59D l.41E+10Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600. OOY 1600. OOY 1. 41E+10Y 1600.00Y 1. 41E+10Y l.41E+l0Y 1. 41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 05 22.6 1. 55 1. 00 1. 02 1. 02 2.03 76.8 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.089E+Ol 8.956E+OO 4.049E-02 l.938E+OO 1.938E-01 6.687E-02 7.064E-02 3.103E-01 4.065E-02 2.859E-01 2.345E+OO 9.310E-01 7.943E-01 8.509E-01 7.943E-01 2.828E+OO 7.943E-01 5.125E-01 5.125E-01 9.310E-01 7.943E-01 5.125E-01 7 .133E-01 7.943E-01 7 .133E-01 3.008E-01 3.091E-02 3.795E+Ol 3.795E+Ol Decay Corr pCi/GRAM 1.089E+Ol 9.438E+OO 9.167E-01 3.004E+OO 1.938E-01 6. 811E-02 7.195E-02 6.312E-01 3.123E+OO 2.859E-01 2.345E+OO 9.310E-01 7.946E-01 8.512E-01 7.946E-01 2.828E+OO 7.946E-01 5.125E-01 5.125E-01 9.310E-01 7.943E-01 5.125E-01 7.133E-01 7.943E-01 7.133E-01 3.008E-01 3. 091E-02 4.378E+Ol 4.378E+Ol 78.57% Decay Corr 2-Sigma Error 0.142E+Ol 11. 85E+OO 11. 51E-01 2 .115E+OO 1.364E-01 4. 221E-02 4.459E-02 5.892E-01 3.295E+OO 0. 718E-01 0.504E+OO l.205E-01 2.212E-01 1. 829E-01 2.212E-01 1.216E+OO 2.212E-01 2.565E-01 2.565E-01 1.205E-01 2.212E-01 2.565E-01 20.56E-01 2.212E-01 20.56E-01 0.829E-01 5.771E-02 "M" Manually accepted . 2-Sigma %Error 13.08 125.53 125.53 70.39 70.39 61.97 61.97 93.36 105.50 25.13 21. 49 12.94 27.84 21. 49 27.84 43.01 27.84 50.05 50.05 12.94 27.84 50.05 288.28 27.84 288.28 27.55 186.67 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4256 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235059 Acquisition date : 3-0CT-2016 07:52:25 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 148.88 20 60 0.66 298.21 296 5 4.52E-03 **** 6.50E+OO 0 179.99 21 118 0.62 360.41 359 8 4.86E-03 **** 5. 96E+OO T 0 186.25 82 129 0.79 372. 93 368 10 l.90E-02 64.2 5.85E+OO T 0 2.09.57 58 121 1. 94 419.57 415 lJ_ l.36E-02 85.0 5.42E+OO T 0 382.20 13 23 0.78 764.75 762 7 3.33E-03 **** 3.35E+OO 0 399.15 22 39 1. 03 798.65 794 11 5.52E-03 **** 3.23E+OO 0 452.96 26 48 1. 83 906.24 896 16 6.46E-03 **** 2.91E+OO T 0 463.12 35 30 1.23 926.56 921 11 8.87E-03 72.7 2.86E+OO T 2 588.34 21 19 1. 93 117 6. 94 1159 27 5.36E-03 98.3 2.35E+OO 0 598.02 11 32 0.50 1196. 30 1187 12 2.78E-03 **** 2.32E+OO 0 657.01 25 19 2.79 1314.27 1305 15 6.58E-03 89.5 2.15E+OO T 0 670.17 7 34 4.30 1340.57 1328 16 l.94E-03 **** 2.12E+OO 0 727 .18 35 29 1. 59 1454.57 1448 14 9.39E-03 76.1 1. 98E+OO T 0 769.31 36 24 6.17 1538.83 1528 19 9.72E-03 74.7 1. 90E+OO 0 963. 99 14 8 0.63 1928.14 1922 9 3.79E-03 95.3 1.59E+OO T 0 1236.82 38 10 4.95 2473.72 2464 20 1. 08E-02 51. 0 l.29E+OO T 0 1244.12 14 3 1. 57 2488.33 2485 8 3.89E-03 71. 4 1.29E+OO 0 1250 .13 21 0 1. 06 2500.33 2494 13 5.83E-03 43.6 1. 28E+OO Flags: "T" = Tentatively associated Page 4257 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:54:12.33 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l * *Acquisition date 3-0CT-2016 07:52:25 Sensitivity 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:26:00 Nuclide Library : SOLID *
  • Sample ID G405235059 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.5422E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Le Nuclide (pCi/GRAM K-40 2.186E-01 KR-85 4.402E+OO SR-85 4.275E-01 CD-109 9.696E-01 SN-126 5.842E-02 BA-137M 2.243E-02 CS-137 2.369E-02 CE-144 2.991E-01 HG-203 l.492E+00 TL-208 2.320E-02 PB-212 3.771E-02 BI-214 4.361E-02 PB-214 5.057E-02 RN-222 4.361E-02 RA-224 4.044E-01 RA-226 4.361E-02 AC-228 8.121E-02 RA-228 8.121E-02 TH-228 3.771E-02 TH-230 4.359E-02 TH-232 8.121E-02 TH-234 8.916E-01 U-234 4.359E-02 U-238 8.916E-01 AM-243 3.284E-02 l.803E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 Le (pCi/GRAM 1.042E+Ol 3.112E-02 O.OOOE+OO 2.142E-02 2.362E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-ll3 CD-ll5 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU_.:150 EU-152 GD-153 Eu.:...154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4259 of 5809 O.OOOE+OO O.OOOE+OO 4.782E-02 3.144E-01 O.OOOE+OO 3.849E-02 3.199E-01 3.884E+OO 2.004E-02 l.131E-01 2.075E+OO 5.889E+OO O.OOOE+OO l.423E-01 O.OOOE+OO O.OOOE+OO 5.036E-01 O.OOOE+OO l.457E-01 4.452E+02 2.589E-02 6.063E-01 l.645E+OO 1. 288E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.700E-02 5.298E-02 3. 219E+OO 4.190E-01 4.190E-01 1. 923E-02 6.717E-02 l.616E-01 O.OOOE+OO O.OOOE+OO 9.524E-02 l.568E+OO 8.122E-02 l.888E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.286E-02 O.OOOE+OO 4.591E-02 l.034E-01 O.OOOE+OO O.OOOE+OO 8.951E-02 O.OOOE+OO O.OOOE+OO l.548E+Ol O.OOOE+OO 4.621E-02 3.982E+OO 3.252E-02 O.OOOE+OO 6.623E+02 O.OOOE+OO 2. 081E-02 8.213E-02 l.312E-Ol 7.561E-02 8.512E-02 l. llOE+OO 4.603E-02 l.548E+Ol l.666E-01 5. 9llE-02 2.004E-02 3.427E+OO 7.658E-01 SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDE:NT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN RE-183 RE-184 W-188 IR-192 BI-207 PB-210 BI-211 PB-211 BI-212 -RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4260 of 5809 2.087E+OO 2.170E+Ol 7.866E+Ol 3.560E-01 4.564E-02 2.392E+OO 3.684E-01 5.221E-01 5.804E-01 2. 722E-01 4.330E-01 1.661E-01 1.661E-01 3.525E-01 3.093E-01 4.330E-01 5.192E-02 2.339E-01 3.101E+00 l.385E-01 5.192E-02 O.OOOE+OO 1.880E-01 2.599E+02 9. 611E-02 7.444E-02 5.193E-02 2.403E-02 2.989E-02 9.357E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN . NOT FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:54:19.23 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235059.CNF;l *
  • Acquisition date 3-0CT-2016 07:52:25 Sensitivity 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.48 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:26:00 Nuclide Library : SOLID *
  • Sample ID G405235059 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.5422E+02 GRAM *
  • Quantity Err(%) : 1.2968E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. CaL. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.089E+Ol 1.508E+OO 1.508E+OO KR-85 9.438E+OO 1.162E+Ol 1.162E+Ol SR-85 9.167E-01 1.128E+OO 1.128E+OO CD-109 1.566E+OO 2 .119E+OO 2 .119E+OO SN-126 1.0lOE-01 1.366E-Ol 1.366E-01 BA-137M 6. 811E-02 4.147E-02 4.147E-02 CS-137 7.195E-02 4.381E-02 4.381E-02 CE-144 6.312E-01 5.785E-01 5.785E-01 HG-203 1.318E+OO 3.264E+OO 3.264E+OO TL-208 2.859E-01 7.143E-02 7.143E-02 PB-212 9.310E-01 1.280E-01 1.280E-01 BI-214 7.946E-01 2.195E-01 2.195E-01 PB-214 8.512E-01 l.827E-01 1.827E-01 RN-222 7.946E-01 2.195E-01 2.195E-01 RA-224 1.048E+OO 1.289E+OO 1.289E+OO RA-226 7.946E-01 2.195E-01 2.195E-01 AC-228 5.125E-01 2.528E-01 2.528E-01 RA-228 5.125E-01 2.528E-01 2.528E-01 TH-228 9.310E-01 l.280E-01 1.280E-01 TH-230 7.943E-01 2.194E-01 2.194E-01 TH-232 5.125E-01 2.528E-01 2.528E-01 TH-234 7.133E-Ol 2. 021E+OO 2. 021E+OO U-234 7.943E-Ol 2.194E-01 2.194E-01 U-238 7.133E-01 2.021E+OO 2.021E+OO AM-243 2.139E-01 '8.617E-02 8.617E-02 ANH-511 3.091E-02 5.657E-02 5.657E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 7.517E+OO l.102E+Ol 1.153E+Ol NOT IDENT. NA-22 -l.128E-02 3. 941E-02 3.974E-02 NOT IDENT. NA-24 1.000E+41 l.107E+41 O.OOOE+OO SHORT HLIF AL-26 1.592E-02 1.804E-02 l.941E-02 NOT IDENT. Page 4261 of 5809 SC-46 4.706E-02 2.583E-01 2.592E-01 FAIL ABUN V-48 -3. 711E+02 8.489E+03 8.491E+03 SHORT HLIF CR-51 l.104E+02 3.035E+02 3.075E+02 SHORT HLIF MN-54 l.713E-02 5.109E-02 5.167E-02 NOT IDENT. C0-56 l.229E-01 3.323E-01 3.369E-01 FAIL ABUN MN-56 l.OOOE+41 2.704E+41 O.OOOE+OO SHORT HLIF C0-57 9.700E-04 4.375E-02 4.376E-02 NOT IDENT. C0-58 -4.837E-01 5.012E-01 5.465E-01 NOT IDENT. FE-59 -l.555E-01 4.542E+OO 4.543E+OO NOT IDENT. C0-60 -3.3.50E-02 3.388E-02 3.709E-02 NOT,IDENT. ZN-65 -9.375E-02 l.762E-01 l.812E-01 NOT IDENT. GE-68 l.547E-01 2.376E+OO 2.377E+OO NOT IDENT. AS-73 l.536E+OO 6.242E+OO 6.281E+OO NOT IDENT. AS-74 -5.451E+02 5.219E+03 5.225E+03 SHORT HLIF SE-75 3.439E-02 l.517E-01 l.525E-01 FAIL ABUN BR-77 l.615E+37 l.361E+38 O.OOOE+OO SHORT HLIF SR-82 -2.799E+02 5.715E+02 5.852E+02 SHORT HLIF RB-83 6.140E-02 5.736E-01 5.742E-01 NOT IDENT. RB-86 5.340E+03 2 .103E+04 2. ll 7E+04 SHORT HLIF Y-88 1. OllE-02 l.654E-01 l.655E-01 NOT IDENT. Y-91 l.307E+02 4.997E+02 5.032E+02 NOT IDENT. NB-94 3.563E-03 3.026E-02 3.030E-02 NOT IDENT. NB-95 1. 723E-01 6.970E-01 7.013E-01 NOT IDENT. NB-95M -6.126E-01 2.043E+OO 2.062E+OO NOT IDENT. ZR-95 l.402E+OO l.312E+00 l.457E+OO NOT IDENT. NB-97 l.OOOE+41 8.783E+40 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 3. 836E+42 O.OOOE+OO SHORT HLIF M0-99 -l.984E+29 l.858E+31 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 6.515E+41 O.OOOE+OO SHORT HLIF RH-101 -2.778E-03 3.109E-02 3 .112E-02 NOT IDENT. RH-102 l.395E-02 6.031E-02 6.064E-02 NOT IDENT. RU-103 -7. 381E-01 3.839E+OO 3.854E+OO FAIL ABUN RH-106 2.025E-01 4.603E-01 4.693E-01 NOT IDENT. RU-106 2.025E-01 4.603E-01 4.693E-01 NOT IDENT. AG-108M -1. 490E-03 2.210E-02 2.211E-02 NOT IDENT. AG-llOM -2. 896E-02 8.183E-02 8.286E-02 FAIL ABUN SN-113 l.070E-01 l.674E-01 l.742E-01 NOT IDENT. CD-115 -7.974E+37 2.581E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -2. 712E+04 5.864E+04 5.990E+04 SHORT HLIF TE-123M -l.493E-02 l.121E-01 l.123E-01 NOT IDENT. SB-124 5.087E-01 1. 730E+OO l.745E+OO NOT IDENT. SB-125 -8.908E-04 9.241E-02 9.241E-02 FAIL ABUN TE-125M -2.700E+Ol 2.166E+02 2.170E+02 NOT IDENT. I-126 9.486E+04 5.753E+05 5.769E+05 SHORT HLIF SB-126 -6.315E+05 7.085E+05 7.636E+05 SHORT HLIF SB-127 -l.457E+21 4.846E+21 O.OOOE+OO SHORT HLIF I-131 6.764E+08 2. 211E+09 2.232E+09 SHORT HLIF I-132 -l.OOOE+41 l.919E+42 O.OOOE+OO SHORT HLIF TE-132 -4.833E+25 6.293E+25 O.OOOE+OO SHORT HLIF BA-133 2.962E-02 3.617E-02 3.856E-02 NOT IDENT. I-133 l.OOOE+41 2.480E+41 O.OOOE+OO SHORT HLIF CS-134 4.534E-02 4.757E-02 5.178E-02 NOT IDENT. CS-135 -7.331E-02 l.202E-01 l.246E-01 NOT IDENT. I-135 l.OOOE+41 8.580E+41 O.OOOE+OO SHORT HLIF CS-136 -l.130E+05 2.055E+05 2. ll 7E+05 SHORT HLIF CE-139 4.492E-02 l.005E-01 l.025E-01 NOT IDENT. BA-140 -6.681E+04 7.700E+05 7.706E+05 SHORT HLIF LA-140 9.152E+04 1. 969E+05 2.012E+05 SHORT HLIF CE-141 -7.395E+OO 2.024E+Ol 2. 051E+Ol NOT IDENT. CE-143 l.OOOE+41 l.588E+41 O.OOOE+OO SHORT HLIF PM-144 -7.689E-03 5.624E-02 5.635E-02 NOT IDENT. PR-144 -7.228E-01 4.857E+OO 4.868E+OO NOT IDENT. PM-146 7.277E-02 9.570E-02 l.012E-01 FAIL ABUN ND-147 4.171E+06 l.914E+07 l.924E+07 SHORT HLIF PM-147 -1. 964E+02 7. 712E+02 7.763E+02 NOT IDENT. PM-149 -6.735E+38 3:389E+39 O.OOOE+OO SHORT HLIF EU-150 l.155E-02 2.409E-02 2.464E-02 FAIL ABUN EU-152 7.353E-02 8.395E-02 9.025E-02 FAIL ABUN GD-153 -2.923E-02 L 502E-01 l.508E-01 NOT IDENT. EU-154 -3.012E-02 9.646E-02 9.741E-02 NOT IDENT. EU-155 l.494E-02 9.464E-02 9.488E-02 FAIL ABUN TB-160 l.505E-01 l.227E+OO l.229E+OO FAIL ABUN H0-166M 2.305E-02 5.075E-02 5.180E-02 NOT IDENT. TM-171 1.147E+Ol l.581E+Ol l.663E+Ol NOT IDENT. HF-172 -4.844E-02 l.950E-01 1. 962E-01 FAIL ABUN LU-172 3.773E-02 6.089E-02 6.322E-02 FAIL ABUN LU-176 1. 2 60E-02 2.083E-02 2.159E-02 FAIL ABUN HF-181 7.512E-01 3.841E+OO 3.856E+OO FAIL ABUN Page 4262 of 5809 TA-182 5.890E-01 7.917E-01 8.350E-01 FAIL ABUN RE-183 1.356E+OO 2.169E+OO 2.253E+OO NOT IDENT. RE-184 1.928E+01 2.179E+Ol 2.346E+Ol NOT IDENT. W-188 2.429E+Ol 9.275E+Ol 9.340E+Ol FAIL ABUN IR-192 -4.843E-02 4.043E-01 4.049E-01 FAIL ABUN BI-207 4.790E-02 4.471E-02 4.965E-02 FAIL ABUN PB-210 1. llOE+OO 2.485E+OO 2.535E+OO NOT IDENT. BI-211 2.345E+OO 5.048E-01 1.171E+OO FAIL ABUN PB-211 -1.553E-01 6.408E-01 6.446E-01 NOT IDENT. .. BI-212 1.300E+OO 9.717E-01 l.135E+OO FAIL ABUN RN-219 -l.461E-01 3.697E-01 3.755E-01 NOT IDENT. RA-223 -4.198E-01 5. 272E-01 5.602E-01 FAIL ABUN AC-227 9.510E-03 1. 800E-01 l.800E-01 NOT IDENT. TH-227 9.510E-03 1. 800E-01 1.800E-01 NOT IDENT. TH-229 -3.598E-01 4.536E-01 4.817E-01 FAIL ABUN PA-231 4.705E-02 3.485E-01 3.492E-01 NOT IDENT. TH-231 -4.198E-01 5. 272E-01 5.602E-01 FAIL ABUN PA-233 1. 272E-02 5.619E-02 5.649E-02 NOT IDENT. PA-234 1.094E-01 2.782E-01 2.826E-01 NOT IDENT. PA-234M -2.999E+OO 3.999E+00 4. 221E+OO NOT IDENT. U-235 -4.179E-02 l.642E-01 l.653E-01 FAIL ABUN NP-237 1. 272E-02 5.619E-02 5.649E-02 NOT IDENT. NP-238 -1. 519E+40 2.882E+40 0.000E+OO SHORT HLIF NP-239 3.381E-03 2 .131E-01 2.131E-01 FAIL ABUN PU-239 -2.255E+Ol 2. 991E+02 2.993E+02 NOT IDENT. AM-241 -4.930E-02 1.178E-01 l.199E-01 NOT IDENT. CM-243 -1. 268E-02 8.495E-02 8.514E-02 FAIL ABUN BK-247 l.355E-02 5.532E-02 5.566E-02 NOT'IDENT. CM-247 -2.023E-02 3.413E-02 3.533E-02 FAIL ABUN CF-249 -2.376E-04 3.370E-02 3.370E-02 NOT IDENT. CF-251 5.777E-02 1.122E-01 l.152E-01 NOT IDENT. Page 4263 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 61.8428 87.09 102. 9616 136.47 51. 4932 45.60 57.4230 87.57 103.0528 140.51 0.0000 46.54 57.5739 88.03 119.2779 143.76 68.8229 49. 72 0.0000 88.34 119. 3454 144.24 61.9794 51. 35 64.1545 88.47 101.1167 145.44 73.5732 51. 87 58.4010 89. 96 88.7174 152.43 67.2784 52.39 58.4795 1093.63 88.8264 153.25 0.0000 52.97 60.5187 91.11 0.0000 323.87 74.4053 53.44 64.5002 9*2. 59 96. 5653 156.02 0.0000 54.07 67.5397 93.35 96.6951 158.56 0.0000 57.36 0.0000 94.56 86.6078 159.00 61.9848 57.53 65.1581 94.65 86.6214 162.33 65.7600 57.98 65.2286 94.67 86.6245 162.66 0.0000 59.27 87.2403 94.87 86.6550 163.33 59. 9610 59.32 87.2507 97.43 64.2096 165.86 61. 3231 59.54 80.6830 98.43 81. 4719 176.31 65.6583 60. 96 72. 9904 98.44 81. 4731 176.60 0.0000 61.17 67.7149 " 99.53 64.4398 177.52 52.5991 62.93 86.9879 100 .11 64.5030 181.07 0.0000 63.29 87.0594 102.03 64. 7113 181.52 52.8375 63.58 87.1170 103.18 68.0762 184.41 67.4647 64.28 82.9090 103.37 68.0978 143.76 49.8673 66.73 95.4640 105.21 68.3035 193.51 73.0042 67.24 85.8119 105.31 68.3146 197.03 54.9584 125.81 88. 9265 106.12 48.8607 198.01 79.4667 67.75 88.9399 106.47 49.9745 201.83 73.6478 69.67 90.6631 109.28 64.3877 203.43 62.7049 70.83 81. 3916 111. 00 72.2227 205.31 54.2031 72.81 72. 5357 111.76 0.0000 210.85 52.0322 72.87 72.5449 114. 06 73.6677 215.65 54.7717 74.66 72.8130 116.30 0.0000 222 .11 41. 7 577 74.82 72.8369 116.74 66.2425 227.09 46.1545 74.97 72. 8596 119.76 68.7633 227.38 52.0432 77 .11 73.1754 121.12 73.3477 228.16 0.0000 78.74 85.4764 121. 22 76.6932 228.18 62.1635 79.69 78.7304 121.78 81.2066 116.74 62.1635 80.12 78.7965 122.06 73.4499 235.69 58.3753 80.19 0.0000 122.92 61.2859 235. 96 52.0430 80.57 65.0300 123.07 61.2993 238.63 45.8097 81. 00 73.3926 265.00 58.0073 238.98 0.0000 81. 07 74.7878 125.81 64.9013 240.99 45.9091 81. 75 78.0064 127.23 75.1253 242.00 45.9514 83.79 79.3555 127.91 54. 9962 244.70 46.0646 84.00 84.9584 129.30 83.2195 252.40 0.0000 85.43 86.5839 131.20 66.1531 252.80 48.9774 86.55 102.8584 133.02 88.9309 254.15 0.0000 8 6. 7 9 102.9040 133.52 79.9432 256.23 37.0599 86.94 102.9332 136.00 57.5141 260.90 0.0000 Page 4264 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 31.2539 355.39 0.0000 584.27 15.8899 2 64. 80 29.5217 356.01 20.9486 595.83 0.0000 265.00 31.2634 364.49 0.0000 427.87 22.4159 268.22 49.6361 366.42 0.0000 602.52 0.0000 269.46 37.4841 372. 51 31. 0698 604.72 17.6461 270.03 37.5025 375.05 26.4067 607.14 ,14.9889 271.23 37.5401 377.52 27.3946 609.32 15.0043 273.65 0.0000 356.01 32.7256 610.33 15. 0111 276.40 27.6195 388.16 30.4388 614.28 8.0560 277.37 34.2226 388.63 0.0000 618.01 21. 5194 277.60 33.3521 391.69 17.1606 620.36 21. 5422 278.00 33.3629 264.66 24.4500 621. 93 16.1682 279.20 33.3961 401.81 30.2247 630.19 0.0000 279.54 33.4054 402.40 31. 6760 631. 29 20.5656 279.70 33.4093 404.85 32.3012 633.25 22.7500 280.46 46.1864 410.95 33.7752 634.78 0.0000 283.69 38.1059 413.71 28.9996 635.95 24.9466 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.6318 423.72 0.0000 645.85 10.8936 285.90 0.0000 427.09 29.2358 657.76 22.9952 287.50 40.7011 427.87 26.3249 657.90 0.0000 290.67 33.2642 433.94 20.5493 661.66 13.1621 293.27 0.0000 439.40 25.5239 664.57 0.0000 351. 93 39.1714 453.88 21.7793 666.33 0.0000 295. 96 39.1947 463.37 21. 8971 ' 666.50 0.0000 879.38 33.4732 468.07 13.4725 667.71 0.0000 299.98 25.4675 473.00 0.0000 677.62 14.3558 300.09 25.4698 475.06 22.0407 685.70 0.0000 300 .13 25.47*09 476.78 28.0786 695.00 0.0000 301.36 29.5209 477.60 23.0749 696.49 23.3729 302.85 42.0937 482.18 27.1566 696. 51 23.3729 256.23 33.1797 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.2673 306.78 30.5434 497.08 17.2369 697.49 23.3823 308.46 38.6774 505.52 22.9161 702.65 18. 9687 311. 90 40.5835 507.63 0.0000 706.68 16.7645 316.51 38.9145 511. 00 16.3428 711. 68 13.4390 319.41 0.0000 514.00 16.3685 720. 70 0.0000 320.08 0.0000 514.00 16.3685 721. 93 0.0000 321. 04 28.1499 520.40 21. 5554 722.78 15.1864 323.87 44.5887 520.69 0.0000 722. 91 11.8125 325.23 50.0978 522.65 0.0000 723.31 11. 8142 328.76 0.0000 527.90 0.0000 724.19 3.3767 333.37 20.8916 528.26 22.6732 727.33 15.7773 333.97 30.2513 529.59 18.5632 733.00 11. 8599 334.37 33. 0110 529.87 0.0000 735.93 9.0465 338.28 28.5056 531. 02 0.0000 333.97 10.1836 338.32 28.5069 537.26 0.0000 739.50 0.0000 311. 90 24.8665 546.56 0.0000 747.24 7.9508 340.48 24.8665 552.55 20.8643 748.06 14.7705 340.55 0.0000 563.25 15.7306 752.31 14.7948 344.28 27.7039 569.33 29.4504 753.82 0.0000 345.93 27.7362 946.00 29.4526 756.73 11. 4001 351.06 29.6921 569.70 28.4030 756.80 11. 4006 351.93 29.7096 583.19 15.8813 884.68 17.1478 Page 4265 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 14.8720 1274.44 12.9998 1620.50 5.4312 766.42 14.8757 1001.03 16.7388 1621.92 2.1731 766.84 14.8778 1002.74 15.8171 1678.03 0.0000 772.60 0.0000 1004.73 12.1030 1690.97 3.3058 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739. 5.0 0.0000 0.0000 1764.49 778.90 16.0958 1028.54 0.0000 1063.66 3.3576 783.70 0.0000 1037.84 9.4037 1771.35 1.1194 785.37 19.5926 1038.76 0.0000 1791.20 0.0000 792.07 24.2633 631.29 16.0288 1808.65 0.0000 794.95 15.0360 1048.07 0.0000 1810.72 0.0000 795.86 11.5702 1049.04 14.1531 1836.06 2.7199 810.06 17.4463 1050.41 11.3269 810.29 17.4475 1063.66 7. 5811 344.28 18.6120 1077.00 0.0000 810.76 18.6139 1077.34 15.2227 815.77 0.0000 1085.87 13. 3523 1048.07 0.0000 1093.63 6. 6911 832.01 16.7056 1099.45 8.6177 834.85 11. 4417 1112. 07 6.5893 835.71 10.5648 1112.84 9.2268 836.80 0.0000 1115.54 15.3896 846.75 0.0000 1120.29 10.5945 846.77 8.8388 1120.55 10.59'58 856.80 0.0000 1221.41 10.5978 860.56 9.9473 1129. 67 6.7599 871.09 15.1536 1131.51 0.0000 873.19 8.9203 1147.95 0.0000 875.33 0.0000 1173.23 17.5924 879.38 8.0456 1177.95 15. 6572 880.51 12.5200 1189.05 10.7966 883.24 5.3707 1204.77 14.7849 884.68 13.4335 1221.41 8.9099 889.28 8. 0725 1231. 02 6.3516 894.76 12.5807 1235.36 0.0000 898. 04 8. 9963 1238.28 12.7273 900. 72 14.4067 1260.41 0.0000 903.28 7.2095 1271.87 8.0234 911. 20 9.0359 1274.44 10.0360 912.08 13.0153 1274.54 10.0360 923.98 0.0000 1291.59 9.0714 926.50 9.0817 1298.22 0.0000 929 .11 9.9983 1312 .11 0.0000 937.49 21. 8745 1332.49 11. 2001 944.13 0.0000 1362. 66 0.0000 946.00 10.9673 1365.19 4.1050 949.00 19.2113 1368.63 0.0000 667.71 0.0000 1384.29 6.1857 962.31 11.7598 1408.01 6.2201 964.08 22.0620 1457.56 0.0000 966 .17 22.0767 1460.82 5.2466 911.20 10.3117 1489.16 4.2241 968. 97 10.3117 1505.03 10.5975 983.53 0.0000 1584.12 9.7020 984.45 0.0000 1596.21 0.0000 Page 4266 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:54:50.50 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM18.CNF;511 Background date : Z-OCT-2016 11:01:02. Sample date 16-DEC-2015 12:33:00 Acquisition date : 3-0CT-2016 07:52:52. Sample ID G405235060 Sample quantity 1.52266E+02 GRAM Detector name : GAM18 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.97 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 4 4 0 4 4 4 0 3 3 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 52.18 63.20* 74.85 77.19* 84.19* 87.07 89.95 92.65* 98.34 105.29 107.63 129. 29 166.52 209.69 238.86* 241.93 277.02 295.58* 328.12 337.01* 352.22* 463.23 511.13* 584.24* 609.73* 661.89 728.51 770.32 794.93* 861.65 912.24* 936.58 970.08* 1072. 48 Page 4267of5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 14 11 151 196 30 93 74 92 83 55 32 30 94 74 414 131 44 199 52 25 359 27 64 130 265 51 50 52 25 30 121 34 53 7 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 130 195 154 142 127 106 119 113 101 98 64 124 215 161 95 68 70 99 96 211 98 44 86 90 89 24 33 55 22 24 35 59 41 31 1. 29 1.10 1.15 1.18 1.13 1. 34 1.16 1.12 2.24 1. 38 1. 04 1.11 5.83 1. 29 1. 23 1. 53 1. 73 1. 08 6.58 1. 46 1. 30 1. 48 3.11 1.10 1.94 2.64 0.90 4.57 2.36 1. 63 1. 79 2.90 1. 53 0.49 105.19 127.21 150.50 155.16 169.15 174.91 180.67 186.05 197.43 211.31 216.00 259.27 333.68 419.95 478.25 484.38 554.50 591. 59 656.64 674.41 704.79 926.66 1022.40 1168.51 1219.48 1323.73 1456.88 1540.47 1589.66 1723.03 1824.15 1872.80 1939.78 2144.48 101 122 146 146 166 172 172 172 193 205 205 255 324 414 473 473 550 586 648 671 698 921 1013 1160 1213 1317 1449 1527 1582 1715 1816 1862 1933 2134 7 3.75E-03142.4 9 2.97E-03243.0 13 4.21E-02 15.8 4.04E-01 13 5.45E-02 12.8 6 8.40E-03 63.6 21 2.58E-02 20.1 2.30E+OO 21 2.05E-02 27.0 21 2.56E-02 24.3 9 2.30E-02 24.8 15 1.52E-02 35.0 l.67E+OO 15 8.93E-03 45.0 8 8.40E-03 67.0 19 2.61E-02 39.1 13 2.05E-02 37.4 16 l.15E-01 6.3 5.06E+OO 16 3.63E-02 17.1 9 1.21E-02 38.2 12 5.53E-02 12.4 16 l.45E-02 44.7 18 6.91E-03140.8 14 9.98E-02 8.0 10 7.47E-03 50.4 19 41.8 19 3.62E-02 20.5 17 7.36E-02 10.5 12 l.42E-02 23.8 14 1.38E-02 28.9 22 1. 45E-02 38. 9 15 7.05E-03 46.7 14 8.39E-03 39.2 18 3.36E-02 15.2 26 9.49E-03 60.8 14 l.47E-02 29.9 16 1.96E-03173.7 Peak Search Report (continued) Page : 2 Sample ID : G405235060 Acquisition date 3-0CT-2016 07:52:52 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1100.48 34 28 8.92 2200.47 2187 23 9.46E-03 44.2 36 0 1121.39* 51 31 2.03 2242.26 2236 12 1.42E-02 27.2 37 0 1238..36 52 8 1. 96 2476.12 2467 1.7 1.43E-02 19.0 38 0 1281. 49 26 17 8.79 2562.33 2551 22 7.34E-03 43.8 39 0 1416.11 14 7 1. 58 2831. 50 2825 14 3.89E-03 48.2 40 0 1461.62* 538 0 2.88 2922.49 2912 20 1.49E-01 4.4 41 0 1624.62 8 7 1. 34 3248.40 3240 13 2.08E-03 79.0 42 0 1766.95* 25 21 1. 91 3533.01 3522 16 7.02E-03 46.2 Flag: "*" = Peak area was modified by background subtraction Page 4268 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:54:52 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 16-DEC-2015 12:33:00 G405235060 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:52:52 152.27 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA18 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 4269 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 RA-224 240.99 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.97 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235060 Acquisition date 3-0CT-2016 07:52:52 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. 911E+OO 1.258E+Ol 1.258E+Ol 8.70 OK AS-73 *53_44 10.30* l.379E+OO 6.226E-01 7. 731E+OO 284.82 OK CD-109 88.03 3.70* 6 .119E+OO 1.619E+OO 2.510E+OO 65. 60 OK SN-126 64.28 9.60 3.086E+OO 2.325E-01 2.325E-01 486.00 OK 86.94 8.90 6 .119E+OO 6.732E-01 6.732E-01 65.60 OK 87.57 37.00* 6 .119E+OO 1.619E-01 l.619E-01 65.60 OK BA-137M 661. 66 89.90* 3.371E+OO 8.731E-02 8.893E-02 47.55 OK CS-137 661. 66 85.10* 3.371E+OO 9.223E-02 9.395E-02 47.55 OK CE-139 165.86 80.00* 7.900E+OO 8.805E-02 3.828E-01 78.21 OK EU-155 86.55 30.70 6 .119E+OO l.952E-01 2.193E-01 65.60 OK 105.31 21.10* 7.389E+OO 2.170E-01 2.439E-01 70.02 OK TM-171 51. 35 0.27 1.379E+OO 2.375E+Ol 3.169E+Ol 284.82 OK 52.39 0.47* 1. 37 9E+OO 1.364E+Ol 1. 821E+Ol 284.82 OK 66.73 0.14 3.622E+OO Line Not Found Absent TL-208 277.37 6.60 6.132E+OO 6.083E-01 6.083E-01 76.34 OK 583.19 85.00* 3.673E+OO 2.195E-01 2.195E-01 41. 05 OK 860.56 12.50 2.812E+OO 4.335E-01 4.335E-01 78.30 OK BI-211 72.87 1. 23 4.495E+OO Line Not -Found Absent 351. 06 12.92* 5.219E+OO 9.795E-02 9.795E-02 868.18 OK PB-212 74.82 10.28 4.756E+OO 1.387E+OO 1.387E+OO 46.14 OK 77 .11 17.10 5.050E+OO 1.440E+OO l.440E+00 25.57 OK 238.63 43.60* 6.719E+OO 8.109E-01 8.109E-01 12. 67 OK 300.09 3.30 5.819E+OO Line Not Found Absent BI-214 609.32 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 OK 1120.29 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 OK 1764.49 15.30 1.634E+OO Line Not Found Absent PB-214 74.82 5.80 4.752E+OO Line Not Found <<INT Reject 77 .11 9.70 5.050E+OO 2.539E+OO 2.540E+OO 25.57 OK 87.09 3.41 6.121E+OO Line Not Found <<INT Reject 242.00 7.25 6.668E+OO Line Not Found <<INT Reject 295.22 18.42 5.877E+OO 1.033E+OO 1.033E+OO 24.89 OK 351. 93 35.60* 5.221E+00 Line Not Found <<INT Reject RN-222 609.32 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 OK 1120.29 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 OK 1764.49 15.30 1.634E+OO Line Not Found Absent RA-224 240.99 4.10* 6.669E+00 9.142E-01 9.142E-01 113. 85 OK RA-226 609.32 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 OK 1120.29 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 OK 1764.49 15.30 1.634E+OO Line Not Found Absent AC-228 105.21 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 OK 338.32 11. 27 5.379E+OO 2.278E-01 2.278E-01 281. 64 OK 794.95 4.25 2.973E+00 l.022E+OO l.022E+OO 93.48 OK 835.71 1. 61 2. 872E+OO Line Not Found Absent 911. 20 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 OK 968.97 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 OK RA-228 105.21 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 OK 338.32 11. 27 5.379E+OO 2.278E-01 2.278E-01 281. 64 OK 794.95 4.25 2.973E+OO 1.022E+OO 1.022E+OO 93.48 OK 835. 71 1. 61 2.872E+OO Line Not Found Absent Page 4270 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235060 Acquisition date 3-0CT-2016 07:52:52 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 911.20 2,P. 8 O* 2.703E+OO 8.687E-01 8.687E-01 30 .. 43 OK 968. 97 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 OK TH-228 74.82 10.28 4.756E+OO 1.387E+OO 1.387E+OO 46.14 OK 77 .11 17.10 5.050E+OO 1.440E+OO 1.440E+OO 25.57 OK 238.63 43.60* 6. 719E+OO 8.109E-01 8.109E-01 12.67 OK 300.09 3.30 5.819E+OO Line Not Found Absent TH-229 85.43 14.70 5.837E+OO 2.220E-01 2.220E-01 127.28 OK 88.47 24.00 6 .119E+OO 2.496E-01 2.497E-01 65.60 OK 193.51 4.41* 7.490E+OO Line Not Found Absent 210.85 2.80 7.213E+OO 2.121E+OO 2 .121E+OO 74.87 OK TH-230 609.32 45.49* 3.566E+OO 8.545E-01 8.545E-01 21. 01 OK 1120. 29 14.92 2.335E+OO 7.203E-01 7.203E-01 54.33 OK 1764.49 15.30 1.634E+OO Line Not Found Absent TH-232 105.21 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 OK 338.32 11. 27 5.379E+OO 2.278E-01 2.278E-01 281.64 OK 835.71 1. 61 2. 872E+OO Line Not Found Absent 911.20 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 OK 968. 97 15.80-2.589E+OO 6.436E-01 6.436E-01 59.83 OK TH-234 63.29 3.70* 3.086E+OO 6.033E-01 6.033E-01 486.00 OK 92.59 4.23 6.599E+OO 2.060E+OO 2.060E+OO 48.52 OK U-234 609.32 45.49* 3.566E+OO 8.545E-01 8.545E-01 21. 01 OK 1120.29 14.92 2.335E+OO 7.203E-01 7.203E-01 54.33 OK 1764.49 15.30 1.634E+OO Line Not Found Absent U-238 63.29 3.70* 3.086E+OO 6.033E-01 6.033E-01 486.00 OK 92.59 4.23 6.599E+OO 2.060E+OO 2.060E+OO 48.52 OK AM-243 43.53 5.90 3.443E-01 Line Not Found Absent 74.66 67.20* 4.756E+OO 2.122E-01 ,2.122E-01 46.14 OK ANH-511 511. 00 100.00* 4.028E+OO 8.422E-02 8.422E-02 83.59 OK Flag: "*" = Keyline Page 4271 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:54:53.45 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l *
  • Acquisition date 3-0CT-2016 07:52:52 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:33:00 Analyst initials: MXRl *
  • Sample ID G405235060 Sample Quantity 1.5227E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM (1.96-sigma) K-40 1.258E+Ol 1.073E+OO AS-73 7.731E+OO 2.158E+Ol CD-109 2.510E+OO 1.614E+OO SN-126 1.619E-01 1.041E-01 BA-137M 8.893E-02 4.144E-02 CS-137 9.395E-02 4.377E-02 CE-139 3.828E-01 2.934E-01 EU-155 2.439E-01 1.674E-01 TM-171 1.821E+Ol 5.082E+Ol TL-208 2.195E-01 8.832E-02 BI-211 9.795E-02 8.334E-01 PB-212 8.109E-01 l.007E-01 BI-214 8.548E-01 1.760E-01 PB-214 1.069E+OO 1.672E-01 RN-222 8.548E-01 l.760E-01 RA-224 9.142E-01 1.020E+OO RA-226 8.548E-01 1.760E-01 AC-228 8.687E-01 2.591E-01 RA-228 8.687E-01 2.591E-01 TH-228 8.109E-01 1.007E-01 TH-229 -3.947E-02 3.454E-01 TH-230 8.545E-01 1.759E-01 TH-232 8.687E-01 2. 591E-01 TH-234 6.033E-01 2.874E+OO U-234 8.545E-01 1. 759E-01 U-238 6.033E-01 2.874E+OO AM-243 2.122E-01 9.595E-02 ANH-511 8.422E-02 6.899E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 4272 of 5809 Key-Line Activity (pCi/GRAM -5.557E+OO 2.268E-02 K.L. Cnt Uncert ( 1. 96-sigma) 8.733E+OO 4.171E-02 MDA (pCi/GRAM 4.220E-01 l.736E+Ol 1.485E+OO 9.638E-02 4.779E-02 5.049E-02 1.495E-01 l.640E-01 4.304E+Ol 4.724E-02 2.654E-01 7.359E-02 1.083E-01 2.692E-01 1.083E-01 7.882E-01 1.083E-01 1.617E-01 1.617E-01 7.359E-02 6.788E-01 1.082E-01 l.617E-01 2.136E+OO l.082E-01 2.136E+OO 7.523E-02 3.998E-02 MDA (pCi/GRAM 1.478E+Ol 7.560E-02 NOT IDENT. NOT IDENT.

NA-24 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF AL-26 -2.989E-04 l.908E-02 4.029E-02 NOT IDENT. SC-46 -7.038E-02 2.922E-01 5.247E-01 FAIL ABUN V-48 O.OOOE+OO 8.240E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 2.845E+02 O.OOOE+OO SHORT HLIF MN-54 l.610E-02 5.573E-02 l.060E-01 NOT IDENT. C0-56 3.776E-01 3.590E-01 7.502E-01 FAIL ABUN MN-56 O.OOOE+OO 9.528E+40 O.OOOE+OO SHORT HLIF C0-57 4.337E-03 3.855E-02 7.303E-02 NOT IDENT. C0-.58 7.600E-02 4.554E-01 S..663E-01 NOT IDENT. FE-59 O.OOOE+OO l.023E+Ol 9.408E+OO FAIL ABUN C0-60 1. 634E-02 2.645E-02 5.680E-02 NOT IDENT. ZN-65 4.146E-02 l.594E-01 2.741E-01 NOT IDENT. GE-68 -4.203E-01 l.888E+OO 3.046E+OO NOT IDENT. AS-74 O.OOOE+OO 3.459E+03 O.OOOE+OO SHORT HLIF SE-75 -4.605E-02 1.588E-01 2.988E-01 NOT IDENT. BR-77 O.OOOE+OO 1.745E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 4.995E+02 O.OOOE+OO SHORT HLIF RB-83 2.200E-01 4.577E-01 9.376E-01 NOT IDENT. KR-85 l.238E+Ol 6.724E+OO 1.359E+Ol NOT IDENT. SR-85 1.198E+OO 6.527E-Ol l.318E+OO NOT IDENT. RB-86 0.000E+OO l.777E+04 0.000E+OO SHORT HLIF Y-88 -4.490E-03 l.644E-01 3.309E-01 NOT IDENT. Y-91 -5.238E+Ol 3.562E+02 6.648E+02 NOT IDENT. NB-94 -2.393E-04 2.378E-02 4.447E-02 NOT IDENT. NB-95 l.615E-01 5.690E-01 1.109E+OO NOT IDENT. NB-95M 9.593E-01 1.887E+OO 3.429E+OO NOT IDENT. ZR-95 8.370E-01 1.007E+OO 2.092E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO l.051E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1. 892E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 3.778E-03 2.789E-02 4.893E-02 NOT IDENT. RH-102 -3.628E-02 4.095E-02 7.046E-02 NOT IDENT. RU-103 -1.015E+00 4.028E+OO 7.599E+00 FAIL ABUN RH-106 -3 .191E-01 3.943E-01 6.886E-01 NOT IDENT. RU-106 -3.191E-01 3.943E-01 6.886E-01 NOT IDENT. AG-108M -2.547E-05 2.128E-02 3.946E-02 NOT IDENT. AG-110M 3.550E-02 7.729E-02 l.529E-01 FAIL ABUN SN-113 -2.955E-05 l.553E-01 2.921E-01 NOT IDENT. CD-115 O.OOOE+OO l.989E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 5.101E+04 O.OOOE+OO SHORT HLIF TE-123M 2.728E-02 l.006E-01 1.880E-01 NOT IDENT. SB-124 2.685E-01 1.046E+OO 2.390E+OO NOT IDENT. SB-125 2.614E-02 8.280E-02 l.580E-01 FAIL ABUN TE-125M -l.277E+02 2.022E+02 3.333E+02 NOT IDENT. I-126 0.000E+OO 5.246E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6.304E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.855E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.065E+09 0.000E+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.094E+25 O.OOOE+OO SHORT HLIF BA-133 7.916E-03 3.483E-02 6.022E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 6.643E-02 6.086E-02 8.178E-02 FAIL ABUN CS-135 2.868E-02 1.188E-01 2.308E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO l.433E+05 O.OOOE+OO SHORT HLIF BA-140 O.OOOE+OO 6.668E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.154E+05 O.OOOE+OO SHORT HLIF CE-141 -1.295E+Ol 1.806E+Ol 3.148E+Ol NOT IDENT. CE-143 0.000E+OO 9.214E+40 O.OOOE+OO SHORT HLIF CE-144 -2.495E-01 2. 813E-01 4.850E-01 NOT IDENT. PM-144 3.621E-02 4.308E-02 8.859E-02 NOT IDENT. PR-144 3.123E+OO 3.726E+OO 7.660E+OO NOT IDENT. PM-146 9. 9'19E-03 3.422E-02 6.507E-02 NOT IDENT. ND-147 O.OOOE+OO l.537E+07 O.OOOE+OO SHORT HLIF PM-147 -7.533E+Ol 6.585E+o2 1.229E+03 NOT IDENT. PM-149 O.OOOE+OO 2.804E+39 O.OOOE+OO SHORT HLIF EU-150 5.816E-03 2.852E-02 3.932E-02 FAIL ABUN EU-152 2.385E-02 8.200E-02 l.428E-01 NOT IDENT. GD-153 0.000E+OO 2.857E-01 2.985E-01 FAIL ABUN EU-154 6 .113E-02 1.034E-01 1. 886E-01 NOT IDENT. TB-160 1. 2 67E-01 1.410E+OO 2.652E+OO FAIL ABUN H0-166M -3.137E-02 4.273E-02 7.382E-02 NOT IDENT. HF-172 -8.909E-02 l.977E-01 3.265E-01 FAIL ABUN LU-172 4.267E-02 6.744E-02 1.248E-01 FAIL ABUN LU-176 -l.803E-04 l.849E-02 3.524E-02 FAIL ABUN Page 4273 of 5809 HF-181 3.068E+OO 3.180E+OO 6.393E+00 NOT IDENT. TA-182 -2.158E-01 7.473E-01 1. 351E+OO FAIL ABUN RE-183 5.465E-01 2.527E+OO 5.193E+OO NOT IDENT. RE-184 5.823E+OO l.670E+Ol 3.349E+Ol NOT IDENT. W-188 9.420E+OO 8.269E+Ol 1. 442E+02 FAIL ABUN IR-192 -8.742E-02 3.319E-01 6.161E-01 FAIL ABUN HG-203 -2.850E-01 l.735E+00 2.937E+OO NOT IDENT. BI-207 l.454E-02 4.325E-02 7.645E-02 FAIL ABUN PB-210 2.770E+OO 4.415E+00 9.309E+OO NOT IDENT. PB-211 l.805E-01 5.147E-01 9.9.13E-01 NOT IDENT. BI-212 O.OOOE+OO 6.855E-01 9.833E-01 FAIL ABUN RN-219 -2.561E-02 2.713E-01 5.031E-01 NOT IDENT. RA-223 l.134E-02 5.329E-01 9.020E-01 FAIL ABUN AC-227 -7.758E-03 l.889E-01 3.623E-01 NOT IDENT. TH-227 -7.758E-03 l.889E-01 3.623E-01 NOT IDENT. PA-231 2.007E-01 3.755E-01 7.107E-01 NOT IDENT. TH-231 l.134E-02 5.329E-01 9.020E-01 FAIL ABUN PA-233 -2.676E-02 4.398E-02 7.919E-02 NOT IDENT. PA-234 -1. 247E-02 2.597E-01 4.351E-01 FAIL ABUN PA-234M -4.999E-01 3.162E+00 5.920E+OO NOT IDENT. U-235 -5.600E-02 l.548E-01 2.781E-01 FAIL ABUN NP-237 -2.676E-02 4.398E-02 7.919E-02 FAIL ABUN NP-238 O.OOOE+OO 2.948E+40 O.OOOE+OO SHORT HLIF NP-239 5.043E-02 l.882E-01 3.640E-01 FAIL ABUN PU-239 3.616E+02 4.747E+02 5 .111E+02 FAIL ABUN AM-241 -3.858E-02 l.363E-01 2.492E-01 NOT IDENT. CM-243 5.940E-03 7.980E-02 l.536E-01 FAIL ABUN BK-247 -l.357E-02' 5.673E-02 l.073E-01 FAIL ABUN CM-247 -2.657E-02 2.618E-02 4.327E-02 FAIL ABUN CF-249 l.658E-03 2.597E-02 4.928E-02 NOT IDENT. CF-251 -4.537E-02 8.860E-02 l.528E-01 NOT IDENT. Page 4274 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:54:51.23 Nuclide Line Activity Report Nuclide Type: . Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Ef f pCi/GRAM pCi7GRAM %Error K-40 1460.82 520 10.66* 1. 911E+OO 1.258E+Ol l.258E+Ol 8.70 AS-73 53.44 18 10.30* 1.379E+OO 6.226E-01 7.731E+OO 284.82 CD-109 88.03 118 3.70* 6 .119E+OO 2. 571E+OO 3.986E+OO 40.27 SN-126 64.28 14 9.60 3.086E+OO 2.325E-01 2.325E-01 486.00 86.94 118 8.90 6 .119E+OO l.069E+OO 1.069E+OO 40.27 87.57 118 37.00* 6 .119E+OO 2.571E-01 2. 571E-01 40.27 BA-137M 661.66 54 89.90* 3.371E+OO 8. 731E-02 8.893E-02 47.55 CS-137 661.66 54 85.10* 3.371E+OO 9.223E-02 9.395E-02 47.55 CE-139 165.86 113 80.00* 7.900E+OO 8.805E-02 3.828E-01 78.21 EU-155 86. 55 118 30.70 6 .119E+OO 3.099E-01 3.482E-01 40.27 105.31 69 21.10* 7.389E+OO 2.170E-01 '2.439E-01 70.02 TM-171 51. 35 18 0.27 1.379E+OO 2.375E+Ol 3.169E+Ol 284.82 52.39 18 0.47* 1.379E+OO 1.364E+Ol 1. 821E+Ol 284.82 66.73 ------0.14 3.622E+OO ------Line Not Found ------TL-208 277.37 50 6.60 6.132E+OO 6.083E-01 6.083E-01 76.34 583.19 139 85.00* 3.673E+00 2*. 195E-01 2.195E-01 41. 05 860.56 31 12.50 2.812E+OO 4.335E-01 4.335E-01 78.30 BI-211 72.87 ------1.23 4.495E+OO ------Line Not Found ------351.06 403 12.92* 5.219E+OO 2.945E+OO 2.945E+OO 15. 96 PB-212 74.82 195 10.28 4.756E+OO 1.970E+OO 1.970E+OO 31. 64 77 .11 252 17.10 5.050E+OO 1.440E+OO 1.440E+OO 25.57 238.63 482 43.60* 6.719E+OO 8.109E-01 8.109E-01 12.67 300.09 ------3.30 5.819E+OO ------Line Not Found ------BI-214 609.32 281 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 1120.29 51 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 1764.49 ------15.30 1.634E+OO ------Line Not Found ------PB-214 74.82 195 5.80 4.756E+OO 3.491E+OO 3.492E+OO 31. 64 77 .11 252 9.70 5.050E+OO 2.539E+OO 2.540E+OO 25.57 87.09 118 3.41 6 .119E+OO 2.790E+OO 2.791E+OO 40.27 242.00 152 7.25 6.669E+OO 1.550E+OO 1. 551E+OO 34.16 295.22 227 18.42 5.877E+00 1.033E+OO 1.033E+OO 24.89 351. 93 403 35.60* 5.219E+OO 1.069E+OO 1.069E+OO 15. 96 RN-222 609.32 281 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 1120.29 51 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 1764.49 ------15.30 l.634E+00 ------Line Not Found ------RA-224 240.99 152 4.10* 6.669E+OO 2. 741E+OO 2. 741E+OO 34.16 RA-226 609.32 281 45.49* 3.566E+OO 8.545E-01 8.548E-01 21. 01 1120.29 51 14.92 2.335E+OO 7.203E-01 7.205E-01 54.33 1764.49 ------15.30 1.634E+OO ------Line Not Found ------AC-228 105.21 69 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 338.32 28 11.27 5.379E+OO 2.278E-01 2.278E-01 281. 64 794.95 26 4.25 2.973E+OO 1.022E+OO 1.022E+OO 93.48 835.71 ------1. 61 2.872E+OO ------Line Not Found ------911.20 123 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 968. 97 53 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 RA-228 105.21 69 1.10 7.389E+OO 4.163E+OO 4.163E+OO 70.02 338.32 28 11. 27 5.379E+OO 2.278E-01 2.278E-01 281.64 Page 4275 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235060 Acquisition date 3-0CT-2016 07:52:52 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 794.95 26 4.25 2.973E+00 1.022E+OO 1.022E+00 93.48 835.71 ------1. 61 2.872E+OO ------Line Not Found ------911.20 123 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 968. 97 53 15.80 2.589E+OO 6.436E-01 6.436E-Ol 59.83 TH-228 74.82 195 10.28 4.756E+OO 1.970E+OO 1.970E+OO 31.64 77 .11 252 17.10 5.050E+OO 1.440E+OO 1.440E+OO 25.57 238.63 482 43.60* 6. 719E+OO 8.109E-01 8.109E-01 12.67 300.09 ------3.30 5.819E+OO ------Line Not Found ------TH-229 85.43 39 14.70 5.837E+OO 2.220E-01 2.220E-01 127.28 88.47 118 24.00 6 .119E+OO 3. 964E-01 3. 965E-01 40.27 193.51 ------4.41* 7.490E+OO ------Line Not Found ------210.85 87 2.80 7.213E+OO 2 .121E+OO 2 .121E+OO 74.87 TH-230 609.32 281 45.49* 3.566E+OO 8.545E-01 8.545E-01 21. 01 1120.29 51 14.92 2.335E+OO 7.203E-01 7.203E-01 54.33 1764.49 ------15.30 1.634E+OO ------Line Not Found ------TH-232 105.21 69 1.10 7.389E+OO 4.163E+OO 4.163E+00 70.02 338.32 28 11. 27 5.379E+OO 2.278E-01 2.278E-01 281. 64 835. 71 ------1. 61 2. 872E+OO ------Line Not Found ------911. 20 123 25.80* 2.703E+OO 8.687E-01 8.687E-01 30.43 968. 97 53 15.80 2.589E+OO 6.436E-01 6.436E-01 59.83 TH-234 63.29 14 3.70* 3.086E+OO 6.033E-01 6.033E-01 486.00 92.59 117 4.23 6.599E+OO 2.060E+OO 2.060E+OO 48.52 U-234 609.32 281 45.49* 3.566E+OO 8.545E-01 8.545E-01 21. 01 1120. 29 51 14.92 2.335E+OO 7.203E-01 7.203E-01 54.33 1764.49 ------15.30 1.634E+OO ------Line Not Found ------U-238 63.29 14 3.70* 3.086E+OO 6.033E-01 6.033E-01 486.00 92.59 117 4.23 6.599E+OO 2.060E+OO 2.060E+OO 48.52 AM-243 43.53 ------5.90 3.443E-01 ------Line Not Found ------74.66 195 67.20* 4.756E+00 3. 013E-01 3.014E-01 31. 64 ANH-511 511. 00 69 100.00* 4.028E+OO 8.422E-02 8.422E-02 83.59 Flag: "*" Key line Page 4276 of 5809 Summary of Nuclide Activity Sample ID : G405235060 Acquisition date Page : 3 3-0CT-2016 07:52:52 Total number of lines in spectrum 42 Number of unidentified lines 6 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 CE-139 EU-155 TM-171 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 80.30D 461.40D 2.30E+05Y 30.08Y 30.08Y 137.64D 4.75Y 1.92Y 1. 41E+10Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+10Y 1.41E+10Y 7340.00Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 12.4 1. 55 1. 00 1. 02 1. 02 4.35 1.12 1. 33 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.258E+Ol 6.226E-01 2.571E+OO 2.571E-01 8.731E-02 9.223E-02 8.805E-02 2.170E-01 1. 364E+Ol 2.195E-01 2.945E+OO 8.109E-01 8.545E-01 1.069E+OO 8.545E-01 2.741E+OO 8.545E-01 8.687E-01 8.687E-01 8.109E-01 3.964E-01 8.545E-01 8.687E-01 6.033E-01 8.545E-01 6.033E-01 3.013E-01 8.422E-02 4.762E+Ol 4.762E+Ol Decay Corr pCi/GRAM 1.258E+Ol 7.731E+OO 3.986E+OO 2.571E-01 8.893E-02 9.395E-02 3.828E-01 2.439E-01 1.821E+Ol 2.195E-01 2.945E+OO 8.109E-01 8.548E-01 1.069E+OO 8.548E-01 2. 741E+OO 8.548E-01 8.687E-01 8.687E-01 8.109E-01 3. 965E-01 8.545E-01 8.687E-01 6.033E-01 8.545E-01 6.033E-01 3.014E-01 8.422E-02 6.103E+Ol 6.103E+Ol 85.71%

  • Decay Corr 2-Sigma Error 0.109E+01 22.02E+OO l.605E+OO l.036E-01 4.228E-02 4.467E-02 2.994E-01 1.708E-01 5.186E+Ol 0. 901E-01 0.470E+OO l.028E-01 1.796E-01 0 .171E+OO 1.796E-01 0.936E+OO 1. 796E-01 2.644E-01 2.644E-01 1.028E-01 1.597E-01 1. 795E-01 2.644E-01 29.32E-01 1. 795E-01 29.32E-01 0.954E-01 7.039E-02 "M" Manually accepted 2-Sigma %Error 8.70 284.82 40.27 40.27 47.55 47.55 78.21 70.02 284.82 41.05 15. 96 12.67 21. 01 15. 96 21. 01 34.16 21. 01 30.43 30.43 12. 67 40.27 21. 01 30.43 486.00 21. 01 486.00 31. 64 83.59 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4277 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235060 Acquisition date : 3-0CT-2016 07:52:52 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 89.95 94 151 1.16 180.67 172 21 2.05E-02 54.1 6.38E+OO T 0 98.34 104 127 2.24 197.43 193 9 2.30E-02 49.6 7.00E+OO T 3 107.63 40 80 1. 04 216.00 205 15 8.93E-03 90.0 7.50E+OO T 0 12 9. 2 9 37 152 1.11 259.27 255 8 8. 40E-03. **** 8.04E+OO T 0. 328.12 59 108 6.58 656.64 648 16 l.45E-02 89.4 5.48E+OO T 0 463.23 29 48 1. 48 926.66 921 10 7.47E-03 **** 4.31E+OO T 0 728. 51 52 35 0.90 1456.88 1449 14 l.38E-02 57.8 3.16E+OO T 0 770.32 54 57 4.57 1540.47 1527 22 1. 45E-02 77.7 3.04E+00 0 936.58 35 60 2.90 1872.80 1862 26 9.49E-03 **** 2.65E+OO T 0 1072. 48 7 31 0.49 2144.48 2134 16 1. 96E-03 **** 2.41E+OO 0 1100. 48 34 28 8.92 2200.47 2187 23 9.46E-03 88.5 2.37E+OO T 0 1238.36 51 8 1. 96 2476.12 2467 17 1. 43E-02 38.1 2.17E+OO T 0 1281.49 26 16 8.79 2562.33 2551 22 7.34E-03 87.6 2.12E+OO 0 1416 .11 14 7 1. 58 2831. 50 2825 14 3.89E-03 96. 4 1. 96E+OO 0 1624.62 7 6 1. 34 3248.40 3240 13 2.08E-03 **** 1. 75E+OO 0 1766.95 24 20 1. 91 3533.01 3522 16 7.02E-03 92.4 1.63E+OO Flags: "T" = Tentatively associated Page 4278 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:55:05.22 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l *
  • Acquisition date 3-0CT-2016 07:52:52 Sensitivity 3.000 *
  • Detector ID GAM18 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:33:00 Nuclide Library : SOLID *
  • Sample ID G405235060 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.5227E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 CD-109 SN-126 BA-137M CS-137 CE-139 EU-155 TM-171 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 1.781E-01 8.124E+00 6.940E-01 4.505E-02 2.160E-02 2.282E-02 6.990E-02 7.686E-02 2.006E+Ol 2.143E-02 1.224E-01 3. 441E-02 4.992E-02 1.309E-01 4.992E-02 3.686E-01 4.992E-02 7 .114E-02 7 .114E-02 3. 441E-02 3.181E-01 4.990E-02 7 .114E-02 1.005E+OO 4.990E-02 1.005E+OO 3.536E-02 1. 828E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4279 of 5809 Le (pCi/GRAM 6.692E+OO 3.389E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 "' FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-12 6 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M HF-172 LU-172 LU-176 HF-181 Page 4280 of 5809 1. 596E-02 2.348E-01 O.OOOE+OO O.OOOE+OO 4.847E-02 3.423E-01 O.OOOE+OO 3.431E-02 3.927E-01 4.229E+OO 2.476E-02 l.240E-01 1.339E+OO O.OOOE+OO l.392E-01 O.OOOE+OO O.OOOE+OO 4.287E-01 6.379E+OO 6.189E-01 O.OOOE+OO l.370E-01 2.953E+02 2.012E-02 5.018E-01 1.617E+OO 9.502E-01 0.0'00E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.292E-02 3 .115E-02 3.481E+OO 3.105E-01 3.lOSE-01 1.804E-02 6.883E-02 l.333E-01 O.OOOE+OO O.OOOE+OO 8.827E-02 9.563E-01 7.281E-02 l.548E+02 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.784E-02 O.OOOE+OO 3.739E-02 1.085E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 1.483E+Ol O.OOOE+OO 2.264E-01 4.062E-02 3.512E+00 2.986E-02 O.OOOE+OO 5.754E+02 O.OOOE+OO 1.831E-02 6.625E-02 1.410E-01 8.464E-02 1.192E+00 3.298E-02 1.527E-01 5.635E-02 1.632E-02 2.956E+OO NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4281 of 5809 6.088E-01 2.429E+00 1. 476E+Ol 6.681E+Ol 2.849E-01 l.361E+00 3.443E-02 4.381E+OO 4. 571E-01 4. 594E-01, 2.295E-01 4.195E-01 l.698E-01 1.698E-01 3.330E-01 4.195E-01 3.641E-02 1. 961E-01 2.642E+OO 1. 311E-01 3.641E-02 O.OOOE+OO 1.705E-01 2.416E+02 l.166E-01 7. 201E-02 4.994E-02 l.962E-02 2.249E-02 7 .114E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:55:10.62 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235060.CNF;l * *Acquisition date 3-0CT-2016 07:52:52 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:33:00 Nuclide Library : SOLID *
  • Sample ID G405235060 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity 1.5227E+02 GRAM *
  • Quantity Err(%) 1.3135E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.258E+Ol 1.258E+OO AS-73 7. 731E+OO 2.164E+Ol CD-109 2.510E+OO 1.637E+OO SN-126 1.619E-01 1.053E-01 BA-137M 8.893E-02 4.161E-02 CS-137 9.395E-02 4. 396E-02 CE-139 3.828E-01 3.033E-01 EU-155 2.439E-01 1.683E-01 TM-171 1.821E+Ol 5.084E+Ol TL-208 2.195E-01 8.882E-02 BI-211 9.795E-02 8.513E-01 PB-212 8.109E-01 1.095E-01 BI-214 8.548E-01 1.798E-01 PB-214 1. 069E+OO 1.730E-01 RN-222 8.548E-01 1.798E-01 RA-224 9.142E-01 1.028E+OO RA-226 8.548E-01 1.798E-01 AC-228 8.687E-01 2.629E-01 RA-228 8.687E-01 2.629E-01 TH-228 8.109E-01 1.095E-01 TH-229 -3.947E-02 3.454E-01 TH-230 8.545E-01 1.797E-01 TH-232 8.687E-01 2.629E-01 TH-234 6.033E-01 2.877E+00 U-234 8.545E-01 1.797E-01. U-238 6.033E-01 2.877E+OO AM-243 2.122E-01 9.750E-02 ANH-511 8.422E-02 6.907E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 Page 4282 of 5809 Key-Line Activity (pCi/GRAM -5.557E+OO 2.268E-02 K.L Act error ( 1. 96-sigma) 8.736E+OO 4.171E-02 TPU (1. 96-sigma) 1.258E+OO 2.164E+Ol 1.637E+OO 1.053E-01 4.161E-02 4.396E-02 3.033E-01 1.683E-01 5.084E+01 8.882E-02 8.513E-01 1.095E-01 1.798E-01 1.730E-01 1. 798E-01 1.028E+OO 1. 798E-01 2.629E-01 2.629E-01 1.095E-01 3.454E-01 1. 797E-01 2.629E-01 2.877E+OO 1. 797E-01 2.877E+OO 9.750E-02 6.907E-02 TPU ( 1. 96-sigma) 9.088E+OO NOT IDENT. 4.295E-02 NOT IDENT.

NA-24 1. OOOE+41 7.562E+41 0.000E+OO SHORT HLIF AL-26 -2.989E-04 1. 908E-02 l.908E-02 NOT IDENT. SC-46 -7.038E-02 2.922E-01 2.939E-01 FAIL ABUN V-48 6.086E+03 8.244E+03 8.688E+03 SHORT HLIF CR-51 7.805E+01 2.845E+02 2.867E+02 SHORT HLIF MN-54 1.610E-02 5.573E-02 5.620E-02 NOT IDENT. C0-56 3.776E-01 3.593E-01 3.976E-01 FAIL ABUN MN-56 l.OOOE+41 9.537E+40 O.OOOE+OO SHORT HLIF C0-57 4.337E-03 3.855E-02 3.860E-02 NOT IDENT. C0-58

  • 7.600E-02 4.554E-01 4.5Ei7E-01 NOT IDENT. FE-59 1.180E+Ol l.027E+Ol 1.156E+Ol FAIL ABUN C0-60 l.634E-02 2.646E-02 2.747E-02 NOT IDENT. ZN-65 4.146E-02 1.594E-01 1.605E-01 NOT IDENT. GE-68 -4.203E-01 l.888E+OO l.897E+OO NOT IDENT. AS-74 -2.237E+03 3.464E+03 3.608E+03 SHORT HLIF SE-75 -4.605E-02 1.588E-01 l.601E-01 NOT IDENT. BR-77 1. 405E+37 1.184E+38 O.OOOE+OO SHORT HLIF SR-82 1.925E+02 4. 996E+02 5.070E+02 SHORT HLIF RB-83 2.200E-01 4.587E-01 4.693E-01 NOT IDENT. KR-85 1.238E+Ol 6.743E+OO 8.753E+OO NOT IDENT. SR-85 l.198E+00 6.545E-01 8.485E-01 NOT IDENT. RB-86 -4.772E+03 l.778E+04 1. 791E+04 SHORT HLIF Y-88 -4.490E-03 1.644E-01 l.644E-01 NOT IDENT. Y-91 -5.238E+Ol 3.562E+02 3.569E+02 NOT IDENT. NB-94 -2.393E-04 2.378E-02 2.378E-02 NOT IDENT. NB-95 1.615E-01 5.690E-01 5.737E-01 NOT IDENT. NB-95M 9.593E-01 1. 889E+OO 1.938E+OO NOT IDENT. ZR-95 8.370E-01 l.007E+OO 1. 076E+OO NOT IDENT. NB-97 -l.000E+41 1. 996E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 l.052E+41 O.OOOE+OO SHORT HLIF M0-99 -3.870E+30 1. 892E+31 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 3. 611E+42 O.OOOE+OO SHORT HLIF RH-101 3.778E-03 2.790E-02 2.795E-02 NOT IDENT. RH-102 -3.628E-02 4.105E-02 4.419E-02 NOT IDENT. RU-103 -l.015E+OO 4.028E+OO 4.054E+OO FAIL ABUN RH-106 -3.191E-01 3.948E-01 4.202E-01 NOT IDENT. RU-106 -3.191E-01 3.948E-01 4.202E-01 NOT IDENT. AG-108M -2.547E-05 2.128E-02 2.128E-02 NOT IDENT. AG-llOM 3.550E-02 7.731E-02 7.895E-02 FAIL ABUN SN-113 -2.955E-05 l.553E-01 l.553E-01 NOT IDENT. CD-115 2.784E+37 1. 989E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 1.238E+04 5.103E+04 5 .133E+04 SHORT HLIF TE-123M 2. 728E-02 l.006E-01 1.013E-01 NOT IDENT. SB-124 2.685E-01 l.046E+OO 1.053E+OO NOT IDENT. SB-125 2.614E-02 8. 281E-02 8.364E-02 FAIL ABUN TE-125M -1.277E+02 2.023E+02 2.103E+02 NOT IDENT. I-126 l.801E+05 5.252E+05 5.314E+05 SHORT HLIF SB-126 2.980E+05 6.328E+05 6.469E+05 SHORT HLIF SB-127 -3.301E+21 5.862E+21 O.OOOE+OO SHORT HLIF I-131 7.324E+08 2.066E+09 2.092E+09 SHORT HLIF I-132 1.000E+41 1.998E+42 O.OOOE+OO SHORT HLIF TE-132 3.772E+24 5.096E+25 O.OOOE+OO SHORT HLIF BA-133 7.916E-03 3.483E-02 3. 501E-02 FAIL ABUN I-133 -l.OOOE+41 3.059E+41 O.OOOE+OO SHORT HLIF CS-134 6.643E-02 6.092E-02 6.788E-02 FAIL ABUN CS-135 2.868E-02 l.188E-01 1.195E-01 NOT IDENT. I-135 -l.000E+41 l.825E+42 O.OOOE+OO SHORT HLIF CS-136 -3.901E+04 1.433E+05 l.444E+05 SHORT HLIF BA-140 7.617E+05 6.676E+05 7.507E+05 SHORT HLIF LA-140 -1.309E+05 2.155E+05 2.235E+05 SHORT HLIF CE-141 -1.295E+Ol l.807E+Ol 1.899E+Ol NOT IDENT. CE-143 1.000E+41 9.268E+40 O.OOOE+OO SHORT HLIF CE-144 -2.495E-01 2.817E-01 3.033E-01 NOT IDENT. PM-144 3. 621E-02 4.314E-02 4.612E-02 NOT IDENT. PR-144 3.123E+OO 3. 728E+OO 3.985E+OO NOT IDENT. PM-146 9. 919E-'03 3.423E-02 3.452E-02 NOT IDENT. ND-147 7.832E+05 l.537E+07 l.538E+07 SHORT HLIF PM-147 -7.533E+Ol 6.585E+02 6.594E+02 NOT IDENT. PM-149 1. 084E+39 2.813E+39 O.OOOE+OO SHORT HLIF EU-150 5.816E-03 2.852E-02 2.864E-02 FAIL ABUN EU-152 2.385E-02 8.201E-02 8. 271E-02 NOT IDENT. GD-153 5.877E-01 2.877E-01 3. 911E-01 FAIL ABUN EU-154 6.113E-02 1.034E-01 1.070E-01 NOT IDENT. TB-160 1. 2 67E-01 1.410E+OO 1. 411E+OO FAIL ABUN H0-166M -3.137E-02 4.277E-02 4.505E-02 NOT IDENT. HF-172 -8.909E-02 1.982E-01 2.023E-01 FAIL ABUN LU-172 4.267E-02 6.757E-02 7.026E-02 FAIL ABUN LU-176 -1.803E-04 1.849E-02 1.849E-02 FAIL ABUN -Page 4283 of 5809 HF-181 3.068E+OO 3.183E+OO 3.471E+OO NOT IDENT. TA-182 -2.158E-01 7.474E-01 7.537E-01 FAIL ABUN RE-183 5.465E-01 2.528E+OO 2.540E+OO NOT IDENT. RE-184 5.823E+OO 1. 67 6E+Ol 1. 696E+Ol NOT IDENT. W-188 9.420E+OO 8.270E+Ol 8.281E+Ol FAIL ABUN IR-192 -8.742E-02 3.320E-01 3.343E-01 FAIL ABUN HG-203 -2.850E-01 1. 735E+OO 1.739E+OO NOT IDENT. BI-207 l.454E-02 4.325E-02 4.375E-02 FAIL ABUN PB-210 2.770E+OO 4.423E+OO 4. 596E+OO NOT IDENT. PB-211 1.805E-01 5.148E-01 5.212E-01 NOT IDENT. BI-212 1.210E+OO 6.882E-01 8.781E-01 FAIL ABUN RN-219 -2.561E-02 2. 714E-01 2.716E-01 NOT IDENT. RA-223 l.134E-02 5.329E-01 5.330E-01 FAIL ABUN AC-227 -7.758E-03 l.889E-01 1.889E-01 NOT IDENT. TH-227 -7.758E-03 1.889E-01 1. 889E-01 NOT IDENT. PA-231 2.007E-01 3.780E-01 3.886E-01 NOT IDENT. TH-231 1.134E-02 5.329E-01 5.330E-01 FAIL ABUN PA-233 -2.676E-02 4.400E-02 4.562E-02 NOT IDENT. PA-234 -1.247E-02 2.601E-01 2.602E-01 FAIL ABUN PA-234M -4.999E-01 3.162E+OO 3.170E+OO NOT IDENT. U-235 -5.600E-02 1.549E-01 1.569E-01 FAIL ABUN NP-237 -2.676E-02 4.400E-02 4.562E-02 FAIL ABUN NP-238 -7.812E+38 2.948E+40 O.OOOE+OO SHORT HLIF NP-239 5.043E-02 l.882E-01 1.896E-01 FAIL ABUN PU-239 3.616E+02 4.750E+02 5.022E+02 FAIL ABUN AM-241 -3.858E-02 1.364E-01 1. 37 5E-01 NOT IDENT. CM-243 5.940E-03 7.980E-02 7.984E-02 FAIL ABUN BK-247 -l.357E-02 5.679E-02 5.712E-02 FAIL ABUN CM-247 -2.657E-02 2.656E-02 2.914E-02 FAIL ABUN CF-249 1.658E-03 2.597E-02 2.598E-02 NOT IDENT. CF-251 -4.537E-02 8.874E-02 9.107E-02 NOT IDENT. Page 4284 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 65. 8718 87.09 68.5842 136.47 72.9871 45.60 66.6366 87.57 68.6937 140.51 0.0000 46.54 63.6707 88.03 68.7978 143.76 90.1889 49. 72 0.0000 88.34 68.8683 144.24 82.2854 51. 35 62.7398 88.47 68.8977 145.44 98.5465 51. 87 62.9030 89.96 69.2342 152.43 86.0864 52.39 63.0653 1093.63 69.3869 153.25 0.0000 52.97 64.9547 91.11 0.0000 323.87 60. 7209 53.44 70.8146 92.59 69. 8211 156.02 0.0000 54.07 65.3026 93.35 69.9888 158.56 0.0000 57.36 0.0000 94.56 70.2553 159.00 71.9414 57.53 61.1352 94.65 70.2750 162.33 64.9100 57.98 65.6367 94.67 70.2793 162.66 0.0000 59.27 70.4227 94.87 62.2862 163.33 69.0060 59.32 70.4385 97.43 49.9532 165.86 69.3538 59.54 77.5589 98.43 50.1049 176.31 75.6458 60.96 70.9540 98.44 50.1064 176.60 0.0000 61.17 71.0193 99.53 58.4234 177.52 73.3722 62.93 84.9819 100 .11 51.0387 181.07 0.0000 63.29 85.1129 102.03 51.3298 181. 52 81. 3086 63.58 85.2182 103.18 74.1632 184.41 146.1388 64.28 85.1714 103.37 74.2044 143.76 78.2078 66.73 93.3158 105.21 74.5994 193.51 77.1954 67.24 96. 5461 105.31 74.6208 197.03 85.2640 125.81 85.7698 106.12 74.7938 198.01 85.4068 67.75 85.7942 106.47 74.8680 201.83 84.2584 69.67 72. 6618 109.28 72. 6664 203.43 76.8036 70.83 89.9334 111. 00 80.0327 205.31 71. 9081 72.81 76.9702 111. 76 0.0000 210.85 70.8349 72.87 76.9879 114. 06 87.0718 215.65 69.9893 74.66 81. 5758 116. 30 0.0000 222 .11 72 .1095 74.82 81.6249 116.74 67.3754 227.09 70.0042 74.97 81.6707 119.76 74.3754 227.38 62.0561 77.11 82.3205 121.12 75.7176 228.16 0.0000 78.74 90.1071 121. 22 75.7368 228.18 66.5695 79.69 85.3210 121.78 82.3463 116.74 66.5695 80.12 80.3503 122.06 78.0677 235.69 76.7451 80.19 0.0000 122.92 57.5919 235. 96 79.4694 80.57 78.5629 123.07 64.1360 238.63 69.4139 81. 00 89.5572 265.00 71. 8557 238.98 0.0000 81. 07 89.5793 125.81 81.7248 240.99 69.6520 81. 75 73.1176 127.23 70.2952 242.00 69.7538 83.79 82.6797 127.91 76.2811 244.70 51. 8366 84.00 82.7389 129.30 76.1710 252.40 0.0000 85.43 70.1516 131.20 63.5832 252.80 59.7890 86.55 68.4603 133. 02 79.0820 254.15 0.0000 86.79 68.5148 133.52 88.0975 256.23 74.8602 86.94 68.5495 136.00 69.5428 260.90 0.0000 Page 4285 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 69.1763 355.39 0.0000 584.27 32.0203 264.80 69.1883 .356.01 45.2559 595.83 0.0000 265.00 66.4007 364.49 0.0000 427.87 57 .1198 268.22 75.1383 366.42 0.0000 602.52 0.0000 269.46 79.9659 372.51 40.2010 604.72 48.8719 270.03 75.3174 375.05. 44.5447 607.14 58.1281 271.23 74.4932 377.52 48.9059 609.32 46.9125 273.65 0.0000 356.01 31.0231 610.33 46.9424 276.40 56.9580 388.16 35.4492 614.28 41.4914 277.37 57.0288 388.63 0.0000 618.01 32.0913 277.60 51.3413 391. 69 36.6466 620.36 34. 7102 278.00 51.3677 264.66 35.8708 621. 93 41.5001 279.20 57.1619 401. 81 38.0854 630.19 0.0000 279.54 57.1875 402.40 50.0823 631.29 32.0372 279.70 52.9086 404.85 40.3754 633.25 32.0765 280.46 52. 9605 410.95 47.1861 634.78 0.0000 283*. 69 56.5297 413. 71 46.2050 635.95 25.3145 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 51. 8511 423. 72 0.0000 645.85 23.5100 285.90 0.0000 427.09 36.7410 657.76 28.4168 287.50 63.5387 427.87 40.1089 657.90 0.0000 290.67 50.7413 433.94 38.0826 661. 66 29.6704 293.27 0.0000 439.40 55.1429 664.57 0.0000 351. 93 56.3704 453.88 33.0392 '666.33 0.0000 295. 96 56.4211 463.37 32.1517 666.50 0.0000 879.38 73.1888 468.07 34.5807 667.71 0.0000 299.98 58.6499 473.00 0.0000 677.62 25.9579 300.09 46.9258 475.06 37.0957 685.70 0.0000 300.13 46.9287 476.78 32.5032 695.00 0.0000 301.36 61.0975 477.60 41.8176 696. 49 27.2530 302.85 72.5833 482.18 32.6433 696.51 27.2.530 256.23 59.9501 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 33.3243 306.78 53.2134 497.08 38.0390 697.49 28.2786 308.46 53.3177 505.52 31. 3409 702.65 25.3227 311. 90 55.5146 507.63 0.0000 706.68 27. 4112 316.51 55.8109 511. 00 38.4452 711. 68 34.6143 319.41 0.0000 514.00 37.2772 720.70 0.0000 320.08 0.0000 514.00 37.2772 721. 93 0.0000 321. 04 61.3083 520.40 30. 6133 722.78 40.9753 323.87 58.7904 520.69 0.0000 722. 91 40.9778 325.23 56.3634 522.65 0.0000 723. 31 40.9875 328.76 0.0000 527.90 0.0000 724 .19 34.4459 333.37 51.7958 528.26 32.6019 727. 33 24.6467 333.97 54.8789 529.59 37.1663 733.00 21. 4271 334.37 61.0034 529.87 0.0000 735.93 23.7314 338.28 63.3043 531. 02 0.0000 333.97 23.7510 338.32 63.3081 537.26 0.0000 739.50 0.0000 311. 90 63.4556 546.56 0.0000 747.24 30.1054 340.48 63.4556 552.55 39.6249 748.06 28.0415 340.55 0.0000 563.25 34.3510 752.31 29.1467 344.28 49.3262 569.33 39.1571 753.82 0.0000 345.93 55.5897 946.00 37.2961 756.73 20.8679 351.06 47.6106 569.70 36.3685 756.80 19.8251 351.93 47.6546 583.19 31. 9974 884.68 23.4609 Page 4286 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 26.2100 1274.44 24.2709 1620.50 11. 452 6 766.42 26.2184 1001.03 22.4479 1621. 92 8.1832 766.84 26.2245 1002.74 21.5277 1678.03 0.0000 772.60 0.0000 1004.73 21. 5457 1690.97 3.8879 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0. OiOOO 1025.87 0.0000 1764..49 9.8991 778.90 24.2782 1028.54 0.0000 1063.66 3.3987 783.70 0.0000 1037.84 24.6835 1771.35 6.7994 785.37 22.2407 1038.76 0.0000 1791.20 0.0000 7 92. 07 25.5051 631.29 21. 9118 1808.65 5.0024 794.95 17.0283 1048.07 0.0000 1810.72 0.0000 795.86 17.0366 1049.04 15.2578 1836.06 8.0563 810.06 32.1725 1050.41 16.2197 810.29 30. 0311 1063.66 22.3786 344.28 30.0328 1077.00 0.0000 810.76 28.9652 1077.34 20.8901 815.77 0.0000 1085.87 15.4773 1048.07 0.0000 1093.63 19.4043 832.01 32.5223 1099.45 21. 3909 834.85 33.6527 1112. 07 23.4469 835.71 42.3551 1112. 84 30.2946 836.80 0.0000 1115. 54 26.0859 846.75 0.0000 1120.29 35.9308 846.77 20.7447 1120. 55 29.4009 856.80 0.0000 1221.41 29.4097 860.56 26.3760 1129. 67 17.7003 871.09 29.8205 1131. 51 0.0000 873.19 24.3220 1147.95 0.0000 875.33 0.0000 1173.23 16.9830 879.38 25.5009 1177.95 26.0178 880.51 25.5142 1189.05 32.1469 883.24 25.5465 1204.77 23.2336 884.68 21.1176 1221. 41 32.5109 889.28 27.8450 1231. 02 27.1810 894.76 24.5647 1235.36 0.0000 898.04 21.2469 1238.28 30.6548 900.72 27.9907 1260.41 0.0000 903.28 14. 5718 1271. 87 16.2383 911.20 17.9985 1274.44 17.2371 912.08 18.9062 1274.54 17.2380 923.98 0.0000 1291.59 17.3348 926.50 16.1081 1298.22 0.0000 929 .11 19.6545 1312 .11 0.0000 937.49 27.3142 1332.49 9.4843 944 .13 0.0000 1362.66 0.0000 946.00 28.9384 1365.19 14.9058 949.00 25.6211 1368.63 0.0000 667.71 0.0000 1384.29 22.4899 962. 31 33.3604 1408.01 13.4833 964.08 26.0942 1457.56 0.0000 966 .17 38.4084 1460.82 9.8609 911.20 35.9931 1489.16 6.4437 968. 97 35.9931 1505.03 15.7203 983.53 0.0000 1584.12 11. 3418 984.45 0.0000 1596.21 0.0000 Page 4287 of 5809 __ J VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:55:45.11 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621361.CNF;l DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM24.CNF;330 Background date : Z-OCT-2016 11:01:18. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 07:53:26. Sample ID G1203621361 Sample quantity : 1.81483E+02 GRAM Detector name : GAM24 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.55 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 46.60* 14 31 0.91 93. 26 89 8 3.93E-03 81. 4 2 3 63.13* 4 36 1. 35 126.33 122 31 1. 24E-03261. 2 3.68E+00 3 3 66.47* 7 27 1. 02 133. 00 122 31 1.89E-03132.6 4 3 73.06 12 36 1. 38 146.17 122 31 3.25E-03 96.2 5 3 75.07* 15 23 1.14 150.21 122 31 4.14E-03 59.1 6 0 84.41* 22 47 0.64 168.88 164 10 6.00E-03 65.9 7 0 181.10 10 12 1.19 362.32 361 4 2.83E-03 59.7 8 1 191.50 19 27 1. 33 383.12 366 21 5.33E-03 47.5 4.49E+OO 9 0 211. 96 16 32 1. 39 424.05 418 9 4.32E-03 73.1 10 0 306.90 18 43 3.21 613.97 605 17 4.86E-03 88.6 11 0 331.10 25 17 0.95 662.39 657 11 7.03E-03 38.5 12 0 337.70 29 8 4.44 675.60 668 15 7.92E-03 28.1 13 0 409.56 10 12 1. 75 819.37 813 8 2. 71E-03 69.4 14 0 569.81 18 3 1. 56 1139.97 1135 10 5.13E-03 28.3 15 0 641.91 7 10 0.86 1284.22 1277 9 2.03E-03 89.2 16 0 781.57 9 2 1. 41 1563.65 1558 9 2.40E-03 46.4 17 0 1294.14 6 0 0. 96 2589.33 2586 6 1.67E-03 40.8 Flag: "*" = Peak area was modified by background subtraction Page 4288 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 08:55:47 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type : Abundance limit Interference Report DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621361.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621361 SOLID GAMMA24 0 01:00:00.00 1. 50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry : Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 07:53:26 181.48 GRAM CAN 0 01:00:01.55 10.00 0.00 % Peak Energy 0.0% No interference correction performed Page 4289 of 5809 Nuclide Line Activity Report Sample ID : G1203621361 Nuclide Type: Nuclide PB-210 AM-243 Flag: "*" Page 4290 of 5809 Energy 46.54 43.53 74.66 Key line Area 22 22 %Abn 4.25* 5.90 67.20* Acquisition date Page : 2 3-0CT-2016 07:53:26 %Eff 1.694E+OO 6.751E+OO Uncorrected Decay Corr pCi/GRAM pCi7GRAM 8.655E-01 8.671E-01 ------Line Not Found l.985E-02 1.985E-02 2-Sigma %Error 162.73 118 .19 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:55:49.37 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621361.CNF;l *
  • Acquisition date 3-0CT-2016 07:53:26 Sensitivity : 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.55 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
  • Sample ID G1203621361 Sample Quantity 1.8148E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 * *Wet wt corr : 1.00000 Dry Weight : 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;?
  • Combine.d Ac ti vi ty-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide PB-210 AM-243 Activity (pCi/GRAM 8.671E-01 l.985E-02 Cnt uncert ( 1. 96-sigma) 1.383E+OO 2.300E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 Page 4291 of 5809 Key-Line Activity (pCi/GRAM 5.083E-02 8.425E-04 O.OOOE+OO -1.587E-02 -l.089E-01 -1.338E-02 -2.147E-02 5.287E-02 -1.049E-02 1.008E-02 0.000E+OO -6.419E-03 7.859E-03 -l.580E-02 l.433E-02 8.535E-03 2.552E-01 -4.145E-02 1.504E-03 1. 002E-02 -2.546E+00 2.193E-02 7.944E-03 -1.077E+Ol -6.lOOE-02 l.950E-01 3.774E-03 -1.230E+00 K.L. Cnt Uncert ( 1. 96-sigma) l.425E-01 1. 088E-02 1.866E+08 l.555E-02 l.708E-01 1. 7 42E-02 3. 061E-02 1.805E-01 l.623E-02 2.022E-02 l.528E+41 8.602E-03 1.802E-02 2.430E-02 l.469E-02 3.984E-02 4.443E-01 1.536E-01 5. 796E-02 l.998E-02 2.272E+Ol 1.853E-01 2.447E-02 5.521E+OO 3.123E-02 3.453E-01 1. 971E-02 7 .191E+OO MDA (pCi/GRAM 1.139E+OO 2.924E-02 MDA (pCi/GRAM 3.198E-01 2. 720E-02 O.OOOE+OO l.019E-02 3.500E-01 3. OOlE-02 5.669E-02 3. 960E-01 2.783E-02 4. 496E-02 O.OOOE+OO l.555E-02 4.075E-02 4.506E-02 4.094E-02 8.774E-02 1.130E+OO 3.019E-01 l.188E-01 4.448E-02 4.783E+Ol 3.552E-01 5.750E-02 8.373E+OO 4.735E-02 8.775E-01 4.743E-02 1.541E+Ol NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

NB-94 4.237E-03 1. 744E-02 3.634E-02 NOT IDENT. NB-95 -5.581E-03 l.674E-02 3.215E-02 NOT IDENT. NB-95M -l.053E-02 4.315E-02 9.025E-02 NOT IDENT. ZR-95 4.166E-03 3.394E-02 7.166E-02 NOT IDENT. NB-97 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 5.550E+08 O.OOOE+OO SHORT HLIF M0-99 -7.767E+OO 2.491E+Ol 4.798E+Ol FAIL ABUN TC-99M O.OOOE+OO 3.637E+23 O.OOOE+OO SHORT HLIF RH-101 1.476E-03 l.077E-02 2.225E-02 NOT IDENT. RH-102 5.533E-03. 2.142E-02 4.788E-02 NOT IDENT. RU-103 -1. 478E-02 1.940E-02 3.474E-02 NOT IDENT. RH-106 3.409E-02 1.318E-01 2.906E-01 NOT IDENT. RU-106 3.409E-02 1.318E-01 2.906E-01 NOT IDENT. AG-108M 6.198E-03 1. 372E-02 3.041E-02 NOT IDENT. CD-109 l.316E-03 2.225E-01 4.290E-01 NOT IDENT. AG-110M -3. 511E-03 2. 331E-02 4.581E-02 NOT IDENT. SN-113 9.437E-03 l.982E-02 4.449E-02 NOT IDENT. CD-115 1.772E+Ol 4.154E+Ol 9.000E+Ol NOT IDENT. SN-117M -4.194E-03 2.848E-02 5.529E-02 NOT IDENT. TE-123M 2.596E-03 1.046E-02 2.161E-02 NOT IDENT. SB-124 -l.053E-02 4.213E-02 8.802E-02 NOT IDENT. SB-125 -4.232E-02 3.698E-02 6.117E-02 NOT IDENT. TE-125M 3.022E-01 3. 727E+OO 7.616E+OO NOT IDENT. I-126 -4.795E-02 1.074E-01 2.039E-01 NOT IDENT. SB-126 -3.335E-02 9.273E-02 1.752E-01 NOT IDENT. SN-126 9.SOOE-03 2.013E-02 4.233E-02 FAIL ABUN SB-127 -6.387E-01 1.336E+OO 2.517E+OO NOT IDENT. I-131 4. llSE-02 7.123E-02 1. 678E-01 NOT IDENT. I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 -1.025E-01 1.097E+OO 2.102E+OO NOT IDENT. BA-133 -6.204E-04 l.870E-02 3.895E-02 NOT IDENT. I-133 O.OOOE+OO 4.340E+05 0.000E+OO SHORT HLIF CS-134 -8.249E-03 l.710E-02 3.159E-02 FAIL ABUN CS-135 1.893E-03 5.851E-02 l.255E-01 NOT IDENT. I-135 O.OOOE+OO 1.148E+22 O.OOOE+OO SHORT HLIF CS-136 -4.382E-02 5.679E-02 1.016E-01 NOT IDENT. BA-137M 2.663E-03 1.359E-02 2.994E-02 NOT IDENT. CS-137 2.814E-03 l.435E-02 3.163E-02 NOT IDENT. CE-139 -1.022E-03 1.249E-02 2.426E-02 NOT IDENT. BA-140 1.999E-01 1. 786E-01 4.315E-01 NOT IDENT. LA-140 -l.503E-02 5.703E-02 1.165E-01 NOT IDENT. CE-141 -2. l 72E-02 2.514E-02 4.379E-02 NOT IDENT. CE-143 O.OOOE+OO 1.000E+03 O.OOOE+OO SHORT HLIF CE-144 3.865E-02 6.539E-02 1.441E-01 NOT IDENT. PM-144 -l.381E-03 1.695E-02 3.374E-02 NOT IDENT. PR-144 -1.144E-01 l.270E+00 2.525E+OO NOT IDENT. PM-146 -1.143E-02 1.823E-02 3.402E-02 NOT IDENT. ND-147 2.901E-02 4.257E-01 8.797E-01 NOT IDENT. PM-147 -l.922E+02 2.532E+02 4. 572E+02 NOT IDENT. PM-149 2.042E+02 2.830E+02 6.421E+02 NOT IDENT. EU-150 7. 724E-03 8.214E-03 1.898E-02 NOT IDENT. EU-152 1.383E-02 4.045E-02 8. 931E-02 NOT IDENT. GD-153 -7.600E-03 3.074E-02 6. 072E-02 NOT IDENT. EU-154 3.944E-03 3.149E-02 7.928E-02 NOT IDENT. EU-155 -1.714E-02 2.941E-02 5.559E-02 NOT IDENT. TB-160 -9.336E-03 5.400E-02 1. 086E-01 FAIL ABUN H0-166M -8.732E-04 2.717E-02 5.555E-02 FAIL ABUN TM-171 -1.036E+OO 2.947E+OO 6.087E+OO FAIL ABUN HF-172 1. 749E-02 6.942E-02 l.445E-01 FAIL ABUN LU-172 -5.810E-03 2.053E-02 4.350E-02 FAIL ABUN LU-176 2.061E-02 3.580E-02 2.683E-02 FAIL ABUN HF-181 -2.601E-03 2.072E-02 4.258E-02 NOT IDENT. TA-182 1.301E-02 5.601E-02 1.361E-01 FAIL ABUN RE-183 7.863E-03 3.921E-02 8.681E-02 FAIL ABUN RE-184 -l.591E-02 6.839E-02 l.304E-01 NOT IDENT. W-188 -3.575E-01 2.727E+b0 5.766E+OO FAIL ABUN IR-192 5.539E-03 l.303E-02 2.992E-02 NOT IDENT. HG-203 l.574E-02 1. 736E-02 4.043E-02 FAIL ABUN BI-207 -1.265E-02 1. 932E...:02 3.591E-02 FAIL ABUN TL-208 1.lOlE-02 2.031E-02 4.155E-02 NOT IDENT. BI-211 -3.067E-02 9.367E-02 1.919E-01 FAIL ABUN PB-211 5.158E-02 3. lOlE-01 6.124E-01 NOT IDENT. BI-212 1. 793E-02 2.377E-01 4.863E-01 NOT IDENT. PB-212 4.675E-03 2.370E-02 5.148E-02 FAIL ABUN BI-214 l.102E-02 3.905E-02 8.256E-02 NOT IDENT. PB-214 -5.032E-03 3.503E-02 7.316E-02 FAIL ABUN RN-219 -1.890E-02 l.356E-01 2.874E-01 NOT IDENT. RN-222 1.102E-02 3.905E-02 8.256E-02 NOT IDENT. Page 4292 of 5809 RA-223 5.608E-02 2.687E-01 5.818E-01 FAIL ABUN RA-224 -2.299E-01 2.271E-01 4.247E-01 NOT IDENT. RA-226 1.102E-02 3.905E-02 8.256E-02 NOT IDENT. AC-227 -2.798E-02 9.981E-02 2.056E-01 NOT IDENT. TH-227 -2.798E-02 9.981E-02 2.056E-01 NOT IDENT. AC-228 2.649E-03 6.232E-02 l.388E-01 FAIL ABUN RA-228 2.649E-03 6.232E-02 1.388E-01 FAIL ABUN TH-228 4.675E-03 2.370E-02 5.148E-02 FAIL ABUN TH-229 -2.463E-02 2.048E-01 3.633E-01 FAIL ABUN l.102E-02 3.905E-02 8.456E-02 NOT IDENT. PA-231 2.464E-02 l.735E-01 3.494E-01 NOT IDENT. TH-231 5.608E-02 2.687E-01 5.818E-01 FAIL ABUN TH-232 2.649E-03 6.232E-02 1. 388E-01 FAIL ABUN PA-233 1.142E-02 2.503E-02 5.313E-02 NOT IDENT. PA-234 5.794E-02 l.336E-01 3.078E-01 FAIL ABUN PA-234M 1.223E+OO 2.026E+OO 4.849E+OO NOT IDENT. TH-234 1.346E-01 6.889E-01 7.164E-01 FAIL ABUN U-234 l.102E-02 3.905E-02 8.256E-02 NOT IDENT. U-235 -l.238E-02 6.765E-02 l.389E-01 NOT IDENT. NP-237 l.142E-02 2.503E-02 5. 313E-02 NOT IDENT. NP-238 0.000E+OO 5.014E+Ol O.OOOE+OO SHORT HLIF u-238 l.346E-01 6.889E-01 7.164E-01 FAIL ABUN NP-239 2.474E-02 9.305E-02 l.957E-01 NOT IDENT. PU-239 -7.617E+Ol 1.164E+02 2.128E+02 NOT IDENT. AM-241 9.456E-03 2.924E-02 6.198E-02 NOT IDENT. CM-243 2.281E-03 3.079E-02 6.483E-02 NOT IDENT. BK-247 9.729E-03 3.420E-02 7.460E-02 FAIL ABUN CM-247 1. 87 9E-03' 1. 2 64E-02 2.818E-02 NOT IDENT. CF-249 1.532E-03 1.453E-02 3 .181E-02 NOT IDENT. CF-251 6.146E-02 5.357E-02 l.195E-01 NOT IDENT. ANH-511 -2.504E-02 3.025E-02 6.659E-02 NOT IDENT. Page 4293 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:55:46.38 Nuclide Line Activity Report Nuclide.Type: Nuclide Energy Area PB-210 46.54 22 AM-243 43.53 ------74.66 22 Flag: "*" Key line Page 4294 of 5809 %Abn %Eff 4.25* 2.450E+OO 5.90 l.694E+OO 67.20* 6.751E+OO

  • Uncorrected Decay Corr pCi/GRAM pCi7GRAM 8.655E-01 8.671E-01 ------Line Not Found l.985E-02 1.985E-02 2-Sigrna %Error 162.73 118 .19 Summary of Nuclide Activity Sample ID : Gl203621361 Acquisition date Page : 2 3-0CT-2016 07:53:26 Total number of lines in spectrum 17 Number of unidentified lines 5 Number of lines tentatively identified by NID 12 Nuclide Type : Nuclide PB-210 AM-243 Hlife 22.20Y 7370.00Y Decay 1. 00 1. 00 Total Activity Grand Total Activity
  • Uncorrected pCi/GRAM 8.655E-01 1.985E-02 8.854E-01 8.854E-01 Decay Corr pCi/GRAM 8.671E-01 l.985E-02 8.870E-01 8.870E-01 70.59% Decay Corr 2-Sigma Error 14.llE-01 2.347E-02 Manually accepted 2-Sigma %Error Flags 162.73 118 .19 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 4295 of 5809 Unidentified Energy Lines Page : 3 Sample ID : Gl203621361 Acquisition date : 3-0CT-2016 07:53:26 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 63.13 7 54 1. 35 126.33 122 31 1.24E-03 **** 5. 51E+OO T 3 66.47 10 40 1. 02 133.00 122 31 1.89E-03 **** 5.92E+OO T 3 73.06 17 53 1. 38 146.17 122 31 3.25E-03 **** 6.58E+OO T 0 84.41 31 67 0. 64
  • 168.88 164 10 6.00E-03 **** 7.36E+OO T. 0 181.10 13 16 1.19 362.32 361 4 2.83E-03 **** 6.81E+OO T 1 191.50 25 36 1. 33 383.12 366 21 5.33E-03 95.0 6.57E+OO 0 211. 96 20 42 1. 39 424.05 418 9 4.32E-03 **** 6.14E+OO T 0 306.90 22 53 3.21 613.97 605 17 4.86E-03 **** 4.64E+OO T 0 331.10 31 20 0.95 662.39 657 11 7.03E-03 77.0 4.36E+OO 0 337.70 35 9 4.44 675.60 668 15 7.92E-03 56.2 4.30E+OO T 0 409.56 12 15 1. 75 819.37 813 8 2. 71E-03 **** 3.68E+OO T 0 569.81 21 3 1. 56 1139. 97 1135 10 5.13E-03 56.5 2.84E+OO T 0 641.91 8 11 0.86 1284.22 1277 9 2.03E-03 **** 2.59E+OO 0 781.57 9 3 1. 41 1563.65 1558 9 2.40E-03 92.8 2.23E+OO 0 1294.14 6 0 0.96 2589.33 2586 6 l.67E-03 81. 6 1.50E+00 Flags: "T" = Tentatively associated Page 4296 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:56:05.18 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621361.CNF;l *
  • Acquisition date 3-0CT-2016 07:53:26 Sensitivity : 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.55 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID : G1203621361 Analyst initials: MXRl *
  • Batch Number :* 1596252 Sample Quantity : 1.8148E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide PB-210 AM-243 Le (pCi/GRAM 5.074E-01 l.322E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 Page 4297 of 5809 Le (pCi/GRAM 1.369E-01 9.778E-03 O.OOOE+OO O.OOOE+OO l.356E-01 1.159E-02 2.054E-02 1. 750E-01 1.105E-02 1. 913E-02 O.OOOE+OO 6.812E-03 1. 706E-02 l.424E-02 1. 655E-02 3.675E-02 4.566E-01 1. 321E-01 5.106E-02 2.00lE-02 2.156E+Ol 1.467E-01 2.363E-02 3.743E+OO 2.116E-02 3.543E-01 1. 77 5E-02 5.923E+OO 1.575E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT 'I DENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 Page 4298 of 5809 1. 283E-02 3.971E-02 2.993E-02 0.000E+OO O.OOOE+OO 1.948E+Ol O.OOOE+OO 9.956E-03 1.991E-02 1.437E-02 1. 221E-01 1.221E-01 1.334E-02 1.913E-01 1. 874E-02 l.951E-02 3.954E+Ol 2.476E-02 9.671E-03 3 .119E-02 2.488E-02 3.434E+OO 7.976E-02 7.246E-02 1. 891E-02 9.570E-01 7.245E-02 O.OOOE+OO 9.302E-01 l.713E-02 O.OOOE+OO 1.264E-02 5.542E-02 O.OOOE+OO 3.834E-02 l.239E-02 1.309E-02 1.093E-02 1. 898E-01 4.310E-02 1. 924E-02 O.OOOE+OO 6.452E-02 1.436E-02 1.074E+OO 1.430E-02 3.821E-01 2.008E+02 2. 8 92E+02 8.046E-03 3. 931E-02 2.743E-02 2.884E-02 2.404E-02 4.269E-02 2.327E-02 2.673E+OO 6.515E-02 1.633E-02 1. 203E-02 1.807E-02 5.274E-02 3.859E-02 5.365E-02 2.500E+OO 1.300E-02 1.818E-02 l.356E-02 1.830E-02 8.483E-02 2.638E-01 2.060E-01 2.328E-02 3.650E-02 3.253E-02 l.195E-01 3.650E-02 2.570E-01 NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230

  • PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 4299 of 5809 1.859E-01 3.650E-02 9.087E-02 9.087E-02 5.810E-02 5.810E-02 2.328E-02 1.604E-01 3.650E-02 1.508E-01 2.570E-01 5.810E-02 2.315E-02 1. 28 9E-01 2.053E+OO 3.273E-01 3.650E-02 6.205E-02 2.315E-02 O.OOOE+OO 3.273E-01 8.804E-02 9.392E+Ol 2.745E-02 2.864E-02 3.343E-02 1.187E-02 1. 355E-02 5.463E-02 3.139E-02 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:56:10.51 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* t
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621361.CNF;l * *Acquisition date 3-0CT-2016 07:53:26 Sensitivity : 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.55 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621361 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity 1.8148E+02 GRAM *
  • Quantity Err(%) 1.1020E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) PB-210 8.671E-01 1.385E+OO 1.385E+OO AM-243 l.985E-02 2.303E-02 2.303E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 5.083E-02 1.425E-01 l.443E-01 NOT IDENT. NA-22 8.425E-04 1.088E-02 1.089E-02 NOT IDENT. NA-24 5.683E+07 l.866E+08 l.883E+08 SHORT HLIF AL-26 -1.587E-02 1.559E-02 1.715E-02 NOT IDENT. K-40 -1.089E-01 1.709E-01 l.778E-01 NOT IDENT. SC-46 -l.338E-02 1.743E-02 1.844E-02 NOT IDENT. V-48 -2.147E-02 3.062E-02 3.211E-02 NOT IDENT. CR-51 5.287E-02 l.806E-01 1.821E-01 NOT IDENT. MN-54 -l.049E-02 1.624E-02 1.691E-02 NOT IDENT. C0-56 1.008E-02 2.023E-02 2.073E-02 NOT IDENT. MN-56 1.000E+41 l.529E+41 O.OOOE+OO SHORT HLIF C0-57 -6.419E-03 8.608E-03 9. 081E-03 NOT IDENT. C0-58 7.859E-03 l.802E-02 1.836E-02 NOT IDENT. FE-59 -1.580E-02 2.433E-02 2.535E-02 NOT IDENT. C0-60 1.433E-02 1.470E-02 1.606E-02 NOT IDENT. ZN-65 S.535E-03 3.984E-02 4.003E-02 NOT IDENT. GE-68 2.552E-01 4.444E-01 4.591E-01 NOT IDENT. AS-73 -4.145E-02 l.538E-01 1.550E-01 NOT IDENT. AS-74 1.504E-03 5. 796E-02 5.796E-02 NOT IDENT. SE-75 l.002E-02 l.999E-02 2.049E-02 NOT IDENT. BR-77 -2.546E+OO 2.278E+Ol 2.281E+Ol NOT IDENT. SR-82 2.193E-02 l.853E-01 1.856E-01 NOT IDENT. RB-83 7.944E-03 2.449E-02 2.475E-02 NOT IDENT. KR-85 -1.077E+Ol 5.538E+OO 7.365E+OO NOT IDENT. SR-85 -6.lOOE-02 3.133E-02 4.168E-02 NOT IDENT. RB-86 1.950E-01 3.454E-01 3.564E-01 NOT IDENT. Y-88 3.774E-03 1. 971E-02 1.978E-02 NOT IDENT. Y-91 -1.230E+OO 7.191E+OO 7.212E+OO NOT IDENT. Page 4300 of 5809 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 Page 4301 of 5809 4.237E-03 -5.581E-03 -1.053E-02 4.166E-03 -1.000E+41 -1. 260E+09 -7.767E+OO 2.463E+23 l.476E-03 5. 533E-03 * -1.478E-02 3.409E-02 3.409E-02 6.198E-03 1.316E-03 -3. 511E-03 9.437E-03 1.772E+Ol -4.194E-03 2. 596E-03 -l.053E-02 -4.232E-02 3.022E-01 -4.795E-02 -3.335E-02 9.800E-03 -6.387E-01 4 .115E-02 -1.000E+41 -l.025E-01 -6.204E-04 2.013E+05 -8.249E-03 1.893E-03 -6.036E+21 -4.382E-02 2.663E-03 2.814E-03 -1.022E-03 1.999E-01 -1.503E-02 -2.172E-02 1.540E+Ol 3.865E-02 -1.381E-03 -l.144E-01 -l.143E-02 2.901E-02 -l.922E+02 2.042E+02 7. 724E-03 l.383E-02 -7.600E-03 3.944E-03 -l.714E-02 -9.336E-03

-8.732E-04 -l.036E+OO 1. 749E-02 -5.810E-03 2.061E-02 -2.601E-03 1.301E-02 7.863E-03 -l.591E-02 -3.575E-01 5.539E-03 1. 574E-02 -1.265E-02 l.lOlE-02 -3.067E-02 5.158E-02 1.793E-02 4.675E-03 l.102E-02 -5.032E-03 -1. 890E-02 1.102E-02 1. 744E-02 1. 67 4E-02 4.315E-02 3.394E-02 3.817E+41 5.573E+08 2.491E+Ol 3.645E+23 1. 078E-02 2.143E-02 l.942E-02 l.318E-01 l.318E-01 1. 372E-02 2.225E-01 2.331E-02 l.982E-02 4.155E+Ol 2.848E-02 1.046E-02 4.213E-02 3.702E-02 3.727E+OO 1.074E-01 9.279E-02 2.014E-02 1.338E+OO 7.125E-02 7. 291E+41 1.097E+OO l.870E-02 4.350E+05 1. 710E-02 5.851E-02 l.185E+22 5.690E-02 l.359E-02 l.435E-02 1.249E-02 1. 788E-01 5.703E-02 2.516E-02 l.000E+03 6.543E-02 1.695E-02 1.270E+OO l.824E-02 4.257E-01 2.534E+02 2.844E+02 8.220E-03 4.046E-02 3.074E-02 3.149E-02 2.944E-02 5. 401E-02 2.717E-02 2.949E+OO 6.948E-02 2.054E-02 3.581E-02 2. 072E-02 5.601E-02 3.922E-02 6.840E-02 2. 728E+OO' 1.304E-02 1.737E-02 1.933E-02 2.032E-02 9.368E-02 3. lOlE-01 2.377E-01 2.370E-02 3.905E-02 3.503E-02 l.356E-01 3.905E-02 l.755E-02 l.693E-02 4.341E-02 3.400E-02 O.OOOE+OO 7.958E+08 2.516E+Ol O.OOOE+OO 1. 080E-02 2.157E-02 2.053E-02 1.327E-01 l.327E-01 l.400E-02 2.225E-01 2.336E-02 2.027E-02 4. 231E+Ol 2.855E-02 l.053E-02 4.240E-02 4.165E-02 3. 729E+OO 1. 096E-01 9.400E-02 2.062E-02 1.369E+OO 7.363E-02 O.OOOE+OO 1.098E+OO l.870E-02 4.443E+05 1. 750E-02 5.852E-02 O.OOOE+OO 6.024E-02 l.364E-02 1.441E-02 1.250E-02 2.003E-01 5.743E-02 2.700E-02 l.000E+03 6. 771E-02 1.696E-02 1. 272E+OO l.896E-02 4.259E-01 2.678E+02 2.989E+02 8.927E-03 4.094E-02 3.093E-02 3.154E-02 3.044E-02 5.417E-02 2.717E-02 2.985E+OO 6.992E-02 2. 071E-02 3.700E-02 2.076E-02 5.632E-02 3.938E-02 6.878E-02 2.732E+OO 1.327E-02 l.877E-02 2.015E-02 2.092E-02 9.470E-02 3. llOE-01 2.379E-01 2.380E-02 3.936E-02 3.510E-02 l.359E-01 3.936E-02 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT I DENT.

  • NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

RA-223 5.608E-02 2.688E-01 2.700E-01 FAIL ABUN RA-224 -2.299E-01 2.274E-01 2.499E-01 NOT IDENT. RA-226 l.102E-02 3.905E-02 3.936E-02 NOT IDENT. AC-227 -2.798E-02 9.988E-02 l.007E-01 NOT IDENT. TH-227 -2.798E-02 9.988E-02 1.007E-01 NOT IDENT. AC-228 2.649E-03 6.232E-02 6.233E-02 FAIL ABUN RA-228 2.649E-03 6.232E-02 6.233E-02 FAIL ABUN TH-228 4.675E-03 2.370E-02 2.380E-02 FAIL ABUN TH-229 -2.463E-02 2.048E-01 2.0SlE-01 FAIL ABUN TH-230 1.102E-02 3.905E-02 3.936E-02 NOT IDENT. PA-231 2.464E-02 1. 736E-01 1. 740E-01 NOT IDENT. TH-231 5.608E-02 2.688E-01 2.700E-01 FAIL ABUN TH-232 2.649E-03 6.232E-02 6.233E-02 FAIL ABUN PA-233 1.142E-02 2.504E-02 2.556E-02 NOT IDENT. PA-234 5.794E-02 l.492E-01 1.514E-01 FAIL ABUN PA-234M 1. 223E+OO 2.027E+OO 2.lOOE+OO NOT IDENT. TH-234 1. 346E-01 6. 896E-01 6.922E-01 FAIL ABUN U-234 1.102E-02 3.905E-02 3.936E-02 NOT IDENT. U-235 -1.238E-02 6. 7 65E-02 6.788E-02 NOT IDENT. NP-237 1.142E-02 2.504E-02 2.556E-02 NOT IDENT. NP-238 -2.515E+Ol 5.015E+Ol 5 .141E+Ol SHORT HLIF U-238 1.346E-01 6.896E-01 6.922E-01 FAIL ABUN NP-239 2.474E-02 9.307E-02 9.374E-02 NOT IDENT. PU-239 -7.617E+Ol 1.164E+02 l.214E+02 NOT IDENT. AM-241 9.456E-03 2.925E-02 2.956E-02 NOT IDENT. CM-243 2.281E-03 3.079E-02 3.081E-02 NOT IDENT. BK-247 9.729E-03 3.426E-02 3.454E-02 FAIL ABUN CM.:...247 l.879E-03 l.264E-02 'l. 267E-02 NOT IDENT. CF-249 1.532E-03 1.454E-02 1.455E-02 NOT IDENT. CF-251 6.146E-02 5.401E-02 6.070E-02 NOT IDENT. ANH-511 -2.504E-02 3.027E-02 3.230E-02 NOT IDENT. Page 4302 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 23.3467 87.09 12.7275 136.47 17.0416 45.60 22.4884 87.57 16.9832 140.51 20.5491 46.54 22. 5396 88.03 22.6610 143.76 18.3359 49.72 21.0634 88.34 21. 2553 144.24 18.3462 51. 35 17.8385 88.47 21. 2598 145.44 29.8542 51. 87 17.8594 89. 96 21. 3104 152.43 39.3530 52.39 21.8536 90.64 38.4002 153.25 22.0117 52.97 22.8766 91.11 59.7777 154.21 23.1952 53.44 17.9220 92.59 34.2383 156.02 27.8903 54.07 23.9291 93.35 22.4953 158.56 26.8029 57.36 0.0000 94.56 67.6123 159.00 20.9864 57.53 22.0989 94.65 60.1084 162.33 17.5518 57.98 19.1034 94. 67 60 .1101 162.66 30.4338 59.27 16.1303 94.87 51.5387 163.33 31.6274 59.32 16.1320 97.43 33.4155 165.86 29.3636 59.54 16.1393 98.43 17.2727 176.31 23.7476 60. 96 21. 5818 98.44 17.2729 176.60 21. 3791 61.17 21. 5910 99.53 34.6023 177.52 20.2103 62.93 29.4543 100.11 28.1386 181.07 14.3172 63.29 29.4754 102.03 18.4504 181. 52 17.5066 63.58 29.4925 103.18 21.7429 184.41 19.1531 64.28 29.5332 103.37 18.4865 185. 72 19.1780 66.73 29.6742 105.21 20.7165 193.51 20.9335 67.24 29.7031 105.31 20.7194 197.03 16. 9644 67.68 29.7281 106.12 25 .1105 198.01 24.2575 67.75 29.7321 106.47 26.2152 201.83 21.9098 69.67 29.8401 109.28 21.9330 203.43 23.1615 70.83 29.9045 111. 00 25.2835 205.31 25.6437 72.81 30.0133 111.76 24.2097 210.85 18.4094 72. 87 30.0167 114. 06 27.5978 215.65 16.0235 74.66 30 .1138 116. 30 19.9308 222 .11 18.5939 74.82 30.1224 116.74 23.2664 227.09 23.6537 74.97 30.1304 119.76 18.9105 227.38 23.6595 77 .11 22.2490 121.12 27.8593 228.16 21.1831 78.74 28.2391 121. 22 27.8629 228.18 21.1836 79.69 30.7296 121.78 24.5373 235.69 20.9002 80.12 25 .1611 122.06 26.7779 235. 96 23.4134 80.19 23.7660 122.92 18.9888 238.63 16.7611 80.57 22.3825 123.07 18.9926 238.98 19.2808 81. 00 22.3989 123.68 26.8341 240.99 29.3888 81. 07 22.4015 125.81 24.6654 242.00 22.6903 81. 75 23.8291 127.23 22.4635 244.70 16.8447 83.79 26.3721 127.91 25.8554 252.40 16.1018 84.00 26.3813 129.30 28.1528 252.80 14. 4114 85.43 26.4437 131.20 25.9620 254.15 0.0000 86.55 19.7809 133. 02 18 .1013 256.23 22.9510 86.79 12. 7213 133.52 16.9805 260.90 23.0350 86.94 12.7244 136.00 22.7094 264.66 20.5352 Page 4303 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 20.5371 364.49 8.2449 600.60 14.4489 265.00 21. 3964 366.42 10.0889 602.52 0.0000 268.22 18.8754 372. 51 8.2852 604. 72 19.6432 269.46 20.6104 375.05 17.5176 607.14 18.6284 270.03 23.1971 377.52 13.8501 609.32 10.3589 271.23 17.1985 383.85 8.3414 610.33 15.5444 273.65 15.5068 388.16 10.2207 614.28 6.2280 276.40 19.8555 388.63 10.2237 618.01 11. 4360 277.37 21. 5973 391.69 12.1039 620.36 5.2032 277.60 20.7373 400.66 8.4230 621. 93 7.2891 278.00 16.4217 401. 81 9.3652 630.19 0.0000 279.20 15.5713 402.40 8.4315 631.29 6.2720 279.54 22.4977 404.85 11. 2576 633.25 10.4614 279.70 22.5003. 410.95 11.2964 634.78 8.3743 280.46 26.8424 413.71 11. 3140 635.95 7.8546 283.69 22.5664 414.70 16.0368 636.99 7.8580 284.31 27.7865 423. 72 15.1689 645.85 8. 4118 285.41 23.4641 427.09 15 .1969 657.76 13.7342 285.90 18.2562 427.87 17.1039 657.90 0.0000 287.50 18.2774 433.94 12.3935 661. 66 6.3486 290.67 15.7024 439.40 18.1666 664.57 0.0000 293.27 0.0000 453.88 15.4157 666.33 7.4204 295.22 14.0033 463.37 16.4598 666.50 8.4808 295.96 14.8861 468.07 11. 6467 667.71 0.0000 298.58 17.5456 473.00 10.7030 677.62 8.5176 299.98 11. 8551 475.06 11. 6880 685.70 6.4082 300.09 6.5866 476.78 4.8743 695.00 10. 7182 300.13 6.5868 477.60 8.7773 696.49 11. 7967 301.36 11. 8 666 482.18 11.7300 696. 51 11. 7967 302.85 9.2392 487.02 12.7379 697.00 15.0168 304.50 13.2141 492.35 14.7363 697.30 13.9458 304.85 13.2172 497.08 14.7705 697.49 13.9469 306.78 13.2349 505.52 12.8537 702.65 11. 8240 308.46 13.2504 507.63 0.0000 706.68 13. 9950 311. 90 10.6252 511. 00 22.8007 711. 68 6.4712 316.51 10.6587 514.00 58. 5727 720.70 10.8215 319.41 15 .1296 514.00 58.5727 721. 93 0.0000 320.08 16.0269 520.40 4.9788 722.78 8.6641 321.04 14.2552 520.69 5.9756 722. 91 5.4152 323.87 16. 9601 522.65 0.0000 723. 31 5.4161 325.23 18.7625 527.90 12.9905 724.19 9.7518 328.76 16 .1195 528.26 10.9942 727.33 6.5088 333.37 2.6948 529.59 13. 0011 733.00 7.6093 333.97 2.6958 529.87 0.0000 735.93 9.7939 334.37 2. 6965 531. 02 14.0103 737.46 8.7106 338.28 9.4618 537.26 7.0253 739.50 8.7168 338.32 9.4620 546.56 0.0000 747.24 3.2780 340.48 17.5969 552.55 10.1062 748.06 3.2789 340.55 17.5977 563.25 8.1240 752.31 4.3786 344.28 14.4736 569.33 6.1094 753.82 7.6665 345.93 14.4886 569.50 6.1099 756.73 7.6745 351. 06 15.4443 569.70 6 .1104 756.80 7.6748 351.93 15.4526 583.19 8.1953 763.94 4. 3966 355.39 0.0000 584.27 8.1992 765.81 7.6993 356.01 18.2263 595.83 12.3599 766.42 12 .1011 Page 4304 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 13.2031 1002.74 4.4452 1678.03 0.0000 772. 60 0.0000 1004.73 7 .1165 1690.97 3.1227 776.52 6.6240 1021.30 0.0000 1750.46 0.0000 777.92 3.3136 1025.87 0.0000 1764.49 4.2205 778.90 8.2870 1028.54 0.0000 1770.23 2 .1124 783.70 8.3008 1037. 84. 3.5916 1771.35 3.1694 785.37 0.0000 1038.76 0.0000 1791.20 0.0000 792.07 6.6597 1046.59 2.7001 1808.65 4.2542 794.95 6.6663 1048.07 8.1035 1810.72 0.0000 795.86 6.6685 1049.04 5.4038 1836.06 2.1373 801.95 1.1137 1050.41 2. ?.030 810.06 5.5839 1063.66 7.2339 810.29 4.4674 1077.00 2.7226 810.45 4. 4 676 1077.34 2.7230 810.76 5.5851 1085.87 3.6389 815.77 5.5945 1093.63 4.5581 818.51 7.8394 1099.45 3.6521 832.01 3.3749 1112. 07 9.1608 834.85 10.1342 1112.84 9.1626 835.71 10 .1371 1115. 54 7.3350 836.80 0.0000 1120.29 6. 42 62 846.75 0.0000 1120.55 6.4266 846.77 6.7825 1121.30 2.7548 856.80 5.6706 1129. 67 5.5217 860.56 4.5418 1131.51 0.0000 871.09 10.2539 1147.95 0.0000 873.19 6.8403 1173.23 0.9306 875.33 0.0000 1177.95 2.7951 879.38 5. 7115 1189.05 5.6056 880.51 5.7135 1204.77 4. 6896 883.24 5. 7186 1221.41 2.8253 884.68 8.0094 1231. 02 0.9440 889.28 5.7294 1235.36 4.7247 894.76 5.7391 1238.28 1. 8912 898.04 10.3411 1260.41 0.0000 900.72 4.5999 1271.87 1. 9065 903.28 9.2070 1274.44 1. 9076 911.20 3.4611 1274.54 1. 9077 912.08 3.4620 1291.59 1. 5322 923.98 0.0000 1298.22 0.0000 926.50 3.4773 1312 .11 6.7355 929 .11 4.6401 1332.49 0. 9667 937.49 3.4889 1362.66 0.0000 944.13 6.9917 1365.19 3.8955 946.00 2.3319 1368.63 0.0000 949.00 7.0017 1384.29 0.9780 954.55 0.0000 1408.01 0.9832 962. 31 7.0295 1457.56 0.0000 964. 0 8 10.5498 1460.82 2.9830 966 .17 7.0374 1489.16 2.0005 968.97 2.6412 1505.03 4.0142 983.53 6.1891 1584.12 1. 0197 984.45 0.0000 1596.21 4.0886 996.26 8.8739 1620.50 2.0541 1001.03 2.6658 1621. 92 5.1364 Page 4305 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:56:39.30 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621362.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM29.CNF;354 Background date : Z-OCT-2016 11:01:41. Sample date 30-NOV-2015 13:27:00 Acquisition date : 3-0CT-2016 07:54:00. Sample ID G1203621362 Sample quantity : 1.81483E+02 GRAM Detector name : GAM29 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.45 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 2 2 0 3 3 3 0 0 0 0 3 3 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 3 3 0 0 0 Page 4306 of 5809 Energy 74.86* 77.22* 84.04* 86.89 90.20 92.91* 128.29 159.92 186.23* 194.46 207.21 209.20 238.64* 241.48 295.24* 329.40 334.02 338.38* 351.93* 397.75 400.82 405.54 463.19 510.81* 547.02* 583.62* 609.36* 662.86 684.20 709.15 712.16 727. 66 750.81 757.59 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 121 181 36 92 44 95 62 49 53 31 28 54 334 84 165 12 19 89 271 7 17 18 32 13 11 116 172 25 11 11 13 27 15 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 162 163 146 125 159 113 170 234 139 116 31 99 85 103 78 69 38 56 64 29 34 45 33 70 29 49 49 41 15 5 18 44 9 16 1. 08 1. 22 1.16 1. 36 1. 35 1. 08 1. 37 3.84 1.26 1. 33 1. 23 1. 55 1. 02 1. 75 1.13 0.49 1. 24 0.94 1. 31 1. 24 3.16 0. 67 2.50 1. 23 0.74 1. 03 1.14 1.13 1. 02 1. 40 1. 80 0.78 1.16 0.52 149.65 154.37 167.99 173.68 180.29 185.69 256.36 319.53 372.08 388.54 414.00 417. 97 476.79 482.45 589.85 658.10 667.34 676.04 703.12 794.65 800.79 810.22 925.42 1020.60 1092.97 1166 .13 1217.57 1324.51 13 67 .17 1417.06 1423.06 1454.05 1500.33 1513.91 145 145 165 171 171 171 251 314 367 383 412 412 472 472 584 652 665 672 698 790 796 805 922 1014 1089 1160 1213 1318 1363 1415 1415 1446 1496 1506 16 3.35E-02 18.8 16 5.02E-02 14.6 7 1. OlE-02 58. 6 32 2.56E-02 21.4 32 1. 23E-02 51. 6 32 2.63E-02 22.4 11 1. 71E-02 43. 3 16 1.36E-02 71.2 9 l.47E-02 45.2 10 8.61E-03 69.6 12 7. 66E-03 31. 6 12 1. 51E-02 37. 0 15 9.29E-02 7.1 15 2.33E-02 27.6 10 4.57E-02 12.8 8 3.28E-03126.0 7 5.28E-03 59.4 10 2.46E-02 19.2 12 7.52E-02 8.6 7 1.82E-03140.4 9 4.62E-03 67.8 10 5.00E-03 73.6 9 8.81E-03 37.5 14 3.72E-03156.3 9 2.95E-03 99.4 12 3.21E-02 15.7 9 4.77E-02 10.8 13 6.94E-03 57.1 8 3.18E-03 66.4 22 3.18E-03 40.0 22 3.70E-03 72.4 16 7.44E-03 58.7 8 4.lOE-03 45.0 11 3.07E-03 77.1 Fit 1.15E+OO l.65E+00 3.06E+00 1.89E+00 1. OlE+OO Peak Search Report (continued) Page : 2 Sample ID : Gl203621362 Acquisition date 3-0CT-2016 07:54:00 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 768.46 19 30 3.80 1535.63 1528 12 5.23E-03 62.7 36 0 795.83 27 25 3.40 1590.35 1585 13 7.58E-03 42.8 37 0 860.59 23 25 4.07 1719.85 1712 14 6.50E-.03 49.5 38 0 894.62 15 12 1. 44 1787.89 1782 11 4.06E-03 55.1 39 0 911. 51* 62 31 1. 57 1821. 68 1817 11 1.71E-02 22.0 40 0 915.66 15 5 1. 47 1829.98 1827 8 4.06E-03 38 .-7 41 0 934.11* 20 11 2.04 1866.87 1860 11 5.68E-03 40.5 42 0 955.28 8 9 0.69 1909.21 1902 9 2.23E-03 76. 0 43 2 964.83 22 11 1. 94 1928.33 1924 24 6.14E-03 38.4 3.59E-01 44 2 968.70* 46 15 1. 95 1936.06 1924 24 1.29E-02 24.1 45 0 984.31 28 41 7.88 1967. 27 1951 26 7.65E-03 69.3 46 0 1000.59* 9 10 0.87 1999.84 1994 10 2.48E-03 79.2 47 0 1120.76* 51 20 1. 49 2240.22 2235 13 l.42E-02 23.2 48 0 1170.26 9 17 1. 84 2339.27 2333 10 2.48E-03 93.6 49 0 1238.99* 16 32 1. 39 2476.79 2469 13 4.39E-03 79.8 50 0 1327.38 6 10 0.56 2653.67 2647 10 1. 61E-03110. 2 51 0 1377.71* 15 2 0.98 2754.40 2750 9 4.05E-03 34.8 52 0 1395. 69 7 5 0.64 2790.38 2785 9 1.81E-03 70.7 53 0 1408.25 7 10 1.19 2815.51 2810 10 2.08E-03 86.8 54 0 1460.91* 473 11 1.85 2920.93 2913 14 1. 31E-01 4. 9 55 0 1593.69 4 7 0.95' 3186.75 3181 7 1. llE-03120. 5 56 0 1730.19 14 3 1.12 3460.08 3454 9 3.98E-03 32.8 57 0 1764.63* 32 0 2.25 3529.05 3523 11 8.89E-03 19.7 58 0 1846.28 10 0 1.05 3692.60 3686 11 2.78E-03 31.6 Flag: "*" = Peak area was modified by background subtraction Page 4307 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 08:56:41 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621362.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 30-NOV-2015 13:27:00 Gl203621362 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 07:54:00 181. 48 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOI.ID GAMMA29 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide ,Page 4308 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243' TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:01.45 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G1203621362 Acquisition date 3-0CT-2016 07:54:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-4.0 1460.82 10.66* l.347E+OO l.339E+Ol 1.339E+Ol 9.73 OK CD-109 88.03 3.70* 6.242E+OO 1.468E+OO 2.330E+OO 70. 96 OK TE-123M 159.00 84.00* 6.985E+OO 4.621E-02 2.767E-01 142.35 OK SN-126 64.28 9.60 3.737E+OO Line Not Found Absent 86.94 8.90 6.242E+OO 6.102E-01 6.102E-01 70. 96 OK 87.57 37.00* 6.242E+OO l.468E-01 l.468E-01 70.96 OK BA-137M 661. 66 89.90* 2.518E+OO 5. 071E-02 5.170E-02 114 .17 OK CS-137 661. 66 85.10* 2.518E+OO 5.357E-02 5.462E-02 114.17 OK TL-208 277.37 6.60 4.914E+OO Line Not Found Absent 583.19 85.00* 2.771E+OO 2.297E-01 2.297E-01 31. 44 OK 860.56 12.50 2.069E+00 3.998E-01 3.998E-01 98.91 OK PB-212 74.82 10.28 5.108E+OO 8.367E-01 8.367E-01 64.85 OK 77.11 17.10 5.368E+OO l.187E+OO 1.187E+OO 29.14 OK 238.63 43.60* 5.496E+OO 7.363E-01 7.363E-01 14.13 OK 300.09 3.30 4.626E+OO Line Not Found Absent BI-214 609.32 45.49* 2.683E+OO 6.541E-01 6.544E-01 21. 56 OK 1120.29 14.92 1.685E+OO 8.658E-01 8. 661E-01 46.46 OK 1764.49 15.30 1.129E+OO 7.309E-01 7. 311E-01 39.34 OK PB-214 74.82 5 .'80 5.103E+OO Line Not Found -----<<INT Reject 77 .11 9.70 5.368E+OO 2.092E+OO 2.093E+OO 29.14 OK 87.09 3.41 6.257E+OO Line Not Found <<INT Reject 242.00 7.25 5.441E+OO Line Not Found <<INT Reject 295.22 18.42 4.685E+OO 9.801E-01 9.805E-01 25.67 OK 351.93 35.60* 4.087E+OO 9.335E-01 9.338E-01 17.17 OK RN-222 609.32 45.49* 2.683E+OO 6. 541E-01 6.544E-01 21. 56 OK 1120.29 14.92 1.685E+OO 8.658E-01 8.661E-01 46.46 OK 1764.49 15.30 1.129E+OO 7.309E-01 7. 311E-01 39.34 OK RA-224 240.99 4.10* 5.449E+OO 2.414E-01 2.414E-01 487.99 OK RA-226 609.32 45.49* 2.683E+OO 6.541E-01 6.544E-01 21. 56 OK 1120.29 14.92 1.685E+OO 8.658E-01 8. 661E-01 46.46 OK 1764.49 15.30 1.129E+OO 7.309E-01 7. 311E-01 39.34 OK AC-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 OK 794.95 4.25 2.196E+OO 1.309E+OO 1.309E+OO 85.63 OK 835.71 1. 61 2 .116E+OO Line Not Found Absent 911.20 25.80* 1.981E+OO 5.294E-01 5.294E-01 43.94 OK 968. 97 15.80 1.890E+OO 6. 731E-01 6. 731E-01 48.20 OK RA-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 OK 794.95 4.25 2 .196E+OO 1.309E+OO 1.309E+OO 85.63 OK 835.71 1. 61 2 .116E+OO Line Not Found Absent 911. 20 25.80* 1.981E+OO 5.294E-01 5.294E-01 43.94 OK 968. 97 15.80 1.890E+OO 6. 731E-01 6.731E-01 48.20 OK TH-228 74.82 10.28 5.108E+OO 8.367E-01 8.367E-01 64.85 OK 77 .11 17 .10 5.368E+OO 1.187E+OO 1.187E+OO 29.14 OK 238.63 43.60* 5.496E+OO 7.363E-01 7.363E-01 14.13 OK 300.09 3.30 4.626E+OO Line Not Found Absent TH-230 609.32 45.49* 2.683E+OO 6.541E-01 6.541E-01 21. 56 OK 1120.29 14.92 1.685E+OO 8.658E-01 8.658E-01 46.46 OK Page 4309 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G1203621362 Acquisition date 3-0CT-2016 07:54:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status

  • 1764.49 15.30 1.129E+OO 7.309E-01
  • 7.309E-01 39.34 OK TH-232 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 OK 835.71 1. 61 2 .116E+OO Line Not Found Absent 911. 20 25.80* 1.981E+OO 5.294E-01 5.294E-01 43.94 OK 968. 97 15.80 1.890E+OO 6.731E-01 6.731E-01 48.20 OK U-234 609.32 45.49* 2.683E+OO 6.541E-01 6.541E-01 21. 56 OK 1120.29 14.92 1. 685E+OO 8.658E-01 8.658E-01 46.46 OK 1764.49 15.30 1.129E+OO 7.309E-01 7.309E-01 39.34 OK U-235 89. 96 3.47 6.473E+OO l.167E+OO 1.167E+00 103.23 OK 93.35 5.60 6.639E+OO 1.505E+OO l.505E+OO 44. 72 OK 143.76 10. 96* 7.247E+OO Line Not Found Absent 163.33 5.08 6.922E+OO Line Not Found Absent 185.72 57.20 6.471E+OO 7.775E-02 7.775E-02 90.32 OK 205.31 5.01 6.095E+OO Line Not Found Absent AM-243 43.53 5.90 7.707E-01 Line Not Found Absent 74.66 67.20* 5.108E+OO 1.280E-01 l.280E-01 64.85 OK ANH-511 511. 00 100.00* 3.065E+OO 2.085E-02 2.085E-02 312.60 OK Flag: "*" = Keyline Page 4310 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:56:42.36 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621362.CNF;l * *Acquisition date 3-0CT-2016 07:54:00 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:27:00 Analyst initials: MXRl *
  • Sample ID G1203621362 Sample Quantity 1.8148E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF'GAM29 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1. 339E+Ol 1.276E+OO 5.070E-01 CD-109 2.330E+OO 1.621E+OO 1.436E+OO TE-123M 2.767E-01 3.860E-01 1.844E-01 SN-126 l.468E-01 1. 021E-01 9.090E-02 BA-137M 5.170E-02 5.785E-02 4.530E-02 CS-137 5.462E-02 6. lllE-02 4.785E-02 TL-208 2.297E-01 7.078E-02 5.229E-02 PB-212 7.363E-01 l.020E-01 7.430E-02 BI-214 6.544E-01 1.383E-01 9.840E-02 PB-214 9.338E-01 1. 572E-01 8. 672E-02 RN-222 6.544E-01 1.383E-01 9.840E-02 RA-224 2.414E-01 1.154E+OO 7. 961E-01 RA-226 6.544E-01 1.383E-01 9.840E-02 AC-228 5.294E-01 2.280E-01 2.060E-01 RA-228 5.294E-01 2.280E-01 2.060E-01 TH-228 7.363E-01 l.020E-01 7.430E-02 TH-230 6.541E-01 1.382E-01 9.837E-02 TH-232 5.294E-01 2.280E-01 2.060E-01 U-234 6.541E-01 1.382E-01 9.837E-02 U-235 -2.847E-02 1.491E-01 2.793E-01 AM-243 1. 280E-01 8 .136E-02 6.750E-02 ANH-511 2.085E-02 6.386E-02 3.988E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) . (pCi/GRAM BE-7 9.094E-01 9.337E+OO 1.918E+Ol NOT IDENT. NA-22 -l.468E-02 2.842E-02 4.947E-02 NOT IDENT. NA-24 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF AL-26 6.821E-04 2.041E-02 4.558E-02 NOT IDENT. SC-46 2.276E-01 2.941E-01 6.lOOE-01 FAIL ABUN V-48 O.OOOE+OO 5.505E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.635E+02 O.OOOE+OO SHORT HLIF MN-54 4.316E-02 4.434E-02 9.957E-02 NOT IDENT. Page 4311 of 5809 C0-56 l.033E-01 3.510E-01 7. 251E-01 FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 4.277E-03 3.403E-02 6.743E-02 NOT IDENT. C0-58 5.487E-02 3.594E-01 7.535E-01 NOT IDENT. FE-59 -2.740E+OO 5.065E+OO 8.886E+OO NOT IDENT. C0-60 -7.006E-03 3.288E-02 6.029E-02 NOT IDENT. ZN-65 2.254E-02 1.305E-01 2.364E-01 NOT IDENT. GE-68 -4.440E-01 1. 798E+OO 3.335E+OO NOT IDENT. AS-73 4.681E+OO 6.756E+OO 1.454E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.841E+03 O.OOOE+OO SHORT HLIF SE-75 1.286E-01 1.656E-01 3.349E-01 FAIL ABUN BR-77 O.OOOE+OO 1.859E+38 O.OOOE+OO SHORT HLIF SR--'82 O.OOOE+OO 6.413E+02 O.OOOE+OO SHORT HLIF RB-83 1.582E-01 4.759E-01 1.002E+OO NOT IDENT. KR-85 3.418E-01 5.153E+OO 9.424E+OO NOT IDENT. SR-85 3.880E-02 5.918E-01 1.082E+OO NOT IDENT. RB-86 O.OOOE+OO 2.904E+04 O.OOOE+OO SHORT HLIF Y-88 1.079E-02 1.566E-01 3.510E-01 NOT IDENT. Y-91 -l.819E+02 4.831E+02 8.560E+02 NOT IDENT. NB-94 6.682E-03 2 .111E-02 4.379E-02 NOT IDENT. NB-95 -2.330E-01 7.290E-01 l.205E+OO NOT IDENT. NB-95M 1.479E+OO 2.217E+OO 4.075E+OO NOT IDENT. ZR-95 l.124E+OO 1.698E+OO 2.308E+OO FAIL ABUN NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 8.295E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.480E+41 O.OOOE+OO SHORT HLIF RH-101' O.OOOE+OO 7.055E-02 5.013E-02 FAIL ABUN RH-102 4.599E-02 3.920E-02 9.085E-02 NOT IDENT. RU-103 -3.314E+OO 4.665E+OO 8.641E+OO FAIL ABUN RH-106 4.064E-02 3.430E-01 7.0lOE-01 NOT IDENT. RU-106 4.064E-02 3.430E-01 7.0lOE-01 NOT IDENT. AG-108M 8. 960E-03 1.862E-02 3. 996E-02 NOT IDENT. AG-110M -l.036E-02 7.142E-02 l.380E-01 NOT IDENT. SN-113 1.274E-01 l.557E-01 3.462E-01 NOT IDENT. CD-115 O.OOOE+OO 2 .181E+40 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 4.072E+05 O.OOOE+OO SHORT HLIF SB-124 -5.048E-01 1.334E+OO 2.677E+OO NOT IDENT. SB-125 l.686E-03 7 .121E-02 l.455E-01 FAIL ABUN TE-125M 1.314E+Ol 2.277E+02 4.490E+02 NOT IDENT. I-126 O.OOOE+OO 9.963E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.227E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 8.784E+22 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 6.253E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO l.650E+27 0.000E+OO SHORT HLIF BA-133 -1.667E-03 2.947E-02 5.432E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 8.629E-02 7.241E-02 9. 031E-02 FAIL ABUN CS-135 -7.265E-02 1.lOOE-01 1.910E-01 NOT IDENT. I-135 O.OOOE+OO 7. 372E+40 0.000E+OO SHORT HLIF CS-136 O.OOOE+OO 3.324E+05 O.OOOE+OO SHORT HLIF CE-139 -6.776E-03 9.510E-02 1.668E-01 NOT IDENT. BA-140 O.OOOE+OO 1.469E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.049E+05 0.000E+OO SHORT HLIF CE-141 3.839E+00 2.286E+Ol 4.447E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.806E+41 O.OOOE+OO SHORT HLIF CE-144 -4.504E-02 2.679E-01 5.138E-01 NOT IDENT. PM-144 -6.136E-04 4.134E-02 8.140E-02 NOT IDENT. PR-144 -6.429E-02 3.605E+OO 7.094E+00 NOT IDENT. PM-146 -2.209E-02 2.514E-02 4.586E-02 NOT IDENT. ND-147 O.OOOE+OO 3.356E+07 O.OOOE+OO SHORT HLIF PM-147 -5.927E-01 6.148E+02 l.202E+03 NOT IDENT. PM-149 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF EU-150 2.388E-02 2.780E-02 3.802E-02 FAIL ABUN EU-152 l.248E-02 6.054E-02 1. 272E-01 FAIL ABUN GD-153 -1. 710E-02 1.401E-01 2.538E-01 NOT IDENT. EU-154 -3.249E-02 7.015E-02 1.240E-01 FAIL ABUN E0-155 4.094E-02 8.398E-02 1. 705E-01 FAIL ABUN TB-160 -8.481E-01 1.164E+OO 2.009E+OO FAIL ABUN H0-166M 4.695E-02 6.660E-02 8.460E-02 FAIL ABUN TM-171 1.623E+OO 1.449E+Ol 3.014E+Ol NOT IDENT. HF-172 l.635E-01 1.695E-01 3.358E-01 FAIL ABUN LU-172 1. 780E-02 5.510E-02 1.130E-01 FAIL ABUN LU-176 -2.430E-02 1.933E-02 3.043E-02 FAIL ABUN HF-181 -8.918E-01 3.035E+00 6.002E+OO NOT IDENT. TA-182 -5.704E-01 7.761E-01 1.283E+OO FAIL ABUN RE-183 7.041E-01 2.223E+OO 4.656E+OO NOT IDENT. Page 4312 of 5809 RE-184 -1.718E+01 2.791E+Ol 4.908E+Ol FAIL ABUN W-188 9.367E+00 8.920E+Ol l.566E+02 NOT IDENT. IR-192 1. 371E-01 3.548E-01 6.946E-01 FAIL ABUN HG-203 2. 471E-01 2.085E+OO 3.934E+OO NOT IDENT. BI-207 4.148E-03 2.953E-02 6.034E-02 FAIL ABUN PB-210 -1. 07 5E+00 2.373E+OO 4.790E+OO NOT IDENT. BI-211 O.OOOE+OO 4.329E-01 6.209E-01 FAIL ABUN PB-211 6.406E-01 9.241E-01 l.076E+OO FAIL ABUN BI-212 7.755E-01 8.917E-01 9.038E-01 FAIL ABUN RN-219 3.362E-01 4.468E-01 4.997E-01 FAIL ABUN RA-223 -1.952E-01 4.837E-01 8.512E-01 FAIL ABUN AC-227 4.606E-02 l.642E-01 3.185E-01 FAIL ABUN TH-227 4.606E-02 l.642E-01 3.185E-01 FAIL ABUN TH-229 6.036E-01 8.236E-01 6.840E-01 FAIL ABUN PA-231 -1.822E-01 3.419E-01 5.962E-01 NOT IDENT. TH-231 -1.952E-01 4.837E-01 8.512E-01 FAIL ABUN PA-233 2.428E-02 4.514E-02 8.861E-02 NOT IDENT. PA-234 -2.679E-02 1. 968E-01 3.775E-01 NOT IDENT. PA-234M 2.492E+OO 3.870E+OO 6.166E+OO FAIL ABUN TH-234 8.227E-01 9.835E-01 2.126E+OO FAIL ABUN NP-237 2.428E-02 4.514E-02 8.861E-02 NOT IDENT. NP-238 O.OOOE+OO l.358E+41 0.000E+OO SHORT HLIF U-238 8.227E-01 9.835E-01 2.126E+OO FAIL ABUN NP-239 -3.416E-02 l.776E-01 3.430E-01 NOT IDENT. PU-239 O.OOOE+OO 6.370E+02 4.999E+02 FAIL ABUN AM-241 -6.995E-02 9.698E-02 l.877E-01 NOT IDENT. CM-243 -6.220E-02 7.506E-02 l.388E-01 NOT IDENT. BK-247 2. 966E-02 5'.635E-02 1. llOE-01 FAIL ABUN CM-247 3.387E-03 2.860E-02 4.380E-02 NOT IDENT. CF-249 -2.697E-02 2.478E-02 4.482E-02 FAIL ABUN CF-251 4.046E-02 8.095E-02 1.621E-01 NOT IDENT. Page 4313 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 08:56:40.12 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 465 10.66* 1.347E+OO 1.339E+Ol 1.339E+Ol 9.73 CD-109 88.03 132 3.70* 6.242E+OO 2.371E+OO 3.765E+OO 42.83 TE-123M 159.00 66 84.00* 6.985E+OO 4.621E-02 2.767E-01 142.35 SN-126 64.28 ------9.60 3.737E+00 ------Line Not Found ------86.94 132 8.90 6.242E+OO 9.857E-01 9.857E-01 42.83 87.57 132 37.00* 6.242E+OO 2.371E-01 2. 371E-01 42.83 BA-137M 661. 66 28 89.90* 2.518E+OO 5. 071E-02 5.170E-02 114 .17 CS-137 661. 66 28 85.10* 2.518E+OO 5.357E-02 5.462E-02 114 .17 TL-208 277.37 ------6.60 4.914E+OO ------Line Not Found ------583.19 131 85.00* 2. 771E+OO 2.297E-01 2.297E-01 31. 44 860.56 25 12.50 2.069E+00 3.998E-01 3.998E-01 98.91 BI-211 72. 87 ------1. 23 4.875E+OO ------Line Not Found ------351.06 328 12.92* 4.087E+OO 2.572E+OO 2.572E+OO 17.17 PB-212 74.82 176 10.28 5.108E+00 1.390E+OO 1.390E+OO 37.69 77 .11 263 17.10 5.368E+OO 1.187E+OO l.187E+00 29.14 238.63 426 43. 60'* 5.496E+OO 7.363E-01 7.363E-01 14.13 300.09 ------3.30 4.626E+OO ------Line Not Found ------BI-214 609.32 193 45.49* 2.683E+00 6. 541E-01 6.544E-01 21. 56 1120. 29 53 14.92 1.685E+OO . 8. 658E-01 8.661E-01 46.46 1764.49 31 15.30 l.129E+OO 7.309E-01 7. 311E-01 39.34 PB-214 74.82 176 5.80 5.108E+OO 2.463E+OO 2.464E+OO 37.69 77 .11 263 9.70 5.368E+OO 2.092E+OO 2.093E+00 29.14 87.09 132 3.41 6.242E+OO 2.573E+OO 2.574E+OO 42.83 242.00 107 7.25 5.449E+OO 1.117E+OO l. ll 7E+OO 55.24 295.22 204 18.42 4.685E+OO 9. 801E-01 9.805E-01 25.67 351. 93 328 35.60* 4.087E+OO 9.335E-01 9.338E-01 17 .17 RN-222 609.32 193 45.49* 2.683E+OO 6.541E-01 6.544E-01 21. 56 1120. 29 53 14.92 1.685E+OO 8.658E-01 8. 661E-01 46.46 1764.49 31 15.30 l.129E+OO 7.309E-01 7. 311E-01 39.34 RA-224 240.99 107 4.10* 5.449E+OO 1. 974E+OO l.974E+00 55.24 RA-226 609.32 193 45.49* 2.683E+OO 6. 541E-01 6.544E-01 21. 56 1120.29 53 14.92 1.685E+OO 8.658E-01 8.661E-01 46.46 1764.49 31 15.30 l.129E+OO 7.309E-01 7. 311E-01 39.34 AC-228 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 108 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 794.95 30 4.25 2.196E+OO 1.309E+OO l.309E+OO 85.63 835. 71 ------1. 61 2 .116E+OO ------Line Not Found ------911. 20 65 25.80* 1. 981E+OO 5.294E-01 5.294E-01 43.94 968. 97 49 15.80 1.890E+OO 6.731E-01 6.731E-01 48.20 RA-228 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 108 11. 27 4.214E+OO 9.416E-01 9.416E-01 38.45 794.95 30 4.25 2 .196E+OO l.309E+OO 1.309E+OO 85.63 835. 71 ------1. 61 2 .116E+OO ------Line Not Found ------911. 20 65 25.80* 1.981E+OO 5.294E-01 5.294E-01 43.94 968. 97 49 15.80 1. 890E+OO 6. 731E-01 6. 731E-01 48.20 TH-228 74.82 176 10.28 5.108E+OO 1.390E+OO 1. 390E+OO 37.69 77 .11 263 17.10 5.368E+OO l.187E+OO 1.187E+OO 29.14 Page 4314 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : Gl203621362 Acquisition date 3-0CT-2016 07:54:00 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Ef f pCi/GRAM pCi/GRAM %Error 238.63 426 43.60* 5. 4,96E+OO 7.363E-01 7.363E-01 14.13 300.09 ------3.30 4.626E+OO ------Line Not Found ------TH-230 609.32 193 45.49* 2.683E+OO 6.541E-01 6. 541E-Ol 21. 56 1120.29 53 14.92 l.685E+OO 8.658E-01 8.658E-01 46.46 1764.49 31 15.30 l.129E+OO 7.309E-01 7.309E-Ol 39.34 TH-232 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 108 11.27 4.214E+OO 9.416E-01 9.416E-01 38.45 835. 71 ------1. 61 2 .116E+OO ------Line Not Found ------911.20 65 25.80* l.981E+OO 5.294E-01 5.294E-01 43.94 968. 97 49 15.80 l.890E+OO 6. 731E-01 6.731E-01 48.20 U-234 609.32 193 45.49* 2.683E+OO 6.541E-01 6. 541E-01 21. 56 1120.29 53 14.92 1. 685E+OO 8.658E-01 8.658E-01 46.46 1764.49 31 15.30 l.129E+OO 7.309E-01 7.309E-01 39.34 U-235 89. 96 63 3.47 6.473E+OO l.167E+OO l.167E+OO 103.23 93.35 135 5.60 6.639E+OO l.505E+OO l.505E+OO 44.72 143.76 ------10. 96* 7.247E+OO ------Line Not Found ------163.33 ------5.08 6.922E+OO ------Line Not Found ------185.72 70 57.20 6.471E+OO 7.775E-02 7.775E-02 90.32 205:31 ------5.01 6.095E+OO ------Lirie Not Found ------AM-243 43.53 ------5.90 7.707E-Ol ------Line Not Found ------74 .. 66 176 67.20* 5.108E+OO 2.126E-01 2.126E-01 37.69 ANH-511 511. 00 15 100.00* 3.065E+OO 2.085E-02 2.085E-02 312.60 Flag: "*" Key line Page 4315 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G1203621362 Acquisition date 3-0CT-2016 07:54:00 Total number of lines in spectrum 58 Number of unidentified lines 15 Number of lines tentatively identified by NID 43 Nuclide Type : Nuclide K-40 ,CD-109 TE-123M SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Hlife 1.25E+09Y 461. 40D 119.20D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 7.04E+08Y 1. 41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600.00Y 1.41E+10Y 1. 41E+10Y. 1.41E+10Y 7.54E+04Y 1. 41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 59 5.99 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.339E+Ol 2.371E+OO 4. 621E-02 2. 371E-01 5. 071E-02 5.357E-02 2.297E-01 2.572E+OO 7.363E-01 6. 541E-01 9.335E-01 6. 541E-:-Ol 1.974E+OO 6.541E-01 5.294E-01 5.294E-01 7.363E-01 6.541E-01 5.294E-01 6.541E-01 7.775E-02 2.126E-01 2.085E-02 2.850E+01 2.850E+Ol
  • Decay Corr pCi/GRAM 1. 339E+Ol 3.765E+OO 2.767E-01 2. 371E-01 5.170E-02 5.462E-02 2.297E-01 2. 572E+OO 7.363E-01 6.544E-01 9.338E-01 6.544E-01 1.974E+OO 6.544E-01 5.294E-01 5.294E-01 7.363E-01 6. 541E-01 5.294E-01 6. 541E-01 7.775E-02 2.126E-01 2.085E-02 3.013E+Ol 3. 013E+Ol 74.14% Decay Corr 2-Sigma Error 0.130E+Ol 1.612E+OO 3.939E-01 l.015E-01 5.903E-02 6.236E-02 0.722E-01 0.442E+OO 1.041E-01 1.411E-01 1.604E-01
  • 1. 411E-01 l.091E+OO 1. 411E-01 2.327E-01 2.327E-01 l.041E-01 l.410E-01 2.327E-01 l.410E-01 7.022E-02 0.801E-01 6.516E-02 "M" Manually accepted 2-Sigma %Error 9.73 42.83 142.35 42.83 114 .17 114 .17 31. 44 17.17 14 .13 21. 56 17.17 21. 56 55.24 21. 56 43.94 43.94 14.13 21. 56 43.94 21. 56 90.32 37.69 312.60 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4316of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : Gl203621362 Acquisition date : 3-0CT-2016 07:54:00 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 84.04 53 211 1.16 167.99 165 7 l.OlE-02 **** 6.02E+OO T 0 128.29 85 235 1. 37 256.36 251 11 l.71E-02 86.6 7.39E+OO T 0 194.46 41 152 1. 33 388.54 383 10 8.61E-03 **** 6. 31E+OO T 3 207.21 36
  • 40 1. 23 414.00 412 12 7.66E-03 63.2 3 209.20 70 129 1. 55 417.97 412 12 l.51E-02 74.0 6.02E+OO 0 329.40 14 85 0.49 658.10 652 8 3.28E-03 **** 4.30E+OO T 0 334.02 23 46 1. 24 667.34 665 7 5.28E-03 **** 4.26E+OO T 0 397.75 8 35 1. 24 794.65 790 7 1.82E-03 **** 3. 72E+OO 0 400.82 20 41 3.16 800.79 796 9 4.62E-03 **** 3.69E+OO T 0 405.54 21 54 0.67 810.22 805 10 5.00E-03 **** 3.66E+OO T 0 463.19 37 39 2.50 925.42 922 9 8.81E-03 74.9 3.30E+OO T 0 547.02 12 33 0.74 1092.97 1089 9 2.95E-03 **** 2. 91E+OO T 0 684.20 13 16 1. 02 1367 .17 1363 8 3.18E-03 **** 2.46E+OO T 3 709.15 13 5 1. 40 1417.06 1415 22 3.18E-03 80.1 2.39E+OO 3 712.16 15 20 1. 80 1423.06 1415 22 3.70E-03 **** 2.39E+OO T 0 727.66 29 48 0.78 1454.05 1446 16 7.44E-03 **** 2.35E+OO T 0 750.81 16 10 1.16 1500.33 1496 8 4.lOE-03 89.9 2.29E+OO 0 757.59 12 17 0.52 1513.91 1506 11 3.07E-03 **** 2.28E+00 T 0 768.46 20 33 3.80 1535.63 1528 12 5.23E-03 **** 2.25E+OO 0 894.62 16 13 1. 44 1787.89 1782 11 4.06E-03 **** 2.0lE+OO T 0 915.66 15 6 1. 47 1829.98 1827 8 4.06E-03 77.5 1. 97E+OO 0 934 .11 22 12 2.04 1866. 87. 1860 11 5. 68E-03 81. 0 1.94E+OO 0 955.28 8 9 0.69 1909.21 1902 9 2.23E-03 **** 1. 91E+OO T 2 964.83 23 11 1. 94 1928.33 1924 24 6.14E-03 76.8 1.90E+OO T 0 984.31 29 43 7.88 1967.27 1951 26 7.65E-03 **** 1.87E+OO T 0 1000.59 9 10 0.87 1999.84 1994 10 2.48E-03 **** 1.84E+OO T 0 1170.26 9 17 1. 84 2339.27 2333 10 2.48E-03 **** 1.63E+OO 0 1238.99 16 33 1. 39 2476.79 2469 13 4.39E-03 **** 1.55E+OO T 0 1327.38 6 10 0.56 2653.67 2647 10 l.61E-03 **** 1.46E+OO 0 1377.71 14 2 0.98 2754.40 2750 9 4.05E-03 69.5 1. 42E+OO 0 1395.69 6 4 0.64 2790.38 2785 9 l.81E-03 **** 1. 40E+OO 0 1408.25 7 9 1.19 2815.51 2810 10 2.08E-03 **** 1.39E+OO T 0 1593.69 4 7 0.95 3186.75 3181 7 l.llE-03 **** 1.24E+OO 0 1730.19 14 3 1.12 3460.08 3454 9 3.98E-03 65.6 1.15E+OO 0 1846.28 9 0 1. 05 3692.60 3686 11 2.78E-03 63.2 1.08E+OO Flags: "T" = Tentatively associated Page 4317 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:56:57.15 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621362.CNF;l *
  • Acquisition date 3-0CT-2016 07:54:00 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:27:00 Nuclide Library : SOLID *
  • Sample ID G1203621362 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN * '* Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 TE-123M SN-126 BA-137M CS-137 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 2.140E-01 6.756E-01 8.596E-02 4.277E-02 2.002E-02 2 .115E-02 2.365E-02 3.463E-02 4.440E-02 3.925E-02 4.440E-02 3.711E-01 4.440E-02 9.169E-02 9.169E-02 3.463E-02 4.438E-02 9.169E-02 4.438E-02 1.319E-01 3 .191E-02 1.801E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4318 of 5809 Le (pCi/GRAM 8.621E+OO 2. OOlE-02 O.OOOE+OO 1. 766E-02 2.684E-01 O.OOOE+OO O.OOOE+OO 4.436E-02 3.187E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-7 5 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page4319of5809 O.OOOE+OO 3.157E-02 3.219E-01 3. 725E+00 2.579E-02 1. 021E-01 1.442E+00 6.857E+OO O.OOOE+OO 1.555E-01 O.OOOE+OO O.OOOE+OO 4.497E-01 4.241E+00 4. 871E-01 O.OOOE+OO 1.368E-01 3.749E+02 1.947E-02 5.304E-01 l.914E+OO l.023E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.360E-02 4.075E-02 3.845E+OO 3.108E-01 3.108E-01 l.809E-02 5.977E-02 1. 57 5E-01 O.OOOE+OO O.OOOE+OO 9.889E-01 6.576E-02 2 .115E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 2.465E-02 O.OOOE+OO 4.106E-02 8. 801E-02 O.OOOE+OO O.OOOE+OO 7.815E-02 O.OOOE+OO O.OOOE+OO 2.099E+Ol O.OOOE+OO 2.409E-01 3.635E-02 3.168E+OO 1.991E-02 O.OOOE+OO 5.646E+02 O.OOOE+OO 1. 7 53E-02 5.798E-02 l .193E.:..01 5.045E-02 8.062E-02 8.238E-01 3.779E-02 1.413E+Ol l.578E-01 4.927E-02 1. 381E-02 2.649E+OO 5.546E-01 2.189E+OO 2.139E+Ol SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN 'NOT I DENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4320 of 5809 7.157E+Ol 3.179E-01 1.820E+OO 2.570E-02 2.260E+OO 2.993E-01 4.950E-01 4.148E-01 2.254E-01 3.912E-01 1. 471E-01 1.471E-01 3.202E-01 2.738E-01 3.912E-01 4.084E-02 1.638E-01 2.711E+OO 1.016E+OO 4.084E-02 O.OOOE+OO 1.016E+OO 1.609E-01 2.367E+02 8.805E-02 6. 513E-02 5.154E-02 1. 966E-02 2.002E-02 7.572E-02 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 08:57:04.76 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621362.CNF;l *
  • Acquisition date 3-0CT-2016 07:54:00 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.45 Half life ratio : ***** *
  • Sample date 30-NOV-2015 13:27:00 Nuclide Library : SOLID *
  • Sample ID G1203621362 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.8148E+02 GRAM *
  • Quantity Err(%) : 1.1020E-03 % *
  • Wet wt corr 1.00000 Wet : 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1. 339E+Ol l.456E+OO 1.456E+OO CD-109 2.330E+OO 1.642E+OO 1.642E+OO TE-123M 2.767E-01 3.862E-01 3.862E-01 SN-126 1. 4 68E-01 1. 031E-01 1. 031E-01 BA-137M 5.170E-02 5.789E-02 5.789E-02 CS-137 5.462E-02 6 .116E-02 6 .116E-02 TL-208 2.297E-01 7.146E-02 7.146E-02 PB-212 7.363E-01 1.092E-01 l.092E-01 BI-214 6.544E-01 1. 411E-01 1. 411E-01 PB-214 9.338E-01 1.619E-01 l.619E-01 RN-222 6.544E-01 l.411E-01 1.411E-01 RA-224 2.414E-01 1.160E+OO 1.160E+OO RA-226 6.544E-01 1. 411E-01 1. 411E-01 AC-228 5.294E-01 2.296E-01 2.296E-01 RA-228 5.294E-01 2.296E-01 2.296E-01 TH-228 7.363E-01 1.092E-01 1.092E-01 TH-230 6. 541E-01 1. 411E-01 l.411E-01 TH-232 5.294E-01 2.296E-01 2.296E-01 U-234 6.541E-01 1. 411E-01 l.411E-01 U-235 -2.847E-02 l.491E-01 1.491E-01 AM-243 1.280E-01 8.244E-02 8.244E-02 ANH-511 2.085E-02 6.387E-02 6.387E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 9.094E-01 9.338E+OO 9.347E+OO NOT IDENT. NA-22 -1. 468E-02 2.842E-02 2.918E-02 NOT IDENT. NA-24 1. OOOE+41 3.468E+41 O.OOOE+OO SHORT HLIF AL-26 6.821E-04 2.041E-02 2. 041E-02 NOT IDENT. SC-46 2.276E-01 2.942E-01 3.116E-01 FAIL ABUN V-48 4.053E+04 5.507E+04 5.803E+04 SHORT HLIF CR-51 9.687E+Ol 3.635E+02 3.661E+02 SHORT HLIF MN-54 4.316E-02 4.438E-02 4.846E-02 NOT IDENT. Page 4321of5809 C0-56 1.033E-01 3.510E-01 3. 541E-01 FAIL ABUN MN-56 1.000E+41 3.321E+41 0.000E+OO SHORT HLIF C0-57 4.277E-03 3.403E-02 3.409E-02 NOT IDENT. C0-58 5.487E-02 3.594E-01 3.603E-01 NOT IDENT. FE-59 -2.740E+OO 5.069E+OO 5.217E+OO NOT IDENT. C0-60 -7.006E-03 3.288E-02 3.304E-02 NOT IDENT. ZN-65 2.254E-02 l.305E-01 l.309E-01 NOT IDENT. GE-68 -4.440E-01 l.798E+OO 1.809E+OO NOT IDENT. AS-73 4.681E+OO 6.824E+OO 7.143E+OO NOT IDENT. AS-74 1. 611E+03 5.843E+03 5.887E+03 SHORT HLIF SE-75 1.286E-01 l.657E-01 1.755E-01 FAIL ABUN BR-77 1.342E+39 1.192E+40 O.OOOE+OO SHORT HLIF SR-82 1.332E+Ol 6.413E+02 6.413E+02 SHORT HLIF RB-83 1.582E-01 4.764E-01 4.817E-01 NOT IDENT. KR-85 3.418E-01 5.153E+OO 5.155E+OO NOT IDENT. SR-85 3.880E-02 5.918E-01 5.920E-01 NOT IDENT. RB-86 -l.577E+04 2.904E+04 2.990E+04 SHORT HLIF Y-88 1.079E-02 1.566E-01 1.566E-01 NOT IDENT. Y-91 -1. 819E+o2 4.831E+02 4.900E+02 NOT IDENT. NB-94 6.682E-03 2. lllE-02 2.132E-02 NOT IDENT. NB-95 -2.330E-01 7.290E-01 7.366E-01 NOT IDENT. NB-95M 1.479E+OO 2.220E+00 2.318E+OO NOT IDENT. ZR-95 1.124E+OO 1.699E+OO 1.773E+OO FAIL ABUN NB-97 l.OOOE+41 7.605E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 2.077E+41 O.OOOE+OO SHORT HLIF M0-99 4.417E+32 8. 301E+32 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.483E+41 O.OOOE+OO SHORT HLIF RH-101 8.318E-02 7.214E-02 8 .131E-02 FAIL ABUN RH-102 4.599E-02 3.938E-02 4.450E-02 NOT IDENT. RU-103 -3.314E+OO 4.668E+OO 4. 901E+OO FAIL ABUN RH-106 4.064E-02 3.430E-01 3.435E-01 NOT IDENT. RU-106 4.064E-02 3.430E-01 3.435E-01 NOT IDENT. AG-108M 8. 960E-03 1. 8 62E-02 l.906E-02 NOT IDENT. AG-llOM -1.036E-02 7.142E-02 7.157E-02 NOT IDENT. SN-113 1.274E-01 1.558E-01 1.660E-01 NOT IDENT. CD-115 -l.050E+39 2.181E+40 O.OOOE+OO SHORT HLIF SN-ll 7M 2.919E+05 4.088E+05 4.294E+05 SHORT HLIF SB-124 -5.048E-01 1.334E+OO 1.354E+OO NOT IDENT. SB-125 1. 68 6E-03 7.122E-02 7.122E-02 FAIL ABUN TE-125M 1.314E+Ol 2.277E+02 2.278E+02 NOT IDENT. I-126 3.437E+05 9.975E+05 1.009E+06 SHORT HLIF SB-126 l.948E+06 1.282E+06 l.554E+06 SHORT HLIF SB-127 6.744E+22 l.295E+23 O.OOOE+OO SHORT HLIF I-131 2.067E+09 6.253E+09 6.322E+09 SHORT HLIF I-132 1.000E+41 1.931E+42 O.OOOE+OO SHORT HLIF TE-132 8.806E+25 l.651E+27 O.OOOE+OO SHORT HLIF BA-133 -1.667E-03 2.947E-02 2.948E-02 NOT IDENT. I-133 l.000E+41 3.076E+41 O.OOOE+OO SHORT HLIF CS-134 8.629E-02 7.251E-02 8.228E-02 FAIL ABUN CS-135 -7.265E-02 l.lOlE-01 1.149E-01 NOT IDENT. I-135 -1.000E+41 6.993E+41 O.OOOE+OO SHORT HLIF CS-136 -l.218E+05 3.326E+05 3. 371E+05 SHORT HLIF CE-139 -6.776E-03 9. 511E-02 9.516E-02 NOT IDENT. BA-140 5.208E+05 l.469E+06 1.487E+06 SHORT HLIF LA-140 -1. 57 9E+05 4.049E+05 4 .112E+05 SHORT HLIF CE-141 3.839E+OO 2.286E+Ol 2.292E+Ol NOT IDENT. CE-143 1.000E+41 1.809E+41 O.OOOE+OO SHORT HLIF CE-144 -4.504E-02 2.679E-01 2.687E-01 NOT IDENT. PM-144 -6.136E-04 4.134E-02 4 .134E-02 NOT IDENT. PR-144 -6.429E-02 3.605E+OO 3.605E+OO NOT IDENT. PM-146 -2.209E-02 2.519E-02 2.709E-02 NOT IDENT. ND-147 2.020E+06 3.356E+07 3.358E+07 SHORT HLIF PM-147 -5.927E-01 6.148E+02 6.148E+02 NOT IDENT. PM-149 -l.993E+40 4.142E+41 O.OOOE+OO SHORT HLIF EU-150 2.388E-02 2.782E-02 2.983E-02 FAIL ABUN EU-152 l.248E-02 6.055E-02 6. 0'81E-02 FAIL ABUN GD-153 -1.710E-02 1. 401E-01 l.404E-01 NOT IDENT. EU-154 -3.249E-02 7.016E-02 7.167E-02 FAIL ABUN EU-155 4.094E-02 8.403E-02 8.603E-02 FAIL ABUN TB-160 -8.481E-01 1.165E+OO 1. 226E+OO FAIL ABUN H0-166M 4.695E-02 6.665E-02 6.993E-02 FAIL ABUN TM-171 1.623E+OO 1.449E+Ol 1.450E+Ol NOT IDENT. HF-172 l.635E-01 1. 716E-01 1. 867E-01 FAIL ABUN LU-172 1. 780E-02 5.513E-02 5. 571E-02 FAIL ABUN LU-176 -2.430E-02 1.936E-02 2.225E-02 FAIL ABUN HF-181 -8.918E-01 3.035E+OO 3.062E+OO NOT IDENT. TA-182 -5.704E-01 7.764E-01 8.179E-01 FAIL ABUN RE-183 7. 041E-01 2.226E+OO 2.248E+OO NOT IDENT. Page 4322 of 5809 RE-184 -1.718E+Ol 2.822E+Ol 2.927E+Ol FAIL ABUN W-188 9.367E+00 8.921E+Ol 8.931E+Ol NOT IDENT. IR-192 1. 371E-01 3.549E-01 3.602E-01 FAIL ABUN HG-203 2.471E-01 2.085E+OO 2.088E+OO NOT IDENT. BI-207 4.148E-03 2.953E-02 2.959E-02 FAIL ABUN PB-210 -1. 07 5E+00 2.375E+OO 2.424E+OO NOT IDENT. BI-211 2. 572E+OO 4.479E-01 l.243E+OO FAIL ABUN PB-211 6.406E-01 9.247E-01 9.687E-01 FAIL ABUN BI-212 7.755E-01 8.926E-Ol 9.586E-01 FAIL ABUN RN-219 3 . .;362E-01 4.487E-Ol 4.736E-01 FAIL ABUN RA-223 -l.952E-01 4.839E-Ol 4.918E-Ol FAIL ABUN AC-227 4.606E-02 l.643E-Ol l.656E-01 FAIL ABUN TH-227 4.606E-02 l.643E-Ol l.656E-01 FAIL ABUN TH-229 6.036E-01 8.241E-01 8.679E-01 FAIL ABUN PA-231 -1.822E-01 3.441E-Ol 3.537E-01 NOT IDENT. TH-231 -l.952E-01 4.839E-Ol 4.918E-01 FAIL ABUN PA-233 2.428E-02 4.515E-02 4.646E-02 NOT IDENT. PA-234 -2.679E-02 l.991E-01 l.995E-01 NOT IDENT. PA-234M 2.492E+OO 3.871E+OO 4.031E+OO FAIL ABUN TH-234 8.227E-01 1.000E+OO 1.067E+OO FAIL ABUN NP-237 2.428E-02 4.515E-02 4.646E-02 NOT IDENT. NP-238 l.000E+41 l.359E+41 O.OOOE+OO SHORT HLIF U-238 8.227E-01 1.000E+OO 1.067E+OO FAIL ABUN NP-239 -3.416E-02 1. 776E-01 l.783E-01 NOT IDENT. PU-239 7.510E+02 6.378E+02 7.221E+02 FAIL ABUN AM-241 -6.995E-02 9.712E-02 1. 021E-01 NOT IDENT. CM-243 -6.220E-02 7.529E-02 8.034E-02 NOT IDENT. BK-247 2. 966E-02 5.666E-02 5.822E-02 FAIL ABUN CM-247 3.387E-03 2.861E-02 2.865E-02 NOT IDENT. CF-249 -2.697E-02 2.488E-02 2.769E-02 FAIL ABUN. CF-251 4.046E-02 8.107E-02 8.310E-02 NOT IDENT. Page 4323 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 79.8228 87.09 84.5897 136.47 72.7609 45.60 90.6690 87.57 84.6464 140.51 0.0000 46.54 87.9756 88.03 84.7007 143.76 94.1019 49.72 0.0000 88.34 84.7372 144.24 81. 0109 51.35 81. 0969 88.47 84.7524 145.44 89.8777 51. 87 83 .1107 89.96 84.9265 152.43 77.2600 52.39 73.5198 1093.63 85.0053 153.25 0.0000 52.97 80.3800 91.11 0.0000 323.87 70.7607 53.44 73.6662 92.59 85.2301 156.02 0.0000 54.07 78.6056 93.35 85.3168 158.56 0.0000 57.36 0.0000 94.56 85.4550 159.00 63.3127 57.53 76.1766 94.65 85.4651 162.33 63.5127 57.98 75.2608 94. 67 85.4676 162.66 0.0000 59.27 87.1897 94.87 85.4897 163.33 63.5718 59.32 95.0355 97.43 85.7779 165.86 76.0196 59.54 95.0725 98.43 85.8895 176.31 72. 2305 60. 96 103.1699 98.44 85.8908 176.60 0.0000 61.17 103.2076 99.53 86.0112 177.52 56.4903 62.93 110.4218 100 .11 86.0756 181.07 0.0000 63.29 99.6382 102.03 75.1525 181.52 72. 5625 63.58 99.6871 103.18 89.1992 184.41 86.3848 64.28 129.4501 103.37 99.3270 143.76 85.3443 66.73 102.1977 105.21 82.7887 193.51 56.1284 67.24 109.2346 105.31 86.9913 197.03 59.7402 125.81 121. 238 6 106.12 84.9798 198.01 62.8547 67.75 121. 2516 106.47 90.2648 201. 83 71. 5096 69.67 97.7024 109.28 86.3624 203.43 69.2926 70.83 103.8762 111. 00 89.7081 205.31 60.1448 72.81 112. 2162 111.76 0.0000 210.85 74.3525 72. 87 112.2264 114.06 78.3836 215.65 64 .1384 74.66 100.4807 116. 30 0.0000 222 .11 65.6310 74.82 100.5051 116.74 81. 8178 227.09 62.3496 74.97 100.5280 119.76 78.9045 227.38 57.6566 77 .11 100.8560 121.12 79.0270 228.16 0.0000 78.74 101.1024 121. 22 79.0354 228.18 52.9823 79.69 95.8447 121.78 79.0857 116.74 52.9823 80.12 91.8530 122.06 69.4895 235.69 63.1445 80.19 0.0000 122.92 94.1694 235.96 63.1567 80.57 83.1280 123.07 87.7631 238.63 62.8849 81. 00 79.1229 265.00 62.8328 238.98 0.0000 81. 07 79.1313 125.81 57.2567 240.99 62.9925 81. 75 93.4263 127.23 90.3203 242.00 63.0386 83.79 96.4181 127.91 90.3882 244.70 54.0243 84.00 96.4470 129.30 90.5253 252.40 0.0000 85.43 77.5870 131.20 76.3137 252.80 47.9431 86.55 80.4360 133.02 76.8231 254.15 0.0000 86.79 80.4630 133.52 80.1121 256.23 43.2521 86.94 84.5720 136.00 68.3833 260.90 0.0000 Page 4324 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41. 0858 355.39 0.0000 584.27 30.2799 264.80 49.5496 356.01 33.2228 595.83 0.0000 265.00 45.9298 364.49 0.0000 427.87 19.0446 268.22 60.5667 366.42 0.0000 602.52 0.0000 269.46 56.9800 372. 51 32.6640 604. 72 28.6121
  • 270.03 44.8736 375.05 28 *. 4044 607.14 31.5015 271.23 57.0475 377.52 40.5082 609.32 28.6609 273.65 0.0000 356.01 38.0497 610.33 25.8047 276.40 41.4105 388.16 39.8682 614.28 25.8431 277.37 49.9675 388.63 0.0000 618.01 21. 08 69 277.60 49.9750 391. 69 22.5760 620. 36 18.2277 278.00 54.8657 264.66 26.1694 621.93 19.1984 279.20 48.8074 401.81 23.5662 630.19 0.0000 279.54 63.4639 402.40 23.5734 631. 2 9 11. 5586 279.70 63.4702 404.85 28.8475 633.25 23.1338 280.46 41. 5205 410.95 36.8278 634.78 0.0000 283.69 44.0552 413.71 32.4887 635.95 12.5435 284.31. 0.0000 414.70 0.0000 636.99 0.0000 285.41 52.6805 423.72 0.0000 645.85 15.4935 285.90 0.0000 427.09 33. 5871 657.76 21. 8811 287.50 39.2568 427.87 29.1791 657.90 0.0000 290.67 36.0579 433.94 23.9436 661.66 19.4767 293.27 0.0000 439.40 32.0090 664.57 0.0000 351.93 39.4492 453.88 25.0662 666.33 0.0000 295.96 32.8898 463.37 31. 4709 666.50 0.0000 879.38 39.5332 468.07 20.2748 667. 71 0.0000 299.98 37.0944 473.00 0.0000 677.62 12.7313 300.09 37.0972 475.06 25.3112 685.70 0.0000 300 .13 37.0981 476.78 20.8077 695.00 0.0000 301.36 53.2146 477.60 25.3403 696.49 23.6582 302.85 43.3537 482.18 22.6720 696.51 23.6582 256.23 27.2791 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.7069 306.78 57. 1182 497.08 31.9502 697.49 18.7356 308.46 27.3456 505.52 19.2406 702.65 17.7810 311. 90 33.6305 507.63 0.0000 706.68 10.3864 316.51 32.4754 511. 00 29.3880 711. 68 20.8077 319.41 0.0000 514.00 26.2073 720. 70 0.0000 320.08 0.0000 514.00 26.2073 721. 93 0.0000 321.04 40.0781 520.40 21. 2078 722.78 19.3937 323.87 51.4364 520.69 0.0000 722.91 20.8864 325.23 43.9444 522.65 0.0000 723.31 20.8889 328.76 0.0000 527.90 0.0000 724.19 23.8799 333.37 42.8922 528.26 17.5775 727.33 18.9250 333.97 40.3828 529.59 14.8099 733.00 16.4651 334.37 40.3926 529.87 0.0000 735.93 15.9818 338.28 32.8928 531. 02 0.0000 333.97 18.9876 338.32 32.8936 537.26 0.0000 739.50 0.0000 311. 90 32.9340 546.56 0.0000 747.24 15.0385 340.48 32.9340 552.55 26.1634 748.06 13.5379 340.55 0.0000 563.25 17.8303 752.31 9.0377 344.28 32.1591 569.33 31.0436 753.82 0.0000 345.93 33.0364 946.00 31.9871 756.73 15.6882 351.06 30.5830 569.70 31. 9884 756.80 15.6882 351.93 30.5984 583.19 30.2669 884.68 12.0957 Page 4325 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 22.6932 1274.44 21. 0171 1620.50 6.4706 766.42 22.1925 1001.03 14.5684 1621.92 5.5477 766.84 22 .1960 1002.74 16.1945 1678.03 0.0000 772.60 0.0000 1004.73 19.4436 1690.97 4. 6796 776.52 0.0000 507.63 0.0000 1750.46 0.0000 7.39. 50 0.0000 1025.87 0.0.000 1764.49 4.7385 778.90 21. 2683 1028.54 0.0000 1063.66 1.2648 783.70 0.0000 1037.84 11. 9838 1771. 35 3.7952 785.37 14.2074 1038.76 0.0000 1791.20 0.0000 792.07 19.8301 631.29 16.3770 1808.65 3.8188 794.95 18.3215 1048.07 0.0000 1810. 72 0.0000 795.86 18.3267 1049.04 18. 5716 1836.06 3.8359 810.06 15.3387 1050.41 4. 3714 810.29 15.3400 1063.66 9.8687 344.28 10.2271 1077.00 0.0000 810.76 10.2283 1077.34 16.5027 815.77 0.0000 1085.87 12.1279 1048.07 0.0000 1093.63 12.1503 832.01 22.6472 1099.45 14.3806 834.85 11. 3330 1112. 07 15.5335 835.71 12.3667 1112.84 15.5369 836.80 0.0000 1115. 54 11. 6595 846.75 0.0000 1120.29 16.6760 846.77 14.4751' 1120.55 16.6772 856.80 0.0000 1221. 41 16.6797 860.56 14.5338 1129. 67 13.3711 871.09 14.5788 1131.51 0.0000 873.19 13.5454 1147.95 0.0000 875.33 0.0000 1173.23 20.2617 879.38 13.5697 1177.95 19.1568 880.51 10.4415 1189.05 19.2052 883.24 7.3147 1204.77 21.5420 884.68 15.6812 1221.41 22.7604 889.28 9.4211 1231.02 20.5283 894.76 23.0653 1235.36 0.0000 898.04 15.7410 1238.28 18.2773 900.72 25.2041 1260.41 0.0000 903.28 22.0698 1271.87 8.0550 911.20 22 .1194 1274.44 10.3623 912.08 22.1245 1274.54 10.3630 923.98 0.0000 1291.59 12.7125 926.50 11.6356 1298.22 0.0000 929 .11 19.0540 1312 .11 0.0000 937.49 11.1404 1332.49 13.9883 944.13 0.0000 1362.66 0.0000 946.00 15.9515 1365.19 7.9222 949.00 12.7720 1368.63 0.0000 667.71 0.0000 1384.29 6.1857 962.31 11. 2156 1408.01 8.8788 964. 08 17.0983 1457.56 0.0000 966.17 17.1081 1460.82 9.8694 911. 20 17.1211 1489.16 9.9231 968.97 17.1211 1505.03 4.5242 983.53 0.0000 1584.12 3.6731 984.45 0.0000 1596.21 0.0000 Page 4326 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:01:10.66 ******************************************************************************** *
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621363.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM11.CNF;517 Background date : Z-OCT-2016 11:00:34. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 05:45:34. Sample ID G1203621363 Sample quantity 1.15000E+02 GRAM Detector name : GAMll Detector geometry: CAN Elapsed live time: 0 00:15:00.00 Elapsed real time: 0 00:15:06.48 0.7% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596252 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 46.43* 58.09 59.50 79.25 83.11* 87.94 122.04 279.02* 346.35 351.38* 484.34 523.51 661.65* 747.77 754.57 812.46 950.54 962. 27* 1116.17 1121. 69* 1173.30 1248.71 1332.59* 1529.97 1609.64 1647.87 1795.57 1916.83 1928.89 BACKGROUND CORRECTED SAMPLE, PEAK REPORT Area 11869 828 23283 191 164 3417 207 95 90 72 47 93 14716 67 53 29 56 28 117 12 9325 6 8448 11 15 8 7 8 19 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 6185 4025 2291 1329 1277 1521 982 512 554 611 493 318 578 337 257 384 457 368 334 194 342 33 127 12 9 14 14 7 3 0.84 1. 41 0.88 1. 39 1. 78 0.83 0.74 1. 69 1.26 2.18 1. 68 1.14 1. 39 0.83 1. 47 1. 80 1. 94 0.94 1.16 0.97 1. 78 0.51 1. 84 1.19 3.90 3.49 1. 34 0.64 0.75 92.73 116. 07 118. 90 158.42 166.16 17 5. 82 244.06 558.24 692.98 703.04 969. 09 1047.47 1323.87 1496 .19 1509.78 1625. 61 1901.83 1925.31 2233.16 2244.20 2347.45 2498.28 2666.03 3060.79 3220.12 3296.57 3591.92 3834.38 3858.50 88 113 113 155 163 171 241 555 689 700 966 1044 1317 1490 1505 1618 1895 1923 2228 2243 2338 2493 2657 3053 3214 3289 3587 3825 3851 9 1. 32E+Ol 1. 5 12 9.20E-01 15.0 1.37E+Ol 12 2.59E+Ol 0.7 8 2.12E-01 33.9 8 1. 82E-01 38. 6 10 3.80E+OO 2.7 8 2.30E-01 27.1 7 l.06E-01 41.0 8 9.98E-02 46.9 9 8.05E-02 62.6 8 5.26E-02 82.2 8 1. 03E-01 35. 0 15 1. 64E+Ol 0. 9 12 7.41E-02 56.5 8 5.85E-02 55.0 11 3.23E-02132.5 10 6.17E-02 73.4 8 3.14E-02118.8 12 1.30E-01 33.1 8 1.29E-02209.7 17 1. 04E+Ol 1. 1 8 7 .14E-03161. 0 19 9. 39E+OO 1.1 13 l.22E-02 73.6 12 1.65E-02 48.1 11 9.09E-03 94.5 9 7.22E-03109.2 14 8.89E-03 78.6 14 2.07E-02 31.4 Flag: "*" = Peak area was modified by background subtraction Page 4327 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 06:01:12 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621363.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621363 SOLID GAMMAll 0 00:15:00.00 1. 50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry : Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 05:45:34 115.00 GRAM CAN 0 00:15:06.48 10.00 0.00 % Peak Energy 0.7% No interference correction performed Page 4328 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : G1203621363 Acquisition date 3-0CT-2016 05:45:34 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57
  • 122.06 217 85.60* 7.219E+OO 9.181E,Ol 9.692E-01 54.18 136.47 ------10.68 7.146E+OO ------Line Not Found ------C0-60 1173.23 8882 99.85 l.491E+OO 1.558E+02 1.570E+02 2.26 1332. 49 8001 99.98* 1.340E+OO 1. 559E+02 1.571E+02 2.27 ZN-65 1115. 54 112 50.60* 1.552E+OO 3. 724E+OO 3.955E+OO 66.10 CD-109 88.03 3628 3.70* 6.296E+OO 4.067E+02 4.199E+02 5.48 SN-126 64.28 ------9.60 4.012E+OO ------Line Not Found ------86.94 3628 8.90 6.296E+OO 1.691E+02 1. 691E+02 5.48 87.57 3628 37.00* 6.296E+OO 4.067E+01 4.067E+Ol 5.48 BA-137M 661.66 14372 89.90* 2.339E+OO 1. 785E+02 1. 787E+02 1. 80 CS-137 661. 66 14372 85.10* 2.339E+OO 1. 886E+02 1.888E+02 1. 80 PM-147 121. 22 217 0.00* 7.219E+OO 2.758E+04 2.800E+04 54.18 HG-203 70.83 ------3.69 4.810E+OO ------Line Not Found ------72. 87 ------6.19 5.033E+OO ------Line Not Found ------279.20 96 81.56* 4.692E+OO 6.570E-01 9.012E-01 82.00 PB-210 46.54 12924 4.25* l.359E+00 5.843E+03 5.854E+03 3.02 BI-211 72.87 ------1. 23 5.033E+OO ------Line Not Found ------351.06 73 12.92* 3.889E+OO 3.777E+OO 3.777E+OO 125.27 AM-241 59.54 25108 35.90* 3.356E+OO 5.441E+02 5.442E+02 1. 46 Flag: "*" Key line Page 4329 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:01:13.81 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621363.CNF;l *
  • Acquisition date 3-0CT-2016 05:45:34 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.48 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
  • Sample ID G1203621363 Sample Quantity l.1500E+02 GRAM *
  • Batch Number 1596252 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM C0-57 9.692E-01 5.146E-01 4.902E-01 C0-60 l.571E+02 3.493E+OO 7.217E-01 ZN-65 3.955E+OO 2.562E+OO 2.638E+OO CD-109 4.199E+02 2.253E+Ol 1.295E+Ol SN-126 4.067E+Ol 2.182E+00 1.260E+OO BA-137M l.787E+02 3.146E+OO 9.642E-01 CS-137 1.888E+02 3.323E+OO 1.019E+OO PM-147 2.800E+04 l.487E+04 l.400E+04 HG-203 9.012E-01 7.241E-01 8.785E-01 PB-210 5.854E+03 1.732E+02 1.041E+02 BI-211 3.777E+OO 4.636E+OO 4.860E+OO AM-241 5.442E+02 7.766E+00 4 .131E+OO Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 2.361E+OO 6.023E+OO 1.078E+Ol NOT IDENT. NA-22 -1.262E-01 3. 311E-01 5.897E-01 NOT IDENT. NA-24 O.OOOE+OO 4.671E+09 O.OOOE+OO SHORT HLIF AL-26 3. 251E-01 2.787E-01 6.182E-01 NOT IDENT. K-40 -1.005E+OO 2.190E+OO 3. 961E+OO NOT IDENT. SC-46 6.565E-01 8.353E-01 1.452E+OO FAIL ABUN V-48 -2.380E-01 l.841E+OO 3.056E+OO NOT IDENT. CR-51 1.364E-01 5.498E+OO 1.003E+Ol NOT IDENT. MN-54 8.471E-03 6.506E-01 1.105E+OO NOT IDENT. C0-56 6. OllE-01 7.259E-01 1. 27 9E+OO NOT IDENT. MN-56 O.OOOE+OO l.223E+41 O.OOOE+OO SHORT HLIF C0-58 1.392E-01 7 .196E-01 l.237E+OO NOT IDENT. FE-59 7.674E-01 1.801E+OO 3.255E+OO NOT IDENT. GE-68 7.808E+OO 2.304E+Ol 4.163E+Ol NOT IDENT. AS-73 -1.905E+Ol 1.565E+Ol 2.782E+Ol NOT IDENT. AS-74 -4.548E-01 1.701E+OO 2.948E+OO NOT IDENT. SE-75 2. 961E-01 6.057E-01 1.029E+OO FAIL ABUN BR-77 8.649E+01 6.523E+02 1.102E+03 NOT IDENT. Page 4330 of 5809 SR-82 -3.962E+00 6.319E+00 1.051E+Ol NOT IDENT. RB-83 -1.573E-01 1. 275E+00 2.005E+00 NOT IDENT. KR-85 -1. 076E+Ol 1. 029E+02 l.809E+02 NOT IDENT. SR-85 -6.062E-02 5.815E-01 1.023E+OO NOT IDENT. RB-86 1.005E+OO 1. 787E+Ol 3.196E+Ol NOT IDENT. Y-88 -7.479E-02 3.186E-01 5.777E-01 NOT IDENT. Y-91 4.385E+Ol 2.053E+02 3.793E+02 NOT IDENT. NB-94 -4.242E-02 4.528E-01 7.821E-01 NOT IDENT. NB-95 -3.273E-01 6.407E-01 1.074E+OO NOT IDENT. NB-95M 7.626E-01 l.537E-J;OO 2.627E+OO NOT IDENT. ZR-95 2.396E-01 l.267E+OO l.971E+OO NOT IDENT. NB-97 O.OOOE+OO l.088E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 9.912E+09 O.OOOE+OO SHORT HLIF M0-99 6.896E+Ol 8.901E+02 1.539E+03 NOT IDENT. TC-99M O.OOOE+OO 7.650E+24 O.OOOE+OO SHORT HLIF RH-101 -l.543E-01 3.223E-01 5.560E-01 NOT IDENT. RH-102 3.538E-02 8.329E-01 l.455E+00 NOT IDENT. RU-103 4.764E-01 7.050E-01 1.277E+OO NOT IDENT. RH-106 2.461E+OO 4.742E+OO 8.469E+OO NOT IDENT. RU-106 2.461E+OO 4.742E+OO 8.469E+OO NOT IDENT. AG-108M 4.979E-01 5.191E-01 9.483E-01 NOT IDENT. AG-llOM -1.126E+OO 9.986E-01 l.600E+00 NOT IDENT. SN-113 -1. 2 61E-01 6:918E-01 1.235E+OO NOT IDENT. CD-115 1.159E+03 1.191E+03 1.992E+03 NOT IDENT. SN-117M 1. 978E-02 7.636E-01 l.322E+00 NOT IDENT. TE-123M -9.382E-02 3.048E-01 5. 213E-01 NOT IDENT. SB-124 1. 480E-01 6.182E-01 l.244E+OO NOT IDENT. SB-125 5.573E-01 1.533E+OO 2.760E+OO NOT IDENT. TE-125M -7.839E+Ol 1.070E+02 1.848E+02 NOT IDENT. I-126 -l.379E+OO 5.035E+OO 7.683E+OO FAIL ABUN SB-126 2.324E+OO 3.009E+OO 5.384E+OO NOT IDENT. SB-127 -1.079E+OO 5.496E+Ol 9.550E+Ol NOT IDENT. I-131 -5.030E-01 2.815E+OO 5.056E+OO FAIL ABUN I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 -2. 361E+Ol 3.447E+Ol 5.667E+Ol NOT IDENT. BA-133 2. 451E-01 6.569E-01 l.086E+OO NOT IDENT. I-133 O.OOOE+OO l.131E+07 O.OOOE+OO SHORT HLIF CS-134 -1.715E-01 6.811E-01 1.150E+OO NOT IDENT. CS-135 1.285E+OO 2.0lOE+OO 3.430E+OO NOT IDENT. I-135 O.OOOE+OO 2.400E+23 O.OOOE+OO SHORT HLIF CS-136 1.699E+OO 2.537E+OO 4.662E+OO NOT IDENT. CE-139 9.897E-03 3.140E-01 5.423E-01 NOT IDENT. BA-140 6.420E-01 5.536E+OO 9.809E+OO NOT IDENT. LA-140 -l.362E-01 7.487E-01 1. 401E+OO NOT IDENT. CE-141 4.788E-01 7.126E-01 l.266E+OO NOT IDENT. CE-143 O.OOOE+OO 3.547E+04 O.OOOE+OO SHORT HLIF CE-144 1.131E-01 2.024E+OO 3.544E+OO FAIL ABUN PM-144 -6.812E-02 4.903E-01 8.444E-01 NOT IDENT. PR-144 -5 .151E+OO 3.681E+Ol 6.339E+Ol NOT IDENT. PM-146 1.784E-01 7.527E-01 1.343E+OO FAIL ABUN ND-147 -1.611E+OO 1.189E+Ol 2.090E+Ol NOT IDENT. PM-149 8.191E+03 8.289E+03 1.428E+04 NOT IDENT. EU-150 -4.957E-02 3.460E-01 6.263E-01 FAIL ABUN EU-152 -1.397E-01 1.476E+OO 2.403E+OO FAIL ABUN GD-153 2.539E-01 8. 941E-01 1.600E+OO NOT IDENT. EU-154 -3.241E-01 9.387E-01 1.678E+OO FAIL ABUN EU-155 1.291E-01 l.072E+OO 1.904E+OO FAIL ABUN TB-160 -1.035E+OO 2.836E+OO 4.706E+OO FAIL ABUN H0-166M -3.273E-01 8.291E-01 1.409E+OO FAIL ABUN TM-171 -1.563E+Ol 3.027E+02 5.472E+02 NOT IDENT. HF-172 -9.408E-01 2.096E+OO 3.341E+OO FAIL ABUN LU-172 -2.990E-01 1.151E+OO 2.030E+OO FAIL ABUN LU-176 1. 367E-01 3.732E-01 6.249E-01 FAIL ABUN HF-181 9.245E-02 8.533E-01 l.364E+OO FAIL ABUN TA-182 7.318E-02 1. 689E+OO 3.091E+OO FAIL ABUN RE-183 O.OOOE+OO 7.846E+OO 9. 511E'+OO FAIL ABUN RE-184 1.196E+OO 2.803E+OO 4.798E+OO NOT IDENT. W-188 -7. 911E+Ol 1.058E+02 1. 702E+02 NOT IDENT. IR-192 -3.021E-01 5.300E-01 8.525E-01 NOT IDENT. BI-207 5.956E-Ol 9.396E-01 1.718E+OO NOT IDENT. TL-208 -4.315E-01 5.089E-01 8.616E-01 NOT IDENT. PB-211 3.525E+OO 1.102E+Ol 1. 992E+Ol NOT IDENT. BI-212 -l.371E+OO 7.064E+OO l.210E+Ol NOT IDENT. PB-212 -2.450E-02 7.074E-01 1.188E+OO NOT IDENT. BI-214 1.150E-01 9.607E-01 1.693E+OO FAIL ABUN PB-214 1.371E+OO l.683E+OO 1.880E+OO FAIL ABUN RN-219 4.541E-01 6.367E+OO 1.143E+Ol NOT IDENT. RN-222 l.150E-01 9.607E-01 1.693E+OO FAIL ABUN Page 4331 of 5809 RA-223 2.893E+OO 8.439E+OO 1. 551E+Ol FAIL ABUN RA-224 -1.636E+OO 7.647E+OO 1.273E+Ol NOT IDENT. RA-226 1.150E-01 9.607E-01 1.693E+OO FAIL ABUN AC-227 1.333E+OO 3. 421E+OO 5.792E+OO FAIL ABUN TH-227 1.333E+OO 3.421E+OO 5.792E+OO FAIL ABUN AC-228 -2.568E+OO 2.820E+OO 4.559E+OO NOT IDENT. RA-228 -2.568E+OO 2.820E+OO 4.559E+OO NOT IDENT. TH-228 -2.450E-02 7.074E-01 1.188E+OO NOT IDENT. TH-229 -8.972E-01 6.039E+OO 1.024E+Ol FAIL ABUN .. TH-230 1.150E-01 9.607E-01 1.693E+OO FAIL ABUN PA-231 -7.880E-01 6.409E+OO 1. 054E+Ol NOT IDENT. TH-231 2.893E+OO 8.439E+OO 1.551E+Ol FAIL ABUN TH-232 -2.568E+OO 2.820E+OO 4.559E+OO NOT IDENT. PA-233 1.358E-01 9.376E-01 1.553E+OO NOT IDENT. PA-234 -3.540E+OO 7.560E+OO 1.094E+Ol NOT IDENT. PA-234M 1.182E+02 8.249E+Ol l.553E+02 NOT IDENT. TH-234 2.714E+OO 1.268E+Ol 2.156E+Ol NOT IDENT. U-234 1.150E-01 9.607E-01 1.693E+OO FAIL ABUN U-235 6.448E-01 2.040E+OO 3.586E+OO NOT IDENT. NP-237 1. 358E-01 9.376E-01 1.553E+OO NOT IDENT. NP-238 O.OOOE+OO 3.044E+03 O.OOOE+OO SHORT HLIF U-238 2. 714E+OO 1. 2 68E+Ol 2.156E+Ol NOT IDENT. NP-239 -l.961E-01 2. 712E+OO 4.764E+OO FAIL ABUN PU-239 2.654E+03 3.394E+03 6.089E+03 NOT IDENT. AM-243 -3.661E-01 5.147E-01 9.083E-01 NOT IDENT. CM-243 -3.044E-01 1.095E+OO 1.923E+OO FAIL ABUN BK-247 3.790E-01 1.055E+OO 1.783E+OO FAIL ABUN CM-247 2.140E-01 5.785E-01 1. 047E+OO FAIL ABUN CF-249 3.677E-02 5.769E-01 1.040E+OO NOT IDENT. CF-251 2.301E-01 1.383E+OO 2.387E+OO NOT IDENT. ANH-511 -l.054E-01 4.336E-01 7. 712E-01 NOT IDENT. Page 4332 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:01:11.57 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 217 85.60* 7.219E+OO 9 .181E-01 9.692E-01 54.18 136.47 ------10.68 7.146E+OO ------Line Not Found ------C0-60 1173.23 8882 99.85 l.491E+OO l.558E+02 1.570E+02 2.26 1332. 49 8001 99.98* 1. 340E+OO 1.559E+02 1. 571E+02 2.27 ZN-65 1115. 54 112 50.60* 1. 552E+OO 3.724E+OO 3.955E+OO 66.10 CD-109 88.03 3628 3.70* 6.296E+OO 4.199E+02 5.48 SN-126 64.28 ------9.60 4.012E+OO ------Line Not Found ------86.94 3628 8.90 6.296E+OO 1.691E+02 1. 691E+02 5.48 87.57 3628 37.00* 6.296E+00 4.067E+Ol 4.067E+Ol . 5. 48 BA-137M 661. 66 14372 89.90* 2.339E+OO 1. 785E+02 1. 787E+02 1. 80 CS-137 661. 66 14372 85.10* 2.339E+OO 1. 8 8 6E+02 1.888E+02 1. 80 PM-147 121. 22 217 0.00* 7.219E+OO 2.758E+04 2.800E+04 54.18 HG-203 70.83 ------3.69 4.810E+00 ------Line Not Found ------72. 87 ------6.19 5.033E+OO ------Line Not Found ------279.20 96 81.56* 4.692E+OO 6.570E-01 9.012E-01 82.00 PB-210 46.54 12924 4.25* 1. 3'59E+OO 5.843E+03 5.854E+03 3.02 BI-211 72.87 ------1.23 5.033E+00 ------Line Not Found ------351.06 73 12.92* 3.889E+OO 3.777E+OO 3.777E+OO 125.27 AM-241 59.54 25108 35.90* 3.356E+OO 5.441E+02 5.442E+02 1. 46 Flag: "*" Key line Page 4333 of 5809 Page : 2 Summary of Nuclide Activity Sample ID : Gl203621363 Acquisition date 3-0CT-2016 05:45:34 Total number of lines in spectrum 29 Number of unidentified lines 10 Number of lines tentatively identified by NID 19 65.52% Nuclide Type : .. Nuclide Hlife Decay Uncorrected Decay Corr Decay Corr 2-Sigma pCi/GRAM pCi/GRAM 2-Sigma Error %Error C0-57 271.74D 1. 06 9.181E-01 9.692E-01 5.251E-01 54.18 C0-60 5.27Y 1. 01 1.559E+02 1. 571E+02 0.036E+02 2.27 ZN-65 244.06D 1. 06 3. 724E+OO 3.955E+OO 2.614E+OO 66.10 CD-109 461.40D 1. 03 4.067E+02 4.199E+02 0.230E+02 5.48 SN-126 2.30E+05Y 1. 00 4.067E+Ol 4.067E+Ol 0.223E+Ol 5.48 BA-137M 30.08Y 1. 00 1. 785E+02 l.787E+02 0.032E+02 1. 80 CS-137 30.08Y 1. 00 1.886E+02 1.888E+02 0.034E+02 1. 80 PM-147 2.62Y 1. 02 2.758E+04 2.800E+04 1.517E+04 54.18 HG-203 46.59D 1. 37 6.570E-01 9.012E-01 7.389E-01 82.00 PB-210 22.20Y 1. 00 5.843E+03 5.854E+03 0.177E+03 3.02 BI-211 7.04E+08Y 1. 00 3.777E+OO 3.777E+OO 4.731E+OO 125.27 AM-241 432.60Y 1. 00 5.441E+02 5.442E+02 0.079E+02 1. 46 ------------------Total Activity 3.494E+04 3.540E+04 Grand Total Activity 3.494E+04 3.540E+04 "M" Manually accepted Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4334 of 5809 Flags Unidentified Energy Lines Page : 3 Sample ID : Gl203621363 Acquisition date : 3-0CT-2016 05:45:34 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 5 58.09 894 4344 1. 41 116. 07 113 12 9.20E-01 30.0 3.15E+OO T 0 79.25 204 1417 1. 39 158.42 155 8 2.12E-01 67.7 5.65E+OO T 0 83 .11 174 1359 1. 78 166.16 163 8 1.82E-01 77.2 5. 96E+OO T 0 .34 6. 35 90 556 1. 26 692.98 689
  • 8 9.98E-02 93.8 3.94E+OO T 0 484.34 47 488 1. 68 969. 09 966 8 5.26E-02 **** 2.99E+OO 0 523.51 92 314 1.14 1047.47 1044 8 l.03E-01 70.0 2.81E+OO T 0 747.77 65 328 0.83 1496 .19 1490 12 7.41E-02 **** 2.13E+OO T 0 754.57 51 250 1. 47 1509.78 1505 8 5.85E-02 **** 2. llE+OO T 0 812.46 28 372 1. 80 1625.61 1618 11 3.23E-02 **** 1.99E+OO 0 950.54 53 440 1. 94 1901.83 1895 10 6.17E-02 **** 1.76E+OO 0 962.27 27 353 0.94 1925.31 1923 8 3.14E-02 **** 1. 7 5E+OO T 0 1121.69 11 185 0.97 2244.20 2243 8 1.29E-02 **** 1.55E+OO T 0 1248. 71 6 31 0.51 2498.28 2493 8 7.14E-03 **** 1.42E+OO 0 1529.97 10 11 1.19 3060.79 3053 13 l.22E-02 **** 1.19E+OO 0 1609.64 14 9 3.90 3220.12 3214 12 1. 65E-02 96.2 1.13E+OO 0 1647.87 8 13 3.49 3296.57 3289 11 9.09E-03 **** 1. llE+OO 0 1795.57 6 13 1. 34 3591. 92 3587 9 7.22E-03 **** 1. 02E+OO 0 1916.83 7 7 0.64 3834.38 3825 14 8.89E-03 **** 9.58E-01 0 1928.89 17 3 0.75 3858.50 3851 14 2.07E-02 62.7 9.52E-01 Flags: "T" = Tentativel¥ associated Page 4335 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:01:28.00 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * * ' DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621363.CNF;l * *Acquisition date 3-0CT-2016 05:45:34 Sensitivity 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.48 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621363 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.1500E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 ZN-65 CD-109 SN-126 BA-137M CS-137 PM-147 HG-203 PB-210 BI-211 AM-241 Le (pCi/GRAM 2.391E-01 3.345E-01 1. 272E+00 6.319E+OO 6.146E-01 4.655E-01 4.917E-01 6.825E+03 4.267E-01 5.148E+Ol 2.360E+OO 2.036E+OO ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 Page 4336 of 5809 Le (pCi/GRAM 5.246E+OO 2.692E-01 O.OOOE+OO 2.745E-01 1. 714E+OO 7.038E-01 1. 477E*+oo 4.873E+OO 5.338E-01 6 .177E-01 O.OOOE+OO 5.971E-01 1. 573E+OO 2.0lOE+Ol 1.375E+Ol 1. 420E+OO 5.008E-01 5. 371E+02 5.054E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 BI-207 TL-208 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 Page 4337 of 5809 9.700E-01 8.764E+Ol 4.954E-01 l.542E+01 2.483E-01 1. 778E+02 3.753E-01 5.158E-01 1. 280E+OO 9.469E-01 O.OOOE+OO O.OOOE+OO 7.409E+02 O.OOOE+OO 2.707E-01 7.016E-01 6.192E-01 4.085E+OO 4.085E+OO 4.624E-01 7.730E-01 6.005E-01 9.620E+02 6.433E-01 2.537E-01 5. 351E-01 1.344E+OO 9.002E+Ol 3.699E+OO 2.594E+OO 4.583E+Ol 2.457E+OO O.OOOE+OO 2. 7 61E+Ol 5.285E-01 O.OOOE+OO 5.544E-01 1.670E+OO O.OOOE+OO 2.249E+OO 2.638E-01 4.739E+OO 5.982E-01 6.166E-01 O.OOOE+OO 1.725E+OO 4.059E-01 3.047E+Ol 6.546E-01 1.008E+Ol 6.947E+03 3.041E-01 1.168E+OO 7. 811E-01 7.666E-01 9.281E-01 2.278E+OO 6.753E-01 2.703E+02 1. 626E+OO 9.793E-01 3.038E-01 6.617E-01 1.443E+OO 4.717E+OO 2.324E+OO 8.272E+Ol 4.141E-01 8.299E-01 4.148E-01 9.694E+OO 5.810E+OO 5.790E-01 8.155E-01 9.149E-01 5.561E+OO 8.155E-01 7.545E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IOENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 4338 of 5809 6.203E+OO 8.155E-01 2.823E+OO 2.823E+OO 2.205E+OO 2.205E+OO 5.790E-01 4.989E+OO 8.155E-01 5.123E+OO 7.545E+OO 2.205E+OO 7.555E-01 5.305E+OO 7. 521E+Ol 1. 053E+Ol 8.155E-01 1.747E+OO 7.555E-01 O.OOOE+OO 1.053E+Ol 2.320E+OO 2. 967E+03 4. 441E-01 9.374E-01 8.676E-01 5.098E-01 5. 051E-01 1.162E+OO 3.734E-01 NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:01:33.73 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621363.CNF;l *
  • Acquisition date 3-0CT-2016 05:45:34 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.48 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621363 Analyst initials: MXRl *
  • Batch Number 1596252 Sample Quantity : 1.1500E+02 GRAM *
  • Quantity Err ( % ) : 1. 7391E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;14
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1. 96-sigma) (1.96-sigma) C0-57 9.692E-01 5.165E-01 5.165E-01 C0-60 1. 571E+02 6.753E+OO 6.753E+OO ZN-65 3.955E+OO 2.566E+OO 2.566E+OO CD-109 4.199E+02 4 .101E+Ol 4.101E+Ol SN-126 4.067E+Ol 3.337E+OO 3.337E+OO BA-137M 1. 787E+02 8.302E+OO 8.302E+OO CS-137 1.888E+02 8. 751E+OO 8.751E+OO PM-147 2.800E+04 1. 492E+04 l.492E+04 HG-203 9.012E-01 7.253E-01 7.253E-01 PB-210 5.854E+03 5.374E+02 5.374E+02 BI-211 3.777E+OO 4.639E+OO 4.639E+OO AM-241 5.442E+02 4.078E+Ol 4.078E+Ol Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 2.361E+OO 6.024E+OO 6. ll 7E+OO NOT IDENT. NA-22 -1.262E-01 3. 311E-01 3.359E-01 NOT IDENT. NA-24 -3.221E+08 4.671E+09 4.673E+09 SHORT HLIF AL-26 3.251E-01 2.795E-01 3.156E-01 NOT IDENT. K-40 -1.005E+OO 2 .191E+OO 2.237E+OO NOT IDENT. SC-46 6.565E-01 8.358E-01 8.866E-01 FAIL ABUN V-48 -2.380E-01 1.841E+OO l.844E+OO NOT IDENT. CR-51 1.364E-01 5.498E+OO 5.498E+OO NOT IDENT. MN-54 8.471E-03 6.506E-01 6.506E-01 NOT IDENT. C0-56 6. OllE-01 7.264E-01 7.753E-Ol NOT IDENT. MN-56 1.000E+41 l.224E+41 O.OOOE+OO SHORT HLIF C0-58 1.392E-01 7.197E-01 7.224E-Ol NOT IDENT. FE-59 7.674E-01 1. 8 OlE+OO 1.834E+OO NOT IDENT. GE-68 7.808E+OO 2.304E+Ol 2.331E+Ol NOT IDENT. AS-73 -1.905E+Ol l.613E+Ol 1.828E+Ol NOT IDENT. AS-74 -4.548E-01 1. 702E+OO 1. 714E+OO NOT IDENT. SE-75 2. 961E-01 6.058E-01 6.204E-01 FAIL ABUN BR-77 8.649E+Ol 6.544E+02 6.556E+02 NOT IDENT. Page 4339 of 5809 SR-82 -3. 962E+OO 6. 321E+OO 6.568E+OO NOT IDENT. RB-83 -1.573E-01 1.275E+00 l.277E+OO NOT IDENT. KR-85 -1.076E+Ol l.029E+02 l.030E+02 NOT IDENT. SR-85 -6.062E-02 5.815E-01 5.822E-01 NOT IDENT. RB-86 1.005E+OO 1.787E+Ol 1.788E+Ol NOT IDENT. Y-88 -7.479E-02 3.186E-01 3.204E-01 NOT IDENT. Y-91 4.385E+Ol 2.053E+02 2.062E+02 NOT IDENT. NB-94 -4.242E-02 4.528E-01 4.532E-01 NOT IDENT. NB-95 -3.273E-01 6.409E-01 6.577E-01 NOT IDENT. NB-95M 7 .* 626E-01 1.538E+OO l.576E+OO NO.;I' IDENT. ZR-95 2. 396E-01 1. 267E+OO 1. 272E+OO NOT IDENT. NB-97 l.OOOE+41 l.089E+41 0.000E+OO SHORT HLIF ZR-97 -2.917E+09 9.913E+09 1.000E+lO SHORT HLIF M0-99 6.896E+Ol 8.901E+02 8.907E+02 NOT IDENT. TC-99M -5.812E+23 7.650E+24 0.000E+OO SHORT HLIF RH-101 -l.543E-01 3.235E-01 3.309E-01 NOT IDENT. RH-102 3.538E-02 8.329E-01 8.330E-01 NOT IDENT. RU-103 4.764E-01 7.054E-01 7.374E-01 NOT IDENT. RH-106 2.461E+OO 4.745E+OO 4.873E+OO NOT IDENT. RU-106 2.461E+OO 4.745E+OO 4.873E+OO NOT IDENT. AG-108M 4.979E-01 5.195E-01 5.659E-01 NOT IDENT. AG-llOM -1.12 6E+OO 1.000E+OO 1.122E+OO NOT IDENT. SN-113 -1.261E-01 6.918E-01 6.941E-01 NOT IDENT. CD-115 1.159E+03 l.193E+03 1.302E+03 NOT IDENT. SN-ll 7M l.978E-02 7.636E-01 7.637E-01 NOT IDENT. TE-123M -9.382E-02 3.048E-01 3.077E-01 NOT IDENT. SB-124 1.480E-01 6.183E-01 6.218E-01 NOT IDENT. SB-125 5.573E-01 1.533E+OO 1.554E+OO NOT IDENT. TE-125M -7.839E+Ol 1.071E+02 l.128E+02 NOT IDENT. I-126 -1. 37 9E+OO 5.036E+OO 5.074E+OO FAIL ABUN SB-126 2.324E+OO 3.018E+OO 3.195E+OO NOT IDENT. SB-127 -1.079E+OO 5.496E+Ol 5.496E+Ol NOT IDENT. I-131 -5.030E-01 2.815E+OO 2.824E+OO FAIL ABUN I-132 l.000E+41 3.210E+41 O.OOOE+OO SHORT HLIF TE-132 -2. 361E+Ol 3.453E+Ol 3.613E+Ol NOT IDENT. BA-133 2.451E-01 6.569E-01 6.662E-01 NOT IDENT. I-133 -9.551E+06 l.139E+07 1.218E+07 SHORT HLIF CS-134 -l.715E-01 6.812E-01 6.856E-01 NOT IDENT. CS-135 1.285E+OO 2.012E+OO 2.094E+OO NOT IDENT. I-135 1.294E+23 2.480E+23 O.OOOE+OO SHORT HLIF CS-136 l.699E+OO 2.541E+OO 2.654E+OO NOT IDENT. CE-139 9.897E-03 3.140E-01 3.141E-01 NOT IDENT. BA-140 6.420E-01 5.536E+OO 5.543E+OO NOT IDENT. LA-140 -l.362E-01 7.487E-01 7.513E-01 NOT IDENT. CE-141 4.788E-01 7.129E-01 7.449E-01 NOT IDENT. CE-143 9.974E+03 3.547E+04 3.575E+04 SHORT HLIF CE-144 1.131E-01 2.024E+OO 2.025E+OO FAIL ABUN PM-144 -6. 812E-02 4.903E-01 4.913E-01 NOT IDENT. PR-144 -5 .151E+OO 3.681E+Ol 3.688E+Ol NOT IDENT. PM-146 1. 784E-01 7.528E-01 7.570E-01 FAIL ABUN ND-147 -1. 611E+OO 1.189E+Ol l.191E+Ol NOT IDENT. PM-149 8 .191E+03 8.362E+03 9 .141E+03 NOT IDENT. EU-150 -4.957E-02 3.460E-01 3.467E-01 FAIL ABUN EU-152 -1.397E-01 1.476E+OO 1. 477E+00 FAIL ABUN GD-153 2.539E-01 8.943E-01 9.016E-01 NOT IDENT. EU-154 -3.241E-01 9.388E-01 9. 501E-01 FAIL ABUN EU-155 1.291E-01 1.072E+OO 1.073E+00 FAIL ABUN TB-160 -1.035E+OO 2.836E+00 2.874E+OO FAIL ABUN H0-166M -3.273E-01 8.293E-01 8.423E-01 FAIL ABUN TM-171 -1.563E+Ol 3.027E+02 3.028E+02 NOT IDENT. HF-172 -9.408E-01 2.102E+OO 2.144E+OO FAIL ABUN LU-172 -2.990E-01 1.152E+OO l.159E+OO FAIL ABUN LU-176 l.367E-01 3.732E-01 3.783E-01 FAIL ABUN HF-181 9.245E-02 8.533E-01 8.543E-01 FAIL ABUN TA-182 7.318E-02 1. 68 9E+00 l.690E+OO FAIL ABUN RE-183 2.665E+Ol 8.325E+OO l.462E+Ol FAIL ABUN RE-184 1.196E+OO 2.804E+00 2.856E+OO NOT IDENT. W-188 -7.911E+Ol l.062E+02 l.120E+02 NOT IDENT. IR-192 -3.021E-01 5.302E-01 5.474E-01 NOT IDENT. BI-207 5.956E-01 9.399E-01 9.775E-01 NOT IDENT. TL-208 -4.315E-01 5.093E-01 5.452E-01 NOT IDENT. PB-211 3.525E+OO 1.102E+Ol l .114E+Ol NOT IDENT. BI-212 -1.371E+OO 7.065E+00 7.092E+OO NOT IDENT. PB-212 -2.450E-02 7.074E-01 7.074E-01 NOT IDENT. BI-214 1.150E-01 9.607E-01 9.621E-01 FAIL ABUN PB-214 1.371E+OO 1.684E+00 1. 793E+OO FAIL ABUN RN-219 4. 541E-01 6.368E+OO 6. 371E+OO NOT IDENT. RN-222 1.150E-01 9.607E-01 9. 621E-01 FAIL ABUN Page 4340 of 5809 RA-223 2.893E+OO 8. 441E+OO 8.541E+OO FAIL ABUN RA-224 -1.636E+OO 7.647E+OO 7.683E+OO NOT IDENT. RA-226 1.150E-01 9.607E-01 9. 621E-01 FAIL ABUN AC-227 1.333E+OO 3.426E+OO 3.478E+OO FAIL ABUN TH-227 1.333E+00 3.426E+OO 3.478E+OO FAIL ABUN AC-228 -2.568E+00 2.823E+OO 3.052E+OO NOT IDENT. RA-228 -2.568E+OO 2.823E+OO 3.052E+OO NOT IDENT. TH-228 -2.450E-02 7.074E-01 7.074E-01 NOT IDENT. TH-229 -8.972E-01 6.039E+OO 6.053E+OO FAIL ABUN . ' TH-230 1.150E-01. 9.607E-01 9. 621E-01 FAIL ABUN PA-231 -7.880E-01 6.411E+OO 6.421E+OO NOT IDENT. TH-231 2.893E+OO 8.441E+OO 8.541E+OO FAIL ABUN TH-232 -2.568E+OO 2.823E+OO 3.052E+OO NOT IDENT. PA-233 1.358E-01 9.376E-01 9. 396E-01 NOT IDENT. PA-234 -3.540E+OO 8.577E+OO 8.724E+OO NOT IDENT. PA-234M 1.182E+02 8.265E+Ol 9.835E+Ol NOT IDENT. TH-234 2. 714E+OO 1.269E+Ol 1. 27 5E+Ol NOT IDENT. U-234 1.150E-01 9.607E-01 9. 621E-01 FAIL ABUN U-235 6.448E-01 2.040E+OO 2.061E+OO NOT IDENT. NP-237 l.358E-01 9.376E-01 9.396E-01 NOT IDENT. NP-238 -2.836E+03 3.046E+03 3.304E+03 SHORT HLIF U-238 2.714E+OO 1.269E+Ol 1.275E+Ol NOT IDENT. NP-239 -1.961E-01 2.712E+OO 2.713E+OO FAIL ABUN PU-239 2.654E+03 3.396E+03 3.600E+03 NOT IDENT. AM-243 -3.661E-01 5.152E-01 5.410E-01 NOT IDENT. CM-243 -3.044E-01 1.095E+OO 1.104E+OO FAIL ABUN BK-247 3.790E-01 1.057E+OO 1.071E+OO FAIL ABUN CM-247 2.140E-01 5.796E-01 5.876E-01 FAIL ABUN CF-249 3.677E-02 5.770E-01 5. 772E-01 NOT IDENT. CF-251 2. 301E-01 l.383E+OO 1.387E+OO NOT IDENT. ANH-511 -1.054E-01 4.336E-01 4.362E-01 NOT IDENT. Page 4341 of 5809
  • GEL Laboratories LLC *
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  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 2607 .1199 87.09 526.4185 136.47 462.4787 45.60 2305.2644 87.57 526.9440 140.51 447.7479 46.54 2312.1226 88.03 527.4438 143.76 456.1200 49. 72 1998.8229 88.34 527.7771 144.24 464.7412 51. 35 2036.0985 88.47 527.9181 145.44 423.9873 51. 87 2091.8289 89. 96 598.8670 152.43 487.0103 52.39 2084.6348 90.64 558.0259 153.25 478.1124 52.97 2249. 9666 91.11 535.8098 154.21 441. 9241 53.44 2294.6055 92. 59 485.7486 156.02 460.9651 54.07 2239.7058 93.35 575.0147 158.56 429.7643 57.36 0.0000 94.56 518.1766 159.00 449.0831 57.53 1544.4453 94.65 518.2677 162.33 436.2131 57.98 1546.3274 94.67 518.2885 162.66 436.4070 59.27 1551.7247 94.87 531. 8596 163.33 443.1870 59.32 1551.9331 97.43 522.9874 165.86 419.0242 59.54 1552.8472 98.43 507.6409 176.31 455.0555 60. 96 1558.7084 98.44 507.6530 176.60 455.2222 61.17 99.53 516.4120 177.52 431. 87 52 62.93 636.6469 100 .11 537.2310 181.07 416.3553 63.29 569.5972 102.03 474.3099 181. 52 443.8521 63.58 561. 7068 103.18 481.1395 184.41 467.3179 64.28 596.0218 103.37 500.7175 185. 72 471.3557 66.73 617.6526 105.21 494.6171 193.51 487.9491 67.24 625.6205 105.31 476.2035 197.03 496.6341 67.68 634.3989 106.12 486.6575 198.01 472.7295 67.75 652.5067 106.47 501.6041 201.83 432.3575 69.67 594.0779 109.28 509.0335 203.43 477.9187 70.83 641.0640 111. 00 462.3766 205.31 458.7520 72. 81 629.4874 111.76 499.4379 210.85 510.1346 72.87 629.5770 114.06 468.7961 215.65 553.6837 74.66 674.2770 116. 30 461. 6581 222 .11 524.4224 74.82 669.9482 116.74 462.0022 227.09 501.9272 74.97 661. 9428 119.76 495.3075 227.38 490.5913 77 .11 588.8037 121.12 497.7583 228.16 513.9859 78.74 658.6654 121. 22 497.8380 228.18 513.9995 79.69 660.0477 121.78 509.9864 235.69 449.6315 80.12 660.6736 122.06 510.2233 235. 96 448.5966 80.19 660.7770 122.92 510.9417 238.63 470.7408 80.57 595.1940 123.07 511. 0659 238.98 460.4400 81. 00 595.7524 123.68 490.4684 240.99 485.8404 81. 07 595.8406 125.81 467.9542 242.00 456.0076 81. 75 596.7222 127.23 477.1027 244.70 495.8334 83.79 591.8694 127.91 436.1330 252.40 461. 8872 84.00 592.1306 129.30 427. 9627 252.80 464.4241 85.43 595.7939 131.20 484.1711 254.15 0.0000 86.55 525.8289 133.02 433. 5213 256.23 454.1367 86.79 526.0895 133.52 439.9770 260.90 416.9625 86.94 526.2561 136.00 429.3574 264.66 401. 7507 Page 4342 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 401. 8022 364.49 397.0626 600.60 234.6748 265.00 406.6546 366.42 382.0649 602.52 0.0000 268.22 404.2838 372.51 385.5010 604. 72 224.1943 269.46 435.8824 375.05 380.9866 607.14 250.4076 270.03 467.2668 1093.63 394.7345 609.32 223.7083 271. 23 429.3968 383.85 402.6404 610.33 .218.8218 273.65 438.7730 388.16 376.6493 614.28 237.2700 276.40 425.8051 388.63 402.2409 618.01 220.6445 277.37 443.8730 391.69 406.6187 620.36 235.9658 277.60 443. 9629 400.66 415.3367 621. 93 224.0798 278.00 428.0396 401.81 431.6240 630.19 0.0000 279.20 374.5297 402.40 414.0597 631.29 237.2089 279.54 380.2926 404.85 411.2007 633.25 244. 501l 279.70 380.3406 410.95 436.9745 634.78 218.3906 280.46 362.8601 413.71 379.7089 635.95 230.6533 283.69 395.4521 414.70 444.3293 636.99 224.6919 284.31 428.4413 423.72 423.5953 645.85 219.5332 285.41 379.0503 427.09 439.8474 657.76 240.6841 285.90 370.7042 427.87 434.6649 657.90 0.0000 287.50 377. 31ll 433.94 443.6139 661.66 256.9849 290.67 440.6077 439.40 432.4403 664.57 0.0000 293.27 0.0000 453.88 460.2279 666.33 233.9375 295.22 410.4895 463.37 501.6549 666.50 204. 7ll5 295. 96 409.5292 468.07 482'.7480 667.71 0.0000 298.58 376.0472 473.00 477.6889 677.62 200.0783 299.98 394.951l 475.06 469.9277 685.70 189.4187 300.09 394.9805 476.78 396.9679 695.00 183.9717 300.13 395.0001 477.60 400.8795 696.49 210.0879 301.36 394.1797 482.18 335.7568 696. 51 210.0961 302.85 377.4106 487.02 378.7976 697.00 202.8552 304.50 410.0557 492.35 327.4431 697.30 195.6039 304.85 410.1671 497.08 311. 4102 697.49 190.4165 306.78 383. 6l18 505.52 318.5909 702.65 191. 8913 308.46 421. 32 69 507.63 0.0000 706.68 196.4071 31l. 90 403.8994 51l. 00 297.7704 711. 68 190.5535 316.51 407.9217 514.00 318.2200 720. 70 199.7025 319.41 388.4661 514.00 318.2200 721. 93 0.0000 320.08 375.3296 520.40 296.0085 722. 78 232.4924 321. 04 376.4664 520.69 290.3381 722. 91 226.1979 323.87 397.3989 522.65 0.0000 723.31 232.5464 325.23 409.5594 527.90 218.2681 724.19 202.1094 328.76 367.8872 528.26 244.7316 727. 33 198.1665 333.37 369.2239 529.59 274.0484 733.00 204.9804 333.97 378.6793 529.87 0.0000 735.93 231.6805 334.37 396.5147 531. 02 253 .16ll 737.46 211. 7187 338.28 365.5723 537.26 264.6047 739.50 218.2547 338.32 365.581l 546.56 0.0000 747.24 214.7154 340.48 418.7523 552.55 247.3840 748.06 214.7894 340.55 418. 7723 563.25 248.7848 752.31 204.5156 344.28 404.2505 569.33 238.8075 753.82 208.9040 345.93 382.2054 569.50 241. 7738 756.73 192.0850 351.06 374.3032 569.70 250.6042 756.80 192.0923 351. 93 374.5527 583.19 257.2723 763.94 195.8672 355.39 0.0000 584.27 246. 5719 765.81 217.4386 356.01 397.5753 595.83 243.0461 766.42 201. 4253 Page 4343 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 221. 8158 1002.74 307.4464 1678.03 0.0000 772.60 0.0000 1004.73 294.4922 1690.97 10.4773 776.52 235.6014 1021.30 0.0000 1750.46 0.0000 777.92 234.6587 1025.87 0.0000 1764.49 17.0215 778.90 218.5950 1028.54 0.0000 1770.23 10.6506 .1783. 70 217.9374 1037.84 1771. 35 20.2408 785.37 233.2002 1038.76 0.0000 1791.20 0.0000 792.07 238.1543 1046.59 253.1845 1808.65 8.5864 794.95 251. 4372 1048.07 222.1985 1810. 72 0.0000 795.86 250.4380 1049.04 215.1472 1836.06 15.1083 801.95 241.2588 1050.41 245.4756 810.06 242.0266 1063.66 242.9307 810.29 242.0537 1077.00 251.1182 810.45 242.0627 1077.34 245.7538 810.76 242.0989 1085.87 227.5209 815.77 240. 9296 1093.63 257.8085 818.51 241. 7367 1099.45 254.6503 832.01 257.2800 1112. 07 259.6199 834.85 266.3713 1112. 84 259.6724 835. 71 251.0449 1115.54 240.5932 836.80 0.0000 1120.29 185.3730 846.75 0.0000 1120.55 185.3855 846.77 225.5571 1121.30 134.5315 856.80 258.5934 1129. 67 180.4285 860.56 257.8470 1131. 51 0.0000 871.09 280.0464 1147.95 0.0000 873.19 255. 6962 1173.23 134.7452 875.33 0.0000 1177.95 134.5538 879.38 315.5977 1189. 05 90.8582 880.51 301.1692 1204.77 69.8410 883.24 267.8441 1221.41 65.4883 884.68 319.5697 1231. 02 49.7166 889.28 286.4081 1235.36 63.8662 894.76 319.6040 1238.28 46.0571 898.04 282.8040 1260.41 0.0000 900. 72 321. 4252 1271.87 40.7875 903.28 290.1080 1274.44 43.6641 911. 20 336.2036 1274.54 43.6641 912.08 297.8120 1291.59 39.0956 923.98 0.0000 1298.22 0.0000 926.50 343.7191 1312 .11 38.3496 929 .11 323.5215 1332.49 53.9731 937.49 325.6116 1362.66 0.0000 944.13 336.6597 1365.19 27.2139 946.00 372.9688 1368.63 0.0000 949.00 330.3398 1384.29 25.3906 954.55 0.0000 1408.01 22.5943 962. 31 337.0367 1457.56 0.0000 964.08 314.7565 1460.82 17.9110 966 .17 299.4028 1489.16 20.0342 968. 97 296.7902 1505.03 22 .1195 983.53 281.9971 1584.12 17.4036 984.45 0.0000 1596. 21 13.3444 996.26 282.0281 1620.50 12.3838 1001.03 245.9951 1621. 92 10.3235 Page 4344 of 5809 Effective 3/25/201 o Radiochemistry Batch Checklist Revision 1 Effective March 2010 26-Sep-2016 Batch#__../_.;:9,'-q-'-4>,__7S'/=-L--Product: , Criteria: Yes No Comments Sample Solids are less than or equal to 100 m11 for GAB. /Vil. Samples have been blank corrected (If required). !VA-Blank correction reoorted Included (If reoulredl. If activity less than 10x MDA/MDC, error Is less than or equal to 1500/o of sample activity. If greater than 10* MDA/ MDC, error Is 400/o or less. IIf hAlnw *"o unA I Mnr .,. * ..,..Is nlrnu ifnstrument source check Is within llmlts. iln.,trument bkn eh.,.,k '" within llmlts. Method RDL/ LLD has been met. v If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 1000/o or less, v If greater 5* MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO Is 0%, 'SGG IJ MJ ll.tJ..r/,;£ Or meets the client's renulred RER acceotance criteria. Tracer yield Is 15-1250/o , Carrier yleld 25-1250/o, (Or meets the client's contract acceptance criteria), N{+-Method blank Is less than the RDL/ LLD. v* (Tf *ft .. < !;O/n nf ln ... M* n.+lulh,\ Samole was run within hold time. v J>e-12--*-Samele was correctlv oreserved If reouired. N1"r !smears Taken for Radioactive batches. /'Jtl-Method Spike and LCS are within 75-1250/o v Ir nr the cllon**s rnn*ra.-t rrlt.*rla \ No blank spaces on data forms. v All line outs Initialed and dated. l*ln n*o -* Aux data Is correct. NA-Client Soeclal reoulrements oaoe has been checked. ,,....-Raw Data and I or soectrum are Included and orooerlv statw*Ad, v MS, LCS, and Dupllcate RPD/RER values uploaded to LIMS and v UftjUAC u .. rlfln .. Hit '" (If NA-.. on>o.a .. ln*n .. v Batch Data Exceotlon Reoorts CDERl comoleted If aoollcable. ,,........ p(;?(Lf:l:_ Batch Data Exception Reports (DER) second reviewed. / Dlsoosition verified to be "omnleted. Aliauot comnlet<'d If rAnnlred. IVA Review sample historical results If available NA--(If REMP, results above MDC have been verified bv historical results recount ar re-analvsls. l . u 16h/t(.? Primary Review Performed By: A-. -Secondary Review Performed By: Page 4345 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 03-0CT-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GAMMA SPECTROMETER DOE HASL 300, 4.5.2.3/Ga-01-R Solid Batch ID: Sample Numbers: 1596254 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Sample received and analyzed out of holding: 1. Reporting Results 405235061,062,063,064,065,066,067,068,069, 070,071,072,073,07 4,075,076,077,078, 1203621365DUP Originator's Name: Data Validator/Group Leader: Tim Winters 03-0CT-16 Bryan Williams 03-0CT-16 Page 1 Page 4346 of 5809 DER Report No.: 1563729 Revision No.: 1
  • Type: Process Client Code: MJWC Gamma Spec Queue Sheet \.G.-to{J[lce 09/16/2016 Batch #:1596254 Analyst: MXRl First Client DueDate:l0/04/2016 Internal Due Date: 09/30/2016 Gamma LCS Isotope: Mixed Gamma LCS Code: lt:;l)b Expiration Date: J.t I 1 /'3! Vol: \.o ;'Ill l.---Initials: K1 Prep Date: __ Library: ¥1JL-l b Balance ____ _ 7 Wet/ ry Hazard A(:>ot Sealing Dateffime Sample ID I ID Type Code Client Matri:x Collect Date Geometry ( l g F) Detector (if Applicable) 405235061-1 5.IB.R.2.2 SAMPLE MJWCOOl SOIL 144.233 g tj' \'1. \Co 405235062-1 5.2.A.R. l.2 SAMPLE MJWCOOI SOIL 146.441 g 405235063-1 5.2-.\.R. l.3 SAMPLE MJWCOOl SOIL 147.883 g I 405235064-1 5.2.A.R.l.4 SAMPLE MJWCOOl SOIL 174.637 g 405235065-1 5.2A.R.2.3 SAMPLE MJWCOOl SOIL 147.836 g 405235066-1 5.2.A.R.2.4 SAMPLE MJWCOOl SOIL 157.422 g 405235067-1 5.2A.R.6.2 SAMPLE MJWCOOl SOIL ll-DEC-1511:30:00'!f 158.21 g 405235068-1 5.2A.R.4.2 SAlHPLE MJWCOOl SOIL l 1-DEC-15 10:27:00'fljZ 140.907 g 405235069-1 5.2.B.R.1.4 SAMPLE M.JWCOOI SOIL 16-DEC-15 12:45:00 156.084 g 405235070-1 5.2.B.R.3.2 SAMPLE MJWCOOI SOIL 11-DEC-15 10:10:00 145.32 g 405235071-1 5.2.B.R.4.2 SAMPLE MJWCOOl SOIL 149.695 g 405235072-1 5.2.B.R.2.4 SAMPLE MJWCOOl SOIL 15-DEC-1: 166.107 g 405235073-1 5.2.B.R.8.2 SAMPLE MJWCOOI SOIL 11-DEC-1:> 11:3:.:00 147.132 g 405235074-1 5.3.A.R.l.3 SAMPLE MJWCOOl SOIL 15-DEC-15 14:10:0 169.068 g 405235075-1 5.4A.R.1.3 SAMPLE MJWCOOI SOIL 16-DEC-15 405235076-1 5.4A.R.4.2 SAMPLE MJWCOOI SOIL l l-DEC-15 14:19:0 405235077-1 5.5A.R.l.3 SAMPLE MJWCOOl SOIL 17-DEC-15 13:30:00 f\: 405235078-1 5.6A.R.l.3 SAMPLE MJWCOOl SOIL 17-DEC-15 12:40:0 1203621364-1 MB MB QC ACCOUNT SOIL CJ h-i..}1 v 1203621365-1 DUP 5.IB.R.2.2(405235061) DUP QC ACCOUNT SOIL 14-DEC-15 13:47:0 I l-f4.'l.2i3 l-1203621366-1 LCS LCS QC ACCOUNT SOIL q hi;"" GEL Laboratories LLC, Radiochemistry Division Data Reviewed By:

VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:54:36.57 ******************************************************************************** *

  • GEL Laboratories LLC ' *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM20.CNF;515 Background date : Sample date 14-DEC-2015 13:47:00 Acquisition date : Z-OCT-2016 11:01:13. 3-0CT-2016 05:52:51. l.44233E+02 GRAM CAN Sample ID G405235061 Sample quantity Detector name : GAM20 Detector geometry: Elapsed live time: 0 01:00:00.00 Elapsed real time: Energy tolerance 1.50000 keV Analyst Initials : Abundance limit 75.00000 Sensitivity Batch ID 1596254 Detector SN# 0 01:00:14.55 0.4% MXRl 3,00000 Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 5 5 0 0 0 0 4 4 0 0 4 4 2 2 0 0 0 0 0 1 1 0 0 0 0 0 0 0 0 0 Energy 47.05* 63.50* 74.92 77.15 87.37 92.64* 129.70 144.40* 186.06* 209.70 238.52* 241.49 270.20 295.09* 299.97 304. 96 351.90* 356.36* 510.90* 583.44* 609.37* 623.21 723. 27 763.00 768.40 796.11 861.13 911. 42* 1001.94* 1120. 51 1156.21 1305. 58 1320 .12 1332.48 Page 4348 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 34 10 168 242 56 75 19 29 86 21 330 70 43 194 43 23 302 19 56 112 203 33 67 19 38 32 19 85 19 58 21 17 5 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 141 165 176 142 225 225 117 125 116 89 77 71 71 30 25 21 38 29 24 29 29 31 42 30 20 14 11 8 8 17 4 2 5 3 1. 86 0.72 1. 23 0.98 1. 29 1. 85 1. 40 1. 38 0.97 1. 39 1.17 1. 43 1. 58 1.17 2.01 2.01 1. 30 1. 71 1. 74 1. 29 1.26 5. 67 11. 05 1. 83 1. 84 3. 96 2.54 1. 78 3.13 2.04 2.57 3. 63 1. 29 1. 23 94.29 127.15 149.98 154.43 174.87 185.40 259.47 288.84 372.12 419.38 476.98 482.93 540.33 590.08 599.84 609.83 703.68 712.60 1021.62 1166. 72 1218.58 1246.28 1446.45 1525.94 1536.75 1592.18 1722.29 1822.93 2004.11 2241. 46 2312.95 2612.04 2641.15 2665.90 88 124 146 146 170 170 253 283 367 415 473 473 535 585 595 595 697 697 1016 1161 1212 1237 1431 1518 1518 1583 1716 1818 1994 2232 2308 2608 2636 2661 10 9.48E-03 68.7 8 2.88E-03224.3 14 4.67E-02 15.0 14 6.73E-02 10.6 22 l.56E-02 44.6 22 2.09E-02 44.6 8 5.17E-03104.l 10 8.03E-03 75.5 10 2.38E-02 27.2 8 5.92E-03 79.9 14 9.16E-02 7.1 14 1. 96E-02 23. 7 9 l.20E-02 38.6 10 5.40E-02 9.0 21 l.20E-02 28.1 21 6.44E-03 53.2 19 8.39E-02 6.8 19 5.26E-03 58.2 13 l.56E-02 28.2 13 3.llE-02 14.2 13 5.64E-02 9.0 18 9.16E-03 43.5 31 l.85E-02 32.5 23 5.18E-03 55.1 23 1. 06E-02 25. 5 18 9.02E-03 31.8 12 5.20E-03 43.4 11 2.35E-02 12.9 16 5.34E-03 41.7 17 l.61E-02 21.0 11 5.70E-03 30.9 10 4.74E-03 29.4 7 1.49E-03 81.9 7 1. 57E-03 68. 6 Fit 2.03E-01 4.08E+OO 4.51E+OO 1. 97E+OO 2.90E+OO 3.60E+OO Peak Search Report (continued) Sample ID : G405235061 Pk It Energy Area Bkgnd 35 0 1460.95* 293 16 36 0 1587.68 19 0 37 -0 1764.42 39 0 FWHM 1. 97 2.16 2 .1,IJ Acquisition date Channel Left Pw 2923.21 2916 16 3177.11 3172 11 3531.26 3525 13 Page : 2 3-0CT-2016 05:52:51 Cts/Sec %Err Fit 8.15E-02 6.6 5.28E-03 22.9 1. 08E-02 16.0 Flag: "*" = Peak area was modified by background subtraction Page 4349 of 5809

.. VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:54:39 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 Configuration Analyses by Sample title Sample date Sample ID MXRl 14-DEC-2015 G405235061 SOLID 13:47:00 Acquisition date : Sample quantity 3-0CT-2016 05:52:51 144.23 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report GAMMA20 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 U-235 143.76 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 ' Sample geometry Detector geometry: Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 CE-141 145.44 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:14.55 10.00 0.00 % Peak Energy 0.4% Page 4350 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : G405235061 Acquisition date 3-0CT-2016 05:52:51 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 lQ.66* 1.312E+00 l.049E+Ol 1.049E+Ol 13 _,,27 OK RH-106 621. 93 9.93* 2.582E+OO 6.971E-01 l.205E+OO 87.04 OK 1050.41 1. 56 1. 721E+OO Line Not Found Absent RU-106 621. 93 9.93* 2.582E+00 6.971E-01 l.205E+OO 87.04 OK 1050.41 1. 56 1. 721E+OO Line Not Found Absent CD-109 88.03 3.70* 6. 851E+OO 2.608E-01 4.055E-01 488.47 OK SN-126 64.28 9.60 4.813E+OO l.467E-01 1.467E-01 448.65 OK 86.94 8.90 6.851E+OO 1.084E-01 1.084E-01 488.47 OK 87.57 37.00* 6.851E+OO 2.608E-02 2.608E-02 488.47 OK CE-141 145.44 48.29* 7.360E+OO l.879E-02 9.847E+OO 411.67 OK TL-208 277.37 6.60 4.947E+OO Line Not Found Absent 583.19 85.00* 2.719E+OO 2. 641E-01 2.641E-01 28.47 OK 860.56 12.50 2.0lOE+OO 3.924E-01 3.924E-01 86.73 OK PB-210 46.54 4.25* 2.063E+OO 2.605E+OO 2. 671E+OO 137.44 OK PB-212 74.82 10.28 6.005E+OO 1.057E+OO l.057E+OO 51. 32 OK 77 .11 17.10 6.187E+OO 1.477E+OO 1.477E+OO 21.12 OK 238.63 43.60* 5.554E+OO 8.023E-01 8.023E-01 14.23 OK 300.09 3.30 4.648E+OO 1.625E+OO 1.625E+OO 56.28 OK BI-214 609.32 45.49* 2.627E+OO 9 *. 221E-01 9.224E-01 18.09 OK 1120.29 14.92 1. 635E+OO 1.218E+OO 1.218E+OO 41. 93 OK 1764.49 15.30 1.106E+OO l .131E+OO 1.132E+OO 32.03 OK PB-214 74.82 5.80 5. 996E+OO Line Not Found <<INT Reject 77 .11 9.70 6.187E+OO 2.603E+OO 2.604E+OO 21.12 OK 87.09 3.41 6.836E+OO Line Not Found <<INT Reject 242.00 7.25 5.503E+OO l.040E+OO 1.040E+OO 47.31 OK 295.22 18.42 4.710E+OO 1.296E+OO 1.297E+OO 18.01 OK 351.93 35.60* 4.084E+OO 1.185E+OO 1.185E+OO 13.60 OK RN-222 609.32 45.49* 2.627E+OO 9.221E-01 9.224E-01 18.09 OK 1120.29 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 OK 1764.49 15.30 1.106E+OO 1.131E+OO 1.132E+OO 32.03 OK RA-226 609.32 45.49* 2.627E+00 9.221E-01 9.224E-01 18.09 OK 1120. 29 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 OK 1764.49 15.30 1.106E+OO 1.131E+OO 1.132E+OO 32.03 OK TH-228 74.82 10.28 6.005E+OO 1.057E+OO 1.057E+OO 51. 32 OK 77 .11 17.10 6.187E+OO 1.477E+OO 1.477E+OO 21.12 OK 238.63 43.60* 5.554E+OO 8.023E-01 8.023E-01 14.23 OK 300.09 3.30 4.648E+OO 1.625E+OO 1.625E+OO 56.28 OK TH-230 609.32 45.49* 2.627E+OO 9. 221E-01 9.221E-01 18.09 OK 1120.29 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41.93 OK 1764.49 15.30 1.106E+OO 1.131E+OO l.131E+OO 32.03 OK PA-231 283.69 1. 70 4.860E+OO Line Not Found Absent 301.36 5.35* 4.648E+OO 1. 003E+OO 1.003E+OO 56.28 OK TH-234 63.29 3.70* 4.813E+OO 3.806E-01 3.806E-01 448.65 OK 92.59 4.23 7.094E+OO 1.596E+OO 1. 596E+OO 89.29 OK U-234 609.32 45.49* 2.627E+OO 9.221E-01 9.221E-01 18.09 OK 1120.29 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 OK 1764.49 15.30 l.106E+OO 1.131E+OO l .131E+OO 32.03 OK U-235 89. 96 3.47 6.978E+OO Line Not Found Absent 93.35 5.60 7.094E+OO 1.205E+OO l.205E+OO 89.29 OK Page 4351 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235061 Acquisition date Nuclide Type: Nuclide U-238 AM-243 ANH-511 Energy 143.76 163.33 185. 72 205.31 63. 29 92.59 43.53 74.66 511.00 %Abn 5.08 57.20 5.01 3.70* 4.23 5.90 67.20* 100.00* Flag: "*" = Keyline Page 4352 of 5809 Uncorrected Decay Corr %Eff pCi/GRAM pCi/GRAM 7.370E+OO Line Not Found 7.024E+OO Line Not Found 6.562E+OO 1.374E-01 1. 374E-01 6. l 71E+OO Line Not Found 4.813E+OO 3.806E-01 3.806E-01 7.094E+OO 1. 596E+OO 1.596E+OO 1.315E+OO Line Not Found 6.005E+OO 1.618E-01 1.618E-01 3.020E+OO 1.028E-01 1.028E-01 Page : 3 3-0CT-2016 05:52:51 2-Sigma %Error Status Reject Absent 54.37 OK Absent 448.65 OK 89.29 OK Absent 51. 32 OK 56.43 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:54:41.50 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l *
  • Acquisition date 3-0CT-2016 05:52:51 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.55 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:47:00 Analyst initials: MXRl *
  • Sample ID G405235061 Sample Quantity l.4423E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKAl'OO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 049E+Ol 1. 365E+OO RH-106 l.205E+OO 1. 028E+OO RU-106 l.205E+OO 1. 028E+OO CD-109 4.055E-01 1. 941E+OO SN-126 2.608E-02 l.249E-01 CE-141 9.847E+OO 3.973E+Ol TL-208 2.641E-01 7.368E-02 PB-210 2.671E+OO 3.598E+OO PB-212 8.023E-01 l .119E-01 BI-214 9.224E-01 l.635E-01 PB-214 l.185E+OO l.580E-01 RN-222 9.224E-01 l.635E-01 RA-226 9.224E-01 l.635E-01 TH-228 8.023E-01 l .119E-01 TH-230 9.221E-01 l.635E-01 PA-231 l.003E+OO 5.530E-01 TH-234 3.806E-01 l.673E+OO U-234 9.221E-01 l.635E-01 U-235 2.202E-01 3.258E-01 U-238 3.806E-01 l.673E+OO AM-243 l.618E-01 8.137E-02 ANH-511 l.028E-01 5.685E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4353 of 5809 Key-Line Activity (pCi/GRAM 2.103E+OO 2.263E-02 O.OOOE+OO 3.341E-03 l.455E-01 O.OOOE+OO O.OOOE+OO l .118E-02 K.L. Cnt Uncert ( 1. 96-sigma) 8.541E+OO 3.835E-02 1. 960E+41 2.llOE-02 3.348E-01 l.073E+04 2.904E+02 5.531E-02 MDA (pCi/GRAM 6.736E-01 8.265E-01 8.265E-01 l.693E+OO l.092E-01 3. 272E+Ol 5.153E-02 2.670E+OO 9.156E-02 l.144E-01 l.019E-01 l.144E-01 l.144E-01 9.156E-02 l.143E-01 5.207E-01 1. 517E+OO l.143E-01 3.296E-01 l.517E+OO 7. llOE-02 4.379E-02 MDA (pCi/GRAM l.735E+Ol 8.532E-02 O.OOOE+OO 5.056E-02 6.793E-01 O.OOOE+OO O.OOOE+OO l.083E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1.252E-01 4.148E-01 8.212E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -1.944E-02 4.150E-02 7.234E-02 NOT IDENT. C0-58 -1.763E-01 4.682E-01 8.355E-01 NOT IDENT. FE-59 1.482E+00 6.619E+OO l.333E+Ol NOT IDENT. C0-60 2.241E-02 3.014E-02 7.007E-02 FAIL ABUN ZN-65 5.364E-02 1.523E-01 2.933E-01 NOT IDENT. GE-68 -1. 2 61E-01 l.861E+OO 3.752E+OO NOT IDENT. AS-73 -5.461E-01 4.568E+OO 8.583E+OO NOT IDENT. AS-74 O.OOOE+OO 4.121E+03 O.OOOEt-00 SHORT HLIF SE-75 -7.514E-03 l.710E-01 3 .196E-01 NOT IDENT. BR-77 O.OOOE+OO 3.342E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 4.979E+02 O.OOOE+OO SHORT HLIF RB-83 -2.305E-01 5.087E-01 9.239E-01 NOT IDENT. KR-85 5 .112E+OO 5.638E+OO 1.141E+Ol NOT IDENT. SR-85 5.040E-01 5.581E-01 l.129E+OO NOT IDENT. RB-86 O.OOOE+OO 1. 716E+04 O.OOOE+OO SHORT HLIF Y-88 3.545E-02 2.028E-01 4.448E-01 NOT IDENT. Y-91 2.840E+02 4.399E+02 9.527E+02 NOT IDENT. NB-94 1.661E-02 3.025E-02 6.099E-02 NOT IDENT. NB-95 2.592E-02 7.292E-01 1. 379E+OO NOT IDENT. NB-95M 8.731E-01 2.068E+OO 3.784E+OO NOT IDENT. ZR-95 9.818E-01 1.218E+OO 2.454E+OO FAIL ABUN NB-97 O.OOOE+OO l.259E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 689E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.388E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 2.804E-03 3.232E-02 5.442E-02 NOT IDENT. RH-102 -2.559E-02 5.229E-02 9.278E-02 NOT IDENT. RU-103 -2.462E-02 4.020E+OO 7.849E+OO FAIL ABUN AG-108M 7.692E-04 2.295E-02 4.483E-02 FAIL ABUN AG-llOM -3. 411E-02 8.526E-02 1.504E-01 FAIL ABUN SN-113 6.533E-02 l.539E-01 3.220E-01 NOT IDENT. CD-115 O.OOOE+OO 3.473E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 6.443E+04 O.OOOE+OO SHORT HLIF TE-123M -3.991E-02 1.152E-01 2.000E-01 NOT IDENT. SB-124 -8.677E-01 1. 251E+OO 2.061E+OO FAIL ABUN SB-125 6.802E-02 8.319E-02 l.778E-01 NOT IDENT. TE-125M 3.041E+Ol 2.320E+02 4.273E+02 NOT IDENT. I-126 O.OOOE+OO 5.188E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6.290E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.595E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.524E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.028E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 8.026E+25 O.OOOE+OO SHORT HLIF BA-133 4.539E-02 5.178E-02 6.865E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 7.700E-02 9.666E-02 FAIL ABUN CS-135 4.088E-02 l.409E-01 2.537E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 1. 572E+05 O.OOOE+OO SHORT HLIF BA-137M 2.377E-02 3.696E-02 7.412E-02 NOT IDENT. CS-137 2. 511E-02 3.904E-02 7.830E-02 NOT IDENT. CE-139 -6.957E-03 9. 511E-02 1.694E-01 NOT IDENT. BA-140 O.OOOE+OO 6.666E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.283E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 1.281E+41 O.OOOE+OO SHORT HLIF CE-144 -2.494E-02 2.867E-01 5.177E-01 NOT IDENT. PM-144 -4.298E-03 4.781E-02 8.976E-02 NOT IDENT. PR-144 -3.856E-01 4 .137E+OO 7.764E+OO NOT IDENT. PM-146 -3.211E-03 3.908E-02 7.458E-02 NOT IDENT. ND-147 O.OOOE+OO l.810E+07 O.OOOE+OO SHORT HLIF PM-147 l.414E+02 7.047E+02 l.308E+03 NOT IDENT. PM-149 O.OOOE+OO 5.532E+39 O.OOOE+OO SHORT HLIF EU-150 -1. 318E-02 2.075E-02 3.774E-02 FAIL ABUN EU-152 3.094E-02 7.822E-02 1.583E-01 NOT IDENT. GD-153 -5.501E-02 l.629E-01 2.674E-01 NOT IDENT. EU-154 3.306E-02 9.801E-02 2.084E-01 FAIL ABUN EU-155 7.278E-02 9 .118E-02 l.782E-01 FAIL ABUN TB-160 4.628E-01 1. 511E+OO 3.047E+OO FAIL ABUN H0-166M -7.262E-03 4.619E-02 8.655E-02 NOT IDENT. TM-171 -3.157E+OO 1.160E+Ol 2.151E+Ol NOT IDENT. HF-172 -2 .114E-02 2.275E-01 3.755E-01 FAIL ABUN LU-172 1.170E-02 8.097E-02 1.618E-01 FAIL ABUN LU-176 -l.219E-03 1. 764E-02 3.133E-02 FAIL ABUN HF-181 1.071E+OO 3.102E+OO 6.336E+OO NOT IDENT. TA-182 -2.480E-01 7.955E-01 1.499E+OO FAIL ABUN RE-183 6.950E-01 1. 742E+OO 3.381E+00 NOT IDENT. Page 4354 of 5809 RE-184 1. 265E+01 2.306E+Ol 4.817E+Ol NOT IDENT. W-188 2.977E+01 8.254E+Ol 1.544E+02 FAIL ABUN IR-192 9.261E-02 3.407E-01 6.881E-01 FAIL ABUN HG-203 -1.126E+00 1.852E+OO 3.412E+OO NOT IDENT. BI-207 9.041E-03 4.043E-02 8.457E-02 FAIL ABUN BI-211 O.OOOE+OO 4.353E-01 8.295E-01 FAIL ABUN PB-211 -6.994E-02 5.213E-01 l.002E+OO NOT IDENT. BI-212 8.436E-01 5.042E-01 1.119E+OO NOT IDENT. RN-219 4.697E-02 3.294E-01 6.471E-01 FAIL ABUN RA-223 -1.475E-01 4. 7.06E-01 8.903E-01 FAIL ABUN RA-224 O.OOOE+OO 8.524E-01 1.364E+OO FAIL ABUN AC-227 -1.198E-01 1. 890E-01 3. 496E-01 FAIL ABUN TH-227 -1.198E-01 1. 890E-01 3.496E-01 FAIL ABUN AC-228 0.000E+OO 2.267E-01 4.972E-01 FAIL ABUN RA-228 O.OOOE+OO 2.267E-01 4.972E-01 FAIL ABUN TH-229 -l.695E-01 3.839E-01 7.320E-01 FAIL ABUN TH-231 -1. 475E-01 4.706E-01 8.903E-01 FAIL ABUN TH-232 O.OOOE+OO 2.267E-01 4.972E-01 FAIL ABUN PA-233 -l.104E-02 4.417E-02 8.476E-02 FAIL ABUN PA-234 2.651E-02 1.818E-01 3.933E-01 FAIL ABUN PA-234M 6.646E+OO 5.427E+OO 7.908E+OO FAIL ABUN NP-237 -l.104E-02 4.417E-02 8.476E-02 FAIL ABUN NP-238 O.OOOE+OO 6.108E+40 O.OOOE+OO SHORT HLIF NP-239 -7.460E-02 2.160E-01 3.816E-01 NOT IDENT. PU-239 2.427E+02 4.952E+02 5.470E+02 FAIL ABUN AM-241 1. 781E-02 9.076E-02 1.726E-01 NOT IDENT. CM-243 -9.227E-03 8.586E-02 l.559E-01 NOT IDENT. BK-247 -3.439E-03 6.820E-02 1.193E..:.01 NOT IDENT. CM-247 9.215E-03 2.991E-02 5.985E-02 NOT IDENT. CF-249 -7.496E-03 2.820E-02 5.354E-02 NOT IDENT. CF-251 5.177E-03 9.199E-02 1. 831E-01 NOT IDENT. Page 4355 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:54:37.31 Nuclide Line Activity Report Nuclide Type: 4 Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 282 10.66* l.312E+OO 1.049E+Ol 1.049E+Ol 13.27 RH-106 621. 93 34 9.93* 2.582E+OO 6. 971E-01 1.205E+OO 87.04 1050.41 ------1. 56 1. 721E+OO ------Line Not Found ------RU-106 621. 93 34 9.93* 2.582E+OO 6. 971E-01 1.205E+OO 87.04 1050.41 ------1. 56 1. 721E+OO ------Line Not Found ------CD-109 88.03 69 3.70* 6.851E+OO 1.412E+OO 2.195E+00 89.18 SN-126 64.28 13 9.60 4.813E+OO 1.467E-01 l.467E-01 448.65 86.94 69 8.90 6.851E+OO 5.870E-01 5.870E-01 89.18 87.57 69 37.00* 6. 851E+OO 1.412E-01 l.412E-01 89.18 CE-141 145.44 34 48.29* 7.360E+OO 4.997E-02 2.619E+Ol 151. 00 TL-208 277.37 ------6.60 4.947E+OO ------Line Not Found ------583.19 117 85.00* 2.719E+OO 2.641E-01 2. 641E-01 28.47 860.56 19 12.50 2.0lOE+OO 3.924E-01 3.924E-01 86.73 PB-210 46.54 44 4.25* 2.063E+OO 2.605E+00 2. 671E+OO 137.44 BI-211 72. 87 ------1. 23 5.823E+OO ------Line Not Found ------. 351. 06 331 12.92* 4.084E+00 3.265Ef00 3.265E+OO 13.60 PB-212 74.82 209 10.28 6.005E+OO 1. 762E+OO 1. 762E+00 30.05 77 .11 300 17.10 6.187E+OO 1.477E+OO 1. 477E+OO 21.12 238.63 373 43.60* 5.554E+00 8.023E-01 8.023E-01 14.23 300.09 48 3.30 4.648E+OO l.625E+OO 1.625E+OO 56.28 BI-214 609.32 212 45.49* 2.627E+OO 9.221E-01 9.224E-01 18.09 1120.29 57 14.92 1.635E+OO l.218E+OO l.218E+00 41. 93 1764.49 37 15.30 1.106E+OO l .131E+OO 1.132E+OO 32.03 PB-214 74.82 209 5.80 6.005E+OO 3.123E+00 3.124E+OO 30.05 77 .11 300 9.70 6.187E+OO 2.603E+OO 2.604E+OO 21.12 87.09 69 3.41 6.851E+00 1. 532E+OO l.533E+OO 89.18 242.00 80 7.25 5.503E+OO l.040E+00 1.040E+OO 47.31 295.22 216 18.42 4. 710E+00 l.296E+OO 1.297E+OO 18.01 351.93 331 35.60* 4.084E+00 l.185E+OO 1.185E+OO 13.60 RN-222 609.32 212 45.49* 2.627E+00 9. 221E-01 9.224E-01 18.09 1120.29 57 14.92 1.635E+OO l.218E+OO 1.218E+00 41. 93 1764.49 37 15.30 1.106E+OO 1.131E+OO 1.132E+OO 32.03 RA-224 240.99 80 4.10* 5.503E+OO 1.838E+OO 1.838E+OO 47.31 RA-226 609.32 212 45.49* 2.627E+OO 9. 221E-01 9.224E-01 18.09 1120.29 57 14.92 1.635E+OO l.218E+OO 1.218E+OO 41. 93 1764.49 37 15.30 1.106E+OO 1.131E+OO 1.132E+OO 32.03 TH-228 74.82 209 10.28 6.005E+OO 1. 762E+OO 1.762E+OO 30.05 77 .11 300 17.10 6.187E+OO 1.477E+OO 1.477E+OO 21.12 238.63 373 43.60* 5.554E+OO 8.023E-01 8.023E-01 14.23 300.09 48 3.30 4.648E+OO 1.625E+OO 1.625E+OO 56.28 TH-230 609.32 212 45.49* 2.627E+00 9.221E-01 9.221E-01 18.09 1120.29 57 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 1764.49 37 15.30 1.106E+OO 1.131E+OO 1.131E+OO 32.03 PA-231 283.69 ------1. 70 4.860E+OO ------Line Not Found ------301.36 48 5.35* 4.648E+OO 1.003E+OO 1. 003E+OO 56.28 TH-234 63.29 13 3.70* 4.813E+00 3.806E-01 3.806E-01 448.65 92.59 92 4.23 7.094E+OO 1. 596E+OO 1.596E+OO 89.29 Page 4356 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235061 Acquisition date Page : 2 3-0CT-2016 05:52:51 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error U-234 609.32 212 45.49* 2.627E+OO 9.221E-01 9.221E-01 18.09 1120.29 57 14.92 1.635E+OO 1.218E+OO 1.218E+OO 41. 93 1764.49 37 15.30 1.106E+OO 1.131E+OO 1.131E+OO 32.03 U-235 89. 96 ------3.47 6.978E+OO ------Line Not Found ------93.35 92 5.60 7.094E+OO 1.205E+OO 1.205E+OO 89.29 143.76 34 10. 96* 7.360E+OO 2.202E-01 2.202E-01 151.00 163.33 ------5.08 7.024E+OO ------Line Not Found ------185.72 99 57.20 6.562E+OO 1.374E-01 1.374E-01 54.37 205.31 ------5.01 6 .171E+OO ------Line Not Found ------U-238 63.29 13 3.70* 4.813E+OO 3.806E-01 3.806E-01 448.65 92.59 92 4.23 7.094E+OO 1. 596E+OO 1.596E+OO 89.29 AM-243 43.53 ------5.90 1.315E+OO ------Line Not Found ------74.66 209 67.20* 6.005E+OO 2.696E-01 2.696E-01 30.05 ANH-511 511. 00 60 100.00* 3.020E+OO 1.028E-01 1.028E-01 56.43 Flag: "*" Key line Page 4357 of 5809 Summary of Nuclide Activity Sample ID : G405235061 Acquisition date Page : 3 3-0CT-2016 05:52:51 Total number of lines in spectrum 37 Number of unidentified lines 5 Number of lines tentatively identified by NID 32 Nuclide Type : Nuclide K-40 RH-106 RU-106 CD-109 SN-126 CE-141 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 371. 80D 371. 80D 461. 40D 2.30E+05Y 32.51D l.41E+l0Y 22.20Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 73 1. 73 1. 55 1. 00 524. 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.049E+Ol 6.971E-01 6.971E-01 l.412E+00 l.412E-01 4.997E-02 2.641E-01 2.605E+00 3.265E+OO 8.023E-01 9.221E-01 l.185E+OO 9.221E-01 1.838E+OO 9. 221E-01 8.023E-01 9.221E-01 1.003E+OO 3.806E-01 9.221E-01 2.202E-01 3.806E-01 2.696E-01 l.028E-01 3.122E+Ol 3.122E+Ol Decay Corr pCi/GRAM 1.049E+Ol l.205E+OO 1.205E+OO 2.195E+OO l.412E-01 2.619E+Ol 2.641E-01 2.671E+OO 3.265E+OO 8.023E-01 9.224E-01 l.185E+00 9.224E-01 1.838E+OO 9.224E-01 8.023E-01 9.221E-01 1.003E+OO 3.806E-01 9. 221E-01 2.202E-01 3.806E-01 2.696E-01 l.028E-01 5.923E+Ol 5.923E+Ol 86.49% Decay Corr 2-Sigma Error 0.139E+Ol 1.049E+OO 1.049E+OO 1.957E+OO l.259E-01 3.955E+Ol 0.752E-01 3.671E+OO 0.444E+00 l.142E-01 1.669E-01 0.161E+OO l.669E-01 0.870E+OO l.669E-01 1.142E-01 l.668E-01 0.564E+OO 17.08E-01 l.668E-01 3.324E-01 17.08E-01 0.810E-01 0.580E-01 "M" Manually accepted 2-Sigma %Error 13.27 87.04 87.04 89.18 89.18 151.00 28.47 137. 44 13.60 14.23 18.09 13.60 18.09 47.31 18.09 14.23 18.09 56.28 448.65 18.09 151.00 448.65 30.05 56.43 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4358 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235061 Acquisition date : 3-0CT-2016 05:52:51 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 129.70 22 140 1. 40 259.47 253 8 5.17E-03 **** 7.53E+oo* T 0 209.70 24 102 1. 39 419.38 415 8 5.92E-03 **** 6.08E+OO T 0 270.20 48 79 1. 58 540.33 535 9 1.20E-02 77.1 5.05E+OO T A 304. 96 26 24 2.01 609.83 ,/595 21 6.44E-03 **** 4.59E+OO T 2 356.36 21 32 1. 71 712. 60 697 19 5.26E-03 **** 4.04E+OO T 0 723. 27 69 43 11. 05 1446.45 1431 31 1.85E-02 64.9 2.30E+OO T 1 763.00 19 31 1. 83 1525.94 1518 23 5.18E-03 **** 2.21E+OO T 1 768.40 39 21 1. 84 1536.75 1518 23 1.06E-02 51.1 2.19E+OO 0 796.11 33 14 3. 96 1592.18 1583 18 9.02E-03 63.6 2.14E+OO T 0 911. 42 85 8 1. 78 1822.93 1818 11 2.35E-02 25.9 1.92E+OO T 0 1001.94 19 8 3.13 2004.11 1994 16 5.34E-03 83.3 1.79E+OO T 0 1156.21 20 4 2.57 2312.95 2308 11 5.70E-03 61. 7 1. 59E+OO 0 1305. 58 17 2 3.63 2612.04 2608 10 4.74E-03 58.8 1. 44E+OO 0 1320.12 5 5 1. 29 2641.15 2636 7 1.49E-03 **** 1. 43E+OO 0 1332. 48 5 3 1. 23 2665.90 2661 7 1.57E-03 **** 1. 42E+OO T 0 1587.68 18 0 2.16 3177.11 3172 11 5.28E-03 45.9 1.22E+OO Flags: "T" = Tentatively associated Page 4359 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:54:54.27 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l * *Acquisition date 3-0CT-2016 05:52:51 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 * *Elapsed.live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.55 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:47:00 Nuclide Library : SOLID *
  • Sample ID G405235061 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4423E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : "DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 RH-106 RU-106 CD-109 SN-126 CE-141 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-226 TH-228 TH-230 PA-231 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.863E-01 3.648E-01 3.648E-01 8.009E-01 5.169E-02 1. 52 6E+Ol 2.265E-02 1.242E+OO 4.275E-02 5 .116E-02 4.594E-02 5 .116E-02 5 .116E-02 4.275E-02 5 .114E-02 2.308E-01 7.161E-01 5 .114E-02 1.557E-01 7.161E-01 3.369E-02 l.950E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4360 of 5809 Le (pCi/GRAM 7.678E+OO 3.670E-02 O.OOOE+OO 1. 87 5E-02 2.983E-01 O.OOOE+OO 0.000E+OO 4.749E-02 3.616E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 Rff-102 RU-103 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 Page 4361 of 5809 O.OOOE+OO 3.375E-02 3.573E-01 5.929E+OO 2.949E-02 1. 269E-01 1.598E+OO 4.012E+00 O.OOOE+OO 1.465E-01 O.OOOE+OO O.OOOE+OO 4.047E-01 5.123E+OO 5.068E-01 O.OOOE+OO 1.775E-01 4.190E+02 2.744E-02 6 .112E-01 1.766E+OO 1.084E+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 2.550E-02 4.055E-02 3.465E+OO 2.009E-02 6.390E-02 l.435E-01 O.OOOE+OO 0.000E+OO 9.318E-02 6.516E-01 8.036E-02 2.010E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.127E-02 O.OOOE+OO 4.320E-02 l.179E-01 O.OOOE+OO O.OOOE+OO 3.376E-02 3.566E-02 7.890E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.406E-01 3.954E-02 3.420E+OO 3.358E-02 0.000E+OO 6 .116E+02 0.000E+OO 1. 706E-02 7.229E-02 1.254E-01 8.953E-02 8.378E-02 1.323E+OO 3.757E-02 1. 006E+Ol 1.760E-01 7.180E-02 1. 396E-02 2.822E+OO 6.474E-01 1.591E+OO 2.104E+Ol SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NQT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 RA-224 AC-227 TH-227 AC-228 RA-228 TH-229 TH-231 TH-232 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4362 of 5809 7.014E+Ol 3.128E-01 1.562E+OO 3.660E-02 4.012E-01 4.481E-01 5.129E-01 2.935E-01 4.033E-01 6. 496E-01 l.601E-01 1.601E-01 2.343E-01 2.343E-01 3.399E-01 4.033E-01 2.343E-01 3.817E-02 1.648E-01 3.480E+00 3.817E-02 O.OOOE+OO l.784E-01 2.579E+02 8.140E-02 7.306E-02 5.489E-02 2.717E-02 2.385E-02 8. 521E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:54:59.66 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235061.CNF;l *
  • Acquisition date 3-0CT-2016 05:52:51 Sensitivity : 3.000 *
  • Detector ID GAM20 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:14.55 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:47:00 Nuclide Library : SOLID *
  • Sample ID G405235061 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : l.4423E+02 GRAM *
  • Quantity Err(%) : l.3866E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 30-JUN-2016 06:52:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM20 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l.049E+Ol l.471E+OO RH-106 l.205E+OO 1. 031E+OO RU-106 l.205E+OO l.031E+OO CD-109 4.084E-01 l.954E+OO SN-126 2.627E-02 l.257E-01 CE-141 9.847E+OO 3.975E+Ol TL-208 2.641E-01 7.453E-02 PB-210 2. 671E+OO 3.604E+OO PB-212 8.023E-01 l.197E-01 BI-214 9.224E-01 l.682E-01 PB-214 l.185E+OO l.655E-01 RN-222 9.224E-01 l.682E-01 RA-226 9.224E-01 l.682E-01 TH-228 8.023E-01 l.197E-01 TH-230 9. 221E-01 l.682E-01 PA-231 l.003E+OO 5.929E-01 TH-234 3.806E-01 1. 675E+OO U-234 9.221E-01 l.682E-01 U-235 2.202E-01 3.260E-01 U-238 3.806E-01 1. 675E+OO AM-243 l.619E-01 8.306E-02 ANH-511 l.028E-01 5. 701E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4363 of 5809 Key-Line Activity (pCi/GRAM ) . 2.103E+OO 2.263E-02 l.OOOE+41 3.341E-03 l.455E-01 -9.514E+02 3.303E+Ol 1. 118E-02 K.L Act error ( 1. 96-sigma) 8.542E+OO 3.836E-02 3.879E+41 2. lllE-02 3.349E-01 l.073E+04 2.904E+02 5.532E-02 TPU ( 1. 96-sigma) l.471E+OO 1. 031E+OO 1. 031E+OO l.954E+OO l.257E-01 3.975E+Ol 7.453E-02 3.604E+OO l.197E-01 l.682E-01 l.655E-01 l.682E-01 l.682E-01 l.197E-01 l.682E-01 5.929E-01 1. 67 5E+OO l.682E-01 3.260E-01 l.675E+OO 8.306E-02 5.701E-02 TPU (1.9()-sigma) 8.594E+OO 3. 969E-02 O.OOOE+OO 2 .116E-02 3.412E-01 l.074E+04 2.908E+02 5.555E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 1.252E-01 4.148E-01 4.187E-01 NOT IDEN'.['. MN-56 l.000E+41 3.350E+41 O.OOOE+OO SHORT HLIF C0-57 -l.944E-02 4 .151E-02 4.243E-02 NOT IDENT. C0-58 -1. 7 63E-01 4.682E-01 4.749E-01 NOT IDENT. FE-59 1.482E+OO 6.620E+OO 6.653E+OO NOT IDENT. C0-60 2.241E-02 3.015E-02 3.180E-02 FAIL ABUN ZN-65 5.364E-02 1.523E-01 l.542E-01 NOT IDENT. GE-68 -1. 2 61E-01 1. 8 61E+OO 1.862E+OO NOT IDENT. AS-73 -5.461E-01 4.569E+OO 4.576E+OO NOT IDENT. AS-74 1.281E+02 4.121E+03 4.122E+03. SHORT HLIF SE-75 -7.514E-03 1. 710E-01 1.711E-01 NOT IDENT. BR-77 2.395E+37 2.031E+38 O.OOOE+OO SHORT HLIF SR-82 -3.985E+02 4.983E+02 5.296E+02 SHORT HLIF RB-83 -2.305E-01 5.097E-01 5.202E-01 NOT IDENT. KR-85 5 .112E+OO 5.642E+OO 6.094E+OO NOT IDENT. SR-85 5.040E-01 5.584E-01 6.029E-01 NOT IDENT. RB-86 -5.600E+03 l.716E+04 l.735E+04 SHORT HLIF Y-88 3.545E-02 2.028E-01 2.034E-01 NOT IDENT. Y-91 2.840E+02 4.401E+02 4.583E+02 NOT IDENT. NB-94 l.661E-02 3.025E-02 3. ll 7E-02 NOT IDENT. NB-95 2.592E-02 7.292E-01 7.293E-01 NOT IDENT. NB-95M 8.731E-01 2.069E+OO 2.106E+OO NOT IDENT. ZR-95 9.818E-01 1.219E+OO l.297E+OO FAIL ABUN NB-97 l.000E+41 1.260E+41 O.OOOE+OO SHORT HLIF ZR-97 1. 000E+41 1. 689E+41 O.OOOE+OO SHORT HLIF M0-99 -l.627E+30 3.388E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 2.919E+41 O.OOOE+OO SHORT HLIF RH-101 2.804E-03 3.232E-02 3.235E-02 NOT IDENT. RH-102 -2.559E-02 5.233E-02 5.359E-02 NOT IDENT. RU-103 -2.462E-02 4.020E+OO 4.020E+OO FAIL ABUN AG-108M 7.692E-04 2.295E-02 2.295E-02 FAIL ABUN AG-llOM -3. 411E-02 8.528E-02 8.665E-02 FAIL ABUN SN-113 6.533E-02 1.540E-01 l.568E-01 NOT IDENT. CD-115 -1.109E+38 3.478E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -l.240E+04 6.445E+04 6.469E+04 SHORT HLIF TE-123M -3.991E-02 1.153E-01 l.167E-01 NOT IDENT. SB-124 -8.677E-01 1.252E+OO 1. 311E+OO FAIL ABUN SB-125 6.802E-02 8.323E-02 8.870E-02 NOT IDENT. TE-125M 3.041E+Ol 2.320E+02 2.324E+02 NOT IDENT. I-126 2.887E+05 5.203E+05 5.363E+05 SHORT HLIF SB-126 -2.392E+05 6.305E+05 6.397E+05 SHORT HLIF SB-127 -3.615E+21 8.197E+21 O.OOOE+OO SHORT HLIF I-131 4.626E+07 2.524E+09 2.524E+09 SHORT HLIF I-132 -1.000E+41 1. 813E+42 O.OOOE+OO SHORT HLIF TE-132 5.459E+25 8.315E+25 O.OOOE+OO SHORT HLIF BA-133 4.539E-02 5 .181E-02 5.571E-02 FAIL ABUN I-133 -1.000E+41 6.569E+41 O.OOOE+OO SHORT HLIF CS-134 l.235E-01 7.718E-02 9.516E-02 FAIL ABUN CS-135 4.088E-02 l.409E-01 l.421E-01 NOT IDENT. I-135 1.000E+41 7.522E+41 O.OOOE+OO SHORT HLIF CS-136 5.635E+04 l.573E+05 1.594E+05 SHORT HLIF BA-137M 2.377E-02 3.697E-02 3.850E-02 NOT IDENT. CS-137 2. 511E-02 3.906E-02 4.067E-02 NOT IDENT. CE-139 -6.957E-03 9.512E-02 9.517E-02 NOT IDENT. BA-140 -1.382E+05 6.667E+05 6. 696E+05 SHORT HLIF LA-140 -4.039E+04 2.283E+05 2.291E+05 SHORT HLIF CE-143 l.000E+41 1.284E+41 O.OOOE+OO SHORT HLIF CE-144 -2.494E-02 2.867E-01 2.869E-01 NOT IDENT. PM-144 -4.298E-03 4.781E-02 4.785E-02 NOT IDENT. PR-144 -3.856E-01 4.137E+OO 4.141E+OO NOT IDENT. PM-146 -3. 211E-03 3.909E-02 3. 911E-02 NOT IDENT. ND-147 8.346E+06 1. 811E+07 l.850E+07 SHORT HLIF PM-147 1.414E+02 7.047E+02 7.076E+02 NOT IDENT. PM-149 -1. 701E+39 5.545E+39 O.OOOE+OO SHORT HLIF EU-150 -l.318E-02 2.076E-02 2.159E-02 FAIL ABUN EU-152 3.094E-02 7.824E-02 7.947E-02 NOT IDENT. GD-153 -5.501E-02 1.629E-01 l.648E-01 NOT IDENT. EU-154 3.306E-02 9.802E-02 9.915E-02 FAIL ABUN EU-155 7.278E-02 9.132E-02 9.704E-02 FAIL ABUN TB-160 4.628E-01 1.511E+OO 1.526E+OO FAIL ABUN H0-166M -7.262E-03 4.620E-02 4.631E-02 NOT IDENT. TM-171 -3.157E+00 1.160E+Ol 1.169E+Ol NOT IDENT. HF-172 -2 .114E-02 2.275E-01 2.277E-01 FAIL ABUN LU-172 1.170E-02 8.098E-02 8 .115E-02 FAIL ABUN LU-176 -l.219E-03 1. 764E-02 1.764E-02 FAIL ABUN HF-181 1.071E+OO 3.103E+00 3.140E+OO NOT IDENT. TA-182 -2.480E-01 7.956E-01 8.034E-01 FAIL ABUN RE-183 6.950E-01 1.746E+OO 1.774E+OO NOT IDENT. Page 4364 of 5809 RE-184 1. 265E+Ol 2.325E+Ol 2.394E+Ol NOT IDENT. W-188 2.977E+01 8.261E+Ol 8.369E+Ol FAIL ABUN IR-192 9. 2 61E-02 3.408E-01 3.433E-01 FAIL ABUN HG-203 -1.126E+OO l.852E+OO 1. 921E+OO NOT IDENT. BI-207 9.041E-03 4.044E-02 4.064E-02 FAIL ABUN BI-211 3.265E+OO 4.589E-01 1.542E+OO FAIL ABUN PB-211 -6.994E-02 5.213E-01 5.222E-01 NOT IDENT. BI-212 8.436E-01 5.060E-01 6.330E-01 NOT IDENT. RN-219 4.697E-02 3.295E-01 3.301E-01 FAIL ABUN RA-223 -l.475E-01 4.706E10l 4.753E-01 FAIL ABUN RA-224 1.838E+OO 8.580E-01 1.193E+OO FAIL ABUN AC-227 -1.198E-01 1. 897E-01 l.972E-01 FAIL ABUN TH-227 -1.198E-01 l.897E-01 1. 972E-01 FAIL ABUN AC-228 8.942E-01 2.313E-01 4.647E-01 FAIL ABUN RA-228 8.942E-01 2. 313E-01 4.647E-01 FAIL ABUN TH-229 -1.695E-01 3.840E-01 3.915E-01 FAIL ABUN TH-231 -1.475E-01 4.706E-01 4.753E-01 FAIL ABUN TH-232 8.942E-01 2.313E-01 4.647E-01 FAIL ABUN PA-233 -l.104E-02 4.417E-02 4.445E-02 FAIL ABUN PA-234 2. 651E-02 l.843E-01 1.847E-01 FAIL ABUN PA-234M 6.646E+OO 5.435E+OO 6.206E+OO FAIL ABUN NP-237 -1.104E-02 4.417E-02 4.445E-02 FAIL ABUN NP-238 -4.446E+39 6.108E+40 0.000E+OO SHORT HLIF NP-239 -7.460E-02 2 .161E-01 2.187E-01 NOT IDENT. PU-239. 2.427E+02 4.953E+02 5. 072E+02 FAIL ABUN AM-241 1. 781E-02 9.077E-02 9.112E-02 NOT IDENT. CM-243 -9.227E-03 8.586E-02 8. 596E-02 NOT IDENT. BK-247 *-3.439E-03 6.820E-02 6.822E-02. NOT IDENT. CM-247 9.215E-03 2.995E-02 3.024E-02 NOT IDENT. CF-249 -7. 496E-03 2.820E-02 2.841E-02 NOT IDENT. CF-251 5.177E-03 9.200E-02 9.203E-02 NOT IDENT. Page 4365 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 75.1192 87.09 102.7180 136.47 55.5957 45.60 58.7096 87.57 102.7840 140.51 0.0000 46.54 58.8187 88.03 102.8478 143.76 53.5666 49.72 0.0000 88.34 102.8904 144.24 53.5914 51. 35 69.0737 88.47 102.9079 145.44 65.0358 51.87 77.7827 89. 96 103 .1115 152.43 71.2017 52.39 77.8568 1093.63 103. 2035 153.25 0.0000 52.97 79.0217 91.11 0.0000 323.87 73.7805 53.44 71.5052 92.59 103.4658 156.02 0.0000 54.07 69.4170 93.35 103.5674 158.56 0.0000 57.36 0.0000 94.56 70.6888 159.00 66.6991 57.53 66.5680 94.65 70. 6972 162.33 84.2467 57.98 75.3564 94.67 70.6991 162.66 0.0000 59.27 86.4683 94.87 70.7169 163.33 64.4827 59.32 86.4756 97.43 81. 7423 165.86 63.3866 59.54 86.5078 98.43 74.1235 176.31 61.8789 60. 96 84.8854 98.44 74.1245 176.60 0.0000 61.17 84.9152 99.53 89.3015 177.52 59.4325 62.93 94.7065 100 .11 74.2778 181.07 0.0000 63.29 94.7624 102.03 63.9832 181.52 61.7345 63.58 94.8072 103.18 90.8665 184.41 65. 6729 64.28 94.9150 103.37 76.9047 143.76 69.9595 66.73 112.2775 105.21 63.0612 193.51 66.1664 67.24 84.2754 105.31 63.0687 197.03 51. 8919 125.81 99.1294 106.12 81. 8347 198.01 56.1890 67.75 99.1403 106.47 81. 8689 201.83 63.1910 69.67 113.5360 109.28 79.7931 203.43 65.8351 70.83 102.5868 111. 00 78.7768 205.31 69.3572 72.81 105.8774 111.76 0.0000 210.85 59.3348 72.87 105.8868 114. 06 53.0956 215.65 51.7841 74.66 108.7861 116.30 0.0000 222.11 58.1043 74.82 108.8120 116.74 78.1096 227.09 49.6129 74.97 108.8356 119.76 71.2473 227.38 49.6234 77 .11 109.1768 121.12 64.2181 228.16 0.0000 78.74 97.7757 121.22 64.2251 228.18 40.0703 79.69 96.4017 121. 78 66.6448 116.74 40.0703 80.12 84.4027 122.06 76.1885 235.69 55.1756 80.19 0.0000 122.92 63 .1526 235. 96 55.1859 80.57 93.5052 123.07 60.7796 238.63 66.6995 81. 00 95.0710 265.00 65.5899 238.98 0.0000 81. 07 104.1359 125.81 78.0913 240.99 66.8100 81. 75 102.7242 127.23 71. 8245 242.00 51.4624 83.79 115.1349 127.91 64.6888 244.70 37.0166 84.00 103.0452 129. 30 55.9856 252.40 0.0000 85.43 121. 4673 131.20 59.3022 252.80 36.3363 86.55 102.6432 133.02 63.8303 254.15 0.0000 86.79 102.6762 133.52 60.2486 256.23 51. 5217 86.94 102.6974 136.00 56. 7771 260.90 0.0000 Page 4366 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 41.8060 355.39 0.0000 584.27 17.7512 264.80 41. 8098 356.01 28.2880 595.83 0.0000 265.00 45.5682 364.49 0.0000 427.87 18.9104 2 68. 22 51.0358 366.42 0.0000 602.52 0.0000 269.46 43.9088 372. 51 29.4863 604.72 12.6260 270.03 43.9247. 375.05 27.6206 607.14, 22 .1151 271.23 45.7529 377.52 32.4242 609.32 24.2410 273.65 0.0000 356.01 36.3564 610.33 24.2503 276.40 38.7045 388.16 25.8887 614.28 19.0056 277.37 47.7347 388.63 0.0000 618.01 23.7891 277.60 49.5439 391.69 17.2899 620. 36 19.0481 278.00 46.8531 264.66 31. 8398 621. 93 19.0583 279.20 50.4959 401.81 29.9272 630.19 0.0000 279.54 50.5062 402.40 28.0047 631. 29 22.3099 279.70 44.1979 404.85 26.1046 633.25 18.0729 280.46 39.7067 410.95 31.0313 634.78 0.0000 283.69 32.5532 413.71 20.3916 635.95 21. 2826 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 38.9250 423.72 0.0000 645.85 20.2896 285.90 0.0000 427.09 27.3631 657.76 11. 7 958 287.50 29.9116 427.87 18.5744 657.90 0.0000 290.67 27.2461 433.94 24.5102 661.66 22.5492 293.27 0.0000 439.40 18.6749 664.57 0.0000 351. 93 32.7861 453.88 28.6938 666.33 0.0000 295.96 16.4008 463.37 22.8545 666.50 0.0000 879.38 16.4268 468.07 24.8937 667. 71 0.0000 299.98 20.5508 473.00 0.0000 677. 62 19.4341 300.09 20.5522 475.06 22.9729 685.70 0.0000 300.13 20.5527 476.78 19.9915 695.00 0.0000 301.36 20.5678 477.60 16.9986 696. 49 19.5579 302.85 20.5861 482.18 18.0344 696. 51 19.5579 256.23 20.6067 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 17.3893 306.78 23.3859 497.08 19.1585 697.49 16.3037 308.46 16.5242 505.52 27.3224 702.65 19.5974 311. 90 31. 2760 507.63 0.0000 706.68 23.9846 316.51 29.5156 511.00 22. 3138 711. 68 16.3800 319.41 0.0000 514.00 13.7098 720.70 0.0000 320.08 0.0000 514.00 13.7098 721. 93 0.0000 321. 04 29.5931 520.40 22.4010 722. 78 15.3433 323.87 36.1253 520.69 0.0000 722.91 15.3438 325.23 42.6421 522.65 0.0000 723.31 15.3461 328.76 0.0000 527.90 0.0000 724.19 15.3507 333.37 28.8695 528.26 17.3652 727. 33 15.3660 333.97 40.0588 529.59 20.4411 733.00 11.5455 334.37 50.3174 529.87 0.0000 735.93 7.7044 338.28 34.5520 531. 02 0.0000 333.97 16.5173 338.32 34.5528 537.26 0.0000 739.50 0.0000 311. 90 86.0179 546.56 0.0000 747.24 15.4640 340.48 86.0179 552.55 18.5662 748.06 17.6777 340.55 0.0000 563.25 26.9310 752.31 16.5948 344.28 30.9187 569.33 14.5355 753.82 0.0000 345.93 39.3870 946.00 17.6509 756.73 9.9708 351.06 28.2123 569.70 17.6523 756.80 9.9712 351.93 28.2257 583.19 17.7436 884.68 19.9871 Page 4367 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 19.9980 1274.44 8.5342 1620.50 4.0537 766.42 20.0024 1001.03 5.3403 1621.92 6.0820 766.84 20.0046 1002.74 5.3427 1678.03 0.0000 772. 60 0.0000 1004.73 8.5523 1690.97 4.1033 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.0385 778.90 8.9242 1028.54 0.0000 1063.66 3 .1183 783.70 0.0000 1037.84 14.3730 1771.35 0.0000 785.37 15.6480 1038.76 0.0000 1791.20 0.0000 792.07 15.1199 631.29 9.9030 1808.65 2.0919 794.95 7.8468 1048.07 0.0000 1810.72 0.0000 795.86 7.8491 1049.04 9.9083 1836.06 4.2021 810.06 11. 2606 1050.41 6.3074 810.29 12.3875 1063.66 11. 7 519 344.28 14.6403 1077.00 0.0000 810.76 15.7682 1077.34 11. 7 908 815.77 0.0000 1085.87 13.6331 1048.07 0.0000 1093.63 19.1210 832.01 11. 3338 1099.45 19.1479 834.85 14.7461 1112. 07 12.5416 835.71 12.4806 1112. 84 10.2443 836.80 0.0000 1115. 54 10.2512 846.75 0.0000 1120.29 11. 9114 846.77 14.7969 1120. 55 11. 9122 8.56. 80 0.0000 1221.41 11. 9146 860.56 10.2847 1129. 67 6.4279 871.09 16.0462 1131. 51 0.0000 873.19 19.4965 1147.95 0.0000 875.33 0.0000 1173.23 11.1299 879.38 11. 4884 1177.95 9.2847 880.51 11. 4921 1189.05 16.7542 883.24 12.6507 1204.77 11.2083 884.68 14.9572 1221.41 16.8739 889.28 12.6722 1231.02 15.9697 894.76 12.6914 1235.36 0.0000 898.04 10.3934 1238.28 19.7580 900.72 11.5568 1260.41 0.0000 903.28 10.4084 1271.87 14.2154 911. 20 11. 58 98 1274.44 9.4818 912.08 11.5926 1274.54 7.5854 923.98 0.0000 1291.59 10.4676 926.50 13. 9658 1298.22 0.0000 929 .11 12.8110 1312 .11 0.0000 937.49 17.5085 1332.49 9.2133 944.13 0.0000 1362.66 0.0000 946.00 7. 8967 1365.19 6. 7 625 949.00 9.6592 1368. 63 0.0000 667. 71 0.0000 1384.29 0. 9697 962. 31 21.1487 1408. 01 2.9229 964.08 22.0398 1457.56 0.0000 966.17 43.2219 1460.82 10.8268 911.20 16.7717 1489.16 2. 9687 968. 97 16.7717 1505.03 3.9700 983.53 0.0000 1584.12 4.8331 984.45 0.0000 1596.21 0.0000 Page 4368 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:55:31.25 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM36.CNF;52 Background date : Z-OCT-2016 11:02:08. Sample date 14-DEC-2015 13:10:00 Acquisition date : 3-0CT-2016 05:53:13. Sample ID G405235062 Sample quantity : l.46441E+02 GRAM Detector name : GAM36 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.31 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 1 1 0 8 8 0 0 0 5 5 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 5 5 Page 4369 of 5809 Energy 63.67* 74.95* 77.07* 87.35 90.00 93.03* 185.92* 209.69 229.01 238.59* 241.87 295.42* 327.91*

329.89* 332.46 338.28 351.98* 388.58 463.83 477.51 482.27 505.99 510.80* 583.24* 609.52* 661. 76 727. 92 754.46 768.34 794.98 820.27 911.40* 964. 75 969.39 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 25 71 133 24 43 79 70 49 19 234 57 89 26 14 16 47 155 27 12 15 14 10 29 56 107 17 8 16 17 16 6 52 18 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 104 111 86 188 59 120 90 87 44 37 56 56 14 9 13 31 32 19 19 21 9 5 26 5 10 9 17 2 3 2 3 9 10 4 1.10 0.94 0.95 0.93 0.95 1. 81 1. 33 1. 93 0.59 1.12 1. 79 1. 07 1. 32 1. 32 1.13 0.98 1.18 0.91 0.68 4.35 1. 43 1. 57 2.46 1. 23 1. 24 1. 30 0.95 2.30 1. 53 1. 00 1. 37 1. 24 2.70 1. 53 127.31 149.86 154 .11 174.68 179.97 186.03 371.83 419.37 458.01 477.16 483.73 590.82 655.80 659.76 664.90 676.54 703.94 777.13 927.63 954.97 964. 50 1011. 94 1021.55 1166.40 1218. 96 1323.41 1455.71 1508.78 1536.53 1589.79 1640.37 1822.58 1929.24 1938.50 123 146 146 169 178 178 366 413 454 465 465 586 652 652 663 672 700 771 921 946 959 1009 1015 1162 1213 1319 1450 1504 1533 1585 1637 1816 1923 1923 8 7.06E-03 73.9 12 l.96E-02 25.9 9.68E-01 12 3.70E-02 14.9 10 6.68E-03108.5 14 1.19E-02 28.1 1.95E+OO 14 2.19E-02 31.7 12 1. 95E-02 30. 6 12 1. 35E-02 41. 8 8 5.17E-03 66.8 24 6.50E-02 8.0 3.77E+OO 24 1.58E-02 33.6 9 2.48E-02 18.7 11 7.36E-03 34.1 2.77E+OO 11 4.00E-03 48.9 6 4.52E-03 42.l 10 1.30E-02 26.4 11 4.31E-02 10.9 11 7.62E-03 36.3 9 3.45E-03 70.5 13 4.30E-03 67.8 9 3.96E-03 46.2 6 2.91E-03 44.6 13 8.0lE-03 49.2 10 1.56E-02 16.0 13 2. 98E-02 11. 9 9 4.72E-03 40.0 11 2.18E-03107.0 10 4.38E-03 31.2 7 4.67E-03 30.4 9 4.41E-03 30.3 6 1.76E-03 58.0 13 1.43E-02 19.2 19 5.0BE-03 42.0 1.21E+OO 19 5.03E-03 33.7 Peak Search Report (continued) Page : 2 Sample ID : G405235062 Acquisition date 3-0CT-2016 05:53:13 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1053.83 6 7 0.60 2107.33 2102 7 1.67E-03 83.7 36 0 1121. 35* 24 9 0.79 2242.31 2234 17 6.62E-03 35.3 37 0

  • 1173.95 9 2 1. 53 2347.47 23..44 7 2.61E-03 39.9 38 0 1188.54 8 3 1. 23 2376.64 2373 7 2.25E-03 51.1 39 0 1233.94 13 0 0.98 2467.38 2462 10 3.61E-03 27.7 40 0 1461.11* 145 6 2.00 2921.49 2915 13 4.04E-02 9.2 41 0 1765.02* 16 0 1. 50 3528.90 3522 11 4.37E-03 28.7 Flag: "*" = Peak area was modified by background subtraction Page 4370of5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:55:33 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 14-DEC-2015 13:10:00 G405235062 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 05:53:13 146.44 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA36 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4371 of 5809 Elapsed real time: Half life ratio : Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.31 10.00 0.00 % Peak Energy 0.0%

Nuclide Lihe Activity Report Page : 2 Sample ID : G405235062 Acquisition date 3-0CT-2016 05:53:13 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status BE-7 477.60 10.44* l.801Ei-OO 4.525E-01 2.075E+Ol 135.53 OK K-40 1460.82 10.66* 6.546E-01 1.027E+Ol 1.027E+Ol 18.32 OK CD-109 88.03 3.70* 4. 301E+OO 6.347E-02 9.868E-023326.46 OK SN-126 64.28 9.60 2.509E+OO 6.880E-01 6.880E-01 147.76 OK 86.94 8.90 4.301E+OO 2.639E-02 2.639E-023326.46 OK 87.57 37.00* 4.301E+OO 6.347E-03 6.347E-033326.46 OK BA-137M 661.66 89.90* 1.335E+OO 7.558E-02 7.699E-02 80.01 OK CS-137 661.66 85.10* l.335E+OO 7.984E-02 8.133E-02 80.01 OK TL-208 277.37 6.60 3. 041E+OO Line Not Found Absent 583.19 85.00* 1. 496E+OO 2.377E-01 2.377E-01 32.07 OK 860.56 12.50 1.058E+OO Line Not Found Absent BI-211 72.87 1. 23 3.327E+OO Line Not Found Absent 351. 06 12.92* 2.414E+OO 1.316E-01 1.316E-01 893.25 OK PB-212 74.82 10.28 3.492E+OO 7.150E-01 7.150E-01 96. 01 OK 77 .11 17.10 3.653E+OO 1. 371E+OO 1. 371E+OO 29.79 OK 238.63 43.60* 3.500E+00 8.970E-01 8.970E-01 15.92 OK 300.09 3.30 2.819E+OO Line Not Found Absent BI-214 609.32 45.49* l.437E+OO 8.806E-01 8.809E-01 23.71 OK 1120.29 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9 .191E-01 57.44 OK PB-214 74.82 5.80 3.482E+OO Line Not Found <<INT Reject 77 .11 9.70 3.653E+OO 2.416E+OO 2.417E+OO 29.79 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 3.455E+OO Line Not Found <<INT Reject 295.22 18.42 2.862E+OO 9.735E-01 9.738E-01 37.36 OK 351. 93 35.60* 2.414E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1.437E+OO 8.806E-01 8.809E-01 23.71 OK 1120.29 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9.191E-01 57.44 OK RA-224 240.99 4.10* 3.457E+OO 6.254E-01 6.254E-01 272.29 OK RA-226 609.32 45.49* 1.437E+OO 8.806E-01 8.809E-01 23.71 OK 1120.29 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9 .191E-01 57.44 OK AC-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 OK 794.95 4.25 1.134E+OO l.725E+OO 1. 725E+OO 60.55 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911. 20 25.80* l.005E+00 1.029E+OO 1.029E+OO 38.34 OK 968.97 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 OK RA-228 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.509E+00 9.408E-01 9.408E-01 52.75 OK 794.95 4.25 1.134E+OO 1. 725E+OO 1. 725E+OO 60.55 OK 835.71 1. 61 1.085E+OO Line Not Found Absent 911.20 25.80* 1.005E+OO 1.029E+00 1. 029E+OO 38.34 OK 968. 97 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 OK TH-228 74.82 10.28 3.492E+OO 7.150E-01 7.150E-01 96. 01 OK 77 .11 17.10 3.653E+00 1. 371E+OO 1. 371E+OO 29.79 OK 238.63 43.60* 3.500E+OO 8.970E-01 8.970E-01 15.92 OK 300.09 3.30 2.819E+OO Line Not Found Absent Page 4372 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235062 Acquisition date 3-0CT-2016 05:53:13 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.3,2 45.49* 1.437E+OO 8.806E-01 8.806E-Ol 23. 71 OK 1120.29 14.92 8.365E-01 9.682E-01 9.682E-Oi 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9.188E-01 57.44 OK TH-232 105.21 1.10 4.933E+OO Line Not Found Absent 338.32 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 OK 835. 71 1. 61 1.085E+OO Line Not Found Absent 911. 20 25.80* 1.005E+OO 1.029E+OO 1.029E+OO 38.34 OK 968. 97 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 OK TH-234 63.29 3.70* 2.509E+OO 1.785E+OO 1. 785E+OO 147.76 OK 92.59 4.23 4.565E+OO 2.580E+00 2.580E+OO 63.39 OK U-234 609.32 45.49* 1.437E+OO 8.806E-0.1 8.806E-01 23. 71 OK 1120.29 14.92 8.365E-01 9.682E-01 9.682E-01 70.51 OK 1764.49 15.30 5.417E-01 9.188E-01 9.188E-01 57.44 OK U-235 89. 96 3.47 4.432E+OO 1. 762E+OO 1. 762E+OO 56.15 OK 93.35 5.60 4.565E+OO 1.949E+OO 1.949E+OO 63.39 OK 143.76 10. 96* 4.954E+OO Line Not Found Absent 163.33 5.08 4.674E+OO Line Not Found Absent 185. 72 57.20 4.300E+OO 1.704E-01 1.704E-01 61.18 OK 205.31 5.01 3.984E+OO Line Not Found Absent U-238 63.29 3.70* 2.509E+OO 1.785E+OO 1.785E+OO 147.76 OK 92.59 4.23 4.565E+00 2.580E+OO 2.580E+OO 63.39 OK AM-243 43.53 5.90 5.957E-01 Line Not Found Absent 74.66 67.20* 3.492E+OO l.094E-01 l.094E-01 96. 01 OK CF-249 252.80 2.50 3.319E+OO Line Not Found Absent 333.37 14.60 2.552E+OO 2.482E-01 2.486E-01 84.24 OK 388.16 66.00* 2.193E+OO 1.062E-01 1.064E-01 72.51 OK ANH-511 511. 00 100.00* l.690E+00 9.326E-02 9.326E-02 98.40 OK Flag: "*" = Keyline Page 4373of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:55:34.75 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l *
  • Acquisition date 3-0CT-2016 05:53:13 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.31 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:10:00 Analyst initials: MXRl *
  • Sample ID G405235062 Sample Quantity 1.4644E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;7 '* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 2.075E+Ol 2.756E+Ol 2.757E+Ol K-40 1.027E+Ol 1.844E+OO 6.783E-01 CD-109 9.868E-02 3. 217E+OO 2.295E+OO SN-126 6.347E-03 2.069E-01 1.484E-01 BA-137M 7.699E-02 6.037E-02 7.037E-02 CS-137 8 .133E-02 6.377E-02 7.434E-02 TL-208 2.377E-01 7.468E-02 6. 431E-02 BI-211 l.316E-01 l.152E+00 4.287E-01 PB-212 8.970E-01 1.399E-01 9.570E-02 BI-214 8.809E-01 2.047E-01 l.436E-01 PB-214 1.022E+OO 2.188E-01 3.941E-01 RN-222 8.809E-01 2.047E-01 1.436E-01 RA-224 6.254E-01 1.669E+OO 1.028E+OO RA-226 8.809E-01 2.047E-01 1.436E-01 AC-228 l.029E+00 3.868E-01 3 .133E-01 RA-228 l.029E+00 3.868E-01 3 .133E-01 TH-228 8.970E-01 l.399E-01 9.570E-02 TH-230 8.806E-01 2.046E-01 l.436E-01 TH-232 1.029E+OO 3.868E-01 3 .133E-01 TH-234 1. 785E+00 2.585E+OO 2.083E+OO U-234 8.806E-01 2.046E-01 l.436E-01 U-235 4.347E-02 l.917E-01 3.691E-01 U-238 1.785E+OO 2.585E+OO 2.083E+OO AM-243 l.094E-01 1.029E-01 8. 911E-02 CF-249 l.064E-01 /.559E-02 8.007E-02 ANH-511 9.326E-02 8.994E-02 6.738E-02 Non-Identified Nuclides ----Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM NA-22 -6.126E-03 5.722E-02 l.193E-01 NOT IDENT. NA-24 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF AL-26 -1.378E-03 4.784E-02 l.048E-01 NOT IDENT. SC-46 -5.265E-02 3.170E-01 6.522E-01 FAIL ABUN Page 4374 of 5809 V-48 O.OOOE+OO l .141E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 4.444E+02 0.000E+OO SHORT HLIF MN-54 -4.324E-02 8.256E-02 1.466E-01 NOT IDENT. C0-56 2.954E-02 6.216E-01 l.240E+OO NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 4.853E-02 4.361E-02 9.479E-02 NOT IDENT. C0-58 -3.751E-01 7.033E-01 l.254E+OO NOT IDENT. FE-59 8.973E-01 7.129E+OO 1.572E+Ol NOT IDENT. C0-60 -3.067E-02 4.656E-02 8.343E-02 FAIL ABUN ZN-65 8.957E-02 1. 722E-01 .. 3.974E-01 NOT IDENT . GE-68 -1.790E+OO 3.451E+OO 5.921E+OO NOT IDENT. AS-73 -4.405E+OO 6.594E+OO l.298E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.829E+03 O.OOOE+OO SHORT HLIF SE-75 9.369E-02 2.400E-01 4.714E-01 NOT IDENT. BR-77 O.OOOE+OO 4.210E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 7.000E+02 O.OOOE+OO SHORT HLIF RB-83 l.164E-01 7. 901E-01 1.640E+OO NOT IDENT. KR-85 3.266E+OO 9.559E+OO 1.828E+Ol NOT IDENT. SR-85 3.223E-01 9.467E-01 1. 811E+OO NOT IDENT. RB-86 O.OOOE+OO 3.064E+04 O.OOOE+OO SHORT HLIF Y-88 -l.449E-01 2.736E-01 4. 941E-01 NOT IDENT. Y-91 --1. 986E+Ol 6.917E+02 l.418E+03 NOT IDENT. NB-94 -1.361E-02 4.281E-02 8.025E-02 NOT IDENT. NB-95 8.616E-01 8.284E-01 l.972E+OO NOT IDENT. NB-95M 1. 931E+OO 2.329E+OO 4.802E+OO NOT IDENT. ZR-95 -4.345E-01 1.564E+OO 2.653E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 8.754E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 4.292E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF RH-101 -3.487E-02 3.226E-02 5.667E-02 NOT IDENT. RH-102 5.146E-02 6.391E-02 l.504E-01 FAIL ABUN RU-103 3.935E+OO 5. 572E+OO 1.270E+Ol FAIL ABUN RH-106 1.0lOE-02 5.234E-01 l.099E+OO NOT IDENT. RU-106 1.0lOE-02 5.234E-01 1.099E+OO NOT IDENT. AG-108M -5.706E-03 2.759E-02 5.582E-02 NOT IDENT. AG-llOM -7.338E-03 1.186E-01 2.375E-01 NOT IDENT. SN-113 -6.791E-02 2.628E-01 4.673E-Ol NOT IDENT. CD-115 O.OOOE+OO 5.243E+38 0.000E+OO SHORT HLIF SN-ll 7M 0.000E+OO 7.064E+04 0.000E+OO SHORT HLIF TE-123M -4. 641E-02 l.303E-01 2.429E-01 NOT IDENT. SB-124 -5.841E-01 1.929E+OO 4.131E+OO NOT IDENT. SB-125 -7.819E-03 9.643E-02 2.005E-01 FAIL ABUN TE-125M 1. 764E+Ol 2.612E+02 5.179E+02 NOT IDENT. I-126 O.OOOE+OO 6.941E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.374E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.084E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.450E+09 O.OOOE+OO SHORT HLIF I-132 0.000E+OO 1.159E+41 0.000E+OO SHORT HLIF TE-132 O.OOOE+OO l.915E+26 O.OOOE+OO SHORT HLIF BA-133 7.281E-03 4.577E-02 8.249E-02 NOT IDENT. I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 1. 123E-01 6.664E-02 l.519E-01 FAIL ABUN CS-135 -7.422E-02 1. 766E-01 3.124E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.865E+05 O.OOOE+OO SHORT HLIF CE-139 *3. 731E-02 l.164E-01 2.298E-01 NOT IDENT. BA-140 O.OOOE+OO 9.772E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.535E+05 O.OOOE+OO SHORT HLIF CE-141 8.082E-01 2.146E+Ol 4.067E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 9.830E-02 3.553E-01 7. lOlE-01 NOT IDENT. PM-144 -3 .112E-02 6.164E-02 l.129E-01 FAIL ABUN PR-144 -2.719E+OO 5.332E+OO 9.750E+OO NOT IDENT. PM-146 3.664E-02 4.769E-02 1.084E-01 NOT IDENT. ND-147 O.OOOE+OO 2.842E+07 O.OOOE+OO SHORT HLIF PM-147 6.002E+02 7.814E+02 1. 648E+03 NOT IDENT. PM-149 O.OOOE+OO 8.538E+39 O.OOOE+OO SHORT HLIF EU-150 1.621E-02 2.924E-02 5.185E-02. FAIL ABUN EU-152 -4.821E-02 1.0lOE-01 1.745E-01 FAIL ABUN GD-153 -1.030E-01 l.758E-01 3.082E-01 NOT IDENT. EU-154 -1.926E-02 l.395E-01 2.892E-01 NOT IDENT. EU-155 -9.589E-03 9.956E-02 1. 966E-01 FAIL ABUN TB-160 -l.407E+OO 2.244E+OO 3.855E+OO FAIL ABUN H0-166M 4.556E-02 5.973E-02 1.410E-01 NOT IDENT. TM-171 4.841E+00 1.591E+Ol 3.442E+Ol NOT IDENT. HF-172 l.951E-01 2.167E-01 4.604E-01 FAIL ABUN LU-172 -9.367E-03 8.663E-02 l.715E-01 FAIL ABUN Page 4375 of 5809 LU-176 -1.640E-02 2.777E-02 4.745E-02 FAIL ABUN HF-181 6.637E+00 6.008E+OO 1.022E+Ol FAIL ABUN TA-182 -7.525E-01 9.199E-01 1.580E+OO FAIL ABUN RE-183 l.549E-01 2.289E+OO 4.795E+00 NOT IDENT. RE-184 -1.067E+Ol 2.735E+Ol 5.103E+Ol NOT IDENT. W-188 1. 8 69E+Ol 1.288E+02 2.282E+02 FAIL ABUN IR-192 -1.938E-01 5.030E-01 8.880E-01 FAIL ABUN HG-203 9.781E-01 2.504E+OO 4.934E+OO NOT IDENT. BI-207 7.678E-02 5.971E-02 1.517E-01 FAIL ABUN -4.107E-01 2.477E+OO 5.103E+OO NOT IDENT. PB-211 -3.912E-01 7.320E-01 l.405E+OO NOT IDENT. BI-212 5.068E-01 1. 063E+OO 1.476E+OO FAIL ABUN RN-219 l.230E-01 4.321E-01 9.147E-01 NOT IDENT. RA-223 9.480E-01 6.396E-01 1.417E+OO FAIL ABUN AC-227 -2.493E-01 2.529E-01 4.131E-01 NOT IDENT. TH-227 -2.493E-01 2.529E-01 4 .131E-01 NOT IDENT. TH-229 l.345E-01 4.614E-01 9.136E-01 FAIL ABUN PA-231 2.593E-01 5.449E-01 1. 071E+OO NOT IDENT. TH-231 9.480E-01 6. 396E-01 1. 417E+OO FAIL ABUN PA-233 2.404E-02 5.971E-02 1.210E-01 NOT IDENT. PA-234 -1.190E-01 3.444E-01 6.363E-01 NOT IDENT. PA_:234M 2.732E+00 5.606E+OO l.244E+Ol NOT IDENT. NP-237 2.404E-02 5.971E-02 1. 210E-01 NOT IDENT. NP-238 O.OOOE+OO 7.189E+40 O.OOOE+OO SHORT HLIF NP-239 -2.750E-02 2 .115E-01 4.157E-01 FAIL ABUN PU-239 2.985E+02 3.061E+02 6.476E+02 NOT IDENT. AM-241 1.746E-02 l.260E-01 2.464E-01 NOT IDENT. CM-243 6.845E-02 9.415E-02 1. 989E-01 FAIL ABUN BK-247 4.815E-02 8.327E-02 1.678E-01 NOT IDENT. CM-247 1. 886E-02 3.649E-02 8.038E-02 NOT IDENT. CF-251 -4.609E-02 1. 096E-01 2.020E-01 NOT IDENT. Page 4376 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:55:32.31 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error BE-7 477.60 17 10.44* 1.801E+OO 4.525E-01 2.075E+Ol 135.53 K-40 1460.82 140 10.66* 6.546E-01 1.027E+Ol 1.027E+Ol 18.32 CD-109 88.03 30 3.70* 4.301E+OO 9.606E-01 1.493E+OO 217.00 SN-126 64.28 32 9.60 2.509E+OO 6.880E-01 6.880E-01 147.76 86.94 30 8.90 4.301E+OO 3.994E-01 3.994E-01 217.00 87.57 30 37.00* 4.301E+OO 9.606E-02 9.606E-02 217.00 BA-137M 661.66 18 89.90* 1.335E+OO 7.558E-02 7.699E-02 80.01 CS-137 661. 66 18 85.10* 1.335E+OO 7.984E-02 8.133E-02 80.01 TL-208 277.37 ------6.60 3. 041E+OO ------Line Not Found ------583.19 59 85.00* 1.496E+OO 2.377E-01 2.377E-01 32.07 860.56 ------12.50 1.058E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 3.327E+OO ------Line Not Found ------351.06 171 12.92* 2.414E+OO 2.814E+OO 2.814E+OO 21. 85 PB-212 74.82 89 10.28 3.492E+OO 1.264E+OO 1.264E+00 51. 81 77 .11 167 17.10 3.653E+OO 1.371E+OO 1. 371E+OO 29.79 238.63 267 43.60* 3. 500E+'OO 8.970E-01 8.970E-01 15.92 300.09 ------3.30 2.819E+OO ------Line Not Found ------BI-214 609.32 112 45.49* l.437E+OO 8.806E-01 8.809E-01 23. 71 1120.29 24 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9.191E-01 57.44 PB-214 74.82 89 5.80 3.492E+OO 2. 241E+OO 2.242E+OO 51. 81 77 .11 167 9.70 3.653E+OO 2.416E+OO 2.417E+OO 29.79 87.09 30 3.41 4. 301E+OO 1.042E+00 1.043E+OO 217.00 242.00 65 7.25 3.457E+OO 1.327E+OO 1.328E+OO 67.19 295.22 100 18.42 2.862E+OO 9.735E-01 9.738E-01 37.36 351. 93 171 35.60* 2.414E+OO 1. 021E+OO 1.022E+OO 21. 85 RN-222 609.32 112 45.49* l.437E+OO 8.806E-01 8.809E-01 23.71 1120.29 24 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9 .191E-01 57.44 RA-224 240.99 65 4.10* 3.457E+OO 2.347E+OO 2.347E+OO 67.19 RA-226 609.32 112 45.49* 1.437E+OO 8.806E-01 8.809E-01 23.71 1120.29 24 14.92 8.365E-01 9.682E-01 9.685E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9.191E-01 57.44 AC-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 52 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 794.95 16 4.25 1.134E+OO 1.725E+OO 1.725E+OO 60.55 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 52 25.80* 1.005E+OO 1.029E+OO 1.029E+OO 38.34 968.97 18 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 RA-228 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 52 11. 27 2.509E+OO 9.408E-01 9.408E-01 52.75 794.95 16 4.25 l .134E+OO 1. 725E+OO 1. 725E+OO 60.55 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911. 20 52 25.80* 1.005E+OO 1. 029E+OO 1. 029E+OO 38.34 968.97 18 15.80 9.522E-01 6.186E-01 6.186E-01 67.37 TH-228 74.82 89 10.28 3.492E+OO 1.264E+OO 1.264E+OO 51. 81 77 .11 167 17.10 3.653E+OO 1. 371E+OO 1. 371E+OO 29.79 Page 4377 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235062 Acquisition date 3-0CT-2016 05:53:13 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 267
  • 43.60* 3.500E+OO 8.970E-01 8.970E-01
  • 15.92 300.09 ------3.30 2.819E+00 ------Line Not Found ------TH-230 609.32 112 45.49* 1.437E+OO 8.806E-01 8.806E-01 23. 71 1120.29 24 14.92 8.365E-01 9.682E-01 9.682E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9.188E-01 57.44 TH-232 105.21 ------1.10 4.933E+OO ------Line Not Found ------338.32 52 11.27 2.509E+OO 9.408E-01 9.408E-01 52.75 835.71 ------1. 61 1.085E+OO ------Line Not Found ------911.20 52 25.80* 1. 005E+OO 1. 029E+OO 1. 029E+OO 38.34 968. 97 18 15.80 9.522E-01 6.186E-01 6.186E-Ol* 67.37 TH-234 63.29 32 3.70* 2.509E+OO 1. 785E+OO 1.785E+OO 147.76 92.59 97 4.23 4.565E+OO 2.580E+OO 2.580E+OO 63.39 U-234 609.32 112 45.49* 1.437E+OO 8.806E-01 8.806E-01 23.71 1120.29 24 14.92 8.365E-01 9.682E-01 9.682E-01 70.51 1764.49 15 15.30 5.417E-01 9.188E-01 9.188E-01 57.44 U-235 89. 96 53 3.47 4.432E+OO 1.762E+OO 1. 762E+OO 56.15 93.35 97 5.60 4.565E+OO 1.949E+OO 1.949E+00 63.39 143.76 ------10. 96* 4.954E+OO ------Line Not Found ------163.33 ------5.08 4.674E+OO ------Line Not Found ------185. 72 82 57.20 4.300E+OO 1.704E-01 1.704E-01 61.18 205.31 ------5.01 3.984E+OO ------Line Not Found ------U-238 63.29 32 3.70* 2.509E+00 1. 785E+00 1. 785E+OO 147.76 92.59 97 4.23 4.565E+OO 2.580E+OO 2.580E+OO 63.39 AM-243 43.53 ------5.90 5.957E-01 ------Line Not Found ------74.66 89 67.20* 3.492E+OO 1.934E-01 1.934E-01 51. 81 CF-249 252.80 ------2.50 3.319E+OO ------Line Not Found ------333.37 18 14.60 2.552E+OO 2.482E-01 2.486E-01 84.24 388.16 30 66.00* 2.193E+00 1.062E-01 1.064E-01 72 .51 ANH-511 511. 00 31 100.00* 1. 690E+00 9.326E-02 9.326E-02 98.40 Flag: "*" Key line Page 4378 of 5809 Surrunary of Nuclide Activity Sample ID : G405235062 Acquisition date Page : 3 3-0CT-2016 05:53:13 Total number of lines in spectrum 41 Number of unidentified lines 3 Number of lines tentatively identified by NIO 38 Nuclide Type : Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CF-249 ANH-511 Hlife 53.220 l.25E+09Y 461. 400 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 7.04E+08Y 1. 41E+10Y 1600. DOY 1600.00Y 1600. DOY 1; 41E+10Y 1600.00Y 1. 41E+10Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 351. DOY l.00E+09Y Decay 45.9 1. 00 1. 55 1. 00 1. 02 1. 02 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 4.525E-01 l.027E+Ol 9.606E-01 9.606E-02 7.558E-02 7.984E-02 2.377E-01 2.814E+OO 8.970E-01 8.806E-01 1.021E+OO 8.806E-01 2.347E+OO 8.806E-01 1.029E+OO 1.029E+OO 8.970E-01 8.806E-01 1.029E+OO 1. 785E+OO 8.806E-01 1.704E-01 1.785E+OO l.934E-01 l.062E-01 9.326E-02 3.177E+Ol 3.177E+Ol Decay Corr pCi/GRAM 2.075E+Ol l.027E+Ol l.493E+OO 9.606E-02 7.699E-02 8 .133E-02 2.377E-01 2.814E+OO 8.970E-01 8.809E-01 1.022E+OO 8.809E-01 2.347E+OO 8.809E-01 1.029E+OO 1.029E+OO 8.970E-01 8.806E-01 1.029E+OO 1.785E+OO 8.806E-01 1.704E-01 1.785E+OO 1.934E-01 l.064E-01 9.326E-02 5.261E+Ol 5.261E+Ol 92.68% .. Decay Corr 2-Sigma Error 2.812E+Ol 0.188E+01 3.241E+OO 20.85E-02 6.160E-02 6.507E-02 0.762E-01 0.615E+OO 1.428E-01 2.089E-01 0.223E+OO 2.089E-01 1.577E+OO 2.089E-01 0.395E+OO 0.395E+OO l.428E-01 2.088E-01 0.395E+OO 2.638E+OO 2.088E-01 l.042E-01 2.638E+OO 1.002E-01 0. 771E-01 9.177E-02 "M" Manually accepted 2-Sigma %Error 135.53 18.32 217.00 217. 00 80.01 80.01 32.07 21. 85 15.92 23.71 21. 85 23.71 67.19 23.71 38.34 38.34 15.92 23. 71 38.34 147.76 23. 71 61.18 147.76 51. 81 72.51 98.40 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4379 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235062 Acquisition date : 3-0CT-2016 05:53:13 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.69 56 101 1. 93 419.37 413 12 1.35E-02 83.6 3.92E+OO T 0 229.01 21 51 0.59 458.01 454 8 5.17E-03 **** 3.63E+OO T 1 327.91 29 16 1. 32 655.80 652 11 7.36E-03 68.3 2.59E+OO T 1 329.89. 16 10 1. 32 659.76 652 11 4. 0..0E-03 97.8 2.57E+OO 0 463.83 13 20 0.68 927.63 921 9 3.45E-03 **** 1. 85E+OO T 0 482.27 15 9 1. 43 964. 5 0 959 9 3. 96E-03 92.4 1. 78E+OO T 0 505.99 11 5 1. 57 1011. 94 1009 6 2. 91E-03 89.1 1. 71E+OO T 0 727.92 8 18 0.95 1455.71 1450 11 2.18E-03 **** 1.23E+OO T 0 754.46 16 2 2.30 1508.78 1504 10 4.38E-03 62.4 1.19E+OO T 0 768.34 17 3 1. 53 1536.53 1533 7 4.67E-03 60.8 1.17E+OO T 0 820.27 6 3 1. 37 1640.37 1637 6 1. 7 **** 1. lOE+OO 5 964. 75 18 10 2.70 1929.24 1923 19 5.08E-03 84.1 9.56E-01 T 0 1053.83 6 7 0.60 2107.33 2102 7 1. 67E-03 **** 8.84E-01 0 1173.95 9 2 1. 53 2347.47 2344 7 2.61E-03 79.7 8.03E-01 T 0 1188.54 8 3 1.23 2376.64 2373 7 2.25E-03 **** 7.94E-01 T 0 1233.94 13 0 0.98 2467.38 2462 10 3. 61E-03 55.5 7.67E-01 T Flags: "T" = Tentatively associated Page 4380 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:55:49.65 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * .. DETECTOR AND SAMPLE DATA ** * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l * *Acquisition date 3-0CT-2016 05:53:13 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.31 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:10:00 Nuclide Library : SOLID *
  • Sample ID G405235062 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : l.4644E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date l-JUN-2016 09:39:12 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;?
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide BE-7 K-40 CD-109 SN-126 BA-137M CS-137 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 CF-249 ANH-511 Le (pCi/GRAM 1.204E+Ol 2.392E-01 1.076E+OO 6.955E-02 2.916E-02 3.080E-02 2.656E-02 1.914E-01 4.310E-02 6.093E-02 1. 888E-01 6.093E-02 4.629E-01 6.093E-02 l.295E-01 1. 295E-01 4.310E-02 6.091E-02 l.295E-01 9.601E-01 6.091E-02 l.711E-01 9.601E-01 4.137E-02 3.507E-02 2.947E-02 ----Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 V-48 Page 4381 of 5809 Le (pCi/GRAM 4.801E-02 O.OOOE+OO 3.924E-02 2.481E-01 O.OOOE+OO NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 4382 of 5809 O.OOOE+OO 6.080E-02 5.280E-01 O.OOOE+OO 4.384E-02 5.141E-01 6.445E+OO 3.084E-02 1.607E-01 2.428E+OO 5.880E+OO O.OOOE+OO 2.146E-01 O.OOOE+OO O.OOOE+OO 7.190E-01 8. lllE+OO 8.032E-01 O.OOOE+OO l.562E-01 5.976E+02 3.451E-02 8.408E-01 2.202E+OO 1.062E+00 O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 2.582E-02 6.461E-02 5.541E+00 4.620E-01 4.620E-01 2.389E-02 9.754E-02 2.039E-01 O.OOOE+OO O.OOOE+OO 1.113E-01 1.306E+OO 8.550E-02 2.400E+02 O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.613E-02 O.OOOE+OO 6. 641E-02 1.418E-01 O.OOOE+OO O.OOOE+OO 1. 063E-01 O.OOOE+OO O.OOOE+OO 1.873E+Ol O.OOOE+OO 3.283E-01 4.663E-02 4.027E+OO 4.775E-02 O.OOOE+OO 7.615E+02 0.000E+OO 2.293E-02 7.580E-02 l.415E-01 1.160E-01 9.032E-02 l.550E+OO 6.00lE-02 l.570E+Ol 2.130E-01 6.818E-02 2.093E-02 SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT I DENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-251 Page 4383 of 5809 4.506E+OO 5.914E-01 2.193E+OO 1.977E+Ol l.027E+02 3.927E-01 2.235E+OO 6.494E-02 2.340E+00 6.12..EiE-01 6.515E-01 4.062E-01 6.395E-01 l.833E-01 1.833E-01 4.173E-01 4.875E-01 6.395E-01 5.362E-02 2.578E-01 5.316E+OO 5.362E-02 O.OOOE+OO 1.896E-01 3.009E+02 l.134E-01 9. 211E-02 7.633E-02 3.549E-02 9.150E-02 FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:55:55.84 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235062.CNF;l * *Acquisition date 3-0CT-2016 05:53:13 Sensitivity : 3.000 *
  • Detector ID GAM36 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.31 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:10:00 Nuclide Library : SOLID *
  • Sample ID G405235062 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4644E+02 GRAM *
  • Quantity Err(%) : 1.3657E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-JUN-2016 09: 39 :'12 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM36 CAN.CNF;?
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) BE-7 2.075E+Ol 2.758E+Ol K-40 1.027E+Ol 1.921E+OO CD-109 9.868E-02 3. 221E+OO SN-126 6.347E-03 2. 072E-01 BA-137M 7.699E-02 6.046E-02 CS-137 8.133E-02 6.387E-02 TL-208 2.377E-01 7.537E-02 BI-211 1.316E-01 1.164E+OO PB-212 8.970E-01 1. 477E-01 BI-214 8.809E-01 2.082E-01 PB-214 1.022E+OO 2.229E-01 RN-222 8.809E-01 2.082E-01 RA-224 6.254E-01 1.673E+OO RA-226 8.809E-01 2.082E-01 AC-228 1.029E+OO 3.904E-01 RA-228 l.029E+00 3.904E-01 TH-228 8.970E-01 1.477E-01 TH-230 8.806E-01 2.081E-01 TH-232 1.029E+OO 3.904E-01 TH-234 1.785E+OO 2.615E+OO U-234 8.806E-01 2.081E-01 U-235 4.347E-02 1. 917E-01 U-238 1.785E+OO 2.615E+OO AM-243 l.094E-01 l.037E-01 CF-249 l.064E-01 7.609E-02 ANH-511 9.326E-02 9.002E-02 Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 Page 4384 of 5809 Key-Line Activity (pCi/GRAM -6.126E-03 -1.000E+41 -l.378E-03 -5.265E-02 K.L Act error (1.96-sigma) 5. 722E-02 3.126E+41 4.784E-02 3.170E-01 TPU ( 1. 96-sigma) 2.758E+Ol 1.921E+OO 3.221E+OO 2.072E-01 6.046E-02 6.387E-02 7.537E-02 l.164E+OO l.477E-01 2.082E-01 2.229E-01 2.082E-01 1.673E+00 2.082E-01 3.904E-01 3.904E-01 1.477E-01 2.081E-01 3.904E-01 2.615E+OO 2.081E-01 1.917E-01 2.615E+OO 1.037E-01 7.609E-02 9.002E-02 TPU ( 1. 96-sigma) 5.729E-02 O.OOOE+OO 4.785E-02 3.179E-01 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN V-48 4.628E+03 l.141E+04 l.160E+04 SHORT HLIF CR-51 -l.408E+02 4.444E+02 4.489E+02 SHORT HLIF MN-54 -4.324E-02 8.258E-02 8.485E-02 NOT IDENT. C0-56 2.954E-02 6.216E-01 6.217E-01 NOT IDENT. MN-56 l.000E+41 1. 785E+42 0.000E+OO SHORT HLIF C0-57 4.853E-02 4.367E-02 4.885E-02 NOT IDENT. C0-58 -3.751E-01 7.035E-01 7.236E-01 NOT IDENT. FE-59 8.973E-01 7.129E+OO 7.141E+OO NOT IDENT. C0-60 -3.067E-02 4.657E-02 4.858E-02 FAIL ABUN ZN-65 8.957E-02 l.722E-01 " 1. 7 69E-01 NOT IDENT. GE-68 -1.790E+OO 3. 451E+OO 3.544E+OO NOT IDENT. AS-73 -4.405E+OO 6.656E+OO 6.946E+OO NOT IDENT. AS-74 3. 8 66E+02 4.829E+03 4.833E+03 SHORT HLIF SE-75 9.369E-02 2.400E-01 2.437E-01 NOT IDENT. BR-77 2.698E+37 2.288E+38 O.OOOE+OO SHORT HLIF SR-82 4.558E+02 7.003E+02 7.299E+02 SHORT HLIF RB-83 1.164E-01 7.902E-01 7.920E-01 NOT IDENT. KR-85 3.266E+OO 9.560E+OO 9.672E+OO NOT IDENT. SR-85 3.223E-01 9.468E-01 9.579E-01 NOT IDENT. RB-86 -l.146E+04 3.064E+04 3.108E+04 SHORT HLIF Y-88 -l.449E-01 2.738E-01 2.815E-01 NOT IDENT. Y-91 -1. 98 6E+Ol 6.917E+02 6.918E+02 NOT IDENT. NB-94 -1.361E-02 4.282E-02 4.326E-02 NOT IDENT. NB-95 8.616E-01 8.292E-01 9.157E-01 NOT IDENT. NB-95M 1. 931E+OO 2.334E+OO 2.491E+OO NOT IDENT. ZR-95 -4.345E-01 1.564E+OO 1.577E+OO NOT IDENT. NB-97 1.000E+41 4.922E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 8.763E+40 O.OOOE+OO SHORT HLIF M0-99 -1.941E+31 4.294E+31 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 3.395E+41 O.OOOE+OO SHORT HLIF RH-101 -3.487E-02 3.287E-02 3.644E-02 NOT IDENT. RH-102 5.146E-02 6.404E-02 6.812E-02 FAIL ABUN RU-103 3.935E+OO 5.575E+OO 5.850E+OO FAIL ABUN RH-106 1.0lOE-02 5.234E-01 5.234E-01 NOT IDENT. RU-106 1.0lOE-02 5.234E-01 5.234E-01 NOT IDENT. AG-108M -5.706E-03 2.759E-02 2. 771E-02 NOT IDENT. AG-llOM -7.338E-03 l.186E-01 l.186E-01 NOT IDENT. SN-113 -6.791E-02 2.628E-01 2.646E-01 NOT IDENT. CD-115 8.343E+37 5.246E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -l.342E+04 7.066E+04 7.092E+04 SHORT HLIF TE-123M -4.641E-02 l.303E-01 1.320E-01 NOT IDENT. SB-124 -5.841E-01 1.929E+OO 1.947E+OO NOT IDENT. SB-125 -7.819E-03 9.644E-02 9.650E-02 FAIL ABUN TE-125M 1. 764E+Ol 2.612E+02 2.613E+02 NOT IDENT. I-126 -l.316E+05 6.943E+05 6.968E+05 SHORT HLIF SB-126 2.394E+05 9.384E+05 9.446E+05 SHORT HLIF SB-127 -2.769E+21 8.005E+21 O.OOOE+OO SHORT HLIF I-131 -2.580E+09 3.452E+09 3.643E+09 SHORT HLIF I-132 -1.000E+41 l.814E+42 O.OOOE+OO SHORT HLIF TE-132 l.462E+26 2. 001E+26 O.OOOE+OO SHORT HLIF BA-133 7.281E-03 4.578E-02 4.589E-02 NOT IDENT. I-133 -l.OOOE+41 4. 481E+41 O.OOOE+OO SHORT HLIF CS-134 1.123E-01 6. 681E-02 8.382E-02 FAIL ABUN CS-135 -7.422E-02 1. 7 67E-01 1. 799E-01 NOT IDENT. I-135 -1.000E+41 1.472E+42 O.OOOE+OO SHORT HLIF CS-136 7.146E+04 2.867E+05 2.885E+05 SHORT HLIF CE-139 3.731E-02 l.166E-01 l.178E-01 NOT IDENT. BA-140 -3.784E+05 9.773E+05 9.921E+05 SHORT HLIF LA-140 -7.554E+04 4.535E+05 4.548E+05 SHORT HLIF CE-141 8.082E-01 2.146E+Ol 2.146E+Ol NOT IDENT. CE-143 1.000E+41 9.032E+42 O.OOOE+OO SHORT HLIF CE-144 9.830E-02 3.553E-01 3.581E-01 NOT IDENT. PM-144 -3.112E-02 6.167E-02 6.325E-02 FAIL ABUN PR-144 -2.719E+OO 5.333E+OO 5.472E+OO NOT IDENT. PM-146 3.664E-02 4.776E-02 5.054E-02 NOT IDENT. ND-147 8 .*488E+05 2.842E+07 2.843E+07 SHORT HLIF PM-147 6.002E+02 7.819E+02 8.274E+02 NOT IDENT. PM-149 -5.573E+39 8.622E+39 O.OOOE+OO SHORT HLIF EU-150 1:621E-02 2.925E-02 3.015E-02 FAIL ABUN EU-152 -4.821E-02 1.0lOE-01 l.033E-01 FAIL ABUN GD-153 -1.030E-01 l.759E-01 1.820E-01 NOT IDENT. EU-154 -1. 926E-02 1.395E-01 l.398E-01 NOT IDENT. EU-155 -9.589E-03 9.956E-02 9. 966E-02 FAIL ABUN TB-160 -1.407E+OO 2.245E+OO 2.333E+OO FAIL ABUN H0-166M 4.556E-02 5.978E-02 6.321E-02 NOT IDENT. TM-171 4.841E+OO 1.592E+Ol 1.607E+Ol NOT IDENT. HF-172 l.951E-01 2.190E-01 2.360E-Ol FAIL ABUN LU-172 -9.367E-03 8.663E-02 8.674E-02 FAIL ABUN Page 4385 of 5809 LU-176 -1. 640E-02 2.778E-02 2.874E-02 FAIL ABUN HF-181 6.637E+OO 6.015E+OO 6.718E+OO FAIL ABUN TA-182 -7.525E-01 9.203E-01 9.809E-01 FAIL ABUN RE-183 l.549E-01 2.290E+OO 2.291E+OO NOT IDENT. RE-184 -1.067E+Ol 2.746E+Ol 2.788E+Ol NOT IDENT. W-188 1.869E+Ol l.288E+02 1.291E+02 FAIL ABUN IR-192 -1.938E-01 5.031E-01 5.106E-01 FAIL ABUN HG-203 9.781E-01 2.505E+OO 2.543E+OO NOT IDENT. BI-207 7.678E-02 5.979E-02 6.908E-02 FAIL ABUN PB-:no -4.107E-01 2.477E+OO 2..484E+OO NOT IDENT. PB-211 -3.912E-01 7.323E-01 7.532E-01 NOT IDENT. BI-212 5.068E-01 1.063E+OO l.087E+00 FAIL ABUN RN-219 1. 230E-01 4.324E-01 4.359E-01 NOT IDENT. RA-223 9.480E-01 6.423E-01 7. 715E-01 FAIL ABUN AC-227 -2.493E-01 2.SSOE-01 2.787E-01 NOT IDENT. TH-227 -2.493E-01 2.SSOE-01 2.787E-01 NOT IDENT. TH-229 1.345E-01 4.615E-01 4.654E-01 FAIL ABUN PA-231 2.593E-01 5.477E-01 5.601E-01 NOT IDENT. TH-231 9.480E-01 6.423E-01 7.715E-01 FAIL ABUN PA-233 2.404E-02 5.972E-02 6.070E-02 NOT IDENT. PA-234 -1.190E-01 3.703E-01 3.742E-01 NOT IDENT. PA-234M 2.732E+OO 5.608E+OO 5.741E+OO NOT IDENT. NP-237 2.404E-02 5.972E-02 6.070E-02 NOT IDENT. NP-238 -9.649E+39 7.189E+40 O.OOOE+OO SHORT HLIF , NP-239 -2.750E-02 2. llSE-01 2 .119E-01 FAIL ABUN PU-239 2.985E+02 3.064E+02 3.346E+02 NOT IDENT. AM-241 1. 746E-02 1.260E-01 1.262E-01 NOT IDENT. CM-243 6.845E-02 9.436E-02 9.928E-02 FAIL ABUN BK-247 4.815E-02 8.383E-02 8.659E-02 NOT IDENT. CM-247 1.886E-02 3.663E-02 3. 761E-02 NOT IDENT. CF-251 -4.609E-02 1.098E-01 1.117E-01 NOT IDENT. Page 4386 of 5809
  • GEL Laboratories LLC *
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  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 74.66 14.0690 105.31 75.1328 131.20 57.5436 879.38 39.3639 86.79 75.1725 133.02 48.0972 46.54 37.1209 86.94 75.1979 133.52 45.2487 228.16 0.0000 87.09 75.2233 136.00 47.3656 52.39 32.8973 87.57 75.3034 136.47 45.4667 1093.63 35.3626 88.03 75.3796 739.50 0.0000 52.39 31.3953 306.78 75.4310 140.51 0.0000 125.81 37.0976 88.47 38.9052 143.76 47.9525 53.44 41.9977 143.76 56.7739 144.24 51.9058 54.07 38.8423 90.64 48.5659 145.44 43.1722 293.27 0.0000 531.02 0.0000 152.43 58.5067 482.18 44. 972"6 92.59 48.7692 1048.07 0.0000 57.98 37.6630 93.35 48.8481 154.21 40.7648 59.27 42.7356 94.56 48.9728 158.56 0.0000 59.32 42.7417 311. 90 48.9820 159.00 47.0595 59.54 41.6723 946.00 48.9840 162.33 40.2423 60. 96 55.0547 94.87 33. 466"5 537.26 0.0000 61.17 44.0700 97.43 45.6604 163.33 48.3596 62.93 46.5021 98.43 39.7337 165.86 44.4881 63.29 46.5484 98.44 39.7347 427.87 47.1820 290.67 46.5856 103.37 39.8226 176.60 0.0000 87.57 46.6752 116. 74 39.8226 177.52 38.0123 66.73 59.2907 100 .11 39.8693 181.07 0.0000 67.24 48.7291 102.03 49.1188 181.52 37.1810 67. 68 47.9446 103.18 31. 908 9 184.41 1221.41 47.9533 103.37 39.2171 185.72 38.4233 97.43 54 .1138 911.20 44.8504 193.51 32.5132 279.20 59.3632 105.31 44.8593 197.03 40.0294 1063.66 47.7298 106.12 44.0127 198.01 40.0781 72. 87 47.7371 106.47 41. 2901 201.83 42.3846 351.06 47.7371 109.28 52.5825 203.43 39.2820 74.66 56.5128 111. 00 48.1255 205.31 31.2128 238.63 56.5350 111.76 0.0000 210.85 35.3460 351. 93 56.5350 114.06 33.5075 215.65 35.5439 238.63 56.5350 116. 30 0.0000 222 .11 28.2118 74.97 56.5561 116.74 38.3480 227.09 45.1005 77 .11 56.8517 119.76 47.9600 227.38 42.2043 78.74 50.7327 264.66 44.3049 228.16 0.0000 256.23 53.1585 121.22 35.8274 228.18 22.9418 133. 52 52.0555 344.28 37.7499 235.69 27.5368 364.49 0.0000 122.06 31.1591 235. 96 27.5448 711.68 46.3204 122.92 52. 00*98 238.63 27.6241 356.01 43.4692 1274.44 52.0232 238.98 0.0000 323.87 43.4761 123.68 53.0255 240.99 27.6936 81. 75 54.8669 125.81 35.1636 242.00 27. 7233 83.79 51.3333 127.23 55.2545 244.70 32.6213 265.00 51. 3580 127.91 55.3186 685.70 0.0000 193.51 74.9447 129.30 39.1964 388.16 28.0369 Page 4387 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 507.63 0.0000 345.93 23.1818 569.50 10.3582 256.23 36.0127 351.06 23.2774 569.70 9.4173 527.90 0.0000 351. 93 23.2937 583.19 7.5889 264.66 28.3737 355.39 0.0000 584.27 7.5931 264.80 28.3775 356.01 14.7590 595.83 0.0000 265.00 24.9769 364.49 0.0000 600.60 13.4024 268.22 39.8621 366.42 0.0000 602.52 0.0000 269.46 33.0693 372.51 22.4231 604. 72 8.6342 270.03 34.2279 375.05 14.9777 607.14 11.5264 401.81 26.2723 377.52 17.5064 609.32 10.5779 273.65 0.0000 383.85 25.1276 610.33 10.5833 276.40 30.9955 388.16 16.8050 614.28 2.8922 583.19 27. 5771 666.33 0.0000 618.01 9.6590 277.60 26.4337 391. 69 18.9546 884.68 17.4067 402.40 27.5940 400.66 21.1980 621. 93 7.7425 279.20 25.3234 401. 81 17.8213 630.19 0.0000 279.54 29.9371 402.40 13. 5837 631.29 5.8342 279.70 31.0935 404.85 19.5607 633.25 11. 67 97 280.46 28.8109 410.95 18.7912 634.78 0.0000 301.36 25.4308 413.71 23. 9622 635.95 9.7461 284.31 0.0000 720.70 0.0000 636.99 0.0000 285.41 30.1030 423.72 0.0000 1690.97 9.7937 285.90 0.0000 427.09 11. 2287 657.76 8. 8 656 287.50 23.2013 427.87 12.0990 657.90 0.0000 290.67 24.8210 433.94 13.8844 661.66 7.8952 293.27 0.0000 439.40 16.5481 664.57 0.0000 295.22 26.8717 453.88 10.5515 666.33 0.0000 316.51 26.8893 463.37 11. 5009 666.50 0.0000 298.58 42.1875 468.07 10.6482 667.71 0.0000 299.98 18.7739 473.00 0.0000 677.62 12.9275 300.09 23.4698 631.29 16.0430 685.70 0.0000 300.13 23.4705 696.49 16.0602 695.00 0.0000 311. 90 23.4705 477.60 16.0682 696.49 12.0386 301.36 27.0205 482.18 9.3998 696. 51 12.0386 302.85 36.4681 487.02 0.0000 697.00 0.0000 304.50 24.7401 492.35 0.0000 697.30 12.0430 304.85 0.0000 497.08 9.0342 697.49 14.0513 306.78 27.1518 505.52 10.8962 702.65 16. 0964 308.46 21. 2805 507.63 0.0000 706.68 11.0868 311. 90 15.4157 511. 00 16.3976 711. 68 5.0509 316.51 25. 0016 514.00 16.4268 720.70 0.0000 319.41 0.0000 514.00 16.4268 721. 93 0.0000 320.08 0.0000 520.40 13.7402 722.78 9.1370 321. 04 35.8557 520.69 0.0000 722.91 6.0916 323.87 9.5847 667. 71 0.0000 723.31 6.0928 325.23 19.1914 527.90 0.0000 756.73 10.6666 1596.21 0.0000 528.26 8.2819 727. 33 9.1556 333.37 20.9325 529.59 11. 9717 733.00 12.2378 333.97 12.0825 529.87 0.0000 735.93 10. 2116 334.37 7.2519 531. 02 0.0000 737.46 8.1748 338.28 25.4637 537.26 0.0000 739.50 0.0000 338.32 25.4643 1260.41 0.0000 747.24 7.1834 340.48 24.2944 552.55 14. 9271 748.06 11.2923 340.55 0.0000 795.86 15.0150 752.31 7.7133 344.28 20. 7141 569.33 10.3573 753.82 0.0000 Page 4388 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 756.73 7.7283 968. 97 5.5929 1505.03 4.8950 756.80 7.7283 983.53 0.0000 1584.12 5.9843 763.94 10.8529 984.45 0.0000 1596. 21 0.0000 765.81 3.1033 996.26 4.5168 1620.50 5.0284 1001.03 9.3124 1001.03 5.6551 1621. 92 2.0120 766.84 9.3138 1002.74 5.6584
  • 1678.03 0.0000 772. 60 0.0000 1004.73 10.1920 1690.97 2.0430 776.52 0.0000 1021.30 0.0000 1750.46 0.0000 777.92 0.0000 1025.87 0.0000 1764.49 1.0377 778.90 5.2008 1028.54 0.0000 1770.23 6.2333 783.70 0.0000 1037.84 5. 7255 1771.35 3 .1174 785.37 7.3008 1038.76 0.0000 1791.20 0.0000 903.28 10.9819 1046.59 9.1868 1808.65 3.1415 794.95 6.2827 1048.07 0.0000 1810.72 0.0000 795.86 10.9990 1049.04 6.8955 1836.06 3.1591 801.95 11. 5514 1050.41 6.8989 810.06 11. 58 99 1063.66 2. 3096 810.29 11. 5908 1077.00 0.0000 810.45 11. 5917 1077.34 11. 5983 810.76 11. 5931 1085.87 4.6520 815.77 0.0000 1093.63 5.8293 818.51 0.0000 1099.45 6.1323 832.01 7.4406 1112. 07 5.2767 834.85 12.7700 1112. 84 8.7970 835.71 9.5808 1115. 54 2.8174 836.80 0.0000 1120.29 7.0537 846.75 0.0000 1120.55 7.0542 846.77 10.6917 1121.30 7.0562 856.80 0.0000 1808.65 7.0742 860.56 8.5993 1131.51 0.0000 871.09 4.3171 1147.95 0.0000 873.19 12. 9614 1332.49 3.5840 875.33 0.0000 1177.95 2. 8713 879.38 10.8268 1189.05 7.2017 880.51 8.6650 1204.77 9.9479 883.24 6.5056 1221.41 8.1788 884.68 7.5939 1231. 02 2.9160 889.28 4.3470 1235.36 0.0000 894.76 6.5339 1238.28 1.4610 1836.06 7.6320 1260.41 0.0000 900. 72 5.4569 1271.87 7.3740 903.28 6.5547 1274.44 6.4570 911.20 7.6694 1274.54 6.4574 912.08 7.6719 1291. 59 2.7805 984.45 0.0000 1298.22 0.0000 926.50 7.7124 1312 .11 0.0000 929 .11 9.9254 1332.49 6.5599 937.49 9.9554 1362.66 0.0000 983.53 0.0000 1365.19 3.7810 946.00 8.8763 1368. 63 0.0000 949.00 4.4429 1384.29 7. 5996 954.55 0.0000 1408.01 2. 8672 962. 31 3.3479 1457.56 0.0000 964. 08 5.5833 1460.82 1. 9370 966 .17 5.5874 1489.16 1. 9504 Page 4389 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:56:28.72 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM44.CNF;lll Background date : Z-OCT-2016 11:02:28. Sample date 14-DEC-2015 13:15:00 Acquisition date : 3-0CT-2016 05:53:40. Sample ID G405235063 Sample quantity 1.47883E+02 GRAM Detector name GAM44 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.75 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 4 4 1 1 0 4 4 4 0 0 0 0 3 3 3 6 6 0 0 0 0 0 1 1 0 0 0 5 5 0 0 0 0 0 Page 4390 of 5809 Energy 63.34* 65.77 74.80 77.17* 84.27 87.25 89.87 92.67* 110.26 144.83 154.39 185.93* 205.54 209.50 211. 70 238.68* 241. 60 270.36 295.45 300.07 338.64 352.00* 401.23 405.01 463.97 511. 35* 520.52 543.58 546.66 583.42* 609.58* 678. 72 711.57 728.58 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 28 22 58 122 35 48 41 54 36 20 21 62 25 35 27 340 77 23 147 37 65 202 24 21 19 56 11 10 15 84 154 7 13 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 84 74 125 99 105 112 142 118 121 98 81 122 60 61 79 65 100 50 79 37 96 51 24 18 37 22 16 6 10 33 53 12 12 31 1. 37 1. 09 0.93 1. 06 1. 37 0.95 1. 45 1. 46 1. 05 1. 24 0.83 1. 29 1. 56 1. 20 1. 57 1.10 1. 82 1. 37 1.11 1. 75 1. 32 1. 30 1. 53 1. 53 2.60 2.47 0.87 1. 56 1. 65 1.19 1. 54 0.61 0.64 1. 89 127.13 131. 99 150.05 154.81 169.00 174. 98 180.22 185.81 221.01 290.17 309.31 372.41 411. 64 419.57 423. 96 477. 96 483.79 541.35 591.55 600.78 677.96 704.69 803.20 810.76 928.75 1023.57 1041. 91 1088.05 1094.23 1167. 77 1220.14 1358.50 1424.23 1458.28 124 124 147 147 167 172 172 172 217 287 306 367 408 408 408 473 473 537 586 597 672 700 799 799 922 1017 1038 1086 1086 1162 1214 1352 1420 1449 11 7.86E-03 11 6.15E-03 13 1.60E-02 13 3.40E-02 6 9.84E-03 20 1. 33E-02 20 1.14E-02 20 1. 50E-02 9 1.00E-02 7 5.65E-03 6 5.83E-03 10 1.73E-02 29 6.99E-03 29 9.60E-03 29 7.55E-03 17 9.44E-02 17 2.14E-02 9 6.37E-03 12 4.08E-02 7 l.02E-02 14 1. 80E-02 10 5.61E-02 19 6.79E-03 19 5.78E-03 10 5.24E-03 16 1.56E-02 8 3.06E-03 12 2.87E-03 12 4.25E-03 10 2.33E-02 15 4.28E-02 8 2.00E-03 8 3.49E-03 14 5.12E-03 55.9 60.8 31. 6 16.3 48.3 35.9 56.1 44.0 57.6 84.0 71. 2 36.6 55.0 42.4 65.5 6.8 34.5 59.2 14.7 32.0 34.2 9.8 38.3 45.3 64.9 28.4 69.8 36. 7 45.8 17.2 13.6 95.1 55.7 68.5 Fit 1.27E+OO 1.70E+OO 7.lOE-01 9.60E-01 9.83E-01 1.54E+OO 8.91E-01 Peak Search Report (continued) Page : 2 Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 746.85 12 5 1. 29 1494.85 1491 7 3.31E-03 43.0 36 0 773.10 15 13 1. 59 1547.37 1541 10 4.21E-03 53.4 37 0 776.26 10 0 0.95 l553.70 1551 6 2.78E-03 31. 6 38 0 795.67 12 27 0.63 1592.54 1584 12 3.37E-03 90.4 39 0 840.54 15 8 1. 51 1682.34 1678 8 4.28E-03 40.6 40 0 862.77 11 31 1. 71 1726.83 1719 15 2. 97E-03116. 3 41 0 911. 20* 87 25 1. 62 1823.77 1815 18 2.41E-02 17.8 42 0 969.25* 31 20 2.05 1939.94 1935 10 8.70E-03 32.7 43 0 1000.74 22 3 0.97 2002.97 1998 11 6.12E-03 25.9 44 0 1120.34 51 17 1. 56 2242.37 2235 14 1. 42E-02 22.2 45 0 1377. 40 7 4 0.55 2756.93 2752 8 1.94E-03 62.3 46 0 1460.71* 261 14 2.25 2923.72 2917 14 7.26E-02 7.0 47 0 1764.37 25 4 2.04 3531.65 3525 11 6.81E-03 27.1 Flag: "*" = Peak area was modified by background subtraction Page 4391 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:56:30 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 14-DEC-2015 13:15:00 G405235063 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 05:53:40 147.88 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA44 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 U-235 143.76 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4392 of 5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 CE-141 145.44 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.75 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10. 6.,6* 1.030E+OO 1.163E+Ol l.163E+Ol 13. 95, OK CD-109 88.03 3.70* 4.459E+OO 7.567E-01 1.176E+OO 179.82 OK TE-125M 109.28 0.27* 5.627E+OO 1.475E+Ol 5 .118E+02 115 .11 OK SN-126 64.28 9.60 2.050E+OO 9.341E-01 9.341E-01 111.73 OK 86.94 8.90 4.459E+OO 3.146E-01 3.146E-01 179.82 OK 87.57 37.00* 4.459E+OO 7.567E-02 7.567E-02 179.82 OK CE-141 145.44 48.29* 5.912E+OO l.345E-02 7.054E+OO 560.68 OK TL-208 277.37 6.60 4.074E+OO Line Not Found Absent 583.19 85.00* 2.178E+OO 2.434E-01 2.434E-01 34.32 OK 860.56 12.50 1.592E+OO Line Not Found Absent PB-212 74.82 10.28 3.338E+OO 4.161E-01 4.161E-01 170.92 OK 77 .11 17.10 3.578E+OO l.279E+OO 1. 27 9E+OO 32.68 OK 238.63 43.60* 4.585E+OO 9.891E-01 9.891E-01 13.62 OK 300.09 3.30 3.818E+OO 1.663E+00 1.663E+OO 64.02 OK BI-214 609.32 45.49* 2.101E+OO 8.600E-01 8.603E-01 27.23 OK 1120.29 14.92 1. 288E+OO 1.341E+OO 1.341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 OK PB-214 74.82 5.80 3.340E+OO Line Not Found <<INT Reject 77 .11 9.70 3.578E+00 2.254E+OO 2.255E+OO 32.68 OK 87.09 3.41 4.447E+OO Line Not Found <<INT Reject 242.00 7.25 4.538E+OO Line Not Found <<INT Reject 295.22 18.42 3.868E+OO 1.177E+OO 1.178E+OO 29.49 OK 351. 93 35.60* 3.336E+OO 9.566E-01 9.569E-01 19.55 OK RN-219 271. 23 10.80 4.160E+OO 2.940E-01 2.940E-01 118.36 OK 401.81 6.60* 2.983E+OO 6.899E-01 6.899E-01 76.53 OK RN-222 609.32 45.49* 2.101E+OO 8.600E-01 8.603E-01 27.23 OK 1120.29 14.92 l.288E+OO 1.341E+OO 1.341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 OK RA-224 240.99 4.10* 4.543E+OO 3.268E-01 3.268E-01 542.80 OK RA-226 609.32 45.49* 2. 101E+OO 8.600E-01 8.603E-01 27.23 OK 1120.29 14.92 l.288E+OO 1.341E+OO 1. 341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 OK AC-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 OK 794.95 4.25 1.695E+OO 8.749E-01 8.749E-01 180.84 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* 1.521E+OO l .136E+OO 1.136E+OO 35.58 OK 968. 97 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 OK RA-228 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 OK 794.95 4.25 1.695E+OO 8.749E-01 8.749E-01 180.84 OK 835. 71 1. 61 l.630E+OO Line Not Found Absent 911. 20 25.80* 1. 521E+OO 1.136E+OO l.136E+OO 35.58 OK 968. 97 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 OK TH-228 74.82 10.28 3.338E+OO 4 .161E-01 4.161E-01 170.92 OK 77 .11 17.10 3.578E+OO 1.279E+OO 1. 27 9E+OO 32.68 OK 238.63 43.60* 4.585E+OO 9. 891E-01 9.891E-01 13. 62 OK 300.09 3.30 3.818E+OO l.663E+OO 1.663E+OO 64.02 OK TH-229 85.43 14.70 4.223E+OO 3.627E-01 3.627E-01 96. 63 OK Page 4393 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status 88.47 24.00 4.459E+OO 1.167E-01 1.167E-01 179.82 OK 193.51 4.41* 5.283E+OO Line Not Found Absent 210.85 2.80 4.994E+OO 1.143E+OO 1.143E+OO 131.04 OK TH-230 609.32 45.49* 2.101E+OO 8.600E-01 8.600E-01 27.23 OK 1120.29 14.92 l.288E+OO 1.341E+OO 1. 341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.855E-01 54.19 OK PA-231 283.69 1. 70 4.000E+OO Line Not Found Absent 301.36 5.35* 3.818E+OO 1.026E+00 1.026E+OO 64.02 OK TH-232 105.21 1.10 5.460E+OO Line Not Found Absent 338.32 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 OK 835.71 1. 61 1.630E+OO Line Not Found Absent 911.20 25.80* 1.521E+OO 1.136E+OO 1.136E+OO 35.58 OK 968. 97 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 OK TH-234 63.29 3.70* 2.050E+OO 2.424E+OO 2.424E+OO 111.73 OK 92.59 4.23 4.835E+OO l.664E+OO 1.664E+OO 88.03 OK U-234 609.32 45.49* 2.101E+OO 8.600E-01 8.600E-01 27.23 OK 1120.29 14.92 l.288E+00 1. 341E+OO 1.341E+OO 44.37 OK 1764.49 15.30 8.674E-01 8.854E-01 8.854E-01 54.19 OK U-235 89. 96 3.47 4.649E+OO 1.608E+OO 1.608E+OO 112. 29 OK 93.35 5.60 4.835E+OO 1.257E+OO 1.257E+OO 88.03 OK 143.76 10. 96* 5.918E+OO Line Not Found <<INT Reject 163.33 5.08 5.731E+OO Line Not Found Absent 185. 72 57.20 5.403E+OO l.197E-01 1.197E-01 73 .11 OK 205.31 5.01 5.091E+OO 5.815E-01 5.815E-01 109.95 OK U-238 63.29 3.70* 2.050E+OO 2.424E+00 2.424E+OO 111. 73 OK 92.59 4.23 4.835E+OO 1.664E+OO 1.664E+OO 88.03 OK AM-243 43.53 5.90 1.573E-01 Line Not Found Absent 74.66 67.20* 3.338E+00 6.366E-02 6.366E-02 170.92 OK CM-247 278.00 3.40 4.067E+OO Line Not Found Absent 287.50 2.00 3.956E+OO Line Not Found Absent 402.40 72. 00* 2.983E+OO 6.324E-02 6.324E-02 76.53 OK ANH-511 511. 00 100.00* 2.429E+OO 1.255E-01 1.255E-01 56.85 OK Flag: "*" = Keyline Page 4394 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:56:32.59 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l *
  • Acquisition date 3-0CT-2016 05:53:40 Sensitivity 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:15:00 Analyst initials: MXRl *
  • Sample ID G405235063 Sample Quantity 1.4788E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.163E+Ol 1.590E+OO CD-109 1.176E+OO 2.073E+OO TE-125M 5 .118E+02 5.773E+02 SN-126 7.567E-02 l.334E-01 CE-141 7.054E+OO 3.876E+Ol TL-208 2.434E-01 8.186E-02 PB-212 9.891E-01 1.321E-01 BI-214 8.603E-01 2.296E-01 PB-214 9.569E-01 l.834E-01 RN-219 6.899E-01 5.174E-01 RN-222 8.603E-01 2.296E-01 RA-224 3.268E-01 1. 738E+OO RA-226 8.603E-01 2. 296E-01 AC-228 1.136E+OO 3.959E-01 RA-228 1.136E+OO 3.959E-01 TH-228 9.891E-01 1.321E-01 TH-229 2.170E-01 4.726E-01 TH-230 8.600E-01 2.295E-Ol PA-231 1. 026E+OO 6.435E-01 TH-232 1.136E+OO 3.959E-01 TH-234 2. 4.24E+OO 2.654E+OO U-234 8.600E-01 2.295E-01 U-235 l.909E-01 3.144E-01 U-238 2.424E+OO 2.654E+OO AM-243 6.366E-02 1.066E-01 CM-247 6.324E-02 4.743E-02 ANH-511 l.255E-01 6.992E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4395 of 5809 Key-Line Activity (pCi/GRAM 3.200E+00 2.212E-02 O.OOOE+OO K.L. Cnt Uncert ( 1 . 96-sigma ) 9.086E+OO 4.504E-02 1.321E+41 MDA (pCi/GRAM 8.231E-01 1.870E+OO 5.037E+02 l.212E-01 4.035E+Ol 7.148E-02 8.930E-02 1.248E-01 1.327E-01 7.187E-01 1.248E-01 9.576E-01 1.248E-01 2.269E-01 2.269E-01 8.930E-02 9. 051E-01 1.248E-01 8. 960E-01 2.269E-01 2.806E+OO 1.248E-01 3.688E-01 2.806E+OO l.039E-01 6.597E-02 4.576E-02 MDA (pCi/GRAM 1.926E+Ol 9.953E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -3.505E-02 3.864E-02 5.583E-02 NOT IDENT. SC-46 -3.425E-01 4.021E-01 7.099E-01 FAIL ABUN V-48 O.OOOE+OO l.221E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.083E+02 O.OOOE+OO SHORT HLIF MN-54 7.283E-02 7 .115E-02 l.545E-01 NOT IDENT. C0-56 -9.726E-02 5.283E-01 9.622E-01 NOT IDENT. MN-56 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF C0-57 1.636E-02 4.904E-02 9.535E-02 NOT IDENT. C0-58 -9.557E-02 4.462E-01 8.454E-01 NOT IDENT. FE-59 8. 441E+OO 6.596E+OO 1.562E+Ol NOT IDENT. C0-60 -1.242E-02 3. 931E-02 7.482E-02 NOT IDENT. ZN-65 7. 991E-02 2.182E-01 4.074E-01 NOT IDENT. GE-68 1.089E+OO l.922E+OO 4.429E+OO NOT IDENT. AS-73 l.684E+OO l.374E+Ol 2.770E+Ol NOT IDENT. AS-74 O.OOOE+OO 4. 651E+03 O.OOOE+OO SHORT HLIF SE-75 -5.889E-02 l.904E-01 3.335E-01 FAIL ABUN BR-77 O.OOOE+OO 3. 969E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 3.812E+02 O.OOOE+OO SHORT HLIF RB-83 5. 872E-01 8.037E-01 1.285E+OO FAIL ABUN KR-85 6.739E+OO 6.693E+OO 1.462E+Ol NOT IDENT. SR-85 6.637E-01 6.624E-01 1.447E+OO NOT IDENT. RB-86 O.OOOE+OO 1. 785E+04 O.OOOE+OO SHORT HLIF Y-88 -1.821E-01 1. 963E-01 3.046E-01 NOT IDENT. Y-91 -2.375E+02 5.230E+02 9.574E+02 NOT IDENT. NB-94 l.326E-02 2. 681E-02 5.712E-02 NOT IDENT. NB-95 1.592E-01 8.432E-01 l.645E+00 NOT IDENT. NB-95M 2.462E-01 2.407E+OO 4.064E+OO NOT IDENT. ZR-95 2.142E-01 1.564E+OO 3.024E+OO NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.899E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.350E+41 O.OOOE+OO SHORT HLIF RH-101 -4.416E-02 3.278E-02 5.433E-02 NOT IDENT. RH-102 3.669E-02 5.999E-02 1.266E-01 NOT IDENT. RU-103 -2.181E+OO 5.050E+OO 9.321E+OO FAIL ABUN RH-106 -3.128E-02 4.938E-01 9. 513E-01 NOT IDENT. RU-106 -3.128E-02 4.938E-01 9.513E-01 NOT IDENT. AG-108M -4.664E-03 2.191E-02 4.286E-02 NOT IDENT. AG-110M 5.776E-03 l.062E-01 2.169E-01 FAIL ABUN SN-113 -1.233E-01 1.936E-01 3.552E-01 NOT IDENT. CD-115 O.OOOE+OO 4.675E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 7.516E+04 O.OOOE+OO SHORT HLIF TE-123M 8.559E-02 1.297E-01 2.549E-01 NOT IDENT. SB-124 -l.613E-01 2.258E+OO 4.571E+OO NOT IDENT. SB-125 9.090E-02 l.187E-01 2.475E-01 FAIL ABUN I-126 O.OOOE+OO 6.620E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8 .110E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.638E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.869E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.095E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.122E+26 O.OOOE+OO SHORT HLIF BA-133 4.348E-02 3.887E-02 8.122E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 5. 696E-02 l.009E-01 1.189E-01 FAIL ABUN CS-135 4.569E-03 1.301E-01 2.381E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.334E+05 O.OOOE+OO SHORT HLIF BA-137M 2.924E-02 4.049E-02 8.363E-02 NOT IDENT. CS-137 3.089E-02 4.277E-02 8.834E-02 NOT IDENT. CE-139 -8.175E-02 l.103E-01 l.906E-01 NOT IDENT. BA-140 O.OOOE+OO 8.554E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.004E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 8.105E+40 O.OOOE+OO SHORT HLIF CE-144 6.516E-02 3.306E-01 6.369E-01 NOT IDENT. PM-144 l.627E-02 5.329E-02 1.078E-01 NOT IDENT. PR-144 l.408E+00 4.614E+OO 9.333E+OO NOT ID.ENT. PM-146 -9.657E-03 4.266E-02 8.149E-02 FAIL ABUN ND-147 O.OOOE+OO 2.385E+07 O.OOOE+OO SHORT HLIF PM-147 3.574E+02 8.541E+02 l.674E+03 NOT IDENT. PM-149 O.OOOE+OO 6.978E+39 O.OOOE+OO SHORT HLIF EU-150 7.598E-03 2.569E-02 4.787E-02 FAIL ABUN EU-152 -5.850E-03 l.064E-01 1.873E-01 NOT IDENT. GD-153 7.267E-02 l.730E-01 3.248E-01 NOT IDENT. EU-154 5.439E-02 l.108E-01 2.448E-01 NOT IDENT. EU-155 1.034E-01 l.159E-01 2.362E-01 FAIL ABUN TB-160 5. 961E-01 1. 754E+OO 3.768E+OO FAIL ABUN H0-166M 6.590E-02 7.199E-02 l.304E-01 FAIL ABUN TM-171 -9.680E+00 3.579E+Ol 6.997E+Ol FAIL ABUN Page 4396 of 5809 HF-172 l.058E-01 2.131E-01 4.231E-01 FAIL ABUN LU-172 -4.453E-02 8.206E-02 l.496E-01 FAIL ABUN LU-176 8.463E-03 2.022E-02 4.260E-02 FAIL ABUN HF-181 -2.553E-01 3. 431E+OO 6.756E+OO NOT IDENT. TA-182 2.742E-01 9. 965E-Ol 2.034E+OO FAIL ABUN RE-183 -5.749E-01 4.043E+OO 7.973E+OO FAIL ABUN RE-184 -8.429E+OO 2.806E+Ol 5.256E+Ol NOT IDENT. W-188 -8.826E+Ol l.089E+02 l.752E+02 FAIL ABUN IR-192 l.715E-02 4.312E-01 8.591E-01 FAIL ABUN HG-203 -6.890E-01 3.655E+OO NOT IDENT. BI-207 l.354E-02 5.154E-02 l.075E-01 FAIL ABUN PB-210 2.430E+OO 7.416E+OO l.544E+Ol NOT IDENT. BI-211 O.OOOE+OO 5.050E-01 8.217E-01 FAIL ABUN PB-211 l.031E+OO 9 .151E-01 l.377E+OO FAIL ABUN BI-212 7.967E-01 l.070E+OO l.324E+OO FAIL ABUN RA-223 2.211E-01 5.556E-01 l.147E+OO FAIL ABUN AC-227 3.202E-02 2.304E-01 4.249E-01 FAIL ABUN TH-227 3.202E-02 2.304E-01 4.249E-01 FAIL ABUN TH-231 2. 211E-01 5.556E-01 l.147E+OO FAIL ABUN PA-233 9.428E-03 5.455E-02 l.108E-01 FAIL ABUN PA-234 -5. 251E-02 2. 831E-01 5.586E-01 FAIL ABUN PA-234M 9.446E+OO 4.798E+OO l.099E+Ol FAIL ABUN NP-237 9.428E-03 5.455E-02 l.108E-01 FAIL ABUN NP-238 O.OOOE+OO 6.618E+40 0.000E+OO SHORT HLIF NP-239 -l.518E-01 2.458E-01 4.429E-01 NOT IDENT. PU-239 3.049E+02 2.953E+02 6.070E+02 NOT IDENT. AM-241 l.400E-01 l.970E-01 4. lllE-01 NOT IDENT. CM-243 -4.340E-02 l.027E-01 1. 901E'-01 NOT IDENT. BK-247 -5.989E-03 6. 501E-02 l.177E-01 FAIL ABUN CF-249 *-8. 936E-03 3.328E-02 6.415E-02 NOT IDENT. CF-251 -8.984E-02 l.146E-01 l.957E-01 NOT IDENT. Page 4397 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:56:29.65 Nuclide Line Activity Report Nuclide Type: .. Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 252 10.66* 1.030E+OO 1.163E+Ol 1.163E+Ol 13.95 CD-109 88.03 60 3.70* 4.459E+00 l.842E+00 2.863E+OO 71. 81 TE-125M 109.28 44 0.27* 5.627E+OO 1.475E+Ol 5 .118E+02 115 .11 SN-126 64.28 36 9.60 2.050E+OO 9. 341E-01 9.341E-01 111.73 86.94 60 8.90 4.459E+OO 7.657E-01 7.657E-01 71. 81 87.57 60 37.00* 4.459E+OO l.842E-01 1.842E-01 71. 81 CE-141 145.44 24 48.29* 5.912E+00 4.332E-02 2.272E+Ol 168.05 TL-208 277.37 ------6.60 4.074E+OO ------Line Not Found ------583.19 89 85.00* 2.178E+OO 2.434E-01 2.434E-01 34.32 860.56 ------12.50 1.592E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 3.135E+OO ------Line Not Found ------351.06 224 12.92* 3.336E+OO 2.636E+OO 2.636E+00 19.55 PB-212 74.82 73 10.28 3.338E+00 1.080E+OO l.080E+OO 63.29 77 .11 154 17.10 3.578E+OO l.279E+OO 1.279E+OO 32.68 238.63 389 43.60* 4.585E+OO 9.891E-01 9.891E-01 13.62 300.09 41 3.30 3.818E+OO 1.663E+OO 1.663E+OO 64.02 BI-214 609.32 162 45.49* 2.lOlE+OO 8.600E-01 8.603E-01 27.23 1120.29 51 14.92 1.288E+OO l.341E+00 1. 341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 PB-214 74.82 73 5.80 3.338E+OO 1.915E+OO 1.915E+OO 63.29 77 .11 154 9.70 3.578E+OO 2.254E+OO 2.255E+OO 32.68 87.09 60 3.41 4.459E+OO 1.998E+OO l.999E+OO 71. 81 242.00 88 7.25 4.543E+OO 1.362E+OO 1.363E+OO 69.10 295.22 165 18.42 3.868E+OO l.177E+00 l.178E+00 29.49 351.93 224 35.60* 3.336E+OO 9.566E-01 9.569E-01 19.55 RN-219 271.23 26 10.80 4.160E+OO 2.940E-01 2.940E-01 118. 36 401.81 27 6.60* 2.983E+00 6.899E-01 6.899E-01 76.53 RN-222 609.32 162 45.49* 2.lOlE+OO 8.600E-01 8.603E-01 27.23 1120. 29 51 14.92 1.288E+OO 1.341E+OO 1.341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 RA-224 240.99 88 4.10* 4.543E+OO 2.409E+OO 2.409E+OO 69.10 RA-226 609.32 162 45.49* 2.101E+OO 8.600E-01 8.603E-01 27.23 1120.29 51 14.92 1. 288E+OO 1.341E+OO 1. 341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.858E-01 54.19 AC-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 72 11. 27 3.448E+00 9.424E-01 9.424E-01 68.32 794.95 12 4.25 1.695E+OO 8.749E-01 8.749E-01 180.84 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 88 25.80* 1.521E+OO l.136E+OO 1.136E+OO 35.58 968. 97 31 15.80 l.448E+00 6.987E-01 6.987E-01 65.47 RA-228 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 72 11.27 3.448E+00 9.424E-01 9.424E-01 68.32 794.95 12 4.25 1.695E+OO 8.749E-01 8.749E-01 180.84 835. 71 ------1. 61 1.630E+OO ------Line Not Found ------911.20 88 25.80* l.521E+OO l.136E+OO 1.136E+OO 35.58 968. 97 31 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 TH-228 74.82 73 10.28 3.338E+OO 1.080E+OO 1.080E+OO 63.29 Page 4398 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 77.J.1 154 17.10 3.578E+OO 1.279E+OO ,1. 279E+OO 32.68 238.63 389 43.60* 4.585E+OO 9.891E-01 9.891E-01 13.62 300.09 41 3.30 3.818E+OO l.663E+OO 1. 663E+OO 64.02 TH-229 85.43 44 14.70 4.223E+OO 3.627E-01 3.627E-01 96. 63 88.47 60 24.00 4.459E+OO 2.839E-01 2.840E-01 71. 81 193.51 ------4.41* 5.283E+OO ------Line Not Found ------210.85 31 2.80 4.994E+OO 1.143E+OO 1.143E+OO 131. 04 TH-230 609.32 162 45.49* 2.101E+OO 8.600E-01 8.600E-01 27.23 1120.29 51 14.92 1.288E+OO 1. 341E+OO 1.341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.855E-01 54.19 PA-231 283.69 ------1. 70 4.000E+OO ------Line Not Found ------301.36 41 5.35* 3.818E+OO 1.026E+OO l.026E+OO 64.02 TH-232 105.21 ------1.10 5.460E+OO ------Line Not Found ------338.32 72 11. 27 3.448E+OO 9.424E-01 9.424E-01 68.32 835.71 ------1. 61 1.630E+OO ------Line Not Found ------911. 20 88 25.80* 1.521E+OO l.136E+OO 1.136E+OO 35.58 968. 97 31 15.80 1.448E+OO 6.987E-01 6.987E-01 65.47 TH-234 63.29 36 3.70* 2.050E+OO 2.424E+OO 2.424E+OO 111.73 92.59 67 4.23 4.835E+OO 1.664E+OO 1.664E+OO 88.03* U-234 609.32 162 45.49* 2.101E+OO 8.600E-01 8.600E-01 27.23 1120.29 51 14.92 l.288E+OO 1.341E+OO 1.341E+OO 44.37 1764.49 23 15.30 8.674E-01 8.854E-01 8.854E-01 54.19 U-235 89. 96 51 3.47 4.649E+OO 1.608E+OO 1.608E+OO 112. 29 93.35 67 5.60 4.835E+OO 1.257E+OO 1.257E+OO 88.03 143.76 24 10. 96* 5.912E+OO 1.909E-01 l.909E-01 168.05 163.33 ------5.08 5.731E+OO ------Line Not Found ------185. 72 73 57.20 5.403E+OO 1.197E-01 1.197E-01 73 .11 205.31 29 5.01 5.091E+OO 5.815E-01 5.815E-01 109.95 U-238 63.29 36 3.70* 2.050E+OO 2.424E+OO 2.424E+OO 111.73 92.59 67 4.23 4.835E+OO 1.664E+OO 1.664E+OO 88.03 AM-243 43.53 ------5.90 1. 573E-01 ------Line Not Found ------74.66 73 67.20* 3.338E+OO 1.653E-01 1. 653E-01 63.29 CM-247 278.00 ------3.40 4.067E+OO ------Line Not Found ------287.50 ------2.00 3.956E+OO ------Line Not Found ------402.40 27 72.00* 2.983E+OO 6.324E-02 6.324E-02 76. 53 ANH-511 511. 00 60 100.00* 2.429E+OO 1.255E-01 1.255E-01 56.85 Flag: "*" Key line Page 4399 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235063 Acquisition date 3-0CT-2016 05:53:40 Total number of lines in spectrum 47 Number of unidentified lines 5 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 CD-109 TE-125M SN-126 CE-141 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Hlife 1. 25E+09Y 461.40D 57.40D 2.30E+05Y 32.51D 1. 41E+l0Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 7.04E+08Y 1600.00Y 1. 41E+10Y 1600. OOY 1. 41E+l0Y 1.41E+10Y 1.41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.56E+07Y l.OOE+09Y Decay 1. 00 1. 55 34.7 1. 00 524. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.163E+Ol 1.842E+OO l.475E+Ol l.842E-01 4.332E-02 2.434E-01 2.636E+OO 9.891E-01 8.600E-01 9.566E-01 6.899E-01 8.600E-01 2.409E+OO 8.600E-01 l.136E+OO l.136E+00 9.891E-01 2.839E-01 8.600E-01 1. 026E+00 1.136E+OO 2.424E+00 8.600E-01 1.909E-01 2.424E+OO l.653E-01 6.324E-02 1.255E-01 5.177E+Ol 5.177E+Ol Decay Corr pCi/GRAM 1.163E+Ol 2.863E+OO 5 .118E+02 l.842E-01 2.272E+Ol 2.434E-01 2.636E+OO 9. 891E-01 8.603E-01 9.569E-01 6.899E-01 8.603E-01 2.409E+OO 8.603E-01 1.136E+OO 1.136E+OO 9.891E-01 2.840E-01 8.600E-01 1. 026E+00 l.136E+OO 2.424E+00 8.600E-01 l.909E-01 2.424E+OO 1.653E-01 6.324E-02 1.255E-01 5.725E+02 5.725E+02 89.36%
  • Decay Corr 2-Sigma Error 0.162E+Ol 2.056E+OO 5. 8 91E+02 1.323E-01 3.818E+Ol 0.835E-01 0.515E+OO 1. 34 7E-01 2.343E-01 1. 871E-01 5.280E-01 2.343E-01 l.664E+00 2.343E-01 0.404E+OO 0.404E+OO 1. 34 7E-01 2.039E-01 2.342E-01 0.657E+OO 0.404E+OO 2.708E+OO 2.342E-01 3.208E-01 2.708E+OO 1. 046E-01 4.840E-02 0. 713E-01 "M" Manually accepted 2-Sigma %Error 13.95 71. 81 115 .11 71. 81 168.05 34.32 19.55 13. 62 27.23 19.55 76.53 27.23 69.10 27.23 35.58 35.58 13.62 71. 81 27.23 64.02 35.58 111.73 27.23 168.05 111.73 63.29 76.53 56. 85 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4400 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235063 Acquisition date : 3-0CT-2016 05:53:40 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 65.77 28 94 1. 09 131.99 124 11 6.15E-03 **** 2.34E+OO T 0 154.39 25 96 0.83 309.31 306 6 5.83E-03 **** 5.83E+OO T 3 209.50 40 71 1. 20 419.57 408 29 9.60E-03 84.7 5.03E+OO
  • 1 405.01 23 20 1. 53 810.76 .799 19 5.78E-03 90.5 2. 96E+OO T 0 463.97 20 40 2.60 928.75 922 10 5.24E-03 **** 2.64E+OO T 0 520.52 12 17 0.87 1041. 91 1038 8 3.06E-03 **** 2.39E+OO T 5 543.58 11 6 1. 56 1088.05 1086 12 2.87E-03 73.4 2.31E+OO 5 546.66 16 11 1. 65 1094.23 1086 12 4.25E-03 91. 6 2.30E+OO T 0 678. 72 8 12 0.61 1358.50 1352 8 2.00E-03 **** 1. 93E+OO T 0 711. 57 13 13 0.64 1424.23 1420 8 3.49E-03 **** 1. 85E+OO T 0 728.58 19 32 1. 89 1458.28 1449 14 5.12E-03 **** 1. 82E+OO T 0 746.85 12 5 1.29 1494.85 1491 7 3. 31E-03 85.9 1.78E+OO T 0 773.10 16 13 1. 59 1547.37 1541 10 4. 21E-03 **** 1.73E+OO T 0 776.26 10 0 0.95 1553.70 1551 6 2.78E-03 63.2 1. 73E+OO T 0 840.54 16 8 1. 51 1682.34 1678 8 4.28E-03 81.1 1.62E+OO 0 862.77 11 32 1. 71 1726.83 1719 15 2.97E-03 **** 1.59E+OO 0 1000.74 22 3 0.97 2002.97 1998 11 6.12E-03 51. 8 1. 41E+OO T 0 1377.40 7 4 0.55 2756.93 2752 8 1. 94E-03 **** 1.08E+OO Flags: "T" = Tentatively associated Page 4401 of 5 809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:56:47.05 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* ** * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l *
  • Acquisition date 3-0CT-2016 05:53:40 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:15:00 Nuclide Library : SOLID *
  • Sample ID G405235063 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4788E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3'
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 TE-125M SN-126 CE-141 TL-208 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 CM-247 ANH-511 Le (pCi/GRAM 3.487E-01 8.669E-01 2.351E+02 5.617E-02 1.884E+Ol 3.193E-02 4.106E-02 5.504E-02 6.037E-02 3.232E-01 5.504E-02 4.403E-01 5.504E-02 9.566E-02 9.566E-02 4.106E-02 4.216E-01 5.502E-02 4.129E-01 9.566E-02 1.306E+00 5.502E-02 1.732E-01 1.306E+00 4:868E-02 2. 967E-02 1. 997E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4402 of 5809 Le (pCi/GRAM 8.423E+OO 4.235E-02 O.OOOE+OO 1.978E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 4403 of 5809 3.038E-01 O.OOOE+OO O.OOOE+OO 6.903E-02 4.206E-01 O.OOOE+OO 4.461E-02 3.481E-01 6.897E+OO 3. 051E-02 1. 793E-01 1.870E+OO 1.287E+Ol 0.000E+OO 1.510E-01 O.OOOE+OO O.OOOE+OO 5.730E-01 6.603E+OO 6.532E-01 O.OOOE+OO 9.627E-02 4.074E+02 2.481E-02 7.262E-01 1.882E+OO 1.336E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.502E-02 5.619E-02 4.102E+OO 4.164E-01 4.164E-01 1. 862E-02 9. 451E-02 *1.565E-01 0.000E+OO 0.000E+OO 1.192E-01 1.814E+OO 1.134E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 3.695E-02 O.OOOE+OO 5.315E-02 1.083E-01 O.OOOE+OO O.OOOE+OO 3.777E-02 3.990E-02 8.833E-02 O.OOOE+OO 0.000E+OO O.OOOE+OO 2.959E-01 4.734E-02 4.099E+OO 3.626E-02 0.000E+OO 7.831E+02 0.000E+OO 2.178E-02 8.547E-02 1.509E-01 l.042E-01 l .110E-01 1.637E+OO 5. 821E-02 3. 241E+Ol 1. 969E-01 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. N,OT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDEl\!T. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 4404of5809 6.347E-02 1. 926E-02 2.958E+OO 8.903E-01 3.709E+OO 2.252E+Ol 7.922E+Ol 3.923E-01 1. 656E+OO 4.668E-02 7.168E+OO 3.945E-01 6.251E-01 6.043E-01 5.235E-01 1. 951E-01 1. 951E-01 5.235E-01 5.040E-02 2.400E-01 4.908E+OO 5.040E-02 O.OOOE+OO 2.056E-01 2.841E+02 l.927E-01 8.842E-02 5.321E-02 2.856E-02 9.031E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FALL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:56:54.34 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235063.CNF;l * *Acquisition date 3-0CT-2016 05:53:40 Sensitivity : 3.000 *
  • Detector ID GAM44 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:15:00 Nuclide Library : SOLID *
  • Sample ID G405235063 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4788E+02 GRAM *
  • Quantity Err(%) : 1.3524E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 04:59:25 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM44 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1. 96-sigma) K-40 1.163E+Ol 1. 702E+OO CD-109 1.176E+OO 2.086E+OO TE-125M 5 .118E+02 5.781E+02 SN-126 7.567E-02 1. 341E-01 CE-141 7.050E+OO 3.878E+Ol TL-208 2.434E-01 8. 251E-02 PB-212 9.891E-01 1. 421E-01 BI-214 8.603E-01 2.325E-01 PB-214 9.569E-01 1. 876E-01 RN-219 6.899E-01 5.246E-01 RN-222 8.603E-01 2.325E-01 RA-224 3.268E-Ol 1. 744E+OO RA-226 8.603E-01 2.325E-01 AC-228 l.136E+OO 4.002E-01 RA-228 l.136E+OO 4.002E-01 TH-228 9.891E-01 l.421E-01 TH-229 2.170E-01 4.727E-01 TH-230 8.600E-01 2.324E-01 PA-231 1.026E+OO 6.797E-01 TH-232 l.136E+OO 4.002E-01 TH-.234 2.424E+OO 2.708E+OO U-234 8.600E-01 2.324E-01 U-235 l.909E-01 3.145E-01 U-238 2.424E+OO 2.708E+OO AM-243 6.366E-02 1. 075E-01 CM-247 6.324E-02 4.861E-02 ANH-511 l.255E-01 7.0lOE-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4405 of 5809 Key-Line Activity (pCi/GRAM 3.200E+00 2.212E-02 -l.OOOE+41 K.L Act error ( 1. 96-sigma) 9.087E+OO 4.505E-02 l.388E+41 TPU ( 1. 96-sigma) 1. 702E+OO 2.086E+OO 5. 781E+02 1. 341E-01 3.878E+Ol 8. 251E-02 l.421E-01 2.325E-01 1. 876E-01 5.246E-01 2.325E-01 1. 744E+OO 2.325E-01 4.002E-01 4.002E-01 l.421E-01 4.727E-01 2.324E-01 6.797E-01 4.002E-01 2.708E+OO 2.324E-01 3.145E-01 2.708E+OO 1. 07 5E-01 4.861E-02 7.0lOE-02 TPU ( 1. 96-sigma) 9.201E+OO 4.614E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -3.505E-02 3.870E-02 4.180E-02 NOT IDENT. SC-46 -3.425E-01 4.024E-01 4.310E-01 FAIL ABUN V-48 4. 727E+Ol 1.221E+04 1. 221E+04 SHORT HLIF CR-51 4.340E+Ol 3.083E+02 3.090E+02 SHORT HLIF MN-54 7.283E-02 7.122E-02 7.842E-02 NOT IDENT. C0-56 -9. 726E-02 5.283E-01 5.301E-01 NOT IDENT. MN-56 -l.000E+41 5.144E+41 O.OOOE+OO SHORT HLIF C0-57 1.636E-02 4.904E-02 4.959E-02 NOT IDENT. C0-58 -9.557E-02 4.462E-01 4.483E-01 NOT IDENT. FE-59 8.441E+00 6.624E+OO 7.639E+OQ NOT IDENT. C0-60 -1.242E-02 3.932E-02 3. 971E-02 NOT IDENT. ZN-65 7.991E-02 2.182E-01 2.212E-01 NOT IDENT. GE-68 1.089E+00 1.922E+OO l.984E+OO NOT IDENT. AS-73 1. 684E+OO 1.375E+Ol 1.377E+Ol NOT IDENT. AS-74 3.817E+02 4. 651E+03 4.654E+03 SHORT HLIF SE-75 -5.889E-02 l.904E-01 l.923E-01 FAIL ABUN BR-77 2.973E+37 2.520E+38 O.OOOE+OO SHORT HLIF SR-82 6 .151E+02 3.823E+02 4.723E+02 SHORT HLIF RB-83 5. 872E-01 8.077E-01 8.500E-01 FAIL ABUN KR-85 6.739E+OO 6.698E+OO 7.355E+OO NOT IDENT. SR-85 6.637E-01 6.630E-01 7.274E-01 NOT IDENT. RB-86 1. 616E+04 1.787E+04 1.930E+04 SHORT HLIF Y-88 -1.821E-01 1. 967E-01 2 .131E-01 NOT IDENT. Y-91 -2.375E+02 5. 231E+02 5.339E+02 NOT IDENT. NB-94 l.326E-02 2.682E-02 2.748E-02 NOT IDENT. NB-95 l.592E-01 8.433E-01 8.463E-01 NOT IDENT. NB-95M 2.462E-01 2.407E+OO 2.410E+00 NOT IDENT. ZR-95 2.142E-01 1.564E+OO 1.567E+OO NOT IDENT. NB-97 1.000E+41 7.694E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 7.676E+41 O.OOOE+OO SHORT HLIF M0-99 2.974E+31 3.905E+31 O.OOOE+OO SHORT HLIF TC-99M l.000E+41 1.353E+41 O.OOOE+OO SHORT HLIF RH-101 -4.416E-02 3.374E-02 3.917E-02 NOT IDENT. RH-102 3.669E-02 6.006E-02 6.230E-02 NOT IDENT. RU-103 -2.181E+OO 5.052E+OO 5.146E+OO FAIL ABUN RH-106 -3.128E-02 4.938E-01 4. 941E-01 NOT IDENT. RU-106 -3.128E-02 4.938E-01 4.941E-01 NOT IDENT. AG-108M -4.664E-03 2. 191E-02 2.201E-02 NOT IDENT. AG-110M 5.776E-03 l.062E-01 l.062E-01 FAIL ABUN SN-113 -l.233E-01 l.937E-01 2.015E-01 NOT IDENT. CD-115 2.448E+38 4. 696E+38 O.OOOE+OO SHORT HLIF SN-117M l.310E+04 7. 518E+04 7.541E+04 SHORT HLIF TE-123M 8.559E-02 1. 2 98E-01 1.354E-01 NOT IDENT. SB-124 -l.613E-01 2.258E+OO 2.259E+OO NOT IDENT. SB-125 9.090E-02 l.187E-01 l.256E-01 FAIL ABUN I-126 -4.375E+05 6.646E+05 6.933E+05 SHORT HLIF SB-126 -1. 847E+05 8 .117E+05 8.160E+05 SHORT HLIF SB-127 -1.244E+21 7.820E+21 O.OOOE+OO SHORT HLIF I-131 -l.666E+09 2.870E+09 2. 967E+09 SHORT HLIF I-132 -l.OOOE+41 1.814E+42 O.OOOE+OO SHORT HLIF TE-132 -5. 729E+25 1.145E+26 O.OOOE+OO SHORT HLIF BA-133 4.348E-02 3. 8 91E-02 4.357E-02 NOT IDENT. I-133 1.000E+41 7.702E+41 O.OOOE+OO SHORT HLIF CS-134 5. 696E-02 1.0lOE-01 l.042E-01 FAIL ABUN CS-135 4.569E-03 l.301E-01 1.301E-01 NOT IDENT. I-135 1. 000E+41 7.470E+41 O.OOOE+OO SHORT HLIF CS-136 -1.183E+05 2.337E+05 2.397E+05 SHORT HLIF BA-137M 2.924E-02 4.051E-02 4.260E-02 NOT IDENT. CS-137 3.089E-02 4.279E-02 4.500E-02 NOT IDENT. CE-139 -8.175E-02 1.116E-01 l.175E-01 NOT IDENT. BA-140 1.573E+05 8.555E+05 8.584E+05 SHORT HLIF LA-140 6.169E+04 3.004E+05 3.017E+05 SHORT HLIF CE-143 1.000E+41 8.166E+40 O.OOOE+OO SHORT HLIF CE-144 6.516E-02 3.306E-01 3.319E-01 NOT IDENT. PM-144 l.627E-02 5.330E-02 5.380E-02 NOT IDENT. PR-144 1.408E+OO 4.615E+OO 4.658E+OO NOT IDENT. PM-146 -9.657E-03 4.266E-02 4.289E-02 FAIL ABUN ND-147 -2.092E+07 2.388E+07 2.567E+07 SHORT HLIF PM-147 3.574E+02 8.542E+02 8.693E+02 NOT IDENT. PM-149 -1.286E+39 6.984E+39 O.OOOE+OO SHORT HLIF EU-150 7.598E-03 2.569E-02 2.592E-02 FAIL ABUN EU-152 -5.850E-03 l.064E-01 1.064E-01 NOT IDENT. GD-153 7.267E-02 1.731E-01 1. 761E-01 NOT IDENT. EU-154 5.439E-02 1.108E-01 l.135E-01 NOT IDENT. EU-155 1.034E-01 1.161E-01 1.251E-01 FAIL ABUN TB-160 5. 961E-01 1. 754E+OO 1. 774E+OO FAIL ABUN H0-166M 6.590E-02 7.208E-02 7. 796E-02 FAIL ABUN TM-171 -9.680E+OO 3.580E+Ol 3.607E+Ol FAIL ABUN Page 4406 of 5809 HF-172 1.058E-01 2.137E-01 2.190E-01 FAIL ABUN LU-172 -4.453E-02 8.219E-02 8.460E-02 FAIL ABUN LU-176 8.463E-03 2.023E-02 2.058E-02 FAIL ABUN HF-181 -2.553E-01 3.431E+OO 3.433E+OO NOT IDENT. TA-182 2.742E-01 9. 965E-01 1.004E+OO FAIL ABUN RE-183 -5.749E-01 4.044E+OO 4.052E+OO FAIL ABUN RE-184 -8.429E+OO 2. 813E+Ol 2.838E+Ol NOT IDENT. W-188 -8.826E+Ol l.093E+02 1.163E+02 FAIL ABUN IR-192 l.715E-02 4.312E-01 4.313E-01 FAIL ABUN HG-203 -6.890E-01 l.883E;l-00 1.908E+OO NOT IDENT. BI-207 l.354E-02 5.154E-02 5.190E-02 FAIL ABUN PB-210 2.430E+OO 7.419E+OO 7.499E+OO NOT IDENT. BI-211 2.636E+OO 5.186E-01 1.296E+OO FAIL ABUN PB-211 1. 031E+OO 9.166E-01 1.028E+OO FAIL ABUN BI-212 7. 967E-Ol 1.071E+OO l.129E+OO FAIL ABUN RA-223 2.211E-Ol 5.557E-01 5.646E-01 FAIL ABUN AC-227 3.202E-02 2.304E-01 2.309E-01 FAIL ABUN TH-227 3.202E-02 2.304E-01 2.309E-01 FAIL ABUN TH-231 2. 211E-01 5.557E-01 5.646E-01 FAIL ABUN PA-233 9.428E-03 5.455E-02 5.471E-02 FAIL ABUN PA-234 -5. 251E-02 2.894E-01 2.904E-01 FAIL ABUN PA-234M 9.446E+OO 4. 816E+OO
  • 6.428E+OO FAIL ABUN NP-237 9.428E-03 5.455E-02 5. 471E-02 FAIL ABUN NP-238 1. 001E+40 6.618E+40 O.OOOE+OO SHORT-HLIF NP-239 -l.518E-01 2.461E-01 2.555E-01 NOT IDENT. PU-239 3.049E+02 2.956E+02 3.260E+02 NOT IDENT. AM-241 1.400E-01 l.973E-01 2.072E-01 NOT IDENT. CM-243 -4.340E-02 1.028E-01 1.046E-01 NOT IDENT. BK-247 -5.989E-03 6.502E-02 6.508E-02 FAIL ABUN CF-249 -8.936E-03 3.329E-02 3.353E-02 NOT IDENT. CF-251 -8.984E-02 1.150E-01 1.220E-01 NOT IDENT. Page 4407 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 55.5689 87.09 53.8617 136.47 61.2174 45.60 47.9465 87.57 53.9151 140.51 0.0000 46.54 49.8688 88.03 53. 9656 143.76 69.4795 49.72 0.0000 88.34 53.9998 144.24 67.3556 51. 35 60.5342 88.47 54.0139 145.44 66.7464 51. 87 64.2452 89.96 54.1766 152.43 61. 5482 52.39 55.2794 1093.63 54.2504 153.25 0.0000 52.97 47.2020 91.11 0.0000 323.87 67.2083 53.44 51.8100 92.59 54.4606 156.02 0.0000 54.07 58.2764 93.35 54.5420 158.56 0.0000 57.36 0.0000 94.56 42.6699 159.00 55.4504 57.53 58.8362 94.65 42.6774 162.33 66.8381 57.98 62.5892 94.67 42.6790 162.66 0.0000 59.27 52.6458 94.87 42.6956 163.33 54.6570 59.32 52.6528 97.43 48.2692 165.86 70.5078 59.54 59.1533 98.43 60.4509 176.31 46.5041 60. 96 68.0330 98.44 60.4520 176.60 0.0000 61.17 68.0702 99.53 65.6244 177.52 64.7504 62.93 59.6769 100 .11 65.6953 181.07 0.0000 63.29 59.7314 102.03 67.9584 181.52 66.9740 63.58 59.7755 103.18 69.1180 184.41 64.1553 64.28 59.8813 103.37 69.1424 143.76 64.2578 66.73 57.7368 105.21 60.1920 193.51 52 .1157 67.24 54.0387 105.31 60.2028 197.03 58.1444 125.81 66.6775 106.12 70.8499 198.01 55.8816 67.75 66.6883 106.47 70.8943 201.83 56.1270 69.67 75.8466 109.28 65.7676 203.43 46.8573 70.83 66.5484 111. 00 65. 9658 205.31 51.6518 72. 81 92. 9632 111.76 0.0000 210.85 51.9707 72.87 92.9765 114.06 55.2616 215.65 52.2440 74.66 72.8967 116. 30 0.0000 222 .11 45.4329 74.82 72.9234 116.74 69.7383 227.09 54.0843 74.97 72.9483 119.76 70.0895 227.38 54.1008 77 .11 73.3003 121.12 60.8099 228.16 0.0000 78.74 60.6591 121.22 60.8201 228.18 64.9753 79.69 55.6121 121.78 68.2224 116.74 64.9753 80.12 64. 7257 122.06" 63.0034 235.69 50.1189 80.19 0.0000 122.92 66.2458 235. 96 50.1322 80.57 62.1973 123.07 65.2104 238.63 43.7816 81. 00 60.9584 265.00 62 .1163 238.98 0.0000 81. 07 50.5900 125.81 49.6517 240.99 43.8849 81. 75 61.0564 127.23 75.1742 242.00 43.9294 83.79 65.2359 127.91 78.4353 244.70 32.6274 84.00 70.4861 129.30 48.8631 252.40 0.0000 85.43 74.6246 131. 20 67.1201 252.80 40.6961 86.55 51.1776 133.02 65.1709 254.15 0.0000 86. 79 51. 2026 133.52 53.4599 256.23 39.5928 86. 94' 51.2188 136.00 54.7346 260.90 0.0000 Page 4408 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 36.1668 355.39 0.0000 584.27 13.9098 264.80 31.1829 356.01 17.4886 595.83 0.0000 265.00 31.1882 364.49 0.0000 427.87 18.6980 268.22 33.7838 366.42 0.0000 602.52 0.0000 269.46 32.5698 372.51 19.9702 604. 72 20.2974 270.03 32.5865 375.05 31. 8291 607.14.i 28.1371 271.23 27.6041 377.52 30.0627 609.32 18.7786 273.65 0.0000 356.01 30.1976 610.33 18.7874 276.40 35.2974 388.16 25.6997 614.28 277.37 44.5807 388.63 0.0000 618.01 17.8100 277.60 44.5894 391.69 26.6825 620.36 18.8789 278.00 34.5062 264.66 26.8471 621. 93 15.7446 279.20 37. 0713 401.81 26.8677 630.19 0.0000 279.54 48.8809 402.40 26.8789 631.29 13.7067 279.70 50.5737 404.85 26.9232 633.25 22.1621 280.46 47.2340 410.95 23.4912 634.78 0.0000 283.69 42.2943 413.71 26.1492 635.95 14.7935 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 47.4414 423. 72 0.0000 645.85 15.9241 285.90 0.0000 427.09 27.3214 657.76 22.4167 287.50 39.8905 427.87 28.2776 657.90 0.0000 290.67 44.6814 433.94 17.0328 661.66 19.2488 293.27 0.0000 439.40 26.5872 664.57 0.0000 351.93 35.8853 453.88 24.9124 666.33 0.0000 295. 96 35.9083 463.37 20.2386 666.50 0.0000 879.38 15.4237 468.07 23.1958 667.71 0.0000 299.98 42.4655 473.00 0.0000 677.62 11. 3101 300.09 42.4696 475.06 23.2930 685.70 0.0000 300.13 42.4706 476.78 18.4592 695.00 0.0000 301.36 46.3799 477.60 12.6361 696. 49 14.1204 302.85 20.6392 482.18 17.5437 696. 51 14.1209 256.23 38.7524 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13. 0391 306.78 24.1588 497.08 23.5947 697.49 14.1267 308.46 25.0564 505.52 16.2996 702.65 9.8020 311.90 31.1931 507.63 0.0000 706.68 9.8192 316.51 36.5295 511. 00 15.8548 711. 68 24. 6011 319.41 0.0000 514.00 15.8815 720. 70 0.0000 320.08 0.0000 514.00 15.8815 721. 93 0.0000 321. 04 30.5524 520.40 16.9343 722. 78 8.2397 323.87 30.6222 520.69 0.0000 722.91 9.8881 325.23 42.9179 522.65 0.0000 723.31 9.8899 328.76 0.0000 527.90 0.0000 724.19 21.4360 333.37 34.3789 528.26 16.0072 727. 33 13.2090 333.97 29.1033 529.59 17.0201 733.00 19.8611 334.37 34.4059 529.87 0.0000 735.93 17.6758 338.28 33.6257 531. 02 0.0000 333.97 19.8984 338.32 33.6265 537.26 0.0000 739.50 0.0000 311. 90 33.6829 546.56 0.0000 747.24 4.9949 340.48 33.6829 552.55 19.2582 748.06 9.9932 340.55 0.0000 563.25 22.4243 752.31 15.5723 344.28 37.3370 569.33 14.3150 753.82 0.0000 345.93 30.2633 946.00 14.3162 756.73 17.8294 351.06 33.9551 569.70 14.3179 756.80 17.8301 351.93 33.9767 583.19 23.6851 884.68 15.6469 Page 4409 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 16.7773 1274.44 7.2983 1620.50 3.2291 766.42 19.0185 1001.03 7.3098 1621. 92 6.4603 766.84 16 .1127 1002.74 8.7765 1678.03 0.0000 772. 60 0.0000 1004.73 11. 7098 1690.97 5.4636 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000
  • 1025.87 0.0000 1764.49 3.5500 778.90 11. 8061 1028.54 0.0000 1063.66 2.2214 783.70 0.0000 1037.84' 12.9447 1771. 35 1.1110 785.37 12.4005 1038.76 0.0000 1791.20 0.0000 792.07 10.1730 631.29 10.1984 1808.65 7.8348 794.95 13.5791 1048.07 0.0000 1810.72 0.0000 795.86 15.2820 1049.04 12.0621 1836.06 5.4015 810.06 12.5214 1050.41 14.8525 810.29 12.5227 1063.66 12.1177 344.28 9.1077 1077.00 0.0000 810.76 9.1090 1077.34 5.6162 815.77 0.0000 1085.87 11.2617 1048.07 0.0000 1093.63 15.9925 832.01 11.4795 1099.45 6. 5967 834.85 11.4917 1112. 07 18.9197 835.71 13.7949 1112. 84 18.3827 836.80 0.0000 1115. 54 13.6362 846.75 0.0000 1120.29 13.2762 846.77 18.4701 1120.55 13.2771 856.80 0.0000 1221.41 13.2797 860.56 12.7635 1129. 67 12.3621 871.09 20.9663 1131.51 0.0000 873.19 17.4854 1147.95 0.0000 875.33 0.0000 1173.23 17.3353 879.38 11. 3913 1177.95 5.7861 880.51 10.5194 1189.05 17.4133 883.24 19.3044 1204.77 15.5469 884.68 14.9248 1221.41 13.6667 889.28 21.1055 1231. 02 13.7026 894.76 15.8604 1235.36 0.0000 898.04 14.9964 1238.28 16.6721 900.72 12.3619 1260.41 0.0000 903.28 15.1507 1271.87 15.8350 911.20 9.7492 1274.44 6.9325 912.08 9.7522 1274.54 6.9325 923.98 0.0000 1291.59 6. 9641 926.50 7.1284 1298.22 0.0000 929 .11 11. 5940 1312 .11 0.0000 937.49 11.6277 1332.49 9.0500 944.13 0.0000 1362.66 0.0000 946.00 14.3530 1365.19 5. 0696 949.00 10.7758 1368.63 0.0000 667. 71 0.0000 1384.29 4.0752 962. 31 16.2367 1408. 01 8.1982 964.08 10.1090 1457.56 0.0000 966 .17 17.3420 1460.82 10.3796 911.20 22.6021 1489.16 4.1797 968.97 22.6021 1505.03 9.4389 983.53 0.0000 1584.12 9.6103 984.45 0.0000 1596. 21 0.0000 Page 4410of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:47:05.68 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM02.CNF;493 Background date : Z-OCT-2016 11:00:01. Sample date 14-DEC-2015 13:25:00 Acquisition date : 3-0CT-2016 05:44:14. Sample ID G405235064 Sample quantity 1.74637E+02 GRAM Detector name : GAM02 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.40 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 3 3 3 0 0 2 2 0 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4411of5809 Energy 63.31* 69.84* 74.62* 77.01 84.14* 87.30 89.95 92.51* 128.68 185.97* 209.88 238.55* 241.65 269.89 276.36 294.95 299.94 315.18 338.30* 351.90* 403.01 438.14 511. 01* 528.15 583.31* 597.29* 609.23* 726.96 793.58 835.02 838.66 859.44* 911. 40* 953.87 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 47 31 111 151 56 57 72 97 33 105 47 398 114 26 25 168 61 13 70 290 12 14 34 18 121 10 204 56 39 18 12 20 81 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 136 203 182 160 149 159 100 159 132 145 118 75 92 99 108 93 42 55 89 62 51 29 55 30 31 28 26 26 12 9 8 24 17 13 1. 09 1. 45 1. 33 1. 47 1. 31 1.13 1. 08 1. 37 0.62 1. 44 0.87 1. 44 1. 65 1. 25 3.45 1. 20 2.83 2.17 1. 01 1. 33 1.34 1. 83 1. 73 3.38 1. 36 1. 89 1. 71 1.16 4.48 1. 57 0.57 0.96 1. 69 2.61 126.12 139.18 148.73 153.51 167.76 174.06 179.37 184.48 256.75 371.24 419.00 476.30 482.49 538.93 551.85 589.00 598.97 629.42 675.63 702.80 804.94 875.14 1020.76 1055.03 1165.26 1193.20 1217.06 1452.34 1585.49 1668.29 1675.58 1717.11 1820.94 1905.84 123 135 135 135 165 172 177 177 252 367 414 469 469 536 547 582 595 624 670 696 799 871 1014 1049 1157 1185 1212 1446 1579 1665 1672 1710 1814 1900 8 1. 30E-02 48. 5 22 8.52E-03 85.4 1.69E+OO 22 3.09E-02 24.2 22 4.19E-02 16.5 7 1. 55E-02 39. 7 6 1.58E-02 37.3 13 2.0lE-02 21.1 3.86E+OO 13 2.69E-02 27.9 8 9. llE-03 63. 2 12 2.91E-02 26.4 10 1.29E-02 46.3 19 1.lOE-01 6.5 1.64E+OO 19 3.18E-02 18.9 8 7.13E-03 70.2 11 6.97E-03 82.4 13 4.67E-02 14.2 8 1. 69E-02 22. 5 8 3. 63E-03101. 4 12 1.95E-02 29.9 15 8.07E-02 8.5 10 3.40E-03112.0 8 4.00E-03 69.1 13 9.44E-03 56.1 11 4.88E-03 65.2 16 3.36E-02 14.1 10 2.84E-03107.0 12 5.67E-02 8.8 12 1.55E-02 23.0 12 1.08E-02 23.9 8 5.06E-03 36.0 8 3.33E-03 50.0 14 5.45E-03 58.9 15 2.24E-02 16.6 12 3.94E-03 56.0 Peak Search Report (continued) Page : 2 Sample ID : G405235064 Acquisition date 3-0CT-2016 05:44:14 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969. 35* 39 32 1. 51 1936.78 1929 14 1. 09E-02 35.9 36 0 1003.26 33 9 1. 70 2004.55 1997 18 9.17E-03 27.5 37 o. 1058.18 12 8 1. 80 2114.32 2UO 9 3.35E-03 52.6 38 0 1074.10 17 13 3.21 2146.13 2139 14 4.76E-03 51.9 39 0 1087.17 8 13 0.74 2172.26 2163 11 2.12E-03100.3 40 0 1119.91* 64 10 2.42 2237.70 2230 14 1.78E-02 17.0 41 0 1125. 22 18 7 2.73 2248.31 2244 10 5.00E-03 36.7 42 0 1232.75 9 14 0.90 2463.23 2457 10 2.49E-03 86.8 43 0 1334.41 9 7 3.85 2666.45 2661 12 2.60E-03 62.2 44 0 1379.13 12 17 2. 96 2755.82 2748 14 3.32E-03 79.5 45 0 1460.70* 341 11 1. 94 2918.88 2911 15 9.47E-02 5.9 46 0 1589.05 9 6 1. 46 3175.44 3166 11 2.43E-03 62.8 47 0 1764.11* 36 0 2.29 3525.39 3518 13 9.98E-03 18.8 48 0 1847.41 11 0 1. 24 3691. 91 3687 9 3.06E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 4412 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:47:08 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl 14-DEC-2015 13:25:00 G405235064 SOLID GAMMA2 0 01:00:00.00 1. 50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry : Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 05:44:14 174.64 GRAM CAN 0 01:00:00.40 10.00 0.00 % Peak Energy 0.0% Interfering Interfered Nuclide Page 4413 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Nuclide RA-224 SN-126 SN-126 CD-109 TH-229 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 88.'47 74.66 74.82 74.82 351. 06 Nuclide Line Activity Report Page : 2 Sample ID : G405235064 Acquisition date 3-0CT-2016 05:44:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.059E;+OO 1. 272E+Ol 1. 272E+Ol 11. 85 OK MN-54 834.85 99.98* 1.673E+OO 4.977E-02 9.556E-02 71. 97 OK CD-109 88.03 3.70* 4.852E+OO 8.019E-01 1.247E+OO 182.02 OK SN-126 64.28 9.60 2.482E+OO 1.218E+OO l.218E+OO 97.07 OK 86.94 8.90 4.852E+OO 3.334E-01 3.334E-01 182.02 OK 87.57 37.00* 4.852E+OO 8.019E-02 8.019E-02 182.02 OK TL-208 277.37 6.60 4.186E+OO 4.795E-01 4.795E-01 164.82 OK 583.19 85.00* 2.233E+OO 3.057E-01 3.057E-01 28.18 OK 860.56 12.50 1.635E+OO 4.371E-01 4. 371E-01 11 7. 87 OK BI-211 72.87 1. 23 3.574E+OO Line Not Found Absent 351.06 12.92* 3.417E+OO 5.lOOE-02 5.lOOE-022158.25 OK PB-212 74.82 10.28 3.755E+OO 1. 086E+OO 1.086E+OO 80.71 OK 77 .11 17.10 3. 991E+OO 1.347E+OO 1. 347E+OO 33.05 OK 238.63 43.60* 4.702E+OO 1. 042E+OO 1.042E+OO 13.04 OK 300.09 3.30 3.912E+00 2.461E+OO 2.461E+OO 44.99 OK BI-214 609.32 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 OK 1120.29 14.92 1.323E+OO 1.424E+OO 1.425E+OO 34.02 OK 1764.49 15.30 8.933E-01 1. 075E+OO 1. 075E+OO 37.62 OK PB-214 74.82 5.80 3.775E+OO Line Not Found <<INT Reject 77 .11 9.70 3.991E+OO 2.375E+OO 2.375E+00 33.05 OK 87.09 3.41 4.837E+OO Line Not Found <<INT Reject 242.00 7.25 4. 651E+OO Line Not Found <<INT Reject 295.22 18.42 3. 967E+OO 1.204E+OO 1.205E+OO 28.34 OK 351. 93 35.60* 3.416E+OO Line Not Found <<INT Reject RN-219 271.23 10.80 4.267E+OO 2.947E-01 2.947E-01 140.49 OK 401. 81 6.60* 3.043E+OO 3.069E-01 3.069E-01 224.08 OK RN-222 609.32 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 OK 1120.29 14.92 l.323E+00 1.424E+OO 1.425E+OO 34.02 OK 1764.49 15.30 8.933E-01 1.075E+OO 1. 075E+OO 37. 62 OK RA-224 240.99 4.10* 4.656E+OO 1.086E+OO 1. 08 6E+OO 125.05 OK RA-226 609.32 45.49* 2.155E+00 9.933E-01 9.937E-01 17.59 OK 1120.29 14.92 1.323E+OO l.424E+OO 1.425E+OO 34.02 OK 1764.49 15.30 8.933E-01 1. 075E+OO 1.075E+OO 37. 62 OK AC-228 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11. 27 3.533E+OO 9.078E-01 9.078E-01 59.76 OK 794.95 4.25 l.742E+00 2.423E+OO 2.423E+OO 47.83 OK 835.71 1. 61 1.673E+OO 3.090E+OO 3.090E+OO 71. 97 OK 911.20 25.80* 1.561E+OO 9.028E-01 9.028E-01 33.11 OK 968.97 15.80 l.486E+OO 7.497E-01 7.497E-01 71.73 OK RA-228 105.21 1.10 5.776E+00 Line Not Found Absent 338.32 11. 27 3.533E+OO 9.078E-01 9.078E-01 59.76 OK 794.95 4.25 1.742E+OO 2.423E+OO 2.423E+OO 47.83 OK 835.71 1. 61 1.673E+OO 3.090E+OO 3.090E+OO 71. 97 OK 911.20 25.80* 1.561E+OO 9.028E-01 9.028E-01 33.11 OK 968. 97 15.80 l.486E+OO 7.497E-01 7.497E-01 71. 73 OK TH-228 74.82 10.28 3.755E+OO 1. 086E+OO 1.086E+OO 80.71 OK 77 .11 17.10 3.991E+OO 1. 34 7E+OO 1.347E+OO 33.05 OK 238.63 43.60* 4.702E+OO 1.042E+OO 1.042E+OO 13. 04 OK 300.09 3.30 3.912E+00 2.461E+OO 2. 461E+OO 44.99 OK Page 4414of5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235064 Acquisition date 3-0CT-2016 05:44:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status TH-229 85.43 14.70 4.615E+OO 4. 966E-01 4. 967E-Ql 79.31 OK 88.47 24.00 4.852E+OO 1.236E-01 1.236E-01 182.02 OK 193.51 4.41* 5.427E+OO Line Not Found Absent 210.85 2.80 5.154E+OO 1.760E+OO 1.760E+OO 92. 62 OK TH-230 609.32 45.49* 2.155E+OO 9.933E-01 9.933E-01 17.59 OK 1120.29 14.92 1.323E+OO l.424E+OO 1.424E+OO 34.02 OK 1764.49 15.30 8.933E-01 1. 075E+OO l.075E+OO 37.62 OK PA-231 283.69 1. 70 4.097E+OO Line Not Found Absent 301.36 5.35* 3.912E+OO 1.518E+OO 1.518E+OO 44.99 OK TH-232 105.21 1.10 5.776E+OO Line Not Found Absent 338.32 11.27 3.533E+OO 9.078E-01 9.078E-01 59.76 OK 835. 71 1. 61 1. 673E+OO 3.090E+OO 3.090E+OO 71. 97 OK 911. 20 25.80* 1.561E+OO 9.028E-01 9.028E-01 33.11 OK 968.97 15.80 1. 486E+OO 7.497E-01 7.497E-01 71.73 OK TH-234 63.29 3.70* 2.482E+00 3.160E+OO 3.160E+OO 97.07 OK 92.59 4.23 5.192E+OO 2.639E+OO 2.639E+OO 55.72 OK U-234 609.32 45.49* 2.155E+OO 9.933E-01 9.933E-01 17.59 OK 1120.29 14.92 1.323E+OO l.424E+OO 1.424E+OO 34.02 OK 1764.49 15.30 8. 933E'.-01 1.075E+OO 1. 075E+OO 37.62 OK U-235 89.96 3.47 5.033E+OO 2.479E+00 2.479E+OO 42 .11 OK 93.35 5.60 5.192E+OO 1.994E+OO 1.994E+00 55. 72 OK 143.76 10. 96* 6.127E+OO Line Not Found Absent 163.33 5.08 5.908E+OO Line Not Found Absent 185.72 57.20 5.554E+OO 1.823E-01 l.823E-01 52.89 OK 205.31 5.01 5.230E+OO Line Not Found Absent U-238 63.29 3.70* 2.482E+OO 3.160E+OO 3.160E+OO 97.07 OK 92.59 4.23 5.192E+OO 2.639E+OO 2.639E+00 55.72 OK AM-243 43.53 5.90 2.878E-01 Line Not Found Absent 74.66 67.20* 3.755E+OO 1. 661E-01 l.661E-01 80. 71 OK CM-247 278.00 3.40 4.166E+OO Line Not Found Absent 287.50 2.00 4.052E+OO Line Not Found Absent 402.40 72. 00* 3.043E+OO 2. 813E-02 2.813E-02 224.08 OK ANH-511 511. 00 100.00* 2.490E+OO 6.665E-02 6.665E-02 112. 29 OK Flag: "*" = Keyline Page 4415 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:47:09.75 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l * *Acquisition date 3-0CT-2016 05:44:14 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:25:00 Analyst initials: MXRl * *Sample ID G405235064 Sample Quantity 1.7464E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1 . 96-sigma ) K-40 1. 272E+Ol 1.477E+OO MN-54 9.556E-02 6.740E-02 CD-109 1.247E+OO 2.224E+OO SN-126 8.019E-02 1.430E-01 TL-208 3.057E-01 8.443E-02 BI-211 5.lOOE-02 1.079E+00 PB-212 l.042E+00 1. 331E-01 BI-214 9.937E-01 1. 713E-01 PB-214 1.223E+OO 2.035E-01 RN-219 3.069E-01 6.739E-01 RN-222 9.937E-01 1.713E-01 RA-224 1.086E+OO 1. 331E+OO RA-22 6 9.937E-01 l.713E-01 AC-228 9.028E-01 2.929E-01 RA-228 9.028E-01 2.929E-01 TH-228 1.042E+OO l.331E-01 TH-229 1.250E-01 4. 421E-01 TH-230 9.933E-01 1. 713E-01 PA-231 1.518E+OO 6.692E-01 TH-232 9.028E-01 2.929E-01 TH-234 3.160E+OO 3.006E+OO U-234 9.933E-01 1. 713E-01 U-235 -7.491E-02 1.838E-01 U-238 3.160E+OO 3.006E+OO AM-243 1. 661E-01 *1. 314E-01 CM-247 2.813E-02 6.177E-02 ANH-511 6.665E-02 7.334E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4416of5809 Key-Line Activity (pCi/GRAM l.088E+Ol -1.702E-02 O.OOOE+OO K.L. Cnt Uncert ( 1 . 96-sigma ) 1.085E+Ol 4. OOlE-02 l.251E+41 MDA (pCi/GRAM 7.189E-01 1.149E-01 1. 967E+OO 1.508E-01 5.768E-02 3.163E-01 8.452E-02 1. 2 91E-01 3.143E-01 6.562E-01 1. 291E-01 9.062E-01 1. 291E-01 2.437E-01 2.437E-01 8.452E-02 9.032E-01 1.291E-01 7.117E-01 2.437E-01 2.481E+OO 1.291E-01 3.330E-01 2.481E+OO 9.466E-02 6.023E-02 5.493E-02 MDA (pCi/GRAM 2.334E+Ol 7.256E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -9.232E-03 2.320E-02 4.616E-02 NOT IDENT. SC-46 -1.475E-02 3.957E-01 7.508E-01 FAIL ABUN V-48 O.OOOE+OO 1.085E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.364E+02 O.OOOE+OO SHORT HLIF C0-56 -2.600E-01 3.995E-Ol 7.243E-01 NOT IDENT. MN-56 O.OOOE+OO l.518E+41 O.OOOE+OO SHORT HLIF C0-57 -6.523E-03 4.895E-02 9.082E-02 NOT IDENT. C0-58 3.314E-01 5.276E-Ol l.143E+OO NOT IDENT. FE-59 -1.219E+OO 6.200E+OO l.175E+Ol NOT IDENT. C0-60 2.207E-02 626E-02 7.555E-02 NOT IDENT. ZN-65 4.758E-02 l.785E-01 3.255E-01 NOT IDENT. GE-68 -1.153E+OO 2.337E+OO 3.562E+OO NOT IDENT. AS-73 -l.207E+Ol l .115E+Ol 2.043E+Ol NOT IDENT. AS-74 O.OOOE+OO 7.512E+03 O.OOOE+OO SHORT HLIF SE-75 -2.044E-01 1. 851E-01 3.319E-01 NOT IDENT. BR-77 O.OOOE+OO 3.984E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.435E+02 O.OOOE+OO SHORT HLIF RB-83 -1. 391E-01 5.710E-01 1.064E+OO FAIL ABUN KR-85 6.033E+OO 7.159E+OO 1.380E+Ol NOT IDENT. SR-85 5.946E-01 7.088E-01 1.366E+OO NOT IDENT. RB-86 O.OOOE+OO 2.096E+04 O.OOOE+OO SHORT HLIF -9.246E-02 1. 747E-01 3.255E-01 NOT IDENT. Y-91 -9.496E+Ol 5.123E+02 9. 572E+02 NOT IDENT. NB-94 3.664E-03 2.747E-02 5.653E-02 NOT IDENT. NB-95 -8.729E-Ol 8.362E-01 1.457E+OO NOT IDENT. NB-95M 2.955E-01 2.090E+OO 3.799E+OO NOT IDENT. ZR-95 8.121E-01 1. 2 61E+OO 2.744E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO l.404E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.338E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.122E+41 O.OOOE+OO SHORT HLIF RH-101 5.339E-02 6. 611E-02 5.970E-02 FAIL ABUN RH-102 4.409E-02 5.775E-02 l.210E-01 NOT IDENT. RU-103 3.718E+OO 4.577E+OO 9.788E+OO FAIL ABUN RH-106 -4.159E-01 5.380E-01 9.006E-01 NOT IDENT. RU-106 -4.159E-01 5.380E-01 9.006E-01 NOT IDENT. AG-108M 5.923E-04 2. 712E-02 4.742E-02 NOT IDENT. AG-llOM 8.109E-02 9.835E-02 2.165E-01 NOT IDENT. SN-113 -l.032E-01 2.043E-01 3.756E-01 NOT IDENT. CD-115 O.OOOE+OO 8. 051E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 6.476E+04 O.OOOE+OO SHORT HLIF TE-123M 4.731E-02 l.162E-01 2.425E-01 NOT IDENT. SB-124 -2.392E-01 l.213E+OO 2. 681E+OO NOT IDENT. SB-125 -3.662E-02 9.281E-02 1. 719E-01 NOT IDENT. TE-125M -2.925E+02 2.589E+02 4.455E+02 NOT IDENT. I-126 O.OOOE+OO 6.235E+05 O.OOOE+OO SHORT HLIF SB-126 0.000E+OO 7.780E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.450E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.725E+09 0.000E+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.878E+25 O.OOOE+OO SHORT HLIF BA-133 -l.518E-02 4.015E-02 6.663E-02 FAIL ABUN I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 4.298E-02 5.356E-02 1.068E-01 NOT IDENT. CS-135 1.528E-01 1.562E-01 3.015E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2. 031E+05 O.OOOE+OO SHORT HLIF BA-137M -3.502E-03 3.806E-02 7.222E-02 NOT IDENT. CS-137 -3.700E-03 4. 021E-02 7.629E-02 NOT IDENT. CE-139 -4.424E-03 1.005E-01 2.034E-01 NOT IDENT. BA-140 O.OOOE+OO 9. 511E+05 0.000E+OO SHORT HLIF LA-140 0.000E+OO 2. 471E+05 O.OOOE+OO SHORT HLIF CE-141 7.282E-01 2.150E+Ol 3.986E+Ol NOT IDENT. CE-143 0.000E+OO 5.038E+40 0.000E+OO SHORT HLIF CE-144 -1. 791E-01 3.233E-01 5. 761E-01 NOT IDENT. PM-144 -1.047E-02 4.936E-02 9.708E-02' NOT IDENT. PR-144 -9.336E-01 4.269E+OO 8.391E+OO NOT IDENT. PM-146 l .112E-02 4.142E-02 8.249E-02 NOT IDENT. ND-147 0.000E+OO 2.362E+07 O.OOOE+OO SHORT HLIF PM-147 6.477E+02 8.134E+02 1.625E+03 NOT IDENT. PM-149 O.OOOE+OO 6.019E+39 O.OOOE+OO SHORT HLIF EU-150 4.356E-03 2.689E-02 4.795E-02 FAIL ABUN EU-152 2.032E-02 8.833E-02 l.763E-01 FAIL ABUN GD-153 3.802E-02 1. 813E-01 3.527E-01 FAIL ABUN EU-154 -3. 965E-02 9.886E-02 1.803E-01 FAIL ABUN EU-155 -7.531E-03 l .115E-01 2.103E-01 FAIL ABUN TB-160 6.434E-01 1.659E+OO 3.503E+OO FAIL ABUN H0-166M 4.141E-02 5.548E-02 l.204E-01 NOT IDENT. Page 4417 of 5809 TM-171 -3.264E+OO 2.766E+Ol 5.478E+Ol NOT IDENT. HF-172 -3.543E-02 2.395E-01 4.074E-01 FAIL ABUN LU-172 4.526E-02 7.501E-02 l.603E-01 FAIL ABUN LU-176 3.419E-03 2.244E-02 4'.478E-02 FAIL ABUN HF-181 1.829E+OO 3. 811E+OO 7.745E+OO NOT IDENT. TA-182 -1.155E-01 8.680E-01 1.641E+OO FAIL ABUN RE-183 -1. 8 69E+OO 3.170E+OO 6.016E+OO NOT IDENT. RE-184 2.810E+Ol 2.895E+Ol 6.354E+Ol NOT IDENT. W-188 -2.330E+Ol l.129E+02 1.943E+02 FAIL ABUN
  • IR-192 3.450E-01 6.857E-01 7.965E-01 FAIL ABUN HG-203 -6.00SE-01 2.439E+OO 4.185E+OO FAIL ABUN BI-207 -2.806E-02 4.443E-02 7.019E-02 FAIL ABUN PB-210 l.929E+OO 5.088E+OO 1.041E+Ol NOT IDENT. PB-211 5.414E-02 6.578E-01 l.161E+00 NOT IDENT. BI-212 O.OOOE+OO 9.352E-01 1.426E+OO FAIL ABUN RA-223 -1.002E-01 5.604E-01 1.079E+00 FAIL ABUN AC-227 -3.852E-02 2.002E-01 3.924E-01 FAIL ABUN TH-227 -3.852E-02 2.002E-01 3.924E-01 FAIL ABUN TH-231 -l.002E-01 5.604E-01 1. 079E+OO FAIL ABUN PA-233 -l.392E-02 5.856E-02 1.013E-01 FAIL ABUN PA-234 7.504E-02 2.552E-01 5.316E-01 NOT IDENT. PA-234M -9.695E-02 4.935E+OO 9.043E+OO NOT IDENT. NP-237 -1.392E-02 5.856E-02 l.013E-01 FAIL ABUN NP-238 O.OOOE+OO 6.697E+40 O.OOOE+OO SHORT HLIF NP-239 -9.472E-02 2.333E-01 4.260E-01 FAIL ABUN PU-239 4.859E+02 6. 018E+02 6.403E+02 FAIL ABUN AM-241 9.787E-02 1.635E-01 3.158E-01 NOT IDENT. CM-243 -2.158E-02 9.944E-02 1.860E-01 FAIL ABUN BK-247 -8.514E-02 6.822E-02 1.207E-01 FAIL ABUN CF-249 3.085E-02 3.463E-02 7.356E-02 NOT IDENT. CF-251 -5.730E-03 l.044E-01 2.106E-01 NOT IDENT. Page 4418of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:47:06.52 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 334 10.66* 1.059E+OO 1.272E+Ol 1.272E+Ol 11. 85 MN-54 834.85 19 99.98* 1.673E+OO 4.977E-02 9.556E-02 71. 97 CD-109 88.03 80 3.70* 4.852E+OO 1.912E+OO 2.972E+OO 74.55 SN-126 64.28 68 9.60 2.482E+OO 1.218E+OO 1.218E+OO 97.07 86.94 80 8.90 4.852E+OO 7.949E-01 7.949E-01 74.55 87.57 80 37.00* 4.852E+OO l.912E-01 1.912E-01 74.55 TL-208 277.37 31 6.60 4.186E+OO 4.795E-01 4.795E-01 164.82 583.19 135 85.00* 2.233E+OO 3.057E-01 3.057E-01 28.18 860.56 21 12.50 1.635E+OO 4. 371E-01 4. 371E-01 117. 87 BI-211 72. 87 ------1. 23 3.574E+OO ------Line Not Found ------351.06 346 12.92* 3.417E+OO 3.370E+OO 3.370E+OO 16.97 PB-212 74.82 158 10.28 3.755E+OO 1.765E+OO 1.765E+OO 48.42 77 .11 214 17.10 3. 991E+OO 1.347E+OO 1.347E+OO 33.05 238.63 497 43.60* 4.702E+OO 1.042E+OO 1.042E+OO 13. 04 300.09 74 3.30 3.912E+OO 2.461E+OO 2.461E+OO 44.99 BI-214 609.32 226 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 1120.29 65 14.92 1.323E+OO 1.424E+OO l.425E+OO 34.02 1764.49 34 15.30 8.933E-01 1.075E+OO 1. 075E+OO 37.62 PB-214 74.82 158 5.80 3.755E+OO 3.128E+OO 3 .130E+OO 48.42 77 .11 214 9.70 3.991E+OO 2.375E+OO 2.375E+00 33.05 87.09 80 3.41 4.852E+OO 2.075E+OO 2.075E+OO 74.55 242.00 143 7.25 4.656E+OO 1.819E+OO 1.819E+OO 37.83 295.22 205 18.42 3. 967E+OO 1.204E+OO 1.205E+OO 28.34 351.93 346 35.60* 3.417E+OO 1.223E+OO 1.223E+OO 16.97 RN-219 271.23 32 10.80 4.267E+OO 2.947E-01 2.947E-01 140.49 401.81 14 6.60* 3.043E+OO 3.069E-01 3.069E-01 224.08 RN-222 609.32 226 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 1120.29 65 14.92 l.323E+OO 1.424E+OO l.425E+OO 34.02 1764.49 34 15.30 8.933E-01 1.075E+OO 1.075E+OO 37.62 RA-2*24 240.99 143 4.10* 4.656E+OO 3.216E+OO 3.216E+OO 37.83 RA-226 609.32 226 45.49* 2.155E+OO 9.933E-01 9.937E-01 17.59 1120.29 65 14.92 1.323E+OO 1.424E+OO 1.425E+OO 34.02 1764.49 34 15.30 8.933E-01 1.075E+OO 11* 075E+OO 37.62 AC-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 84 11. 27 3.533E+OO 9.078E-01 9.078E-01 59.76 794.95 42 4.25 1.742E+OO 2.423E+OO 2.423E+OO 47.83 835.71 19 1. 61 1.673E+OO 3.090E+OO 3.090E+OO 71. 97 911.20 85 25.80* 1.561E+OO 9.028E-01 9.028E-01 33.11 968. 97 41 15.80 l.486E+OO 7.497E-01 7.497E-01 71. 73 RA-228 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 84 11.27 3.533E+OO 9.078E-01 9.078E-01 59.76 794.95 42 4.25 1.742E+OO 2.423E+OO 2.423E+OO 47.83 835.71 19 1. 61 1.673E+OO 3.090E+OO 3.090E+OO 71. 97 911. 20 85 25.80* 1.561E+OO 9.028E-01 9.028E-01 33 .11 968.97 41 15.80 1.486E+OO 7.497E-01 7.497E-01 71. 73 TH-228 74.82 158 10.28 3.755E+OO 1. 765E+OO 1. 765E+OO 48.42 77 .11 214 17.10 3.991E+OO 1.347E+OO 1.347E+OO 33.05 Page 4419of5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235064 Acquisition date 3-0CT-2016 05:44:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 4 97
  • 43.60* 4.702E+OO l.042E+OO 1. 042E+OO
  • 13.04 300.09 74 3.30 3.912E+OO 2.461E+OO 2.461E+OO 44.99 TH-229 85.43 78 14.70 4.615E+OO 4. 966E-01 4. 967E-01 79.31 88.47 80 24.00 4.852E+OO 2.948E-01 2.948E-01 74.55 193.51 ------4.41* 5.427E+OO ------Line Not Found ------210.85 59 2.80 5.154E+OO 1.760E+OO 1. 760E+OO 92. 62 TH-230 609.32 226 45.49* 2.155E+OO 9.933E-01 9.933E-01 17.59 1120.29 65 14.92 1.323E+OO 1.424E+OO l.424E+OO 34.02 1764.49 34 15.30 8.933E-01 1.075E+OO 1. 07 5E+OO 37.62 PA-231 283.69 ------1. 70 4.097E+OO ------Line Not Found ------301.36 74 5.35* 3.912E+OO 1.518E+OO 1.518E+OO 44.99 TH-232 105.21 ------1.10 5.776E+OO ------Line Not Found ------338.32 84 11. 27 3.533E+OO 9.078E-01 9.078E-01 59.76 835. 71 19 1. 61 l.673E+00 3.090E+OO 3.090E+OO 71. 97 911.20 85 25.80* 1.561E+OO 9.028E-01 9.028E-01 33 .11 968. 97 41 15.80 1.486E+OO 7.497E-01 7.497E-01 71. 73 TH-234 63.29 68 3.70* 2.482E+OO 3.160E+OO 3.160E+OO 97.07 92.59 135 4.23 5.192E+OO 2.639E+OO 2.639E+OO 55. 72 U-234 609.32 226 45.49* 2.155E+OO 9.933E-01 9.933E-01 17.59 1120.29 65 14.92 1.323E+OO 1.424E+OO 1.424E+OO 34.02 1764.49 34 15.30 8.933E-01 1.075E+OO 1.075E+OO 37.62 U-235 89. 96 101 3.47 5.033E+OO 2.479E+00 2.479E+OO 42 .11 93.35 135 5.60 5.192E+OO 1.994E+OO 1.994E+OO 55.72 143.76 ------10.96* 6.127E+OO ------Line Not Found ------163.33 ------5.08 5.908E+OO ------Line Not Found ------185.72 135 57.20 5.554E+00 1.823E-01 1.823E-01 52.89 205.31 ------5.01 5.230E+00 ------Line Not Found ------U-238 63.29 68 3.70* 2.482E+OO 3.160E+OO 3.160E+OO 97.07 92.59 135 4.23 5.192E+OO 2.639E+00 2.639E+OO 55. 72 AM-243 43.53 ------5.90 2.878E-01 ------Line Not Found ------74.66 158 67.20* 3.755E+OO 2.700E-01 2.700E-01 48.42 CM-247 278.00 ------3.40 4.166E+OO ------Line Not Found ------287.50 ------2.00 4.052E+OO ------Line Not Found ------402.40 14 72.00* 3.043E+OO 2. 813E-02 2. 813E-02 224.08 ANH-511 511. 00 39 100.00* 2.490E+OO 6.665E-02 6.665E-02 112. 29 Flag: "*" Key line Page 4420 of 5809 Summary of Nuclide Activity Sample ID : G405235064 Acquisition date Page : 3 3-0CT-2016 05:44:14 Total number of lines in spectrum 48 Number of unidentified lines 9 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 MN-54 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234. U-235 U-238 AM-243 CM-247 ANH-511 Hlife 1.25E+09Y 312.05D 461.40D 2.30E+05Y 1. 41E+l0Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 7.04E+08Y 1600. OOY 1.41E+10Y 1600. OOY 1.41E+10Y 1. 41E+10Y 1. 41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.56E+07Y l.00E+09Y Decay 1. 00 1. 92 1. 55 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 272E+Ol 4.977E-02 1. 912E+OO 1.912E-01 3.057E-01 3.370E+OO l.042E+OO 9.933E-01 1.223E+OO 3.069E-01 9.933E-01 3.216E+OO 9.933E-01 9.028E-01 9.028E-01 *1. 042E+OO 2.948E-01 9.933E-01 1.518E+OO 9.028E-01 3.160E+OO 9.933E-01 1.823E-01 3.160E+OO 2.700E-01 2. 813E-02 6.665E-02 4.173E+Ol 4.173E+Ol Decay Corr pCi/GRAM l.272E+Ol 9.556E-02 2.972E+OO 1.912E-Ol 3.057E-01 3.370E+OO 1.042E+OO 9.937E-01 1.223E+OO 3.069E-01 9.937E-01 3.216E+OO 9.937E-01 9.028E-01 9.028E-01 1.042E+OO 2.948E-01 9.933E-01 1.518E+OO 9.028E-01 3.160E+OO 9.933E-01 1.823E-01 3.160E+OO 2.700E-01 2.813E-02 6.665E-02 4.284E+Ol 4.284E+Ol 81.25%
  • Decay Corr 2-Sigma Error 0.151E+Ol 6.877E-02 2.216E+00 l.425E-01 0.862E-01 0.572E+00 0.136E+OO l.748E-01 0.208E+OO 6.876E-01 1. 748E-01 1.216E+OO 1. 748E-01 2.989E-01 2.989E-01 0.136E+OO 2.198E-01 1.748E-01 0.683E+OO 2.989E-01 3.068E+OO 1. 748E-01 0.964E-01 3.068E+OO 1.308E-01 6.303E-02 7.484E-02 "M" Manually accepted 2-Sigma %Error 11. 85 71.97 74.55 74.55 28.18 16.97 13. 04 17.59 16.97 224.08 17.59 37.83 17.59 33.11 33.11 13. 0'4 74.55 17.59 44.99 33 .11 97.07 17.59 52.89 97.07 48.42 224.08 112. 29 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4421of5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235064 Acquisition date : 3-0CT-2016 05:44:14 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 3 69.84 44 291 1. 45 139.18 135 22 8.52E-03 **** 3.25E+OO T 0 128.68 44 177 0.62 256.75 252 8 9. llE-03 **** 6.17E+00 T 0 315.18 16 66 2.17 629.42 624 8 3.63E-03 **** 3.75E+OO T 0 17 33 1. 83 875.14 871 8 4.IJOE-03 **** 2.83E+OO T 0 528.15 20 34 3.38 1055.03 1049 11 4.88E-03 **** 2.42E+OO T 0 597.29 11 31 1. 89 1193.20 1185 10 2.84E-03 **** 2.19E+OO T 0 726.96 60 29 1.16 1452.34 1446 12 1.55E-02 45.9 1.87E+OO T 0 838.66 13 8 0.57 1675.58 1672 8 3.33E-03 **** 1.67E+OO 0 953.87 15 13 2.61 1905. 84 1900 12 3.94E-03 **** l.51E+OO T 0 1003.26 34 9 1. 70 2004.55 1997 18 9.17E-03 55.0 1. 45E+00 T 0 1058.18 12 8 1. 80 2114. 32 2110 9 3.35E-03 **** 1.39E+OO 0 1074.10 18 13 3.21 2146.13 2139 14 4.76E-03 **** 1. 37E+00 0 1087.17 8 14 0.74 2172.26 2163 11 2.12E-03 **** l.36E+00 T 0 1125. 22 18 7 2.73 2248.31 2244 10 5.00E-03 73.5 1.32E+OO 0 1232.75 9 14 0.90 2463.23 2457 10 2.49E-03 **** 1.22E+OO 0 1334.41 9 7 3.85 2666.45 2661 12 2.60E-03 *'r** 1.14E+OO 0 1379.13 12 17 2. 96 2755.82 2748 14 3.32E-03 **** 1. llE+OO 0 1589.05 8 6 1. 46 3175.44 3166 11 2.43E-03 **** 9.83E-01 0 1847.41 10 0 1.24 3691. 91 3687 9 3.06E-03 60.3 8.55E-01 Flags: "T" = Tentatively associated Page 4422 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:47:25.30 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l *
  • Acquisition date 3-0CT-2016 05:44:14 Sensitivity 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:25:00 Nuclide Library : SOLID *
  • Sample ID G405235064 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity : 1.7464E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 MN-54 CD-109 SN-126 TL-208 BI-211 PB-212 BI-214 PB-214 RN-219 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232r TH-234 U-234 U-235 U-238 AM-24'3 CM-247 ANH-511 Le (pCi/GRAM 3.073E-01 5.055E-02 9.283E-01 7.183E-02 2.564E-02 1.442E-01 3.922E-02 5.837E-02 1.522E-01 2.976E-01 5.837E-02 4.205E-01 5.837E-02 1.070E-01 1.070E-01 3.922E-02 4.254E-01 5.835E-02 3.261E-01 1. 070E-01 1.170E+OO 5.835E-02 1.571E-01 1.170E+OO 4.477E-02 2.732E-02 2.502E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4423 of 5809 Le (pCi/GRAM 1.065E+Ol 3. OllE-02 O.OOOE+OO 1.635E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147. PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 Page 4424 of 5809 3.327E-01 O.OOOE+OO O.OOOE+OO 3 .115E-01 O.OOOE+OO 4.284E-02 5.091E-01 5 .114E+OO 3.204E-02 1.424E-01 1.494E+OO 9.587E+OO O.OOOE+OO 1.526E-01 O.OOOE+OO O.OOOE+OO 4.735E-01 6.304E+OO 6.238E-01 O.OOOE+OO 1.165E-01 4.193E+02 2. 511E-02 6.479E-01 1. 772E+OO 1.225E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.805E-02 5.453E-02 4.424E+OO 4.005E-01 4.005E-01 2.133E-02 9.663E-02 1.700E-01 O.OOOE+OO O.OOOE+OO 1.143E-01 9.497E-01 7.725E-02 2.088E+02 0. OOOE+.00 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.022E-02 O.OOOE+OO 4.809E-02 1. 417E-01 O.OOOE+OO O.OOOE+OO 3.271E-02 3.456E-02 9.579E-02 O.OOOE+OO O.OOOE+OO 1.881E+01 O.OOOE+OO 2.691E-01 4.304E-02 3.719E+OO 3.746E-02 O.OOOE+OO 7.676E+02 O.OOOE+OO 2.215E-02 8.120E-02 1.669E-01 7.497E-02 9.927E-02 1.544E+OO 5.435E-02 2.577E+Ol FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT I DENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 BI-212 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 4425 of 5809 1.914E-01 7.073E-02 2.067E-02 3.519E+00 7.150E-01 2.817E+OO 2.863E+Ol 9.006E+Ol 3.667E-01 1.948E+OO 2.921E-02 4.908E+OO 5.267E-01 6.646E-01 4.971E-01 1.814E-01 1.814E-01 4.971E-01 4.642E-02 2.329E-01 4.031E+OO 4.642E-02 O.OOOE+OO l.997E-01 3.038E+02 1. 489E-01 8.753E-02 5.555E-02 3.381E-02 9.890E-02 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:47:31.94 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235064.CNF;l *
  • Acquisition date 3-0CT-2016 05:44:14 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.40 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:25:00 Nuclide Library : SOLID *
  • Sample ID G405235064 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity 1.7464E+02 GRAM *
  • Quantity Err(%) 1.1452E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.272E+Ol 1.619E+OO l.619E+00 MN-54 9.556E-02 6.752E-02 6.752E-02 CD-109 1. 24 7E+OO 2.236E+OO 2.236E+OO SN-126 8.019E-02 l.438E-01 l.438E-01 TL-208 3.057E-01 8.543E-02 8.543E-02 BI-211 5.lOOE-02 1.098E+OO 1.098E+OO PB-212 1.042E+OO l.442E-01 1.442E-01 BI-214 9.937E-01 l.766E-01 l.766E-01 PB-214 1.223E+OO 2.098E-01 2.098E-01 RN-219 3.069E-01 6.750E-01 6.750E-01 RN-222 9.937E-01 1.766E-01 1. 766E-01 RA-224 1.086E+OO 1.339E+OO 1.339E+OO RA-226 9.937E-01 1.766E-01 1. 7 66E-01 AC-228 9.028E-01 2. 965E-01 2.965E-01 RA-228 9.028E-01 2. 965E-01 2. 965E-01 TH-228 1.042E+OO 1.442E-01 1.442E-01 TH-229 1.250E-01 4.422E-01 4.422E-01 TH-230 9.933E-01 l.765E-01 1. 7 65E-01 PA-231 1.518E+OO 7.436E-01 7.436E-01 TH-232 9.028E-01 2. 965E-01 2. 965E-01 TH-234 3.160E+OO 3.087E+OO 3.087E+00 U-234 9.933E-01 1. 765E-01 1. 765E-01 U-235 -7.491E-02 1.839E-01 1.839E-01 U-238 3.160E+00 3.087E+00 3.087E+OO AM-243 1.661E-01 1.324E-01 1.324E-01 CM-247 2.813E-02 6.195E-02 6.195E-02 ANH-511 6.665E-02 7.339E-02 7.339E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 1.088E+Ol 1.086E+Ol 1.192E+Ol NOT IDENT. NA-22 -l.702E-02 4.00lE-02 4.074E-02 NOT IDENT. NA-24 l.OOOE+41 1.322E+41 O.OOOE+OO SHORT HLIF Page 4426 of 5809 AL-26 -9.232E-03 2. 321E-02 2.358E-02 NOT IDENT. SC-46 -1. 475E-02 3.957E-01 3.957E-01 FAIL ABUN V-48 4.653E+03 1.085E+04 1.105E+04 SHORT HLIF CR-51 2.221E+02 3.366E+02 3.512E+02 SHORT HLIF C0-56 -2.600E-01 3. 996E-01 4.165E-Ol NOT IDENT. MN-56 -l.OOOE+41 l.518E+41 O.OOOE+OO SHORT HLIF C0-57 -6.523E-03 4.895E-02 4.904E-02 NOT IDENT. C0-58 3.314E-01 5.278E-01 5.486E-01 NOT IDENT. FE-59 -l.219E+OO 6.201E+OO 6.225E+OO NOT IDENT. C.0-60 2.207E-02 3.627E-02
  • 3.761E-02 NOT IDENT. ZN-65 4.758E-02 l.785E-01 1. 798E-01 NOT IDENT. GE-68 -1.153E+OO 2.337E+OO 2.394E+OO NOT IDENT. AS-73 -l.207E+Ol 1.142E+Ol 1. 265E+Ol NOT IDENT. AS-74 3.580E+03 7.517E+03 7.689E+03 SHORT HLIF SE-75 -2.044E-01 1.853E-01 2.070E-01 NOT IDENT. BR-77 3 .119E+37 2.644E+38 0.000E+OO SHORT HLIF SR-82 -2.871E+02 5.437E+02 5.588E+02 SHORT HLIF RB-83 -l.391E-01 5.713E-01 5.748E-01 FAIL ABUN KR-85 6.033E+OO 7.163E+OO 7.662E+OO NOT IDENT. SR-85 5.946E-01 7.092E-01 7.581E-01 NOT IDENT. RB-86 -3.928E+03 2. 096E+04 2.103E+04 SHORT HLIF Y-88 -9.246E-02 1. 748E-01 1. 797E-01 NOT IDENT. Y-91 -9. 496E+Ol 5.123E+02 5 .141E+02 NOT IDENT. NB-94 3.664E-03 2.747E-02 2.752E-02 NOT IDENT. NB-95 -8. 729E-01 8. 371E-01 9.250E-01 NOT IDENT. NB-95M 2.955E-01 2.090E+OO 2.094E+OO NOT IDENT. ZR-95 8.121E-01 l.262E+OO 1.314E+OO NOT IDENT. NB-97 1.000E+41 2. 401E+41 O.OOOE+OO SHORT 'HLIF ZR-97 1.000E+41 1. 404E+41 O.OOOE+OO SHORT HLIF M0-99 1.398E+31 3.340E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.127E+41 O.OOOE+OO SHORT HLIF RH-101 5.339E-02 6.682E-02 7.102E-02 FAIL ABUN RH-102 4.409E-02 5.787E-02 6.118E-02 NOT IDENT. RU-103 3.718E+OO 4. 581E+OO 4.878E+OO FAIL ABUN RH-106 -4.159E-01 5.387E-01 5.704E-01 NOT IDENT. RU-106 -4.159E-01 5.387E-01 5.704E-01 NOT IDENT. AG-108M 5.923E-04 2. 712E-02 2. 712E-02 NOT IDENT. AG-llOM 8.109E-02 9.844E-02 1.050E-01 NOT IDENT. SN-113 -l.032E-01 2.044E-01 2. 096E-01 NOT IDENT. CD-115 6.303E+38 8.129E+38 O.OOOE+OO SHORT HLIF SN-117M 2. 618E+04 6.483E+04 6.590E+04 SHORT HLIF TE-123M 4.731E-02 l.162E-01 l.181E-01 NOT IDENT. SB-124 -2.392E-01 1.213E+OO 1.218E+OO NOT IDENT. SB-125 -3.662E-02 9.282E-02 9.428E-02 NOT IDENT. TE-125M -2.925E+02 2.594E+02 2.910E+02 NOT IDENT. I-126 3.144E+05 6.250E+05 6.408E+05 SHORT HLIF SB-126 1. 351E+05 7.784E+05 7.808E+05 SHORT HLIF SB-127 -4.343E+21 8.707E+21 O.OOOE+OO SHORT HLIF I-131 1. 720E+09 2.726E+09 2.834E+09 SHORT HLIF I-132 1.000E+41 l.827E+42 O.OOOE+OO SHORT HLIF TE-132 1.081E+26 1.078E+26 O.OOOE+OO SHORT HLIF BA-133 -1.518E-02 4.015E-02 4.073E-02 FAIL ABUN I-133 l.000E+41 3.479E+41 O.OOOE+OO SHORT HLIF CS-134 4.298E-02 5.360E-02 5.699E-02 NOT IDENT. CS-135 1. 528E-01 1.565E-01 1.710E-01 NOT IDENT. I-135 1.000E+41 7.010E+41 O.OOOE+OO SHORT HLIF CS-136 4.291E+04 2.032E+05 2.041E+05 SHORT HLIF BA-137M -3.502E-03 3.806E-02 3.810E-02 NOT IDENT. CS-137 -3.700E-03 4.021E-02 4.025E-02 NOT IDENT. CE-139 -4.424E-03 1.005E-01 l.005E-01 NOT IDENT. BA-140 5.977E+05 9.515E+05 9.889E+05 SHORT HLIF LA-140 -2.225E+04 2.471E+05 2.473E+05 SHORT HLIF CE-141 7.282E-01 2.150E+Ol 2.151E+Ol NOT IDENT. CE-143 1.000E+41 5.136E+40 O.OOOE+OO SHORT HLIF CE-144 -1.791E-01 3.235E-01 3.334E-01 NOT IDENT. PM-144 -L 047E-02 4.936E-02 4.959E-02 , NOT IDENT. PR-144 -9.336E-01 4.270E+OO 4.290E+OO NOT IDENT. PM-146 1.112E-02 4.143E-02 4.173E-02 NOT IDENT. ND-147 6.753E+06 2.362E+07 2.382E+07 SHORT HLIF PM-147 6.477E+02 8 .139E+02 8.647E+02 NOT IDENT. PM-149 -2.136E+39 6.037E+39 O.OOOE+OO SHORT HLIF EU-150 4.356E-03 2.689E-02 2. 696E-02 FAIL ABUN EU-152 2.032E-02 8.834E-02 8.881E-02 FAIL ABUN GD-153 3.802E-02 1.813E-01 1.821E-01 FAIL ABUN EU-154 -3.965E-02 9.887E-02 1.005E-01 FAIL ABUN EU-155 -7.531E-03 l .115E-01 1.116E-01 FAIL ABUN TB-160 6.434E-01 l.660E+OO l.685E+OO FAIL ABUN H0-166M 4.141E-02 5.553E-02 5.858E-02 NOT IDENT. Page 4427 of 5809 TM-171 -3.264E+OO 2.766E+Ol 2.770E+Ol NOT IDENT. HF-172 -3.543E-02 2. 396E-01 2.401E-01 FAIL ABUN LU-172 4.526E-02 7.515E-02 7.787E-02 FAIL ABUN LU-176 3.419E-03 2.244E-02 2.249E-02 FAIL ABUN HF-181 l.829E+OO 3.812E+OO 3.900E+OO NOT IDENT. TA-182 -l.155E-01 8.680E-01 8.696E-01 FAIL ABUN RE-183 -1.869E+OO 3.184E+OO 3.293E+OO NOT IDENT. RE-184 2.810E+Ol 2. 969E+Ol 3.228E+Ol NOT IDENT. W-188 -2.330E+Ol 1.130E+02 l.134E+02 FAIL ABUN IR-.192 3.450E-01 6.859E-01 033E-01 FAIL ABUN HG-203 -6.008E-01 2.440E+OO 2.455E+OO FAIL ABUN BI-207 -2.806E-02 4.444E-02 4.621E-02 FAIL ABUN PB-210 1.929E+00 5.091E+OO 5.165E+OO NOT IDENT. PB-211 5.414E-02 6.578E-01 6.583E-01 NOT IDENT. BI-212 2.079E+OO 9. 411E-01 1.328E+OO FAIL ABUN RA-223 -1.002E-01 5.604E-01 5.622E-01 FAIL ABUN AC-227 -3.852E-02 2.003E-01 2.0lOE-01 FAIL ABUN TH-227 -3.852E-02 2.003E-01 2.0lOE-01 FAIL ABUN TH-231 -1.002E-01 5.604E-01 5.622E-01 FAIL ABUN PA-233 -1.392E-02 5.857E-02 5.890E-02 FAIL ABUN PA-234 7.504E-02 2.692E-01 2. 713E-01 NOT IDENT. PA-234M -9.695E-02 4.935E+OO 4.935E+OO NOT IDENT. NP-237 -l.392E-02 5.857E-02 5.890E-02 FAIL ABUN NP-238 -1.062E+40 6.697E+40 O.OOOE+OO SHORT HLIF NP-239 -9.472E-02 2.335E-01 2.373E-01 FAIL ABUN PU-239 4.859E+02 6.022E+02 6.408E+02 FAIL ABUN AM-241 9.787E-02 1. 636E-01 l.695E-01 NOT IDENT. CM-243 -2.158E-02 9.946E-02 9.993E-02 FAIL ABUN BK-247 -8.514E-02 7.035E-02 8.014E-02 FAIL ABUN CF-249 3.085E-02 3.473E-02 3.741E-02 NOT IDENT. CF-251 -5.730E-03 l.044E-01 1.045E-01 NOT IDENT. Page 4428 of 5809
  • GEL Laboratories LLC *
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  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 85.3859 87.09 112.3177 136.47 82.6104 45.60 87.9392 87.57 134.9020 140.51 0.0000 46.54 74.8432 88.03 94. 5115 143.76 89.5613 49.72 0.0000 88.34 94.5660 144.24 93. 3011 51. 35 84.1319 88.47 94.5884 145.44 92.2199 51. 87 90.4867 89.96 100.8687 152.43 100.5022 52.39 87.4844 1093.63 100.9935 153.25 0.0000 52.97 109.5193 91.11 0.0000 323.87 72.1274 53.44 106.5184 92.59 101.3485 156.02 0.0000 54.07 76.3562 93.35 101.4862 158.56 0.0000 57.36 0.0000 94.56 66.7905 159.00 80.0664 57.53 97.0614 94.65 66.8012 162.33 82.9069 57.98 87.6618 94.67 66.8034 162.66 0.0000 59.27 80.5184 94.87 66.8267 163.33 89.7153 59.32 80.5279 97.43 86.9583 165.86 89.1485 59.54 74.9162 98.43 71.0617 176.31 85.9934 60. 96 79.4233 98.44 71. 0631 176.60 0.0000 61.17 92.2331 99.53 98.7551 177.52 80.9970 62.93 90.8300 100 .11 116. 0939 181.07 0.0000 63.29 90.9049 102.03 83.0286 181.52 87.3616 63.58 90. 9655 103.18 83.1879 184.41 76.0448 64.28 91.1106 103.37 91.3046 143.76 85.1909 66.73 75.4458 105.21 96.2189 193.51 80.7118 67.24 66.8986 105.31 96.2347 197.03 94.0836 125.81 87.8445 106.12 88.2357 198.01 54.9391 67.75 87.8575 106.47 84.8011 201.83 88.4325 69.67 100.8815 109.28 106.1907 203.43 80.6862 70.83 101.1320 111. 00 91. 2700 205.31 80.4041 72. 81 101.5556 111.76 0.0000 210.85 62.3028 72.87 101.5683 114. 06 83.4788 215.65 69.2648 74.66 101. 9465 116. 30 0.0000 222 .11 75.0697 74.82 101.9799 116.74 86.1857 227.09 71. 8408 74. 97 102. 0118 119.76 88.9532 227.38 67.3691 77 .11 102.4567 121.12 74.8731 228.16 0.0000 78.74 116. 4234 121.22 74.8841 228.18 53.9368 79.69 100.4014 121. 7 8 92.7910 116.74 53.9368 80.12 93.0978 122.06 96.4001 235.69 61.1115 80.19 0.0000 122.92 98.9057 235. 96 61.1272 80.57 95.3984 123.07 98.9279 238.63 55.3781 81. 00 103.6207 265.00 88.2798 238.98 0.0000 81. 07 103.6349 125.81 84.5663 240.99 55.4991 81.75 103.7717 127.23 76.7454 242.00 55.5506 83.79 99. 7155 127.91 87.6243 244.70 58.8835 84.00 99.7551 129.30 104.2351 252.40 0.0000 85.43 111. 9690 131.20 70.7498 252.80 55.1758 86.55 112.2047 133.02 95.5158 254.15 0.0000 86.79 112.2551 133.52 81. 0633 256.23 54.4212 86.94 112.2864 136.00 72.8439 260.90 0.0000 Page 4429 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 65.9717 355.39 0.0000 584.27 21. 5598 264.80 70.6269 356.01 38.8754 595.83 0.0000 265.00 70.6392 364.49 0.0000 427.87 13.7217 268.22 57.3197 366.42 0.0000 602.52 0.0000 269.46 74.1738 372.51 42.3384 604.72 10.3107 270.03 70.0089 .:n5.05 47.4590 607.14 18. 271.23 57.9333 377.52 50.5707 609.32 29.8499 273.65 0.0000 356.01 32.5000 610.33 29.8636 276.40 61.0010 388.16 28.5178 614.28 10.3561 277.37 61.0499 388.63 0.0000 618.01 21. 8999 277.60 61.0618 391.69 38.7909 620.36 19.6154 278.00 69.0692 264.66 24.6401 621. 93 33.4864 279.20 66.3161 401.81 31.8502 630.19 0.0000 279.54 57.8665 402.40 31.8615 631.29 17.3932 279.70 57.8740 404.85 30.8813 633.25 22.0507 280.46 48.0231 410.95 27.8992 634.78 0.0000 283.69 57.5921 413. 71 26.9119 635.95 18.5911 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 54.8364 423.72 0.0000 645.85 29.7593 285.90 0.0000 427.09 35.4810 657.76 22.8754 287.50 42.6178 427.87 32.3661 657,90 0.0000 290.67 58.3932 433.94 26.7202 661. 66 27.3208 293.27 0.0000 439.40 26.8069 664.57 0.0000 351. 93 38.5941 453.88 28.6243' 666.33 0.0000 295.96 38.6172 463.37 28.7803 666.50 0.0000 879.38 25.7981 468.07 28.8567 667.71 0.0000 299.98 41. 6096 473.00 0.0000 677.62 25.7325 300.09 41.6132 475.06 26.8239 685.70 0.0000 300 .13 41. 6140 476.78 20.4055 695.00 0.0000 301.36 40.2184 477.60 21.4893 696. 49 23.2531 302.85 37.3885 482.18 25.8525 696. 51 23.2531 256.23 48.3800 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 24.1556 306.78 45.1956 497.08 18.4609 697.49 21. 4731 308.46 47.1796 505.52 21. 2714 702.65 19.7253 311. 90 40.5465 507.63 0.0000 706.68 24.2487 316.51 47.9551 511. 00 35.0081 711. 68 18.8986 319.41 0.0000 514.00 23.0104 720. 70 0.0000 320.08 0.0000 514.00 23.0104 721. 93 0.0000 321.04 40.8276 520.40 25.2854 722.78 20.2487 323.87 49.6802 520.69 0.0000 722. 91 18.8037 325.23 39.9798 522.65 0.0000 723. 31 18.8068 328.76 0.0000 527.90 0.0000 724.19 13.0245 333.37 55.9134 528.26 26.4922 727.33 19.0178 333.97 45.6334 529.59 26.5107 733.00 15.5603 334.37 41. 2292 529.87 0.0000 735.93 19.0832 338.28 41. 3463 531.02 '0.0000 333.97 20.9132 338.32 41.3472 537.26 0.0000 739.50 0.0000 311. 90 42.8902 546.56 0.0000 747.24 20.0812 340.48 42.8902 552.55 35.7578 748.06 22.8264 340.55 0.0000 563.25 26.9600 752.31 26.5229 344.28 41.5232 569.33 20.2800 753.82 0.0000 345.93 46.0260 946.00 20.2815 756.73 15.5743 351.06 35.7620 569.70 16.9031 756.80 17.4072 351. 93 35.7832 583.19 21.5490 884.68 22.9675 Page 4430 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 32.1780 1274.44 14.3314 1620.50 7.4547 766.42 22.9897 1001.03 15.9473 1621. 92 6.5249 766.84 16.5547 1002.74 13. 9615 1678.03 0.0000 772.60 0.0000 1004.73 13.9701 1690.97 2.8361 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000
  • 1764.49 3 .1971 778.90 11. 0874 1028.54 0.0000 1063.66 2.7434 783.70 0.0000 1037.84 14 .1111 1771. 35 3.2013 785.37 16.6718 1038.76 0.0000 1791.20 0.0000 792.07 15.7850 631.29 12.1274 1808.65 3.8691 794.95 20.8216 1048.07 0.0000 1810.72 0.0000 795.86 16.3652 1049.04 7.0795 1836.06 4.8616 810.06 15.8903 1050.41 15.1767 810.29 14.0222 1063.66 14.8976 344.28 14.0231 1077.00 0.0000 810.76 14.9595 1077.34 14.6856 815.77 0.0000 1085.87 8.1787 1048.07 0.0000 1093.63 12.2959 832.01 27.1354 1099.45 17.4482 834.85 18.1090 1112.07 16.4805 835. 71 0.0000 1112. 84 14.8359 836.80 0.0000 1115. 54 13.1977 846.75 0.0000 1120.29 18.1715 846.77 19.8907 1120.55 18.1726 856.80 0.0000 1221.41 8.2617 860.56 14.2767 1129. 67 14.9063 871.09 12.4184 1131. 51 0.0000 873.19 21.9872 1147.95 0.0000 875.33 0.0000 1173.23 17.8104 879.38 14.3701 1177.95 14.6862 880.51 21.0842 1189.05 17.8871 883.24 18.2259 1204.77 19.0195 884.68 13. 4365 1221.41 16.9805 889.28 19.2249 1231. 02 18. 7258 894.76 15.4087 1235.36 0.0000 898.04 13.4976 1238.28 20.7104 900. 72 20.2643 1260.41 0.0000 903.28 15.4531 1271.87 11. 8271 911.20 17.4309 1274.44 11. 8352 912.08 17.4359 1274.54 11. 8352 923.98 0.0000 1291. 59 18.3696 926.50 7.7864 1298.22 0.0000 929 .11 28.2495 1312 .11 0.0000 937.49 27.3506 1332.49 5.2397 944.13 0.0000 1362.66 0.0000 946.00 13. 7133 1365.19 6.6017 949.00 14 .1187 1368.63 0.0000 667.71 0.0000 1384.29 0.0000 962. 31 20.4807 1408.01 12.2266 964.08 11. 0346 1457.56 0.0000 966 .17 23.6609 1460.82 11. 7013 911.20 24.6689 1489.16 6.3410 968. 97 24.6689 1505.03 9.9994 983.53 0.0000 1584.12 7.7063 984.45 0.0000 1596.21 0.0000 Page 4431 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:58:23.64 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM25.CNF;357 Background date : Z-OCT-2016 11:01:25. Sample date 14-DEC-2015 13:56:00 Acquisition date : 3-0CT-2016 05:57:14. Sample ID G405235065 Sample quantity : 1.47836E+02 GRAM Detector name : GAM25 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.55 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 0 0 4 4 0 0 0 0 7 7 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4432 of 5809 Energy 46.44* 63.16* 77.20* 84.17* 87.07 89.80 92.88* 128.38 143.37* 186.18* 208.76 238.80* 241.74 270.43 295.25* 300.81 338.56* 352.23* 463.82 481.66 493.76 511.14* 567.01 583.50* 609.37* 629.40 678.03 703.73 719.29 723 .13 728.25 756.56 764.38 768.17 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 40 25 369 35 109 70 90 43 23 92 42 442 94 52 191 54 117 322 61 24 2 30 15 143 203 13 9 13 15 9 21 16 9 31 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 119 241 186 110 150 82 190 118 136 138 80 73 101 53 78 35 69 62 24 31 16 57 9 34 45 20 6 36 9 14 30 24 19 13 0.86 0.77 0.79 1. 21 1. 36 0.89 1. 27 1. 40 0. 62 1. 08 0.99 1.11 1. 44 1. 66 1. 08 1. 68 1. 25 1.13 2.14 2.95 1. 29 1. 51 1. 64 1. 29 1. 56 0.64 1. 27 0.62 0.56 0.78 2.45 0.95 0.99 1. 38 92.38 125.82 153.89 167.84 173.63 179.09 185.25 256.24 286.21 371.83 416.97 477.05 482.93 540.33 589.95 601.08 676.58 703.92 927 .11 962. 81 987.00 1021.77 1133. 53 1166. 52 1218.28 1258.35 1355. 63 1407.06 1438.19 1445.87 1456 .11 1512.75 1528.39 1535.97 89 123 152 166 171 177 177 254 283 367 414 470 470 536 584 597 670 698 921 957 984 1016 1130 1160 1211 1253 1352 1398 1434 1441 1449 1506 1520 1531 7 1. lOE-02 51. 5 8 6.83E-03115.5 6 1.02E-01 8.0 5 9.62E-03 50.4 6 3.04E-02 20.0 15 1.95E-02 19.5 15 2.49E-02 30.8 8 l.21E-02 45.9 8 6.28E-03 93.7 10 2.55E-02 27.2 7 1.16E-02 38. 6 19 1. 23E-01 5. 8 19 2.62E-02 22.1 9 1.46E-02 29.0 12 5. 32E-02 11. 9 11 1.49E-02 26.0 14 3.24E-02 18.1 12 8.96E-02 7.5 14 1. 70E-02 21. 4 11 6.80E-03 48.0 6 5.86E-04317.8 15 8.24E-03 65.8 7 4.18E-03 41.6 14 3.97E-02 12.2 14 5.63E-02 10.1 12 3.54E-03 76.8 7 2.44E-03 59.5 11 3.71E-03 90.9 8 4.17E-03 44.2 9 2.60E-03 78.2 11 5.70E-03 56.5 12 4.44E-03 66.1 11 2.55E-03 98.0 9 8.52E-03 28.1 Fit 1.37E+OO 2.17E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 788.47 30 21 5.45 1576.59 1568 19 8.33E-03 42.7 36 0 795.50 14 11 1.86 1590.66 1586 9 3.78E-03 52.l 37 0 860.86 16 24 1. 03 ,1721. 44 1711 16 4.58E-03 70.8 38 0 870.66* 11 15 1.03 1741.04 1737 10 3.lOE-03 73.1 39 0 877.54 13 20 0.85 1754.80 1748 14 3.67E-03 78.l 40 0 911. 22* 102 12 1.80 1822.20 1814 16 2.83E-02 12.8 41 0 929.74 16 5 1. 04 1859.25 1853 9 4.40E-03 35.2 42 0 969.29* 67 10 1. 34 1938.39 1934 11 1.85E-02 16.7 43 0 1008. 96 8 4 2. 72 2017. 77 2013 8 2.29E-03 54.2 44 0 1064.60 16 13 4.05 2129.13 2122 16 4.46E-03 54.6 45 0 1120.51* 56 13 1. 51 2241. 02 2233 17 l.57E-02 19.9 46 0 1339 .15 8 6 0.64 2678.61 2669 14 2.22E-03 77.6 47 0 1460.76* 366 9 2.07 2922.03 2913 16 l.02E-01 5.6 48 0 1571. 36 9 3 0.63 3143.45 3137 11 2.59E-03 47.4 49 0 1730.34 7 4 0.81 3461.74 3455 9 1.84E-03 69.3 50 2 1763.43 26 8 2.44 3528.00 3519 18 7.29E-03 31.2 9.69E-01 51 2 1765.85* 12 4 1. 97 3532.83 3519 18 3.21E-03 52.6 Flag: "*" = Peak area was modified by background subtraction Page 4433 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:58:25 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 14-DEC-2015 13:56:00 G405235065 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 05:57:14 147.84 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA25 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 351.93 Page 4434 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86. 94 SN-126 87.57 CD-109 88.03 BI-211 351.06 CAN 0 01:00:00.55 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10. fii6* 1.131E+OO 1.486E+Ol 1.486E+Ol 11.10 OK NB-94 702.65 99.81* 2.143E+OO 3.288E-02 3.288E-02 181. 73 OK 871. 09 99.89 1. 793E+OO 3.212E-02 3.212E-02 146.30 OK NB-95 765.81 99.81* 2.000E+OO 2.402E-02 5. 772E-01 196.03 OK ZR-95 724.19 44.27 2.095E+OO 5.293E-02 1.272E+OO 156.31 OK 756.73 54.38* 2.017E+OO 7.627E-02 1.833E+OO 132.29 OK CD-109 88.03 3.70* 9.279E+OO 8.157E-01 1.268E+OO 105.12 OK SN-126 64.28 9.60 9.545E+OO 1.744E-01 1.744E-01 231.10 OK 86.94 8.90 9.279E+OO 3.391E-01 3.391E-01 105.12 OK 87.57 37.00* 9.279E+OO 8.157E-02 8.157E-02 105.12 OK TL-208 277.37 6.60 4.809E+OO Line Not Found Absent 583.19 85.00* 2.509E+OO 3.592E-01 3.592E-01 24.49 OK 860.56 12.50 1.810E+OO 3.759E-01 3.759E-01 141.57 OK PB-210 46.54 4.25* 9.121E+OO 6.790E-01 6.963E-01 102.93 OK BI-211 72.87 1. 23 9.424E+OO Line Not Found Absent 351.06 12.92* 3.891E+OO l.187E-02 l.187E-028508.91 OK PB-212 74.82 10.28 9.405E+OO Line Not Found Absent 77 .11 17.10 9.382E+OO 1.471E+OO 1.471E+OO 16.04 OK 238.63 43.60* 5.475E+OO 1.078E+OO 1.078E+OO 11. 56 OK 300.09 3.30 4.476E+OO 2.071E+OO 2.071E+OO 52.03 OK BI-214 609.32 45.49* 2.419E+OO 9.839E-01 9.843E-01 20 .11 OK 1120. 29 14.92 l.443E+OO l.318E+OO l.318E+OO 39.79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.803E-01 62.46 OK PB-214 74.82 5.80 9.405E+OO Line Not Found Absent 77 .11 9.70 9.382E+OO 2.594E+00 ,2.595E+OO 16.04 OK 87.09 3.41 9.279E+OO Line Not Found <<INT Reject 242.00 7.25 5.413E+OO Line Not Found <<INT Reject 295.22 18.42 4.551E+OO l.304E+OO l.305E+OO 23.76 OK 351. 93 35.60* 3.894E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.419E+OO 9.839E-01 9.843E-01 20 .11 OK 1120.29 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39.79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.803E-01 62.46 OK RA-224 240.99 4.10* 5.418E+OO l.653E-01 l.653E-01 738.01 OK RA-226 609.32 45.49* 2.419E+OO 9.839E-01 9.843E-01 20 .11 OK 1120.29 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39.79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.803E-01 62.46 OK AC-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11.27 4.030E+OO 1.448E+OO 1.448E+OO 36.11 OK 794.95 4.25 1.934E+OO 8. 621E-01 8.621E-01 104.16 OK 835.71 1. 61 1.856E+OO Line Not Found Absent 911.20 25.80* 1. 725E+OO 1.174E+OO 1.174E+OO 25.50 OK 968. 97 15.80 1.637E+OO 1. 313E+OO 1.313E+OO 33.42 OK RA-228 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11.27 4.030E+OO 1.448E+OO 1.448E+OO 36.11 OK 794.95 4.25 1.934E+OO 8. 621E-01 8. 621E-01 104.16 OK 835.71 1. 61 1.856E+OO Line Not Found Absent 911. 20 25.80* 1. 725E+OO 1.174E+OO 1.174E+OO 25.50 OK 968. 97 15.80 l.637E+OO 1.313E+OO 1. 313E+OO 33.42 OK TH-228 74.82 10.28 9.405E+OO Line Not Found Absent Page 4435 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77 .11 9.382E+OO 1.471E+OO l.471E+OO 16.04 OK 238.63 43.60* 5.475E+OO 1.078E+OO 1.078E+OO 11. 56 OK 300.09 3.30 4.476E+OO 2. 071E+OO 2.071E+OO 52.03 OK TH-229 85.43 14.70 9.312E+OO l.608E-01 1.608E-01 100.75 OK 88.47 24.00 9.244E+OO 1.997E-01 1.997E-01 38.94 OK 193.51 4.41* 6. 496E+OO Line Not Found Absent 210.85 2.80 6.071E+OO Line Not Found Absent TH-230 609.32 45.49* 2.419E+OO 9.839E-01 9.839E-01 20 .11 OK 1120.29 14.92 l.443E+OO 1.318E+OO 1.318E+00 39. 79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.800E-01 62.46 OK PA-231 283.69 1. 70 4. 715E+OO Line Not Found Absent 301. 36 5.35* 4.476E+00 1.278E+OO 1.278E+OO 52.03 OK TH-232 105.21 1.10 8.977E+OO Line Not Found Absent 338.32 11. 27 4.030E+OO 1.448E+OO 1.448E+OO 36.11 OK 835.71 1. 61 l.856E+00 Line Not Found Absent 911.20 25.80* 1.725E+OO 1.174E+OO 1.174E+OO 25.50 OK 968.97 15.80 1.637E+OO 1.313E+OO 1.313E+OO 33.42 OK TH-234 63. 29 3.70* 9.545E+OO 4.526E-01 4.526E-01 231.10 OK 92.59 4.23 9.201E+OO 1.453E+OO 1.453E+OO 61. 52 OK U-234 609.32 45.49* 2.419E+OO 9.839E-01 9.839E-01 20 .11 OK 1120. 29 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39.79 OK 1764.49 15.30 9.342E-01 8.800E-01 8.800E-01 62.46 OK U-235 89. 96 3.47 9.244E+OO 1.381E+OO 1.381E+00 38.94 OK 93.35 5.60 9.201E+OO 1.098E+OO 1.098E+OO 61. 52 OK 143.76 10. 96* 7.933E+OO 1.581E-01 1.581E-01 187.34 OK 163.33 5.08 7.333E+OO Line Not Found Absent 185. 72 57.20 6.688E+OO 1.426E-01 1. 42 6E-01 54.41 OK 205.31 5.01 6.202E+OO Line Not Found Absent U-238 63.29 3.70* 9.545E+OO 4.526E-01 4.526E-01 231.10 OK 92.59 4.23 9.201E+OO l.453E+00 1.453E+OO 61. 52 OK ANH-511 511. 00 100.00* 2.809E+OO 5.731E-02 5. 731E-02 131. 62 OK Flag: "*" = Keyline Page 4436 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:58:27.09 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l * *Acquisition date 3-0CT-2016 05:57:14 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:56:00 Analyst initials: MXRl *
  • Sample ID G405235065 Sample Quantity 1.4784E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;15 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 48 6E+Ol 1.616E+OO NB-94 3.288E-02 5.856E-02 NB-95 5.772E-01 1.109E+OO ZR-95 1.833E+OO 2.376E+OO CD-109 1.268E+OO 1.306E+OO SN-126 8.157E-02 8.404E-02 TL-208 3.592E-01 8. 621E-02 PB-210 6.963E-01 7.023E-01 BI-211 1.187E-02 9.898E-01 PB-212 1.078E+OO 1. 221E-01 BI-214 9.843E-01 1.940E-01 PB-214 1.309E+OO 1.920E-01 RN-222 9.843E-01 1.940E-01 RA-224 1.653E-01 1.196E+OO RA-226 9.843E-01 1.940E-01 AC-228 1.174E+OO 2.934E-01 RA-228 1.174E+OO 2.934E-01 TH-228 1. 078E+OO 1.221E-01 TH-229 -1. 970E-01 3.778E-01 TH-230 9.839E-01 1.939E-01 PA-231 1.278E+OO 6.515E-01 TH-232 1.174E+OO 2.934E-01 TH-234 4.526E-01 1.025E+OO U-234 9.839E-01 1.939E-01 U-235 1.581E-01 2.903E-01 U-238 4.526E-01 1.025E+OO ANH-511 5.731E-02 7.393E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4437 of 5809 Key-Line Activity (pCi/GRAM -6.901E+OO -4.344E-03 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.161E+Ol 4.848E-02 1. 960E+41 MDA (pCi/GRAM 7.067E-01 5.875E-02 9.378E-01 2.466E+OO 1.203E+OO 6.914E-02 5.023E-02 5.653E-01 2.940E-01 7. 821E-02 1.289E-01 3.340E-01 l.289E-01 8.397E-01 1.289E-01 2.334E-01 2.334E-01 7. 821E-02 6.735E-01 1. 289E-01 6.390E-01 2.334E-01 7.537E-01 1.289E-01 2.564E-01 7.537E-01 5.250E-02 MDA (pCi/GRAM l.818E+Ol 9.269E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -l.085E-02 2. 661E-02 5.204E-02 NOT IDENT. SC-46 -5.542E-02 3.828E-01 7.426E-01 FAIL ABUN V-48 O.OOOE+OO l.104E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 2.892E+02 O.OOOE+OO SHORT HLIF MN-54 -3.158E-03 5. 967E-02 l.184E-01 NOT IDENT. C0-56 1.014E-02 4.465E-01 8.920E-01 NOT IDENT. MN-56 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF C0-57 4.635E-03 3.497E-02 6.847E-02 NOT IDENT. C0-58 3.920E-02 4.089E-01 8.651E-01 NOT IDENT. FE-59 -l.522E+OO 6.602E+OO 1. 260.E+Ol NOT IDENT. C0-60 2.932E-02 4.520E-02 9.091E-02 NOT IDENT. ZN-65 2.576E-02 1.345E-01 2.573E-01 NOT IDENT. GE-68 1. 431E-01 2.646E+OO 5.160E+OO NOT IDENT. AS-73 -3. 791E-02 l.465E+OO 2.988E+OO NOT IDENT. AS-74 O.OOOE+OO 4.502E+03 O.OOOE+OO SHORT HLIF SE-75 l.137E-01 l.752E-01 3.437E-01 NOT IDENT. BR-77 O.OOOE+OO 3.641E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.229E+02 0.000E+OO SHORT HLIF RB-83 2.900E-01 5.290E-01 1.112E+00 NOT IDENT. KR-85 -2.600E+OO 6.358E+OO 1.163E+Ol NOT IDENT. SR-85 -2.606E-01 6.293E-01 1.150E+OO NOT IDENT. RB-86 O.OOOE+OO 2.452E+04 O.OOOE+OO SHORT HLIF Y-88 -8.054E-02 1.823E-01 3.509E-01 NOT IDENT. Y-91 -2.273E+02 5.631E+02 1.008E+03 NOT IDENT. NB-95M 2.939E-01 1. 931E+OO 3.343E+00 NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.757E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 O.OOOE+OO 4.981E-02 4.539E-02 FAIL ABUN RH-102 -l.785E-02 5.444E-02 8.725E-02 FAIL ABUN RU-103 -9. 891E-01 6.045E+OO 1.00lE+Ol FAIL ABUN RH-106 3.707E-01 4.672E-01 9.915E-01 NOT IDENT. RU-106 3.707E-01 4. 672E-01 9.915E-01 NOT IDENT. AG-108M 5.613E-03 2.548E-02 5.105E-02 FAIL ABUN AG-llOM l.575E-02 1.022E-01 2.017E-01 FAIL ABUN SN-113 -8.336E-02 2.169E-01 4.077E-01 NOT IDENT. CD-115 O.OOOE+OO 3.930E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 5.153E+04 O.OOOE+OO SHORT HLIF TE-123M 5.296E-02 9.254E-02 1.856E-01 NOT IDENT. SB-124 5.497E-02 1. 745E+OO 3.873E+OO FAIL ABUN SB-125 -1. 972E-02 8.097E-02 l.560E-01 FAIL ABUN TE-125M 5.498E+Ol 1. 728E+02 3.461E+02 NOT IDENT. I-126 O.OOOE+OO 6.895E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 8.695E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 7.675E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.636E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.377E+25 O.OOOE+OO SHORT HLIF BA-133 1.043E-02 3.553E-02 6.661E-02 NOT IDENT. I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 5.612E-02 5.729E-02 1.050E-01 FAIL ABUN CS-135 2.022E-02 1.320E-01 2.266E-01 NOT IDENT. I-135 O.OOOE+OO l.398E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.470E+05 O.OOOE+OO SHORT HLIF BA-137M 3.077E-02 3.495E-02 7.330E-02 NOT IDENT. CS-137 3.251E-02 3.693E-02 7.743E-02 NOT IDENT. CE-139 -8.346E-02 8. 969E-02 1. 565E-01 NOT IDENT. BA-140 O.OOOE+OO 7.917E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.978E+05 O.OOOE+OO SHORT HLIF CE-141 -4.775E+00 1.867E+Ol 3.237E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.565E+40 O.OOOE+OO SHORT HLIF CE-144 -2 .116E-01 2.579E-01 4.657E-01 NOT IDENT. PM-144 -1.456E-02 6.253E-02 9. 960E-02 NOT IDENT. PR-144 -1.218E+OO 5.419E+OO 8.647E+OO NOT IDENT. PM-146 1.254E-b2 3.599E-02 7.402E-02 NOT IDENT. ND-147 0.000E+OO 2.163E+07 O.OOOE+OO SHORT HLIF PM-147 -1.949E+Ol 6.185E+02 1.197E+03 NOT IDENT. PM-149 O.OOOE+OO 5.747E+39 O.OOOE+OO SHORT HLIF EU-150 l.532E-02 2.339E-02 4.532E-02 FAIL ABUN EU-152 6. 961E-02 7.899E-02 1.597E-01 NOT IDENT. GD-153 -7.477E-02 l.056E-01 l.809E-01 NOT IDENT. EU-154 2.279E-02 l.154E-01 2.332E-01 FAIL ABUN EU-155 4.990E-02 7.185E-02 l.476E-01 FAIL ABUN TB-160 -4.775E-01 1. 793E+OO 3.005E+OO FAIL ABUN H0-166M -l.525E-02 6.095E-02 l.097E-01 NOT IDENT. TM-171 l.164E+00 3.402E+OO 7.105E+OO NOT IDENT. HF-172 8.276E-02 1. 772E-01 3.322E-01 FAIL ABUN Page 4438 of 5809 LU-172 -2.428E-02 8.992E-02 l.664E-01 FAIL ABUN LU-176 5.709E-04 2.073E-02 3.787E-02 FAIL ABUN HF-181 6.843E+OO 6.438E+OO 8.037E+00 FAIL ABUN TA-182 -1. 7 54E-02 *1. 012E+OO l.920E+OO FAIL ABUN RE-183 -5.597E-01 7.075E-01 l.382E+00 NOT IDENT. RE-184 1.302E+Ol 3.003E+Ol 6.065E+Ol NOT IDENT. W-188 -2.242E+Ol 9.657E+Ol 1. 562E+02 FAIL ABUN IR-192 -1.148E-01 3.812E-01 7.391E-01 FAIL ABUN HG-203 4.076E-01 2.104E+OO 3.893E+OO NOT IDENT. BI-207 7.335E-02 7.851E-02 9. 962E-02 FAIL ABUN PB-211 -5. 729E-01 5.527E-01 9.563E-01 NOT IDENT. BI-212 7.749E-01 8.578E-01 l.269E+OO FAIL ABUN RN-219 9.840E-02 3.435E-01 6.934E-01 FAIL ABUN RA-223 -l.676E-01 4. 941E-01 9.544E-01 FAIL ABUN AC-227 -l.276E-01 1.984E-01 3.376E-01 FAIL ABUN TH-227 -1. 276E-01 l.984E-01 3.376E-01 FAIL ABUN TH-231 -l.676E-01 4. 941E-01 9.544E-01 FAIL ABUN PA-233 -2.903E-02 5 .116E-02 9.687E-02 FAIL ABUN PA-234 -8.797E-02 2.785E-01 5.257E-01 NOT IDENT. PA-234M 2.684E+OO 4.477E+OO 9. 596E+OO NOT IDENT. NP-237 -2.903E-02 5 .116E-02 9.687E-02 FAIL ABUN NP-238 O.OOOE+OO 6.207E+40 O.OOOE+OO SHORT HLIF NP-239 -l.210E-01 1. 705E-01 3.152E-01 NOT IDENT. PU-239 O.OOOE+OO 4.534E+02 4. 901E+02 FAIL ABUN AM-241 5.032E-03 3.900E-02 7. 996E-02 NOT IDENT. AM-243 O.OOOE+OO 3. 511E-02 7. 741E-02 NOT IDENT. CM-243 -2.975E-02 6.169E-02 1.175E-01 NOT IDENT. BK-247 7.139E-02 6.064E-02 1.258E-01 FAIL ABUN CM-247 5.325E-03 3.107E-02 6.211E-02 NOT IDENT. CF-249 9.598E-03 3.310E-02 6.711E-02 NOT IDENT. CF-251 -2.393E-02 9.529E-02 1. 755E-01 NOT IDENT. Page 4439 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:58:24.43 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 353 10.66* l.131E+OO 1. 486E+Ol 1.486E+Ol 11.10 NB-94 702.65 14 99.81* 2.143E+OO 3.288E-02 3.288E-02 181. 73 871.09 11 99.89 1. 793E+OO 3.212E-02 3.212E-02 146.30 NB-95 765.81 9 99.81* 2.000E+OO 2.402E-02 5.772E-01 196. 03 ZR-95 724 .19 10 44.27 2.095E+OO 5.293E-02 1. 272E+OO 156.31 756.73 16 54.38* 2.017E+OO 7.627E-02 1.833E+OO 132.29 CD-109 88.03 136 3.70* 9.279E+OO 2.018E+OO 3.136E+OO 40.08 SN-126 64.28 31 9.60 9.545E+OO l.744E-01 l.744E-01 231.10 86.94 136 8.90 9.279E+OO 8.388E-01 8.388E-01 40.08 87.57 136 37.00* 9.279E+OO 2.018E-01 2.018E-01 40.08 TL-208 277.37 ------6.60 4.809E+OO ------Line Not Found ------583.19 151 85.00* 2.509E+OO 3.592E-01 3.592E-01 24.49 860.56 17 12.50 1.810E+OO 3.759E-01 3.759E-01 141.57 PB-210 46.54 52 4.25* 9 .121E+OO 6.790E-01 6. 963E-01 102.93 BI-211 72.87 ------1. 23 9.424E+OO ------Line Not Found ------351.06 357 12.92* 3.891E+OO 3.605E+OO 3.605E+OO 14.97 PB-212 74.82 ------10.28 9.405E+OO ------Line Not Found ------77 .11 465 17.10 9.382E+OO 1. 471E+OO 1.471E+OO 16.04 238.63 507 43.60* 5.475E+OO 1. 078E+OO 1.078E+OO 11. 56 300.09 60 3.30 4.476E+OO 2. 071E+OO 2. 071E+00 52.03 BI-214 609.32 213 45.49* 2.419E+OO 9.839E-01 9.843E-01 20.11 1120.29 56 14.92 1. 443E+OO 1.318E+00 l.318E+00 39.79 1764.49 25 15.30 9.342E-01 8.800E-01 8.803E-01 62. 46 PB-214 74.82 ------5.80 9.405E+OO ------Line Not Found ------77 .11 465 9.70 9.382E+00 2.594E+OO 2.595E+OO 16.04 87.09 136 3.41 9.279E+OO 2.189E+OO 2.190E+OO 40.08 242.00 108 7.25 5.418E+OO 1.398E+OO 1.398E+OO 44 .11 295.22 215 18.42 4.551E+OO 1.304E+OO 1.305E+OO 23.76 351.93 357 35.60* 3.891E+OO 1.308E+OO 1.309E+OO 14.97 RN-222 609.32 213 45.49* 2.419E+OO 9.839E-01 9.843E-01 20.11 1120. 29 56 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39.79 1764.49 25 15.30 9.342E-01 8.800E-01 8.803E-01 62.46 RA-224 240.99 108 4.10* 5.418E+00 2.471E+OO 2.471E+OO 44 .11 RA-226 609.32 213 45.49* 2.419E+OO 9.839E-01 9.843E-01 20 .11 1120. 29 56 14.92 1.443E+OO 1.318E+OO 1.318E+OO 39.79 1764.49 25 15.30 9.342E-01 8.800E-01 8*.803E-01 62.46 AC-228 105.21 ------1.10 8.977E+00 ------Line Not Found ------338.32 130 11.27 4.030E+OO 1.448E+OO 1.448E+OO 36.11 794.95 14 4.25 1.934E+OO 8. 621E-01 8. 621E-01 104.16 835.71 ------1. 61 1. 856E+OO ------Line Not Found ------911.20 103 25.80* 1.725E+OO l.174E+OO 1.174E+OO 25.50 968.97 67 15.80 1.637E+OO 1.313E+OO 1.313E+OO 33.42 RA-228 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 130 11. 27 4.030E+OO 1.448E+OO 1.448E+OO 36 .11 794.95 14 4.25 1.934E+OO 8.621E-01 8. 621E-01 104.16 835. 71 ------1. 61 1.856E+OO ------Line Not Found ------911. 20 103 25.80* 1. 725E+OO 1.174E+OO 1.174E+OO 25.50 Page 4440 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 968 .S7 67 15.80 l.637E+OO l.313E+OO .l.313E+OO 33.42 TH-228 74.82 ------10.28 9.405E+OO ------Line Not Found ------77 .11 465 17.10 9.382E+OO l.471E+OO l.471E+OO 16.04 238.63 507 43.60* 5.475E+OO l.078E+OO l.078E+OO 11. 56 300.09 60 3.30 4.476E+OO 2.071E+OO 2.071E+OO 52.03 TH-229 85.43 43 14.70 9.312E+OO l.608E-01 l.608E-01 100.75 88.47 87 24.00 9.244E+OO l.997E-01 l.997E-01 38.94 193.51 ------4.41* 6.496E+OO ------Line Not Found ------210.85 ------2.80 6. 071E+OO ------Line Not Found ------TH-230 609.32 213 45.49* 2.419E+OO 9.839E-01 9.839E-01 20 .11 1120.29 56 14.92 l.443E+OO l.318E+OO l.318E+OO 39.79 1764.49 25 15.30 9.342E-01 8.800E-01 8.800E-01 62.46 PA-231 283.69 ------1. 70 4. 715E+OO ------Line Not Found ------301.36 60 5.35* 4.476E+OO l.278E+OO l.278E+OO 52.03 TH-232 105.21 ------1.10 8.977E+OO ------Line Not Found ------338.32 130 11. 27 4.030E+OO l.448E+OO l.448E+OO 36 .11 835.71 ------1. 61 l.856E+00 ------Line Not Found ------911.20 103 25.80* 1. 725E+OO l.174E+OO l.174E+OO 25.50 968.97 67 15. 80 ' l.637E+OO l.313E+OO l.313E+OO 33.42 TH-234 63.29 31 3.70* 9.545E+OO 4.526E-01 4.526E-01 231.10 92.59 111 4.23 9.201E+OO l.453E+OO l.453E+OO 61. 52 U-234 609.32 213 45.49* 2.419E+OO 9.839E-01 9.839E-01 20 .11 1120.29 56 14.92 l.443E+OO l.318E+OO l.318E+OO 39.79 1764.49 25 15.30 9.342E-01 8.800E-01 8.800E-01 62.46 U-235 89. 96 87 3.47 9.244E+OO 1. 381E+OO 1. 381E+OO 38.94 93.35 111 5.60 9.201E+OO l.098E+OO l.098E+OO 61.52 143.76 27 10.96* 7.933E+OO l.581E-01 1. 581E-01 187.34 163.33 ------5.08 7.333E+00 ------Line Not Found ------185. 72 107 57. 2.0 6.688E+OO l.426E-01 1. 426E-01 54.41 205.31 ------5.01 6.202E+OO ------Line Not Found ------U-238 63.29 31 3.70* 9.545E+OO 4.526E-01 4.526E-01 231.10 92.59 111 4.23 9.201E+OO l.453E+OO l.453E+OO 61. 52 ANH-511 511. 00 32 100.00* 2.809E+OO 5.731E-02 5.731E-02 131. 62 Flag: "*" Key line Page 4441 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235065 Acquisition date 3-0CT-2016 05:57:14 Total number of lines in spectrum 51 Number of unidentified lines 9 Number of lines tentatively identified by NID 42 Nuclide Type : Nuclide K-40 NB-94 NB-95 ZR-95 CD-109 SN-126 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 ANH-511 Hlife l.25E+09Y 20300.00Y 64.03D 64.03D 461. 40D 2.30E+05Y 1.41E+10Y 22.20Y 7.04E+08Y 1.41E+10Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+10Y 1600.00Y l.41E+l0Y 1. 41E+10Y 1.41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1.41E+10Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y l.00E+09Y Decay 1. 00 1. 00 24.0 24.0 1. 55 1. 00 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.486E+Ol 3.288E-02 2.402E-02 7.627E-02 2.018E+OO 2.018E-01 3.592E-01 6.790E-01 3.605E+OO 1.078E+OO 9.839E-01 1.308E+OO 9.839E-01 2.471E+OO 9.839E-01 l.174E+OO. l.174E+00 1. 078E+OO l.997E-01 9.839E-01 l.278E+OO l.174E+OO 4.526E-01 9.839E-01 1.581E-01 4.526E-01 5.731E-02 3.883E+Ol 3.883E+Ol Decay Corr pCi/GRAM 1.486E+Ol 3.288E-02 5.772E-01 1.833E+OO 3.136E+OO 2.018E-01 3.592E-01 6.963E-01 3.605E+00 1.078E+OO 9.843E-01 1.309E+00 9.843E-01 2.471E+OO 9.843E-01 l.174E+00 1.174E+OO 1.078E+OO 1.997E-01 9.839E-01 1.278E+OO 1.174E+OO 4.526E-01 9.839E-01 1.581E-01 4.526E-01 5. 731E-02 4.227E+Ol 4.227E+Ol 82.35% Decay Corr 2-Sigma Error 0.165E+Ol 5.976E-02 11. 31E-01 2.424E+OO 1.257E+OO 0.809E-01 0.880E-01 7.167E-01 0.540E+OO 0.125E+OO 1.979E-01 0 .196E+OO 1. 979E-01 l.090E+00 1.979E-01 0.299E+OO 0.299E+OO 0.125E+00 0.778E-01 1.979E-01 0.665E+OO 0.299E+OO 10.46E-01 l.979E-01 2.962E-01 10.46E-01 7.543E-02 "M" Manually accepted 2-Sigma %Error 11.10 181. 73 196. 03 132.29 40.08 40.08 24.49 102.93 14.97 11. 56 20 .11 14.97 20 .11 44 .11 20 .11 25.50 25.50 11. 56 38.94 20 .11 52.03 25.50 231.10 20 .11 187.34 231.10 131. 62 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4442 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235065 Acquisition date : 3-0CT-2016 05:57:14 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 128.38 53 142 1. 40 256.24 254 8 1.21E-02 91. 8 8.38E+OO T 0 208.76 48 93 0.99 416.97 414 7 1.16E-02 77.2 6.12E+OO 0 270.43 59 60 1. 66 540.33 536 9 1.46E-02 58.0 4.92E+OO T
  • 0 463.82 66 26 2.14 927.11. 921 14 1.70E-02 42.8 3.05E+OO T 0 481. 66 26 33 2.95 962. 81 957 11 6.80E-03 96. 0 2. 96E+OO T 0 493.76 2 17 1. 29 987.00 984 6 5.86E-04 **** 2.89E+OO T 0 567 .,01 16 9 1. 64 1133. 53 1130 7 4.18E-03 83.3 2.57E+OO 0 629.40 13 21 0.64 1258.35 1253 12 3.54E-03 **** 2.35E+OO T 0 678.03 9 6 1. 27 1355.63 1352 7 2.44E-03 **** 2.21E+OO T 0 719.29 16 9 0.56 1438.19 1434 8 4.17E-03 88.4 2.lOE+OO T 0 728. 25 21 32 2.45 1456 .11 1449 11 5.70E-03 **** 2.08E+OO T 0 768.17 32 14 1. 38 1535.97 1531 9 8.52E-03 56.2 1. 99E+OO T 0 788.47 31 22 5.45 1576.59 1568 19 8.33E-03 85.3 1. 95E+OO 0 877.54 13 20 0.85 1754.80 1748 14 3.67E-03 **** 1. 78E+OO 0 929.74 16 5 1. 04 1859.25 1853 9 4.40E-03 70.4 1.70E+OO T 0 1008. 96 8 4 2. 72 2017.77 2013 8 2.29E-03 **** 1.58E+OO 0 1064.60 16 13 4.05 2129.13 2122 16 4.46E-03 **** 1.51E+OO T 0 1339.15 8 6 0.64 2678.61 2669 14 2.22E-03 **** 1.23E+OO 0 1571. 36 9 3 0.63 3143.45 3137 11 2.59E-03 94.8 1. 05E+OO 0 1730.34 6 4 0.81 3461.74 3455 9 1.84E-03 **** 9.53E-01 2 1765.85 11 4 1. 97 3532.83 3519 18 3.21E-03 **** 9.33E-01 Flags: "T" = Tentatively associated Page 4443 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:58:39.29 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l * *Acquisition date 3-0CT-2016 05:57:14 Sensitivity 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:56:00 Nuclide Library : SOLID *
  • Sample ID G405235065 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4784E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 1-AUG-2016 08:41:33 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;15
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 NB-94 NB-95 ZR-95 CD-109 SN-126 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 ANH-511 Le (pCi/GRAM 2. 961E-01 2.610E-02 3.843E-01 1.080E+OO 5. 681E-01 3.243E-02 2.181E-02 2.630E-01 1. 32 9E-01 3.610E-02 5.807E-02 1.619E-01 5.807E-02 3.877E-01 5.807E-02 1.0lOE-01 1.0lOE-01 3.610E-02 3 .116E-01 5.805E-02 2.896E-01 1.0lOE-01 3.560E-01 5.805E-02 1* .199E-01 3.560E-01 2.374E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4444of5809 Le (pCi/GRAM 8.046E+OO 3. 967E-02 O.OOOE+OO 1.844E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-95M NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 4445 of 5809 3.263E-01 O.OOOE+OO O.OOOE+OO 5.199E-02 3.929E-01 O.OOOE+OO 3.213E-02 3. 672E-01 5.488E+OO 3.923E-02 l.068E-01 2.274E+OO 1.400E+OO O.OOOE+OO 1.586E-01 0.000E+OO O.OOOE+OO 4.956E-01 5.199E+OO 5.141E-01 O.OOOE+OO 1.232E-01 4.401E+02 1.546E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2 .119E-02 3.741E-02 4.525E+OO 4.443E-01 4.443E-01 2.310E-02 8.859E-02 1.857E-Ol O.OOOE+OO O.OOOE+OO 8.641E-02 1.500E+OO 6.910E-02 l.625E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.017E-02 O.OOOE+OO 4.696E-02 l.043E-01 O.OOOE+OO O.OOOE+OO 3.312E-02 3.499E-02 7.277E-02 O.OOOE+OO O.OOOE+OO 1.519E+Ol O.OOOE+OO 2.166E-Ol 4.408E-02 3.828E+OO 3.314E-02 O.OOOE+OO 5.617E+02 O.OOOE+OO 2.081E-02 7.284E-02 8.402E-02 l.002E-01 6.949E-02 l.285E+OO 4.873E-02 3.333E+00 1.558E-01 7. 313E-02 FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 AM-243 CM-243 BK-247 CM....:247 CF-249 CF-251 Page 4446 of 5809 1. 720E-02 3.656E+OO 8.462E-01 6.498E-01 2.702E+Ol 7. 096E+Ol 3.378E-01 1.802E+OO 4.354E-02 4.235E-01 5.841E-01 3.156E-01 4.346E-01 1.542E-01 1.542E-01 4.346E-01 4.415E-02 2.281E-01 4.278E+OO 4.415E-02 O.OOOE+OO 1.470E-01 2.313E+02 3.784E-02 3.755E-02 5.482E-02 5.813E-02 2.820E-02 3.053E-02 8. l 72E-02 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NO';!:' IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:58:44.63 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235065.CNF;l * *Acquisition date 3-0CT-2016 05:57:14 Sensitivity : 3.000 *
  • Detector ID GAM25 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.55 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:56:00 Nuclide Library : SOLID *
  • Sample ID G405235065 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity 1.4784E+02 GRAM *
  • Quantity Err(%) 1.3529E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 08:41:33 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM25 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.486E+Ol 1.793E+OO NB-94 3.288E-02 5.858E-02 NB-95 5.772E-01 1.109E+OO ZR-95 1.833E+OO 2.377E+OO CD-109 1.268E+OO 1.331E+OO SN-126 8.157E-02 8.550E-02 TL-208 3.592E-01 8.755E-02 PB-210 6.963E-01 7.049E-01 BI-211 l.187E-02 1.014E+OO PB-212 1.078E+OO l.347E-01 BI-214 9.843E-01 1.985E-01 PB-214 1.309E+OO 1.995E-01 RN-222 9.843E-01 l.985E-01 RA-224 1.653E-01 1.205E+OO RA-226 9.843E-01 1.985E-01 AC-228 1.174E+OO 2.995E-01 RA-228 1.174E+OO 2.995E-01 TH-228 1.078E+OO l.347E-01 TH-229 -1.970E-01 3.779E-01 TH-230 9.839E-01 l.985E-01 PA-231 1.278E+00 7.062E-01 TH-232 1.174E+OO 2.995E-01 TH-234 4.526E-01 l.030E+OO U-234 9.839E-01 l.985E-01 U-235 1. 581E-01' 2.904E-01 U-238 4.526E-01 1.030E+OO ANH-511 5.731E-02 7.396E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4447of5809 Key-Line Activity (pCi/GRAM -6.901E+OO -4.344E-03 1.000E+41 K.L Act error (1.96-sigma) 1.161E+Ol 4.848E-02 4.017E+41 TPU (1.96-sigma) 1. 793E+OO 5.858E-02 1.109E+OO 2.377E+OO 1.331E+OO 8.550E-02 8.755E-02 7.049E-01 1.014E+OO l.347E-01 1.985E-01 l.995E-01 1.985E-01 1. 205E+OO l.985E-01 2.995E-01 2.995E-01 1. 34 7E-01 3.779E-01 1.985E-01 7.062E-01 2.995E-01 1.030E+OO 1.985E-01 2.904E-01 l.030E+OO 7. 396E-02 TPU (1.96-sigma) l.202E+Ol 4.852E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 -1.085E-02 2.662E-02 2.706E-02 NOT IDENT. SC-46 -5.542E-02 3.828E-01 3.836E-01 FAIL ABUN V-48 -3.132E+03 1.104E+04 l .113E+04 SHORT HLIF CR-51 -4.443E+Ol 2.892E+02 2.899E+02 SHORT HLIF MN-54 -3.158E-03 5. 967E-02 5. 969E-02 NOT IDENT. C0-56 l.014E-02 4.465E-01 4.465E-01 NOT IDENT. MN-56 1.000E+41 3.824E+42 O.OOOE+OO SHORT HLIF C0-57 4.635E-03 3.497E-02 3.504E-02 NOT IDENT. C0-58 3.920E-02 4.089E-01 4.093E-01 NOT IDENT. FE-59 -1.522E+OO 6.603E+OO 6. 638E+O.O NOT IDENT. C0-60 2.932E-02 4.521E-02 4.711E-02 NOT IDENT. ZN-65 2.576E-02 l.345E-01 l.350E-01 NOT IDENT. GE-68 1. 431E-01 2.646E+OO 2.647E+OO NOT IDENT. AS-73 -3. 791E-02 l.465E+OO 1.465E+OO NOT IDENT. AS-74 -4.534E+02 4.502E+03 4.507E+03 SHORT HLIF SE-75 l.137E-01 1. 753E-01 l.826E-01 NOT IDENT. BR-77 3.215E+37 2.726E+38 0.000E+OO SHORT HLIF SR-82 1.189E+02 6.229E+02 6.253E+02 SHORT HLIF RB-83 2.900E-01 5.305E-01 5.463E-01 NOT IDENT. KR-85 -2.600E+00 6.359E+OO 6.466E+OO NOT IDENT. SR-85 -2.606E-01 6.294E-01 6.402E-01 NOT IDENT. RB-86 2.732E+03 2.452E+04 2.455E+04 SHORT HLIF Y-88 -8.054E-02 1.824E-01 1. 860E-01 NOT IDENT. Y-91 -2.273E+02 5.632E+02 5.724E+02 NOT IDENT. NB-95M 2.939E-01 1. 931E+OO l.935E+OO NOT IDENT. NB-97 -1.000E+41 l.996E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 3.460E+41 O.OOOE+OO SHORT HLIF M0-99 -8.368E+30 3.758E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 3.833E+41 O.OOOE+OO SHORT HLIF RH-101 5.539E-02 5.081E-02 5.662E-02 FAIL ABUN RH-102 -1. 785E-02 5.445E-02 5.505E-02 FAIL ABUN RU-103 -9.891E-01 6.046E+OO 6.062E+OO FAIL ABUN RH-106 3.707E-01 4.678E-01 4. 968E-01 NOT IDENT. RU-106 3.707E-01 4.678E-01 4. 968E-01 NOT IDENT. AG-108M 5.613E-03 2.548E-02 2.561E-02 FAIL ABUN AG-llOM 1. 575E-02 1.022E-01 1.025E-01 FAIL ABUN SN-113 -8.336E-02 2.169E-01 2.201E-01 NOT IDENT. CD-115 -1.938E+38 3.945E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 2.954E+04 5.165E+04 5.334E+04 SHORT HLIF TE-123M 5.296E-02 9.257E-02 9.560E-02 NOT IDENT. SB-124 5.497E-02 1.745E+00 1. 746E+OO FAIL ABUN SB-125 -1.972E-02 8.098E-02 8.146E-02 FAIL ABUN TE-125M 5.498E+Ol 1. 728E+02 l.746E+02 NOT IDENT. I-126 -l.155E+04 6.895E+05 6. 896E+05 SHORT HLIF SB-126 1.003E+06 8.890E+05 9.974E+05 SHORT HLIF SB-127 -2.120E+21 8.188E+21 O.OOOE+OO SHORT HLIF I-131 -2.499E+08 2.636E+09 2.639E+09 SHORT HLIF I-132 1.000E+41 1.866E+42 O.OOOE+OO SHORT HLIF TE-132 4.300E+25 9.532E+25 O.OOOE+OO SHORT HLIF BA-133 1.043E-02 3.553E-02 3.584E-02 NOT IDENT. I-133 1.000E+41 3.942E+41 O.OOOE+OO SHORT HLIF CS-134 5.612E-02 5.734E-02 6. 2 67E-02 FAIL ABUN CS-135 2.022E-02 l.320E-01 1.323E-01 NOT IDENT. I-135 -l.000E+41 6.781E+41 O.OOOE+OO SHORT HLIF CS-136 -2. 961E+04 2.470E+05 2.474E+05 SHORT HLIF BA-137M 3.077E-02 3.498E-02 3. 7 63E-02 NOT IDENT. CS-137 3.251E-02 3.695E-02 3.975E-02 NOT IDENT. CE-139 -8.346E-02 9.125E-02 9.870E-02 NOT IDENT. BA-140 4.143E+05 7.919E+05 8 .136E+05 SHORT HLIF LA-140 2.034E+05 2.979E+05 3 .117E+05 SHORT HLIF CE-141 -4.775E+00 l.867E+Ol 1.879E+Ol NOT IDENT. CE-143 1.000E+41 5.654E+40 O.OOOE+OO SHORT HLIF CE-144 -2 .116E-01 2.581E-01 2.752E-01 NOT IDENT. PM-144 -1.456E-02 6.253E-02 6.288E-02 NOT IDENT. PR-144 -1.218E+OO 5.420E+OO 5.447E+OO NOT IDENT. PM-146 l.254E-02 3.600E-02 3.644E-02 NOT IDENT. ND-147 -8.930E+06 2.164E+07 2.201E+07 SHORT HLIF PM-147 -1.949E+Ol 6.185E+02 6.185E+02 NOT IDENT. PM-149 -1.566E+39 5.757E+39 O.OOOE+OO SHORT HLIF EU-150 l.532E-02 2.340E-02 2.440E-02 FAIL ABUN EU-152 6. 961E-02 7.909E-02 8.508E-02 NOT IDENT. GD-153 -7.477E-02 1.057E-01 l.109E-01 NOT IDENT. EU-154 2.279E-02 l.154E-01 l.158E-01 FAIL ABUN EU-155 4.990E-02 7.194E-02 7.537E-02 FAIL ABUN TB-160 -4.775E-01 1. 793E+OO 1.806E+OO FAIL ABUN H0-166M -l.525E-02 6.095E-02 6.134E-02 NOT IDENT. TM-171 l.164E+OO 3.403E+00 3.443E+OO NOT IDENT. HF-172 8.276E-02 l.777E-01 l.816E-01 FAIL ABUN Page 4448 of 5809 LU-172 -2.428E-02 8. 996E-02 9.062E-02 FAIL ABUN LU-176 5.709E-04 2.073E-02 2.073E-02 FAIL ABUN HF-181 6.843E+OO 6.445E+00 7.145E+OO FAIL ABUN TA-182 -1.754E-02 l.012E+OO 1. 012E+OO FAIL ABUN RE-183 -5.597E-01 7.127E-01 7. 561E-01 NOT IDENT. RE-184 l.302E+Ol 3.019E+Ol
  • 3.076E+Ol NOT IDENT. W-188 -2.242E+Ol 9.660E+Ol 9.713E+Ol FAIL ABUN IR-192 -l.148E-01 3.812E-01 3.847E-01 FAIL ABUN HG-203 4.076E-01 2.104E+OO 2 .112E+OO NOT IDENT. BI-207 7.335E-02 7.856li:-02 8.523E-02 FAIL ABUN PB-211 -5.729E-01 5.534E-01 6.107E-01 NOT IDENT. BI-212 7.749E-01 8.587E-01 9.270E-01 FAIL ABUN RN-219 9.840E-02 3.437E-01 3.466E-01 FAIL ABUN RA-223 -1.676E-01 4.942E-01 5.000E-01 FAIL ABUN AC-227 -l.276E-01 1.991E-01 2.072E-01 FAIL ABUN TH-227 -l.276E-01 1. 991E-01 2. 072E-01 FAIL ABUN TH-231 -1.676E-01 4.942E-01 5.000E-01 FAIL ABUN PA-233 -2.903E-02 5. ll 7E-02 5.282E-02 FAIL ABUN PA-234 -8.797E-02 2. 961E-01 2.988E-01 NOT IDENT. PA-234M 2.684E+OO 4.478E+OO 4.639E+OO NOT IDENT. NP-237 -2.903E-02 5. ll 7E-02 5.282E-02 FAIL ABUN NP-238 4.101E+40 6.210E+40 O.OOOE+OO SHORT HLIF NP-239 -1. 210E-01 l.708E-01 1. 7 93E-01 NOT IDENT. PU-239 5.042E+02 4.539E+02 5.077E+02 FAIL ABUN AM-241 5.032E-03 3.900E-02 3.907E-02 NOT IDENT. AM-243 1.656E-01 3.655E-02 8.313E-02 NOT IDENT. CM-243 -2.975E-02 6.175E-02 6.319E-02 NOT IDENT. BK-247 7 .139E-02 6.232E-02 7.014E-02 FAIL ABUN CM-247 5.325E-03 3 .109E-02 I 3 .118E-02 NOT IDENT. CF-249 9.598E-03 3. 311E-02 3.339E-02 NOT IDENT. CF-251 -2.393E-02 9.533E-02 9.594E-02 NOT IDENT. Page 4449 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 43.2225 87.09 76.7587 136.47 81. 2058 45.60 59.6870 87.57 76.8707 140.51 0.0000 46.54 59.9619 88.03 97.5052 143.76 68. 7161 49. 72 0.0000 88.34 97. 5965 144.24 68.7845 51. 35 74.7906 88.47 97.6348 145.44 73.5501 51. 87 70.4681 89. 96 84.8797 152.43 75.9177 52.39 66.8749 1093.63 85.0506 153.25 0.0000 52.97 67.0474 91.11 0.0000 323.87 61.1471 53.44 71. 7157 92.59 85.5377 156.02 0.0000 54.07 74.9415 93.35 85. 7258 158.56 0.0000 57.36 0.0000 94.56 86.0247 159.00 49.5720 57.53 90.6494 94.65 86.0465 162.33 66.1733 57.98 98.5142 94.67 86.0518 162.66 0.0000 59.27 83.5621 94.87 86.1007 163.33 58.1368 59.32 95 .1872 97.43 69.1454 165.86 80.9528 59.54 95.2726 98.43 52.8850 176.31 59.5127 60. 96 111.1378 98.44 52.8864 176.60 0.0000 61.17 111.2309 99.53 64.5389 177.52 66. 9619 62.93 96. 5634 100 .11 61. 9849 181.07 0.0000 63.29 96.6986 102.03 61.4189 181.52 68.8295 63.58 96.8069 103.18 75.0016 184.41 69.1679 64.28 97.0678 103.37 75.0400 143.76 64. 7222 66.73 100.8901 105.21 69.1227 193.51 62.3348 67.24 107.4656 105.31 69.1409 197.03 51. 8804 125.81 100.7129 106.12 65.6884 198.01 60. 6211 67.75 101. 5384 106.47 81. 9605 201.83 63.1658 69.67 115.9398 109.28 71. 6703 203.43 62.2324 70.83 122.8900 111. 00 77.4508 205.31 55.4793 72. 81 237.7312 111.76 0.0000 210.85 83.9252 72. 87 237.7802 114. 06 86.3084 215.65 60.0612 74.66 133. 2836 116. 30 0.0000 222 .11 57.2645 74.82 128.9833 116.74 81.3318 227.09 66.7216 74.97 118.1129 119. 76 65.1668 227.38 72.4063 77 .11 179.2810 121.12 78.4520 228.16 0.0000 78.74 78.6349 121. 22 78.4706 228.18 53.2336 79.69 85.5456 121. 78 73.8968 116. 74 53.2336 80.12 77.8777 122.06 74.8816 235.69 47.3092 80.19 0.0000 122.92 83.4735 235. 96 47.3268 80.57 86.9042 123.07 79.7498 238.63 48.2664 81. 00 94.5558 265.00 79.8626 238.98 0.0000 81. 07 94.5773 125.81 65.4634 240.99 48.4215 81. 75 83.8791 127.23 70.7263 242.00 48.4875 83.79 84.4223 127.91 67.0412 244.70 61. 7 952 84.00 90.1099 129.30 68.5195 252.40 0.0000 85.43 69.5810 131. 20 67.5364 252.80 57.3845 86.55 76.6324 133.02 78.6818 254.15 0.0000 86.79 76.6880 133.52 77.8075 256.23 49.4052 86.94 76.7237 136.00 77.2607 260.90 0.0000 Page 4450 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 35.6689 355.39 0.0000 584.27 14.6711 264.80 29.7295 356.01 26.2988 595.83 0.0000 265.00 28.5476 364.49 0.0000 427.87 26.4699 268.22 41.4005 366.42 0.0000 602.52 0.0000 269.46 43.0587 372.51 39.1866 604.72 23.8834 270.03
  • 43.0895 375.05 35.7088 607.14 27.6398 271.23 43.1532 377.52 37.5806 609.32 27.6779 273.65 0.0000 356.01 26.1007 610.33 27.6948 276.40 50.6633 388.16 29.8176 614.28 20.8211 277.37 50.7222 388.63 0.0000 618.01 25.6846 277.60 50.7363 391.69 41.6969 620. 36 30.0075 278.00 55.5950 264.66 29.2389 621. 93 15.0180 279.20 44.7821 401. 81 30.1835 630.19 0.0000 279.54 53.2759 402.40 30.1990 631.29 16.1816 279.70 53.2866 404.85 34.8496 633.25 30. 7811 280.46 41. 2134 410.95 36.8791 634.78 0.0000 283.69 34.0712 413. 71 29.5736 635.95 15.1444 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 45 .1141 423.72 0.0000 645.85 20.6730 285.90 0.0000 427.09 29.9108 657.76 18.6256 287.50 29.3350 427.87 23.3831 657.90 0.0000 290.67 37.6221 433.94 27.2613 661. 66 17.5690 293.27 0.0000 439.40 24.5506 664.57 0.0000 351. 93 19.7319 453.88 20.0618 666.33 0.0000 295.96 19.7485 463.37 27.9120 666.50 0.0000 879.38 24.7595 468.07 18.8371 667.71 0.0000 299.98 31. 4115 473.00 0.0000 677.62 14.4044 300.09 31.4154 475.06 24.2803 685.70 0.0000 300.13 31.4170 476.78 24.7981 695.00 0.0000 301.36 31. 4602 477.60 29.1925 696.49 23.5122 302.85 29.8542 482.18 20.5057 696. 51 23.5131 256.23 26.5859 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 20.1628 306.78 32.4841 497.08 31.1014 697.49 20.1643 308.46 36.7168 505.52 19. 3719 702.65 21. 3448 311. 90 45.2318 507.63 0.0000 706.68 25.3317 316.51 42.9327 511. 00 29.9207 711. 68 24.8359 319.41 0.0000 514.00 29.9841 720.70 0.0000 320.08 0.0000 514.00 29.9854 721. 93 0.0000 321.04 33.8371 520.40 16.0645 722.78 13.6270 323.87 37.3327 520.69 0.0000 722. 91 13.6279 325.23 45.8833 522.65 0.0000 723.31 13.6309 328.76 0.0000 527.90 0.0000 724.19 13.6372 333.37 39.8474 528.26 19.1825 727. 33 27.3193 333.97 30.8687 529.59 17.1785 733.00 15.0708 . 334.37 36.0280 529.87 0.0000 735.93 17.1515 338.28 26.6993 531. 02 0.0000 333.97 10.2993 338.32 26.6999 537.26 0.0000 739.50 0.0000 311. 90 26.7586 546.56 0.0000 747.24 12.6516 340.48 26.7586 552.55 25.6612 748.06 16.1089 340.55 0.0000 563.25 23.2599 752.31 13.8379 344.28 22. 0962 569.33 18.6826 753.82 0.0000 345.93 29.5100 946.00 20.2411 756.73 16.6430 351.06 29.6608 569.70 20.2443 756.80 16.6436 351.93 29.6864 583.19 14.6614 884.68 10.4399 Page 4451of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 6. 9663 1274.44 15.4409 1620.50 1. 8811 766.42 6. 9685 1001.03 12.5695 1621. 92 3.7635 766.84 6.9700 1002.74 11. 057 5 1678.03 0.0000 772.60 0.0000 1004.73 23.2390 1690.97 3.8291 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 8.7697 778.90 13.1474 1028.54 0.0000 1063.66 16.5883 783.70 0.0000 1037.84 12.7509 1771.35 7.8082 785.37 16.8826 1038.76 0.0000 1791.20 0.0000 792.07 0.0000 631.29 13.7778 1808.65 3.9383 794.95 14.1348 1048.07 0.0000 1810.72 0.0000 795.86 14 .1411 1049.04 18.7159 1836.06 3. 9631 810.06 10.6787 1050.41 9.8553 810.29 9.7898 1063.66 20.8000 344.28 9.7908 1077.00 0.0000 810.76 9.7922 1077.34 17.9198 815.77 0.0000 1085.87 7.9897 1048.07 0.0000 1093.63 21. 0320 832.01 17.9834 1099.45 15.0549 834.85 18.0072 1112. 07 15.1245 835.71 18.9153 1112.84 16.1367 836.80 0.0000 1115. 54 6.4609 846.75 0.0000 1120. 29 12.1348 846.77 18.1067 1120.55 12.1362 856.80 0.0000 1221.41 12.1392 860.56 9 .1107 1129. 67 11.1611 871. 09 19.0404 1131.51 0.0000 873.19 14.6602 1147.95 0.0000 875.33 0.0000 1173.23 24. 7251 879.38 14.7007 1177.95 14.4460 880.51 13.2372 1189.05 19.6796 883.24 13.2535 1204.77 20.8252 884.68 15.7879 1221.41 18.8470 889.28 19.3792 1231.02 13.6554 894.76 15. 7258 1235.36 0.0000 898.04 21. 3070 1238.28 24.2171 900.72 20.4041 1260.41 0.0000 903.28 16.9782 1271.87 10.6439 911. 20 13.9751 1274.44 10.6525 912.08 13.9806 1274.54 12.7837 923.98 0.0000 1291.59 9.6394 926.50 12.0039 1298.22 0.0000 929 .11 13.5193 1312 .11 0.0000 937.49 18.8434 1332.49 6.9422 944.13 0.0000 1362. 66 0.0000 946.00 17.9650 1365.19 8.7642 949.00 13.2536 1368.63 0.0000 667.71 0.0000 1384.29 3.3052 962. 31 20.9419 1408.01 7.7661 964.08 16.7659 1457.56 0.0000 966 .17 12.2039 1460.82 9.0107 911. 20 20.0445 1489.16 6.3574 968.97 20.0445 1505.03 7.2977 983.53 0.0000 1584.12 6.5218 984.45 0.0000 1596.21 0.0000 Page 4452 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:59:13.60 ********************************************************************************
  • GEL Laboratories LLC i
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM33.CNF;235 Background date : Z-OCT-2016 11:02:02. Sample date 14-DEC-2015 14:00:00 Acquisition date : 3-0CT-2016 05:57:37. Sample ID G405235066 Sample quantity 1.57422E+02 GRAM Detector name : GAM33 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.75 0.0% Energy tolerance : 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID : 1596254 Detector SN# : Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 2 2 0 0 0 0 0 0 0 0 0 0 0 0 4 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 1 1 0 0 Page 4453 of 5809 Energy 74.91* 77.25 87.89 93.42* 125.24 143.63* 186.03* 209.91 232.51 238.60* 241. 76 269.71 295.54 300.53 327.86* 332.76 338.30* 352.00* 403.07 479.37 482.57 493.30 511.28* 537.31 547.20 550.83 583.44* 609.29* 665.62 727.48 761. 4 7 768.68 781.60 822.07 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 77 157 65 92 25 36 88 49 23 292 98 57 205 27 25 26 80 256 8 12 7 16 27 18 13 16 134 181 66 30 16 22 18 10 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 158 131 258 176 45 103 81 96 45 139 80 82 67 42 45 28 23 27 45 47 25 20 80 29 15 15 24 43 20 19 24 26 9 13 1. 21 1. 22 1.16 1.16 0.94 1.16 1. 28 1. 09 0.97 1. 00 1. 44 1. 73 1. 28 1. 79 1. 91 1. 31 1. 38 1. 34 1. 03 3.51 1. 47 2.85 1. 90 0.55 0.76 1. 50 1. 52 1.19 4.94 0.73 1. 76 1. 77 1.12 0.85 149.90 154.58 175.82 186.86 250.43 287.15 371.86 419.56 464.70 476.88 483.18 539.02 590.63 600.60 655.21 665.00 676.08 703.46 805.49 957.98 964.37 985.82 1021.76 1073.78 1093.56 1100.81 1165.99 1217.67 1330.28 1453.95 1521.90 1536.32 1562.17 1643.08 145 145 171 182 249 283 368 415 462 473 481 533 585 598 646 646 646 700 800 945 960 980 1014 1066 1087 1098 1159 1211 1319 1449 1507 1507 1557 1636 15 2.14E-02 29.0 1.19E+OO 15 4.35E-02 15.3 11 1.80E-02 49.8 11 2;55E-02 32.0 4 6.95E-03 42.7 8 1.00E-02 54.3 8 2.44E-02 22.9 10 1.35E-02 40.5 6 6.26E-03 51.6 8 8.12E-02 9.3 6 2.72E-02 18.1 13 1. 60E-02 34. 9 13 5. 68E-02 11. 0 8 7.38E-03 45.9 37 7.03E-03 55.2 1.28E+OO 37 7.30E-03 41.0 37 2.21E-02 16.4 9 7.12E-02 7.3 10 2.33E-03150.6 14 3.44E-03122.5 8 1. 93E-03128. 9 11 4.34E-03 60.4 19 7.51E-03 90.0 14 5.06E-03 68.9 10 3. 67E-03 61. 2 7 4.55E-03 45.5 16 3.72E-02 12.2 14 5.03E-02 10.8 28 1.84E-02 23.0 10 8.44E-03 32.7 40 4.46E-03 62.3 2.89E+OO 40 6.19E-03 46.4 9 5.00E-03 38.2 9 2.77E-03 73.2 Peak Search Report (continued) Page : 2 Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 831.18 10 9 1. 62 1661.31 1656 9 2.77E-03 62.8 36 0 849.74 12 7 1. 61 1698. 41 1695 7 3.21E-03 48.4 37 0 861. 28 19 8 2.06.1721.49 1717 11 5.39E-03 36. 4 38 0 873.87 14 1 1.76 1746.67 1744 6 3.81E-03 30.2 39 0 911. 84* 75 43 1. 50 1822. 62 1815 17 2.09E-02 23.2 40 0 934.32 28 12 0.99 1867.57 1860 16 7.91E-03 32.9 41 0 964. 85 15 13 1. 04 1928.63 1925 8 4.23E-03 49.1 42 0 969.82* 49 30 1. 84 1938.57 1933 16 1.36E-02 28.7 43 0 1079.64 16 7 1. 58 2158. 25 2154 10 4.47E-03 40.2 44 0 1121.57* 16 27 1.67 2242.13 2233 12 4.51E-03 69.7 45 0 1209.50 16 22 3.74 2418.06 2408 18 4.39E-03 74.7 46 0 1225.89 11 5 1.39 2450.86 2448 7 3.12E-03 44.7 47 0 1279.54 10 7 1. 01 2558. 22 2552 10 2.88E-03 57.6 48 0 1295.04 11 6 3.42 2589.24 2582 11 2.92E-03 53.1 49 0 1378.23 12 3 1.29 2755.74 2750 9 3.46E-03 35.9 50 0 1461. 07* 356 4 1. 78 2921. 53 2914 17 9.90E-02 5.5 51 0 1764.76* 43 0 1.87 3529.59 3524 11 1.19E-02 16.0 Flag: "*" = Peak area was modified by background subtraction Page 4454 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 06:59:15 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 14-DEC-2015 14:00:00 G405235066 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 05:57:37 157.42 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA33 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4455 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.75 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10 ..c66* 1.133E+OO 1.363E+Ol l.363E+Ol 11. 0.2 OK CD-109 88.03 3.70* 4.949E+OO 8.003E-01 1.244E+OO 275.99 OK SN-126 64.28 9.60 2.578E+OO Line Not Found Absent 86.94 8.90 4.949E+OO 3.327E-01 3.327E-01 275.99 OK 87.57 37.00* 4.949E+OO 8.003E-02 8.003E-02 275.99 OK CS-135 268.22 16.00* 4.353E+OO 4.598E-01 4.598E-01 69.88 OK TL-208 277.37 6.60 4.258E+OO Line Not Found Absent 583.19 85.00* 2.333E+OO 3.468E-01 3.468E-01 24.30 OK 860.56 12.50 1. 726E+00 4.421E-01 4.421E-01 72. 71 OK PB-212 74.82 10.28 3.809E+OO 3.818E-01 3.818E-01 194.45 OK 77.11 17.10 4.047E+OO l.422E+OO 1.422E+OO 30.55 OK 238.63 43.60* 4.776E+OO 7.919E-01 7.919E-01 18.50 OK 300.09 3.30 3.995E+00 1. lllE+OO 1. lllE+OO 91. 90 OK BI-214 609.32 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 OK 1120.29 14.92 1.406E+OO 3.689E-01 3. 690E-0.l 139.45 OK 1764.49 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 OK PB-214 74.82 5.80 3.800E+OO Line Not Found <<INT Reject 77 .11 9.70 4.047E+OO 2.507E+00 2.508E+OO 30.55 OK 87.09 3.41 4.892E+OO Line Not Found <<INT Reject 242.00 7.25 4. 727E+OO Line Not Found <<INT Reject 295.22 18.42 4.049E+OO 1.515E+OO 1.516E+00 21. 95 OK 351.93 35.60* 3.512E+OO 1.112E+OO 1.112E+OO 14.65 OK RN-222 609.32 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 OK 1120.29 14.92 l.406E+OO 3.689E-01 3.690E-01 139.45 OK 1764.49 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 OK RA-224 240.99 4.10* 4.731E+OO l.683E-01 1.683E-01 703.88 OK RA-226 609.32 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 OK 1120. 29 14.92 1.406E+OO 3.689E-01 3.690E-01 139.45 OK 1764.49 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 OK AC-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11.27 3.628E+OO 1.061E+00 1. 061E+OO 32.79 OK 794.95 4.25 1.835E+OO Line Not Found Absent 835.71 1. 61 1. 766E+OO Line Not Found Absent 911.20 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 OK 968. 97 15.80 1. 57 5E+OO 9.513E-01 9.513E-01 57.44 OK RA-228 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.628E+OO 1.061E+OO 1.061E+OO 32.79 OK 794.95 4.25 1.835E+OO Line Not Found Absent 835.71 1. 61 1.766E+OO Line Not Found Absent 911.20 25.80* 1.652E+OO 8.612E-01 8.612E-01 46. 46 OK 968. 97 15.80 l.575E+00 9.513E-01 9.513E-01 57.44 OK TH-228 74.82 10.28 3.809E+OO 3.818E-01 3.818E-01 194.45 OK 77 .11 17.10 4.047E+OO 1.422E+OO 1.422E+OO 30.55 OK 238.63 43.60* 4.776E+OO 7.919E-01 7.919E-01 18.50 OK 300.09 3.30 3.995E+OO 1. lllE+OO 1. lllE+OO 91.90 OK TH-230 609.32 45.49* 2.255E+OO 9.030E-01 9.030E-01 21. 54 OK 1120.29 14.92 l.406E+00 3.689E-01 3.689E-01 139.45 OK 1764.49 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 OK PA-231 283.69 1. 70 4.183E+OO Line Not Found Absent Page 4456 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status .. 301.36 .5. 35* 3.995E+OO 6.853E-Oi 6.853E-01 91. 90 OK TH-232 105.21 1.10 5.839E+OO Line Not Found Absent 338.32 11. 27 3.628E+OO 1.061E+OO l.061E+OO 32.79 OK 835. 71 1. 61 1. 766E+OO Line Not Found Absent 911. 20 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 OK 968. 97 15.80 1.575E+OO 9.513E-01 9.513E-01 57.44 OK U-234 609.32 45.49* 2.255E+OO 9.030E-01 9.030E-01 21. 54 OK 1120.29 14.92 l.406E+OO 3.689E-01 3.689E-01 139.45 OK 1764.49 15.30 9.590E-01 1.318E+OO 1.318E+OO 31.95 OK U-235 89.96 3.47 5.092E+OO Line Not Found Absent 93.35 5.60 5.306E+OO 1.904E+OO 1.904E+OO 64.00 OK 143.76 10. 96* 6.182E+OO 3.160E-01 3.160E-01 108.58 OK 163.33 5.08 5. 963E+OO Line Not Found Absent 185.72 57.20 5. 613E+OO 1. 57 9E-01 1.579E-01 45.87 OK 205.31 5.01 5.295E+OO Line Not Found Absent AM-243 43.53 5.90 2.461E-01 Line Not Found Absent 74.66 67.20* 3.809E+OO 5.841E-02 5.842E-02 194.45 OK CM-247 278.00 3.40 4.251E+OO Line Not Found Absent 287.50 2 .*oo 4.139E+OO Line Not Found Absent 402.40 72.00* 3.142E+OO 1.980E-02 1. 980E-02 301.27 OK ANH-511 511. 00 100.00* 2.591E+OO 5.441E-02 5. 441E-02 179.92 OK Flag: "*" = Keyline Page 4457 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:59:16.99 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l *
  • Acquisition date 05:57:37 Sensitivity : 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 14-DEC-2015 14:00:00 Analyst initials: MXRl *
  • Sample ID G405235066 Sample Quantity 1.5742E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.363E+Ol 1.472E+OO CD-109 1.244E+OO 3.365E+OO SN-126 8.003E-02 2.165E-01 CS-135 4.598E-01 3.149E-01 TL-208 3.468E-01 8.259E-02 PB-212 7.919E-01 1.436E-01 BI-214 9.033E-01 l.907E-01 PB-214 l .112E+OO 1.597E-01 RN-222 9.033E-01 1.907E-01 RA-224 1.683E-01 1.161E+OO RA-226 9.033E-01 1.907E-01 AC-228 8.612E-01 3. 921E-01 RA-228 8.612E-01 3. 921E-01 TH-228 7.919E-01 1. 436E-01 TH-230 9.030E-01 1.906E-01 PA-231 6.853E-01 6.171E-01 TH-232 8.612E-01 3. 921E-01 U-234 9.030E-01 l.906E-01 U-235 3.160E-01 3.363E-01 AM-243 5.842E-02 l .113E-01 CM-247 l.980E-02 5.846E-02 ANH-511 5.441E-02 9.595E-02 Non-Identifie9 Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4458 of 5809 Key-Line Activity (pCi/GRAM -7.443E+OO 5.034E-03 0.000E+OO l.OOlE-02 -1.658E-02 0.000E+OO O.OOOE+OO -9.583E-03 K.L. Cnt Uncert ( 1. 96-sigma) 1.216E+Ol 3.635E-02 l.084E+41 2.018E-02 2.739E-01 8.568E+03 2.904E+02 7.195E-02 MDA (pCi/GRAM 5.902E-01 2.309E+OO l.495E-01 2.140E-01 5.293E-02 l.133E-01 9.393E-02 l.158E-01 9.393E-02 1.280E+OO 9.393E-02 2.092E-01 2.092E-01 l.133E-01 9.390E-02 6.582E-01 2.092E-01 9.390E-02 3.024E-01 9.349E-02 5.853E-02 5.050E-02 MDA (pCi/GRAM 1.933E+Ol 7.094E-02 O.OOOE+OO 5.505E-02 5.499E-01 O.OOOE+OO O.OOOE+OO l.188E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 9.684E-03 3.839E-01 6.840E-01 NOT IDENT. MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 3.917E-02 4.439E-02 9.045E-02 NOT IDENT. C0-58 3.632E-02 4.861E-01 9.623E-Ol NOT IDENT. FE-59 -1.466E+OO 4.479E+OO 8.864E+OO NOT IDENT. C0-60 -2.054E-03 3.394E-02 6.952E-02 NOT IDENT. ZN-65 8.785E-02 1.742E-01 3.432E-01 NOT 'IDENT. GE-68 -7.222E-02 2.336E+OO 4.200E+OO NOT IDENT. AS-73 -8.102E+OO 9.377E+OO 1. 747E+Ol NOT IDENT. AS-74 O.OOOE+OO

  • 4 .162E+03 O.OOOE+OO SHORT HLIF SE-75 4.292E-03 1. 801E-01 3.074E-01 NOT IDENT. BR-77 O.OOOE+OO 4.280E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.437E+02 0.000E+OO SHORT HLIF RB-83 -3.002E-01 6.108E-01 l.125E+OO NOT IDENT. KR-85 3.992E-01 6.342E+OO l.252E+Ol NOT IDENT. SR-85 3. 821E-02 6.279E-01 1.239E+OO NOT IDENT. RB-86 O.OOOE+OO 2.069E+04 O.OOOE+OO SHORT HLIF Y-88 -2.956E-03 l.405E-01 3.267E-01 NOT IDENT. Y-91 -8.607E+Ol 4.232E+02 7.321E+02 NOT IDENT. NB-94 1.978E-02 2.529E-02 5.579E-02 NOT IDENT. NB-95 3.569E-02 6.525E-01 1.295E+OO NOT IDENT. NB-95M -8.355E-02 2.648E+OO 3.860E+OO NOT IDENT. ZR-95 1.340E+OO 1.345E+OO 2.946E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 626E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.769E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF RH-101 -l.292E-02 3.346E-02 5.627E-02 NOT IDENT. RH-102 9.594E-03 5.214E-02 l.054E-01 NOT IDENT. RU-103 3. 710E+OO 4.479E+OO 9.260E+OO FAIL ABUN RH-106 -3.908E-02 4 .115E-01 8.046E-01 NOT IDENT. RU-106 -3.908E-02 4 .115E-01 8.046E-01 NOT IDENT. AG-108M -5.630E-03 2.295E-02 4.462E-02 NOT IDENT. AG-llOM -4.578E-02 8.237E-02 l.433E-01 NOT IDENT. SN-113 -9.855E-02 1. 996E-01 3.762E-01 NOT IDENT. CD-115 O.OOOE+OO 4.335E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 6.958E+04 O.OOOE+OO SHORT HLIF TE-123M -7.498E-02 l.300E-01 2.304E-01 NOT IDENT. SB-124 -3. 960E-01 1. 728E+OO 3.476E+OO NOT IDENT. SB-125 -4.793E-02 8.678E-02 1.618E-01 NOT IDENT. TE-125M 1.504E+02 2.528E+02 5.027E+02 NOT IDENT. I-126 O.OOOE+OO 1.505E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 7.793E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 6.305E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.421E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 9.296E+25 O.OOOE+OO SHORT HLIF BA-133 -5.271E-03 4.182E-02 7.372E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 3.738E-02 5.386E-02 1.113E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO l.999E+05 O.OOOE+OO SHORT HLIF BA-137M 4.766E-02 3.147E-02 7. 311E-02 NOT IDENT. CS-137 5.035E-02 3.325E-02 7. 724E-02 NOT IDENT. CE-139 3.106E-02 1.lOlE-01 2.090E-01 NOT IDENT. BA-140 O.OOOE+OO 1. 802E+06 O.OOOE+OO SHORT HLIF LA-140 0.000E+OO 2.768E+05 O.OOOE+OO SHORT HLIF CE-141 -3.102E+OO 1. 965E+Ol 3.367E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 727E+41 0.000E+OO SHORT HLIF CE-144 -8.942E-02 3.272E-01 6.048E-01 NOT IDENT. PM-144 -5. OllE-02 4. 621E-02 7.339E-02 NOT IDENT. PR-144 -4.339E+OO 4.00lE+OO 6.355E+OO NOT IDENT. PM-146 7.869E-03 4.209E-02 8.461E-02 NOT IDENT. ND-147 O.OOOE+OO 2 .171E+07 O.OOOE+OO SHORT HLIF PM-147 4.383E+02 7.779E+02 l.549E+03 NOT IDENT. 'PM-149 O.OOOE+OO 5.583E+39 0.000E+OO SHORT HLIF EU-150 4 .121E-02 3.312E-02 4.265E-02 FAIL ABUN EU-152 -l.339E-02 8.072E-02 l.523E-01 FAIL ABUN GD-153 -7.730E-02 1. 786E-01 3.028E-01 NOT IDENT. EU-154 2.384E-02 9.217E-02 l.843E-01 FAIL ABUN EU-155 8.918E-02 9.900E-02 2.042E-01 FAIL ABUN TB-160 -1. 679E+OO 1. 57 9E+OO 2.394E+OO FAIL ABUN H0-166M 3.825E-02 4.747E-02 1.048E-01 NOT IDENT. TM-171 -4.540E+OO 2.330E+Ol 4.649E+Ol NOT IDENT. HF-172 2.887E-01 2.414E-01 4.283E-01 FAIL ABUN LU-172 4.950E-02 7.020E-02 l.572E-01 FAIL ABUN LU-176 -l.364E-02 2.107E-02 3.977E-02 FAIL ABUN HF-181 2.028E+OO 5.125E+OO 7.441E+OO FAIL ABUN Page 4459 of 5809 TA-182 1.052E-01 1.00lE+OO 1. 788E+OO FAIL ABUN RE-183 1.676E+OO 3.108E+OO 6.473E+OO NOT IDENT. RE-184 8.704E-01 2.489E+Ol 4.835E+Ol NOT IDENT. W-188 -6. 511E+OO 1.029E+02 1.851E+02 NOT IDENT. IR-192 1. 746E-01 3.605E-01 7. 621E-01 FAIL ABUN HG-203 1.610E-01 2.000E+OO 4.038E+OO NOT I DENT'. BI-207 5.367E-03 3.978E-02 8.420E-02 FAIL ABUN PB-210 4.628E+OO 4.679E+OO 1.033E+Ol NOT IDENT. BI-211 O.OOOE+OO 4.400E-01 7.767E-01 FAIL ABUN PB-211 -9.432E-02 6,. 22 6E-01 l.093E+OO FAIL ABUN BI-212 1.163E+OO 7.461E-01 1.189E+OO FAIL ABUN RN-219 2.160E-01 6.377E-01 7.285E-01 FAIL ABUN RA-223 -2. 711E-01 5.497E-01 9.297E-01 FAIL ABUN AC-227 9.681E-02 2.199E-01 4.205E-01 FAIL ABUN TH-227 9.681E-02 2.199E-01 4.205E-01 FAIL ABUN TH-229 -4.881E-01 4.351E-01 7.145E-01 FAIL ABUN TH-231 -2. 711E-01 5.497E-01 9.297E-01 FAIL ABUN PA-233 1.288E-02 5.506E-02 1.123E-01 FAIL ABUN PA-234 -2.113E-01 2.665E-01 4.331E-01 FAIL ABUN PA-234M 3.533E+OO 4.433E+OO 9.538E+OO NOT IDENT. TH-234 -2.287E-01 1.460E+OO 2.912E+OO FAIL ABUN NP-237 1.288E-02 5.506E-02 .l.123E-01 FAIL ABUN NP-238 O.OOOE+OO 5.388E+40 O.OOOE+OO SHORT HLIF U-238 -2.287E-01 1.460E+OO 2.912E+00 FAIL ABUN NP-239 1.425E-01 2.245E-01 4.513E-01 NOT IDENT. PU-239 3.127E+02 3 .111E+02 6.297E+02 NOT IDENT. AM-241 6.229E-02 l.526E-01 3.129E-01 NOT IDENT. CM-243 -9.302E-02 9.417E-02 1.660E-01 NOT IDENT. BK-247 -2.424E-02 6.537E-02 1.043E-01 NOT IDENT. CF-249 -l.814E-02 3.201E-02 5.995E-02 FAIL ABUN CF-251 6.243E-02 l.047E-01 2.058E-01 NOT IDENT. Page 4460 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 06:59:14.34 Nuclide Line Activity Report Nuclide Type:*
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 345 10.66* 1.133E+OO l.363E+Ol 1.363E+Ol 11. 02 CD-109 88.03 84 3.70* 4.949E+OO 2.197E+OO 3.415E+OO 99.57 SN-126 64.28 ------9.60 2.578E+OO ------Line Not Found ------86.94 84 8.90 4.949E+OO 9.133E-01 9.133E-01 99.57 87.57 84 37.00* 4.949E+OO 2.197E-01 2.197E-01 99.57 CS-135 268.22 67 16.00* 4.353E+OO 4.598E-01 4.598E-01 69.88 TL-208 277.37 ------6.60 4.258E+OO ------Line Not Found ------583.19 144 85.00* 2.333E+OO 3.468E-01 3.468E-01 24.30 860.56 20 12.50 1. 726E+OO 4.421E-01 4.421E-01 72.71 BI-211 72.87 ------1. 23 3.591E+OO ------Line Not Found ------351.06 291 12.92* 3.512E+00 3.064E+00 3.064E+OO 14.65 PB-212 74.82 102 10.28 3.809E+OO 1.237E+OO 1.237E+OO 58.08 77 .11 206 17.10 4.047E+OO l.422E+OO 1.422E+00 30.55 238.63 346 43.60* 4.776E+OO 7.919E-01 7.919E-01 18.50 300.09 31 3.30 3.995E+OO 1. lllE+OO 1. lllE+OO 91. 90 BI-214 609.32 194 45.49* 2.255E+OO 9.030E-01 9.033E-01 21'.54 1120.29 16 14:92 1. 406E+OO, 3.689E-01 3.690E-01 139.45 1764.49 41 15.30 9.590E-01 1.318E+00 1.318E+OO 31. 95 PB-214 74.82 102 5.80 3.809E+OO 2.192E+OO 2.193E+OO 58.08 77 .11 206 9.70 4.047E+OO 2.507E+OO 2.508E+00 30.55 87.09 84 3.41 4.949E+OO 2.384E+OO 2.384E+OO 99.57 242.00 116 7.25 4. 731E+OO l.610E+OO 1. 611E+OO 36.10 295.22 237 18.42 4.049E+OO 1.515E+OO 1.516E+OO 21. 95 351. 93 291 35.60* 3.512E+OO 1.112E+OO 1.112E+OO 14.65 RN-222 609.32 194 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 1120.29 16 14.92 l.406E+OO 3.689E-01 3.690E-01 139.45 1764.49 41 15.30 9.590E-01 1.318E+OO l.318E+OO 31. 95 RA-224 240.99 116 4.10* 4. 731E+OO 2.848E+OO 2.848E+OO 36.10 RA-226 609.32 194 45.49* 2.255E+OO 9.030E-01 9.033E-01 21. 54 1120.29 16 14.92 l.406E+OO 3.689E-01 3.690E-01 139.45 1764.49 41 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 AC-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 91 11. 27 3.628E+OO 1.061E+OO 1.061E+OO 32.79 794.95 ------4.25 1.835E+OO ------Line Not Found ------835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 77 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 968.97 50 15.80 1. 57 5E+OO 9. 513E-01 9.513E-01 57.44 RA-228 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 91 11. 27 3.628E+OO 1.061E+OO 1.061E+OO 32.79 794.95 ------4.25 1.835E+OO ------Line Not Found ------835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911. 20 77 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 968. 97 50 15.80 1.575E+OO 9.513E-01 9.513E-01 57.44 TH-228 74.82 102 10.28 3.809E+OO 1.237E+00 l.237E+OO 58.08 77 .11 206 17.10 4.047E+OO l.422E+OO 1.422E+OO 30.55 238.63 346 43.60* 4.776E+OO 7.919E-01 7.919E-01 18.50 300.09 31 3.30 3.995E+OO 1. lllE+OO 1. lllE+OO 91. 90 Page 4461 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error TH-230 609.32 194 45.49* 2.255E+OO 9.030E-01 ,j 9.030E-01 21. 54 1120.29 16 14.92 1.406E+OO 3.689E-01 3.689E-01 139.45 1764.49 41 15.30 9.590E-01 1. 318E+OO 1.318E+00 31. 95 PA-231 283.69 ------1. 70 4.183E+OO ------Line Not Found ------301.36 31 5.35* 3.995E+OO 6.853E-01 6.853E-01 91. 90 TH-232 105.21 ------1.10 5.839E+OO ------Line Not Found ------338.32 91 11. 27 3.628E+OO 1.061E+OO 1.061E+OO 32.79 835.71 ------1. 61 1. 766E+OO ------Line Not Found ------911.20 77 25.80* 1.652E+OO 8.612E-01 8.612E-01 46.46 968.97 50 15.80 1.575E+OO 9.513E-01 9. 513E-01 57.44 U-234 609.32 194 45.49* 2.255E+OO 9.030E-01 9.030E-01 21.54 1120. 29 16 14.92 1.406E+OO 3.689E-01 3.689E-01 139.45 1764.49 41 15.30 9.590E-01 1.318E+OO 1.318E+OO 31. 95 U-235 89. 96 ------3.47 5.092E+OO ------Line Not Found ------93.35 119 5.60 5.306E+OO 1.904E+OO 1.904E+OO 64.00 143.76 45 10. 96* 6.182E+OO 3.160E-01 3.160E-01 108.58 163.33 ------5.08 5.963E+OO ------Line Not Found ------185. 72 106 57.20 5. 613E+OO 1.579E-01 1.579E-01 45.87 205.31 ------5. 01' 5.295E+OO ------Line Not Found ------AM-243 43.53 ------5.90 2.461E-01 ------Line Not Found ------74.66 102 67.20* 3.809E+OO 1. 892E-01 1.892E-01 58.08 CM-247 278.00 ------3.40 4. 251E+OO ------Line Not Found ------287.50 ------2.00 4.139E+00 ------Line Not Found ------402.40 9 72.00* 3.142E+OO 1.980E-02 1.980E-02 301.27 ANH-511 511.00 30 100.00* 2.591E+OO 5. 441E-02 5.441E-02 179.92 Flag: "*" Key line Page 4462of5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235066 Acquisition date 3-0CT-2016 05:57:37 Total number of lines in spectrum 51 Number of unidentified lines 15 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 CD-109 SN-126 CS-135 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 CM-247 ANH-511 Hlife 1.25E+09Y 461.40D 2.30E+05Y 2.30E+06Y 1.41E+l0Y 7.04E+08Y 1.41E+10Y 1600. OOY 1600. OOY 1600.00Y 1.41E+10Y 1600.00Y 1.41E+10Y 1. 41E+10Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 2.45E+05Y 7.04E+08Y 7370.00Y 1. 56E+07Y 1.00E+09Y Decay 1. 00 1. 55 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.363E+Ol 2.197E+OO 2.197E-01 4.598E-01 3.468E-01 3.064E+OO 7.919E-01 9.030E-01 1.112E+OO 9.030E-01 2.848E+OO 9.030E-01 8.612E-Ol 8.612E-01 7.919E-01 9.030E-01 6.853E-01 8.612E-01 9.030E-01 3.160E-01 1.892E-01 1. 980E-02 5. 441E-02 3.382E+Ol 3.382E+Ol
  • Decay Corr pCi7GRAM l.363E+Ol 3.415E+OO 2.197E-01 4.598E-01 3.468E-01 3.064E+OO 7.919E-01 9.033E-01 1.112E+OO 9.033E-01 2.848E+OO 9.033E-01 8.612E-01 8.612E-01 7.919E-01 9.030E-01 6.853E-01 8.612E-01 9.030E-01 3.160E-01 1.892E-01 l.980E-02 5.441E-02 3.504E+Ol 3.504E+Ol 70.59% Decay Corr 2-Sigma Error 0.150E+Ol 3.400E+OO 2.187E-01 3.213E-01 0.843E-01 0.449E+OO l.465E-01 l.946E-01 0.163E+OO l.946E-01 l.028E+00 1.946E-01 4.00lE-01 4.00lE-01 l.465E-01 1.945E-01 6.297E-01 4.00lE-01 1.945E-01 3. 431E-01 1.099E-01 5. 965E-02 9.790E-02 "M" Manually accepted 2-Sigma %Error 11. 02 99.57 99.57 69.88 24.30 14.65 18.50 21. 54 14.65 21. 54 36.10 21. 54 46.46 46.46 18.50 21. 54 91. 90 46.46 21. 54 108.58 58.08 301.27 179.92 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4463 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235066 Acquisition date : 3-0CT-2016 05:57:37 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 125.24 32 57 0.94 250.43 249 4 6.95E-03 85.3 6.21E+OO T 0 209.91 58 115 1. 09 419.56 415 10 1. 35E-02 80.9 5.22E+OO T 0 232.51 27 54 0.97 464.70 462 6 6.26E-03 **** 4.87E+OO 4 327.86 29 52 1. 91 655. 21. 646 37 7.03E-03 **** 3.72E+OO T 4 332.76 30 33 1. 31 665.00 646 37 7.30E-03 82.0 3.68E+OO T 0 479.37 14 51 3.51 957.98 945 14 3.44E-03 **** 2.73E+OO 0 482.57 8 28 1. 47 964.37 960 8 1. 93E-03 **** 2. 71E+OO T 0 493.30 17 22 2.85 985.82 980 11 4.34E-03 **** 2.67E+OO T 0 537.31 20 31 0.55 1073.78 1066 14 5.06E-03 **** 2.49E+OO T 0 547.20 14 16 0.76 1093.56 1087 10 3.67E-03 **** 2.45E+OO T 0 550.83 18 16 1. 50 1100.81 1098 7 4.55E-03 90.9 2.44E+OO 0 665.62 70 21 4.94 1330. 28 1319 28 1. 84E-02 46.0 2.lOE+OO T 0 727. 48 32 20 0.73 1453.95 1449 10 8.44E-03 65.5 1.97E+OO T 1 7 61. 4 7 17 25 1. 76 1521. 90 1507 40 4.46E-03 **** 1.90E+OO 1 768.68 23 27 1. 77 1536.32 1507 40 6.19E-03 92.9 1. 88E+OO 0 781. 60 19 9 1.12 1562.17 1557 9 5.00E-03 76.4 l.86E+00 0 822.07 10 14 0.85 1643.08 1636 9 2.77E-03 **** 1.79E+OO 0 831.18 10 9 1. 62 1661.31 1656 9 2.77E-03 **** 1.77E+OO T 0 849.74 12 8 1. 61 1698.41 1695 7 3. 21E-03 96. 8 l.74E+00 0 873.87 14 1 1. 76 1746.67 1744 6 3.81E-03 60.5 1. 71E+OO T 0 934.32 29 12 0.99 1867.57 1860 16 7.91E-03 65.9 l.62E+00 0 964.85 16 13 1. 04 1928.63 1925 8 4.23E-03 98.3 1.58E+OO T 0 1079.64 16 7 1. 58 2158.25 2154 10 4.47E-03 80.3 1.45E+OO 0 1209.50 16 22 3.74 2418.06 2408 18 4.39E-03 **** l.32E+00 0 1225.89 11 5 1. 39 2450.86 2448 7 3.12E-03 89.5 1.31E+OO 0 1279.54 10 7 1. 01 2558.22 2552 10 2.88E-03 **** 1.27E+OO 0 1295.04 10 5 3.42 2589.24 2582 11 2.92E-03 **** 1.25E+OO 0 1378.23 12 2 1. 29 2755.74 2750 9 3.46E-03 71. 9 1.19E+OO Flags: "T" = Tentatively associated Page 4464of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:59:28.94 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l *
  • Acquisition date 3-0CT-2016 05:57:37 Sensitivity 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 14-DEC-2015 14:00:00 Nuclide Library : SOLID *
  • Sample ID G405235066 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.5742E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 CS-135 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 CM-247 ANH-511 Le (pCi/GRAM 2. 413E-01 1.096E+OO 7.093E-02 9.730E-02 2.310E-02 5.339E-02 4.047E-02 5.248E-02 4.047E-02 6.051E-01 4.047E-02 8.915E-02 8.915E-02 5.339E-02 4.046E-02 2.973E-01 8.915E-02 4.046E-02 1.410E-01 4.399E-02 2.630E-02 2.267E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4465 of 5809 Le (pCi/GRAM 8.591E+OO 2.909E-02 0.000E+OO 2.061E-02 2.305E-01 O.OOOE+OO O.OOOE+OO 5.223E-02 2.893E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT.

MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4466 of 5809 O.OOOE+OO 4.246E-02 4.162E-01 3.644E+OO 2.884E-02 1.505E-01 1.803E+OO 8.016E+OO O.OOOE+OO 1.394E-01 O.OOOE+OO O.OOOE+OO 5.007E-01 5.630E+OO 5. 572E-01 O.OOOE+OO l.157E-01 3.047E+02 2.460E-02 5.632E-01 1. 793E+OO l.320E+00 O.OOOE+OO 0.000E+OO O.OOOE+OO O.OOOE+OO 2.620E-02 4.644E-02 4 .135E+OO 3.501E-01 3. 501E-01 l.980E-02 5.953E-02 l.692E-01 O.OOOE+OO O.OOOE+OO 1.077E-01 1. 336E+OO 7.168E-02 2.364E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.357E-02 O.OOOE+OO 5.012E-02 O.OOOE+OO O.OOOE+OO 3.300E-02 3.486E-02 9.816E-02 O.OOOE+OO O.OOOE+OO 1.562E+Ol O.OOOE+OO 2.820E-01 3.094E-02 2.679E+00 3.831E-02 0.000E+OO 7.260E+02 O.OOOE+OO l.938E-02 6.875E-02 1.413E-01 7.647E-02 9.576E-02 9.815E-01 4.627E-02 2.138E+Ol 2.009E-01 6.883E-02 l.804E-02 3.348E+OO 7.852E-01 SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF I DENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF *sHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237. NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CF-249 CF-251 Page 4467 of 5809 3.024E+OO 2. 091E+Ol 8.493E+Ol 3.474E-01 l.864E+00 3.600E-02 4.800E+OO 3.737E-01 4.898E-01 5.439E-01 3.319E-01 4.198E-01 l.944E-01 l.944E-01 3.290E-01 4.198E-01 5.164E-02 l.824E-01 4.261E+OO l.379E+OO 5.164E-02 O.OOOE+OO 1. 379E+OO 2 .114E-01 2.973E+02 l.465E-01 7.714E-02 4.699E-02 2.682E-02 9.599E-02 NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 06:59:34.59 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235066.CNF;l *
  • Acquisition date 3-0CT-2016 05:57:37 Sensitivity : 3.000 *
  • Detector ID GAM33 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.75 Half life ratio : ***** *
  • Sample date 14-DEC-2015 14:00:00 Nuclide Library : SOLID *
  • Sample ID G405235066 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity 1.5742E+02 GRAM *
  • Quantity Err(%) 1.2705E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 10-JUN-2016 07:00:49 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM33 CAN.CNF;8
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Nuclide (pCi/GRAM K-40 CD-109 SN-126 CS-135 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 U-234 U-235 AM-243 CM-247 ANH-511 1.363E+Ol l.244E+00 8.003E-02 4.598E-01 3.468E-01 7.919E-01 9.033E-01 l .112E+00 9.033E-01 1.683E-01 9.033E-01 8.612E-01 8.612E-01 7.919E-01 9.030E-01 6.853E-01 8.612E-01 9.030E-01 3.160E-01 5.842E-02 l.980E-02 5.441E-02 Act Error (1.96-sigma) 1.634E+OO 3.377E+00 2. l 72E-01 3.164E-01 8.389E-02 1. 496E-01 1.946E-01 1.662E-01 l.946E-01 1.174E+OO 1.946E-01 3.946E-01 3.946E-01 1. 496E-01 l.945E-01 6.342E-01 3.946E-01 1.945E-01 3.366E-01 l.126E-01 5.855E-02 9.597E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4468 of 5809 Key-Line Activity (pCi/GRAM -7.443E+OO 5.034E-03 1.000E+41 1.00lE-02 -1.658E-02 -2.537E+03 -5.744E+Ol -9.583E-03 K.L Act error ( 1. 96-sigma) 1.216E+Ol 3.635E-02 1.165E+41 2.019E-02 2.739E-01 8.568E+03 2.904E+02 7 .196E-02 TPU ( 1. 96-sigma) l.634E+00 3.377E+OO 2 .172E-01 3.164E-01 8.389E-02 1. 496E-01 l.946E-01 l.662E-01 l.946E-01 l.174E+OO 1.946E-01 3.946E-01 3.946E-01 1. 496E-01 1.945E-01 6.342E-01 3.946E-01 1.945E-01 3.366E-01 l.126E-01 5.855E-02 9.597E-02 TPU ( 1. 96-sigma) l.262E+Ol 3.642E-02 O.OOOE+OO 2,069E-02 2.740E-01 8.644E+03 2.915E+02 7.209E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 9.684E-03 3.839E-01 3.839E-01 NOT IDENT. MN-56 l.000E+41 2.699E+42 O.OOOE+OO SHORT HLIF C0-57 3.917E-02 4.443E-02 4. 781E-02 NOT IDENT. C0-58 3.632E-02 4.861E-01 4.864E-01 NOT IDENT. FE-59 -1. 466E+OO 4.480E+OO 4.529E+OO NOT IDENT. C0-60 -2.054E-03 3.394E-02 3.395E-02 NOT IDENT. ZN-65 8.785E-02 1. 742E-01 1.787E-01 NOT IDENT. GE-68 -7.222E-02 2.336E+OO 2.336E+OO NOT IDENT. AS-73 -8.102E+00 9.525E+OO l.020E+Ol NOT IDENT. AS-74 9.235E+02 4. l.63E+03 4.184E+03 SHORT HLIF SE-75 4.292E-03 1. 801E-01 1.801E-01 NOT IDENT. BR-77 2.360E+37 2.001E+38 O.OOOE+OO SHORT HLIF SR-82 3.193E+02 6.439E+02 6.597E+02 SHORT HLIF RB-83 -3.002E-01 6.122E-01 6.270E-01 NOT IDENT. KR-85 3.992E-01 6.342E+OO 6.344E+OO NOT IDENT. SR-85 3. 821E-02 6.279E-01 6.281E-01 NOT IDENT. RB-86 9.919E+03 2.069E+04 2. ll 7E+04 SHORT HLIF Y-88 -2.956E-03 1.405E-01 l.405E-01 NOT IDENT. Y-91 -8.607E+Ol 4.232E+02 4.250E+02 NOT IDENT. NB-94 l.978E-02 2.530E-02 2.682E-02 NOT IDENT. NB-95 3.569E-02 6.525E-01 6.527E-01 NOT IDENT. NB-95M -8.355E-02 2.648E+OO 2.648E+OO NOT IDENT. ZR-95 1.340E+OO 1.346E+OO 1.475E+OO NOT IDENT. NB-97 1.000E+41 1.627E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 2.008E+41 O.OOOE+OO SHORT HLIF M0-99 -2.504E+31 3.774E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 2. 972E+42 O.OOOE+OO SHORT HLIF RH-101 -l.292E-02 3.354E-02 3.405E-02 NOT IDENT. RH-102 9.594E-03 5.215E-02 5.233E-02 NOT IDENT. RU-103 3.710E+OO 4.483E+OO 4.784E+OO FAIL ABUN RH-106 -3.908E-02 4 .115E-01 4 .119E-01 NOT IDENT. RU-106 -3.908E-02 4.115E-01 4.119E-01 NOT IDENT. AG-108M -5.630E-03 2.295E-02 2.309E-02 NOT IDENT. AG-llOM -4.578E-02 8.240E-02 8.495E-02 NOT IDENT. SN-113 -9.855E-02 1. 996E-01 2.045E-01 NOT IDENT. CD-115 -2.108E+38 4.352E+38 O.OOOE+OO SHORT HLIF SN-ll 7M 1. 847E+04 6. 962E+04 7. 011E+04 SHORT HLIF TE-123M -7.498E-02 1.301E-01 l.344E-01 NOT IDENT. SB-124 -3.960E-01 1. 728E+OO 1.737E+OO NOT IDENT. SB-125 -4.793E-02 8.680E-02 8.945E-02 NOT IDENT. TE-125M 1. 504E+02 2.530E+02 2.619E+02 NOT IDENT. I-126 3.335E+06 1.569E+06 2.173E+06 SHORT HLIF SB-126 2.235E+05 7.803E+05 7.868E+05 SHORT HLIF SB-127 3 .196E+21 7.634E+21 O.OOOE+OO SHORT HLIF I-131 -1.141E+08 2. 421E+09 2.421E+09 SHORT HLIF I-132 1. 000E+41 1.824E+42 O.OOOE+OO SHORT HLIF TE-132 7.402E+25 9.752E+25 O.OOOE+OO SHORT HLIF BA-133 -5.271E-03 4.182E-02 4.189E-02 NOT IDENT. I-133 1.000E+41 3.070E+41 O.OOOE+OO SHORT HLIF CS-134 3.738E-02 5.388E-02 5.645E-02 NOT IDENT. I-135 l.000E+41 8.986E+41 O.OOOE+OO SHORT HLIF CS-136 -l.602E+05 2.007E+05 2.133E+05 SHORT HLIF BA-137M 4.766E-02 3.154E-02 3.816E-02 NOT IDENT. CS-137 5.035E-02 3.332E-02 4. 031E-02 NOT IDENT. CE-139 3.106E-02 l.103E-01 1.112E-01 NOT IDENT. BA-140 1. 335E+06 1.803E+06 1. 901E+06 SHORT HLIF LA-140 -3.256E+05 2. 772E+05 3.137E+05 SHORT HLIF CE-141 -3.102E+OO 1. 965E+Ol 1.970E+Ol NOT IDENT. CE-143 1.000E+41 1. 730E+41 O.OOOE+OO SHORT HLIF CE-144 -8.942E-02 3.272E-01 3.297E-01 NOT IDENT. PM-144 -5. OllE-02 4.631E-02 5.152E-02 NOT IDENT. PR-144 -4.339E+OO 4.005E+OO 4.457E+OO NOT IDENT. PM-146 7.869E-03 4.210E-02 4.225E-02 NOT IDENT. ND-147 5.131E+06 2. l 71E+07 2.183E+07 SHORT HLIF PM-147 4.383E+02 7. 781E+02 8.028E+02 NOT IDENT. PM-1'49 1. 719E+39 5.595E+39 o*. OOOE+OO SHORT HLIF EU-150 4.121E-02 3.316E-02 3.801E-02 FAIL ABUN EU-152 -l.339E-02 8.072E-02 8.095E-02 FAIL ABUN GD-153 -7.730E-02 l.787E-01 I.820E-01 NOT IDENT. EU-154 2.384E-02 9.217E-02 9.280E-02 FAIL ABUN EU-155 8.918E-02 9.920E-02 1.070E-01 FAIL ABUN TB-160 -1. 679E+OO 1.582E+OO 1.754E+OO FAIL ABUN H0-166M 3.825E-02 4.751E-02 5.055E-02 NOT IDENT. TM-171 -4.540E+OO 2.330E+Ol 2.339E+Ol NOT IDENT. HF-172 2.887E-01 2.459E-01 2.782E-Ol FAIL ABUN LU-172 4.950E-02 7.038E-02 7.383E-02 FAIL ABUN LU-176 -1.364E-02 2.107E-02 2.195E-02 FAIL ABUN HF-181 2.028E+OO 5.126E+OO 5.207E+OO FAIL ABUN Page 4469 of 5809 TA-182 1.052E-01 1.00lE+OO 1.002E+00 FAIL ABUN RE-183 1. 676E+OO 3 .119E+OO 3.209E+00 NOT IDENT. RE-184 8.704E-01 2.489E+Ol 2.489E+Ol NOT IDENT. W-188 -6. 511E+OO 1.029E+02 1.029E+02 NOT IDENT. IR-192 1. 746E-01 3.606E-01 3.691E-01 FAIL ABUN HG-203 1.610E-01 2.000E+OO 2.002E+OO NOT IDENT. BI-207 5.367E-03 3.978E-02 3.985E-02 FAIL ABUN PB-210 4.628E+OO 4.698E+OO 5.140E+OO NOT IDENT. BI-211 3.064E+OO 4.606E-01 1. 456E+OO FAIL ABUN PB-211 -9.432E-02 6.226,E-01 6. 241E-01 FAIL ABUN BI-212 l.163E+OO 7.484E-01 9.136E-01 FAIL ABUN RN-219 2.160E-01 6.383E-01 6.457E-01 FAIL ABUN RA-223 -2. 711E-01 5.500E-01 5.634E-01 FAIL ABUN AC-227 9. 681E-02 2.203E-01 2.245E-01 FAIL ABUN TH-227 9. 681E-02 2.203E-01 2.245E-01 FAIL ABUN TH-229 -4.881E-01 4.358E-01 4.882E-01 FAIL ABUN TH-231 -2.711E-01 5.500E-01 5.634E-01 FAIL ABUN PA-233 1.288E-02 5.506E-02 5.537E-02 FAIL ABUN PA-234 -2 .113E-01 3.598E-01 3. 722E-01 FAIL ABUN PA-234M 3.533E+OO 4.435E+OO 4.713E+OO NOT IDENT. TH-234 -2.287E-01 l.461E+OO 1.464E+OO FAIL ABUN NP-237 1.288E-02 5.506E-02 5.537E-02 FAIL ABUN NP-238 -2.737E+40 5.389E+40 O.OOOE+OO SHORT HLIF U-238 -2.287E-01 1.461E+OO 1.464E+OO FAIL ABUN NP-239 1.425E-01 2.248E-01 2.338E-01 NOT IDENT. PU-239 3.127E+02 3 .114E+02 3.418E+02 NOT IDENT. AM-241 6.229E-02 1.527E-01 1.552E-01 NOT IDENT. CM-243 -9.302E-02 9.457E-02 l.034E-01 NOT IDENT. BK-247 -2.424E-02 6.556E-02 6.646E-02 NOT IDENT. CF-249 -1.814E-02 3.204E-02 3.307E-02 FAIL ABUN CF-251 6.243E-02 l.050E-01 1.087E-01 NOT IDENT. Page 4470 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 55.1871 87.09 114.4678 136.47 67.9837 45.60 62.9993 87.57 114.5592 140.51 0.0000 46.54 39.5842 88.03 114. 6464 143.76 64.1632 49. 72 0.0000 88.34 114. 7049 144.24 61. 98 66 51. 35 49.5758 88.47 114.7292 145.44 59 .1187 51. 87 43.9083 89. 96 88.3109 152.43 72.6410 52.39 47.7835 1093.63 88.4080 153.25 0.0000 52.97 62.2008 91.11 0.0000 323.87 62. 7103 53.44 58.4355 92.59 64.6240 156.02 0.0000 54.07 45.0879 93.35 64.7020 158.56 0.0000 57.36 0.0000 94.56 64.8263 159.00 83.3166 57.53 63.7998 94.65 64.8354 162.33 65.5438 57.98 56.1207 94.67 64.8373 162.66 0.0000 59.27 63.0674 94.87 64.8578 163.33 90.5042 59.32 63.0741 97.43 73.4298 165.86 72.6035 59.54 63.1034 98.43 54 .1165 176.31 58.5018 60. 96 91.5297 98. 44' 54.1173 176.60 0.0000 61.17 84.7509 99.53 65.6748 177.52 51.6838 62.93 74.3043 100 .11 68. 8626 181.07 0.0000 63.29 87.0782 102.03 50.2273 181.52 77.2684 63.58 87.1295 103.18 62.8917 184.41 74.0254 64.28 89.2136 103.37 80.7339 143.76 78.7557 66.73 77.8283 105.21 60.9785 193.51 70.0287 67.24 77.9061 105.31 55.7298 197.03 69. 0965 125.81 77.9730 106.12 62 .1125 198.01 67.9900 67.75 75.0224 106.47 66.3574 201.83 62.3552 69.67 79.2651 109.28 64.5123 203.43 62.4498 70.83 66.2003 111. 00 79.5130 205.31 64.5280 72.81 93.0257 111. 76 0.0000 210.85 52.2043 72.87 93.0364 114. 06 67.0788 215.65 60.7757 74.66 85.0097 116. 30 0.0000 222 .11 58.7311 74.82 85.0350 116.74 58.7786 227.09 55.3774 74.97 85.0584 119. 76 74.0437 227.38 56.5956 77 .11 85.3891 121.12 68.8042 228.16 0.0000 78.74 77.9133 121.22 61. 2870 228.18 39.7651 79.69 72.6619 121. 78 51.6486 116.74 39.7651 80.12 63.2906 122.06 58.1265 235.69 58.2155 80.19 0.0000 122.92 66.0955 235.96 58.2290 80.57 70.0787 123.07 66.1086 238.63 89.1624 81. 00 79.5717 265.00 66.1620 238.98 0.0000 81. 07 79.5813 125.81 47.5973 240.99 99.8975 81. 75 85.0773 127.23 70.8051 242.00 52.0234 83.79 75.8897 127.91 78.0988 244.70 35.8462 84.00 75.9165 129.30 69.5449 252.40 0.0000 85.43 105.9971 131.20 64.2684 252.80 38 .1355 86.55 114.3652 133. 02 73.1504 254.15 0.0000 86.79 114.4105 133.52 69.9189 256.23 41. 9418 86.94 114. 4396 136. 00 71. 2316 260.90 0.0000 Page 4471 of 5809

ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY . MDA COUNTS 7 65. 81 12.8267 1274.44 10.3597 1620.50 5.0052 766.42 12.8291 1001.03 10.3740 1621. 92 5.0064 766.84 12. 8311 1002.74 17.2986 1678.03 0.0000 772.60 0.0000 1004.73' 19.6161 1690.97 5.0739 776.52 0.0000 507.63 0.0000 1750.46 0.0000 "739.50 0.0000 1025.87 o,. 0 0 00 1764.49 3.0862 778.90 16.1078 1028.54 0.0000 1063.66 7.2089 783.70 0.0000 1037.84 9.3190 1771.35 2.0601 785.37 14.5300 1038.76 0.0000 1791.20 0.0000 792.07 17.2611 631.29 9.6337 1808.65 1.0370 794.95 8.6390 1048.07 0.0000 1810.72 0.0000 795.86 18.3641 1049.04 18.4045 1836.06 2.0842 810.06 11. 9408 1050.41 12.2739 810.29 11.9417 1063.66 9.6794 344.28 13.0278 1077.00 0.0000 810.76 13.0293 1077.34 12.7187 815.77 0.0000 1085.87 8.0943 1048.07 0.0000 1093.63 9.7586 832.01 18.0449 1099.45 9.7740' 834.85 19.7036 1112. 07 13.3731 835. 71 19.7095 1112.84 16.0510 836.80 0.0000 1115. 54 11. 4227 846.75 0.0000 1120.29. 16.0829 846.77 9.8910 1120.55 16.0840 856.'80 0.0000 1221.41 12.8698 860.56 12.1438 1129. 67 11. 6448 871. 09 8.3081 1131. 51 0.0000 873.19 15.5193 1147.95 0.0000 875.33 0.0000 1173.23 10.8706 879.38 17.7715 1177.95 16.3257 880.51 10.0001 1189.05 11.8241 883.24 11.1210 1204.77 10. 2272 884.68 J,3. 3511 1221.41 16.1380 889.28 7.7998 1231.02 12.2550 894.76 11.1617 1235.36 0.0000 898.04 7.8215 1238.28 ii.0493 900.72 13.4194 1260.41 0.0000 903.28 13.4302 1271.87 4.6414 911.20 11. 2195 1274.44 5.9445 912.08 11.2227 1274.54 5.9445 923.98 0.0000 1291.59 14.9219 926.50 12.4001 1298.22 0.0000 929 .11 11.8463 1312 .11 0.0000 937.49 11. 87 66 1332.49 8.4743 944.13 0.0000 1362. 66 0.0000 946.00 18.1445 1365.19 5.6917 949.00 12.4856 1368.63 0.0000 667. 71 0.0000 1384.29 1. 9054 962.31 11.9659 1408.01 4.7888 964.08 8.5516 1457.56 0.0000 966 .17 6.8455 1460.82 6.7817 911.20 15.4149 1489.16 3.8984 968. 97 15.4149 1505.03 3. 9116 '983.53 0.0000 1584.12 4. 9692 ;*. 984.45 0.0000 1596.21 0.0000 Page 4473 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:00:03.63 ******************************************************************************** *

  • GEL LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235067.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM41.CNF;l19 Background date : Z-OCT-2016 11:02:18. Sample date 11-DEC-2015 11:30:00 Acquisition date : 3-0CT-2016 05:58:05. Sample ID G405235067 Sample quantity 1.58210E+02 GRAM Detector name : GAM41 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:05.88 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 5 5 1 1 1 0 0 0 0 0 0 0 4 4 1 1 6 6 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4474 of 5809 Energy 46.36* 63.36* 74.94* 77.28* 84.37* 87.42 89.99 92. 8 6* 108.64* 122.75 130.29 143.77* 185.75* 209.29 238.88* 242.00 270.56 277.33 295.55 300.50 339.27 352.36* 463.71* 484.21 511.76* 533.36 583.70* 610.08* 656.84 661.99* 680.22 714.94 727.83* 861. 59 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 10 68 208 317 44 94 82 83 23 27 25 18 99 57 313 113 45 34 115 32 77 213 23 9 22 28 76 127 30 21 30 14 39 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 138 157 133 145 97 130 123 155 77 89 152 168 125 78 40 50 37 30 53 70 48 62 29 45 15 18 21 31 4 6 12 21 15 10 1. 04 0.77 0.76 1.10 1. 37 1.18 1. 38 1. 06 1. 29 1. 67 0.60 0.61 1.15 0.93 1. 01 1. 75 1. 63 1. 63 1. 65 2. 67 1. 24 1. 40 1. 69 4.26 2.56 1. 91 1.16 1. 20 4.81 1. 69 1. 94 1. 55 1.21 0.65 93.03 127.01 150.15 154.84 169.01 175.10 180.25 185.99 217.53 245.75 260.83 287.78 371. 70 418.78 477.94 484.19 541.30 554.82 591.25 601.17 678.68 704.86 927.53 968.53 1023.62 1066.81 1167. 49 1220.24 1313.76 1324.07 1360.53 1429.97 1455.74 1723.29 89 123 147 147 166 166 166 183 215 241 254 282 366 414 474 474 534 534 585 585 674 699 920 956 1018 1060 1161 1213 1306 1321 1352 1423 1450 1716 9 2.82E-03225.4 7 1.88E-02 36.1 20 5.78E-02 10.6 2.56E+OO 20 8.80E-02 8.5 17 1.23E-02 41.4 4.30E+OO 17 2.61E-02 22.5 17 2.29E-02 22.4 8 2.32E-02 31.4 6 6.30E-03 66.8 8 7.54E-03 63.8 12 6.84E-03102.4 13 4.93E-03155.3 13 2.75E-02 26.3 10 1.59E-02 31.6 24 8.70E-02 6.5 1.44E+OO 24 3.14E-02 17.6 39 1.24E-02 30.8 2.82E+OO 39 9.50E-03 38.0 25 3.19E-02 15.2 2.44E+OO 25 8.91E-03 65.2 12 2.14E-02 21.6 14 5.92E-02 10.5 13 6.27E-03 55.7 16 2.58E-03163.1 11 6.09E-03 58.5 12 7.86E-03 35.4 12 2.llE-02 17.0 14 3.53E-02 13.1 15 8.44E-03 22.8 8 5.79E-03 31.6 16 8.36E-03 31.5 15 3.94E-03 77.1 12 1.08E-02 26.1 9 2.51E-03 73.5 Peak Search Report (continued) Page : 2 Sample ID : G405235067 Acquisition date 3-0CT-2016 05:58:05 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 912.10* 50 14 1. 65 1824.31 1819 10 l.38E-02 20.7 36 0 970.45* 32 37 2.02 1941. 03 1936 17 8.90E-03 46.0 37 0 1059.63 12 6 4.05 2119.42 2114 11 3.26E-03 54. 3 38 0 1071. 72 8 4 1. 03 2143.61 2140 6 2.12E-03 56.8 39 0 1120.90 21 13 0.67 2241. 98 2237 11 5.77E-03 40.8 40 0 1127. 20 20 12 6.46 2254.59 2247 16 5.46E-03 45.5 41 0 1142.06 10 8 0.90 2284.33 2278 10 2.65E-03 68.6 42 0 1170.74 12 3 3.30 2341.70 2335 12 3.41E-03 39.9 43 0 1202.84 11 13 0.73 2405.91 2400 13 3.06E-03 74.0 44 5 1318.88 8 3 1. 80 2638.06 2636 12 2.21E-03 41. 9 6.98E-01 45 5 1321. 68 12 2 2.43 2643.67 2636 12 3.37E-03 35.1 46 0 1455.16 5 2 1.19 2910.73 2906 8 l.39E-03 66.3 47 0 1461.81* 232 0 1. 46 2924.02 2916 15 6.44E-02 6.6 48 0 1766.28 26 7 1. 71 3533.27 3525 14 7.17E-03 29.4 Flag: "*" = Peak area was modified by background subtraction Page 4475 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:00:05 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235067.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID ll-DEC-2015 11:30:00 G405235067 Acquisition date : Sample quantity Sample geometry Detector geometry: 3-0CT-2016 05:58:05 158.21 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA41 0 01:00:00.00 1. 50 keV No Empirical 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4476of5809 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:05.88 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235067 Acquisition date 3-0CT-2016 05:58:05 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status K-40 14.60.82 10.66* 8.926E-01 l.120E+Ol 1.120E+Ol 13.29 OK C0-57 122.06 85.60* 6.593E+OO 2.890E-02 6.162E-02 127.57 OK 136.47 10.68 6.262E+OO Line Not Found Absent CD-109 88.03 3.70* 7.447E+OO 1.261E+OO 1.970E+OO 78.21 OK TE-125M 109.28 0.27* 6.943E+OO 7.351E+OO 2.647E+02 133.58 OK SN-126 64.28 9.60 7.794E+OO 5.773E-01 5.773E-01 72 .11 OK 86.94 8.90 7.447E+OO 5.244E-01 5.244E-01 78.21 OK 87.57 37.00* 7.447E+OO 1.261E-01 1.261E-01 78.21 OK BA-137M 661.66 89.90* 1.826E+00 6.412E-02 6.533E-02 63.26 OK CS-137 661.66 85.10* 1. 826E+00 6.773E-02 6.901E-02 63.26 OK TL-208 277.37 6.60 3.908E+OO 7.353E-01 7.353E-01 76.06 OK 583.19 85.00* 2.050E+00 2.228E-01 2.228E-01 34.08 OK 860.56 12.50 1.432E+OO 2.477E-01 2.477E-01 147.07 OK PB-210 46.54 4.25* 7.546E+OO 2.074E-01 2.127E-01 450.83 OK BI-211 72. 87 1. 23 7. 711E+OO Line Not Found Absent 351.06 12.92* 3.210E+OO 2.328E-01 2.328E-01 417.38 OK PB-212 74.82 10.28 7.682E+OO 1.135E+OO 1.135E+OO 34.02 OK 77 .11 17.10 7.644E+OO 1.520E+OO 1.520E+OO 17.07 OK 238.63 43.60* 4.383E+00 9. 221E-01 9.221E-01 13.08 OK 300.09 3.30 3.664E+OO 1.459E+OO 1.459E+OO 130.43 OK BI-214 609.32 45.49* 1. 969E+OO 7.239E-01 7. 241E-01 26.14 OK 1120.29 14.92 1.128E+OO 5.864E-01 5.866E-01 81. 62 OK 1764.49 15.30 7.620E-01 Line Not Found Absent PB-214 74.82 5.80 7.683E+OO Line Not Found <<INT Reject 77 .11 9.70 7.644E+OO 2.679E+OO 2.680E+OO 17.07 OK 87.09 3.41 7.454E+OO Line Not Found <<INT Reject 242.00 7.25 4.340E+OO Line Not Found <<INT Reject 295.22 18.42 3.714E+OO 9.238E-01 9.241E-01 30.44 OK 351.93 35.60* 3.214E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 1. 969E+OO 7.239E-01 7. 241E-01 26.14 OK 1120.29 14.92 1.128E+OO 5.864E-01 5.866E-01 81.62 OK 1764.49 15.30 7.620E-01 Line Not Found Absent RA-224 240.99 4.10* 4.340E+OO 1.934E+OO 1.934E+OO 69.81 OK RA-226 609.32 45.49* 1. 969E+OO 7.239E-01 7.241E-01 26.14 OK 1120.29 14.92 1.128E+OO 5.864E-01 5.866E-01 81.62 OK 1764.49 15.30 7.620E-01 Line Not Found Absent AC-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.315E+OO 1.122E+OO 1.122E+OO 43.21 OK 794.95 4.25 1.543E+OO Line Not Found Absent 835. 71 1. 61 1.473E+OO Line Not Found Absent 911.20 25.80* 1.360E+OO 6.909E-01 6.909E-01 41.42 OK 968. 97 15.80 1.285E+OO 7.632E-01 7.632E-01 91. 98 OK RA-228 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11.27 3.315E+OO 1.122E+OO 1.122E+OO 43.21 OK 794.95 4.25 1.543E+OO Line Not Found Absent 835.71 1. 61 1. 473E+OO Line Not Found Absent 911.20 25.80* 1.360E+OO 6.909E-01 6.909E-01 41. 42 OK 968. 97 15.80 1.285E+OO 7.632E-01 7.632E-01 91. 98 OK TH-228 74.82 10.28 7.682E+OO 1.135E+OO 1.135E+OO 34.02 OK Page 4477 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235067 Acquisition date 3-0CT-2016 05:58:05 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 77 *. 11 17.10 7.644E+OO 1.520E+OO l.520Et00 17.07 OK 238.63 43.60* 4.383E+OO 9. 221E-01 9.221E-01 13.08 OK 300.09 . 3. 30 3.664E+OO 1.459E+OO l.459E+OO 130.43 OK TH-229 85.43 14.70 7. 511E+OO 2.497E-01 2.497E-01 82.75 OK 88.47 24.00 7.447E+OO 1.945E-01 l.945E-01 78.21 OK 193.51 4.41* 5.088E+OO Line Not Found Absent 210.85 2.80 4.797E+OO Line Not Found Absent TH-230 609.32 45.49* 1. 969E+OO 7.239E-01 7.239E-01 26.14 OK 1120.29 14.92 l.128E+OO 5.864E-01 5.864E-01 81.62 OK 1764.49 15.30 7.620E-01 Line Not Found Absent PA-231 283.69 1. 70 3.838E+OO Line Not Found Absent 301.36 5.35* 3.664E+00 9.000E-01 9.000E-01 130.43 OK TH-232 105.21 1.10 7.028E+OO Line Not Found Absent 338.32 11. 27 3.315E+OO l.122E+OO 1.122E+OO 43.21 OK 835.71 1. 61 1.473E+OO Line Not Found Absent 911.20 25.80* 1.360E+OO 6.909E-01 6.909E-01 41. 42 OK 968. 97 15.80 1. 285E+OO 7.632E-01 7.632E-01 91. 98 OK TH-234 63. 29 3. 7*0* 7.794E+OO 1.498E+OO 1.498E+OO 72.11 OK 92. 59 4.23 7.325E+00 1. 661E+OO 1. 661E+OO 62.80 OK U-234 609.32 45.49* 1. 969E+OO 7.239E-01 7.239E-01 26.14 OK 1120.29 14.92 l.128E+OO 5.864E-01 5.864E-01 81. 62 OK 1764.49 15.30 7.620E-01 Line Not Found Absent U-235 89. 96 3.47 7.390E+00 1.986E+OO 1. 986E+OO 44.73 OK 93.35 5.60 7.325E+OO l.254E+00 l.254E+00 62.80 OK 143.76 10. 96* 6.093E+OO 1.572E-01 1.572E-01 310.61 OK 163.33 5.08 5.667E+OO Line Not Found Absent 185.72 57.20 5.228E+OO 1. 913E-01 1. 913E-01 52.56 OK 205.31 5.01 4.887E+OO Line Not Found Absent U-238 63.29 3.70* 7.794E+OO l.498E+00 1.498E+OO 72.11 OK 92.59 4.23 7.325E+OO 1.661E+OO 1. 661E+OO 62.80 OK AM-243 43.53 5.90 7.421E+OO Line Not Found Absent 74.66 67.20* 7.682E+OO 1.736E-01 1.736E-01 34.02 OK ANH-511 511. 00 100.00* 2. 311E+OO 4.929E-02 4.929E-02 117. 03 OK Flag: "*" = Keyline Page 4478of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:00:06.86 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * . 4 *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235067.CNF;l *
  • Acquisition date 3-0CT-2016 05:58:05 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
  • real time: O Half life ratio : *
  • Sample date 11-DEC-2015 11:30:00 Analyst initials: MXRl *
  • Sample ID G405235067 Sample Quantity 1.5821E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File . : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.120E+Ol 1.459E+OO C0-57 6.162E-02 7.703E-02 CD-109 1.970E+OO 1.510E+OO TE-125M 2.647E+02 3.466E+02 9.668E-02 BA-137M 6.533E-02 4.050E-02 CS-137 6.901E-02 4.278E-02 TL-208 2.228E-01 7.439E-02 PB-210 2.127E-01 9. 399E-01"' BI-211 2.328E-01 9. 521E-01 PB-212 9.221E-01 1.182E-01 BI-214 7. 241E-01 1.855E-01 PB-214 1.009E+OO 2.085E-01 RN-222 7.241E-01 l.855E-01 RA-224 1.934E+OO 1.323E+OO RA-226 7.241E-01 1.855E-01 AC-228 6.909E-01 2.805E-01 RA-228 6.909E-01 2.805E-01 TH-228 9.221E-01 1.182E-01 TH-229 -2.520E-01 4.320E-01 TH-230 7.239E-01 l.854E-01 PA-231 9.000E-01 1.150E+OO TH-232 6.909E-01 2.805E-01 TH-234 1.498E+OO 1.058E+OO U-234 7.239E-01 l.854E-01 U-235 1. 572E-01 4.786E-01 U-238 l.498E+OO 1.058E+OO AM-243
  • l.736E-01 5.788E-02 ANH-511 4.929E-02 5.653E-02 Non-Identified Nuclides Nuclide BE-7 Page 4479 of 5809 Key-Line Activity (pCi/GRAM -1.889E+OO K.L. Cnt Uncert ( 1. 96-sigrna) l.376E+Ol MDA (pCi/GRAM 6.988E-01 7.738E-02 l.481E+OO 4.037E+02 9.469E-02 3.484E-02 3.681E-02 6.020E-02 6.838E-01 3.580E-01 8.785E-02 1. 211E-01 3.241E-01 l.211E-01 9 .. 416E-01 1. 211E-01 2.554E-01 2.554E-01 8.785E-02 8.075E-01 l.211E-01 7.548E-01 2.554E-01 9.162E-01 1.211E'....Ol 3.320E-01 9.162E-01 5.389E-02 4.634E-02 MDA (pCi/GRAM 2.280E+Ol NOT IDENT.

NA-22 -2.462E-02 5.315E-02 9.581E-02 NOT IDENT. NA-24 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF AL-26 8.693E-04 1. 724E-02 4.787E-02 NOT IDENT. SC-46 6.380E-02 3.158E-01 6.845E-01 FAIL ABUN V-48 O.OOOE+OO l.094E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.056E+02 O.OOOE+OO SHORT HLIF MN-54 -5.215E-02 6.438E-02 l.128E-01 NOT IDENT. C0-56 -l.095E-01 4.586E-01 8.952E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF -C0-58 -1. 871E-02 6.181E-01. 1.238E+OO NOT IDENT. FE-59 3.198E+OO 5.907E+OO 1.338E+Ol NOT IDENT. C0-60 -3.032E-02 4.305E-02 7.252E-02 NOT IDENT. ZN-65 2.595E-01 1.927E-01 4.427E-01 NOT IDENT. GE-68 -1. 969E+OO 2.512E+OO 4.277E+OO NOT IDENT. AS-73 -l.159E-01 2.165E+OO 4.036E+OO NOT IDENT. AS-74 O.OOOE+OO 5.143E+03 O.OOOE+OO SHORT HLIF SE-75 1.035E-01 2.093E-01 3. 901E-01 NOT IDENT. BR-77 O.OOOE+OO 8.710E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.916E+02 O.OOOE+OO SHORT HLIF RB-83 -2.336E-01 5.900E-01 1.066E+OO NOT IDENT. KR-85 6.789E+00 8.319E+OO 1.581E+Ol NOT IDENT. SR-85 6.906E-01 8.508E-01 1.616E+OO NOT IDENT. RB-86 O.OOOE+OO 2.855E+04 O.OOOE+OO SHORT HLIF Y-88 6.631E-03 1. 686E-01 4.156E-01 NOT IDENT. Y-91 2.555E+02 6.723E+02 1.254E+03 NOT IDENT. NB-94 1.316E-03 3.469E-02 6.958E-02 NOT IDENT. NB-95 -8.016E-02 7.291E-01 1.466E+OO NOT IDENT. NB-95M 2.899E-01 2.157E+OO 3. 851E+OO NOT IDENT. ZR-95 5.122E-02 1.445E+OO 2.938E+OO NOT IDENT. NB-97 O.OOOE+OO 4.472E+40 O.OOOE+OO SHORT HLIF ZR-97 0.000E+OO 1.449E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 9.300E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF RH-101 l.038E-02 2.916E-02 5.473E-02 NOT IDENT. RH-102 3. 301E-03 6. OOlE-02 l.228E-01 NOT IDENT. RU-103 -2.782E+OO 5.290E+OO 9.339E+OO FAIL ABUN RH-106 -8.336E-02 4.480E-01 8.374E-01 NOT IDENT. RU-106 -8.336E-02 4.480E-01 8.374E-01 NOT IDENT. AG-108M -5.505E-03 2.352E-02 4.433E-02 NOT IDENT. AG-llOM 2.327E-02 1.036E-01 2. 231E-01 FAIL ABUN SN-113 -1.883E-02 2.125E-01 4.061E-01 NOT IDENT. CD-115 O.OOOE+OO l.617E+39 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 7.601E+04 O.OOOE+OO SHORT HLIF TE-123M -2.405E-02 1.206E-01 2.352E-01 NOT IDENT. SB-124 -5.155E-02 1.693E+OO 3.940E+00 NOT IDENT. SB-125 -3.137E-02 1.174E-01 2.155E-01 FAIL ABUN I-126 O.OOOE+OO 7.319E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.051E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.146E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.829E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. 948E+26 0.000E+OO SHORT HLIF BA-133 4.767E-03 4.588E-02 7.999E-02 FAIL ABUN I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 3.471E-02 4. 968E-02 l.102E-01 NOT IDENT. CS-135 7.849E-02 l.303E-01 2. 681E-01 NOT IDENT. I-135 O.OOOE+OO 1. 774E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.006E+05 O.OOOE+OO SHORT HLIF CE-139 -3.591E-02 1.008E-01 1.937E-01 NOT IDENT. BA-140 O.OOOE+OO 1.283E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.136E+05 0.000E+OO SHORT HLIF CE-141 2.541E+OO 2.167E+Ol 4.320E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -4.287E-03 3.443E-01 6.178E-01 NOT IDENT. PM-144 l.602E-02 6.033E-02 l.245E-01 NOT IDENT. PR-144 1. 705E+OO 5 .171E+OO l.077E+01 NOT IDENT. PM-146 -2.274E-02 4.022E-02 7 .112E-02 NOT IDENT. ND-147 O.OOOE+OO 3 .111E+07 O.OOOE+OO SHORT HLIF PM-147 -5.293E+02 8.555E+02 l.452E+03 NOT IDENT. PM-149 O.OOOE+OO 1.644E+40 O.OOOE+OO SHORT HLIF EU-150 -1.177E-04 2.422E-02 4.474E-02 FAIL ABUN EU-152 -2.768E-02 1.120E-01 1.847E-01 FAIL ABUN GD-153 -7.463E-02 1.388E-01 2.576E-01 NOT IDENT. EU-154 -4.760E-02 1.267E-01 2.335E-01 FAIL ABUN EU-155 6.449E-02 9.823E-02 l.876E-01 FAIL ABUN TB-160 4.565E-01 1.873E+OO 3.943E+OO FAIL ABUN H0-166M -2.157E-02 7.509E-02 1.253E-01 FAIL ABUN TM-171 1.387E+OO 5.056E+OO 9.653E+00 NOT IDENT. Page 4480 of 5809 HF-172 5.805E-02 2.498E-01 3.785E-01 FAIL ABUN LU-172 -1.890E-02 8.107E-02 1.558E-01 FAIL ABUN LU-176 -5.312E-03 2.280E-02 3.849E-02 FAIL ABUN HF-181 -4.713E-03 4.331E+OO 8.258E+OO NOT IDENT. TA-182 -6.420E-01 1.116E+OO 1.957E+OO FAIL ABUN RE-183 4.663E-01 1.020E+OO 1.959E+OO NOT IDENT. RE-184 5.259E+Ol 3.567E+Ol 8.327E+Ol NOT IDENT. W-188 -2.689E+OO 1.130E+02 l.957E+02 FAIL ABUN IR-192 3.864E-01 4.272E-01 9.067E-01 FAIL ABUN HG-203 l.482Et00 2. 211E+OO 4.557E+OO NOT IDENT. BI-207 -1.844E-02 3.889E-02 6.003E-02 FAIL ABUN PB-211 2.869E-02 6.683E-01 1.287E+OO NOT IDENT. BI-212 O.OOOE+OO 8.883E-01 1.521E+OO FAIL ABUN RN-219 8.025E-02 3.445E-01 6.876E-01 FAIL ABUN RA-223 -1.621E-01 5.794E-01 1.084E+OO FAIL ABUN AC-227 -1. 213E-01 2.188E-01 4.030E-01 FAIL ABUN TH-227 -1.213E-01 2.188E-01 4.030E-01 FAIL ABUN TH-231 -l.621E-01 5.794E-01 1.084E+OO FAIL ABUN PA-233 2.280E-02 5.585E-02 1.132E-01 FAIL ABUN PA-234 -6.323E-02 2.680E-01 5.236E-01 FAIL ABUN PA-234M -2.854E-01 4.223E+OO 8.354E+OO NOT IDENT. NP-237 2.280E-02 5.585E-02 1.132E-01 FAIL ABUN NP-238 O.OOOE+OO 1.275E+41 O.OOOE+OO SHORT HLIF NP-239 -4.410E-03 2.216E-01 4.420E-01 FAIL ABUN PU-239 3.638E+02 7.300E+02 5.759E+02 FAIL ABUN AM-241 1. 8 92E-02 5.751E-02 1.009E-01 NOT IDENT. CM-243 -6.583E-02 8. lllE-02 1. 546E-01 FAIL ABUN BK-247 l.824E-02 7. 491E-02' l.351E-01 FAIL ABUN CM-247 -1.947E-03 3.173E-02 6.094E-02 FAIL ABUN CF-249 2.034E-02 3.709E-02 7.582E-02 NOT IDENT. CF-251 -4.218E-02 1.064E-01 2.033E-01 NOT IDENT. Page 4481of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:00:04.44 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 225 10.66* 8.926E-01 1.120E+Ol 1.120E+Ol 13. 29 C0-57 122.06 34 85.60* 6.593E+OO 2.890E-02 6.162E-02 127.57 136.47 ------10.68 6.262E+OO ------Line Not Found ------CD-109 88.03 123 3.70* 7.447E+OO 2 .113E+OO 3.300E+OO 45.06 TE-125M 109.28 29 0.27* 6.943E+OO 7.351E+OO 2.647E+02 133.58 SN-126 64.28 91 9.60 7.794E+OO 5.773E-01 5.773E-01 72.11 86. 94 123 8.90 7.447E+OO 8.783E-01 8.784E-01 45.06 87.57 123 37.00* 7.447E+OO 2 .113E-01 2 .113E-01 45.06 BA-137M 661. 66 22 89.90* 1. 826E+OO 6.412E-02 6.533E-02 63. 26 CS-137 661.66 22 85.10* 1. 826E+OO 6.773E-02 6.901E-02 63. 26 TL-208 277.37 40 6.60 3.908E+00 7.353E-01 7.353E-01 76.06 583.19 82 85.00* 2.050E+OO 2.228E-01 2.228E-01 34.08 860.56 9 12.50 l.432E+OO 2.477E-01 2.477E-01 147.07 PB-210 46.54 14 4.25* 7.546E+OO 2.074E-01 2.127E-01 450.83 BI-211 72.87 ------1. 23 7. 711E+00 ------Line Not Found ------351.06 243 12.92* 3.210E+OO 2.778E+OO 2.778E+00 21.10 PB-212 74.82 276 10.28 7.682E+OO 1.656E+OO 1.656E+OO 21. 25 77 .11 419 17.10 7.644E+00 1.520E+OO l.520E+OO 17.07 238.63 371 43.60* 4.383E+OO 9.221E-01 9.221E-01 13. 08 300.09 37 3.30 3.664E+OO 1.459E+OO 1.459E+OO 130.43 BI-214 609.32 137 45.49* 1. 969E+OO 7.239E-01 7.241E-01 26.14 1120.29 21 14.92 1.128E+OO 5.864E-01 5.866E-01 81. 62 1764.49 ------15.30 7.620E-01 ------Line Not Found ------PB-214 74.82 276 5.80 7.682E+00 2.935E+00 2.936E+00 21. 25 77 .11 419 9.70 7.644E+OO 2.679E+00 2.680E+OO 17.07 87.09 123 3.41 7.447E+OO 2.292E+OO 2.293E+OO 45.06 242.00 134 7.25 4.340E+00 2.018E+00 2.018E+00 35.19 295.22 133 18.42 3.714E+OO 9.238E-01 9. 241E-01 30.44 351.93 243 35.60* 3.210E+OO 1.008E+OO 1.009E+OO 21.10 RN-222 609.32 137 45.49* 1. 969E+OO 7.239E-01 7. 241E-01 26.14 1120.29 21 14.92 l.128E+OO 5.864E-01 5.866E-01 81. 62 1764.49 ------15.30 7.620E-01 ------Line Not Found ------RA-224 240.99 134 4.10* 4.340E+OO 3.568E+OO 3.568E+OO 35.19 RA-226 609.32 137 45.49* 1. 969E+OO 7.239E-01 7.241E-01 26.14 1120. 29 21 14.92 l.128E+OO 5.864E-01 5.866E-01 81. 62 1764.49 ------15.30 7.620E-01 ------Line Not Found ------AC-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 88 11. 27 3.315E+OO l.122E+OO 1.122E+OO 43.21 794.95 ------4.25 1.543E+OO ------Line Not Found ------835.71 ------1. 61 l.473E+OO ------Line Not Found ------911.20 51 25.80* 1.360E+OO 6.909E-01 6.909E-01 41. 42 968. 97 33 15.80 1.285E+OO 7.632E-01 7.632E-01 91. 98 RA-228 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 88 11. 27 3.315E+00 1.122E+OO 1.122E+OO 43.21 794.95 ------4.25 1.543E+00 ------Line Not Found ------835. 71 ------1. 61 1.473E+OO ------Line Not Found ------911.20 51 25.80* l.360E+OO 6.909E-01 6.909E-01 41. 42 Page 4482 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235067 Acquisition date 3-0CT-2016 05:58:05 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error . 968. 97 33 15.80 1.285E+OO ,7. 632E-01 7.632E-01 91. 98 TH-228 74.82 276 10.28 7.682E+OO 1.656E+OO 1.656E+OO 21. 25 77.11 419 17.10 7.644E+OO 1.520E+OO 1. 520E+00 17.07 238.63 371 43.60* 4.383E+OO 9.221E-01 9.221E-01 13. 08 300.09 37 3.30 3.664E+OO 1.459E+OO 1.459E+OO 130.43 TH-229 85.43 58 14.70 7. 511E+OO 2.497E-01 2.497E-01 82.75 88.47 123 24.00 7.447E+OO 3.257E-01 3.257E-01 45.06 193.51 ------4.41* 5.088E+OO ------Line Not Found ------210.85 ------2.80 4.797E+OO ------Line Not Found ------TH-230 609.32 137 45.49* 1. 969E+OO 7.239E-01 7.239E-01 26.14 1120. 29 21 14.92 1.128E+OO 5.864E-01 5.864E-01 81. 62 1764.49 ------15.30 7.620E-01 ------Line Not Found ------PA-231 283.69 ------1. 70 3.838E+OO ------Line Not Found ------301.36 37 5.35* 3.664E+OO 9.000E-01 9.000E-01 130.43 TH-232 105.21 ------1.10 7.028E+OO ------Line Not Found ------338.32 88 11. 27 3.315E+OO 1.122E+OO 1.122E+OO 43.21 835.71 ------1. 61 1. 473E+OO ------Line Not Found ------911. 20 51 25.80* 1.360E+OO 6.909E-01 6.909E-01 41. 42 968.97 '33 15.80 1. 285E+OO 7.632E-01 7. 632E_..:01 91. 98 TH-234 63.29 91 3.70* 7.794E+OO 1.498E+OO 1. 498E+OO 72 .11 92.59 108 4.23 7.325E+OO 1.661E+OO 1.661E+OO 62.80 U-234 609.32 137 45.49* 1. 969E+OO 7.239E-01 7.239E-01 26 .14 1120.29 21 14.92 1.128E+OO 5.864E-01 5.864E-01 81.62 1764.49 ------15.30 7.620E-01 ------Line Not Found ------U-235 89.96 107 3.47 7.390E+OO 1.986E+OO 1.986E+OO 44.73 93.35 108 5.60 7.325E+OO 1.254E+OO 1.254E+OO 62.80 143.76 22 10. 96* 6.093E+OO 1. 572E-01 l.572E-01 310.61 163.33 ------5.08 5.667E+OO ------Line Not Found ------185.72 121 57.20 5.228E+OO l.913E-01 l.913E-01 52.56 205.31 ------5.01 4.887E+OO ------Line Not Found ------U-238 63.29 91 3.70* 7.794E+OO 1.498E+OO 1.498E+OO 72 .11 92.59 108 4.23 7.325E+OO 1.661E+OO 1.661E+OO 62.80 AM-243 43.53 ------5.90 7. 421E+OO ------Line Not Found ------74.66 276 67.20* 7.682E+OO 2.533E-01 2.534E-01 21. 25 ANH-511 511. 00 24 100.00* 2. 311E+OO 4.929E-02 4.929E-02 117. 03 Flag: "*" Key line Page 4483 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235067 Acquisition date 3-0CT-2016 05:58:05 Total number of lines in spectrum 48 Number of unidentified lines 15 Number of lines tentatively identified by NID 33 Nuclide Type : Nuclide K-40 C0-57 CD-109 TE-125M SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 271. 74D 461. 40D 57.40D 2.30E+05Y 30.08Y 30.08Y 1.41E+10Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600.00Y 1600.00Y 1.41E+l0Y 1600.00Y 1.41E+10Y 1. 41E+10Y 1. 41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 2.13 1. 56 36.0 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00' 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.120E+Ol 2.890E-02 2 .113E+OO 7.351E+OO 2 .113E-01 6.412E-02 6.773E-02 2.228E-01 2.074E-01 2.778E+OO 9. 221E-01 7.239E-01 1.008E+OO 7.239E-01 3.568E+00 7.239E-01 6.909E-01 6.909E-01 9. 221E-01 3.257E-01 7.239E-01 9.000E-01 6.909E-01 1. 498E+OO 7.239E-01 1.572E-01 l.498E+00 2.533E-01 4.929E-02 4.104E+Ol 4.104E+Ol Decay Corr pCi/GRAM 1.120E+Ol 6.162E-02 3.300E+OO 2.647E+02 2 .113E-01 6.533E-02 6.901E-02 2.228E-01 2.127E-01 2.778E+OO 9.221E-01 7. 241E-01 1.009E+OO 7. 241E-01 3.568E+00 7. 241E-01 6.909E-01 6.909E-01 9. 221E-01 3.257E-01 7.239E-01 9.000E-01 6.909E-01 1.498E+OO 7.239E-01 1. 572E-01 l.498E+00 2.534E-01 4.929E-02 2.997E+02 2.997E+02 68.75% Decay Corr 2-Sigma Error 0.149E+Ol 7.860E-02 1.487E+OO 3.536E+02 0.952E-01 4 .133E-02 4.366E-02 0.759E-01 9.591E-01 0.586E+OO l.206E-01 l.893E-01 0.213E+OO 1.893E-01 1.256E+OO l.893E-01 2.862E-01 2.862E-01 l.206E-01 1.468E-01 l.892E-01 11.74E-01 2.862E-01 1.080E+OO 1. 892E-01 4.883E-01 1.080E+OO 0.538E-01 5.769E-02 "M" Manually accepted 2-Sigma %Error 13.29 127.57 45.06 133.58 45.06 63.26 63. 26 34.08 450.83 21.10 13.08 26.14 21.10 26.14 35.19 26.'14 41. 42 41. 42 13. 08 45.06 26.14 130. 43 41. 42 72.11 26.14 310.61 72.11 21. 25 117.03 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4484 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235067 Acquisition date : 3-0CT-2016 05:58:05 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 130.29 31 192 0.60 260.83 254 12 6.84E-03 **** 6. 41E+OO T 0 209.29 69 93 0.93 418.78 414 10 1. 59E-02 63.3 4.82E+OO 1 270.56 52 43 1. 63 541.30 534 39 l.24E-02 61. 6 3.98E+OO T 0 463.71 25 32 1. Q9 927.53 920 13 6.27E-03 **** 2. 53E+OO, T 0 484.21 10 49 4. 26 968. 53 956 16 2.58E-03 **** 2.43E+OO 0 533.36 31 19 1. 91 1066.81 1060 12 7.86E-03 70.7 2.23E+OO 0 656.84 32 4 4.81 1313.76 1306 15 8.44E-03 45.6 1.84E+OO T 0 680.22 32 13 1. 94 1360.53 1352 16 8.36E-03 63.0 1.78E+OO 0 714. 94 15 22 1. 55 1429.97 1423 15 3.94E-03 **** 1. 70E+OO 0 727. 83 41 16 1. 21 1455.74 1450 12 1. OBE-02 52.2 1. 67E+OO T 0 1059.63 12 6 4.05 2119.42 2114 11 3.26E-03 **** 1.19E+OO 0 1071.72 8 4 1. 03 2143.61 2140 6 2.12E-03 **** 1.17E+OO 0 1127.20 20 12 6.46 2254.59 2247 16 5.46E-03 91. 0 l.12E+OO 0 1142.06 10 8 0.90 2284.33 2278 10 2.65E-03 **** 1. llE+OO 0 1170.74 12 3 3.30 2341.70 2335 12 3.41E-03 79.9 1. 08E+OO 0 1202.84 11 13 0.73 2405.91 2400 13 3.06E-03 **** 1. 06E+OO 5 1318.88 8 3 1. 80 2638.06 2636 12 2. 21E-03 83.7 9.76E-01 5 1321.68 12 2 2.43 2643.67 2636 12 3.37E-03 70.3 9.74E-01 0 1455.16 5 2 1.19 2910.73 2906 8 l.39E-03 **** 8.96E-01 0 1766.28 24 7 1. 71 3533.27 3525 14 7.17E-03 58.7 7.61E-01 Flags: "T" = Tentatively associated Page 4485 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:00:20.59 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* ' *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235067.CNF;l *
  • Acquisition date 3-0CT-2016 05:58:05 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:05.88 Half life ratio : ***** *
  • Sample date 11-DEC-2015 11:30:00 Nuclide Library : SOLID *
  • Sample ID G405235067 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.5821E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 C0-57 CD-109 TE-125M SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.814E-01 3.609E-02 7. OllE-01 1.886E+02 4.482E-02 l.331E-02 l.406E-02 2.630E-02 3.193E-01 1.628E-01 4.038E-02 5.316E-02 1.562E-01 5.316E-02 4.328E-01 5.316E-02 1. 090E-01 1.090E-01 4.038E-02 3.734E-01 5.314E-02 3.429E-01 l.090E-01 4.338E-01 5.314E-02 l.557E-01 4.338E-01 2.560E-02 2.029E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 Page 4486 of 5809 Le (pCi/GRAM 1.016E+Ol NOT IDENT. 3.988E-02 NOT IDENT.

NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN..,.ll 7M TE-123M SB-124 SB-125 I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 Page 4487 of 5809 O.OOOE+OO 1.529E-02 2.873E-01 O.OOOE+OO O.OOOE+OO 4.776E-02 3.828E-01 O.OOOE+OO 5.396E-01 5.666E+OO 2.879E-02 1.949E-01 1.768E+OO 1.904E+OO O.OOOE+OO 1. 7 93E-01 O.OOOE+OO O.OOOE+OO 4.623E-01 7.204E+OO 7.363E-01 O.OOOE+OO 1.473E-01 5.473E+02 3.097E-02 6.301E-01 1.772E+OO 1.283E+OO 0.000E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 551E-02 5.420E-02 4.087E+OO 3.587E-01 3.587E-01 l.940E-02 9.685E-02 l.820E-01 O.OOOE+OO O.OOOE+OO 1. 096E-01 1.446E+OO 9.763E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.641E-02 O.OOOE+OO 4.854E-02 1.235E-01 O.OOOE+OO 0.000E+OO 9.007E-02 O.OOOE+OO O.OOOE+OO 2.029E+Ol O.OOOE+OO 2.888E-01 5.555E-02 4.803E+OO 3 .114E-02 O.OOOE+OO 6.809E+02 O.OOOE+OO 2.025E-02 8.433E-02 1.210E-01 9.703E-02 8.857E-02 1. 705E+OO 5.549E-02 4.567E+OO 1. 766E-01 SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT.IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4488 of 5809 6.575E-02 1.724E-02 3.694E+OO 8.395E-01 9.300E-01 3.745E+Ol 8.936E+Ol 4.157E-01 2.102E+OO 2 . .247E-02 5.815E-01 7.015E-01 3.084E-01 4.930E-01 1.843E-01 l.843E-01 4.930E-01 5.166E-02 2.203E-01 3.553E+00 5.166E-02 O.OOOE+OO 2. 081E-01 2. 710E+02 4.796E-02 7.255E-02 6.200E-02 2. 722E-02 3.447E-02 9.429E-02 FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:00:27.59 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * " .
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235067.CNF;l *
  • Acquisition date 3-0CT-2016 05:58:05 Sensitivity : 3.000 *
  • Detector ID GAM41 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:05.88 Half life ratio : ***** *
  • Sample date 11-DEC-2015 11:30:00 Nuclide Library : SOLID *
  • Sample ID G405235067 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.5821E+02 GRAM *
  • Quantity Err(%) : 1.2641E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 26-JAN-2016 06:01:47 Eff. Geometry : 'CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM41 CAN.CNF;3
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.120E+Ol 1. 744E+OO 1. 744E+OO C0-57 6.162E-02 7.737E-02 7.737E-02 CD-109 1. 970E+OO 1.538E+OO 1.538E+OO TE-125M 2.647E+02 3.478E+02 3.478E+02 SN-126 1. 261E-01 9. 821E-02 9.821E-02 BA-137M 6.533E-02 4.085E-02 4.085E-02 CS-137 6.901E-02 4.315E-02 4.315E-02 TL-208 2.228E-01 7.679E-02 7.679E-02 PB-210 2.127E-01 9.403E-01 9.403E-01 BI-211 2.328E-01 1.002E+OO 1.002E+00 PB-212 9.221E-01 1. 470E-01 l.470E-01 BI-214 7. 241E-01 l.953E-01 1.953E-01 PB-214 1.009E+OO 2.256E-01 2.256E-01 RN-222 7.241E-01 1.953E-01 1.953E-01 RA-224 1.934E+OO 1.352E+OO 1.352E+OO RA-226 7. 241E-01 l.953E-01 1.953E-01 AC-228 6.909E-01 2.922E-01 2.922E-01 RA-228 6.909E-01 2.922E-01 2.922E-01 TH-228 9.221E-01 1.470E-Ol 1.470E-01 TH-229 -2.520E-01 4.327E-01 4.327E-01 TH-230 7.239E-01 1.953E-01 1.953E-01 PA-231 9.000E-01 1.168E+OO 1.168E+OO TH-232 6.909E-01 2.922E-01 2.922E-01 TH-234 1.498E+OO 1.121E+OO 1.121E+OO U-234 7.239E-01 1.953E-01 1. 953E-01' U-235 1. 572E-01 4.789E-Ol 4.789E-01 U-238 l.498E+OO 1.121E+OO 1.121E+OO AM-243 1.736E-01 6.234E-02 6.234E-02 ANH-511 4.929E-02 5.669E-02 5.669E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.889E+OO 1.376E+Ol 1. 379E+Ol NOT IDENT. Page 4489 of 5809 NA-22 -2.462E-02 5.319E-02 5.434E-02 NOT IDENT. NA-24 -l.OOOE+41 3.243E+41 O.OOOE+OO SHORT HLIF AL-26 8.693E-04 1.724E-02 l.725E-02 NOT IDENT. SC-46 6.380E-02 3.158E-01 3.171E-01 FAIL ABUN V-48 -1. 470E+03 1.094E+04 1. 096E+04 SHORT HLIF CR-51 -1.358E+02 4.058E+02 4.104E+02 SHORT HLIF MN-54 -5.215E-02 6.460E-02 6.875E-02 NOT IDENT. C0-56 -l.095E-01 4.587E-01 4.614E-01 NOT IDENT. MN-56 -l.OOOE+41 4.343E+41 O.OOOE+OO SHORT HLIF .co-58 -1.871E-02 6.181E-01 6.182E-01 NOT IDENT. FE-59 3.198E+OO 5.936E+OO 6.109E+OO NOT IDENT. C0-60 -3.032E-02 4. 311E-02 4.523E-02 NOT IDENT. ZN-65 2.595E-01 1.983E-01 2.302E-01 NOT IDENT. GE-68 -1. 969E+OO 2.533E+OO 2.684E+OO NOT IDENT. AS-73 -l.159E-01 2.165E+OO 2.165E+OO NOT IDENT. AS-74 2.401E+03 5.150E+03 5.262E+03 SHORT HLIF SE-75 l.035E-01 2.095E-01 2.146E-01 NOT IDENT. BR-77 6.797E+37 5.823E+38 O.OOOE+OO SHORT HLIF SR-82 -5.021E+Ol 5.916E+02 5.920E+02 SHORT HLIF RB-83 -2.336E-01 5. 911E-01 6.004E-01 NOT IDENT. KR-85 6.789E+00 8.340E+OO 8.884E+OO NOT IDENT. SR-85 6.906E-01 8.528E-01 9.079E-01 NOT IDENT. RB-86 -2.624E+04 2.889E+04 3 .121E+04 SHORT HLIF Y-88 6.631E-03 1. 68 6E-01 1.687E-01 NOT IDENT. Y-91 2.555E+02 6.726E+02 6.824E+02 NOT IDENT. NB-94 l.316E-03 3.469E-02 3.469E-02 NOT IDENT. NB-95 -8.016E-02 7.291E-01 7.300E-01 NOT IDENT. NB-95M 2.899E-01 2.157E+OO 2.161E+OO NOT IDENT. ZR-95 5.122E-02 1.445E+OO 1.445E+OO NOT IDENT. NB-97 1.000E+41 4.547E+40 O.OOOE+OO SHORT HLIF ZR-97 -1.000E+41 1. 451E+41 0.000E+OO SHORT HLIF M0-99 1.673E+31 9.302E+31 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 8.210E+41 O.OOOE+OO SHORT HLIF RH-101 l.038E-02 2.924E-02 2.961E-02 NOT IDENT. RH-102 3.301E-03 6. OOlE-02 6.003E-02 NOT IDENT. RU-103 -2.782E+OO 5.296E+OO 5.442E+OO FAIL ABUN RH-106 -8.336E-02 4.481E-01 4. 496E-01 NOT IDENT. RU-106 -8.336E-02 4.481E-01 4. 496E-01 NOT IDENT. AG-108M -5.505E-03 2.352E-02 2.365E-02 NOT IDENT. AG-llOM 2.327E-02 1. 036E-01 1. 041E-01 FAIL ABUN SN-113 -1.883E-02 2.125E-01 2.127E-01 NOT IDENT. CD-115 -6.921E+38 1.623E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 2.576E+02 7. 601E+04 7. 601E+04 SHORT HLIF TE-123M -2.405E-02 1. 207E-01 l.212E-01 NOT IDENT. SB-124 -5.155E-02 1.693E+OO 1.694E+OO NOT IDENT. SB-125 -3.137E-02 1.174E-01 l.182E-01 FAIL ABUN I-126 l.052E+06 7.491E+05 8.866E+05 SHORT HLIF SB-126 3.624E+05 l.054E+06 l.067E+06 SHORT HLIF SB-127 6.846E+20 1.149E+22 0.000E+OO SHORT HLIF I-131 -1.144E+09 3.830E+09 3.865E+09 SHORT HLIF I-132 1.000E+41 1.845E+42 O.OOOE+OO SHORT HLIF TE-132 3.680E+25 1.954E+26 O.OOOE+OO SHORT HLIF BA-133 4.767E-03 4.588E-02 4.593E-02 FAIL ABUN I-133 -l.000E+41 9.978E+41 O.OOOE+OO SHORT HLIF CS-134 3.471E-02 4.979E-02 5.219E-02 NOT IDENT. CS-135 7.849E-02 1.305E-01 l.353E-01 NOT IDENT. I-135 -1.000E+41 6.937E+41 O.OOOE+OO SHORT HLIF CS-136 -9.018E+03 3.006E+05 3.007E+05 SHORT HLIF CE-139 -3.591E-02 1. OllE-01 l.024E-01 NOT IDENT. BA-140 -9.103E+05 1. 2 8 5E+O 6 l.349E+06 SHORT HLIF LA-140 l.562E+05 4.138E+05 4.198E+05 SHORT HLIF CE-141 2.541E+00 2.167E+Ol 2.170E+Ol NOT IDENT. CE-143 -l.OOOE+41 2.068E+42 O.OOOE+OO SHORT HLIF CE-144 -4.287E-03 3.443E-01 3.443E-01 NOT IDENT. PM-144 1.602E-02 6.035E-02 6.078E-02 NOT IDENT. PR-144 *1. 705E+00 5.173E+OO 5.230E+OO NOT IDENT. PM-146 -2.274E-02 4.029E-02 4.157E-02 NOT IDENT. ND-147 2.742E+06 3 .111E+07 3 .114E+07 SHORT HLIF PM-147 ..:.5.293E+02 8.577E+02 8.903E+02 NOT IDENT. PM-149 -7.583E+39 l.654E+40 O.OOOE+OO SHORT HLIF EU-150 -1.177E-04 2.422E-02 2.422E-02 FAIL ABUN EU-152 -2.768E-02 1.120E-01 l.127E-01 FAIL ABUN GD-153 -7.463E-02 1.390E-01 l.430E-01 NOT IDENT. EU-154 -4.760E-02 l.267E-01 l.285E-01 FAIL ABUN EU-155 6.449E-02 9.849E-02 l.027E-01 FAIL ABUN TB-160 4.565E-01 1.874E+OO 1.885E+OO FAIL ABUN H0-166M -2.157E-02 7.512E-02 7.574E-02 FAIL ABUN TM-171 1.387E+00 5.059E+OO 5.097E+OO NOT IDENT. Page 4490 of 5809 HF-172 5.805E-02 2.500E-01 2.514E-01 FAIL ABUN LU-172 -l.890E-02 8.115E-02 8.160E-02 FAIL ABUN LU-176 -5.312E-03 2.280E-02 2.293E-02 FAIL ABUN HF-181 -4. 713E-03 4.331E+OO 4. 331E+OO NOT IDENT. TA-182 -6.420E-01 l. ll 7E+OO l.154E+OO FAIL ABUN RE-183 4.663E-01 l.024E+OO l.045E+OO NOT IDENT. RE-184 5.259E+01 3.818E+Ol 4.494E+Ol NOT IDENT. W-188 -2.689E+OO l.130E+02 l.130E+02 FAIL ABUN IR-192 3.864E-01 4.285E-01 4.626E-01 FAIL ABUN HG-203 1.482E+OO . 2.214E+OO 2.313E+OO NOT I DENT .* BI-207 -l.844E-02 3.901E-02 3.988E-02 FAIL ABUN PB-211 2.869E-02 6.683E-01 6.684E-01 NOT IDENT. BI-212 1. 735E+OO 9.030E-01 l.195E+OO FAIL ABUN RN-219 8.025E-02 3.447E-01 3.466E-01 FAIL ABUN RA-223 -1.621E-01 5.796E-01 5.842E-01 FAIL ABUN AC-227 -1.213E-01 2 .196E-01 2.263E-01 FAIL ABUN TH-227 -1.213E-01 2 .196E-01 2.263E-01 FAIL ABUN TH-231 -1. 621E-01 5.796E-01 5.842E-01 FAIL ABUN PA-233 2.280E-02 5.589E-02 5.683E-02 FAIL ABUN PA-234 -6.323E-02 2.777E-01 2.791E-01 FAIL ABUN PA-234M -2.854E-01 4.223E+OO 4.225E+OO NOT IDENT. NP-237 2.280E-02 5.589E-02 5.683E-02 FAIL ABUN NP-238 -l.000E+41 l.282E+41 O.OOOE+OO SHORT HLIF NP-239 -4.410E-03 2.216E-01 2.216E-01 FAIL ABUN PU-239 3.638E+02 7. 311E+o2 7.493E+02 FAIL ABUN AM-241 l.892E-02 5.757E-02 5.820E-02 NOT IDENT. CM-243 -6.583E-02 8.152E-02 8.676E-02 FAIL ABUN 'BK-24 7 l.824E-02 7.546E-02 FAIL ABUN CM-247 -1.947E-03 3.174E-02 3.175E-02 FAIL ABUN CF-249 2.034E-02 3.716E-02 3.827E-02 NOT IDENT. CF-251 -4.218E-02 l.066E-01 1.083E-01 NOT IDENT. Page 4491of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 71. 4845 87.09 105.1814 136.47 73.4068 45.60 66.7140 87.57 105.2499 140.51 0.0000 46.54 66.8393 88.03 105.3153 143.76 76.6191 49.72 0.0000 88.34 105.3595 144.24 76.6559 51. 35 85.2130 88.47 105.3775 145.44 76.7460 51. 87 85.2957 89. 96 120. 6716 152.43 69.1805 52.39 88.9352 1093.63 108.1994 153.25 0.0000 52.97 91. 4043 91.11 0.0000 323.87 63.8974 53.44 87.9185 92.59 88.2952 156.02 0.0000 54.07 96.3454 93.35 88.3823 158.56 0.0000 57.36 0.0000 94.56 74.6107 159.00 67.8009 57.53 98.1373 94.65 74.6192 162.33 68.0092 57.98 103.0045 94.67 74.6210 162.66 0.0000 59.27 102.4339 94.87 77.1705 163.33 68.9786 59.32 108.8454 97.43 94.4304 165.86 66.4080 59.54 110.4878 98.43 89.8052 176.31 66.1062 '60. 96 118.7802 98.44 89. 8'063 176.60 0.0000 61.17 118. 8.220 99.53 76.3545 177.52 63.4178 62.93 106.2881 100 .11 79.8059 181. 07 0.0000 63.29 106.3510 102.03 92.7610 181. 52 55.3351 63.58 124.1357 103.18 95.4479 184.41 57. 3196 64.28 132.3481 103.37 97.1750 143.76 57.3827 66.73 121.5294 105.21 76.8883 193.51 62.4104 67.24 109.4657 105.31 76.8979 197.03 54.1815 125.81 111. 97 62 106.12 85.9526 198.01 52.3542 67.75 111. 9881 106.47 91. 122 6 201. 83 56.2653 69.67 155.0593 109.28 66.9606 203.43 65.7261 70.83 130.8748 111. 00 85.1597 205.31 55.0092 72.81 137.4049 111.76 0.0000 210.85 49.5803 72.87 150.5051 114. 06 71. 6494 215.65 49.2885 74.66 119.7441 116.30 0.0000 222 .11 52.3861 74.82 119. 7723 116. 74 87.4539 227.09 48.7552 74.97 119.7990 119.76 76.8901 227.38 49.7217 77 .11 120.1778 121.12 92.6680 228.16 0.0000 78.74 120.4622 121.22 92.6783 228.18 49.7508 79.69 120.6270 121. 78 64.4361 116.74 49.7508 80.12 120.7013 122.06 64.4557 235.69 41. 8450 80.19 0.0000 122.92 58.8496 235. 96 41.8530 80.57 120.7785 123.07 58.8593 238.63 43.3786 81. 00 120.8528 265.00 64.1338 238.98 0.0000 81. 07 120.8647 125.81 55.0987 240.99 43.4509 81. 75 120.9805 127.23 55.1824 242.00 43.4821 83.79 59.8323 127.91 64.4267 244.70 43.5645 84.00 107.2310 129.30 71.1049 252.40 0.0000 85.43 104.9436 131.20 71. 2483 252.80 31.1527 86.55 105.1045 133. 02 68. 7396 254.15 0.0000 86.79 105.1384 133.52 68.7753 256.23 48.7895 86.94 105.1602 136.00 74.2554 260.90 0.0000 Page 4492 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 33. 8549 355.39 0.0000 584.27 16.0758 264.80 36.8027 356.01 32.6414 595.83 0.0000 265.00 36.8073 364.49 0.0000 427.87 23 .1071 268.22 35.4097 366.42 0.0000 602.52 0.0000 269.46 35.4390 372. 51 20.9074 604.72 26.0358 270.03 *I 35.4521 375.05 28.2623 607.14 17.3724 271.23 35.4800 377.52 24.1062 609.32 17.3865 273.65 0.0000 356.01 23.1337 610.33 17.3932 276.40 35.5986 388.16 25.2920 614.28 15.6764 277.37 35.6206 388.63 0.0000 618.01 11. 6280 277.60 35.6257 391.69 26.3931 620. 36 16.2935 278.00 35.6353 264.66 32.8751 621.93 13.9736 279.20 35.6624 401.81 22.2830 630.19 0.0000 279.54 35.6704 402.40 24.4122 631. 29 18.4026 279.70 35.6741 404.85 28.6930 633.25 17.5385 280.46 35.6909 410.95 21.3175 634.78 0.0000 283.69 35.7642 413.71 34.1543 635.95 20.1889 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 28.3440 423.72 0.0000 645.85 16.7369 285.90 0.0000 427.09 33.3008 657.76 8.4920 287.50 35.8499 427. 87 35.4620 657.90 0.0000 290.67 37.4176 433.94 19.3986 661. 66 3.5431 293.27 0.0000 439.40 20.5288 664.57 0.0000 351.93 33.0201 453.88 23.9296 666.33 *o.oooo 295.96 33.0349 463.37 18.5706 666.50 0.0000 879.38 33.0880 468.07 19.7043 667. 71 0.0000 299.98 33 .1161 473.00 0.0000 677.62 8.9066 300.09 33 .1182 475.06 24.7069 685.70 0.0000 300.13 33 .1195 476.78 13.1870 695.00 0.0000 301.36 33.1437 477.60 24.7343 696. 49 19.7200 302.85 33.1739 482.18 24.2335 696. 51 18.8236 256.23 27.1692 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 19.7253 306.78 28.7180 '497.08 23.2813 697.49 18.8300 308.46 36.3120 505.52 16.6891 702.65 21. 5574 311. 90 30.3217 507.63 0.0000 706.68 26.9824 316.51 26.3502 511. 00 16.7276 711. 68 24.5047 319.41 0.0000 514.00 21.7733 720.70 0.0000 320.08 0.0000 514.00 21. 7733 721. 93 0.0000 321. 04 32.5169 520.40 19.0323 722.78 10.1268 323.87 38. 6772 520.69 0.0000 722. 91 13.0210 325.23 40.7446 522.65 0.0000 723.31 11. 5758 328.76 0.0000 527.90 0.0000 724.19 20.2631 333.37 24.5605 528.26 25.2713 727.33 12.6772 333.97 30.7111 529.59 20.2280 733.00 17.4182 334.37 39.9331 529.87 0.0000 735.93 15.4369 338.28 28.7332 531.02 *0.0000 333.97 14.5361 338.32 28.7337 537.26 0.0000 739.50 0.0000 311. 90 28.7685 546.56 0.0000 747.24 12.7589 340.48 28.7685 552.55 14.7451 748.06 14.5850 340.55 0.0000 563.25 22.7799 752.31 18.2562 344.28 41. 698 9 569.33 27.4004 753.82 0.0000 345.93 30.9167 946.00 30.8276 756.73 15. 5396 351.06 34.1038 569.70 30.8298 756.80 15. 5396 351.93 34 .1199 583.19 16.0690 884.68 14.6582 Page 4493 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 13.7503 1274.44 9.7833 1620.50 5.5801 766.42 15.5868 1001.03 9.7952 1621.92 4.4653 766.84 13.7549 1002.74 15.6792 1678.03 0.0000 772. 60 0.0000 1004.73 9.8044 1690.97 2. 7114 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 3.6602 778.90 17.4878 1028.54 0.0000 1063.66 1. 52 64 783.70 0.0000 1037.84 17.7957 1771. 35 10.9928 785 .. 37 25.8228 1038.76 0.0000 1791.20 0.0000 792.07 28.6481 631.29 17.8341 1808.65 0.9216 794.95 12.9494 1048.07 0.0000 1810.72 0.0000 795.86 11.1024 1049.04 11. 8967 1836.06 1. 8515 810.06 18.5834 1050.41 5.9506 810.29 19.5138 1063.66 6.3680 344.28 17.6565 1077.00 0.0000 810.76 15.7995 1077.34 14.9744 815.77 0.0000 1085.87 15.0046 1048.07 0.0000 1093.63 12.0264 832.01 14.0286 1099.45 6.0216 834.85 18.7207 1112. 07 12.0791 835.71 12.1712 1112.84 18.1219 836.80 0.0000 1115. 54 4.8357 846.75 0.0000 1120.29 14.5230 846.77 14.0891 1120.55 14.5239 856.80 0.0000 1221. 41 14.5266 860.56 12.0707 1129. 67 11. 3203 871.09 9.4586 1131. 51 0.0000 873.19 16.0890 1147.95 0.0000 875.33 0.0000 1173.23 17.9685 879.38 11.3771 1177.95 15.3305 880.51 13.2771 1189.05 8.1968 883.24 10.4401 1204.77 11. 5158 884.68 9.4949 1221.41 18.5757 889.28 7.6057 1231.02 11. 37 53 894.76 18.0914 1235.36 0.0000 898.04 15.2485 1238.28 l3.4650 900. 72 24.7971 1260.41 0.0000 903.28 9.5441 1271.87 8.3462 911.20 11.4781 1274.44 11. 4821 912.08 11. 4807 1274.54 12.5266 923.98 0.0000 1291.59 11. 5244 926.50 15.3682 1298.22 0.0000 929 .11 11. 5342 1312 .11 0.0000 937.49 15.4136 1332.49 10.5658 944.13 0.0000 1362.66 0.0000 946.00 11.5865 1365 .19 6.3820 949.00 11. 5957 1368. 63 0.0000 667.71 0.0000 1384.29 4.2710 962. 31 18.4248 1408.01 7.5093 964.08 12.1966 1457.56 0.0000 966 .17 15. 5313 1460.82 5.7803 911.20 27.9773 1489.16 5.4483 968. 97 27.9773 1505.03 6.5574 983.53 0.0000 1584.12 3.3265 984.45 0.0000 1596.21 0.0000 Page 4494 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:05:45.47 ********************************************************************************
  • GEL LLC "*
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235068.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM31.CNF;306 Background date : Z-OCT-2016 11:01:52. Sample date ll-DEC-2015 10:27:00 Acquisition date : 3-0CT-2016 06:05:07. Sample ID G405235068 Sample quantity : l.40907E+02 GRAM Detector name : GAM31 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:06.51 0.2% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 5 5 4 4 4 4 0 0 4 4, 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4495 of 5809 Energy 46.54* 63.01* 74.84 77.04* 84.04* 87.12* 90.01 92.77* 115. 24 143.81* 185.93* 187.50 209.79 238.61* 242.06* 277.62 295.32* 329.09 338.68* 351. 8 9* 463.26 511.42* 519.95 552.89 583.71* 609.71* 632.56 661.91 719.56 729.51 769.36* 803.84* 836.89* 840. 72 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 51 141 145 244 20 64 32 95 26 36 70 24 34 209 43 15 104 16 44 152 22 33 14 18 76 102 13 22 22 25 16 8 8 13 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 278 338 128 136 161 129 135 105 91 84 57 56 59 76 54 47 48 34 45 45 14 29 20 10 12 32 17 12 10 19 11 5 6 1 0.94 1. 37 0.83 1.12 1. 39 1.19 1. 41 1.24 0.60 0.83 1. 54 1. 65 1. 59 0.93 1.13 3.13 0.88 0.77 1.21 1.10 0.71 1. 93 1. 44 2 .11 1. 66 1.26 1. 69 2.02 2.39 4.46 3.26 1. 40 0.98 1. 48 92.73 125.65 149.28 153.68 167.67 173.83 179.60 185 .11 230.03 287.13 371.31 374.45 418.99 476.58 483.48 554.56 589.92 657.42 676.58 702.99 925.57 1021. 84 1038.87 1104.71 1166. 31 1218.29 1263.95 1322.62 1437.84 1457.73 1537.38 1606.30 1672. 36 1680.01 88 120 145 145 162 162 .162 162 226 284 366 366 415 471 481 548 585 652 672 697 922 1015 1031 1101 1161 1213 1257 1315 1433 1448 1532 1602 1668 1677 10 1. 43E-02 64. 0 12 3.91E-02 28.3 15 4.02E-Ot 13.7 3.96E+OO 15 6.78E-02 10.9 29 5.48E-03108.6 l.75E+OO 29 1. 78E-02 31. 7 29 8.85E-03 67.8 29 2.63E-02 23.4 8 7.14E-03 68.0 8 9.92E-03 48.6 14 l.95E-02 24.6 2.42E+OO 14 6.76E-03 74.7 8 9.49E-03 42.3 9 5.80E-02 10.5 7 l.18E-02 34. 2 9 4.18E-03 86.2 10 2.88E-02 16.1 8 4.56E-03 66.2 11 1. 23E-02 33. 6 12 4.21E-02 12.4 8 6.20E-03 35.8 13 9.20E-03 47.4 10 3.86E-03 66.0 8 4.96E-03 40.4 12 2.llE-02 15.3 12 2.82E-02 15.1 11 3.61E-03 70.1 12 6.09E-03 38.2 13 5.99E-03 37.0 16 6.85E-03 45.2 11 4.54E-03 50.7 7 2.34E-03 60.9 9 2.15E-03 76.5 7 3.50E-03 32.8 Peak Search Report (continued) Page : 2 Sample ID : G405235068 Acquisition date 3-0CT-2016 06:05:07 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 875.20 13 5 1. 52 1748.92 1744 10 3.61E-03 42.5 36 0 911.73* 30 7 2.07 1821.94 1817 9 8.32E-03 25.5 37 0 946.61. 10 6 0.95 1891.67 1886 9 2.:?0E-03 57.5 38 0 969. 85 36 9 1. 30 1938.12 1933 12 9.86E-03 23.7 39 0 1002.44* 6 10 2.92 2003.25 1993 13 1. 73E-03113. 4 40 0 1120. 52 45 3 2. 02 2239.27 2234 12 1. 24E-02 16.9 41 0 1157. 48 8 15 1. 52 2313.16 2306 12 2.17E-03105.7 42 0 1231. 7 9 6 5 1. 47 2461.70 2458 7 1. 72E-03 72.7 43 0 1238.29 10 15 1. 44 2474.70 2468 12 2.76E-03 84.3 44 0 1461.56* 155 0 1. 76 2921. 00 2914 13 4.30E-02 8.2 Flag: "*" = Peak area was modified by background subtraction Page 4496 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:05:47 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235068.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID ll-DEC-2015 10:27:00 G405235068 Acquisition date : Sample quantity S.ample geometry : 3-0CT-2016 06:05:07 140.91 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA31 0 01:00:00.00 1.50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4497 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:06.51 10.00 0.00 % Peak Energy 0.2%

Nuclide Line Activity Report Page : 2 Sample ID : G405235068 Acquis_ition date 3-0CT-2016 06:05:07 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status "K-40 1460.82 10.66* 6.944E-01 1.069.E+Ol 1.069E+Ol 16.44 OK CD-109 88.03 3.70* 5.391E+OO 9.560E-01 1. 493E+OO 141.28 OK SN-126 64.28 9.60 5.591E+OO 1.731E+OO 1. 731E+OO 56.68 OK 86.94 8.90 5. 391E+OO 3.974E-01 3.974E-01 141.28 OK 87.57 37.00* 5. 391E+OO 9.560E-02 9.560E-02 141.28 OK BA-137M 661. 66 89.90* l.340E+OO 9. 971E-02 1.016E-01 76.37 OK CS-137 661. 66 85.10* 1.340E+OO l.053E-01 1.073E-01 76.37 OK TL-208 277.37 6.60 2.813E+OO 4.776E-01 4.776E-01 172. 42 OK 583.19 85.00* 1.486E+OO 3.334E-01 3.334E-01 30.59 OK 860.56 12.50 1.084E+OO Line Not Found Absent PB-210 46.54 4.25* 5.485E+OO l.485E+OO 1.523E+OO 128.02 OK PB-212 74.82 10.28 5.476E+OO 9.929E-01 9.929E-01 50.45 OK 77 .11 17.10 5.460E+OO 1.698E+OO 1.698E+OO 21. 86 OK 238.63 43.60* 3.203E+OO 8.924E-01 8.924E-01 21. 09 OK 300.09 3.30 2.629E+OO Line Not Found Absent BI-214 609.32 45.49* 1.433E+OO 8.612E-01 8.615E-01 30.24 OK 1120.29 14.92 8.738E-01 1. 793E+00 1. 794E+00 33.81 OK 1764.49 15.30 5.813E-01 Line Not Found Absent PB-214 74.82 5. 80 5.476E+OO Line Not Found <<INT Reject 77 .11 9.70 5.460E+OO 2.994E+OO 2.995E+OO 21. 86 OK 87.09 3.41 5.392E+OO Line Not Found <<INT Reject 242.00 7.25 3.165E+OO 1.106E+OO 1.106E+OO 68.50 OK 295.22 18.42 2.666E+OO 1.238E+OO 1.238E+OO 32.25 OK 351.93 35.60* 2.286E+OO 1.077E+OO 1.077E+OO 24.83 OK RN-222 609.32 45.49* l.433E+00 8.612E-01 8.615E-01 30.24 OK 1120.29 14.92 8.738E-01 1. 793E+OO 1.794E+OO 33.81 OK 1764.49 15.30 5.813E-01 Line Not Found Absent RA-226 609.32 45.49* 1.433E+OO 8.612E-01 8.615E-01 30.24 OK 1120.29 14.92 8.738E-01 1. 793E+OO 1. 794E+OO 33.81 OK 1764.49 15.30 5.813E-01 Line Not Found Absent AC-228 105.21 1.10 5.215E+OO Line Not Found Absent 338.32 11. 27 2.364E+OO 9.611E-01 9. 611E-01 67. 21 OK 794.95 4.25 1.156E+OO Line Not Found Absent 835.71 1. 61 1.109E+OO 2.330E+OO 2.330E+OO 153.03 OK 911.20 25.80* l.035E+00 5.983E-01 5.983E-01 51. 06 OK 968.97 15.80 9.841E-01 1.211E+OO 1.211E+OO 47.47 OK RA-228 105.21 1.10 5.215E+OO Line Not Found Absent 338.32 11.27 2.364E+00 9. 611E-01 9. 611E-01 67.21 OK 794.95 4.25 1.156E+OO Line Not Found Absent 835.71 1. 61 1.109E+OO 2.330E+OO 2.330E+OO 153.03 OK 911.20 25.80* 1.035E+OO 5.983E-01 5.983E-01 51. 06 OK 968. 97 15.80 9.841E-01 1.211E+OO 1.211E+OO 47.47 OK TH-228 74.82 10.28 5.476E+OO 9.929E-01 9.929E-01 50.45 OK 77 .11 17.10 5.460E+OO 1.698E+OO 1.698E+OO 21. 86 OK 238.63 43.60* 3.203E+OO 8.924E-01 8.924E-01 21. 09 OK 300.09 3.30 2.629E+OO Line Not Found Absent TH-229 85.43 14.70 5.413E+OO 1. 601E-01 l.602E-01 217.11 OK 88.47 24.00 5.391E+OO 1.474E-01 l.474E-01 141.28 OK 193.51 4.41* 3.791E+OO Line Not Found Absent Page 4498 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235068 Acquisition date 3-0CT-2016 06:05:07 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 210.85 2.80, 3.560E+OO 2.065E+OO 2.065E+OO 84.64 .. OK TH-230 609.32 45.49* 1.433E+OO 8.612E-Ol 8.612E-01 30.24 OK 1120. 29 14.92 8.738E-01 1. 793E+OO 1. 793E+OO 33.81 OK 1764.49 15.30 5.813E-01 Line Not Found Absent TH-232 105.21 1.10 5.215E+OO Line Not Found Absent 338.32 11.27 2.364E+OO 9. 611E-01 9. 611E-01 67. 21 OK 835.71 1. 61 l.109E+OO 2.330E+OO 2.330E+OO 153.03 OK 911.20 25.80* 1.035E+OO 5.983E-01 5.983E-01 51. 06 OK 968. 97 15.80 9.841E-01 1.211E+OO 1. 211E+OO 47.47 OK TH-234 63.29 3.70* 5.591E+OO 4.492E+OO 4.492E+OO 56.68 OK 92.59 4.23 5.346E+OO 2.688E+OO 2.688E+OO 46.83 OK U-234 609.32 45.49* 1.433E+OO 8.612E-01 8.612E-01 30.24 OK 1120.29 14.92 8.738E-01 1. 793E+OO l.793E+00 33.81 OK 1764.49 15.30 5.813E-01 Line Not Found Absent U-235 89. 96 3.47 5.369E+OO 1.098E+OO 1.098E+OO 135.57 OK 93.35 5.60 5.346E+OO 2.030E+OO 2.030E+00 46.83 OK 143.76 10. 96* 4.610E+OO 4.384E-01 4.384E-01 97 .11 OK 163.33 5.08 4.273E+OO Line Not Found Absent 185.72 57.20 3.905E+OO 1.909E-01 1.909E-01 49.24 OK 205.31 5.01 3.621E+OO Line Not Found Absent U-238 63.29 3.70* 5.591E+OO 4.492E+OO 4.492E+OO 56.68 OK 92.59 4.23 5.346E+OO 2.688E+OO 2. 688E+OO 46.83 OK AM-243 43.53 5.90 5.049E+OO Line Not Found Absent 74.66 67.20* 5.476E+OO 1.519E-01 1.519E-01 50.45 OK ANH-511 511. 00 100.00* 1.658E+OO l.120E-01 1.120E-01 94.85 OK Flag: "*" = Keyline Page 4499 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:05:48.74 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235068.CNF;l *
  • Acquisition date 3-0CT-2016 06:05:07 Sensitivity : 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.51 Half life ratio : ***** *
  • Sample date ll-DEC-2015 10:27:00 Analyst initials: MXRl *
  • Sample ID G405235068 Sample Quantity 1.4091E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN * *' Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.069E+Ol 1.723E+OO CD-109 1.493E+OO 2.067E+OO SN-126 9.560E-02 1.324E-01 BA-137M l.016E-01 7.604E-02 CS-137 1. 073E-01 8.032E-02 TL-208 3.334E-01 9.993E-02 PB-210 1.523E+OO 1. 911E+OO PB-212 8.924E-01 1.844E-01 BI-214 8.615E-01 2.553E-01 PB-214 1. 077E+OO 2.622E-01 RN-222 8.615E-01 2.553E-01 RA-226 8.615E-01 2.553E-01 AC-228 5.983E-01 2.994E-01 RA-228 5.983E-01 2.994E-01 TH-228 8.924E-01 1.844E-01 TH-229 -3.292E-01 5.827E-01 TH-230 8.612E-01 2.552E-01 TH-232 5.983E-01 2.994E-01 TH-234 4.492E+OO 2.495E+OO U-234 8.612E-01 2.552E-01 U-235 4.384E-01 4. l 72E-01 U-238 4.492E+OO 2.495E+00 AM-243 l.519E-01 7.510E-02 ANH-511 l.120E-01 l.041E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4500 of 5809 Key-Line Activity (pCi/GRAM 4.472E+OO 1.986E-02 O.OOOE+OO -2.300E-02 1.296E-01 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.606E+Ol 5.325E-02 l.960E+41 5.199E-02 4.540E-01 1. 731E+04 MDA (pCi/GRAM 1.958E-01 1. 713E+00 1. 096E-01 8.583E-02 9.067E-02 7.921E-02 1.254E+OO l.300E-01 1.601E-01 1. 575E-01 1. 601E-01 1.601E-01 4.099E-01 4.099E-01 l.300E-01 1.0llE+OO 1.600E-01 4.099E-01 1.421E+OO l.600E-01 4.212E-01 l.421E+OO 7.344E-02 8.199E-02 MDA (pCi/GRAM 3.280E+Ol 1.227E-01 O.OOOE+OO 1.013E-01 1.007E+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 4.574E+02 0.000E+OO SHORT HLIF MN-54 3.464E-02 8.857E-02 l.764E-01 NOT IDENT. C0-56 -2.422E-01 5.957E-Ol l.060E+OO FAIL ABUN MN-56 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF C0-57 2.620E-02 4.980E-02 1. OOlE-01 NOT IDENT. C0-58 8.435E-02 8.493E-Ol l.667E+OO NOT IDENT. FE-59 -1. 391E+OO 1.012E+Ol 1.986E+Ol NOT IDENT. C0-60 -1.952E-02 6.536E-02 l.234E-01 NOT IDENT. ZN-65 2.643E-01 1. 996E-01 5.108E-01 NOT IDENT. GE-68 1. 726E+OO 3.942E+OO 8. 369E+OO NOT IDENT. AS-73 -1.626E+OO 3.600E+OO 6.757E+OO NOT IDENT. AS-74 O.OOOE+OO 6.846E+03 O.OOOE+OO SHORT HLIF SE-75 -1.112E-02 2.482E-01 4.557E-01 NOT IDENT. BR-77 O.OOOE+OO 1.379E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 9.864E+02 0.000E+OO SHORT HLIF RB-83 1.149E+OO 1.487E+OO 1.993E+OO FAIL ABUN KR-85 l.320E+Ol 1.337E+Ol 2.325E+Ol NOT IDENT. SR-85 1.348E+OO l.369E+OO 2.379E+OO NOT IDENT. RB-86 O.OOOE+OO 4.144E+04 O.OOOE+OO SHORT HLIF Y-88 -1.357E-01 3.765E-01 7.483E-01 NOT IDENT. Y-91 3.099E+Ol 8.319E+02 1. 653E+03 NOT IDENT. NB-94 -2.935E-03 5.579E-02 1.028E-01 NOT IDENT. NB-95 2.340E-01 l.267E+OO 2.272E+OO NOT IDENT. NB-95M -1.254E+OO 3.164E+OO 5. OllE+OO NOT IDENT. ZR-95 7.702E-01 1.988E+OO 4.129E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 1.176E+32 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -4.569E-02 4.167E-02 7. 096E-02 NOT IDENT. RH-102 1.068E-01 1.467E-01 1.980E-01 FAIL ABUN RU-103 3.633E+OO 7.298E+OO 1.547E+Ol FAIL ABUN RH-106 3.073E-01 7.155E-01 1.489E+OO NOT IDENT. RU-106 3.073E-01 7.155E-01 l.489E+OO NOT IDENT. AG-108M 5.132E-04 3.671E-02 7.318E-02 NOT IDENT. AG-llOM -3.555E-02 1.357E-01 2.689E-01 NOT IDENT. SN-113 -2.922E-01 2.722E-01 4.615E-01 NOT IDENT. CD-115 O.OOOE+OO 1.599E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 9.773E+04 0.000E+OO SHORT HLIF TE-123M 9.658E-02 1. 4 95E-01 3.000E-01 NOT IDENT. SB-124 -8.631E-01 3.515E+OO 6.777E+OO NOT IDENT. SB-125 -4.405E-02 l.232E-01 2.350E-01 FAIL ABUN TE-125M 8.862E+Ol 2.626E+02 5.215E+02 NOT IDENT. I-126 0.000E+OO 1.130E+06 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 2.173E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1. 97 5E+22 O.OOOE+OO SHORT HLIF I-131 0.000E+OO 4.617E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.994E+26 0.000E+OO SHORT HLIF BA-133 -6.029E-03 5.625E-02 9.980E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 7.486E-02 6. 960E-02 l.593E-01 NOT IDENT. CS-135 -1.805E-01 2.255E-01 3.666E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 3.749E+05 O.OOOE+OO SHORT HLIF CE-139 -6.925E-02 l.348E-01 2.385E-01 NOT IDENT. BA-140 O.OOOE+OO l.453E+06 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 5.563E+05 O.OOOE+OO SHORT HLIF CE-141 3.398E+OO 3.00lE+Ol 5.182E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -8.120E-02 4.275E-01 7.934E-01 NOT IDENT. PM-144 1.596E-02 8.657E-02 l.700E-01 NOT IDENT. PR-144 3.554E+OO 7.147E+OO l.479E+Ol NOT IDENT. PM-146 1.583E-03 5. 641E-02 l.128E-01 FAIL ABUN ND-147 O.OOOE+OO 3.638E+07 O.OOOE+OO SHORT HLIF PM-147 5.748E+02 8.385E+02 l.718E+03 NOT IDENT. PM-149 0.000E+OO 2.235E+40 O.OOOE+OO SHORT HLIF EU-150 3.462E-03 3.452E-02 6.337E-02 FAIL ABUN EU-152 -9.092E...:02 l.277E-01 2.204E-01 NOT IDENT. GD-153 -1.268E-01 1. 727E-01 2.838E-01 NOT IDENT. EU-154 5.290E-02 l.320E-01 3.051E-01 NOT IDENT. EU-155 6.667E-02 1.076E-Ol 2.185E-01 FAIL ABUN TB-160 -1.441E+00 3. OllE+OO 4.846E+OO FAIL ABUN H0-166M -2.656E-02 9. 723E-02 l.684E-01 NOT IDENT. TM-171 -3.650E+00 8.279E+OO 1.557E+Ol NOT IDENT. HF-172 l.495E-01 2.639E-01 5.260E-01 FAIL ABUN LU-172 6. 4 72E-03 l.243E-01 2.507E-01 FAIL ABUN LU-176 -2.207E-02 2. 811E-02 5.161E-02 FAIL ABUN Page 4501of5809 HF-181 -l.574E-01 6.308E+00 l.228E+Ol NOT IDENT. TA-182 -3.451E-01 1.191E+OO 2.281E+OO FAIL ABUN RE-183 1.749E+OO 1.582E+OO 3.254E+OO NOT IDENT. RE-184 -1.444E+Ol 3.955E+Ol 7.653E+Ol NOT IDENT. W-188 l.201E+02 1.436E+02 2.909E+02 FAIL ABUN IR-192 3.002E-01 5.801E-01 1.226E+00 FAIL ABUN HG-203 -1.136E+OO 3.446E+OO 5.433E+OO NOT IDENT. BI-207 -2.036E-02 3.990E-02 7.650E-02 FAIL ABUN BI-211 O.OOOE+OO 7.221E-01 1.104E+OO FAIL ABUN PB-211 -3.059E-01 9.182E-01 1. 742E+.00 NOT IDENT. BI-212 5.943E-01 7.658E-01 l.579E+OO NOT IDENT. RN-219 7.448E-01 5.228E-01 1.196E+OO NOT IDENT. RA-223 2.950E-01 8.190E-01 l.558E+OO FAIL ABUN RA-224 O.OOOE+OO 1.312E+OO 1.923E+OO FAIL ABUN AC-227 -1.052E-01 2.873E-01 5.016E-01 NOT IDENT. TH-227 -1.052E-01 2.873E-01 5.016E-01 NOT IDENT. PA-231 4.789E-01 5.909E-01 1.264E+OO NOT IDENT. TH-231 2.950E-01 8.190E-01 l.558E+00 FAIL ABUN PA-233 3.054E-02 8.027E-02 l.663E-01 NOT IDENT. PA-234 4.288E-01 4.830E-01 8.629E-01 FAIL ABUN PA-234M 4.103E+OO 9.122E+OO 1.297E+Ol FAIL ABUN NP-237 3.054E-02 8.027E-02 1.663E-01 NOT IDENT. NP-238 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF NP-239 4.019E-01 5.354E-01 4.900E-01 FAIL ABUN PU-239 9. 966E+Ol 3.697E+02 7.145E+02 NOT IDENT. AM-241 2.063E-03 8.357E-02 l.514E-01 NOT IDENT. CM-243 -2.183E-02 l.OOlE-01 1. 891E-01 FAIL ABUN BK-247 2.102E-02 8.871E-02 1.692E-01 FAIL ABUN CM-247 2. 711E-02 5.036E-02 1.050E-01 FAIL ABUN CF-249 3.777E-02 4.634E-02 1.021E-01 NOT IDENT. CF-251 1.857E-01 1.365E-01 2.907E-01 NOT IDENT. ,, Page 4502 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:05:46.26 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 149 10.66* 6.944E-01 1.069E+Ol 1.069E+Ol 16.44 CD-109 88.03 78 3.70* 5.391E+OO 2.070E+OO 3.234E+OO 63.31 SN-126 64.28 174 9.60 5.591E+OO 1.731E+OO 1. 731E+OO 56.68 86.94 78 8.90 5.391E+OO 8.607E-01 8.607E-01 63.31 87.57 78 37.00* 5.391E+OO 2.070E-01 2.070E-01 63.31 BA-137M 661.66 23 89.90* 1.340E+OO 9. 971E-02 1.016E-01 76.37 CS-137 661. 66 23 85.10* 1.340E+OO l.053E-01 1.073E-01 76.37 TL-208 277.37 17 6.60 2. 813E+OO 4.776E-01 4.776E-01 172.42 583.19 79 85.00* 1. 486E+OO 3.334E-01 3.334E-01 30.59 860.56 ------12.50 1.084E+OO ------Line Not Found ------PB-210 46.54 65 4.25* 5.485E+OO 1.485E+00 1.523E+OO 128.02 BI-211 72.87 ------1. 23 5.491E+OO ------Line Not Found ------351.06 164 12.92* 2.286E+OO 2.967E+OO 2. 967E+OO 24.83 PB-212 74.82 177 10.28 5.476E+OO 1. 675E+00 1.675E+OO 27.44 77 .11 298 17.10 5.460E+OO 1.698E+OO 1.698E+OO 21. 86 238.63 234 43.60* 3.203E+OO 8.924E-01 8.924E-01 21. 09 300.09 ------3.30 2.629E+OO ------Line Not Found ------BI-214 609.32 105 45.49* 1.433E+OO 8.612E-01 8.615E-01 30.24 1120.29 44 14.92 8.738E-01 1. 793E+00 1. 794E+OO 33.81 1764.49 ------15.30 5. 813E-01 ------Line Not Found ------PB-214 74.82 177 5.80 5.476E+OO 2.969E+00 2.970E+OO 27.44 77 .11 298 9.70 5.460E+OO 2.994E+OO 2.995E+OO 21. 86 87.09 78 3.41 5.391E+OO 2.247E+00 2.247E+OO 63.31 242.00 48 7.25 3.165E+OO l.106E+00 1.106E+OO 68.50 295.22 114 18.42 2.666E+OO 1.238E+00 1.238E+OO 32.25 351. 93 164 35.60* 2.286E+OO 1.077E+00 1.077E+OO 24.83 RN-222 609.32 105 45.49* 1.433E+OO 8.612E-01 8.615E-01 30.24 1120.29 44 14.92 8.738E-01 1. 793E+00 1. 794E+OO 33.81 1764.49 ------15.30 5.813E-01 ------Line Not Found ------RA-224 240.99 48 4.10* 3.165E+OO l.955E+00 l.955E+OO 68.50 RA-22 6 609.32 105 45.49* l.433E+OO 8.612E-01 8.615E-01 30.24 1120.29 44 14.92 8.738E-01 1. 793E+OO 1. 794E+OO 33.81 1764.49 ------15.30 5.813E-01 ------Line Not Found ------AC-228 105.21 ------1.10 5.215E+OO ------Line Not Found ------338.32 48 11.27 2.364E+OO 9. 611E-01 9. 611E-01 67. 21 794.95 ------4.25 l.156E+OO ------Line Not Found ------835. 71 8 1. 61 l.109E+OO 2.330E+00 2.330E+OO 153.03 911. 20 30 25.80* 1.035E+OO 5.983E-01 5.983E-01 51. 06 968. 97 35 15.80 9.841E-01 1. 211E+00 1.211E+OO 47.47 RA-228 105.21 ------1.10 5.215E+OO ------Line Not Found ------338.32 48 11. 27 2.364E+OO 9. 611E-01 9. 611E-01 67.21 794.95 ------4.25 1.156E+OO ------Line Not Found ------835.71 8 1. 61 1.109E+OO 2.330E+00 2.330E+OO 153.03 911.20 30 25.80* 1.035E+OO 5.983E-01 5.983E-01 51. 06 968.97 35 15.80 9.841E-01 1.211E+OO 1.211E+OO 47.47 TH-228 74.82 177 10.28 5.476E+OO l.675E+00 1.675E+OO 27.44 77 .11 298 17.10 5.460E+OO 1.698E+OO 1.698E+OO 21. 86 Page 4503 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235068 Acquisition date 3-0CT-2016 06:05:07 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 238.63 234 43.60* .3.203E+OO 8.924E-01 8.924E-01 21. 09 . 300.09 ------3.30 2.629E+OO ------Line Not Found ------TH-229 85.43 24 14.70 5.413E+OO 1.601E-01 1.602E-01 217 .11 88.47 78 24.00 5.391E+OO 3.192E-01 3.192E-01 63.31 193.51 ------4.41* 3.791E+OO ------Line Not Found ------210.85 39 2.80 3.560E+OO 2.065E+OO 2.065E+OO 84.64 TH-230 609.32 105 45.49* 1.433E+OO 8.612E-01 8.612E-01 30.24 1120.29 44 14.92 8.738E-01 1. 793E+OO 1. 793E+OO 33.81 1764.49 ------15.30 5.813E-01 ------Line Not Found ------TH-232 105.21 ------1.10 5.215E+OO ------Line Not Found ------338.32 48 11.27 2.364E+OO 9.611E-01 9.611E-01 67.21 835. 71 8 1. 61 1.109E+00 2.330E+OO 2.330E+OO 153.03 911.20 30 25.80* 1.035E+OO 5.983E-01 5.983E-01 51. 06 968.97 35 15.80 9.841E-01 1. 211E+OO 1. 211E+OO 47.47 TH-234 63.29 174 3.70* 5.591E+00 4.492E+OO 4.492E+OO 56.68 92.59 114 4.23 5.346E+OO 2.688E+OO 2.688E+OO 46.83 U-234 609.32 105 45.49* 1.433E+OO 8.612E-01 8.612E-01 30.24 1120.29 44 14.92 8.738E-01 1.793E+OO 1. 793E+00 33.81 1764.49 ------15.30 5.813E-01 ------*Line Not Found ------U-235 89.96 38 3.47 5.369E+OO 1.098E+OO 1.098E+OO 135.57 93.35 114 5.60 5.346E+OO 2.030E+OO 2.030E+OO 46.83 143.76 42 10.96* 4.610E+OO 4.384E-01 4.384E-01 97 .11 163.33 ------5.08 4.273E+OO ------Line Not Found ------,, 185.72 80 57.20 3.905E+00 l.909E-01 1.909E-01 49.24 205.31 ------5.01 3. 621E+OO ------Line Not Found ------U-238 63.29 174 3.70* 5.591E+OO 4.492E+OO 4.492E+00 56.68 92.59 114 4.23 5.346E+OO 2.688E+OO 2.688E+OO 46.83 AM-243 43.53 ------5.90 5.049E+OO ------Line Not Found ------74.66 177 67.20* 5.476E+00 2.563E-01 2.563E-01 27.44 ANH-511 511. 00 35 100.00* 1.658E+OO l.120E-01 1.120E-01 94.85 Flag: "*" Keyline Page 4504of5809 Summary of Nuclide Activity Sample ID : G405235068 Acquisition date Page : 3 3-0CT-2016 06:05:07 Total number of lines in spectrum 44 Number of unidentified lines 6 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+10Y 22.20Y 7.04E+08Y l.41E+l0Y 1600. OOY 1600. OOY 1600.00Y 1. 41E+l0Y 1600.00Y 1. 41E+l0Y l.41E+l0Y l.41E+l0Y 7340.00Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 56 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.069E+01 2.070E+OO 2.070E-01 9. 971E-02 l.053E-01 3.334E-01 1.485E+OO 2. 967E+OO 8.924E-01 8.612E-01 l.077E+00 8.612E-01 1.955E+00 8.612E-01 5.983E-01 5. 983E-01 . 8.924E-01 3.192E-01 8.612E-01 5.983E-01 4.492E+00 8.612E-01 4.384E-01 4.492E+OO 2.563E-01 l.120E-01 3.899E+Ol 3.899E+Ol Decay Corr pCi/GRAM l.069E+Ol 3.234E+OO 2.070E-01 1.016E-01 1.073E-01 3.334E-01 1.523E+OO 2. 967E+OO 8.924E-01 8.615E-01 1.077E+OO 8.615E-01 1.955E+OO 8.615E-01 5.983E-01 5.983E-01 8.924E-01 3.192E-01 8.612E-01 5.983E-01 4.492E+OO 8.612E-01 4.384E-Ol 4.492E+OO 2.563E-01 1.120E-01 4.019E+Ol 4.019E+Ol 86.36% Decay Corr 2-Sigma Error 0.176E+01 2.047E+OO 1. 311E-01 0.776E-01 0.820E-01 1.020E-01 1.950E+OO 0.737E+OO l.882E-01 2.605E-01 0.268E+OO 2.605E-01 1.339E+OO 2.605E-01 3.055E-01 3.055E-01 l.882E-01 2.021E-01 2.604E-01 3.055E-01 2.546E+OO 2.604E-01 4.257E-01 2.546E+OO 0.703E-01 1.062E-01 "M" Manually accepted 2-Sigma %Error 16.44 63.31 63.31 76.37 76.37 30.59 128.02 24.83 21. 09 30.24 24.83 30.24 68.50 30.24 51. 06 51. 06 21. 09 63.31 30.24 51 .* 06 5 6 .'68 30.24 97 .11 56.68 27.44 94.85 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4505 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235068 Acquisition date : 3-0CT-2016 06:05:07 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 115. 24 30 108 0.60 230.03 226 8 7.14E-03 **** 5.08E+OO T 4 187.50 28 64 1. 65 374.45 366 14 6.76E-03 **** 3.88E+OO 0 329.09 18 37 0.77 657.42 652 8 4.56E-03 **** 2.42E+OO T 0 463.26 24
  • 15 0. 71 925.57 922 8 6.20E-03 71. 'J l.80E+OO T 0 519.95 15 21 1. 44 1038.87 1031 10 3.86E-03 **** l.64E+OO T 0 552.89 19 11 2 .11 1104. 71 1101 8 4. 96E-03 80.8 1. 55E+OO T 0 632.56 13 18 1. 69 1263.95 1257 11 3. 61E-03 **** 1.39E+OO T 0 719.56 22 11 2.39 1437.84 1433 13 5.99E-03 74.1 1.25E+OO T 0 729.51 25 20 4.46 1457.73 1448 16 6.85E-03 90.4 l.24E+OO 0 769.36 17 11 3.26 1537.38 1532 11 4.54E-03 **** 1.19E+OO 0 803.84 9 5 1. 40 1606.30 1602 7 2.34E-03 **** 1.15E+OO 0 840.72 13 1 1. 48 1680.01 1677 7 3.50E-03 65.5 l. lOE+OO 0 875.20 13 5 1. 52 1748.92 1744 10 3.61E-03 85.0 1.07E+OO T 0 946.61 10 6 0.95 1891.67 1886 9 2.70E-03 **** 1. OOE+OO T 0 1002.44 6 10 2.92 2003.25 1993 13 1. 73E-03 **** 9.58E-01 T 0 1157.48 8 15 1. 52 2313 .16 2306 12 2.17E-03 **** 8.50E-01 0 1231. 79 6 5 1. 47 2461. 70 2458 7 l.72E-03 **** 8.07E-01 T 0 1238.29 10 15 1. 44 2474.70 2468 12 2.76E-03 **** 8.03E-01 T Flags: "T" = Tentatively associated Page 4506 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:06:01.43 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* ":. * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235068.CNF;l *
  • Acquisition date 3-0CT-2016 06:05:07 Sensitivity 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.51 Half life ratio : ***** *
  • Sample date 11-DEC-2015 10:27:00 Nuclide Library : SOLID *
  • Sample ID G405235068 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4091E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff. Geometry : CAN *
  • Eff. File DKAlOO: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;?
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-22 6 AC-228 RA-228 TH-228 TH-229 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM O.OOOE+OO 7.970E-01 5.097E-02 3.670E-02 3.877E-02 3.378E-02 5.933E-01 5. 966E-02 6.876E-02 6. 960E-02 6.876E-02 6.876E-02 1.777E-01 1.777E-01 5. 966E-02 4.606E-01 6.874E-02 l.777E-01 6.735E-01 6.874E-02 l.957E-01 6.735E-01 3.465E-02 3.655E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4507 of 5809 Le (pCi/GRAM 1.448E+Ol 4.986E-02 O.OOOE+OO 3.792E-02 4.227E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-..73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4508 of 5809 7.550E-02 4.341E-01 O.OOOE+OO 4.627E-02 7;156E-01 8.454E+OO 5.098E-02 2.174E-01 3.650E+OO 3.209E+OO O.OOOE+OO 2.037E-01 O.OOOE+OO O.OOOE+OO 8.875E-01 1.054E+Ol 1.078E+00 O.OOOE+OO 2.847E-01 7.125E+02 4.567E-02 9.828E-01 2.274E+OO 1. 786E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.278E-02 8.806E-02 6.833E+OO 6.534E-01 6.534E-01 3.229E-02 l.128E-01 1. 979E-01 O.OOOE+OO O.OOOE+OO l.384E-01 2.625E+OO 1.017E-01 2. 411E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 4.432E-02 O.OOOE+OO 6. 991E-02 1.672E-01 O.OOOE+OO O.OOOE+OO 1.093E-01 O.OOOE+OO O.OOOE+OO 2.400E+Ol O.OOOE+OO 3.674E-01 7.488E-02 6.520E+00 4.953E-02 O.OOOE+OO 7.928E+02 o. a*ooE+oo 2.840E-02 9.771E-02 1.303E-01 1.243E-01 1.015E-01 2.031E+OO 7.349E-02 7.400E+OO 2.446E-01 1. 079E-01 2.271E-02 5.463E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 RA-224 AC-227 TH-227 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-'247 CF-249 CF-251 Page 4509 of 5809 9.409E-01 1.552E+OO 3.212E+01 1. 324E+02 5.546E-01 2.446E+OO 2.736E-02 5.269E-01 7.739E-01 7.013E-01 5.431E-01 7.029E-01 9.044E-01 2.247E-01 2.247E-01 5.791E-01 7.029E-01 7.553E-02 3.710E-01 5.579E+OO 7.553E-02 O.OOOE+OO 2.261E-01 3.326E+02 7.193E-02 8.745E-02 7. 611E-02 4.746E-02 4.569E-02 1.346E-01 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:06:07.38 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235068.CNF;l *
  • Acquisition date 3-0CT-2016 06:05:07 Sensitivity : 3.000 *
  • Detector ID GAM31 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:06.51 Half life ratio : ***** *
  • Sample date 11-DEC-2015 10:27:00 Nuclide Library : SOLID *
  • Sample ID G405235068 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4091E+02 GRAM *
  • Quantity Err(%) : 1.4194E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 15-JUN-2016 06:54:07 Eff. G'eometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM31 CAN.CNF;?
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM (1.96-sigma) K-40 l.069E+Ol 1. 811E+OO CD-109 1.494E+OO 2.082E+OO SN-126 9.563E-02 l.332E-01 BA-137M 1.016E-01 7.616E-02 CS-137 l.073E-01 8.046E-02 TL-208 3.334E-01 1.009E-01 PB-210 1.523E+OO 1.915E+OO PB-212 8.924E-01 1.904E-01 BI-214 8.615E-01 2.580E-01 PB-214 1.077E+OO 2.660E-01 RN-222 8.615E-01 2.580E-01 RA-226 8.615E-01 2.580E-01 AC-228 5.983E-01 3.0lOE-01 RA-228 5.983E-01 3.0lOE-01 TH-228 8.924E-01 1.904E-01 TH-229 -3.292E-01 5.829E-01 TH-230 8.612E-01 2.579E-01 TH-232 5.983E-01 3.0lOE-01 TH-234 4.492E+OO 2.686E+OO U-234 8.612E-01 2.579E-01 U-235 4.384E-01 4.178E-01 U-238 4.492E+OO 2.686E+OO AM-243 l.519E-01 7.678E-02 ANH-511 1.120E-01 l.042E-01 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4510 of 5809 Key-Line Activity (pCi/GRAM 4.472E+OO 1. 986E-02 -1.000E+41 -2.300E-02 1.296E-01 9.762E+03 K.L Act error ( 1. 96-sigma) 1.606E+Ol 5.325E-02 9.957E+41 5.202E-02 4.540E-01 l.731E+04 TPU ( 1. 96-sigma) l.811E+00 2.082E+OO 1.332E-01 7.616E-02 8.046E-02 1.009E-01 1.91.5E+OO l.904E-01 2.580E-01 2.660E-01 2.580E-01 2.580E-01 3.0lOE-01 3.0lOE-01 1.904E-01 5.829E-01 2.579E-01 3.0lOE-01 2.686E+OO 2.579E-01 4.178E-01 2.686E+OO 7.678E-02 l.042E-01 TPU ( 1. 96-sigma) 1.619E+Ol 5.400E-02 0.000E+OO 5.304E-02 4.577E-01 1.787E+04 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 -2.614E+02 4.575E+02 4.725E+02 SHORT HLIF MN-54 3.464E-02 8.859E-02 8.995E-02 NOT IDENT. C0-56 -2.422E-01 5.958E-01 6.057E-01 FAIL ABUN MN-56 -1.000E+41 2.461E+41 O.OOOE+OO SHORT HLIF C0-57 2.620E-02 4. 981E-02 5 .119E-02 NOT IDENT. C0-58 8.435E-02 8.493E-01 8.502E-01 NOT IDENT. FE-59 -1.391E+OO 1.012E+Ol 1.014E+Ol NOT IDENT. C0-60 -1.952E-02 6.536E-02 6.595E-02 NOT IDENT. ZN-65 2.643E-01 1.998E-01 2.327E-01 NOT IDENT. GE-68 1.726E+OO 3.943E+OO 4. 019E+O.O NOT IDENT. AS-73 -1. 626E+OO 3.615E+OO 3.689E+OO NOT IDENT. AS-74 5. 962E+03 6.864E+03 7.371E+03 SHORT HLIF SE-75 -1.112E-02 2.482E-01 2.482E-01 NOT IDENT. BR-77 6.672E+37 5.718E+38 0.000E+OO SHORT HLIF SR-82 -1.086E+03 9.878E+02 1.102E+03 SHORT HLIF RB-83 1.149E+OO 1.495E+OO 1.582E+OO FAIL ABUN KR-85 1.320E+Ol 1.339E+Ol 1.465E+Ol NOT IDENT. SR-85 1.348E+OO l.370E+OO 1.499E+OO NOT IDENT. RB-86 1.194E+04 4.144E+04 4.179E+04 SHORT HLIF Y-88 -l.357E-01 3.766E-01 3.815E-01 NOT IDENT. Y-91 3.099E+Ol 8.319E+02 8.320E+02 NOT IDENT. NB-94 -2.935E-03 5.579E-02 5.581E-02 NOT IDENT. NB-95 2.340E-01 1. 2 67E+OO 1.271E+OO NOT IDENT. NB-95M -1.254E+OO 3.166E+OO 3.216E+OO NOT IDENT. ZR-95 7.702E-01 1.988E+OO 2.018E+OO NOT IDENT. NB-97 l.000E+41 5 .111E+41 0.000E+OO SHORT HLIF ZR-97 -l.000E+41 1.889E+42 0.000E+OO SHORT HLIF M0-99 -9.004E+31 'l.178E+32 O.OOOE+OO SHORT HLIF TC-99M 1.000E+41 3.359E+41 O.OOOE+OO SHORT HLIF RH-101 -4.569E-02 4.248E-02 4.721E-02 NOT IDENT. RH-102 1.068E-01 l.469E-01 1.546E-01 FAIL ABUN RU-103 3.633E+OO 7.300E+OO 7.482E+OO FAIL ABUN RH-106 3.073E-01 7.158E-01 7.291E-01 NOT IDENT. RU-106 3.073E-01 7.158E-01 7. 291E-01 NOT IDENT. AG-108M 5.132E-04 3. 671E-02 3. 671E-02 NOT IDENT. AG-llOM -3.555E-02 l.357E-01 1.366E-01 NOT IDENT. SN-113 -2.922E-01 2. 724E-01 3.026E-01 NOT IDENT. CD-115 -1.152E+38 l.599E+39 0.000E+OO SHORT HLIF SN-ll 7M 1.887E+04 9.776E+04 9. 813E+o4 SHORT HLIF TE-123M 9.658E-02 1. 496E-01 1.558E-01 NOT IDENT. SB-124 -8.631E-01 3.515E+OO 3.537E+OO NOT IDENT. SB-125 -4.405E-02 l.232E-01 1.248E-01 FAIL ABUN TE-125M 8.862E+Ol 2.626E+02 2.657E+02 NOT IDENT. I-126 1.288E+06 l.144E+06 1.283E+06 SHORT HLIF SB-126 2.993E+06 2.243E+06 2.618E+06 SHORT HLIF SB-127 3.589E+21 2.034E+22 O.OOOE+OO SHORT HLIF I-131 1.256E+09 4.617E+09 4.651E+09 SHORT HLIF I-132 l.000E+41 1.870E+42 O.OOOE+OO SHORT HLIF TE-132 2.186E+26 3.120E+26 O.OOOE+OO SHORT HLIF BA-133 -6.029E-03 5.625E-02 5.632E-02 FAIL ABUN I-133 -l.000E+41 1. 2 62E+42 O.OOOE+OO SHORT HLIF CS-134 7.486E-02 6. 968E-02 7.742E-02 NOT IDENT. CS-135 -1.805E-01 2.258E-01 2.400E-01 NOT IDENT. I-135 1.000E+41 7.283E+41 O.OOOE+OO SHORT HLIF CS-136 -4.616E+05 3.782E+05 4.317E+05 SHORT HLIF CE-139 -6.925E-02 l.355E-01 1.391E-01 NOT IDENT. BA-140 -2.903E+05 l.453E+06 1.459E+06 SHORT HLIF LA-140 3.038E+05 5.565E+05 5.731E+05 SHORT HLIF CE-141 3.398E+OO 3.00lE+Ol 3.005E+Ol NOT IDENT. CE-143 1.000E+41 2 .112E+41 O.OOOE+OO SHORT HLIF CE-144 -8.120E-02 4.275E-01 4.291E-01 NOT IDENT. PM-144 1. 596E-02 8.658E-02 8.688E-02 NOT IDENT. PR-144 3.554E+OO 7.149E+OO 7.326E+OO NOT IDENT. PM-146 1.583E-03 5. 641E-02 5. 641E-02 FAIL ABUN ND-147 8.682E+06 3.638E+07 3.659E+07 SHORT HLIF PM-147 5.748E+02 8.389E+02 8.780E+02 NOT IDENT. PM-149 -3.291E+39 2.236E+40 0.000E+OO SHORT HLIF EU-150 3.462E-03 3.452E-02 3.456E-02 FAIL ABUN EU-152 -9.092E-02 l.278E-01 1.342E-01 NOT IDENT. GD-153 -1.268E-01 l.728E-01 1. 821E-01 NOT IDENT. EU-154 5.290E-02 1.320E-01 1.341E-01 NOT IDENT. EU-155 6.667E-02 1.077E-01 1.118E-Ol FAIL ABUN TB-160 -1.441E+OO 3. 013E+OO 3.082E+OO FAIL ABUN H0-166M -2.656E-02 9.724E-02 9.797E-02 NOT IDENT. TM-171 -3.650E+OO 8.285E+OO 8.447E+OO NOT IDENT. HF-172 1.495E-01 2.651E-01 2.735E-01 FAIL ABUN LU-172 6.472E-03 l.243E-01 1.244E-01 FAIL ABUN LU-176 -2.207E-02 2. 813E-02 2.984E-02 FAIL ABUN Page 4511 of 5809 HF-181 -1.574E-01 6.308E+OO 6.308E+OO NOT IDENT. TA-182 -3. 451E-01 l.191E+00 1. 201E+OO FAIL ABUN RE-183 1. 749E+OO 1.605E+OO 1. 788E+OO NOT IDENT. RE-184 -1.444E+Ol 3. 969E+Ol 4.023E+Ol NOT IDENT. W-188 1. 201E+02 1.442E+02 l.541E+02 FAIL ABUN IR-192 3.002E-01 5.803E-01 5.958E-01 FAIL ABUN HG-203 -1.136E+OO 3.446E+OO 3.484E+OO NOT IDENT. BI-207 -2.036E-02 3.991E-02 4.095E-02 FAIL ABUN BI-211 2. 967E+OO 7.342E-01 1.526E+OO FAIL ABUN PB-211 .-3. 059E-01 9.183E-01 9.286E-01
  • NOT IDENT . BI-212 5.943E-01 7.664E-01 8 .119E-01 NOT IDENT. RN-219 7.448E-01 5. 311E-01 6.283E-01 NOT IDENT. RA-223 2.950E-01 8.192E-01 8.300E-01 FAIL ABUN RA-224 l.955E+OO l.316E+OO 1.584E+OO FAIL ABUN AC-227 -l.052E-01 2.877E-01 2.916E-01 NOT IDENT. TH-227 -1.052E-01 2.877E-01 2.916E-01 NOT IDENT. PA-231 4.789E-01 5.997E-01 6.374E-01 NOT IDENT. TH-231 2.950E-01 8.192E-01 8.300E-01 FAIL ABUN PA-233 3.054E-02 8.029E-02 8.146E-02 NOT IDENT. PA-234 4.288E-01 6.884E-01 7.150E-01 FAIL ABUN PA-234M 4.103E+OO 9.124E+OO 9.309E+OO FAIL ABUN NP-237 3.054E-02 8.029E-02 8.146E-02 NOT IDENT. NP-238 1.000E+41 2.463E+41 O.OOOE+OO SHORT HLIF NP-239 4.019E-01 5.364E-01 5.662E-01 FAIL ABUN PU-239 9. 966E+Ol 3.697E+02 3.724E+02 NOT IDENT. AM-241 2.063E-03 8.357E-02 8.357E-02 NOT IDENT. CM-243 -2.183E-02 1.00lE-01 1. 006E-01 FAIL ABUN BK-247 2.102E-02 8: 881E-02 8. 931E-02 FAIL ABUN CM-247 2.711E-02 5.056E-02 5.202E-02 FAIL ABUN CF-249 3.777E-02 4.644E-02 4.946E-02 NOT IDENT. CF-251 l.857E-01 1.381E-01 1.615E-01 NOT IDENT. Page 4512of5809
  • GEL Laboratories LLC *
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  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 89.4408 87.09 59.3402 136.47 49.3451 45.60 101.7740 87.57 59.4031 140.51 0.0000 46.54 102.0990 88.03 59.4632 143.76 57. 3511 49. 72 0.0000 88.34 59.5039 144.24 57.3940 51. 35 127.2471 88.47 59.5204 145.44 46.8521 51. 87 130.0749 89. 96 59. 7139 152.43 45.1973 52.39 127.6637 1093.63 59.8014 153.25 0.0000 52.97 118.2579 91.11 0.0000 323.87 47.4744 53.44 123.6934 92. 59 60.0507 156.02 0.0000 54.07 117.7796 93.35 60.1472 158.56 0.0000 57.36 0.0000 94.56 53.1677 159.00 35.8551 57.53 122.5588 94.65 53.1777 162.33 56.7687 57.98 110.2696 94.67 53.1798 162.66 0.0000 59.27 123.7735 94.87 53.2023 163.33 36.0776 59.32 123.7909 97.43 57.3973 165.86 50.4690 59.54 119 .1050 98.43 51.9592 176.31 50.0819 60. 96 109. 4218 98.44 51. 9600 '176.60 0.0000 61.17 109.4865 99.53 53.0574 177.52 27.8679 62.93 110.0245 100 .11 47.2170 181.07 0.0000 63.29 110.1341 102.03 59.2474 181.52 34.3657 63.58 110.2216 103.18 55.4232 184.41 33.7450 64.28 110.4324 103.37 55.4442 143.76 33.8022 66.73 112.9843 105.21 44.7133 193.51 45.5164 67.24 105.8374 105.31 44. 7219 197.03 54.8584 125.81 116.9219 106.12 45.7873 198.01 37.7605 67.75 116. 9424 106.47 44.8222 201.83 52.8815 69.67 103.7563 109.28 44. 0611 203.43 42.6170 70.83 120.3337 111. 00 48.2219 205.31 51.9482 72.81 95.0218 111. 76 0.0000 210.85 43.3809 72.87 95.0359 114. 06 52.5368 215.65 32.7177 74.66 92.9794 116. 30 0.0000 222 .11 42.3759 74.82 93.0153 116.74 44.6707 227.09 40.2448 74.97 93.0496 119.76 53.0779 227.38 36.7051 77 .11 93.5341 121.12 35.8112 228.16 0.0000 78.74 93.8988 121.22 35.8174 228.18 39.1079 79.69 52.7017 121. 78 35.8526 116.74 39.1079 80.12 65.9433 122.06 39. 9694 235.69 39.8275 80.19 0.0000 122.92 40.0295 235. 96 35.0585 80.57 66.0127 123.07 54.4132 238.63 41.5512 81. 00 79.2947 265.00 65.7759 238.98 0.0000 81. 07 79.3076 125.81 47.4494 240.99 67.2896 81. 75 66.1938 127.23 73.4140 242.00 35.2845 83.79 58.9031 127.91 57.9709 244.70 32.1680 84.00 58.9315 129.30 54.9935 252.40 0.0000 85.43 59.1217 131.20 55.1674 252.80 32.8440 86.55 59.2692 133.02 50.1130 254.15 0.0000 86.79 59.3005 133. 52 56.4233 256.23 30.5172 86. 94 59.3208 136. 00 51.4060 2 60. 90 0.0000 Page 4513 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 24.6204 355.39 0.0000 584.27 11. 3160 264. 80 24.6234 356.01 22.6725 595.83 0.0000 265.00 23. 3969 364.49 0.0000 427.87 13.4882 268.22 51.8835 366.42 0.0000 602.52 0.0000 269.46 33.3940 372.51 26.1143 604.72 14.0367 270.03 19.7998 375.05 29.7733 607.14 12.4927 271.23 28.4952 377.52 24.4056 609.32 12.5068 273.65 0.0000 356.01 20.8877 610.33 12.5132 276.40 33.6173 388.16 14.5768 614.28 12.5386 277.37 33.2332 388.63 0.0000 618.01 20.9367 277.60 33.2406 391.69 24.6621 62 0. 36 15.7214 278.00 29.9282 264.66 26.6612 621. 93 12.5869 279.20 33.2910 401.81 13.8016 630.19 0.0000 279.54 28.3064 402.40 22.0918 631. 29 11.5922 279.70 28.3105 404.85 25.8188 633.25 7. 9114 280.46 46.6632 410.95 16.6692 634.78 0.0000 283.69 26.7454 413.71 23 .1964 635.95 9.5065 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 31. 8112 423.72 0.0000 645.85 20.1674 285.90 0.0000 427.09 17.7924 657.76 9.6083 287.50 36.9057 427.87 17.8021 657.90 0.0000 290.67 21.4513 433.94 18.8159 661. 66 11. 7 654 293.27 0.0000 439.40 10.3866 664.57 0.0000 351.93 21'. 9629 453.88 17.1584 666.33 0.0000 295. 96 21.9777 463.37 22.0590 666.50 0.0000 879.38 30.5024 468.07 21.9326 667. 71 0.0000 299.98 28.5045 473.00 0.0000 677.62 19.3982 300.09 28.5072 475.06 15.4590 685.70 0.0000 300.13 28.5086 476.78 18.3773 695.00 0.0000 301.36 27.1810 477.60 14.5157 696.49 16.3074 302.85 39.1241 482.18 22.3210 696. 51 13.0459 256.23 24.7015 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 16.3135 306.78 28.1653 497.08 13.7106 697.49 16.3147 308.46 23.0784 505.52 19.1937 702.65 20. 7140 311. 90 27.4342 507.63 0.0000 706.68 22. 9371 316.51 23.2399 511. 00 22.7122 711. 68 17.5150 319.41 0.0000 514.00 14.8389 720.70 0.0000 320.08 0.0000 514.00 14.8389 721.93 0.0000 321. 04 24.1947 520.40 14.8944 722. 78 13.2017 323.87 23.3866 520.69 0.0000 722.91 13.2026 325.23 28.6158 522.65 0.0000 723.31 13.2051 328.76 0.0000 527.90 0.0000 724 .19 13.2100 333.37 20.9536 528.26 13.9647 727.33 11. 9057 333.97 23.5844 529.59 16. 9696 733.00 9.9463 334.37 24.9027 529.87 0.0000 735.93 7.7460 338.28 28.0508 531. 02 0.0000 333.97 11. 0730 338.32 28.0514 537.26 0.0000 739.50 0.0000 311. 90 25.0274 546.56 0.0000 747.24 16.6803 340.48 25.0274 552.55 18.2021 748.06 13.3491 340.55 0.0000 563.25 19.3263 752.31 15.6025 344.28 30.6539 569.33 21.4315 753.82 0.0000 345.93 15.8767 946.00 21.4332 756.73 10.0492 351.06 19.4841 569.70 21.4358 756.80 7.8163 351. 93 19.4975 583.19 11. 3097 884.68 11.7604 Page 4514 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 11. 7 698 1274.44 8.8081 1620.50 5.4456 766.42 13.4546 1001.03 9.1898 1621. 92 3.2684 766.84 13. 4570 1002.74 10.2987 1678.03 0.0000 772. 60 0.0000 1004.73 7. 3611 1690.97 5.5310 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000. 1025.87 0.0000 1764.49
  • 1.1237 778.90 10.1440 1028.54 0.0000 1063.66 9.0000 783.70 0.0000 1037.84 12.0947 1771. 35 3.6010 785.37 18.0827 1038.76 0.0000 1791.20 0.0000 792.07 21. 5327 631.29 13.9957 1808.65 5.4431 794.95 10.2118 1048.07 0.0000 1810.72 0.0000 795.86 6.8105 1049.04 12.1391 1836.06 5.4735 810.06 10.2751 1050.41 7.4736 810.29 13.7012 1063.66 4.6912 344.28 13.7021 1077.00 0.0000 810.76 11. 4201 1077.34 11. 3086 815.77 0.0000 1085.87 11. 3394 1048.07 0.0000 1093.63 12.3145 832.01 8.6380 1099.45 12.3367 834.85 5.1887 1112. 07 10.4797 835.71 6.9207 1112. 84 9.5294 836.80 0.0000 1115. 54 1. 5260 846.75 0.0000 1120.29 9.5514 846.77 10.4260 1120.55 9.5526 856.80 0.0000 1221. 41 9.5544 860.56 12. 8114 1129. 67 10.5374 871.09 11.2262 1131. 51 0.0000 873.19 9.8308 1147.95 0.0000 875.33 0.0000 1173.23 10.6764 879.38 14.0767 1177.95 10.6912 880.51 10.5623 1189.05 8.7764 883.24 7.9297 1204.77 12.7350 884.68 11.4603 1221.41 9.8431 889.28 7.0647 1231. 02 13.5368 894.76 7. 9640 1235.36 0.0000 898.04 7.9739 1238.28 10.1733 900.72 6.2081 1260.41 0.0000 903.28 12.4277 1271.87 7.9878 911. 20 14.2446 1274.44 3. 9966 912.08 15.6745 1274.54 3.9968 923.98 0.0000 1291.59 15.0586 926.50 7.1624 1298.22 0.0000 929 .11 7.1689 1312 .11 0.0000 937.49 19.7744 1332.49 10.1501 944.13 0.0000 1362.66 0.0000 946.00 7.2126 1365.19 10.2380 949.00 5.7762 1368.63 0.0000 667.71 0.0000 1384.29 4 .1157 962. 31 14.5088 1408.01 5.1758 964.08 6.0490 1457.56 0.0000 966 .17 10.1698 1460.82 0.0000 911. 20 14.5425 1489.16 7.3935 968. 97 14.5425 1505.03 2.1206 983.53 0.0000 1584.12 6.4808 984.45 0.0000 1596.21 0.0000 Page 4515of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:06:37.26 ******************************************************************************** *
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235069.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM43.CNF;l51 Background date : Z-OCT-2016 11:02:23. Sample date 16-DEC-2015 12:45:00 Acquisition date : 3-0CT-2016 06:05:34. Sample ID G405235069 Sample quantity 1.56084E+02 GRAM Detector name : GAM43 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.70 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 4 4 4 4 0 0 4 4 0 0 4 4 0 1 1 0 0 0 0 0 0 0 0 0 7 7 0 0 0 0 0 4 4 Page 4516of5809 Energy 63.50* 72. 58 74.74 77.04 83.40* 86.99 92.73* 129.16 131.74 150.51 185.71* 238.54* 241. 67 273.05 294.98* 299.95* 338.69 351.93* 395. 96 465.08 504.15 510.37* 578.09 583.14* 601.94 609.06* 615.09 728.05 796 .10 808.59 836.58 854.30 910.97 914.78 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 20 41 95 164 37 31 46 59 30 33 64 317 104 34 141 55 63 273 31 19 13 41 21 110 23 186 20 28 17 9 11 11 102 11 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 102 80 130 118 112 123 207 109 24 98 151 73 75 113 67 55 74 60 79 54 15 38 25 22 17 11 31 35 22 21 16 11 7 4 1.18 1. 32 1.11 1.14 1. 38 0.75 1. 82 1. 82 1. 26 1. 39 1. 28 1. 04 1. 57 4.09 1. 65 1. 66 1.11 1.12 6.20 3.26 0.87 1. 81 0.93 1. 81 3.84 1. 99 3.60 0.70 1. 42 2.87 1. 34 1. 53 2.42 1. 43 126.79 144.95 149.27 153.88 166.59 173.79 185.27 258.15 263.32 300.86 371. 27 476.97 483.23 546.01 589.88 599.82 677.33 703.81 791.90 930.17 1008.32 1020.77 1156.22 1166. 34 1203.94 1218.19 1230.25 1456.21 1592.32 1617.31 1673.30 1708.74 1822.10 1829.73 124 143 143 143 143 171 181 254 254 297 366 471 471 534 585 585 672 699 779 920 1005 1012 1149 1161 1197 1210 1210 1445 1585 1606 1666 1704 1816 1816 6 5.49E-03 86.4 29 1.14E-02 32.2 3.71E+OO 29 2.64E-02 22.1 29 4.56E-02 13.5 29 1.03E-02 56.0 7 8. 61E-03 61. 9 10 1. 29E-02 61. 7 12 1.63E-02 34.0 6.29E+OO 12 8.26E-03 31.7 8 9.llE-03 55.1 11 1.78E-02 40.0 29 8.81E-02 7.1 l.14E+OO 29 2.90E-02 19.5 16 9.46E-03 72.6 21 3.91E-02 13.5 2.88E+OO 21 1. 53E-02 30. 0 12 1.74E-02 30.4 12 7.60E-02 8.4 24 8.74E-03 76.4 15 5.18E-03 90.3 7 3.47E-03 57.4 15 1.15E-02 41. 5 13 5.79E-03 54.9 11 3.06E-02 12.8 14 6.36E-03 43.9 31 5.16E-02 8.5 1.73E+OO 31 5.61E-03 79.2 18 7.87E-03 52.9 13 4.62E-03 63.9 15 2.38E-03124.8 11 3.05E-03 77.6 8 2.94E-03 64.0 17 2.85E-02 11.3 2.18E+OO 17 3.00E-03 41.6 Peak Search Report (continued) Page : 2 Sample ID : G405235069 Acquisition date 3-0CT-2016 06:05:34 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 6 964 .12* 17 9 2.70 1928.42 1924 18 4.63E-03 41. 5 1.72E+OO 36 6 968. 71 32 13 1. 71 1937.59 1924 18 8.77E-03 27.5 37 Q 987.78 18 3 3.72 1975.75 J.968 13 4.88E-03 32.0 38 0 1121.30 35 50 1. 06 2242.81 2232 20 9. 72E-03 52.3 39 0 1347.63 11 6 3.92 2695.49 2688 13 3.09E-03 55.5 40 0 1351.24 7 0 0.58 2702.71 2700 7 1.94E-03 37.8 41 0 1401. 29 6 4 0.87 2802.83 2798 8 1.67E-03 70.7 42 0 1460.73* 316 8 2.13 2921.71 2913 16 8.78E-02 6.0 43 0 1589.05 7 6 1. 34 3178.36 3168 12 1. 94E-03 79.5 44 0 1620.74 11 0 0.62 3241. 73 3235 12 3.06E-03 30.2 45 0 1764.78* 32 0 2.06 3529.80 3523 13 8.93E-03 18.6 Flag: "*" = Peak area was modified by background subtraction Page 4517 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:06:39 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235069.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 16-DEC-2015 12:45:00 G405235069 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:05:34 156.08 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA43 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4518of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.70 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235069 Acquisition date 3-0CT-2016 06:05:34 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1.00lE+OO 1.378E+Ol 1. 378E+Ol 12.06 OK CD-109 88.03 3.70* 4.279E+OO 2.403E-01 3.725E-01 637. 96 OK SN-126 64.28 9.60 1. 895E+OO 6.959E-01 6.959E-01 172.79 OK 86.94 8.90 4.279E+OO 9.991E-02 9. 991E-02 637. 96 OK 87.57 37.00* 4.279E+OO 2.403E-02 2.403E-02 637. 96 OK TL-208 277.37 6.60 4.205E+OO Line Not Found Absent 583.19 85.00* 2.199E+OO 3.050E-01 3.050E-01 25.69 OK 860.56 12.50 1.582E+OO Line Not Found Absent BI-211 72. 87 1.23 2.909E+OO 7.277E+OO 7.277E+OO 64.49 OK 351.06 12.92* 3.426E+OO 4.410E-01 4.410E-01 220.90 OK BI-212 727. 33 6.67* 1. 821E+OO 1.177E+OO 1.177E+OO 105.88 OK 785.37 1.10 1. 708E+OO Line Not Found Absent 1620.50 1. 47 9.085E-01 3.788E+OO 3.788E+OO 60.30 OK PB-212 74.82 10.28 3 .139E+OO 1.263E+OO 1.263E+OO 66.43 OK 77 .11 17.10 3.375E+OO 1. 791E+OO 1. 791E+OO 27.05 OK 238.63 43.60* 4.740E+OO 8.697E-01 8.697E-01 14.13 OK 300.09 3.30 3.937E+OO 2.347E+OO 2.347E+OO 59.94 OK BI-214 609.32 45.49* 2 .118E+OO 9.923E-01 9.927E-01 17.02 OK 1120.29 14.92 1.265E+OO 8.909E-01 8.912E-01 104.59 OK 1764.49 15.30 8.361E-01 1.144E+OO l.145E+OO 37.13 OK PB-214 74.82 5.80 3.147E+OO Line Not Found <<INT Reject 77 .11 9.70 3.375E+OO 3.158E+OO 3.159E+OO 27.05 OK 87.09 3.41 4.287E+OO Line Not Found <<INT Reject 242.00 7.25 4.688E+OO Line Not Found <<INT Reject 295.22 18.42 3.993E+OO 1.062E+OO 1. 062E+OO 27.09 OK 351. 93 35.60* 3.426E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2 .118E+OO 9.923E-01 9.927E-01 17.02 OK 1120.29 14.92 1.265E+OO 8.909E-01 8.912E-01 104. 5,9 OK 1764.49 15.30 8.361E-01 1.144E+OO 1.145E+OO 37.13 OK RA-224 240.99 4.10* 4.693E+OO 1.193E+OO l.193E+OO 109.08 OK RA-226 609.32 45.49* 2 .118E+OO 9.923E-01 9.927E-01 17.02 OK 1120.29 14.92 1.265E+OO 8.909E-01 8.912E-01 104.59 OK 1764.49 15.30 8. 361E-01 1.144E+OO 1.145E+OO 37.13 OK AC-228 105.21 1.10 5. 396E+OO Line Not Found Absent 338.32 11. 27 3.543E+OO 8.576E-01 8.576E-01 60.80 OK 794.95 4.25 1.689E+OO 1.157E+OO l.157E+OO 127.82 OK 835.71 1. 61 1.620E+OO 2.088E+OO 2.088E+OO 155.20 OK 911. 20 25.80* 1.508E+OO 1.295E+OO 1.295E+OO 22.53 OK 968.97 15.80 1.432E+OO 6.816E-01 6.816E-01 54.95 OK RA-228 105.21 1.10 5. 396E+OO Line Not Found Absent 338.32 11. 27 3.543E+OO 8.576E-01 8.576E-01 60.80 OK 794.95 4.25 1. 689E+OO 1.157E+OO l.157E+OO 127.82 OK 835. 71 1. 61 1.620E+OO 2.088E+OO 2.088E+OO 155.20 OK 911. 20 25.80* 1.508E+OO 1.295E+OO 1.295E+OO 22.53 OK 968. 97 15.80 1.432E+OO 6.816E-01 6.816E-01 54.95 OK TH-228 74.82 10.28 3.139E+OO 1.263E+OO 1.263E+OO 66.43 OK 77 .11 17.10 3.375E+OO 1.791E+OO 1. 791E+OO 27.05 OK 238.63 43.60* 4.740E+OO 8.697E-01 8.697E-01 14 .13 OK 300.09 3.30 3.937E+OO 2.347E+OO 2.347E+OO 59.94 OK Page 4519 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235069 Acquisition date 3-0CT-2016 06:05:34 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 45.49* 2 .118E+OO 9.923E-Ol 9.923E-01 17.02 OK 1120.29 14.92 1. 2 65E+OO 8.909E-01 8.909E-01 104.59 OK 1764.49 15.30 8.361E-01 1.144E+OO 1.144E+OO 37.13 OK PA-231 283.69 1. 70 4.127E+OO Line Not Found Absent 301.36 5.35* 3.937E+OO 1.448E+OO 1.448E+OO 59.94 OK TH-232 105.21 1.10 5.396E+OO Line Not Found Absent 338.32 11. 27 3.543E+OO 8.576E-01 8.576E-01 60.80 OK 835.71 1. 61 1.620E+OO 2.088E+OO 2.088E+OO 155.20 OK 911.20 25.80* 1.508E+00 1.295E+OO 1.295E+OO 22.53 OK 968. 97 15.80 l.432E+OO 6.816E-01 6.816E-01 54.95 OK TH-234 63.29 3.70* l.895E+00 1.806E+OO 1.806E+OO 172.79 OK 92.59 4.23 4.706E+OO 1. 441E+OO 1. 441E+OO 123.42 OK U-234 609.32 45.49* 2 .118E+OO 9.923E-01 9.923E-01 17.02 OK 1120.29 14.92 1.265E+OO 8.909E-01 8.909E-01 104.59 OK 1764.49 15.30 8.361E-01 1.144E+OO 1.144E+OO 37 .13 OK U-238 63.29 3.70* 1.895E+OO 1.806E+OO 1.806E+OO 172.79 OK 92.59 4.23 4.706E+OO 1.441E+OO 1. 441E+OO 123.42 OK AM-243 43.53 5.90 1.216E-01 Line Not Found Absent 74.66 67.20* 3.139E+OO 1. 931E-01 1.9'32E-01 66.43 OK ANH-511 511. 00 100.00* 2.468E+OO 8.804E-02 8.804E-02 83.01 OK Flag: "*" = Keyline Page 4520 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:06:40.24 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235069.CNF;l *
  • Acquisition date 3-0CT-2016 06:05:34 Sensitivity : 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.70 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:45:00 Analyst initials: MXRl *
  • Sample ID G405235069 Sample Quantity l.5608E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;?
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.378E+Ol 1.629E+OO 6.354E-01 CD-109 3. 725E-01 2.329E+OO 2. 725E+00 SN-126 2.403E-02 1.502E-01 1.772E-01 TL-208 3.050E-01 7.678E-02 6.104E-02 BI-211 4.410E-01 9.548E-01 3.603E-01 BI-212 1. l 77E+OO 1.221E+OO 8.565E-01 PB-212 8.697E-01 1. 204E-01 9.402E-02 BI-214 9.927E-01 l.656E-01 1.230E-01 PB-214 1.222E+OO 2.015E-01 3.443E-01 RN-222 9.927E-01 l.656E-01 l.230E-01 RA-224 1.193E+OO 1.275E+OO 1.008E+00 RA-22 6 9.927E-01 1.656E-01 1.230E-01 AC-228 1. 295E+OO 2.859E-01 2.241E-01 RA-228 1.295E+OO 2.859E-01 2.241E-01 TH-228 8.697E-01 1. 204E-01 9.402E-02 TH-230 9.923E-01 1.655E-01 1.229E-01 PA-231 1.448E+OO 8.505E-01 7.827E-01 TH-232 1.295E+OO 2.859E-01 2.241E-01 TH-234 1.806E+OO 3.058E+OO 3. 671E+OO U-234 9.923E-01 l.655E-01 1.229E-01 U-238 1. 806E+OO 3.058E+OO 3.671E+00 AM-243 1.932E-01 1.257E-01 l.184E-01 ANH-511 8.804E-02 7.163E-02 4.285E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -l.182E-01 1.022E+Ol 1.942E+Ol NOT IDENT. NA-22 5.040E-03 5.459E-02 l.102E-01 NOT IDENT. NA-24 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF AL-26 -3.007E-02 3.264E-02 4.684E-02 NOT IDENT. SC-46 -4.310E-01 3.735E-01 5.770E-01 FAIL ABUN V-48 O.OOOE+OO 1.015E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 3.077E+02 O.OOOE+OO SHORT HLIF Page 4521of5809 MN-54 l.263E-02 7. 291E-02 1.439E-01 NOT IDENT. C0-56 3.948E-01 4. 723E-01 l.030E+00 NOT IDENT. MN-56 O.OOOE+OO l.184E+41 0.000E+OO SHORT HLIF C0-57 -1.324E-02 4.895E-02 8.752E-02 NOT IDENT. C0-58 1.931E-01 4.925E-01 9.692E-01 NOT IDENT. FE-59 l.494E+OO 6.201E+OO 1.253E+Ol NOT IDENT. C0-60 1.627E-02 3. 651E-02 8.274E-02 NOT IDENT. ZN-65 2.258E-02 2.152E-01 3.669E-01 NOT IDENT. GE-68 1.245E+OO 2.709E+OO 5.549E+OO NOT IDENT. AS-73 1.136E+Ol 1.621E+Ol 3.305E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.762E+03 O.OOOE+OO SHORT HLIF SE-75 -l.661E-01 2.107E-01 3.278E-01 NOT IDENT. BR-77 0.000E+OO 2.037E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.735E+02 O.OOOE+OO SHORT HLIF RB-83 2.223E-01 6.118E-01 1.279E+OO NOT IDENT. KR-85 -4 .196E+OO 7.971E+OO 1.18 6E+Ol NOT IDENT. SR-85 -4.080E-01 7.734E-01 l.150E+OO NOT IDENT. RB-86 O.OOOE+OO 2.412E+04 O.OOOE+OO SHORT HLIF Y-88 5.372E-02 l.884E-01 4.576E-01 NOT IDENT. Y-91 -1.397E+02 5.780E+02 l.103E+03 NOT IDENT. NB-94 2.263E-02 3.569E-02 7.447E-02 NOT IDENT. NB-95 -2.544E-02 8.328E-01 l.614E+OO NOT IDENT. NB-95M 8.597E-01 2.418E+OO 4.330E+OO NOT IDENT. ZR-95 -l.380E-01 l.183E+OO 2.331E+00 NOT IDENT. NB-97 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 6.776E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.565E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.015E+41 O.OOOE+OO SHORT HLIF RH-101 -2.695E-02 4.441E-02 6.940E-02 NOT IDENT. RH-102 1. 739E-02 5.970E-02 1.232E-01 NOT IDENT. RU-103 5.258E+OO 4.849E+OO 1. 051E+Ol FAIL ABUN RH-106 8.447E-02 5.125E-01 9.385E-01 NOT IDENT. RU-106 8.447E-02 5.125E-01 9.385E-01 NOT IDENT. AG-108M -2.233E-03 2.943E-02 5.489E-02 FAIL ABUN AG-llOM 7.245E-02 9.693E-02 2.144E-01 NOT IDENT. SN-113 -1.002E-01 2.244E-01 4.026E-01 NOT IDENT. CD-115 O.OOOE+OO 2.363E+38 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 6.205E+04 O.OOOE+OO SHORT HLIF TE-123M -9.444E-02 l.238E-01 2.328E-01 NOT IDENT. SB-124 -1.440E+OO 1. 621E+OO 2.333E+OO NOT IDENT. SB-125 3.652E-02 9. 672E-02 l.935E-01 FAIL ABUN TE-125M l.199E+02 2.548E+02 4. 921E+02 NOT IDENT. I-126 O.OOOE+OO 5. 716E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 1.012E+06 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.229E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 2.380E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 6.815E+25 O.OOOE+OO SHORT HLIF BA-133 3.409E-02 3.625E-02 7.280E-02 NOT IDENT. I-133 O.OOOE+OO 9.279E+40 O.OOOE+OO SHORT HLIF CS-134 7.520E-02 9.420E-02 l.278E-01 FAIL ABUN CS-135 1.237E-02 l.408E-01 2.473E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2. l 72E+05 0.000E+OO SHORT HLIF BA-137M -3.844E-03 3.893E-02 7.517E-02 NOT IDENT. CS-137 -4.061E-03 4 .112E-02 7.941E-02 NOT IDENT. CE-139 -5.548E-02 1.023E-01 1.950E-01 NOT IDENT. BA-140 O.OOOE+OO 7. 911E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.208E+05 O.OOOE+OO SHORT HLIF CE-141 -3.590E+00 1.994E+Ol 3.930E+Ol NOT IDENT. CE-143 O.OOOE+OO 4.571E+40 O.OOOE+OO SHORT HLIF CE-144 -3.943E-01 3.251E-01 5.175E-01 NOT IDENT. PM-144 -4.560E-02 5.301E-02 9. l 72E-02 NOT IDENT. PR-144 -3.929E+OO 4.588E+OO 7.944E+OO NOT IDENT. PM-146 3 .130E-03 4.088E-02 7.977E-02 NOT IDENT. ND-147 O.OOOE+OO l°. 874E+07 O.OOOE+OO SHORT HLIF PM-147 -3.148E+02 8.952E+02 l.587E+03 NOT IDENT. PM-149 0.000E+OO 3.697E+39 0.000E+OO SHORT HLIF EU-150 3 .119E-02 2. 741E-02 5.373E-02 FAIL ABUN EU-152 -8.435E-02 1. 039E-01 1.550E-01 FAIL ABUN GD-153 -2.290E-02 2.087E-01 3.548E-01 NOT IDENT. EU-154 2.002E-02 1.314E-01 2.686E-01 NOT IDENT. EU-155 8.122E-02 1.140E-01 2.245E-01 FAIL ABUN TB-160 -4.907E-01 1.890E+OO 3.536E+OO FAIL ABUN H0-166M 4.226E-02 6.155E-02 1.307E-01 FAIL ABUN TM-171 -2.948E+00 4.409E+Ol 8.449E+Ol NOT IDENT. HF-172 1.328E-02 2.849E-01 4.778E-01 FAIL ABUN LU-172 5.397E-02 7.858E-02 l.705E-01 FAIL ABUN Page 4522 of 5809 LU-176 -7. 496E-03 2. 331E-02 4.335E-02 FAIL ABUN HF-181 7.016E-01 4.094E+OO 7.835E+OO FAIL ABUN TA-182 -2.958E-01 1.087E+OO 2.056E+OO FAIL ABUN RE-183 -1. 474E+OO 4.416E+OO 8.325E+OO NOT IDENT. RE-184 5.lOlE-01 2. 696E+Ol 5.292E+Ol NOT IDENT. W-188 -3.071E+Ol 1.123E+02 1. 8 62E+02 FAIL ABUN IR-192 -8.633E-02 3.999E-01 7.523E-Ol FAIL ABUN HG-203 -1.00lE+OO 2.190E+OO 4.028E+OO FAIL ABUN BI-207 1. 757E-02 5.006E-02 l.030E-01 FAIL ABUN . PB-210 -7.036E+OO l.050E+Ol 1. 947E+Ol NOT IDENT. PB-211 -7.835E-02 6.945E-01 1.293E+OO NOT IDENT. RN-219 -l.800E-01 4.582E-01 7.216E-01 NOT IDENT. RA-223 1.17 6E-01 5.974E-01 1.162E+OO FAIL ABUN AC-227 -3.002E-02 2.275E-01 4.345E-01 FAIL ABUN TH-227 -3.002E-02 2.275E-01 4.345E-01 FAIL ABUN TH-229 -2.261E-02 4.409E-01 8.622E-01 FAIL ABUN TH-231 1.176E-01 5.974E-01 1.162E+OO FAIL ABUN PA-233 -4.434E-02 5.780E-02 1.019E-01 FAIL ABUN PA-234 -l.343E-01 2.937E-01 5.271E-01 FAIL ABUN PA-234M 6.350E-01 4.614E+OO 9.076E+OO NOT IDENT. U-235 1.525E-01 1. 7 92E-01 3.744E-01 FAIL ABUN NP-237 -4.434E-02 5.780E-02 1.019E-01 FAIL ABUN NP-238 O.OOOE+OO 4.034E+40 O.OOOE+OO SHORT HLIF NP-239 1.184E-01 2.617E-01 4.994E-01 NOT IDENT. PU-239 O.OOOE+OO 6.224E+02 6.849E+02 FAIL ABUN AM-241 -1. 567E-01 2.280E-01 4.146E-01 NOT IDENT. CM-243 -4.719E-02 l.106E-01 l.974E-01 NOT IDENT. BK-247 -4.650E-03 7.054E-02 1.221E-01 FAIL ABUN CM-247 -3.701E-03 4.146E-02 6.864E-02 NOT IDENT. CF-249 6.166E-03 4.148E-02 7 .188E-02 NOT IDENT. CF-251 -9.060E-02 1.148E-01 2.135E-01 NOT IDENT. Page 4523 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:06:37.94 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error K-40 1460.82 306 10.66* l.OOlE+OO 1.378E+Ol l.378E+Ol 12.06 CD-109 88.03 40 3.70* 4.279E+OO 1.219E+OO 1.889E+OO 123.88 SN-126 64.28 26 9.60 1. 895E+OO 6.959E-01 6.959E-01 172.79 86.94 40 8.90 4.279E+OO 5.068E-01 5.068E-01 123.88 87.57 40 37.00* 4.279E+OO l.219E-01 l.219E-01 123.88 TL-208 277.37 ------6.60 4.205E+OO ------Line Not Found ------583.19 119 85.00* 2.199E+OO 3.050E-01 3.050E-01 25.69 860.56 ------12.50 1.582E+OO ------Line Not Found ------BI-211 72. 87 54 1. 23 2.909E+OO 7.277E+OO 7.277E+00 64.49 351.06 310 12.92* 3.426E+OO 3.367E+OO 3.367E+OO 16.82 BI-212 727.33 30 6.67* 1.821E+OO 1.177E+OO 1.177E+OO 105.88 785.37 ------1.10 1.708E+OO ------Line Not Found ------1620.50 11 1. 47 9.085E-01 3.788E+OO 3.788E+00 60.30 PB-212 74.82 125 10.28 3 .139E+OO 1.862E+OO 1. 862E+OO 44.20 77' 11 215 17.10 3.375E+OO 1. 791E+OO 1. 791E+OO 27.05 238.63 374 43.60* 4.740E+OO 8.697E-01 8.697E-01 14.13 300.09 63 3.30 3.937E+OO 2.347E+00 2.347E+00 59.94 BI-214 609.32 199 45.49* 2 .118E+OO 9.923E-01 9.927E-01 17.02 1120.29 35 14.92 1.265E+OO 8.909E-01 8.912E-01 104.59 1764.49 30 15.30 8.361E-01 1.144E+OO 1.145E+OO 37.13 PB-214 74.82 125 5.80 3.139E+OO 3.300E+OO 3. 301E+OO 44.20 77 .11 215 9.70 3.375E+OO 3.158E+OO 3.159E+00 27.05 87.09 40 3.41 4.279E+OO 1.323E+00 1.323E+OO 123.88 242.00 123 7.25 4.693E+OO 1.737E+OO 1.737E+OO 39.01 295.22 162 18.42 3.993E+OO 1.062E+OO 1.062E+OO 27.09 351.93 310* 35.60* 3.426E+OO 1.222E+OO 1.222E+00 16.82 RN-222 609.32 199 45.49* 2 .118E+OO 9.923E-01 9.927E-01 17.02 1120.29 35 14.92 1.265E+OO 8.909E-01 8.912E-01 104.59 1764.49 30 15.30 8.361E-01 1.144E+OO 1.145E+OO 37.13 RA-224 240.99 123 4.10* 4.693E+OO 3. 071E+OO 3.071E+00 39.01 RA-226 609.32 199 45.49* 2 .118E+OO 9.923E-01 9.927E-01 17.02 1120.29 35 14.92 l.265E+00 8.909E-01 8.912E-01 104.59 1764.49 30 15.30 8.361E-01 1.144E+OO 1.145E+OO 37.13 AC-228 105.21 ------1.10 5.396E+OO ------Line Not Found ------338.32 71 11. 27 3.543E+OO 8.576E-01 8.576E-01 60.80 794.95 17 4.25 1.689E+OO 1.157E+OO 1.157E+OO 127.82 835.71 11 1. 61 1.620E+OO 2.088E+OO 2.088E+OO 155.20 911.20 105 25.80* l.508E+00 1.295E+OO 1.295E+OO 22.53 968. 97 32 15.80 1.432E+OO 6.816E-01 6.816E-01 54.95 RA-228 105.21 ------1.10 5. 396E+OO ------Line Not Found ------338.32 71 11. 27 3.543E+OO 8.576E-01 8.576E-01 60.80 794.95 17 4.25 1. 689E+OO 1.157E+OO 1.157E+OO 127.82 835. 71 11 1. 61 1. 620E+OO 2.088E+OO 2.088E+OO 155.20 911.20 105 25.80* l.508E+00 1.295E+OO 1.295E+OO 22.53 968. 97 32 15.80 1.432E+OO 6.816E-01 6.816E-01 54.95 TH-228 74.82 125 10.28 3.139E+OO 1.862E+OO 1. 8 62E+OO 44.20 77 .11 215 17.10 3.375E+OO 1. 791E+OO 1. 791E+OO 27.05 Page 4524 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235069 Acquisition date 3-0CT-2016 06:05:34 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 238.63 374. 43.60* 4.740E+OO 8.697E-01 8. 697E-01.. 14.13 300.09 63 3.30 3.937E+00 2.347E+OO 2.347E+OO 59.94 TH-230 609.32 199 45.49* 2 .118E+OO 9.923E-01 9.923E-01 17.02 1120.29 35 14.92 1.265E+00 8.909E-01 8.909E-01 104.59 1764.49 30 15.30 8. 361E-01 1.144E+OO 1.144E+OO 37 .13 PA-231 283.69 ------1. 70 4.127E+00 ------Line Not Found ------301.36 63 5.35* 3.937E+00 1.448E+OO 1.448E+OO 59.94 TH-232 105.21 ------1.10 5.396E+00 ------Line Not Found ------338.32 71 11.27 3.543E+OO 8.576E-01 8.576E-01 60.80 835.71 11 1. 61 1.620E+OO 2.088E+OO 2.088E+OO 155.20 911.20 105 25.80* 1.508E+OO 1.295E+OO 1.295E+OO 22.53 968.97 32 15.80 1.432E+00 6.816E-01 6.816E-01 54.95 TH-234 63.29 26 3.70* 1.895E+00 1.806E+OO 1.806E+OO 172.79 92.59 60 4.23 4.706E+OO 1.441E+OO 1.441E+OO 123.42 U-234 609.32 199 45.49* 2 .118E+OO 9.923E-01 9.923E-01 17.02 1120.29 35 14.92 1.265E+00 8.909E-01 8.909E-01 104.59 1764.49 30 15.30 8.361E-01 1.144E+OO 1.144E+OO 37.13 U-238 63.29 26 3.70* 1.895E+00 1.806E+OO 1. 806E+OO 172.79 92.59 60 4.23 4.706E+OO 1.441E+OO 1.441E+OO 123.42 AM-243 43.53 ------5.90 1.216E-01 ------Line Not Found ------74.66 125 67.20* 3.139E+OO 2.848E-01 2.848E-01 44.20 ANH-511 511. 00 45 100.00* 2.468E+00 8.804E-02 8.804E-02 83.01 Flag: "*" Key line Page 4525 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235069 Acquisition date 3-0CT-2016 06:05:34 Total number of lines in spectrum 45 Number of unidentified lines 11 Number of lines tentatively identified by NID 34 Nuclide Type : Nuclide K-40 CD-109 SN-126 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 1.41E+10Y 7.04E+08Y 1. 41E+10Y l.41E+l0Y 1600. OOY 1600.00Y 1600.00Y 1.41E+10Y 1600.00Y l.41E+l0Y 1.41E+10Y 1.41E+10Y 7.54E+04Y 7.04E+08Y 1. 41E+10Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 55 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity " Uncorrected pCi/GRAM 1. 378E+Ol l.219E+OO l.219E-01 3.0SOE-01 3.367E+OO 1.177E+OO 8.697E-01 9.923E-01 1.222E+OO 9.923E-01 3. 071E+00 9.923E-01 1.295E+OO 1.295E+OO 8.697E-01 9.923E-01 1. 448E+OO l.295E+00 1.806E+OO 9.923E-01 1.806E+OO 2.848E-01 8.804E-02 4.029E+Ol 4.029E+Ol Decay Corr pCi/GRAM 1.378E+Ol 1.889E+OO 1.219E-01 3.0SOE-01 3.367E+OO 1.177E+OO 8.697E-01 9.927E-01 1.222E+OO 9.927E-01 3. 071E+OO 9. 927E-(H 1.295E+OO 1.295E+OO 8.697E-01 9.923E....'.Ol 1.448E+OO 1.295E+OO 1. 806E+OO 9.923E-01 1.806E+OO 2.848E-01 8.804E-02 4.096E+Ol 4. 096E+Ol 75.56% Decay Corr 2-Sigma Error 0.166E+Ol 2.341E+OO 1.510E-01 0.783E-01 0.566E+OO 1.246E+OO 1.229E-01 1.690E-01 0.206E+OO 1.690E-01 1.198E+OO l.690E-01 0.292E+OO 0.292E+OO 1.229E-01 l.689E-01 0.868E+OO 0.292E+OO 3.120E+OO 1.689E-01 3.120E+OO 1.259E-01 7.309E-02 "M" Manually accepted . 2-Sigma %Error 12.06 123.88 123.88 25.69 16.82 105.88 14 .13 17.02 16.82 17.02 39.01 17.02 22.53 22.53 14.13 17.02 59.94 22.53 172.79 17.02 172.79 44.20 83.01 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4526 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235069 Acquisition date : 3-0CT-2016 06:05:34 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 4 83:40 48 145 1. 38 166.59 143 29 l.03E-02 **** 3.98E+OO T 4 129.16 73 137 1. 82 258.15 254 12 1.63E-02 68.1 5.98E+OO T 4 131.74 37 30 1. 26 263.32 254 12 8.26E-03 63.5 6.00E+OO T 0 150.51 40 121 1. 39 300.86 297 8 9 -llE-03 **** 5.99E+OO 0 185. 71 77 183 1.28 371.27 366 11 l.78E-02 80.1 5.57E+OO T 0 273.05 40 131 4.09 546.01 534 16 9.46E-03 **** 4.26E+OO T 0 395. 96 35 88 6.20 791. 90 779 24 8.74E-03 **** 3.09E+OO 0 465.08 21 60 3.26 930.17 920 15 5.18E-03 **** 2.68E+OO 0 504.15 14 16 0.87 1008.32 1005 7 3.47E-03 **** 2.49E+OO T 0 578.09 22 27 0.93 1156.22 1149 13 5.79E-03 **** 2.22E+OO 0 601. 94 25 18 3.84 1203.94 1197 14 6.36E-03 87.8 2.14E+OO T 7 615.09 22 33 3.60 1230.25 1210 31 5.61E-03 **** 2.lOE+OO T 0 808.59 9 22 2.87 1617.31 1606 15 2.38E-03 **** 1. 67E+OO T 0 854.30 11 12 1. 53 1708.74 1704 8 2.94E-03 **** 1. 59E+OO 4 914.78 11 4 1. 43 1829.73 1816 17 3.00E-03 83.1 1. 50E+OO 6 964 .12 17 9 2.70 1928.42 1924 18 4.63E-03 83.0 1. 44E+OO T 0 987.78 18 3 3.72 1975.75 1968 13 4.88E-03 63.9 l.41E+OO 0 1347.63 11 6 3.92 2695.49 2688 13 3.09E-03 **** 1.08E+OO 0 1351. 24 7 0 0.58 2702.71 2700 7 1.94E-03 75.6 1.07E+OO 0 1401. 29 6 4 0.87 2802.83 2798 8 1. 67E-03 **** 1.04E+OO 0 1589.05 7 6 1. 34 3178.36 3168 12 1.94E-03 **** 9.26E-01 Flags: "T" = Tentatively associated Page 4527 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:06:56.22 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235069.CNF;l *
  • Acquisition date 3-0CT-2016 06:05:34 Sensitivity 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.70 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:45:00 Nuclide Library : SOLID *
  • Sample ID G405235069 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.5608E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-22 6 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.563E-01 1.295E+OO 8.423E-02 2.693E-02 1.648E-01 3.733E-01 4.369E-02 5.452E-02 1.666E-01 5.452E-02 4.685E-01 5.452E-02 9.496E-02 9. 496E-02 4.369E-02 5.450E-02 3.588E-01 9.496E-02 1. 733E+OO 5.450E-02 1. 733E+OO 5.583E-02 1. 8 69E-02 ----Non-Identified Nucl{des Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4528 of 5809 Le (pCi/GRAM 8.606E+OO 4.793E-02 O.OOOE+OO l.540E-02 2.403E-01 0.000E+OO O.OOOE+OO 6. 411E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147' PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 4529 of 5809 4.581E-01 O.OOOE+OO 4.085E-02 4.147E-01 5. 411E+OO 3.466E-02 1.600E-01 2.444E+OO l.547E+Ol O.OOOE+OO l.495E-01 O.OOOE+OO O.OOOE+OO 5.749E-01 5.262E+OO 5.104E-01 O.OOOE+OO 1.743E-01 4.842E+02 3.367E-02 7.171E-01 2.029E+OO 1.002E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.267E-02 5.485E-02 4.749E+OO 4.134E-01 4.134E-01 2.482E-02 9.392E-02 1.819E-Ol O.OOOE+OO O.OOOE+OO 1. 088E-01 7 .131E-01 8. 710E-02 2.303E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.300E-02 O.OOOE+OO 5.790E-02 1.138E-01 O.OOOE+OO O.OOOE+OO 3.375E-02 3.565E-02 9.106E-02 O.OOOE+OO O.OOOE+OO 1.845E+Ol O.OOOE+OO 2.375E-Ol 3.965E-02 3.435E+OO 3.568E-02 0.000E+OO 7.422E+02 0.000E+OO 2.486E-02 6.989E-02 1.662E-01 l.166E-01 1.054E-01 1.535E+OO 5.872E-02 3. 941E+Ol 2.250E-01 7.436E-02 l.979E-02 NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4530 of 5809 3.536E+OO 9.065E-01 3. 872E+OO 2.299E+Ol 8.549E+Ol 3.422E-01 1.860E+OO 4.471E-02 9.089E+OO 5.873E-01 3.271E-01 5.346E-01 2.012E-01 2.012E-01 4.024E-01 5.346E-01 4.632E-02 2.257E-01 3. 972E+OO 1. 767E-01 4.632E-02 O.OOOE+OO 2.345E-01 3.240E+02 l.937E-01 9.226E-02 5.584E-02 3.123E-02 3.266E-02 9.972E-02 FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:07:02.65 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235069.CNF;l *
  • Acquisition date 3-0CT-2016 06:05:34 Sensitivity : 3.000 *
  • Detector ID GAM43 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.70 Half life ratio : ***** *
  • Sample date 16-DEC-2015 12:45:00 Nuclide Library : SOLID *
  • Sample ID G405235069 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.5608E+02 GRAM *
  • Quantity Err(%) : l.2814E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 6-SEP-2016 07:25:20 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM43 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.378E+Ol 1. 781E+OO 1. 781E+OO CD-109 3.725E-01 2.337E+OO 2.337E+OO SN-126 2.403E-02 1.508E-01 1.508E-01 TL-208 3.050E-01 7.788E-02 7.788E-02 BI-211 4.410E-01 9. 720E-01 9.720E-01 BI-212 l.177E+OO 1.223E+OO 1.223E+OO PB-212 8.697E-01 1.291E-01 1.291E-01 BI-214 9.927E-01 l.710E-01 l.710E-01 PB-214 1.222E+OO 2.080E-01 2.080E-01 RN-222 9.927E-01 1. 710E-01 1. 710E-01 RA-224 l.193E+OO l.283E+OO l.283E+OO RA-22 6 9.927E-01 l.710E-01 1.710E-01 AC-228 l.295E+OO 2.935E-01 2.935E-01 RA-228 l.295E+OO 2.935E-01 2.935E-01 TH-228 8.697E-01 l.291E-Ol l.291E-01 TH-230 9.923E-01 l.710E-01 1.710E-01 PA-231 l.448E+OO 9.049E-01 9.049E-01 TH-232 l.295E+OO 2.935E-01 2.935E-01 TH-234 1.806E+OO 3.084E+OO 3.084E+OO U-234 9.923E-01 l.710E-01 1. 710E-01 U-238 l.806E+OO 3.084E+OO 3.084E+OO AM-243 l.932E-01 l.269E-01 l.269E-01 ANH-511 8.804E-02 7.172E-02 7.172E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -l.182E-01 l.022E+Ol l.022E+Ol NOT IDENT. NA-22 5.040E-03 5.459E-02 5.463E-02 NOT IDENT. NA-24 -1.000E+41 7.518E+41 O.OOOE+OO SHORT HLIF AL-26 -3.007E-02 3. 270E-02 3.540E-02 NOT IDENT. SC-46 -4.310E-01 3.740E-01 4.214E-01 FAIL ABUN V-48 4.458E+Ol l.015E+04 l.015E+04 SHORT HLIF CR-51 -8.230E+Ol 3.077E+02 3.100E+02 SHORT HLIF Page 4531 of 5809 MN-54 1.263E-02 7.292E-02 7.314E-02 NOT IDENT. C0-56 3.948E-01 4.726E-01 5.050E-01 NOT IDENT. MN-56 1.000E+41 1.184E+41 O.OOOE+OO SHORT HLIF C0-57 -1.324E-02 4. 896E-02 4.932E-02 NOT IDENT. C0-58 1. 931E-01 4.925E-01 5.002E-01 NOT IDENT. FE-59 1.494E+OO 6.201E+OO 6.238E+OO NOT IDENT. C0-60 1.627E-02 3.652E-02 3. 725E-02 NOT IDENT. ZN-65 2.258E-02 2.152E-01 2.154E-01 NOT IDENT. GE-68 1.245E+OO 2.710E+OO 2.767E+OO NOT IDENT. AS-73 l.136E+,01 1.638E+Ol 1. 716E+Ol NOT IDENT. AS-74 1.251E+OO 4.762E+03 4.762E+03 SHORT HLIF SE-75 -l.661E-01 2.109E-01 2.238E-01 NOT IDENT. BR-77 1.471E+37 1.239E+38 O.OOOE+OO SHORT HLIF SR-82 -l.577E+02 5.735E+02 5.779E+02 SHORT HLIF RB-83 2.223E-01 6.126E-01 6.207E-01 NOT IDENT. KR-85 -4.196E+OO 7.973E+OO 8.194E+OO NOT IDENT. SR-85 -4.0SOE-01 7.735E-01 7. 951E-01 NOT IDENT. RB-86 8.346E+03 2.412E+04 2. 441E+04 SHORT HLIF Y-88 5. 372E-02 1.884E-01 1.900E-01 NOT IDENT. Y-91 -1.397E+02 5.780E+02 5.814E+02 NOT IDENT. NB-94 2.263E-02 3. 571E-02 3. 713E-02 NOT IDENT. NB-95 -2.544E-02 8.328E-01 8.329E-01 NOT IDENT. NB-95M 8.597E-01 2.419E+00 2.450E+OO NOT IDENT. ZR-95 -1.380E-01 1.183E+OO l.185E+OO NOT IDENT. NB-97 1.000E+41 4.463E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 6.788E+40 O.OOOE+OO SHORT HLIF M0-99 l.685E+30 2.565E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 1.020E+41 O.OOOE+OO SHORT HLIF RH-101 -2.695E-02 4.467E-02 4.630E-02 NOT IDENT. RH-102 1. 739E-02 5. 971E-02 6.023E-02 NOT IDENT. RU-103 5.258E+OO 4.855E+OO 5.403E+OO FAIL ABUN RH-106 8.447E-02 5.125E-01 5.140E-01 NOT IDENT. RU-106 8.447E-02 5.125E-01 5.140E-01 NOT IDENT. AG-108M -2.233E-03 2.943E-02 2.945E-02 FAIL ABUN AG-110M 7.245E-02 9.700E-02 1.024E-01 NOT IDENT. SN-113 -1.002E-01 2.245E-01 2.290E-01 NOT IDENT. CD-115 6.576E+37 2.366E+38 O.OOOE+OO SHORT HLIF SN-117M -5.366E+04 6.236E+04 6.689E+04 SHORT HLIF TE-123M -9.444E-02 l.239E-01 l.310E-01 NOT IDENT. SB-124 -1.440E+OO 1.623E+OO 1.748E+OO NOT IDENT. SB-125 3.652E-02 9.673E-02 9.812E-02 FAIL ABUN TE-125M 1.199E+02 2.549E+02 2.605E+02 NOT IDENT. I-126 5.916E+04 5.717E+05 5.723E+05 SHORT HLIF SB-126 -4.837E+05 1.016E+06 l.039E+06 SHORT HLIF SB-127 1.282E+21 5.503E+21 O.OOOE+OO SHORT HLIF I-131 5.478E+08 2.380E+09 2.393E+09 SHORT HLIF I-132 -1.000E+41 l.810E+42 O.OOOE+OO SHORT HLIF TE-132 -4. 726E+25 7.067E+25 O.OOOE+OO SHORT HLIF BA-133 3.409E-02 3.628E-02 3.940E-02 NOT IDENT. I-133 -1.000E+41 1.990E+41 O.OOOE+OO SHORT HLIF CS-134 7.520E-02 9.425E-02 l.002E-01 FAIL ABUN CS-135 l.237E-02 1.408E-01 1.409E-01 NOT IDENT. I-135 -1.000E+41 7.222E+41 O.OOOE+OO SHORT HLIF CS-136 1.936E+05 2.182E+05 2.350E+05 SHORT HLIF BA-137M -3.844E-03 3.893E-02 3.897E-02 NOT IDENT. CS-137 -4. 061E-03 4 .112E-02 4 .117E-02 NOT IDENT. CE-139 -5.548E-02 l.029E-01 1.059E-01 NOT IDENT. BA-140 2.565E+05 7.912E+05 7. 996E+05 SHORT HLIF LA-140 -1.289E+05 2.209E+05 2.284E+05 SHORT HLIF CE-141 -3.590E+OO 1.994E+Ol 2.00lE+Ol NOT IDENT. CE-143 1.000E+41 4.678E+40 0.000E+OO SHORT HLIF CE-144 -3.943E-01 3.258E-01 3.711E-01 NOT IDENT. PM-144 -4.560E-02 5.308E-02 5.692E-02 NOT IDENT. PR-144 -3.929E+00 4.591E+OO 4.921E+OO NOT IDENT. PM-146 3.130E-03 4.088E-02 4.091E-02 NOT IDENT. ND-147 -4.202E+06 1.875E+07 l.884E+07 SHORT HLIF PM-147 -3.148E+02 8.953E+02 9.065E+02 NOT IDENT. PM-149 2.626E+39 3.740E+39 O.OOOE+OO SHORT HLIF EU-150 3 .119E-02 2.744E-02 3.083E-02 FAIL ABUN EU-152 -8.435E-02 l.041E-01 l.lOBE-01 FAIL ABUN GD-153 -2.290E-02 2.087E-01 2.090E-01 NOT IDENT. EU-154 2.002E-02 1. 314E-01 l.317E-01 NOT IDENT. EU-155 8.122E-02 1.142E-01 l.199E-01 FAIL ABUN TB-160 -4.907E-01 1. 890E+OO 1.903E+OO FAIL ABUN H0-166M 4.226E-02 6.159E-02 6.447E-02 FAIL ABUN TM-171 -2.948E+OO 4.409E+Ol 4. 411E+Ol NOT IDENT. HF-172 1.328E-02 2.849E-01 2.850E-01 FAIL ABUN LU-172 5.397E-02 7.877E-02 8.244E-02 FAIL ABUN Page 4532 of 5809 LU-176 -7. 496E-03 2.331E-02 2.356E-02 FAIL ABUN HF-181 7.016E-01 4.094E+OO 4.106E+OO FAIL ABUN TA-182 -2.958E-01 1.087E+OO 1. 096E+OO FAIL ABUN RE-183 -l.474E+00 4.422E+OO 4.472E+OO NOT IDENT. RE-184 5.lOlE-01 2.696E+Ol 2.696E+Ol NOT IDENT. W-188 -3.071E+Ol 1.123E+02 l .132E+02 FAIL ABUN IR-192 -8.633E-02 3.999E-01 4.018E-01 FAIL ABUN HG-203 -1.00lE+OO 2.190E+OO 2.236E+OO FAIL ABUN BI-207 1. 757E-02 5.006E-02 5.069E-02 FAIL ABUN PB.-210 -7.036E+00 1.053E+Ol ,l.lOOE+Ol NOT IDENT. PB-211 -7.835E-02 6.945E-01 6.954E-01 NOT IDENT. RN-219 -1.800E-01 4.587E-01 4.659E-01 NOT IDENT. RA-223 l.176E-01 5.974E-01 5.997E-01 FAIL ABUN AC-227 -3.002E-02 2.275E-01 2.279E-01 FAIL ABUN TH-227 -3.002E-02 2.275E-01 2.279E-01 FAIL ABUN TH-229 -2.261E-02 4.409E-01 4.410E-01 FAIL ABUN TH-231 1.176E-01 5.974E-01 5.997E-01 FAIL ABUN PA-233 -4.434E-02 5.784E-02 6.119E-02 FAIL ABUN PA-234 -l.343E-01 3.315E-01 3.370E-01 FAIL ABUN PA-234M 6.350E-01 4.614E+OO 4.623E+OO NOT IDENT. U-235 1.525E-01 1. 793E-01 1. 921E-01 FAIL ABUN NP-237 -4.434E-02 5.784E-02 6.119E-02 FAIL ABUN NP-238 -1.640E+40 4.035E+40 O.OOOE+OO SHORT HLIF NP-239 1.184E-01 2.619E-01 2.673E-01 NOT IDENT. PU-239 9.327E+02 6.238E+02 7.522E+02 FAIL ABUN AM-241 -l.567E-01 2.283E-01 2.389E-01 NOT IDENT. CM-243 -4.719E-02 1.107E-01 1.127E-01 NOT IDENT. BK-247 -4. 650E-'03 7.055E-02 7.058E-02 FAIL ABUN CM-247 -3.701E-03 4.146E-02 4.150E-02 NOT IDENT. CF-249 6.166E-03 4.149E-02 4.158E-02 NOT IDENT. CF-251 -9.060E-02 1.153E-01 l.223E-01 NOT IDENT. Page 4533 of 5809
  • GEL Laboratories LLC *
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  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 72.9704 87.09 122.7173 136.47 68.6578 45.60 82.7768 87.57 122.8402 140.51 0.0000 46.54 81. 9877 88.03 122.9582 143.76 69.4136 49. 72 0.0000 88.34 96.8917 144.24 68.6157 51. 35 83.2067 88.47 96.9174 145.44 83.1620 51. 87 72.7863 89. 96 97.2147 152.43 88.7168 52.39 63.3895 1093.63 97.3499 153.25 0.0000 52.97 65.6137 91.11 0.0000 323.87 82.4941 53.44 52.9865 92.59 109.3688 156.02 0.0000 54.07 59.4529 93.35 109.5352 158.56 0.0000 57.36 0.0000 94.56 80.9860 159.00 86.5041 57.53 66.4677 94.65 81.0003 162.33 68.6493 57.98 66.5498 94.67 81.0035 162.66 0.0000 59.27 68.9385 94.87 79.4774 163.33' 78.3133 59.32 78.6435 97.43 73.6111 165.86 79.4519 59.54 84.0801 98.43 87.0914 176.31 60.1834 60. 96 80.7934 98.44 87.0931 176.60 0.0000 61.17 80.8384 99.53 76.6603 177.52 85.9821 62.93 88.4641 100 .11 75.5645 181.07 0.0000 63.29 95.8045 102.03 91. 2436 181.52 61.4707 63.58 95.8765 103.18 79.5640 184.41 78.6785 64.28 78.5859 103.37 79.5927 143.76 78.8056 66.73 79.0752 105.21 60.7917 193.51 66.8946 67.24 82.4747 105.31 60.8026 197.03 68.0809 125.81 79.2625 106.12 76.4146 198.01 70.8859 67.75 79.2757 106.47 75.2686 201.83 69.3752 69.67 88.5010 109.28 60.0407 203.43 67.6737 70.83 82.8322 111. 00 79.4964 205.31 76.9846 72. 81 92.1404 111.76 0.0000 210.85 78.3888 72.87 92.1536 114. 06 73.8686 215.65 56.5558 74.66 92.5402 116. 30 0.0000 222 .11 62.5562 74.82 92.5743 116.74 68.1274 227.09 64.7668 74.97 92.6064 119.76 86.8183 227.38 68.5422 77 .11 93.0618 121.12 78.4365 228.16 0.0000 78.74 93.4043 121.22 78.4497 228.18 72.3590 79.69 93.6023 121. 78 72.3879 116.74 72.3590 80.12 93.6919 122.06 72.4217 235.69 65.3501 80.19 0.0000 122.92 68.8370 235. 96 63.9473 80.57 93.7846 123.07 71.3128 238.63 57.9476 81. 00 93.8735 265.00 77.5383 238.98 0.0000 81. 07 93.8880 125.81 85.6299 240.99 58.0866 81. 75 94.0280 127.23 105.6315 242.00 58.1462 83.79 94.4437 127.91 89.2246 244.70 58.3038 84.00 94.4865 129.30 65.8246 252.40 0.0000 85.43 55.0305 131. 20 66.0228 252.80 51.0650 86.55 110. 3210 133.02 66.6276 254.15 0.0000 86.79 110.3760 133.52 68.7634 256.23 55.1019 86.94 110:4111 136.00 64.4251 260.90 0.0000 Page 4534 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 52.6234 355.39 0.0000 584.27 17.4381 264.80 42.3973 356.01 17.3631 595.83 0.0000 265.00 39.4807 364.49 0.0000 427.87 17.5828 268.22 42.5336 366.42 0.0000 602.52 0.0000 269.46 40.1350 372.51 34.0879 604.72 0.0000 270.03 40.1567 .375.05 38.4192 607.14 20 . .5803 271. 23 40.2017 377.52 28.8660 609.32 20.6021 273.65 0.0000 356.01 25.7749 610.33 20.6124 276.40 38.4224 388.16 30.7016 614.28 20.6527 277.37 48.5143 388.63 0.0000 618.01 20.6903 277.60 48.5243 391.69 36.7171 620. 36 16.2755 278.00 51.3049 264.66 37.4901 621. 93 16.2878 279.20 58.2750 401.81 39.1509 630.19 0.0000 279.54 64.2211 402.40 35.9024 631.29 18.5931 279.70 64.2303 404.85 34.8730 633.25 23.2628 280.46 53.3969 410.95 28.4518 634.78 0.0000 283.69 57.5197 413.71 25.2157 635.95 20.4981 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 46.6825 423.72 0.0000 645.85 18.7219 285.90 0.0000 427.09 17.6976 657.76 18.8269 287.50 35.8228 427.87 22.1334 657.90 0.0000 290.67 47.8984 433.94 31.1092 661. 66 27.3486 293.27 0.0000 439.40 31. 218 6 664.57 0.0000 351:93 50.0926 453.88 20.2537 666.33 0.0000 295. 96 50.1251 463.37 23.7686 666.50 0.0000 879.38 50.2380 468.07 25. 5396 667.71 0.0000 299.98 50.2991 473.00 0.0000 677.62 14.2497 300.09 50.3042 475.06 22.7979 685.70 0.0000 300 .13 50.3052 476.78 30.8090 695.00 0.0000 301.36 40.7900 477.60 20.5496 696.49 23.9510 302.85 42.3546 482.18 26.3298 696. 51 23.9510 256.23 40.8996 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 23.0010 306.78 42. 4965 497.08 15. 0130 697.49 23.0032 308.46 36.4768 505.52 17.4072 702.65 21.1346 311. 90 46.7440 507.63 0.0000 706.68 22.1346 316.51 37.7422 511. 00 15.7155 711. 68 17.3606 319.41 0.0000 514.00 29.7355 720.70 0.0000 320.08 0.0000 514.00 29.7355 721. 93 0.0000 321.04 36.8591 520.40 21. 9437 722.78 29.4611 323.87 41. 0490 520.69 0.0000 722. 91 29.4630 325.23 53.4219 522.65 0.0000 723. 31 27.9167 328.76 0.0000 527.90 0.0000 724 .19 15.5151 333.37 29.4706 528.26 24.6846 727. 33 15.5361 333.97 29.4846 529.59 29.1137 733.00 23.3606 334.37 27.9415 529.87 0.0000 735.93 17.5424 338.28 39.4465 531.02 0.0000 333.97 16.5787 338.32 39.4480 537.26 0.0000 739.50 0.0000 311. 90 26.5163 546.56 0.0000 747.24 18.6057 340.48 26.5163 552.55 16.0796 748.06 20.5713 340.55 0.0000 563.25 30.5458 752.31 18.6451 344.28 43.8030 569.33 35.1492 753.82 0.0000 345.93 33.4160 946.00 32.4481 756.73 13.7637 351.06 38.7893 569.70 33.3528 756.80 13.7642 351. 93 38.8149 583.19 18.8811 884.68 26.6234 Page 4535 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 21. 7100 1274.44 12.8895 1620.50 4.0613 766.42 18.7542 1001.03 15.0613 1621. 92 3.3854 766.84 15.7959 1002.74 21.5283 1678.03 0.0000 772. 60 0.0000 1004.73 15.0797 1690.97 5.1543 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 102.5. 87 0.0000 1764.49 0. 00.00 778.90 15.8735 1028.54 0.0000 1063.66 5.2400 783.70 0.0000 1037.84 16.3312 1771.35 8.3859 785.37 14.9203 1038.76 0.0000 1791.20 0.0000 792.07 11.1706 631.29 18.5605 1808.65 6.3369 794.95 10.9839 1048.07 0.0000 1810.72 0.0000 795.86 10.9876 1049.04 9.8339 1836.06 2.1238 810.06 4.8217 1050.41 20.7697 810.29 6.4295 1063.66 10.9766 344.28 6.4299 1077.00 0.0000 810.76 8.0383 1077.34 13.2283 815.77 0.0000 1085.87 9.9476 1048.07 0.0000 1093.63 8.8633 832.01 19.4514 1099.45 11.0992 834.85 20.2838 1112. 07 14.8551 835. 71 20.2905 1112. 84 16.0479 836.80 0.0000 1115. 54 14.2758 846.75 0.0000 1120.29 10.0525 846.77 12.2260 1120.55 10.0530 856.80 0.0000 1221.41 10.0552 860.56 11.2652 1129.67 12.8006 871.09 13.3658 1131. 51 0.0000 873.19 12.3472 1147.95 0.0000 875.33 0.0000 1173.23 19.0589 879.38 17.5318 1177.95 12.7230 880.51 19.6024 1189.05 22.7930 883.24 15.4912 1204.77 20.1470 884.68 9.2994 1221.41 22.0816 889.28 20.7001 1231. 02 15.6827 894.76 11.4079 1235.36 0.0000 898.04 13.4979 1238.28 8.3193 900.72 19.7468 1260.41 0.0000 903.28 14.5635 1271.87 18.6582 911.20 10.4321 1274.44 13. 0696 912.08 10.4352 1274.54 14.0032 923.98 0.0000 1291.59 11. 2541 926.50 12.5863 1298.22 0.0000 929 .11 10.4984 1312 .11 0.0000 937.49 20.0054 1332.49 5.6877 944.13 0.0000 1362.66 0.0000 946.00 16.8965 1365.19 6.6917 949.00 13.7423 1368.63 0.0000 667.71 0.0000 1384.29 11. 5271 962.31 16.9912 1408.01 1.9326 964.08 17.0015 1457.56 0.0000 966.17 17.0132 1460.82 5.8729 911.20 18.7328 1489.16 3.9418 968. 97 18.7328 1505.03 9.8911 983.53 0.0000 1584.12 6.7145 984.45 0.0000 1596.21 0.0000 Page 4536 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:08:27.00 ******************************************************************************** * ' GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235070.CNF;l Background file DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM11.CNF;517 Background date : Z-OCT-2016 11:00:34. Sample date ll-DEC-2015 10:10:00 Acquisition date : 3-0CT-2016 06:08:01. Sample ID G405235070 Sample quantity : l.45320E+02 GRAM Detector name : GAMll Detector geometry: CAN Elapsed live 0 01:00:00.00 Elapsed real time: 0 01:00:00.53 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 0 3 3 0 6 6 0 9 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4537 of 5809 Energy 46.66* 63.35* 74.90* 77.10* 87.10 89.83 92.82* 155.71 185.88* 188.16 209.06 238.62* 241.81 270.20 291.11 295.31* 328.14 338.55* 352.00* 424.17 467.76 511. 03* 564.18 583.18* 609.05* 661.73* 708.02 727.64* 768.99 803.82* 832.04 911.52* 925.66 938.05 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 29 13 100 208 73 33 16 10 100 24 35 329 91 39 15 154 21 42 244 26 10 47 12 104 203 32 8 37 10 9 10 51 13 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 106 218 143 112 134 42 152 108 50 56 66 57 88 57 46 70 58 65 45 33 60 60 17 25 30 33 22 27 23 21 10 32 3 5 1.19 0.79 0.88 0.85 1.16 1. 03 1.16 1. 44 0.92 1. 57 0.95 1. 05 1. 89 1. 62 1.12 1. 05 0.61 0.82 1.13 3.35 5.36 2.58 1. 43 1. 43 1. 44 1. 59 1.11 1. 58 1. 64 2.37 1.14 1. 53 4.39 0.84 93.20 126.60 149.72 154.12 174.14 179.60 185.58 311.46 371.84. 376.39 418.23 477.39 483.76 540.58 582.41 590.82 656.53 677.35 704.27 848.69 935.92 1022.50 1128.85 1166.86 1218.62 1324.04 1416.65 1455.89 1538.63 1608.32 1664.77 1823.77 1852.07 1876.85 90 123 146 146 171 178 178 305 366 366 415 471 471 536 579 586 651 675 699 843 922 1014 1122 1159 1211 1317 1411 1450 1534 1600 1661 1816 1846 1874 8 8.18E-03 65.2 9 3.49E-03217.5 15 2.79E-02 19.6 2.44E+OO 15 5.77E-02 10.7 7 2.02E-02 28.9 12 9.12E-03 27.1 l.26E+OO 12 4.42E-03138.0 8 2.80E-03182.l 14 2.77E-02 16.6 2.12E+OO 14 6.56E-03 59.9 7 9. 85E-03 41. 3 19 9.14E-02 6.7 1.94E+OO 19 2.52E-02 27.2 9 1.09E-02 38.6 7 4. 03E-03 81. 5 10 4.27E-02 13.1 10 5.90E-03 70.2 9 1.18E-02 39.5 12 6.77E-02 8.6 12 7.15E-03 48.8 16 2.64E-03184.9 20 1.29E-02 47.0 10 3.38E-03 70.1 14 2.90E-02 14.4 15 5.63E-02 9.3 12 8.82E-03 41.6 10 2.19E-03118.l 15 1.02E-02 35.1 9 2.64E-03 95.7 12 2.52E-03110.3 7 2. 82E-03 61. 0 16 l.42E-02 29.0 12 3.60E-03 38.6 6 1. 72E-03 68. 2 Peak Search Report (continued) Page : 2 Sample ID : G405235070 Acquisition date 3-0CT-2016 06:08:01 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 954.20 5 11 0.76 1909.16 1902 10 1.41E-03134.9 36 0 964 .16 27 7 3.99 1929.08 1923 13 7.56E-03 27.3 37 0 969. OH 35 2 1. 43 1938.79 1935 9 9.,76E-03 19.7 38 0 1033.74 15 8 3.09 2068.28 2061 12 4.05E-03 48.5 39 0 1037.83 11 2 0.57 2076.46 2073 8 2.98E-03 38.4 40 0 1062.58 6 9 1. 60 2125.97 2118 9 1.68E-03 98.4 41 0 1072.97 14 12 2.24 2146. 74 2135 14 3.97E-03 55.4 42 0 1100.06 8 10 0.72 2200.94 2195 9 2.22E-03 82.3 43 0 1121. 08* 29 21 1. 40 2242.98 2235 16 8.00E-03 42.7 44 0 1238.46 17 26 1. 06 2477.77 2471 12 4.71E-03 65.7 45 0 1307.89 11 0 0.66 2616.64 2611 9 3.06E-03 30.2 46 0 1333.34* 6 2 1.13 2667.54 2664 7 1.59E-03 63.2 47 0 1340.33 6 5 1. 51 2681. 52 2677 7 1.59E-03 78.5 48 0 1379.10 13 8 1.15 2759.06 2751 11 3.55E-03 51. 7 49 0 1460.97* 310 5 2.03 2922.80 2917 15 8.61E-02 5.9 50 0 1764.82* 31 10 0.57 3530.44 3524 17 8.51E-03 29.6 Flag: "*" = Peak area was modified by background subtraction Page 4538 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:08:28 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235070.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID ll-DEC-2015 10:10:00 G405235070 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:08:01 145.32 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAll 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4539 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 ' PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351.93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351. 06 CAN 0 01:00:00.53 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235070 Acquisition date 3-0CT-2016 06:08:01 Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status

  • K-40 1460.82 10.66* 1.238E+OO 1.16:7E+Ol 1.167E+Ol 11. 80 OK CD-109 88.03 3.70* 6.243E+OO 1.014E+OO l.583E+OO 117. 01 OK SN-126 64.28 9.60 3.889E+OO 2.201E-01 2.201E-01 434.94 OK 86.94 8.90 6.243E+OO 4.215E-01 4.215E-01 117. 01 OK 87.57 37.00* 6.243E+OO 1.014E-01 1.014E-01 117. 01 OK BA-137M 661.66 89.90* 2.339E+OO 8. 096E-02 8.249E-02 83.12 OK CS-137 661.66 85.10* 2.339E+OO 8.553E-02 8.715E-02 83.12 OK TL-208 277.37 6.60 4.714E+OO Line Not Found Absent 583.19 85.00* 2.582E+OO 2.579E-01 2.579E-01 28.75 OK 860.56 12.50 1.907E+OO Line Not Found Absent PB-210 46.54 4.25* 1.394E+OO 3.323E+00 3.408E+OO 130.43 OK PB-212 74.82 10.28 5.242E+00 5. 963E-01 5. 963E-01 83.22 OK 77 .11 17.10 5.455E+OO l.434E+OO 1.434E+OO 21. 33 OK 238.63 43.60* 5.300E+OO 8.358E-01 8.358E-01 13.43 OK 300.09 3.30 4.425E+OO Line Not Found Absent BI-214 609.32 45.49* 2. 496E+OO 9.653E-01 9.657E-01 18.59 OK 1120.29 14.92 1.547E+OO 6.361E-01 6.363E-01 85.47 OK 1764.49 15.30 1.040E+OO 9.388E-01 9. 391E-01 59.16 OK PB-214 74.82 5.80 5.234E+OO Line Not Found <<INT Reject 77.11 9.70 5.455E+OO 2.528E+OO 2.529E+OO 21. 33 OK 87.09 3.41 6.242E+OO Line Not Found <<INT Reject 242.00 7.25 5.244E+00 Line Not Found <<INT Reject 295.22 18.42 4.483E+OO 1.073E+OO 1.073E+00 26.29 OK 351. 93 35.60* 3.883E+OO 1.00lE+OO l.002E+OO 17.18 OK RN-222 609.32 45.49* 2.496E+OO 9.653E-01 9.657E-01 18.59 OK 1120.29 14.92 1.547E+OO 6.361E-01 6.363E-01 85.47 OK 1764.49 15.30 1. 040E+OO 9.388E-01 9. 391E-01 59.16 OK RA-224 240.99 4.10* 5.247E+OO 5. 761K-01 5. 761E-01 249.15 OK RA-226 609.32 45.49* 2. 496E+OO 9.653E-01 9.657E-01 18.59 OK 1120. 29 14.92 1. 54 7E+OO 6.361E-01 6.363E-01 85.47 OK 1764.49 15.30 1.040E+OO 9.388E-01 9. 391E-01 59.16 OK AC-228 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4.009E+OO 5.350E-01 5.350E-01 79.08 OK 794.95 4.25 2.028E+OO Line Not Found Absent 835. 71 1. 61 1. 951E+OO Line Not Found Absent 911.20 25.80* 1.823E+OO 5.658E-01 5.658E-01 58.05 OK 968.97 15.80 1.738E+OO 6.622E-01 6.622E-01 39.33 OK RA-228 105.21 1.10 7.023E+00 Line Not Found Absent 338.32 11. 27 4.009E+OO 5.350E-01 5.350E-01 79.08 OK 794.95 4.25 2.028E+OO Line Not Found Absent 835.71 1. 61 1. 951E+OO Line Not Found Absent 911. 20 25.80* 1.823E+OO 5.658E-01 5.658E-01 58.05 OK 968. 97 15.80 1. 738E+OO 6.622E-01 6.622E-01 39.33 OK TH-228 74.82 10.28 5.242E+OO 5. 963E-01 5. 963E-01 83.22 OK 77 .11 17.10 5.455E+00 1.434E+OO l.434E+OO 21. 33 OK 238.63 43.60* 5.300E+OO 8.358E-01 8.358E-01 13.43 OK 300.09 3.30 4.425E+OO Line Not Found Absent TH-230 609.32 45.49* 2. 496E+OO 9.653E-01 9.653E-01 18.59 OK 1120. 29 14.92 1.547E+OO 6.361E-01 6. 361E-01 85.47 OK Page 4540 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235070 Acquisition date 3-0CT-2016 06:08:01 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 1764.49 15.3Q 1.040E+OO 9.388E-01 9.388E-01 59.16. OK TH-232 105.21 1.10 7.023E+OO Line Not Found Absent 338.32 11. 27 4.009E+OO 5.350E-01 5.350E-01 79.08 OK 835. 71 1. 61 1. 951E+OO Line Not Found Absent 911. 20 25.80* 1.823E+00 5.658E-01 5.658E-01 58.05 OK 968.97 15.80 1.738E+OO 6.622E-01 6.622E-01 39.33 OK TH-234 63.29 3.70* 3.889E+OO 5.709E-01 5.709E-01 434.94 OK 92.59 4.23 6.570E+OO 3.632E-01 3.632E-01 276.07 OK U-234 609.32 45.49* 2. 496E+OO 9.653E-01 9.653E-01 18.59 OK 1120.29 14.92 1. 547E+OO 6.361E-01 6.361E-01 85.47 OK 1764.49 15.30 1.040E+OO 9.388E-01 9.388E-01 59.16 OK U-235 89. 96 3.47 6.410E+OO 9.390E-01 9.390E-01 54.30 OK 93.35 5.60 6.570E+OO 2.743E-01 2.743E-01 276.07 OK 143.76 10. 96* 7.059E+OO Line Not Found Absent 163.33 5.08 6.731E+OO Line Not Found Absent 185. 72 57.20 6.286E+OO 1.665E-01 1.665E-01 33 .11 OK 205.31 5.01 5.902E+OO Line Not Found Absent U-238 63.29 3.70* 3.889E+OO 5.709E-01 5.709E-01 434.94 OK 92.59 4.23 6.570E+OO 3.632E-01 3.632E-01 276.07 OK AM-243 43.53 5.90 9.310E-01 Line Not Found Absent 74.66 67.20* 5.242E+OO 9.122E-02 9.122E-02 83.22 OK ANH-511 511. 00 100.00* 2.868E+OO 8.924E-02 8.924E-02 94.03 OK Flag: "*" = Keyline Page 4541of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:08:29.97 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235070.CNF;l *
  • Acquisition date 3-0CT-2016 06:08:01 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.53 Half life ratio : ***** *
  • Sample date 11-DEC-2015 10:10:00 Analyst initials: MXRl *
  • Sample ID G405235070 Sample Quantity 1.4532E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1 . 96-sigma ) K-40 1.167E+Ol l.350E+00 CD-109 1.583E+OO 1.816E+OO SN-126 l.014E-01 l.162E-01 BA-137M 8.249E-02 6.719E-02 CS-137 8. 715E-02 7.098E-02 TL-208 2.579E-01 7.266E-02 PB-210 3.408E+OO 4.356E+OO PB-212 8.358E-01 1.lOOE-01 BI-214 9.657E-01 1. 759E-01 PB-214 1.002E+OO 1.686E-01 RN-222 9.657E-01 1. 759E-01 RA-224 5.761E-01 1. 407E+OO. RA-22 6 9.657E-01 1. 759E-01 AC-228 5.658E-01 3.219E-01 RA-228 5.658E-01 3.219E-01 TH-228 8.358E-01 l.lOOE-01 TH-230 9.653E-01 1. 758E-01 TH-232 5.658E-01 3.219E-01 TH-234 5.709E-01 2.434E+OO U-234 9.653E-01 1. 758E-01 U-235 2.754E-02 1.494E-01 U-238 5.709E-01 2.434E+OO AM-243 9.122E-02 7.440E-02 ANH-511 8.924E-02 8.223E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 Page 4542 of 5809 Key-Line Activity (pCi/GRAM -3.262E+OO l.054E-02 O.OOOE+OO -l.122E-03 4.365E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.117E+Ol 3.934E-02 1.812E+41 2.541E-02 2.870E-01 1.407E+04 MDA (pCi/GRAM 5.150E-01 1.632E+OO 1.050E-01 6.223E-02 6.574E-02 5.770E-02 3.737E+OO 7.582E-02 1.048E-01 l.004E-01 1.048E-01 8 .130E-01 1. 048E-01 2.216E-01 2.216E-01 7.582E-02 1. 048E-01 2.216E-01 1. 789E+OO 1.048E-01 2.868E-01 1. 789E+OO 7.361E-02 4.533E-02 MDA (pCi/GRAM 2 .113E+Ol 8.378E-02 O.OOOE+OO 5.493E-02 5.819E-01 0.000E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF CR-51 O.OOOE+OO 3.008E+02 0.000E+OO SHORT HLIF MN-54 2.320E-02 6.648E-02 l.209E-01 NOT IDENT. C0-56 -l.392E-01 3.889E-Ol 7.029E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.030E-02 3.701E-02 7.277E-02 NOT IDENT. C0-58 -2.431E-01 4.814E-01 8.474E-01 NOT IDENT. FE-59 4.693E+OO 7.567E+OO l.257E+Ol FAIL ABUN C0-60 2. 391E-02 2.964E-02 7.534E-02 FAIL ABUN ZN-65 3.441E-03 l.700E-01 3.039E-01 NOT IDENT. GE-68 . 2.213E-01 2.143E+OO 4.279E+OO NOT IDENT. AS-73 2.370E+OO 5.355E+OO 1.119E+Ol NOT IDENT. AS-74, O.OOOE+OO 4.364E+03 O.OOOE+OO SHORT HLIF SE-75 l.242E-01 l.839E-01 3.612E-01 NOT IDENT. BR-77 O.OOOE+OO 8.255E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.995E+02 0.000E+OO SHORT HLIF RB-83 5.316E-02 5.372E-01 1. 07 6E+OO NOT IDENT. KR-85 2. 996E+OO 6.061E+OO 1.251E+Ol NOT IDENT. SR-85 3.054E-01 6.203E-01 1.280E+OO NOT IDENT. RB-86 0.000E+OO 2.468E+04 0.000E+OO SHORT HLIF Y-88 -2.212E-02 2.032E-01 4.180E-01 NOT IDENT. Y-91 -7.389E+Ol 4.686E+02 9.109E+02 NOT IDENT. NB-94 1.224E-02 3.322E-02 6. 051E-02 NOT IDENT. NB-95 1. 517E-Ol 8.418E-01 1.484E+OO NOT IDENT. NB-95M -2.286E-01 2.109E+OO 3. 513E+OO NOT IDENT. ZR-95 4. 511E-02 1.139E+OO 2.245E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.255E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 6.357E+31 O.OOOE+OO SHORT HLIF TC-99M 0.000E+OO l.241E+41 O.OOOE+OO SHORT HLIF RH-101 -9.025E-03 2.576E-02 4.784E-02 NOT IDENT. RH-102 -7.239E-03 4.809E-02 9.256E-02 NOT IDENT. RU-103 -3.861E+OO 4.462E+OO 7.776E+OO FAIL ABUN RH-106 2.061E-03 4.354E-01 8. 511E-01 NOT IDENT. RU-106 2.061E-03 4.354E-01 8. 511E-01 NOT IDENT. AG-108M -1. 589E-02 2.096E-02 3.781E-02 NOT IDENT. AG-llOM -3.045E-02 8. 511E-02 1.534E-01 FAIL ABUN SN-113 -1. 898E-01 1.828E-01 3.201E-01 NOT IDENT. CD-115 0.000E+OO l.252E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 6.644E+04 O.OOOE+OO SHORT HLIF TE-123M 4.518E-02 1.029E-01 2.021E-01 NOT IDENT. SB-124 -l.159E+OO 1.580E+OO 2.548E+OO NOT IDENT. SB-125 -1.824E-02 9.016E-02 1.567E-01 NOT IDENT. TE-125M 1.050E+02 1.958E+02 3.969E+02 NOT IDENT. I-126 0.000E+OO 6. 931E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 7.604E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 1.122E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.024E+09 O.OOOE+OO SHORT HLIF I-132 0.000E+OO 8.034E+40 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1. 761E+26 O.OOOE+OO SHORT HLIF BA-133 -1. 802E-02 3.626E-02 6.075E-02 NOT IDENT. I-133 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF CS-134 2.558E-02 4.143E-02 8.824E-02 FAIL ABUN CS-135 2.486E-02 1.327E-01 2.289E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.353E+05 O.OOOE+OO SHORT HLIF CE-139 1.815E-04 9.058E-02 1. 701E-01 NOT IDENT. BA-140 O.OOOE+OO 9.207E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 3.259E+05 0.000E+OO SHORT HLIF CE-141 -1. 480E+Ol 1.959E+Ol 3.457E+Ol NOT IDENT. CE-143 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -7. 716E-02 2. 771E-01 5.160E-01 NOT IDENT. PM-144 5.051E-03 4.876E-02 9.556E-02 NOT IDENT. PR-144 4.523E-Ol 4.231E+OO 8.296E+OO NOT IDENT. PM-146 2.999E-02 3.774E-02 8.120E-02 NOT IDENT. ND-147 0.000E+OO 2.493E+07 0.000E+OO SHORT HLIF PM-147 4.292E+02 6.456E+02 l.310E+03 NOT IDENT. PM-149 O.OOOE+OO 1.517E+40 O.OOOE+OO SHORT HLIF EU-150 l.285E-02 2.188E-02 4.583E-02 FAIL ABUN EU-152 2.666E:.._02 7.828E-02 1.560E-01 FAIL'ABUN GD-153 -1. 276E-01 1.299E-01 2.318E-01 NOT IDENT. EU-154 2.362E-02 9.607E-02 2. 041E-01 NOT IDENT. EU-155 6.683E-02 8.250E-02 l.702E-01 FAIL ABUN TB-160 3. 716E-01 1.504E+OO 3.064E+OO FAIL ABUN H0-166M -6.542E-03 5.000E-02 8.500E-02 FAIL ABUN TM-171 2.933E+OO 1.300E+Ol 2.678E+Ol NOT IDENT. HF-172 -7.933E-02 1. 730E-01 3.184E-Ol FAIL ABUN LU-172 -l.162E-02 6.856E-02 1.257E-01 FAIL ABUN LU-176 9.543E-03 2.141E-02 4 .112E-02 FAIL ABUN Page 4543 of 5809 HF-181 -8.376E-01 3.554E+OO 6.816E+00 NOT IDENT. TA-182 6.822E-01 9.614E-01 2.042E+OO FAIL ABUN RE-183 1.224E+OO 2.109E+00 4.370E+OO NOT IDENT. RE-184 -1.286E+Ol 2.688E+Ol 4.680E+Ol NOT IDENT. W-188 8.761E+Ol l.399E+02 1. 954E+02 FAIL ABUN IR-192 -2.867E-01 3.905E-01 6.375E-01 FAIL ABUN HG-203 -1.115E+OO 2.170E+OO 3.701E+OO NOT IDENT. BI-207 2.612E-02 5.037E-02 8.917E-02 FAIL ABUN BI--:211 O.OOOE+OO 4.645E-01 7.574E-01 FAIL ABUN PB-211 2.210E-01 5.519E-01 l.145Ei-00 FAIL ABUN BI-212 O.OOOE+OO 9.300E-01 1. 280E+OO FAIL ABUN RN-219 9.000E-02 2.981E-01 6 .. 166E-Ol FAIL ABUN RA-223 8.487E-02 5.232E-01 9.679E-01 FAIL ABUN AC-227 5.257E-03 2.163E-01 3.951E-01 NOT IDENT. TH-227 5.257E-03 2.163E-01 3.951E-01 NOT IDENT. TH-229 -1.258E-01 3.926E-01 7. 071E-01 FAIL ABUN PA-231 -6.136E-02 4.025E-01 7.149E-01 NOT IDENT. TH-231 8.487E-02 5.232E-01 9.679E-01 FAIL ABUN PA-233 -2.102E-02 5.476E-02 9.432E-02 NOT IDENT. PA-234 -2.132E-02 2.438E-01 4.601E-01 FAIL ABUN PA-234M 3.620E+OO 3.540E+OO 8.234E+OO NOT IDENT. NP-237 -2.102E-02 5.476E-02 9.432E-02 NOT IDENT. NP-238 O.OOOE+OO 9.865E+40 O.OOOE+OO SHORT HLIF NP-239 -9.0lSE-03 1.987E-01 3.800E-01 NOT IDENT. PU-239 1.468E+02 2.473E+02 4.944E+02 NOT IDENT. AM-241 6.535E-03 l.112E-01 2.066E-01 NOT IDENT. CM-243 -7.364E-03 7.517E-02 1.448E-01 NOT IDENT. BK-247 4.298E-02 6.384E-02 l.257E-01 NOT IDENT. CM-247 5. 901E-04 2.674E-02 5.377E-02 NOT IDENT. CF-249 2.225E-02 2.870E-02 6.255E-02 NOT IDENT. CF-251 -9.785E-02 9.424E-02 1.581E-01 NOT IDENT. Page 4544 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:08:27.75 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 298 10.66* l.238E+OO l.167E+Ol l.167E+Ol 11. 80 CD-109 88.03 90 3.70* 6.243E+OO 2.002E+OO 3.128E+OO 57.80 SN-126 64.28 16 9.60 3.889E+OO 2.201E-Ol 2.201E-01 434.94 86. 94 90 8.90 6.243E+OO 8.325E-Ol 8.325E-01 57.80 87.57 90 37.00* 6.243E+OO 2.002E-01 2.002E-01 57.80 BA-137M 661.66 33 89.90* 2.339E+OO 8.096E-02 8.249E-02 83.12 CS-137 661. 66 33 85.10* 2.339E+OO 8.553E-02 8. 715E-02 83.12 TL-208 277.37 ------6.60 4.714E+OO ------Line Not Found ------583.19 llO 85.00* 2.582E+OO 2.579E-01 2.579E-01 28.75 860.56 ------12.50 l.907E+OO ------Line Not Found ------PB-210 46.54 38 4.25* l.394E+OO 3.323E+OO 3.408E+OO 130.43 BI-2ll 72.87 ------1. 23 5.033E+OO ------Line Not Found ------351. 06 268 12.92* 3.883E+OO 2.759E+OO 2.759E+OO 17.18 PB-212 74.82 125 10.28 5.242E+OO l.202E+OO l.202E+OO 39.12 77. ll 259 17.10 5.455E+OO l.434E+OO l.434E+OO 21. 33 238.63 374 43.60* 5.300E+OO 8.358E-01 8.358E-01 13. 43 300.09 ------3.30 4.425E+OO ------Line Not Found ------BI-214 609.32 212 45.49* 2.496E+OO 9.653E-01 9.657E-01 18.59 ll20.29 28 14.92 l.547E+OO 6.361E-01 6.363E-01 85.47 1764.49 29 15.30 l.040E+OO 9.388E-01 9. 391E-01 59.16 PB-214 74.82 125 5.80 5.242E+OO 2.130E+OO 2.130E+OO 39.12 77. ll 259 9.70 5.455E+OO 2.528E+OO 2.529E+OO 21. 33 87.09 90 3.41 6.243E+OO 2.173E+OO 2.173E+OO 57.80 242.00 103 7.25 5.247E+OO l.398E+OO l.399E+OO 54.42 295.22 171 18.42 4.483E+OO l.073E+OO l.073E+OO 26. 29 351. 93 268 35.60* 3.883E+OO l.OOlE+OO l.002E+OO 17.18 RN-222 609.32 212 45.49* 2. 496E+OO 9.653E-01 9.657E-01 18.59 ll20.29 28 14.92 l.547E+OO 6.361E-01 6.363E-01 85.47 1764.49 29 15.30 l.040E+OO 9.388E-01 9.391E-01 59.16 RA-224 240.99 103 4.10* 5.247E+OO 2.473E+OO 2.473E+OO 54.42 RA-226 609.32 212 45.49* 2.496E+OO 9.653E-01 9.657E-01 18.59 ll20.29 28 14.92 l.547E+OO 6.361E-01 6.363E-01 85.47 1764.49 29 15.30 l.040E+OO 9.388E-01 9. 391E-01 59.16 AC-228 105.21 ------1.10 7'.023E+OO ------Line Not Found ------338.32 47 11. 27 4.009E+OO 5.350E-01 5.350E-01 79.08 794.95 ------4.25 2.028E+OO ------Line Not Found ------835.71 ------1. 61 l.951E+OO ------Line Not Found ------911.20 52 25.80* l.823E+OO 5.658E-01 5.658E-01 58.05 968.97 35 15.80 l.738E+OO 6.622E-01 6.622E-01 39.33 RA-228 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 47 11. 27 4.009E+OO 5.350E-01 5.350E-01 79.08 794.95 ------4.25 2.028E+OO ------Line Not Found ------835.71 ------1. 61 1. 951E+OO ------Line Not Found ------9ll. 20 52 25.80* l.823E+OO 5.658E-01 5.658E-01 58.05 968.97 35 15.80 l.738E+OO 6.622E-01 6.622E-01 39.33 TH-228 74.82 125 10.28 5.242E+OO l.202E+OO l.202E+OO 39.12 77. ll 259 17.10 5.455E+OO l.434E+OO l.434E+OO 21. 33 Page 4545 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235070 Acquisition date 3-0CT-2016 06:08:01 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error 238.63 374 43.60*
  • 5. 300E+OO 8.358E-01 8.358E-01 13. 43
  • 300.09 ------3.30 4.425E+OO ------Line Not Found ------TH-230 609.32 212 45.49* 2.496E+OO 9.653E-01 9.653E-01 18.59 1120. 29 28 14.92 1.547E+OO 6.361E-01 6.361E-01 85.47 1764.49 29 15.30 1.040E+OO 9.388E-01 9.388E-01 59.16 TH-232 105.21 ------1.10 7.023E+OO ------Line Not Found ------338.32 47 11. 27 4.009E+OO 5.350E-01 5.350E-01 79.08 835.71 ------1. 61 1.951E+OO ------Line Not Found ------911.20 52 25.80* 1.823E+00 5.658E-01 5.658E-01 58.05 968. 97 35 15.80 1.738E+00 6.622E-01 6.622E-01 39.33 TH-234 63.29 16 3.70* 3.889E+OO 5.709E-01 5.709E-01 434.94 92.59 20 4.23 6.570E+OO 3.632E-01 3.632E-01 276.07 U-234 609.32 212 45.49* 2. 496E+00 9.653E-01 9.653E-01 18.59 1120,29 28 14.92 1.547E+OO 6.361E-01 6.361E-01 85.47 1764.49 29 15.30 1.040E+OO 9.388E-01 9.388E-01 59.16 U-235 89. 96 40 3.47 6.410E+00 9.390E-01 9.390E-01 54.30 93.35 20 5.60 6.570E+OO 2.743E-01 2.743E-01 276.07 143.76 ------10. 96* 7.059E+OO ------Line Not Found ------'163.33 ------5.08 6.731E+OO ------Line Not Found ------185. 72 116 57.20 6.286E+00 l.665E-01 1.665E-01 33.11 205.31 ------5.01 5.902E+OO ------Line Not Found ------U-238 63.29 16 3.70* 3.889E+OO 5.709E-01 5.709E-01 434.94 92.59 20 4.23 6.570E+OO 3.632E-01 3.632E-01 276.07 AM-243 43.53 ------5.90 9.310E-01 ------Line Not Found ------74.66 125 67.20* 5.242E+OO l.838E-01 l.838E-01 39.12 ANH-511 511.00 50 100.00* 2.868E+OO 8.924E-02 8.924E-02 94.03 Flag: "*" Key line Page 4546 of 5809 Summary of Nuclide Activity Sample ID : G405235070 Acquisition date Page : 3 3-0CT-2016 06:08:01 Total number of lines in spectrum 50 Number of unidentified lines 9 Number of lines tentatively identified by NID 41 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 ' TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 461. 40D 2.30E+05Y 30.08Y 30.08Y 1. 41E+l0Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY l.41E+l0Y 1600. OOY l.41E+l0Y 1.41E+10Y 1.41E+l0Y 7.54E+04Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 56 1. 00 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.167E+Ol 2.002E+OO 2.002E-01 8. 096E-02 8.553E-02 2.579E-01 3.323E+OO 2.759E+OO 8.358E-01 9.653E-01 1.00lE+OO 9.653E-01 2.473E+OO 9.653E-01 5.658E-01 5. 658E-01' 8.358E-01 9.653E-01 5.658E-01 5.709E-01 9.653E-01 1.665E-01 5.709E-01 l.838E-01 8.924E-02 3.363E+Ol 3.363E+Ol Decay Corr pCi/GRAM l.167E+Ol 3.128E+OO 2.002E-01 8.249E-02 8. 715E-02 2.579E-01 3.408E+OO 2.759E+OO 8.358E-01 9.657E-01 1.002E+OO 9.657E-01 2.473E+OO 9.657E-01 5.658E-01 5.658E-01 8.358E-01 9.653E-01 5.658E-01 5.709E-01 9.653E-01 1.665E-01 5.709E-01 1.838E-01 8.924E-02 3.484E+Ol 3.484E+Ol 82.00% Decay Corr 2-Sigma Error 0.138E+01 l.808E+OO 1.157E-01 6.856E-02 7.243E-02 0.741E-01 4.445E+OO 0.474E+OO l.122E-01 1. 795E-01 0.172E+OO 1. 795E-01 1.346E+OO 1. 795E-01 3.284E-01 3.284E-01 1.122E-01 1. 794E-01 3.284E-01 24.83E-01 1.794E-01 0.551E-01 24.83E-01 0.719E-01 8.391E-02 "M" Manually accepted 2-Sigma %Error 11.80 57.80 57.80 83.12 83.12 28.75 130.43 17.18 13.43 18.59 17.18 18.59 54.42 18.59 58.05 58.05 13.43 18.59 58.05 434.94 18.59 33.11 434.94 39.12 94.03 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page4547 of5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235070 Acquisition date : 3-0CT-2016 06:08:01 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Ef f Flags 0 155.71 12 127 1. 44 311.46 305 8 2.80E-03 **** 6.87E+OO T 6 188.16 27 65 1. 57 376.39 366 14 6.56E-03 **** 6.24E+OO 0 209.06 41 75 0.95 418.23 415 7 9.85E-03 82.6 5.83E+OO 0 270.20 44.; 64 1. 62 540.58 536 9 1. 09E-02 77 .,2 4.81E+OO T 0 291.11 16 51 1.12 582.41 579 7 4.03E-03 **** 4.53E+OO T 0 328.14 23 64 0.61 656.53 651 10 5.90E-03 **** 4. llE+OO T 0 424.17 28 36 3.35 848.69 843 12 7.15E-03 97.7 3.33E+OO T 0 467.76 10 65 5.36 935.92 922 16 2.64E-03 **** 3.08E+OO T 0 564.18 13 18 1. 43 1128. 85 1122 10 3.38E-03 **** 2.65E+OO T 0 708.02 8 23 1.11 1416.65 1411 10 2.19E-03 **** 2.22E+OO T 0 727. 64 38 28 1. 58 1455.89 1450 15 1. 02E-02 70.2 2.17E+OO T 0 768.99 10 23 1. 64 1538.63 1534 9 2.64E-03 **** 2.08E+OO 0 803.82 9 21 2.37 1608.32 1600 12 2.52E-03 **** 2.0lE+OO 0 832.04 10 10 1.14 1664.77 1661 7 2.82E-03 **** 1. 96E+OO T 0 925.66 13 3 4.39 1852.07 1846 12 3.60E-03 77.1 1. 80E+OO T 0 938.05 6 5 0.84 1876.85 1874 6 1.72E-03 **** 1. 78E+OO T 0 954.20 5 11 0.76 1909.16 1902 10 1.41E-03 **** 1. 76E+OO T 0 964 .16 27 7 3.99 1929.08 1923 13 7.56E-03 54.6 1. 74E+OO T 0 1033.74 15 8 3.09 2068.28 2061 12 4.05E-03 97.0 1.65E+00 0 1037.83 11 2 0.57 2076.46 2073 8 2.98E-03 76.8 1.65E+OO T 0 1062.58 6 9 1. 60 2125.97 2118 9 1. 68E-03 **** 1. 62E+OO T 0 1072. 97 14 12 2.24 214'6.74 2135 14 3.97E-03 **** 1.60E+OO 0 1100.06 8 10 0. 72 2200.94 2195 9 2.22E-03 **** 1. 57E+OO T 0 1238.46 17 25 1. 06 2477.77 2471 12 4. 71E-03 **** 1.43E+OO T 0 1307.89 11 0 0.66 2616.64 2611 9 3.06E-03 60.3 1.36E+OO 0 1333.34 6 2 1.13 2667.54 2664 7 1.59E-03 **** 1.34E+OO T 0 1340.33 6 5 1. 51 2681.52 2677 7 1.59E-03 **** 1.33E+OO 0 1379.10 12 8 1.15 2759.06 2751 11 3.55E-03 **** 1.30E+OO Flags: "T" = Tentatively associated Page 4548of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:08:41.77 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* .(" .; *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235070.CNF;l *
  • Acquisition date 3-0CT-2016 06:08:01 Sensitivity 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.53 Half life ratio : ***** *
  • Sample date 11-DEC-2015 10:10:00 Nuclide Library : SOLID *
  • Sample ID G405235070 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : l.4532E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM11 CAN.CNF;l4
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.043E-01 7.665E-01 4.928E-02 2.766E-02 2.922E-02 2.559E-02 1.737E+OO 3.476E-02 4.609E-02 4.498E-02 4.609E-02 3. 727E-01 4.609E-02 9.571E-02 9. 571E-02 3.476E-02 4.607E-02 9.571E-02 8.423E-01 4.607E-02 1.339E-01 8.423E-01 3.468E-02 2.016E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4549 of 5809 Le (pCi/GRAM 9.479E+OO 3.561E-02 O.OOOE+OO 2.056E-02 2.464E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS.r73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 "LU-176 HF-181 Page 4550 of 5809 5.341E-02 2.986E-01 O.OOOE+OO 3.384E-02 3.584E-01 5.477E+OO 3.183E-02 1.311E-01 1.846E+OO 5.212E+OO O.OOOE+OO l.665E-01 O.OOOE+OO O.OOOE+OO 4.767E-01 5.643E+OO 5.775E-01 0.000E+OO 1.605E-01 3.929E+02 2.706E-02 6.569E-01 1.620E+OO 9.678E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.214E-02 4.016E-02 3.379E+00 3.746E-01 3.746E-01 l.647E-02 6.478E-02 l.414E-01 O.OOOE+OO O.OOOE+OO 9.384E-02 8.590E-01 6.940E-02 1. 846E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2. 718E-02 O.OOOE+OO 3.873E-02 1.051E-01 O.OOOE+OO O.OOOE+OO 7.895E-02 O.OOOE+OO O.OOOE+OO 1.607E+Ol O.OOOE+OO 2.389E-01 4.216E-02 3.660E+OO 3. 672E-02 O.OOOE+OO 6.104E+02 O.bOOE+OO 2.103E-02 7.085E-02 l.070E-01 8.662E-02 7.950E-02 1.315E+OO 3.653E-02 1.245E+Ol 1.470E-01 5.324E-02 l.878E-02 3.027E+OO NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237, NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM:.._247 CF-249 CF-251 Page 4551 of 5809 9.120E-01 2.053E+OO 2.00lE+Ol 9.014E+Ol 2.852E-01 1.693E+OO 3.862E-02 3.644E-01 5.172E-01 5. 911E-01 2.769E-01 4.403E-01 1.823E-01 1.823E-01 3.265E-01 3.267E-01 4.403E-01' 4.277E-02 1. 967E-01 3.620E+OO 4.277E-02 O.OOOE+OO 1.771E-01 2.310E+02 9.710E-02 6. 721E-02 5.787E-02 2.400E-02 2.822E-02 7.248E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:08:47.13 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235070.CNF;l *
  • Acquisition date 3-0CT-2016 06:08:01 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.53 Half life ratio : ***** *
  • Sample date 11-DEC-2015 10:10:00 Nuclide Library : SOLID *
  • Sample ID G405235070 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4532E+02 GRAM *
  • Quantity Err(%) : 1.3763E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* *
  • CALIBRATION INFORMATION * * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;14
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.167E+Ol 1.481E+OO 1.481E+OO CD-109 1.583E+OO 1.830E+OO l.830E+OO SN-126 1.014E-01 1.171E-01 l.171E-01 BA-137M 8.249E-02 6.729E-02 6.729E-02 CS-137 8. 715E-02 7.108E-02 7.108E-02 TL-208 2.579E-01 7.349E-02 7.349E-02 PB-210 3.408E+OO 4.365E+OO 4.365E+OO PB-212 8.358E-01 1.185E-01 1.185E-01 BI-214 9.657E-01 1.807E-01 l.807E-01 PB-214 l.002E+OO 1.737E-01 l.737E-01 RN-222 9.657E-01 1.807E-01 1.807E-01 RA-224 5.761E-01 1.412E+OO 1.412E+OO RA-226 9.657E-01 1.807E-01 1.807E-01 AC-228 5.658E-01 3.232E-01 3,232E-01 RA-228 5.658E-01 3.232E-01 3.232E-01 TH-228 8.358E-01 1.185E-01 l.185E-01 TH-230 9.653E-01 1.807E-01 1.807E-01 TH-232 5.658E-01 3.232E-01 3.232E-01 TH-234 5.709E-01 2.437E+OO 2.437E+OO U-234 9.653E-01 1.807E-01 1.807E-01 U-235 2.754E-02 l.494E-01 1.494E-01 U-238 5.709E-01 2.437E+OO 2.437E+OO AM-243 9.122E-02 7.553E-02 7.553E-02 ANH-511 8.924E-02 8. 231E-02 8. 231E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1 . 96-sigma) ( 1. 96-sigma) BE-7 -3.262E+OO 1.117E+Ol 1.127E+Ol NOT IDENT. NA-22 l.054E-02 3.934E-02 3. 962E-02 NOT IDENT. NA-24 1.000E+41 1. 862E+41 O.OOOE+OO SHORT HLIF AL-26 -1.122E-03 2.541E-02 2.541E-02 NOT IDENT. SC-46 4.365E-02 2.870E-01 2.877E-01 FAIL ABUN V-48 -7.055E+03 1.408E+04 1.443E+04 SHORT HLIF Page 4552 of 5809 CR-51 7.217E+01 3,008E+02 3.026E+02 SHORT HLIF MN-54 2.320E-02 6.649E-02 6.731E-02 NOT IDENT. C0-56 -l.392E-01 3.889E-01 3.939E-01 FAIL ABUN MN-56 -1.000E+41 2.729E+41 0.000E+OO SHORT HLIF C0-57 l.030E-02 3.701E-02 3.730E-02 NOT IDENT. C0-58 -2.431E-01 4.815E-01 4.938E-01 NOT IDENT. FE-59 4.693E+00 7.574E+OO 7.864E+OO FAIL ABUN C0-60 2.391E-02 2. 965E-02 3.155E-02 FAIL ABUN ZN-65 3. 441E-03 1.700E-01 l.700E-01 NOT IDENT. GE-68 2.213E-01 2.143E+OO 2.145E+OO NOT IDENT. AS-73 2.370E+OO 5.377E+OO 5.482E+OO NOT IDENT. AS-74 -4.752E+03 4.382E+03 4.878E+03 SHORT HLIF SE-75 l.242E-01 1.840E-01 1.923E-01 NOT IDENT. BR-77 6.274E+37 5.376E+38 O.OOOE+OO SHORT HLIF SR-82 6.995E+Ol 5.995E+02 6.003E+02 SHORT HLIF RB-83 5.316E-02 5. 372E-01 5.378E-01 NOT IDENT. KR-85 2. 996E+OO 6.062E+OO 6. 211E+OO NOT IDENT. SR-85 3.054E-01 6.205E-01 6.356E-01 NOT IDENT. RB-86 -5.303E+03 2.468E+04 2.480E+04 SHORT HLIF Y-88 -2.212E-02 2.032E-01 2.035E-01 NOT IDENT. Y-91 -7.389E+Ol 4.686E+02 4.698E+02 NOT IDENT. NB-94 1.224E-02 3.322E-02 3.368E-02 NOT IDENT. NB-95 1. 517E-01 8.418E-01 8,446E-01 NOT IDENT. NB-95M -2.286E-01 2.109E+OO 2.112E+OO NOT IDENT. ZR-95 4. 511E-02 l.139E+OO 1.139E+OO NOT IDENT. NB-97 -l.000E+41 2.188E+42 0.000E+OO SHORT HLIF ZR-97 1.000E+41 1.256E+41 O.OOOE+OO SHORT HLIF M0-99 1. 326E+31 6.357E+31 O.OOOE+OO SHORT HLIF TC-99M -l.000E+41 l.244E+41 O.OOOE+OO SHORT HLIF RH-101 -9.025E-03 2.582E-02 2.614E-02 NOT IDENT. RH-102 -7.239E-03 4.810E-02 4.821E-02 NOT IDENT. RU-103 -3.861E+OO 4.466E+OO 4.793E+OO FAIL ABUN RH-106 2.061E-03 4.354E-01 4.354E-01 NOT IDENT. RU-106 2.061E-03 4.354E-01 4.354E-01 NOT IDENT. AG-108M -l.589E-02 2.097E-02 2.216E-02 NOT IDENT. AG-llOM -3.045E-02 8.513E-02 8.623E-02 FAIL ABUN SN-113 -l.898E-01 l.829E-01 2.020E-01 NOT IDENT. CD-115 l.650E+38 l.252E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 1.083E+04 6.645E+04 6.663E+04 SHORT HLIF TE-123M 4.518E-02 l.029E-01 l.049E-01 NOT IDENT. SB-124 -l.159E+OO l.581E+OO 1. 665E+OO NOT IDENT. SB-125 -l.824E-02 9.016E-02 9.054E-02 NOT IDENT. TE-125M l.050E+02 l.959E+02 2.016E+02 NOT IDENT. I-126 3.378E+05 6.946E+05 7 .111E+05 SHORT HLIF SB-126 2.028E+05 7.614E+05 7.669E+05 SHORT HLIF SB-127 -l.127E+21 l.132E+.22 O.OOOE+OO SHORT HLIF I-131 -3.540E+08 3.024E+09 3.028E+09 SHORT HLIF I-132 -1.000E+41 1. 831E+42 O.OOOE+OO SHORT HLIF TE-132 -2.052E+25 1. 7 63E+2 6 O.OOOE+OO SHORT HLIF BA-133 -l.802E-02 3.627E-02 3.717E-02 NOT IDENT. I-133 l.OOOE+41 2.945E+41 O.OOOE+OO SHORT HLIF CS-134 2.558E-02 4.144E-02 4.302E-02 FAIL ABUN CS-135 2.486E-02 1.327E-01 l.332E-01 NOT IDENT. I-135 1.000E+41 7.219E+41 O.OOOE+OO SHORT HLIF CS-136 -2. 431E+04 2.353E+05 2.355E+05 SHORT HLIF CE-139 1. 815E-04 9.058E-02 9.058E-02 NOT IDENT. BA-140 2.953E+05 9.207E+05 9.303E+05 SHORT HLIF LA-140 -3.335E+05 3.262E+05 3.592E+05 SHORT HLIF CE-141 -1.480E+Ol 1. 960E+Ol 2.070E+Ol NOT IDENT. CE-143 1.000E+41 2.702E+41 O.OOOE+OO SHORT HLIF CE-144 -7.716E-02 2. 772E-01 2.793E-01 NOT IDENT. PM-144 5.051E-03 4.876E-02 4. 881E-02 NOT IDENT. PR-144 4.523E-01 4. 231E+OO 4.236E+OO NOT IDENT. PM-146 2.999E-02 3.781E-02 4.015E-02 NOT IDENT. ND-147 2.274E+06 2.493E+07 2.495E+07 SHORT HLIF PM-147 4.292E+02 6.459E+02 6.743E+02 NOT IDENT. PM-149 -l.717E+39 1.517E+40 O.OOOE+OO SHORT HLIF EU-150 l.285E-02 2.189E-02 2.264E-02 FAIL ABUN EU-152 2.666E-02 7.830E-02 7.921E-02 FAIL ABUN GD-153 -l.276E-01 l.301E-01 l.423E-01 NOT IDENT. EU-154 2.362E-02 9.607E-02 9.666E-02 NOT IDENT. EU-155 6.683E-02 8.264E-02 8.796E-02 FAIL ABUN TB-160 3.716E-01 1.504E+OO 1. 513E+OO FAIL ABUN H0-166M -6.542E-03 5.000E-02 5.009E-02 FAIL ABUN TM-171 2.933E+OO l.300E+Ol 1.307E+Ol NOT IDENT. HF-172 -7.933E-02 1.734E-Ol 1.771E-01 FAIL ABUN LU-172 -1.162E-02 6.857E-02 6.877E-02 FAIL ABUN LU-176 9.543E-03 2.141E-02 2.184E-02 FAIL ABUN Page 4553 of 5809 HF-181 -8.376E-01 3.554E+OO 3.574E+OO NOT IDENT. TA-182 6.822E-01 9.618E-01 l.OlOE+OO FAIL ABUN RE-183 1. 224E+OO 2 .117E+OO 2.188E+OO NOT IDENT. RE-184 -l.286E+Ol 2.706E+Ol 2.767E+Ol NOT IDENT. W-188 8.761E+Ol l.403E+02 1.457E+02 FAIL ABUN IR-192 -2.867E-01 3.907E-01 4 .115E-01 FAIL ABUN HG-203 -l .115E+OO 2.171E+OO 2.228E+OO NOT IDENT. BI-207 2.612E-02 5.038E-02 5.174E-02 FAIL ABUN BI-211 2.759E+OO 4.806E-01 1.334E+OO FAIL ABUN PB-211 -! 2.210E-01 5.520E-01 5.609E-Ol. FAIL ABUN BI-212 1.353E+OO 9.325E-01 l .114E+OO FAIL ABUN RN-219 9.000E-02 2.983E-01 3.0lOE-01 FAIL ABUN RA-223 8.487E-02 5.232E-01 5.246E-01 FAIL ABUN AC-227 5.257E-03 2.163E-01 2.163E-01 NOT IDENT. TH-227 5.257E-03 2.163E-01 2.163E-01 NOT IDENT. TH-229 -1.258E-01 3.926E-01 3. 967E-01 FAIL ABUN PA-231 -6.136E-02 4.027E-01 4.036E-01 NOT IDENT. TH-231 8.487E-02 5.232E-01 5.246E-01 FAIL ABUN PA-233 -2.102E-02 5.476E-02 5.558E-02 NOT IDENT. PA-234 -2.132E-02 2.450E-01 2.452E-01 FAIL ABUN PA-234M 3.620E+OO 3.544E+OO 3.902E+OO NOT IDENT. NP-237 -2.102E-02 5.476E-02 5.558E-02 NOT IDENT. NP-238 l.OOOE+41 9.873E+40 O.OOOE+OO SHORT HLIF NP-239 -9.015E-03 l.987E-01 l.988E-01 NOT IDENT. PU-239 l.468E+02 2.474E+02 2. 561E+02 NOT IDENT. AM-241 6.535E-03 l .112E-01 l .113E-01 NOT IDENT. CM-243 -7.364E-03 7.518E-02 7.525E-02 NOT IDENT. BK-247 4.298E-02 6.442E-02 6.728E-02 NOT IDENT. CM-247 5. 901E-04 2.674E-02 2.674E-02 NOT IDENT. CF-249 2.225E-02 2.876E-02 3.046E-02 NOT IDENT. CF-251 -9.785E-02 9.487E-02 l.046E-01 NOT IDENT. Page 4554 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 47.0761 87.09 78.9628 136.47 70.7562 45.60 50.7767 87.57 79.0416 140.51 0.0000 46.54 57.7182 88.03 79.1166 143.76 52.8685 49. 72 0.0000 88.34 79.1666 144.24 63.2795 51. 35 64.5970 88.47 79.1877 145.44 75.8605 51. 87 64.6957 89. 96 75.6464 152.43 75.5706 52.39 54.4269 1093.63 75.7501 153.25 0.0000 52.97 49.3262 91.11 0.0000 323.87 51. 5578 53.44 51.9926 92.59 76.0468 156.02 0.0000 54.07 61. 6353 93.35 76.1609 158.56 0.0000 57.36 0.0000 94.56 72.5256 159.00 47.6621 57.53 71. 8754 94.65 72.5384 162.33 57.4525 57.98 67.5750 94.67 72.5413 162.66 0.0000 59.27 87.1854 94.87 61.1113 163.33 59.6598 59.32 87 .1972 97.43 69.0919 165.86 55.5848 59.54 79.9044 98.43 47.1106 176.31 46.5890 60. 96 74.3085 98.44 47.1117 176.60 0.0000 61.17 74.3495 99.53 52.9900 177.52 61.8515 62.93 87.1388 100.11 54.9770 181.07 0.0000 63.29 87.2196 102.03 53.2389 181. 52 53.8003 63.58 87.2842 103.18 63.0526 184.41 50.3434 64.28 87.4403 103.37 58.2230 143.76 50.4241 66.73 73.0171 105.21 49.6564 193.51 55.3230 67.24 70.7119 105.31 49.6654 197.03 58.8850 125.81 82.7868 106.12 57.5407 198.01 58.9521 67.75 81.0008 106.47 60.5048 201.83 58.0945 69.67 84.0932 109.28 48.0590 203.43 61.5586 70.83 92.4873 111. 00 54.1079 205.31 56.8299 72.81 103.2444 111.76 0.0000 210.85 54.1736 72.87 103.2591 114.06 67.2534 215.65 39.7109 74.66 88.7447 116.30 0.0000 222.11 51. 4140 74.82 88.7773 116.74 63.5874 227.09 51.6859 74.97 88.8084 119.76 61. 9134 227.38 55.1484 77 .11 89.2406 121.12 49.0419 228.16 0.0000 78.74 89.5662 121.22 49.0497 228.18 47.1454 79.69 66.6216 121. 78 53.1027 116.74 47.1454 80.12 76.5640 122.06 53.1274 235.69 49.4440 80.19 0.0000 122.92 64.2441 235. 96 46.3666 80.57 76.6397 123.07 64.2598 238.63 40.6813 81. 00 65.5761 265.00 58.2934 238.98 0.0000 81. 07 65.5858 125.81 57.4858 240.99 40.7780 81. 75 69.4007 127.23 58.6270 242.00 40.8191 83.79 74.6838 127.91 57.6788 244.70 42.0991 84.00 69.7357 129.30 54.7630 252.40 0.0000 85.43 79.9388 131. 20 71.2016 252.80 31. 8260 86.55 78.8743 133.02 56.1028 254.15 0.0000 86.79 78.9134 133. 52 58 .1872 256.23 47.3059 86.94 78.9384 136. 00 62.5079 260.90 0.0000 Page 4555 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 34.5720 355.39 0.0000 584.27 20.7120 264.80 34.5764 356.01 32.1663 595.83 0.0000 265.00 33.3910 364.49 0.0000 427.87 23.8652 268.22 38.2754 366.42 0.0000 602.52 0.0000 269.46 32.3319 372. 51 26.0474 604.72 19.4302 270.03 32.3492 37 5 .,05 28.7045 607.14 17.9575. 271.23 38.3818 377.52 24.3986 609.32 17.9766 273.65 0.0000 356.01 30.6357 610.33 17.9854 276.40 30.1277 388.16 18.4374 614.28 18.0205 277.37 41. 0100 388.63 0.0000 618.01 26.0762 277.60 42.2247 391.69 33.4448 620.36 20.0822 278.00 43.4476 264.66 20.3683 621. 93 18. 0872 279.20 45.9101 401.81 22.1573 630.19 0.0000 279.54 36.2567 402.40 23.0526 631. 29 16.1504 279.70 36.2613 404.85 23.9793 633.25 14.1447 280.46 27.8193 410.95 33.8878 634.78 0.0000 283.69 35.1783 413. 71 24.1227 635.95 18.2095 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 29.1577 423.72 0.0000 645.85 16.2617 285.90 0.0000 427.09 32.4478 657.76 18. 3962 287.50 34.0797 427.87 22.9958 657.90 0.0000 290.67 42. 3114 433.94 24.4440 661.66 21. 5007 293.27 0.0000 439.40 20.8952 664.57 0.0000 351. 93 37.5771 453.88 19.2526 666.33 0.0000 295.96 37.6015 463.37 23.0540 666.50 0.0000 879.38 47.5179 468.07 30.5186 667.71 0.0000 299.98 38.1417 473.00 0.0000 677.62 10.3133 300.09 38.1445 475.06 27.8613 685.70 0.0000 300.13 38.1464 476.78 26.9603 695.00 0.0000 301.36 40.6498 477.60 29.7637 696.49 17.6807 302.85 37.0010 482.18 24.2491 696. 51 17.6814 256.23 29.6426 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 19.7685 306.78 29.6990 497.08 25.4020 697.49 22.8916 308.46 33.4583 505.52 25.5251 702.65 18.7720 311. 90 38.5258 507.63 0.0000 706.68 13.5813 316.51 36.1765 511. 00 21.8112 711. 68 14.1345 319.41 0.0000 514.00 21.8479 720.70 0.0000 320.08 0.0000 514.00 21.8479 721. 93 0.0000 321. 04 35.0590 520.40 19.0666 722.78 15.7800 323.87 31. 3736 520.69 0.0000 722.91 17.3594 325.23 30.1516 522.65 0.0000 723. 31 15.7837 328.76 0.0000 527.90 0.0000 724 .19 9.4739 333.37 32.8761 528.26 19 .1496 727.33 13.7030 333.97 32.0486 529.59 20.1224 733.00 14.2641 334.37 33.4085 529.87 0.0000 735.93 9. 5211 338.28 34. 2724 531.02 0.0000 333.97 11. 6445 338.32 34.2732 537.26 0.0000 739.50 0.0000 311. 90 35.6024 546.56 0.0000 747.24 10.6295 340.48 35.6024 552.55 22.3131 748.06 5.3166 340.55 0.0000 563.25 20.4882 752.31 12.7822 344.28 27.5451 569.33 23.4893 753.82 0.0000 345.93 29.7933 946.00 18.5980 756.73 12.8057 351.06 24.7826 569.70 19.5784 756.80 12.8062 351.93 24.7992 583.19 20.7001 884.68 11. 2383 Page 4556 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 17.6736 1274.44 5.8270 1620.50 4.1279 766.42 24.1068 1001.03 7.8788 1621. 92 3.0970 766.84 20.8957 1002.74 15.7665 1678.03 0.0000 772.60 0.0000 1004.73 13.1470 1690.97 5.2386 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 n64. 49 5.3192 778.90 13.9987 1028.54 0.0000 1063.66 5 .1123 783.70 0.0000 1037.84 7.0869 1771. 35 5 .1135 785.37 8.6370 1038.76 0.0000 1791.20 0.0000 792.07 12.9902 631.29 9.7720 1808.65 3.2199 794.95 7.5865 1048.07 0.0000 1810.72 0.0000 795.86 10.8415 1049.04 13.3356 1836.06 4.3167 810.06 13. 0825 1050.41 9.7834 810.29 17. 4453 1063.66 7.1450 344.28 17.4460 1077.00 0.0000 810.76 15.2675 1077.34 12.3005 815.77 0.0000 1085. 8'7 10.7915 1048.07 0.0000 ' 1093.63 12.0190 832 . .01 14.2933 1099.45 11. 7392 834.85 14.8596 1112. 07 11. 7844 835.71 11.5613 1112. 84 14.5068 836.80 0.0000 1115. 54 13.0667 846.75 0.0000 1120.29 10.9043 846.77 14.3737 1120.55 10.9050 856.80 0.0000 1221. 41 10.9080 860.56 15.5597 1129. 67 10.0238 871. 09 17.8516 1131.51 0.0000 873.19 13.3989 1147. 95 0.0000 875.33 0.0000 1173.23 14.7666 879.38 10.0723 1177.95 10.1655 880.51 8.9567 1189.05 14.8340 883.24 10.0862 1204.77 14.8994 884.68 13. 4556 1221.41 14.9688 889.28 8.9854 1231. 02 15.0088 894.76 13.5044 1235.36 0.0000 898.04 11. 2671 1238.28 18.7988 900.72 18.0449 1260.41 0.0000 903.28 16.9324 1271.87 8.5369 911.20 13. 5840 1274.44 8.5430 912.08 13.5884 1274.54 8.5430 923.98 0.0000 1291.59 11. 4426 926.50 6.8289 1298.22 0.0000 929.11 11. 9612 1312 .11 0.0000 937.49 13. 7100 1332.49 5.7828 944.13 0.0000 1362.66 0.0000 946.00 12.6042 1365.19 7.7754 949.00 13.7642 1368.63 0.0000 667.71 0.0000 1384.29 1. 9531 962. 31 10.3704 1408.01 6.8765 964.08 12.1060 1457.56 0.0000 966 .17 0.0000 1460.82 4.9753 911.20 10.3934 1489.16 3.0051 968. 97 10.3934 1505.03 4.0217 983.53 0.0000 1584.12 9.2137 984.45 0.0000 1596.21 0.0000 Page 4557 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:45:58.26 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235071.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM01.CNF;402 Background date : Z-OCT-2016 10:59:55. Sample date 11-DEC-2015 10:25:00 Acquisition date : 3-0CT-2016 06:45:24. Sample ID G405235071 Sample quantity 1.49695E+02 GRAM Detector name : GAMOl Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.34 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 2 2 0 0 0 0 0 0 0 3 3 0 0 0 0 0 0 5 5 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4558 of 5809 Energy 35.40* 63.01* 74.91 77.18* 87. 26 93.35* 109.02 127.83 144.45* 185.91* 210.30 238.68* 241. 72* 295.31* 302.16 323.36 339.39* 351.99* 439.77 485.75 490.62 511. 30* 525.23 565.74* 583.25* 604.89 609.30* 662.51 684.91 727.80 769.50 777.65* 785.41 840.23 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 6 18 91 142 58 36 46 13 45 44 31 260 97 99 28 13 34 209 18 20 18 15 18 37 73 11 129 31 11 24 27 5 15 18 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 43 124 143 119 91 204 109 116 138 112 106 60 69 75 83 45 88 44 26 2 11 38 25 28 9 10 25 15 18 27 33 9 10 5 1. 35 0.92 1. 45 1.12 0.99 1.18 1.12 0.66 4.23 1.19 1. 02 1. 22 1. 80 1.19 0.75 1. 01 1. 08 1. 05 3.21 2.40 2.40 1. 20 0.97 1. 87 1. 01 1. 06 1. 25 4.18 1. 04 1. 95 1. 24 1. 83 3.84 1. 63 71. 50 126. 71 150.50 155.06 175.21 187.38 218.73 256.35 289.57 372.49 421.27 478.02 484 .11 591. 28 604. 96 647.35 679.40 704.61 880.13 972.09 981.82 1023.17 1051.02 1132. 02 1167. 04 1210.31 1219.12 1325.51 1370.31 1456.08 1539.45 1555.74 1571.25 1680.86 67 123 144 144 173 181 214 253 285 368 415 472 472 586 597 643 673 699 873 968 968 1017 1046 1123 1163 1207 1214 1320 1366 1451 1532 1549 1563 1676 9 l.69E-03223.1 9 4. 98E-03119. 5 19 2.52E-02 26.9 19 3.94E-02 15.4 6 1. 62E-02 28. 9 11 9.97E-03 83.6 11 1.28E-02 46.7 10 3.74E-03151.7 13 1.25E-02 56.5 9 1. 23E-02 48. 9 11 8.60E-03 67.1 18 7.23E-02 8.0 18 2.69E-02 23.3 11 2.75E-02 19.9 15 7.83E-03 74.0 8 3.65E-03 93.2 13 9.49E-03 60.0 12 5.81E-02 9.6 13 4.94E-03 63.8 19 5.53E-03 30.2 19 5.03E-03 40.1 12 4.29E-03102.5 11 4. 93E-03 61. 3 16 1.02E-02 37.5 9 2.02E-02 14.5 7 3.16E-03 55.1 12 3.59E-02 11.9 12 8.74E-03 30.3 10 3.07E-03 77.1 11 6.78E-03 46.1 14 7.53E-03 49.8 9 1. 42E-03121. 9 13 4.22E-03 49.6 9 4.86E-03 32.4 Fit 2.72E+OO 1.39E+OO 1.13E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235071 Acquisition date 3-0CT-2016 06:45:24 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 873.82 8 11 0.58 1748.02 1744 9 2.27E-03 81. 3 36 0 904.15* 16 10 0.80 1808.67 1804 11 4.42E-03 44.3 37 2 907.76 13 2 1. 65 181.5. 89 1814 17 3.54E-03 26.1 1. OlE+OO 38 2 911. 34* 63 6 1. 88 1823.03 1814 17 1.76E-02 15.4 39 0 933.57 13 4 0.52 1867.48 1863 8 3.66E-03 37.9 40 0 969.81 45 11 1. 58 1939.93 1932 16 l.26E-02 22.5 41 0 1120.46* 49 4 1. 47 2241.12 2235 14 1.36E-02 16.7 42 0 1284.19 6 3 1. 38 2568.46 2565 6 1. 76E-03 58.0 43 0 1460.65* 264 9 1. 86 2921.21 2915 15 7.33E-02 6.6 44 0 1599.00* 6 3 1. 37 3197.77 3191 9 l.60E-03 68.2 45 0 1660.72 7 0 0.55 3321.14 3318 7 l.94E-03 37.8 46 0 1764.46* 38 0 1. 61 3528.51 3523 10 l.07E-02 16.9 Flag: "*" = Peak area was modified by background subtraction Page 4559 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:46:00 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235071.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID ll-DEC-2015 10:25:00 G405235071 Acquisition date : Sample quantity Samp.J.e geometry Detector geometry: 3-0CT-2016 06:45:24 149.70 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMAl 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4560 of 5809 PB-214 U-235 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 143.76 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 CE-141 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 145.44 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.34 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235071 Acquisition date 3-0CT-2016 06:45:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66*. 9.709E-01 1.233E+Ol l.233E+Ol 13.29 OK CD-109 88.03 3.70* 4.584E+OO 1.421E+OO 2.220E+OO 90. 72 OK TE-125M 109.28 0.27* 5.636E+OO 1.879E+Ol 6.772E+02 93.47 OK SN-126 64.28 9.60 2.269E+OO 5.335E-01 5.335E-01 239.02 OK 86.94 8.90 4.584E+OO 5.909E-01 5.909E-01 90.72 OK 87.57 37.00* 4.584E+OO 1.421E-01 l.421E-01 90.72 OK BA-137M 661. 66 89.90* 1.881E+OO 9.767E-02 9.951E-02 60.65 OK CS-137 661.66 85.10* 1.881E+OO 1.032E-01 1. 051E-01 60.65 OK CE-141 145.44 48.29* 5.863E+OO 7.637E-02 4.284E+Ol 144.09 OK TL-208 277.37 6.60 3.944E+OO Line Not Found Absent 583.19 85.00* 2.090E+OO 2.173E-01 2.173E-01 29.01 OK 860.56 12.50 1.520E+OO Line Not Found Absent BI-211 72.87 1. 23 3.328E+OO Line Not Found Absent 351.06 12.92* 3.216E+OO 5.613E-01 5.613E-01 186.04 OK BI-212 727.33 6.67* 1. 742E+OO 1.092E+OO 1.092E+OO 92.27 OK 785.37 1.10 1.637E+OO 4. 351E+OO 4.351E+OO 99.20 OK 1620.50 1. 47 8.816E-01 Line Not Found Absent PB-212 74.82 10.28 3.531E+OO 1.134E+OO l .134E+OO 77.41 OK 77 .11 17 .10 3.749E+OO 1.410E4-00 1.410E+OO 30.81 OK 238.63 43.60* 4.454E+OO 7.749E-01 7.749E-01 15.95 OK 300.09 3.30 3.690E+OO Line Not Found Absent BI-214 609.32 45.49* 2.015E+OO 7.458E-01 7.460E-01 23.71 OK 1120.29 14.92 1.223E+OO 1.338E+OO 1.338E+OO 33.36 OK 1764.49 15.30 8 .116E-01 1.466E+OO 1.467E+OO 33.76 OK PB-214 74.82 5.80 3.522E+OO Line Not Found <<INT Reject 77 .11 9.70 3.749E+OO 2.486E+OO 2.487E+OO 30.81 OK 87.09 3.41 4.572E+OO Line Not Found <<INT Reject 242.00 7.25 4.406E+OO Line Not Found <<INT Reject 295.22 18.42 3.740E+OO 8.162E-01 8.165E-01 39.79 OK 351. 93 35.60* 3.216E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.015E+OO 7.458E-01 7.460E-01 23.71 OK 1120.29 14.92 1.223E+OO 1.338E+OO 1.338E+OO 33.36 OK 1764.49 15.30 8 .116E-01 1.466E+OO 1.467E+OO 33.76 OK RA-224 240.99 4.10* 4.410E+OO 1.654E+OO 1.654E+OO 93.84 OK RA-226 609.32 45.49* 2.015E+OO 7.458E-01 7.460E-01 23.71 OK 1120.29 14.92 1.223E+OO 1.338E+OO 1. 338E+OO 33.36 OK 1764.49 15.30 8 .116E-01 1.466E+OO 1.467E+OO 33. 76 OK AC-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11.27 3.319E+OO 5 .115E-01 5 .115E-01 119. 92 OK 794.95 4.25 1.621E+OO Line Not Found Absent 835.71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* 1. 451E+OO 8.606E-01 8.606E-01 30.88 OK 968.97 15.80 1.379E+OO 1.052E+OO 1.052E+OO 44. 96 OK RA-228 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.319E+OO 5 .115E-01 5 .115E-01 119. 92 OK 794.95 4.25 1. 621E+OO Line Not Found Absent 835.71 1. 61 1.557E+OO Line Not Found Absent 911. 20 25.80* 1.451E+OO 8.606E-01 8.606E-01 30.88 OK 968. 97 15.80 1.379E+OO 1.052E+OO 1.052E+OO 44. 96 OK Page 4561 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235071 Acquisition date 3-0CT-2016 06:45:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-228 74.82 10.28 ] . 531E+OO 1. 134E+00 1.134E+OO 77.41 ,OK 77 .11 17.10 3.749E+OO 1. 410E+00 1.410E+OO 30.81 OK 238.63 43.60* 4.454E+OO 7.749E-01 7.749E-01 15.95 OK 300.09 3.30 3.690E+OO Line Not Found Absent TH-230 609.32 45.49* 2.015E+OO 7.458E-01 7.458E-01 23.71 OK 1120.29 14.92 1. 223E+OO 1.338E+OO 1.338E+OO 33.36 OK 1764.49 15.30 8 .116E-01 1.466E+OO 1. 466E+OO 33.76 OK PA-231 283.69 1. 70 3.870E+OO Line Not Found Absent 301. 36 5.35* 3.668E+OO 8.130E-01 8.130E-01 147.90 OK TH-232 105.21 1.10 5.519E+OO Line Not Found Absent 338.32 11. 27 3.319E+OO 5 .115E-01 5 .115E-01 119. 92 OK 835.71 1. 61 1.557E+OO Line Not Found Absent 911.20 25.80* l.451E+00 8.606E-01 8.606E-01 30.88 OK 968. 97 15.80 1. 379E+OO 1.052E+OO l.052E+00 44.96 OK TH-234 63.29 3.70* 2.269E+OO 1.384E+OO 1. 384E+OO 239.02 OK 92.59 4.23 4.978E+00 l.070E+00 1.070E+OO 167.26 OK U-234 609.32 45.49* 2.015E+OO 7.458E-01 7.458E-01 23.71 OK 1120.29 14.92 1.223E+OO 1.338E+OO 1.338E+OO 33.36 OK 1764.49 15.30 8 .116E-01 l.466E+OO 1.466E+OO 33.76 OK U-235 89. 96 3.47 4.769E+OO Line Not Found Absent 93.35 5.60 4.978E+OO 8.079E-01 8.079E-01 167.26 OK 143.76 10. 96* 5.868E+OO Line Not Found <<INT Reject 163.33 5.08 5.647E+00 Line Not Found Absent 185. 72 57.20 5.294E+OO 8.622E-02 8.622E-02 97.79 OK 205.31 5.01 4.973E+OO Line Not Found Absent U-238 63.29 3.70* 2.269E+OO l.384E+00 1.384E+OO 239.02 OK 92.59 4.23 4.978E+OO 1.070E+OO l.070E+00 167.26 OK AM-243 43.53 5.90 3.822E-01 Line Not Found Absent 74.66 67.20* 3.531E+OO 1. 735E-01 1. 735E-01 77.41 OK ANH-511 511. 00 100.00* 2.333E+OO 3.569E-02 3.569E-02 205.07 OK Flag: "*" = Keyline Page 4562 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:46:02.22 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235071.CNF;l *
  • Acquisition date 3-0CT-2016 06:45:24 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *
  • Sample date 11-DEC-2015 10:25:00 Analyst initials: MXRl *
  • Sample ID G405235071 Sample Quantity 1.4970E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 * *Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9 * ******************************************************************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.233E+Ol 1.605E+OO 6.186E-01 CD-109 2.220E+OO 1. 974E+OO 2.628E+OO TE-125M 6.772E+02 6.203E+02 5.226E+02 SN-126 1.421E-01 1.264E-01 1.548E-01 BA-137M 9. 951E-02 5.915E-02 5.730E-02 CS-137 1. 051E-01 6.249E-02 6.053E-02 CE-141 4.284E+Ol 6.049E+Ol 4. 372E+Ol TL-208 2.173E-01 6.177E-02 5.326E-02 BI-211 5.613E-01 1.023E+OO 2.816E-01 BI-212 1. 092E+OO 9.873E-01 9.940E-01 PB-212 7.749E-01 1. 211E-01 9.289E-02 BI-214 7.460E-01 1. 733E-01 1.074E-01 PB-214 1.020E+OO l.915E-01 3.343E-01 RN-222 7.460E-01 1.733E-01 1.074E-01 RA-224 1.654E+OO 1.521E+OO 9.958E-01 RA-226 7.460E-01 1.733E-01 l.074E-01 AC-228 8.606E-01 2.605E-01 2.202E-01 RA-228 8.606E-01 2.605E-01 2.202E-01 TH-228 7.749E-01 1. 211E-01 9.289E-02 TH-230 7.458E-01 1.733E-01 1.073E-01 PA-231 8 .130E-01 1.178E+OO 8.461E-01 TH-232 8.606E-01 2.605E-01 2.202E-01 TH-234 1.384E+OO 3.242E+OO 2.763E+OO U-234 7.458E-Ol 1.733E-01 1.073E-01 U-235 4.227E-01 4.679E-01 3.983E-01 U-238 1.384E+OO 3.242E+OO 2.763E+OO AM-243 1.735E-01 1.316E-01 1.084E-01 ANH-511 3.569E-02 7.172E-02 6.354E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1.96-sigma) (pCi/GRAM BE-7 1.055E+OO l.101E+Ol 2.207E+Ol NOT IDENT. NA-22 -3.103E-03 3. 451E-02 7.415E-02 NOT IDENT. Page 4563 of 5809 NA-24 0.000E+OO 1.960E+41 O.OOOE+OO SHORT HLIF AL-26 -8.SOOE-03 3 .113E-02 6.419E-02 NOT IDENT. SC-46 -2.686E-01 4.271E-01 7.270E-01 FAIL ABUN V-48 O.OOOE+OO 1.480E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 4.560E+02 O.OOOE+OO SHORT HLIF MN-54 7.563E-03 6.846E-02 l.291E-01 NOT IDENT. C0-56 4.086E-02 4.253E-01 8.568E-01 NOT IDENT. MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 -6.152E-02 4.473E-02 8.063E-02 NOT IDENT. C0-58 2.084E-01 4.987E-01 l.077E+OO NOT IDENT. FE-59 8. 911E-01 4. 7 66E+OO 1.029E+Ol NOT IDENT. C0-60 2.858E-02 3.633E-02 8.904E-02 NOT IDENT. ZN-65 4.636E-02 l.503E-01 2. 966E-01 NOT IDENT. GE-68 3.024E-01 1. 895E+OO 3.986E+OO NOT IDENT. AS-73 -1.825E-01 1.195E+Ol 2.243E+Ol NOT IDENT. AS-74 O.OOOE+OO 5.320E+03 O.OOOE+OO SHORT HLIF SE-75 2.123E-01 1.927E-01 4.184E-01 NOT IDENT. BR-77 O.OOOE+OO 9 .131E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 8.478E+02 O.OOOE+OO SHORT HLIF RB-83 -3.731E-01 7.278E-01 1.146E+OO NOT IDENT. KR-85 -2.479E-02 7.976E+OO 1.382E+Ol NOT IDENT. SR-85 -2.860E-03 8.167E-01 1.415E+OO NOT IDENT. RB-86 O.OOOE+OO 2.058E+04 O.OOOE+OO SHORT HLIF Y-88 2. 731E-03 l.724E-01 4.150E-01 NOT IDENT. Y-91 9.958E+Ol 5.534E+02 l.153E+03 NOT IDENT. NB-94 -8.420E-03 3.496E-02 6.472E-02 NOT IDENT. NB-95 3.359E-01 1.000E+OO 1.823E+OO NOT IDENT. NB-95M 6.256E-01 2.328E+OO 4.241E+OO NOT IDENT. ZR-95 5.072E-02 1.414E+OO 2.764E+OO NOT IDENT. NB-97 O.OOOE+OO l.321E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 7.564E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.228E+41 O.OOOE+OO SHORT HLIF RH-101 2.427E-02 7.218E-02 6.154E-02 FAIL ABUN RH-102 -3.131E-03 5.615E-02 1.098E-01 NOT IDENT. RU-103 3.026E+OO 5.038E+OO 1.080E+Ol FAIL ABUN RH-106 1.462E-01 5 .131E-01 1.043E+OO NOT IDENT. RU-106 1.462E-01 5.131E-01 l.043E+00 NOT IDENT. AG-108M 1.838E-02 2.489E-02 5. llOE-02 NOT IDENT. AG-llOM 2.525E-02 l.OOlE-01 2.053E-01 NOT IDENT. SN-113 -1.442E-01 2.123E-01 3.821E-01 NOT IDENT. CD-115 O.OOOE+OO 1.197E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 8.069E+04 0.000E+OO SHORT HLIF TE-123M 7.455E-02 l.267E-01 2.617E-01 NOT IDENT. SB-124 2.305E+OO 2. 541E+OO 6.327E+OO NOT IDENT. SB-125 -3.577E-02 l.064E-01 l.993E-01 NOT IDENT. I-126 O.OOOE+OO 8.379E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.834E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 2 .116E+22 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.505E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.054E+26 O.OOOE+OO SHORT HLIF BA-133 -1.183E-04 3.892E-02 6. 941E-02 FAIL ABUN I-133 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-134 4. 872E-02 4.956E-02 1.115E-01 FAIL ABUN CS-135 -3 .115E-02 l.465E-01 2.807E-01 NOT IDENT. I-135 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.225E+05 O.OOOE+OO SHORT HLIF CE-139 3. 413E-02 1.036E-01 2.106E-01 NOT IDENT. BA-140 O.OOOE+OO 9.357E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 4.300E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -6.014E-03 3.752E-01 7.145E-01 NOT IDENT. PM-144 8.923E-03 5.285E-02 1.062E-01 NOT IDENT. PR-144 7.568E-01 4.580E+OO 9.200E+OO NOT IDENT. PM-146 3.942E-02 3.957E-02 8.854E-02 NOT IDENT. ND-147 O.OOOE+OO 2.287E+07 O.OOOE+OO SHORT HLIF PM-147 -l.250E+03 7.655E+02 l.346E+03 NOT IDENT. PM-149 O.OOOE+OO 1.676E+40 0.000E+OO SHORT HLIF EU-150 l.220E-02 2.624E-02 4.941E-02 FAIL ABUN EU-152 -3.946E-03 9.415E-02 l.659E-01 FAIL ABUN GD-153 9.993E-02 2.253E-01 3.930E-01 NOT IDENT. EU-154 -l.594E-02 8.942E-02 l.864E-01 FAIL ABUN EU-155 5.562E-02 l.183E-01 2.102E-01 FAIL ABUN TB-160 5.274E-01 1.830E+OO 3.774E+OO FAIL ABUN H0-166M 4.663E-03 5 .113E-02 l.028E-01 FAIL ABUN TM-171 -4.573E+OO 2.976E+Ol 5.521E+Ol NOT IDENT. HF-172 -3.366E-02 2.528E-01 4.506E-01 FAIL ABUN Page 4564 of 5809 LU-172 3.434E-02 7.336E-02 1. 579E-01 FAIL ABUN LU-176 l.472E-02 2.645E-02 5.005E-02 FAIL ABUN HF-181 -1.367E+00 3.447E+OO 5. 671E+OO NOT IDENT. TA-182 2.346E-01 9.147E-01 1.943E+OO FAIL ABUN RE-183 9.287E-02 3.552E+OO 6.700E+OO NOT IDENT. RE-184 4.869E+Ol 4.227E+Ol 7.180E+Ol FAIL ABUN W-188 1.165E+02 l.062E+02 2.162E+02 FAIL ABUN IR-192 -9.704E-02 4.092E-Ol 7.881E-01 FAIL ABUN HG-203 -1.953E-01 2.315E+OO 4.496E+OO NOT IDENT. BI-207 4.516E-02 5.800.E-02 1.241E-01 FAIL ABUN PB-210 -2.691E+OO 4.744E+OO 8.679E+OO NOT IDENT. PB-211 -l.540E-01 5.372E-01 l.032E+OO NOT IDENT. RN-219 1.894E-02 3.456E-01 6.876E-01 NOT IDENT. RA-223 5.353E-01 9.780E-01 l.212E+OO FAIL ABUN AC-227 6.872E-02 2.122E-01 4.315E-01 NOT IDENT. TH-227 6.872E-02 2.122E-01 4.315E-01 NOT IDENT. TH-229 l.453E-01 4.659E-01 9.377E-01 FAIL ABUN TH-231 5.353E-01 9.780E-01 1.212E+OO FAIL ABUN PA-233 -4.974E-03 5.439E-02 l.064E-01 FAIL ABUN PA-234 9.748E-02 2.745E-01 5.737E-01 FAIL ABUN PA-234M 3.856E+OO 5.028E+OO 1.109E+Ol NOT IDENT. NP-237 -4.974E-03 5.439E-02 l.064E-01 FAIL ABUN NP-238 O.OOOE+OO 1.657E+41 O.OOOE+OO SHORT HLIF NP-239 -5.854E-02 2.836E-01 5.027E-01 NOT IDENT. PU-239 2.205E+02 6.558E+02 6.224E+02 FAIL ABUN AM-241 4.229E-02 1.814E-01 3.216E-01 NOT IDENT. CM-243 -3.215E-02 1.076E-01 l.909E-01 NOT IDENT. BK-247 5.405E-02 6.806E-02 1. 441E-01 NOT IDENT. CM-247 5.505E-03 3.091E-02 6.265E-02 NOT IDENT. CF-249 3.092E-02 3.622E-02 7.794E-02 NOT IDENT. CF-251 1.532E-02 1.182E-01 2.351E-01 NOT IDENT. Page 4565 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:45:59.00 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1-460.82 254 10.66* 9.709E-01 1.233E+Ol 1.233E+Ol 13.29 CD-109 88.03 74 3.70* 4.584E+OO 2.173E+OO 3.395E+OO 57.70 TE-125M 109.28 57 0.27* 5.636E+OO 1.879E+Ol 6. 772E+02 93.47 SN-126 64.28 23 9.60 2.269E+OO 5.335E-01 5.335E-01 239.02 86.94 74 8.90 4.584E+OO 9.036E-01 9.036E-01 57.70 87.57 74 37.00* 4.584E+OO 2.173E-01 2.173E-01 57.70 BA-137M 661. 66 33 89.90* 1. 881E+OO 9. 7 67E-02 9.951E-02 60.65 CS-137 661. 66 33 85.10* l.881E+OO l.032E-01 1.051E-01 60.65 CE-14l 145.44 54 48.29* 5.863E+OO 9.594E-02 5 .. 381E+Ol 112. 96 TL-208 277.37 ------6.60 3.944E+00 ------Line Not Found ------583.19 77 85.00* 2.090E+OO 2.173E-01 2.173E-01 29.01 860.56 ------12.50 1. 520E+OO ------Line Not Found ------BI-211 72. 87 ------1. 23 3.328E+OO ------Line Not Found ------351.06 233 12.92* 3.216E+OO 2.810E+OO 2.810E+00 19.15 BI-212 727. 33 25 6.67* 1. 742E+00 1.092E+OO 1. 092E+00 92.27 785.37 16 1.10 1. 637E+OO 4.351E+00 4.351E+OO 99.20 1620.50 ------1. 47 8.816E-01 ------Line Not Found ------PB-212 74.82 115 10.28 3. 531E+OO 1.594E+OO l.594E+00 53.84 77 .11 180 17.10 3.749E+OO 1.410E+OO l.410E+OO 30.81 238.63 300 43.60* 4.454E+OO 7.749E-01 7.749E-01 15.95 300.09 ------3.30 3.690E+OO ------Line Not Found ------BI-214 609.32 136 45.49* 2.015E+OO 7.458E-01 7.460E-01 23.71 1120.29 49 14.92 l.223E+00 l.338E+OO l.338E+OO 33.36 1764.49 36 15.30 8 .116E-01 l.466E+OO l.467E+OO 33.76 PB-214 74.82 115 5.80 3. 531E+OO 2.826E+OO 2.827E+OO 53.84 77 .11 180 9.70 3.749E+OO 2.486E+OO 2.487E+OO 30.81 87.09 74 3.41 4.584E+OO 2.358E+OO 2.359E+OO 57.70 242.00 112 7.25 4.410E+OO 1. 752E+OO 1. 752E+OO 46.56 295.22 112 18.42 3.740E+OO 8.162E-01 8.165E-01 39.79 351. 93 233 35.60* 3.216E+OO l.020E+OO 1. 020E+OO 19.15 RN-222 609.32 136 45.49* 2.015E+OO 7.458E-01 7.460E-01 23.71 1120.29 49 14.92 1.223E+OO l.338E+OO l.338E+OO 33.36 1764.49 36 15.30 8.116E-01 l.466E+OO l.467E+OO 33.76 RA-224 240.99 112 4.10* 4.410E+OO 3.097E+OO 3.097E+00 46.56 RA-226 609.32 136 45.49* 2.015E+OO 7.458E-01 7.460E-01 23.71 1120.29 49 14.92 1.223E+OO l.338E+OO l.338E+OO 33.36 1764.49 36 15.30 8 .116E-01 l.466E+00 l.467E+OO 33.76 AC-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 38 11. 27 3.319E+OO 5 .115E-01 5 .115E-01 119. 92 794.95 ------4.25 1. 621E+OO ------Line Not Found ------835. 71 ------1. 61 l.557E+OO ------Line Not Found ------911.20 64 25.80* 1. 451E+OO 8.606E-01 8.606E-01 30.88 968.97 46 15.80 1. 379E+OO l.052E+OO l.052E+OO 44. 96 RA-228 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 38 11. 27 3.319E+OO 5 .115E-01 5.115E-01 119. 92 794.95 ------4.25 1. 621E+OO ------Line Not Found ------835. 71 ------1. 61 l.557E+OO ------Line Not Found ------Page 4566 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235071 Acquisition date 3-0CT-2016 06:45:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911. 20 . 64 25.80* 1. 451E+OO 8.606E-01 8.606E-01 30.88 968.97 46 15.80 1. 37 9E+OO 1.052E+OO 1.052E+OO 44. 96 TH-228 74.82 115 10.28 3.531E+OO 1.594E+OO l.594E+00 53.84 77 .11 180 17.10 3.749E+OO l.410E+OO 1.410E+OO 30.81 238.63 300 43.60* 4.454E+OO 7.749E-01 7.749E-01 15.95 300.09 ------3.30 3.690E+OO ------Line Not Found ------TH-230 609.32 136 45.49* 2.015E+OO 7.458E-01 7.458E-01 23. 71 1120.29 49 14.92 1.223E+OO 1.338E+OO 1.338E+OO 33.36 1764.49 36 15.30 8 .116E-01 1.466E+OO 1.466E+OO 33.76 PA-231 283.69 ------1. 70 3.870E+OO ------Line Not Found ------301.36 32 5.35* 3.668E+OO 8.130E-01 8.130E-01 147.90 TH-232 105.21 ------1.10 5.519E+OO ------Line Not Found ------338.32 38 11.27 3.319E+OO 5 .115E-01 5 .115E-01 119. 92 835.71 ------1. 61 1.557E+OO ------Line Not Found ------911. 20 64 25.80* 1.451E+OO 8.606E-01 8.606E-01 30.88 968. 97 46 15.80 1.379E+OO 1. 052E+OO 1.052E+OO 44.96 TH-234 63.29 23 3.70* 2.269E+OO 1.384E+OO 1.384E+OO 239.02 92.59 45 4.23 4.978E+OO 1.070E+OO 1.070E+OO 167.26 U-234 609.32 136 45.49* 2'. 015E+OO 7.458E-01 7.458E-01 23.71 1120.29 49 14.92 l.223E+OO 1.338E+OO 1.338E+OO 33.36 1764.49 36 15.30 8 .116E-01 1.466E+OO 1.466E+OO 33.76 U-235 89. 96 ------3.47 4.769E+OO ------Line Not Found ------93.35 45 5.60 4.978E+OO 8.079E-01 8.079E-01 167.26 143.76 54 10. 96* 5.863E+OO 4.227E-01 4.227E-01 112. 96 163.33 ------5.08 5.647E+OO ------Line Not Found ------185.72 52 57.20 5.294E+OO 8.622E-02 8.622E-02 97.79 205.31 ------5.01 4.973E+OO ------Line Not Found ------U-238 63.29 23 3.70* 2.269E+OO l.384E+OO l.384E+OO 239.02 92.59 45 4.23 4.978E+OO l.070E+OO l.070E+OO 167.26 AM-243 43.53 ------5.90 3.822E-01 ------Line Not Found ------74.66 115 67.20* 3. 531E+OO 2.439E-01 2.439E-01 53.84 ANH-511 511. 00 17 100.00* 2.333E+OO 3.569E-02 3.569E-02 205.07 Flag: "*" Key line Page 4567 of 5809 Page : 3 Summary of Nuclide Activity Sample ID : G405235071 Acquisition date 3-0CT-2016 06:45:24 Total number of lines in spectrum 46 Number of unidentified lines 11 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 CE-141 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 461. 40D 57.40D 2.30E+05Y 30.08Y 30.08Y 32.51D 1. 41E+10Y 7.04E+08Y l.41E+l0Y 1. 41E+l0Y 1600.00Y 1600. ODY 1600. DOY 1. 41E+l0Y 1600. DOY 1. 41E+l0Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 56 36.0 1. 00 1. 02 1. 02 561. 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. 233E+Ol 2.173E+OO 1.879E+Ol 2.173E-01 9.767E-02 l.032E-01 9.594E-02 2.173E-01 2.810E+OO 1.092E+OO 7.749E-01 7.458E-01 1.020E+OO 7.458E-01 3.097E+OO 7.458E-01 8.606E-01 8.606E-01 7.749E-01 7.458E-01 8.130E-01 8.606E-01 1.384E+OO 7.458E-01 4.227E-01 1.384E+OO 2.439E-01 3.569E-02 5.418E+Ol 5.418E+Ol Decay Corr pCi/GRAM 1.233E+Ol 3.395E+OO 6.772E+02 2.173E-01 9.951E-02 1. 051E-01 5. 381E+Ol 2.173E-01 2.810E+00 1. 092E+OO 7.749E-01 7.460E-01 1. 020E+OO 7.460E-01 3.097E+OO 7.460E-01 8.606E-01 8.606E-01 7.749E-01 7.458E-01 8.130E-01 8.606E-01 1.384E+OO 7.458E-01 4.227E-01 1.384E+OO 2.439E-01 3.569E-02 7.676E+02 7.676E+02 76.09% Decay Corr 2-Sigma Error 0.164E+Ol 1.959E+OO 6.330E+02 1.254E-01 6.036E-02 0.638E-01 6.079E+Ol 0.630E-01 0.538E+OO 1.007E+OO 1.236E-01 l.769E-01 0.195E+OO 1.769E-01 1.442E+OO l.769E-01 2.658E-01 2.658E-01 1. 236E-01 1. 7 68E-01 12.03E-01 2.658E-01 3.308E+OO 1. 768E-01 4.775E-01 3.308E+OO 1. 313E-01 7.318E-02 "M" Manually accepted 2-Sigma %Error 13.29 57.70 93.47 57.70 60.65 60.65 112. 96 29.01 19.15 92.27 15.95 23.71 19.15 23. 71 46.56 23.71 30.88 30.88 15.95 '23.71 147.90 30.88 239.02 23.71 112. 96 239.02 53.84 205.07 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4568 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235071 Acquisition date : 3-0CT-2016 06:45:24 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 35.40 8 58 1. 35 71. 50 67 9 1. 69E-03 **** 4.12E-02 0 127.83 16 141 0.66 256.35 253 10 3.74E-03 **** 5. 91E+OO T 0 210.30 36 124 1. 02 421.27 415 11 8.60E-03 **** 4.89E+OO T 0 .. 323.36 15 -50 1. 01 647.35 64.3 8 3.65E-03 **** 3.46E+OO T 0 439.77 19 29 3.21 880.13 873 13 4.94E-03 **** 2.65E+OO T 5 485.75 21 3 2.40 972.09 968 19 5.53E-03 60.3 2.44E+OO T 5 490.62 20 12 2.40 981.82 968 19 5.03E-03 80.2 2.42E+OO 0 525.23 19 27 0.97 1051. 02 1046 11 4.93E-03 **** 2.28E+OO 0 565.74 39 30 1. 87 1132. 02 1123 16 l.02E-02 75.1 2.14E+OO 0 604.89 12 10 1. 06 1210.31 1207 7 3.16E-03 **** 2.03E+OO T 0 684.91 12 19 1. 04 1370.31 1366 10 3.07E-03 **** 1.83E+OO T 0 769.50 28 34 1.24 1539.45 1532 14 7.53E-03 99.7 1.66E+OO 0 777.65 5 9 1. 83 1555.74 1549 9 1.42E-03 **** 1. 65E+OO T 0 840.23 18 5 1. 63 1680.86 1676 9 4.86E-03 64.8 1.55E+OO 0 873.82 8 11 0.58 1748.02 1744 9 2.27E-03 **** 1.50E+OO T 0 904.15 16 10 0.80 1808.67 1804 11 4.42E-03 88.6 l.46E+OO T 2 907.76 13 2 1. 65 1815.89 1814 17 3.54E-03 52.1 1.46E+OO 0 933.57 13 4 0.52 1867.48 1863 8 3.66E-03 75.9 l.42E+OO 0 1284.19 6 3 1. 38 2568.46 2565 6 1. 7 6E-03 **** 1.09E+OO 0 1599.00 6 3 1. 37 3197.77 3191 9 1.60E-03 **** 8.93E-01 0 1660. 72 7 0 0.55 3321.14 3318 7 1.94E-03 75.6 8.61E-01 Flags: "T" = Tentatively associated Page 4569 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:46:14.79 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235071.CNF;l *
  • Acquisition date 3-0CT-2016 06:45:24 Sensitivity 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *
  • Sample date 11-DEC-2015 10:25:00 Nuclide Library : SOLID *
  • Sample ID G405235071 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4970E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 TE-125M SN-126 BA-137M CS-137 CE-141 TL-208 BI-211 BI-212 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.434E-01 1.248E+OO 2.442E+02 7.316E-02 2.446E-02 2.584E-02 2.044E+Ol 2.270E-02 1.238E-01 4.374E-01 4.279E-02 4.609E-02 1. 611E-01 4.609E-02 4.587E-01 4.609E-02 9.165E-02 9.165E-02 4.279E-02 4.607E-02 3.871E-01 9.165E-02 1.296E+00 4.607E-02 1. 88bE-01 1.296E+00 5. lllE-02 2.878E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4570 of 5809 Le (pCi/GRAM 9.736E+OO 2.931E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 'ND-14 7 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 Page 4571 of 5809 2.350E-02 3.091E-01 O.OOOE+OO 0.000E+OO 5. 596E-02 3.639E-01 O.OOOE+OO 3. 725E-02 4.591E-01 4.149E+OO 3.730E-02 1. 226E-01 l.632E+OO 1.047E+Ol O.OOOE+OO 1.929E-01 O.OOOE+OO O.OOOE+OO 4. 996E-01 6.181E+OO 6.328E-01 O.OOOE+OO l.470E-01 4.993E+02 2.848E-02 8. 081E-01 1. 962E+OO l.194E+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 2.864E-02 4.750E-02 4.793E+OO 4.602E-01 4.602E-01 2.266E-02 8.810E-02 l.690E-01 0.000E+OO 0.000E+OO 1.224E-01 2.649E+OO 8. 901E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO O.OOOE+OO 3.094E-02 O.OOOE+OO 4.918E-02 1.294E-01 O.OOOE+OO O.OOOE+OO 9.819E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.347E-01 4.629E-02 4.009E+OO 3. 964E-02 O.OOOE+OO 6.195E+02 O.OOOE+OO 2.249E-02 7. 451E-02 1.852E-01 7.414E-02 9.810E-02 1.622E+OO 4.417E-02 2.575E+Ol 2.107E-01 6.714E-02 NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT,IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 PB-211 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4572 of 5809 2.294E-02 2.380E+OO 8.367E-01 3 .114E+OO 3.176E+Ol 9.924E+Ol 3.547E-Ol 2.064E+OO 5.473E-02 4.044E+OO 4.505E-01 3.067E-01 5.548E-01 1. 980E-01 l.980E-01 4.376E-01 5.548E-01 4.808E-02 2.460E-01 4.935E+OO 4.808E-02 O.OOOE+OO 2.357E-01 2.919E+02 1.500E-01 8.897E-02 6.629E-02 2. 791E-02 3.536E-02 1.099E-01 FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IOENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:46:20.33 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA *
  • *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235071.CNF;l *
  • Acquisition date 3-0CT-2016 06:45:24 Sensitivity : 3.000 *
  • Detector ID GAMOl Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.34 Half life ratio : ***** *
  • Sample date ll-DEC-2015 10:25:00 Nuclide Library : SOLID *
  • Sample ID G405235071 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4970E+02 GRAM *
  • Quantity Err(%) : 1.3360E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 20-JUL-2016 07:03:55 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMOl CAN.CNF;9 * ***********************************************x*****x************************* Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) K-40 1.233E+Ol 1. 730E+OO 1. 730E+OO CD-109 2.220E+OO 1.987E+OO 1.987E+OO TE-125M 6.772E+02 6.216E+02 6.216E+02 SN-126 1.42lE-01 1. 270E-01 l.270E-01 BA-137M 9. 951E-02 5.930E-02 5.930E-02 CS-137 1. 051E-01 6.265E-02 6.265E-02 CE-141 4.284E+Ol 6.052E+Ol 6.052E+Ol TL-208 2.173E-01 6.246E-02 6.246E-02 BI-211 5.613E-01 1.033E+OO 1.033E+OO BI-212 1.092E+OO 9.889E-01 9.889E-01 PB-212 7.749E-01 l.279E-01 1.279E-01 BI-214 7.460E-01 1. 7 63E-01 1. 763E-01 PB-214 1. 020E+OO 1. 962E-01 1. 962E-01 RN-222 7.460E-01 1. 763E-01 1. 763E-01 RA-224 1.654E+OO 1.527E+OO 1.527E+OO RA-226 7.460E-01 1. 763E-01 1. 763E-01 AC-228 8.606E-01 2.642E-01 2.642E-01 RA-228 8.606E-01 2.642E-01 2.642E-01 TH-228 7.749E-01 1. 27 9E-01 1.279E-01 TH-230 7.458E-01 1. 762E-01 1. 762E-01 PA-231 8 .130E-Ol 1.191E+OO 1.191E+OO TH-232 8.606E-Ol 2.642E-01 2.642E-01 TH-234 1.384E+OO 3.257E+OO 3.257E+OO U-234 7.458E-Ol l.762E-01 1.762E-01 U-235 4.227E-Ol 4.684E-01 4.684E-Ol U-238 1.384E+OO 3.257E+OO 3.257E+OO AM-243 1.735E-Ol l.323E-01 l.323E-01 ANH-511 3.569E-02 7.173E-02 7.173E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 1.055E+OO 1. lOlE+Ol 1.102E+Ol NOT IDENT. NA-22 -3.103E-03 3.451E-02 3.454E-02 NOT IDENT. Page 4573 of 5809 NA-24 -1.000E+41 2.452E+41 O.OOOE+OO SHORT HLIF AL-26 -8.500E-03 3 .113E-02 3.137E-02 NOT IDENT. SC-46 -2.686E-01 4. 272E-01 4.440E-01 FAIL ABUN V-48 -5.962E+03 1.480E+04 l.504E+04 SHORT HLIF CR-51 -2.089E+02 4. 561E+02 4.657E+02 SHORT HLIF MN-54 7.563E-03 6.846E-02 6.854E-02 NOT IDENT. C0-56 4.086E-02 4.253E-01 4.257E-01 NOT IDENT. MN-56 1.000E+41 l.090E+42 O.OOOE+OO SHORT HLIF C0-57 -6.152E-02 4.482E-02 5.271E-02 NOT IDENT . C0-58 .2.084E-01 4.987E-01 5.075E-01 NOT IDENT. FE-59 8. 911E-01 4.766E+OO 4.783E+OO NOT IDENT. C0-60 2.858E-02 3.634E-02 3.856E-02 NOT IDENT. ZN-65 4.636E-02 1.503E-01 1. 517E-01 NOT IDENT. GE-68 3.024E-01 1.895E+OO 1.900E+OO NOT IDENT. AS-73 -l.825E-01 1.195E+Ol l.195E+Ol NOT IDENT. AS-74 -4.557E+03 5.333E+03 5. 715E+03 SHORT HLIF SE-75 2.123E-01 1.930E-01 2.154E-01 NOT IDENT. BR-77 5.843E+37 5.007E+38 O.OOOE+OO SHORT HLIF SR-82 3.548E+02 8.479E+02 8.629E+02 SHORT HLIF RB-83 -3.731E-01 7.296E-01 7.488E-01 NOT IDENT. KR-85 -2.479E-02 7.976E+OO 7.976E+OO NOT IDENT. SR-85 -2.860E-03 8.167E-01 8.167E-01 NOT IDENT. RB-86 3.283E+03 2.058E+04 2.063E+04 SHORT HLIF Y-88 2.731E-03 1. 724E-01 1. 724E-01 NOT IDENT. Y-91 9.958E+Ol 5.534E+02 5.552E+02 NOT IDENT. NB-94 -8.420E-03 3.496E-02 3.517E-02 NOT IDENT. NB-95 3.359E-01 1.000E+OO 1.012E+OO NOT IDENT. NB-95M 6.256E-01 2.328E+OO 2.345E+OO NOT IDENT. ZR-95 5. 072E-02 l.414E+OO 1.414E+OO NOT IDENT. NB-97 1.000E+41 l.321E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 4.513E+41 O.OOOE+OO SHORT HLIF M0-99 -1.176E+31 7.564E+31 O.OOOE+OO SHORT HLIF TC-99M l.OOOE+41 1.232E+41 0.000E+OO SHORT HLIF RH-101 2.427E-02 7.232E-02 7.314E-02 FAIL ABUN RH-102 -3 .131E-03 5.615E-02 5.617E-02 NOT IDENT. RU-103 3.026E+OO 5.040E+00 5. 221E+OO FAIL ABUN RH-106 1. 462E-01 5.132E-01 5.174E-01 NOT IDENT. RU-106 1. 462E-01 5.132E-01 5.174E-01 NOT IDENT. AG-108M l.838E-02 2.490E-02 2.625E-02 NOT IDENT. AG-llOM 2.525E-02 l.OOlE-01 1.007E-01 NOT IDENT. SN-113 -l.442E-01 2.124E-01 2. 221E-01 NOT IDENT. CD-115 3.212E+38 l.198E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 6.853E+04 8 .110E+04 8.678E+04 SHORT HLIF TE-123M 7.455E-02 1. 268E-01 l.311E-01 NOT IDENT. SB-124 2.305E+00 2.544E+OO 2.748E+OO NOT IDENT. SB-125 -3.577E-02 1.064E-01 1.076E-01 NOT IDENT. I-126 -7. 351E+05 8.438E+05 9.065E+05 SHORT HLIF SB-126 -l.052E+06 l.003E+06 l.109E+06 SHORT HLIF SB-127 l.401E+22 2.849E+22 O.OOOE+OO SHORT HLIF I-131 -1. 780E+09 3.506E+09 3.597E+09 SHORT HLIF I-132 1.000E+41 2.016E+42 0.000E+OO SHORT HLIF TE-132 4.412E+25 2.061E+26 O.OOOE+OO SHORT HLIF BA-133 -1.183E-04 3.892E-02 3.892E-02 FAIL ABUN I-133 l.000E+41 6.574E+41 O.OOOE+OO SHORT HLIF CS-134 4.872E-02 4. 960E-02 5.425E-02 FAIL ABUN CS-135 -3.115E-02 1.465E-01 1. 472E-01 NOT IDENT. I-135 -1.000E+41 1.693E+42 O.OOOE+OO SHORT HLIF CS-136 6.413E+04 2.226E+05 2.245E+05 SHORT HLIF CE-139 3.413E-02 1.038E-01 1.050E-01 NOT IDENT. BA-140 -4. 251E+05 9.359E+05 9.553E+05 SHORT HLIF LA-140 -9.956E+04 4.301E+05 4.324E+05 SHORT HLIF CE-143 1.000E+41 4. 717E+41 O.OOOE+OO SHORT HLIF CE-144 -6.014E-03 3.752E-01 3.752E-01 NOT IDENT. PM-144 8.923E-03 5.285E-02 5.300E-02 NOT IDENT. PR-144 7.568E-01 4. 581E+OO 4.593E+OO NOT IDENT. PM-146 3.942E-02 3. 967E-02 4.347E-02 NOT IDENT. ND-147 -7.704E+06 2.287E+07 2.313E+07 SHORT HLIF PM-147 -l.250E+03 7.677E+02 9.524E+02 NOT IDENT. PM-149 1. 320E+40 1. 700E+40 0.000E+OO SHORT HLIF EU-150 l.220E-02 2.625E-02 2.682E-02 FAIL ABUN EU-152 -3.946E-03 9.415E-02 9.417E-02 FAIL ABUN GD-153 9.993E-02 2.253E-01 2.298E-01 NOT IDENT. EU-154 -1.594E-02 8.942E-02 8.971E-02 FAIL ABUN EU-155 5.562E-02 1.184E-01 1.210E-01 FAIL ABUN TB-160 5.274E-01 1.830E+OO 1.845E+OO FAIL ABUN H0-166M 4.663E-03 5 .113E-02 5 .118E-02 FAIL ABUN TM-171 -4.573E+OO 2.977E+01 2.984E+Ol NOT IDENT. HF-172 -3.366E-02 2.529E-01 2.534E-01 FAIL ABUN Page 4574 of 5809 LU-172 3.434E-02 7.345E-02 7.506E-02 FAIL ABUN LU-176 1. 472E-02 2.646E-02 2.728E-02 FAIL ABUN HF-181 -1.367E+OO 3.447E+OO 3.502E+OO NOT IDENT. TA-182 2.346E-01 9.148E-01 9.209E-01 FAIL ABUN RE-183 9.287E-02 3.552E+OO 3.552E+OO NOT IDENT. RE-184 4.869E+Ol 4.382E+Ol 4.901E+Ol FAIL ABUN W-188 1.165E+02 1.070E+02 l.192E+02 FAIL ABUN IR-192 -9.704E-02 4.093E-01 4 .116E-01 FAIL ABUN HG-203 -1.953E-01 2.315E+OO 2.317E+OO NOT IDENT. BI-207 4.516E-02 5.802E-02. 6.149E-02 FAIL ABUN PB-210 -2.691E+OO 4.750E+OO 4.902E+OO NOT IDENT. PB-211 -1.540E-Ol 5.372E-01 5.417E-01 NOT IDENT. RN-219 1.894E-02 3.456E-01 3.457E-01 NOT IDENT. RA-223 5.353E-01 9.786E-01 1. 008E+OO* FAIL ABUN AC-227 6.872E-02 2.124E-01 2.147E-01 NOT IDENT. TH-227 6.872E-02 2.124E-01 2.147E-01 NOT IDENT. TH-229 l.453E-01 4.659E-01 4.705E-01 FAIL ABUN TH-231 5.353E-01 9.786E-01 l.008E+OO FAIL ABUN PA-233 -4.974E-03 5.439E-02 5.444E-02 FAIL ABUN PA-234 9.748E-02 2. 963E-01 2. 996E-01 FAIL ABUN PA-234M 3.856E+00 5.031E+OO 5.323E+OO NOT IDENT. NP-237 -4.974E-03 5.439E-02 5.444E-02 FAIL ABUN NP-238 -l.000E+41 1.657E+41 O.OOOE+OO SHORT HLIF NP-239 -5.854E-02 2.836E-01 2.848E-01 NOT IDENT. PU-239 2.205E+02 6.559E+02 6.634E+02 FAIL ABUN AM-241 4.229E-02 1.814E-01 l.824E-01 NOT IDENT. CM-243 -3.215E-02 l.076E-01 1. 086E-01 NOT IDENT. BK-247 5.405E-02 6.892E-02 7.310E-02 NOT IDENT. CM-247 5.505E-03 3.093E-02 3.103E-02 NOT IDENT. CF-249 3.092E-02 3.631E-02 3.890E-02 NOT IDENT. CF-251 1.532E-02 1.183E-01 1.185E-01 NOT IDENT. Page 4575 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 57. 7724 87.09 92.3055 136.47 69.1708 45.60 55.6225 87.57 98.4230 140.51 0.0000 46.54 66.1370 88.03 119.1317 143.76 68.6873 49. 72 0.0000 88.34 9'9. 7110 144.24 68.7104 51. 35 70.0637 88.47 99.7229 145.44 68.7689 51. 87 68.9421 89. 96 119. 3485 152.43 72.5151 52.39 67.8187 1093.63 119.4240 153.25 0.0000 52.97 72.5493 91.11 0.0000 323.87 58.0826 53.44 65.5675 92.59 94.0030 156.02 0.0000 54.07 56.2452 93.35 94.0682 158.56 0.0000 57.36 0.0000 94.56 73.3809 159.00 58.2701 57.53 70.6071 94.65 73.3868 162.33 60.1164 57.98 57.6937 94.67 73.3882 162.66 0.0000 59.27 58.1759 94.87 78.2949 163.33 61.8750 59.32 58.1795 97.43 73.5709 165.86 56.8121 59.54 58.1947 98.43 79.7727 176.31 69.3237 60. 96 66.1695 98.44 79.7737 176.60 0.0000 61.17 70.9133 99.53 78.6221 177.52 66.7742 62.93 75.7954 100 .11 77.4330 181.07 0.0000 63.29 75.8268 102.03 70.1759 181.52 83.4580 63.58 75.8519 103.18 70.2459 184.41 61. 3978 64.28 82.2385 103.37 70.2576 143.76 66.2402 66.73 77.7075 105.21 54.3195 193.51 58.6693 67.24 87.2724 105.31 54.3242 197.03 63.1780 125.81 90.4901 106.12 52. 7142 198.01 54.4348 67.75 77.3983 106.47 60. 9688 201.83 55.4352 69.67 85.9142 109.28 68.1332 203.43 59.0094 70.83 87.6149 111. 00 67.8170 205.31 43.6433 72. 81 90.9928 111.76 0.0000 210.85 65.4493 72. 87 90.9986 114. 06 72. 9618 215.65 51. 4356 74.66 91.1696 116. 30 0.0000 222 .11 53.3978 74.82 91.1847 116.74 81.0139 227.09 51.7566 74.97 91.198 9 119.76 61.2190 227.38 56.2273 77 .11 91. 4004 121.12 73.3745 228.16 0.0000 78.74 91.5523 121. 22 78.3835 228.18 50.8938 79.69 91. 6399 121. 78 78.4180 116. 74 50.8938 80.12 91. 67 93 122.06 78.4352 235.69 45.7176 80.19 0.0000 122.92 61.7882 235. 96 51.1037 80.57 94.9387 123.07 61. 7954 238.63 45.7881 81. 00 107.8581 265.00 43.8622 238.98 0.0000 81. 07 107.8656 125.81 72.8053 240.99 45.8442 81. 75 120.8267 127.23 75.3976 242.00 45.8680 83.79 74.2554 127.91 75.4367 244.70 43.2295 84.00 74.2708 129.30 75.5164 252.40 0.0000 85.43 95.3925 131. 20 79.4056 252.80 42.5029 86.55 110.0621 133.02 73.2027 254.15 0.0000 86.79 92.2788 133.52 73.7352 256.23 36.2345 86.94 92.2922 136.00 64.9312 260.90 0.0000 Page 4576 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 28.1984 355.39 0.0000 584.27 16.8874 264.80 30.9294 356.01 22.7300 595.83 0.0000 265.00 30.9322 364.49 0.0000 427.87 23 .1372 268.22 51.0269 366.42 0.0000 602.52 0.0000 269.46 40 .1167 372. 51 18.1129 604.72 18.5317 270.03 43.7754 375.05 24.8109 607.14 6.1814 271.23 40.1507 377.52 23.8795 609.32 12.3706 273.65 0.0000 356.01 21.0654 610.33 12.3740 276.40 35.6762 388.16 20.1408 614.28 20 .1300 277.37 32.9465 388.63 0.0000 618.01 18.6013 277.60 35. 6960 391. 6'9 28.8116 62 0. 3 6 19.6479 278.00 37.5341 264.66 21.1997 621. 93 15.5182 279.20 43. 9668 401.81 22.1732 630.19 0.0000 279.54 45.8059 402.40 20.2493 631.29 14.5212 279.70 41.2289 404.85 19.3026 633.25 8.3024 280.46 36.6610 410.95 27.0846 634.78 0.0000 283.69 39.4700 413.71 30.0167 635.95 10.3857 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 31.2338 423.72 0.0000 645.85 10.4138 285.90 0.0000 427.09 32.1084 657.76 9.4028 287.50 43.2182 427.87 28.2247 657.90 0.0000 290.67 23.4824 433.94 11. 7043 661. 66 11. 5044 293.27 0.0000 439.40 18.5678 664.57 0.0000 351. 93 47.0623 453.88 '12. 7683 666.33 0.0000 295. 96 47.0779 463.37 18.7221 666.50 0.0000 879.38 38.8162 468.07 22. 6996 667. 71 0.0000 299.98 38.8409 473.00 0.0000 677.62 14.7041 300.09 38.8427 475.06 14.8389 685.70 0.0000 300 .13 38.8435 476.78 19.7965 695.00 0.0000 301.36 38.8649 477.60 17.8217 696.49 13.7210 302.85 38.8905 482.18 13.3868 696. 51 13.7210 256.23 41.6995 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 10.5570 306.78 30.6105 497.08 13. 9504 697.49 12.6689 308.46 40.8445 505.52 26.9775 702.65 21.1426 311. 90 30.6797 507.63 0.0000 706.68 14.8152 316.51 30.7415 511. 00 31.0287 711. 68 11. 6557 319.41 0.0000 514.00 24.0449 720.70 0.0000 320.08 0.0000 514.00 24.0449 721. 93 0.0000 321.04 30.8019 520.40 22.5879 722. 78 11.1571 323.87 33.6431 520.69 .o. 0000 722. 91 11.1575 325.23 43.4802 522.65 0.0000 723.31 7.9703 328.76 0.0000 527.90 0.0000 724.19 17.5386 333.37 29.2748 528.26 6.0383 727.33 18.0846 333.97 26.7483 529.59 10. 5714 733.00 15.9796 334.37 33.7932 529.87 0.0000 735.93 13.8590 338.28 33.8481 531.02 0.0000 333.97 9.5984 338.32 33.8489 537.26 0.0000 739.50 0.0000 311.90 33.8789 546.56 0.0000 747.24 13.8982 340.48 33.8789 552.55 20.2783 748.06 13. 9008 340.55 0.0000 563.25 13. 2232 752.31 10.7039 344.28 26.8631 569.33 24.4561 753.82 0.0000 345.93 21. 6940 946.00 22.9285 756.73 11.7873 351.06 17.9586 569.70 22.9303 756.80 11. 7873 351.93 17.9648 583.19 11. 254 7 884.68 16.1017 Page 4577 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 16.1090 1274.44 10.1700 1620.50 2.8242 766.42 12.8892 1001.03 7.9174 1621.92 3.7664 766.84 16 .1133 1002.74 16.9720 1678.03 0.0000 772.60 0.0000 1004.73 15.8468 1690.97 2.8522 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 1.9207 778.90 12.9282 1028.54 0.0000 1063.66 3.8442 783.70 0.0000 1037.84 3.4182 1771. 35 2.8835 785.37 6.4741 1038.76 0.0000 1791.20 0.0000 792.07 21.6146 631.29 9.1309 1808.65 3.8638 794.95 8.6517 1048.07 0.0000 1810.72 0.0000 795.86 8.6536 1049.04 6. 8511 1836.06 1.9388 810.06 4.3411 1050.41 7.9952 810.29 6.5122 1063.66 10.3059 344.28 6.5125 1077.00 0.0000 810.76 7.5984 1077.34 5.7406 815.77 0.0000 1085.87 3.4500 1048.07 0.0000 1093.63 6.9102 832.01 6.5449 1099.45 4.6120 834.85 13.0981 1112. 07 5.7784 835.71 13 .1011 1112. 84 8.0909 836.80 0.0000 1115. 54 5.2039 846.75 0.0000 1120.29 9.2598 846.77 9.8503 1120.55 9'. 2604 856.80 0.0000 1221. 41 9.2617 860.56 8.7832 1129. 67 12.7546 871.09 14.8563 1131.51 0.0000 873.19 9.9089 1147.95 0.0000 875.33 0.0000 1173.23 6.1357 879.38 9.9225 1177.95 13.1598 880.51 9.9247 1189.05 7.0322 883.24 15.4481 1204.77 12.3406 884.68 9.9338 1221. 41 10.6091 889.28 17.6784 1231. 02 7.9700 894.76 17.6992 1235.36 0.0000 898.04 12.1767 1238.28 12.4132 900. 72 11. 6301 1260.41 0.0000 903.28 9.9741 1271. 87 5.3507 911. 20 8.3261 1274.44 6.2451 912.08 8.3276 1274.54 5.3533 923.98 0.0000 1291.59 7.1582 926.50 14.4790 1298.22 0.0000 929 .11 13.3726 1312 .11 0.0000 937.49 3.3491 1332.49 3.6035 944.13 0.0000 1362.66 0.0000 946.00 8.9469 1365.19 6.3399 949.00 8.9525 1368.63 0.0000 667. 71 0.0000 1384.29 6.3591 962.31 17.9551 1408.01 5. 4712 964.08 11. 7873 1457.56 0.0000 966.17 15.1617 1460.82 4.5972 911.20 15.7318 1489.16 6.4638 968.97 15.7318 1505.03 6.4792 983.53 0.0000 1584.12 4.6826 984.45 0.0000 1596.21 0.0000 Page 4578 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:46:50.30 ******************************************************************************** *
  • GEL Laboratories LLd *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA .. GAMMA .ARCHIVE. GAMMA] G405235072. CNF; 1 Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM05.CNF;477 Background date : Z-OCT-2016 11:00:07. Sample date 15-DEC-2015 13:35:00 Acquisition date : 3-0CT-2016 06:45:49. Sample ID G405235072 Sample quantity : 1.66107E+02 GRAM Detector name : GAM05 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.62 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 1 1 1 0 0 0 0 3 3 0 5 5 0 9 9 9 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4579 of 5809 Energy 46.07* 63.10* 72. 69 74.54* 76.70* 85.98* 91.75* 143.43* 147.00 182.34 185.52* 208.86 238.31* 241.33 251.16 268.62 271. 63 276.81 294.80* 299.62 328.23 338.26* 351. 62* 356.95 409.49 464.18 510.86* 565.60 583.03* 609.14* 627.20 727.24 768.80* 798.59 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 47 76 26 207 425 217 159 38 19 23 94 75 410 156 25 62 24 25 223 18 24 94 300 10 27 57 63 26 136 235 22 39 30 14 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 160 262 187 183 177 269 266 107 103 92 92 105 61 92 131 65 52 58 98 84 63 52 38 52 49 57 44 20 18 22 20 14 22 47 0.74 1. 05 0.93 0.94 0.94 1.14 1. 40 1. 66 1. 31 1. 40 1. 40 2.00 0.92 1. 82 1. 37 2.75 1. 55 1. 56 1.13 1. 01 0.94 1. 37 1. 29 0.92 1. 88 1. 54 1. 36 2.99 1. 21 1. 48 1. 91 0.69 1. 08 5.69 93.97 128.00 147.16 150.86 155.17 173.72 185.27 288.55 295.69 366.31 372.66 419.32 478.18 484.21 503.85 538.75 544.77 555.12 591.08 600.70 657.89 677.94 704.64 715. 28 820.30 929.61 1022.91 1132.32 1167 .14 1219.34 1255.42 1455.38 1538.44 1597.99 90 124 144 144 144 167 179 285 293 362 362 414 473 473 498 533 533 533 584 597 653 673 700 710 816 922 1016 1128 1163 1214 1250 1450 1533 1584 8 1.30E-02 52.0 9 2.llE-02 41.1 24 7.33E-03 83.6 1.68E+OO 24 5.74E-02 12.7 24 1.18E-01 7 .1 12 6.02E-02 16.7 12 4.41E-02 22.6 8 1. 04E-02 51.1 8 5.40E-03 93.4 21 6.28E-03 75.1 1.44E+OO 21 2. 60E-02 21. 5 10 2.09E-02 28.2 21 1.14E-01 5.6 2.29E+OO 21 4.34E-02 16.9 14 6.96E-03 98.4 32 1.72E-02 31.1 2.20E+OO 32 6.65E-03 64.3 32 7.02E-03 59.3 14 6.19E-02 11.6 9 4.92E-03 96.0 9 6.56E-03 64.8 10 2.62E-02 17.9 9 8.33E-02 7.0 11 2.70E-03150.4 11 7.43E-03 53.5 17 1.58E-02 33.6 15 1.74E-02 30.6 9 7.llE-03 37.4 9 3.78E-02 10.4 11 6. 52E-02 7. 7 10 6.14E-03 43.4 11 1.09E-02 24.3 11 8.45E-03 35.5 18 3.85E-03121.5 Peak Search Report (continued) Page : 2 Sample ID : G405235072 Acquisition date 3-0CT-2016 06:45:49 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 876.60 9 5 0.91 1753.91 1751 6 2.62E-03 50.9 36 1 911. 20* 104 14 1. 69 1823.05 1816 28 2.88E-02 12.1 1.44E+OO 37 1 00 16 7 1. 90 1836.65 1816.. 28 4.45E-03 49.9 38 0 927.77 11 19 1. 07 1856.18 1850 12 3.19E-03 79.9 39 1 964. 69 28 23 1. 93 1929.97 1925 25 7.90E-03 32.8 1.58E+OO 40 1 969 .10 50 21 1. 90 1938.79 1925 25 l.38E-02 23.6 41 0 991.00 22 13 0.66 1982.57 1976 17 6.04E-03 43.5 42 0 1094.78 5 9 0.56 2190.00 2182 9 1.39E-03117.0 43 0 1120. 05* 51 14 1. 87 2240.51 2234 11 1.41E-02 20.3 44 0 1276.52 6 14 0.56 2553.25 2542 14 l.64E-03140.8 45 0 1289.30 15 16 0.54 2578.80 2572 16 4.17E-03 65.0 46 0 1314.43 9 1 0.95 2629.03 2626 6 2.40E-03 40.5 47 0 1461.05* 450 8 2.15 2922.09 2914 15 1.25E-01 4. 9 48 0 1728.71 15 3 4.93 3457.09 3450 13 4.14E-03 35.9 49 0 1764.67 37 0 1. 83 3528.97 3523 12 1. 03E-02 16.4 Flag: "*" = Peak area was modified by background subtraction Page 4580 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 07:46:53 DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235072.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 13:35:00 G405235072 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:45:49 166.11 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type : Abundance limit SOLID GAMMAS 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Page 4581of5809 PB-214 PB-214 PB-214 PB-214 'PB-214 Line 242.00 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 AM-243 TH-228 PB-212 BI-211 Line 240.99 74.66 74.82 74.82 351. 06' CAN 0 01:00:00.62 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235072 Acquisition date 3-0CT-2016 06:45:49 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* 1.244E+OQ 1.496E+Ol 1.496E+Ol 9.85 OK CS-135 268.22 16.00* 5.054E+OO 4.157E-01 4.157E-01 62 .11 OK TL-208 277.37 6.60 4. 931E+OO 4.200E-01 4.200E-01 118. 59 OK 583.19 85.00* 2.674E+OO 2.973E-01 2.973E-01 20.89 OK 860.56 12.50 1.959E+OO Line Not Found Absent PB-210 46.54 4.25* 9.664E+OO 7.421E-01 7.609E-01 104.03 OK PB-212 74.82 10.28 8.979E+OO 5. 272E-01 5. 272E-01 75.04 OK 77 .11 17.10 8. 967E+OO 1.716E+OO 1.716E+OO 14 .11 OK 238.63 43.60* 5.565E+OO 9.286E-01 9.286E-01 11.25 OK 300.09 3.30 4.619E+OO 6.232E-01 6.232E-01 191. 97 OK BI-214 609.32 45.49* 2.582E+OO 9.853E-01 9.856E-01 15.44 OK 1120.29 14.92 1.576E+00 9. 851E-01 9.854E-01 40.60 OK 1764.49 15.30 l.032E+OO 1.005E+OO l.005E+OO 32.88 OK PB-214 74.82 5.80 8.977E+OO Line Not Found <<INT Reject 77 .11 9.70 8. 967E+OO 3.026E+OO 3.027E+OO 14 .11 OK 87.09 3.41 8.919E+OO 4.361E+OO 4.362E+OO 33.31 OK 242.00 7.25 5.497E+OO Line Not Found <<INT Reject 295.22 18.42 4.682E+OO 1.387E+OO 1.388E+OO 23.28 OK 3'51. 93 35.60* 4.044E+OO 1.097E+OO 1.097E+OO 13.95 OK RN-222 609.32 45.49* 2.582E+OO 9.853E-01 9.856E-01 15.44 OK 1120.29 14.92 1. 576E+OO 9. 851E-01 9.854E-01 40.60 OK 1764.49 15.30 1. 032E+00 1.005E+OO 1.005E+OO 32.88 OK RA-224 240.99 4.10* 5.509E+OO 1.101E+OO 1.101E+OO 127.23 OK RA-226 609.32 45.49* 2.582E+OO 9.853E-01 9.856E-01 15.44 OK 1120.29 14.92 1. 576E+OO 9. 851E-01 9.854E-01 40.60 OK 1764.49 15.30 1.032E+OO 1.005E+OO 1.005E+OO 32.88 OK AC-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.176E+OO 1.061E+OO 1. 061E+OO 35.82 OK 794.95 4.25 2.087E+OO Line Not Found Absent 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1.870E+OO 1.007E+OO 1.007E+OO 24.25 OK 968. 97 15.80 1.778E+OO 8.216E-01 8.216E-01 47.25 OK RA-228 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.176E+OO 1.061E+OO 1.061E+OO 35.82 OK 794.95 4.25 2.087E+00 Line Not Found Absent 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* 1. 870E+00 1.007E+OO 1.007E+OO 24.25 OK 968. 97 15.80 1. 778E+00 8.216E-01 8.216E-01 47.25 OK TH-228 74.82 10.28 8.979E+OO 5.272E-01 5.272E-01 75.04 OK 77 .11 17.10 8. 967E+OO 1.716E+OO 1. 716E+OO 14 .11 OK 238.63 43.60* 5.565E+OO 9.286E-01 9.286E-01 11.25 OK 300.09 3.30 4.619E+OO 6.232E-01 6.232E-01 191.97 OK TH-230 609.32 45.49* 2.582E+OO 9.853E-01 9.853E-01 15.44 OK 1120.29 14.92 1. 576E+OO 9. 851E-01 9. 851E-01 40.60 OK 1764.49 15.30 1.032E+OO 1.005E+OO 1.005E+OO 32.88 OK TH-232 105.21 1.10 8.704E+OO Line Not Found Absent 338.32 11. 27 4.176E+00 1.061E+OO 1.061E+OO 35.82 OK 835.71 1. 61 2.005E+OO Line Not Found Absent 911.20 25.80* l.870E+00 1.007E+OO 1.007E+OO 24.25 OK Page 4582 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235072 Acquisition date 3-0CT-2016 06:45:49 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 968.97. 15.80 l.778E+OO 8.216E-01 8.216E-01 .47.25 OK TH-234 63.29 3.70* 9 .118E+OO l.421E+OO l.421E+OO 82.23 OK 92.59 4.23 8.875E+OO 2.571E+OO 2.571E+OO 45.21 OK U-234 609.32 45.49* 2.582E+OO 9.853E-01 9.853E-01 15.44 OK 1120.29 14.92 l.576E+00 9.851E-01 9. 851E-01 40.60 OK 1764.49 15.30 l.032E+OO l.005E+OO l.005E+OO 32.88 OK U-235 89. 96 3.47 8.890E+OO Line Not Found Absent 93.35 5.60 8.860E+OO Line Not Found Absent 143.76 10. 96* 7.817E+OO 2.542E-01 2.542E-01 102.12 OK 163.33 5.08 7.279E+OO Line Not Found Absent 185. 72 57.20 6.705E+OO l.380E-01 l.380E-01 42.95 OK 205.31 5.01 6.238E+OO Line Not Found Absent U-238 63.29 3.70* 9 .118E+OO 1. 421E+OO 1. 421E+OO 82.23 OK 92.59 4.23 8.875E+OO 2. 571E+OO 2.571E+OO 45.21 OK AM-243 43.53 5.90 9.491E+OO Line Not Found Absent 74.66 67.20* 8.979E+OO 8.065E-02 8.066E-02 75.04 OK ANH-511 511. 00 100.00* 2.974E+OO l.060E-01 l.060E-01 61. 27 OK Flag: "*" = Keyline Page 4583 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:46:54.75 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235072.CNF;l *
  • Acquisition date 3-0CT-2016 06:45:49 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
  • Sample date 15-DEC-2015 13:35:00 Analyst initials: MXRl *
  • Sample ID G405235072 Sample Quantity l.6611E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight P.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.496E+Ol l.444E+OO 3.744E-01 CS-135 4.157E-01 2. 531E-01 l.877E-01 TL-208 2.973E-01 6.087E-02 5.624E-02 PB-210 7.609E-01 7.758E-01 5.284E-01 PB-212 9.286E-01 1.024E-01 7.575E-02 BI-214 9.856E-01 1.492E-01 9.824E-02 PB-214 1.097E+OO l.501E-01 9.580E-02 RN-222 9.856E-01 1.492E-01 9.824E-02 RA-224 1.101E+OO l.372E+OO 8.127E-01 RA-226 9.856E-01 l.492E-01 9.824E-02 AC-228 l.007E+00 2.394E-01 2.055E-01 RA-228 1.007E+OO 2.394E-01 2.055E-01 TH-228 9.286E-01 1.024E-01 7.575E-02 TH-230 9.853E-01 l.491E-01 9. 821E-02 TH-232 1.007E+OO 2.394E-01 2.055E-01 TH-234 1.421E+OO 1.145E+OO 7. l 72E-01 U-234 9.853E-01 l.491E-01 9. 821E-02 U-235 2.542E-01 2.544E-01 2.041E-01 U-238 1.421E+OO 1.145E+OO 7 .172E-01 AM-243 8.066E-02 5.932E-02 4.205E-02 ANH-511 1.060E-01 6.366E-02 3.644E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 1.787E+OO 8.867E+OO 1.807E+Ol NOT IDENT. NA-22 2.279E-03 3.783E-02 7.665E-02 NOT IDENT. NA-24 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF AL-26 l.227E-02 l.987E-02 5.345E-02 NOT IDENT. SC-46 8.697E-03 2.843E-01 5.517E-01 FAIL ABUN V-48 O.OOOE+OO 8.278E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 2.745E+02 O.OOOE+OO SHORT HLIF MN-54 3.214E-02 5.679E-02 1.160E-01 NOT IDENT. C0-56 -3.0l3E-01 3.805E-01 6.530E-01 NOT IDENT. Page 4584 of 5809 MN-56 O.OOOE+OO l.251E+41 0.000E+OO SHORT HLIF C0-57 -7.065E-03 3.012E-02 5.877E-02 NOT IDENT. C0-58 -l.845E-02 4.293E-01 8.269E-01 NOT IDENT. FE-59 5.799E-02 3.309E+OO 7.132E+OO NOT IDENT. C0-60 -3.315E-03 3.259E-02 6.436E-02 NOT IDENT. ZN-65 -l.151E-02 l.671E-01 2.889E-Ol NOT IDENT. GE-68 -3.516E-01 1.942E+OO 3.805E+OO NOT IDENT. AS-73 -4.905E-01 l.325E+OO 2. 722E+OO NOT IDENT. AS-74 0.000E+OO 3.861E+03 O.OOOE+OO SHORT HLIF
  • SE-75 4.661E-02 1.536E-01 2.788E-01 NOT IDENT . BR-77 O.OOOE+OO 2.314E+36 0.000E+OO SHORT HLIF SR-82 O.OOOE+OO 4.614E+02 O.OOOE+OO SHORT HLIF RB-83 4.759E-02 4.161E-Ol 8.550E-01 NOT IDENT. KR-85 1. 969E+OO 4.954E+OO 9.576E+OO NOT IDENT. SR-85 l.918E-01 4.856E-01 9.383E-01 NOT IDENT. RB-86 O.OOOE+OO 1.884E+04 O.OOOE+OO SHORT HLIF Y-88 -l.090E-01 2.182E-01 3.822E-01 NOT IDENT. Y-91 -2.568E+02 4.756E+02 8.592E+02 NOT IDENT. NB-94 1. 808E-02 2.783E-02 5.753E-02 NOT IDENT. NB-95 2.038E-01 6.381E-01 l.179E+OO NOT IDENT. NB-95M -4.897E-01 1.833E+OO 3.076E+OO NOT IDENT. ZR-95 2.356E-01 1. 072E+OO 2.148E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF ZR-97 O.OOOE+OO 1.325E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 2.200E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF RH-101 3.333E-03 2.230E-02 4.454E-02 NOT IDENT. RH-102 -l.997E-02 5.073E-02 8.359E-02 NOT IDENT. RU-103 -2.317E+OO 3.669E+OO 6.758E+OO FAIL ABUN RH-106 l.885E-01 3.463E-01 6.979E-01 NOT IDENT. RU-106 1.885E-01 3.463E-01 6.979E-01 NOT IDENT. AG-108M 4.047E-03 2. 011E-02 4.154E-02 NOT IDENT. CD-109 5.695E-01 6.892E-01 1.242E+OO NOT IDENT. AG-110M -1. 771E-02 8. 051E-02 l.488E-01 NOT IDENT. SN-113 4.927E-02 l.683E-01 3.492E-01 NOT IDENT. CD-115 O.OOOE+OO 2.977E+38 O.OOOE+OO SHORT HLIF-SN-117M O.OOOE+OO 4.893E+04 O.OOOE+OO SHORT HLIF TE-123M -4.039E-02 9.131E-02 1.709E-01 NOT IDENT. SB-124 1. 260E+OO 1.345E+OO 3.639E+OO NOT IDENT. SB-125 -9.854E-03 7.258E-02 1.448E-01 FAIL ABUN TE-125M 1. 4 7 5E+02 l.606E+02 3.403E+02 NOT IDENT. I-126 O.OOOE+OO 5.304E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 5.869E+05 O.OOOE+OO SHORT HLIF SN-126 O.OOOE+OO 4.877E-02 9.672E-02 FAIL ABUN SB-127 O.OOOE+OO 4.712E+21 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 1. 961E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 0.000E+OO 6.030E+25 O.OOOE+OO SHORT HLIF BA-133 2.171E-02 6.399E-02 6.253E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 l.934E-02 4.461E-02 8. 969E-02 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 1.590E+05 O.OOOE+OO SHORT HLIF BA-137M l.507E-02 2.502E-02 5.338E-02 NOT IDENT. CS-137 l.592E-02 2.643E-02 5.639E-02 NOT IDENT. CE-139 2.238E-03 7.297E-02 1.422E-01 NOT IDENT. BA-140 0.000E+OO 6.730E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.747E+05 O.OOOE+OO SHORT HLIF CE-141 -1. 611E+OO 1.546E+Ol 2.454E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.767E+40 O.OOOE+OO SHORT HLIF CE-144 5.135E-02 2.338E-01 4.684E-01 NOT IDENT. PM-144 3.495E-02 3.899E-02 8. 651E-02 NOT IDENT. PR-144 3.00lE+OO 3.370E+OO 7.474E+OO NOT IDENT. PM-146 5.918E-03 3.232E-02 6.630E-02 NOT IDENT. ND-147 O.OOOE+OO 1.882E+07 O.OOOE+OO SHORT HLIF PM-147 *1. 777E+02 5.317E+02 1.082E+03 NOT IDENT. PM-149 O.OOOE+OO 4.109E+39 0.000E+OO SHORT HLIF EU-150 -l.169E-03 2.218E-02 3.720E-02 FAIL ABUN EU-152 '2.161E-03 6.020E-02 l.245E-01 FAIL ABUN GD-153 -1. 761E-02 l.003E-01 1.988E-01 NOT IDENT. EU-154 3.650E-03 9. 2 67E-02 l.873E-01 NOT IDENT. EU-155 3.248E-02 6.840E-02 1.410E-01 FAIL ABUN TB-160 2.444E-01 1.373E+OO 2.508E+OO FAIL ABUN H0-166M 3.751E-03 4.616E-02 9 .113E-02 FAIL ABUN TM-171 6.665E-01 3.032E+OO 6.484E+OO NOT IDENT. HF-172 -5.775E-02 l.396E-01 2.683E-01 FAIL ABUN LU-172 3.043E-02 6.982E-02 l.184E-01 FAIL ABUN LU-176 9.729E-03 l.883E-02 3.712E-02 NOT IDENT. Page 4585 of 5809 HF-181 9. 718E-01 3.072E+OO 6.332E+00 NOT IDENT. TA-182 1. 802E-01 8. l 72E-01 1.643E+00 FAIL ABUN RE-183 2.070E-01 6.314E-01 1.345E+00 NOT IDENT. RE-184 -1.943E+OO 2.031E+Ol 3.855E+Ol NOT IDENT. W-188 5.085E-01 7.919E+Ol 1.370E+02 FAIL ABUN IR-192 1.880E-01 3.030E-01 6.133E-01 FAIL ABUN HG-203 1. 047E+OO 1. 696E+OO 3.365E+OO FAIL ABUN BI-207 -6.739E-04 3.605E-02 7.343E-02 FAIL ABUN BI-211 O.OOOE+OO 4.133E-01 7.597E-01 FAIL ABUN PS-211 6.997E-02 5.292E-01 .9. 827E-01 NOT IDENT. BI-212 O.OOOE+OO 6.029E-01 1.051E+OO FAIL ABUN RN-219 5.616E-02 3.177E-01 6.446E-01 FAIL ABUN RA-223 -2.212E-02 4.977E-01 8.408E-01 FAIL ABUN AC-227 7.335E-02 1.819E-01 3.327E-01 FAIL ABUN TH-227 7.335E-02 1.819E-01 3.327E-01 FAIL ABUN TH-229 1.201E-01 3.342E-01 6.608E-01 FAIL ABUN PA-231 6.946E-02 4.092E-01 7.075E-01 NOT IDENT. TH-231 -2.212E-02 4.977E-01 8.408E-01 FAIL ABUN PA-233 7.768E-03 5.146E-02 9.625E-02 FAIL ABUN PA-234 -1.275E-01 2.098E-01 3.547E-01 FAIL ABUN PA-234M -5.074E-01 3.779E+OO 7.502E+OO NOT IDENT. NP-237 7.768E-03 5.146E-02 9.625E-02 FAIL ABUN NP-238 O.OOOE+OO 3.830E+40 O.OOOE+OO SHORT HLIF NP-239 2. 872E-02 1.518E-01 3.070E-01 FAIL ABUN PU-239 1.050E+02 2.002E+02 4.108E+02 NOT IDENT. AM-241 3.381E-03 3.674E-02 7.184E-02 NOT IDENT. CM-243 -2.971E-02 6.136E-02 1.189E-01 FAIL ABUN BK-247 3.738E:....03 5.418E-02 9.547E-02 NOT IDENT. CM-247 -2.302E-02 2.753E-02 5.057E-02 FAIL ABUN CF-249 9.972E-03 2.726E-02 5.724E-02 NOT IDENT. CF-251 1.083E-02 8.530E-02 1.658E-01 NOT IDENT. Page 4586 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:46:51.64 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 439 10.66* 1.244E+OO* 1. 496E+Ol 1.496E+Ol 9.85 CS-135 268.22 74 16.00* 5.054E+OO 4.157E-01 4.157E-01 62.11 TL-208 277.37 30 6.60 4.931E+OO 4.200E-01 4.200E-01 118. 59 583.19 149 85.00* 2.674E+OO 2.973E-01 2.973E-01 20.89 8 60. 56 ------12.50 1.959E+OO ------Line Not Found ------PB-210 46.54 67 4.25* 9.664E+OO 7.421E-01 7.609E-01 104.03 BI-211 72.87 36 1. 23 8.991E+OO 1.484E+OO 1.484E+OO 167.21 351.06 349 12.92* 4.044E+OO 3.023E+OO 3.023E+OO 13. 95 PB-212 74.82 284 10.28 8.979E+OO 1.389E+OO 1. 389E+OO 25.44 77 .11 582 17.10 8. 967E+OO 1.716E+OO 1.716E+OO 14 .11 238.63 498 43.60* 5.565E+OO 9.286E-01 9.286E-01 11. 25 300.09 21 3.30 4.619E+OO 6.232E-01 6.232E-01 191.97 BI-214 609.32 256 45.49* 2.582E+OO 9.853E-01 9.856E-01 15.44 1120.29 51 14.92 1.576E+OO 9. 851E-01 9.854E-01 40.60 1764.49 35 15.30 1.032E+OO 1.005E+OO 1.005E+OO 32.88 PB...:214 74.82 284 5.80 8.979E+OO" 2.462E+OO 2.463E+OO 25.44 77 .11 582 9.70 8.967E+OO 3.026E+OO 3.027E+OO 14 .11 87.09 293 3.41 8.919E+OO 4.361E+OO 4.362E+OO 33.31 242.00 190 7.25 5.509E+OO 2.150E+OO 2.151E+OO 33.79 295.22 265 18.42 4.682E+OO 1.387E+OO l.388E+OO 23.28 351. 93 349 35.60* 4.044E+OO 1.097E+OO 1.097E+OO 13.95 RN-222 609.32 256 45.49* 2.582E+OO 9.853E-01 9.856E-01 15.44 1120.29 51 14.92 1.576E+OO 9.851E-01 9.854E-01 40.60 1764.49 35 15.30 1.032E+OO 1.005E+OO 1.005E+OO 32.88 RA-224 240.99 190 4.10* 5.509E+OO 3.801E+OO 3.801E+OO 33.79 RA-226 609.32 256 45.49* 2.582E+OO 9.853E-01 9.856E-01 15.44 1120.29 51 14.92 1.576E+OO 9.851E-01 9.854E-01 40.60 1764.49 35 15.30 1.032E+OO 1.005E+OO 1.005E+OO 32.88 AC-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 110 11.27 4.176E+OO 1.061E+OO 1. 061E+OO 35.82 794.95 ------4.25 2.087E+OO ------Line Not Found ------835.71 ------1. 61 2.005E+OO ------Line Not Found ------911.20 108 25.80* 1.870E+OO 1.007E+OO 1.007E+OO 24.25 968.97 51 15.80 1.778E+OO 8.216E-01 8.216E-01 47.25 RA-228 105.21 ------1.10 8.704E+OO ------Line Not Found ------338.32 110 11. 27 4.176E+OO 1.061E+OO 1. 061E+OO 35.82 794.95 ------4.25 2.087E+OO ------Line Not Found ------835.71 ------1. 61 2.005E+OO ------Line Not Found ------911. 20 108 25.80* 1.870E+OO 1.007E+OO 1.007E+OO 24.25 968.97 51 15.80 1.778E+OO 8.216E-01 8..216E-01 47.25 TH-228 74.82 284 10.28 8.979E+OO 1.389E+OO l.389E+OO 25.44 77 .11 582 17.10 8. 967E+OO 1. 716E+OO 1. 716E+OO 14 .11 238.63 498 43.60* 5.565E+OO 9.286E-01 9.286E-01 11. 25 300.09 21 3.30 4.619E+OO 6.232E-01 6.232E-01 191. 97 TH-230 609.32 256 45.49* 2.582E+OO 9.853E-01 9.853E-01 15.44 1120.29 51 14.92 1.576E+OO 9.851E-01 9. 851E-01 40.60 1764.49 35 15.30 1.032E+OO 1.005E+OO 1.005E+OO 32.88 Page 4587 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235072 Acquisition date 3-0CT-2016 06:45:49 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM * %Error TH-232 105.21 ------* 1.10 8.704E+OO ------Line Not Found ,-----338.32 110 11. 27 4.176E+OO 1.061E+OO 1. 061E+OO 35.82 835.71 ------1. 61 2.005E+OO ------Line Not Found ------911. 20 108 25.80* 1.870E+OO 1.007E+OO 1.007E+OO 24.25 968. 97 51 15.80 1.778E+OO 8.216E-01 8.216E-01 47.25 TH-234 63.29 106 3.70* 9 .118E+OO 1.421E+OO 1.421E+OO 82.23 92.59 214 4.23 8.875E+OO 2.571E+OO 2.571E+OO 45.21 U-234 609.32 256 45.49* 2.582E+OO 9.853E-01 9.853E-01 15.44 1120.29 51 14.92 1. 576E+OO 9.851E-01 9. 851E-01 40.60 1764.49 35 15.30 1.032E+OO 1.005E+OO 1.005E+OO 32.88 U-235 89. 96 ------3.47 8.890E+OO ------Line Not Found ------93.35 ------5.60 8.860E+OO ------Line Not Found ------143.76 48 10. 96* 7.817E+OO 2.542E-01 2.542E-01 102.12 163.33 ------5.08 7.279E+OO ------Line Not Found ------185. 72 117 57.20 6.705E+OO 1. 380E-01 l.380E-01 42.95 205.31 ------5.01 6.238E+OO ------Line Not Found ------U-238 63.29 106 3.70* 9 .118E+OO 1.421E+OO 1.421E+OO 82.23 92.59 214 4.23 8.875E+OO 2. 571E+OO 2.571E+OO 45.21 AM-243 43.53 ------5.90 9.491E+OO ------Line Not Found ------74.66 284 67.20* 8.979E+OO 2.125E-01 2.125E-01 25.44 ANH-511 511. 00 70 100.00* 2.974E+OO 1.060E-01 l.060E-01 61. 27 Flag: "*" Key line Page 4588 of 5809 Summary of Nuclide Activity Sample ID : G405235072 Acquisition date Page : 3 3-0CT-2016 06:45:49 Total number of lines in spectrum 49 Number of unidentified lines 12 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CS-135 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 2.30E+06Y l.41E+10Y 22.20Y 7.04E+08Y 1. 41E+10Y 1600. OOY 1600. OOY 1600. OOY l.41E+l0Y 1600. OOY 1. 41E+l0Y 1. 41E+10Y 1.41E+10Y 7.54E+04Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 1. 00 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM l.496E+Ol 4.157E-01 2.973E-01 7. 421E-01 3.023E+OO 9.286E-01 9.853E-01 1.097E+OO 9.853E-01 3.801E+OO 9.853E-01 1.007E+OO 1.007E+OO 9.286E-01 9.853E-01 1.007E+OO 1. 421E+OO 9.853E-01 2.542E-01 1. 421E+OO 2.125E-01 1.060E-01 3.755E+Ol 3.755E+Ol Decay Corr pCi/GRAM 1.496E+Ol 4.157E-01 2.973E-01 7.609E-01 3.023E+OO 9.286E-01 9.856E-01 1.097E+OO 9.856E-01 3. 801E+OO 9.856E-01 1.007E+OO 1.007E+OO 9.286E-01 9.853E-01 1.007E+OO 1.421E+OO 9.853E-01 2.542E-01 1. 421E+OO 2.125E-01 1.060E-01 3.757E+Ol 3.757E+Ol 75.51% . Decay Corr 2-Sigma Error 0.147E+01 2.582E-01 0. 621E-01 7.916E-01 0.422E+OO l.045E-01 l.522E-01 0.153E+OO 1.522E-01 1.284E+OO l.522E-01 0.244E+OO 0.244E+OO l.045E-01 1.522E-01 0.244E+OO l.169E+OO l.522E-01 2. 596E-01 1.169E+OO 0.541E-01 0.650E-01 "M" Manually accepted 2-Sigma %Error 9.85 62 .11 20.89 104.03 13.95 11.25 15.44 13.95 15.44 33.79 15.44 24.25 24.25 11. 25 15.44 24.25 82.23 15.44 102.12 82.23 25.44 61. 27 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4589 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235072 Acquisition date : 3-0CT-2016 06:45:49 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 147.00 25 131 1. 31 295.69 293 8 5.40E-03 **** 7.72E+OO 3 182.34 28 115 1. 40 366.31 362 21 6.28E-03 **** 6.78E+OO T 0 208.86 93 129 2.00 419.32 414 10 2.09E-02 56.4 6.16E+OO 0 251.16 . 30 158 1. 37 503.85 498 14 6. 96&-03 **** 5.34E+OO T 9 271. 63 29 63 1. 55 544.77 533 32 6. 65E.-03 **** 5.0lE+OO T 0 328.23 28 74 0.94 657.89 653 9 6.56E-03 **** 4.28E+OO T 0 356.95 11 61 0.92 715. 28 710 11 2.70E-03 **** 3.99E+OO T 0 409.49 31 56 1. 88 820.30 816 11 7.43E-03 **** 3.56E+OO T 0 464.18 64 64 1. 54 929.61 922 17 l.58E-02 67.3 3.22E+OO T 0 565.60 28 22 2.99 1132. 32 1128 9 7. llE-03 74.8 2.74E+OO 0 627.20 24 22 1. 91 1255.42 1250 10 6.14E-03 8 6. 8 2.52E+OO 0 727.24 42 15 0.69 1455.38 1450 11 1. 09E-02 48.7 2.24E+00 T 0 768.80 32 23 1. 08 1538.44 1533 11 8.45E-03 71.1 2.14E+00 0 798.59 15 50 5.69 1597.99 1584 18 3.85E-03 **** 2.08E+OO 0 876.60 10 5 0.91 1753.91 1751 6 2.62E-03 **** 1. 93E+OO T 1 918.00 17 7 1. 90 1836.65 1816 28 4.45E-03 99.8 l.86E+OO 0 927.77 12 19 1. 07 1856.18 1850 12 3.19E-03 **** l.84E+00 T 1 964. 69 29 24 1. 93 1929.97 1925 25 7.90E-03 65.6 1. 7 9E+00 T 0 991.00 22 14 0.66 1982.57 1976 17 6.04E-03 86.9 1.75E+OO 0 1094.78 5 9 0.56 2190.00 2182 9 1.39E-03 **** 1. 61E+OO T 0 1276.52 6 14 0.56 2553.25 2542 14 1.64E-03 **** 1. 41E+OO 0 1289.30 15 16 0.54 2578.80 2572 16 4.17E-03 **** 1. 39E+OO . 0 1314.43 9 1 0.95 2629.03 2626 6 2.40E-03 80.9 1.37E+OO 0 1728.71 14 3 4.93 3457.09 3450 13 4.14E-03 71. 8 1. 05E+OO Flags: "T" = Tentatively associated Page 4590 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:47:07.28 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * * . DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235072.CNF;l * *Acquisition date 3-0CT-2016 06:45:49 Sensitivity 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
  • Sample date 15-DEC-2015 13:35:00 Nuclide Library : SOLID *
  • Sample ID G405235072 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity : 1.6611E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File. : DKAlOO: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CS-135 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM l.406E-01 8.585E-02 2.533E-02 2. 472E-01 3.519E-02 4. 372E-02 4.342E-02 4. 372E-02 3.776E-01 4. 372E-02 8.976E-02 8.976E-02 3.519E-02 4.370E-02 8.976E-02 3.386E-01 4.370E-02 9.434E-02 3.386E-01 1.991E-02 1.607E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 Page 4591of5809 Le (pCi/GRAM 8.155E+OO 3.287E-02 O.OOOE+OO 2.061E-02 2.388E-01 O.OOOE+OO O.OOOE+OO 5.198E-02 2.826E-01 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4592 of 5809 2.743E-02 3.595E-01 2.907E+OO 2.710E-02 1.266E-01 1.651E+OO 1. 27 4E+OO O.OOOE+OO 1.277E-01 O.OOOE+OO O.OOOE+OO 3.766E-01 4.265E+OO 4.178E-01 O.OOOE+OO 1.492E-01 3.779E+02 2.602E-02 5.198E-01 1.427E+OO 9.471E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.087E-02 3.656E-02 2.974E+OO 3.055E-01 3.055E-01 1. 8 68E-02 5.898E-01 6.425E-02 l.590E-01 O.OOOE+OO 0.000E+OO 7. 963E-02 1.471E+OO 6.475E-02 1.604E+02 O.OOOE+OO O.OOOE+OO 4.634E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.853E-02 O.OOOE+OO 4.023E-02 O.OOOE+OO O.OOOE+OO 2. 372E-02 2.506E-02 6.610E-02 O.OOOE+OO O.OOOE+OO 1.136E+Ol O.OOOE+OO 2.192E-01 3.847E-02 3.323E+OO 2.983E-02 O.OOOE+OO 5.069E+02 O.OOOE+OO l.698E-02 5. 611E-02 9.333E-02 8.022E-02 6.644E-02 1.075E+OO 4.044E-02 3.039E+OO 1.246E-01 5.093E-02 1. 703E-02 2.861E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT.

TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4593 of 5809 7.289E-01 6.338E-01 l.658E+Ol 6.226E+01 2.790E-01 l.556E+OO 3.155E-02 3.677E-01 4.441E-01 4. 834&-01 2.954E-01 3.830E-01 l.533E-01 l.533E-01 3.076E-01 3.275E-01 3.830E-Ol 4.437E-02 l.485E-01 3.322E+OO 4.437E-02 O.OOOE+OO l.436E-01 l.926E+02 3.388E-02 5. 572E-02 4.350E-02 2.282E-02 2.600E-02 7.742E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:47:13.24 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235072.CNF;l *
  • Acquisition date 3-0CT-2016 06:45:49 Sensitivity : 3.000 *
  • Detector ID GAM05 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.62 Half life ratio : ***** *
  • Sample date 15-DEC-2015 13:35:00 Nuclide Library : SOLID *
  • Sample ID G405235072 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity 1.6611E+02 GRAM *
  • Quantity Err(%) 1.2040E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 4-SEP-2016 08:00:28 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM05 CAN.CNF;20
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1.496E+Ol 1.642E+00 l.642E+00 CS-135 4.157E-01 2.546E-01 2.546E-01 TL-208 2.973E-01 6.217E-02 6.217E-02 PB-210 7.609E-01 7.790E-01 7.790E-01 PB-212 9.286E-01 l.137E-01 l.137E-01 BI-214 9.856E-01 1. 551E-01 l.551E-01 PB-214 1.097E+OO 1. 569E-01 1.569E-01 RN-222 9.856E-01 1. 551E-01 1.551E-01 RA-224 1.119E+OO 1.384E+OO 1.384E+OO RA-226 9.856E-01 1. 551E-01 1. 551E-01 AC-228 1.007E+OO 2.449E-01 2.449E-01 RA-228 1.007E+OO 2.449E-01 2.449E-01 TH-228 9.286E-01 l .137E-01 l.137E-01 TH-230 9.853E-01 1.550E-01 1.550E-01 TH-232 l.007E+OO 2.449E-01 2.449E-01 TH-234 l.421E+OO 1.188E+OO l.188E+00 U-234 9.853E-01 l.550E-01 1.550E-01 U-235 2.542E-01 2.547E-01 2.547E-01 U-238 1. 421E+OO 1.188E+OO 1.188E+OO AM-243 8.156E-02 6.176E-02 6.176E-02 ANH-511 1.060E-01 6.381E-02 6.381E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-s.igma) ( 1. 96-sigma) BE-7 1.787E+OO 8.867E+OO 8.903E+OO NOT IDENT. NA-22 2.279E-03 3.783E-02 3.784E-02 NOT IDENT. NA-24 -l.OOOE+41 6.140E+41 O.OOOE+OO SHORT HLIF AL-26 1.227E-02 l.988E-02 2.064E-02 NOT IDENT. SC-46 8.697E-03 2.843E-01 2.843E-01 FAIL ABUN V-48 -3.004E+03 8.279E+03 8.389E+03 SHORT HLIF CR-51 1.607E+02 2.746E+02 2.840E+02 SHORT HLIF MN-54 3.214E-02 5.680E-02 5.862E-02 NOT IDENT. C0-56 -3.013E-01 3.807E-01 4.042E-01 NOT IDENT. Page 4594 of 5809 MN-56 -l.OOOE+41 l.251E+41 0.000E+OO SHORT HLIF C0-57 -7.065E-03 3.012E-02 3.029E-02 NOT IDENT. C0-58 -l.845E-02 4.293E-01 4.294E-01 NOT IDENT. FE-59 5.799E-02 3.309E+OO 3.309E+OO NOT IDENT. C0-60 -3.315E-03 3.259E-02 3.262E-02 NOT IDENT. ZN-65 -l.151E-02 l.671E-01 1.672E-01 NOT IDENT. GE-68 -3.516E-01 l.942E+OO l.949E+OO NOT IDENT. AS-73 -4.905E-01 l.328E+OO 1.347E+OO NOT IDENT. AS-74 -5. 819E+02 3.861E+03 3.870E+03 SHORT HLIF SE-15 4.661E-02 l.536E-01 J..551E-01 NOT IDENT. BR-77 2.099E+37 l.773E+38 O.OOOE+OO SHORT HLIF SR-82 -2. 272E+01 4.614E+02 4.616E+02 SHORT HLIF RB-83 4.759E-02 4.162E-01 4.167E-01 NOT IDENT. KR-85 1. 969E+OO 4.955E+OO 5.034E+OO NOT IDENT. SR-85 1.918E-01 4.857E-01 4.933E-01 NOT IDENT. RB-86 -6 .119E+03 l.884E+04 1.904E+04 SHORT HLIF Y-88 -1.090E-01 2.183E-01 2.238E-01 NOT IDENT. Y-91 -2.568E+02 4.757E+02 4. 896E+02 NOT IDENT. NB-94 l.808E-02 2.784E-02 2.901E-02 NOT IDENT. NB-95 2.038E-01 6.382E-01 6.448E-01 NOT IDENT. NB-95M -4.897E-01 1. 833E+OO 1. 847E+OO NOT IDENT. ZR-95 2.356E-01 1. 072E+OO 1.077E+OO NOT IDENT. NB-97 -l.OOOE+41 1. 968E+41 O.OOOE+OO SHORT HLIF ZR-97 1. OOOE+41 l.325E+41 0.000E+OO SHORT HLIF M0-99 -7.353E+30 2.201E+31 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 3.351E+41 O.OOOE+OO SHORT HLIF RH-101 3.333E-03 2.231E-02 2.236E-02 NOT IDENT. RH-102 -1.997E-02 5.076E-02 5.155E-02 NOT IDENT. RU-103 -2.317E+OO 3.671E+OO 3.816E+OO FAIL ABUN RH-106 l.885E-01 3.465E-01 3.568E-01 NOT IDENT. RU-106 l.885E-01 3.465E-01 3.568E-01 NOT IDENT. AG-108M 4.047E-03 2. OllE-02 2.019E-02 NOT IDENT. CD-109 5.695E-01 6.907E-01 7.369E-01 NOT IDENT. AG-llOM -1. 771E-02 8.051E-02 8.091E-02 NOT IDENT. SN-113 4.927E-02 1.683E-01 l.697E-01 NOT IDENT. CD-115 -7.590E+37 2.980E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -2.330E+04 4.900E+04 5.012E+04 SHORT HLIF TE-123M -4.039E-02 9.132E-02 9.312E-02 NOT IDENT. SB-124 1.260E+OO l.347E+OO 1.462E+OO NOT IDENT. SB-125 -9.854E-03 7.258E-02 7.271E-02 FAIL ABUN TE-125M 1. 4 7 5E+02 l.609E+02 1.741E+02 NOT IDENT. I-126 3.973E+05 5.330E+05 5.623E+05 SHORT HLIF SB-126 -3.384E+05 5.902E+05 6. 096E+05 SHORT HLIF SN-126 1.150E-01 4.929E-02 7.154E-02 FAIL ABUN SB-127 -2. 051E+21 5.457E+21 O.OOOE+OO SHORT HLIF I-131 -2.296E+09 1. 964E+09 2.220E+09 SHORT HLIF I-132 -l.OOOE+41 4.913E+42 0.000E+OO SHORT HLIF TE-132 -3.787E+24 6.032E+25 O.OOOE+OO SHORT HLIF BA-133 2.171E-02 6.400E-02 6.474E-02 FAIL ABUN I-133 -1.000E+41 2.727E+41 O.OOOE+OO SHORT HLIF CS-134 1.934E-02 4.462E-02 4.546E-02 NOT IDENT. I-135 -1. OOOE+41 l.232E+42 O.OOOE+OO SHORT HLIF CS-136 -l.560E+04 l.591E+05 1.592E+05 SHORT HLIF BA-137M 1.507E-02 2.502E-02 2.593E-02 NOT IDENT. CS-137 l.592E-02 2.644E-02 2.739E-02 NOT IDENT. CE-139 2.238E-03 7.297E-02 7.298E-02 NOT IDENT. BA-140 3.949E+04 6.730E+05 6.733E+05 SHORT HLIF LA-140 -l.564E+05 2.748E+05 2.837E+05 SHORT HLIF CE-141 -1.611E+OO l.546E+Ol 1.547E+Ol NOT IDENT. CE-143 l.OOOE+41 5.853E+40 O.OOOE+OO SHORT HLIF CE-144 5 .135E-02 2.338E-01 2.349E-01 NOT IDENT. PM-144 3.495E-02 3.904E-02 4.210E-02 NOT IDENT. PR-144 3.00lE+OO 3.372E+OO 3.634E+OO NOT IDENT. PM-146 5.918E-03 3.232E-02 3.243E-02 NOT IDENT. ND-147 -5.677E+06 l.882E+07 1.900E+07 SHORT HLIF PM-147 l.777E+02 5.317E+02 5.377E+02 NOT IDENT. PM-149 -2.357E+39 4.140E+39 O.OOOE+OO SHORT HLIF EU-150 -1.169E-03 2.218E-02 2.218E-02 FAIL ABUN EU-152 2.161E-03 6.020E-02 6.021E-02 FAIL ABUN GD-153 -1. 761E-02 1.003E-01 1.006E-01 NOT IDENT. EU-154 3.650E-03 9.267E-02 9.269E-02 NOT IDENT. EU-155 3.248E-02 6.844E-02 6.999E-02 FAIL ABUN TB-160 2.444E-01 1.373E+OO 1.378E+OO FAIL ABUN H0-166M 3.751E-03 4.616E-02 4.619E-02 FAIL ABUN TM-171 6.665E-01 3.033E+OO 3.047E+OO NOT IDENT. HF-172 -5.775E-02 1. 399E-01 1.423E-01 FAIL ABUN LU-172 3.043E-02 6.988E-02 7.122E-02 FAIL ABUN LU-176 9.729E-03 1.884E-02 1.934E-02 NOT IDENT. Page 4595 of 5809 HF-181 9.718E-01 3. 072E+OO 3.103E+OO NOT IDENT. TA-182 l.802E-01 8.173E-01 8.213E-01 FAIL ABUN RE-183 2.070E-01 6.322E-01 6.390E-01 NOT IDENT. RE-184 -1.943E+OO 2.032E+Ol 2.034E+Ol NOT IDENT. W-188 5.085E-01 7.919E+Ol 7.919E+Ol FAIL ABUN IR-192 l.880E-01 3.031E-01 3.147E-01 FAIL ABUN HG-203 1.047E+OO 1.697E+OO 1. 761E+OO FAIL ABUN BI-207 -6.739E-04 3.605E-02 3.605E-02 FAIL ABUN BI-211 3.023E+OO 4.349E-01 1.430E+OO FAIL ABUN PB-211 6.997E-02 5.292E-01 5.302E-01 NOT IDENT. BI-212 1.264E+OO 6.063E-01 8.319E-01 FAIL ABUN RN-219 5.616E-02 3.178E-01 3.188E-01 FAIL ABUN RA-223 -2.212E-02 4.977E-01 4.978E-01 FAIL ABUN AC-227 7.335E-02 l.822E-01 .l.852E-01 FAIL ABUN TH-227 7.335E-02 1.822E-01 1.852E-01 FAIL ABUN TH-229 l.201E-01 3.343E-01 3.386E-01 FAIL ABUN PA-231 6.946E-02 4.095E-01 4.107E-01 NOT IDENT. TH-231 -2.212E-02 4.977E-01 4.978E-01 FAIL ABUN PA-233 7.768E-03 5.146E-02 5.158E-02 FAIL ABUN PA-234 -l.275E-01 2.555E-01 2.619E-01 FAIL ABUN PA-234M -5.074E-01 3.779E+OO 3.786E+00 NOT IDENT. NP-237 7.768E-03 5.146E-02 5.158E-02 FAIL ABUN NP-238 -5.538E+39 3.830E+40 O.OOOE+OO SHORT HLIF NP-239 2. 872E-02 1.519E-01 1.524E-01 FAIL ABUN PU-239 l.050E+02 2.002E+02 2.058E+02 NOT IDENT. AM-241 3.381E-03 3.674E-02 3.677E-02 NOT IDENT. CM-243 -2.971E-02 6.142E-02 6.287E-02 FAIL ABUN BK-247 3.738E-03 5.418E-02 5. 421E-02 NOT IDENT. CM-247 -2.302E-02 2.780E-02 2. 968E-02 FAIL ABUN CF-249 9. 972E-03 2.727E-02 2.764E-02 NOT IDENT. CF-251 1.083E-02 8.531E-02 8.545E-02 NOT IDENT. Page 4596 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 60.3801 87.09 70.2527 136.47 65.2058 45.60 70.4172 87.57 86.1620 140.51 0.0000 46.54 70.6720 88.03 86.2592 143.76 49.9415 49.72 0.0000 88.34 86.3242 144.24 49.9825 51.35 66.4043 88.47 86.3519 145.44 55.3566 51. 87 60.1914 89. 96 81.3584 152.43 67.0061 52.39 60.3022 1093.63 81. 4918 153.25 0.0000 52.97 59.6297 91.11 0.0000 323.87 70.2094 53.44 70.0804 92.59 81. 8708 156.02 0.0000 54.07 71. 8296 93.35 82.0175 158.56 0.0000 57.36 0.0000 94.56 69.1376 159.00 72.7734 57.53 79.1330 94.65 69.1523 162.33 60. 9631 57.98 81. 6761 94.67 69.1553 162.66 0.0000 59.27 98.5324 94.87 69.1871 163.33 76.3229 59.32 98.5486 97.43 78.2955 165.86 58.2333 59.54 88.8650 98.43 85.6890 176.31 65.3811 60. 96 100.1561 98.44 85.6908 176.60 0.0000 61.17 98.0438 99.53 81. 3805 177.52 63.4173 62.93 95.3001 100 .11 77.8647 181.07 0.0000 63.29 95.4065 102.03 71. 8318 181.52 59.6032 63.58 95.4919 103.18 97.5369 184.41 59.8493 64.28 95.6970 103.37 86.6337 143.76 59.9606 66.73 108.5971 105.21 74.1620 193.51 53.1693 67.24 101.5478 105.31 76.9254 197.03 55.5610 125.81 96.6794 106.12 77.0594 198.01 57.7738 67.75 105.8685 106.47 97.3144 201.83 55.9181 69.67 117.3634 109.28 67.4177 203.43 51.7258 70.83 103.1752 111. 00 88.0507 205.31 51.8540 72. 81 106.0101 111. 76 0.0000 210.85 55.1283 72. 87 106.0283 114. 06 74.6143 215.65 58.0197 74.66 106.5561 116.30 0.0000 222.11 56.2801 74.82 106.6030 116.74 66.5788 227.09 61. 0643 74.97 106.6469 119.76 57.5440 227.38 52.2001 77 .11 107.2694 121.12 65.2639 228.16 0.0000 78.74 107.7380 121.22 65.2766 228.18 47.8042 79.69 108.0086 121. 78 64.4001 116.74 47.8042 80.12 108 .1300 122.06 71. 0684 235.69 61.3190 80.19 0.0000 122.92 60.7456 235. 96 61. 3390 80.57 108.2572 123.07 56.9655 238.63 57.4030 81. 00 108.3786 265.00 61. 7845 238.98 0.0000 81. 07 108.3987 125.81 65.8530 240.99 57.5602 81. 75 108.5890 127.23 70.8133 242.00 57.6279 83.79 69.6753 127.91 65.1549 244.70 57.8061 84.00 69. 7125 129.30 63.4017 252.40 0.0000 85.43 69. 9640 131.20 76.1564 252.80 44.6099 86.55 70.1593 133.02 58.9997 254.15 0.0000 86.79 70.2008 133. 52 65.8293 256.23 38.2731 86.94 70.2271 136.00 56.3999 260.90 0.0000 Page 4597 of 5809

ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 14.5811 1274.44 18.4863 1620.50 6.3875 766.42 17.8260 1001.03 18. 6961 1621.92 3.1"948 766.84 19.4502 1002.74 19.5984 1678.03 0.0000 772.60 0.0000 1004.73 17.8290 1690.97 1.0821 776.52 0.0000 507.63 b.0000 1750.46 0.0000 739.50 .o. 0000 1025.87 0.0000 1764.49 0.0000 778.90 8.6914 1028.54 0.0000 1063.66 4.4053 783.70 0.0000 1037.84 10.8230 1771.35 0.0000 785.37 8.7165 1038.76 0.0000 1791.20 0:0000 792.07 21. 3091 631. 29 12.6653 1808.65 1.1105 794.95 19.6948 1048.07 0.0000 1810.72 0.0000 795.86 19.7029 1049.04 12.6764 1836.06 7.8190 810.06 15.4190 1050.41 10.8706 810.29 16.5216 1063.66 12.7396 344.28 16.5228 1077.00 0.0000 810.76 15.4236 1077.34 16.4564 815.77 0.0000 1085.87 12.8362 1048.07 o. *oooo 1093.63 4.4124 832 .-01 28.9030 1099.45 6.4471 834.85 17.8079 1112. 07 16. 6476' 835. 71 20.0413 1112.84 14.8008 836.80 0.0000 1115. 54 17.7773 846.75 0.0000 1120.29 14.8369 84El.77 19.0150 1120.55 14.8389 856.80 0.0000 1221.41 10. 38.93 860.56 7.8744 1129.67 14.8828 871. 09 16.9458 1131.51 0.0000 873.19 15.2644 1147. 95 0.0000 875.33 0.0000 1173.23 16.0330 879.38 10.2015 1177.95 18.8904 880.51 8.5052 1189.05 18.9563 883.24 18.1641 1204.77 24.7622 884.68 15.9027 1221.41 18.1871 '889.28 13.6563 1231. 02 22.0805 894.76 12.5451 1235.36 0.0000 898.04 17.1295 1238.28 17.3177 900. 72 5.7157 1260.41 0.0000 903.28 13.7314 1271.87 10.8828 911.20 16.0701 1274.44 11.6689 912.08 16.0753 1274.54 11. 668 9 923.98 0.0000 1291.59 14.6585 926.50 13.8560 1298.22 0.0000 929 .11 13.8696 .1312 .11 0.0000 937.49 16.2331 1332.49 9.8865 944 .13 0.0000 1362. 66 0.0000 946.00 15.1222 1365.19 2.9930 949.00 8.1519 1368.63 0.0000 667.71 0.0000 1384.29 4. 0115 962. 31 9. 8311 1408. 01 10.0928 964.08 16.6888 1457.56 0.0000 966.17 16.7015 1460.82 3.0701 911.20 16.7189 1489.16 6.1853 968. 97 16.7189 1505.03 7.2452 983.53 0.0000 1584.12 13. 7197 ,.*, 984.45 0.0000 '1596.21 0.0000 Page 4599 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:47:44.50 ******************************************************************************** *

  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235073.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM06.CNF;499 Background date : Z-OCT-2016 11:00:12. Sample date 11-DEC-2015 11:35:00 Acquisition date : 3-0CT-2016 06:46:12. Sample ID G405235073 Sample quantity 1.47132E+02 GRAM Detector name : GAM06 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.59 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4600 of 5809 Energy 51. 75 74.82* 77.25 87.33 92.75* 99.04 128.86 185.91* 209.20 238.64* 242.05* 270.26* 295.16* 310.56 331.22 338.20 351.84 369.32 449.15 463.46* 510.24* 535.74 557.39 583.02* 609.08* 633.92 646.75 660.92 688.74 791.58 794.51 852.07 886.86 900 .11 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 14 46 136 65 52 25 33 67 26 258 45 50 124 22 8 49 221 14 16 27 49 47 12 107 156 19 16 39 10 6 12 8 19 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 123 201 125 124 103 67 68 121 64 129 66 34 82 20 33 33 26 12 7 13 37 25 10 23 12 6 9 12 5 6 4 14 7 9 0.49 0.75 0.78 0.91 1.11 1. 33 0.70 1.15 0.79 1. 07 0.88 1. 59 0.99 1.15 1. 51 1. 21 1.16 1. 07 1. 02 2.26 2 .11 6.71 0.79 1. 39 1. 49 1. 96 1. 01 0.78 1. 53 1. 43 2.04 1. 00 2.47 0.85 103.23 149.34 154.19 174.34 185.17 197.74 257.33 371.34 417. 89 476.72 483.54 539.93 589.69 620.48 661. 7 6 675.72 702.98 737.93 897.49 926.09 1019.62 1070.60 1113.88 1165 .12 1217. 21 1266.87 1292.52 1320.86 1376.48 1582 .11 1587. 96 1703.05 1772.63 1799.12 102 147 152 170 182 196 255 366 415 473 481 536 585 617 659 672 698 735 894 922 1009 1061 1110 1157 1211 1262 1287 1315 1374 1578 1584 1696 1765 1795 8 3.90E-03140.5 6 1.29E-02 50.4 5 3.77E-02 15.2 8 1.81E-02 32.3 7 1. 44E-02 35. 8 6 6.86E-03 55.6 6 9.25E-03 42.5 11 1. 87E-02 34. 8 7 7.25E-03 54.2 9 7.16E-02 10.2 7 1. 25E-02 35. 6 9 1.38E-02 26.3 11 3.45E-02 16.9 8 6.llE-03 41.2 7 2.09E-03134.2 7 1.36E-02 24.2 11 6.14E-02 8.1 6 3.89E-03 47.4 7 4.35E-03 37.9 8 7.38E-03 32.1 19 1. 35E-02 38 .1 20 1.30E-02 30.0 10 3.26E-03 58.5 16 2.98E-02 14.2 12 4.34E-02 9.4 9 5.21E-03 33.8 12 4.57E-03 43.8 10 1.07E-02 23.4 6 2.86E-03 45.3 7 1. 64E-03 83. 2 8 3.33E-03 40.8 11 2.33E-03 92.2 15 5.41E-03 37.8 8 2.34E-03 68.3 Fit Peak Search Report (continued) Page : 2 Sample ID : G405235073 Acquisition date 3-0CT-2016 06:46:12 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 911.13* 44 28 1. 48 1821.17 1814 14 l.22E-02 29.9 36 0 992.50 11 2 1. 62 1983.90 1979 9 3.00E-03 39.3 37 0 1070.25 12 6 0.69 2U9. 39 2132 12 3.33E-03 50.0 38 0 1119.91* 43 12 2.23 2238.72 2233 15 1. 21E-02 22.9 39 0 1139.80 12 0 1. 04 2278.50 2274 8 3.33E-03 28.9 40 0 1192. 44 10 3 0.89 2383.80 2381 6 2.65E-03 46.6 41 0 1200.72 10 14 0.93 2400.35 2395 9 2.82E-03 72 .5 42 0 1302.42 10 3 1. 36 2603.78 2600 9 2.90E-03 40.8 43 0 1310.46 4 3 1. 25 2619.88 2616 6 l. llE-03 84.8 44 0 1376.95 15 5 2.66 2752.88 2747 10 4.18E-03 37.9 45 0 1459.92* 256 0 2.14 2918.87 2912 15 7.lOE-02 6.3 Flag: "*" = Peak area was modified by background subtraction Page 4601 of 5 809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 07:47:46 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235073.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID ll-DEC-2015 11:35:00 G405235073 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:46:12 147.13 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA6 0 01:00:00.00 1.50 keV No Empirical 75.00 Interference Report Interfering Nuclide Page 4602 of 5809 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 PB-214 Line 242.00 87.09 87.09 87.09 74.82 74.82 74.82 351. 93 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide RA-224 SN-126 SN-126 CD-109 AM-243 TH-228 PB-212 BI-211 Line 240.99 86.94 87.57 88.03 74.66 74.82 74.82 351.06 CAN 0 01:00:00.59 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235073 Acquisition date 3-0CT-2016 06:46:12 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10. 66* .. 1.005E+OO 1.172E+Ol 1.172E+Ol 12.65 OK CD-109 88.03 3.70* 5.207E+OO 1.249E+OO 1.951E+OO 112.90 OK SN-126 64.28 9.60 2.772E+OO Line Not Found Absent 86.94 8.90 5.207E+OO 5.194E-01 5.194E-01 112. 90 OK 87.57 37.00* 5.207E+OO 1.249E-01 1. 249E-01 112. 90 OK BA-137M 661.66 89.90* 2.029E+OO 1.127E-01 l.149E-01 46. 89 OK CS-137 661.66 85.10* 2.029E+OO 1.191E-01 l.213E-01 46. 89 OK TM-171 51. 35 0.27 1.144E+OO 3.006E+Ol 4.031E+Ol 280.95 OK 52.39 0.47* 1.144E+OO 1. 727E+Ol 2.315E+Ol 280.95 OK 66.73 0.14 3.097E+OO Line Not Found Absent TL-208 277.37 6.60 3.958E+OO Line Not Found Absent 583.19 85.00* 2.244E+OO 3.026E-01 3.026E-01 28.44 OK 860.56 12.50 1.624E+OO Line Not Found Absent BI-211 72. 87 1. 23 3.859E+OO Line Not Found Absent 351.06 12.92* 3.304E+OO 2.408E-01 2.408E-01 393.74 OK PB-212 74.82 10.28 4.080E+OO 1.643E-01 1.643E-01 448.58 OK 77 .11 17.10 4.339E+OO 1.172E+OO 1.172E+OO 30.49 OK 238.63 43.60* 4.429E+OO 7.792E-01 7.792E-01 20.34 OK 300.09 3.30 3.729E+OO -----Line Not Found Absent BI-214 609.32 45.49* 2.167E+OO 8.485E-01 8.488E-01 18.87 OK 1120.29 14.92 1.280E+OO 1.149E+OO 1.149E+OO 45.81 OK 1764.49 15.30 8.592E-01 Line Not Found Absent PB-214 74.82 5.80 4.080E+OO Line Not Found <<INT Reject 77 .11 9.70 4.339E+OO 2.067E+OO 2.067E+OO 30.49 OK 87.09 3.41 5.190E+OO Line Not Found <<INT Reject 242.00 7.25 4.383E+OO 8.248E-01 8.251E-01 71. 23 OK 295.22 18.42 3.776E+OO 1.022E+OO 1.022E+OO 33.83 OK 351. 93 35.60* 3.304E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.167E+OO 8.485E-01 8.488E-01 18.87 OK 1120. 29 14.92 1.280E+OO 1.149E+OO 1.149E+OO 45.81 OK 1764.49 15.30 8.592E-01 Line Not Found Absent RA-226 609.32 45.49* 2.167E+OO 8.485E-01 8.488E-01 18.87 OK 1120.29 14.92 1.280E+OO 1.149E+OO 1.149E+OO 45.81 OK 1764.49 15.30 8.592E-01 Line Not Found Absent TH-228 74.82 10.28 4.080E+OO 1.643E-Ol 1.643E-01 448.58 OK 77 .11 17.10 4.339E+OO 1.172E+OO 1.172E+OO 30.49 OK 238.63 43.60* 4.429E+OO 7.792E-01 7.792E-01 20.34 OK 300.09 3.30 3.729E+OO Line Not Found Absent TH-230 609.32 45.49* 2.167E+OO 8.485E-01 8.485E-01 18.87 OK 1120.29 14.92 1.280E+OO 1.149E+OO 1.149E+OO 45.81 OK 1764.49 15.30 8.592E-01 Line Not Found Absent PA-233 300.13 6.63 3.729E+OO Line Not Found Absent 311. 90 38.50* 3.633E+OO 8.967E-02 8.967E-02 82.32 OK 340.48 4.45 3.388E+OO Line Not Found Absent U-234 609.32 45.49* 2.167E+OO 8.485E-01 8.485E-01 18.87 OK 1120.29 14.92 1.280E+OO 1.149E+OO 1.149E+OO 45.81 OK 1764.49 15.30 8.592E-01 Line Not Found Absent AM-243 43.53 5.90 3.924E-01 Line Not Found Absent 74.66 67.20* 4.080E+OO 2. 513E-02 2.513E-02 448.58 OK Page 4603 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235073 Acquisition date Page : 3 3-0CT-2016 06:46:12 Nuclide Type: Nuclide ANH-511 Energy 511. 00 Uncorrected Decay Corr 2-Sigma %Abn %Eff pCi/GRAM pCi/GRAM %Error 100.00* 1.065E-01 l.065E-01 76.26 Flag: "*" = Keyline Page 4604 of 5809 Status <OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:47:47.99 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235073.CNF;l *
  • Acquisition date 3-0CT-2016 06:46:12 Sensitivity 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 11-DEC-2015 11:35:00 Analyst initials: MXRl *
  • Sample ID G405235073 Sample Quantity 1.4713E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.172E+Ol 1.453E+OO 3.547E-01 CD-109 1. 951E+OO 2.159E+OO 1. 951E+OO SN-126 1.249E-01 l.382E-01 l.228E-01 BA-137M l.149E-01 5.278E-02 5.898E-02 CS-137 1.213E-01 5.576E-02 6.230E-02 TM-171 2.315E+Ol 6.375E+Ol 4.934E+Ol TL-208 3.026E-01 8.434E-02 6.034E-02 BI-211 2.408E-01 9.291E-01 3.185E-01 PB-212 7.792E-01 l.553E-01 1.161E-01 BI-214 8.488E-01 1.570E-01 1.143E-01 PB-214 1.059E+OO l.688E-01 3.281E-01 RN-222 8.488E-01 1. 570E-01 l.143E-01 RA-226 8.488E-01 l.570E-01 1.143E-01 TH-228 7.792E-01 1.553E-01 l.161E-01 TH-230 8.485E-01 1.569E-01 1.142E-01 PA-233 8. 967E-02 7.234E-02 1.018E-01 U-234 8.485E-01 1.569E-01 1.142E-01 AM-243 2. 513E-02 1.105E-01 l .141E-01 ANH-511 l.065E-01 7. 960E-02 3.925E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM. (1. 96-sigma) (pCi/GRAM BE-7 8. 696E+OO 1.169E+Ol 2.505E+Ol NOT IDENT. NA-22 -l.775E-02 4.616E-02 8.688E-02 NOT IDENT. NA-24 0.000E+OO 1.635E+41 0.000E+OO SHORT HLIF AL-26 2. 272E-03 2.651E-02 6.166E-02 NOT IDENT. SC-46 -6.740E-02 3.432E-01 5.695E-Ol FAIL ABUN V-48 O.OOOE+OO 1.291E+04 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.847E+02 O.OOOE+OO SHORT HLIF MN-54 -3.033E-02 6.419E-02 l.124E-01 NOT IDENT. C0-56 5.099E-01 4. 371E-Ol 9.806E-Ol NOT IDENT. MN-56 O.OOOE+OO 8.573E+40 0.000E+OO SHORT HLIF C0-57 1.696E-02 4.361E-02 8.630E-02 NOT IDENT. Page 4605 of 5809 C0-58 l.609E-01 4. 722E-01 l.002E+OO NOT IDENT. FE-59 -l.564E+OO 6.316E+OO l.234E+Ol NOT IDENT. C0-60 -3.295E-02 3.972E-02 6.599E-02 NOT IDENT. ZN-65 5.307E-04 l.680E-01 3.065E-01 NOT IDENT. GE-68 2.602E+OO 2.179E+OO 5.324E+OO NOT IDENT. AS-73 -2.331E-01 9.750E+OO 1. 968E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.774E+03 O.OOOE+OO SHORT HLIF SE-75 -7.990E-03 2.025E-01 3.699E-01 NOT IDENT. BR-77 O.OOOE+OO l.155E+37 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.647E+02 O.OOOE+QO SHORT HLIF RB-83 -l.123E-01 5.074E-01 9.878E-01 NOT IDENT. KR-85 -3.848E-01 6.623E+OO l.162E+Ol NOT IDENT. SR-85 -4.215E-02 6.774E-01 l.188E+OO NOT IDENT. RB-86 O.OOOE+OO 2.367E+04 O.OOOE+OO SHORT HLIF Y-88 -l.404E-01 1. 589E-01 l .151E-01 NOT IDENT. Y-91 -3.265E+02 6.517E+02 l.005E+03 NOT IDENT. NB-94 l.304E-02 3.285E-02 6.642E-02 NOT IDENT. NB-95 l.190E-01 9.777E-01 l.864E+OO NOT IDENT. NB-95M -6.651E-01 2.687E+OO 4.366E+OO NOT IDENT. ZR-95 l.326E+OO 1. 2 91E+OO 2.944E+OO NOT IDENT. NB-97 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 8.735E+40 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 8.205E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -1. 8 61E-02 3.015E-02 4.965E-02 NOT IDENT. RH-102 -6.297E-03 5.049E-02 8.819E-02 NOT IDENT. RU-103 -8.989E-01 4.454E+00 8.685E+OO FAIL ABUN RH-106 2.00lE-02 4.138E-Ol 8.320E-01 NOT IDENT. RU-106 2.00lE-02 4.138E-01 8.320E-01 NOT IDENT. AG-108M 4.304E-03 2.572E-02 5.224E-02 NOT IDENT. AG-llOM l.059E-01 8.914E-02 2.134E-01 NOT IDENT. SN-113 l.026E-02 2.061E-01 4.143E-01 NOT IDENT. CD-115 O.OOOE+OO l.328E+39 O.OOOE+OO SHORT HLIF SN-ll 7M O.OOOE+OO 7.269E+04 O.OOOE+OO SHORT HLIF TE-123M 3.409E-03 l.157E-01 2.195E-01 NOT IDENT. SB-124 -8.150E-01 l.521E+OO 2. 718E+OO FAIL ABUN SB-125 -6.022E-02 9.465E-02 l.733E-01 FAIL ABUN TE-125M -9.234E+Ol 2.202E+02 4 .110E+02 NOT IDENT. I-126 O.OOOE+OO 6.546E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.454E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 9.494E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.288E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 2.039E+26 0.000E+OO SHORT HLIF BA-133 2.086E-02 3.330E-02 6.795E-02 NOT IDENT. I-133 O.OOOE+OO l.833E+41 O.OOOE+OO SHORT HLIF CS-134 5.532E-02 4.427E-02 8.943E-02 FAIL ABUN CS-135 -l.763E-03 l.382E-01 2.338E-01 NOT IDENT. I-135 O.OOOE+OO l.384E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.440E+05 O.OOOE+OO SHORT HLIF CE-139 -5.410E-02 l.057E-01 l.887E-01 NOT IDENT. BA-140 O.OOOE+OO l.016E+06 O.OOOE+OO SHORT HLIF LA-140 0.000E+OO 3.603E+05 O.OOOE+OO SHORT HLIF CE-141 -l.536E+Ol 1. 981E+Ol 3.480E+Ol NOT IDENT. CE-143 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CE-144 -4.808E-02 3 .135E-01 5.906E-01 NOT IDENT. PM-144 -9.689E-03 5.049E-02 9.524E-02 NOT IDENT. PR-144 -9.049E-01 4.368E+OO 8.218E+OO NOT IDENT. PM-146 l.883E-02 3.876E-02 8.210E-02 FAIL ABUN ND-147 O.OOOE+OO 2.894E+07 O.OOOE+OO SHORT HLIF PM-147 -4.483E+Ol 7.763E+02 l.479E+03 NOT IDENT. PM-149 O.OOOE+OO l.631E+40 O.OOOE+OO SHORT HLIF EU-150 -4.274E-03 3.054E-02 4.291E-02 FAIL ABUN EU-152 l.744E-02 8.992E-02 l.829E-01 NOT IDENT. GD-153 -3.497E-02 1. 467E-01 2.595E-01 NOT IDENT. EU-154 -3. 811E-02 l.146E-01 2.180E-01 NOT IDEN.T. EU-155 -l.597E-02 9.890E-02 l.885E-01 FAIL ABUN TB-160 8.000E-01 l.756E+OO 3.692E+OO FAIL ABUN H0-166M 2. 571E-02. 4.849E-02 l.042E-01 FAIL ABUN HF-172 8. 331E-02 2.164E-01 4.002E-01 FAIL ABUN LU-172 3.106E-03 7.922E-02 l.614E-01 FAIL ABUN LU-176 6.703E-04 2.094E-02 3.889E-02 FAIL ABUN HF-181 7.189E-01 3.657E+OO 7.486E+OO NOT IDENT. TA-182 5.694E-01 8.243E-01 l.874E+OO FAIL ABUN RE-183 -2. 721E-01 2.944E+OO 5.890E+OO NOT IDENT. RE-184 -5.328E+OO 3.591E+Ol 5.833E+Ol FAIL ABUN W-188 6.099E+Ol l.048E+02 l.943E+02 NOT IDENT. IR-192 -l.868E-01 4.035E-01 7.746E-01 FAIL ABUN Page 4606 of 5809 HG-203 -1.432E+OO 2 .133E+OO 3.553E+OO NOT IDENT. BI-207 -l.432E-02 5.007E-02 8.504E-02 FAIL ABUN PB-210 1.023E+OO 4.036E+OO 8.377E+OO NOT IDENT. PB-211 -l.584E-01 5.352E-01 1.040E+OO NOT IDENT. BI-212 6.776E-01 5.129E-01 1.148E+OO NOT IDENT. RN-219 2.059E-01 3.617E-01 7.623E-01 FAIL ABUN RA-223 2.992E-01 5.381E-01 1.139E+OO FAIL ABUN RA-224 O.OOOE+OO l.018E+OO l.435E+OO FAIL ABUN AC-227 -8.144E-02 2.328E-01 4.086E-01 NOT IDENT. TH-227 -8.144E-02 2.32BE-01 4.086E-01 NOT IDENT. AC-228 O.OOOE+OO 3.33BE-01 5 .196E-01 FAIL ABUN RA-228 0.000E+OO 3.338E-01 5 .196E-01 FAIL ABUN TH-229 -2.064E-01 4.488E-01 7.955E-01 FAIL ABUN PA-231 -4.488E-02 3.882E-01 7.737E-01 NOT IDENT. TH-231 2.992E-01 5.381E-01 1.139E+OO FAIL ABUN TH-232 O.OOOE+OO 3.338E-01 5 .196E-01 FAIL ABUN PA-234 9.156E-02 2.675E-01 5.775E-01 FAIL ABUN PA-234M 4.321E+OO 3.920E+OO 9.263E+OO NOT IDENT. TH-234 4.782E-01 1. 285E+OO 2.611E+OO FAIL ABUN U-235 4.420E-02 1.693E-01 3.279E-01 FAIL ABUN NP-237 8. 967E-02 7.234E-02 9. 272E-02 FAIL ABUN NP-238 O.OOOE+OO 1.677E+41 O.OOOE+OO SHORT HLIF U-238 4.782E-01 1.285E+OO 2.611E+OO FAIL ABUN NP-239 9.0lOE-02 l.844E-01 3.766E-01 FAIL ABUN PU-239 5.275E+02 4. 391E+02 6.095E+02 FAIL ABUN AM-241 -l.982E-02 l.405E-01 2.787E-01 NOT IDENT. CM-243 -4. 651E-02 8.880E-02 1.644E-01 FAIL ABUN BK-247 2.00lE-02 7.155E-02 l.357E-01 NOT IDENT. CM-247 4.746E-03 3.120E-02 6.345E-02 NOT IDENT. CF-249 3.557E-02 3.660E-02 7.976E-02 NOT IDENT. CF-251 1.450E-03 l.043E-01 l.962E-01 NOT IDENT. Page 4607 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:47:45.37 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 246 10.66* 1.005E+OO 1.172E+Ol 1.172E+Ol 12.65 CD-109 88.03 81 3.70* 5.207E+OO 2.144E+OO 3.349E+OO 64.52 SN-126 64.28 ------9.60 -2. 772E+OO ------Line Not Found ------86.94 81 8.90 5.207E+OO 8.915E-01 8.915E-01 64.52 87.57 81 37.00* 5.207E+OO 2.144E-01 2.144E-01 64.52 BA-137M 661. 66 40 89.90* 2.029E+OO 1.127E-01 1.149E-01 46.89 CS-137 661.66 40 85.10* 2.029E+OO 1.191E-01 1. 213E-01 46.89 TM-171 51. 35 18 0.27 1.144E+OO 3.006E+Ol 4.031E+Ol 280.95 52.39 18 0.47* 1.144E+OO 1.727E+Ol 2.315E+Ol 280.95 66.73 ------0.14 3.097E+OO ------Line Not Found ------TL-208 277.37 ------6.60 3.958E+OO ------Line Not Found ------583.19 113 85.00* 2.244E+OO 3.026E-01 3.026E-01 28.44 860.56 ------12.50 1.624E+00 ------Line Not Found ------BI-211 72.87 ------1.23 3.859E+OO ------Line Not Found ------351.06 244 12.92* 3.304E+OO 2.917E+00 2.917E+OO 16. 26 PB-212 *74. 82 59 10.28 4.080E+OO 7.121E-01 7 .121E-01 100.74 77 .11 170 17.10 4.339E+OO l.172E+OO 1. l 72E+OO 30.49 238.63 295 43.60* 4.429E+OO 7.792E-01 7.792E-01 20.34 300.09 ------3.30 3.729E+OO ------Line Not Found ------BI-214 609.32 164 45.49* 2.167E+OO 8.485E-01 8.488E-01 18.87 1120.29 43 14.92 1.280E+OO 1.149E+OO 1.149E+OO 45.81 1764.49 ------15.30 8.592E-01 ------Line Not Found ------PB-214 74.82 59 5.80 4.080E+OO 1.262E+OO 1.263E+OO 100.74 77 .11 170 9.70 4.339E+OO 2.067E+OO 2.067E+OO 30.49 87.09 81 3.41 5.207E+OO 2.327E+OO 2.327E+OO 64.52 242.00 51 7.25 4.383E+00 8.248E-01 8. 251E-01 71. 23 295.22 139 18.42 3.776E+OO 1.022E+00 1.022E+OO 33.83 351.93 244 35.60* 3.304E+OO 1.058E+OO 1.059E+OO 16.26 RN-222 609.32 164 45.49* 2.167E+OO 8.485E-01 8.488E-01 18.87 1120.29 43 14.92 1. 280E+OO 1.149E+OO 1.149E+00 45.81 1764.49 ------15.30 8.592E-01 ------Line Not Found ------RA-224 240.99 51 4.10* 4.383E+00 1.458E+OO 1.458E+OO 71 .. 23 RA-226 609.32 164 45.49* 2.167E+OO 8.485E-01 8.488E-01 18.87 1120.29 43 14.92 l.280E+00 1.149E+OO 1.149E+OO 45.81 1764.49 ------15.30 8.592E-01 ------Line Not Found ------TH-228 74.82 59 10.28 4.080E+OO 7.121E-01 7.121E-01 100.74 77 .11 170 17.10 4.339E+OO 1.172E+OO 1.172E+OO 30.49 238.63 295 43.60* 4.429E+OO 7.792E-01 7.792E-01 20.34 300.09 ------3.30 3. 729E+OO ------Line Not Found ------TH-230 609.32 164 45.49* 2.167E+OO 8.485E-01 8.485E-01 18.87 1120.29 43 14.92 1. 280E+OO 1.149E+OO 1.149E+OO 45.81 1764.49 ------15.30 8.592E-01 ------Line Not Found ------PA-233 300 .13 ------6.63 3.729E+OO ------Line Not Found ------311. 90 25 38.50* 3.633E+00 8. 967E-02 8.967E-02 82.32 340.48 ------4.45 3.388E+OO ------Line Not Found ------U-234 609.32 164 45.49* 2.167E+OO 8.485E-01 8.485E-01 18.87 1120.29 43 14.92 1. 280E+OO 1.149E+OO 1.149E+OO 45.81 Page 4608 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235073 Acquisition date Page : 2 3-0CT-2016 06:46:12 Nuclide Type: Nuclide Energy Area 1764.49. ------AM-243 43.53 ------74.66 59 ANH-511 511. 00 52 Flag: "*" Key line Page 4609 of 5809 %Abn %Eff 15.30 8.592E-01 5.90 3.924E-01 67.20* 4.080E+OO 100.00* 2.490E+OO Uncorrected Decay Corr 2-Sigma pCi/GRAM pCi/GRAM %Error ------Line Not Found ------------Line Not Found ------1. 089E-0 l 1.089E-01 100.74 1.065E-Ol 1.065E-01 76.26 Page : 3 Summary of Nuclide Activity Sample ID : G405235073 Acquisition date 3-0CT-2016 06:46:12 Total number of lines in spectrum 45 Number of unidentified lines 17 Number of lines tentatively identified by NID 28 Nuclide Type : Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TM-171 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-230 PA-233 U-234 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 30.08Y 30.08Y 1.92Y 1. 41E+l0Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600. OOY 1600. OOY 1. 41E+l0Y 1600.00Y 1. 41E+10Y 7.54E+04Y 2.14E+06Y 2.45E+05Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 56 1. 00 1. 02 1. 02 1. 34 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1. l 72E+Ol 2.144E+OO 2.144E-01 l.127E-01 l.191E-01 1.727E+Ol 3.026E-01 2.917E+00 7.792E-01 8.485E-01 1.058E+OO 8.485E-01 1.458E+OO 8.485E-01 7.792E-01 8.485E-01 8.967E-02 8.485E-01 1. 089E-01 1.065E-01 4.342E+Ol 4.342E+Ol Decay Corr pCi/GRAM 1.172E+Ol 3.349E+OO 2.144E-01 l.149E-01 l.213E-01 2.315E+Ol 3.026E-01 2.917E+00 7.792E-01 8.488E-01 l.059E+00 8.488E-01 1.458E+OO 8.488E-01 7.792E-01 '8.485E-01 8.967E-02 8.485E-01 1.089E-01 1.065E-01 5.052E+Ol 5.052E+Ol 62.22% Decay Corr 2-Sigma Error 0.148E+Ol 2.161E+OO l.384E-01 0.539E-01 0.569E-01 6.505E+Ol 0.861E-01 0.474E+00 1.585E-01 1.602E-01 0. l 72E+00 l.602E-01 1.039E+OO 1.602E-01 1.585E-01 1. 601E-01 7.382E-02 l.601E-01 1.097E-01 0.812E-01 "M" Manually accepted 2-Sigma %Error 12.65 64.52 64.52 46.89 46. 89 280.95 28.44 16.26 20.34 18.87 16.26 18.87 71. 23 18.87 20.34 18.87 82.32 18.87 100.74 76.26 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4610 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235073 Acquisition date : 3-0CT-2016 06:46:12 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 92.75 64 128 1.11 185.17 182 7 1. 44E-02 71. 5 5.54E+OO T 0 99.04 30 83 1. 33 197.74 196 6 6.86E-03 **** 5.82E+OO T 0 128.86 40 82 0.70 257.33 255 6 9.25E-03 84.9 6.15E+OO T o. 185.91 79 141 1.15 371.34 366 11 l.87E-02 69.5 5.26E+OO T 0 209.20 30 74 '0.79 417.89 415 7 7.25E-03 **** 4.87E+OO 0 270.26 56 39 1. 59 539.93 536 9 1.38E-02 52.6 4.04E+OO T 0 331.22 8 37 1. 51 661.76 659 7 2.09E-03 **** 3.46E+OO 0 338.20 54 37 1. 21 675.72 672 7 l.36E-02 48.3 3. 41E+OO T 0 369.32 15 13 1. 07 737.93 735 6 3.89E-03 94.8 3.18E+OO 0 449.15 17 8 1. 02 897.49 894 7 4.35E-03 75.8 2.75E+OO 0 463.46 29 15 2.26 926.09 922 8 7.38E-03 64.3 2.68E+OO T 0 535.74 50 27 6.71 1070.60 1061 20 1. 30E-02 59.9 2.40E+OO 0 557.39 12 11 0.79 1113.88 1110 10 3.26E-03 **** 2,32E+OO 0 633.92 20 7 1. 96 1266.87 1262 9 5.21E-03 67. 6 2.lOE+OO T 0 646.75 17 9 1. 01 1292.52 1287 12 4.57E-03 87.6 2.07E+OO T 0 688.74 11 5 1. 53 1376.48 1374 6 2.86E-03 90.6 1.96E+OO 0 791.58 6 6 1. 43 1582 .11 1578 7 1.64E-03 **** 1. 75E+OO T 0 794.51 12 4 2.04 1587. 96 1584 8 3.33E-03 81. 6 1.74E+OO T 0 852.07 9 14 1. 00 1703.05 1696 11 2.33E-03 **** 1.64E+OO 0 886.86 20 7 2.47 1772.63 1765 15 5.41E-03 75.6 1.58E+OO 0 900 .11 9 9 0.85 1799.12 1795 8 2.34E-03 **** 1.56E+OO T 0 911.13 44 28 1. 48 1821.17 1814 14 l.22E-02 59. 9' 1.54E+OO T 0 992.50 11 2 1. 62 1983.90 1979 9 3.00E-03 78.6 1.43E+OO 0 1070.25 12 6 0.69 2139. 39 2132 12 3.33E-03 **** 1.33E+OO 0 1139. 80 12 0 1. 04 2278.50 2274 8 3.33E-03 57.7 1.26E+OO 0 1192. 44 9 3 0.89 2383.80 2381 6 2.65E-03 93.2 l.21E+OO 0 1200.72 10 14 0.93 2400.35 2395 9 2.82E-03 **** 1. 20E+OO 0 1302. 42 10 3 1. 36 2603.78 2600 9 2.90E-03 81. 5 1. llE+OO 0 1310.46 4 3 1. 25 2619.88 2616 6 1. llE-03 **** 1. llE+OO 0 1376.95 15 5 2.66 2752.88 2747 10 4.18E-03 75.8 1.06E+OO Flags: "T" = Tentatively associated Page 4611 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:48:00.08 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235073.CNF;l *
  • Acquisition date 3-0CT-2016 06:46:12 Sensitivity 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 11-DEC-2015 11:35:00 Nuclide Library : SOLID *
  • Sample ID G405235073 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4713E+02 GRAM * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 BA-137M CS-137 TM-171 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-226 TH-228 TH-230 PA-233 U-234 AM-243 ANH-511 Le (pCi/GRAM 1.124E-01 9.163E-01 5.758E-02 2.554E-02 2.698E-02 2.292E+Ol 2.646E-02 1.425E-01 5.433E-02 4.995E-02 1.580E-01 4.995E-02 5.433E-02 4:994E-02 4.578E-02 4.994E-02 5.436E-02 1.677E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 Page 4612 of 5809 Le (pCi/GRAM 1.128E+Ol 3.583E-02 O.OOOE+OO 2.262E-02 2.329E-01 O.OOOE+OO O.OOOE+OO 4.805E-02 4.291E-01 O.OOOE+OO 4.020E-02 4.254E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT.

FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 . EU-155 TB-160 H0-166M HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 Page 4613 of 5 809 5.202E+OO 2.590E-02 1.283E-01 2.313E+OO 9.143E+OO O.OOOE+OO 1.684E-01 O.OOOE+OO O.OOOE+OO 4.238E-01 5.114E+OO 5.227E-01 O.OOOE+OO 0.000E+OO 4.269E+02 2.955E-02 8.348E-01 2.021E+OO 1.295E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.276E-02 3. 712E-02 3.762E+OO 3.579E-01 3.579E-01 2.332E-02 9.282E-02 l.856E-01 O.OOOE+OO O.OOOE+OO 1.013E-01 8.591E-01 7.633E-02 l.894E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.026E-02 O.OOOE+OO 3.850E-02 1.058E-01 O.OOOE+OO O.OOOE+OO 8. 714E-02 O.OOOE+OO O.OOOE+OO 1.598E+Ol O.OOOE+OO 2. 731E-01 4 .119E-02 3. 551E+OO 3.660E-02 O.OOOE+OO 6. 881E+02 O.OOOE+OO 1. 925E-02 8.308E-02 1.194E-01 9.030E-02 8.775E-02 1.594E+OO 4.528E-02 1.859E-01 6.924E-02 l.735E-02 3.308E+OO 8.051E-01 2.732E+OO 2.521E+Ol 8.824E+Ol 3.480E-01 1.591E+OO NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF I DENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT . FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 RA-224 AC-227 TH-227 AC-228 RA-228 TH-229 PA-231 TH-231 TH-232 PA-234 PA-234M TH-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4614 of 5809 3.542E-02 3.898E+00 4.562E-01 5.177E-01 3.450E-01 5.186E-01 6.779E-01 1. 863E-01 1.863E-01 2.423E-01 2.423E-01 3.657E-01 3.507E-01 5.186E-01 2.423E-01 2.497E-01 4.045E+OO 1.230E+OO 1.528E-01 4.121E-02 O.OOOE+OO 1.230E+OO 1.734E-01 2.859E+02 1.297E-01 7.621E-02 6.201E-02 2.840E-02 3.635E-02 9.035E-02 FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL .A.BUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:48:06.70 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235073.CNF;l *
  • Acquisition date 3-0CT-2016 06:46:12 Sensitivity 3.000 *
  • Detector ID GAM06 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance *limit : 75.000 *
  • Elapsed real time: 0 01:00:00.59 Half life ratio : ***** *
  • Sample date 11-DEC-2015 11:35:00 Nuclide Library : SOLID *
  • Sample ID G405235073 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4713E+02 GRAM *
  • Quantity Err(%) : l.3593E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0. 00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 8-MAR-2016 07:26:53 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM06 CAN.CNF;l4
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 l. l 72E+Ol l.762E+OO CD-109 1.955E+OO 2.177E+OO SN-126 1.252E-01 1. 392E-01 BA-137M 1.149E-01 5.363E-02 CS-137 l.213E-01 5.665E-02 TM-171 2.315E+Ol 6.379E+Ol TL-208 3.026E-01 8.825E-02 BI-211 2.475E-01 9.812E-01 PB-212 7.792E-01 1. 704E-01 BI-214 8.488E-01 1. 728E-01 PB-214 1.059E+OO 1.937E-01 RN-222 8.488E-01 1. 728E-01 RA-22 6 8.488E-01 1. 728E-01 TH-228 7.792E-01 l.704E-01 TH-230 8.485E-01 1. 727E-01 PA-233 8. 967E-02 7.285E-02 U-234 8.485E-01 1.727E-01 AM-243 2.534E-02 l .112E-01 ANH-511 l.065E-01 8. 013E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 4615 of 5809 Key-Line Activity (pCi/GRAM 8. 696E+OO -1.775E-02 1.000E+41 2. 272E-03 -6.740E-02 7.679E+02 2. 411E+02 -3.033E-02 5. 099E-'-01 l.OOOE+41 1. 696E-02 K.L Act error ( 1. 96-sigma) 1.171E+Ol 4.618E-02 1.692E+41 2.651E-02 3.433E-01 l.291E+04 3.853E+02 6.428E-02 4.410E-01 8.649E+40 4.363E-02 TPU ( 1. 96-sigma) 1. 762E+00 2.177E+00 1.392E-01 5.363E-02 5.665E-02 6.379E+Ol 8.825E-02 9.812E-01 1.704E-01 1. 728E-01 l.937E-01 1. 728E-01 1. 728E-01 l.704E-01 1.727E-01 7.285E-02 1. 727E-01 l .112E-01 8. 013E-02 TPU ( 1. 96-sigma) 1.235E+Ol 4.687E-02 O.OOOE+OO 2.653E-02 3.446E-01 1.292E+04 4.004E+02 6. 572E-02 4.973E-01 O.OOOE+OO 4.429E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

C0-58 1. 609E-01 4. 725E-01 4.780E-01 NOT IDENT. FE-59 -1.564E+OO 6.323E+OO 6.362E+OO NOT IDENT. C0-60 -3.295E-02 3.981E-02 4.249E-02 NOT IDENT. ZN-65 5.307E-04 1.680E-01 l.680E-01 NOT IDENT. GE-68 2.602E+OO 2.222E+OO 2. 513E+00 NOT IDENT. AS-73 -2.331E-01 9.750E+OO 9.751E+OO NOT IDENT. AS-74 -5.684E+03 4.815E+03 5.455E+03 SHORT HLIF SE-75 -7.990E-03 2.025E-01 2.025E-01 NOT IDENT. BR-77 5.793E+37 4. 965E+38 O.OOOE+OO SHORT HLIF SR-82 ,3.949E+Ol 6.647E+02 6.650E+02 *SHORT HLIF RB-83 -l.123E-01 5.077E-01 5.103E-01 NOT IDENT. KR-85 -3.848E-01 6.623E+OO 6.625E+OO NOT IDENT. SR-85 -4.215E-02 6.774E-01 6.777E-01 NOT IDENT. RB-86 3.816E+04 2.454E+04 2.997E+04 SHORT HLIF Y-88 -1.404E-01 l.593E-01 1.714E-01 NOT IDENT. Y-91 -3.265E+02 6.523E+02 6.687E+02 NOT IDENT. NB-94 1.304E-02 3.287E-02 3.339E-02 NOT IDENT. NB-95 1.190E-01 9.778E-01 9.792E-01 NOT IDENT. NB-95M -6.651E-01 2.688E+OO 2.705E+OO NOT IDENT. ZR-95 1.326E+OO 1.297E+OO 1.428E+OO NOT IDENT. NB-97 1.000E+41 1.110E+42 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 8.777E+40 O.OOOE+OO SHORT HLIF M0-99 -5.549E+30 8.205E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 l.005E+42 O.OOOE+OO SHORT HLIF RH-101 -1. 8 61E-02 3.036E-02 3.149E-02 NOT IDENT. RH-102 -6.297E-03 5.049E-02 5.057E-02 NOT IDENT. RU-103 -8.989E-01 4.455E+OO 4.473E+OO FAIL ABUN RH-106 2.00lE-02 4.138E-01 4.139E-01 NOT IDENT. RU-106 2.00lE-02 4.138E-01 4.139E-01 NOT IDENT. AG-108M 4.304E-03 2. 572E-02 2.579E-02 NOT IDENT. AG-llOM 1.059E-01 9.012E-02 1.020E-01 NOT IDENT. SN-113 l.026E-02 2.061E-01 2.061E-01 NOT IDENT. CD-115 1.093E+39 1.345E+39 O.OOOE+OO SHORT HLIF SN-ll 7M 4.596E+04 7.293E+04 7.582E+04 SHORT HLIF TE-123M 3.409E-03 1.157E-01 1.157E-01 NOT IDENT. SB-124 -8.150E-01 1. 523E+OO 1.566E+OO FAIL ABUN SB-125 -6.022E-02 9.479E-02 9.860E-02 FAIL ABUN TE-125M -9.234E+Ol 2.203E+02 2.242E+02 NOT IDENT. I-126 4.003E+04 6.546E+05 6.548E+05 SHORT HLIF SB-126 5.930E+05 9.531E+05 9.899E+05 SHORT HLIF. SB-127 1.133E+22 1. 812E+22 O.OOOE+OO SHORT HLIF I-131 2.609E+09 3.296E+09 3.500E+09 SHORT HLIF I-132 -1.000E+41 2.135E+42 O.OOOE+OO SHORT HLIF TE-132 8.092E+25 2.065E+26 0.000E+OO SHORT HLIF BA-133 2.086E-02 3.335E-02 3.465E-02 NOT IDENT. I-133 -l.OOOE+41 2.564E+41 O.OOOE+OO SHORT HLIF CS-134 5.532E-02 4.465E-02 5 .114E-02 FAIL ABUN CS-135 -1. 7 63E-03 1.382E-01 1.382E-01 NOT IDENT. I-135 -1.000E+41 6.848E+41 O.OOOE+OO SHORT HLIF CS-136 3.707E+04 2.441E+05 2.447E+05 SHORT HLIF CE-139 -5.410E-02 l.063E-01 1. 091E-01 NOT IDENT. BA-140 l.287E+06 1.022E+06 l.175E+06 SHORT HLIF LA-140 -1. 77 5E+05 3.606E+05 3.694E+05 SHORT HLIF CE-141 -1. 53 6E+Ol l.984E+Ol 2.102E+Ol NOT IDENT. CE-143 1.000E+41 2.508E+41 O.OOOE+OO SHORT HLIF CE-144 -4.808E-02 3 .135E-01 3.143E-01 NOT IDENT. PM-144 -9.689E-03 5.050E-02 5.069E-02 NOT IDENT. PR-144 -9.049E-01 4.368E+OO 4.387E+OO NOT IDENT. PM-146 1. 883E-02 3.881E-02 3.973E-02 FAIL ABUN ND-147 -2. 972E+07 2.907E+07 3.201E+07 SHORT HLIF PM-147 -4.483E+Ol 7.763E+02 7.766E+02 NOT IDENT. PM-149 5.622E+39 1.636E+40 O.OOOE+OO SHORT HLIF EU-150 -4.274E-03 3.054E-02 3.060E-02 FAIL ABUN EU-152 1. 744E-02 8.994E-02 9.028E-02 NOT IDENT. GD-153 -3.497E-02 l.467E-01 l.476E-01 NOT IDENT. EU-154 -3. SllE-02 1.146E-01 1.159E-01 NOT IDENT. EU-155 -l.597E-02 9.891E-02 9.918E-02 FAIL ABUN TB-160 8.000E-01 1. 759E+OO 1. 796E+OO FAIL ABUN H0-166M 2. 571E-02 4.856E-02 4.992E-02 FAIL ABUN HF-172 8.331E-02 2.169E-01 2.201E-01 FAIL ABUN LU-172 3.106E-03 7.922E-02 7.923E-02 FAIL ABUN LU-176 6.703E-04 2.094E-02 2.094E-02 FAIL ABUN HF-181 7.189E-01 3.657E+OO 3.671E+OO NOT IDENT. TA-182 5.694E-01 8.259E-01 8.648E-01 FAIL ABUN RE-183 -2.721E-01 2.945E+OO 2.947E+OO NOT IDENT. RE-184 -5.328E+OO 3.594E+Ol 3.602E+Ol FAIL ABUN W-188 6.099E+Ol 1. 051E+02 1. 087E+02 NOT IDENT. IR-192 -1.868E-01 4.039E-01 4.125E-01 FAIL ABUN Page 4616of5809 HG-203 -1.432E+00 2.137E+OO 2.233E+OO NOT IDENT. BI-207 -1.432E-02 5.012E-02 5.054E-02 FAIL ABUN PB-210 1.023E+OO 4.037E+OO 4.063E+OO NOT IDENT. PB-211 -1. 584E-01 5.354E-01 5.401E-01 NOT IDENT. BI-212 6.776E-01 5.170E-01 6.005E-01 NOT IDENT. RN-219 2.059E-01 3.630E-01 3.746E-01 FAIL ABUN RA-223 2.992E-01 5.390E-01 5.556E-01 FAIL ABUN RA-224 1.458E+OO l.027E+OO 1.219E+OO FAIL ABUN AC-227 -8.144E-02 2.331E-01 2.360E-01 NOT IDENT. TH-227 -8.144E-02 2. 331E-OJ. 2.360E-01 NOT IDENT. AC-228 5.687E-01 3.421E-01 4.275E-01 FAIL ABUN RA-228 5.687E-01 3. 421E-01 4.275E-01 FAIL ABUN TH-229 -2.064E-01 4.490E-01 4.586E-01 FAIL ABUN PA-231 -4.488E-02 3.883E-01 3.888E-01 NOT IDENT. TH-231 2.992E-01 5.390E-01 5.556E-01 FAIL ABUN TH-232 5.687E-01 3.421E-01 4.275E-01 FAIL ABUN PA-234 9.156E-02 2.875E-01 2.905E-01 FAIL ABUN PA-234M 4. 321E+OO 3.973E+OO 4.425E+OO NOT IDENT. TH-234 4.782E-01 1.290E+OO 1.307E+OO FAIL ABUN U-235 4.420E-02 1.694E-01 1. 705E-01 FAIL ABUN NP-237 8.967E-02 7.285E-02 8.332E-02 FAIL ABUN NP-238 -2.640E+40 1.677E+41 0.000E+OO SHORT HLIF U-238 4.782E-01 1. 2 90E+OO 1.307E+OO FAIL ABUN NP-239 9.0lOE-02 l.846E-01 1. 891E-01 FAIL ABUN PU-239 5.275E+02 4.407E+02 5.008E+02 FAIL ABUN AM-241 -1.982E-02 l.405E-01 1. 408E-01 NOT IDENT; CM-243 -4.651E-02 8.894E-02 9 .137E-02 FAIL ABUN BK-247 '2. OOlE-02 7.168E-02 7.225E-02 NOT IDENT. CM-247 4.746E-03 3.121E-02 3.128E-02 NOT IDENT. CF-249 3.557E-02 3.681E-02 4.015E-02 NOT IDENT. CF-251 1.450E-03 1.043E-01 l.043E-01 NOT IDENT. Page 4617 of 5809

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 53.5821 87.09 76.2207 136.47 48.9091 45.60 47.9530 87.57 76.2976 140.51 0.0000 46.54 48.9570 88.03 80.1894 143.76 53.6591 49.72 0.0000 88.34 80.2413 144.24 55.8030 51. 35 60.4416 88.47 68.7969 145.44 58. 0112 51. 87 57.6251 89. 96 69.0090 152.43 55.4039 52.39 57.7140 1093.63 53.7488 153.25 0.0000 52.97 57.8124 91.11 0.0000 323.87 66.2250 53.44 57.8920 92.59 64.5617 156.02 0.0000 54.07 50.3821 93.35 64.6604 158.56 0.0000 57.36 0.0000 94.56 61. 914 6 159.00 47.3133 57.53 53.2455 94.65 61.9258 162.33 57.2514 57.98 56.8657 94.67 61.9282 162.66 0.0000 59.27 51.7173 94.87 61.9526 163.33 54.0840 59.32 61. 5339 97.43 49.2932 165.86 59.6955 59.54 62.4631 98.43 46.7893 176.31 28.6081 60. 96 57.3281 98.44 46.7904 176.60 0.0000 61.17 75.2855 99.53 48.8422 177.52 45.1822 62.93 65.7316 100 .11 65.1957 181.07 0.0000 63.29 67. 5960 102.03 54. 9644 181. 52 39.8732 63.58 66.7451 103.18 64.9194 184.41 50.0214 64.28 64.1552 103.37 64.9426 143.76 50.1025 66.73 69.1035 105.21 64.1773 193.51 52.8262 67.24 77.3860 105.31 64.1892 197.03 37.2464 125.81 77.4709 106.12 54.3949 198.01 45.1990 67.75 77.4846 106.47 51. 4608 201.83 43 .1310 69.67 66.8619 109.28 54.7079 203.43 50.0338 70.83 87.2578 111. 00 51. 8834 205.31 44.4439 72. 81 82.4428 111.76 0.0000 210.85 44.3414 72. 87 89.8383 114. 06 52.1638 215.65 34.5872 74.66 134.7088 116.30 0.0000 222 .11 52.2482 74.82 134.7587 116.74 36.2813 227.09 52.5277 74.97 134.8063 119.76 51.6634 227.38 53.7118 77 .11 113 .1011 121.12 60. 9196 228.16 0.0000 78.74 69.8587 121.22 60.9297 228.18 40.9024 79.69 60.0063 121. 7 8 62.0029 116.74 40.9024 80.12 63.8180 122.06 53.8965 235.69 58.1076 80.19 0.0000 122.92 64.1574 235. 96 54.9823 80.57 66.7001 123.07 62.1360 238.63 70.8856 81. 00 63.0027 265.00 63.2185 238.98 0.0000 81. 07 63.0124 125.81 49 .1144 240.99 90.0053 81. 75 67.8159 127.23 53.3296 242.00 39.5162 83.79 63.0722 127.91 62.9711 244.70 26.9447 84.00 54.2666 129.30 46.3046 252.40 0.0000 85.43 84.8146 131.20 56.4217 252.80 28.7600 86.55 76.1340 133.02 46.5779 254.15 0.0000 86. 79 76.1719 133.52 53.8654 256.23 42.0824 86.94 76.1963 136.00 50.9537 260.90 0.0000 Page 4618of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 35.1517 355.39 0.0000 584.27 17.0865 264.80 30.3070 356.01 14.4026 595.83 0.0000 265.00 32.7373 364.49 0.0000 427.87 20.2694 268.22 30.8101 366.42 0.0000 602.52 0.0000 269.46 30.4405 372. 51 21. 2080 604.72 16.7565 270.03 30.4565
  • 375.05 23.9030 607.14 . 16.7766 271.23 30.4909 377.52 21. 2852 609.32 16.2858 273.65 0.0000 356.01 23.1642 610.33 13.7483 276.40 31.8621 388.16 21. 4482 614.28 12.2446 277.37 44.1563 388.63 0.0000 618.01 11.2448 277.60 44.1650 391.69 24.1891 620.36 17.3984 278.00 39.2725 2 64. 66 24.3408 621.93 12.2905 279.20 35.6296 401. 81 22.5555 630.19 0.0000 279.54 31.9533 402.40 22.5647 631.29 10.8033 279.70 31. 9581 404.85 20.7946 633.25 8.2386 280.46 24.6002 410.95 27.2363 634.78 0.0000 283.69 20.9714 413.71 22.7392 635.95 12.3740 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 33.3586 423.72 0.0000 645.85 7.2524 285.90 0.0000 427.09 24.7780 657.76 9.3768 287.50 23.5186 427.87 26.6270 657.90 0.0000 290.67 23.1710 433.94 21.2017 661. 66 14.0905 293.27 0.0000 439.40 18.5014 664.57 0.0000 351. 93 28.6644 453.88 '16.8051 666.33 0.0000 295. 96 28.6826 463.37 15.9655 666.50 0.0000 879.38 44.9978 468.07 10.1720 667.71 0.0000 299.98 26.2801 473.00 0.0000 677.62 14.7201 300.09 26.2827 475.06 31.2134 685.70 0.0000 300.13 26.2833 476.78 20.8309 695.00 0.0000 301.36 33.4115 477.60 17.9992 696.49 15.9064 302.85 33.4538 482.18 17.0988 696. 51 15.9064 256.23 20.9381 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 16.9727 306.78 22.6571 497.08 16.2913 697.49 14.8525 308.46 18.9079 505.52 2.8890 702.65 17.0130 311. 90 26.5480 507.63 0.0000 706.68 14.9132 316.51 32.9951 511. 00 11.5925 711.68 9.6079 319.41 0.0000 514.00 18.8700 720.70 0.0000 320.08 0.0000 514.00 18.8700 721. 93 0.0000 321. 04 35.6656 520.40 14.5679 722.78 22.5270 323.87 26.3858 520.69 0.0000 722. 91 19.3103 325.23 31. 527 4 522.65 0.0000 723. 31 21. 4591 328.76 0.0000 527.90 0.0000 724 .19 24.6874 333.37 25.7306 528.26 17.5591 727. 33 11. 8231 333.97 28.3171 529.59 19.0358 733.00 6.4646 334.37 20.6011 529.87 0.0000 735.93 7.5514 338.28 27.5527 531. 02 0.0000 333.97 9.7156 338.32 32.2899 537.26 0.0000 739.50 0.0000 311. 90 27.1690 546.56 0.0000 747.24 14.0918 340.48 27.1690 552.55 14.2348 748.06 11. 9279 340.55 0.0000 563.25 11.9297 752.31 21.7253 344.28 30.2775 569.33 16.9550 753.82 0.0000 345.93 25.9857 946.00 16.9564 756.73 7.6181 351.06 24.3490 569.70 16.9578 756.80 '7. 6181 351. 93 24.3650 583.19 17.0775 884.68 22.9226 Page 4619 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 22.9397 1274.44 8.5635 1620.50 4.2180 766.42 17.4824 1001.03 5.3606 1621. 92 3.1646 766.84 13 .1143 1002.74 8.0456 1678.03 0.0000 772. 60 0.0000 1004.73 11. 6289 1690.97 3.2122 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 5.4364 778.90 15.3757 1028.54 0.0000 1063.66 4.3540 783.70 0.0000 1037.84 8.1381 1771.35 3.2664 785.37 9.9104 1038.76 0.0000 1791.20 0.0000 792.07 0.0000 631.29 13. 6011 1808.65 2.1941 794.95 14.9227 1048.07 0.0000 1810.72 0.0000 795.86 6.6348 1049.04 9.9822 1836.06 3.3091 810.06 10.0082 1050.41 11. 8019 810.29 7.7850 1063.66 10. 2108 344.28 6.6733 1077.00 0.0000 810.76 7.7864 1077.34 4.5779 815.77 0.0000 1085.87 10.0977 1048.07 0.0000 1093.63 11. 9622 832.01 8.9727 1099.45 11. 9836 834.85 16.8420 1112. 07 11.1042 835.71 13.4780 1112.84 12.9584 836.80 0.0000 1115. 54 8.8928 846.75 0.0000 1120.29 5.5660 846.77 5.0757 1120.55 5.5664 856.80 0.0000 1221. 41 5. 567 9 860.56 15.8736 1129.67 12.0939 871. 09 12.5209 1131. 51 0.0000 873.19 12.5308 1147.95 0.0000 875.33 0.0000 1173.23 15.0771 879.38 9.1341 1177.95 6.6052 880.51 8.5669 1189.05 15.1455 883.24 15.4358 1204.77 16.7353 884.68 4.5760 1221.41 6.6873 889.28 8.5944 1231. 02 9.5789 894.76 9.6448 1235.36 0.0000 898.04 6.8975 1238.28 10.5576 900.72 15.5341 1260.41 0.0000 903.28 15.5484 1271.87 6.7808 911.20 9.2402 1274.44 10.6630 912.08 9.2432 1274.54 10.6630 923.98 0.0000 1291. 59 3.8953 926.50 8.1291 1298.22 0.0000 929 .11 12.7863 1312 .11 0.0000 937.49 10.4923 1332.49 10.8281 944.13 0.0000 1362.66 0.0000 946.00 10.5234 1365.19 3.9707 949.00 7.9008 1368.63 0.0000 667.71 0.0000 1384.29 2.9925 962. 31 10.5824 1408.01 7.0244 964.08 27.3549 1457.56 0.0000 966 .17 29.1409 1460.82 1. 0165 911.20 12.3743 1489.16 5 .1169 968. 97 12.3743 1505.03 9.2450 983.53 0.0000 1584.12 9.4142 984.45 0.0000 1596.21 0.0000 Page 4620 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:48:36.53 ******************************************************************************** *
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration : DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235074.CNF;l Background file : DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM07.CNF;484 Background date : Z-OCT-2016 11:00:17. Sample date : 15-DEC-2015 14:10:00 Acquisition date : 3-0CT-2016 06:46:37. Sample ID : G405235074 Sample quantity : 1.69068E+02 GRAM Detector name : GAM07 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.52 0.0% Energy tolerance : 1.50000 keV Analyst Initials : MXRl Abundance limit : 75.00000 Sensitivity : 3.00000 Batch ID : 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 1 1 0 0 0 0 0 0 0 2 2 0 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4621of5809 Energy 46.66* 63.21* 74.83* 77.15 86.91 93.50* 118. 70 129.94 186.11* 204.67 209.40 238.59* 241. 62 270.04 277.32 281. 69 295.26* 302.74 338.34* 351.94* 463.85 511.44* 564.19 583.08* 609.27* 727.17* 744.83 768.72 803.54* 894.73 911.72* 927.72 934 .11 954.52 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 38 22 128 233 58 30 34 49 83 25 39 391 94 39 25 25 205 29 87 282 38 35 34 112 184 29 20 17 18 14 53 15 15 8 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 153 141 178 154 154 214 84 136 143 79 84 62 68 56 56 43 87 70 61 61 41 69 22 24 60 13 11 12 3 19 41 9 6 4 0.86 1. 02 1.13 1.13 1.19 1. 46 0.75 1. 69 1. 38 1. 05 0.90 1. 25 1. 54 1. 63 1. 45 1. 45 1. 39 4.08 1. 70 1. 43 1. 85 1. 97 3.16 1. 43 1. 29 1. 43 2.49 1. 50 3.94 0.61 1. 87 2.38 2.53 0.97 93.83 126.92 150.15 154.79 174.29 187.48 237.87 260.35 372. 64 409.76 419.23 477.58 483.65 540.48 555.03 563.77 590.90 605.86 677.05 704.25 928.01 1023.17 1128. 65 1166.43 1218.80 1454.56 1489.87 1537.64 1607.28 1789.64 1823.60 1855.60 1868.38 1909.19 89 124 146 146 171 181 234 255 368 407 415 474 474 536 552 552 584 598 670 696 922 1016 1121 1160 1212 1450 1485 1533 1601 1781 1815 1851 1865 1906 10 l.07E-02 7 6.02E-03 14 3.55E-02 14 6.48E-02 7 1. 61E-02 9 8.39E-03 7 9.54E-03 10 l.37E-02 13 2.29E-02 8 6.97E-03 8 1.08E-02 14 l.09E-01 14 2.61E-02 9 1. lOE-02 15 7.0lE-03 15 7.05E-03 15 5.70E-02 12 8.16E-03 15 2.41E-02 15 7.84E-02 14 l.06E-02 18 9.79E-03 15 9.46E-03 12 3.lOE-02 14 5. llE-02 11 7.95E-03 9 5.55E-03 8 4.77E-03 12 5.05E-03 14 3.94E-03 14 1. 46E-02 11 4.25E-03 8 4.29E-03 6 2.15E-03 63.3 96.8 19.4 11. 5 37.8 93.0 47.7 46.9 32.8 64.2 43.7 6.3 21. 0 37.7 49.8 48.7 12.2 61. 3 22.5 8. 6 39.3 65.7 34.8 13.2 11. 7 32.2 39.2 44.0 35.4 72.8 30.1 44.7 37.2 55.9 Fit 1. 71E+OO 2.42E+OO 2.97E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235074 Acquisition date 3-0CT-2016 06:46:37 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 965. 47 7 22 2.09 1931.10 1922 12 1.86E-03143.0 36 0 968.79* 62 7 1. 61 1937.73 1933 14 1.74E-02 16.0 37 0 J_002.17 19 13 4.53 2004.47 14 5.36E-03 46.7 38 0 1120. 90 31 24 2.18 2241. 90 2234 14 8.72E-03 37.8 39 0 1144.39 17 7 1. 71 2288.89 2284 10 4.67E-03 38.9 40 0 1161. 83 15 10 0.86 2323.75 2317 12 4. 23E-03 51. 2 41 0 1237.69 19 14 2.49 2475.47 2470 11 5.34E-03 43.8 42 0 1248.96 14 17 0.69 2498.00 2491 13 3.90E-03 69.2 43 0 1328.22 5 11 1. 45 2656.52 2649 14 1.49E-03135.1 44 0 1376.11 11 3 3.18 2752.28 2747 11 3.09E-03 41.8 45 0 1391.79 11 3 3.33 2783.64 2777 12 3. llE-03 42.9 46 0 1460.42* 356 3 2.04 2920.89 2914 14 9.90E-02 5.5 47 0 1764.49* 31 8 2.87 3528.99 3523 13 8.69E-03 28.0 Flag: "*" = Peak area was modified by background subtraction Page 4622 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:48:38 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235074.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 15-DEC-2015 14:10:00 G405235074 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:46:37 169.07 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA7 0 01:00:00.00 1.50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 . PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4623 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:00.52 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235074 Acquisition date 3-0CT-2016 06:46:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.122E+0.0 1.291E+Ol 1.291E+Ol 10.97 OK CD-109 88.03 3.70* 5.724E+OO 3.499E-01 5.431E-01 371.35 OK SN-126 64.28 9.60 3.489E+OO 4.059E-01 4.059E-01 193.59 OK 86.94 8.90 5.724E+OO 1.455E-01 1.455E-01 371.35 OK 87.57 37.00* 5.724E+OO 3.499E-02 3.499E-02 371.35 OK TL-208 277.37 6.60 4.378E+OO 4.681E-01 4.681E-01 99.58 OK 583.19 85.00* 2.366E+OO 2. 719E-01 2.719E-01 26.46 OK 860.56 12.50 1. 736E+OO Line Not Found Absent PB-210 46.54 4.25* l.120E+OO 5.209E+OO 5.341E+OO 126.67 OK PB-212 74.82 10.28 4.782E+OO 8.006E-01 8.006E-01 81. 51 OK 77 .11 17.10 4.994E+OO 1. 679E+OO l.679E+OO 23.00 OK 238.63 43.60* 4. 931E+OO 9.923E-01 9.923E-01 12.62 OK 300.09 3.30 4.103E+OO Line Not Found Absent BI-214 609.32 45.49* 2.284E+OO 8.628E-01 8.631E-01 23.39 OK 1120.29 14.92 l.405E+OO 6.739E-01 6.741E-01 75.57 OK 1764.49 15.30 9.422E-01 9.156E-01 9.159E-01 55.98 OK PB-214 74.82 5.80 4.781E+OO Line Not Found <<INT Reject 77 .11 9.70 4.994E+00 2. 960E+OO 2. 961E+OO 23.00 OK '87.09 3.41 5.736E+OO Line Not'Found <<INT Reject 242.00 7.25 4.877E+OO Line Not Found <<INT Reject 295.22 18.42 4.159E+OO 1.426E+OO l.427E+00 24.36 OK 351.93 35.60* 3.592E+OO 1.151E+OO 1.152E+OO 17.12 OK RN-222 609.32 45.49* 2.284E+OO 8.628E-01 8. 631E-01 23.39 OK 1120.29 14.92 1. 405E+OO 6.739E-01 6.741E-01 75.57 OK 1764.49 15.30 9.422E-01 9.156E-01 9.159E-01 55.98 OK RA-224 240.99 4.10* 4.883E+OO 3.579E-02 3.579E-023461.28 OK RA-226 609.32 45.49* 2.284E+OO 8.628E-01 8.631E-01 23.39 *OK 1120.29 14.92 1.405E+OO 6.739E-01 6.741E-01 75.57 OK 1764.49 15.30 9.422E-01 9.156E-01 9.159E-01 55.98 OK AC-228 105.21 1.10 6.488E+00 Line Not Found Absent 338.32 11.27 3.713E+OO 1.088E+OO 1.088E+OO 45.09 OK 794.95 4.25 1.849E+OO Line Not Found Absent 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.659E+OO 5.680E-01 5.680E-01 60.24 OK 968. 97 15.80 1.580E+OO 1.148E+OO 1.148E+OO 31. 90 OK RA-228 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3.713E+OO 1.088E+00 1.088E+OO 45.09 OK 794.95 4.25 1.849E+OO Line Not Found Absent 835. 71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* l.659E+00 5.680E-01 5.680E-01 60.24 OK 968. 97 15.80 1.580E+OO 1.148E+OO 1.148E+OO 31. 90 OK TH-228 74.82 10.28 4.782E+OO 8.006E-01 8.006E-01 81. 51 OK 77 .11 17.10 4.994E+OO 1.679E+OO 1.679E+OO 23.00 OK 238.63 43.60* 4.931E+OO 9.923E-01 9.923E-01 12.62 OK 300.09 3.30 4.103E+OO Line Not Found Absent TH-230 609.32 45.49* 2.284E+OO 8.628E-01 8.628E-01 23.39 OK 1120.29 14.92 1.405E+OO 6.739E-01 6.739E-01 75.57 OK 1764.49 15.30 9.422E-01 9.156E-01 9.156E-01 55.98 OK PA-231 283.69 1. 70 4.298E+OO Line Not Found Absent Page 4624 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235074 Acquisition date 3-0CT-2016 06:46:37 Nuclide Type: Nuclide Uncorrected Decay Corr 2-Sigma Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 301. 36. 5.35* 4.074E+OO 7.154E-01 OK TH-232 105.21 1.10 6.488E+OO Line Not Found Absent 338.32 11. 27 3. 713E+OO 1.088E+OO l.088E+OO 45.09 OK 835.71 1. 61 1.777E+OO Line Not Found Absent 911.20 25.80* 1.659E+OO 5.680E-01 5.680E-01 60.24 OK 968. 97 15.80 1.580E+OO 1.148E+OO 1.148E+OO 31. 90 OK TH-234 63.29 3.70* 3.489E+OO 1.053E+OO 1.053E+OO 193.59 OK 92.59 4.23 6.082E+OO 7.081E-01 7.081E-01 185.99 OK U-234 609.32 45.49* 2.284E+OO 8.628E-01 8.628E-01 23.39 OK 1120.29 14.92 1.405E+OO 6.739E-01 6.739E-01 75.57 OK 1764.49 15.30 9.422E-01 9.156E-01 9.156E-01 55.98 OK U-235 89. 96 3.47 5.903E+OO Line Not Found Absent 93.35 5.60 6.082E+OO 5.348E-01 5.348E-01 185.99 OK 143.76 10. 96* 6.563E+OO Line Not Found Absent 163.33 5.08 6.266E+OO Line Not Found Absent 185.72 57.20 5.850E+OO 1.384E-01 1.384E-01 65.53 OK 205.31 5.01 5.507E+OO 5.048E-01 5.048E-01 128.45 OK U-238 63.29 3.70* 3.489E+OO 1.053E+OO 1.053E+OO 193.59 OK 92.59 4.23 6.082E+OO 7.081E-01 7. 081E-01 185.99 OK AM-243 43.53 5.90 6.933E-01 Line Not Found Absent 74.66 67.20* 4.782E+OO 1.225E-01 l.225E-01 81. 51 OK ANH-511 511. 00 100.00* 2.632E+OO 6.672E-02 6.672E-02 131. 38 OK Flag: "*" = Keyline Page 4625 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:48:39.55 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235074.CNF;l *
  • Acquisition date 3-0CT-2016 06:46:37 Sensitivity : 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.52 Half life ratio : ***** *
  • Sample date 15-DEC-2015 14:10:00 Analyst initials: MXRl *
  • Sample ID G405235074 Sample Quantity 1.6907E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;15 *' Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1. 291E+Ol 1.388E+OO CD-109 5. 431E-01 1.976E+OO SN-126 3.499E-02 1.273E-01 TL-208 2.719E-01 7.050E-02 PB-210 5.341E+OO 6.630E+00 PB-212 9.923E-01 1.227E-01 BI-214 8. 631E-01 1. 97 9E-01 PB-214 1.152E+OO 1. 931E-01 RN-222 8.631E-01 1. 979E-01 RA-224 3.579E-02 1. 214E+OO RA-226 8. 631E-01 1. 979E-01 AC-228 5.680E-01 3.353E-01 RA-228 5.680E-01 3.353E-01 TH-228 9.923E-01 1.227E-01 TH-230 8.628E-01 1.978E-01 PA-231 7.154E-01 8.590E-01 TH-232 5.680E-01 3.353E-01 TH-234 1.053E+OO 1.998E+OO U-234 8.628E-01 1.978E-01 U-235 1.094E-02 1.439E-01 U-238 1.053E+OO 1.998E+OO AM-243 1.225E-01 9.783E-02 ANH-511 6. 672E-02 8.590E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 Page 4626 of 5809 Key-Line Activity (pCi/GRAM 1.379E+OO 1.616E-02 O.OOOE+OO -1.698E-02 3.538E-02 0.000E+OO O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 9.796E+OO 3.987E-02 1. 811E+41 2.135E-02 3.648E-01 9. 221E+03 2.936E+02 MDA (pCi/GRAM 6.084E-01 2.046E+OO 1.245E-01 5.559E-02 4.223E+OO 7.712E-02 1.150E-01 1.118E-01 1.150E-01 8.268E-01 1.150E-01 2.552E-01 2.552E-01 7.712E-02 1.150E-01 7. 581E-01 2.552E-01 1. 867E+OO 1.150E-01 2. 729E-01 1. 867E+OO 7.747E-02 4.377E-02 MDA (pCi/GRAM 1.955E+Ol 8.558E-02 O.OOOE+OO 3.580E-02 6.660E-01 O.OOOE+OO O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF MN-54 -1.193E-03 4.952E-02 1.015E-01 NOT IDENT. C0-56 1.121E-01 4.324E-01 8.956E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 l.245E-03 4.138E-02 7.333E-02 NOT IDENT. C0-58 -l.831E-01 4.291E-01 7.633E-Ol NOT IDENT. FE-59 7.519E-01 4. 631E+OO 9.756E+OO NOT IDENT. C0-60 1. 621E-02 4.335E-02 8.233E-02 NOT IDENT. ZN-65 1. 749E-02 1.862E-01 3.289E-01 NOT IDENT. GE-68 -6.209E-01 2.298E+OO 4.375E+OO NOT IDENT.
  • AS-73 5.133E+OO 5.878E+OO 1. 266E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.002E+03 O.OOOE+OO SHORT HLIF SE-75 l.098E-02 1.604E-01 3.261E-01 NOT IDENT. BR-77 O.OOOE+OO 2.755E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.139E+02 O.OOOE+OO SHORT HLIF RB-83 -2.077E-01 5.486E-01 1.018E+OO NOT IDENT. KR-85 5.421E+OO 6.179E+OO l.315E+Ol NOT IDENT. SR-85 5.304E-01 6.056E-01 1.289E+OO NOT IDENT. RB-86 O.OOOE+OO 2.165E+04 O.OOOE+OO SHORT HLIF Y-88 -1.139E-01 l.709E-01 3.090E-01 NOT IDENT. Y-91 -8.441E+Ol 4.387E+02 8.409E+02 NOT IDENT. NB-94 l.578E-02 2. 87.0E-02 5.890E-02 NOT IDENT. NB-95 7.035E-01 6.530E-01 1. 388E+OO NOT IDENT. NB-95M 8.784E-01 1.878E+OO 3.588E+OO NOT IDENT. ZR-95 4. 396E-01 1.016"E+OO 2.142E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 3.026E+31 0.000E+OO SHORT HLIF TC-99M O.OOOE+OO 1.918E+41 O.OOOE+OO SHORT HLIF RH-101 -l.570E-02 3.102E-02 5.157E-02 NOT IDENT. RH-102 -2.730E-02 5.185E-02 9.234E-02 NOT IDENT. RU-103 -1.949E+OO 4.364E+OO 8.059E+OO FAIL ABUN RH-106 3.814E-01 3.336E-01 7.947E-01 NOT IDENT. RU-106 3.814E-01 3.336E-01 7.947E-01 NOT IDENT. AG-108M l.630E-03 2. 201E-02 4.419E-02 NOT IDENT. AG-110M 2.177E-02 7. 901E-02 1.695E-01 NOT IDENT. SN-113 4.530E-02 l.894E-01 3.841E-01 NOT IDENT. CD-115 O.OOOE+OO 2. 811E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 5.789E+04 O.OOOE+OO SHORT HLIF TE-123M -7.530E-02 l.120E-01 1. 971E-01 NOT IDENT. SB-124 -1.410E-01 *1.804E+OO 3.654E+OO NOT IDENT. SB-125 2.016E-02 8.248E-02 1.687E-01 FAIL ABUN TE-125M -5. 511E+Ol 2.020E+02 3.796E+02 NOT IDENT. I-126 O.OOOE+OO 5.217E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 6.826E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 5.306E+21 0.000E+OO SHORT HLIF I-131 .0. OOOE+OO 2. 372E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 7.666E+25 O.OOOE+OO SHORT HLIF BA-133 1.648E-02 2.977E-02 5.936E-02 FAIL ABUN I-133 O.OOOE+OO 8.338E+40 O.OOOE+OO SHORT HLIF CS-134 4.064E-02 5.273E-02 1.083E-01 FAIL ABUN CS-135 4.233E-02 1. 229E-01 2.321E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO l.702E+05 0.000E+OO SHORT HLIF BA-137M 3.669E-03 2.941E-02 5.778E-02 NOT IDENT. CS-137 3.876E-03 3.107E-02 6.104E-02 NOT IDENT. CE-139 -2.574E-03 l.022E-01 1.895E-01 NOT IDENT. BA-140 O.OOOE+OO 7.914E+05 0.000E+OO SHORT HLIF LA-140 0.000E+OO 2.330E+05 O.OOOE+OO SHORT HLIF CE-141 -4.315E+OO 1. 672E+Ol 3.089E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.998E+40 0.000E+OO SHORT HLIF CE-144 -2.569E-02 3.251E-01 5.638E-01 NOT IDENT. PM-144 9.287E-03 4.718E-02 9.331E-02 NOT IDENT. PR-144 7. 641E-01 4.077E+OO 8.054E+OO NOT IDENT. PM-146 1.456E-02 3.638E-02 7.524E-02 NOT IDENT . ND-147 . 0. OOOE+OO 1.655E+07 O.OOOE+OO SHORT HLIF PM-147 3.898E+02 6.729E+02 1. 272E+03 NOT IDENT. PM-149 O.OOOE+OO 3.918E+39 0.000E+OO SHORT HLIF EU-150 -9.227E-03 2 .113E-02 3.573E-02 FAIL ABUN EU-152 -4.740E-02 8.633E-02 1.427E-01 FAIL ABUN GD-153 -2.473E-01 1.418E-01 2.336E-01 NOT IDENT. EU-154 4.404E-02 9.900E-02 2.134E-01 NOT IDENT. EU-155 5.616E-02 9.474E-02 1.901E-01 FAIL ABUN TB-160 -1.526E-01 1.334E+OO 2.718E+OO FAIL ABUN H0-166M 4.475E-02 5.012E-02 l.085E-01 FAIL ABUN TM-171 7.249E+OO l.545E+Ol 3.228E+Ol NOT IDENT. HF-172 -6.858E-03 2.106E-01 3.688E-01 FAIL ABUN LU-172 6.000E-02 7.494E-02 1.643E-01 FAIL ABUN Page 4627 of 5809 LU-176 2.334E-02 1. 980E-02 4.154E-02 FAIL ABUN HF-181 -1.163E+OO 3.168E+00 5.949E+OO NOT IDENT. TA-182 -2.031E-01 9.016E-01 1.694E+OO FAIL ABUN RE-183 -1.566E+OO 2.066E+OO 3. 911E+OO NOT IDENT. RE-184 4 .132E+OO 2. 413E+Ol 4.986E+Ol FAIL ABUN W-188 -2.021E+Ol 8.555E+Ol l.509E+02 FAIL ABUN IR-192 -l.709E-01 3.781E-01 7 .133E-01 FAIL ABUN HG-203 -l.304E+OO l.800E+OO 3.384E+OO NOT IDENT. BI-207 -7.806E-03 3.805E-02 7.494E-02 FAIL ABUN BI-211 O.OOOE+OO 5.320E-01 7. 852E-01 FAIL ABUN PB-211 -l.405E-02 6.006E-01 l.177E+OO NOT IDENT. BI-212 1.031E+OO 6.514E-01 1.099E+OO FAIL ABUN RN-219 -8.120E-02 3.420E-01 6.557E-01 FAIL ABUN RA-223 -l.114E-01 4.941E-01 9.646E-01 FAIL ABUN AC-227 -l.214E-01 l.802E-01 3.433E-01 NOT IDENT. TH-227 -l.214E-01 l.802E-01 3.433E-01 NOT IDENT. TH-229 -l.267E-01 4.297E-01 7.703E-01 FAIL ABUN TH-231 -l.114E-01 4.941E-01 9.646E-01 FAIL ABUN PA-233 2.157E-02 4.847E-02 1.012E-01 NOT IDENT. PA-234 -4.405E-02 2.375E-01 4.692E-01 FAIL ABUN PA-234M 6.816E+OO 6.236E+OO 7. 961E+OO FAIL ABUN NP-237 2.157E-02 4.847E-02 1.012E-01 FAIL ABUN NP-238 O.OOOE+OO 4.139E+40 O.OOOE+OO SHORT HLIF NP-239 -1.309E-01 2.234E-01 3. 710E-01 FAIL ABUN PU-239 O.OOOE+OO 6.267E+02 5.819E+02 FAIL ABUN AM-241 -1.059E-02 1.126E-01 2.068E-01 NOT IDENT. CM-243 -6.749E-02 7. 911E-02 1.421E-01 FAIL ABUN BK-247 -3.673E-03 6.076E-02 1.167E-01 FAIL ABUN CM-247 -8.305E-03 3.172E-02 6. 061E-02 FAIL ABUN CF-249 -2.462E-02. 3.240E-02 5.873E-02 NOT IDENT. CF-251 -3.022E-02 9. 719E-02 1. 758E-01 NOT IDENT. Page 4628 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:48:37.26 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 348 10.66* 1.122E+OO 1.291E+Ol 1.291E+Ol 10.97 CD-109 88.03 79 3.70* 5.724E+OO 1.664E+OO 2.583E+OO 75.67 SN-126 64.28 31 9.60 3.489E+OO 4.059E-01 4.059E-01 193.59 8 6. 94 79 8.90 5. 724E+OO 6.918E-01 6.918E-01 75.67 87.57 79 37.00* 5.724E+OO l.664E-01 1.664E-01 75.67 TL-208 277.37 30 6.60 4.378E+00 4. 681E-01 4. 681E-Ol 99.58 583.19 123 85.00* 2.366E+00 2. 719E-01 2.719E-01 26.46 860.56 ------12.50 1.736E+OO ------Line Not Found ------PB-210 46.54 56 4.25* l.120E+00 5.209E+OO 5.341E+OO 126. 67 BI-211 72. 87 ------1. 23 4. 591E+OO ------Line Not Found ------351. 06 331 12.92* 3.592E+OO 3.172E+OO 3.172E+OO 17.12 PB-212 74.82 178 10.28 4.782E+OO 1.605E+OO 1.605E+OO 38.77 77 .11 323 17.10 4.994E+00 1.679E+OO l.679E+OO 23.00 238.63 480 43.60* 4.931E+OO 9.923E-01 9.923E-01 12. 62 300.09 ------3.30 4.103E+00 ------Line Not Found ------BF-214 609.32 202 45.49* 2.284E+OO 8.628E-01 8.631E-01 23.39 1120.29 32 14.92 l.405E+00 6.739E-01 6.741E-01 75.57 1764.49 30 15.30 9.422E-01 9.156E-01 9.159E-01 55.98 PB-214 74.82 178 5.80 4.782E+00 2.845E+OO 2.846E+OO 38.77 77 .11 323 9.70 4.994E+00 2.960E+OO 2. 961E+OO 23.00 87.09 79 3.41 5.724E+00 1.806E+OO 1.806E+OO 75.67 242.00 115 7.25 4.883E+00 1.446E+OO l.447E+OO 42.06 295.22 246 18.42 4.159E+OO 1.426E+OO 1.427E+OO 24.36 351. 93 331 35.60* 3.592E+OO 1.151E+OO 1. 152E+OO 17.12 RN-222 609.32 202 45.49* 2.284E+00 8.628E-01 8.631E-01 23.39 1120.29 32 14.92 l.405E+00 6.739E-01 6.741E-01 75.57 1764.49 30 15.30 9.422E-01 9.156E-01 9.159E-01 55.98 RA-224 240.99 115 4.10* 4.883E+OO 2.557E+OO 2.557E+OO 42.06 RA-226 609.32 202 45.49* 2.284E+00 8.628E-01 8. 631E-01 23.39 1120.29 32 14.92 l.405E+00 6.739E-01 6.741E-01 75.57 1764.49 30 15.30 9.422E-01 9.156E-01 9.159E-01 55.98 AC-228 105.21 ------1.10 6.488E+00 ------Line Not Found ------338.32 103 11.27 3.713E+00 1.088E+OO 1.088E+OO 45.09 794.95 ------4.25 1.849E+OO ------Line Not Found ------835.71 ------1. 61 l.777E+00 ------Line Not Found ------911. 20 55 25.80* l.659E+00 5.680E-01 5.680E-01 60.24 968. 97 65 15.80 1.580E+OO 1.148E+OO l.148E+OO 31. 90 RA-228 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 103 11. 27 3. 713E+00 . 1.088E+OO 1.088E+OO 45.09 794.95 ------4.25 1.849E+OO ------Line Not Found ------835.71 ------1. 61 1.777E+00 ------Line Not Found ------911. 20 55 25.80* 1.659E+00 5.680E-01 5.680E-01 60.24 968. 97 65 15.80 1.580E+OO 1.148E+OO 1.148E+OO 31. 90 TH-228 74.82 178 10.28 4.782E+00 1.605E+OO 1.605E+OO 38.77 77 .11 323 17.10 4.994E+00 1. 679E+OO 1. 679E+OO 23.00 238.63 480 43.60* 4.931E+00 9.923E-01 9.923E-01 12. 62 300.09 ------3.30 4.103E+OO ------Line Not Found ------Page 4629 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235074 Acquisition date 3-0CT-2016 06:46:37 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi7GRAM %Error TH-230 609.32 202 .45.49* 2.284E+OO 8.628E-01 8.628E-01
  • 23.39 1120.29 32 14.92 l.405E+OO 6.739E-01 6.739E-01 75.57 1764.49 30 15.30 9.422E-01 9.156E-01 9.156E-01 55.98 PA-231 283.69 ------1. 70 4.298E+OO ------Line Not Found ------301.36 35 5.35* 4.074E+OO 7.154E-01 7.154E-01 122.52 TH-232 105.21 ------1.10 6.488E+OO ------Line Not Found ------338.32 103 11. 27 3. 713E+OO 1.088E+OO 1.088E+OO 45.09 835.71 ------1. 61 1.777E+OO ------Line Not Found ------911. 20 55 25.80* 1.659E+OO 5.680E-01 5.680E-01 60.24 968.97 65 15.80 1.580E+OO 1.148E+OO 1.148E+OO 31. 90 TH-234 63.29 31 3.70* 3.489E+OO 1.053E+OO 1.053E+OO 193.59 92.59 41 4.23 6.082E+OO 7.081E-01 7.081E-01 185.99 U-234 609.32 202 45.49* 2.284E+OO 8.628E-01 8.628E-01 23.39 1120.29 32 14.92 1.405E+OO 6.739E-01 6.739E-01 75.57 1764.49 30 15.30 9.422E-01 9.156E-01 9.156E-01 55.98 U-235 89. 96 ------3.47 5.903E+OO ------Line Not Found ------93.35 41 5.60 6.082E+OO 5.348E-01 5.348E-01 185.99 143.76 ------10.96* 6.563E+OO ------Line Not Found ------163.33 ------5.08 6.266E+OO ------Line Not Found ------185. 72 104 57.20 5.850E+OO 1.384E-01 l.384E-01 65.53 205.31 31 5.01 5.507E+OO 5.048E-01 5.048E-01 128.45 U-238 63.29 31 3.70* 3.489E+OO 1.053E+OO 1.053E+OO 193.59 92.59 41 4.23 6.082E+OO 7. 081E-01 7. 081E-01 185.99 AM-243 43.53 ------5.90 6.933E-01 ------Line Not Found ------74.66 178 67.20* 4.782E+OO 2.455E-01 2.456E-01 38.77 ANH-511 511. 00 40 100.00* 2.632E+OO 6.672E-02 6.672E-02 131.38 Flag: "*" Key line Page 4630 of 5809 Summary of Nuclide Activity Sample ID : G405235074 Acquisition date Page : 3 3-0CT-2016 06:46:37 Total number of lines in spectrum 47 Number of unidentified lines 10 Number of lines tentatively identified by NID 37 Nuclide Type : Nuclide K-40 CD-109 SN-126 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1.25E+09Y 461. 40D 2.30E+05Y l.41E+10Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600. OOY 1600.00Y 1600.00Y 1. 41E+l0Y 1600.00Y 1.41E+10Y 1.41E+10Y l.41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 1. 55 1. 00 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.291E+Ol l.664E+00 l.664E-01 2.719E-01 5.209E+00 3.172E+00 9.923E-01 8.628E-01 1.151E+00 8.628E-01 2.557E+00 8.628E-01 5.680E-01 5.680E-01 9.923E-01 8.'628E-01 7.154E-01 5.680E-01 1.053E+00 8.628E-01 1.384E-01 l.053E+00 2.455E-01 6.672E-02 3.838E+01 3.838E+Ol Decay Corr pCi/GRAM l.291E+Ol 2.583E+OO 1.664E-01 2.719E-01 5.341E+OO 3 .172E+OO 9.923E-01 8.631E-01 l.152E+OO 8. 631E-01 2.557E+OO 8.631E-01 5.680E-01 5.680E-01 9.923E-01 8.628E-01 7.154E-01 5.680E-01 1.053E+OO 8.628E-01 l.384E-01 1.053E+OO 2.456E-01 6. 672E-02 3.943E+Ol 3.943E+Ol 78.72% . Decay Corr 2-Sigma Error 0.142E+Ol 1.955E+OO 1.259E-01 0.719E-01 6.765E+OO 0.543E+OO 1.253E-01 2.019E-01 0.197E+OO 2.019E-01 1. 076E+OO 2.019E-01 3.422E-01 3.422E-01 1.253E-01 2.018E-01 8.765E-01 3.422E-01 2.039E+OO 2.018E-01 0.907E-01 2.039E+OO 0.952E-01 8.766E-02 "M" Manually accepted 2-Sigma %Error 10.97 75.67 75.67 26. 46 126.67 17.12 12. 62 23.39 17.12 23.39 42.06 23.39 60.24 60.24 12. 62 23.39 122.52 60.24 193.59 23.39 65.53 193.59 38.77 131. 38 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4631 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235074 Acquisition date : 3-0CT-2016 06:46:37 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 118.70 46 111 0.75 237.87 234 7 9.54E-03 95.3 6.68E+OO T 0 129.94 65 178 1. 69 260.35 255 10 1.37E-02 93.8 6.68E+OO T 0 209.40 49 105 0.90 419.23 415 8 l.08E-02 87.5 5.42E+00 T 0 270.04 .. 48 67 1. 63 540.48 536 9 1. lOE-02 75.5 4.47E+OO T 1 281.69 31 52 1. 45 563.77 552 15 7.05E-03 97.5 4.32E+OO T 0 463.85 43 46 1. 85 928.01 922 14 1.06E-02 78.7 2.85E+OO T 0 564.19 38 24 3.16 1128.65 1121 15 9.46E-03 69.6 2.43E+OO T 0 727.17 31 14 1. 43 1454.56 1450 11 7.95E-03 64.5 1.98E+OO T 0 744.83 21 12 2.49 1489.87 1485 9 5.55E-03 78.5 1.95E+OO 0 768.72 18 13 1. 50 1537.64 1533 8 4.77E-03 87.9 1. 90E+OO 0 803.54 19 3 3.94 1607.28 1601 12 5.05E-03 70.7 1. 83E+00 0 894.73 15 20 0.61 1789.64 1781 14 3.94E-03 **** l.68E+00 T 0 927.72 16 9 2.38 1855.60 1851 11 4.25E-03 89.4 l.64E+OO T 0 934 .11 16 6 2.53 1868.38 1865 8 4.29E-03 74.4 1. 63E+OO 0 954.52 8 4 0.97 1909.19 1906 6 2.15E-03 **** l.60E+OO T 0 965. 47 7 23 2.09 1931.10 1922 12 1. 8 6E-03 **** l.58E+OO T 0 1002.17 20 13 4.53 2004.47 1998 14 5.36E-03 93.4 1. 54E+OO T 0 1144. 39 17 7 1. 71 2288.89 2284 10 4.67E-03 77.8 l.38E+00 0 1161. 83 15 10 0.86 2323.75 2317 12 4.23E-03 **** 1.36E+OO 0 1237.69 19 14 2.49 2475.47 2470 11 5.34E-03 87.6 1.29E+OO T 0 1248.96 14 17 0.69 2498.00 2491 13 3.90E-03 **** l.28E+OO 0 1328. 22 5 11 l .'45 2656.52 2649 14 1.49E-03 **** 1. 22E+00' 0 1376.11 11 3 3.18 2752.28 2747 11 3.09E-03 83.6 l.18E+OO 0 1391. 7 9 11 3 3.33 2783.64 2777 12 3. llE-03 85.8 1. l 7E+OO Flags: "T" = Tentatively associated Page 4632 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:48:51.51 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA ** * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235074.CNF;l *
  • Acquisition date 3-0CT-2016 06:46:37 Sensitivity 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.52 Half life ratio : ***** *
  • Sample date 15-DEC-2015 14:10:00 Nuclide Library : SOLID *
  • Sample ID G405235074 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity : 1.6907E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 19-AUG-2016 11:09:59 Eff. Geometry : CAN *
  • Eff. File' : DKA100: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.534E-01 9.754E-01 5.917E-02 2.469E-02 1. 964E+OO 3.557E-02 5.150E-02 5.093E-02 5.150E-02 3.814E-01 5.150E-02 1.132E-01 l .132E-01 3.557E-02 5.148E-02 3.499E-01 1.132E-01 8.823E-01 5.148E-02 1. 274E-01 8.823E-01 3.667E-02 l.950E-02 ----Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4633 of 5809 Le (pCi/GRAM 8.797E+OO 3.681E-02 O.OOOE+OO 1.132E-02 2.919E-01 O.OOOE+OO O.OOOE+OO 4.406E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 Page 4634 of 5809 3.992E-01 O.OOOE+OO 3.426E-02 3.217E-01 4.151E+OO 3.560E-02 1.448E-01 1.910E+OO 5.947E+OO O.OOOE+OO 1. 501E-01 O.OOOE+OO O.OOOE+OO 4.525E-01 5.995E+OO 5.875E-01 0.000E+OO 1.095E-01 3.635E+02 2.640E-02 6.165E-01 1.670E+OO 9. 301E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO . 2.409E-02 4.035E-02 3.579E+OO 3.491E-01 3.491E-01 l.978E-02 7.349E-02 1. 748E-01 O.OOOE+OO 0.000E+OO 9.187E-02 l.450E+OO 7.586E-02 1.771E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.665E-02 O.OOOE+OO 4.903E-02 1. 072E-01 O.OOOE+OO O.OOOE+OO 2.559E-02 2.703E-02 8.905E-02 O.OOOE+OO O.OOOE+OO l.439E+Ol O.OOOE+OO 2.639E-01 4.133E-02 3.566E+OO 3.393E-02 O.OOOE+OO 5.934E+02 O.OOOE+OO 1. 607E-02 6.453E-02 1.084E-01 9.197E-02 8. 968E-02 1.160E+OO 4.855E-02 1.518E+Ol 1. 728E-01 7.300E-02 1.908E-02 FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4635 of 5809 2.635E+OO 7.453E-01 1.829E+OO 2.194E+01 6.854E+Ol 3.260E-01 1.552E+OO 3.176E-02 3.791E-01 5.025E-01 2.981E-01 4.409E-01 l.572E-01 l.572E-01 3. 596E-01 4.409E-01 4.644E-02 2.027E-01 3.505E+OO 4.644E-02 O.OOOE+OO 1. 731E-01 2.755E+02 9.722E-02 6.605E-02 5.367E-02 2.757E-02 2.646E-02 8.167E-02 NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:48:56.91 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235074.CNF;l *
  • Acquisition date 3-0CT-2016 06:46:37 Sensitivity : 3.000 *
  • Detector ID GAM07 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.52 Half life ratio : ***** *
  • Sample date 15-DEC-2015 14:10:00 Nuclide Library : SOLID *
  • Sample ID G405235074 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.6907E+02 GRAM *
  • Quantity Err ( % ) : 1.1830E-03 % *
  • Wet wt corr : 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 19-AUG-2016 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM07 CAN.CNF;l5
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) K-40 1.291E+Ol 1.543E+OO l.543E+OO CD-109 5.431E-01 1. 993E+OO 1.993E+OO SN-126 3.499E-02 1. 284E-01 l.284E-01 TL-208 2.719E-01 7.144E-02 7.144E-02 PB-210 5.341E+OO 6.645E+00 6.645E+OO PB-212 9.923E-01 l.336E-01 l.336E-01 BI-214 8.631E-01 2. 013E-01 2.013E-01 PB-214 1.152E+OO 1.990E-01 1.990E-01 RN-222 8.631E-01 2.013E-01 2.013E-01 RA-224 3.579E-02 1.225E+OO 1.225E+OO RA-226 8.631E-01 2.013E-01 2. 013E-01 AC-228 5.680E-01 3.366E-01 3.366E-01 RA-228 5.680E-01 3.366E-01 3.366E-01 TH-228 9.923E-01 1.336E-01 1.336E-01 TH-230 8.628E-01 2.012E-01 2.012E-01 PA-231 7.154E-01 8. 725E-01 8. 725E-01 TH-232 5.680E-01 3.366E-01 3.366E-01 TH-234 1. 053E+OO 2.012E+OO 2.012E+OO U-234 8.628E-01 2.012E-01 2.012E-01 U-235 1.094E-02 1.439E-01 1.439E-01 U-238 1.053E+OO 2.012E+OO 2.012E+OO AM-243 1.225E-01 9.935E-02 9.935E-02 ANH-511 6. 672E-02 8.595E-02 8.595E-02 Non-Identified Nuclides Key-Line K.L Act error Activity TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 l.379E+00 9.796E+OO 9.816E+OO NOT IDENT. NA-22 1.616E-02 3.988E-02 4.054E-02 NOT IDENT. NA-24 l.OOOE+41 1.861E+41 O.OOOE+OO SHORT HLIF AL-26 -1.698E-02 2.138E-02 2.271E-02 NOT IDENT. SC-46 3.538E-02 3.649E-01 3.652E-01 FAIL ABUN V-48 -l.384E+03 9. 221E+03 9.242E+03 SHORT HLIF CR-51 4.274E+Ol 2.936E+02 2.942E+02 SHORT HLIF Page 4636 of 5809 MN-54 -1.193E-03 4.952E-02 4.952E-02 NOT IDENT. C0-56 1.121E-01 4.324E-01 4.354E-01 FAIL ABUN MN-56 1.000E+41 3.951E+41 O.OOOE+OO SHORT HLIF C0-57 1.245E-03 4.138E-02 4.138E-02 NOT IDENT. C0-58 -l.831E-01 4.291E-01 4.370E-01 NOT IDENT. FE-59 7.519E-01 4. 631E+OO 4.644E+OO NOT IDENT. C0-60 1. 621E-02 4.336E-02 4.397E-02 NOT IDENT. ZN-65 1. 749E-02 1.862E-01 1. 864E-01 NOT IDENT. GE-68 -6.209E-01 2.299E+OO 2.315E+OO NOT IDENT. AS-.7 3 5.133E+OO 5. 972E+OO .6.405E+OO NOT IDENT. AS-74 -7.415E+Ol 4.002E+03 4.002E+03 SHORT HLIF SE-75 1.098E-02 1.604E-01 1.605E-01 NOT IDENT. BR-77 2.227E+37 l.882E+38 O.OOOE+OO SHORT HLIF SR-82 1.991E+02 5.139E+02 5.217E+02 SHORT HLIF RB-83 -2.077E-01 5.494E-01 5.573E-01 NOT IDENT. KR-85 5.421E+OO 6.183E+OO 6.649E+OO NOT IDENT. SR-85 5.304E-01 6.060E-01 6.515E-01 NOT IDENT. RB-86 -2.099E+03 2.165E+04 2.167E+04 SHORT HLIF Y-88 -l.139E-01 l.711E-01 1.786E-01 NOT IDENT. Y-91 -8.441E+Ol 4.387E+02 4.404E+02 NOT IDENT. NB-94 1.578E-02 2.871E-02 2.958E-02 NOT IDENT. NB-95 7.035E-01 6.537E-01 7.266E-01 NOT IDENT. NB-95M 8.784E-01 1. 879E+OO 1. 921E+OO NOT IDENT. ZR-95 4. 396E-01 1.016E+OO 1.035E+OO NOT IDENT. NB-97 -l.000E+41 2.671E+41 O.OOOE+OO SHORT HLIF ZR-97 -l.OOOE+41 l.242E+42 O.OOOE+OO SHORT HLIF M0-99 -2.867E+30 3.026E+31 O.OOOE+OO SHORT HLIF TC-99M -1. OOOE+41 l.921E+41 O.OOOE+OO SHORT HLIF RH-101 -1.570E-02 3 .115E-02 3.194E-02 NOT IDENT. RH-102 -2.730E-02 5.190E-02 5.334E-02 NOT IDENT. RU-103 -l.949E+OO 4.365E+OO 4.452E+00 FAIL ABUN RH-106 3.814E-01 3.344E-01 3.760E-01 NOT IDENT. RU-106 3.814E-01 3.344E-01 3.760E-01 NOT IDENT. AG-108M l.630E-03 2. 201E-02 2.202E-02 NOT IDENT. AG-llOM 2.177E-02 7.902E-02 7.962E-02 NOT IDENT. SN-113 4.530E-02 l.894E-01 1.905E-01 NOT IDENT. CD-115 -2.862E+38 2.857E+38 0.000E+OO SHORT HLIF SN-ll 7M -1. 371E+03 5.789E+04 5.789E+04 SHORT HLIF TE-123M -7.530E-02 1.121E-01 1.171E-01 NOT IDENT. SB-124 -l.410E-01 1.804E+OO 1.805E+OO NOT IDENT. SB-125 2.016E-02 8.249E-02 8.299E-02 FAIL ABUN TE-125M -5. 511E+Ol 2.021E+02 2.036E+02 NOT IDENT. I-126 -2.982E+05 5.232E+05 5.402E+05 SHORT HLIF SB-126 1.339E+05 6. 831E+05 6.857E+05 SHORT HLIF SB-127 1. 725E+21 5.789E+21 O.OOOE+OO SHORT HLIF I-131 l.107E+08 2.372E+09 2.372E+09 SHORT HLIF I-132 l.000E+41 1.828E+42 O.OOOE+OO SHORT HLIF TE-132 5.041E+25 7.923E+25 O.OOOE+OO SHORT HLIF BA-133 1.648E-02 2.978E-02 3.069E-02 FAIL ABUN I-133 1.000E+41 l.953E+41 O.OOOE+OO SHORT HLIF CS-134 4.064E-02 5.276E-02 5.585E-02 FAIL ABUN CS-135 4.233E-02 1.229E-01 1.244E-01 NOT IDENT. I-135 1.000E+41 7.434E+41 O.OOOE+OO SHORT HLIF CS-136 3.186E+04 1.702E+05 1. 709E+05 SHORT HLIF BA-137M 3.669E-03 2. 941E-02 2.946E-02 NOT IDENT. CS-137 3.876E-03 3.107E-02 3.112E-02 NOT IDENT. CE-139 -2.574E-03 1.022E-01 1.022E-01 NOT IDENT. BA-140 -l.893E+05 7.914E+05 7. 960E+05 SHORT HLIF LA-140 -l.903E+05 2.332E+05 2.485E+05 SHORT HLIF CE-141 -4.315E+OO 1.672E+Ol 1.684E+Ol NOT IDENT. CE-143 1.000E+41 6.081E+40 O.OOOE+OO SHORT HLIF CE-144 -2.569E-02 3. 251E-01 3.253E-01 NOT IDENT. PM-144 9.287E-03 4.718E-02 4.737E-02 NOT IDENT. PR-144 7.641E-01 4.077E+OO 4.092E+OO NOT IDENT. PM-146 1.456E-02 3.640E-02 3.698E-02 NOT IDENT. ND-147 9.381E+06 1.656E+07 1. 709E+07 SHORT HLIF PM-147 3.898E+02 6.731E+02 6.957E+02 NOT IDENT. PM-149 -l.804E+39 3.937E+39 O.OOOE+OO SHORT HLIF EU-150 -9.227E-03 2 .114E-02 2.154E-02 FAIL ABUN EU-152 -4.740E-02 8.637E-02 8.897E-02 FAIL ABUN GD-153 -2.473E-01 1.426E-01 1.810E-01 NOT IDENT. EU-154 4.404E-02 9.902E-02 1.0lOE-01 NOT IDENT. EU-155 5.616E-02 9.482E-02 9.814E-02 FAIL ABUN TB-160 -1.526E-01 1.334E+OO 1.336E+OO FAIL ABUN H0-166M 4.475E-02 5.018E-02 5.409E-02 FAIL ABUN TM-171 7.249E+00 1.547E+Ol 1. 581E+Ol NOT IDENT. HF-172 -6.858E-03 2.106E-01 2.107E-01 FAIL ABUN LU-172 6.000E-02 7.518E-02 7.990E-02 FAIL ABUN Page 4637 of 5809 LU-176 2.334E-02 1.983E-02 2.245E-02 FAIL ABUN HF-181 -1.163E+OO 3.168E+OO 3. 211E+OO NOT IDENT. TA-182 -2.031E-01 9.016E-01 9.063E-01 FAIL ABUN RE-183 -1.566E+OO 2.080E+OO 2 .196E+OO NOT IDENT. RE-184 4.132E+OO 2.415E+Ol 2.422E+Ol FAIL ABUN W-188 -2.021E+Ol 8.558E+Ol 8.606E+Ol FAIL ABUN IR-192 -l.709E-01 3.782E-01 3.860E-01 FAIL ABUN HG-203 -1.304E+OO 1. 8 OlE+OO 1.895E+OO NOT IDENT. BI-207 -7.806E-03 3.805E-02 3.822E-02 FAIL ABUN BI-21.1 3. l 72E+OO 5.506E-01 l .;532E+OO FAIL ABUN PB-211 -l.405E-02 6.006E-01 6.006E-01 NOT IDENT. BI-212 1. 031E+OO 6.535E-01 8.020E-01 FAIL ABUN RN-219 -8.120E-02 3.421E-01 3. 441E-01 FAIL ABUN RA-223 -l .114E-01 4.942E-01 4. 967E-01 FAIL ABUN AC-227 -1.214E-01 1. 809E-01 l.890E-01 NOT IDENT. TH-227 -l.214E-01 1.809E-01 1. 890E-01 NOT IDENT. TH-229 -1. 2 67E-01 4.297E-01 4.335E-01 FAIL ABUN TH-231 -1.114E-01 4.942E-01 4. 967E-01 FAIL ABUN PA-233 2.157E-02 4.849E-02 4.945E-02 NOT IDENT. PA-234 -4.405E-02 2.428E-01 2.436E-01 FAIL ABUN PA-234M 6.816E+OO 6.243E+OO 6.958E+OO FAIL ABUN NP-237 2.157E-02 4.849E-02 4.945E-02 FAIL ABUN NP-238 4.525E+39 4.139E+40 O.OOOE+OO SHORT HLIF NP-239* -l.309E-01 2.237E-01 2.313E-01 FAIL ABUN PU-239 6.817E+02 6.274E+02 6.986E+02 FAIL ABUN AM-241 -l.059E-02 1. 12 6E-01 1.127E-01 NOT IDENT. CM-243 -6.749E-02 7.936E-02 8.499E-02 FAIL ABUN BK-247 -3.673E-03. 6.076E-02 6.078E-02 FAIL ABUN. CM-247 -8.305E-03 3.175E-02 3.197E-02 FAIL ABUN CF-249 -2.462E-02 3.247E-02 3. 431E-02 NOT IDENT. CF-251 -3.022E-02 9. 725E-02 9.820E-02 NOT IDENT. Page 4638 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 77.3828 87.09 105.0629 136.47 81. 7833 45.60 59.3371 87.57 121. 9809 140.51 0.0000 46.54 59.4930 88.03 138.9237 143.76 59.6465 49. 72 0.0000 88.34 139.0022 144.24 65.4227 51. 35 70.9588 88.47 109.5431 145.44 67.8253 51. 87 63.2678 89. 96 118.2899 152.43 73.0783 52.39 71.1501 1093.63 122.6650 153.25 0.0000 52.97 63.4471 91.11 0.0000 323.87 65.1046 53.44 60. 5911 92.59 103.9934 156.02 0.0000 54.07 86.1376 93.35 104 .1332 158.56 0.0000 57.36 0.0000 94.56 55.3722 159.00 79.5277 57.53 87.8647 94.65 55.3809 162.33 79.8514 57.98 87.9597 94.67 55.3829 162.66 -o. 0000 59.27 86.2490 94.87 55.4023 163.33 101.1106 59.32 86.2592 97.43 87.7531 165.86 82.5504 59.54 84.6510 98.43 67.5359 176.31 54.9142 60. 96 80.9530 98.44 67.5369 176.60 0.0000 61.17 98.2530 99.53 54.7739 177.52 64.5535 62.93 97.9864 100.11 70.9533 181.07 0.0000 63.29 98.0669 102.03 80.8891 181.52 59.2420 63.58 98.1318 103.18 78.8819 184.41 61.0395 64.28 89.5952 103.37 78.9070 143.76 63.9427 66.73 73.9510 105.21 76.9770 193.51 73.0042 67.24 89.8501 105.31 76.9894 197.03 78.1631 125.81 101. 0529 106.12 78.1771 198.01 47.6800 67.75 101.0681 106.47 80.3938 201.83 42.5520 69.67 103.5183 109.28 67.6616 203.43 52.4590 70.83 94.9569 111. 00 72. 2227 205.31 54.2031 72.81 102.1629 111. 76 0.0000 210.85 54.5099 72. 87 102.1759 114. 06 70.3691 215.65 51.0373 74.66 104.6046 116.30 0.0000 222 .11 54.2850 74.82 104.6389 116.74 80.9631 227.09 61.2596 74.97 104.6716 119.76 63.5875 227.38 53.7220 77 .11 105.1252 121.12 54.8255 228.16 0.0000 78. 74* 89.6124 121.22 51. 8698 228.18 63.8436 79.69 96.6865 121.78 51.9129 116.74 63.8436 80.12 89.8557 122.06 66.7726 235.69 50.7611 80.19 0.0000 122.92 78.0002 235. 96 48.2349 80.57 76.0989 123.07 78.0173 238.63 47.5063 81. 00 84.4707 265.00 73.6246 238.98 0.0000 81. 07 81.7126 125.81 74.5992 240.99 47.6095 81. 75 106.0887 127.23 80.7317 242.00 47.6533 83.79 94.6697 127.91 65.8458 244.70 62.6990 84.00 97.4933 129.30 61.8523 252.40 0.0000 85.43 111.7212 131.20 61. 6426 252.80 38.6664 86.55 104.9576 133.02 67.8287 254.15 0.0000 86.79 105.0041 133. 52 73.9097 256.23 51.7114 86.94 105.0339 136.00 80.5954 260.90 0.0000 Page 4639 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 43.4082 355.39 0.0000 584.27 20.6569 264.80 43.7616 356.01 18.1555 595.83 0.0000 265.00 44.8109 364.49 0.0000 427.87 28.8204 268.22 41.7988 366.42 0.0000 602.52 0.0000 269.46 40.0993 372.51 32. 0113 604.72 24.0628 270.03 40.1190 33.9514 607.14 32 .1191 271.23 37.9767 377.52 23.6160 609.32 24.6499 273.65 0.0000 356.01 24.6628 610.33 24.6612 276.40 59.1847 388.16 39.9509 614.28 33.8353 277.37 54.4052 388.63 0.0000 618.01 24.7473 277.60 54.4165 391. 69 30.5078 620.36 21.5422 278.00 54.4342 264.66 23.0117 621.93 6.4673 279.20 54.4884 401.81 37.4210 630.19 0.0000 279.54 54.5035 402.40 38.3952 631. 29 22.7303 279.70 54.5098 404.85 35.5697 633.25 17.3333 280.46 54.5439 410.95 34.7402 634.78 0.0000 283.69 43.6630 413.71 27.0663 635.95 19.5234 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 32.8588 423.72 0.0000 645.85 11. 9829 285.90 0.0000 427.09 16.5670 657.76 24.0903 287.50 38.0467 427.87 23.3999 657.90 0.0000 290.67 37.2559 433.94 23.4849 661. 66 18.6463 293.27 0.0000 439.40 27.4873 664.57 0.0000 351.93 36.0555 453.88 22.7693 666.33 0.0000 295. 96 36.0769 463.37 22.8924 666.50 0.0000 879.38 16.0671 468.07 17.9634 667.71 0.0000 299.98 40.2118 473.00 0.0000 677.62 ' 20. 9815 300.09 40.2155 475.06 24.0444 685.70 0.0000 300.13 40.2173 476.78 27.0758 695.00 0.0000 301. 36 48.3069 477.60 25.0814 696. 49 17.8079 302.85 48.3629 482.18 25.1450 696. 51 17.8079 256.23 34.9732 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 15.5871 306.78 22.9076 497.08 27.3763 697.49 16.7017 308.46 43.1748 505.52 24.4438 702.65 17.8529 311. 90 34.2705 507.63 0.0000 706.68 18.9998 316.51 43.4395 511. 00 22.4713 711. 68 13.4390 319.41 0.0000 514.00 22.5067 720.70 0.0000 320.08 0.0000 514.00 22.5067 721. 93 0.0000 321.04 37.2305 520.40 26.6877 722.78 18.5612 323.87 41. 8588 520.69 0.0000 722. 91 18.5625 325.23 40.0782 522.65 0.0000 723. 31 16.8774 328.76 0.0000 527.90 0.0000 724.19 16.8835 333.37 26.1146 528.26 23.7038 727.33 21. 4121 333.97 34.3765 529.59 8.2503 733.00 16.2650 334.37 34.3864 529.87 0.0000 735.93 15.8315 338.28 28.5056 531.02 0.0000 333.97 12.4466 338.32 28.5069 537.26 0.0000 739.50 0.0000 311. 90 28.5504 546.56 0.0000 747.24 17.0374 340.48 28.5504 552.55 22.9507 748.06 8.5214 340.55 0.0000 563.25 16.7793 752.31 23.8993 344.28 40.1706 569.33 12.6216 753.82 0.0000 345.93 31.8966 946.00 12.6226 756.73 10.2601 351.06 35.2593 569.70 6. 3118 756.80 10.2605 351. 93 35.2802 583.19 21.1751 884.68 13.7183 Page 4640 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 8.5800 1274.44 14.8569 1620.50 5.4312 766.42 17 .1643 1001.03 11.1592 1621.92 8.6924 766.84 17.1667 1002.74 11.1650 1678.03 0.0000 772.60 0.0000 1004.73 8.9376 1690.97 5. 5096 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 .0.0000 1025.87 0.0000 .J.764.49 5.5899 778.90 20.6946 1028.54 0.0000 1063.66 5. 5960 783.70 0.0000 1037.84 14.1055 1771.35 1.1194 785.37 17.2876 1038.76 0.0000 1791.20 0.0000 792.07 27.7295 631.29 11. 3145 1808.65 4.5098 794.95 16.1926 1048.07 0.0000 1810.72 0.0000 795.86 19.6694 1049.04 14.1531 1836.06 5.4398 810.06 12.7939 1050.41 11. 32 69 810.29 12.7948 1063.66 12.3192 344.28 13. 9590 1077.00 0.0000 810.76 13. 9604 1077.34 19.0283 815.77 0.0000 1085.87 13.3523 1048.07 0.0000 1093.63 12.4263 832.01 20.2226 1099.45 9.5752 834.85 14.9622 1112. 07 10.5703 835. 71 16.7276 1112. 84 8.7874 836.80 .0.0000 1115. 54 16.9286 846.75 0.0000 1120.29 16.3733 846.77 19.4454 1120.55 16.3754 856.80 0.0000 1221.41 16.3785 860. 56 12.4341 1129.67 11. 5884 871.09 14.2622 1131. 51 0.0000 873.19 12.4884 1147.95 0.0000 875.33 0.0000 1173.23 8. 7962 879.38 12.5153 1177.95 17.6144 880.51 12.5200 1189.05 17.6671 883.24 12.5316 1204.77 15. 7705 884.68 11. 6424 1221.41 20.7898 889.28 15.7862 1231.02 7.9395 894.76 15.2766 1235.36 0.0000 898.04 12.9546 1238.28 17.5001 900.72 15.4358 1260.41 0.0000 903.28 16.2213 1271.87 18.0527 911. 20 20.7827 1274.44 9.0324 912.08 20.7883 1274.54 9.0324 923.98 0.0000 1291. 59 20.1587 926.50 13.0777 1298.22 0.0000 929 .11 19.3906 1312 .11 0.0000 937.49 7.2915 1332. 49 9.7746 944.13 0.0000 1362.66 0.0000 946.00 15.5370 1365.19 6.1575 949.00 14.6372 1368.63 0.0000 667.71 0.0000 1384.29 9.4258 962. 31 13.2297 1408.01 8.2935 964.08 19.1204 1457.56 0.0000 966 .17 0.0000 1460.82 8.3945 911. 20 11. 7848 1489.16 4.2241 968. 97 11.7848 1505.03 6.3585 983.53 0.0000 1584.12 14.0140 984.45 0.0000 1596.21 0.0000 Page 4641of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 11:49:10.15 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235075.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM18.CNF;511 Background date : Z-OCT-2016 11:01:02. Sample date 16-DEC-2015 09:31:00 Acquisition date : 3-0CT-2016 06:47:01. Sample ID G405235075 Sample quantity 1.51411E+02 GRAM Detector name : GAM18 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.97 0.0% Energy tolerance 2.00000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 3 3 0 4 4 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4642 of 5809 Energy 74.64 77.07* 86.99 89. 96 92.84* 124.62 128.95 186.41* 214.25 238.84* 241. 7 9 259.99 270.61 285.78 295.47* 300.86 338.67* 352.28* 425.73 431.33 438.51 463.97 476.44 485.39 511.42* 583.82* 609.82* 697.07 721.82 727.32 795.87* 862.42 911. 76* 935.82 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 121 201 81 61 112 25 27 92 35 380 128 19 60 19 205 38 90 339 14 22 55 69 27 36 31 162 283 23 28 49 29 28 142 25 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 140 166 158 122 163 83 112 129 128 102 114 64 107 76 96 85 75 91 45 41 60 30 39 61 112 52 59 102 24 16 24 38 30 21 1. 25 1. 26 1. 43 1. 27 1. 46 1. 45 0.80 1. 62 3.86 1.12 1. 99 1. 68 1. 91 1. 27 1. 21 1. 76 1. 54 1. 27 0.48 4.31 5.93 2 .11 3.44 8. 72 1. 57 1. 37 1. 55 6.91 2.42 2.73 1. 90 1. 26 1. 97 3.41 150.08 154.93 174.74 180.69 186 .. 44 249.95 258.60 373.44 429.07 478.21 484.10 520.48 541.69 572.01 591.38 602.16 677.71 704.92 851. 72 862.90 877.25 928.13 953.07 970.94 1022.98 1167. 68 1219.64 1394.04 1443.52 1454.51 1591.54 1724. 57 1823.19 1871.28 144 144 172 178 178 248 255 368 424 474 474 516 535 568 585 597 673 698 844 856 8 68 922 948 959 1014 1160 1213 1363 1435 1450 1584 1713 1816 1863 19 3.36E-02 18.8 19 5.58E-02 13.6 7 2.24E-02 28.2 13 1. 71E-02 30. 3 13 3.llE-02 24.2 6 6.84E-03 61.5 7 7.49E-03 68.2 10 2.57E-02 26.7 11 9.82E-03 64.4 19 1. 05E-01 6. 8 19 3.55E-02 25.4 8 5.30E-03 76.9 12 1. 65E-02 37. 9 10 5.19E-03 90.0 12 5.70E-02 12.0 10 l.06E-02 48.2 10 2.50E-02 21.6 13 9.42E-02 8.1 9 3.85E-03 94.1 12 6.04E-03 63.3 20 l.53E-02 37.0 15 1. 92E-02 21.1 11 7.45E-03 48.9 22 9.98E-03 59.7 18 8.63E-03 91.1 16 4.50E-02 13.0 15 7.87E-02 8.6 34 6.39E-03136.9 15 7.81E-03 43.6 9 l.37E-02 20.3 14 7.94E-03 42.4 20 7.85E-03 57.7 17 3.95E-02 12.6 17 7.02E-03 46.2 Fit 1. llE+OO 8.94E-01 2.06E+OO Peak Search Report (continued) Page : 2 Sample ID : G405235075 Acquisition date 3-0CT-2016 06:47:01 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 945.53 4 19 0.69 1890.71 1885 10 1. 24E-03221. l 36 0 950.97 48 5 5.73 1901.58 1894 18 1.33E-02 17.9 37 0 971. 05* 34 67 1.27 71 1931 15 9.42E-03 57.3 38 0 1077.34 21 8 1. 64 2154.20 2150 10 5.90E-03 32.6 39 0 1121.91* 54 49 2.02 2243.30 2233 17 1.51E-02 33.5 40 0 1155.68 34 35 0.74 2310.81 2301 23 9.32E-03 48.7 41 0 1239.87 42 36 1. 39 2479.13 2465 23 1.16E-02 42.1 42 0 1293.60 34 0 6.25 2586.56 2578 19 9.44E-03 17.1 43 0 1310.05 15 8 1. 65 2619.44 2613 11 4.llE-03 45.7 44 0 1339.54 8 9 0.68 2678.41 2673 10 2.35E-03 82.0 45 0 1378.25 24 10 3.32 2755.80 2748 14 6.57E-03 35.6 46 0 1461.62* 577 0 2.82 2922.48 2911 20 1.60E-01 4.2 47 0 1482.32 9 16 4.43 2963.87 2946 22 2. 62E-03114. 2 48 0 1766.19* 41 4 2.75 3531. 49 3522 16 1.13E-02 20. 8 Flag: "*" = Peak area was modified by background subtraction Page 4643 of 5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-201? 11:49:12 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235075.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID 16-DEC-2015 09:31:00 G405235075 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:47:01 151.41 GRAM type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA18 0 01:00:00.00 2.00 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351. 93 Page 4644 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line RA-224 240.99 TH-229 85.43 SN-126 86.94 SN-126 87.57 CD-109 88.03 TH-229 88.47 BI-211 72. 87 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:00.97 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235075 Acquisition date 3-0CT-2016 06:47:01 Nuclide Type: Uncorrected Decay Corr 2-Sigrha Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status BE-7 477.60 10.44t 4.230E+OO 3.268E-01 1.463E+Ol 97.83 . OK K-40 1460.82 10.66* 1. 911E+OO 1.356E+Ol l.356E+Ol 8.40 OK GE-68 1077.34 3.22* 2.403E+OO l.357E+OO 2.864E+OO 65.12 OK CD-109 88.03 3.70* 6. lllE+OO l.254E+OO 1.944E+OO 102.28 OK SN-126 64.28 9.60 3.252E+OO Line Not Found Absent 86.94 8.90 6. lllE+OO 5.214E-01 5.214E-01 102.28 OK 87.57 37.00* 6.lllE+OO l.254E-01 l.254E-01 102.28 OK PR-144 696. 51 1.34* 3.253E+OO 2.733E+OO 5.561E+OO 273.88 OK 1489.16 0.28 1.883E+OO Line Not Found Absent TL-208 277.37 6.60 6.127E+OO Line Not Found Absent 583.19 85.00* 3.674E+OO 2.735E-01 2.735E-01 26.03 OK 860.56 12.50 2.810E+OO 4.079E-01 4.079E-01 115. 37 OK PB-212 74.82 10.28 4.729E+OO 9.828E-01 9.828E-01 62.52 OK 77 .11 17.10 5.036E+OO 1.482E+OO 1.482E+OO 27.30 OK 238.63 43.60* 6.719E+OO 7.454E-01 7.454E-01 13 .59 OK 300.09 3.30 5.809E+OO 1.116E+OO l .116E+OO 96. 40 OK BI-214 609.32 45.49* 3.566E+OO 9.175E-01 9.178E-01 17.15 OK 1120.29 14.92 2.334E+OO 7.699E-01 7.702E-01 66.96 OK 1764.49 15.30 1.632E+OO 7.609'E-01 7. 611E-01 41.66 OK PB-214 74.82 5.80 4.752E+OO Line Not Found <<INT Reject 77 .11 9.70 5.036E+OO 2.613E+OO 2.614E+OO 27.30 OK 87.09 3.41 6 .121E+OO Line Not Found <<INT Reject 242.00 7.25 6.668E+OO Line Not Found <<INT Reject 295.22 18.42 5.879E+OO 1.069E+OO 1.069E+OO 24.01 OK 351. 93 35.60* 5.218E+OO 1.012E+OO 1.012E+OO 16.14 OK RN-222 609.32 45.49* 3.566E+OO 9.175E-01 9.178E-01 17.15 OK 1120.29 14.92 2.334E+OO 7.699E-01 7.702E-01 66. 96 OK 1764.49 15.30 1.632E+OO 7.609E-01 7. 611E-,01 41. 66 OK RA-224 240.99 4.10* 6.671E+OO 7.942E-01 7.942E-01 180.90 OK RA-226 609.32 45.49* 3.566E+OO 9.175E-01 9.178E-01 17.15 OK 1120.29 14.92 2.334E+OO 7.699E-01 7.702E-01 66. 96 OK 1764.49 15.30 1.632E+OO 7.609E-01 7. 611E-01 41. 66 OK TH-228 74.82 10.28 4.729E+OO 9.828E-01 9.828E-01 62.52 OK 77 .11 17.10 5.036E+OO 1.482E+OO l.482E+OO 27.30 OK 238.63 43.60* 6.719E+OO 7.454E-01 7.454E-01 13.59 OK 300.09 3.30 5.809E+OO l .116E+OO 1.116E+OO 96. 40 OK TH-229 85.43 14.70 6. lllE+OO 3.157E-01 3.157E-01 102.28 OK 88.47 24.00 6. lllE+OO 1.933E-01 1.934E-01 102.28 OK 193.51 4.41* 7.490E+OO Line Not Found Absent 210.85 2.80 7.193E+OO Line Not Found Absent TH-230 609.32 45.49* 3.566E+OO 9.175E-01 9.175E-01 17.15 OK 1120. 29 14.92 2.334E+OO 7.699E-01 7.699E-01 66. 96 OK 1764.49 15.30 1.632E+OO 7.609E-01 7.609E-01 41. 66 OK PA-231 283.69 1. 70 6.038E+OO Line Not Found Absent 301.36 5.35* 5.809E+OO 6.882E-01 6.882E-01 96. 40 OK U-234 609.32 45.49* 3.566E+OO 9.175E-01 9.175E-01 17.15 OK 1120.29 14.92 2.334E+OO 7.699E-01 7.699E-01 66. 96 OK 1764.49 15.30 1.632E+OO 7.609E-01 7.609E-01 41. 66 OK U-235 89. 96 3.47 6.379E+OO 1.742E+OO 1.742E+OO 60.67 OK Page 4645 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235075 Acquisition date Nuclide Type: Nuclide AM-243 ANH-511 Energy 93.35 143.76 163.33 185. 72 205.31 43.53 74.66 511. 00 %Abn 5.60 10. 96* 5.08 57.20 5.01 5.90 67.20* 100.00* Flag: "*" = Keyline Page 4646 of 5809 Uncorrected Decay Corr %Eff pCi/GRAM pCi/GRAM "6. 614E+OO l.893E+OO l.893E+OO 8.086E+OO Line Not Found 7.938E+OO Line Not Found 7.607E+OO 1.250E-01 l.250E-01 7.289E+OO Line Not Found 3.443E-01 Line Not Found 4.729E+00 l.503E-01 l.504E-01 4.027E+OO 4.127E-02 4.127E-02 Page : 3 3-0CT-2016 06:47:01 2-Sigma %Error Status 48.41

  • OK Absent Absent 53.45 OK Absent Absent 62.52 OK 182.29 OK VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 11:49:13.03 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235075.CNF;l * *Acquisition date 3-0CT-2016 06:47:01 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 2.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
  • Sample date 16-DEC-2015 09:31:00 Analyst initials: MXRl *
  • Sample ID G405235075 Sample Quantity 1.5141E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) BE-7 1.463E+Ol 1.403E+Ol K-40 1.356E+Ol 1.116E+OO GE-68 2.864E+OO 1.828E+OO CD-109 1.944E+OO 1.949E+OO SN-126 1.254E-01 l.257E-01 PR-144 5.561E+OO 1.493E+Ol TL-208 2.735E-01 6.975E-02 PB-212 7.454E-01 9.929E-02 BI-214 9.178E-01 1.543E-01 PB-214 1.012E+OO 1.601E-01 RN-222 9.178E-01 1.543E-01 RA-224 7.942E-01 1.408E+OO RA-226 9.178E-01 1.543E-01 TH-228 7.454E-01 9.929E-02 TH-229 -2.647E-01 3.684E-01 TH-230 9.175E-01 1.542E-01 PA-231 6.882E-01 6.502E-01 U-234 9.175E-01 l.542E-01 U-235 1. 441E-02 l.549E-01 AM-243 l.504E-01 9.212E-02 ANH-511 4.127E-02 7.372E-02 Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 Page 4647of5809 Key-Line Activity (pCi/GRAM 1.205E-02 O.OOOE+OO -6.523E-03 2.231E-02 O.OOOE+OO O.OOOE+OO 3.338E-02 -2.341E-01 O.OOOE+OO K.L. Cnt Uncert (1.96-sigma) 3.385E-02 1.418E+41 2.273E-02 2.676E-01 7.566E+03 2.526E+02 5.283E-02 3.380E-01 l.431E+41 MDA (pCi/GRAM 1.501E+Ol 4.038E-01 3.973E+OO 1.550E+OO 1.152E-01 6.430E+OO 4.279E-02 7.166E-02 9.800E-02 1.008E-01 9.800E-02 7.675E-01 9.800E-02 7.166E-02 6.931E-01 9.797E-02 5.957E-01 9.797E-02 2.877E-01 7.758E-02 3.931E-02 MDA (pCi/GRAM 6.818E-02 O.OOOE+OO 4.363E-02 5.073E-01 O.OOOE+OO 0.000E+OO 1.049E-01 5.712E-01 O.OOOE+OO NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF C0-57 3.387E-02 3.683E-02 7.040E-02 NOT IDENT. C0-58 -2.150E-01 3.637E-01 6.309E-01 NOT IDENT. FE-59 1.195E+OO 4.325E+OO 8.679E+00 NOT IDENT. C0-60 -2.430E-03 3.190E-02 5.471E-02 NOT IDENT. ZN-65 -l.210E-01 1.907E-01 2.795E-01 NOT IDENT. AS-73 4.013E+OO 8.785E+OO l.837E+Ol NOT IDENT. AS-74 O.OOOE+OO 3.581E+03 O.OOOE+OO SHORT HLIF SE-75 -7.183E-02 1.762E-01 2.913E-01 NOT IDENT. BR-77 0.000E+OO 1. 761E+36 O.OOOE+OO SHORT HLIF SR-82 0.000E+OO 4.654E+02 0. OOOE+,00 SHORT HLIF RB-83 -5.849E-02 4.055E-01 7.901E-01 NOT IDENT. KR-85 1.123E+Ol 6.380E+OO 1.296E+Ol NOT IDENT. SR-85 1.090E+OO 6.200E-01 1.259E+OO NOT IDENT. RB-86 0.000E+OO 1.672E+04 O.OOOE+OO SHORT HLIF Y-88 4.812E-02 1. 679E-01 3.578E-01 NOT IDENT. Y-91 -2.872E+Ol 3.778E+02 7.081E+02 NOT IDENT. NB-94 -2.436E-03 2.588E-02 4.768E-02 NOT IDENT. NB-95 -3.067E-01 6.457E-01 1.139E+OO NOT IDENT. NB-95M -5.350E-01 1.918E+OO 3.249E+OO NOT IDENT. ZR-95 4.326E-01 1.075E+OO 2 .116E+OO NOT IDENT. NB-97 O.OOOE+OO l.394E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.629E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 1.855E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 3.551E-02 4.744E-02 5.073E-02 FAIL ABUN RH-102 -2.539E-02 4.192E-02 7.512E-02 FAIL ABUN RU-103 -3.951E+OO 3.633E+OO 6.238E+OO FAIL ABUN RH-106 -2.152E-01 3.926E-01 7.077E-01 NOT IDENT. RU-106 -2.152E-01 3.926E-01 7.077E-01 NOT IDENT. AG-108M 1.594E-02 2.394E-02 3.730E-02 FAIL ABUN AG-110M -1.923E-02 8.748E-02 l.567E-01 FAIL ABUN SN-113 5.205E-03 1.700E-01 3.183E-01 NOT IDENT. CD-115 O.OOOE+OO 1. 831E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 5.213E+04 O.OOOE+OO SHORT HLIF TE-123M -3.510E-02 1.035E-01 l.834E-01 NOT IDENT. SB-124 2. 851E-01 1. 346E+OO 2.880E+OO FAIL ABUN SB-125 9.162E-02 9.071E-02 1.500E-01 FAIL ABUN TE-125M -6. 411E+Ol 2.069E+02 3.832E+02 NOT IDENT. I-126 O.OOOE+OO 4.465E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.468E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.925E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1. 968E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.306E+25 O.OOOE+OO SHORT HLIF BA-133 -8.624E-03 3.351E-02 5.451E-02 FAIL ABUN I-133 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 7.524E-02 6.253E-02 8.948E-02 FAIL ABUN CS-135 6.801E-02 1.226E-01 2.228E-01 NOT IDENT. I-135 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 1.526E+05 O.OOOE+OO SHORT HLIF BA-137M 2.403E-03 2.539E-02 4.908E-02 NOT IDENT. CS-137 2.539E-03 2.683E-02 5.185E-02 NOT IDENT. CE-139 -2.102E-02 8.839E-02 1.572E-01 NOT IDENT. BA-140 O.OOOE+OO 6.325E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 1. 773E+05 O.OOOE+OO SHORT HLIF CE-141 -2.452E+OO 1. 706E+Ol 3. ll 7E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.391E+41 O.OOOE+OO SHORT HLIF CE-144 -4.473E-02 2.613E-01 4.811E-01 NOT IDENT. PM-144 6.429E-02 l.725E-01 7.926E-02 FAIL ABUN PM-146 l.698E-02 3.312E-02 6.473E-02 NOT IDENT. ND-147 O.OOOE+OO 1.474E+07 O.OOOE+OO SHORT HLIF PM-147 8.289E+Ol 6.407E+02 l.220E+03 NOT IDENT. PM-149 O.OOOE+OO 5.389E+39 O.OOOE+OO SHORT HLIF EU-150 l.250E-02 2.336E-02 4.153E-02 FAIL ABUN EU-152 -6.710E-02 6.891E-02 1.174E-01 NOT IDENT. GD-153 -7.773E-02 1.406E-01 2.586E-01 NOT IDENT. EU-154 2.967E-02 8.333E-02 l.678E-01 FAIL ABUN EU-155 -1.404E-02 8.521E-02 1.606E-01 FAIL ABUN TB-160 3.656E-01 1.327E+OO 2.577E+OO FAIL ABUN H0-166M -1. 231E-02 4.318E-02 7.918E-02 NOT IDENT. TM-171 3.459E+00 2.229E+Ol 4.588E+Ol NOT IDENT. HF-172 2.242E-01 2.702E-01 3.560E-01 FAIL ABUN LU-172 -3.125E-02 6.071E-02 1.088E-01 FAIL ABUN LU-176 -7.025E-03 1.914E-02 3.525E-02 FAIL ABUN HF-181 3.022E-01 3.199E+OO 5.313E+00 NOT IDENT. TA-182 -3.427E-01 6.963E-01 l.229E+OO FAIL ABUN RE-183 -1. 478E+OO 2.659E+OO 5.153E+OO NOT IDENT. RE-184 -l.035E+01 2.363E+Ol 4.093E+Ol NOT IDENT. Page 4648 of 5809 W-188 2.423E+Ol 1. 012E+02 1. 445E+02 NOT IDENT. IR-192 2.261E-01 3.295E-01 6.633E-01 FAIL ABUN HG-203 -5.106E-01 1.632E+OO 3.050E+OO FAIL ABUN BI-207 -3.773E-02 3.947E-02 6.658E-02 FAIL ABUN PB-210 -6.934E-01 4.293E+OO 8.614E+OO NOT IDENT. BI-211 O.OOOE+OO 4.409E-01 6.582E-01 FAIL ABUN PB-211 -3.278E-01 5.107E-01 8.842E-01 FAIL ABUN BI-212 O.OOOE+OO 4.808E-01 9.675E-01 FAIL ABUN RN-219 3.722E-02 2.798E-01 5.302E-01 FAIL ABUN RA-223 2.392E-01 4.346E-01 8.668E-01 FAIL ABUN AC-227 -8.802E-02 l.888E-01 3 .116E-01 FAIL ABUN TH-227 -8.802E-02 l.888E-01 3 .116E-01 FAIL ABUN AC-228 0.000E+OO 2.529E-01 4.542E-01 FAIL ABUN RA-228 O.OOOE+OO 2.529E-01 4.542E-01 FAIL ABUN TH-231 2.392E-Ol 4.346E-01 8.668E-01 FAIL ABUN TH-232 O.OOOE+OO 2.529E-01 4.542E-01 FAIL ABUN PA-233 -4.997E-03 4.418E-02 8.340E-02 FAIL ABUN PA-234 7.105E-02 3.078E-01 3.669E-01 FAIL ABUN PA-234M 2.768E-01 3.170E+OO 6. ll 7E+OO NOT IDENT. TH-234 -6.789E-02 1.118E+OO 2.270E+OO FAIL ABUN NP-237 -4.997E-03 4.418E-02 8.340E-02 FAIL ABUN NP-238 O.OOOE+OO 2.773E+40 O.OOOE+OO SHORT HLIF U-238 -6.789E-02 l .118E+OO 2.270E+OO FAIL ABUN NP-239 -1. 441E-01 1.819E-01 3.211E-01 NOT IDENT. PU-239 3.236E+02 4.323E+02 4.927E+02 FAIL ABUN AM-241 3.070E-02 1.327E-01 2.704E-01 NOT IDENT. CM-243 -2.792E-02 7.976E-02 l.483E-01 NOT IDENT. BK-247 -2.290E-02 6.286E-02 1.044E-01 FAIL ABUN CM-247 -9.026E-03 2. 681E-02 4.812E-02 FAIL ABUN CF-249 1.310E-02 2.918E-02 5.684E-02 NOT IDENT. CF-251 4.555E-02 9.384E-02 1.762E-01 FAIL ABUN Page 4649 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 11:49:10.90 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigrna Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error BE-7 477.60 29 10.44* 4.230E+OO 3.268E-01 l.463E+Ol 97.83 K-40 1460.82 557 10.66* 1. 911E+OO 1.356E+Ol 1.356E+Ol 8.40 GE-68 1077.34 21 3.22* 2.403E+OO 1.357E+OO 2.864E+OO 65.12 CD-109 88.03 102 3.70* 6. lllE+OO 2.239E+OO 3.471E+OO 56.31 SN-126 64.28 ------9.60 3.252E+OO ------Line Not Found ------86.94 102 8.90 6. lllE+OO 9.308E-01 9.309E-01 56.31 87.57 102 37.00* 6. lllE+OO 2.239E-01 2.239E-01 56.31 PR-144 696. 51 24 1. 34* 3.253E+OO 2.733E+OO 5.561E+00 273.88 1489.16 ------0.28 1.883E+OO ------Line Not Found ------TL-208 277.37 ------6.60 6.127E+OO ------Line Not Found ------583.19 172 85.00* 3.674E+OO 2.735E-01 2.735E-01 26.03 860.56 29 12.50 2.810E+OO 4.079E-01 4.079E-01 115. 37 BI-211 72. 87 155 1. 23 4.729E+OO l.325E+Ol 1.325E+Ol 37.66 351.06 379 12.92* 5.218E+OO 2.788E+OO 2.788E+OO 16.14 PB-212 74.82 155 10.28 4. 729E+OO 1. 58 6E+OO 1.586E+OO 37.66 ' 77 .11 257 17.10 5.036E+OO 1.482E+00 l.482E+OO 27.30 238.63 440 43.60* 6.719E+OO 7.454E-01 7.454E-01 13.59 300.09 43 3.30 5.809E+OO l .116E+00 1.116E+OO 96. 40 BI-214 609.32 300 45.49* 3.566E+OO 9.175E-01 9.178E-01 17.15 1120. 29 54 14.92 2.334E+OO 7.699E-01 7.702E-01 66. 96 1764.49 38 15.30 1.632E+00 7.609E-01 7. 611E-01 41. 66 PB-214 74.82 155 5.80 4. 729E+OO 2.811E+OO 2.812E+OO 37.66 77 .11 257 9.70 5.036E+OO 2. 613E+00 2.614E+00 27.30 87.09 102 3.41 6. lllE+OO 2.429E+OO 2.430E+OO 56.31 242.00 148 7.25 6.671E+OO 1.518E+OO 1.518E+OO 50.79 295.22 233 18.42 5.879E+00 1.069E+OO 1.069E+OO 24.01 351. 93 379 35.60* 5.218E+OO 1.012E+OO 1.012E+OO 16.14 RN-222 609.32 300 45.49* 3.566E+OO 9.175E-01 9.178E-01 17.15 1120.29 54 14.92 2.334E+OO 7.699E-01 7.702E-01 66. 96 1764.49 38 15.30 l.632E+00 7.609E-01 7. 611E-01 41.66 RA-224 240.99 148 4.10* 6.671E+OO 2.684E+OO 2.684E+OO 50.79 RA-226 609.32 300 45.49* 3.566E+00 9.175E-01 9.178E-01 17.15 1120.29 54 14.92 2.334E+00 7.699E-01 7.702E-01 66. 96 1764.49 38 15.30 l.632E+00 7.609E-01 7. 611E-01 41.66 TH-228 74.82 155 10.28 4.729E+OO 1.586E+00 1.586E+00 37.66 77 .11 257 17.10 5.036E+OO 1.482E+OO 1.482E+OO 27.30 238.63 440 43.60* 6. 719E+OO 7.454E-01 7.454E-01 13.59 300.09 43 3.30 5.809E+OO 1.116E+OO 1.116E+OO 96. 40 TH-229 85.43 102 14.70 6. lllE+OO 5.636E-01 5.636E-01 56.31 88.47 102 24.00 6. lllE+OO 3.452E-01 3.452E-01 56.31 193.51 ------4.41* 7.490E+OO ------Line Not Found ------210.85 ------2.80 7.193E+OO ------Line Not Found ------TH-230 609.32 300 45.49* 3.566E+OO 9.175E-01 9.175E-01 17.15 1120.29 54 14.92 2.334E+OO 7.699E-01 7.699E-01 66. 96 1764.49 38 15.30 1.632E+00 7.609E-01 7.609E-01 41.66 PA-231 283.69 ------1. 70 6.038E+OO ------Line Not Found ------301. 36 43 5.35* 5.809E+OO 6.882E-01 6.882E-01 96. 40 Page 4650 of 5809 Nuclide Line Activity Report (continued) Sample ID : G405235075 Acquisition date Page : 2 3-0CT-2016 06:47:01 Nuclide Type: Nuclide U-234 U-235 AM-243 ANH-511 Flag: "*" Page 4651 of 5 809 Energy 609. 1120.29 1764.49 89. 96 93.35 143.76 163.33 185. 72 205.31 43.53 74.66 511.00 Key line Area %Abn 300 45.49* 54 14.92 38 15.30 78 3.47 141 5.60 ------10. 96* ------5.08 110 57.20 ------5.01 ------5.90 155 67.20* 34 100.00* Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCi/GRAM %Error 3.566E+OO 9.175E-01 9,. l 75E-01 17.15 2.334E+OO 7.699E-01 7.699E-01 66. 96 1.632E+OO 7.609E-01 7.609E-01 41. 66 6.379E+OO l.742E+OO l.742E+OO 60.67 6.614E+OO l.893E+00 l.893E+OO 48.41 8.086E+OO ------Line Not Found ------7.938E+OO ------Line Not Found ------7.607E+OO l.250E-01 1.250E-01 53.45 7.289E+OO ------Line Not Found ------3.443E-01 ------Line Not Found ------4.729E+OO 2.426E-01 2.426E-01 37.66 4.027E+OO 4.127E-02 4.127E-02 182.29 Summary of Nuclide Activity Sample ID : G405235075 Acquisition date Page : 3 3-0CT-2016 06:47:01 Total number of lines in spectrum 48 Number of unidentified lines 8 Number of lines tentatively identified by NID 40 Nuclide Type : Nuclide BE-7 K-40 GE-68 CD-109 SN-126 PR-144 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-229 TH-230 PA-231 U-234 U-235 AM-243 ANH-511 Hlife 53.22D l.25E+09Y 270.95D 4 61. 40D 2.30E+05Y 284.91D 1.41E+10Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600.00Y 1.41E+l0Y 7340.00Y 7.54E+04Y 7.04E+08Y 2.45E+05Y 7.04E+08Y 7370.00Y l.00E+09Y Decay 44.8 1. 00 2 .11 .1. 55 1. 00 2.03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 3.268E-01 l.356E+Ol 1.357E+OO 2.239E+OO 2.239E-01 2.733E+OO 2.735E-01 2.788E+OO 7.454E-01 9.175E-01 1.012E+OO 9.175E-01 2.684E+OO 9.175E-01 7.454E-01 3.452E-01 9 .175E-01 6.882E-01 9.175E-01 1.250E-01 2.426E-01 4.127E-02 3.472E+Ol 3.472E+Ol Decay Corr pCi/GRAM l.463E+Ol 1.356E+Ol 2.864E+OO 3.471E+OO 2.239E-01 5. 561E+OO 2.735E-01 2.788E+OO 7.454E-01 9.178E-01 1.012E+OO 9.178E-01 2.684E+OO 9.178E-01 7.454E-01 3.452E-01 9.175E-01 6.882E-01 9.175E-01 1.250E-01 2.426E-01 4.127E-02 5.459E+Ol 5.459E+Ol 83.33% Decay Corr 2-Sigma Error l.432E+Ol 0 .114E+Ol 1. 865E+OO 1.955E+00 1.261E-01 15.23E+OO 0.712E-01 0.450E+OO 1.013E-01 1.574E-01 0.163E+OO l.574E-01 1.363E+OO 1. 574E-01 1.013E-01 l.944E-01 1.573E-01 6.635E-01 l.573E-01 0.668E-01 0.914E-01 7.522E-02 "M" Manually accepted 2-Sigma %Error 97.83 8.40 65.12 56.31 56.31 273.88 26.03 16.14 13.59 17.15 16.14 17.15 50.79 17.15 13.59 56.31 17.15 96.40 17.15 53.45 37.66 182.29 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4652 of 5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : G405235075 Acquisition date : 3-0CT-2016 06:47:01 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 124.62 30 103 1. 45 249.95 248 6 6.84E-03 **** 7.98E+OO T 0 128.95 33 137 0.80 258.60 255 7 7.49E-03 **** 8.03E+OO T 0 214.25 41 150 3.86 429.07 424 11 9.82E-03 **** 7.13E+OO T Q 259.99 22 74 1. 68 520.48 516 8 5.30E-03 **** 6.38E+OO T 0 270.61 68 123 1. 91 541.69 535 12 1.65E-02 75.8 6.22E+OO T 0 285.78 21 87 1. 27 572. 01 568 10 5.19E-03 **** 6.0lE+OO T 0 338.67 101 85 1. 54 677. 71 673 10 2.50E-02 43.3 5.36E+OO T 0 425.73 15 50 0.48 851. 72 844 9 3.85E-03 **** 4.57E+OO T 0 431. 33 24 45 4.31 862.90 856 12 6.04E-03 **** 4.53E+OO 0 438.51 60 66 5.93 877.25 868 20 1.53E-02 74.1, 4.48E+OO T 0 463.97 75 33 2 .11 928.13 922 15 1.92E-02 42.2 4. 31E+OO T 0 485.39 39 66 8.72 970.94 959 22 9.98E-03 **** 4.18E+OO T 0 721. 82 29 25 2.42 1443.52 1435 15 7.81E-03 87.3 3.18E+OO T 0 727. 32 51 16 2.73 1454.51 1450 9 1.37E-02 40.5 3.16E+OO T 0 795.87 29 25 1. 90 1591.54 1584 14 7.94E-03 84.8 2.97E+OO T 0 911. 76 145 31 1. 97 1823.19 1816 17 3.95E-02 25.1 2.70E+OO T 0 935.82 26 21 3.41 1871.28 1863 17 7.02E-03 92.4 2.66E+OO T 0 945.53 5 19 0.69 1890.71 1885 10 1.24E-03 **** 2.64E+OO T 0 950.97 48 5 5.73 1901.58 1894 18 1.33E-02 35.7 2.63E+OO T 0 971. 05 34 68 1. 27 1941.71 1931 15 9.42E-03 **** 2.59E+OO 0 1155. 68 33 35 0.74 2310.81 2301 23 9.32E-03 97.5 2.28E+OO 0 1239.87 41 36 1. 39 2479.13 2465 23 1.16E-02 84.2 2.17E+OO T 0 1293.60 33 0 6.25 2586.56 2578 19 9.44E-03 34.3 2.lOE+OO 0 1310.05 14 8 1. 65 2619.44 2613 11 4.llE-03 91.3 2.08E+OO 0 1339.54 8 8 0.68 2678.41 2673 10 2.35E-03 **** 2.05E+OO 0 1378.25 23 10 3.32 2755.80 2748 14 6.57E-03 71.1 2.00E+OO 0 1482.32 9 15 4.43 2963.87 2946 22 2.62E-03 **** 1.89E+OO Flags: "T" = Tentatively associated Page 4653 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 11:49:26.23 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235075.CNF;l *
  • Acquisition date 3-0CT-2016 06:47:01 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 2.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
  • Sample date 16-DEC-2015 09:31:00 Nuclide Library : SOLID *
  • Sample ID G405235075 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.5141E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO'
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide BE-7 K-40 GE-68 CD-109 SN-126 PR-144 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 TH-228 TH-229 TH-230 PA-231 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 6.804E+OO 1.688E-01 1.801E+OO 7.265E-01 5.444E-02 2.895E+OO 1.919E-02 3.343E-02 4.476E-02 4.667E-02 4.476E-02 3.581E-01 4.476E-02 3.343E-02 3.252E-01 4.475E-02 2.753E-01 4.475E-02 1.358E-01 3.652E-02 1.794E-02 ----Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 Page 4654 of 5809 'Le (pCi/GRAM 3.015E-02 O.OOOE+OO 1. 7 60E-02 2.259E-01 0.000E+OO O.OOOE+OO 4.790E-02 2.526E-01 O.OOOE+OO 3.299E-02 NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT.

C0-58 FE-59 C0-60 ZN-65 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU...:106 AG-108M AG-llOM SN-l13 CD-l15 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 Page 4655 of 5809 2.746E-01 3.861E+OO 2.370E-02 1.267E-01 8.625E+OO 0.000E+OO l.354E-01 0.000E+OO 0.000E+OO 3.547E-01 6.061E+OO 5.889E-01 O.OOOE+OO 1.503E-01 3.167E+02 2.171E-02 5.164E-01 1.526E+OO 9.617E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.382E-02 3.346E-02 2.798E+OO 3.199E-01 3.199E-01 1.695E-02 7. 072E-02 1.464E-01 O.OOOE+OO O.OOOE+OO 8.592E-02 1.200E+OO 6.874E-02 1. 797E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.497E-02 O.OOOE+OO 4.122E-02 1.044E-01 0.000E+OO O.OOOE+OO 2.223E-02 2.349E-02 7. 371E-02 0.000E+OO O.OOOE+OO 1.467E+Ol O.OOOE+OO 2.244E-01 3.593E-02 2. 967E-02 O.OOOE+OO 5.712E+02 O.OOOE+OO 1.940E-02 5.355E-02 l.210E-01 7. 421E-02 7.515E-02 1.154E+OO 3.564E-02 2.147E+Ol 1.674E-01 4.830E-02 l.632E-02 2.414E+OO 5.478E-01 2.408E+OO 1.847E+Ol 6.690E+Ol NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NO:r' IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 AC-228 RA-228 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4656 of 5809 3.084E-01 1.416E+OO 2.947E-02 4.032E+OO 3.189E-01 4.033E-01 4.513E-01 2.430E-01 4.017E-01 l.443E-01 1.443E-01 2.174E-01 2.174E-01 4.017E-01 2.174E-01 3.850E-02 l.619E-01 2.739E+OO 1. 072E+OO 3.850E-02 O.OOOE+OO 1. 072E+OO l.490E-01 2.323E+02 1. 271E-01 6.937E-02 4. 851E-02 2.203E-02 2.626E-02 8.283E-02 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 11:49:31.46 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235075.CNF;l *
  • Acquisition date 3-0CT-2016 06:47:01 Sensitivity : 3.000 *
  • Detector ID GAM18 Energy tolerance: 2.000 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.97 Half life ratio : ***** *
  • Sample date 16-DEC-2015 09:31:00 Nuclide Library : SOLID *
  • Sample ID G405235075 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.5141E+02 GRAM *
  • Quantity Err(%) : 1.3209E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 08:25:19 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM18 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error Nuclide (pCi/GRAM ( 1. 96-sigma) BE-7 1.463E+Ol 1.404E+Ol K-40 1.356E+Ol 1.321E+OO GE-68 2.864E+OO 1.831E+OO CD-109 1.944E+OO 1. 965E+OO SN-126 1.254E-01 1. 2 65E-01 PR-144 5. 561E+OO 1.493E+Ol TL-208 2.735E-01 7. 071E-02 PB-212 7.454E-01 1.068E-01 BI-214 9.178E-01 1.592E-01 PB-214 1.012E+OO 1.655E-01 RN-222 9.178E-01 1.592E-01 RA-224 7.942E-01 1.414E+OO RA-226 9.178E-01 1.592E-01 TH-228 7.454E-01 1.068E-01 TH-229 -2.647E-01 3.686E-01 TH-230 9.175E-01 1.592E-01 PA-231 6.882E-01 6.666E-01 U-234 9.175E-01 1.592E-01 U-235 1.441E-02 1. 549E-01 AM-243 1.504E-01 9.333E-02 ANH-511 4.127E-02 7.374E-02 Non-Identified Nuclides Nuclide NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 Page 4657 of 5809 Key-Line Activity (pCi/GRAM 1.205E-02 1.000E+41 -6.523E-03 2.231E-02 4.834E+OO -3.929E+Ol 3.338E-02 -2.341E-01 -1.000E+41 K.L Act error ( 1 . 96-sigma ) 3.386E-02 1.480E+41 2.273E-02 2.676E-01 7.566E+03 2.526E+02 5.285E-02 3.382E-01 l.432E+41 TPU ( 1. 96-sigma) 1.404E+Ol 1.321E+OO 1. 831E+OO 1. 965E+OO 1.265E-01 1.493E+Ol 7.071E-02 1.068E-01 1.592E-01 1.655E-01 1.592E-01 1.414E+OO 1.592E-01 1.068E-01 3.686E-01 1.592E-01 6.666E-01 1.592E-01 1.549E-01 9.333E-02 7.374E-02 TPU ( 1. 96-sigma ) 3.429E-02 O.OOOE+OO 2.292E-02 2.678E-01 7.566E+03 2.532E+02 5.495E-02 3.543E-01 O.OOOE+OO NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF C0-57 3.387E-02 3.686E-02 3.990E-02 NOT IDENT. C0-58 -2.150E-01 3.638E-01 3.765E-01 NOT IDENT. FE-59 1.195E+OO 4.326E+OO 4.359E+OO NOT IDENT. C0-60 -2.430E-03 3.190E-02 3.192E-02 NOT IDENT. ZN-65 -1.210E-01 1.907E-01 l.984E-01 NOT IDENT. AS-73 4.013E+OO 8.824E+OO 9.007E+OO NOT IDENT. AS-74 -2.189E+03 3.585E+03 3.719E+03 SHORT HLIF SE-75 -7.183E-02 1. 7 63E-01 1. 792E-01 NOT IDENT. BR-77 1.322E+37 1.114E+38 O.OOOE+OO SHORT HLIF SR-82 .-1. 618E+02 4.655E+02 4. 711E+02
  • SHORT HLIF RB-83 -5.849E-02 4.056E-01 4.064E-01 NOT IDENT. KR-85 l.123E+Ol 6.397E+OO 8.158E+OO NOT IDENT. SR-85 1.090E+OO 6.216E-01 7.924E-01 NOT IDENT. RB-86 2.619E+04 l.676Et04 2.050E+04 SHORT HLIF Y-88 4.812E-02 1. 679E-01 l.693E-01 NOT IDENT. Y-91 -2. 872E+Ol 3.778E+02 3.780E+02 NOT IDENT. NB-94 -2.436E-03 2.588E-02 2.590E-02 NOT IDENT. NB-95 -3.067E-01 6.458E-01 6.604E-01 NOT IDENT. NB-95M -5.350E-01 1.918E+OO 1.933E+OO NOT IDENT. ZR-95 4.326E-01 1. 076E+OO 1.093E+OO NOT IDENT. NB-97 -l.000E+41 1.394E+41 O.OOOE+OO SHORT HLIF ZR-97 l.000E+41 1.629E+41 O.OOOE+OO SHORT HLIF M0-99 -1. 696E+29 l.855E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 6.181E+41 O.OOOE+OO SHORT HLIF RH-101 3.551E-02 4.788E-02 5.048E-02 FAIL ABUN RH-102 -2.539E-02 4.197E-02 4.351E-02 FAIL ABUN RU-103 -3.951E+OO 3.637E+OO 4.050E+OO FAIL ABUN RH-106 -2.152E-01 3:928E-01 4.046E-01 NOT IDENT. RU-106 -2.152E-01 3.928E-01 4.046E-01 NOT IDENT. AG-108M 1.594E-02 2.395E-02 2.500E-02 FAIL ABUN AG-llOM -1.923E-02 8.749E-02 8.792E-02 FAIL ABUN SN-113 5.205E-03 1.700E-01 1.700E-01 NOT IDENT. CD-115 -l.217E+38 1. 843E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -l.668E+04 5.217E+04 5.271E+04 SHORT HLIF TE-123M -3.510E-02 1.035E-01 l.047E-01 NOT IDENT. SB-124 2.851E-01 1. 34 7E+OO 1.353E+OO FAIL ABUN SB-125 9.162E-02 9.079E-02 9.974E-02 FAIL ABUN TE-125M -6. 411E+Ol 2.069E+02 2.089E+02 NOT IDENT. I-126 5.721E+05 4.529E+05 5.212E+05 SHORT HLIF SB-126 1.107E+06 9.685E+05 l.089E+06 SHORT HLIF SB-127 l.510E+21 4.415E+21 O.OOOE+OO SHORT HLIF I-131 6.237E+08 1.968E+09 l.988E+09 SHORT HLIF I-132 -l.000E+41 1.869E+42 O.OOOE+OO SHORT HLIF TE-132 -l.153E+24 5.306E+25 O.OOOE+OO SHORT HLIF BA-133 -8.624E-03 3. 351E-02 3.374E-02 FAIL ABUN I-133 1.000E+41 l.483E+42 O.OOOE+OO SHORT HLIF CS-134 7.524E-02 6.261E-02 7 .121E-02 FAIL ABUN CS-135 6.801E-02 l.227E-01 1. 2 65E-01 NOT IDENT. I-135 1.000E+41 1. 07 5E+42 O.OOOE+OO SHORT HLIF CS-136 l.009E+05 1.530E+05 1. 596E+05 SHORT HLIF BA-137M 2.403E-03 2.539E-02 2.542E-02 NOT IDENT. CS-137 2.539E-03 2.683E-02 2.685E-02 NOT IDENT. CE-139 -2.102E-02 8.849E-02 8.899E-02 NOT IDENT. BA-140 7.162E+04 6.325E+05 6.333E+05 SHORT HLIF LA-140 l.068E+05 1. 774E+05 1.838E+05 SHORT HLIF CE-141 -2.452E+OO 1. 706E+Ol 1.710E+Ol NOT IDENT. CE-143 1.000E+41 1. 394E+41 O.OOOE+OO SHORT HLIF CE-144 -4.473E-02 2. 613E-01 2.621E-01 NOT IDENT. PM-144 6.429E-02 1. 726E-01 1. 750E-01 FAIL ABUN PM-146 1.698E-02 3.315E-02 3.402E-02 NOT IDENT. ND-147 2.731E+06 l.474E+07 1.479E+07 SHORT HLIF PM-147 8.289E+Ol 6.407E+02 6.418E+02 NOT IDENT. PM-149 3.055E+39 5.430E+39 O.OOOE+OO SHORT HLIF EU-150 1.250E-02 2.337E-02 2.404E-02 FAIL ABUN EU-152 -6. 710E-02 6.901E-02 7.535E-02 NOT IDENT. GD-153 -7.773E-02 1.406E-01 1.449E-01 NOT IDENT. EU-154 2. 967E-02 8.334E-02 8.440E-02 FAIL ABUN EU-155 -1.404E-02 8.522E-02 8.545E-02 FAIL ABUN TB-160 3.656E-01 1.327E+OO 1.338E+OO FAIL ABUN H0-166M -1.231E-02 4.319E-02 4.354E-02 NOT IDENT. TM-171 3.459E+00 2.229E+Ol 2.234E+Ol NOT IDENT. HF-172 2.242E-01 2.726E-01 2.907E-01 FAIL ABUN LU-172 -3.125E-02 6.079E-02 6.240E-02 FAIL ABUN LU-176 -7.025E-03 l.915E-02 1.941E-02 FAIL ABUN HF-181 3.022E-01 3.199E+00 3.202E+OO NOT IDENT. TA-182 -3.427E-01 6. 964E-01 7.134E-01 FAIL ABUN RE-183 -1.478E+OO 2.668E+00 2.750E+OO NOT IDENT. RE-184 -1.035E+Ol 2.375E+Ol 2.420E+Ol NOT IDENT. Page 4658 of 5809 W-188 2.423E+Ol 1.012E+02 1.018E+02 NOT IDENT. IR-192 2. 261E-Ol 3.296E-01 3.450E-01 FAIL ABUN HG-203 -5.106E-01 1. 632E+OO 1.648E+OO FAIL ABUN BI-207 -3.773E-02 3.950E-02 4.301E-02 FAIL ABUN PB-210 -6.934E-01 4.294E+OO 4.305E+OO NOT IDENT. BI-211 2.788E+OO 4.581E-01 1.338E+OO FAIL ABUN PB-211 -3.278E-01 5. llOE-01 5.319E-01 FAIL ABUN BI-212 l.211E+OO 4.846E-01 7.299E-01 FAIL ABUN RN-219 3.722E-02 2.798E-01 2.803E-01 FAIL ABUN RA-223 2.392E-01 4.349E-01 4.480E-01 FAIL ABUN AC-227 -8.802E-02 1. 891E-Ol l.933E-01 FAIL ABUN TH-227 -8.802E-02 1. 891E-01 1.933E-01 FAIL ABUN AC-228 1.028E+OO 2.583E-Ol 5.304E-01 FAIL ABUN RA-228 1.028E+OO 2.583E-01 5.304E-01 FAIL ABUN TH-231 2.392E-01 4.349E-01 4.480E-01 FAIL ABUN TH-232 1.028E+OO 2.583E-01 5.304E-01 FAIL ABUN PA-233 -4.997E-03 4.418E-02 4.424E-02 FAIL ABUN PA-234 7.105E-02 3.184E-01 3.200E-01 FAIL ABUN PA-234M 2.768E-01 3.170E+OO 3.173E+OO NOT IDENT. TH-234 -6.789E-02 1.118E+OO 1.119E+OO FAIL ABUN NP-237 -4.997E-03 4.418E-02 4.424E-02 FAIL ABUN NP-238 -2.365E+40 2.775E+40 O.OOOE+OO SHORT HLIF U-238 -6.789E-02 1.118E+OO 1.119E+OO FAIL ABUN NP-239 -l.441E-01 1.823E-01 1.935E-01 NOT IDENT. PU-239 3.236E+02 4.325E+02 4.565E+02 FAIL ABUN AM-241 3.070E-02 1.328E-01 l.335E-01 NOT IDENT. CM-243 -2.792E-02 7.980E-02 8.079E-02 NOT IDENT. BK-247 *-2. 2 90E-02 6.303E-02 6.387E-02 . FAIL ABUN CM-247 -9.026E-03 2.685E-02 2. 716E-02 FAIL ABUN CF-249 1.310E-02 2.920E-02 2.979E-02 NOT IDENT. CF-251 4.555E-02 9.398E-02 9.620E-02 FAIL ABUN Page 4659 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 74.66 63.4321 105.31 99.1045 131. 20 72. 4552 879.38 67.4593 86.79 99.1833 133.02 70.1713 46.54 68.6321 86.94 99.2336 133. 52 68.0246 228.16 0.0000 87.09 99.2838 136.00 72.9078 52.39 68.6747 87.57 99.4423 136.47 71. 8643 1093.63 82.4539 88.03 74.6948 739.50 0.0000 52.39 68.1787 306.78 74.7713 140.51 0.0000 125.81 63.2454 88.47 74.8032 143.76 83.3391 53.44 68.5303 143.76 88.3560 144.24 74.2854 54.07 63.5842 90.64 88.5509 145.44 79.0664 293.27 0.0000 531. 02 0.0000 152.43 97.7197 482.18 78.6024 92.59 89.1050 1048.07 0.0000 57.98 Bl. 38 95 93.35 89.3190 154.21 92.2490 59.27 82.7466 94.56 73.6008 158.56 0.0000 59.32 82.7653 311. 90 73.6215 159.00 82.5557 59.54 77.5589 946.00 73.6259 162.33 70.0553 60. 96 83'. 3709 94.87 73.6718 537.26 0.0000 61.17 83.4477 97. 43. 85.0555 163.33 73.7650 62.93 74.2474 98.43 79.2199 165.86 82. 5071 63.29 77 *. 9455 98.44 79.2223 427.87 93.9471 290.67 83.4241 103.37 73.3689 176.60 0.0000 87.57 80.0731 116.74 73.3689 177. 52 69.7036 66.73 88.1653 100 .11 84.7243 181.07 0.0000 67.24 97.4569 102.03 70.8351 181. 52 91.9855 67.68 90.3321 103.18 73.1332 184.41 99.0771 1221.41 90.3577 103.37 78.3269 185. 72 79.4492 97.43 83.3924 911.20 74.5994 193.51 94.8161 279.20 91.1653 105.31 74.6208 197.03 91.1733 1063.66 85.6604 106.12 61. 2894 198.01 88.7892 72. 87 85.6801 106.47 74.8680 201.83 89.3649 351.06 85.6801 109.28 83.8458 203.43 76.8036 74.66 86.2640 111. 00 80.0327 205.31 76.1883 238.63 86.3160 111.76 0.0000 210.85 85.5202 351.93 86.3160 114.06 60.5255 215.65 76.6052 238.63 86.3160 116. 30 0.0000 222 .11 54.5218 74.97 86.3644 116.74 73.7921 227.09 59.3706 77 .11 87.0516 119. 76 75.4533 227.38 68.2617 78.74 87.5689 264.66 68.1459 228.16 0.0000 256.23 87.8679 121. 22 68.1632 228.18 70.1199 133.52 95.6551 344.28 46.2295 235.69 87.5163 364.49 0.0000 122.06 52.0452 235. 96 98.3266 711.68 83.0340 122.92 73.8915 238.63 64.9065 356.01 78.0427 1274.44 73.9195 238.98 0.0000 323.87 78.0619 123.68 66.7750 240.99 65.1292 81. 75 94.9247 125.81 87.5623 242.00 65.2244 83.79 94.3065 127.23 87.8690 244.70 47.7442 265.00 82.7389 127.91 70.4133 685.70 0.0000 193.51 113. 0219 129.30 83.8985 388.16 58.8691 Page 4660 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 507.63 0.0000 345.93 53 .1191 569.50 43.8230 256.23 63.7698 351.06 51. 7 507 569.70 43.8287 527.90 0.0000 351.93 51. 7 985 583.19 25.4097 264.66 68.7089 355.39 0.0000 584.27 25.4279 264.80 68. 7208 356.01 45.2559 595.83 0.0000 265.00 65.9331. 364.49 0.0000 600.60. 35.2238 268.22 60.5803 366.42 0.0000 602.52 0.0000 269.46 60.2096 372. 51 44.4327 '604.72 36.6539 270.03 60.2539 375.05 45.6053 607.14 36.7125 401.81 60.3490 377.52 45.7164 609.32 37.3385 273.65 0.0000 383.85 48.1393 610.33 37.3623 276.40 55.0594 388.16 40.8203 614.28 39.9547 583.19 46.5735 666.33 0.0000 618.01 34.6586 277.60 53.2428 391.69 43.1136 884.68 36.6385 402.40 57.0752 400.66 42.3928 621. 93 38.6047 279.20 63.8307 401. 81 38.0854 630.19 0.0000 279.54 68.6250 402.40 45. 7273 631.29 31.0664 279.70 61. 0117 404.85 48. 0140 633.25 26.2444 280.46 61. 0716 410.95 47.1861 634.78 0.0000 301.36 54. 6134 413.71 37.4040 635.95 26.2881 284.31 0.0000 720. 70 0.0000 636.99 0.0000 285.41 47.0500 423. 72 0.0000 1690.97 20.5713 285.90 0.0000 427. 09 33.4009 657.76 39.4678 287.50 49.0981 427.87 20.0544 657.90 0.0000 290.67 46.3921 433.94 20.1614 661. 66 29.6704 293.27 0.0000 439.40 27.0088 664.57 0.0000 295.22 58.3142 453.88 28.4821 666.33 0.0000 316.51 58.3667 463.37 27.5586 666.50 0.0000 298.58 49.7684 468.07 27.6646 667.71 0.0000 299.98 49.8524 473.00 0.0000 677.62 33.0892 300.09 49.8586 631. 29 26.0829 685.70 0.0000 300.13 49.8618 696.49 27.8599 695.00 0.0000 311. 90 49.8618 477.60 31.3632 696.49 27.4548 301.36 49.9354 482.18 31.4775 696. 51 27.4548 302.85 50.0236 487.02 0.0000 697.00 0.0000 304.50 50.1222 492.35 0.0000 697.30 35.5459 304.85 0.0000 497.08 36.2698 697.49 35.5502 306.78 60 .1114 505.52 37.0392 702.65 31.4002 308.46 51.3430 507.63 0.0000 706.68 32.4873 311. 90 50.5580 511. 00 36.6570 711. 68 31. 5601 316.51 44.8480 514.00 32.9760 720.70 0.0000 319.41 0.0000 514.00 32.9760 7 21. 93 0.0000 320.08 0.0000 520.40 27.9121 722.78 4.0975 321.04 52.0920 520.69 0.0000 722.91 4.0978 323.87 43.2135 667.71 0.0000 723.31 4.0988 325.23 68.4413 527.90 0.0000 756.73 4.1007 1596.21 0.0000 528.26 34.4131 727. 33 18.0743 333.37 62.1550 529.59 30.8208 733.00 31.7875 333.97 54.8789 529.87 0.0000 735.93 30.9540 334.37 48.8027 531.02 0.0000 737.46 26.8490 338.28 62.2832 537.26 0.0000 739.50 0.0000 338.32 62.2870 1260.41 0.0000 747.24 23.8767 340.48 52.1974 552.55 28.5668 748.06 28.0415 340.55 0.0000 795.86 26.9238 752.31 38.5153 344.28 54.4643 569.33 39.1571 753.82 0.0000 Page 4661 of 5 809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 756.73 27.1283 968. 97 43.3763 1505.03 15.7203 756.80 26.0857 983.53 0.0000 1584.12 23.6287 763.94 37.7051 984.45 0.0000 1596.21 0.0000 765.81 39.8392 996.26 23.3374 1620.50 4.7719 1001.03 41. 9495 1001.03 20.5772 1621.92 6.6830 766.84 44. 0.572 1002.74 19.6557 1678 ... 03 0.0000 772. 60 0.0000 1004.73 15.9250 1690.97 6.8038 776.52 0.0000 1021. 30 0.0000 1750.46 0.0000 777.92 0.0000 1025.87 0.0000 1764.49 6.9294 778.90 33.7783 1028.54 0.0000 1770.23 6.7974 783.70 0.0000 1037.84 19.9367 1771. 35 10.1991 785.37 30.7134 1038.76 0.0000 1791.20 0.0000 903.28 27.2055 1046.59 19.0537 1808.65 8.0039 794.95 22.3497 1048.07 0.0000 1810.72 0.0000 795.86 22.3606 1049.04 23.8403 1836.06 7.0493 801.95 34.1777 1050.41 20.9902 810.06 21. 4484 1063.66 33.5679 810.29 23.5959 1077.00 0.0000 810.45 23.5972 1077.34 31.8173 810.7ti 22.5285 1085.87 34.8240 815.77 0.0000 1093.63 28.1362 818.51 0.0000 1099.45 18.4740 832.01 27.1019 1112. 07 20.7603 834.85 27 .1393 1112. 84 19.5449 835. 71 27.1507 1115. 54 44.0200 836.80 0.0000 1120. 29 28.4180 846.75 0.0000 1120.55 28.4209 846.77 29.4793 1121.30 28.4293 856.80 0.0000 1808.65 25 .1300 860.56 21. 98 00 1131. 51 0.0000 871.09 17.6714 1147.95 0.0000 873.19 28.7442 1332.49 20.9790 875.33 0.0000 1177.95 26.0178 879.38 21. 0659 1189.05 22.1010 880.51 26.6235 1204.77 25.2539 883.24 24.4358 1221.41 29.4630 884.68 32.2321 1231. 02 42.4703 889.28 21.1622 1235.36 0.0000 894.76 27.9144 1238.28 22.4802 1836.06 27.9564 1260.41 0.0000 900.72 31.3496 1271.87 17.5669 903.28 35.8691 1274.44 15.5134 911.20 29.2476 1274.54 15.5142 912.08 33.3108 1291.59 19.0683 984.45 0.0000 1298.22 0.0000 926.50 16.3094 1312 .11 0.0000 929 .11 . 19. 6545 1332.49 15.0544 937.49 17.2990 1362. 66 0.0000 983.53 0.0000 1365.19 14.9058 946.00 0.0000 1368.63 0.0000 949.00 0.0000 1384.29 16.0642 954.55 0.0000 1408.01 21. 5732 962. 31 29.1425 1457.56 0.0000 964.08 30.6991 1460.82 8.7652 966 .17 35.3357 1489.16 14.3603 Page 4662 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:50:13.83 ******************************************************************************** '* GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235076.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM24.CNF;330 Background date : Z-OCT-2016 11:01:18. Sample date 11-DEC-2015 14:19:00 Acquisition date : 3-0CT-2016 06:47:24. Sample ID G405235076 Sample quantity : l.44470E+02 GRAM Detector name : GAM24 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.98 0.1% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 6 6 6 0 0 0 0 0 0 0 4 4 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4663 of 5809 Energy 63.59* 74.90* 77.12* 80.76 87.22 93.18* 105.19 129.31 144.24* 185.91* 209.65 238.73* 241.66 270.64 295.42 300.21 328.26 338.50 352.10* 412. 07 462.53 474.56 511.31* 521.35 538.80 583.34* 609.51* 661. 41 727.70* 860.52 872. 90 890.17* 911.29* 951.40 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 39 157 251 39 56 89 42 46 35 82 29 337 107 29 170 37 38 71 279 13 30 16 11 19 13 95 196 26 22 19 8 15 72 12 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 178 136 124 148 189 223 68 94 102 135 116 63 70 80 63 38 51 60 46 60 45 21 70 12 54 38 39 23 22 14 3 2 21 5 0.82 1.16 1.18 1. 86 1. 27 1. 47 1. 06 0.64 1. 43 1. 58 1. 48 1.12 1. 85 1. 08 1.13 1. 90 0.79 1. 07 1.18 3.49 3.93 1. 43 2.72 2.23 7.25 1. 06 1. 51 3.21 1. 43 3.15 1.35 1. 87 2. 02 3.95 127.25 149.86 154.31 161. 60 174.51 186.43 210.46 258.70 288.58 371.94 419.43 477.60 483.46 541.44 591.00 600.59 656.71 677.20 704.40 824.38 925.33 949.40 1022.93 1043.02 1077.92 1167. 04 1219.39 1323.23 1455.88 1721. 63 1746.40 1780.95 1823.21 1903.47 123 144 144 144 172 182 207 255 285 366 415 473 473 536 586 597 651 671 700 813 919 944 1016 1039 1066 1162 1214 1316 1449 1716 1743 1776 1817 1898 9 1. 08E-02 65. 3 22 4.36E-02 14.8 1.90E+OO 22 6.98E-02 10.0 22 l.09E-02 59.7 7 1. 55E-02 42. 9 12 2.47E-02 36.6 7 l.17E-02 36.1 8 1.27E-02 39.5 9 9.74E-03 55.3 12 2.29E-02 31.2 9 7. 95E-03 71. 0 16 9.35E-02 6.8 2.14E+OO 16 2.98E-02 23.3 10 8.16E-03 59.8 12 4.73E-02 12.l 7 1. 02E-02 32. 4 11 1.04E-02 40.7 10 l.97E-02 23.6 11 7.74E-02 7.8 14 3.70E-03125.8 12 8.26E-03 48.7 8 4.45E-03 56.2 20 3.12E-03206.4 9 5.37E-03 38.8 18 3.61E-03135.4 11 2.65E-02 16.6 13-5.44E-02 9.8 13 7.29E-03 42.2 11 6.05E-03 48.4 11 5.15E-03 45.4 6 2.25E-03 48.7 10 4.18E-03 36.4 14 2.00E-02 18.4 11 3.46E-03 45.5 Peak Search Report (continued) Page : 2 Sample ID : G405235076 Acquisition date 3-0CT-2016 06:47:24 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 969.45* 41 15 1. 45 1939.59 1935 13 l.15E-02 26.5 36 0 1051.57 9 13 1. 34 2103.92 2096 10 2. 61E-03 77.7 37 0 1063.31 7 15 0.81 2127.40 2118 12 1. 96E-03115. 8 38 0 1121.11* 44 19 0.93 2243.06 2235 17 1. 22E-02 28.7 39 0 1234.43 10 16 1. 03 2469.83 2463 10 2.67E-03 87.0 40 0 1304.20 8 8 0.88 2609.45 2602 11 2.21E-03 78.l 41 0 1319.96 3 15 0.50 2641.00 2633 10 8.33E-04248.3 42 0 1460.88* 331 7 1. 59 2923.02 2917 14 9.20E-02 5.8 43 0 1569.66 7 0 0.50 3140. 71 3134 11 1.94E-03 37.8 44 0 1764.67* 29 7 3.59 3531.03 3524 13 8.12E-03 27.1 45 0 1982.88 5 3 0.94 3967. 79 3960 11 1.46E-03 75.1 Flag: "*" = Peak area was modified by background subtraction Page 4664 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:50:15 DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235076.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Configuration Analyses by Sample title Sample date Sample ID ll-DEC-2015 14:19:00 G405235076 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:47:24 144.47 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report SOLID GAMMA24 0 01:00:00.00 1. 50 keV No Linear 75.00 Interfering ------------------Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 242.00 U-235 143.76 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 4665 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered ------------------Nuclide Line EU-155 86.55 SN-126 86.94 SN-126 87.57 CD-109 88.03 RA-224 240.99 CE-141 145.44 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351. 06 CAN 0 01:00:01.98 10.00 0.00 % Peak Energy 0.1%

Nuclide Line Activity Report Page : 2 Sample ID : G405235076 Acquisition date 3-0CT-2016 06:47:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* l.146E+Ol 1.146E+Ol 11. 61 QK SC-46 889.28 99.98* 2.021E+OO 3.906E-02 4.546E-01 72. 80 OK 1120.55 99.99 l.688E+OO l.329E-01 1.547E+OO 57.46 OK CD-109 88.03 3.70* 7.495E+OO 2.536E-01 3. 961E-01 445.54 OK SN-126 64.28 9.60 5.569E+OO 4.768E-01 4.768E-01 130.55 OK 86. 94 8.90 7.495E+OO 1.054E-01 l.054E-01 445.54 OK 87.57 37.00* 7.495E+OO 2.536E-02 2.536E-02 445.54 OK BA-137M 661. 66 89.90* 2.534E+OO 6.206E-02 6.323E-02 84.46 OK CS-137 661.66 85.10* 2.534E+OO 6.556E-02 6.680E-02 84.46 OK CE-141 145.44 48.29* 7.611E+OO 2.922E-02 1.633E+Ol 230.51 OK EU-155 86.55 30.70 7.495E+OO 3.057E-02 3.441E-02 445.54 OK 105.31 21.10* 7.950E+OO l.583E-01 l.782E-01 72.30 OK TL-208 277.37 6.60 5.023E+OO Line Not Found Absent 583.19 85.00* 2.790E+OO 2.192E-01 2.192E-01 33.24 OK 860.56 12.50 2.074E+00 3.760E-01 3.760E-01 90.75 OK PB-212 74.82 10.28 6.737E+OO 8.329E-01 8.329E-01 55.13 OK 77 .11 17.10 6.908E+OO l.371E+OO l.371E+OO 20.03 OK 238.63 43.60* 5.636E+OO 8.067E-01 8.067E-01 13. 54 OK 300.09 3.30 4.719E+OO 1. 365E+00' 1.365E+OO 64.85 OK BI-214 609.32 45.49* 2.698E+OO 8.666E-01 8.670E-01 19.69 OK 1120.29 14.92 1. 688E+OO 8.905E-01 8.909E-01 57.46 OK 1764.49 15.30 l.138E+00 8.231E-01 8.233E-01 54.25 OK PB-214 74.82 5.80 6.730E+OO Line Not Found <<INT Reject 77 .11 9.70 6.908E+OO 2.417E+OO 2.418E+00 20.03 OK 87.09 3.41 7.489E+00 Line Not Found <<INT Reject 242.00 7.25 5.579E+OO Line Not Found <<INT Reject 295.22 18.42 4.779E+OO 1.120E+OO 1.120E+OO 24.10 OK 351. 93 35.60* 4.154E+OO l.074E+OO 1.074E+00 15.50 OK RN-222 609.32 45.49* 2.698E+OO 8.666E-01 8.670E-01 19.69 OK 1120.29 14.92 1.688E+OO 8.905E-01 8.909E-01 57.46 OK 1764.49 15.30 1.138E+OO 8.231E-01 8.233E-01 54.25 OK RA-224 240.99 4.10* 5.585E+OO 7.794E-01 7.794E-01 176.01 OK RA-226 609.32 45.49* 2.698E+00 8.666E-01 8.670E-01 19.69 OK 1120.29 14.92 l.688E+00 8.905E-01 8.909E-01 57.46 OK 1764.49 15.30 l.138E+00 8.231E-01 8.233E-01 54.25 OK AC-228 105.21 1.10 7.950E+OO 3.036E+OO 3.036E+00 72.30 OK 338.32 11. 27 4.287E+OO 8.401E-01 8.401E-01 47.22 OK 794.95 4.25 2.203E+OO Line Not Found Absent 835.71 1. 61 2 .121E+OO Line Not Found Absent 911.20 25.80* 1.985E+OO 7.337E-01 7.337E-01 36. 72 OK 968. 97 15.80 l.892E+OO 7.190E-01 7.190E-01 52.98 OK RA-228 105.21 1.10 7.950E+OO 3.036E+OO 3.036E+00 72.30 OK 338.32 11. 27 4.287E+OO 8.401E-01 8.401E-01 47.22 OK 794.95 4.25 2.203E+OO Line Not Found Absent 835. 71 1. 61 2 .121E+OO Line Not Found Absent 911.20 25.80* 1.985E+OO 7.337E-01 7.337E-01 36. 72 OK 968. 97 15.80 1. 892E+OO 7.190E-01 7.190E-01 52.98 OK TH-228 74.82 10.28 6.737E+OO 8.329E-01 8.329E-01 55.13 OK 77 .11 17.10 6.908E+OO 1. 371E+OO 1. 371E+OO 20.03 OK Page 4666 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235076 Acquisition date 3-0CT-2016 06:47:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Ene.rgy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status 43.60* 5.636E+OO 8.067E-01 8.0..67E-01 13. 54 OK 300.09 3.30 4.719E+OO 1.365E+OO 1.365E+OO 64.85 OK TH-230 609.32 45.49* 2.698E+OO 8.666E-01 8.667E-01 19.69 OK 1120.29 14.92 1.688E+OO 8.905E-01 8.906E-01 57.46 OK 1764.49 15.30 1.138E+OO 8. 231E-01 8.231E-01 54.25 OK PA-231 283.69 1. 70 4.935E+OO Line Not Found Absent 301.36 5.35* 4. 719E+OO 8.420E-01 8.420E-01 64.85 OK TH-232 105.21 1.10 7.950E+OO 3.036E+OO 3.036E+OO 72. 30 OK 338.32 11. 27 4.287E+OO 8.401E-01 8.401E-01 47.22 OK 835. 71 1. 61 2 .121E+OO Line Not Found Absent 911. 20 25.80* 1.985E+00 7.337E-01 7.337E-01 36. 72 OK 968.97 15.80 1.892E+OO 7.190E-01 7.190E-01 52.98 OK TH-234 63.29 3.70* 5.569E+OO l.237E+OO 1.237E+OO 130. 55 OK 92.59 4.23 7.717E+OO 1. 734E+OO 1. 734E+OO 73.16 OK U-234 609.32 45.49* 2.698E+OO 8.666E-01 8.667E-01 19.69 OK 1120.29 14.92 1.688E+OO 8.905E-01 8.905E-01 57.46 OK 1764.49 15.30 1.138E+OO 8.231E-01 8. 231E-01 54.25 OK U-235 89. 96 3.47 7.607E+OO Line Not Found Absent 93.35 5.60 7: 717E+OO 1.310E+OO 1.310E+OO 73.16 OK 143.76 10. 96* 7.620E+OO Line Not Found <<INT Reject 163.33 5.08 7.206E+OO Line Not Found Absent 185.72 57.20 6.698E+OO l.293E-01 l.293E-01 62. 31 OK 205.31 5.01 6.280E+OO Line Not Found Absent U-238 63.29 3.70* 5.569E+OO l.237E+OO l.237E+OO 130.55 OK 92.59 4.23 7. 717E+OO 1.734E+OO 1. 734E+OO 73.16 OK AM-243 43.53 5.90 1.694E+OO Line Not Found Absent 74.66 67.20* 6.737E+OO 1.274E-01 1. 27 4E-01 55 .13 OK ANH-511 511. 00 100.00* 3.090E+OO 2.004E-02 2.004E-02 412.83 OK Flag: "*" = Keyline Page 4667 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:50:16.80 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235076.CNF;l *
  • Acquisition date 3-0CT-2016 06:47:24 Sensitivity : 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.98 Half life ratio : ***** *
  • Sample date 11-DEC-2015 14:19:00 Analyst initials: MXRl *
  • Sample ID G405235076 Sample Quantity 1.4447E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.146E+Ol 1.305E+OO SC-46 4.546E-01 3.244E-01 CD-109 3. 961E-01 1. 729E+OO SN-126 2.536E-02 1.107E-01 BA-137M 6.323E-02 5.234E-02 CS-137 6.680E-02 5.529E-02 CE-141 1.633E+Ol 3.689E+Ol EU-155 1.782E-01 1. 2 62E-01 TL-208 2.192E-01 7.139E-02 PB-212 8.067E-01 1.071E-01 BI-214 8.670E-01 1.673E-01 PB-214 1. 074E+OO 1.632E-01 RN-222 8.670E-01 1. 673E-01 RA-224 7.794E-01 1.344E+OO RA-226 8.670E-01 1.673E-01 AC-228 7.337E-01 2.640E-01 RA-228 7.337E-01 2.640E-01 TH-228 8.067E-01 1. 071E-01 TH-230 8.667E-01 1. 672E-01 PA-231 8.420E-01 5. 351E-01 TH-232 7.337E-01 2.640E-01 TH-234 1.237E+OO 1.583E+OO U-234 8.667E-01 1.672E-01 U-235 2.580E-01 2.799E-01 U-238 1.237E+00 1.583E+OO AM-243 1.274E-01 6.884E-02 ANH-511 2.004E-02 8.107E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4668 of 5809 Key-Line Activity (pCi/GRAM 8.034E+00 -1.233E-02 O.OOOE+OO K.L. Cnt Uncert ( 1. 96-sigma) 1.085E+01 4.464E-02 1.960E+41 MDA (pCi/GRAM 5.092E-01 5.106E-01 1.746E+OO 1.121E-01 4.903E-02 5.180E-02 3.062E+Ol 1.426E-01 4.973E-02 8.648E-02 1.059E-01 1.056E-01 1.059E-01 9. 271E-01 1.059E-01 1.987E-01 1.987E-01 8.648E-02 1.059E-01 6.090E-01 1.987E-01 1. 2 69E+OO 1.059E-01 3.009E-01 1.269E+OO 5.730E-02 4.632E-02 MDA (pCi/GRAM 2 .117E+Ol 8.424E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 1.102E-02 3.065E-02 6.872E-02 NOT IDENT. V-48 O.OOOE+OO 8.958E+03 O.OOOE+OO SHORT HLIF CR-51 O.OOOE+OO 3.388E+02 0.000E+OO SHORT HLIF MN-54 -6.691E-04 4. 960E-02 9. 501E-02 NOT IDENT. C0-56 -1.534E-01 4.212E-01 7.466E-01 NOT IDENT. MN-56 O.OOOE+OO 1.960E+41 0.000E+OO SHORT HLIF C0-57 -1. 403E-03 3.525E-02 6.550E-02 NOT IDENT. C0-58 2.948E-02 3.568E-01 7.266E-01 NOT IDENT. FE-59 1.537E+OO 4.603E+OO 1.002E+Ol NOT IDENT. C0-60 2.040E-02 2. 964E;-02 6.926E-02 NOT IDENT. ZN-65 7.236E-03 1.498E-01 2.703E-01 NOT IDENT. GE-68 -8.030E-01 1.743E+OO 3.282E+OO NOT IDENT. AS-73 -8.083E-01 3.874E+OO 7.270E+OO NOT IDENT. AS-74 0.000E+OO 4.063E+03 O.OOOE+OO SHORT HLIF SE-75 -4. 396E-02 1.774E-01 3.423E-01 NOT IDENT. BR-77 O.OOOE+OO 7.704E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 5.857E+02 0.000E+OO SHORT HLIF RB-83 8.438E-Ol 6.423E-01 1.079E+OO FAIL ABUN KR-85 -1.079E+OO 5.732E+OO l.080E+Ol NOT IDENT. SR-85 -1.136E-01 5.855E-01 1.103E+OO NOT IDENT. RB-86 O.OOOE+OO l.871E+04 O.OOOE+OO SHORT HLIF Y-88 5. 096E-02 1. 576E-01 3.829E-01 NOT IDENT. Y-91 -3. 241E+02 4 .137E+02 7.162E+02 NOT IDENT. NB-94 3.978E-03 2.342E-02 4.663E-02 NOT IDENT. NB-95 -6.355E-01 7.999E-01 1.323E+OO NOT IDENT. NB-95M 1.268E+OO 1.903E+OO 3.642E+OO NOT IDENT. ZR-95 5.277E-02 1.032E+OO 2.032E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 960E+41 0. OOOE+OO' SHORT HLIF ZR-97 0.000E+OO 1.439E+41 0.000E+OO SHORT HLIF M0-99 O.OOOE+OO 6. 911E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 -8.359E-03 2.923E-02 4.833E-02 NOT IDENT. RH-102 1. 135E-02 5.035E-02 1. OOlE-01 FAIL ABUN RU-103 -1.052E+OO 4.418E+OO 8.344E+OO FAIL ABUN RH-106 -9.982E-03 3.898E-01 7.556E-01 FAIL ABUN RU-106 -9.982E-03 3.898E-01 7.556E-01 FAIL ABUN AG-108M -1.150E-02 2.108E-02 3.856E-02 NOT IDENT. AG-llOM 3.083E-02 8.597E-02 l.681E-01 NOT IDENT. SN-113 -2.004E-01 1. 836E-01 3 .132E-01 NOT IDENT. CD-115 O.OOOE+OO 9.433E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 7.193E+04 O.OOOE+OO SHORT HLIF TE-123M 1. 810E-02 1.143E-01 2. llOE-01 NOT IDENT. SB-124 5.994E-01 1.135E+OO 3.092E+OO NOT IDENT. SB-125 -3.358E-02 9.077E-02 1.689E-01 FAIL ABUN TE-125M -2. OllE+Ol 2.014E+02 3. 723E+02 NOT IDENT. I-126 O.OOOE+OO 6.547E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 7.896E+05 0.000E+OO SHORT HLIF SB-127 O.OOOE+OO 1.174E+22 0.000E+OO SHORT HLIF I-131 O.OOOE+OO 3.000E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 796E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.842E+26 O.OOOE+OO SHORT HLIF BA-133 6.873E-03 3.025E-02 5.646E-02 FAIL ABUN I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 1.627E-02 4.345E-02 8.735E-02 NOT IDENT. CS-135 -1.650E-02 1.255E-01 2.200E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.405E+05 O.OOOE+OO SHORT HLIF CE-139 -2.307E-02 8.946E-02 1.594E-01 NOT IDENT. BA-140 O.OOOE+OO 9.162E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.770E+05 O.OOOE+OO SHORT HLIF CE-143 O.OOOE+OO l.411E+41 O.OOOE+OO SHORT HLIF CE-144 -5.348E-04 2.688E-01 4.983E-01 FAIL ABUN PM-144 1.297E-02 4.880E-02 9.610E-02 NOT IDENT. PR-144 1.125E+OO 4.232E+OO 8.334E+OO NOT IDENT. PM-146 -3.708E-03 3.603E-02 6.940E-02 NOT IDENT. ND-147 . O.OOOE+OO 2.481E+07 O.OOOE+OO SHORT HLIF PM-147 l.903E+02 5.791E+02 1.119E+03 NOT IDENT. PM-149 O.OOOE+OO l.393E+40 O.OOOE+OO SHORT HLIF EU-150 6.993E-03 2.014E-02 3.776E-02 FAIL ABUN EU-152 -2.907E-04 7.430E-02 l.461E-01 NOT IDENT. GD-153 -2.566E-02 1.392E-01 2.367E-01 NOT IDENT. EU-154 -3.238E-02 1.092E-01 2.055E-01 FAIL ABUN TB-160 2.261E-02 l.343E+OO 2.624E+OO FAIL ABUN H0-166M -4.392E-02 5.217E-02 8.629E-02 FAIL ABUN TM-171 -6.614E+OO 8.566E+OO 1.561E+Ol NOT IDENT. HF-172 7.565E-02 1.872E-01 3.352E-01 FAIL ABUN LU-172 2.317E-02 6.281E-02 1.338E-01 FAIL ABUN LU-176 -7.537E-03 2.099E-02 3.984E-02 FAIL ABUN Page 4669 of 5809 HF-181 4.085E-01 3.175E+OO 6.341E+OO NOT IDENT. TA-182 -5.091E-01 7. 371E-01 1. 299E+OO FAIL ABUN RE-183 -2. 471E-01 1.419E+OO 2.702E+OO NOT IDENT. RE-184 4.579E+OO 2.413E+Ol 4.748E+Ol NOT IDENT. W-188 -1.064E+02 9.662E+Ol l.467E+02 FAIL ABUN IR-192 8.082E-02 3.923E-01 7.823E-01 FAIL ABUN HG-203 8.830E-01 1. 895E+OO 3.877E+OO NOT IDENT. BI-207 2.821E-02 6.402E-02 9.033E-02 FAIL ABUN PB-210 -9.385E-03 1. 265E+OO 2.503E+00 NOT IDENT. BI-211 O.OOOE+OO 4. 494E-Cll 7.370E-01 FAIL ABUN PB-211 1.264E-01 5.341E-01 9.856E-01 NOT IDENT. BI-212 7.403E-01 7.023E-01 1.084E+OO FAIL ABUN RN-219 -1. 396E-01 2. 961E-01 5.490E-01 FAIL ABUN RA-223 5.766E-02 5.249E-01 9.426E-01 FAIL ABUN AC-227 -l.566E-01 2.002E-01 3.693E-01 FAIL ABUN TH-227 -1.566E-01 2.002E-01 3.693E-01 FAIL ABUN TH-229 -7.687E-02 3.976E-01 7.052E-01 FAIL ABUN TH-231 5.766E-02 5.249E-01 9.426E-01 FAIL ABUN PA-233 -2.916E-02 4.728E-02 8.758E-02 FAIL ABUN PA-234 7.290E-02 2.359E-01 4.536E-01 FAIL ABUN PA-234M -1.645E+OO 3.640E+OO 6.858E+OO NOT IDENT. NP-237 -2.916E-02 4. 728E-02 8.758E-02 FAIL ABUN NP-238 O.OOOE+OO l.334E+41 O.OOOE+OO SHORT HLIF NP-239 -l.OOlE-01 1.819E-01 3.224E-01 FAIL ABUN PU-239 0.000E+OO 4.431E+02 5.109E+02 FAIL ABUN AM-241 -2.917E-02 7.466E-02 1.281E-01 NOT IDENT. CM-243 -5.446E-02 7.939E-02 1. 272E-01 NOT IDENT. BK-247 '-1. 683E-02 6.494E-02 l.194E-01 FAIL ABUN CM-247 -1.183E-02 2.779E-02 5.176E-02 NOT IDENT. CF-249 l.326E-02 3.677E-02 7.312E-02 NOT IDENT. CF-251 4.753E-02 9.379E-02 1. 792E-01 NOT IDENT. Page 4670 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:50:14.53 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 318 10.66* 1.354E+OO 1.146E+Ol 1.146E+Ol 11. 61 SC-46 889.28 15 99.98* 2. 021E+OO 3.906E-02 4.546E-01 72. 80 1120. 55 43 99.99 1.688E+OO l.329E-01 1.547E+OO 57.46 CD-109 88.03 69 3.70* 7.495E+OO 1.286E+OO 2.008E+OO 85.73 SN-126 64.28 49 9.60 5.569E+OO 4.768E-01 4.768E-01 130. 55 86.94 69 8.90 7.495E+OO 5.345E-01 5.345E-01 85.73 87.57 69 37.00* 7.495E+OO 1.286E-01 1.286E-01 85.73 BA-137M 661.66 27 89.90* 2.534E+OO 6.206E-02 6.323E-02 84.46 CS-137 661. 66 27 85.10* 2.534E+OO 6.556E-02 6.680E-02 84.46 CE-141 145.44 41 48.29* 7.611E+OO 5.857E-02 3.274E+Ol 110. 68 EU-155 86.55 69 30.70 7.495E+OO 1.550E-01 1. 745E-01 85.73 105.31 51 21.10* 7.950E+OO l.583E-01 1.782E-01 72.30 TL-208 277.37 ------6.60 5.023E+OO ------Line Not Found ------583.19 100 85.00* 2.790E+OO 2.192E-01 2.192E-01 33.24 860.56 19 12.50 2.074E+OO 3.760E-01 3.760E-01 90.75 BI-211 72. 87 ------1. 23 6.'565E+OO ------Line Not Found ------351.06 306 12.92* 4.154E+OO 2.959E+OO 2.959E+OO 15.50 PB-212 74.82 195 10.28 6.737E+OO 1.465E+OO 1.465E+OO 29.57 77 .11 312 17.10 6.908E+OO 1. 371E+OO 1.371E+OO 20.03 238.63 381 43.60* 5.636E+OO 8.067E-01 8.067E-01 13. 54 300.09 41 3.30 4.719E+OO 1.365E+OO 1.365E+OO 64.85 BI-214 609.32 205 45.49* 2.698E+OO 8.666E-01 8.670E-01 19.69 1120.29 43 14.92 1. 688E+OO 8.905E-01 8.909E-01 57.46 1764.49 28 15.30 1.138E+OO 8. 231E-01 8.233E-01 54.25 PB-214 74.82 195 5.80 6.737E+OO 2.596E+OO 2.597E+OO 29.57 77 .11 312 9.70 6.908E+OO 2. 417E+OO 2.418E+OO 20.03 87.09 69 3.41 7.495E+OO 1.395E+OO 1. 396E+OO 85.73 242.00 122 7.25 5.585E+OO 1. 561E+OO 1. 561E+OO 46.61 295.22 190 18.42 4.779E+OO 1.120E+OO l.120E+OO 24.10 351. 93 306 35.60* 4.154E+OO 1.074E+OO l.074E+OO 15.50 RN-222 609.32 205 45.49* 2.698E+OO 8.666E-01 8.670E-01 19.69 1120.29 43 14.92 1.688E+OO 8.905E-01 8.909E-01 57.46 1764.49 28 15.30 1.138E+OO 8.231E-01 8.233E-01 54.25 RA-224 240.99 122 4.10* 5.585E+OO 2.760E+OO 2.760E+OO 46.61 RA-226 609.32 205 45.49* 2.698E+OO 8.666E-01 8.670E-01 19.69 1120.29 43 14.92 1.688E+OO 8.905E-01 8.909E-01 57.46 1764.49 28 15.30 1.138E+OO 8. 231E-01 8.233E-01 54.25 AC-228 105.21 51 1.10 7.950E+OO 3.036E+OO 3.036E+OO 72.30 338.32 78 11. 27 4.287E+OO 8.401E-01 8. 401E-01 47.22 794.95 ------4.25 2.203E+OO ------Line Not Found ------835. 71 ------1. 61 2.121E+OO ------Line Not Found ------911.20 72 25.80* 1.985E+OO 7.337E-01 7.337E-01 36.72 968.97 41 15.80 1.892E+OO 7.190E-01 7.190E-01 52.98 RA-228 105.21 51 1.10 7.950E+OO 3.036E+OO 3.036E+OO 72.30 338.32 78 11. 27 4.287E+OO 8.401E-01 8.401E-01 47.22 794.95 ------4.25 2.203E+OO ------Line Not Found ------835. 71 ------1. 61 2.121E+OO ------Line Not Found ------Page 4671 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235076 Acquisition date 3-0CT-2016 06:.47:24 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911.20 72 25.80* 1.985E+OO 7.337E-01 7.337E-01 36. 72 968. 97 41 15.80 1.892E+OO 7.190E-01 7.190E-01 52.98 TH-228 74.82 195 10.28 6.737E+OO 1.465E+OO l.465E+OO 29.57 77 .11 312 17.10 6.908E+OO 1.371E+OO l.371E+OO 20.03 238.63 381 43.60* 5.636E+OO 8.067E-01 8.067E-01 13.54 300.09 41 3.30 4. 719E+OO 1.365E+OO 1.365E+OO 64.85 TH-230 609.32 205 45.49* 2.698E+OO 8.666E-01 8.667E-01 19.69 1120.29 43 14.92 1. 688E+OO 8.905E-01 8.906E-01 57.46 1764.49 28 15.30 1.138E+OO 8. 231E-01 8.231E-01 54.25 PA-231 283.69 ------1. 70 4.935E+OO ------Line Not Found ------301.36 41 5.35* 4. 719E+00 8.420E-01 8.420E-01 64.85 TH-232 105.21 51 1.10 7.950E+OO 3.036E+00 3.036E+OO 72. 30 338.32 78 11. 27 4.287E+OO 8.401E-01 8.401E-01 47.22 835. 71 ------1. 61 2.121E+00 ------Line Not Found ------911.20 72 25.80* 1.985E+OO 7.337E-01 7.337E-01 36.72 968.97 41 15.80 1. 892E+OO 7.190E-01 7.190E-01 52.98 TH-234 63.29 49 3.70* 5.569E+OO l.237E+OO 1.237E+OO 130.55 92.59 109 4.23 7.717E+OO 1. 734E+OO 1.734E+OO 73.16 U-234 609.32 205 45.49* 2.698E+OO 8.666E-01 8.667E-01 19.69 1120.29 43 14.92 1.688E+OO 8.905E-01 8.905E-01 57.46 1764.49 28 15.30 1.138E+OO 8. 231E-01 8. 231E-01 54.25 U-235 89.96 ------3.47 7.607E+OO ------Line Not Found ------93.35 109 5.60 7.717E+OO 1.310E+OO 1.310E+OO 73.16 143.76 41 10. 96* 7. 611E+OO 2.580E-01 2.580E-01 110. 68 163.33 ------5.08 7.206E+OO ------Line Not Found ------185. 72 95 57.20 6.698E+OO l.293E-01 l.293E-01 62.31 205.31 ------5.01 6.280E+00 ------Line Not Found ------U-238 63.29 49 3.70* 5.569E+00 l.237E+OO 1.237E+OO 130.55 92.59 109 4.23 7. 717E+OO 1.734E+OO 1. 734E+OO 73.16 AM-243 43.53 ------5.90 1.694E+OO ------Line Not Found ------74.66 195 67.20* 6.737E+00 2. 241E-01 2.241E-01 29.57 ANH-511 511. 00 12 100.00* 3.090E+OO 2.004E-02 2.004E-02 412.83 Flag: "*" Key line Page 4672 of 5809 Summary of Nuclide Activity Sample ID : G405235076 Acquisition date Page : 3 3-0CT-2016 06:47:24 Total number of lines in spectrum 45 Number of unidentified lines 6 Number of lines tentatively identified by NID 39 Nuclide Type : Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 CE-141 EU-155 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife 1. 25E+09Y 83.79D 461. 40D 2.30E+05Y 30.08Y 30.08Y 32. 510 4.75Y 1. 41E+10Y 7.04E+08Y 1.41E+l0Y 1600.00Y 1600. OOY 1600.00Y 1.41E+10Y 1600. OOY 1. 41E+10Y 1. 41E+10Y 1. 41E+l0Y 7.54E+04Y 7.04E+08Y l.41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y l.00E+09Y Decay 1. 00 11. 6 1. 56 1. 00 1. 02 1. 02 559. 1.13 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1'. 00 1. 00 1. 00 1. 00 1. 00 1; 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.14 6E+Ol 3.906E-02 1.286E+OO 1.286E-01 6.206E-02 6.556E-02 5.857E-02 1.583E-01 2.192E-01 2.959E+OO 8.067E-01 8.666E-01 1.074E+OO 8.666E-01 2.760E+OO 8.666E-01 7.337E-01 7.337E-01 8.067E-01 8.666E-01 8.420E-01 7.337E-01 1.237E+OO 8.666E-01 2.580E-01 1.237E+OO 2.241E-01 2.004E-02 3.224E+Ol 3.224E+Ol Decay Corr pCi/GRAM 1.146E+Ol 4.546E-01 2.008E+OO 1. 28 6E-01 6.323E-02 6.680E-02 3.274E+Ol l.782E-01 2.192E-Ol 2.959E+OO 8.067E-01 8.670E-01 1. 074E+OO 8.670E-01 2.760E+OO 8.670E-01 7.337E-01 7.337E-01 8.067E-01 8.667E-01 8.420E-01 7.337E-01 1.237E+OO 8.667E-01 2.580E-01 l.237E+OO 2.241E-01 2.004E-02 6.608E+Ol 6.608E+Ol 86.67% Decay Corr 2-Sigma Error 0.133E+Ol 3.310E-01 1. 721E+OO l.102E-01 5.341E-02 5.642E-02 3.623E+Ol 1.288E-01 0.728E-01 0.459E+OO 1. 093E-01 1.707E-01 0.167E+OO 1. 707E-01 1. 286E+OO 1. 707E-01 2.694E-01 2.694E-01 1.093E-01 1.706E-01 5.460E-01 2.694E-01 1.615E+OO l.706E-01 2.856E-01 1.615E+OO 0.663E-01 8.273E-02 "M" Manually accepted 2-Sigma %Error 11.61 72.80 85.73 85.73 84.46 84.46 110. 68 72.30 33.24 15.50 13.54 19.69 15.50 19.69 46.61 '19.69 36.72 36.72 13.54 19.69 64.85 36.72 130.55 19.69 110. 68 130. 55 29.57 412.83 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4673 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID :* G405235076 Acquisition date : 3-0CT-2016 06:47:24 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 6 80.76 48 183 1. 86 161.60 144 22 1.09E-02 **** 7.15E+OO T 0 129.31 55 112 0.64 258.70 255 8 1.27E-02 79.1 7.86E+OO T 0 209.65 33 133 1. 48 419.43 415 9 7.95E-03 **** 6.19E+OO T 0 :no. 64 33 89 1. 08 541.44 536 10 8.16E-03 **** 5.12E+OO T 0 328.26 41 57 0.79 656.71 651 11 1.04E-02 81. 3 4.39E+OO T 0 412.07 14 65 3.49 824.38 813 14 3.70E-03 **** 3.66E+OO T 0 462.53 32 48 3.93 925.33 919 12 8.26E-03 97.4 3.34E+OO T 0 474.56 17 22 1. 43 949.40 944 8 4.45E-03 **** 3.28E+OO T 0 521.35 20 12 2.23 1043.02 1039 9 5.37E-03 77.7 3.04E+00 T 0 538.80 14 57 7.25 1077.92 1066 18 3.61E-03 **** 2.97E+OO 0 727.70 22 23 1. 43 1455.88 1449 11 6.05E-03 96. 8 2.36E+OO T 0 872.90 8 3 1. 35 1746.40 1743 6 2.25E-03 97.3 2.05E+OO T 0 951.40 12 5 3.95 1903.47 1898 11 3.46E-03 90.9 1. 92E+OO 0 1051.57 9 13 1. 34 2103.92 2096 10 2. 61E-03 **** 1.78E+OO T 0 1063.31 7 15 0.81 2127.40 2118 12 1. 96E-03 **** 1. 7 6E+OO T 0 1234.43 9 16 1. 03 2469.83 2463 *10 2.67E-03 **** 1.56E+OO T 0 1304.20 8 8 0.88 2609.45 2602 11 2.21E-03 **** 1.49E+OO 0 1319.96 3 15 0.50 2641.00 2633 10 8.33E-04 **** l.48E+OO 0 1569.66 7 0 0.50 3140.71 3134 11 l.94E-03 75.6 1.27E+OO 0 1982.88 5 3 0.94 3967.79 3960 11 1.46E-03 **** 1. OlE+OO Flags: "T" = Tentatively' associated Page 4674 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:50:29.16 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235076.CNF;l * *Acquisition date 3-0CT-2016 06:47:24 Sensitivity 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: O 01:00:01.98 Half life ratio : ***** *
  • Sample date ll-DEC-2015 14:19:00 Nuclide Library : SOLID *
  • Sample ID G405235076 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : l.4447E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF 'GAM24 CAN.CNF;?
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 SC-46 CD-109 SN-126 BA-137M CS-137 CE-141 EU-155 TL-208 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 PA-231 TH-232 TH-234 U-234 U-235 l'.J-238 AM-243 ANH-511 Le (pCi/GRAM 2.057E-01 2.142E-01 8.314E-01 5.337E-02 2.130E-02 2. 251E-02 1.418E+Ol 6.631E-02 2.183E-02 4.027E-02 4.712E-02 4.786E-02 4.712E-02 4.317E-01 4.712E-02 8.545E-02 8.545E-02 4.027E-02 4.710E-02 2.755E-Ol 8.545E-02 5.980E-01 4. 710E-02 l.416E-01 5.980E-01 2.699E-02 2.083E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 Page 4675 of 5809 Le (pCi/GRAM 9.573E+OO 3.634E-02 O.OOOE+OO 2.803E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT.

V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM_:._147 PM-149 EU-150 EU-152 GD-153 EU-154 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 Page 4676 of 5809 O.OOOE+OO O.OOOE+OO 4.lOOE-02 3.245E-01 O.OOOE+OO 3.043E-02 3.029E-01 4.265E+OO 2.926E-02 l.159E-01 1.371E+OO 3.395E+OO O.OOOE+OO l.579E-01 O.OOOE+OO O.OOOE+OO 4.826E-01 4.832E+OO 4.932E-01 O.OOOE+OO l.470E-01 3.006E+02 2.035E-02 5.829E-01 1.693E+OO 8.729E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.253E-02 4.437E-02 3.699E+OO 3.304E-01 3.304E-01 1. 700E-02 7.306E-02 1. 391E-01 O.OOOE+OO O.OOOE+OO 9.875E-02 1.166E+OO 7.609E-02 1.737E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.523E-02 O.OOOE+OO 3.869E-02 1.012E-01 O.OOOE+OO O.OOOE+OO 7.394E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.315E-01 4.284E-02 3.715E+OO 3.107E-02 O.OOOE+OO 5.190E+02 O.OOOE+OO 1. 711E-02 6.633E-02 1.106E-01 8.855E-02 1.112E+OO 3.762E-02 7.232E+OO l.564E-01 5.808E-02 1.824E-02 2.816E+OO SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 PB-210 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4677 of 5809 5.488E-01 1.264E+OO 2.062E+Ol 6.623E+Ol 3.596E-01 1. 791E+OO 3. 967E-02 1.176E+OO 3.551E-01

  • 4.412E-01 4. 967E-01 2. 451E-01 4.302E-01 1.703E-01 1. 703E-01 3.271E-01 4.302E-01 3. 965E-02 1. 960E-01 2.970E+OO 3. 965E-02 O.OOOE+OO 1.495E-01 2.406E+02 5.987E-02 5.901E-02 5.504E-02 2.318E-02 3.370E-02 8.342E-02 FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT . FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:50:37.64 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235076.CNF;l *
  • Acquisition date 3-0CT-2016 06:47:24 Sensitivity : 3.000 *
  • Detector ID GAM24 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.98 Half life ratio : ***** *
  • Sample date 11-DEC-2015 14:19:00 Nuclide Library : SOLID *
  • Sample ID G405235076 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4447E+02 GRAM *
  • Quantity Err(%) : 1.3844E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 17-JUN-2016 07:45:20 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM24 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1. 96-sigma) K-40 1.146E+Ol 1.435E+OO 1.435E+OO SC-46 4.546E-01 3.249E-01 3.249E-01 CD-109 3. 961E-01 1. 741E+OO 1. 741E+OO SN-126 2.536E-02 1.115E-01 1.115E-01 BA-137M 6.323E-02 5.241E-02 5.241E-02 CS-137 6.680E-02 5.537E-02 5.537E-02 CE-141 1.633E+Ol 3.692E+Ol 3.692E+01 EU-155 1. 782E-01 1.269E-01 1. 2 69E-01 TL-208 2.192E-01 7.199E-02 7.199E-02 PB-212 8.067E-01 1.152E-01 1.152E-01 BI-214 8.670E-01 1.713E-01 1. 713E-01 PB-214 l.074E+00 1.691E-01 1. 691E-01 RN-222 8.670E-01 1. 713E-01 1. 713E-01 RA-224 7.794E-01 1. 351E+OO 1.351E+OO RA-226 8.670E-01 1.713E-01 1. 713E-01 AC-228 7.337E-01 2.667E-01 2.667E-01 RA-228 7.337E-01 2.667E-01 2.667E-01 TH-228 8.067E-01 1.152E-01 1.152E-01 TH-230 8.667E-01 l.713E-01 1.713E-01 PA-231 8.420E-01 5.645E-01 5.645E-01 TH-232 7.337E-01 2.667E-01 2.667E-01 TH-234 1.237E+OO 1.606E+OO l.606E+OO U-234 8.667E-01 1.713E-01 1. 713E-01 U-235 2.580E-01 2.802E-01 2.802E-01 U-238 1.237E+OO 1. 606E+OO 1.606E+OO AM-243 1.274E-01 7.035E-02 7.035E-02 ANH-511 2.004E-02 8.108E-02 8.108E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1.96-sigma) ( 1. 96-sigma) BE-7 8.034E+OO 1.086E+Ol 1.145E+Ol NOT IDENT. NA-22 -1.233E-02 4.465E-02 4.499E-02 NOT IDENT. NA-24 -1.000E+41 8.509E+41 O.OOOE+OO SHORT HLIF Page 4678 of 5809 AL-26 l.102E-02 3.065E-02 3.105E-02 NOT IDENT. V-48 -2.543E+03 8.959E+03 9.032E+03 SHORT HLIF CR-51 -l.599E+02 3.389E+02 3.464E+02 SHORT HLIF MN-54 -6.691E-04 4. 960E-02 4. 960E-02 NOT IDENT. C0-56 -1.534E-01 4.212E-01 4.268E-01 NOT IDENT. MN-56 -1. OOOE+41 l.278E+42 O.OOOE+OO SHORT HLIF C0-57 -l.403E-03 3.525E-02 3.526E-02 NOT IDENT. C0-58 2.948E-02 3.568E-01 3.570E-01 NOT IDENT. FE-59 l.537E+OO 4.604E+OO 4.656E+OO NOT IDENT. C0-60 2.040E-02 2.965E-021 3.104E-02 NOT IDENT. ZN-65 7.-236E-03 1.498E-01 1.498E-01 NOT IDENT. GE-68 -8.030E-01 1. 743E+OO 1. 780E+OO NOT IDENT. AS-73 -8.083E-01 3.877E+OO 3.895E+OO NOT IDENT. AS-74 l.201E+03 4.064E+03 4.100E+03 SHORT HLIF SE-75 -4. 396E-02 l.774E-01 1.785E-01 NOT IDENT. BR-77 5.804E+37 4.971E+38 O.OOOE+OO SHORT HLIF SR-82 -2.830E+02 5.858E+02 5. 996E+02 SHORT HLIF RB-83 8.438E-01 6.526E-01 7.554E-01 FAIL ABUN KR-85 -1.079E+OO 5.732E+OO 5.753E+OO NOT IDENT. SR-85 -l.136E-01 5.855E-01 5.878E-01 NOT IDENT. RB-86 -5.422E+03 1. 872E+04 1.887E+04 SHORT HLIF Y-88 5. 096E-02 1.577E-01 l.593E-01 NOT IDENT. Y-91 -3. 241E+02 4.139E+02 4.389E+02 NOT IDENT. NB-94 3.978E-03 2.342E-02 2.349E-02 NOT IDENT. NB-95 -6.355E-01 8.003E-01 8. 501E-01 NOT IDENT. NB-95M 1.268E+OO 1.906E+OO 1.990E+OO NOT IDENT. ZR-95 5.277E-02 1.032E+OO 1.033E+OO NOT IDENT. NB-97 1'. OOOE+41 4.647E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 1.440E+41 O.OOOE+OO SHORT HLIF M0-99 3.362E+31 6.915E+31 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 4.028E+41 O.OOOE+OO SHORT HLIF RH-101 -8.359E-03 2.927E-02 2.952E-02 NOT IDENT. RH-102 1.135E-02 5.035E-02 5.061E-02 FAIL ABUN RU-103 -1.052E+OO 4.418E+OO 4.444E+OO FAIL ABUN RH-106 -9.982E-03 3.898E-01 3.899E-01 FAIL ABUN RU-106 -9.982E-03 3.898E-01 3.899E-01 FAIL ABUN AG-108M -1.150E-02 2.108E-02 2 .171E-02 NOT IDENT. AG-110M 3.083E-02 8.599E-02 8.710E-02 NOT IDENT. SN-113 -2.004E-01 1.838E-01 2.048E-01 NOT IDENT. CD-115 l.268E+38 9.436E+38 O.OOOE+OO SHORT HLIF SN-117M -2.446E+04 7.199E+04 7.283E+04 SHORT HLIF TE-123M l.810E-02 1.143E-01 l.146E-01 NOT IDENT. SB-124 5.994E-01 1.136E+OO l.168E+OO NOT IDENT. SB-125 -3.358E-02 9.078E-02 9.203E-02 FAIL ABUN TE-125M -2. 011E+Ol 2.014E+02 2.016E+02 NOT IDENT. I-126 3.228E+05 6.562E+05 6. 721E+05 SHORT HLIF SB-126 1.463E+05 7.901E+05 7.928E+05 SHORT HLIF SB-127 -8.481E+21 1. 646E+22 O.OOOE+OO SHORT HLIF I-131 -5.825E+08 3.000E+09 3.012E+09 SHORT HLIF I-132 -l.OOOE+41 1.838E+42 O.OOOE+OO SHORT HLIF TE-132 3.270E+24 1.842E+26 O.OOOE+OO SHORT HLIF BA-133 6.873E-03 3.025E-02 3.041E-02 FAIL ABUN I-133 1.000E+41 6.233E+41 O.OOOE+OO SHORT HLIF CS-134 l.627E-02 4.345E-02 4.407E-02 NOT IDENT. CS-135 -l.650E-02 l.255E-01 1.257E-01 NOT IDENT. I-135 l.000E+41 7.685E+41 O.OOOE+OO SHORT HLIF CS-136 -1.117E+05 2.408E+05 2.460E+05 SHORT HLIF CE-139 -2.307E-02 8.958E-02 9.019E-02 NOT IDENT. BA-140 -3.426E+05 9.163E+05 9.292E+05 SHORT HLIF LA-140 -9.405E+04 2.770E+05 2.802E+05 SHORT HLIF CE-143 l.000E+41 1.415E+41 O.OOOE+OO SHORT HLIF CE-144 -5.348E-04 2.688E-01 2.688E-01 FAIL ABUN PM-144 l.297E-02 4.881E-02 4.915E-02 NOT IDENT. PR-144 1.125E+OO 4.232E+OO 4.262E+OO NOT IDENT. PM-146 -3.708E-03 3.603E-02 3.607E-02 NOT IDENT. ND-147 7.718E+06 2.482E+07 2.506E+07 SHORT HLIF PM-147 l.903E+02 5.792E+02 5.855E+02 NOT IDENT. PM-149 -9.092E+39 l.407E+40 O.OOOE+OO SHORT HLIF EU-150 6.993E-03 2.014E-02 2.039E-02 FAIL ABUN EU-152 -2.907E-04 7.430E-02 7.430E-02 NOT IDENT. GD-153 -2.566E-02 1.392E-01 1.397E-01 NOT IDENT. EU-154 -3.238E-02 1.092E-01 1.102E-01 FAIL ABUN TB-160 2.261E-02 1.343E+OO 1.343E+OO FAIL ABUN H0-166M -4.392E-02 5.222E-02 5.585E-02 FAIL ABUN TM-171 -6.614E+OO 8.586E+OO 9.089E+OO NOT IDENT. HF-172 7.565E-02 1.876E-01 l.907E-01 FAIL ABUN LU-172 2.317E-02 6.285E-02 6. 371E-02 FAIL ABUN LU-176 -7.537E-03 2.lOOE-02 2.127E-02 FAIL ABUN Page 4679 of 5809 HF-181 4.085E-01 3.175E+OO 3.180E+OO NOT IDENT. TA-182 -5.091E-01 7.373E-01 7.722E-01 FAIL ABUN RE-183 -2.471E-01 1.420E+OO l.424E+OO NOT IDENT. RE-184 4.579E+OO 2.415E+Ol 2.424E+Ol NOT IDENT. W-188 -1.064E+02 9.735E+Ol l.085E+02 FAIL ABUN IR-192 8.082E-02 3.924E-01 3.941E-01 FAIL ABUN HG-203 8.830E-01 l.895E+OO 1. 937E+OO NOT IDENT. BI-207 2.821E-02 6.403E-02 6.528E-02 FAIL ABUN PB-210 -9.385E-03 1.265E+OO 1.265E+OO NOT IDENT. BI-211 2.959E+OO 4.683E-01 1.414E+OO FAIL ABUN PB-211 1. 2 64E-01 5.342E-01 5. 372E-01 NOT IDENT. BI-212 7.403E-01 7.033E-01 7.785E-01 FAIL ABUN RN-219 -1. 396E-01 2. 966E-01 3.032E-01 FAIL ABUN RA-223 5.766E-02 5.249E-01 5.255E-01 FAIL ABUN AC-227 -l.566E-01 2.013E-01 2.133E-01 FAIL ABUN TH-227 -1.566E-01 2.013E-01 2 .133E-01 FAIL ABUN TH-229 -7.687E-02 3.976E-01 3.991E-01 FAIL ABUN TH-231 5.766E-02 5.249E-01 5.255E-01 FAIL ABUN PA-233 -2.916E-02 4.730E-02 4.909E-02 FAIL ABUN PA-234 7.290E-02 2.502E-01 2.524E-01 FAIL ABUN PA-234M -1.645E+OO 3.640E+OO 3.715E+OO NOT IDENT. NP-237 -2.916E-02 4.730E-02 4.909E-02 FAIL ABUN NP-238 -1.273E+40 1. 334E+41 O.OOOE+OO SHORT HLIF NP-239 -l.OOlE-01 l.821E-01 1. 876E-01 FAIL ABUN PU-239 5.716E+02 4.438E+02 5 .131E+02 FAIL ABUN AM-241 -2.917E-02 7.469E-02 7.584E-02 NOT IDENT. CM-243 -5.446E-02 7.955E-02 8.325E-02 NOT IDENT. BK-247 -1. 6'83E-02 6.503E-02 6.547E-02 FAIL ABUN CM-247 -1.183E-02 2.786E-02 2.836E-02 NOT IDENT. CF-249 l.326E-02 3.679E-02 3. 727E-02 NOT IDENT. CF-251 4.753E-02 9.394E-02 9.635E-02 NOT IDENT. Page 4680 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 67.1217 87.09 131.5173 136.47 77.2554 45.60 60.6209 87.57 131.6194 140.51 0.0000 46.54 67.6189 88.03 131.7169 143.76 52.7158 49.72 0.0000 88.34 138.8682 144.24 52.7453 51. 35 72.3450 88.47 138.8971 145.44 52.8190 51. 87 71. 4378 89. 96 123.6005 152.43 60.1869 52.39 69.5343 1093.63 121.6008 153.25 0.0000 52.97 72.6082 91.11 0.0000 323.87 78.8636 53.44 69. 6967 92.59 112.3444 156.02 0.0000 54.07 59.8228 93.35 112.4765 158.56 0.0000 57.36 0.0000 94.56 112. 6872 159.00 67.6227 57.53 77.3460 94.65 112.7032 162.33 73.7176 57.98 74.4025 94.67 112.7065 162.66 0.0000 59.27 77. 9632 94.87 112.7409 163.33 56.2266 59.32 77.9714 97.43 73.2985 165.86 61.0764 59.54 78.0068 98.43 79.1666 176.31 59.3689 60. 96 78.2340 98.44 79.1677 176.60 0.0000 61.17 78.2673 99.53 65. 9606 177. 52 49.9314 62. 93 88.3630 100 .11 67.0997 181.07 0.0000 63.29 88.4262 102.03 70.9075 181.52 50.9284 63.58 88.4774 103.18 62.3295 184.41 53.8680 64.28 88.5997 103.37 72. 4960 143.76 53.9381 66.73 100. 9603 105.21 58.8783 193.51 59.1774 67.24 94.2307 105.31 58.8866 197.03 55.7403 125.81 90.2095 106.12 53.8601 198.01 57.0051 67.75 103.5498 106.47 53.8868 201.83 45.0367 69.67 91. 5782 109.28 62.5090 203.43 71. 9225 70.83 90.7446 111. 00 74.7511 205.31 58.6143 72.81 87.9701 111.76 0.0000 210.85 54.0010 72.87 87.9799 114. 06 70.6504 215.65 50.5356 74.66 88.2645 116.30 0.0000 222 .11 54.5421 74.82 88.2898 116.74 66.4755 227.09 62.2467 74.97 88.3132 119.76 57.8438 227.38 62. 2620 77 .11 88.6485 121.12 47.9180 228.16 0.0000 78.74 88.9007 121. 22 47.9242 228.18 57.3203 79.69 89.0460 121. 78 59 .1127 116.74 57.3203 80.12 89.1121 122.06 58.0188 235.69 43.8905 80.19 0.0000 122.92 65.9024 235. 96 45.1544 80.57 89.1802 123.07 65.9154 238.63 61.1779 81. 00 89.2457 265.00 65. 9672 238.98 0.0000 81. 07 89.2561 125.81 55.3103 240.99 61.2967 81. 75 102.3251 127.23 70.3857 242.00 61. 3480 83.79 88.6104 127.91 58.4558 244.70 36.6372 84.00 88.6412 129.30 49.5490 252.40 0.0000 85.43 117.0573 131.20 36.1211 252.80 54.2546 86.55 128.5760 133.02 58.8293 254.15 0.0000 86.79 131.4529 133.52 57.7337 256.23 62.0527 86.94 131. 4851 136.00 65.8571 260.90 0.0000 Page 4681 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 52.1935 355.39 0.0000 584.27 17.4233 264.80 52.1985 356.01 20.5046 595.83 0.0000 265.00 51.3513 364.49 0.0000 427.87 29.9299 268.22 46.3304 366.42 0.0000 602.52 0.0000 269.46 42.9382 372.51 27.6172 604.72 18.6094 270.03 42.9576 375.05 24.8934 607.14 271.23 42. 9962 377.52 24.9302 609.32 21. 7537 273.65 0.0000 356.01 37.0728 610.33 21. 7622 276.40 44.8906 388.16 39.9538 614.28 23.3551 277.37 42.3307 388.63 0.0000 618.01 22.8719 277.60 44.9308 391.69 37.2428 620.36 15.6097 278.00 43.2149 264.66 30.8845 621. 93 16.6608 279.20 40.6584 401.81 29.9688 630.19 0.0000 279.54 43.2648 402.40 30.9153 631.29 17.7706 279.70 43.2699 404.85 21.1079 633.25 16.7383 280.46 45.0260 410.95 26.3582 634.78 0.0000 283.69 28.6420 413. 71 29.6992 635.95 13.6147 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 44.3210 423. 72 0.0000 645.85 15.7721 285.90 0.0000 427.09 34.1931 657.76 12.6777 287.50 26.9809 427.87 33.2575 657.90 0.0000 290.67 49.7242 433.94 25.7404 661. 66 14.8135 293.27 0.0000 439.40 26.7718 664.57 0.0000 '351. 93 32.8201 453.88 26.'0140 666.33 0.0000 295.96 32.8369 463.37 26.1420 666.50 0.0000 879.38 31. 5820 468.07 27.1757 667.71 0.0000 299.98 40.8341 473.00 0.0000 677.62 11. 7117 300.09 43.4716 475.06 26.2980 685 .. 70 0.0000 300.13 43.4726 476.78 24.8588 695.00 0.0000 301.36 30.3258 477.60 19.0176 696.49 19.3037 302.85 30.3574 482.18 19.5500 696. 51 19.3037 256.23 47.5708 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 19. 3096 306.78 45.8809 497.08 23.6328 697.49 23.6024 308.46 37.9846 505.52 17.7975 702.65 13.9738 311. 90 40.7301 507.63 0.0000 706.68 15.0715 316.51 39.9701 511. 00 26.7660 711.68 23. 7277 319.41 0.0000 514.00 26.8044 720.70 0.0000 320.08 0.0000 514.00 26.8044 721. 93 0.0000 321.04 40.9837 520.40 25.8900 722. 78 16.2451 323.87 34.8129 520.69 0.0000 722 .-91 16.2457 325.23 33.5045 522.65 0.0000 723. 31 11. 3737 328.76 0.0000 527.90 0.0000 724 .19 14.6277 333.37 30.5406 528.26 20.9889 727.33 19.5264 333.97 25.6101 529.59 25.0020 733.00 21.7407 334.37 36.4024 529.87 0.0000 735.93 11. 9704 338.28 36.0449 531.02 0.0000 333.97 19.5989 338.32 36.0457 537.26 0.0000 739.50 0.0000 311.90 50.0835 546.56 0.0000 747.24 15.2971 340.48 50.0835 552.55 15.1593 748.06 17.4876 340.55 0.0000 563.25 19.2946 752.31 18.6090 344.28 32.5657 569.33 19.3464 753.82 0.0000 345.93 42.5603 946.00 19.3479 756.73 12.0599 351.06 31. 7971 569.70 19.3494 756.80 12.0603 351. 93 31. 8142 583.19 17.4150 884.68 18.6857 Page 4682 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 29.6971 1274.44 10.6487 1620.50 5.1352 766.42 26.4023 1001.03 15.9950 1621. 92 6.1637 766.84 24.2057 1002.74 8. 0013 1678.03 0.0000 772.60 0.0000 1004.73 14.2329 1690.97 1.0409 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 .; 1764.49 4.2205 778.90 19.8889 1028.54 0.0000 1063.66 5.0698 783.70 0.0000 1037.84 10.7747 1771. 35 1.2074 785.37 27.6845 1038.76 0.0000 1791.20 0.0000 792.07 21. 0889 631.29 18. 7205 1808.65 4.2542 794.95 6.6663 1048.07 0.0000 1810.72 0.0000 795.86 13.3369 1049.04 11. 5281 1836.06 2.1373 810.06 10.0510 1050.41 13.5150 810.29 6.7012 1063.66 14.4678 344.28 7.8183 1077.00 0.0000 810.76 7.8192 1077.34 12.7072 815.77 0.0000 1085.87 9.0973 1048.07 0.0000 1093.63 10.9395 832.01 10.1246 1099.45 8.2172 834.85 13. 5122 1112. 07 12.8251 835.71 14.6425 1112.84 12.8276 836.80 0.0000 1115. 54 11. 7359 846.75 0.0000 1120.29 7.3442 846.77 19.2170 1120. 55 7.3447 856.80 0.0000 1221. 41 7.3462 860.56 15.8964 1129. 67 6.4420 871.09 15.3809 1131. 51 0.0000 873.19 11.9706 1147.95 0.0000 875.33 0.0000 1173.23 7.4448 879.38 10 .. 2806 1177.95 12 .1121 880.51 14.8551 1189.05 13.0797 883.24 10.2935 1204.77 16.8827 884.68 10.9844 1221.41 16.9519 889.28 9.1670 1231.02 21.1449 894.76 13.7739 1235.36 0.0000 898.04 14. 9371 1238.28 12.1039 900. 72 14.9498 1260.41 0.0000 903.28 12. 6597 1271.87 11. 4390 911. 20 12.6906 1274.44 16.2145 912.08 12.6941 1274.54 16.2156 923.98 0.0000 1291. 59 9.5764 926.50 9. 2728 1298.22 0.0000 929 .11 6. 9602 1312 .11 0.0000 937.49 23.2593 1332.49 4.8337 944.13 0.0000 1362.66 0.0000 946.00 6.9956 1365.19 3.8955 949.00 9.8024 1368. 63 0.0000 667. 71 0.0000 1384.29 1.9561 962.31 20.2099 1408.01 7.8652 964. 08 15.2386 1457.56 0.0000 966.17 26.7419 1460.82 5. 9659 911.20 18.4884 1489.16 2.0005 968.97 18.4884 1505.03 8.0283 983.53 0.0000 1584.12 9.1774 984.45 0.0000 1596. 21 0.0000 Page 4683 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:51:11.29 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235077.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM29.CNF;354 Background date : Z-OCT-2016 11:01:41. Sample date 17-DEC-2015 13:30:00 Acquisition date : 3-0CT-2016 06:47:53. Sample ID G405235077 Sample quantity : l.72799E+02 GRAM Detector name GAM29 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.46 0.0% Energy tolerance 1.50000 keV Analyst Initials : MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 3 3 0 2 2 8 8 5 5 0 0 0 1 1 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Energy 74.82* 77.21* 87.20 89. 96 92.75* 127.53 129.12 184.18 185.91* 209.03 218.67 223.06 238.66* 240.87 242 .13 251.09 277. 71 295.23* 338.31* 351. 92* 462.94 510.90* 583.19* 609.50* 727. 37 737.97 768.22 794.89 911.46* 925.26 935.94* 970.17* 1120.74* 1138. 49 Page 4684 of 5809 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 158 238 93 64 95 19 55 34 119 44 23 18 381 55 124 27 95 173 94 343 35 32 133 221 39 17 36 38 129 12 12 43 62 9 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 219 141 252 83 160 57 117 54 117' 99 84 70 91 78 49 81 127 78 54 66 27 84 18 43 39 15 14 13 10 12 21 63 25 10 1. 34 1. 00 1. 81 1. 05 1. 25 1. 34 1. 39 1. 04 1. 42 1. 55 0.79 0.50 1. 09 1. 29 1. 08 0.89 1. 77 1.14 1. 08 1. 48 1. 48 2.07 1. 59 1. 58 0.99 1. 87 2.12 3.39 1. 54 1. 42 3.37 1. 29 1. 43 1. 47 149.57 154.35 174.29 179.81 185.39 254.84 258.03 368.00 371.45 417.63 436.89 445.66 476.82 481.24 483.76 501. 65 554.83 589.83 675.90 703.08 924.93 1020.78 1165.26 1217.84 1453.48 1474.68 1535.16 1588.47 1821. 58 1849.18 1870.53 1939.00 2240.19 2275.71 144 144 169 178 178 253 253 366 366 415 433 443 471 471 471 499 546 585 672 697 920 1014 1161 1213 1448 1470 1531 1583 1816 1843 1861 1929 2233 2272 14 4.38E-02 14 6.61E-02 9 2.59E-02 14 1.77E-02 14 2.64E-02 9 5.34E-03 9 l.52E-02 12 9.48E-03 12 3.30E-02 8 l.22E-02 7 6.34E-03 6 4.93E-03 17 l.06E-01 1 7 1. 52E-02 17 3.45E-02 8 7.44E-03 19 2.64E-02 10 4.81E-02 8 2.62E-02 10 9.54E-02 10 9.64E-03 18 8.82E-03 9 3.70E-02 12 6.13E-02 12 l.09E-02 10 4. 72E-03 8 l.OOE-02 13 l.06E-02 15 3.59E-02 11 3.30E-03 14 3.47E-03 14 l.18E-02 14 l.73E-02 8 2.63E-03 18.4 10.8 32.7 24.1 25.6 62.4 37.8 36. 0 19.8 41. 7 70.2 78.9 6.7 47.4 14.4 61.1 30.4 12.3 17.2 7.1 33.0 76.5 10.7 9.4 35.5 49.0 24.4 25.4 10.7 66.2 85.4 43.6 21. 6 65.9 Fit 5.99E-01 l.37E+OO 2. 71E+OO l.23E+OO 1. 76E+00 Peak Search Report (continued) Page : 2 Sample ID : G405235077 Acquisition date 3-0CT-2016 06:47:53 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1172.64 20 14 3.84 2344.02 2338 11 5.69E-03 41. 4 36 0 1214.03 3 13 2.61 2426.84 2421 7 9.llE-04186.5 37 0 1238.08* 45 16 2.19 2474.96 2467 16 l.26E-02 25.3 38 0 1295.74 12 7 1. 68 2590.35 2585 9 3.42E-03 47.5 39 0 1343.16 11 4 1. 69 2685.25 2682 7 3.09E-03 41. 3 40 0 1352.13 15 0 1. 24 2703.20 2698 10 4.17E-03 25.8 41 0 1365.02 6 0 1. 44 2729.00 2725 7 1.67E-03 40.8 42 0 1377.56* 22 6 1. 28 2754.08 2747 12 6.08E-03 32.2 43 0 1460.95* 440 4 1. 83 2921. 00 2913 15 l.22E-01 4.9 44 0 1729.40 16 4 1. 77 3458.50 3453 9 4.51E-03 33.8 45 0 1764.87* 33 5 1. 29 3529.53 3524 10 9.17E-03 23.1 46 0 1846.08 11 0 3.50 3692.18 3687 10 3.06E-03 30.2 Flag: "*" = Peak area was modified by background subtraction Page 4685 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:51:13 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235077.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl' Sample title Sample date Sample ID 17-DEC-2015 13:30:00 G405235077 Acquisition date : Sample quantity Sample geometry : 06:47:53 172.80 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA29 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 87.09 PB-214 87.09 PB-214 87.09 TL-208 277.37 ps..:214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 4686of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line SN-126 86.94 SN-126 87.57 CD-109 88.03 HG-203 279.20 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:01.46 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235077 Acquisition date 3-0CT-2016 06:47:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* 1. 34 7E+OO 1.304E+Ol 1.304E+Ol

  • 9. 81 OK CD-109 88.03 3.70* 6.265E+OO 1.327E+OO 2.054E+OO 120.88 OK SN-126 64.28 9.60 3.737E+OO Line Not Found Absent 86.94 8.90 6.265E+OO 5.517E-01 5.517E-01 120.88 OK 87.57 37.00* 6.265E+OO 1.327E-01 l.327E-01 120.88 OK HG-203 70.83 3.69 4.623E+OO Line Not Found Absent 72.87 6.19 4.875E+OO Line Not Found Absent 279.20 81.56* 4.910E+OO 1.036E-01 7. 831E+OO 73.85 OK TL-208 277.37 6.60 4.914E+OO Line Not Found <<INT Reject 583.19 85.00* 2.773E+OO 2.734E-01 2.734E-01 21. 46 OK 860.56 12.50 2.069E+OO Line Not Found Absent BI-211 72.87 1.23 4.875E+OO Line Not Found Absent 351.06 12.92* 4.088E+OO 4.913E-02 4.913E-021607.86 OK PB-212 74.82 10.28 5.103E+OO 1.169E+OO 1.169E+OO 59.09 OK 77 .11 17.10 5.367E+OO 1.585E+OO 1.585E+OO 21. 55 OK 238.63 43.60* 5.496E+OO 8.586E-01 8.586E-01 13.34 OK 300.09 3.30 4,626E+OO Line Not Found Absent BI-214 609.32 45.49* 2.682E+OO 8.688E-01 8. 691E-01 18.75 OK 1120.29 14.92 1. 685E+OO. 1.092E+OO 1. 092E+OO 43.21 OK 1764.49 15.30 1.129E+OO 7.897E-01 7.900E-01 46.20 OK PB-214 74.82 5.80 5.103E+OO Line Not Found <<INT Reject 77 .11 9.70 5.367E+OO 2.795E+OO 2.796E+OO 21. 55 OK 87.09 3.41 6.257E+OO Line Not Found <<INT Reject 242.00 7.25 5.438E+OO 1.699E+OO 1. 700E+OO 28.71 OK 295.22 18.42 4.685E+OO 1.056E+OO 1.056E+OO 24.64 OK 351.93 35.60* 4.087E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.682E+OO 8.688E-01 8. 691E-01 18.75 OK 1120.29 14.92 l.685E+OO 1.092E+OO 1.092E+OO 43.21 OK 1764.49 15.30 1.129E+OO 7.897E-01 7.900E-01 46.20 OK RA-224 240.99 4.10* 5.459E+OO 1.320E+OO 1.320E+OO 94.74 OK RA-226 609.32 45.49* 2.682E+OO 8.688E-01 8.691E-01 18.75 OK 1120.29 14.92 1.685E+OO 1.092E+OO 1.092E+OO 43.21 OK 1764.49 15.30 1.129E+OO 7.897E-01 7.900E-01 46. 20 OK AC-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 1.026E+OO 1. 02 6E+OO 34.50 OK 794.95 4.25 2.197E+OO 1.886E+OO 1. 886E+OO 50.82 OK 835.71 1. 61 2 .116E+OO Line Not Found Absent 911.20 25.80* 1.981E+OO 1.151E+OO l .151E+OO 21. 32 OK 968. 97 15.80 1.888E+OO 6.445E-01 6.445E-01 87.30 OK RA-228 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11. 27 4.215E+OO 1.026E+OO 1. 026E+OO 34.50 OK 794.95 4.25 2.197E+OO 1.886E+OO 1.886E+OO 50.82 OK 835. 71 1. 61 2 .116E+OO Line Not Found Absent 911. 20 25.80* 1.981E+OO 1.151E+OO l.151E+OO 21. 32 OK 968.97 15.80 1.888E+OO 6.445E-01 6.445E-01 87.30 OK TH-228 74.82 10.28 5.103E+OO 1.169E+OO l.169E+OO 59.09 OK 77 .11 17.10 5.367E+OO 1.585E+OO 1.585E+OO 21. 55 OK 238.63 43.60* 5.496E+OO 8.586E-01 8.586E-01 13.34 OK 300.09 3.30 4.626E+OO Line Not Found Absent Page 4687 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235077 Acquisition date 3-0CT-2016 06:47:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Ef f pCi/GRAM pCi/GRAM %Error Status TH-230 609.32 2.682E+OO 8.688E-01 8.688E-01 18;. 7 5 OK 1120.29 14.92 1. 685E+OO 1. 092E+OO 1. 092E+OO 43.21 OK 1764.49 15.30 1.129E+OO 7.897E-01 7.897E-01 46.20 OK TH-232 105.21 1.10 7.155E+OO Line Not Found Absent 338.32 11.27 4.215E+OO 1. 026E+OO 1.026E+OO 34.50 OK 835. 71 1. 61 2 .116E+00 Line Not Found Absent 911.20 25.80* 1.981E+OO 1.151E+OO 1.151E+OO 21. 32 OK 968. 97 15.80 l.888E+OO 6.445E-01 6.445E-01 87.30 OK U-234 609.32 45.49* 2.682E+OO 8.688E-01 8.688E-01 18.75 OK 1120.29 14.92 l.685E+OO 1.092E+OO 1.092E+OO 43.21 OK 1764.49 15.30 1.129E+OO 7.897E-01 7.897E-01 46.20 OK U-235 89. 96 3.47 6.457E+OO 1. 710E+OO 1.710E+OO 48.23 OK 93.35 5.60 6.630E+OO 1.533E+OO l.533E+00 51.14 OK 143.76 10. 96* 7.247E+OO Line Not Found Absent 163.33 5.08 6.922E+OO Line Not Found Absent 185.72 57.20 6.477E+OO 1. 779E-01 1. 779E-01 39.57 OK 205.31 5.01 6.095E+OO Line Not Found Absent AM-243 43.53 5.90 7.707E-01 Line Not Found Absent 74.66 67.20* 5.103E+OO 1. 788E-01 1.788E-01 59.09 OK ANH-511 511. 00 100.00* 3.065E+OO 5.093E-02 5.093E-02 152.97 OK Flag: "*" = Keyline Page 4688 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:51:14.70 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* t * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235077.CNF;l *
  • Acquisition date 3-0CT-2016 06:47:53 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.46 Half life ratio : ***** *
  • Sample date 17-DEC-2015 13:30:00 Analyst initials: MXRl * *Sample ID G405235077 Sample Quantity 1.7280E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File ': DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 1.304E+Ol 1.253E+OO CD-109 2.054E+OO 2.433E+OO SN-126 l.327E-01 1.572E-01 HG-203 7.831E+OO 5.668E+OO TL-208 2.734E-01 5.749E-02 BI-211 4. 913E-02 7. 741E-01 PB-212 8. 58.6E-01 1.123E-01 BI-214 8.691E-01 1.597E-01 PB-214 1.216E+OO l.684E-01 RN-222 8.691E-01 1.597E-01 RA-224 1.320E+OO l.226E+OO RA-226 8.691E-01 1.597E-01 AC-228 1.151E+OO 2.404E-01 RA-228 1.151E+OO 2.404E-01 TH-228 8.586E-01 l.123E-01 TH-230 8.688E-01 l.596E-01 TH-232 1.151E+OO 2.404E-01 U-234 8.688E-01 1. 596E-01 U-235 -1.220E-02 l.552E-01 AM-243 1. 788E-01 1.035E-01 ANH-511 5.093E-02 7.635E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4689 of 5809 Key-Line Activity (pCi/GRAM -1. 707E+OO -2.923E-02 O.OOOE+OO -2.267E-03 9.933E-02 O.OOOE+OO O.OOOE+OO -1. 566E-02 1.349E-01 K.L. Cnt Uncert ( 1. 96-sigma) 7.783E+OO 3.572E-02 1.839E+41 2.294E-02 2.556E-01 7.409E+03 2.382E+02 5. 096E-02 3.133E-01 MDA (pCi/GRAM 4.405E-01 l.431E+OO l.189E-01 2.640E+OO 4.798E-02 2.636E-01 8.003E-02 1.012E-01 2. 960E-01 l.012E-01 8.576E-01 l.012E-01 1. 745E-01 1. 745E-01 8.003E-02 l.012E-01 1.745E-Ol l.012E-01 2.903E-01 7.546E-02 3.856E-02 MDA (pCi/GRAM l.532E+Ol 5.691E-02 O.OOOE+OO 4.869E-02 5.348E-01 O.OOOE+OO O.OOOE+OO 9.450E-02 6.576E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 2.531E-02 3.514E-02 7.185E-02 NOT IDENT. C0-58 -9.627E-02 3.990E-01 7.572E-01 NOT IDENT. FE-59 2.615E-01 3.991E+OO 7.935E+OO NOT IDENT. C0-60 -l.598E-02 3.102E-02 5.329E-02 FAIL ABUN ZN-65 -5.625E-02 1.581E-01 2.468E-01 NOT IDENT. GE-68 8.721E-02 l.630E+OO 3.219E+OO NOT IDENT. AS-73 2.482E+OO 6.275E+OO 1.306E+Ol NOT IDENT. AS-74 O.OOOE+OO 3.139E+03 0.000E+OO SHORT HLIF SE.-75 -6.033E-02 l.657E-01 2.953E-01 NOT IDENT. BR-77 0.000E+OO 1. 418E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 4.058E+02 O.OOOE+OO SHORT HLIF RB-83 9.791E-02 4.289E-01 8.892E-01 NOT IDENT. KR-85 2.271E+OO 4.990E+OO 1.045E+Ol NOT IDENT. SR-85 2.179E-01 4.791E-01 1.004E+OO NOT IDENT. RB-86 O.OOOE+OO 1.473E+04 O.OOOE+OO SHORT HLIF Y-88 2.658E-02 l.142E-01 2.861E-01 NOT IDENT. Y-91 -6. 611E+Ol 3.781E+02 6. 968E+02 NOT IDENT. NB-94 -1. 748E-02 2.433E-02 4.313E-02 NOT IDENT. NB-95 5.373E-01 6.213E-01 1.252E+OO NOT IDENT. NB-95M 7.756E-01 2.027E+OO 3.577E+00 NOT IDENT. ZR-95 -2. 724E-01 9.177E-01 1. 741E+OO NOT IDENT. NB-97 O.OOOE+OO 1. 769E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.423E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 2.621E-02 3.205E-02 5.231E-02 FAIL ABUN RH-102 -3. 24 7E-'02 3. 712E-02 6.464E-02 FAIL ABUN RU-103 5.318E-01 3.859E+00 7.816E+00 FAIL ABUN RH-106 l.270E-01 3.779E-01 7. 801E-01 NOT IDENT. RU-106 l.270E-01 3.779E-01 7.801E-01 NOT IDENT. AG-108M 1.316E-02 1.846E-02 4.061E-02 NOT IDENT. AG-llOM 4.264E-02 5.688E-02 1.316E-01 NOT IDENT. SN-113 -2.062E-02 1. 613E-01 3.224E-01 NOT IDENT. CD-115 0.000E+OO 1. 366E+38 O.OOOE+OO SHORT HLIF SN-117M O.OOOE+OO 4.918E+04 O.OOOE+OO SHORT HLIF TE-123M -3.585E-02 1.014E-01 l.872E-01 NOT IDENT. SB-124 -6. 113E-01 1. 362E+OO 2.616E+OO NOT IDENT. SB-125 6.864E-03 7.459E-02 1.523E-01 FAIL ABUN TE-125M -2.256E+02 1. 996E+02 3.547E+02 NOT IDENT. I-126 O.OOOE+OO 4.257E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 4.928E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.233E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO l.864E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 5.099E+25 O.OOOE+OO SHORT HLIF BA-133 -2.124E-02 2.828E-02 5.045E-02 FAIL ABUN I-133 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CS-134 O.OOOE+OO 6.lOOE-02 9.289E-02 FAIL ABUN CS-135 -1.156E-01 1.304E-01 2.192E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO l.625E+05 O.OOOE+OO SHORT HLIF BA-137M -8.577E-03 2.583E-02 4.879E-02 NOT IDENT. CS-137 -9.061E-03 2. 729E-02 5.154E-02 NOT IDENT. CE-139 4.906E-02 8.374E-02 1.664E-01 NOT IDENT. BA-140 O.OOOE+OO 5.600E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.002E+05 O.OOOE+OO SHORT HLIF CE-141 5.457E+OO 1.628E+Ol 3.178E+Ol NOT IDENT. CE-143 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF CE-144 -1.102E-01 2.798E-01 5.208E-01 NOT IDENT. PM-144 -4.159E-02 4.143E-02 7.0lOE-02 NOT IDENT. PR-144 -3.519E+OO 3.593E+OO 6.105E+00 NOT IDENT. PM-146 9.930E-03 3. lllE-02 6.506E-02 NOT IDENT. ND-147 O.OOOE+OO 1.294E+07 O.OOOE+OO SHORT HLIF PM-147 2. 496E+02 6.267E+02 1. 251E+03 NOT IDENT. PM-149 O.CiOOE+OO 2.086E+39 O.OOOE+OO SHORT HLIF EU-150 -1.079E-02 2.302E-02 3.971E-02 FAIL ABUN EU-152 l.903E-02 6.495E-02 1.362E-01 NOT IDENT. GD-153 -7.336E-04 1.490E-01 2.688E-01 NOT IDENT. EU-154 -7. 372E-02 8.764E-02 1.387E-01 NOT IDENT. EU-155 -2.474E-02 8.269E-02 1. 57 6E-01 FAIL ABUN TB-160 1.150E+OO 1.127E+OO 2. 621E+OO FAIL ABUN H0-166M 5.292E-03 3.908E-02 7.930E-02 FAIL ABUN TM-171 5.679E+OO 1.584E+Ol 3.295E+Ol NOT IDENT. HF-172 8.430E-02 1. 759E-01 3.302E-01 FAIL ABUN LU-172 -4.549E-04 5.334E-02 l.042E-01 FAIL ABUN LU-176 5.432E-03 2.082E-02 3.929E-02 FAIL ABUN HF-181 -7.485E-01 2.559E+OO 5.007E+OO NOT IDENT. Page 4690 of 5809 TA-182 3.799E-01 7.649E-01 1. 534E+OO FAIL ABUN RE-183 l.109E-02 2.056E+00 4 .151E+OO NOT IDENT. RE-184 -1. 471E+Ol 1.760E+Ol 2.939E+Ol NOT IDENT. W-188 -2.102E+OO 9.121E+Ol 1.541E+02 NOT IDENT. IR-192 -2.234E-01 3.605E-01 6.143E-01 FAIL ABUN BI-207 -2.686E-02 4.313E-02 7.398E-02 FAIL ABUN PB-210 -9.434E-01 2.514E+OO 5.033E+OO NOT IDENT. PB-211 2.608E-01 5.103E-01 1.075E+OO NOT IDENT. BI-212 O.OOOE+OO 8.197E-01 1. 026E+OO FAIL ABUN RN-219 -1.996E-01 2.800E-01 5.250E-01 NOT IDENT. RA-223 -2.056E-01 3.819E-01 7.443E-01 FAIL ABUN AC-227 5.558E-02 1. 903E.-01 3.629E-01 NOT IDENT. TH-227 5.558E-02 1.903E-01 3.629E-01 NOT IDENT. TH-229 -6.302E-02 3.898E-Ol 7.212E-01 FAIL ABUN PA-231 -4.858E-03 3.891E-01 7.105E-01 NOT IDENT. TH-231 -2.056E-01 3.819E-01 7.443E-01 FAIL ABUN PA-233 -5.542E-02 4.916E-02 7. 751E-02 NOT IDENT. PA-234 -5.341E-02 2.094E-01 3.915E-01 FAIL ABUN PA-234M 1.000E+OO 3.804E+OO 7.350E+OO NOT IDENT. TH-234 -1.972E-01 9.622E-01 1. 960E+OO FAIL ABUN NP-237 -5.542E-02 4.916E-02 7.751E-02 NOT IDENT. NP-238 O.OOOE+OO 1.936E+40 O.OOOE+OO SHORT HLIF U-238 -1.972E-01 9.622E-01 1. 960E+OO FAIL ABUN NP-239 1. 546E-02 1. 791E-01 3.506E-01 FAIL ABUN PU-239 O.OOOE+OO 5.036E+02 5.483E+02 FAIL ABUN AM-241 6.447E-03 l.066E-01 2 .151E-01 NOT IDENT. CM-243 -l.466E-02 7.442E-02 l.433E-01 FAIL ABUN BK...:.247 1. 704E-02 5.566E-02 1. 072E-01 NOT IDENT. CM-247 -8.548E-03 2. 591E-02 5.062E-02 FAIL ABUN CF-249 1.509E-02 2.653E-02 5.683E-02 NOT IDENT. CF-251 -4.428E-02 9.765E-02 1. 772E-01 NOT IDENT. Page 4691of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:51:12.37 Nuclide Line Activity Report Nuclide Type:
  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 431 10.66* 1.347E+OO 1.304E+Ol 1.304E+Ol 9.81 CD-109 88.03 130 3.70* 6.265E+OO 2.431E+OO 3.763E+OO 65.41 SN-126 64.28 ------9.60 3.737E+OO ------Line Not Found ------86.94 130 8.90 6.265E+OO 1. OllE+OO 1.0llE+OO 65.41 87.57 130 37.00* 6.265E+OO 2.431E-01 2.431E-01 65.41 HG-203 70.83 ------3.69 4.623E+OO ------Line Not Found ------72.87 ------6.19 4.875E+OO ------Line Not Found ------279.20 116 81.56* 4.910E+OO 1.257E-01 9.504E+OO 60.73 TL-208 277.37 116 6.60 4.910E+00 1.553E+OO 1.553E+OO 60.73 583.19 148 85.00* 2.773E+OO 2.734E-01 2.734E-01 21. 46 860.56 ------12.50 2.069E+OO ------Line Not Found ------BI-211 72.87 ------1. 23 4.875E+OO ------Line Not Found ------351.06 407 12.92* 4.088E+OO 3.350E+00 3.350E+OO 14 .13 PB-212 74.82 223 10.28 5.103E+OO 1.845E+OO 1.845E+OO 36. 77 77 .11 335 17.10 5.367E+OO 1.585E+00 1.585E+OO 21. 55 238.63 474 43.60* 5.496E+OO 8.586E-01 8.586E-01 13.34 300.09 ------3.30 4.626E+OO ------Line Not Found ------BI-214 609.32 244 45.49* 2.682E+OO 8.688E-01 8. 691E-01 18.75 1120.29 63 14.92 1.685E+OO 1. 092E+OO 1.092E+00 43.21 1764.49 31 15.30 1.129E+OO 7.897E-01 7.900E-01 46.20 PB-214 74.82 223 5.80 5.103E+OO 3.269E+OO 3.270E+00 36.77 77 .11 335 9.70 5.367E+OO 2.795E+OO 2.796E+OO 21. 55 87.09 130 3.41 6.265E+OO 2.638E+OO 2.639E+OO 65.41 242.00 154 7.25 5.438E+OO 1.699E+OO 1.700E+OO 28.71 295.22 210 18.42 4.685E+OO 1.056E+OO l.056E+OO 24.64 351.93 407 35.60* 4.088E+00 1.216E+OO 1.216E+OO 14.13 RN-222 609.32 244 45.49* 2.682E+OO 8.688E-01 8. 691E-01 18.75 1120.29 63 14.92 1.685E+OO 1.092E+OO 1.092E+OO 43.21 1764.49 31 15.30 1.129E+OO 7.897E-01 7.900E-01 46.20 RA-224 240.99 68 4.10* 5.459E+OO 1.320E+OO 1.320E+OO 94.74 RA-226 609.32 244 45.49* 2.682E+00 8.688E-01 8. 691E-01 18.75 1120.29 63 14.92 1.685E+00 1.092E+OO 1.092E+OO 43.21 1764.49 31 15.30 1.129E+OO 7.897E-01 7.900E-01 46.20 AC-228 105.21 ------1.10 7.155E+00 ------Line Not Found ------338.32 112 11.27 4.215E+00 1.026E+OO 1.026E+OO 34.50 794.95 41 4.25 2.197E+OO 1.886E+00 1.886E+OO 50.82 835.71 ------1. 61 2 .116E+OO ------Line Not Found ------911. 20 135 25.80* 1. 981E+OO 1.151E+OO 1.151E+OO 21. 32 968. 97 44 15.80 1.888E+OO 6.445E-01 6.445E-01 87.30 RA-228 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 112 11. 27 4.215E+OO 1.026E+OO 1. 026E+OO 34.50 794.95 41 4.25 2.197E+00 1.886E+OO 1. 886E+OO 50.82 835.71 ------1. 61 2 .116E+OO ------Line Not Found ------911.20 135 25.80* 1.981E+00 1.151E+OO 1.151E+OO 21. 32 968. 97 44 15.80 1. 888E+OO 6.445E-01 6.445E-01 87.30 TH-228 74.82 223 10.28 5.103E+OO 1.845E+OO 1.845E+OO 36.77 77 .11 335 17.10 5.367E+OO 1.585E+OO 1.585E+OO 21. 55 Page 4692 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235077 Acquisition date 3-0CT-2016 06:47:53 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 474 43.60* 5. 496E+OO 8.586E-.Ol 8.586E-01 13.34 300.09 ------3.30 4.626E+OO ------Line Not Found ------TH-230 609.32 244 45.49* 2.682E+OO 8.688E-01 8.688E-01 18.75 1120.29 63 14.92 1.685E+OO 1.092E+OO 1.092E+OO 43.21 1764.49 31 15.30 1.129E+OO 7.897E-01 7.897E-01 46.20 TH-232 105.21 ------1.10 7.155E+OO ------Line Not Found ------338.32 112 11. 27 4.215E+OO 1. 026E+OO 1.026E+OO 34.50 835.71 ------1. 61 2 .116E+OO ------Line Not Found ------911.20 135 25.80* 1. 981E+OO 1.151E+OO 1.151E+OO 21. 32 968. 97 44 15.80 l.888E+OO 6.445E-01 6.445E-01 87.30 U-234 609.32 244 45.49* 2.682E+OO 8.688E-01 8.688E-01 18.75 1120.29 63 14.92 1.685E+OO 1. 092E+OO 1.092E+OO 43.21 1764.49 31 15.30 1.129E+OO 7.897E-01 7.897E-01 46.20 U-235 89. 96 88 3.47 6.457E+OO 1. 710E+OO 1. 710E+OO 48.23 93.35 131 5.60 6.630E+OO 1.533E+OO 1.533E+OO 51.14 143.76 ------10.96* 7.247E+OO ------Line Not Found ------163.33 ------5.08 6.922E+OO ------Line Not Found ------185. 72 152 57.20 6.477E+OO l.779E-01 1.779E-01 39.57 205.31 ------5.01 6.095E+OO ------Line Not Found ------AM-243 43.53 ------5.90 7.707E-01 ------Line Not Found ------74.66 223 67.20* 5.103E+OO 2.822E-01 2.822E-01 36. 77 ANH-511 511. 00 36 100.00* 3.065E+OO 5.093E-02 5.093E-02 152.97 Flag: "*" Key line Page 4693 of 5809 Summary of Nuclide Activity Sample ID : G405235077 Acquisition date Page : 3 3-0CT-2016 06:47:53 Total number of lines in spectrum 46 Number of unidentified lines 11 Number of lines tentatively identified by NID 35 Nuclide Type : Nuclide K-40 CD-109 SN-126 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Hlife l.25E+09Y 461.40D 2.30E+05Y 46.59D 1.41E+10Y 7.04E+08Y 1.41E+10Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+10Y 1600.00Y 1. 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7.54E+04Y l.41E+l0Y 2.45E+05Y 7.04E+08Y 7370.00Y l.OOE+09Y Decay 1. 00 1. 55 1. 00 75.6 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 1.304E+Ol 2.431E+OO 2.431E-01 1.257E-01 2.734E-01 3.350E+OO 8.586E-01 8.688E-01 l.216E+00 8.688E-01 1.320E+OO 8.688E-01 l.151E+00 1.151E+OO 8.586E-01 8.688E-01 l.151E+00 8.688E-01 1.779E-01 2.822E-01 5.093E-02 3.202E+Ol 3.202E+Ol Decay Corr pCi7GRAM 1.304E+Ol 3.763E+OO 2. 431E-01 9.504E+OO 2.734E-01 3.350E+OO 8.586E-01 8.691E-01 1.216E+OO 8.691E-01 1.320E+OO 8.691E-01 1.151E+OO 1.15.lE+OO 8.586E-01 8.688E-01 1.151E+OO 8.688E-01 1.779E-01 2.822E-01 5.093E-02 4.273E+Ol 4.273E+Ol 76.09%
  • Decay Corr 2-Sigma Error 0.128E+Ol 2.461E+OO 1.590E-01 5.772E+OO 0.587E-01 0.473E+OO 1.145E-01 1. 629E-01 0.172E+OO 1.629E-01 1. 251E+OO l.629E-01 0.245E+OO 0.245E+OO 1.145E-01 1. 629E-01 0.245E+OO 1.629E-01 0.704E-01 l.038E-01 7. 791E-02 "M" Manually accepted 2-Sigma %Error 9.81 65.41 65.41 60.73 21. 46 14.13 13.34 18.75 14.13 18.75 94.74 18.75 21. 32 21. 32 13.34 18.75 21. 32 18.75 39.57 36.77 152.97 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4694 of 5809 Flags K Unidentified Energy Lines Page : 4 Sample ID : G405235077 Acquisition date : 3-0CT-2016 06:47:53 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 8 127.53 26 76 1. 34 254.84 253 9 5.34E-03 **** 7.39E+OO T 8 129.12 73 156 1. 39 258.03 253 9 l.52E-02 75.6 7.39E+OO T 5 184.18 44 69 1. 04 368.00 366 12 9.48E-03 72.0 6.51E+OO T 0 209.03 55 125 1. 55 41:;7. 63 415 8 l.22E-02 83.4 6.02E+OO 0 218.67 29 106 0.79 436.89 433 7 6.34E-03 **** 5.84E+OO 0 223.06 22 88 0.50 445.66 443 6 4.93E-03 **** 5.76E+OO T 0 251.09 33 100 0.89 501. 65 499 8 7.44E-03 **** 5.30E+OO T 0 462.94 40 31 1. 48 924.93 920 10 9.64E-03 65.9 3.30E+OO T 0 727.37 43 42 0.99 1453.48 1448 12 1.09E-02 71.0 2.35E+OO T 0 737.97 18 16 1. 87 1474.68 1470 10 4.72E-03 98.l 2.32E+OO T 0 768.22 39 15 2.12 1535.16 1531 8 l.OOE-02 48.9 2.25E+OO T 0 925.26 12 13 1. 42 1849.18 1843 11 3.30E-03 **** 1. 96E+OO T 0 935.94 13 22 3.37 1870.53 1861 14 3.47E-03 **** 1.94E+OO 0 1138.49 10 10 1. 47 2275.71 2272 8 2.63E-03 **** 1.66E+OO 0 1172.64 21 14 3.84 2344.02 2338 11 5.69E-03 82.8 1.62E+OO T 0 1214.03 3 13 2.61 2426.84 2421 7 9.llE-04 **** 1.58E+OO 0 1238.08 45 16 2.19 2474.96 2467 16 1.26E-02 50.5 1.55E+OO T 0 1295.74 12 7 1. 68 2590.35 2585 9 3.42E-03 95.0 1. 50E+OO 0 1343;16 11 4 1. 69 2685.25 2682 7 3.09E-03 82.6 1. 45E+OO 0 1352.13 15 0 1. 24 2703.20 2698 10 4.17E-03 51.6 1. 44E+OO 0 1365. 02 6 0 1. 44 2729.00 2725 7 l.67E-03 81.6 1. 43E+OO T 0 1377.56 22 6 1. 28 2754.08 2747 12 64.3 1.42E+OO 0 1729.40 15 4 1. 77 3458.50 3453 9 4.51E-03 67.6 1.15E+OO 0 1846.08 10 0 3.50 3692.18 3687 10 3.06E-03 60.3 1. 08E+OO Flags: "T" = Tentatively associated Page 4695 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:51:30.65 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * * *Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235077.CNF;l *
  • Acquisition date 3-0CT-2016 06:47:53 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.46 Half life ratio : ***** *
  • Sample date 17-DEC-2015 13:30:00 Nuclide Library : SOLID *
  • Sample ID G405235077 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity : 1.7280E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 25-JUN-2016 09:55:57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.'CNF;lO * ******************************************************************************* Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 CD-109 SN-126 HG-203 TL-208 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 U-234 U-235 AM-243 ANH-511 Le (pCi/GRAM 1. 788E-01 6.727E-01 5.668E-02 l.201E+00 2 .139E-02 1.200E-01 3.739E-02 4.558E-02 1.438E-01 4.558E-02 4.007E-01 4.558E-02 7.544E-02 7.544E-02 3.739E-02 4.557E-02 7.544E-02 4.557E-02 1. 371E-01 3.583E-02 1.727E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 Page 4696 of 5809 Le (pCi/GRAM 6.854E+OO 2.358E-02 O.OOOE+OO l.897E-02 2.342E-01 O.OOOE+OO O.OOOE+OO 4.179E-02 2.895E-01 0.000E+OO NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4697 of 5809 3.379E-02 3.302E-01 3.392E+OO 2.210E-02 1. 074E-01 1.384E+OO 6.157E+OO O.OOOE+OO 1.364E-01 O.OOOE+.00 O.OOOE+OO 3.977E-01 4.738E+OO 4.549E-01 O.OOOE+OO 1.067E-01 3.030E+02 1.903E-02 5.632E-01 1.682E+OO 7.563E-01 O.OOOE+OO O.OOOE+OO 0.000E+OO 0.000E+OO 2.465E-02 2.746E-02 3.541E+OO 3.500E-01 3.500E-01 l.834E-02 5.660E-02 l.466E-01 O.OOOE+OO 0.000E+OO 8.773E-02 1.007E+OO 6.894E-02 1.663E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.261E-02 O.OOOE+OO 4.223E-02 1.018E-01 O.OOOE+OO O.OOOE+OO 2.165E-02 2.287E-02 7.820E-02 O.OOOE+OO O.OOOE+OO 1.499E+Ol O.OOOE+OO 2.445E-01 3.065E-02 2. 672E+OO 2.940E-02 O.OOOE+OO 5.881E+02 O.OOOE+OO 1. 831E-02 6.222E-02 1. 269E-01 5.732E-02 7.402E-02 1.150E+OO 3.493E-02 l.552E+Ol 1.548E-01 4.463E-02 l.818E-02 2.226E+OO 6. 851E-01 NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT.IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN . NOT IDENT. NOT IDENT. NOT IDENT.' FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 BI-207 PB-210 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M TH-234 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4698 of 5809 1.954E+OO 1.233E+Ol 7 .115E+Ol 2.811E-01 3.233E-02 2.376E+OO 4.929E-01 4.741E-01 2.370E-01 3.362E-01 1. 688E-01 l.688E-01 3.379E-01 3.299E-01 3.362E-01 3.514E-02 1. 696E-01 3.286E+OO 9.309E-01 3.514E-02 O.OOOE+OO 9.309E-01 1.643E-01 2.604E+02 1.015E-01 6. 723E-02 4.946E-02 2.297E-02 2.593E-02 8.305E-02 NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:51:36.79 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • 1
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235077.CNF;l *
  • Acquisition date 3-0CT-2016 06:47:53 Sensitivity : 3.000 *
  • Detector ID GAM29 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.46 Half life ratio : ***** *
  • Sample date 17-DEC-2015 13:30:00 Nuclide Library : SOLID *
  • Sample ID G405235077 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity l.7280E+02 GRAM *
  • Quantity Err(%) 1.1574E-03 % * *Wet wt corr 1.00000 wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 25'-JUN-2016 09: 55: 57 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM29 CAN.CNF;lO
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 1.304E+Ol 1.426E+OO 1.426E+00 CD-109 2.053E+OO 2.448E+OO 2.448E+00 SN-126 1. 326E-01 1.580E-01 1.580E-01 HG-203 7. 831E+OO 5.682E+OO 5.682E+OO TL-208 2.734E-01 5.866E-02 5.866E-02 BI-211 4.757E-02 7.943E-01 7.943E-01 PB-212 8.586E-01 1.211E-01 1.211E-01 BI-214 8.691E-01 1.640E-01 1.640E-01 PB-214 1.216E+OO 1.759E-01 1.759E-01 RN-222 8.691E-01 1.640E-01 1.640E-01 RA-224 1.320E+OO 1.228E+OO 1.228E+00 RA-226 8. 691E-01 1.640E-01 1.640E-01 AC-228 1.151E+OO 2.476E-01 2.476E-01 RA-228 1.151E+OO 2.476E-01 2.476E-01 TH-228 8.586E-01 1. 211E-01 1.211E-01 TH-230 8.688E-01 1.639E-01 1.639E-01 TH-232 1.151E+OO 2.476E-01 2.476E-01 U-234 8.688E-01 1.639E-01 1.639E-01 U-235 -1.220E-02 1.552E-01 1.552E-01 AM-243 1.787E-01 l.049E-01 1.049E-01 ANH-511 5.093E-02 7.638E-02 7.638E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.707E+OO 7.783E+OO 7.821E+OO NOT IDENT. NA-22 -2.923E-02 3.574E-02 3.809E-02 NOT IDENT. NA-24 1.000E+41 l.888E+41 O.OOOE+OO SHORT HLIF AL-26 -2.267E-03 2.294E-02 2. 296E-02 NOT IDENT. SC-46 9.933E-02 2.556E-01 2.595E-01 FAIL ABUN V-48 -5.002E+Ol 7.409E+03 7.409E+03 SHORT HLIF CR-51 1.677E+02 2.383E+02 2.500E+02 SHORT HLIF MN-54 -l.566E-02 5. 096E-02 5.145E-02 NOT IDENT. C0-56 1.349E-01 3.133E-01 3.192E-01 FAIL ABUN Page 4699 of 5809 MN-56 1.000E+41 2.342E+41 O.OOOE+OO SHORT HLIF C0-57 2.531E-02 3.516E-02 3. 696E-02 NOT IDENT. C0-58 -9.627E-02 3.990E-01 4.014E-01 NOT IDENT. FE-59 2.615E-01 3.992E+OO 3.993E+OO NOT IDENT. C0-60 -1.598E-02 3.103E-02 3.185E-02 FAIL ABUN ZN-65 -5.625E-02 1. 581E-01 1.602E-01 NOT IDENT. GE-68 8.721E-02 1.630E+00 l.630E+OO NOT IDENT. AS-73 2.482E+OO 6. 296E+OO 6.394E+OO NOT IDENT. AS-74 -1.353E+03 3.141E+03 3.199E+03 SHORT HLIF SE-75 -6.033E-02 1.657E-01 1. 6:79E-01 NOT IDENT. BR-77 1. 084E+37 9.100E+37 O.OOOE+OO SHORT HLIF SR-82 -1. 647E+02 4.059E+02 4. 12 6E+02 SHORT HLIF RB-83 9.791E-02 4.291E-01 4.314E-01 NOT IDENT. KR-85 2.271E+OO 4.991E+OO 5.095E+OO NOT IDENT. SR-85 2.179E-01 4.792E-01 4.891E-01 NOT IDENT. RB-86 -3.269E+02 1.473E+04 l.473E+04 SHORT HLIF Y-88 2.658E-02 l.142E-01 l.148E-01 NOT IDENT. Y-91 -6. 611E+Ol 3.781E+02 3.792E+02 NOT IDENT. NB-94 -l.748E-02 2.434E-02 2.559E-02 NOT IDENT. NB-95 5.373E-01 6.218E-01 6.673E-01 NOT IDENT. NB-95M 7.756E-01 2.028E+OO 2.058E+OO NOT IDENT. ZR-95 -2. 724E-01 9.178E-01 9.260E-01 NOT IDENT. NB-97 l.000E+41 1. 770E+41 O.OOOE+OO SHORT HLIF ZR-97 l.OOOE+41 5.541E+41 O.OOOE+OO SHORT HLIF M0-99 -2 .117E+30 1.423E+31 0.000E+OO SHORT HLIF TC-99M -l.000E+41 4.981E+41 O.OOOE+OO SHORT HLIF RH-101 2.621E-02 3.240E-02 3.449E-02 FAIL ABUN RH-102 -3.247E-02 3.722E-02 3.999E-02 FAIL ABUN RU-103 5.318E-01 3.859E+OO 3.866E+OO FAIL ABUN RH-106 1. 27 OE-01 3.780E-01 3.823E-01 NOT IDENT. RU-106 1.270E-01 3.780E-01 3.823E-01 NOT IDENT. AG-108M 1.316E-02 1. 847E-02 1.940E-02 NOT IDENT. AG-llOM 4.264E-02 5.692E-02 6.008E-02 NOT IDENT. SN-113 -2.062E-02 1.613E-01 1.616E-01 NOT IDENT. CD-115 4.634E+37 1.369E+38 O.OOOE+OO SHORT HLIF SN-117M -l.691E+04 4.922E+04 4.981E+04 SHORT HLIF TE-123M -3.585E-02 l.014E-01 l.027E-01 NOT IDENT. SB-124 -6.113E-01 1. 362E+OO 1.390E+OO NOT IDENT. SB-125 6.864E-03 7.459E-02 7.466E-02 FAIL ABUN TE-125M -2.256E+02 2.000E+02 2.244E+02 NOT IDENT. I-126 3.623E+04 4.257E+05 4.261E+05 SHORT HLIF SB-126 -1.364E+05 4.934E+05 4. 972E+05 SHORT HLIF SB-127 8.457E+20 3.424E+21 O.OOOE+OO SHORT HLIF I-131 5.685E+08 1.864E+09 1.881E+09 SHORT HLIF I-132 -1.000E+41 l.853E+42 O.OOOE+OO SHORT HLIF TE-132 -3.936E+25 5.330E+25 O.OOOE+OO SHORT HLIF BA-133 -2.124E-02 2.830E-02 2.987E-02 FAIL ABUN I-133 l.OOOE+41 3.583E+41 O.OOOE+OO SHORT HLIF CS-134 1.225E-01 6.122E-02 8.244E-02 FAIL ABUN CS-135 -1.156E-01 1.307E-01 1.407E-01 NOT IDENT. I-135 l.OOOE+41 3.375E+42 O.OOOE+OO SHORT HLIF CS-136 -9.083E+04 l.627E+05 1.678E+05 SHORT HLIF BA-137M -8.577E-03 2.583E-02 2.612E-02 NOT IDENT. CS-137 -9.061E-03 2.729E-02 2.759E-02 NOT IDENT. CE-139 4.906E-02 8.432E-02 8. 717E-02 NOT IDENT. BA-140 -2.107E+05 5. 601E+05 5.681E+05 SHORT HLIF LA-140 -2.276E+05 2.005E+05 2.252E+05 SHORT HLIF CE-141 5.457E+OO 1.628E+Ol l.646E+Ol NOT IDENT. CE-143 l.000E+41 1.947E+44 O.OOOE+OO SHORT HLIF CE-144 -l.102E-01 2.798E-01 2.842E-01 NOT IDENT. PM-144 -4.159E-02 4 .151E-02 4.554E-02 NOT IDENT. PR-144 -3.519E+OO 3.596E+OO 3.930E+OO NOT IDENT. PM-146 9.930E-03 3 .112E-02 3.144E-02 NOT IDENT. ND-147 -6.509E+06 1.295E+07 1.328E+07 SHORT HLIF PM-147 2. 496E+02 6.268E+02 6.369E+02 NOT IDENT. PM-149 -4.423E+37 2.086E+39 O.OOOE+OO SHORT HLIF EU-150 -1.079E-02 2.302E-02 2.353E-02 FAIL ABUN EU-152 1.903E-02 6. 496E-02 6.552E-02 NOT IDENT. GD-153 -7. 336E:.._04 1.490E-01 1.490E-01 NOT IDENT. EU-154 -7.372E-02 8.769E-02 9.377E-02 NOT IDENT. EU-155 -2.474E-02 8.271E-02 8.346E-02 FAIL ABUN TB-160 1.150E+OO 1.129E+OO l.242E+OO FAIL ABUN H0-166M 5.292E-03 3.908E-02 3.915E-02 FAIL ABUN TM-171 5.679E+OO 1.584E+Ol l.605E+Ol NOT IDENT. HF-172 8.430E-02 1. 7 65E-01 1.805E-01 FAIL ABUN LU-172 -4.549E-04 5.334E-02 5.334E-02 FAIL ABUN LU-176 5.432E-03 2.082E-02 2. 096E-02 FAIL ABUN HF-181 -7.485E-01 2.560E+OO 2.582E+OO NOT IDENT. Page 4700of5809 TA-182 3.799E-01 7.651E-01 7.840E-01 FAIL ABUN RE-183 l.109E-02 2.056E+OO 2.056E+OO NOT IDENT. RE-184 -1.471E+Ol 1. 793E+Ol 1. 912E+Ol NOT IDENT. W-188 -2.102E+OO 9.121E+Ol 9.121E+Ol NOT IDENT. IR-192 -2.234E-01 3.606E-01 3.744E-01 FAIL ABUN BI-207 -2.686E-02 4.315E-02 4.481E-02 FAIL ABUN PB-210 -9.434E-01 2.515E+OO 2.551E+OO NOT IDENT. PB-211 2.608E-01 5.105E-01 5.239E-Ol NOT IDENT. BI-212 1.179E+OO 8.218E-01 9.787E-01 FAIL ABUN RN-219 -1.996E-01 21* 811E-01 2.952E-Ol NOT IDENT. RA-223 -2.056E-01 3. 821E-01 3.932E-01 FAIL ABUN AC-227 5.558E-02 l.905E-01 l.921E-01 NOT IDENT. TH-227 5.558E-02 l.905E-01 1.921E-01 NOT IDENT. TH-229 -6.302E-02 3.899E-01 3.909E-01 FAIL ABUN PA-231 -4.858E-03 3.891E-01 3.892E-01 NOT IDENT. TH-231 -2.056E-01 3.821E-01 3.932E-01 FAIL ABUN PA-233 -5.542E-02 4.923E-02 5.520E-02 NOT IDENT. PA-234 -5.341E-02 2.182E-01 2.195E-01 FAIL ABUN PA-234M 1.000E+OO 3.804E+OO 3.831E+OO NOT IDENT. TH-234 -1.972E-01 9.632E-01 9.673E-01 FAIL ABUN NP-237 -5.542E-02 4.923E-02 5.520E-02 NOT IDENT. NP-238 3.421E+39 1.936E+40 O.OOOE+OO SHORT HLIF U-238 -1. 972E-01 9.632E-01 9.673E-01 FAIL ABUN NP-239 l.546E-02 1. 791E-01 1. 792E-01 FAIL ABUN PU-239 6.795E+02 5.045E+02 5.902E+02 FAIL ABUN AM-241 6.447E-03 1.066E-01 1.066E-01 NOT IDENT. CM-243 -1.466E-02 7.443E-02 7. 472E-02 FAIL ABUN BK-247' 1. 704E-02 5.576E-02 5.629E-02 NOT IDENT. CM-247 -8.548E-03 2.595E-02 2.624E-02 FAIL ABUN CF-249 1.509E-02 2.656E-02 2.741E-02 NOT IDENT. CF-251 -4.428E-02 9.778E-02 9.979E-02 NOT IDENT. Page 4701 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 85.5244 87.09 137.7993 136.47 91.2226 45.60 101.1675 87.57 137.8918 140.51 0.0000 46.54 88.9319 88.03 81. 9684 143.76 90.8192 49.72 0.0000 88.34 82.0038 144.24 87.5793 51. 35 96.5439 88.47 82.0184 145.44 83.3013 51. 87 101. 4724 89. 96 86. 2962 152.43 107.0603 52.39 79.3240 1093.63 86.3763 153.25 0.0000 52. 97 67.7903 91.11 0.0000 323.87 80.7115 53.44 81. 4205 92.59 86.6048 156.02 0.0000 54.07 83.4578 93.35 86.6929 158.56 0.0000 57.36 0.0000 94.56 86.8333 159.00 83.3061 57.53 92.7792 94.65 86.8435 162.33 71.3125 57.98 86.0124 94.67 86.8461 162.66 0.0000 59.27 92.0880 94.87 103.4149 163.33 89.2236 59.32 93.0760 97.43 95.4625 165.86 67.0761 59.54 93 .1123 98.43 102. 8596 176.31 69.9733 60.96 101.2048 98.44 102.8611 176.60 o. *oooo 61.17 101.2417 99.53 78.0344 177.52 86.9951 62.93 96. 6190 100 .11 88.5051 181.07 0.0000 63.29 98.6517 102.03 91.8531 181.52 86.1680 63.58 98.7001 103.18 76.3071 184.41 79.5650 64.28 93.8760 103.37 81.5527 143.76 79.6547 66.73 119. 0652 105.21 77.5489 193.51 77.8925 67.24 118.1720 105.31 86.9913 197.03 94.2057 125.81 114.2823 106.12 80.7833 198.01 66.6873 67.75 114.2946 106.47 80.8185 201.83 56.5157 69.67 119.6356 109.28 106.3732 203.43 65.8280 70.83 134.5064 111. 00 93.9297 205.31 57.0605 72. 81 117.2258 111.76 0.0000 210.85 71.2545 72. 87 117.2365 114.06 87.9168 215.65 74.6338 74.66 117.5624 116. 30 0.0000 222 .11 56.2551 74.82 117.5909 116.74 72.2547 227.09 68.2316 74.97 117.6177 119. 76 78.9045 227.38 74.1300 77 .11 118.0015 121.12 71.5515 228.16 0.0000 78.74 102.4505 121. 22 71.5591 228.18 72.9978 79.69 95.8447 121.78 70.5359 116.74 72.9978 80.12 89.1514 122.06 66.2823 235.69 72.6162 80.19 0.0000 122.92 73.8373 235.96 72. 6302 80.57 102.7273 123.07 77.0603 238.63 67.6310 81. 00 116.6556 265.00 88.8942 238.98 0.0000 81. 07 116.6679 125.81 62.9823 240.99 67.7466 81. 75 136.0774 127.23 80.2847 242.00 67. 7962 83.79 115. 4301 127.91 86.0840 244.70 36.5458 84.00 122.2568 129.30 86.2146 252.40 0.0000 85.43 137.4787 131. 20 83.5131 252.80 55.9336 86. 55 137.6955 133. 02 93.0534 254.15 0.0000 86.79 137.7418 133.52 88.7729 256.23 52.8636 86.94 137.7705 136.00 90.0923 260.90 0.0000 Page 4702of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 56.7950 355.39 0.0000 584.27 25.5487 264.80 48.3411 356.01 36.8007 595.83 0.0000 265.00 42.3038 364.49 0.0000 427.87 23.8057 268.22 78.7367 366.42 0.0000 602.52 0.0000 269.46 63.0417 372. 51 32.6640 604. 72 28.6121 270.03 6-a.2784 375.05 27.5436 Q07.14 30. 0696 271.23 46.9327 377.52 35.3370 609.32 27.7055 273.65 0.0000 356.01 38.0497 610.33 27. 7161 276.40 34.1028 388.16 27:7344 614.28 17.2288 277.37 34.1241 388.63 0.0000 618.01 23.0039 277.60 34.1293 391.69 35.6006 620.36 21.1057 278.00 34.1387 264.66 34.0203 621. 93 21.1182 279.20 34.1652 401.81 40.1499 630.19 0.0000 279.54 34.1729 402.40 37.5428 631. 29 20.2275 279.70 34.1763 404.85 32.3441 633.25 13.4947 280.46 34.1934 410.95 36.8278 634.78 0.0000 283.69 42.4235 413.71 42.1475 635.95 16.4030 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 40.4292 423. 72 0.0000 645.85 25.1769 285.90 0.0000 427.09 35.3548 657.76 21. 3949 287.50 50.2978 427.87 29.1791 657.90 0.0000 290.67 49.1699 433.94 19.5096 661.66 25.3197 293.27 0.0000 439.40 28.4525 664.57 0.0000 351. 93 46.8459 453.88 25.0662 666.33 0.0000 295. 96 46.8680 463.37 19.7817 666.50 0.0000 879.38 52.7109 468.07 23.7891 667.71 0.0000 299.98 48.2227 473.00 0.0000 677.62 27.4212 300.09 48.2263 475.06 20.7913 685.70 0.0000 300.13 48.2275 476.78 26.2358 695.00 0.0000 301.36 56.9272 477.60 27.1503 696.49 29.5728 302.85 70.6046 482.18 25.3927 696.51 29.5728 256.23 49.5984 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 22.6790 306.78 45.9429 497.08 29.2116 697.49 22.6799 308.46 48.4763 505.52 21.9893 702.65 28.6472 311. 90 51.0686 507.63 0.0000 *706. 68 16.8160 316.51 51.2112 511. 00 24.7961 711. 68 16.8444 319.41 0.0000 514.00 24.8280 720.70 0.0000 320.08 0.0000 514.00 24.8280 721.93 0.0000 321.04 40.9131 520.40 21.2078 722.78 17.9019 323.87 37.6364 520.69 0.0000 722.91 10.4432 325.23 34.3185 522.65 0.0000 723.31 10.4445 328.76 0.0000 527.90 0.0000 724.19 16.4174 333.37 50.4614 528.26 19.4277 727.33 15.9368 333.97 56.7883 529.59 18.5124 733.00 7.9831 334.37 53.0153 529.87 0.0000 735.93 19.4778 338.28 50.6042 531.02 0.0000 333.97 11. 9922 338.32 50.6055 537.26 o.oboo 739.50 0.0000 311. 90 49.4010 546.56 0.0000 747.24 18.0461 340.48 49.4010 552.55 25.2290 748.06 20.0562 340.55 0.0000 563.25 25.3378 752.31 11.0461 344.28 33.0054 569.33 29.1621 753.82 0.0000 345.93 39.6437 946.00 30.1055 756.73 18.1018 351.06 34.8307 569.70 30.1068 756.80 18.1018 351. 93 34.8482 583.19 22.7002 884.68 19.6555 Page 4703 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 15.1288 1274.44 14. 0114 1620.50 4.6219 766.42 21.1837 1001.03 18.3454 1621. 92 8.3216 766.84 21.1871 1002.74 19.4333 1678.03 0.0000 772. 60 0.0000 1004.73 12. 9624 1690.97 6.5514 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0. 0000 . 1764.49 2.8431 778.90 20.2555 1028.54 0.0000 1063.66 2.5296 783.70 0.0000 1037.84 9.8049 1771.35 2.8464 785.37 22.3258 1038.76 0.0000 1791.20 0.0000 792.07 13. 7285 631. 29 19.6523 1808.65 4.7736 794.95 18.3215 1048.07 0.0000 1810.72 0.0000 795.86 18.3267 1049.04 24.0339 1836.06 1.9180 810.06 19.4291 1050.41 9.8357 810.29 19.4306 1063.66 24.1234 344.28 18.4087 1077.00 0.0000 810.76 18.4109 1077.34 12.1020 815.77 0.0000 1085.87 15.4355 1048.07 0.0000 1093.63 12.1503 832.01 21.6178 1099.45 11.0620 834.85 23. 6963 1112. 07 17.7526 835.71 22.6723 1112.84 18.8663 836.80 0.0000 1115. 54 19.9878 846.75 0.0000 1120.29 13.3408 846.77 13.4412 1120. 55* 13.3418 856.80 0.0000 1221.41 13.3438 860.56 10.3813 1129. 67 15. 5996 871.09 20.8268 1131.51 0.0000 873.19 12.5034 1147. 95 0.0000 875.33 0.0000 1173.23 16.8848 879.38 7.3068 1177.95 10.8180 880.51 21. 9271 1189.05 7.9080 883.24 14.6295 1204.77 17.0068 884.68 6.2725 1221. 41 17.0703 889.28 12.5615 1231. 02 12.3170 894.76 16.7747 1235.36 0.0000 898.04 15.7410 1238.28 15.9927 900.72 17.8529 1260.41 0.0000 903.28 16.8151 1271.87 5.7536 911.20 13.6930 1274.44 16 .1191 912.08 13. 6961 1274.54 16.1203 923.98 0.0000 1291.59 8. 667 6 926.50 7.9333 1298.22 0.0000 929 .11 0.0000 1312 .11 0.0000 937.49 17.5064 1332.49 12.8226 944 .13 0.0000 1362.66 0.0000 946.00 17.0150 1365.19 9.8588 949.00 18.0936 1368. 63 0.0000 667.71 0.0000 1384.29 12. 3713 962. 31 35.8900 1408.01 7.9909 964. 08 22.4415 1457.56 0.0000 966 .17 30.4738 1460.82 6.2805 911.20 24.6116 1489.16 5.4126 968. 97 24.6116 1505.03 16.2872 983.53 0.0000 1584.12 9.1827 984.45 0.0000 1596.21 0.0000 Page 4704 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:52:09.72 ********************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235078.CNF;l Background file DKAlOO:[CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM30.CNF;300 Background date : Z-OCT-2016 11:01:47. Sample date 17-DEC-2015 12:40:00 Acquisition date : 3-0CT-2016 06:48:14. Sample ID G405235078 Sample quantity l.56072E+02 GRAM Detector name : GAM30 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:01.31 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 0 4 4 0 0 0 0 0 0 0 3 3 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Page 4705 of 5809 Energy 38.83 47.70* 63.18* 74.89 77.16* 83.46* 87.95 92.85* 129.64* 186.34* 198.63* 209.02 238.75* 241.74 270.33 292.88 295.32* 324.56 338.50*

352.14* 463.52 511. 39* 583.76* 609.77* 624. 46 632. 85 672. 50 728.27 795.16 799.55 817.17 869.21 882.67 911. 27 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 11 21 44 146 174 36 134 61 26 85 19 22 267 82 27 19 145 12 46 213 20 30 99 152 16 6 20 28 22 6 10 11 6 64 Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 82 89 108 158 114 135 191 105 49 110 94 81 74 57 54 23 46 43 66 57 20 43 27 37 10 32 21 26 0 8 6 6 13 5 1. 24 0.82 1.16 1. 45 1. 04 0.58 4.13 1. 81 0.55 1. 57 1. 43 0.93 1. 26 1. 58 0.67 1. 49 1.12 0.91 0'. 9 8 1.10 0.91 2.31 1. 44 1. 46 1. 48 2.71 6.53 1.15 1. 68 1. 45 2.35 0.59 1. 22 1. 20 77.39 95.12 126.08 149.50 154.04 166.65 175.62 185.43 259.00 372. 42 397.01 417.78 477.24 483.21 540.41 585.52 590.39 648.87 67 6. 7 6 704.04 926.85 1022.60 1167.36 1219.40 1248.79 1265.58 1344.89 1456.45 1590.27 1599.07 1634.31 1738.42 1765.34 1822.57 76 90 123 145 145 163 170 182 257 366 393 415 473 473 536 584 584 644 671 698 923 1017 1161 1213 1245 1253 1336 1449 1587 1593 1629 1735 1760 1817 7 3.09E-03138.6 9 5.76E-03 86.8 8 1. 23E-02 45. 0 13 4.04E-02 18.4 1.57E+OO 13 4.84E-02 12.7 8 9.97E-03 59.0 12 3.72E-02 22.4 7 1. 71E-02 32. 8 6 7.25E-03 48.2 13 2.37E-02 28.3 9 5.27E-03 97.7 8 6.09E-03 74.0 20 7.43E-02 8.1 2.95E+OO 20 2.27E-02 24.8 9 7.50E-03 52.7 12 5.14E-03 35.1 4.llE+OO 12 4. 02E-02 11. 6 8 3.35E-03 97.9 12 1.28E-02 38.7 12 5.93E-02 9.9 9 5.42E-03 47.4 13 8.20E-03 62.4 14 2.74E-02 15.9 13 4.21E-02 11.9 8 4. 55E-03 41. 4 16 1.55E-03230.9 17 5.47E-03 58.2 13 7.85E-03 43.2 7 6.llE-03 21.3 8 1.79E-03 85.2 11 2.85E-03 54.4 8 3.19E-03 46.9 10 1.67E-03118.l 11 1.77E-02 14.4 Peak Search Report (continued) Page : 2 Sample ID : G405235078 Acquisition date 3-0CT-2016 06:48:14 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 968.22* 64 40 5.55 1936.51 1923 33 1.78E-02 33.0 36 0 1002.42* 5 27 2.36 2004.93 1993 15 1.31E-03248.1 .J7 0 1014.04 7 9 0.87 2028 .J9 2021 10 1.82E-03 97.6 38 0 1021. 51 3 8 0.92 2043.13 2039 6 8. 96E-04146.2 39 0 1115. 50 13 8 0.53 2231.17 2225 11 3. 51E-03 52.3 40 0 1120.47* 55 5 1.14 2241.13 2236 12 l.54E-02 16.4 41 0 1156.85 5 9 0.50 2313.93 2308 7 1. 33E-03118. 9 42 0 1171.69 10 7 3.36 2343.61 2338 10 2.74E-03 60.7 43 0 1199. 66 5 15 0.57 2399.58 2393 9 l.33E-03155.9 44 0 1212.17 10 9 0.61 2424.60 2419 9 2.78E-03 62.6 45 0 1220.79 7 8 1. 46 2441.86 2438 8 1.94E-03 79.5 46 0 1239.72 11 8 1. 63 2479.73 2475 8 3.06E-03 53.8 47 0 1286.97 11 10 4.32 2574.27 2567 11 3.16E-03 62.9 48 0 1293.60 5 5 1.26 2587.54 2583 6 l .. 33E-03 90.8 49 0 1378.36 12 8 0.91 2757.14 2751 10 3.19E-03 53.4 50 0 1408.55 6 2 1.27 2817.55 2813 7 1.70E-03 54.3 51 0 1442.45 7 2 0.54 2885.40 2881 8 1.99E-03 50.3 52 0 1461.16* 294 14 2.26 2922.84 2917 11 8.16E-02 6.4 53 0 1509.73 14 7 1.10 3020.04 3012 13 3.75E-03 47.5 54 0 1731.04 6 5 1. 26 3462.91 3457 7 1.57E-03 79.7 55 0 1764.92* 28 6 2.00 3530. 72 3524 11 7.90E...:03 25.9 Flag: "*" = Peak area was modified by background subtraction Page 4706 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:52:13 Configuration Analyses by DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235078.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 17-DEC-2015 12:40:00 G405235078 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:48:14 156.07 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID

  • GAMMA30 0 01:00:00.00 1.50 keV No Empirical 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 87.09 PB-214 87.09 PB-214 87.09 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 351.93 Page 4707of5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 SN-126 86.94 SN-126 87.57 CD-109 88.03 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-211 351.06 CAN 0 01:00:01.31 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : G405235078 Acquisition date 3-0CT-2016 06:48:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status K-40 1460.82 10.66* J..307E+OO 9.815E+OO 9.815E+OO 12.77 ,OK ZN-65 1115. 54 50.60* 1. 651E+OO 7.274E-02 1.661E-01 104.56 OK CD-109 88.03 3.70* 6.598E+OO 2.546E+OO 3. 941E+OO 60.62 OK SN-126 64.28 9.60 3.864E+OO 7.620E-01 7.620E-01 89.95 OK 86.94 8.90 6.598E+OO 1.058E+OO 1.058E+OO 60.62 OK 87.57 37.00* 6.598E+OO 2.546E-01 2.546E-01 60.62 OK TL-208 277.37 6.60 4.820E+OO Line Not Found Absent 583.19 85.00* 2.798E+OO 2.144E-01 2.144E-01 31. 88 OK 860.56 12.50 2.059E+OO Line Not Found Absent PB-210 46.54 4.25* 1.414E+OO 2.264E+OO 2.321E+OO 173.62 OK PB-212 74.82 10.28 5.449E+OO l.107E+OO 1.107E+OO 55.62 OK 77 .11 17.10 5. 696E+OO 1.127E+OO 1.127E+OO 25.44 OK 238.63 43.60* 5.355E+OO 6.491E-01 6.491E-01 16.20 OK 300.09 3.30 4.556E+OO Line Not Found Absent BI-214 609.32 45.49* 2.706E+OO 6.339E-01 6.341E-01 23.85 OK 1120.29 14.92 1.645E+00 1.085E+OO 1.085E+OO 32.84 OK 1764.49 15.30 1.122E+OO 7.547E-01 7.549E-01 51. 87 OK PB-214 74.82 5.80 5.442E+OO Line Not Found <<INT Reject 77 .11 9.70 5.696E+OO 1.986E+OO 1.987E+OO 25.44 OK 87.09 3.41 6.542E+OO Line Not Found <<INT Reject 242.00 7.25 5.305E+OO Line Not Found <<INT Reject 295.22 18.42 4.609E+OO 9.449E-01 9.452E-01 23.13 OK 351.93 35.60* 4.059E+OO 8.049E-01 8.052E-01 19.87 OK RN-222 609.32 45.49* 2.706E+OO 6.339E-01 6. 341E-01 23.85 OK 1120.29 14.92 l.645E+00 1.085E+OO l.085E+OO 32.84 OK 1764.49 15.30 1.122E+OO 7.547E-01 7.549E-01 51. 87 OK RA-224 240.99 4.10* 5.309E+OO 4.540E:-01 4.540E-01 247.54 OK RA-226 609.32 45.49* 2.706E+OO 6.339E-01 6.341E-01 23.85 OK 1120.29 14.92 1. 645E+OO 1.085E+OO 1. 085E+OO 32.84 OK 1764.49 15.30 1.122E+OO 7.547E-01 7.549E-01 51. 87 OK AC-2*28 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 5.374E-01 5.374E-01 77.38 OK 794.95 4.25 2 .196E+OO 1.178E+OO 1.178E+OO 42.64 OK 835. 71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1. 963E+OO 6.178E-01 6.178E-01 28.85 OK 968. 97 15.80 1.865E+OO l.065E+00 1.065E+OO 65.95 OK RA-228 105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 5.374E-01 5.374E-01 77.38 OK 794.95 4.25 2.196E+OO 1.178E+OO 1.178E+OO 42.64 OK 835.71 1. 61 2.109E+OO Line Not Found Absent 911.20 25.80* 1.963E+OO 6.178E-01 6.178E-01 28.85 OK 968. 97 15.80 1.865E+OO l.065E+00 1.065E+OO 65.95 OK TH-228 74.82 10.28 5.449E+00 1.107E+OO l.107E+00 55. 62" OK 77 .11 17.10 5. 696E+OO 1.127E+OO 1.127E+OO 25.44 OK 238.63 43.60* 5.355E+00 6.491E-01 6.491E-01 16.20 OK 300.09 3.30 4.556E+OO Line Not Found Absent TH-230 609.32 45.49* 2.706E+00 6.339E-01 6.339E-01 23.85 OK 1120.29 14.92 l.645E+00 1.085E+OO 1.085E+OO 32.84 OK 1764.49 15.30 1.122E+OO 7.547E-01 7.547E-01 51. 87 OK Page 4708 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G405235078 Acquisition date 3-0CT-2016 06:48:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi/GRAM %Error Status TH-232 .105.21 1.10 7.278E+OO Line Not Found Absent 338.32 11. 27 4.177E+OO 5.374E-01 5.374E-01 77.38 OK 835. 71 1. 61 2.109E+OO Line Not Found Absent 911.20 *25.80* 1.963E+OO 6.178E-01 6.178E-01 28.85 OK 968. 97 15.80 1.865E+OO 1.065E+OO 1.065E+OO 65.95 OK TH-234 63.29 3.70* 3.864E+OO 1.977E+OO 1. 977E+OO 89.95 OK 92. 59 4.23 6.873E+OO 1.308E+OO 1.308E+OO 65.63 OK U-234 609.32 45.49* 2.706E+OO 6.339E-01 6.339E-01 23.85 OK 1120.29 14.92 1.645E+OO 1.085E+OO 1.085E+OO 32.84 OK 1764.49 15.30 1.122E+OO 7.547E-01 7.547E-01 51. 87 OK U-238 63.29 3.70* 3.864E+OO 1.977E+OO 1. 977E+OO 89.95 OK 92. 59 4.23 6.873E+OO l.308E+00 1.308E+00 65. 63 OK AM-243 43.53 5.90 8.765E-01 Line Not Found Absent 74.66 67.20* 5.449E+OO 1.693E-01 1.694E-01 55.62 OK ANH-511 511. 00 100.00* 3.089E+OO 5.009E-02 5.009E-02 124.84 OK Flag: "*" = Keyline Page 4709 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:52:15.60 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235078.CNF;l *
  • Acquisition date 3-0CT-2016 06:48:14 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.31 Half life ratio : ***** *
  • Sample date 17-DEC-2015 12:40:00 Analyst initials: MXRl *
  • Sample ID G405235078 Sample Quantity 1.5607E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) K-40 9.815E+OO 1.228E+OO ZN-65 1.661E-01 1. 702E-01 CD-109 3.941E+OO 2.341E+OO SN-126 2.546E-01 l.513E-01 TL-208 2.144E-01 6.699E-02 PB-210 2.321E+OO 3.948E+OO PB-212 6.491E-01 1.030E-01 BI-214 6.341E-01 l.482E-01 PB-214 8.052E-01 l.568E-01 RN-222 6.341E-01 l.482E-01 RA-224 4.540E-01 1.101E+OO RA-226 6.341E-01 1.482E-01 AC-228 6.178E-01 1.747E-01 RA-228 6.178E-01 1. 747E-01 TH-228 6.491E-01 l.030E-01 TH-230 6.339E-01 l.481E-01 TH-232 6.178E-01 1. 747E-01 TH-234 1.977E+OO 1. 743E+OO U-234 6.339E-01 1. 481E-01 U-238 1.977E+OO 1. 743E+OO AM-243 l.694E-01 9.231E-02 ANH-511 5.009E-02 6.129E-02 Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 Page 4710 of 5809 Key-Line Activity (pCi/GRAM -1.176E+OO -2.631E-03 O.OOOE+OO -4.231E-03 1. 8 63E-01 O.OOOE+OO O.OOOE+OO -1.007E-03 K.L. Cnt Uncert ( 1. 96-sigma) 6.480E+OO 2.835E-02 1.317E+41 l.906E-02 2.351E-01 6.782E+03 2.633E+02 4.994E-02 MDA (pCi/GRAM 5.615E-01 1.770E-01 1.287E+OO 8.354E-02 4.379E-02 3.356E+OO 7.403E-02 8.492E-02 9.700E-02 8.492E-02 7.931E-01 8.492E-02 2.017E-01 2.017E-01 7.403E-02 8.490E-02 2.017E-01 1.452E+OO 8.490E-02 1.452E+OO 6.302E-02 4.407E-02 MDA (pCi/GRAM l.296E+Ol 5.953E-02 O.OOOE+OO 4.077E-02 5.377E-01 O.OOOE+OO O.OOOE+OO 9.652E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT.

C0-56 2.865E-02 3.062E-01 6.160E-01 FAIL ABUN MN-56 O.OOOE+OO l.960E+41 0.000E+OO SHORT HLIF C0-57 l.973E-02 3.802E-02 7. 541E-02 NOT IDENT. C0-58 1. 630E-01 3.813E-01 8. 096E-01 NOT IDENT. FE-59 2.014E+OO 4.725E+OO 9.794E+OO NOT IDENT. C0-60 6.653E-03 l.943E-02 4.786E-02 NOT IDENT. GE-68 -1.030E-01 l.378E+OO 2. 811E+OO NOT IDENT. AS-73 6.373E+OO 5 .119E+OO 1.133E+Ol NOT IDENT. AS-74 0.000E+OO 2.563E+03 O.OOOE+OO SHORT HLIF SE-75 -l .196E-02 1. 508£-01 2.768E-01 NOT IDENT. BR-77 O.OOOE+OO 1.315E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 3.545E+02 O.OOOE+OO SHORT HLIF RB-83 1.385E-01 4.499E-01 9.337E-01 NOT IDENT. KR-85 1.887E+OO 4.406E+00 8.742E+OO NOT IDENT. SR-85 1. 797E-01 4.230E-01 8.388E-01 NOT IDENT. RB-86 O.OOOE+OO 1.294E+04 O.OOOE+OO SHORT HLIF Y-88 -l.435E-01 l.654E-01 2.743E-01 NOT IDENT. Y-91 l.927E+02 4.056E+02 8.287E+02 NOT IDENT. NB-94 3.970E-03 2.442E-02 4.859E-02 NOT IDENT. NB-95 4.956E-02 6.033E-01 1.184E+OO NOT IDENT. NB-95M -l.015E+OO 1.898E+OO 3.038E+OO NOT IDENT. ZR-95 3.793E-01 9.186E-01 1.945E+OO NOT IDENT. NB-97 O.OOOE+OO 1.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO l.080E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF RH-101 2.166E-02 2.533E-02 4.908E-02 FAIL ABUN RH-102 8.932E-03 3.900E-02 7.507E-02 NOT IDENT. RU-103 -7.143E-01 3.530E+OO 6.891E+OO FAIL ABUN RH-106 4.069E-02 3.362E-01 6.288E-01 NOT IDENT. RU-106 4.069E-02 3.362E-01 6.288E-01 NOT IDENT. AG-108M 8.300E-03 l.877E-02 4.009E-02 NOT IDENT. AG-llOM -7.034E-02 8.199E-02 l.098E-01 NOT IDENT. SN-113 2.053E-02 1.539E-01 3.156E-01 NOT IDENT. CD-115 O.OOOE+OO l.192E+38 0.000E+OO SHORT HLIF SN-ll 7M O.OOOE+OO 4.575E+04 O.OOOE+OO SHORT HLIF TE-123M -9.552E-02 9.484E-02 l.614E-01 NOT IDENT. SB-124 -2.323E-01 8.245E-01 1.834E+OO NOT IDENT. SB-125 -2.694E-02 7.290E-02 1.405E-01 FAIL ABUN TE-125M -9.698E+Ol l.854E+02 3. 351E+02 NOT IDENT. I-126 O.OOOE+OO 3.651E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 5.648E+05 O.OOOE+OO SHORT HLIF SB-127 O.OOOE+OO 3.099E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 1.585E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO l.960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 4.226E+25 O.OOOE+OO SHORT HLIF BA-133 -8 .116E-03 3.171E-02 5.579E-02 NOT IDENT. I-133 0.000E+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-134 7.645E-02 3.195E-02 8.602E-02 FAIL ABUN CS-135 4.547E-02 l.005E-01 1.859E-01 NOT IDENT. I-135 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO l.388E+05 O.OOOE+OO SHORT HLIF BA-137M l.134E-02 l.929E-02 4.337E-02 NOT IDENT. CS-137 l.198E-02 2.038E-02 4.582E-02 NOT IDENT. CE-139 9. 951E-02 8.064E-02 l.689E-01 NOT IDENT. BA-140 O.OOOE+OO 5.668E+05 O.OOOE+OO SHORT HLIF LA-140 O.OOOE+OO 2.071E+05 O.OOOE+OO SHORT HLIF CE-141 -2.798E+OO l.418E+Ol 2.649E+Ol NOT IDENT. CE-143 0.000E+OO 6.878E+40 O.OOOE+OO SHORT HLIF CE-144 2. 731E-02 2.591E-01 5.008E-01 NOT IDENT. PM-144 -8.166E-03 4.169E-02 8 .132E-02 NOT IDENT. PR-144 -6. 821E-01 3.608E+OO 7.044E+OO NOT IDENT. PM-146 -1.093E-02 2.745E-02 5.291E-02 FAIL ABUN ND-147 0.000E+OO 1. 091E+07 O.OOOE+OO SHORT HLIF PM-147 5.975E+02 6.558E+02 1.342E+03 NOT IDENT. PM-149' O.OOOE+OO 2 .112E+39 O.OOOE+OO SHORT HLIF EU-150 2.492E-03 1. 868E-02 3.499E-02 FAIL ABUN EU-152 5.074E-02 6.744E-02 1. 463E-01 FAIL ABUN GD-153 -6.355E-02 l.176E-01 2.152E-01 NOT IDENT. EU-154 -8.478E-03 6.928E-02 1. 447E-01 NOT IDENT. EU-155 6.282E-02 7.776E-02 1.601E-01 FAIL ABUN TB-160 3.852E-01 l .116E+OO 2.229E+OO FAIL ABUN H0-166M -4.039E-02 4.343E-02 7.258E-02 NOT IDENT. TM-171 -l.457E+Ol l.341E+Ol 2.453E+Ol NOT IDENT. HF-172 -5.288E-02 l.701E-01 3.165E-01 FAIL ABUN LU-172 -4.014E-03 4.828E-02 9.473E-02 FAIL ABUN LU-176 -l.292E-02 1.840E-02 3.053E-02 FAIL ABUN HF-181 3.400E-01 2.616E+OO 5.355E+OO NOT IDENT. Page 4711of5809 TA-182 4.702E-01 7.330E-01 l.413E+OO FAIL ABUN RE-183 -6.013E-01 1.767E+OO 3.438E+OO NOT IDENT. RE-184 -2.243E+OO 1. 708E+Ol 3.314E+Ol NOT IDENT. W-188 4.427E+Ol 9.458E+Ol 1. 688E+02 FAIL ABUN IR-192 1. 420E-01 3.145E-01 6.637E-01 FAIL ABUN HG-203 1.478E-01 1. 741E+OO 3.221E+OO NOT IDENT. BI-207 -2.272E-02 3.368E-02 5.619E-02 FAIL ABUN BI-211 O.OOOE+OO 4.318E-01 6.439E-01 FAIL ABUN PB-211 l.003E-01 4.856E-01 9.977E-01 NOT IDENT. BI-212 9.066E-01 7. 9.778E-01 FAIL ABUN RN-219 -1. 700E-02 2.515E-01 5.068E-01 FAIL ABUN RA-223 3.853E-01 7.392E-01 9.522E-01 FAIL ABUN AC-227 -l.940E-02 l.623E-01 2.982E-01 NOT IDENT. TH-227 -1.940E-02 1.623E-01 2.982E-01 NOT IDENT. TH-229 -2.685E-01 3.798E-01 6.580E-01 FAIL ABUN PA-231 1.333E-02 3.252E-01 6.024E-01 NOT IDENT. TH-231 3.853E-01 7.392E-01 9.522E-01 FAIL ABUN PA-233 1.786E-02 4.329E-02 9.122E-02 NOT IDENT. PA-234 9.735E-02 2.069E-01 4.384E-01 FAIL ABUN PA-234M 1.506E+OO 7.325E+OO 7.840E+OO FAIL ABUN U-235 3.018E-02 1.377E-01 2.657E-01 FAIL ABUN NP-237 1. 786E-02 4.329E-02 9.122E-02 NOT IDENT. NP-238 O.OOOE+OO 1. 757E+40 O.OOOE+OO SHORT HLIF NP-239 -1.500E-02 l.751E-01 3.346E-01 NOT IDENT. PU-239 3.395E+02 3.208E+02 4.538E+02 FAIL ABUN AM-241 l.034E-01 9.534E-02 l.943E-01 NOT IDENT. CM-243 -7. OllE-02 6.979E-02 1.230E-01 NOT IDENT. BK-247 -l.690E-02 5.467E-02 9.745E-02 FAIL ABUN CM-247 -9.582E-03 2.323E-02 4.480E-02 NOT IDENT. CF-249 -l.732E-03 2.670E-02 5.352E-02 NOT IDENT. CF-251 -2.684E-02 8.971E-02 l.635E-01 NOT IDENT. Page 4712of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:52:11.41 Nuclide Line Activity Report Nuclide Type:

  • Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 284 10.66* 1.307E+OO 9.815E+OO 9.815E+OO 12.77 ZN-65 1115. 54 13 50.60* 1.651E+OO 7.274E-02 1. 661E-01 104.56 CD-109 88.03 173 3.70* 6.598E+OO 3.417E+OO 5.289E+OO 44.78 SN-126 64.28 59 9.60 3.864E+OO 7.620E-01 7.620E-01 89.95 86.94 173 8.90 6.598E+OO 1.420E+OO 1.421E+OO 44.78 87.57 173 37.00* 6.598E+OO 3.417E-01 3.417E-01 44.78 TL-208 277.37 ------6.60 4.820E+OO ------Line Not Found ------583.19 106 85.00* 2.798E+OO 2.144E-01 2.144E-01 31. 88 860.56 ------12.50 2.059E+OO ------Line Not Found ------PB-210 46.54 28 4.25* 1.414E+OO 2.264E+00 2.321E+OO 173.62 BI-211 72. 87 ------1. 23 5. 213E+OO ------Line Not Found ------351.06 242 12.92* 4.059E+OO 2.218E+OO 2.218E+OO 19.87 PB-212 74.82 191 10.28 5.449E+OO 1.640E+OO 1.640E+OO 36.78 77.11 228 17.10 5.696E+OO 1.127E+OO 1.127E+OO 25.44 238.63 315 43.60* 5.355E+OO 6.491E-01 6.491E-01 16.20 300.09 ------3.30 4.556E+OO ------Line Not Found ------BI-214 609.32 162 45.49* 2.706E+OO 6.339E-01 6.341E-01 23.85 1120. 29 55 14.92 1.645E+OO 1.085E+OO 1.085E+OO 32.84 1764.49 27 15.30 1.122E+OO 7.547E-01 7.549E-01 51. 87 PB-214 74.82 191 5.80 5.449E+OO 2.907E+OO 2.908E+OO 36.78 77 .11 228 9.70 5.696E+OO 1. 986E+OO l.987E+OO 25.44 87.09 173 3.41 6.598E+OO 3.707E+OO 3.709E+OO 44.78 242.00 96 7.25 5.309E+OO 1. 202E+OO l.202E+OO 49.67 295.22 167 18.42 4.609E+OO 9.449E-01 9.452E-01 23.13 351. 93 242 35.60* 4.059E+OO 8.049E-01 8.052E-01 19.87 RN-222 609.32 162 45.49* 2.706E+OO 6.339E-01 6.341E-01 23.85 1120.29 55 14.92 1.645E+OO 1.085E+OO 1.085E+OO 32.84 1764.49 27 15.30 1.122E+OO 7.547E-01 7.549E-01 51. 87 RA-224 240.99 96 4.10* 5.309E+OO 2.125E+OO 2.125E+OO 49.67 RA-226 609.32 162 45.49* 2.706E+OO 6.339E-01 6. 341E-01 23.85 1120.29 55 14.92 1.645E+OO 1.085E+OO 1.085E+OO 32.84 1764.49 27 15.30 1.122E+OO 7.547E-01 7.549E-01 51. 87 AC-228 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 53 11. 27 4.177E+OO 5.374E-01 5.374E-01 77.38 794.95 23 4.25 2.196E+OO 1.178E+OO 1.178E+OO 42.64 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911. 20 65 25.80* 1. 963E+OO 6.178E-01 6.178E-01 28.85 968.97 65 15.80 1.865E+OO 1.065E+OO 1.065E+OO 65.95 RA-228 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 53 11. 27 4.177E+OO 5.374E-01 5.374E-01 77.38 794.95 23 4.25 2 .196E+OO 1.178E+OO 1.178E+OO 42. 64 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911.20 65 25.80* 1. 963E+OO 6.178E-01 6.178E-01 28.85 968.97 65 15.80 l.865E+OO 1.065E+OO 1.065E+OO 65.95 TH-228 74.82 191 10.28 5.449E+OO 1.640E+OO 1.640E+OO 36.78 77 .11 228 17.10 5. 696E+OO 1.127E+OO 1.127E+OO 25.44 238.63 315 43.60* 5.355E+OO 6.491E-01 6.491E-01 16.20 Page 4713 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G405235078 Acquisition date 3-0CT-2016 06:48:14 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 300.09 ------3.30 4.556E+OO ------Line Not.Found ------TH-230 609.32 162 45.49* 2.706E+OO 6.339E-01 6.339E-01 23.85 1120.29 55 14.92 1.645E+OO 1.085E+OO 1.085E+OO 32.84 1764.49 27 15.30 1.122E+OO 7.547E-01 7.547E-01 51. 87 TH-232 105.21 ------1.10 7.278E+OO ------Line Not Found ------338.32 53 11.27 4.177E+OO 5.374E-01 5.374E-01 77.38 835.71 ------1. 61 2.109E+OO ------Line Not Found ------911. 20 65 25.80* 1. 963E+OO 6.178E-01 6.178E-01 28.85 968. 97 65 15.80 1.865E+OO 1.065E+OO 1.065E+OO 65.95 TH-234 63.29 59 3.70* 3.864E+OO 1.977E+OO 1.977E+OO 89.95 92.59 79 4.23 6.873E+OO 1.308E+OO 1.308E+OO 65. 63 U-234 609.32 162 45.49* 2.706E+OO 6.339E-01 6.339E-01 23.85 1120.29 55 14.92 1.645E+OO 1.085E+OO 1.085E+OO 32.84 1764.49 27 15.30 1.122E+OO 7.547E-01 7.547E-01 51. 87 U-238 63. 29 59 3.70* 3.864E+OO 1.977E+OO 1.977E+OO 89.95 92.59 79 4.23 6.873E+OO 1.308E+OO 1.308E+OO 65.63 AM-243 43.53 ------5.90 8.765E-01 ------Line Not Found ------74.66 191 67.20* 5.449E+00 2.509E-01 2.509E-01 36.78 ANH-511 511. 00 32 100.00* 3.089E+OO 5.009E-02 5.009E-02 124.84 Flag: "*" Keyline Page 4714 of 5809 Summary of Nuclide Activity Sample ID : G405235078 Acquisition date Page : 3 3-0CT-2016 06:48:14 Total number of lines in spectrum 55 Number of unidentified lines 17 Number of lines tentatively identified by NID 38 Nuclide Type : Nuclide K-40 ZN-65 CD-109 SN-126 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Hlife l.25E+09Y 244.06D 461. 40D 2.30E+05Y 1. 41E+l0Y 22.20Y 7.04E+08Y 1. 41E+l0Y 1600.00Y 1600.00Y 1600.00Y 1. 41E+l0Y 1600. OOY l.41E+l0Y l.41E+l0Y l.41E+l0Y 7.54E+04Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 4.47E+09Y 7370.00Y l.OOE+09Y Decay 1. 00 2.28 1. 55 1. 00 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity Uncorrected pCi/GRAM 9.815E+00 7.274E-02 3.417E+OO 3.417E-01 2.144E-01 2.264E+00 2.218E+00 6. 491E-01 6.339E-01 8.049E-01 6.339E-01 2.125E+00 6.339E-01 6.178E-01 6.178E-01 6.491E-01 6.339E-01 6.178E-01 l.977E+00 6.339E-01 l.977E+00 2.509E-01 5.009E-02 3.185E+Ol 3.185E+Ol
  • Decay Corr pCi/GRAM 9.815E+OO 1. 661E-Ol 5.289E+OO 3.417E-01 2.144E-01 2.321E+OO 2.218E+OO 6. 491E-01 6.341E-01 8.052E-01 6.341E-01 2.125E+OO 6.341E-01 6.178E-01 6.178E-01 6.491E-01 6.339E-01 6.178E-01 1. 977E+OO 6.339E-01 l.977E+OO 2.509E-01 5.009E-02 3.387E+Ol 3.387E+Ol 69.09% Decay Corr 2-Sigma Error l.253E+OO l.737E-01 2.368E+OO l.530E-01 0.684E-01 4.029E+OO 0.441E+OO l.051E-01 l.512E-01 l.600E-01 l.512E-01 l.055E+OO l.512E-01 l.782E-01 l.782E-01 l.051E-01 l.512E-01 l.782E-01 l.778E+OO l.512E-01 l.778E+00 0.923E-01 6.254E-02 "M" Manually accepted 2-Sigma %Error 12.77 104.56 44.78 44.78 31. 88 173. 62 19.87 16.20 23.85 19.87 23.85 49.67 23.85 28.85 28.85 16.20 23.85 28.85 89.95 23.85 89.95 36.78 124.84 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4715 of 5809 Flags Unidentified Energy Lines Page : 4 Sample ID : G405235078 Acquisition date : 3-0CT-2016 06:48:14 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 38.83 15 114 1.24 77.39 76 7 3.09E-03 **** 4.25E-01 0 83.46 47 175 0.58 166.65 163 8 9.97E-03 **** 6.28E+OO T 0 129.64 33 62 0.55 259.00 257 6 7.25E-03 96.4 7.32E+OO T 0 .186.34 103 132 1. 57 372.42 366 J.3 2.37E-02 56.5 6.29E+OO T 0 198.63 23 113 1. 43 397.01 393 9 5.27E-03 **** 6.05E+OO T 0 209.02 26 97 0.93 417.78 415 8 6.09E-03 **** 5.85E+OO 0 270.33 31 63 0.67 540.41 536 9 7.50E-03 **** 4.91E+OO T 2 292.88 21 27 1. 49 585.52 584 12 5.14E-03 70.2 4.64E+OO T 0 324.56 14 49 0.91 648.87 644 8 3.35E-03 **** 4.31E+OO T 0 463.52 21 23 0.91 926.85 923 9 5.42E-03 94.8 3.32E+00 T 0 624.46 17 10 1. 48 1248.79 1245 8 4.55E-03 82.8 2.66E+OO 0 632.85 6 35 2.71 1265.58 1253 16 1.55E-03 **** 2.63E+OO T 0 672. 50 21' 23 6.53 1344.89 1336 17 5.47E-03 **** 2.51E+OO 0 728.27 30 27 1.15 1456.45 1449 13 7.85E-03 86.4 2.36E+OO T 0 799.55 7 8 1. 45 1599.07 1593 8 1.79E-03 **** 2.19E+OO 0 817.17 11 6 2.35 1634.31 1629 11 2.85E-03 **** 2.15E+OO T 0 869.21 12 6 0.59 1738.42 1735 8 3.19E-03 93.9 2.04E+OO 0 882.67 6 13 1. 22 1765.34 1760 10 1. 67E-03 **** 2.02E+00 T 0 1002.42 5 27 2.36 2004.93 1993 15 l.31E-03 **** l.81E+OO T 0 1014.04 7 10 0.87 2028.19 2021 10 l.82E-03 **** 1.79E+OO 0 1021.51 3 8 0.92 2043.13 2039 6 8.96E-04 **** 1.78E+00 T 0 1156. 85 5 9 0.50 2313.93 2308 7 1. 33E-03 **** 1. 60E+OO 0 1171. 69 10 7 3.36 2343.61 2338 10 2.74E-03 **** 1.58E+OO 0 1199. 66 5 15 0.57 2399.58 2393 9 1. 33E-03 **** 1.55E+OO 0 1212.17 10 9 0.61 2424.60 2419 9 2.78E-03 **** l.54E+OO 0 1220.79 7 8 1. 46 2441. 86 2438 8 l.94E-03 **** 1.53E+OO T 0 1239. 72 11 8 1. 63 2479.73 2475 8 3.06E-03 **** 1.51E+OO T 0 1286.97 11 9 4.32 2574.27 2567 11 3.16E-03 **** 1.46E+OO 0 1293. 60 5 5 1.26 2587.54 2583 6 l.33E-03 **** 1. 45E+00 0 1378.36 11 7 0.91 2757.14 2751 10 3.19E-03 **** l.37E+OO 0 1408.55 6 2 1. 27 2817.55 2813 7 1. 70E-03 **** 1.35E+OO T 0 1442.45 7 2 0.54 2885.40 2881 8 l.99E-03 **** l.32E+00 0 1509.73 13 6 1.10 3020.04 3012 13 3.75E-03 95.0 1.27E+OO 0 1731. 04 5 5 1. 26 3462.91 3457 7 1.57E-03 **** l.14E+00 Flags: "T" = Tentatively associated Page 4716of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:52:28.54 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * *
  • DETECTOR AND SAMPLE DATA * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235078.CNF;l *
  • Acquisition date 3-0CT-2016 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.31 Half life ratio : ***** *
  • Sample date 17-DEC-2015 12:40:00 Nuclide Library : SOLID *
  • Sample ID G405235078 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.5607E+02 GRAM *
  • Wet wt corr : 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date ll-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF'GAM30 CAN.CNF;7
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 ZN-65 CD-109 SN-126 TL-208 PB-210 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-230 TH-232 TH-234 U-234 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.337E-01 7.043E-02 5.992E-01 3.888E-02 1.907E-02 1.540E+OO 3.408E-02 3.701E-02 4.380E-02 3.701E-02 3.651E-01 3.701E-02 8.774E-02 8.774E-02 3.408E-02 3.700E-02 8.774E-02 6.767E-01 3.700E-02 6.767E-01 2.958E-02 l.986E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 Page 4717 of 5809 Le (pCi/GRAM 5.602E+OO 2.423E-02 O.OOOE+OO l.444E-02 2.321E-01 O.OOOE+OO O.OOOE+OO 4.225E-02 2.646E-01 .NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN MN-56 C0-57 C0-58 FE-59 C0-60 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103' RH-106 RU-106 AG-108M AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 BA-137M CS-137 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 Page 4718 of 5809 O.OOOE+OO 3.539E-02 3.516E-01 4.249E+OO l.877E-02 l.152E+OO 5.294E+OO 0.000E+OO 1.259E-01 O.OOOE+OO O.OOOE+OO 4.160E-01 3.839E+OO 3.683E-01 O.OOOE+OO 9.720E-02 3.630E+02 2.153E-02 5.232E-01 1.400E+OO 8.476E-01 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.289E-02 3.227E-02 3.047E+OO 2.708E-01 2.708E-01 1.790E-02 4.470E-02 1.418E-01 O.OOOE+OO O.OOOE+OO 7.414E-02 5.797E-01 6.237E-02 l.557E+02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 2.503E-02 O.OOOE+OO 3.838E-02 8.430E-02 O.OOOE+OO O.OOOE+OO 1.870E-02 1. 97 6E-02 7.889E-02 O.OOOE+OO O.OOOE+OO 1.225E+Ol O.OOOE+OO 2.329E-01 3.587E-02 3.lOBE+OO 2.305E-02 O.OOOE+OO 6.301E+02 O.OOOE+OO l.579E-02 6.669E-02 9.971E-02 5.874E-02 7.492E-02 9. 372E-01 3 .114E-02 1.131E+Ol 1.470E-01 3.898E-02 l.364E-02 2.376E+OO 6.137E-01 SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT.HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN RE-183 RE-184 W-188 IR-192 HG-203 BI-207 BI-211 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-229 PA-231 TH-231 PA-233 PA-234 PA-234M U-235 NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4719of5809 1.598E+OO 1. 395E+Ol 7.786E+Ol 3. 031E-01 1.478E+00 2.285E-02 3.091E-01 4.500E-01 4.465E-01
  • 2. 255E-01 4.365E-01 1.350E-01 1.350E-01 3.036E-01 2.731E-Ol 4.365E-01 4.161E-02 1. 901E-01 3.485E+OO i.239E-01 4 .161E-02 O.OOOE+OO l.554E-01 2 .118E+02 9 .113E-02 5.681E-02 4.414E-02 1.984E-02 2.404E-02 7.557E-02 NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:52:35.25 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA *
  • *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G405235078.CNF;l *
  • Acquisition date 3-0CT-2016 06:48:14 Sensitivity : 3.000 *
  • Detector ID GAM30 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:01.31 Half life ratio : ***** *
  • Sample date 17-DEC-2015 12:40:00 Nuclide Library : SOLID *
  • Sample ID G405235078 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity 1.5607E+02 GRAM *
  • Quantity Err(%) 1.2815E-03 % * *Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION *
  • Eff. Cal. date 11-MAR-2016 05:58:49 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM30 CAN.CNF;7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activi'ty Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 9.815E+OO 1.508E+OO 1.508E+OO ZN-65 l.661E-01 1.734E-01 l.734E-01 CD-109 3.941E+OO 2.380E+OO 2.380E+OO SN-126 2.546E-01 l.532E-01 l.532E-01 TL-208 2.144E-01 6.925E-02 6.925E-02 PB-210 2.321E+00 3.953E+OO 3.953E+OO PB-212 6.491E-01 1.159E-01 l.159E-01 BI-214 6.341E-01 l.568E-01 1.568E-01 PB-214 8.052E-01 1.703E-01 1. 703E-01 RN-222 6.341E-01 1.568E-01 1.568E-01 RA-224 4.540E-01 1.119E+OO l .119E+00 RA-226 6.341E-01 l.568E-01 1.568E-01 AC-228 6.178E-01 1.948E-01 l.948E-01 RA-228 6.178E-01 1.948E-01 1.948E-01 TH-228 6.491E-01 l.159E-01 l.159E-01 TH-230 6.339E-01 l.568E-01 1.568E-01 TH-232 6.178E-01 1. 948E-01 1.948E-01 TH-234 1.977E+OO 1. 798E+OO 1. 798E+OO U-234 6.339E-01 1.568E-01 1.568E-01 U-238 1.977E+OO 1. 798E+OO 1. 798E+OO AM-243 l.694E-01 9. 396E-02 9. 396E-02 ANH-511 5.009E-02 6.143E-02 6.143E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) BE-7 -1.176E+OO 6.481E+OO 6.503E+OO NOT IDENT. NA-22 -2.631E-03 2.835E-02 2.838E-02 NOT IDENT. NA-24 l.OOOE+41 1.385E+41 O.OOOE+OO SHORT HLIF AL-26 -4.231E-03 1.907E-02 l.916E-02 NOT IDENT. SC-46 1. 8 63E-01 2.363E-01 2.508E-01 FAIL ABUN V-48 -l.344E+03 6.785E+03 6.812E+03 SHORT HLIF CR-51 -2.545E+02 2.642E+02 2.880E+02 SHORT HLIF MN-54 -l.007E-03 4.994E-02 4.994E-02 NOT IDENT. Page 4720 of 5809 C0-56 2.865E-02 3.063E-01 3.065E-01 FAIL ABUN MN-56 1.000E+41 l. ll 7E+42 O.OOOE+OO SHORT HLIF C0-57 1. 973E-02 3.805E-02 3.907E-02 NOT IDENT. C0-58 1.630E-01 3.817E-01 3.887E-01 NOT IDENT. FE-59 2.014E+00 4.743E+OO 4.829E+OO NOT IDENT. C0-60 6.653E-03 l.944E-02 1.967E-02 NOT IDENT. GE-68 -l.030E-01 1.378E+OO 1. 379E+OO NOT IDENT. AS-73 6.373E+OO 5.285E+OO 6.015E+OO NOT IDENT. AS-74 -7.197E+02 2.564E+03 2.585E+03 SHORT HLIF SE-75 -1.196E-02 l.508E-OJ. l.509E-01 NOT IDENT. BR-77 8.282E+36 6.952E+37 0.000E+OO SHORT HLIF SR-82 -3.910E+Ol 3.545E+02 3.550E+02 SHORT HLIF RB-83 1.385E-01 4.504E-01 4.547E-01 NOT IDENT. KR-85 1.887E+OO 4.409E+OO 4.490E+OO NOT IDENT. SR-85 1.797E-01 4.232E-01 4.309E-01 NOT IDENT. RB-86 2.407E+03 l.294E+04 1.299E+04 SHORT HLIF Y-88 -1.435E-01 1.657E-01 1. 779E-01 NOT IDENT. Y-91 l.927E+02 4.060E+02 4.152E+02 NOT IDENT. NB-94 3.970E-03 2.442E-02 2.449E-02 NOT IDENT. NB-95 4.956E-02 6.033E-01 6.037E-01 NOT IDENT. NB-95M -1.015E+OO 1.901E+OO 1.955E+OO NOT IDENT. ZR-95 3.793E-01 9.194E-01 9.351E-01 NOT IDENT. NB-97 -l.000E+41 7.238E+41 0.000E+OO SHORT HLIF ZR-97 l.OOOE+41 6.405E+41 O.OOOE+OO SHORT HLIF M0-99 6.912E+30 1.082E+31 O.OOOE+OO SHORT HLIF TC-99M -1.000E+41 4.799E+41 0.000E+OO SHORT HLIF RH-101 2.166E-02 2.565E-02 2.745E-02 FAIL ABUN RH-102 8.932E-03 3. 901E-02 3.922E-02 NOT IDENT. RU-103 -7.143E-01 3.530E+OO 3.545E+OO FAIL ABUN RH-106 4.069E-02 3.362E-01 3.367E-01 NOT IDENT. RU-106 4.069E-02 3.362E-01 3.367E-01 NOT IDENT. AG-108M 8.300E-03 1.879E-02 1.916E-02 NOT IDENT. AG-llOM -7.034E-02 8.252E-02 8.840E-02 NOT IDENT. SN-113 2.053E-02 1.539E-01 1.541E-01 NOT IDENT. CD-115 -7.301E+37 1.200E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -4.269E+04 4.607E+04 4.993E+04 SHORT HLIF TE-123M -9.552E-02 9.507E-02 l.044E-01 NOT IDENT. SB-124 -2.323E-01 8.247E-01 8. 313E-01 NOT IDENT. SB-125 -2.694E-02 7.294E-02 7.394E-02 FAIL ABUN TE-125M -9.698E+Ol l.855E+02 l.906E+02 NOT IDENT. I-126 3.887E+05 3. 696E+05 4.090E+05 SHORT HLIF SB-126 -7.254E+04 5.650E+05 5.659E+05 SHORT HLIF SB-127 -1.667E+21 3.815E+21 O.OOOE+OO SHORT HLIF I-131 5.672E+08 l.586E+09 l.606E+09 SHORT HLIF I-132 -l.OOOE+41 1. 821E+42 O.OOOE+OO SHORT HLIF TE-132 -9.298E+24 4.242E+25 O.OOOE+OO SHORT HLIF BA-133 -8 .116E-03 3.172E-02 3.193E-02 NOT IDENT. I-133 1.000E+41 1.217E+42 O.OOOE+OO SHORT HLIF CS-134 7.645E-02 3.298E-02 4.770E-02 FAIL ABUN CS-135 4.547E-02 1.006E-01 1.027E-01 NOT IDENT. I-135 1.000E+41 9.651E+41 0.000E+OO SHORT HLIF CS-136 6.714E+04 1.395E+05 l.427E+05 SHORT HLIF BA-137M 1.134E-02 l.931E-02 1.998E-02 NOT IDENT. CS-137 1.198E-02 2.040E-02 2. llOE-02 NOT IDENT. CE-139 9.951E-02 8.324E-02 9.456E-02 NOT IDENT. BA-140 -4.959E+05 5.683E+05 6.107E+05 SHORT HLIF LA-140 1. 408E+05 2.074E+05 2.169E+05 SHORT HLIF CE-141 -2.798E+OO l.418E+Ol 1.424E+Ol NOT IDENT. CE-143 1.000E+41 6.985E+40 O.OOOE+OO SHORT HLIF CE-144 2.731E-02 2.591E-01 2.594E-01 NOT IDENT. PM-144 -8.166E-03 4.170E-02 4.186E-02 NOT IDENT. PR-144 -6.821E-01 3.609E+OO 3.622E+OO NOT IDENT. PM-146 -1.093E-02 2.748E-02 -2.791E-02 FAIL ABUN ND-147 -5.260E+04 1.091E+07 1. 091E+07 SHORT HLIF PM-147 5.975E+02 6.571E+02 7.102E+02 NOT IDENT. PM-149 l.474E+38 2 .113E+39 O.OOOE+bO SHORT HLIF EU-150 2.492E-03 1. 8 68E-02 1.872E-02 FAIL ABUN EU-152 5.074E-02 6.759E-02 7.136E-02 FAIL ABUN GD-153 -6.355E-02 l.177E-01 1. 211E_:Ol NOT IDENT. EU-154 -8.478E-03 6.928E-02 6.939E-02 NOT IDENT. EU-155 6.282E-02 7.794E-02 8.293E-02 FAIL ABUN TB-160 3.852E-01 l.117E+OO 1.130E+OO FAIL ABUN H0-166M -4.039E-02 4.359E-02 4.724E-02 NOT IDENT. TM-171 -1.457E+Ol 1.348E+Ol 1. 499E+Ol NOT IDENT. HF-172 -5.288E-02 1.703E-01 1. 720E-01 FAIL ABUN LU-172 -4.014E-03 4.829E-02 4.833E-02 FAIL ABUN LU-176 -1.292E-02 l.843E-02 l.933E-02 FAIL ABUN HF-181 3.400E-01 2.616E+OO 2.620E+OO NOT IDENT. Page 4721 of 5809 TA-182 4.702E-01 7.343E-01 7.643E-01 FAIL ABUN RE-183 -6.013E-01 l.770E+00 1.790E+OO NOT IDENT. RE-184 -2.243E+OO 1.709E+Ol 1.712E+Ol NOT IDENT. W-188 4.427E+Ol 9.476E+Ol 9.684E+Ol FAIL ABUN IR-192 l.420E-01 3.147E-01 3.212E-01 FAIL ABUN HG-203 1.478E-01 1. 741E+OO 1. 742E+OO NOT IDENT. BI-207 -2.272E-02 3.394E-02 3.545E-02 FAIL ABUN BI-211 2.218E+OO 4.704E-01 l.105E+OO FAIL ABUN PB-211 1.003E-01 4.857E-01 4.878E-01 NOT IDENT. BI-212 9.066E-01 7. 728E-01
  • 8.742E-01 FAIL ABUN RN-219 -1. 700E-02 2.515E-01 2.516E-01 FAIL ABUN RA-223 3.853E-01 7.401E-01 7.602E-01 FAIL ABUN AC-227 -1.940E-02 1.623E-01 1.625E-01 NOT IDENT. TH-227 -l.940E-02 l.623E-01 1.625E-01 NOT IDENT. TH-229 -2.685E-01 3.803E-01 3.991E-01 FAIL ABUN PA-231 l.333E-02 3.252E-01 3.252E-01 NOT IDENT. TH-231 3.853E-01 7.401E-01 7.602E-01 FAIL ABUN PA-233 1.786E-02 4.332E-02 4.406E-02 NOT IDENT. PA-234 9.735E-02 2.354E-01 2.394E-01 FAIL ABUN PA-234M 1. 506E+OO 7.329E+OO 7.361E+OO FAIL ABUN U-235 3.018E-02 l.378E-01 1.384E-01 FAIL ABUN NP-237 1. 786E-02 4.332E-02 4.406E-02 NOT IDENT. NP-238 -2. 272E+39 1. 757E+40 O.OOOE+OO SHORT HLIF NP-239 -l.500E-02 1. 7 52E-01 1. 753E-01 NOT IDENT. PU-239 3.395E+02 3.216E+02 3.562E+02 FAIL ABUN AM-241 1.034E-01 9.569E-02 1.064E-01 NOT IDENT. CM-243 -7. OllE-02 7.017E-02 7. 696E-02 NOT IDENT. BK-247 -1.690E-02 5.479E-02 5.532E-02 FAIL ABUN CM-247 -9.582E-03 2.330E-02 2.370E-02 NOT IDENT. CF-249 -1.732E-03 2.671E-02 2. 672E-02 NOT IDENT. CF-251 -2.684E-02 8.977E-02 9.058E-02 NOT IDENT. Page 4722 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 39.5407 87.09 60.4024 136.47 61.2992 45.60 44.7008 87.57 60.4472 140.51 0.0000 46.54 41.9982 88.03 60.4903 143.76 54.2213 49. 72 0.0000 88.34 60.5191 144.24 61. 8463 51. 35 50.9409 88.47 60.5315 145.44 54.3236 51. 87 59.4977 89. 96 60.6697 152.43 55.8373 52.39 69.9641 1093.63 60.7324 153.25 0.0000 52.97 50.1713 91.11 0.0000 323.87 46.0721 53.44 42.6407 92.59 73.0937 156.02 0.0000 54.07 48.3903 93.35 73.1766 158.56 0.0000 57.36 0.0000 94.56 47.5144 159.00 63.9482 57.53 59.2475 94.65 47.5208 162.33 55.3192 57.98 65.0397 94. 67 47.5222 162.66 0.0000 59.27 46.0287 94.87 55.6852 163.33 56.4840 59.32 46.0333 97.43 60.3247 165.86 41.0853 59.54 51.1702 98.43 59.3877 176.31 46.0061 60. 96 61.5757 98.44 '59.3886 176.60 0.0000 61.17 61.6008 99.53 62.5581 177.52 56.1714 62.93 62.7756 100 .11 54.3987 181.07 0.0000 63.29 62.8187 102.03 56.6050 181.52 46.6154 63.58 62.8532 103.18 63.9124 184.41 59.9388 64.28 62.9365 103.37 70.1162 143.76 60.0132 66.73 58.3607 105.21 53.7551 193.51 62.7335 67.24 55.8194 105.31 53.7627 197.03 59.5029 125.81 60. 4111 106.12 53.8226 198.01 52.6842 67.75 60.4187 106.47 47.6351 201.83 42.9058 69.67 78.2312 109.28 67.5676 203.43 43.7340 70.83 64.0209 111. 00 68.7654 205.31 43.0385 72.81 89.1552 111.76 0.0000 210.85 60.2385 72.87 89.1642 114. 06 62.7667 215.65 46.5295 74.66 77.9320 116. 30 0.0000 222 .11 40. 9371 74.82 77.9531 116.74 58.7869 227.09 39.9325 74.97 77.9730 119.76 65. 3372 227.38 48 .16.57 77 .11 78.2568 121.12 58.0598 228.16 0.0000 78.74 78.1391 121.22 58.0674 228.18 44.6710 79.69 77.5983 121.78 64.4472 116.74 44. 6710 80.12 65.7064 122.06 65.5269 235.69 53.6182 80.19 0.0000 122.92 63.4813 235. 96 53.6300 80.57 77.7108 123.07 66.6679 238.63 45.0508 81. 00 79.7589 265.00 66.7183 238.98 0.0000 81. 07 79.7681 125.81 63.7083 240.99 45.1354 81. 75 70.5400 127.23 45.3825 242.00 45.1714 83.79 73.4419 127.91 58.1947 244.70 45.2676 84.00 73.4665 129.30 65.4016 252.40 0.0000 85.43 64.2617 131. 20 54.1503 252.80 35. 9628 86.55 60.3516 133.02 55.6959 254.15 0.0000 86.79 60.3740 133.52 53.5858 256.23 32.4514 86.94 60.3882 136.00 63.4149 260.90 0.0000 Page 4723of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 35.0774 355.39 0.0000 584.27 15.3672 264.80 36.2906 356.01 29.5684 595.83 0.0000 265.00 36.2961 364.49 0.0000 427.87 16.4390 268.22 24.2548 366.42 0.0000 602.52 0.0000 269.46 37.6289 372. 51 29.4263 604. 72 18.8882 270.03 37.6450 375.05 29.4698 607.14 . 29.0881 271.23 40.5141 377.52 25.1720 609.32 15.5273 273.65 0.0000 356.01 22.6506 610.33 15.5339 276.40 43.9200 388.16 27.0727 614.28 10.2103 277.37 34.1831 388.63 0.0000 618.01 16.5559 277.60 40.2943 391.69 24. 5011 620.36 13.1594 278.00 47.6348 264.66 23.7448 621.93 11.7051 279.20 40.3406 401.81 22.8801 630.19 0.0000 279.54 40.3507 402.40 25.5284 631. 2 9 10.2800 279.70 44.0233 404.85 25.5626 633.25 10.2881 280.46 39.1533 410.95 24.7638 634.78 0.0000 283.69 39.2432 413.71 24.8008 635.95 10.2988 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 27.0126 423. 72 0.0000 645.85 15.7546 285.90 0.0000 427.09 32 .1160 657.76 9.8922 287.50 40.5783 427.87 25.8818 657.90 0.0000 290.67 37.7933 433.94 17.9065 661.66 7.9255 293.27 0.0000 439.40 26.9360 664.57 0.0000 351. 93 45.7419 453.88 19'. 9004 666.33 0.0000 295. 96 45.7656 463.37 15.4509 666.50 0.0000 879.38 42.9557 468.07 13.6649 667. 71 0.0000 299.98 31.4208 473.00 0.0000 677.62 22.4258 300.09 31. 4231 475.06 10. 9695 685.70 0.0000 300.13 29.7700 476.78 20.1277 695.00 0.0000 301.36 31.0364 477.60 15.5595 696.49 17.0636 302.85 34.7958 482.18 19.2632 696. 51 17.0636 256.23 23.6381 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 13.0524 306.78 34.8881 497.08 22.1729 697.49 14.0575 308.46 27.4429 505.52 30.0527 702.65 17.1017 311. 90 30.0066 507.63 0.0000 706.68 22.1647 316.51 30.0974 511. 00 27.8976 711. 68 23.2143 319.41 0.0000 514.00 12.5711 720.70 0.0000 320.08 0.0000 514.00 12.5711 721. 93 0.0000 321.04 27.6712 520.40 18.6792 722.78 21. 2803 323.87 30.2417 520.69 0.0000 722.91 19.7610 325.23 39.0972 522.65 0.0000 723.31 19.7642 328.76 0.0000 527.90 0.0000 724.19 21. 2914 333.37 35.4973 528.26 15.9340 727.33 15.2246 333.97 26.6326 529.59 15.9437 733.00 13.7302 334.37 25.3711 529.87 0.0000 735.93 17.3078 338.28 29.6722 531. 02 0.0000 333.97 12.2236 338.32 29.6730 537.26 0.0000 739.50 0.0000 311. 90 29.2884 546.56 0.0000 747.24 13.2878 340.48 29.2884 552.55 14.2120 748.06 9.2018 340.55 0.0000 563.25 20.9419 752.31 13.3110 344.28 24.6776 569.33 18.1333 753.82 0.0000 345.93 28.1096 946.00 19.0894 756.73 11. 2806 351. 06 29.0527 569.70 19. 0'910 756.80 16.4089 351.93 29.0680 583.19 15.3600 884.68 18.5054 Page 4724of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 18.5171 1274.44 9.9412 1620.50 3.8220 766.42 21.6075 1001.03 9.9543 1621. 92 4.7791 766.84 15.4364 1002.74 13.2788 1678.03 0.0000 772.60 0.0000 1004.73 9. 9646 1690.97 1. 9364 776.52 0.0000 507.63 0.0000 1750.46 0.0000 7 39. 5.0 0.0000 1025.87 0. 0000
  • 1764.49 2.9434 778.90 8.2666 1028.54 0.0000 1063.66 10.8033 783.70 0.0000 1037.84 11.1727 1771.35 4. 9115 785.37 10.3556 1038.76 0.0000 1791.20 0.0000 792.07 7.7841 631.29 6. 7197 1808.65 2. 9663 794.95 9.3501 1048.07 0.0000 1810.72 0.0000 795.86 0.0000 1049.04 12.3276 1836.06 5. 9608 810.06 13.5734 1050.41 6.7266 810.29 14.6187 1063.66 12.3759 344.28 12.5308 1077.00 0.0000 810.76 10.4431 1077.34 5.6458 815.77 0.0000 1085.87 9.0534 1048.07 0.0000 1093.63 7.9377 832.01 18.9280 1099.45 10.2209 834.85 16.8405 1112. 07 3.4180 835. 71 15.7922 1112. 84 3.4187 836.80 0.0000 1115. 54 5 .1317 846.75 0.0000 1120.29 1. 7126 846.77 11.6217 1120. 55 1. 7128 856.80 0.0000 1221.41 1. 7130 860.56 6.3667 1129. 67 6.8667 871. 09 11.1785 1131. 51 0.0000 873.19 4.7939 1147.95 0.0000 875.33 0.0000 1173.23 12.1483 879.38 6.4041 1177.95 12.7420 880.51 9.6094 1189.05 20.9063 883.24 8.0145 1204.77 11. 6593 884.68 16.0364 1221.41 12.6422 889.28 6.4236 1231. 02 15.8390 894.76 9.6515 1235.36 0.0000 898.04 5.3672 1238.28 12.6932 900. 72 9.6687 1260.41 0.0000 903.28 10.7515 1271.87 7.9953 911.20 15.0881 1274.44 7 .1113 912.08 15.0920 1274.54 7 .1113 923. 98 0.0000 1291.59. 9.5189 926.50 10.8264 1298.22 0.0000 929 .11 10.8346 1312 .11 0.0000 937.49 19.5505 1332.49 2.7019 944.13 0.0000 1362.66 0.0000 946.00 9.7994 1365.19 8.1645 949.00 17.4368 1368.63 0.0000 667.71 0.0000 1384.29 10.0204 962.31 13.1279 1408.01 5.4935 964.08 9.8511 1457.56 0.0000 966 .17 9.8569 1460.82 8.3320 911.20 9. 8 646 1489.16 4.6558 968.97 9.8646 1505.03 4.4839 983.53 0.0000 1584.12 4.7443 984.45 0.0000 1596.21 0.0000 Page 4725 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:55:27.28 ********************************************************************************
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621364.CNF;l DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM02.CNF;493 Background date : Z-OCT-2016 11:00:01. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 06:55:01. Sample ID G1203621364 Sample quantity 1.74637E+02 GRAM Detector name : GAM02 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.17 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** BACKGROUND CORRECTED SAMPLE PEAK REPORT Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 1 0 53.79 24 53 1.11 107.10 103 9 6.76E-03 57.2 2 0 85.37* 24 75 1. 88 170.21 165 11 6.57E-03 78.1 3 0 92.58* 10 73 1. 20 184.61 179 12 2.65E-03217.2 4 0 126.60 40 50 1. 41 252.59 248 13 1. lOE-02 39. 9 5 0 185.88* 11 63 1.19 371. 05 366 12 3.14E-03165.0 6 0 218.78* 18 35 2142 436.78 429 11 5.02E-03 70.2 7 0 239.41* 9 39 2. 62 478.02 472 10 2.57E-03139.6 8 0 244.18 27 23 2.46 487.54 483 10 7.57E-03 38.9 9 0 482.44 15 9 1. 69 963. 68 959 10 4.17E-03 46.7 10 0 555.89 25 5 3.51 1110. 45 1103 17 7.05E-03 27.3 11 0 566.80 20 16 6.77 1132. 26 1123 17 5.51E-03 52.5 12 0 575.39 14 15 0.97 1149.43 1144 10 3.89E-03 58.2 13 0 611. 24 29 26 6.00 1221.07 1209 21 8.04E-03 48.0 14 4 660.51 17 3 2.58 1319.55 1315 14 4.71E-03 27.1 3.90E-01 15 4 664.00* 4 0 1. 53 1326.50 1315 14 1. 09E-03110. 8 16 0 910.83* 15 0 1. 99 1819.81 1813 13 4.12E-03 33.4 17 0 1000.98* 13 6 2.46 1999.99 1994 13 3.50E-03 56.0 18 0 1382.40 5 3 0.93 2762.36 2755 10 1.25E-03 80.9 19 0 1460.22* 1 0 0.67 2917.92 2913 9 4.15E-04259.9 Flag: "*" = Peak area was modified by background subtraction Page 4 726 of 5809 VMS Nuclide Identification Report V3.1 Generated 3-0CT-2016 07:55:29 Configuration Analyses by Sample title Sample date Sample ID Sample type Detector name : Elapsed.live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621364.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621364 SOLID GAMMA2 0 01:00:00.00 1. 50 keV No Linear 75.00 Acquisition date : Sample quantity Sample geometry : Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 06:55:01 174.64 GRAM CAN 0 01:00:00.17 10.00 0.00 % Peak Energy 0.0% No interference correction performed Page 4727 of 5809 Nuclide Line Activity Report Sample ID : G1203621364 Nuclide Type: Nuclide Energy Area K-40 1460.82 1 AS-73 53.44 36 BA-137M 661. 66 19 CS-137 661.66 19 Flag: "*" Key line Page 4728 of 5809 %Abn 10.66* .. 10.30* 89.90* 85.10* Acquisition date Page : 2 3-0CT-2016 06:55:01 Uncorrected Decay Corr 2-Sigma %Eff pCi/GRAM pCi/GRAM %Error l.060E+OO 5. 571E-02 5.571E-02 519.84. 1. 313E+OO l.138E+OO 1.367E+OO 114. 35 2.018E+OO 4.413E-02 4.419E-02 54.10 2.018E+OO 4.662E-02 4.668E-02 54.10 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:55:29.90
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* *
  • DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621364.CNF;l * *Acquisition date 3-0CT-2016 06:55:01 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.17 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl * *Sample ID G1203621364 Sample Quantity 1.7464E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 5. 571E-02 2.838E-01 5. 964E-01 AS-73 1.367E+OO 1.532E+OO 1.282E+OO BA-137M 4.419E-02 2.343E-02 4.262E-02 CS-137 4.668E-02 2.475E-02 4.502E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM (1. 96-sigma) (pCi/GRAM BE-7 -1.944E-02 2.159E-01 3.844E-01 NOT IDENT. NA-22 -4.508E-03 1.684E-02 3.476E-02 NOT IDENT. NA-24 O.OOOE+OO 5.025E+08 O.OOOE+OO SHORT HLIF AL-26 -4.778E-03 9.364E-03 1.347E-02 NOT IDENT. SC-46 -8. 785E-,03 2.712E-02 4.877E-02 NOT IDENT. V-48 1.598E-03 5.024E-02 1.083E-01 NOT IDENT. CR-51 4.440E-02 2.606E-01 5.402E-01 NOT IDENT. MN-54 -3.990E-03 1. 4 63E-02 3.087E-02 NOT IDENT. C0-56 -1.689E-02 2.526E-02 4.591E-02 NOT IDENT. MN-56 0.000E+OO 1. 496E+41 O.OOOE+OO SHORT HLIF C0-57 1.058E-02 1.374E-02 2.804E-02 NOT IDENT. C0-58 5.046E-03 2.303E-02 5.153E-02 NOT IDENT. FE-59 9.143E-03 3.568E-02 8.935E-02 NOT IDENT. C0-60 -7.938E-03 1. 965E-02 3.736E-02 NOT IDENT. ZN-65 2.152E-02 4.921E-02 l.123E-01 NOT IDENT. GE-68 -3.180E-01 4.597E-01 7.795E-01 NOT IDENT. AS-74 2.008E-02 7.774E-02 1.608E-01 NOT IDENT. SE-75 -l.662E-02 2.789E-02 5.295E-02 NOT IDENT. BR-77 2.297E+Ol 6.285E+Ol 6.937E+Ol FAIL ABUN SR-82 l.660E-02 1.735E-01 3.976E-01 NOT IDENT. RB-83 l.264E-02 4.998E-02 l.034E-01 NOT IDENT. KR-85 -9.343E+OO 6.934E+OO l.095E+Ol NOT IDENT. SR-85 -5.290E-02 3.921E-02 6.190E-02 NOT IDENT. RB-86 -2.477E-01 3.582E-01 6.074E-01 NOT IDENT. Y-88 1.174E-02 2.253E-02 6.267E-02 NOT IDENT. Y-91 1. 026E+OO l.020E+Ol 2.255E+Ol NOT IDENT. Page 4729 of 5809 NB-94 -2.243E-03 l.561E-02 3.332E-02 NOT IDENT. NB-95 -2.880E-02 3.063E-02 5.404E-02 NOT IDENT. NB-95M -2.465E-02 7.095E-02 1.247E-01 NOT IDENT. ZR-95 9.647E-03 4. 518E-02 9.951E-02 NOT IDENT. NB-97 O.OOOE+OO 1.365E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 6.639E+08 O.OOOE+OO SHORT HLIF M0-99 -1.288E+Ol 3.078E+Ol 6.091E+Ol NOT IDENT. TC-99M O.OOOE+OO 4.814E+23 O.OOOE+OO SHORT HLIF RH-101 O.OOOE+OO 4.315E-02 3.057E-02 FAIL ABUN RH-102 5.78.BE-03 3.376E-02 6.982E-02 NOl' IDENT. RU-103 -9.283E-04 2.500E-02 5.063E-02 FAIL ABUN RH-106 -8.160E-02 2.320E-01 4.232E-01 NOT IDENT. RU-106 -8.160E-02 2.320E-01 4.232E-01 NOT IDENT. AG-108M 2.689E-03 l.834E-02 3.780E-02 NOT IDENT. CD-109 9.285E-02 4.402E-01 7.512E-01 NOT IDENT. AG-llOM -1.087E-02 3.257E-02 6.360E-02 NOT IDENT. SN-113 -l.084E-02 2.703E-02 5.139E-02 NOT IDENT. CD-115 -4.043E+Ol 4.939E+Ol 8.276E+Ol NOT IDENT. SN-117M 1.480E-02 4.053E-02 8.772E-02 NOT IDENT. TE-123M 3.055E-03 l.580E-02 3.373E-02 NOT IDENT. SB-124 6.791E-04 3.352E-02 9.229E-02 NOT IDENT. SB-125 -5.414E-02 5.975E-02 1.019E-01 NOT IDENT. TE-125M 1. 756E+OO 6.155E+OO 1.242E+Ol NOT IDENT. I-126 -l.494E-01 1.936E-01 2.883E-01 NOT IDENT. SB-126 2.213E-02 1.246E-01 2. 701E-01 NOT IDENT. SN-126 9.987E-04 4.565E-02 7. 451E-02 NOT IDENT. SB-127 -9.483E-01 2.105E+OO 4.163E+OO NOT IDENT. I-131 5.333E-03 1. 312E...:01 2.645E-01 NOT IDENT. I-132 O.OOOE+OO 1.745E+41 0.000E+OO SHORT HLIF TE-132 -6.675E-01 1.553E+OO 2. 964E+OO NOT IDENT. BA-133 2.143E-02 2.558E-02 5. 727E-02 NOT IDENT. I-133 O.OOOE+OO 4.615E+05 O.OOOE+OO SHORT HLIF CS-134 -5.021E-03 1. 741E-02 3.630E-02 NOT IDENT. CS-135 -1.516E-02 8.665E-02 l.737E-01 NOT IDENT. I-135 O.OOOE+OO 1.943E+22 O.OOOE+OO SHORT HLIF CS-136 7.948E-02 7.613E-02 l.998E-01 NOT IDENT. CE-139 1.834E-03 1.473E-02 3.155E-02 NOT IDENT. BA-140 -9.229E-02 2. 571E-01 4.764E-01 NOT IDENT. LA-140 2.136E-03 5.539E-02 1. 37 6E-01 NOT IDENT. CE-141 -1.843E-02 4.280E-02 7.725E-02 NOT IDENT. CE-143 O.OOOE+OO 1.625E+03 O.OOOE+OO SHORT HLIF CE-144 9.747E-02 l.132E-01 2.405E-01 NOT IDENT. PM-144 1.822E-02 l.935E-02 4.752E-02 NOT IDENT. PR-144 1.382E+OO 1.456E+OO 3.577E+OO NOT IDENT. PM-146 9.452E-03 2.874E-02 5.992E-02 NOT IDENT. ND-147 2.564E-01 4. 965E-01 1. 096E+OO FAIL ABUN PM-147 -1.00lE+Ol 3.947E+02 7.706E+02 NOT IDENT. PM-149 1.498E+02 3.454E+02 7.473E+02 NOT IDENT. EU-150 1.793E-03 1.562E-02 3.223E-02 NOT IDENT. EU-152 -4.121E-04 5.423E-02 1.107E-01 FAIL ABUN GD-153 -4.494E-02 5.592E-02 9. 311E-02 NOT IDENT. EU-154 -1.273E-02 4.756E-02 9.819E-02 NOT IDENT. EU-155 -2.994E-03 6.585E-02 1.279E-01 FAIL ABUN TB-160 -4.000E-02 7.773E-02 1. 472E-01 FAIL ABUN H0-166M 4.181E-03 3.140E-02 6.974E-02 FAIL ABUN TM-171 2.546E+Ol 2.853E+Ol 2.737E+Ol FAIL ABUN HF-172 O.OOOE+OO 2.621E-01 2.176E-01 FAIL ABUN LU-172 -1. 072E-02 2.064E-02 3.900E-02 FAIL ABUN LU-176 -1.089E-02 1. 551E-02 2. 8 63E-02. NOT IDENT. HF-181 4. 972E-02 4.547E-02 7.250E-02 FAIL ABUN TA-182 -4.503E-03 9.393E-02 1. 967E-01 NOT IDENT. RE-183 3.777E-02 1.412E-01 2.799E-01 NOT IDENT. RE-184 3.720E-02 6.880E-02 l.661E-01 NOT IDENT. W-188 1.050E+OO 4.274E+OO 9.014E+OO NOT IDENT. IR-192 -5.557E-03 2.218E-02 4.359E-02 NOT IDENT. HG-203 -3.079E-03 2.066E-02 4.202E-02 NOT IDENT. BI-207 -1.719E-02 2. 621E-02 4.620E-02 NOT IDENT. TL-208 6.255E-03 2.809E-02 5.788E-02 NOT IDENT. PB-210 1.250E+OO 3.459E+OO 7.256E+OO NOT IDENT. BI-211 -5.828E-02 1.288E-01 2.483E-01 NOT IDENT. PB-211 7.507E-02 3. 971E-01 8. 341E-01 NOT IDENT. BI-212 -4.815E-03 3.432E-01 7.092E-01 NOT IDENT. PB-212 2.434E-02 6.659E-02 7.129E-02 FAIL ABUN BI-214 -l.398E-02 6.002E-02 1.156E-01 NOT IDENT. PB-214 -3.079E-02 4.849E-02 9.083E-02 NOT IDENT. RN-219 -l.144E-01 2.448E-01 4.581E-01 NOT IDENT. RN-222 -1.398E-02 6.002E-02 1.156E-01 NOT IDENT. RA-223 -2.105E-01 3.769E-01 7.078E-01 NOT IDENT. Page 4730 of 5809 RA-224 3.746E-02 4.015E-01 6.127E-01 NOT IDENT. RA-226 -1.398E-02 6.002E-02 l.156E-01 NOT IDENT. AC-227 1.090E-01 1.355E-Ol 3.049E-01 NOT IDENT. TH-227 l.090E-01 1.355E-01 3.049E-01 NOT IDENT. AC-228 l.660E-01 1.087E-01 2.516E-01 FAIL ABUN RA-228 l.660E-01 1.087E-01 2.516E-01 FAIL ABUN TH-228 2.434E-02 6.659E-02 7.129E-02 FAIL ABUN TH-229 -l.260E-01 2. 962E-01 5.874E-01 FAIL ABUN TH-230 -1.398E-02 6. OOlE-02 l.156E-01 NOT IDENT. ,PA-231 -l.423E-01 2.615E-01 4.959E-01 NOT IDENT. TH-231 -2.105E-01 3.769E-01 7.078E-01 NOT IDENT. TH-232 1.660E-01 l.087E-01 2.516E-01 FAIL ABUN PA-233 -3.820E-02 3.686E-02 6.412E-02 NOT IDENT. PA-234 -1.267E-02 1.402E-01 3.026E-01 NOT IDENT. PA-234M 4.606E+OO 5.059E+OO 8. 723E+OO FAIL ABUN TH-234 -9.082E-01 9.504E-01 1. 996E+OO FAIL ABUN U-234 -l.398E-02 6.00lE-02 1.156E-01 NOT IDENT. U-235 -6.055E-02 1.285E-01 2.365E-01 FAIL ABUN NP-237 -3.820E-02 3.686E-02 6.412E-02 NOT IDENT. NP-238 O.OOOE+OO 8.274E+Ol O.OOOE+OO SHORT HLIF U-238 -9.082E-01 9.504E-01 1. 996E+OO FAIL ABUN NP-239 1.615E-03 l.228E-01 2. 451E-01 NOT IDENT. PU-239 9.747E+Ol l.808E+02 3.746E+02 NOT IDENT. AM-241 -6.373E-02 9.264E-02 1.745E-01 NOT IDENT. AM-243 -4.628E-02 3.630E-02 6.950E-02 NOT IDENT. CM-243 3. 671E-02 6.795E-02 l.401E-01 NOT IDENT. BK-247 -1.837E-02 4.828E-02 9.417E-02 FAIL ABUN CM-247 -7.784E-03 2.082E-02 3.980E-02 NOT IDENT. CF-249 1.665E-02 2.173E-02 4.970E-02 NOT IDENT. CF-251 -7.601E-02 6.884E-02 l.277E-01 NOT IDENT. ANH-511 -5.082E-02 3.543E-02 7.581E-02 NOT IDENT. Page 4731 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:55:28.01 Nuclide Line Activity Report Nuczlide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi./GRAM pCi/GRAM %Error K-40 1460.82 1 10.66* 1.060E+OO 5.571E-02 5.571E-02 519.84 AS-73 53.44 36 10.30* 1.313E+OO 1,138E+OO 1.367E+OO 114. 35 BA-137M 661.66 19 89.90* 2.018E+OO 4.413E-02 4.419E-02 54.10 CS-137 661.66 19 85.10* 2.018E+OO 4.662E-02 4.668E-02 54.10 Flag: "*" Key line Page 4732of5809 Summary of Nuclide Activity Sample ID : Gl203621364 Acquisition date Page : 2 3-0CT-2016 06:55:01 Total number of lines in spectrum 19 Number of unidentified lines 5 Number of lines tentatively identified by NID 14 Nuclide Type : Nuclide K-40 AS-73 BA-137M CS-137 Hlife l.25E+09Y 80.30D 30.08Y 30.08Y Decay 1. 00 1. 20 1. 00 1. 00 Total Activity Grand Total Activity 'f Uncorrected pCi/GRAM 5.571E-02 l.138E+OO 4.413E-02 4.662E-02 l.284E+OO l.284E+OO Decay Corr pCi/GRAM 5.571E-02 l.367E+OO 4.419E-02 4.668E-02 l.514E+OO l.514E+OO 73.68% Decay Corr 2-Sigma Error 28. 96E-02 l.564E+OO 2.391E-02 2.526E-02 Manually accepted . 2-Sigma %Error 519.84 114. 35 54.10 54.10 Flags: "K" "E" Keyline not found Manually edited "M" "A" Nuclide specific abn. limit Page 4733 of 5809 Flags Unidentified Energy Lines Page : 3 Sample ID : Gl203621364 Acquisition date : 3-0CT-2016 06:55:01 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 85.37 33 105 1. 88 170.21 165 11 6.57E-03 **** 4. 71E+OO T 0 92.58 13 101 1. 20 184.61 179 12 2.65E-03 **** 5.20E+OO T 0 126.60 53 68 1. 41 252.59 248 13 l.lOE-02 79.7 6.16E+OO T 0 185.88 15 80 Ll9 371. 05 366 12 3.14E-03 **** 5. 56EHlO T 0 218.78 23 45 2.42 436.78 429 11 5.02E-03 **** 5.0lE+OO 0 239.41 12 49 2. 62 478.02 472 10 2.57E-03 **** 4.69E+OO T 0 244.18 34 28 2.46 487.54 483 10 7.57E-03 77.9 4.62E+OO T 0 482.44 17 10 1. 69 963.68 959 10 4.17E-03 93.3 2.61E+OO T 0 555.89 28 5 3.51 1110. 45 1103 17 7.05E-03 54.7 2.32E+OO 0 566.80 22 18 6.77 1132.26 1123 17 .5. 51E-03 **** 2.29E+OO 0 575.39 16 17 0.97 1149.43 1144 10 3.89E-03 **** 2.26E+OO 0 611. 24 32 29 6.00 1221.07 1209 21 8.04E-03 96. 0 2.15E+00 T 4 664.00 4 0 1. 53 1326.50 1315 14 l.09E-03 **** 2. OlE+OO T 0 910.83 16 0 1. 99 1819.81 1813 13 4.12E-03 66.8 l.56E+00 T 0 1000.98 13 7 2.46 1999.99 1994 13 3.50E-03 **** 1. 45E+OO T 0 1382.40 4 2 0.93 2762.36 2755 10 l.25E-03 **** l. llE+OO Flags: "T" = Tentatively associated Page 4734of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:55:43.56 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621364.CNF;l *
  • Acquisition date 3-0CT-2016 06:55:01 Sensitivity 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: O 01:00:00.17 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID Gl203621364 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity : 1.7464E+02 GRAM *
  • wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * * *
  • CALIBRATION INFORMATION * *
  • Eff. Cal. date 22-AUG-2016 09:02:05 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;l5
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 AS-73 BA-137M CS-137 Le (pCi/GRAM 2.460E-01 5.810E-01 1. 796E-02 1. 8 97E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 ZN-65 GE-68 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 Page 4735 of 5809 Le (pCi/GRAM 1.628E-01 1.232E-02 0.000E+OO O.OOOE+OO 1.989E-02 4.387E-02 2.413E-01 l.167E-02 l.855E-02 O.OOOE+OO 1.273E-02 2.141E-02 3.373E-02 l.348E-02 4.674E-02 2.464E-01 6. 962E-02 2.371E-02 3.180E+Ol 1. 584E-01 4.516E-02 4.905E+OO 2.773E-02 1.920E-01 2.346E-02 8.915E+OO 1. 350E-02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT.

NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RU-103 RH-106 RU-106 AG-108M CD-109 AG-llOM SN-113 CD-115 SN-ll 7M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 PB-210 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 RA-224 Page 4736 of 5809 2.278E-02 5.565E-02 4.204E-02 O.OOOE+OO 0.000E+OO 2.462E+Ol 0.000E+OO 1.374E-02 2. 968E-02 2.147E-02 l.816E-01 l.816E-01 l.653E-02 3.389E-01 2.632E-02 2.223E-02 3.443E+Ol 4.023E-02 1.543E-02 2.917E-02 4.371E-02 5.689E+OO 1.153E-01 1.153E-01 3.367E-02 1.692E+OO 1.179E-01 O.OOOE+OO 1.334E+OO 2.568E-02 O.OOOE+OO 1. 401E-02 7.778E-02 O.OOOE+OO 8.352E-02 1.428E-02 2.048E-01 4.874E-02 3.523E-02 0.000E+OO l.105E-01 2.049E-02 1.543E+00 2. 651E-02 4.738E-01 3.481E+02 3.344E+02 1. 431E-02 4.864E-02 4.223E-02 3.479E-02 5.862E-02 5.837E-02 2.899E-02 1.244E+Ol 9.941E-02 1.233E-02 l.259E-02 3.213E-02 7.807E-02 l.271E-01 6.784E-02 4. 031E+OO l.935E-02 l.848E-02 1. 729E-02 2.574E-02 3.336E+OO l.102E-01 3.633E-01 3.061E-01 3.259E-02 5.161E-02 4.033E-02 1. 984E-01 5.161E-02 3 .115E-01 2.736E-01 NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT.HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-241 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 4737of5809 5.161E-02 l.377E-01 1.377E-01 1.109E-01 l.109E-01 3.259E-02 2.674E-01 5 .161E-02 2 .181E-01 3 .115E-01 l.109E-01 2.780E-02 1.184E-01 3.871E+OO 9.271E-01 5.161E-02 l.088E-01 2.780E-02 O.OOOE+OO 9.271E-01 l.092E-01 1. 709E+02 7.825E-02 3.219E-02 6.467E-02 4.229E-02 1. 709E-02 2.188E-02 5.745E-02 3.546E-02 NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT .* FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:55:49.45 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621364.CNF;l *
  • Acquisition date 3-0CT-2016 06:55:01 Sensitivity : 3.000 *
  • Detector ID GAM02 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 01:00:00.17 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621364 Analyst initials: MXRl * *Batch Number 1596254 Sample Quantity : 1.7464E+02 GRAM *
  • Quantity Err ( % ) : 1. 1452E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 22-AUG-2016 09: 02: 05 Eff. Geometry . : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM02 CAN.CNF;15
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) K-40 5. 571E-02 2.838E-01 2.838E-01 AS-73 1. 367E+00 1.558E+OO 1.558E+OO BA-137M 4.419E-02 2. 351E-02 2.351E-02 CS-137 4.668E-02 2.483E-02 2.483E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1 . 96-sigma ) ( 1 . 96-sigma ) BE-7 -1.944E-02 2.159E-01 2.161E-01 NOT IDENT. NA-22 -4.508E-03 1.684E-02 1. 696E-02 NOT IDENT. NA-24 -4.273E+07 5.025E+08 5.029E+08 SHORT HLIF AL-26 -4.778E-03 9.369E-03 9.614E-03 NOT IDENT. SC-46 -8.785E-03 2.713E-02 2.741E-02 NOT IDENT. V-48 1.598E-03 5.024E-02 5.024E-02 NOT IDENT. CR-51 4.440E-02 2.606E-01 2.614E-01 NOT ID'ENT. MN-54 -3.990E-03 1.463E-02 1. 474E-02 NOT IDENT. C0-56 -1.689E-02 2.527E-02 2.639E-02 NOT IDENT. MN-56 -1.000E+41 1. 496E+41 O.OOOE+OO SHORT HLIF C0-57 1.058E-02 1.375E-02 1.455E-02 NOT IDENT. C0-58 5.046E-03 2.303E-02 2.314E-02 NOT IDENT. FE-59 9.143E-03 3.569E-02 3.592E-02 NOT IDENT. C0-60 -7.938E-03 1. 965E-02 1.997E_..:02 NOT IDENT. ZN-65 2.152E-02 4.922E-02 5.016E-02 NOT IDENT. GE-68 -3.180E-01 4.599E-01 4.817E-01 NOT IDENT. AS-74 2.008E-02 7.776E-02 7. 828E.:..02 NOT IDENT. SE-75 -1.662E-02 2.790E-02 2.889E-02 NOT IDENT. BR-77 2.297E+Ol 6.442E+Ol 6.525E+Ol FAIL ABUN SR-82 1.660E-02 1. 735E-01 1.737E-01 NOT IDENT. RB-83 1.264E-02 5.00lE-02 5.033E-02 NOT IDENT. KR-85 -9.343E+OO 6.945E+OO 8.122E+OO NOT IDENT. SR-85 -5.290E-02 3.927E-02 4.594E-02 NOT IDENT. RB-86 -2.477E-01 3.583E-01 3.753E-01 NOT IDENT. Y-88 1.174E-02 2.255E-02 2.316E-02 NOT IDENT. Y-91 1.026E+OO 1.020E+Ol 1.021E+Ol NOT IDENT. Page 4738 of 5809 NB-94 -2.243E-03 1.561E-02 1.564E-02 NOT IDENT. NB-95 -2.880E-02 3.065E-02 3.329E-02 NOT IDENT. NB-95M -2.465E-02 7.098E-02 7.184E-02 NOT IDENT. ZR-95 9.647E-03 4.518E-02 4.539E-02 NOT IDENT. NB-97 -1.000E+41 1. 366E+41 O.OOOE+OO SHORT HLIF ZR-97 -1. 24 7E+09 6.659E+08 8.715E+08 SHORT HLIF M0-99 -1.288E+Ol 3.079E+Ol 3.133E+Ol NOT IDENT. TC-99M 2.887E+22 4.814E+23 0.000E+OO SHORT HLIF RH-101 5.523E-02 4.427E-02 5.079E-02 FAIL ABUN RH-102 5.788E.;--03 3.377E-02 3.387E-02 NOT IDENT. RU-103 -9.283E-04 2.500E-02 2.500E-02 FAIL ABUN RH-106 -8.160E-02 2.320E-01 2.349E-01 NOT IDENT. RU-106 -8.160E-02 2.320E-01 2.349E-01 NOT IDENT. AG-108M 2.689E-03 l.834E-02 l.838E-02 NOT IDENT. CD-109 9.285E-02 4.402E-01 4.422E-01 NOT IDENT. AG-110M -1.087E-02 3.257E-02 3.294E-02 NOT IDENT. SN-113 -1. 084E-02 2.704E-02 2.747E-02 NOT IDENT. CD-115 -4.043E+Ol 4.945E+Ol 5.270E+Ol NOT IDENT. SN-117M 1.480E-02 4.053E-02 4.108E-02 NOT IDENT. TE-123M 3.055E-03 l.580E-02 l.586E-02 NOT IDENT. SB-124 6. 7 91E-04 3.352E-02 3.352E-02 NOT IDENT. SB-125 -5.414E-02 5.979E-02 6.457E-02 NOT IDENT. TE-125M 1. 756E+OO 6.155E+OO 6.206E+OO NOT IDENT. I-126 -1.494E-01 1.939E-01 2.052E-01 NOT IDENT. SB-126 2. 213E-02 l.246E-01 1.250E-01 NOT IDENT. SN-126 9.987E-04 4.565E-02 4.566E-02 NOT IDENT. SB-127 -9.483E-01 2.108E+OO 2 .151E+OO NOT IDENT. I-131 5.333E-03 1.312E-OI 1.312E-01 NOT IDENT. I-132 -l.OOOE+41 2.185E+41 O.OOOE+OO SHORT HLIF TE-132 -6.675E-01 1.554E+OO 1.583E+OO NOT IDENT. BA-133 2.143E-02 2.559E-02 2.735E-02 NOT IDENT. I-133 5. 962E+05 4.695E+05 5.409E+05 SHORT HLIF CS-134 -5. 021E-03 l.741E-02 1. 756E-02 NOT IDENT. CS-135 -l.516E-02 8.666E-02 8.693E-02 NOT IDENT. I-135 -9.856E+21 2.001E+22 O.OOOE+OO SHORT HLIF CS-136 7.948E-02 7.641E-02 8.440E-02 NOT IDENT. CE-139 l.834E-03 l.474E-02 l.476E-02 NOT IDENT. BA-140 -9.229E-02 2.571E-01 2.604E-01 NOT IDENT. LA-140 2.136E-03 5.539E-02 5.539E-02 NOT IDENT. CE-141 -l.843E-02 4.281E-02 4.361E-02 NOT IDENT. CE-143 l.270E+03 1. 62 6E+03 l.724E+03 SHORT HLIF CE-144 .9.747E-02 1.133E-01 l.216E-01 NOT IDENT. PM-144 l.822E-02 1.936E-02 2.103E-02 NOT IDENT. PR-144 l.382E+OO 1.457E+OO 1.585E+OO NOT IDENT. PM-146 9.452E-03 2.875E-02 2.907E-02 NOT IDENT. ND-147. 2.564E-01 4. 967E-01 5.lOOE-01 FAIL ABUN PM-147 -1.00lE+Ol 3.947E+02 3.947E+02 NOT IDENT. PM-149 1.498E+02 3.460E+02 3.525E+02 NOT IDENT. EU-150 1. 793E-03 l.562E-02 1.564E-02 NOT IDENT. EU-152 -4 .121E-04 5.423E-02 5.423E-02 FAIL ABUN GD-153 -4.494E-02 5.598E-02 5.953E-02 NOT IDENT. EU-154 -l.273E-02 4.756E-02 4.790E-02 NOT IDENT. EU-155 -2.994E-03 6.585E-02 6.587E-02 FAIL ABUN TB-160 -4.000E-02 7.776E-02 7.983E-02 FAIL ABUN H0-166M 4.181E-03 3.140E-02 3.145E-02 FAIL ABUN TM-171 2.546E+Ol 2.862E+Ol 3.084E+Ol FAIL ABUN HF-172 3.355E-01 2.677E-01 3.075E-01 FAIL ABUN LU-172 -1. 072E-02 2.067E-02 2.122E-02 FAIL ABUN LU-176 -1. 089E-02 1. 551E-02 1.627E-02 NOT IDENT. HF-181 4 .'972E-02 4.552E-02 5.074E-02 FAIL ABUN TA-182 -4.503E-03 9.393E-02 9.395E-02 NOT IDENT. RE-183 3.777E-02 l.413E-01 l.423E-01 NOT IDENT. RE-184 3. 720E-02 6.885E-02 7.087E-02 NOT IDENT. W-188 l.050E+OO 4.276E+OO 4.302E+OO NOT IDENT. IR-192 -5.557E-03 2.218E-02 2.232E-02 NOT IDENT. HG-203 -3.079E-03 2.066E-02 2.071E-02 NOT IDENT. BI-207 -1. 719E-02 2.622E-02 2.734E-02 NOT IDENT. TL-208 6.255E-03 2.809E-02 2.823E-02 NOT IDENT. PB-210 1.250E+OO 3.461E+OO 3.506E+OO NOT IDENT. BI-211 -5.828E-02 l.288E-01 1.315E-01 NOT IDENT; PB-211 7.507E-02 3.971E-01 3.986E-01 NOT IDENT. BI-212 -4.815E-03 3.432E-01 3.432E-01 NOT IDENT. PB-212 2.434E-02 6.660E-02 6.750E-02 FAIL ABUN BI-214 -l.398E-02 6.002E-02 6.035E-02 NOT IDENT. PB-214 -3.079E-02 4.851E-02 5.045E-02 NOT IDENT. RN-219 -l.144E-01 2.452E-01 2.506E-01 NOT IDENT. RN-222 -l.398E-02 6.002E-02 6.035E-02 NOT IDENT. RA-223 -2.105E-01 3. 772E-Ol 3.889E-01 NOT IDENT. Page 4739of5809 RA-224 3.746E-02 4.016E-01 4.019E-01 NOT IDENT. RA-226 -l.398E-02 6.002E-02 6.035E-02 NOT IDENT. AC-227 1.090E-01 1.363E-01 1.448E-01 NOT IDENT. TH-227 l.090E-01 1. 363E-01 1.448E-01 NOT IDENT. AC-228 l.660E-01 1.090E-01 l.323E-01 FAIL ABUN RA-228 l.660E-01 1.090E-01 l.323E-01 FAIL ABUN TH-228 2.434E-02 6.660E-02 6.750E-02 FAIL ABUN TH-229 -1.260E-01 2.963E-01 3.017E-01 FAIL ABUN TH-230 -1.398E-02 6.002E-02 6.035E-02 NOT IDENT. PA-231 -1.423E-OJ. 2.632E-01 2.709E-01 NOT IDEN:i'. TH-231 -2.105E-01 3. 772E-01 3.889E-01 NOT IDENT. TH-232 l.660E-01 l.090E-01 l.323E-01 FAIL ABUN PA-233 -3.820E-02 3.690E-02 4.072E-02 NOT IDENT. PA-234 -l.267E-02 l.410E-01 1. 411E-01 NOT IDENT. PA-234M *4. 606E+OO 5.063E+OO 5.472E+OO FAIL ABUN TH-234 -9.082E-01 9. 715E-01 1.054E+OO FAIL ABUN U-234 -1.398E-02 6.002E-02 6.035E-02 NOT IDENT. U-235 -6.055E-02 1.285E-01 l.314E-01 FAIL ABUN NP-237 -3.820E-02 3.690E-02 4.072E-02 NOT IDENT. NP-238 4.701E+Ol 8.277E+Ol 8.544E+Ol SHORT HLIF U-238 -9.082E-01 9.715E-01 1.054E+OO FAIL ABUN NP-239 1.615E-03 1. 228E-01 1.228E-01 NOT IDENT. PU-239 9.747E+Ol l.809E+02 1. 8 61E+02 NOT IDENT. AM-241 -6.373E-02 9.276E-02 9.711E-02 NOT IDENT. AM-243 -4.628E-02 3.641E-02 4 .196E-02 NOT IDENT. CM-243 3. 671E-02 6.804E-02 7.002E-02 NOT IDENT. BK-247 -1.837E-02 4.843E-02 4.913E-02 FAIL ABUN CM-247 -7.784E-03 2.086E-02 2 .115E-02 NOT IDENT. CF-249 l.665E-02 2.177E-02 2.303E-02 NOT IDENT. CF-251 -7.601E-02 6.937E-02 7.737E-02 NOT IDENT. ANH-511 -5.082E-02 3.549E-02 4.224E-02 NOT IDENT. Page 4740 of 5809
  • GEL Laboratories LLC *
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  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 36.5939 87.09 26.9562 136.47 42.5201 45.60 29.6539 87.57 29.2288 140.51 25.6527 46.54 31.7827 88.03 24.7530 143.76 39.2598 49.72 28.9574 88.34 24.7673 144.24 39.2847 51. 35 29.0826 88.47 29.2774 145.44 44.2656 51. 87 20.8015 89. 96 29.3573 152.43 28.5377 52.39 22.2183 1093.63 27.1326 153.25 42.2302 52.97 31.2912 91.11 27.1556 323.87 28.6022 53.44 31.3289 92.59 27.2280 156.02 43.6240 54.07 31.3792 93.35 27.2650 158.56 35.0103 57.36 0.0000 94.56 31. 8773 159.00 35.8631 57.53 21.1003 94.65 31. 8824 162.33 28.4731 57.98 28.1644 94.67 31.8835 162.66 31. 8356 59.27 38.1403 94.87 31. 8946 163.33 27.6692 59.32 38.1448 97.43 36.6140 165.86 28.5948 59.54 36.0446 98.43 28.6539 176.31 30.6511 60. 96 48.9305 98.44 28.6545 176.60 34.0682 61.17 47.8903 99.53 27. 5596 177.52 44.3352 62.93 35.2634 100.11 25.2878 181.07 30.8177 63.29 33.1536 102.03 39.2080 181.52 44.9655 63.58 27.8248 103.18 45.0601 184.41 22.3408 64.28 38.5880 103.37 38 .1399 143.76 22.3734 66.73 32.3339 105.21 41. 7335 193.51 41.6577 67.24 35.6073 105.31 41.7404 197.03 31.3612 125.81 39.9620 106.12 41. 7958 198.01 34.8820 67.75 39.9680 106.47 39.4964 201.83 38.5251 69.67 21.6949 109.28 35.0079 203.43 33. 3269 70.83 52 .1971 111. 00 38.6142 205.31 35.1493 72.81 43.6798 111. 76 38.6605 210.85 30.9305 72. 87 43.6853 114. 06 32.9212 215.65 25.3083 74.66 51.5214 116. 30 34.2150 222 .11 24.1295 74.82 51.5382 116. 74 22.4319 227.09 34.1244 74.97 50.4574 119.76 29.6511 227.38 36. 8284 77 .11 52.8809 121.12 29.7115 228.16 29.6646 78.74 24.3163 121.22 29.7159 228.18 29.6652 79.69 43.1874 121. 7 8 28.5511 116.74 29.6652 80.12 42 .1157 122.06 20.6288 235.69 28.5187 80.19 43.2299 122.92 17.4773 235. 96 28.5260 80.57 39.9342 123.07 17.4812 238.63 21. 7881 81. 00 32.5665 265.00 23.8594 238.98 21. 7952 81. 07 32. 5710 125.81 27.5239 240.99 21. 8357 81. 75 26.6841 127.23 27.5804 242.00 21.8560 83.79 35. 7190 127.91 27.6077 244.70 17.8020 84.00 35.7332 129.30 27.6624 252.40 25.7396 85.43 35.8301 131. 20 32.1590 252.80 24.8291 86.55 .35.9055 133.02 30.2265 254.15 0.0000 86.79 35.9216 133.52 27.8277 256.23 18.4479 86.94 26.9487 136.00 43.7064 260.90 22.2280 Page 4741of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.66 33.4504 355.39 0.0000 584.27 12.4820 264.80 31.5962 356.01 14.9521 595.83 11. 4095 265.00 31.6018 364.49 22.0577 427.87 17.1521 268.22 27.0288 366.42 18.0707 602.52 0.0000 269.46 28.9231 372.51 14 .1128 604. 72 10.3107 270.Q3 28.0035 375.05 19.1855. 607.14 14.9101 271.23 23.3602 377.52 17.1940 609.32 14.9249 273.65 30.8986 356.01 16.2500 610.33 14.9318 276.40 24.4004 388.16 10.1849 614.28 13.8081 277.37 27.2377 388.63 9.1692 618.01 8.6447 277.60 27.2430 391.69 18.3746 620.36 11.5385 278.00 29.1312 264.66 16.4268 621. 93 16.1659 279.20 19.7537 401.81 19.5211 630.19 0.0000 279.54 20.7002 402.40 16.4447 631.29 9.2764 279.70 19.7618 404.85 13.3819 633.25 12.7662 280.46 17.8910 410.95 12.3997 634.78 10.4520 283.69 26.4357 413. 71 11. 3858 635.95 6.9717 284.31 23.6155 414.70 19.6784 636.99 9.2998 285.41 17.0182 423. 72 15.6216 645.85 7.8775 285.90 18.9168 427.09 17.7405 657.76 19.7080 287.50 20.8354 427.87 22. 9695 657.90 0.0000 290.67 20.8886 433.94 14.6699 661.66 9.6945 293.27 0.0000 439.40 16.8200 664.57 0.0000 351. 93 21.9177 453.88 15.9024 666.33 12. 7165 295. 96 25.7448 463.37 10.6594 666.50 12.7173 879.38 15.2878 468.07 14.9627 667.71 0.0000 299.98 17.2178 473.00 17.1475 677.62 6. 2113 300.09 17.2192 475.06 8.5837 685.70 9.7939 300 .13 17.2196 476.78 7.7326 695.00 11. 6194 301.36 24.8971 477.60 11.2819 696. 49 5.3661 302.85 25.8843 482.18 14.0035 696. 51 5.3661 256.23 17.2786 487.02 11. 3404 697.00 6.2617 304.85 14.4028 492.35 10.8317 697.30 7.1572 306.78 26.9250 497.08 10.8594 697.49 7.1577 308.46 22.1455 505.52 13.0901 702.65 7.1729 311. 90 23.1694 507.63 0.0000 706.68 8.0829 316.51 24.2198 511. 00 20.7861 711. 68 7.1995 319.41 25.2436 514.00 48.2123 720.70 9.9355 320.08 21.3702 514.00 48.2123 721. 93 0.0000 321.04 23.3301 520.40 13.1924 722.78 12.6555 323.87 25.3271 520.69 13 .1948 722. 91 12.6563 325.23 22.4277 522.65 0.0000 723.31 13.5626 328.76 23.4634 527.90 16.5546 724.19 14.4717 333.37 19.6187 528.26 14.3499 727.33 13. 5841 333.97 19.6273 529.59 4.4185 733.00 21.7844 334.37 29.4495 529.87 0.0000 735.93 5.4523 338.28 12.7977 531.02 8.8434 333.97 10. 9113 338.32 12.7979 537.26 16.6339 739.50 9.1000 311. 90 18.7337 546.56 0.0000 747.24 2.7383 340.48 18.7337 552.55 10.0569 748.06 7.3044 340.55 18.7344 563.25 11. 2333 752.31 8.2312 344.28 17.7957 569.33 11.2667 753.82 4.5757 345.93 17.8165 946.00 11. 2675 756.73 8.2452 351.06 17.8810 569.70 11. 2687 756.80 8.2455 351.93 20.8735 583.19 12.4757 884.68 10.1057 Page 4742 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 14.7100 1274.44 6.3695 1620.50 3.7273 766.42 13.7938 1001.03 7.9736 1621. 92 4.6606 766.84 11. 9562 1002.74 4.7868 1678.03 0.0000 772.60 0.0000 1004.73 6.3863 1690.97 0.9454 776.52 4.6156 507.63 0.0000 1750.46 0.0000 739.50 8.3125 0.0000 1764.49 O.OQOO 778.90 6.4677 1028.54 0.0000 1063.66 3.8408 783.70 8.3307 1037.84 5.0397 1771. 35 2.8812 785.37 5.5573 1038.76 0.0000 1791.20 0.0000 792.07 4.6426 631.29 6.0637 1808.65 0. 967 3 794.95 7.4363 1048.07 2.0221 1810.72 0.0000 795.86 5.5790 1049.04 5.0568 1836.06 0.9723 810.06 8.4125 1050.41 7.0825 810.29 10.2830 1063.66 7 .1102 344.28 10.2836 1077.00 4.0789 810.76 6.5448 1077.34 4.0793 815.77 7.4934 1085.87 6.1340 1048.07 8.4386 1093.63 3.0740 832.01 1.8844 1099.45 2.0527 834.85 4. 7159 1112. 07 8.2402 835.71 6.6042 1112. 84 8.2422 836.80 0.0000 1115. 54 5.1553 846.75 0.0000 1120.29 7.2273 846.77 11.3661 1120.55 6.1952 856.80 11.4064 1221.41 4.1309 860.56 4.7589 1129. 67 6.2109 871.09 7.6421 1131.51 0.0000 873.19 6.6917 1147.95 0.0000 875.33 0.0000 1173.23 5.2383 879.38 8.6221 1177.95 4.1960 880.51 9.5837 1189.05 2.1044 883.24 5.7556 1204.77 4.2266 884.68 10.5572 1221. 41 5.3064 889.28 7.6899 1231. 02 8. 5117 894.76 9.6304 1235.36 5.3259 898.04 2.8923 1238.28 8.5278 900.72 6.7548 1260.41 0.0000 903.28 3. 3114 1271.87 1.0752 911.20 4.8419 1274.44 3.2278 912.08 4. 6496 1274.54 3.2278 923.98 0.0000 1291.59 7.5640 926.50 6.8131 1298.22 0.0000 929 .11 8. 7 671 1312 .11 4.3445 937.49 6.8376 1332.49 4.3665 944.13 3.9156 1362.66 0.0000 946.00 4.8976 1365.19 3.3008 949.00 7.8438 1368.63 0.0000 667.71 0.0000 1384.29 0.0000 962. 31 11. 8158 1408.01 5.5576 964. 08 6.8966 1457.56 0.0000 966 .17 8.8728 1460.82 7.5008 911.20 6.9073 1489.16 5.4352 968.97 6.9073 1505.03 3.6361 983.53 5.9478 1584.12 3.6990 984.45 0.0000 1596.21 1.8542 Page 4743 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:56:49.47 ******************************************************************************** *
  • GEL Laboratories LLC * *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621365.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM19.CNF;561 Background date : Z-OCT-2016 11:01:07. Sample date 14-DEC-2015 13:47:00 Acquisition date : 3-0CT-2016 06:55:29. Sample ID G1203621365 Sample quantity l.44233E+02 GRAM Detector name : GAM19 Detector geometry: CAN Elapsed live time: 0 01:00:00.00 Elapsed real time: 0 01:00:00.73 0.0% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 0 0 1 1 4 4 4 0 0 2 2 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1 1 Page 4744of5809 Energy 45.95* 63.18* 74.70* 77.06* 84.16 89.71 92.57* 185.85* 209.01 238.58* 241. 79 249.44 270.58 295.21* 300.44 338.26 351.72* 462 .11 497.26 510.51* 543.22 569.45* 583.21* 586.97 609.28* 661. 7 9 727. 31 768.94 836.78 861.57 911.26* 933.90 965.03 968. 91 BACKGROUND CORRECTED SAMPLE PEAK REPORT Area 19 22 123 224 45 66 96 45 11 342 88 31 22 161 16 74 302 43 15 22 19 26 86 12 229 54 33 32 14 24 62 22 21 76 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 101 136 154 123 203 174 151 159 174 80 70 43 75 84 72 76 56 45 31 59 15 42 34 8 17 17 27 25 18 29 38 9 0 .o 0.65 1. 26 1. 30 1. 20 1. 76 1. 66 1. 57 0.94 0.74 1.15 1. 72 1. 53 1. 41 1. 40 1. 91 1. 37 1.23 2.01 1. 37 1. 94 0. 67 1.24 1.17 1. 42 1. 44 1. 88 1. 01 0.80 0.92 0.72 1. 22 1. 06 2.13 2.08 92.68 127.14 150.19 154.93 169.12 180.22 185.95 372.59 418.93 478.10 484.52 499.81 542.12 591.40 601.87 677.53 704.46 925.34 995.67 1022.19 1087.64 1140.12 1167. 65 1175.17 1219.80 1324.87 1455.97 1539.27 1675.00 1724.60 1824.03 1869.33 1931. 61 1939.39 90 123 145 145 162 162 162 368 411 472 472 496 538 584 597 671 697 918 991 1014 1085 1133 1163 1173 1213 1318 1449 1532 1670 1715 1817 1865 1922 1922 7 5.28E-03 92.4 8 6.21E-03 96.0 15 3.41E-02 19.7 15 6.24E-02 11.0 33 1. 2 6E-02 61. 7 33 1.83E-02 41.0 33 2.66E-02 26.9 11 1.24E-02 58.3 13 3.15E-03242.0 24 9.49E-02 6.9 24 2.44E-02 26.4 8 8.71E-03 40.1 8 6.18E-03 70.9 14 4.48E-02 14.6 8 4.38E-03 96.6 11 2.05E-02 25.8 14 8.40E-02 7.9 14 1.18E-02 36.9 10 4.15E-03 75.5 15 6 .14E-03 91. 3 7 5.18E-03 42.1 14 7.12E-03 73.5 11 2.39E-02 17.2 5 3.19E-03 46.3 14 6.35E-02 7.8 14 l.49E-02 21.4 11 9.lOE-03 35.6 16 8.88E-03 38.7 9 3.77E-03 62.8 17 6.53E-03 57.0 14 l.71E-02 25.4 11 6.16E-03 33.0 27 5.93E-03 29.6 27 2.lOE-02 10.9 Fit 2.57E+OO 2.64E+OO 2.50E+00 2.62E+OO Peak Search Report (continued) Page : 2 Sample ID : Gl203621365 Acquisition date 3-0CT-2016 06:55:29 Pk It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err Fit 35 0 1063.56* 30 13 1. 86 2128.76 2123 14 8.38E-03 48.3 36 4 1116. 62 13 0 1. 81 2234.94 2233 17 3.48E-03 26.5 1.50E+OO 37. 4 1119. 81 30 0 1. 49 2241.32. 2233 17 8.47E-03 21. 5 38 4 1122.38 12 0 1. 51 2246.45 2233 17 3.33E-03 37.3 39 0 1179.51 15 9 2.65 2360.78 2356 11 4.22E-03 44.9 40 0 1224.88 10 4 2.01 2451.55 2448 8 2.78E-03 46.9 41 1 1238.18 24 12 2.28 2478.15 2474 22 6.76E-03 30.5 2.35E+OO 42 1 1242.81 18 12 2.29 2487.42 2474 22 5.08E-03 52.2 43 0 1279.83 19 3 1. 04 2561. 49 2554 14 5.16E-03 31. 5 44 0 1372.91 9 7 3.78 2747.75 2742 12 2.53E-03 63.9 45 0 1377. 71 13 4 1. 98 2757.35 2753 8 3. 61E-03 38.5 46 0 1460.64 294 4 2.14 2923.28 2915 14 8.16E-02 6.0 47 0 1594.69 8 7 0.57 3191.49 3186 9 2.33E-03 65.4 48 0 1727.95 15 4 5.08 3458.13 3450 16 4.29E-03 38.3 49 0 1764.32* 28 0 2.36 3530.91 3524 13 7.73E-03 20.5 50 0 1769.74* 2 0 1. 00 3541. 7 5 3538 8 6.87E-04146.4 Flag: "*" = Peak area was modified by background subtraction Page 4745of5809 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 07:56:51 Configuration Analyses by DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621365.CNF;l PEAK Vl6.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4,INTERF V2.4 MXRl Sample title Sample date Sample ID 14-DEC-2015 13:47:00 G1203621365 Acquisition date : Sample quantity Sample geometry : 3-0CT-2016 06:55:29 144.23 GRAM Sample type Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit SOLID GAMMA19 0 01:00:00.00 1. 50 keV No Linear 75.00 Interference Report Interfering Nuclide Line PB-214 242.00 PB-214 74.82 PB-214 74.82 PB-214 74.82 PB-214 74'.82 PB-214 351. 93 Page 4746 of 5809 Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at Interfered Nuclide Line RA-224 240.99 AM-243 74.66 TH-228 74.82 PB-212 74.82 BI-207 74.97 BI-211 351.06 CAN 0 01:00:00.73 10.00 0.00 % Peak Energy 0.0%

Nuclide Line Activity Report Page : 2 Sample ID : Gl203621365 Acquisition date 3-0CT-2016 06:55:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status K-40 1460.82 10.66* l .1.61E+OO l.188E+Ol l.188E+Ol 11. 99 OK. ZN-65 1115.54 50.60* l.441E+00 8.816E-02 2.030E-01 52.99 OK RU-103 497.08 91.00* 2.722E+OO 3.336E-02 5. 963E+OO 151.06 OK 610.33 5.76 2.310E+00 9.336E+OO l.669E+03 15.63 OK BA-137M 661. 66 89.90* 2.163E+00 l.491E-01 l.519E-01 42.77 OK CS-137 661. 66 85.10* 2.163E+OO l.575E-01 l.605E-01 42.77 OK BI-207 72. 81 21. 40 4.355E+OO Line Not Found Absent 74.97 35.70 4.533E+00 2.940E-Ol 2.991E-01 68.56 OK 569.70 97.76 2.438E+OO 5.876E-02 5.976E-02 147.08 OK 1063.66 74.60* l.497E+OO l.394E-01 l.417E-01 96.53 OK 1770.23 6.87 9.835E-01 l.796E-01 l.827E-01 292.76 OK TL-208 277.37 6.60 4.415E+OO Line Not Found Absent 583.19 85.00* 2.392E+OO 2.305E-01 2.305E-01 34.42 OK 860.56 12.50 1. 761E+OO 5. 621E-01 5. 621E-01 113. 91 OK PB-210 46.54 4.25* 8.307E-01 3.608E+OO 3.700E+OO 184.75 OK BI-211 72. 87 1. 23 4.361E+OO Line Not Found Absent 351.06 12.92* 3.631E+OO 3.461E-01 3.461E-01 327.17 OK PB-212 74.82 10.28 4.533E+OO l.021E+OO l.021E+OO 68.56 OK 77 .11 17 .10 4.743E+OO l.785E+OO 1. 785E+OO 21. 98 OK 238.63 43.60* 4. 960E+OO 9.313E-01 9.313E-01 13.80 OK 300.09 3.30 4 .138E+OO 6. 672E-01 6.672E-01 193.28 OK BI-214 609.32 45.49* 2.310E+OO l.182E+OO l.183E+OO 15.63 OK 1120.29 14.92 l.437E+OO 7.298E-01 7. 301E-01 43.01 OK 1764.49 15.30 9.862E-01 9.052E-01 9.055E-01 41. 00 OK PB-214 74.82 5.80 4.544E+OO Line Not Found <<INT Reject 77 .11 9.70 4.743E+OO 3.147E+OO 3.148E+OO 21. 98 OK 87.09 3.41 5.478E+OO Line Not Found Absent 242.00 7.25 4.908E+OO Line Not Found <<INT Reject 295.22 18.42 4.198E+OO l.209E+OO l.209E+OO 29.23 OK 351. 93 35.60* 3.629E+OO Line Not Found <<INT Reject RN-222 609.32 45.49* 2.310E+OO l.182E+OO l.183E+OO 15.63 OK 1120.29 14.92 l.437E+OO 7.298E-01 7.301E-01 43.01 OK 1764.49 15.30 9.862E-01 9.052E-01 9.055E-01 41.00 OK RA-224 240.99 4.10* 4. 911E+OO 4.352E-01 4.352E-01 343.01 OK RA-226 609.32 45.49* 2.310E+OO l.182E+OO l.183E+OO 15.63 OK 1120.29 14.92 l.437E+OO 7.298E-01 7. 301E-01 43.01 OK 1764.49 15.30 9.862E-01 9.052E-01 9.055E-01 41. 00 OK AC-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3.751E+OO 9.976E-01 9.976E-01 51. 61 OK 794.95 4.25 1. 875E+OO Line Not Found Absent 835. 71 1. 61 l.802E+OO 2.467E+OO 2.467E+OO 125.56 OK 911.20 25.80* l.687E+OO 7.410E-01 7.410E-01 50.73 OK 968. 97 15.80 l.609E+OO l.548E+OO l.548E+OO 21. 82 OK RA-228 105.21 1.10 6.259E+OO Line Not Found Absent 338.32 11. 27 3. 751E+OO 9.976E-01 9.976E-01 51. 61 OK 794.95 4.25 l.875E+OO Line Not Found Absent 835.71 1. 61 l.802E+OO 2.467E+OO 2.467E+OO 125.56 OK 911. 20 25.80* l.687E+OO 7.410E-01 7.410E-01 50.73 OK 968.97 15.80 l.609E+OO l.548E+OO l.548E+OO 21. 82 OK Page 4747 of 5809 Nuclide Line Activity Report (continued) Page : 3 Sample ID : G1203621365 Acquisition date 3-0CT-2016 06:55:29 Nuclide Type: Uncorrected Decay Corr 2-S.igma Nuclide Energy %Abn %Eff pCi/GRAM pCi7GRAM %Error Status TH-228 74.82 1.0. 28 4.533iE+OO 1.021E+OO 1.021E+OO 68. 56 OK ' 77 .11 17.10 4.743E+OO 1.785E+OO 1. 785E+OO 21. 98 OK 238.63 43.60* 4.960E+OO 9.313E-01 9.313E-01 13.80 OK 300.09 3.30 4.138E+00 6. 672E-01 6. 672E-01 193.28 OK TH-229 85.43 14.70 5.288E+OO 3.734E-01 3.734E-01 123.34 OK 88.47 24.00 5. 631E+OO 3.108E-01 3.109E-01 81. 93 OK 193.51 4.41* 5.711E+OO Line Not Found Absent 210.85 2.80 5.411E+OO Line Not Found Absent TH-230 609 .. 32 45.49* 2.310E+OO 1.182E+OO 1.182E+OO 15.63 OK 1120.29 14.92 l.437E+OO 7.298E-01 7.299E-01 43.01 OK 1764.49 15.30 9.862E-01 9.052E-01 9.052E-01 41. 00 OK PA-231 283.69 1. 70 4.336E+OO Line Not Found Absent 301.36 5.35* 4.138E+OO 4 .116E-01 4 .116E-01 193.28 OK TH-232 105.21 1.10 6.259E+00 Line Not Found Absent 338.32 11.27 3. 7 51E+OO 9.976E-01 9.976E-01 51. 61 OK 835.71 1. 61 1.802E+OO 2.467E+OO 2.467E+OO 125.56 OK 911.20 25.80* l.687E+OO 7.410E-01 7.410E-01 50.73 OK 968. 97 15.80 l.609E+00 l.548E+00 1.548E+OO 21. 82 OK TH-234 63. 29 3.70* 3.291E+OO 1.202E+OO 1.202E+OO 191.99 OK 92.59 4.23 5.782E+OO 2.492E+OO 2.492E+OO 53.70 OK U-234 609.32 45.49* 2.310E+OO 1.182E+OO 1.182E+OO 15.63 OK 1120.29 14.92 1.437E+OO 7.298E-01 7.298E-01 43.01 OK 1764.49 15.30 9.862E-01 9.052E-01 9.052E-01 41. 00 OK U-235 89. 96 3.47 5. 631E+OO 2.150E+OO 2.150E+OO 81. 93 OK 93.35 5.60 5.782E+OO 1.883E+OO 1.883E+00 53.70 OK 143. 7 6 10. 96* 6.462E+00 Line Not Found Absent 163.33 5.08 6.216E+00 Line Not Found Absent 185. 72 57.20 5.844E+OO 8.039E-02 8.039E-02 116. 63 OK 205.31 5.01 5.506E+OO Line Not Found Absent U-238 63. 29 3.70* 3.291E+00 1.202E+OO 1.202E+OO 191.99 OK 92.59 4.23 5.782E+OO 2.492E+OO 2.492E+OO 53.70 OK AM-243 43.53 5.90 5.190E-01 Line Not Found Absent 74.66 67.20* 4.533E+OO l.562E-01 1.562E-01 68. 56 OK ANH-511 511. 00 100.00* 2.664E+OO 4.581E-02 4.581E-02 182.54 OK Flag: "*" = Keyline Page 4748 of 5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:56:52.78 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621365.CNF;l *
  • Acquisition date 3-0CT-2016 06:55:29 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:47:00 Analyst initials: MXRl *
  • Sample ID Gl203621365 Sample Quantity l.4423E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 * *Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;l7
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM K-40 1.188E+Ol 1. 396E+OO 5.250E-01 ZN-65 2.030E-01 l.054E-01 3.047E-01 RU-103 5. 963E+OO 8.828E+OO 9.880E+OO BA-137M 1.519E-01 6.366E-02 6.332E-02 CS-137 1.605E-01 6.725E-02 6.689E-02 BI-207 1. 417E-01 1.341E-01 9.332E-02 TL-208 2.305E-01 7.774E-02 6.467E-02 PB-210 3.700E+OO 6.698E+OO 6.093E+OO BI-211 3.461E-01 1. llOE+OO 3.888E-01 PB-212 9.313E-01 1.259E-01 1.023E-01 BI-214 1.183E+OO 1.811E-01 l.015E-01 PB-214 1.335E+OO 2.058E-01 3.534E-01 RN-222 1.183E+OO 1.811E-01 1.015E-01 RA-224 4.352E-01 1.463E+OO 1.097E+OO RA-226 1.183E+OO 1. 811E-01 1.015E-01 AC-228 7.410E-01 3.684E-01 2.395E-01 RA-228 7.410E-01 3.684E-01 2.395E-01 TH-228 9. 313E-01 1.259E-01 1.023E-01 TH-229 4.209E-01 4.488E-01 9.279E-01 TH-230 1.182E+OO l.811E-01 1.015E-01 PA-231 4 .116E-01 7. 796E-01 8.638E-01 TH-232 7.410E-01 3.684E-01 2.395E-01 TH-234 1.202E+OO 2.262E+OO 2.127E+OO U-234 1.182E+OO 1. 811E-01 1.015E-01 U-235 -1.003E-01 1.828E-01 3.362E-01 U-238 1.202E+OO 2.262E+OO 2.127E+OO AM-243 l.562E-01 1.050E-01 8.959E-02 ANH-511 4.581E-02 8.194E-02 5.930E-02 Non-Identified Nuclides Key-Line Activity K.L. Cnt Uncert MDA Nuclide (pCi/GRAM ( 1. 96-sigma) (pCi/GRAM BE-7 -1.290E+OO 1.230E+Ol 2.279E+Ol NOT IDENT. NA-22 5.037E-02 4.732E-02 1.044E-01 NOT IDENT. Page 4749 of 5809 NA-24 O.OOOE+OO 1.159E+41 O.OOOE+OO SHORT HLIF AL-26 6.178E-03 2.305E-02 5.824E-02 NOT IDENT. SC-46 -1. 491E-02 3.752E-01 7.388E-01 FAIL ABUN V-48 O.OOOE+OO 1.120E+04 0.000E+OO SHORT HLIF CR-51 O.OOOE+OO 3.785E+02 O.OOOE+OO SHORT HLIF MN-54 7.263E-02 7.410E-02 1.504E-01 NOT IDENT. C0-56 l.848E-01 4.232E-01 9.002E-01 FAIL ABUN MN-56 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF C0-57 1.255E-02 4.427E-02 8.942E-02 NOT IDENT. C0-58 5.201E-01 9.209E-01
  • NOT IDENT . FE-59 1. 226E+OO 5.113E+OO 1.082E+Ol NOT IDENT. C0-60 -2.284E-02 3.477E-02 5.908E-02 NOT IDENT. GE-68 -6.558E-01 2.083E+OO 3.927E+OO NOT IDENT. AS-73 4.108E-01 8.373E+OO 1.567E+Ol NOT IDENT. AS-74 O.OOOE+OO 4.998E+03 O.OOOE+OO SHORT HLIF SE-75 1.042E-01 2.130E-01 4.232E-01 NOT IDENT. BR-77 O.OOOE+OO 3.807E+36 O.OOOE+OO SHORT HLIF SR-82 O.OOOE+OO 6.993E+02 O.OOOE+OO SHORT HLIF RB-83 -3.777E-01 6.506E-01 1.122E+OO NOT IDENT. KR-85 4.360E+OO 9.630E+OO 1.675E+Ol NOT IDENT. SR-85 4.339E-01 9.544E-01 1.661E+OO NOT IDENT. RB-86 O.OOOE+OO 2.062E+04 O.OOOE+OO SHORT HLIF Y-88 8.869E-02 1.786E-01 4.576E-01 NOT IDENT. Y-91 -2.645E+02 4. 771E+02 8.392E+02 NOT IDENT. NB-94 8.232E-03 3.750E-02 7.475E-02 NOT IDENT. NB-95 6.482E-02 8.103E-01 1.452E+OO NOT IDENT. NB-95M 8.383E-02 2.635E+OO 4.514E+OO NOT IDENT. ZR-95 -1.057E+OO 1.3'25E+OO 2.339E+OO NOT IDENT. NB-97 O.OOOE+OO 1.919E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF M0-99 O.OOOE+OO 3.813E+31 O.OOOE+OO SHORT HLIF TC-99M O.OOOE+OO l.646E+41 O.OOOE+OO SHORT HLIF RH-101 -1.055E-02 3. 511E-02 6.767E-02 NOT IDENT. RH-102 1.720E-02 6.221E-02 l.210E-01 NOT IDENT. RH-106 -4. 272E-01 5.475E-01 8.949E-01 NOT IDENT. RU-106 -4.272E-01 5.475E-01 8.949E-01 NOT IDENT. AG-108M 2.936E-02 2.909E-02 6 .118E-02 NOT IDENT. CD-109 O.OOOE+OO 1.219E+OO 2.549E+OO NOT IDENT. AG-llOM -4. 969E-04 9.653E-02 1.925E-01 NOT IDENT. SN-113 6.222E-02 2.362E-01 4.585E-01 NOT IDENT. CD-115 O.OOOE+OO 5.028E+38 O.OOOE+OO SHORT HLIF SN-117M 0.000E+OO 7.397E+04 O.OOOE+OO SHORT HLIF TE-123M -4.353E-02 l.310E-01 2.493E-01 NOT IDENT. SB-124 -4.543E-01 1.447E+OO 3.024E+OO NOT IDENT. SB-125 8.192E-02 1.071E-01 2.199E-01 FAIL ABUN TE-125M -8.579E+OO 2.843E+02 5.078E+02 NOT IDENT. I-126 O.OOOE+OO 6.055E+05 O.OOOE+OO SHORT HLIF SB-126 O.OOOE+OO 9.180E+05 O.OOOE+OO SHORT HLIF SN-126 O.OOOE+OO 7.885E-02 1.651E-01 FAIL ABUN SB-127 O.OOOE+OO 7.499E+21 O.OOOE+OO SHORT HLIF I-131 O.OOOE+OO 3.086E+09 O.OOOE+OO SHORT HLIF I-132 O.OOOE+OO 1. 960E+41 O.OOOE+OO SHORT HLIF TE-132 O.OOOE+OO 1.056E+26 O.OOOE+OO SHORT HLIF BA-133 -1.373E-02 4.701E-02 7.634E-02 NOT IDENT. I-133 O.OOOE+OO 1.557E+41 O.OOOE+OO SHORT HLIF CS-134 7.845E-03 5.772E-02 1.142E-01 FAIL ABUN CS-135 -1. 065E-02 1.766E-01 2.980E-01 NOT IDENT. I-135 0.000E+OO 1. 733E+41 O.OOOE+OO SHORT HLIF CS-136 O.OOOE+OO 2.282E+05 O.OOOE+OO SHORT HLIF CE-139 -l.159E-01 1.041E-01 1. 8 62E-01 NOT IDENT. BA-140 O.OOOE+OO l.013E+06 0.000E+OO SHORT HLIF LA-140 O.OOOE+OO 4.088E+05 O.OOOE+OO SHORT HLIF CE-141 -1.785E+00 2 .119E+Ol 4 .119E+Ol NOT IDENT. CE-143 O.OOOE+OO 5.717E+40 O.OOOE+OO SHORT HLIF CE-144 -2.712E-01 3.314E-01 6.160E-01 NOT IDENT. PM-144 3.108E-03 6.842E-02 1.343E-01 NOT IDENT. PR-144 2.386E-01 5.920E+OO 1.162E+Ol NOT IDENT. PM-146 -1.276E-02 4.763E-02 8.654E-02 NOT IDENT. ND-147 0.000E+OO 2.428E+07 O.OOOE+OO SHORT HLIF PM-147 1.225E+Ol 7.688E+02 1.527E+03 NOT IDENT. PM-149 O.OOOE+OO 7.192E+39 O.OOOE+OO SHORT HLIF EU-150 -2.268E-02 3.271E-02 5.022E-02 FAIL ABUN EU-152 -5.343E-02 9.420E-02 l.682E-Ol FAIL ABUN GD-153 -l.167E-Ol 1.972E-01 3.097E-01 NOT IDENT. EU-154 1.263E-01 1.169E-01 2.581E-01 NOT IDENT. EU-155 -3.201E-02 1.162E-01 2.039E-01 NOT IDENT. TB-160 1.782E-01 1.910E+OO 3.811E+OO FAIL ABUN H0-166M -l.054E-02 5.059E-02 9.909E-02 FAIL ABUN Page 4750of5809 TM-171 1. 965E+01 2.022E+Ol 4.081E+Ol NOT IDENT. HF-172 -8.408E-03 2.383E-01 4.673E-01 FAIL ABUN LU-172 9.034E-02 7.589E-02 1. 763E-01 FAIL ABUN LU-176 2.248E-02 2.388E-02 4.975E-02 FAIL ABUN HF-181 l.676E+OO 4.540E+OO 8. 831E+OO NOT IDENT. TA-182 7.037E-02 1. 060E+OO l.816E+OO FAIL ABUN RE-183 4.016E-01 2.786E+OO 5.228E+OO NOT IDENT. RE-184 7.938E+OO 2.845E+Ol 5.824E+Ol NOT IDENT. W-188 -8.179E+Ol l.254E+02 l.953E+02 FAIL ABUN IR-192 -4.372E-01 4. 544E-01. 7.794E-01 FAIL ABUN HG-203 -8.527E-01 2.377E+OO 4.375E+OO NOT IDENT. PB-211 4.668E-01 6.831E-01 1. 388E+OO NOT IDENT. BI-212 l.307E+OO 9.106E-01 l.376E+OO FAIL ABUN RN-219 9.379E-02 4.107E-01 7.919E-01 FAIL ABUN RA-223 -8.290E-02 6.493E-01 l.212E+OO FAIL ABUN AC-227 -2.973E-02 2.267E-01 4.298E-01 FAIL ABUN TH-227 -2.973E-02 2.267E-01 4.298E-01 FAIL ABUN TH-231 -8.290E-02 6.493E-01 l.212E+OO FAIL ABUN PA-233 -2.888E-03 6.060E-02 l.149E-01 FAIL ABUN PA-234 -2.859E-03 2.568E-01 5.132E-01 FAIL ABUN PA-234M 8.409E-01 4.574E+OO 9.330E+OO NOT IDENT. NP-237 -2.888E-03 6.060E-02 l.149E-01 FAIL ABUN NP-238 O.OOOE+OO 7.002E+40 O.OOOE+OO SHORT HLIF NP-239 -3.367E-02 2.162E-01 4.262E-01 NOT IDENT. PU-239 l.634E+02 3.232E+02 6.525E+02 NOT IDENT. AM-241 -1. 269E-01 l.449E-01 2.250E-01 NOT IDENT. CM-243 l.427E-02 l.027E-01 l.876E-01 NOT IDENT. BK-247 2.946E-02 7.782E-02 l.530E-01 FAIL ABUN CM-247 l.372E-02 3.665E-02 7 .196E-02 NOT IDENT. CF-249 2.316E-02 3.907E-02 7. 851E-02 NOT IDENT. CF-251 -3.052E-02 l.166E-01 2.218E-01 NOT IDENT. Page 4751of5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 07:56:50.47 Nuclide Line Activity Report 1 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error K-40 1460.82 282 10.66* 1.161E+OO 1.18 8E+Ol 1.188E+Ol 11. 99 ZN-65 1115.54 12 50.60* 1. 441E+OO 8.816E-02 2.030E-01 52.99 RU-103 497.08 16 91.00* 2.722E+OO 3.336E-02 5. 963E+OO 151. 06 610.33 239 5.76 2.310E+OO 9.336E+OO 1.669E+03 15.63 BA-137M 661. 66 56 89.90* 2.163E+OO 1. 491E-01 l.519E-01 42.77 CS-137 661. 66 56 85.10* 2.163E+OO 1. 57 5E-01 l.605E-01 42.77 BI-207 72.81 ------21. 40 4.355E+OO ------Line Not Found ------74.97 152 35.70 4.533E+OO 4.904E-01 4.988E-01 39.41 569.70 27 97.76 2.438E+OO 5.876E-02 5.976E-02 147.08 1063.66 30 74.60* 1.497E+OO 1.394E-01 l.417E-01 96.53 1770.23 2 6.87 9.835E-01 1. 796E-01 1.827E-01 292.76 TL-208 277.37 ------6.60 4.415E+OO ------Line Not Found ------583.19 90 85.00* 2.392E+OO 2.305E-01 2.305E-01 34.42 860.56 24 12.50 1. 761E+OO 5. 621E-01 5. 621E-01 113. 91 PB-210 46.54 24 4.25* 8.307E-01 3.608E+OO 3.700E+OO 184.75 BI-211 72. 87 ------1. 23 4.361E+OO ------Line 'Not Found ------351.06 331 12.92* 3.631E+00 3.677E+OO 3.677E+OO 15.74 PB-212 74.82 152 10.28 4.533E+OO 1.703E+OO 1.703E+OO 39.41 77 .11 278 17.10 4.743E+OO 1.785E+OO 1. 785E+OO 21. 98 238.63 387 43.60* 4. 960E+OO 9.313E-01 9.313E-01 13.80 300.09 18 3.30 4.138E+OO 6. 672E-01 6.672E-01 193.28 BI-214 609.32 239 45.49* 2.310E+OO l.182E+OO 1.183E+OO 15.63 1120.29 30 14.92 1.437E+OO 7.298E-01 7.301E-01 43.01 1764.49 26 15.30 9.862E-01 9.052E-01 9.055E-01 41. 00 PB-214 74.82 152 5.80 4.533E+OO 3.019E+00 3.020E+OO 39.41 77 .11 278 9.70 4.743E+OO 3.147E+OO 3.148E+OO 21.98 87.09 ------3.41 5.478E+OO ------Line Not Found ------242.00 100 7.25 4. 911E+OO l.455E+00 1.455E+OO 52.70 295.22 180 18.42 4.198E+OO l.209E+00 1.209E+OO 29.23 351. 93 331 35.60* 3.631E+OO 1.334E+OO 1.335E+OO 15.74 RN-222 609.32 239 45.49* 2.310E+00 l.182E+OO l.183E+OO 15.63 1120.29 30 14.92 1.437E+OO 7.298E-01 7.301E-01 43.01 1764.49 26 15.30 9.862E-01 9.052E-01 9.055E-01 41. 00 RA-224 240.99 100 4.10* 4. 911E+OO 2.573E+OO 2.573E+OO 52.70 RA-226 609.32 239 45.49* 2.310E+OO l.182E+OO 1.183E+OO 15.63 1120.29 30 14.92 1.437E+OO 7.298E-01 7.301E-01 43.01 1764.49 26 15.30 9.862E-01 9.052E-01 9.055E-01 41. 00 AC-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 81 11. 27 3.751E+OO 9.976E-01 9.976E-01 51. 61 794.95 ------4.25 1. 875E+OO ------Line Not Found ------835. 71 14 1. 61 1.802E+OO 2.467E+OO 2.467E+OO 125.56 911.20 62 25.80* l.687E+OO 7.410E-01 7.410E-01 50.73 968. 97 76 15.80 1.609E+OO l.548E+OO l.548E+00 21. 82 RA-228 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 81 11. 27 3. 7 51E+OO 9.976E-01 9.976E-01 51.61 794.95 ------4.25 1.875E+OO ------Line Not Found ------835. 71 14 1. 61 1.802E+OO 2.467E+OO 2.467E+OO 125.56 Page 4752 of 5809 Nuclide Line Activity Report (continued) Page : 2 Sample ID : G1203621365 Acquisition date 3-0CT-2016 06:55:29 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error 911. 20 .62 25.80* 1.687E+OO 7.410E-01 50.73 968. 97 76 15.80 l.609E+OO 1.548E+OO 1.548E+OO 21.82 TH-228 74.82 152 10.28 4.533E+OO 1.703E+OO 1. 703E+OO 39.41 77 .11 278 17.10 4.743E+OO 1. 785E+OO 1. 785E+OO 21. 98 238.63 387 43.60* 4. 960E+OO 9.313E-01 9.313E-01 13.80 300.09 18 3.30 4.138E+OO 6.672E-01 6. 672E-01 193.28 TH-229 85.43 56 14.70 5.288E+OO 3.734E-01 3.734E-01 123.34 88.47 81 24.00 5.631E+OO 3.108E-01 3.109E-01 81. 93 193.51 ------4.41* 5. 711E+OO ------Line Not Found ------210.85 ------2.80 5.411E+OO ------Line Not Found ------TH-230 609.32 239 45.49* 2.310E+OO 1.182E+OO 1.182E+OO 15.63 1120.29 30 14.92 l.437E+OO 7.298E-01 7.299E-01 43.01 1764.49 26 15.30 9.862E-01 9.052E-01 9.052E-01 41. 00 PA-231 283.69 ------1. 70 4.336E+OO ------Line Not Found ------301.36 18 5.35* 4.138E+OO 4 .116E-01 4 .116E-01 193.28 TH-232 105.21 ------1.10 6.259E+OO ------Line Not Found ------338.32 81 11. 27 3.751E+OO 9.976E-01 9.976E-01 51. 61 835.71 14 1. 61 1. 802E+OO 2.467E+OO 2.467E+OO 125.56 911.20 62 25.80* 1.687E+OO 7.410E-01 7.410E-01 50.73 968. 97 76 15.80 1.609E+OO 1.548E+OO 1.548E+OO 21. 82 TH-234 63.29 28 3.70* 3.291E+OO 1.202E+OO 1.202E+OO 191.99 92.59 117 4.23 5.782E+OO 2.492E+OO 2.492E+OO 53.70 U-234 609.32 239 45.49* 2.310E+OO 1.182E+OO 1.182E+OO 15.63 1120.29 30 14.92 l.437E+OO 7.298E-01 7.298E-01 43.01 1764.49 26 15.30 9.862E-01 9.052E-01 9.052E-01 41. 00 U-235 89. 96 81 3.47 5.631E+OO 2.150E+OO 2.150E+OO 81. 93 93.35 117 5.60 5.782E+OO 1.883E+OO 1. 883E+OO 53.70 143.76 ------10. 96* 6.462E+OO ------Line Not Found ------163.33 ------5.08 6.216E+OO ------Line Not Found ------185.72 52 57.20 5.844E+OO 8.039E-02 8.039E-02 116. 63 205.31 ------5.01 5.506E+OO ------Line Not Found ------U-238 63.29 28 3.70* 3.291E+OO 1.202E+OO 1.202E+OO 191.99 92. 59 117 4.23 5.782E+OO 2.492E+OO 2.492E+OO 53.70 AM-243 43.53 ------5.90 5.190E-01 ------Line Not Found ------74.66 152 67.20* 4.533E+OO 2.605E-01 2.606E-01 39.41 ANH-511 511. 00 23 100.00* 2.664E+OO 4. 581E-02 4. 581E-02 182.54 Flag: "*" Key line Page 4753of5809 Summary of Nuclide Activity Sample ID : Gl203621365 Acquisition date : 3 3-0CT-2016 06:55:29 Total number of lines in spectrum 50 Number of unidentified lines 14 Number of lines tentatively identified by NID 36 Nuclide Type : Nuclide K-40 ZN-65 RU-103 BA-137M CS-137 BI-207 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 At:-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Hlife l.25E+09Y 244.06D 39.26D 30.08Y 30.08Y 32.90Y l.41E+10Y 22.20Y 7.04E+08Y l.41E+l0Y 1600.00Y 1600.00Y 1600.00Y l.41E+l0Y 1600.00Y 1. 41E+10Y 1. 41E+l0Y 1. 41E+10Y 7340.00Y 7.54E+04Y 7.04E+08Y 1. 41E+l0Y 4.47E+09Y 2.45E+05Y 7.04E+08Y 4.47E+09Y 7370.00Y 1.00E+09Y Decay 1. 00 2.30 179. 1. 02 1. 02 1. 02 1. 00 1. 03 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 1. 00 Total Activity Grand Total Activity
  • Uncorrected pCi/GRAM l.188E+Ol 8.816E-02 3.336E-02 1.491E-01 1. 575E-01 l.394E-01 2.305E-01 3.608E+00 3.677E+OO 9.313E-01 l.182E+00 1.334E+OO 1.182E+OO 2.573E+OO 1.182E+00 7.410E-01 7.410E-01 9. 313E-01 3.108E-01 1.182E+OO 4 .116E-01 7.410E-01 1.202E+OO l.182E+00 8.039E-02 1.202E+OO 2.605E-01 4.581E-02 3.738E+Ol 3.738E+Ol Decay Corr pCi7GRAM 1.188E+Ol 2.030E-01 5. 963E+OO 1.519E-01 l.605E-01 1.417E-01 2.305E-01 3.700E+OO 3.677E+OO 9.313E-01 1.183E+OO 1.335E+OO 1.183E+OO 2.573E+OO 1.183E+OO 7.410E-01 7.410E-01 9. 313E-01 3.109E-01 1.182E+OO 4.116E-01 7.410E-01 1.202E+OO 1.182E+OO 8.039E-02 1.202E+OO 2.606E-01 4.581E-02 4.353E+Ol 4.353E+Ol 72.00% Decay Corr 2-Sigma Error 0.142E+Ol 1. 07 6E-01 9.008E+OO 0.650E-01 0.686E-01 1.368E-01 0.793E-01 6.835E+OO 0.579E+OO 1.285E-01 0.185E+OO 0.210E+OO 0.185E+OO l.356E+00 0.185E+00 3.759E-01 3.759E-01 l.285E-01 2.547E-01 0.185E+OO 7.955E-01 3.759E-01 2.308E+OO 0.185E+OO 9.376E-02 2.308E+OO 1.027E-01 8.361E-02 "M" Manually accepted 1 2-Sigma %Error 11. 99 52.99 151.06 42.77 42.77 96.53 34.42 184.75 15.74 13.80 15.63 15.74 15.63 52.70 15.63 50.73 50.73 13.80 81. 93 15.63 193.28 50.73 191.99 15.63 116. 63 191.99 39.41 182.54 Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4754of5809 Flags K K Unidentified Energy Lines Page : 4 Sample ID : Gl203621365 Acquisition date : 3-0CT-2016 06:55:29 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 0 209.01 13 199 0.74 418.93 411 13 3.15E-03 **** 5.44E+OO 0 249.44 35 48 1. 53 499.81 496 8 8.71E-03 80.2 4.80E+OO 0 270.58 25 84 1. 41 542.12 538 8 6.18E-03 **** 4.50E+OO T 0 46.2 .11 46 49 2.01 925.34 918 14 .. 1.18E-02 73.8 2.89E+OO T 0 543.22 20 16 0.67 1087.64 1085 7 5. lBE-03 84.2 2.53E+OO 0 586.97 12 8 1. 42 1175.17 1173 5 3.19E-03 92.6 2.38E+OO 0 727. 31 34 28 1. 01 1455.97 1449 11 9.lOE-03 71.1 2.0lE+OO T 0 768.94 33 26 0.80 1539.27 1532 16 8.88E-03 77.4 1. 92E+OO 0 933.90 22 9 1. 06 1869.33 1865 11 6.16E-03 66.0 1. 66E+OO 1 965.03 21 0 2.13 1931. 61 1922 27 5.93E-03 59.2 1.61E+OO T 4 1122. 38 12 0 1. 51 2246.45 2233 17 3.33E-03 74.5 1.43E+OO T 0 1179.51 15 9 2.65 2360.78 2356 11 4.22E-03 89.9 1.38E+OO 0 1224.88 10 4 2.01 2451.55 2448 8 2.78E-03 93.8 l.34E+OO 1 1238.18 24 12 2.28 2478.15 2474 22 6.76E-03 60.9 l.33E+OO T 1 1242.81 18 11 2.29 2487.42 2474 22 5.08E-03 **** 1.32E+OO 0 1279.83 18 3 1. 04 2561.49 2554 14 5.16E-03 63.0 1.29E+OO 0 1372.91 9 7 3.78 2747.75 2742 12 2.53E-03 **** 1.22E+OO 0 1377.71 13 4 1. 98 2757.35 2753 8 3. 61E-03 76.9 1. 22E+OO 0 1594.69 8 6 0.57 3191. 49 3186 9 2.33E-03 **** 1.08E+OO 0 1727.95 15 3 5.08 3458.13 3450 16 4.29E-03 76.6 1. OOE+OO Flags: "T" = Tentatively associated Page 4755of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:57:07.89 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * *******************************************************************************
  • o( *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621365.CNF;l *
  • Acquisition date 3-0CT-2016 06:55:29 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: 0 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:47:00 Nuclide Library : SOLID *
  • Sample ID G1203621365 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4423E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10:35:16 Eff. Geometry : CAN *
  • Eff. File : DKA100: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide K-40 ZN-65 RU-103 BA-137M CS-137 BI-207 TL-208 PB-210 BI-211 PB-212 BI-214 PB-214 RN-222 RA-224 RA-226 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-232 TH-234 U-234 U-235 U-238 AM-243 ANH-511 Le (pCi/GRAM 2.053E-01 1.299E-01 4.419E+OO 2.790E-02 2.947E-02 4.018E-02 2.879E-02 2.847E+OO 1. 789E-01 4.779E-02 4.391E-02 1. 711E-01 4. 391E-02 5.123E-01 4.391E-02 1.033E-01 1.033E-01 4.779E-02 4.348E-01 4.389E-02 3.989E-01 l.033E-01 1.002E+OO 4.389E-02 1. 576E-Oi 1.002E+OO 4.234E-02 2.694E-02 ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 Page 4756 of 5809 Le (pCi/GRAM 1.027E+Ol 4.541E-02 O.OOOE+OO NOT IDENT. NOT IDENT. SHORT HLIF AL-26 SC-46 V-48 CR-51 MN-;--54 C0-56 MN-56 C0-57 C0-58 FE-59 C0-60 GE-68 AS-73 AS-74 SE-75 BR-77 SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 , NB-94 NB-95 NB-95M ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RH-106 RU-106 AG-108M CD-109 AG-110M SN-113 CD-115 SN-117M TE-123M SB-124 SB-125 TE-125M I-126 SB-126 SN-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-1'44 PM-146 ND-147 PM-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 Page 4757 of 5809 2.180E-02 3.222E-01 0.000E+OO O.OOOE+OO 6.759E-02 3.942E-01 0.000E+OO 4.190E-02 3.914E-01 4.571E+OO 2.324E-02 1. 647E+OO 7.362E+OO O.OOOE+OO 1. 968E-01 0.000E+OO O.OOOE+OO 4. 963E-01 7.715E+OO 7.648E-01 O.OOOE+OO 1.785E-01 3.543E+02 3.390E-02 6.367E-01 2 .115E+OO 1.007E+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 0.000E+OO 3.186E-02 5.387E-02 3.923E-01 3.923E-01 2.796E-02 1.218E+OO 8.341E-02 2.095E-01 O.OOOE+OO O.OOOE+OO 1.169E-01 1. 086E+OO l.003E-01 2.388E+02 O.OOOE+OO O.OOOE+OO 7.888E-02 O.OOOE+OO O.OOOE+OO O.OOOE+OO O.OOOE+OO 3.473E-02 O.OOOE+OO 5.126E-02 1. 389E-01 0.000E+OO O.OOOE+OO 8.654E-02 0.000E+OO O.OOOE+OO 1. 935E+Ol O.OOOE+OO 2. 871E-01 6.108E-02 5.283E+OO 3.907E-02 O.OOOE+OO 7.142E+02 O.OOOE+OO 2.308E-02 7.637E-02 1. 449E-01 l.124E-01 9.561E-02 1.677E+OO 4.305E-02 1.920E+Ol NOT IDENT. FAIL ABUN SHORT HLIF SHORT HLIF NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF SHORT HLIF SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF SHORT HLIF NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IOENT. SHORT HLIF FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT.

HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 PB-211 BI-212 RN-219 RA-223 AC-227 TH-227 TH-231 PA-233 PA-234 PA-234M NP-237 NP-238 NP-239 PU-239 AM-241 CM-243 BK-247 CM-247 CF-249 CF-251 Page 4758 of 5809 2.201E-01 7.780E-02 2.296E-02 4.023E+OO 7.922E-01 2.459E+OO 2.565E+Ol 8.973E+Ol 3.546E-01 2.026E+OO 6.346E-01 6.346E-01 3. 621E-01 5.593E-01 l.985E-01 l.985E-01 5.593E-01 5.275E-02 2.203E-01 4.125E+OO 5.275E-02 O.OOOE+OO 1. 986E-01 3.083E+02 l.050E-01 8.793E-02 7. ll 7E-02 3.287E-02 3. 596E-02 l.038E-01 FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT I DENT .* NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 07:57:14.31 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621365.CNF;l * *Acquisition date 3-0CT-2016 06:55:29 Sensitivity : 3.000 *
  • Detector ID GAM19 Energy tolerance: 1.500 *
  • Elapsed live time: O 01:00:00.00 Abundance limit : 75.000 * *Elapsed real time: 0 01:00:00.73 Half life ratio : ***** *
  • Sample date 14-DEC-2015 13:47:00 Nuclide Library : SOLID *
  • Sample ID G1203621365 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.4423E+02 GRAM *
  • Quantity Err(%) : 1.3866E-03 % *
  • Wet wt corr 1.00000 Wet Weight : 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 15-JUN-2016 10': 35: 16 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAM19 CAN.CNF;17
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) (1.96-sigma) K-40 1.188E+Ol 1.528E+OO 1.528E+OO ZN-65 2.030E-01 1.057E-01 1.057E-01 RU-103 5.963E+OO 8.833E+OO 8.833E+OO BA-137M 1.519E-01 6.400E-02 6.400E-02 CS-137 1.605E-01 6. 761E-02 6. 7 61E-02 BI-207 1. 417E-01 1.342E-01 1.342E-01 TL-208 2.305E-01 7.837E-02 7.837E-02 PB-210 3.700E+OO 6.709E+OO 6.709E+OO BI-211 3.461E-01 1.128E+OO 1.128E+OO PB-212 9.313E-01 1.353E-01 1.353E-01 BI-214 1.183E+OO 1.882E-01 1.882E-01 PB-214 1.335E+OO 2 .132E-01 2.132E-01 RN-222 1.183E+OO 1.882E-01 1.882E-01 RA-224 4.352E-01 1.470E+OO 1. 470E+OO RA-22 6 1.183E+OO 1.882E-01 1. 882E-01 AC-228 *7. 410E-01 3.703E-01 3.703E-01 RA-228 7.410E-01 3.703E-01 3.703E-01 TH-228 9.313E-01 1.353E-01 1.353E-01 TH-229 4.209E-01 4.492E-01 4.492E-01 TH-230 1.182E+OO l.881E-01 1.881E-01 PA-231 4 .116E-01 7.845E-01 7.845E-01 TH-232 7.410E-01 3.703E-01 3.703E-01 TH-234 1.202E+OO 2.278E+OO 2.278E+OO U-234 1.182E+OO 1.881E-01 1.881E-01 U-235 -1.003E-01 1.829E-01 1.829E-01 U-238 1.202E+OO 2.278E+OO 2.278E+OO AM-243 1.562E-01 1.062E-01 1.062E-01 ANH-511 4.581E-02 8 .196E-02 8 .196E-02 Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM (1. 96-sigma) ( 1. 96-sigma) BE-7 -1.290E+OO 1.230E+Ol 1. 231E+Ol NOT IDENT. NA-22 5.037E-02 4.736E-02 5.252E-02 NOT IDENT. Page 4759 of 5809 NA-24 l.000E+41 1.235E+41 O.OOOE+OO SHORT HLIF AL-26 6.178E-03 2.306E-02 2.322E-02 NOT IDENT. SC-46 -l.491E-02 3.752E-01 3.753E-01 FAIL ABUN V-48 1.166E+04 l .121E+o4 1.239E+04 SHORT HLIF CR-51 1. 731E+02 3.785E+02 3.865E+02 SHORT HLIF MN-54 7.263E-02 7.417E-02 8.107E-02 NOT IDENT. C0-56 l.848E-01 4.233E-01 4.314E-01 FAIL ABUN MN-56 l.OOOE+41 2.309E+41 O.OOOE+OO SHORT HLIF C0-57 1.255E-02 4.427E-02 4.463E-02 NOT IDENT. C0-58 -3.849E-01 5.203E-01 5.485E-01 NOT IDENT. FE-59 l.226E+OO 5. 114E+OO 5.144E+00 NOT IDENT. C0-60 -2.284E-02 3.478E-02 3.627E-02 NOT IDENT. GE-68 -6.558E-01 2.083E+OO 2.104E+OO NOT IDENT. AS-73 4.108E-01 8.373E+OO 8.375E+OO NOT IDENT. AS-74 -1.699E+03 5.000E+03 5.058E+03 SHORT HLIF SE-75 1.042E-01 2.131E-01 2.182E-01 NOT IDENT. BR-77 2.816E+37 2.388E+38 O.OOOE+OO SHORT HLIF SR-82 -3.318E+02 6.995E+02 7.153E+02 SHORT HLIF RB-83 -3.777E-01 6.527E-01 6.745E-01 NOT IDENT. KR-85 4.360E+OO 9.632E+OO 9.830E+OO NOT IDENT. SR-85 4.339E-01 9.546E-01 9.744E-01 NOT IDENT. RB-86 -4.856E+03 2.062E+04 2.073E+04 SHORT HLIF Y-88 8.869E-02 l.787E-01 1. 831E-01 NOT IDENT. Y-91 -2.645E+02 4. 772E+02 4.919E+02 NOT IDENT. NB-94 8.232E-03 3.750E-02 3.769E-02 NOT IDENT. NB-95 6.482E-02 8.103E-01 8.108E-01 NOT IDENT. NB-95M 8.383E-02 2.635E+OO 2.635E+OO NOT IDENT. ZR-95 -1.057E+OO 1. 326E+'OO 1.409E+OO NOT IDENT. NB-97 -1.000E+41 1. 920E+41 O.OOOE+OO SHORT HLIF ZR-97 1.000E+41 5.169E+41 O.OOOE+OO SHORT HLIF M0-99 2.386E+31 3.817E+31 O.OOOE+OO SHORT HLIF TC-99M -l.OOOE+41 l.649E+41 O.OOOE+OO SHORT HLIF RH-101 -1.055E-02 3.516E-02 3.548E-02 NOT IDENT. RH-102 1.720E-02 6.223E-02 6.271E-02 NOT IDENT. RH-106 -4. 272E-01 5.482E-01 5.810E-01 NOT IDENT. RU-106 -4. 272E-01 5.482E-01 5.810E-01 NOT IDENT. AG-108M 2.936E-02 2. 911E-02 3.198E-02 NOT IDENT. CD-109 3.009E+OO 1. 243E+OO 1. 840E+OO NOT IDENT. AG-llOM -4. 969E-04 9.653E-02 9.653E-02 NOT IDENT. SN-113 6.222E-02 2.362E-01 2.378E-01 NOT IDENT. CD-115 -3.132E+38 5.059E+38 O.OOOE+OO SHORT HLIF SN-ll 7M -2. 971E+04 7.405E+04 7.525E+04 SHORT HLIF TE-123M -4.353E-02 1. 311E-01 1.325E-01 NOT IDENT. SB-124 -4.543E-01 1. 447E+OO l.461E+OO NOT IDENT. SB-125 8.192E-02 1. 071E-01 1.133E-01 FAIL ABUN TE-125M -8.579E+OO 2.843E+02 2.843E+02 NOT IDENT. I-126 1.595E+05 6.059E+05 6.101E+05 SHORT HLIF SB-126 -8.258E+05 9.307E+05 1.002E+06 SHORT HLIF SN-126 1. 961E-01 7.980E-02 l.191E-01 FAIL ABUN SB-127 3.655E+21 8.970E+21 O.OOOE+OO SHORT HLIF I-131 1.348E+09 3.086E+09 3.146E+09 SHORT HLIF I-132 l.OOOE+41 1.840E+42 O.OOOE+OO SHORT HLIF TE-132 -5.000E+25 1. 07 4E+2 6 O.OOOE+OO SHORT HLIF BA-133 -l.373E-02 4.702E-02 4.742E-02 NOT IDENT. I-133 l.OOOE+41 2.359E+41 O.OOOE+OO SHORT HLIF CS-134 7.845E-03 5. 772E-02 5.783E-02 FAIL ABUN CS-135 -1.065E-02 1.766E-01 1.766E-01 NOT IDENT. I-135 -l.000E+41 6.859E+41 O.OOOE+OO SHORT HLIF CS-136 -1.940E+04 2.283E+05 2.284E+05 SHORT HLIF CE-139 -l.159E-01 1.067E-01 l.188E-01 NOT IDENT. BA-140 -2.554E+04 1.013E+06 1.013E+06 SHORT HLIF LA-140 l.256E+05 4.088E+05 4.127E+05 SHORT HLIF CE-141 -1. 785E+00 2 .119E+Ol 2.120E+Ol NOT IDENT. CE-143 1.000E+41 5.804E+40 O.OOOE+OO SHORT HLIF CE-144 -2.712E-01 3.318E-01 3.536E-01 NOT IDENT. PM-144 3.108E-03 6.B42E-02 6.843E-02 NOT IDENT. PR-144 2.386E-01 5.920E+OO 5.921E+OO NOT IDENT. PM-146 -1.276E-02 4.764E-02 4.799E-02 NOT IDENT. ND-147 -5. 996E+06 2.428E+07 2.443E+07 SHORT HLIF PM-147 1.225E+Ol 7.688E+02 7.688E+02 NOT IDENT. PM-149 4.562E+39 7.260E+39 0.000E+OO SHORT HLIF EU-150 -2.268E-02 3.272E-02 3.428E-02 FAIL ABUN EU-152 -5.343E-02 9.425E-02 9.728E-02 FAIL ABUN GD-153 -l.167E-01 1.974E-01 2.043E-01 NOT IDENT. EU-154 l.263E-01 l.170E-01 l.301E-01 NOT IDENT. EU-155 -3. 201E-02 1.162E-01 1.171E-01 NOT IDENT. TB-160 l.782E-01 1.910E+OO 1.912E+OO FAIL ABUN H0-166M -l.054E-02 5.059E-02 5.082E-02 FAIL ABUN Page 4760of5809 TM-171 1. 965E+Ol 2.030E+Ol 2.215E+Ol NOT IDENT. HF-172 -8.408E-03 2.383E-01 2.383E-01 FAIL ABUN LU-172 9.034E-02 7.644E-02 8.661E-02 FAIL ABUN LU-176 2.248E-02 2.390E-02 2.596E-02 FAIL ABUN HF-181 1.676E+OO 4.541E+OO 4. 6.Q3E+OO NOT IDENT. TA-182 7.037E-02 1.060E+OO 1.060E+OO FAIL ABUN RE-183 4.016E-01 2.787E+OO 2.793E+OO NOT IDENT. RE-184 7.938E+OO 2. 851E+Ol 2.873E+Ol NOT IDENT. W-188 -8.179E+Ol 1.257E+02 l.310E+02 FAIL ABUN .IR-192 -4. 372E-01 4.548E-01 4.957E-01 FAIL ABUN HG-203 -8.527E-01 2.378E+OO 2.409E+OO NOT IDENT. PB-211 4.668E-01 6.835E-01 7.151E-01 NOT IDENT. BI-212 l.307E+OO 9.130E-01 l.087E+OO FAIL ABUN RN-219 9.379E-02 4.109E-01 4.131E-01 FAIL ABUN RA-223 -8.290E-02 6.493E-01 6.504E-01 FAIL ABUN AC-227 -2.973E-02 2.267E-01 2. 271E-01 FAIL ABUN TH-227 -2.973E-02 2.267E-01 2. 271E-01 FAIL ABUN TH-231 -8.290E-02 6.493E-01 6.504E-01 FAIL ABUN PA-233 -2.888E-03 6.060E-02 6.061E-02 FAIL ABUN PA-234 -2.859E-03 2.568E-01 2.568E-01 FAIL ABUN PA-234M 8.409E-01 4.574E+OO 4.590E+OO NOT IDENT. NP-237 -2.888E-03 6.060E-02 6.061E-02 FAIL ABUN NP-238 3.822E+40 7.004E+40 O.OOOE+OO SHORT HLIF NP-239 -3.367E-02 2.162E-01 2.167E-01 NOT IDENT. PU-239 1.634E+02 3.232E+02 3.315E+02 NOT IDENT. AM-241 -1.269E-01 1.453E-01 1.561E-01 NOT IDENT. CM-243 l.427E-02 1.027E-01 1.029E-01 NOT IDENT. BK-247 2.946E-02 7.805E-02 7.917E-02 FAIL 'ABUN CM-247 1.372E-02 3.672E-02 3.724E-02 NOT IDENT. CF-249 2.316E-02 3.912E-02 4.049E-02 NOT IDENT . CF-251 . -3. 052E-02 l.166E-01 1.175E-01 NOT IDENT. Page 4761 of 5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 74.5300 87.09 77.4165 136.47 83.3179 45.60 67.3888 87.57 77.4717 140.51 0.0000 46.54 67.5282 88.03 77.5244 143.76 85.7176 49.72 0.0000 88.34 77.5596 144.24 93.5585 51. 35 89.8228 88.47 77.5747 145.44 82.4021 51.87 70.5693 89. 96 77.7437 152.43 76.0197 52.39 61.5287 1093.63 77.8208 153.25 0.0000 52.97 68.4455 91.11 0.0000 323.87 84.0381 53.44 78.7868 92.59 78.0391 156. 02 0.0000 54.07 74.3132 93.35 78.1235 158.56 0.0000 57.36 0.0000 94.56 78.2578 159.00 84.4492 57.53 71. 3651 94.65 78.2676 162.33 62.6660 57.98 80.6427 94.67 78.2700 162.66 0.0000 59.27 83.1502 94.87 78.2920 163.33 69.7960 59.32 83.1580 97.43 80.2087 165.86 83.2550 59.54 90.8953 98.43 86.8760 176.31 69.7806 60. 96 64.8769. 98.44 86.8776 17 6. 60 . 0.0000 61.17 71. 0835 99.53 57.8679 177.52 77.0250 62.93 88.3663 100 .11 82.5580 181.07 0.0000 63.29 88.4241 102.03 77.8310 181. 52 87.6502 63.58 88.4705 103.18 71. 7 641 184.41 82.4751 64.28 80.8115 103.37 71. 7823 143.76 84.8299 66.73 87.4066 105.21 83.1233 193.51 53.6170 67.24 89.0468 105.31 83.1340 197.03 69.2801 125.81 91. 4604 106.12 80.7387 198.01 66.6026 67.75 91.4711 106.47 80.7754 201.83 69.5685 69.67 111. 77 68 109.28 84.8122 203.43 67.3728 70.83 89.5977 111. 00 92.4989 205.31 64.7261 72.81 115.1289 111.76 0.0000 210.85 91.3170 72. 87 115.1407 114. 06 68.5969 215.65 78.7165 74.66 98.4751 116. 30 0.0000 222 .11 74.4759 74.82 98.5004 116.74 66.3075 227.09 56.0797 74.97 98.5245 119.76 69.9223 227.38 57.0280 77 .11 98.8665 121.12 69.1933 228.16 0.0000 78.74 85.9861 121. 22 69.2017 228.18 66.4188 79.69 86.1152 121.78 67.5594 116.74 66.4188 80.12 86.1735 122.06 67.5822 235.69 73.3972 80.19 0.0000 122.92 78.6452 235. 96 76.2358 80.57 81. 4431 123.07 78.6589 238.63 66.4896 81. 00 81.4976 265.00 87.1802 238.98 0.0000 81. 07 86.3009 125.81 89.0968 240.99 66.6101 81. 75 76.7930 127.23 94.3442 242.00 66.6610 83.79 77.0332 127.91 102.0752 244.70 66.7973 84.00 77.0581 129.30 85.1990 252.40 0.0000 85.43 77.2246 131. 20 87.0928 252.80 44.3250 86.55 77.3545 133.02 83.8509 254.15 0.0000 86.79 77.3818 133.52 81.3304 256.23 51. 6039 86.94 77.3994 136.00 85.8500 260.90 0.0000 Page 4762 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 2 64. 66 49.0348 355.39 0.0000 584.27 22.1938 264.80 50.0015 356.01 39 .. 7633 595.83 0.0000 265.00 51.9313 364.49 0.0000 427.87 27.4951 268.22 65.0638 366.42 0.0000 602.52 0.0000 269.46 63.6730 372. 51 39.1110 604.72 29.2613 270.03 55.9775 375.05 40.1973 607.14 13.7832 271.23 44.9163 377.52 40.2529 609.32 13.7949 273.65 0.0000 356.01 34.1803 610.33 13.8003 276.40 47.5026 388.16 30.1080 614.28 15.5495 277.37 43.6542 388.63 0.0000 618.01 17.3029 277.60 43.6615 391.69 33.2865 620.36 23.0908 278.00 36.8798 264.66 31. 3574 621. 93 27.7266 279.20 55.3649 401. 81 34.5140 630.19 0.0000 279.54 73.8368 402.40 31.3867 631. 29 18.5508 279.70 73.8461 404.85 27.2373 633.25 19.7254 280.46 62.2188 410.95 35.7321 634.78 0.0000 283.69 55.5353 413.71 34.7315 635.95 12.7765 284.31 0.0000 414.70 0.0000 636.99 0.0000 285.41 61.4529 423.72 0.0000 645.85 19.8202 285.90 0.0000 427.09 39.2116 657.76 23.8905 287.50 48.8413 427.87 24.3842 657.90 0.0000 290.67 51.3934 433.94 22.3326 661. 66 18.4718 293.27 0.0000 439.40 26.6591 664.57 0.0000 351.93 39.7667 453.88 33.2951 666.33 0.0000 295.96 39.7856 463.37 29.1324 666.50 0.0000 879.38 29.5221 468.07 25.9541 667.71 0.0000 299.98 51.7107 473.00 0.0000 677.62 21.2344 300.09 51. 7149 475.06 21. 7004 685.70 0.0000 300 .13 51. 7160 476.78 31. 4910 695.00 0.0000 301.36 48.8001 477.60 29.3307 696.49 30.2875 302.85 54.7683 482.18 29.3939 696. 51 30.2875 256.23 55.7161 487.02 0.0000 697.00 0.0000 304.85 0.0000 492.35 0.0000 697.30 31.1868 306.78 31.6589 497.08 24 .1158 697.49 32.0801 308.46 48.5295 505.52 21. 457 9 702.65 28.5684 311. 90 42.6816 507.63 0.0000 706.68 16.9862 316.51 51. 7 651 511. 00 33.0933 711. 68 17.0164 319.41 0.0000 514.00 36.4509 720.70 0.0000 320.08 0.0000 514.00 36.4509 721.93 0.0000 321.04 34.9416 520.40 27.6937 722.78 15.8238 323.87 50.0041 520.69 0.0000 722.91 15.8243 325.23 58.0543 522.65 0.0000 723.31 15.8265 328.76 0.0000 527.90 0.0000 724.19 17.2705 333.37 58.8475 528.26 27.7893 727.33 17.2893 333.97 58.8690 529.59 17.7956 733.00 15.3383 334.37 52.8439 529.87 0.0000 735.93 23.4824 338.28 47.4198 531. 02 0.0000 333.97 18.9761 338.32 47.4217 537.26 0.0000 739.50 0.0000 311. 90 45.4623 546.56 0.0000 747.24 13.5997 340.48 45.4623 552.55 19.0953 748.06 15.4171 340.55 0.0000 563.25 18.6169 752.31 18.1635 344.28 42.5281 569.33 23.7549 753.82 0.0000 345.93 36.4885 946.00 23.7566 756.73 21. 8291 351.06 44.7323 569.70 23.7583 756.80 17.2814 351. 93 44.7546 583.19 22.1835 884.68 18.9643 Page 4763of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 765.81 16.0563 1274.44 14.6626 1620.50 2.2465 766.42 11.6797 1001.03 12.7243 1621.92 1.1235 766.84 11. 6813 1002.74 15.6675 1678.03 0.0000 772. 60 0.0000 1004.73 20.5751 1690.97 3.6408 776.52 0.0000 507.63 0.0000 1750.46 0.0000 739.50 0.0000 1025.87 0.0000 1764.49 4 .* 6104 778.90 14.6597 1028.54 0.0000 1063.66 3. 07 67 783.70 0.0000 1037.84 9.8846 1771.35 1.5386 785.37 14.6909 1038.76 0.0000 1791.20 0.0000 792.07 28.5261 631.29 9.9072 1808.65 1.8581 794.95 17.5000 1048.07 0.0000 1810.72 0.0000 795.86 23.9537 1049.04 16.8527 1836.06 1. 8667 810.06 24.0632 1050.41 15. 8672 810.29 24.0648 1063.66 12.9365 344.28 22.2151 1077.00 0.0000 810.76 18.5144 1077.34 11. 9832 815.77 0.0000 1085.87 11. 0087 1048.07 0.0000 1093.63 7.0192 832.01 19.3845 1099.45 8.0342 834.85 13.4319 1112. 07 4.0298 835.71 14.9282 1112.84 4.8366 836.80 0.0000 1115. 54 11.2930 846.75 0.0000 1120.29 4.0378 846.77 12.1704 1120.55 4.0381 856.80 0.0000 1221.41 4.0391 860.56 17.8629 1129. 67 14.1658 871.09 10.3746 1131.51 0.0000 873.19 10.3813 1147.95 0.0000 875.33 0.0000 1173.23 19.8673 879.38 17.0189 1177.95 21. 2938 880.51 15 .1333 1189.05 11. 2907 883.24 15.1455 1204.77 15.4541 884.68 14.2049 1221.41 14.8931 889.28 16.1212 1231.02 17.6215 894.76 14.2474 1235.36 0.0000 898.04 7.6060 1238.28 15.5740 900. 72 16.1756 1260.41 0.0000 903.28 15.2354 1271. 87 10.7616 911.20 13.3617 1274.44 5.0250 912.08 13. 3651 1274.54 5.0250 923.98 0.0000 1291.59 4.2034 926.50 13. 4211 1298.22 0.0000 929 .11 7.6750 1312 .11 0.0000 937.49 16.9254 1332.49 9.5427 944 .13 0.0000 1362.66 0.0000 946.00 12.5319 1365.19 10.6781 949.00 10.6129 1368.63 0.0000 667. 71 0.0000 1384.29 6.4325 962. 31 2.9052 1408.01 3.2324 964.08 2.9067 1457.56 0.0000 966 .17 2.9084 1460.82 4.3564 911. 20 2.9106 1489.16 5.4764 968. 97 2.9106 1505.03 6.5925 983.53 0.0000 1584.12 8.9248 984.45 0.0000 1596.21 0.0000 Page 4764 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:44:24.21 ******************************************************************************** *
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************** Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621366.CNF;l Background file DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]BKG GAM11.CNF;517 Background date : Z-OCT-2016 11:00:34. Sample date 12-SEP-2016 00:00:00 Acquisition date : 3-0CT-2016 05:28:46. Sample ID G1203621366 Sample quantity 1.15000E+02 GRAM Detector name GAMll Detector geometry: CAN Elapsed live time: O 00:15:00:00 Elapsed real time: 0 00:15:06.51 0.7% Energy tolerance 1.50000 keV Analyst Initials MXRl Abundance limit 75.00000 Sensitivity 3.00000 Batch ID 1596254 Detector SN# Matrix Spike ID : LCS ID : 1556 ******************************************************************************** Pk It 1 10 2 10 3 0 4 0 5 0 6 0 7 0 8 0 9 0 10 0 11 0 12 0 13 0 14 0 15 0 16 0 17 0 18 0 19 0 20 0 21 0 22 0 23 0 24 0 25 0 26 0 27 0 28 0 Energy 45.21* 46.49* 59.46 87.98 122.09 157.59 281. 91
  • 455.52 498.20 519.40 619.78 661.65* 690.94 738.07 795.59 92 0. 8 5 1173.30 1215.76 1332. 61* 1356. 81 1400.13 1508.05 1861.65 1865.43 1943.17 1961.35 1996.81 2032.40 BACKGROUND *CORRECTED SAMPLE PEAK REPORT Area 1236 11339 23984 3343 226 79 79 70 49 34 71 15167 44 55 40 44 9458 35 8588 11 12 17 11 13 14 11 10 6 Bkgnd FWHM Channel Left Pw Cts/Sec %Err 4471 3275 4575 1556 845 652 615 651 479 373 231 592 205 321 195 271 332 98 77 44 39 40 7 2 4 5 13 5 1. 98 0.84 0.82 0.85 0.84 0.80 1. 25 1. 78 1. 74 1. 00 2.36 1. 40 1. 99 1. 80 0.78 1.18 1. 75 0.93 1. 80 5.80 3.28 7.53 1. 71 1. 42 1. 48 3.21 1. 45 3.44 90. 29 92.87 118. 83 175.90 244.17 315.22 564.01 911. 43 996. 82 1039.24 1240.11 1323.88 1382.48 1476.78 1591.86 1842.45 2347.44 2432.38 2666.09 2714. 48 2801.13 3016. 96 3724.04 3731. 61 3887.05 3923.40 3994.30 4065.45 87 87 114 171 241 313 560 908 994 1036 1237 1316 1380 1474 1589 1840 2337 2428 2658 2702 2790 3003 3718 3728 3883 3917 3987 4058 10 1.37E+OO 9.8 10 1.26E+Ol 1.2 10 2.66E+Ol 0.8 10 3.71E+OO 2.8 7 2.52E-01 22.3 7 8.80E-02 54.5 8 8.77E-02 55.7 8 7.75E-02 64.4 9 5.41E-02 82.1 8 3.83E-02 98.4 7 7.84E-02 37.8 16 1.69E+Ol 0.9 8 4.93E-02 57.8 11 6.09E-02 64.6 6 4.41E-02 58.0 6 4. 85E-02 61. 7 20 1.05E+Ol 1.1 12 3.86E-02 59.1 18 9.54E+OO 1.1 16 1. 25E-02135. 6 15 1.36E-02116.8 21 1. 83E-02100. 8 10 1.19E-02 56.7 9 1. 48E-02 33. 7 8 1. 60E-02 35. 3 12 1. 23E-02 52. 7 11 1.llE-02 83.1 10 6.97E-03 77.3 Flag: "*" = Peak area was modified by background subtraction Page 4765 of 5809 Fit 6.70E+00 VMS Nuclide Identification Report V3.l Generated 3-0CT-2016 05:44:26 Configuration Analyses by Sample title Sample date Sample ID Sample type
  • Detector name : Elapsed live time: Energy tolerance : Errors propagated: Efficiency type Abundance limit Interference Report DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621366.CNF;l PEAK V16.9,PEAKEFF V2.2,ENBACK Vl.6,NID V3.4 MXRl 12-SEP-2016 00:00:00 G1203621366 SOLID GAMMAll 0 00:15:00.00 1.50 keV No Linear 75.00 Acquisition date : Sample quantity : Sample geometry * : Detector geometry: Elapsed real time: Half life ratio Systematic Error Efficiencies at 3-0CT-2016 05:28:46 115. 00 GRAM CAN 0 00:15:06.51 10.00 0.00 % Peak Energy 0.7% No interference correction performed Page 4766 of 5809 Nuclide Line Activity Report Page : 2 Sample ID : G1203621366 Acquisition date 3-0CT-2016 05:28:46 Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 237 85.60* 7..219E+OO 1.003E+OO 1.059E+OO 44.65 136.47 ------10.68 7.146E+OO ------Line Not Found ------C0-60 1173.23 9009 99.85 1.491E+OO 1.581E+02 1.593E+02 2.26 1332.49 8134 99.98* 1.340E+OO 1.585E+02 1.597E+02 2.21 RU-103 497.08 48 91.00* 2.926E+OO 4.719E-01 6.865E-01 164.14 610.33 ------5.76 2.491E+OO ------Line Not Found ------CD-109 88.03 3550 3.70* 6.299E+OO 3.978E+02 4.107E+02 5.62 SN-ll 7M 156.02 ------2 .11 6.864E+OO ------Line Not Found ------158.56 82 86.40* 6.837E+OO 3.631E-01 1.072E+OO 109.05 TE-123M 159.00 82 84.00* 6.837E+OO 3.735E-01 4.225E-01 109.05 SN-126 64.28 ------9.60 4.012E+OO ------Line Not Found ------86.94 3550 8.90 6.299E+OO 1.654E+02 1. 654E+02 5.62 87.57 3550 37.00* 6.299E+OO 3.978E+Ol 3.978E+Ol 5.62 BA-137M 661. 66 14813 89.90* 2.339E+OO 1.840E+02 1.842E+02 1. 78 CS-137 . 661.66 14813 85.10* 2.339E+OO 1.943E+02 1.946E+02 1. 78 PM-147 121. 22 237 0.00* 7.219E+OO 3.013E+04 3.060E+04 44.65 PB-210 46.54 12346 4.25* 1.369E+OO 5. 541E+03 5.551E+03 2.46 AM-241 59.54 25865 35.90* 3. 351E+OO 5.614E+02 5.615E+02 1. 68 Flag: "*" Keyline Page 4767of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:44:27.17 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * .. DETECTOR AND SAMPLE DATA * * * *
  • Configuration DKA100: [CANBERRA.GAMMA.ARCHIVE.GAMMA]G1203621366.CNF;l *
  • Acquisition date 3-0CT-2016 05:28:46 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.51 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Analyst initials: MXRl *
  • Sample ID G1203621366 Sample Quantity l.1500E+02 GRAM *
  • Batch Number 1596254 Wet Weight 0.00000 *
  • Wet wt corr 1.00000 Dry Weight 0.00000 *
  • Nuclide Library : SOLID.NLB;6 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;14
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Cnt uncert Nuclide (pCi/GRAM ( 1. 96-sigma) C0-57 l.059E+OO 4.633E-Ol C0-60 l.597E+02 3.464E+OO RU-103 6.865E-01 l.104E+OO CD-109 4.107E+02 2.262E+Ol SN-117M 1. 072E+OO 1.145E+OO TE-123M 4.225E-01 4.516E-01 SN-126 3.978E+Ol 2.191E+OO BA-137M 1. 842E+02 3.205E+OO CS-137 l.946E+02 3.386E+OO PM-147 3.060E+04 1.339E+04 PB-210 5.551E+03 1.340E+02 AM-241 5.615E+02 9.261E+OO Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 *sc-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 ZN-65 GE-68 AS-73 AS-74 SE-75 Page 4768of5809 Key-Line Activity (pCi/GRAM -8.704E-01 2.687E-02 O.OOOE+OO 2.181E-01 7.487E-01 -8.330E-01

-6.875E-01 3.103E-01 -1.652E-01 -2.012E-01 O.OOOE+OO 1.262E-01 -9.855E-01 1.700E+OO -5.485E+OO 7.524E+OO 5.140E-01 -3.644E-01 K.L. Cnt Uncert ( 1. 96-sigma) 6.073E+OO 3.285E-01 4.939E+09 2.590E-01 2.536E+OO 8.161E-01 1.864E+OO 5.747E+OO 6.324E-01 7.753E-01 1. 960E+41 6.897E-01 1.725E+OO 1.597E+OO 2.256E+Ol 1.573E+Ol 1.673E+OO 6.076E-01 MDA (pCi/GRAM 4.893E-01 6.389E-01 l.210E+OO 1.351E+Ol 1.303E+OO 5.128E-01 1.314E+OO 8.989E-01 9.496E-01 l.450E+04 1.039E+02 4. 231E+OO MDA (pCi/GRAM 1.069E+Ol 6.130E-01 O.OOOE+OO 5.615E-01 5.009E+OO 1.314E+OO 3.060E+OO 1.048E+Ol 1. 062E+OO 1.299E+OO O.OOOE+OO 1.188E+OO 3.004E+00 2.945E+OO 3.988E+Ol 2.859E+Ol 2.973E+OO 9.908E-01 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN BR-77 -4.754E+02 6.489E+o2* 1.063E+03 FAIL ABUN SR-82 -1. 819E+00 6. 231E+OO 1.054E+Ol NOT IDENT. RB-83 8.277E-01 1.596E+OO 2.032E+OO FAIL ABUN KR-85 2.274E+Ol 9.999E+Ol 1. 782E+02 NOT IDENT. SR-85 1.282E-01 5. 651E-Ol 1.007E+OO NOT IDENT. RB-86 -2.647E+OO 1. 761E+Ol 3.124E+Ol NOT IDENT. Y-88 -9.316E-02 2.892E-01 5.200E-01 NOT IDENT. Y-91 -2. 211E+Ol 2.216E+02 3.987E+02 NOT IDENT. NB-94 2.673E-01 4.533E-Ol 8.093E-01 NOT IDENT. NB-95 3.170E-01 6.798E-Ol 1.191E+O.O NOT IDENT. NB-95M -7.525E-01 1.560E+OO 2.578E+OO NOT IDENT. ZR-95 8.566E-01 1.131E+OO 2.021E+OO NOT IDENT. NB-97 0.000E+OO l.960E+41 O.OOOE+OO SHORT HLIF ZR-97 O.OOOE+OO 1.003E+10 O.OOOE+OO SHORT HLIF M0-99 l.132E+03 1.433E+03 l.560E+03 FAIL ABUN TC-99M O.OOOE+OO 7.589E+24 O.OOOE+OO SHORT HLIF RH-101 9.529E-02 3.257E-01 5.757E-01 NOT IDENT. RH-102 1.736E-01 8.159E-01 l.437E+OO NOT IDENT. RH-106 -8.737E-01 5.319E+OO 8.227E+OO NOT IDENT. RU-106 -8.737E-01 5.319E+OO 8.227E+OO NOT IDENT. AG-108M -8.745E-03 4.956E-01 8.820E-01 NOT IDENT. AG-llOM -9.137E-01 1.007E+OO 1. 630E+OO FAIL ABUN SN-113 3. 096E-01 7.181E-01 1.305E+OO NOT IDENT. CD-115 -2.414E+02 1.166E+03 2.043E+03 NOT IDENT. SB-124 -3. 531E-01 7.538E-01 1.312E+OO NOT IDENT. SB-125 8.206E-01 1.549E+OO 2.802E+OO NOT IDENT. TE-125M 1.033E+Ol 1.042E+02 l.847E+02 NOT IDENT. I-126 2.516E+OO 4.724E+OO 7.595E+OO NOT IDENT. SB-126 -l.828E-01 3.044E+OO 5.241E+OO NOT IDENT. SB-127 -5.lOOE+OO 5.494E+Ol 9.512E+Ol NOT IDENT. I-131 5.600E-01 2.835E+OO 5.149E+OO NOT IDENT. I-132 O.OOOE+OO 1. 960E+41 0.000E+OO SHORT HLIF TE-132 3.491E+OO 3.443E+Ol 5.816E+Ol NOT IDENT. BA-133 2.748E-01 5.901E-01 1.082E+OO NOT IDENT. I-133 O.OOOE+OO 1.181E+07 0.000E+OO SHORT HLIF CS-134 5.910E-01 6.719E-01 1.187E+OO FAIL ABUN CS-135 -5. 726E-02 2.033E+OO 3.383E+OO NOT IDENT. I-135 0.000E+OO 2.535E+23 O.OOOE+OO SHORT HLIF CS-136 -l.162E+OO 2.612E+OO 4.589E+OO NOT IDENT. CE-139 2.746E-01 3. 096E-01 5.506E-01 NOT IDENT. BA-140 3.139E+OO 5.569E+OO 1.004E+Ol NOT IDENT. LA-140 -3.882E-01 8.190E-01 l.440E+OO NOT IDENT. CE-141 4.839E-01 7.159E-01 1.272E+OO NOT IDENT. CE-143 O.OOOE+OO 3.495E+04 O.OOOE+OO SHORT HLIF CE-144 -7. 741E-01 2 .114E+OO 3.648E+OO NOT IDENT. PM-144 -2.054E-02 5.057E-01 8.339E-01 NOT IDENT. PR-144 -1. 579E+OO 3.797E+Ol 6.260E+Ol NOT IDENT. PM-146 3.605E-01 8.337E-01 1.350E+OO NOT IDENT. ND-147 3.074E+OO 1.246E+Ol 2.220E+Ol NOT IDENT. PM-149 1.241E+04 8.285E+03 l.453E+04 NOT IDENT. EU-150 -2. 911E-01 3.482E-01 6.168E-01 FAIL ABUN EU-152 7.043E-01 1.314E+OO 2.421E+OO FAIL ABUN GD-153 6.273E-01 8.571E-01 l.556E+OO NOT IDENT. EU-154 8.668E-02 9.290E-01 1.735E+OO FAIL ABUN EU-155 -5.699E-01 1.056E+OO 1.839E+OO FAIL ABUN TB-160 -2. 213E+OO 2.693E+OO 4.381E+OO FAIL ABUN H0-166M -l.287E-01 8.484E-01 l.459E+OO FAIL ABUN TM-171 -2 .118E+02 3.080E+02 5.520E+02 NOT IDENT. HF-172 -1.315E+OO 1. 962E+OO 3.366E+OO FAIL ABUN LU-172 -4.697E-01 l.182E+OO 2.072E+OO FAIL ABUN LU-176 2.949E-02 3.708E-01 6.141E-01 FAIL ABUN HF-181 2.570E-02 8. 051E-01 l.426E+OO NOT IDENT. TA-182 8.640E-01 l.939E+OO 3.254E+OO NOT IDENT. RE-183 0.000E+OO 1.196E+Ol 9.352E+OO FAIL ABUN RE-184 -1.749E-01 2.844E+OO 4.768E+OO NOT IDENT. W-188 -8.503E+Ol l.042E+02 1. 671E+02 NOT IDENT. IR-192 1.034E-01 5.315E-01 8.819E-01 NOT IDENT. HG-203 -2.234E-01 6.052E-01 9.092E-01 NOT IDENT. BI-207 -5 .154E-02 . 9. 071E-01 l.618E+OO NOT IDENT. TL-208 6.817E-02 4.978E-01 8.808E-01 NOT IDENT. BI-211 1.243E+OO 2.735E+OO 5.025E+OO NOT IDENT. PB-211 3.043E+OO l.040E+Ol 1.883E+Ol NOT IDENT. BI-212 -l.197E+00 7.372E+OO 1. 2 63E+Ol NOT IDENT. PB-212 -7.383E-02 6.855E-01 l.150E+OO NOT IDENT. BI-214 l.834E-01 9.554E-01 1. 689E+OO NOT IDENT. PB-214 3.724E-01 9.999E-01 1.832E+OO FAIL ABUN RN-219 -2. 611E+00 6.060E+OO l.072E+Ol NOT IDENT. RN-222 1.834E-01 9.554E-01 1.689E+OO NOT IDENT. Page 4769 of 5809 RA-223 -4.867E+OO 8.255E+OO l.477E+Ol NOT IDENT. RA-224 9.109E-01 7.575E+00 1. 276E+01 NOT IDENT. RA-226 1.834E-01 9.554E-01 1. 689E+OO NOT IDENT. AC-227 -7. 211E-01 3.245E+OO 5.382E+OO NOT IDENT. TH-227 -7. 211E-01 3.245E+OO 5.382E+OO NOT IDENT. AC-228 -1.644E+00 2.910E+OO 4.773E+OO FAIL ABUN RA-228 -1.644E+OO 2.910E+OO 4.773E+OO FAIL ABUN TH-228 -7.383E-02 6.855E-01 1.150E+OO NOT IDENT. TH-229 l.475E+OO 5.860E+OO 1.008E+Ol FAIL ABUN TH-230 1.834E-01 9.554E-01 1. 689E+OO

  • NOT I DENT .. PA-231 -2.709E+OO 6.486E+OO 1. 054E+Ol NOT IDENT. TH-231 -4.867E+OO 8.255E+OO 1.477E+Ol NOT IDENT. TH-232 -1.644E+OO 2.910E+OO 4.773E+OO NOT IDENT. PA-233 -3.803E-02 9.261E-01 1.524E+OO NOT IDENT. PA-234 5.891E-01 6. 871E+OO l.150E+Ol NOT IDENT. PA-234M 4.607E+Ol 8.094E+Ol 1.482E+02 NOT IDENT. TH-234 -4.166E+OO 1. 272E+Ol 2.127E+Ol NOT IDENT. U-234 1.834E-01 9.554E-01 1.689E+OO NOT IDENT. U-235 -9.682E-01 2. 021E+OO 3.462E+OO NOT IDENT. NP-237 -3.803E-02 9.261E-01 1.524E+OO NOT IDENT. NP-238 O.OOOE+OO 3.092E+03 O.OOOE+OO SHORT HLIF U-238 -4.166E+OO 1.272E+Ol 2.127E+Ol NOT IDENT. NP-239 -5.909E-01 2.681E+OO 4.690E+OO NOT IDENT. PU-239 -l.522E+03 3.490E+03 6.021E+03 NOT IDENT. AM-243 -2.756E-02 5.215E-01 9.356E-01 NOT IDENT. CM-243 9.497E-01 1.090E+OO 1. 981E+OO NOT IDENT. BK-247 -4.077E-01 1.035E+OO 1. 701E+OO NOT IDENT. CM-247 -3.028E-01 5.578E-01 9.831E-01 NOT IDENT. CF-249 -2.765E-01 5.953E-01 1.055E+OO NOT IDENT. CF-251 -3.808E-01 l.372E+OO 2.332E+OO NOT IDENT. ANH-511 -2.276E-03 4.458E-01 7.983E-01 NOT IDENT. Page 4770 of 5809 VAX/VMS Nuclide Identification Report Generated 3-0CT-2016 05:44:24.98 Nuclide Line Activity Report Nuclide Type: Uncorrected Decay Corr 2-Sigma Nuclide Energy Area %Abn %Eff pCi/GRAM pCi/GRAM %Error C0-57 122.06 237 85.60* 7.219E+OO 1.003E+OO 1.059E+OO 44.65 136.47 ------10.68 7.146E+OO ------Line Not Found ------C0-60 1173.23 9009 99.85 1.491E+OO 1.581E+02 1.593E+02 2.26 1332.49 8134 99.98* 1.340E+OO 1.585E+02 1.597E+02 2.21 RU-103 497.08 48 91.00* 2.926E+OO 4.719E-01 6.865E-01 164.14 610.33 ------5.76 2. 491E+OO ------Line Not Found ------CD-109 88.03 3550 3.70* 6.299E+OO 3.978E+02 4.107E+02 5.62 SN-117M 156.02 ------2 .11 6.864E+OO ------Line Not Found ------158.56 82 86.40* 6.837E+OO 3. 631E-01 1. 072E+OO 109.05 TE-123M 159.00 82 84.00* 6.837E+OO 3.735E-01 4.225E-01 109.05 SN-126 64.28 ------9.60 4.012E+OO ------Line Not Found ------86.94 3550 8.90 6.299E+OO 1.654E+02 1.654E+02 5.62 87.57 3550 37.00* 6.299E+OO 3.978E+Ol 3.978E+Ol 5.62 BA-137M 661.66 14813 89.90* 2.339E+OO 1.840E+02 1.842E+02 1. 78 CS-137 661.66 14813 85.10* 2.339E+OO 1.943E+02 1.946E+02 1. 78 PM-147 1'21. 22 237 0.00* 7.219E+OO 3. 013E+04 3.060E+04 44.65 PB-210 46.54 12346 4.25* 1.369E+OO 5. 541E+03 5. 551E+03 2.46 AM-241 59.54 25865 35.90* 3.351E+OO 5.614E+02 5.615E+02 1. 68 Flag: "*" Key line Page 4 771 of 5809 Surrunary of Nuclide Activity Sample ID : G1203621366 Acquisition date Page : 2 3-0CT-2016 05:28:46 Total number of lines in spectrum 28 Number of unidentified lines 13 Number of lines tentatively identified by NID 15 53.57% Nuclide Type :
  • Nuclide Hlife Decay Uncorrected Decay Corr Decay Corr 2-Sigma pCi/GRAM pCi/GRAM 2-Sigma Error %Error C0-57 271. 7 4D 1. 06 1.003E+OO 1.059E+OO 0.473E+OO 44.65 C0-60 5 .27Y 1. 01 l.585E+02 l.597E+02 0.035E+02 2.21 RU-103 3 9. 2 6D 1. 45 4.719E-01 6.865E-01 11.27E-01 164.14 CD-109 461.40D 1. 03 3.978E+02 4.107E+02 0. 231E+02 5.62 SN-117M 13.60D 2.95 3.631E-01 1.072E+OO l.169E+OO 109.05 TE-123M 119.20D 1.13 3.735E-01 4.225E-01 4.608E-01 109.05 SN-126 2.30E+05Y 1. 00 3.978E+Ol 3.978E+Ol 0.224E+Ol 5. 62 BA-137M 30.08Y 1. 00 1.840E+02 1.842E+02 0.033E+02 1. 78 CS-137 30.08Y 1. 00 l.943E+02 1.946E+02 0.035E+02 1. 78 PM-147 2.62Y 1. 02 3.013E+04 3.060E+04 1.366E+04 44.65 PB-210 22.20Y 1. 00 5. 541E+03 5. 551E+03 0.137E+03 2.46 AM-241 432.60Y 1. 00 5.614E+02 5.615E+02 0.094E+02 1. 68 ------------------Total Activity 3. 721E+04 3.770E+04 Grand Total Activity 3. 721E+04 3.770E+04 "M" Manually accepted Flags: "K" Keyline not found "E" = Manually edited "A" = Nuclide specific abn. limit Page 4772 of 5809 Flags Unidentified Energy Lines Page : 3 Sample ID : Gl203621366 Acquisition date : 3-0CT-2016 05:28:46 It Energy Area Bkgnd FWHM Channel Left Pw Cts/Sec %Err %Eff Flags 10 45.21 1348 4874 1. 98 90.29 87 10 1. 37E+OO 19.6 l.17E+OO T 0 281.91 80 623 1. 25 564.01 560 8 8.77E-02 **** 4.65E+OO T 0 455.52 69 646 1. 78 911. 43 908 8 7.75E-02 **** 3.15E+OO 0 519.40 34 .. 368 1. 00 1039.24 1036 8 3.83E-02 ***** 2.83E+OO T 0 619.78 69 227 2.36 1240 .11 1237 7 7.84E-02 75.5 2.46E+OO T 0 690.94 43 200 1. 99 1382.48 1380 8 4.93E-02 **** 2.26E+OO 0 738.07 53 312 1. 80 1476.78 1474 11 6.09E-02 **** 2.15E+OO T 0 795.59 38 189 0.78 1591.86 1589 6 4.41E-02 **** 2.03E+OO T 0 920.85 42 261 1.18 1842.45 1840 6 4.85E-02 **** 1. 81E+OO 0 1215.76 33 93 0.93 2432.38 2428 12 3.86E-02 **** 1. 45E+OO 0 1356.81 11 41 5.80 2714.48 2702 16 l.25E-02 **** l.32E+OO 0 1400.13 12 37 3.28 2801.13 2790 15 l.36E-02 **** l.28E+OO 0 1508.05 16 37 7.53 3016. 96 3003 *21 1. 83E-02 **** l.20E+OO 0 18 61. 65 *10 7 1. 71 3724.04 3718 10 1.19E-02 **** 9.86E-01 0 1865.43 12 2 1. 42 3731. 61 3728 9 l.48E-02 67.4 9.84E-01 0 1943.17 13 3 1. 48 3887.05 3883 8 1. 60E-02 70.6 9.45E-01 0 1961. 35 10 5 3.21 3923.40 3917 12 l.23E-02 **** 9.36E-01 0 1996. 81 9 12 1. 45 3994.30 3987 11 l. llE-02 **** 9.19E-01 0 2032.40 6 4 3.44 4065.45 4058 10 6.97E-03 **** 9.02E-01 Flags: "T" = Tentatively associated Page 4773of5809 VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:44:40.20 *******************************************************************************
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * *
  • DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621366.CNF;l * *Acquisition date 3-0CT-2016 05:28:46 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.51 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621366 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity : 1.1500E+02 GRAM *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff. Cal. date 2-AUG-2016 10:31:39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;14
  • Combined Critical Level Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Nuclide C0-57 C0-60 RU-103 CD-109 SN-ll 7M TE-123M SN-126 BA-137M CS-137 PM-147 PB-210 AM-241 Le (pCi/GRAM 2.386E-01 2.931E-01 5.861E-01 6.600E+00 6.338E-01 2.494E-01 6.420E-01 4.328E-01 4. 572E-01 7.076E+03 5.137E+Ol 2.087E+OO ----Non-Identified Nuclides Nuclide BE-7 NA-22 NA-24 AL-26 K-40 SC-46 V-48 CR-51 MN-54 C0-56 MN-56 C0-58 FE-59 ZN-65 GE-68 AS-73 AS-74 SE-75 BR-77 Page 4774of5809 Le (pCi/GRAM 5.199E+OO 2.809E-01 O.OOOE+OO 2.462E-01 2.239E+OO 6.346E-01 1.479E+OO 5.098E+OO 5.122E-01 6.275E-01 O.OOOE+OO 5.722E-01 1.447E+OO 1.425E+OO 1.923E+Ol 1.413E+Ol 1.433E+OO 4.816E-01 5.177E+02 NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN SR-82 RB-83 KR-85 SR-85 RB-86 Y-88 Y-91 NB-94 NB-95 ZR-95 NB-97 ZR-97 M0-99 TC-99M RH-101 RH-102 RH-106 RU-106 AG-108M AG-110M SN-113 CD-115 SB-124 SB-125 TE-125M I-126 SB-126 SB-127 I-131 I-132 TE-132 BA-133 I-133 CS-134 CS-135 I-135 CS-136 CE-139 BA-140 LA-140 CE-141 CE-143 CE-144 PM-144 PR-144 PM-146 ND-147 PM-149 EU-150 EU-152 GD-153 EU-154 EU-155 TB-160 H0-166M TM-171 HF-172 LU-172 LU-176 HF-181 TA-182 RE-183 RE-184 W-188 IR-192 HG-203 BI-207 TL-208 BI-211 PB-211 BI-212 PB-212 BI-214 PB-214 RN-219 RN-222 RA-223 Page 4775of5809 5.069E+OO 9.835E-01 8.626E+01 4.874E-01 l.506E+01 2.194E-01 1.875E+02 3.889E-01 5.743E-01 1.256E+OO 9.721E-01 O.OOOE+OO O.OOOE+OO 7.515E+02 O.OOOE+OO 2.805E-01 6.927E-01 3. 964E+OO 3. 964E+OO 4.292E-01 7.880E-01 6.352E-01 9.875E+02 5.693E-01 1.365E+OO 8.995E+Ol 3.655E+OO 2.523E+OO 4.565E+Ol 2.503E+OO O.OOOE+OO 2.836E+Ol 5.261E-01 O.OOOE+OO 5.727E-01 1.646E+OO 0.000E+OO 2.213E+OO 2.680E-01 4.854E+OO 6.179E-01 6.195E-01 0.000E+OO 1. 778E+OO 4.007E-01 3.008E+Ol 6.580E-01 1.074E+Ol 7.074E+03 2.994E-01 1.177E+OO 7.590E-01 7.954E-01 8.953E-01 2 .115E+OO 7.003E-01 2.727E+02 1.639E+OO 1.000E+OO 2.984E-01 6.927E-Ol 1.525E+OO 4.637E+OO 2.309E+OO 8.120E+Ol 4. 28'7E-01 4.420E-01 7.800E-01 4.245E-01 2.443E+OO 9.149E+OO 6.075E+OO 5.596E-01 8 .137E-01 8.907E-01 5.208E+OO 8 .137E-01 7 .172E+OO NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF SHORT HLIF FAIL ABUN SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. SHORT HLIF FAIL ABUN NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN FAIL ABUN FAIL ABUN NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT.

RA-224 RA-226 AC-227 TH-227 AC-228 RA-228 TH-228 TH-229 TH-230 PA-231 TH-231 TH-232 PA-233 PA-234 PA-234M TH-234 U-234 U-235 NP-237 NP-238 U-238 NP-239 PU-239 AM-243 CM-243 BK-247 CM-247 CF-249 CF-251 ANH-511 Page 4776 of 5809 6.219E+OO 8.137E-01 2.617E+00 2.617E+OO 2.313E+00 2.313E+OO 5. 596E-01 4.909E+OO 8.137E-01 5.122E+OO 7 .172E+OO 2.313E+OO 7.408E-01 5.587E+OO 7.163E+Ol 1.039E+Ol 8.137E-01 1.685E+OO 7.408E-01 O.OOOE+OO 1.039E+Ol 2.283E+OO 2.933E+03 4.577E-01 9.662E-01 8.267E-01 4.776E-01 5.125E-01 1.135E+OO 3.870E-01 NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. FAIL ABUN FAIL ABUN NOT IDENT. FAIL ABUN NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. SHORT HLIF NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. NOT IDENT. 'NOT I DENT. NOT IDENT. NOT IDENT. VAX/VMS Nuclide Identification Report Generated 03-0CT-2016 05:44:46.13 *******************************************************************************

  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 * ******************************************************************************* * * * < DETECTOR AND SAMPLE DATA * * *
  • Configuration DKAlOO: [CANBERRA.GAMMA.ARCHIVE.GAMMA]Gl203621366.CNF;l * *Acquisition date 3-0CT-2016 05:28:46 Sensitivity : 3.000 *
  • Detector ID GAMll Energy tolerance: 1.500 *
  • Elapsed live time: 0 00:15:00.00 Abundance limit : 75.000 *
  • Elapsed real time: 0 00:15:06.51 Half life ratio : ***** *
  • Sample date 12-SEP-2016 00:00:00 Nuclide Library : SOLID *
  • Sample ID G1203621366 Analyst initials: MXRl *
  • Batch Number 1596254 Sample Quantity 1.1500E+02 GRAM *
  • Quantity Err(%) l.7391E-03 % *
  • Wet wt corr 1.00000 Wet Weight 0.00000 *
  • Dry Weight : 0.00000 * ******************************************************************************* * *
  • CALIBRATION INFORMATION * * *
  • Eff .' Cal. date 2-AUG-2016 10: 31: 39 Eff. Geometry : CAN *
  • Eff. File : DKAlOO: [CANBERRA.GAMMA]EFF GAMll CAN.CNF;14
  • Combined Activity-MDA Report NOTE: Not all "Identified Nuclides" are valid. Please refer to Certificate of Analysis. Identified Nuclides Activity Act Error TPU Nuclide (pCi/GRAM ( 1. 96-sigma) ( 1. 96-sigma) C0-57 l.059E+OO 4.659E-01 4.659E-01 C0-60 1.597E+02 6. 821E+OO 6. 821E+OO RU-103 6.S65E-01 1.105E+OO 1.105E+OO CD-109 4.107E+02 4.043E+Ol 4.043E+Ol SN-ll 7M 1. 072E+OO 1.146E+OO 1.146E+OO TE-123M 4.225E-01 4.520E-01 4.520E-01 SN-126 3.978E+Ol 3.300E+OO 3.300E+OO BA-137M 1.842E+02 8.542E+OO 8.542E+OO CS-137 l.946E+02 9.005E+OO 9.005E+OO PM-147 3.060E+04 1.346E+04 1. 346E+04 PB-210 5.551E+03 4.949E+02 4.949E+02 AM-241 5.615E+02 4.237E+Ol 4.237E+Ol Non-Identified Nuclides Key-Line Activity K.L Act error TPU Nuclide (pCi/GRAM ( 1 . 96-sigma ) ( 1. 96-sigma) BE-7 -8.704E-01 6.073E+OO 6-. 085E+OO NOT IDENT. NA-22 2.687E-02 3.285E-01 3.287E-01 NOT IDENT. NA-24 -4. 711E+08 4.939E+09 4.944E+09 SHORT HLIF AL-26 2.181E-01 2.594E-01 2.774E-01 NOT IDENT. K-40 7.487E-01 2.536E+OO 2.558E+OO NOT IDENT. st-46 -8.330E-01 8.169E-01 8.990E-01 NOT IDENT. V-48 -6.875E-01 1. 864E+OO 1. 889E+OO NOT IDENT. CR-51 3.103E-01 5.747E+OO 5.749E+OO NOT IDENT. MN-54 -l.652E-01 6.324E-01 6.368E-01 NOT IDENT. C0-56 -2.012E-01 7.753E-01 7.806E-01 NOT IDENT. MN-56 -1.000E+41 3.754E+41 O.OOOE+OO SHORT HLIF C0-58 1.262E-01 6.897E-01 6.920E-01 NOT IDENT. FE-59 -9.855E-01 1. 727E+OO 1.783E+OO NOT IDENT. ZN-65 l.700E+OO 1.598E+OO 1. 772E+OO NOT IDENT. GE-68 -5.485E+OO 2.256E+Ol 2.269E+Ol NOT IDENT. AS-73 7.524E+00 l.581E+Ol 1.617E+Ol NOT IDENT. AS-74 5.140E-01 l.674E+OO 1.690E+OO NOT IDENT. SE-75 -3.644E-01 6.079E-01 6.297E-01 FAIL ABUN Page 4777of5809 BR-77 -4.754E+02 7. ll 7E+02 7.433E+02 FAIL ABUN SR-82 -1.819E+OO 6.231E+OO 6.285E+OO NOT IDENT. RB-83 8.277E-01 1.600E+OO 1.643E+OO FAIL ABUN KR-85 2.274E+Ol l.000E+02 l.005E+02 NOT IDENT. SR-85 1.282E-01 5.651E-01 5.680E-01 NOT IDENT. RB-86 -2.647E+OO 1. 7 61E+Ol 1.765E+Ol NOT IDENT. Y-88 -9.316E-02 2.892E-01 2.923E-01 NOT IDENT. Y-91 -2. 211E+Ol 2.216E+02 2.218E+02 NOT IDENT. NB-94 2.673E-01 4.534E-01 4.692E-01 NOT IDENT. NB-95 3.170E-01 6.800E-01 6.948E-01 NOT IDENT. NB-95M -7.525E-01 1.561E+OO 1.598E+OO NOT IDENT. ZR-95 8.566E-01 1.132E+OO 1.196E+OO NOT IDENT. NB-97 1.000E+41 2.345E+41 O.OOOE+OO SHORT HLIF ZR-97 -1.515E+09 l.003E+10 1.006E+l0 SHORT HLIF M0-99 l.132E+03 l.435E+03 l.523E+03 FAIL ABUN TC-99M 2.461E+24 7.593E+24 O.OOOE+OO SHORT HLIF RH-101 9.529E-02 3.262E-01 3.290E-01 NOT IDENT. RH-102 1.736E-01 8.161E-01 8.198E-01 NOT IDENT. RH-106 -8.737E-01 5.320E+OO 5.334E+OO NOT IDENT. RU-106 -8.737E-01 5.320E+OO 5.334E+OO NOT IDENT. AG-108M -8.745E-03 4.956E-01 4.956E-01 NOT IDENT. AG-llOM -9.137E-01 1.008E+OO l.089E+OO FAIL ABUN SN-113 3. 096E-01 7.182E-01 7.317E-01 NOT IDENT. CD-115 -2.414E+02 l.167E+03 1.172E+03 NOT IDENT. SB-124 -3. 531E-01 7.541E-01 7.707E-01 NOT IDENT. SB-125 8.206E-01 1.550E+OO 1.593E+OO NOT IDENT. TE-125M 1.033E+Ol 1. 042E+02 1.043E+02 NOT IDENT. I-126 2.516E+OO 4.726E+OO 4. 861E+OO NOT IDENT. SB-126 -1.828E-01 3.045E+OO 3.046E+OO NOT IDENT. SB-127 -5.lOOE+OO 5.495E+Ol 5.500E+Ol NOT IDENT. I-131 5.600E-01 2.835E+OO 2.846E+OO NOT IDENT. I-132 1.000E+41 4.850E+41 O.OOOE+OO SHORT HLIF TE-132 3.491E+OO 3.443E+Ol 3.447E+Ol NOT IDENT. BA-133 2.748E-01 5.902E-01 6.030E-01 NOT IDENT. I-133 9.890E+05 1.181E+07 1.182E+07 SHORT HLIF CS-134 5.910E-01 6.724E-01 7.232E-01 FAIL ABUN CS-135 -5. 726E-02 2.033E+OO 2.033E+OO NOT IDENT. I-135 7.483E+22 2.561E+23 O.OOOE+OO SHORT HLIF CS-136 -1.162E+OO 2.613E+OO 2.665E+OO NOT IDENT. CE-139 2.746E-01 3.145E-01 3.380E-01 NOT IDENT. BA-140 3.139E+OO 5.571E+OO 5.748E+OO NOT IDENT. LA-140 -3.882E-01 8.192E-01 8.377E-01 NOT IDENT. CE-141 4.839E-01 7.162E-01 7.487E-01 NOT IDENT. CE-143 1.937E+03 3.495E+04 3.496E+04 SHORT HLIF CE-144 -7.741E-01 2 .115E+OO 2.143E+OO NOT IDENT. PM-144 -2.054E-02 5.057E-01 5.058E-01 NOT IDENT. PR-144 -1.579E+OO 3.797E+Ol 3.797E+Ol NOT IDENT. PM-146 3.605E-01 8.341E-01 8.498E-01 NOT IDENT. ND-147 3.074E+00 1. 246E+Ol 1.254E+Ol NOT IDENT. PM-149 1.241E+04 8.452E+03 1.014E+04 NOT IDENT. EU-150 -2. 911E-01 3.484E-01 3. 723E-01 FAIL ABUN EU-152 7.043E-01 1. 315E+OO 1.352E+OO FAIL ABUN GD-153 6.273E-01 8.579E-01 9.033E-01 NOT IDENT. EU-154 8.668E-02 9.290E-01 9.298E-01 FAIL ABUN EU-155 -5.699E-01 1.057E+OO 1.087E+OO FAIL ABUN TB-160 -2.213E+OO 2.696E+00 2.875E+OO FAIL ABUN H0-166M -1.287E-01 8.484E-01 8.504E-01 FAIL ABUN TM-171 -2.118E+02 3.086E+02 3.230E+02 NOT IDENT. HF-172 -l.315E+00 1.974E+OO 2.061E+OO FAIL ABUN LU-172 -4.697E-01 1.183E+OO 1.202E+OO FAIL ABUN LU-176 2.949E-02 3.708E-01 3.710E-01 FAIL ABUN HF-181 2.570E-02 8.051E-01 8.052E-01 NOT IDENT. TA-182 8.640E-01 1.940E+OO 1.978E+OO NOT IDENT. RE-183 7.251E+02 7.537E+Ol 3.355E+02 FAIL ABUN RE-184 -1. 749E-01 2.844E+OO 2.845E+OO NOT IDENT. W-188 -8.503E+Ol l.046E+02 i .114E+02 NOT IDENT. IR-192 l.034E-01 5.316E-01 5.336E-01 NOT IDENT. HG-203 -2.234E-01 6.053E-01 6.136E-01 NOT IDENT. BI-'207 -5.154E-02 9.071E-01 9.074E-01 NOT IDENT. TL-208 6.817E-02 4.978E-01 4.987E-01 NOT IDENT. BI-211 l.243E+OO 2.736E+OO 2.793E+OO NOT IDENT. PB-211 3.043E+OO 1.041E+Ol 1.050E+Ol NOT IDENT. BI-212 -1.197E+OO 7.372E+OO 7.392E+OO NOT IDENT. PB-212 -7.383E-02 6.855E-01 6.863E-01 NOT IDENT. BI-214 1.834E-01 9.554E-01 9.590E-01 NOT IDENT. PB-214 3. 724E-01 1.000E+OO 1.014E+OO FAIL ABUN RN-219 -2.611E+OO 6.069E+OO 6.182E+OO NOT IDENT. RN-222 l.834E-01 9.554E-01 9.590E-01 NOT IDENT. Page 4778of5809 RA-223 -4.867E+OO 8.260E+OO 8.546E+OO NOT IDENT. RA-224 9.109E-01 7.575E+OO 7.586E+OO NOT IDENT. RA-22 6 1.834E-01 9.554E-01 9.590E-01 NOT IDENT. AC-227 -7 .211E-01 3.246E+OO 3.262E+OO NOT IDENT. TH-227 -7. 211E-01 3.246E+OO 3.262E+OO NOT IDENT. AC-228 -1.644E+OO 2. 911E+OO 3.004E+OO FAIL ABUN RA-228 -1.644E+OO 2. 911E+OO 3.004E+OO FAIL ABUN TH-228 -7.383E-02 6.855E-01 6.863E-01 NOT IDENT. TH-229 1. 4 7 5E+OO 5.861E+OO 5.898E+OO FAIL ABUN TH-230 .1. 834E-01 9.554E-01 9.590E-01 .NOT IDENT. PA-231 -2.709E+OO 6.512E+OO 6.625E+OO NOT IDENT. TH-231 -4.867E+OO 8.260E+OO 8.546E+OO NOT IDENT. TH-232 -1.644E+OO 2. 911E+OO 3.004E+OO NOT IDENT. PA-233 -3.803E-02 9.261E-Ol 9.263E-01 NOT IDENT. PA-234 5.891E-01 6.904E+OO 6.909E+OO NOT IDENT. PA-234M 4.607E+Ol 8. 096E+Ol 8.358E+Ol NOT IDENT. TH-234 -4.166E+OO 1.276E+Ol l.289E+Ol NOT IDENT. U-234 l.834E-01 9.554E-01 9.590E-01 NOT IDENT. U-235 -9.682E-01 2.021E+OO 2.068E+OO NOT IDENT. NP-237 -3.803E-02 9.261E-01 9.263E-01 NOT IDENT. NP-238 -5.092E+Ol 3.092E+03 3.092E+03 SHORT HLIF U-238 -4.166E+OO 1. 276E+Ol 1.289E+Ol NOT IDENT. NP-239 -5.909E-01 2.682E+OO 2.695E+OO NOT IDENT. PU-239 -l.522E+03 3.490E+03 3.557E+03 NOT IDENT. AM-243 -2.756E-02 5.215E-01 5.217E-01 NOT IDENT. CM-243 9.497E-01 1.094E+OO l. l 74E+OO NOT IDENT. BK-247 -4.077E-01 1.038E+OO 1.054E+OO NOT IDENT. CM-247 -3.028E-01 5. 601E-01 5.765E-01 NOT IDENT. CF-249 -2.765E-Ol 5.957E-01 6.086E-01 NOT IDENT. CF-251 -3.808E-01 1.373E+OO 1.383E+OO NOT IDENT. ANH-511 -2.276E-03 4.458E-01 4.458E-01 NOT IDENT. Page 4779of5809
  • GEL Laboratories LLC *
  • 2040 Savage Road *
  • Charleston, SC 29407 *
  • GAMMA SPECTROSCOPY BACKGROUND REPORT * ******************************************************************************* ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 43.53 2618.3286 87.09 574.3602 136.47 466.5805 45.60 2295.9553 87.57 574.9335 140.51 458.0647 46.54 2302.7859 88.03 575.4789 143.76 470.6329 49. 72 2052.5364 88.34 575.8425 144.24 465.7786 51. 35 2087.7761 88.47 575.9963 145.44 428.1440 51.87 2133.2341 89. 96 514.3953 152.43 411.4397 52.39 2200.3999 90.64 521.4133 153.25 411. 9122 52.97 2213.6208 91.11 509.2720 154.21 436.3124 53.44 2202.7520 92.59 487.6498 156.02 406.4651 54.07 2265.7490 93.35 495.0458 158.56 419.1790 57.36 0.0000 94.56 480.9595 159.00 416.6023 57.53 2527. 9116 94.65 481.0441 162.33 401.1032 57.98 1623.5559 94.67 481.0633 162.66 401.2816 59.27 1629.2229 94.87 473.6128 163.33 418.6839 59.32 1629.4417 97.43 466.3705 165.86 383.7492 59.54 1630.4014 98.43 501.8722 176.31 423.6350 60. 96 593.2881. 98.44 501. 8842 176.60 423.7902 61.17 593.6157 99.53 518.3389 177.52 437.3008 62.93 614.1212 100 .11 499.6152 181.07 444.6936 63.29 590.9571 102.03 495.6055 181.52 461. 3008 63.58 615.1461 103.18 494.7201 184.41 515.4725 64.28 602.2675 103.37 460.9318 185.72 517.3951 66.73 643.6874 105.21 476.1176 193.51 448.1165 67.24 645.3959 105.31 482.0464 197.03 469.9692 67. 68 661. 3946 106.12 478.8554 198.01 526.1201 67.75 669.6068 106.47 478.1829 201.83 504.9756 69.67 650.1401 109.28 458.0321 203.43 477.9187 70.83 691.8413 111. 00 457.4577 205.31 535.0237 72. 81 652.2618 111.76 448.2135 210.85 533.8355 72. 87 652.3547 114. 06 432.2023 215.65 538.9340 74.66 667. 8727 116. 30 455.7012 222.11 511. 8545 74.82 667.2025 116.74 456.0409 227.09 503.0758 74.97 688.4938 119.76 488.6501 227.38 469.9106 77 .11 676.2043 121.12 535.1235 228.16 492.1386 78.74 664.8212 121.22 535.2092 228.18 492.1517 79.69 677.3201 121.78 507.9825 235.69 492.5087 80.12 657.5864 122.06 508.2184 235. 96 488.0082 80.19 657.6893 122.92 473.8005 238.63 444.0074 80.57 671.2157 123.07 473.9158 238.98 483.6946 81. 00 691. 332 6 123.68 460.9867 240.99 467.1990 81. 07 691.4349 125.81 486.1076 242.00 475.8340 81. 75 643.1959 127.23 463. 9622 244.70 493.4945 83.79 687.0913 127.91 447.2640 252.40 459.5306 84.00 681.1681 129.30 489.8246 252.80 446.7430 85.43 711. 9550 131.20 464.8449 254.15 0.0000 86.55 573.7169 133.02 505.9448 256.23 424.5705 86.79 574.0012 133.52 493.0601 260.90 445.4727 86.94 574.1830 136.00 492.8900 264.66 433.9385 Page 4780of5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 264.80 433.9940 364.49 392.7467 600.60 218.7646 265.00 411. 4247 366.42 389.8445 602.52 0.0000 268.22 431.7943 372.51 382.8962 604. 72 243.1263 269.46 415.5253 375.05 376.6374 607.14 227.4619 270.03 430.1251 1093.63 364.2362 609.32 219.7135 271.23 441. 3911 383.85 6331 610.33 227.8145 273.65 424.3476 388.16 416.1580 614.28 208.2370 276.40 406.1216 388.63 436.4929 618.01 219.6416 277.37 412.5125 391.69 419.8206 620.36 218.3939 277.60 403.7488 400.66 398.5107 621. 93 239.6548 278.00 379.7645 401.81 405.0352 630.19 0.0000 279.20 425. 2725 402.40 410.5131 631.29 224.0867 279.54 430.2463 404.85 366.7946 633.25 199.0360 279.70 430.3007 410.95 416.4634 634.78 253.7780 280.46 419.3050 413. 71 404. 7250 635.95 230.6533 283.69 407.5825 414.70 416.6145 636.99 215.5828 284.31 399.7167 423. 72 441. 5823 645.85 247.9912 285.41 377.4304 427.09 438.9460 657.76 245.2832 285.90 359.7654 427.87 439.1739 657.90 0.0000 287.50 415.0422 433.94 431.8445 661.66 222.1742 290.67 429.6230 439.40 470.5968 664.57 0.0000 293.27 0.0000 453.88 451.0601 666.33 192.3828 295.22 437.4470 463.37 467.5350 666.50 172.3887 295. 96 407 .'0769 468.07 489.2217 667.71 0.0000 298.58 387.1074 473.00 470.2685 677.62 199.0470 299.98 402.3333 475.06 442.0664 685.70 191.4889 300.09 402.3633 476.78 417.4206 695.00 188.6489 300 .13 402.3832 477.60 423.2022 696.49 200.9355 301.36 411.4250 482.18 373.0631 696. 51 200.9434 302.85 389.7443 487.02 361.9622 697.00 199.7344 304.50 403.8801 492.35 329.3196 697.30 198. 7252 304.85 403.9899 497.08 309.0581 697.49 180.0112 306.78 386.0867 505.52 334.6622 702.65 179.3766 308.46 411. 4133 507.63 0.0000 706.68 205.8095 311. 90 398.9283 511. 00 309.1501 711. 68 194.7415 316.51 390. 4572 514.00 292.5724 720.70 221.7749 319.41 397.6359 514.00 292.5724 721. 93 0.0000 320.08 409.5263 520.40 265.9786 722.78 216.7124 321.04 387.3181 520.69 278.8962 722.91 215.6771 323.87 406.6018 522.65 0.0000 723. 31 200.9790 325.23 401.1840 527.90 290.0668 724.19 207.3726 328.76 413.2432 528.26 273.8390 727. 33 215.0317 333.37 381. 0256 529.59 281.7141 733.00 197.5842 333.97 403.1375 529.87 0.0000 735.93 220.5726 334.37 402.4202 531.02 269.4632 737.46 211.1895 338.28 370.6497 537.26 257.8693 739.50 215.0762 338.32 370.6586 546.56 0.0000 747.24 215.7784 340.48 424.6860 552.55 241.5632 748.06 186.0799 340.55 424.7064 563.25 226.3454 752.31 215.1675 344.28 376.6203 569.33 242. 7223 753.82 190.7848 345.93 385.6104 569.50 240.7949 756.73 181. 4136 351.06 375.1578 569.70 235.9203 756.80 181. 4205 351. 93 381. 3939 583.19 225.7294 763.94 211. 9219 355.39 0.0000 584.27 221.9147 765.81 223.8654 356.01 391.1421 595.83 223.2056 766.42 229.2820 Page 4781 of 5809 ENERGY MDA COUNTS ENERGY MDA COUNTS ENERGY MDA COUNTS 766.84 223.9589 1002.74 257.5192 1678.03 0.0000 772.60 0.0000 1004.73 262.9395 1690.97 19.9069 776.52 222.6918 1021. 30 0.0000 1750.46 0.0000 777.92 224.9709 1025.87 0.0000 1764.49 14.8938 778.90 227. 2096 1028.54 0.0000 1770.23 15.9760
  • 783.70 226.5686 1037.84 1771.35 11. 7184 785.37 223.4835 1038.76 0.0000 1791.20 0.0000 792.07 256.5571 1046.59 250.5194 1808.65 8.5864 794.95 200.4995 1048.07 261. 3054 1810.72 0.0000 795.86 223.3343 1049.04 259.5991 1836.06 12.9500 801.95 235.8250 1050.41 257.0378 810.06 235.4854 1063.66 241.1444 810.29 227.8794 1077.00 248.4276 810.45 227.8879 1077.34 248.4445 810.76 222.4692 1085.87 273.3848 815.77 241.4759 1093.63 274.9356 818.51 248.2997 1099.45 255.5533 832.01 244.0862 1112. 07 281.0132 834.85 257.5657 1112.84 291.0434 835. 71 256.5503 1115.54 254.0747 836.80 0.0000 1120.29 233.5337 846.75 0.0000 1120. 55 233.5494 846.77 283.0521 1121.30 216.3412 856.80 276.35'09 1129. 67 157.6471 860.56 271.1839 1131. 51 0.0000 871. 09 281.1621 1147.95 0.0000 873.19 267.9785 1173.23 131.9765 875.33 0.0000 1177.95 131.5966 879.38 295.4531 1189.05 104.7650 880.51 288.8538 1204.77 85. 6716 883.24 290.2579 1221.41 62.8687 884.68 319.5697 1231. 02 57.2210 889.28 314.4873 1235.36 51.6565 894.76 306.0996 1238.28 55.4565 898.04 281. 6772 1260.41 0.0000 900.72 302.2524 1271.87 40.7875 903.28 310.4268 1274.44 38.9180 911.20 348.6556 1274.54 38.9180 912.08 322.7240 1291.59 35.2814 923.98 0.0000 1298.22 0.0000 926.50 357.3769 1312 .11 32.5972 929 .11 332.6348 1332.49 41.4437 937.49 367.8840 1362.66 0.0000 944.13 359.5617 1365.19 23.3262 946.00 376.9792 1368.63 0.0000 949.00 359.0152 1384.29 12.6953 954.55 0.0000 1408.01 20.6296 962.31 349.1355 1457.56 0.0000 964.08 338. 9685 1460.82 18.9061 966 .17 316.1324 1489.16 23.0393 968. 97 321.0416 1505.03 19.1032 983.53 294.7624 1584.12 14.3324 984.45 0.0000 1596. 21 17.4503 996.26 266.8778 1620.50 13. 4158 1001.03 256.5002 1621. 92 10.3235 Page 4782of5809 Page 4783 of 5809 Continuing Calibration Data 1f;:; \,,Cfc. {c_ce: d Ol-d Review of Gamma Spectrometer QA results (Daily calibration & background checks) 27-SEP-2016 10:19:49.31 Run Date Detector Parameter Flag 27-SEP-2016 GAMOl All Parameters Passed 27-SEP-2016 GAM02 All Parameters Passed 5-JUL-2016 GAM03 Cal Check may not have run since 27-SEP-2016 t-18-SEP-2016 GAM03 Bkg Check may not have run since 27-SEP-2016 27-SEP-2016 GAM05 Cal Check PSFWHM-662 Investigate O:tl 27-SEP-2016 GAM05 Cal Check PSFWHM-59 Action Bc.,\a1v' \. Ol'.' 27-SEP-2016 GAM06 All Parameters Passed 27-SEP-2016 GAM07 Cal Check PSFWHM-59 Investigate O\( 27-SEP-2016 GAM08 All Parameters Passed 27-SEP-2016 GAM09 All Parameters Passed 25-SEP-2016 GAMlO Cal Check may not have run since 27-SEP-2016-)k: 24-SEP-2016 GAMlO Bkg Check may not have run since 27-SEP-2016f\Ol J L-l.'3-'< 27-SEP-2016 GAMll Cal Check PSFWHM-662 Investigate OJ( 27-SEP-2016 GAM12 All Parameters Passed -----------GAM13 Cal Check may not have run since 27-SEP-2016¢?" 3-JUL-2016 GAM13 Bkg Check may not have run since 27-SEP-2016 27-SEP-2016 GAM14 All Parameters Passed 27-SEP-2016 GAM16 Cal Check NLACTVTY-662 Investigate 0'< 27-SEP-2016 GAM16 Cal Check NLACTVTY-59 Investigate 10-AUG-2016 GAM17 Cal Check may not have run since 25-SEP-2016 GAM17 Bkg Check may not have run since 27-SEP-2016 27-SEP-2016 GAM18 All Parameters Passed 27-SEP-2016 GAM19 All Parameters Passed 27-SEP-2016 GAM20 All Parameters Passed -----------GAM21 Cal Check may not have run since 27-SEP-2016
  • 25-SEP-2016 GAM21 Bkg Check may not have run since 27-SEP-2016 8-JUL-2016 GAM22 Cal Check may not have run since 27-SEP-2016
  • 7-AUG-2016 GAM22 Bkg Check may not have run since 27-SEP-2016 27-SEP-2016 GAM24 All Parameters Passed Page 4784of5809 27-SEP-2016 GAM25 All Parameters Passed 25-SEP-2016 GAM26 Cal Check may not have run 24-SEP-2016 GAM26 Bkg Check may not have run 27-SEP-2016 GAM27 All Parameters Passed 27-SEP-2016 GAM28 Cal Check NLACTVTY-662 27-SEP-2016 GAM29 Cal Check PSFWHM-662 27-SEP-2016 GAM29 Cal Check NLACTVTY-59 27-SEP-2016 GAM30 All Parameters Passed 27-SEP-2016 GAM31 Bkg Check BACKRATE 27-SEP-2016 GAM32 All Parameters Passed 27-SEP-2016 GAM33 All Parameters Passed 27-SEP-2016 GAM36 All Parameters Passed 27-SEP-2016 GAM39 All Parameters Passed -----------GAM40 Cal Check may not have run 26-JUN-2016 GAM40 Bkg Check may not have run 27-SEP-2016 GAM41 All Parameters Passed Weekly Background check completed on 27-SEP-2016. No daily Bkg Check necessary. 27-SEP-2016 GAM43 All Parameters Passed 27-SEP-2016 GAM44 All Parameters Passed 27-SEP-2016 WELL Cal Check PSFWHM-1332 27-SEP-2016 XRAYl All Parameters Passed 27-SEP-2016 XRAY2 All Parameters Passed 27-SEP-2016 XRAY3 Cal Check PSFWHM-59 27-SEP-2016 XRAY3 Cal Check PSFWHM-109 27-SEP-2016. XRAY3 Cal Check PSFWHM-210 27-SEP-2016 XRAY3 Bkg Check BACKRATE 27-SEP-2016 XRAY4 All Parameters Passed 27-SEP-2016 XRAY5 All Parameters Passed 27-SEP-2016 XRAY6. All Parameters Passed ttf 11L1.t; APPROVAL DATE: APPROVAL TIME: Lo\ 1..) .., f2i 1 APPROVED BY: PROCEDURE # GL-RAD-I-001 Page 4785 of 5809 since 27-SEP-2016--/v 0o'i' since 27-SEP-2016 tA$C!..J Investigate o1( Investigate D'(' Investigate rl/t_ Investigate C\L since 27-SEP-2016"/v since 27-SEP-2016 Investigate t:?l( Action ..A? Action ':14 Action Action if';:;. Luc..."(:_cd CA_.,t;..\ Review of Gamma Spectrometer QA results (Daily calibration & background checks) 28-SEP-2016 09:34:33.92 Run Date Detector Parameter Flag 28-SEP-2016 GAMOl All Parameters Passed 28-SEP-2016 GAM02 All Parameters Passed 5-JUL-2016 GAM03 Cal Check may not have run since 18-SEP-2016 GAM03 Bkg Check may not have run since 28-SEP-20161 28-SEP-2016 GAM05 Cal Check NLACTVTY-662 28-SEP-2016 GAM05 Cal Check NLACTVTY-59 Investigatecr-28-SEP-2016 .GAM05 Cal Check PSFWHM-59 Investigate0/( 28-SEP-2016 GAM06 Bkg Check BACKRATE Investigate<l.ll 28-SEP-2016 GAM07 Cal Check PSFWHM-59 Investigate oiJ( 28-SEP-2016 GAM08 All Parameters Passed 28-SEP-2016 GAM09 Cal Check PSFWHM-662 Investigate 28-SEP-2016 GAM09 Cal Check NLACTVTY-1332 Investigate O)(_ 28-SEP-2016 GAMlO All Parameters Passed 28-SEP-2016 GAMll All Parameters Passed 28-SEP-2016 GAM12 Cal Check PSFWHM-1332 Investigate ei'f------------GAM13 Cal Check may not have run since 28-SEP-2016 "/1r 3-JUL-2016 GAM13 Bkg Check may not have run since 28-SEP-2016 28-SEP-2016 GAM14 All Parameters Passed 28-SEP-2016 GAM16 Cal Check NLACTVTY-59 Investigate OIL 10-AUG-2016 GAMl 7 Cal Check may not have run since 28-SEP-2016js> 25-SEP-2016 GAM17 Bkg Check may not have run since 28-SEP-2016 28-SEP-2016 GAM18 All Parameters Passed 28-SEP-2016 GAM19 Cal Check PSFWHM-662 28-SEP-2016 GAM20 All Parameters Passed -----------GAM21 Cal Check may not have run since 25-SEP-2016 GAM21 Bkg Check may not have run since 28-SEP-2016 8-JUL-2016 GAM22 Cal Check not have run since 7-AUG-2016 GAM22 Bkg Check may not have run since 28-SEP-2016 28-SEP-2016 GAM24 All Parameters Passed Page 4786 of 5809 28-SEP-2016 GAM25 All Parameters Passed 28-SEP-2016 GAM26 Cal Check PSFWHM-1332 28-SEP-2016 GAM27 Cal Check PSFWHM-1332 Investigatec,K 28-SEP-2016 GAM28* All Parameters Passed 28-SEP-2016 GAM29 Cal Check NLACTVTY-662 Investigate D( 28-SEP-2016 GAM30 Cal Check PSFWHM-662 28-SEP-2016 GAM30 Cal Check NLACTVTY-59 Investigate 28-SEP-2016 GAM31 Cal Check NLACTVTY-662 Investigate Dl< 28-SEP-2016 GAM31 Cal Check NLACTVTY-1332 Investigate c.>\(_ 28-SEP-2016 GAM32 All Parameters Passed 28-SEP-2016 GAM33 All Parameters Passed 28-SEP-2016 GAM36 All Parameters Passed 28-SEP-2016 GAM39 All Parameters Passed -----------GAM40 Cal Check may not have run since 26-JUN-2016 GAM40 Bkg Check may not have run since 28-SEP-2016 28-SEP-2016 GAM41 All Parameters Passed 28-SEP-2016 GAM43 All Parameters Passed 28-SEP-2016 GAM44 Cal Check NLACTVTY-1332 Investigate Oil.. 28-SEP-2016 WELL All Parameters Passed 28-SEP-2016 XRAYl Cal Check NLACTVTY-109 Investigate O'/( 28-SEP-2016 XRAY2 All Parameters Passed 27-SEP-2016 XRAY3 Cal Check may not have run since 28-SEP-2016; 25-SEP-2016 XRAY3 Bkg Check may not have run since 28-SEP-2016 28-SEP-2016 XRAY4 All Parameters Passed 28-SEP-2016 XRAY5 All Parameters Passed 28-SEP-2016 XRAY6 All Parameters Passed APPROVAL DATE: \ \6 APPROVAL TIME: 30 APPROVED BY : i?-+-PROCEDURE # GL-RAD-I-001 Report completed at 28-SEP-2016 09:38:38.88 Page 4787of5809 Review of Gamma Spectrometer QA results (Daily calibration & background checks) 29-SEP-2016 08:42:59.81 . . Run Date Detector Parameter Flag 29-SEP-2016 GAMOl Cal Check PSFWHM-1332 Investigate OI( 29-SEP-2016 GAM02 Cal Check PSFWHM-662 Investigate CfJl 5-JUL-2016 GAM03 Cal Check may not have run since 18-SEP-2016 GAM03 Bkg Check may not have run since 29-SEP-2016 29-SEP-2016 GAM05 Cal Check PSFWHM-59 Action lo\( 29-SEP-2016 GAM06 All Parameters Passed 29-SEP-2016 GAM07 All Parameters Passed 29-SEP-2016 GAM08 Cal Check PSFWHM-662 . ol( Investigate (!..\( 29-SEP-2016 GAM08 Cal Check NLACTVTY-59 Investigate 29-SEP-2016 GAMOB Cal Check PSFWHM-59 Investigate (!)\( 29-SEP-2016 GAM09 Cal Check PSFWHM-662 Investigate Cll( 29-SEP-2016 GAMlO Bkg Check BACKRATE Investigate q( *29-SEP-2016 GAMll All Parameters Passed 29-SEP-2016 GAM12 All Parameters Passed -----------GAM13 Cal Check may not have run since 3-JUL-2016 GAM13 Bkg Check may not have run since 29-SEP-2016 29-SEP-2016 GAM14 All Parameters Passed 29-SEP-2016 GAM16 Cal Check NLACTVTY-1332 Investigate e>l(__ 10-AUG-2016 GAM17 Cal Check may not have run since 29-SEP-2016:/P 25-SEP-2016 GAM17 Bkg Check may not have run since 29-SEP-2016. 29-SEP-2016 GAM18 All Parameters Passed 29-SEP-2016 GAM19 All Parameters Passed 29-SEP-2016 GAM20 All .Parameters Passed -----------GAM21 Cal Check may not have run since 29-SEP-2016 t 25-SEP-2016 GAM21 Bkg Check may not have run since 29-SEP-2016 ' 8-JUL-2016 GAM22 Cal Check may not have run since 29-SEP-2016 t 7-AUG-2016 GAM22 Bkg Check may not have run since 29-SEP-2016 29-SEP-2016 GAM24 All Parameters Passed 29-SEP-2016 GAM25 All Parameters Passed Page 4788of5809 29-SEP-2016 GAM26 All Parameters Passed 29-SEP-2016 GAM27 All Parameters Passed 29-SEf-2016 GAM28 All Parameters Passed
  • 29-SEP-2016 GAM29 Cal Check NLACTVTY-59 Investigate Ol( 29-SEP-2016 GAM30 All Parameters Passed 29-SEP-2016 GAM31 All Parameters Passed 29-SEP-2016 GAM32 All Parameters Passed 29-SEP-2016 GAM33 All Parameters Passed 29-SEP-2016 GAM36 All Parameters Passed 29-SEP-2016 GAM39 All Parameters Passed -----------GAM40 Cal Check may not have run since 29-SEP-2016 t-26-JUN-2016 GAM40 Bkg Check may not have run since 29-SEP-2016 29-SEP-2016 GAM41 All Parameters Passed 29-SEP-2016 GAM43 All Parameters Passed 29-SEP-2016 GAM44 All Parameters Passed 29-SEP-2016 WELL All Parameters Passed 29-SEP-2016 XRAYl All Parameters Passed 29-SEP-2016 XRAY2 All Parameters Passed 27-SEP-2016 XRAY3 Cal Check may not have run since 29-SEP-2016 25-SEP-2016 XRAY3 Bkg Check may not have run since 29-SEP-2016 29-SEP-2016 XRAY4 All Parameters Passed 29-SEP-2016 XRAY5 All Parameters Passed 29-SEP-2016 XP..AY6 Cal Check PSFWHM-210 Investigate c>t( 29-SEP-2016 XP..AY6 Bkg Check BACKRATE Investigate APPROVAL DATE: \ APPROVAL TIME: q l7 APPROVED BY: \2-t PROCEDURE # GL-RAD-I-001 Report completed at 29-SEP-2016 .08:47:14.82 Page 4789of5809
  • _ L c cJ ot.-4 Review of Gamma Spectrometer QA results (Daily calibration & background checks) 3-0CT-2016 09:29:18.00 Run Date Detector Parameter 3-0CT-2016 GAMOl Cal Check NLACTVTY-662 3-0CT-2016 GAM02 Cal Check PSFWHM-59 5-JUL-2016 GAM03 Cal Check may not have run 18-SEP-2016 GAM03 Bkg Check may not have run 3-0CT-2016 GAM05 Cal Check NLACTVTY-662 3-0CT-2016 GAM05 Cal Check PSFWHM-59 3-0CT-2016 GAM06 Cal Check NLACTVTY-662 3-0CT-2016 GAM06 Cal Check NLACTVTY-1332 3-0CT-2016 GAM07 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAM08 Cal Check NLACTVTY-662 3-0CT-2016 GAM09 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAMlO Cal Check NLACTVTY-662 3-0CT-2016 GAMll All Parameters Passed Weekly Background check completed on 3-0CT-2016 No daily Bkg Check necessary. 3-0CT-2016 GAM12 Cal Check PSFWHM-59 -----------GAM13 Cal Check may not have run 3-,JUL-2016 GAM13 Bkg Check may not have run 3-0CT-2016 GAM14 Cal Check PSFWHM-59 3-0CT-2016 GAM16 Cal Check NLACTVTY-1332 10-AUG-2016 GAM17 Cal Check may not have run 3-0CT-2016 GAM18 Cal Check PSFWHM-1332 3-0CT-2016 GAM18 Cal Check PSFWHM-59 3-0CT-2016 GAM19 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAM20 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. Page 4790 of 5809 Flag Investigate 0 K. Investigate Ci(l since 3-0CT-2016 since 3-0CT-2016 Investigate alt_ Action l CJ \2 Investigate Investigate Investigate of(_ Investigate c.irt since since 3-0CT-2016 Action ...... s 1' c I( InvestigateOll. since Investigate cl(. Investigate CJ((

GAM21 Cal Check may not have run since 3-0CT-2016 25-SEP-2016 GAM21 Bkg Check may not have run since 3-0CT-2016 8-JUL-2016 GAM22 Cal Check may not have run since 3-0CT-2016)"h-7-AUG-2016 GAM22 Check may not have run since 3-0CT-20],6 3-0CT-2016 GAM24 *All Parameters Passed Weekly Background check completed on 3-0CT-2016 _No daily Bkg Check necessary. 3-0CT-2016 GAM25 Cal Check PSFWHM-662 3-0CT-2016 GAM26 All Parameters Passed 3-0CT-2016 GAM27 Cal Check PSFWHM-662 3-0CT-2016 GAM28 All Parameters Passed Weekly Background check completed on 3-0CT-2016 No .daily Bkg Check necessary. 3-0CT-2016 GAM29 Cal Check NLACTVTY-1332 3-0CT-2016 Cal Check NLACTVTY-59 3-0CT-2016 GAM31 Cal Check PSFWHM-662 3-0CT-2016 GAM32 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAM33 Cal Check PSFWHM-662 3-0CT-2016 GAM36 Cal Check PSFWHM-662 3-0CT-2016 GAM39 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. * "J_ l C>[( Action P Investigate ol(, Investigate Investigate l'l( Investigate Ol( Investigate tP/( 26-JUN-2016 GAM40 GAM40 Cal Check may not have run since Bkg Check may not have run since 3-0CT-2016('r 3-0CT-2016 GAM41 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAM43 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 GAM44 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 WELL Cal Check PSFWHM-1332 3-0CT-2016 XRAYl All Parameters Passed Weekly Background check completed on 3-0CT-2016 . 'No daily Bkg Check necessary. Page 4791 of 5809 3-0CT-2016 XRAY2 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 XRAY3 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 XRAY4 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg*check necessary. 3-0CT-2016 XRAY5 All Parameters Passed Weekly Background check completed on 3-0CT-2016 . No daily Bkg Check necessary. 3-0CT-2016 XRAY6 All Parameters Passed Weekly Background check completed on 3-0CT-2016 No daily Bkg Check necessary. APPROVAL DATE: lD l \ APPROVAL TIME: l l. i \l APPROVED BY: PROCEDURE # GL-RAD-I-001 Report completed at 3-0CT-2016 09:33:35.49 Page 4792 of 5809 Page 4793 of 5809 Background and Efficiency Data QA filenal""le Paral""leter NaMe Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM01_500MLMB.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:13:18 through 1-0CT-2016 12:00:00 57.5400 through 61.5400 61 ............ * ............. * ............ * ............. * ............. * .......... .. ....... """ N I a: 0::: LLJ z LLJ . . . . . 60 ........... * ............. * ...................................................... . :,..::: a: LLJ 59 .................................................................. '* ............ . CL 58 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Til""le UP LOW QA filena!'le Paral'leter Nal'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM01_500MLMB.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13:18 through 1-0CT-2016 12: 00: 00 1.02147 +-5. 951646E-02 (5.83 %) ..-! v N I ::E <J: E I 3 u_* :::..::: <I: UJ 0.. 1.1 1 . x . . . x . . : x : x: xx : x : -* ........................................ *X ................................ . . . . x xx . . X *X X : X X :x x*X X X x x xx x . x x x x . x x >x x x . >¢< x . x xx xx x

  • x x ;.x* x x X X X x>X : )( X X * ',( : X X . X : ' X xx 0 xx;i_xx
  • f:-. * * %
  • x *; >><:,* :,_ x;<* ><#. .. *'* X.. ;,_" .. x. "; X ....... t> .': . . \* . ". ... x ... . ;\ . X -X X X X X* x x: *X x I .g r-* * * * * * * * * * * *, * * * * * * * * * * ' * ., * * * * * * * * * * * * ,* * * * * * * * * * * * *' * * * * * * * * * * * * *o * * * * * ' * * * * * *
  • x . 8 -* ........... ; ............. ; ............ ; ............. ; ............. ; ............ . 4-16 5-16 6-16 7-16 8-16 9-16 Measure!'lent Date/Til'le ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM01_500MLMB.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-201606:13:18 through 1-0CT-2016 12: 00:00 63306.3 +-2800.78 (4.42 %) H t-u a: D LLJ t-u LL.I 0:: Ct:: D u. >-a: u LL.I D 70000 65000 60000 ' . . . . . . . . x . . -* .......................................................................... . . . . . . v x x x x xxx x Xx x *x x x x x x x x x x x: x x ,.,., x x x-""" . x x.,: x xx x x x x'. x . x 0 x . 0 . . -* .x * * * * >.:: * * * *:'1-* * * * )'.( *
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  • 0 x x x x x x x :x x x *x x x x ACT INV MEAN 1. 4 -* * * * * * * * * * * ** * * * * * . . . . . . . .. . . . . . . . . . . . . .. . . . . . . . . . . . ... . . . . . . . . . . . .. . . . . . . . . . . . . . INV I I I I I ACT 4-16 7-16 5-16 8-16 9-16 6-16 Measuref"fJent Date/Tif"fJe QA filenarrie Pararrieter NaMe Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM02_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-201607:17:47 through 1-0CT-2016 12:00:00 57.5400 through 61.5400 61 ............ * ............. * ........... '* ............. * ............. * ............ . ..... ""'" N I :a:: <I (!) Ct'. LLJ z LLJ 60 . . . . . ............................................................................ . . . . . ::..:: <I LLJ 59 ................................................................................ . Q. 58 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie UP LOW QA filenaMe ParaMe ter NafY'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM02_CAN.QAF; 1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 07:17:47 through 1-0CT-2016 12:00:00 1.13371 +-3. 136154E-02 (2.77 %) 1.2 -* ' o ' ' o ' o o o ' II o o 0 o I o o o o I I o : o I I o o o o o o o o o ', o o 0 o o o I o o 0 0 o 0 o o I 0 o o o 0 I o o o 01 0 o o o o I I o o o o o o .-I """ N I E <r: E I 3 LL ::..:: <r: UJ 0. x x x x x x x v x xx x . . . . . x x x x x £ 0 x xx ,*, r x x x , ' x x x: x . x v "A x x x x x x xx x x* x x :x x x x x xx x x?<x x x >s< x x x x :xx
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  • X X X X x . x x x x . x >'<< x .;<-v w 0:: 0.:: x 0 u >-a: u UJ x x x x x x x xx D 62000 ,_, ............... ' ..................... '" ......................... ... . . x . . x . . x . . . . . >'<< x x x x x x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenaf"!'le Paraf"l'leter Naf"!'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM05.QAF;1 BACKRATE (SpectruM Background Rate) 3-APR-2016 12:18:01 through 1-0CT-2016 12:00: 00 1.53310 +-2.296009E-02 (1.50 %) 1. 6 -* ................. r... ............................................................. . 'D c ::::; 0 J,... "0.0 .Y. (J llj CCI E ::::; J,... "'-' (J" ID D.. (f) 1.55 1.5 x x X* . . . -* ................................................... *'* ..................... x ... . x x x x x x .x x x x x x . . . . x x x* x x x :x -* .......................................................................... . x . . x . x . . I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tif"!'le ACT INV MEAN INV ACT QA filenaMe DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM06_500MLMB.QAF;1 ParaMeter NaMe PSENERGY-59 (PEAK ENERGY AM-241) Start/End Dates 4-APR-201606:13:24 through 1-0CT-2016 12: 00: 00 Lower/Upper LMts: 57.5000 through 61. 5000 UP 61 ........... * ............. * .............. * ........... *.* ........... * ............. . 60 59 . . . . . ............................................................................ . . o o o o I 58 ............................................................................ -. . . . . 4-16 5-16 6-16 7-16 8-16 9-16 LOW MeasureMent Date/TiMe QA filenaMe . ParaMeter NaMe Start/End Dates Mean +-Std Dev x x x DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM06_500MLMB.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13: 24 through 1-0CT-2016 12: 00:00 0.936438 +-4.566342E-02 (4.88 %) x x x x *x . . . . x x 1 . x . x* x x . x ......... -: ............ ?!:* .. ....... * ............. * .. .:>< .... .-..... ><' *:* .. . XX:X X X . X X x X X )(:X "<"! ""'" N I ::?::: a: ::?::: I 3 LL :::..:: a: UJ 0.. x x x x x xx x x x x x. xx x xx x x x X* X x x :x X X Xv: X xX x x x x x xx x x "X A ;<.. xx x x x x
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  • I I I I 9-01 9-08 9-15 9-22 9-29 Measurer.-.ent Date/Tir.-.e ACT INV MEAN INV ACT QA filenarrie Pararrie ter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM07.QAF;1 BACKRATE (Spectrurri Background Rate) 3-SEP-2016 10:23:03 through 1-0CT-2016 12:00:00 1.33664 +-2.151268E-02 (1.61 %) 1. 4 -* .................. * ................. * ................... : ................. *.* . 1. 35 -* ................. * ................... * .................. * ................... * .. x x x X* 1. 3 -* .................. * ................. * .................... * ................. *.* . ... ACT INV MEAN INV I I I 10-01 ACT I 9-03 9-10 9-17 9-24 Measurerrient Date/Tirrie QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA10G: [CANBERRA.GAMMA.5CU5R.QA]QCC_GAM08_JAR.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:13:29 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 ..--! v N I E a: (t'. LL.I z LL.I ::...::: a: LL.I 0... 61 ........... * ............. * .............. * ........... *.* ........... * ............. . 60 : : : : : x x ;.s: xx * ;;:. x ::><< x x x x : x< x Xf:-;? x . . . . . x xx x x x 59 ........... *:* ........... -:* .......... *:-........... *:* ........... -: ....... *x. *x. 58 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOuJ QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev x DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM08_JAR.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13:29 through 1-0CT-2016 12:00: 00 1.07206 +-3.912322E-02 (3.65 %) x: x x x ' x X Xx X X XX X X :x x x x: x: x X :X X X X X X X X x ....... "'3" 1.1 N I ::?:: a: ::?:: X X* XX: X
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  • x* *** * * * * * * * * * * * .. * * * * * * * * * * * * * . . . x . . x x I I I I. I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM08_JAR.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:13:29 through 1-0CT-2016 12:00:00 59199.1 +-2092. 11 (3.53 %) x 65000 -* ............................................................................... . H 1-u a: D LLl 1-u LLl 0::: 0::: Cl u :r a: u LLl D 60000 x 65000 4-16 x x x x x x Xx x x x *X x V* I 5-16 x x x '** x x xx . x *X 0 I 6-16 xx x x *x x x x x x x *X I 7-16 x x x >&< x x *x :x x x. XX* * *X I 8-1*6 Measurer.-.ent Date/Tir.-.e y x x >X x x x x x: x x x. x :x x v I 9-16 x x x v x x x x x x x x ACT INV MEAN INV ACT QA filenar.-.e Parar.-.eter Nar.-.e Start/ End Da*tes Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM08.QAF;1 BACKRATE (Spectrur.-. Background Rate) 3-APR-2016 12:18:12 through 1-0CT-2016 12:00:00 1.43104 +-1.778290E-02 (1.24 t) . . . . . 1. 45 ............... * ........ x .... * ............ * ...... * ....... * ............. * ............ . x x: x x x x x x x x *x x x. x x x x x x *X X* x x x 1. 4 -* .......... *: ............ *' ........................ ,' *:* ........... *: ............ . I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e ACT INV MEAN INV ACT QA filenart'le Parart'le ter Nart'le Start/End Dates lrrlts: DKA100: [CANBERRA.GAMMA.5CU5R.QA]QCC_GAM09_500MLMB.QAF;1 P5ENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06: 24:11 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 61 ........... * ............. * .............. * ........... *.* ........... * ............. . ..-I ""'" N I ::E a:* (!) 0:: LJJ z LJJ a: LJJ CL 60 59 . . . . . ........................................................ -.................. . . . . . . . . . . . 58 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurert'lent Date/Tirrle UP LOW QA filenaMe ParaMeter NaMe Start/End Date8 Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM09_500MLMB.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:24:11 through 1-0CT-2016 12: 00:00 0.843482 +-5. 677858E-02 (6. 73 %) ""'"" v N I :E a: :E I 3 LL :,,::: a: LiJ 0... x 1 -* * * * * * * * * * * *:* * * * * * * * * * * * *: * * * * * * * * * * * *:* * * * * * * * * * * * *:* * * * *
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  • 0 0 0 0 0 0 0 0 0 0 0 0 0 "0 0 0 0 0 0 0 0 0 0 0 0 0 I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenar.-.e ParaMeter Nar.-.e 5tart/End Dates Mean +-Std Dev DKA100: NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:24:11 through 1-0CT-2016 12:00: 00 62249.4 +-1409.24 (2.26 %) . x 10000 * * * * * * * * * * * *. *x * * * * * * * * * * *. * * * * * * * * * * * * ** * * * * * * * * * * * *.* * * * * * * * * * * * "* * * * * * * * * * * *
  • H 1-u a: D I.LI 1-u I.LI Cl:'. Cl:'. 0 u a: u I.LI D 65000 x x x xx x . x . . . . x x x . '* ...... . x x *x x x x x %x x x x *X :?< x x x ... xx* x *; . x X< x. x x .. x . x % x X X *X ;x
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  • x x ........... " ......................... x" ......................... " ............ . 55000 4-16. 5-16 6-16 7-16 8-16 9-16 Me.asurer.-.ent Date/ Tir.-.e ACT INV MEAN INV ACT 0 >-+, Vi 00 0 \0 QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM09.QAFJ1 BACKRATE (Spectrur.-. Background Rate) 3-APR-2016 12:18:18 through 1-0CT-20i6 12:00:00 1.26523 +-1.466291E-02 (1.16 %) ' . . . . 1. 3 -* I 0 I o I I o o o I ', o o o I o o o 0 I I I 0 o, 0 I I o o o I I o o o I,' o I o o o I o o o I I ',' o o I o. o I I I o o o o, I o o o I I o o o o o o o x x x x x: 1.28 x . x . x . . . -* .......... *.* ........... * ............ *.* ........... *.*. x* ........ * ............. . x x x x x ?< *X x x* x v *x 1.26 x : : : : x : -* .................. -...... , ................................................... . x x 1. 2.4 -* I ,*, o I o o o o o o, o o I I*' I 0 I 0 I I o o, o I I o o o I I o o 0 I ,1 I o I 0 I 0 0 o 0 0 I 0,0 0 0 I 0 I 0 0 I I I o 1, I o o 0 o I o Io o o I o I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e ACT INV MEAN INV ACT QA filenaMe DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM11_JAR.QAF;1 ParaMeter NaMe PSENERGY-59 (PEAK ENERGY AM-241) Start/End Dates 4-APR-2016 06:24:16 through 1-0CT-2016 12:00: 00 Lower/Upper LMts: 57.5000 through 61.5000 -M '<:!" N I ::E <I (.!) et:: LLJ z LLJ <I LLJ 0.. 61 ........... " ............ * ............. " ........... *.* ........... " ............ . 60 59 . . . . . ............................................................................ 0 I I 0 o . . . 58 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe UP LOW QA filena!Yle Para!Yleter Na!Yle Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM11_JAR.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:24:16 through 1-0CT-2016 12:00:00 0.811280 +-2. 896658E-02 (3.57 %) "<"'i "'1" N I E a: E I 3 LL :::..::: a: UJ CL '85 . 8 xx x *x x x x x . . . . x x . . x . x . . . -* .. )( . *x .................... *x .............. *x. % .. *x:* ..... ?< .......... *x .... .. x x x . x x x x x x* x* x Xx * ;x x x x . x x x v .x v " w : x : x " x x : x v x x xxx . N X . X X X . X *x X X . X -* .......... *: ....... ... *: .... x ... *x* ..... x ..... *x* .. >:§< .. xx* ... x .. ........... . xX X
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  • x t I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measure!Ylent Date/Ti!Yle ACT INV MEAN INV ACT QA f i len*arrie Pararrieter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM11_JAR.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06:24:16 through 1-0CT-2016 12:00: 00 60054.4 +-1312.98 (2.19 %) x x x x 62000 H. f-u 0: D I.LI f-u w --.R ........ .......... -: ........... -:-........... ?<* ...... ........... . . X . XX . . X** . . x . . x . x x x x xx w x x x x : x x x x: x x >>< xxx
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  • x * * * * * * * * : x xx : x x : x x xx : x x X \ X X: XX X
  • X ;: X X :x -}/-X XX X >>< ><;: X :x x x x ':<x x* x* x . . x;.;:: . x* x . x . x . . x . x . * . x x x . . x . x . . -* ..... *X ...... X-x* ................................. X .......................... *-;(.* . x . x . . . x x v x x x 56000 -* ............................................................................... . I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenarrie Paraf"l'leter Naf"l'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM11.QAF;1 BACKRATE (Spectruf"l'l Background Rate) 3-APR-2016 12:18:24 through 1-0CT-2016 12:00:00 1. 54973 +-1.740346E-02 (1.12 %) 1. 6 -* .......... ,* ................................................................. .;. .. (J c ::J 0 "0.0 .Y. (.) l(i co E ::J -I.lo (.) ID 0.. 01 x x x x* x x x :x: x x x x x x x x: *X 1 55 -* ........... * ............. : ............ * ......... )(, ............... : ............ . . . . x . . . x x x .x x x 1. * *-......... *; ............ *; ............ ;* ........... *;* ........... *; ............ . 4-16 5-16 6-16 7-16 8-16 9-16 Meaauref"l'lent Date/Tirrie ACT INV MEAN INV ACT QA filenarrie Pararrieter Narrie Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM12_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:13:35 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 61 ........... * ............. * .............. * ........... *.* ........... * ............. . ::..:: a: w CL 60 59 .......................... * ....................................... : ............ . . . . . . . . . . . 58 ............................................................................ . . . . . 4-16" 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie UP LOW QA filenarrie Pararrie ter Narrie Start/End Dates Mean +-Std Dev x DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM12_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13:35 through 1-0CT-2016 12:00: 00 1.20109 +-5.234504E-02 (4.36 %) x x 1.4 ............ : ............. : ............ : ............. :.x ........ x .. : ............ . ..-! v N I ::E: a: E I 3 LL :,.::: a: LLJ CL x x x x x x Xx X: x x x x Xx x x Xx xx :x x :x X* x x x x x x x x x x x xx x x x x x x x x x Xx :xxx x x >\ x x* x ><>< x x x )<( x xx xx X* x x x % 1 ........... " ....... : .... " ............ " ......................... " ............ . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenafY'le ParafY'le ter NafY'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM12_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-201606:13:35 through 1-0CT-2016 12:00:00 62074.4 +-1703.29 (2.74 %) H f-u a: D LLJ f-u LLJ. Q'. 0:: 0 u >-a: u LLJ D 65000 60000 x x x x x x Xx x X *X x x x v X X " , " A , X " " X
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  • x* x 1<x A x x x )$( x :x x -* ........... * ............ : ............ * ............. * .... x ..................... . x x . . . . x x x x . . . . . x 5 5 0 0 0 -* * * * * * * * * * * *I * * * * * * * * * * * * .I * * * * * * * * * * *
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  • 4-16 5-16 6-16 7-16 8-16 9-16 MeasurefY'lent Date/TifY'le ACT INV MEAN INV ACT QA filenarrie Parar.-.eter Nar.-.e Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM12.QAF;1 BACKRATE (5pectrur.-. Background Rate) 3-APR-2016 12:18:29 through 1-0CT-2016 12:00:00 1.34296 +-2.081&31E-02 (1.55 %) . . . . . 1. 4 -* .. -................................................... -................... . I I I I x x x 1. ;35 -*: * * * * * * * * * * * * * * * * * * * * .:
  • x* * * * * * * * * .:. * * * * * * * * * * * .:. * * * * * * * * * .>s:: .: * ..... * * * *X *
  • x x x x 'X ....,.* "A x *x x .x x x X* x x x :x x x x x x x x x x 1. 3 -* I o o o o ' o O O I II O o o 1 o o o o o 1 o O OI O O I o O o 1 1 o o o o oo o o o o 1 o o o o ,' 1 ooo o 1 o o o O I O O o O '"O O O O O o o o o o o 1 o 1 1 1 1 1 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tirrie ACT INV MEAN INV ACT QA filenaMe Pararrieter Narrie Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM16_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06: 24:31 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 61 ........... * ............. * .............. * ........... *.* ........... * ............. . ...,. N I ::?::: <I 0::: LLJ z LLJ ;:,.::: <I LLJ 0.. 60 59 . . . . . ............................................................................ . . . . . . . . . . 58 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Tirrie UP LOW QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev x DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM16_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06: 24:31 through 1-0CT-2016 12:00:00 1. 00429 +-4.727185E-02 (4.71 %) -. . . . . 1. 1 xX ..-I """ N I E a: E x x xx X xX X X-X XX xx x ).( x x x x .)( x x . v " ' vx x %* x -}!:< x . v . . *. x x x x I 1 3 LL l..:: a: LU o.: ................ -: x:* .... -.... ;:<, * ..-::-x*x* ......... :-. % ........ <* .. '. X* .. x* 'x<'< ...... .... <' .. : X X : X X: x: X X : X X 1-xX :XX X X>< x x x x x x x x. x x >§(< X* xx xxx x x x x . x x xx x x x xx x x x % x x x x x xx x :x x x. . *9 .. _ .......... * ............. * ............ * ............. * ..... *x ...... * ............ . I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenarrie Pararrieter Narrie Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM16_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-2016 06: 24:31 through 1-0CT-2016 12:00: 00 67102.8 +-1970. 09 (2.94 %) H 1-u a: 0 LL.I 1-u LL.I D u a: u LL.I 0 70000 -* .......... * ............. * .............. * ........... *.* ........... * ............. . 65000 x x x x . x : x 0 . xx* x . x x x x x x xx x x *x x v x x
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  • o 1° I 0 o ' o o o o o o I o o . . . . . 1J c :'i 0 S-"0.0 .Y. (J l1j co E x :'i x S-+) (J Q) 0. 01 1.5 X. x X* X x x x x x *x x x x: . . . x . . x . . . x . . x . ......... x .... '* ............ '* ............ *' ...... x ................... ")<* .......... . x x I I 1 I I 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrrent Date/Tirrre ACT INV MEAN INV ACT QA filenar.-.e Parar.-.eter Narrie Start I End oa*tes Lower/Upper Lrrits: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM18_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06:13:40 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 61 ........... * ............. * ............. " ........... *.* ........... " ............ . ..-i """ N I. ::?:: <I: (.!) et:: Ll.J z Ll.J ::...::: <I: Ll.J 0.. 60 59 ............ * ............. * ............ * ............. * .............. * ............ . . . . . . . . . 58 ............................................................................ . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tir.-.e UP LOW QA filenarrie Pararrie ter Narrie Start/End Date8 Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM18_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:13:40 through 1-0CT-2016 12:00:00 0.960465 +-3.090899E-02 (3.22 %) x 1. 1 ........... * ............. * .. ' ........... * ........... *.* ........... * ............. . "<-i """ N I ::E <J: ::E I 3 LL :::..: <J: UJ 0.. x x . . . . . 1 . *:X: ......... : .....*....... : .....*..*... : .......... ** .:.-............ : ............ . . >x . x x x x . x x . x x x . xx x. xx );(x: x x . >x x x<x x ?: x x : x .8 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 MeaBurerrient Date/Tirrie ACT INV MEAN INV ACT QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM18_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 4-APR-201606:13:40 through 1-0CT-2016 12: 00:00 63719.3 +-1431.59 (2.25 %) H 1-u a: D w 1-u w Ct:: Ct:: 0 u a: u w D 66000 64000 62000 60000 x x x . . x . x . -* ................................................... *x ......................... . x x x x x . x x . x . X . X . . xX . X *X *
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  • x* x x x \ * . x xx x x x x x x x . x x x*. xx x x x x x . ><xx xX x x x x : x -)}<. : x : xx >f >-* .*.*.*.. xx .*. . x ..... : .. *;x* .... : ........... x .:x . *x ... *xx .. * .. ....... 0. x . x . . . . x 9 x x :x x x x *x x x x *y x -x xx x x x* ...... ' .......... * ............ .' ............ * .......................... : ............ . . . . . . x x I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenal'le Paral'leter Nal'le Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_GAM18.QAF;1 BACKRATE (Spectrul'I Background Rate) 3-APR-2016 12:18: 51 through 1-0CT-2016 12:00:00 2.12760 +-2. 980382E-02 (1.40 %) x 2.2 1-o* ************************ *' ****** ' ******************************** *' ************* x x. x x 2.15 -* .... ' .......................................................................... . x x x x x x x x* x x .x x . . . . . x x . . x . x . . 2. 1 -* * * * * * * * * * * ** * * * * * * * * * * * * ** * * * * * * * * * * * * ** * * * * * * * * * * * *** * * * * * * * * * * * ** x* * * * * * * * * * *
  • x x . . . . 2. 05 1--* ********** * ************* * ************** * *********** *** *********** *, ************* I I I I I 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/Til'le ACT INV MEAN INV ACT QA filenar.-.e Parar.-.eter Nar.-.e Start/End Dates Lower/Upper Lr.-.ts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_GAM19_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 4-APR-2016 06: 54:25 through 1-0CT-2016 12:00:00 57.5000 through 61.5000 61 ........... * ............. * .............. * ........... *.* ........... * ............. . "<-i ""'" N I E <I: (!) a::: llJ z ll.J* ::..: a: llJ a.. 60 59 . . . . . ............................................................................ . . I I ' o ' 58 ............................................................................. . . . . . 4-16 5-16 6-16 7-16 8-16 9-16 Measurer.-.ent Date/Tir.-.e UP LOW QA filenaMe ParaMeter NaMe 5tart/End Dates Mean +-5td Dev DKA100: P5FWHM-59 (PEAK FWHM AM-241) 4-APR-2016 06:54: 25 through 1-0CT-2016 12: 00:00 1.02481 +-2.522724E-02 (2.46 %) -M "it N I ::E <I: ::E I 3 LL ::..:: <I: LU CL 1.05 x X* x x x *x x x x x x x % x . . x . . . 0 ............... *.********x*: ............ * ......... .. * .. xx ........ : ............ . : xx : xx: : x : X Xx X X Q X xx Xx x* x x XX X X v v* x X A *x x.x. X xX. x x A x x* x* , x x X X X: X X . X X Q >5< X x* XX X x. x % xx x x x x x x *X X *
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  • ACT INV MEAN INV I I 1 I I 1 9-1u ACT 3-16 6-16 8-16 7-16 4-16 5-16 Meaaurel'tent Date/Til'te QA filenaMe ParaMeter NaMe Start/End Dates Lower/Upper LMts: DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_XRAY6_CAN.QAF;1 PSENERGY-59 (PEAK ENERGY AM-241) 2-MAR-2016 05:59:50 through 1-SEP-2016 12:00:00 58.5400 through 60.5400 60.5 ........... '* .......................... * .......................... * ............. *. 60 . . . . . . ............................................................................ . . . . . . "<"i -.;t-N. I E <I: )-0::: 59. 5 w ............. * ........... * .......................... * ............. .' .............
  • z w ;:,..! <I: w 0.. 59 UP 3-16 4-16 5-16 6-16 7-16 8-16 9-1Li LOW MeasureMent Date/TiMe QA filenaMe ParaMeter NaMe Start/End Dates Mean +-Std Dev DKA100: [CANBERRA.GAMMA.SCUSR.QA]QCC_XRAY6_CAN.QAF;1 PSFWHM-59 (PEAK FWHM AM-241) 2-MAR-2016 05:59: 50 through 1-SEP-2016 12:00:00 0.422584 +-8.876291E-03 (2.10 %) o:-1 """ N I E a: E I 3 LL :::.::: a: w CL . 44 -* ............ * ........... * ....... ............ *x: .... x* .................. x* ...... * . 42 x x: x :xx x x x x x x 0x X:* x x x x x :>> x x x xx XX A.
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  • Xx x I 1 I I I I 3-16. 4-16 5-16 6-16 7-16 8-16 9-16 MeasureMent Date/TiMe ACT INV MEAN INV ACT QA filenarrie Pararrieter Narrie 5tart/End Dates Mean +-5td Dev DKA100: [CANBERRA.GAMMA.5CU5R.QA]QCC_XRAY6_CAN.QAF;1 NLACTVTY-59 (DECAY CORRECTED ACTIVITY AM-241) 2-MAR-2016 05:59: 50 through 1-5EP-2016 12:00:00 52108.9 +-758.036 (1.45 %) . . . . x . . 5 4 0 0 0 '-* ............ * ........... * ............. : ........... * ............. : .............
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  • X*: * * * * * * * * * * * *. * ........... : ................... : ..... : ............ ." x x x I I ; I I I 3-16 4-16 5-16 6-16 7-16 8-16 9-16 Measurerrient Date/Tirrie ACT INV MEAN INV ACT 0 ....., Vi 00 0 "° QA filenaMe Paraf"l"Je ter NaMe Start/End Dates Mean +-Std Dev . 22 LI c ::J x DKA100: [CANBERRA.GAMMA.SCUSR.QA]LBC_XRAY6.QAF;1 BACKRATE (SpectruM Background Rate) 6-MAR-2016 12:05:17 through 1-SEP-2016 12: 00: 00 0.206552 +-5. 056256E-03 (2.45 %) . . . . . . 0 . 21 1--. * * * * * * * * * * ** * * * * * * * * * * * * ** * * * * * * * * * * * * : * * * * * * * * * * * ** * * * * * * * * * *** : * * * * * * * * * * * * ** $.... "0.0 *X .:£. 0 (rj co. x x E ::J x x $.... .µ x x 0 x ID 0.. ({) .2 x: x x x x x x x x* ................ :* ........... : ............ : ....... x ... '. ............ : ............ :* x :x x x x I ACT INV MEAN INV I I I I I 3-16 8-16 9-1u ACT 4-16 5-16 7-16 6-16 MeasureMent Date/TiMe Page 4922 of 5809 RAD Standards Traceability

,, ... (i) Nuthmul Justitutt nf i':tmWurhs & UJt.r4unlngy <tTrrtiftrutr * ' . "' . Standard Reference Material 4949C Iodine-129 Radioactivity Standard J'-170 This Standard Reference Material (SRM) consists of radioactive iodine-129 as sodium ic;>dide, sodium hydroxide, and sodium sulphite dissolved in 5 mL of distilled water .. The solution is contained in a sealed NIST borosilicate-glass* ampoule. The SRM is intended for the calibration of beta-particle c:Ounting instruments and for the monitoring of radiochemical procedures.

  • Radiological Huard: The SRM ampoule contains iodine-129 with a total activity of approxiinately 17 kBq. Iodine-129 decays by beta-particle emission. None of the beta particles escape from the SRM ampoule. During the decay process, X-rays and gamma rays with from 4 keV to 40 keV are also emitted. Most of these photons escape from the SRM ampoule but their are so small that they do not represent a significant radiation hazard. Appropriate shielding and/or distance should be to ininimize personnel exposure. The SRM should be used only by persons qualified to handle radioactive material. Chemical Huard: The SRM ampoule contairui sodiiim hydroxide (NaOH),with a concentration of0.01 mole per liter of water. The solution is mildly corrosive and represents a health hazard if it comes in contact with eyes or skin. If the ampoule is to be OP<<?ned to transfer the solution, the recommended procedure is given on page 2. The ampoule should be opened only by.persons qualified.to handle*both radioactive material and alkaline s61ution. Storage and Handling: The. SRM should be stored and used at a temperature between 5 and 65 °C. The solution in an unopened ampoule should remain stable and homogeneous for at least five (5) years after receipt. The ampoule (or any subsequent container) should be clearly *as containing radioactive material. If the ampoule is it sbould'be packed, marked, labeled, and shipped in accordanee with the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous good (hu.a.rdous material) because of both the radioactivity and the strong base. Preparation: This Standard Reference Material was prepared in the Physics LaboratoIY., Ionizing Radiation Division, Radioactivity Group, J.M.R. Hutchinson, Group Leader. The overall technical direction and physical measurements leading to certification were provided by L.L. Lucas, the Radioactivity _.Group. The** support aspects involved in the preparation, certification, and .. of this SRM were coordinated through the Standard Reference Materials Gaithersburg, Maryland 20899 July 1995 Text revised and expiration date extended April 2006 SRM4949C,page I or(;* Lisa.R.. Karam, Deputy Chief Ionizing Radiation Division Robert L. Watters, Jr., Chief Measurement Services Division

**--------**------*---Silica in the SRM Ampoule The solution in the SRM ampoule bas a pH of approximately 11 and will slowly etch microgram quantities of silica from the glass ampoule. You may be able to see this silica at times, as it bas a density greater than that of the SRM solution and tends to settle. Tests have shown that this silica does not affect the iodine-129 concentration. lf desired, the silica may be redispersed in the SRM solution by shaking well. Alternatively, if desired, the silica may be filtered out m the transfer 1) 2) 3) 4) 5) 6) ?> 8) Recommended Procedure for Opening the SRM Ampoule .. _ , . *-*--* II -,,. * ..,._._, ____ r ............

  • If the SRM solution is to be diluted, it is recommended that the diluting solution *have a composition comparable to that SRM solution. Wear eye protection, gloves, and protective clothing and work over a tray with paper in it. Work in' a fwDe hood. In to the material, the solution contains strong base and is corrosive. .. -. . Shake the ampoule to wet all of the inside surface of the ampoule. Return the ampoule to the upright position. Check that all of the liquid bas drained out of the neck of the ampoule. If necessary, gently tap the neck to speed the process. Holding the ampoule upright, score the narrowest part of the neck. around its entire circumference with a scribe or diamond pencil. Lightly wet the scored line. This reduces the crack propagation velocity and makes for a cleaner break. / Hold the ampoule upright with a paper towel, a wiper, or a support jig. Using a paper towel or wiper to avoid contamination, snap off the top of the ampoule by pressing the narrowest part of the neck away from you while pulling the tip of the ampoule towards you. Transfer the solution from the ampoule using.a pycnometer or a pipet with dispenser handle. NEVER PIPETTE BY MOUTH. 9) Seal any unused SRM solution in a tlame-sealed glass ampoule, if possible, to minimize the evaporation loss. See also reference [ 4]*. SRM 4949C, page 2 of 6 '"Notes and rcfcmiccs arc on pages S and 6. Page 4924 of 5809 I I I r; PROPERTIES OF SRM 4949C . Certified values Radionuclide lodine-129
  • Reference time 1200 EST, 21 .. -. Massie activity of the solution [al* 3451 Ba *Jf1 Relative emanded uncertainty (k=2) * . 0.64% lblfcl ' Uncertified values ,r* Physical Properties: Source description ' Liquid in.flame-sealed NIST borosilicate-glass amooule Ampoule specifications . Body outside diameter {16.5 +/- O.S)'mm ... ,* Wall thickness (0.60 +/- 0.04) mm Barium content Less than 2.5% Lead-oxide content Less than 0.02% Other heavy elements Trace quantities : Solution density (1.003 +/- 0:002) 2
  • mL*I at ' 21.2°C [d] ,. ... Solution mass Aonroximately 5.0 a .. Chemical Properties: J J Solution composition Chemical Concentration Mass Fraction .* Formula (mol*L-1) (g*g-1) H20 SS r . 1.00 NaOH 0.01 0.0004 NaiS03 0.006 0.0008 Na129I 0.004 0.0006 . Radiological Properties: . . .. Photon.:emitting impurities < None detected [el H8If lives used Iodine-129: (1.57 :!: 0.04) x 107 a [5][fl Calibration method and measuring NIST *couriting system. instrument ....... _____ _, ... ,, SRM 4949C, page 3 of6 *Notes and n:fercnccs an: on pages S and 6. PL"'_ 4925 of 5809 -

EVALUATION OF THE UNCERTAINTY OF .THE MASSIC ACTNJTY [b]* Input Quantity x,, the source of.uncertainty -(and individual uncertainty components where appropriate) Massie scintillation count rate, corrected for background and decay . Background Mass calibration of the balance Decay iodine-129 Decay-scheme data !:Live time [n] Extrapolation particle-count-rate versus gamma:niy-count-rate to ,zero gamma-rav-count-rate Photon-emitting inmurities .. Method Used To Evaluate u(x,), the standard uncertainty of x, (A) denotes evaluation:by. statistieal methods (B) de'iiotes evatuatlon by other methods

  • Relative Uncertainty Of Input Quantity, u(x1)1x,, {%) [g] Standard deviation of the mean o: 12 for 6 sets of repeated measurements. (A) "" **--***-----; * -** *
  • Standard deviation* of the mean for .6 sets of repeated measurements. (Al Estimated from manufacturer's* data (B) .J Standard uncertainty of the half life **.:,: . \ -Standard uncertainty;of the probability of beta-particle emission to the excited ffi) Estimated (B) Estimated (B) Limit of detection (B) [p] 1.0 0.05 2.55 [k] 0.10 0.10 0.25 100 Relative Combined Standard Uncertainty of the Output Quantity, u0(y)ly, (%) Coverage Factor, k Relative Expanded Uncertainty of the Uly, (%) Relative Sensitivity Factor, 1ay1ax,!* [h] 1.0 [j] 0.01 0.00 [m] 1.0 .. 1.0 0.00002 Relative Uncertainty Of Output Quantity, ui(y)ly, {%) [i] o.i2 0.01 0.05 0.00 .?: 0.10 . 0.10 0.25 0.002 0.32 ..xl.: 0.64 SRM 4949C, page 4 of 6 *Notes and rcfc:rc:nccs arc on pages S and 6. ... """'*"'r .... * *** "*-"-""'" '"-** * '

,;rJ;*.f )* . . If ' . *' L iJ l l I *. r-* , ,...,.I I ,b.t'."1""11, &:i ; ' ....... [ . ****-. ( ' : lb --'["' , . .._, __ \'[-.. . ..

  • Page 4927 of 5809 [a] [b] [c] [d] [e] [t] [g] [h] [i] rn NOTES Massie activity is the preferred name for the quantity activity divided by the total mass of the sample. See reference [1]. *
  • The reported vaiue, y, of massic activity (activity per unit mass) at the reference time was not measured directly but was derived from measurements and calculations of other quantities. This can be expressed as y = j{x1,x:z, xJ, .* x.), where /is a mathematical function derived*from the assumed model of the measurement process. The value, x,. used for each input quantity i bas a standard uncertainty, u(x,), that generates a corresponding uncertainty iny, uh)= lc3)118x1l*u(x,), called a of combined standard uncertainty*ofy. The combined standard uncertainty ofy, uc(y), is the positive square root of the sum of the squares of the components of combined standard uncertainty. The combined standard uncertainty is multiplied by a coverage factor of k = 2 to. obtain U, the expanded uncertainty ofy. Since it can be assumed that the possible estimated values of the massic activity are approximately normally distributed with approximate standard deviation uc(y), the unknown value of the massic activity is believed to lie in the interval y :!: U with a level of confidence of approximately 95 percent For further infonnation on the expression of uncertainties, see references (2] and (3]. .. ' The value of each component of combined standard uncertainty, and hence the value of the expanded uncertainty itself, is a best estimate based upon all available information, but is only approximately known. That is to say, the uncertainty of the uncertainty" is large and not well known. This is true for evaluated by statistical methods (e.g., the relative standard de\liation of the standard deviation of the mean for the massic response is approximately 50%) and.for uncertainties evaluated by other methods (which could easily be over estimated or under estimated by substantial amounts). The unknown value;qfithe expa,nded uncertainty is believed to lie in the interval U/2 to 2U (i.e., within a factor of 2 of the estimated value).
  • The stated uncertainty is two times the standard uncertainty. The estimated limit of detection for photon-emitting impurities, expressed as massic photon emission rates, is: 0.07 s***g** for energies between 43 keV and 2700 keV. The stated uncertainty is the standard uncertainty. Relative standard uncertainty of the input quantity .x,
  • The relative change in th.e output quantity y divided by the relative change in the input quantity x, . If lc3.)lla.x,l*(x/y)= 1.0, thena 1 %cbangeinx1resultsina1%changeiny. If lc3)1Jax,jo(x/y) =0.05, then a 1 % change in x, results in a 0.05% change in y. Relative component of stBndard iinceiiainty of output quantity y; rounded to two significant figures or less. The relative component of combined standard uncertainty of y is given by u,(y)ly = I ay1ax1 I *u(x,)ly = I ay1ax, I *(xly)
  • u(x,)lx1* The numerical values of u(x,)lx,, I ay1ax1 I *(xJy), and u,(y)ly, all dimensionless quantities, are listed in columns 3, 4, respectively. Thus, the value in column Sis equal to the value in column 4 multiplied by the value in column 3. The input quantities are independent, or very nearly so. Hence the covariances are zero or negligible. 1ay1ax1l*(x/y) =(average background count rate)/(avemge net sample count rate) SRM 4949C. page S of 6

. *---*-"' '-'**-_:,;,..:, _.:_ *--. *--. . .. , ...... ..,. .. -* -.... -hlZLE [k] [m] [n] fp) The relative standard uncertainty of l*t is determined by the relative standard uncertainty of A. (i.e., of the half life). The relative standard unceJ:!ainty of t is negligible . . , lc3ylax,l*(x/y) = jA.*tl The live time is determined by counting the pulses from a gated oscillator. The uncertainty for each undetected impurity that might reasonably be* expected to be present is estimated to be equal .to the estimated limit of 'detection for that impurity, i.e. u(X;)lx, = 100%. I oylox,1-(x,Jy) = {(response per Bq of-impurity)/(response per Bq of iodine-129)}*{(Bq of impurity)/Q3q of:iodine-.129.).} *. Thus, is the relative *change in y if the impurity were present with a *massic activity equal to the estimatea lliDtf ofaetecti'Oif." ........ *.;-* REFERENCES ., [1] International. Organiz.ation for Standardization (ISO), ISO Standards Handbook -QUdntities and Units, 1993. Available from Global Engineering Documents, 12 Inverness Way East, Englewood, "co .80112, U.S.A' Telephone 1-800-854-7179. * * [2] International Organization for Standardization (ISO), Guide to the Expression of Uncertainty in Measurement, 1993 (corrected and reprinted, 1995). Available from Global Engineering Documents, 12 Inverness Way East, Englewood,1 CO 80112, U.S.A Telephone 1-800-854-7179. Ir: [3] B. N. Taylor and C. E* Kuyatt, Guidelines for Evaluating and Expressing the Uncertainty of NIST NIST Technical Note 1297, 1994. *Available from the Superintendent of Documents, U.S. Government Printing Office, DC 20407, U.S*.A. '" [4] National Council on Radiation Protection and Measurements Report No. 58, A Handbook of Radioactivity Measurements Procedures, Second Edition, 1985; 'Available from pie National Council on Radiation Protection and Measurements, 7910 Woodmont Avenue, Bethesda, MD 2081,4 U.S.A. [5] Evaluated Nuclear Structure Data File (ENSDF), July 1995. SRM 4949C, page 6 of 6 Q9. . . .. . . . ... ...,. ... ---**** . . .. . . . .. . ..*. !,{ Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Iodine-129 " Parent Code: 1470 Prepared By: Michael Hilton Prepared By: Bethany Fiem Prep Date: 04/04/2011 Carrier Cone: Aqueous NaOH Verification Date: 03/30/2015 Reference Date: 03/2111993 Expiration Date: 03/30/2016 Ampoule Mass (g): 4.9632 g Primary Code: 1470-A Uncertainty: +!-.64 % Dilution(mL): lOOmL LogBookNo: RC-S-060-017 Mass of Parent(g): 4.4624 g Density(g/mL): 1.0125 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq/g)) *(conversion dpm to Bq) I (Dilution Vol)= Parent Activity (dpm/mL) (Mass ofparent(g)) * (Parm Activity (Bq/g)) *(conversion dpm to Bq) I Density (g/mL)/ (Dilution Vol)= Parent Activity (dpm/g) (4.4624 g) * (3451 Bq/g) * (60 dpm/Bq) I (100 mL) = 9239.8454 dpm/mL (4.4624 g) * (3451 Bq/g) * (60 dpm/Bq) I ( 1.0125 g/mL) I (100 mL) = 9125.6201 dpm/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone dpm/mL Verification Expiration Primary (mL) Date Date 04/11/2011 Michael 2.9988 100 1470-B 277.8282 04/11/2011 04/11/2012 Hilton dpm/mL 04/11/2011 Michael 1.0002 100 1470-C 92.6066 04/11/2011 04/11/2012 Hilton dpm/mL 08/18/2011 Andrew 10.8742 100 1470-D 992.3382 08/31/2011 08/31/2012 Willis dpm/mL 09/16/2011 Michael 10.112 100 1470-E 923.98454 09/21/2012 09/21/2013 Hilton dpm/mL 08/13/2012 Michael .9995 100 1470-F 92.1545 09/15/2011 09/15/2012 Hilton dpm/mL 08/14/2012 Michael 10.0979 100 1470-G 936.206 08/14/2012 08/13/2013 Hilton dpm/mL 09/11/2012 Michael 10.0683 100 1470-H 923.98454 09/08/2014 09/07/2015 Hilton dpm/mL 05/13/2013 Michael 10.095 100 1470-I 923.98454 05/27/2016 05/27/2017 Hilton dpm/mL Page 4929 of 5809 06/10/2014 Michael Hilton 03/27/2015 Michael Hilton GEL Laboratories LLC Version 1.0 9/18/2000 Page 4930 of 5809 5.0681 9.9722 1 1470-J 9239.8454 06/13/2016 06/13/2017 dpm/mL 100 1470-K 923.98454 03/30/2016 03/30/2017 dpm/mL Verification for 1-129 Standard v1.1.2 Noah Postell 3/30/2016 Mean Value (Counting) = Stdev= Certificate Value = Two sigma= 10 % of Mean= Rule A (Pass/Fail) Verification Rules Isotope 1-129 1-129 N1 1-129 N2 1-129 N3 42.17 1.771 41.6 3.541769802 4.217333333 Pass Result pCi/L 40 43 44 pCi/L pCi/L pCi/L 101.327 1470-K Pass Rule B (Pass/Fail) Rule A = The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule 8 =The determined mean value shall be within 5% of the certificate value.

0 I : Eckert & Ziegler Analytics 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com CERTIFICATE OF CALIBRATION Standard Radionuclide Source 84680-278 I 00 mL Solid in Aluminum Can Customer: GEL Labs P.O. No.: 489884RP, Item 3 Reference Date: Ol-Apr-2011 12:00 PM EST Grams of Master Source: 0.0066498 This standard radionuclide source was prepared using aliquots measured gravimetrically from master radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer system. At the time of calibration no interfering gamma-ray emitting impurities were detecteQ. The gamma ray emission rates for the most intense gamma-ray lines are given. Eckert & Ziegler Analytics (EZA) maintains traceability to the *National Institute of Standards and Technology through* a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this source was produced in accordance with the HPS accreditation requirements. Customers may report any concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101. Density ofsolid matrix 1.15 g/ cc. Gamma-Ray Nuclide Energy (keV) Pb-210 46.5 Am-241 . 59.5 Cd-109 88.0 Co-57 122.l Ce-139 165.9 Hg-203 279.2 Sn .. 113 391.7 Cs-137 661.7 Y-88 898.0 Zn-65 1115.6 Co-60 1173.2 Co-60 1332.5 Y-88 1836.1 Half-Life, Days* 8.120E+03 l.580E+05 4.626E+02 2.718E+02 l.376E+02 4.661E+Ol l.161E+02 l.098E+04 l.066Ei-02 2.441E+02 l.925E+03 l.925E+03 l.066E+02 Master Source* res/gram l.659E+05 8.949E+04 l.247E+OS 2.899E+05 l.739E+05 l.107E+OS 4.246E+05 2.118E+05 2.118E+05 4.495E+05 This Source yps l.129E+03 7.538E+02 l.103E+03 5.951E+02 8.292E+02 l.928E+03 l.156E+03 7.361E+02 2.824E+03 1.445E+03 l.408E+03 l.408E+03 2.989E+03
  • Master 8-isotope mixture which is calibrated quarterly. Uncertainty, % Type Calibration UA U9 u Method 0.1 2.1 4.1 4nLS 0.1 1.7 3.5 4nLS 0.6 2.3 4.8 HP Ge 0.6 2.0 4.2 HP Ge 0.6 1.9 4.0 HP Ge 0.6 1.9 4.0 HP Ge 0.6 1.9 4.0 HP Ge a.a 1.9 4.1 HP Ge 0.6 1.9 4.0 HP Ge 0.1 1.7 3.5 IC 0.7 1.9 4.0 HP Ge 0.7 1.9 4.0 HP Ge 0.7 1.9 4.0 HP Ge *. Methods: 4 pi Liquid Scintillation Counting, HPGe -High Purity Germanium Gamma-Ray Spectrometer, IC -IonizattOn ChalllbaL Uncatainty: U -Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for the Uncertainty of NIST Measurement Results." -* .. ..** *.* .. *-(Certificate continued on reverse side) -.. -.. .... , -. ' ... .. ""'-* -o'" I or,po-Joi MGS Certificate, Rev 2 09-28-2009 Pa e1 of2 Corporate Office Laboratory 24937 Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318 Page 4932 of 5809 This standard will expire one year after the reference date. Source Prepared by: M:WillifOidJOCilemist QA Approved: J. D. Mccorvey, QA Manager Alternate MGS Certificate, Rev 2 09-28-2009 Page 4933 of 5809 I; Date: --*-.. , . * .. * .* _, . Page2 of2 Serial ID: 1556 Name: Mixed Gamma LCS CAN Type: Source Material Employee: Maggie Stamps Supplier: Eckert & Zeigler Analytics

Description:

84680-278 Comments: None Analyte Americium-241 Cobalt-60 Report run on: 09-APR-15 Page 4934 of 5809 Standard Logbook Open/Reference Date: 01-APR-11 Received: 01-APR-11 Expires: 01.-APR-37 Verified: 14-JUL-11 Concentration Analyte 125983.3 dpm/mL Cesium-137 84496.9 dpm/mL Aliquot: 1 ml Density: Lot Number: Hand Calculated 84680-278 Concentration 51898.9 dpm/mL GEL Laboratories LLC Page: _________ _ Verification for Mixed Gamma Standard Michael Hilton 7/1412011 Mean Value (CounJing) = stdev= CertHlcate Value = Lower Limit= Upper Limit = Rule 1 Pass/Fall Twoslgma= 10%of Mean= Rule 2 (Pass/Fall) Verification Rules Isotope Pb-210 Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 722433.33 30102.713 717965.0 662227.9072 782638.7594 Pa8s 60205.42611 72243.33333 Pass Result pCUL 722900 752300 692100 pCi/L 100.622 pCi/L pCl/L pCi/L pCl/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 {Pass/Fall) Rule 1 = lbe certificate value (NOT Including any uncertainty) shall Ile within the 95% confidence Interval detennlned from the mean and two sigma standard deviation of the three measurements Rule 2 = lbe two sigma value used for the 95% confidence .Interval shall not exceed 1 O"k of the mean value of the three verfficatlon measurements. Rule 3 = lbe detennlned mean value .shall be within 5% of the certificate value. CAN 0.0425 1129 Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Isotope Am-241 Result pCl/L 1556 CAN Mixed Gamma N1 58390 Isotopic Abundance: 0.359 Mean Value (Counting)= Stdev= CertHlcate Value= Lower Limit = Upper Limit= Rule 1 PasSJFall Two sigma= 10%ofMean= Rule 2 (Pass/Fall) VerHlcatlon Rules Mixed Gamma N2 Mixed Gamma N3 58966.67 1566.727 56749.2 ss833.212n 62100.12057 Pass 3133.453898 5896.666667 Pass 60740 Certificate Value. (dps): 753.8 smo pCi/L 103.9074 Pass pCi/L Rule 3 (Pass/Fall) pCi/l pCi/l pCi/l Rule 1 = The certHlcate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10".k of the mean value of the three verification measurements. Rule 3 =The detennlned mean value shall be within 5% of the certificate value. -1,v\'l 1rat'1 Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Mean Value (Counting) = Stdev= CertHlcate Value = Lower Limit = Upper Limit =

  • Rule 1 Pass/Fall Two sigma= 10%ofMean = Rule 2 (Pass/Fall) .VerHlcatlon Rules Isotope Cd-109 Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 793700.00 27107.010 805697.6 739485.9797 847914.0203 Pass 54214.02033 79370 Pass Result pCl/L 818400 798000 764700 pCVL 98.51091
  • pCVL pCl/L pCiJL. pCl/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) Rule 1 =The certHlcate value (NOT lncludlng any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verification measurements. Rule 3 =The determined mean value shall be within 5% of the certHlcate value. CAN 0.037 1103 ""'ll'IPl \I Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Isotope C0-57 Result pCl/L 1556 CAN Mixed Gamma N1 19090 Isotopic Abundance: 0.856 Mean Value (Counting) = Stdev= Certificate Value = Lower Limit= Upper Limit = Rule 1 Pass/Fail Two sigma= 10%ofMean:: Rule 2 (Pass/Fall) Verification Rules Mixed Gamma N2 Mixed Gamma N3 18913.33 153.080 18789.5 18607.17433 19219.49233 Pass 306.1590001 1891.333333 Pass 18820 Certificate Value (dps): 595.1 18830 pCl/L 100.6592 Pass pCl/L Rule 3 (Pass/Fall) pCl/L pCl/L pCl/L Rule *1 =The certificate value (NOT Including any uncertainty) shall lie within the 95% conftdence Interval determined f{om the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used.for the 95% confidence Interval shall not exceed 10% of the mean value of the three verHlcaUon measurements. Rule 3 =The determined mean value shall be within 5% of the certificate value.

Verification for Mixed Gamma Standard 1556 Michael Hilton Isotope Result 7/1412011 Ce-139 pCl/L Mixed Gamma N1 28740 Isotopic Abundance: Mixed Gamma N2 29410 CertificateValue (dps): Mixed Gamma N3 27560 Mean Value (Counting) = 28570.00 pCl/L 101.9865 Pass Stdev= 936.643 pCi/L Rule 3 (Pass/Fall) Certificate Value = 28013.5 pCi/L Lower Limit = 26696.71412 pCi/L Upper Limit = 30443.28588 pCl/L Rule 1 Pass/Fall Pass Two sigma= 1873.285883 10%ofMean= 2857 Rule 2 (Pass/Fall) Pass Verification Rules Rule 1 =The certHlcate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verification measurements. Rule 3 = The determined mean value shall be within 5% of the certificate value. CAN 0.8 829.2 Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Mean Value (Counting) = Stdev= Value = Lower Limit = Upper Limit = Rule 1 Pass/Fall Two sigma= 10%of Mean= Rule 2. (Pass/Fall) Verification Rules -Isotope Hg-203 Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 66320.00 1850.081 63889.3 62619.83784 70020.16216 Pass 3700.162159 6632 Pass Result pCl/L 6!)300 68180 64480 pCUL 103.8046 pCUL pCUL pCUL pCUL 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) Rule 1 =The certHlcate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements CAN 0.8156 1928 Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verHlcatlon measurements. Rule 3 = The determined mean value shall be within 5% of the certHlcate value. 0 ""+-> Vl 00 0 \0 Verification for Mixed Gamma Standard Michael Hilton Isotope Result 7/14/2011 Sn-113 pCl/L Mixed Gamma N1 49560 Mixed Gamma N2 49620 Mixed Gamma N3 48300 Mean Value (Counting) = 49160.00 pCVL 102.2277 stdev= 745.386 pCVL Certificate Value = 48088.7 pCVL Lower Umlt= 47669.22839 pCVL Upper Limit = 50650. 77161 pCVL Rule 1 Pass/Fall Pass Twoslgma= 1490.771612 10%of Mean= 4916 Rule 2 (Pass/Fall) Pass VerHlcatlon Rules 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 {Pass/Fall) .. CAN 0.6497 1156 Rule 1 = The certificate value {NOT lncludlng any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10",{, of the mean value of the three verification measurements. Rule-3 =The determined mean value shall be within 5% of the certfficate value. Verification for Mixed Gamma Standard Michael Hilton 7/1412011 Mean Value (Counting) = Stdev= Isotope Cs-137 Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 23900.00 170.587 Result pCl/L 23710 23950 24040 pCl/L 102.2333 pCi/L pCi/L pCl/L pCi/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) Certificate Value = Lower Limit = Upper Limit= Rule 1 Pass/Fall Twoslgma= 10%ofMean= Rule 2 (Pass/Fall) 23377.9 23558.82556 24241.17444 Fall 341.1744422 2390 Pass *exception taken due to full recovery of standard Verification Rules Rule 1 =The certlftcate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value Ot the three verHlcatlon measurements. Rule 3 =The determined mean value shall be within 5% of the certHlcate value. CAN 0.851 736.1 Verification for Mixed Gamma Standard 1556 CAN Michael Hilton Isotope Result 7/1412011 Y-88(898) pCl/L Mixed Gamma N1 82690 Isotopic Abundance: 0.937 Mixed Gamma N2 81320 Certificate Value (dps): 2824 Mixed Gamma N3 80940 Mean Value (Counting)= 81650.00 pCi/L 100.2381 Pass Stdev= 920.489 pCi/L Rule 3 (Pass/Fall) Certificate Value = 81456.1 pCi/L Lower Limit = 79809.022 pCi/L Upper Limit = 83490.978 pCi/L Rule 1 Pass/Fall Pass Two sigma= 1840.978001

  • 10%ofMean= 8165 Rule 2 (Pass/Fall) Pass VerHicallon Rules Rule 1 =The certificate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verHlcatlori measurements. Rule 3 =The determined mean value shall be within 5% of the certfficate value.

Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Mean Value (Counting) = Stdev= Isotope Co-60 (1173) Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 39166.67 506.392 Result pCl/L 38910 39750 38840 pCi/L 102.7694 pCi/L pCi/L pCi/L pCi/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) CertHlcate Value = Lower Limit = Upper Limit = Rule 1 Pass/Fall Twoslgma= 10%of Mean= Rule 2 (Pass/Fall) 38111.2 38153.88173 40179.45161 Fall 1012.784939 3916.666667 Pass *exc:eP<<on taken due to full recovery of standard Verification Rules Rule 1 =The certificate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval detennlned from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value

  • of the three verification measurements. Rule 3 =The detennlned mean value shall be within 5% of the certificate value. CAN 0.9985 1408 Verification for Mixed Gamma Standard Micllael Hilton 7/14/2011 Mean Value (Counting) = Stdev= Isotope Co-60 (1332.50) Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 39430.00 675.056 Result pCUL 38940 40200 39150 pCilL 103.595 pCi/L pCi/L pCilL pCi/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) Certificate Value = Lower Limit= Upper Limit = Rule 1 Pass/Fall Two sigma= 10%otMean= Rule 2 (Pass/Fall) 38061.7 38079.88889 40780.11111 Fall 1350.111107 3943 Pass *exception taken .due to full recovery of standard VerHlcaOon Rules * '. Rule 1 =The certlffcate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval determined from the mean and two sigma standard deviation of the three measurements Rule 2 .. The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three vermcauon measurements. Rule 3 =The determined mean value shall be within 5% of the certificate value. CAN 0.9998 1408 Verification for Mixed Gamma Standard Michael Hilton 7/14/2011 Mean Value (Counting) = Stdev= Isotope V-88 (1836.1) Mixed Gamma N1 Mixed Gamma N2 Mixed Gamma N3 83530.00 967.006
  • Result pCl/L 82870 83080 84640 pCi/L 102.5723 pCi/L pCi/L pCi/L pCi/L 1556 Isotopic Abundance: Certificate Value (dps): Pass Rule 3 (Pass/Fall) Certificate Value = Lower Limit = Upper Limit= Rule 1 PasslFall Two sigma= 10%ofMean=_ Rule 2 (Pass/Fall) 81435.3 81595.98862 85464.01138 Fall 1934.011375 8353 Pass taken due to full recovery of standard VerHlcatlon Rule& Rule 1 =The certificate value (NOT Including any uncertainty) shall lie within the 95% confidence Interval detennlned from the mean and two sigma standard deviation of the three measurements Rule 2 =The two sigma value used for the 95% confidence Interval shall not exceed 10% of the mean value of the three verHlcaUon measurements. Rule 3 =The determined mean value shall be within 5% of the certHlcate value. CAN 0.992 2989 Runlogs Page 4947 of 5809 Instrument Run Log Instrument Type: GAMMA SPECTROMETER Batch ID: 1596247 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235001 SAMPLE MXR1 GAM02 OCT-03-16 07:56:53 DONE CAN 22-AUG-16 00:00 405235002 SAMPLE MXR1 GAM30 OCT-03-16 07:57:26 DONE CAN 11-MAR-16 00:00 405235003 SAMPLE MXR1 GAM08 OCT-03-16 08:01:06 DONE CAN 21-JUL-16 00:00 405235004 SAMPLE MXR1 GAM09 OCT-03-16 08:01:44 DONE CAN 03-JUN-16 00:00 405235005 SAMPLE MXR1 GAM19 OCT-03-16 08:02:09 DONE CAN 15-JUN-16 00:00 405235006 SAMPLE MXR1 GAM20 OCT-03-16 08:02:32 DONE CAN 30-JUN-16 00:00 405235007 SAMPLE MXR1 GAM32 OCT-03-16 08:02:54 DONE CAN 23-AUG-16 00:00 405235008 SAMPLE MXR1* GAM39 OCT-03-16 08:03:23 DONE CAN 27-JUL-16 00:00 405235009 SAMPLE MXR1 GAM25 OCT-03-16 08:06:24 DONE CAN 01-AUG-16 00:00 405235010 SAMPLE MXR1 GAM28 OCT-03-16 08:06:48 DONE CAN 01-AUG-16 00:00 405235011 SAMPLE MXR1 GAM33 OCT-03-16 08:07:11 DONE CAN 10-JUN-16 00:00 405235012 SAMPLE MXR1 GAM36 OCT-03-16 08:07:40 DONE CAN 01-JUN-16 00:00 405235013 SAMPLE MXR1 GAM41 OCT-03-16 08:10:29 DONE CAN 26-JAN-16 00:00 405235014 SAMPLE MXR1 GAM43 OCT-03-16 08:11:15 DONE CAN 06-SEP-16 00:00 405235015 SAMPLE MXR1 GAM44 OCT-03-16 08:11:39 DONE CAN 06-SEP-16 0.0:00 405235016 SAMPLE MXR1 GAM12 OCT-03-16 08:15:34* DONE CAN 22-SEP-16 00:00 405235017 SAMPLE MXR1 GAM16 OCT-03-16 08:16:00 DONE CAN 23-SEP-16 00:00 405235018 SAMPLE MXR1 GAM27 OCT-03-16 08:16:22 DONE CAN 03-0CT-16 00:00 405235019 SAMPLE MXR1 GAM11 OCT-03-16 08:21:03 DONE CAN 02-AUG-16 00:00 1203621350 MB MXR1 GAM31 OCT-03-16 08:50:58 DONE CAN 15-JUN-16 00:00 405235020 SAMPLE MXR1 GAM01 OCT-03-16 08:53:24 DONE CAN 20-JUL-16 00:00 1203621351 DUP MXR1 GAM05 OCT-03-16 08:53:50 DONE CAN 04-SEP-16 00:00 1203621352 LCS MXR1 GAM06 OCT-03-16 08:54:28 DONE CAN OS:-MAR-16 00:00 Page 4948 of 5809 Instrument Run Log Instrument Type: GAMMA SPECTROMETER Batch ID: 1596249 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type *
  • 405235021 SAMPLE MXR1 GAM07 OCT-03-16 08:57:41 DONE CAN 19-AUG-16 00:00 405235022 SAMPLE MXR1 GAM18 OCT-03-16 08:58:12 DONE CAN 25-JUN-16 00:00 405235023 SAMPLE MXR1 GAM24 OCT-03-16 08:58:40 DONE CAN 17-JUN-16 00:00 405235024 SAMPLE MXR1 GAM29 OCT-03-16 08:59:12 DONE CAN 25-JUN-16 00:00 405235025 SAMPLE MXR1 GAM02 OCT-03-16 09:01:15 DONE CAN 22-AUG-16 00:00 405235026 SAMPLE MXR1 GAM30 OCT-03-16 09:01 :37 DONE CAN 11-MAR-16 00:00 405235027 SAMPLE MXR1 GAM08 OCT-03-16 09:08:01 DONE CAN 21-JUL-16 00:00 405235028 SAMPLE MXR1 GAM09 OCT-03-16 09:08:29 DONE CAN 03-JUN-16 00:00 405235029 SAMPLE MXR1 GAM19 OCT-03-16 09:08:53 DONE CAN 15-JUN-16 00:00 405235030 SAMPLE MXR1 GAM20 OCT-03-16 09:09:22 DONE CAN 30-JUN-16 00:00 405235031 SAMPLE MXR1 GAM32 OCT-03-16 09:09:51 DONE CAN 23-AUG-16 00:00 405235032 SAMPLE MXR1 GAM39 OCT-03-16 09:10:21 DONE CAN 27-JUL-16 00:00 1203621356 LCS MXR1 GAM06 OCT-03-16 09:11:02 DONE CAN 08-MAR-16 00:00 405235033 SAMPLE MXR1 GAM25 OCT-03-16 09:15:18 DONE CAN 01-AUG-16 00:00 405235034 SAMPLE MXR1 GAM28 OCT-03-16 09:15:46 DONE CAN 01-AUG-16 00:00 405235035 SAMPLE MXR1 GAM33 OCT-03-16 09:16:17 DONE CAN 10-JUN-16 00:00 405235036 SAMPLE MXR1 GAM36 OCT-03-16 09:16:44 DONE CAN 01-JUN-16 00:00 405235037 SAMPLE MXR1 GAM41 OCT-03-16 09:17:13 DONE CAN 26-JAN-16 00:00 405235038 SAMPLE MXR1 GAM43 OCT-03-16 09:17:37 DONE CAN 06-SEP-16 00:00 405235039 SAMPLE MXR1 GAM44 OCT-03-16 09:18:06 DONE CAN 06-SEP-16 00:00 405235040 SAMPLE MXR1 GAM12 OCT-03-16 09:20:08 DONE CAN 22-SEP-16 00:00 . 1203621354 MB MXR1 GAM16 OCT-03-16 09:20:38 DONE CAN 23-SEP-16 00:00 1203621355 DUP MXR1 GAM27 OCT-03-16 09:21:06 DONE CAN 03-0CT-16 00:00 Page 4949of5809 Instrument Run Log Instrument Type: GAMMA SPECTROMETER Batch ID: 1596252 Sample . Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type * .. 1203621363 LCS MXR1 GAM11 OCT-03-16 05:45:34 DONE CAN 02-AUG-16 00:00 405235041 SAMPLE MXR1 GAM28 OCT-03-16 05:54:08 DONE CAN 01-AUG-16 00:00 405235042 SAMPLE MXR1 GAM08 OCT-03-16 06:55:55 DONE CAN 21-JUL-16 00:00 405235043 SAMPLE MXR1 GAM09 OCT-03-16 06:56:18 DONE CAN. 03-JUN-16 00:00 405235044 SAMPLE MXR1 GAM32 OCT-03-16 06:56:59 DONE CAN 23-AUG-16 00:00 405235045 SAMPLE MXR1 GAM39 OCT-03-16 06:57:26 DONE CAN 27-JUL-16 00:00 405235046 SAMPLE MXR1 GAM20 OCT-03-16 06:57:53 DONE CAN 30-JUN-16 00:00 405235047 SAMPLE MXR1 GAM25 OCT-03-16 07:00:30 DONE CAN 01-AUG-16 00:00 405235048 SAMPLE MXR1 GAM28 OCT-03-16 07:00:55 DONE CAN 01-AUG-16 00:00 405235049 SAMPLE MXR1 GAM33 OCT-03-16 07:01:16 DONE CAN 10-JUN-16 00:00 405235050 SAMPLE MXR1 GAM36 OCT-03-16 07:01:40 DONE CAN 01-JUN-16 00:00 405235051 SAMPLE MXR1 GAM41 OCT-03-16 07:04:39 'DONE CAN 26-JAN-16 00:00 405235052 SAMPLE MXR1 GAM44 OCT-03-16 07:04:59 DONE CAN 06-SEP-16 00:00 405235053 SAMPLE MXR1 GAM31 OCT-03-16 07:06:55 DONE CAN 15-JUN-16 00:00 405235054 SAMPLE MXR1 GAM43
  • OCT-03-16 07:07:21 DONE CAN 06-SEP-16 00:00 405235055 SAMPLE MXR1 GAM11 OCT-03-16 07:18:44 DONE CAN 02-AUG-16 00:00 405235056 SAMPLE MXR1 GAM01 OCT-03-16 07:50:44 DONE CAN 20-JUL-16 00:00 405235057 SAMPLE MXR1 GAM05 OCT-03-16 07:51 :32 DONE CAN 04-SEP-16 00:00 405235058 SAMPLE MXR1 GAM06 OCT-03-16 07:51:57 DONE CAN 08-MAR-16 00:00 405235059 SAMPLE MXR1 GAM07 . OCT-03-16 07:52:25 DONE CAN 19-AUG-16 00:00 405235060 SAMPLE MXR1 GAM18 OCT-03-16 07:52:52 DONE CAN 25-JUN-16 00:00 1203621361 MB MXR1 GAM24 OCT-03-16 07:53:26 DONE CAN 17-JUN-16 00:00 1203621362 DUP MXR1 GAM29 OCT-03-16 07:54:00 DONE CAN 25-JUN-16 00:00 Page 4950 of 5809 Instrument Run Log Instrument Type: GAMMA SPECTROMETER Batch ID: 1596254 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 1203621366 LCS MXR1 GAM11 OCT-03-16 05:28:46 DONE CAN 02-AUG-16 00:00 405235064 SAMPLE MXR1 GAM02 OCT-03-16 05:44:14 DONE CAN 22-AUG-16 00:00 405235061 SAMPLE MXR1 GAM20 OCT-03-16 05:52:51 DONE CAN 30-JUN-16 00:00 405235062 SAMPLE MXR1 GAM36 OCT-03-16 05:53:13 DONE CAN 01-JUN-16 00:00 405235063 SAMPLE MXR1 GAM44 OCT-03-16 05:53:40 DONE CAN 06-SEP-16 00:00 405235065 SAMPLE MXR1 GAM25 OCT-03-16 05:57:14 DONE CAN 01-AUG-16 00:00 405235066 SAMPLE MXR1 GAM33
  • OCT-03-16 05:57:37 DONE CAN 10-JUN-16 00:00 405235067 SAMPLE MXR1 GAM41 OCT-03-16 05:58:05 DONE CAN 26-JAN-16 00:00 405235068 SAMPLE MXR1 GAM31 OCT-03-16 06:05:07 DONE CAN 15-JUN-16 00:00 405235069 SAMPLE MXR1 GAM43 OCT-03-16 06:05:34 DONE CAN 06-SEP-16 00:00 405235070 SAMPLE* MXR1 GAM11 OCT-03-16 06:08:01 DONE CAN 02-AUG-16 00:00 405235071 SAMPLE MXR1 GAM01 OCT-03-16 06:45:24 DOl';JE CAN 20-JUL-16 00:00 405235072 SAMPLE MXR1 GAM05 OCT-03-16 06:45:49 DONE CAN 04-SEP-16 00:00 405235073 SAMPLE MXR1 GAM06 OCT-03-16 06:46:12 DONE CAN* 08-MAR-16 00:00 405235074 SAMPLE MXR1 GAM07 OCT-03-16 06:46:37 DONE CAN 19-AUG-16 00:00 405235075 SAMPLE MXR1 GAM18 OCT-03-16 06:47:01 DONE CAN 25-JUN-16 00:00 405235076 SAMPLE MXR1 GAM24 OCT-03-16 06:47:24 _ DONE CAN 17-JUN-16 00:00 405235077 SAMPLE MXR1 GAM29 OCT-03-16 06:47:53 DONE CAN 25-JUN-16 00:00 405235078 SAMPLE MXR1 GAM30 'OCT-03-16 06:48:14 DONE CAN 11-MAR-16 00:00 1203621364 MB MXR1 GAM02 OCT-03-16 06:55:01 DONE CAN 22-AUG-16 00:00 1203621365 DUP MXR1 GAM19 OCT-03-16 06:55:29 DONE CAN 15-JUN-16 00:00 Page 4951 of 5809 Instrument Run Log Instrument Type: GAMMA SPECTROMETER Batch ID: 1598618 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235001 SAMPLE MJH1 XRAY4 SEP-27-16 12:26:55 DONE 1129 17-JUN-16 00:00 405235002 SAMPLE MJH1 XRAY2 SEP-27-16 12:27:18 DONE 1129 27-JUL-16 00:00 405235003 SAMPLE MJH1 XRAY5 SEP-27*16 12:27:38 DONE 1129 30-AUG-16 00:00 405235004 SAMPLE MJH1 XRAY6 SEP-27-16 12:27:59 DONE 1129 26-JAN-16 00:00 405235005 SAMPLE MJH1 XRAY4 SEP-27-16 15:11:29 DONE 1129 17-JUN-16 00:00 405235006 SAMPLE MJH1 XRAY5 SEP-27-16 15:11:52 DONE 1129 30-AUG-16 00:00 405235007 SAMPLE MJH1 XRAY6 SEP-27-16 15:12:14 DONE 1129 26-JAN-16 00:00 405235009 SAMPLE MJH1 XRAY2 SEP-27-16 16:18:41 DONE 1129 27-JUL-16 00:00 405235008 SAMPLE MJH1 XRAY1 SEP-27-16 16:19:05 DONE 1129 09-JUN-16 00:00 405235010 SAMPLE MJH1 XRAY4 SEP-27-16 16:19:26 DONE 1129 00:00 405235011 SAMPLE MJH1 XRAY5 16:19:47 DONE 1129 30-AUG-16 00:00 405235012 SAMPLE MJH1 XRAY6 . SEP-27-16 16:20:09 DONE 1129 00:00 405235013 SAMPLE MJH1 XRAY2 SEP-28-16 06:36:49 DONE 1129 27-JUL-16 00:00 405235014 SAMPLE MJH1 XRAY4 SEP-28-16 06:45:16 DONE 1129 17-JUN-16 00:00 405235015 SAMPLE MJH1 XRAY6 SEP-28-16 06:48:23 DONE 1129 26-JAN-16 00:00. 405235016 SAMPLE MJH1 XRAY5 SEP-28-16 06:55:30 DONE 1129 30-AUG-16 00:00 405235017 SAMPLE MJH1 XRAY2 SEP-28-16 07:22:16 DONE 1129 27-JUL-16 00:00 405235018 SAMPLE MJH1 XRAY4 SEP-28-16 07:22:56 DONE 1129 17-JUN-16 00:00 405235019 SAMPLE MJH1 XRAY6 07:23:18 DONE 1129 26-JAN-16 00:00 405235020 SAMPLE MJH1 XRAY5 SEP-28-16 07:27:31 DONE 1129. 30-AUG-16 00:00 1203627430 MB MJH1 XRAY1 SEP-28-16 07:39:35 DONE 1129 09-JUN-16 00:00 1203627431 DUP MJH1 XRAY2. SEP-28-16 08:03:53 DONE 1129 27-JUL-16 00:00 1203627432 MS MJH1 XRAY4 . SEP-28-16 08:04:20 DONE 1129 17-JUN-16 00:00 1203627 433 LCS MJH1 XRAY1 SEP-28-16 08:11:05 DONE 1129 09-JUN-16 00:00 Page 4952 of 5809 Run Log Instrument Type: GAMMA SPECTROMETER Batch ID: 1598620 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235021 SAMPLE MJH1 XRAY1 SEP-28-16 08:45:02 DONE 1129 09-JUN-16 00:00 405235022 SAMPLE MJH1 XRAY2 SEP-28-16 08:45:25 DONE 1129 27-JUL-16 00:00 405235023 SAMPLE MJH1 XRAY4 SEP-28-16 08:45:52 DONE 1129 17-JUN-16 00:00 405235024 SAMPLE MJH1 XRAY5 SEP-28-16 08:46:16 DONE 1129 30-AUG-16 00:00 405235025 SAMPLE MJH1 XRAY6 SEP-28-16 08:46:38
  • DONE 1129 26-JAN-16 QO:OO 405235026 SAMPLE MJH1 XRAY1 SEP-28-16 09:28:33 DONE 1129 09-JUN-16 00:00 405235027 . SAMPLE MJH1 XRAY2 SEP-28-16 09:28:55 .DONE 1129 27-JUL-16 00:00 405235028 SAMPLE MJH1 XRAY4 SEP-28-16 09:29:20 DONE 1129 . 17-JUN-16 00:00 405235029 SAMPLE MJH1 XRAY5 09:29:56 DONE 1129 30-AUG-16 00:00 405235030 SAMPLE MJH1 XRAY6 SEP-28-16 09:30:21 DONE 1129 26-JAN-16 00:00 405235031 SAMPLE MJH1 XRAY1 SEP-28-16 10:17:59 DONE 1129 09-JUN-16 00:00 405235032 SAMPLE MJH1 XRAY2 SEP-28-16 10:18:25 DONE 1129' 27-JUL-16 00:00 405235033 SAMPLE MJH1
  • XRAY4 SEP-28-16 10:18:47 DONE 1129 17-JUN-16 00:00 405235034 SAMPLE MJH1 XRAY5 SEP-28-16 10:19:14 DONE 1129 30-AUG-16 00:00 405235035 SAMPLE MJH1 XRAY6 . SEP-28-16 10:19:45 DONE 1129 26-JAN-16 00:00 405235036 SAMPLE MJH1 XRAY1. SEP-28-16 11:17:38 DONE !129 09-JUN-16 00:00 405235037 SAMPLE MJH1 XRAY2 .SEP-28-16 11:18:01 DONE 1129 27-JUL-16 00:00 405235038 SAMPLE MJH1 XRAY4 SEP-28-1611:18:47 DONE 1129 17-JUN-16 00:00 405235039 SAMPLE MJH1 XRAY5 SEP-28-16 11:19:10
  • DONE 1129 30-AUG-16 00:00 405235040. SAMPLE MJH1 XRAY6 SEP-28-16 11: 19:53 DONE 1129 26-JAN-16 00:00 1203627437 MB MJH1 XRAY1
  • SEP-28-16 12:50:58 . DONE 1129 09-JUN-16 00:00 1203627438 DUP MJH1 XRAY2 SEP-28-16 12:51:32 DONE 1129. 27-JUL-16 00:00 1203627 439 MS MJH1 XRAY4 12:52:05 . DONE 1129* 17-JUN-16 00:00 1203627 440 LCS MJH1 XRAY5. SEP-28-16 12:52:43
  • DONE 1129
  • 30-AUG-16 00:00 Page 4953 of 5809 Instrument Run Log Instrument Type: GAMMA SPECTROMETER Batch ID: 1598647 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235041 SAMPLE MJH1 XRAY6 SEP-28-16 12:50:10 DONE 1129 26-JAN-16 00:00 405235042 SAMPLE MJH1 XRAY1 SEP-28-16 13:34:32 DONE 1129 09-JUN-16 00:00 405235043 SAMPLE MJH1 XRAY2 SEP-28-16 13:34:57 DONE 1129 27-JUL-16 00:00 405235044 SAMPLE MJH1 XRAY4 SEP-28-16 13:35:27 DONE 1129 17-JUN-16 00:00 405235045 SAMPLE MJH1 XRAY5 SEP-28-16 13:35:51 DONE 1129 30-AUG-16 00:00 405235046 SAMPLE MJH1 XRAY6 SEP-28-16 13:36:13 DONE 1129 26-JAN-16 00:00 405235047 SAMPLE MJH1 XRAY1 SEP-28-16 14:39:43 DONE 1129 09-JUN-16 00:00 405235048 SAMPLE MJH1 XRAY2 SEP-28-16 14:40:07 DONE 1129 27-JUL-16 00:00 405235049 SAMPLE MJH1 XRAY4 SEP-28-16 14:40:29 DONE 1129 17-JUN-16 00:00 405235050 SAMPLE MJH1 XRAY5 SEP-28-16 14:40:52 DONE 1129 30-AUG-16 00:00 405235051 SAMPLE MJH1 XRAY6 SEP-28-16 14:41:12 DONE 1129 26-JAN-16 00:00 405235052 SAMPLE . MJH1 XRAY1 SEP-28-16 15:14:01 DONE 1129 09-JUN-16 00:00 405235053 SAMPLE MJH1 XRAY2 SEP-28-16 15:14:23 DONE 1129 27-JUL-16 00:00 405235054 SAMPLE MJH1 XRAY4
  • SEP-28-16 15:14:44 DONE 1129 17-JUN-16 00:00 405235055 SAMPLE MJH1 XRAY5 SEP-28-16 15:15:08 DONE 1129 30-AUG-16 00:00 405235056 SAMPLE MJH1 XRAY6 SEP-28-16 15:15:30 DONE 1129 26-JAN-16 00:00 405235057 SAMPLE MJH1 XRAY1 SEP-28-16 15:48:44 DONE 1129 09-JUN-16 00:00 405235058 SAMPLE MJH1 XRAY2 SEP-28-16 15:49:08 DONE 1129 27-JUL-16 00:00 405235059 SAMPLE MJH1 XRAY4 SEP-28-16 15:49:42 DONE 1129 17-JUN-16 00:00 -405235060 SAMPLE MJH1 XRAY5 SEP-28-16 15:50:06 DONE 1129 30-AUG-16 00:00 1203627502 MB MJH1 XRAY6 SEP-28-16 15:50:32 DONE 1129 26-JAN-16 00:00 1203627503 DUP MJH1 GAM05 SEP-28-16 19:04:24 DONE 1129 06-SEP-16 00:00 1203627504 MS MJH1 XRAY1 SEP-28-16 19:05:16 DONE 1129 09-JUN-16 00:00 1203627505 LCS MJH1 XRAY2 SEP-28-16 19:05:55 DUSE 1129 27-JUL-16 00:00 1203627505 LCS MJH1 XRAY1 SEP-29-16 09:10:18 DONE 1129 09-JUN-16 00:00 Page 4954 of 5809 Instrument Run Log Instrument Type: GAMMA SPECTROMETER Batch ID: 1598663 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type i
  • 405235061 SAMPLE MJH1 XRAY4 SEP-28-16 19:09:16 DONE 1129 17-JUN-16 00:00 405235062 SAMPLE MJH1 XRAY5 SEP-28-16 19:09:43 DONE 1129 30-AUG-16 00:00 405235063 SAMPLE MJH1 XRAY6 SEP-28-16 19:10:13 DONE 1129 26-JAN-16 00:00 405235064 SAMPLE MJH1 GAM05 SEP-29-16 06:19:44 DONE 1129 06-SEP-16 00:00 405235065 SAMPLE MJH1 XRAY1 SEP-29-16 06:20:10 DONE 1129 09-JUN-16 00:00 405235066 SAMPLE MJH1 XRAY2 SEP-29-16 06:30:34 DONE 1129 27-JUL-16 00:00 405235067 SAMPLE MJH1 XRAY4 SEP-29-16 06:34:44 DONE 1129 00:00 405235068 SAMPLE MJH1 XRAY6 SEP-29-16 06:45:27 DONE 1129 26-JAN-16 00:00 405235069 SAMPLE MJH1 XRAY5 SEP-29-16 06:46:52 . DONE 1129 30-AUG-16 00:00 405235070 SAMPLE MJH1 XRAY1 SEP-29-16 06:53:16 DONE 1129 09-JUN-16 00:00 405235071 SAMPLE MJH1 XRAY2 SEP-29-16 07:04:23 DONE 1129 27-JUL-16 00:00 405235072 SAMPLE MJH1 XRAY4 SEP-29-16 07:11:09 DONE 1129 17-JUN-16 00:00 405235073 SAMPLE MJH1 XRAY5 SEP-29-16 07:18:28 DONE 1129 30-AUG-16 00:00 405235074 SAMPLE MJH1 XRAY6 SEP-29-16 07:18:54 DONE 1129 26-JAN-16 00:00 405235075 SAMPLE MJH1 XRAY1 SEP-29-16 07:24:37. DONE 1129 09-JUN-16 00:00 405235076 SAMPLE MJH1 GAM05 SEP-29-16 08:01 :20 DONE 1129 06-SEP-16 00:00 405235077 SAMPLE MJH1 XRAY1 SEP-29-16 08:02:10 DONE 1129 09-JUN-16 00:00 405235078 SAMPLE MJH1 XRAY2 SEP-29-16 08:02:53 DONE 1129 27-JUL-16 00:00
  • 1203627531 MB MJH1 XRAY4 SEP-29-16 08:03:29 DONE 1129 17-JUN-16 00:00 1203627532 DUP MJH1 XRAY5 SEP-29-16 08:03:56 DONE 1129 30-AUG-16 00:00 1203627533 MS MJH1 XRAY6 SEP-29-16 08:04:21 DONE 1129 26-JAN-16 00:00 1203627534 LCS MJH1 XRAY1 SEP-29-16 08:33:28 DONE 1129 09-JUN-16 00:00 Page 4955 of 5809 Gas Flow Raw Data Page 4956 of 5809 Effective 3/25/201 o Revision 1 Effective March 2010 Radiochemistry Batch Checklist 1 9-Sep-2016 *1c:c,17e 17 Batch# __ ....;-v __ D __ ll) __ _ Product: ___ L'-'--* n_r:s_._ __ ., Criteria: Yes No Comments Samole Solids are less than or eQual to 100 mQ for GAB. I Samples have been blank corrected (If required). Blank correction reoo11ed Included Cif reaulredl. If activity less than 10x MDA/MDC, error Is less than or eQual to 150% of sample activity. I lf greater than 10* MDA/ MDC, error is 400/o or less. IIfh .. lnLUth<> MDA/ Mnr -......... ... Instrument source check Is within limits. In..trument bka check Is within limits. / Method RDL/ LLD has been met. I / If duolicate activities are: Less than 5* MDA/ MDC, then RPD Is 1000/o or less, I If greater 5* MDA/ MDC, then RPD 20%' or less, If below the MDA/ MDC, the RPD Is 0%, Or meets the client's reaulred RER acceotance criteria. Tracer yield is 15-1250/o
  • Carrier yield 25-1250/o. (Or meets the client's contract acceptance criteria). fir' Method blank Is less than the RDL/ LLD. / lrlf .,. ... "'""""'""' < 5% nf *-.. *--* --****'""' Sample was run within hold time. ./ DtlZ Samole was correctlv oreserved If reaulred. / Smears Taken for Radioactive batches. ./ Method Spike and LCS are within 75-1250/o / !1 or """'ets the client's con*r".-t-"rr<>nt,.nce criteria). No blank spaces on data forms. / All line outs lnltialed and dated. ,.,_ -------*-Aux data is correct. M* Client Soecial reauirements oaae has been checked. / Raw Data and I or soectrum are included and orooerlv statused. / MS, LCS, and Duplicate RPD/RER values uploaded to UMS and ) '"""'"'verified ... ,. (If fl!'> ,.,_._,. --*-*-.. *-*-r---** / n1 ci lw/11 Batch Data Exceotion Reports CDER) comnleted. If annllcable. 'v-lrd l)f)l.._ r:-ft'F>7l Batch Data Exception Reports (DER) second reviewed. / k Olsoosition verified to be comnleted. Allauot Correctlnn romnleted If r"n11lrM' 11 .... Review sample historical results If available / (If REMP, results above MDC have been verified bv historical results recount or re-analvsis.) Primary Review Perfonned By: ____ ______ _ 'V Secondary Review Performed By:. ___ _____ _ Page 4957 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1
GEL Laboratories LLC Form GEL-DER .; DATA EXCEPTION REPORT' Mo.Day Yr. Division
Quality Criteria: 20-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GFPC EPA 900.0/SW846 9310/SM 711 OB Solid . *-Batch ID: Sample Numbers: 1597816 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, 1203625450, 1203625451, and 1203625452 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Nat Long 20-SEP-16 Kenshalla Oston 21-SEP-16 Page 1 Page 4958 of 5809 DER Report No.: 1559577 Revision No.: 2 Type: Process Client Code: MJWC Logbook The Determination of Gross Alpha And Gross Non-Volatile Beta in Soil, Filters, Solid Matrices And Direct Count Air Filters Batch ID: 1597816 Due Dates for Lab: 30-SEP-2016 Hold: 30*MA Y*2016 Package: 02-0CT-2016 SDG: 04-0C'f-2016 Analyst: Jasmine Conley Lab SOP: GL-RAD-A-OOlB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B Modified Instrument: BAL-16107662 Sample ID 405235001 405235002 405235003 405235004 405235005 405235006 405235Q07 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203625449 MB 1203625450 DUP (405235013) 1203625451 MS (405235013) 1203625452 :'>!SD (405235013) 1203625453 LCS Run Date J'4-SEP-2016 11:00 ;14-SEP-2016 11:00 jl4-SEP-2016 I 1:00 :14-SEP-2016I1:00 ; jl4-SEP-2016 11:00 il4-SEP-2016I1:00 !14-SEP-201611:00 j14-SEP-2016 11:00 /14-SEP-2016 11:00 fsEP-201611:00--114-SEP-2016I1:00 ! It Dry or Wet lntennediate Unadjusted Aliquot Initial Weight Final Weight Residue Detector Aliquot Aliquot (g) (gl (g) Weight w *-'---; I ! 15 ! D i 0.11 ! 0.11 l 7.5808 7.6083 27.5 I ! ! 16i D i ; 0.101 ! ! 0.101 i 7.55oi" I 7-5738 i 23.7 i r 17 j D ! 0.103 i 0.103 I 7.6397 ! 7.6659 l 26.2 l H ! ! I I 18 i D --+ 0.106 I 0.106 I 7.6637 ! 7.6892 ! 25.5 ! -I ' 19 j D 0.104 i 0.104 l 7.6148 i 7.6394 I 24.6 I ! i ! i 20 ! D ! 0.104 I 0.104 i 7.6314 I 7.6562 ! 24.8 I i I ' ! ' !14-SEP-20!6I1:00 j 21 j D 0.11 0.11 7.6119 7.6128 0.9 fS"EP-2016I1:00 22 i D 0.109 0.109 7.581 7.6088 I 27.8 !14-sEr-2016 11:00 ;14-SEP-2016 11:00 24 i D 7.5958 7.6224 I 26.6 -----------*----------------Analytical Lojlbook version 1 11-04-2004 GEL Laboratories LLC JI I .* /

Logbook The Determination of Gross Alpha And Gross. Non-Volatile Beta in Soil, Filters, Solid Matrices And Direct Count Air Filters Batch ID: 1597816 Analyst: Jasmine Conley Instrument: BAL-16107662 Lab SOP: GL-RAD-A-OOIB REV# 17 Method: EPA'900.0/SW846 9310/SM 7110B Modified Sample ID Run Date # Dry or \Vet lntennediate Umidjusted Aliquot Initial Weight Final Weight Residue Detector Type Name Serial Number RGNT RGF-Hydrotluoric Acid ! 2429436.1 RGNT RGF-IM Nitric Acid ! 2446509 RGJ\'T RGF-Hydrochloric Acid I 2447606.13 RGl\'T RGF-Nitric Acid SPIKE Strontium-90 SPIKE 2450046.4 1243-0 SPIKE Thorium-230 SPIKE I 1493-B L.-Analytical Logbook version 111-04-2004 Aliquot Aliquot (g) (,g) (g) Weight () m) Spike Amount Spike Units 10 I mL ! ; 5 ! mL I ' 5 I mL I I I 25 l mL l .J =4---::--t* GEL Laboratories LLC Spike Pipet ID: RAD-GFC-4497063 Planchets Flamed: Yes 0 ....., Vo 00 0 \0 Filename GAB.XLS Frie type Excel Version# 1.3.10 Batch: 1597816 Analyst : JAS02031 Prep Date: 9114/2016 Alpha Method Uncertainty : 0.0928 Beta Method Uncertainty : 0.0628 Geometry: 2 inch Planchett Sample Characteristics Sample Sample Sample Aliquot Residue Wt Pos. ID G (mg) 1 405235001.1 0.1030 27.1 2 405235002.1 0.0990 28.4 3 405235003.1 0.1030 25.5 4 405235004.1 0.1040 27.3 5 405235005.1 0.1030 26.6 6 405235006.1 0.1010 27 7 405235007.1 0.1070 26.2 8 405235006. 1 0.1040 27.4 9 405235009.1 0.1020 26.4 10 405235010.1 0.1090 27 11 405235011.1 0.1020 25.1 12 405235012.1 0.1040 25.6 13 405235013.1 0.1100 28 14 405235014.1 0.1030 26.1 15 405235015.1 0.1100 27.5 16 405235016.1 0.1010 23.7 17 405235017.1 0.1030 26.2 18 405235018.1 0.1060 25.5 19 405235019.1 0.1040 24.6 20 405235020.1 0.1040 24.B 21 1203625449.1 0.1100 0.9 22 1203625450.1 0.1090 27.8 23 1203625451. 1 0.1100 26.6 24 1203625452.1 0.1090 26.6 25 1203625453.1 0.1100 1.3 Sample Aliquot S!Dev. G 3.2298E-03 4.3263E--04 3.2296E-03 3.2299E-03 3.2298E-03 3.2296E--03 3.2302E-03 3.2299E-03 3.2297E-03 3.2304E-03 3.2297E-03 3.2299E-03 3.2305E--03 3.2298E--03 3.230SE-03 3.2296E-03 3.2298E-03 32301E-03 3.2299E-03 3.2299E-03 3.2305E-03 3.2304E-03 3.2305E--03 32304E-03 3.2305E-03 AB1597816r1.xls Gross Alpha/Beta Solid Count Raw Data Sample Detector Datemme ID 121101201514:20 14C 12110/2015 14:30 130 12110/2015 14:35 140 121912015 14:00 12C 12110/2015 13:15 12D 12110/2015 13:25 14A 12110/2015 13:55 C2 1211012015 14:05 J2 12/10/2015 10:30 H1 12110/2015 10:35 G2 12191201510:13 F3 12110/201511:25 G4 12181201511:23 12A 12/8/2015 10:49 B4 1218/2015 10:56 F4 12/8/201511:29 F2 12/2/2015 10;02 H3 12/2/201510:19 J1 12/812015 14:30 SC 12/8/201513:50 81 9/14/2016 0:00 140 1218/201511:23 120 12/8/2015 11 :23 14C 12/8/2015 11:23 140 9/1412016 0:00 1D Pagel Procedure Code : GFCGANBS Pannname1 : Alpha Pannname2 : Beta Required Alpha MDA : 4 Required Beta MDA: 10 Counting Time Gross Counts (min.) Alpha Beta 160 93 557 60 74 200 260 167 936 260 264 1043 230. 159 819 90 39 246 180 124 584 160 111 601 180 133 622 180 109 718 160 109 646 180 68 690 100 70 385 160 101 641 180 117 693 160 105 691 180 105 654 180 117 573 100 81 276 160 119 682 70 15 52 140 121 534 60 243 3055 60 239 3163 60 466 3086 pCl/G pCl/G Count Start Datemme 9/1612016 10:57 9/1612016 10:57 9/16/2016 10:58 9/161201610:58 9/1612016 10:58 9/16/2016 10:58 9/19/201612:41 9/19/2016 12:32 9119/2016 12:32 9/1912016 12:32 9119/2016 12:32 9/19/201612:32 9120/201611:56 9/191201614:16 9/19/2016 12:32 9/19/201612:32 9/19/2016 12:32 9/19/2016 12:32 9119/2016 12:30 9/1912016 14:16 9/19/2016 12:20 9120/201611:56 9/20/2016 11 :56 9/20/2016 11:56 9/191201612:37 Pipet, 0.1 ml Stdev: +/-0.000200 ml Pipe!, 0.5 ml Stdev: +/* 0.001000 ml Pipe!, 1 ml Stdev : +/-0.002000 ml Analytical SOP: GL-RAD*Ml01B Instrument SOP: GL-RAD-1-016. GL-RAD-1-006 Calibration Data Alpha Calibration Calibration Detector Counted Calibration Due Source Efficiency Pos. on Date Date Used (cpm/dpm) PIC 1211/2015 11/30/2016 Th230 0.1457 2 PIC 121112015 11/3012016 Th230 0.1257 3 PIC 1211/2015 11/30/2016 Th230 0.1364 4 PIC 1211/2015 11/30/2016 Th230 0.1535 5 PIC 121112015 11/30/2016 Th230 0.1520 6 PIC 1211/2015 11130/2016 Th230 0.1402 7 LB4100 1211/2015 11/30/2016 Th230 0.1547 8 LB4100 121112015 11/30/2016 Th230 0.1536 9 LB4100 12/1/2015 11/3012016 Th230 0.1311 10 LB4100 1211/2015 11/30/2016 Th230 0.1247 11 LB4100 121112015 11/3012016 Th230 0.1504 12 LB4100 1211/2015 11/30/2016 Th230 0.1414 13 PIC 1211/2015 11/30/2016 Th230 0.1459 14 LB4100 121112015 11/30/2016 Th230 0.1206 15 LB4100 1211/2015 11/30/2016 Th230 0.1164 16 lB4100 1211/2015 11/30/2016 Th230 0.1344 17 lB4100 1211/2015 11/30/2016 Th230 0.1190 18 LB4100 1211/2015 11/30/2016 Th230 0.1481 19 PIC 1211/2015 11/30/2016 Th230 0.1800 20 LB4100 1211/2015 11/30/2016 Th230 0.1579 21 PIC 1211/2015 11/30/2016 Th230 0.2484 22 PIC 1211/2015 11/30/2016 Th230 0.1494 23 PIC 1211/2015 11/30/2016 Th230 0.1470 24 PIC 1211/2015 11/30/2016 Th230 0.1337 25 PIC 1211/2015 11/3012016 Th230 0.2796 AB 1597816r1.xls Det.Eff. Calibration Error Calibration Due (cpm/dpm) X-Talk Date Date 0.02173 0.18747 1211/2015 11/30/2016 0.01236 0.26740 1211/2015 11/30/2016 0.01512 029598 121112015 11/3012016 0.02199 0.08779 1211/2015 11/30/2016 0.01863 0.12384 121112015 11/30/2016 0.02505 0.21106 1211/2015 11/30/2016 0.02436 0.21445 12/1/2015 11/30/2016 0.00765 0.02390 1211/2015 11/30/2016 0.01393 0.03342 1211/2015 11/30/2016 0.01976 0.02932 12/1/2015 11/30/2016 0.02244 0.03271 1211/2015 11/30/2016 0.02077 0.03070 1211/2015 11/30/2016 0.01685 0.17032 12/1/2015 11/30/2016 0.02055 0.03077 12/112015 11/30/2016 0.02862 0.04145 1211/2015 11/30/2016 0.03128 0.02996 121112015 11/30/2016 0.01513 0.03349 1211/2015 11/30/2016 0.01256 0.02187 121112015 11/30/2016 0.01161 0.06015 121112015 11/30/2016 0.01406 0.01841 12/112015 11/30/2016 0.01512 0.23521 121112015 11/3012016 0.01863 0.12437 1211/2015 11/30/2016 0.02173 0.18712 121112015 11/30/2016 0.01512 0.29676 121112015 11/3012016 0.00996 0.03816 121112015 11/30/2016 Page2 Beta Weekly Background Calibration Detector Del.Elf. Count Count Source Efficiency Error CPM Start Trme Used (cpm/dpm) (cpm/dpm) X-Talk Alpha Beta Date/Trme (min.) Sr90 0.4667 0.01828 0.00032 0.142 1.268 9/9/201617:55 500 Sr90 0.4361 0.01144 0.00027 0.032 0.322 9/9/201617:54 500 Sr90 0.4645 0.00738 0.00033 0.212 0.860 9/9/201617:55 500 Sr90 0.4824 0.01666 0.00051 0.282 0.748 9/912016 17:58 500 Sr90 0.4876 0.01845 0.00043 0.222 1.428 919/2016 17:59 500 Sr90 0.4650 0.02119 0.00031 0.056 0.428 9/9/201617:54 500 Sr90 0.4978 0.02351 0.00026 0.190 1.220 9/1612016 17:48 500 Sr90 0.4781 0.01035 0.00034 0.098 0.726 9/16/2016 17:29 500 Sr90 0.4862 0.00965 0.00035 0.066 0.960 9/1612016 17:44 500 Sr90 0.4920 0.01349 0.00018 0.126 1.174 9/161201617:43 500 Sr90 0.5060 0.00981 0.00026 0.122 0.942 9/16/201617:44 500 Sr90 0.4949 0.00938 0.00022 0.110 0.988 9/1612016 17:43 500 Sr90 0.4800 0.01954 0.00028 0.088 0.888 9/1612016 18:00 500 Sr90 0.4607 0.00972 0.00037 0.074 1.284 9/16/2016 17:32 500 Sr90 0.5124 0.00850 0.00029 0.110 1.394 9/16/2016 17:44 500 Sr90 0.5073 0.01365 0.00039 0.098 1.138 9/1612016 17:44 500 Sr90 0.5136 0.00824 0.00027 0.054 1.130 9/16/2016 17:44 500 Sr90 0.4818 0.01589 0.00041 0.184 0.788 9/16/201617:29 500 Sr90 0.4990 0.00657 0.00367 0.132 0.856 9/16/2016 17:25 500 Sr90 0.4887 0.01796 0.00042 0.188 1.314 9/16/2016 17:32 500 Sr90 0.4735 0.00738 0.00033 0212 0.793 9/161201617:23 1000 Sr90 0.4872 0.01845 0.00043 0.146 1.342 9/16/201618:01 500 Sr90 0.4670 0.01828 0.00032 0.135 1.297 9/16/201617:23 1000 Sr90 0.4641 0.00738 0.00033 0.212 0.793 9/16/2016 17:23 1000 Sr90 0.4959 0.00692 0.00767 0.190 1.456 9/1612016_.17:24 500 Notes: 1 -Reference data for Spike Activity (dpm/ml) is the batch Prep Date Alpha Results Decision Critical Required Sample Act Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 2.3933 1.6897 4 3.9420 13.1484 14.75% 2 1.8164 1.2824 4 3.9219 32.2936 12.15% 3 2.5673 1.8125 4 3.9686 12.2892 13.60% 4 2.6064 1.8401 4 3.9826 20.6122 9.62% 5 2.5170 1.7770 4 3.9293 13.4606 13.04% 6 2.0084 1.4180 4 3.8964 11.9765 19.04% 7 2.4030 1.6965 4 3.8468 13.5567 13.57% 8 1.7879 1.2623 4 2.9945 14.5940 12.04% 9 1.7525 1.2373 4 3.0359 22.6230 10.27% 10 2.3829 1.6824 4 3.9172 15.8720 13.04% 11 2.0767 1.4661 4 3.4216 14.1675 13.01% 12 2.0580 1.4529 4 3.4165 11.5824 14.78% 13 2.1247 1.5000 4 3.8419 17.1432 14.25% 14 1.99n 1.4104 4 3.4251 17.6140 12.32% 15 2.3637 1.6688 4 3.9241 18.9622 12.17% 16 2.1045 1.4858 4 3.5248 16.0598 12.88% 17 1.7290 1.2207 4 3.0537 19.4111 11.47% 18 2.4921 1.7595 4 3.9970 13.3302 13.93% 19 2.2317 1.5756 4 3.8732 16.0717 13.89"/o 20 2.4081 1.7001 4 3.8573 12.9305 13.87% 21 2.1863 1.5435 4 3.7935 0.0336 2503.03% *22 2.3544 1.6622 4 3.9171 19.8204 11.73% 23 3.1694 2.2376 4 5.8679 108.5909 7.58% 24 4.4088 3.1126 4 1.n12 116.0610 7.61% 25 2.0319 1.4346 4 3.6013 105.1736 5.68% AB1597816r1.xls Alpha Spike SIN : Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: Spike Nuclide: Alpha LCS SIN : LCS Exp Dale: LCS Activity (dpm/ml): LCS Volume Added: LCS Nuclide: 2SIGMA Net Count NetCounl Counting Rate Rate Error Uncertainty CPM CPM pCi/G 0.4393 0.0626 3.6812 0.8930 0.1078 7.6484 0.3844 0.0505 3.1757 0.7323 0.0647 3.5789 0.4693 0.0587 3.3127 o.3n3 0.0702 4.3765 0.4989 0.0649 3.4605 0.5187 0.0602 3.3263 0.6729 0.0651 4.2971 0.4796 0.0601 3.9068 0.4836 0.0601 3.4562 0.3789 0.0542 3.2538 0.6120 0.0847 4.6591 0.4871 0.0571 4.0610 0.5400 0.0619 4.2690 0.4853 0.0586 3.8140 0.5293 0.0579 4.1669 0.4660 0.0631 3.5467 0.6780 0.0915 4.3139 0.4731 0.0636 3.4200 0.0023 0.0572 1.8483 0.7183 0.0804 4.3588 3.9150 0.2601 14.19n 3.n13 02581 15.6391 7.5767 0.3603 10.3414 Page3 1493-B 6/812017 266.08 0.10 Th-230 1493*8 618/2017 266.08 0.10 Th-230 2SIGMA Total Prop. Uncertainty pCi/G 4.5024 9.6820 3.9n2 5.4142 4.2355 4.9834 4.3752 4.3569 6.1498 4.9854 4.4472 3.9709 5.7239 5.3382 5.7011 5.0127 5.6245 4.3860 5.3425 4.2445 1.8489 5.8235 25.6114 27.4266 23.6571 Sample QC 405235013.1 405235013.1 405235013.1 Sample Nominal Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP 14.5% MS 108.9599 83.9% MSD 6.7% 109.9595 90.0% LCS 108.9599 96.5% AB1597816r1.xls Notes: Beta Spike SIN : 1243-0 1 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date Spike Exp Date: 12/18/2016 Spike Activity ( dpmfmt}: 483.55 Spike Volume Added: 0.10 Spike Nuclide: Sr-90 Beta LCS SIN : 1243-0 LCS Exp Date : 12/1812016 LCS Activity (dpmfml): 483.55 LCS Volume Added: 0.10 LCS Nuclide: Sr-90 Beta Results 2SIGMA 2SIGMA Decision Critical Required SampleAcL SampleAcL Net Count Net Count Counting Total Prop. Level Level MDA MDA Cone. Error Rate Rate Error Uncertainty Uncertainty Sample Sample Nominal Pas. pCi/G pCi/G pCi/G pCi/G pCilG % CPM CPM pCi/G pCi/G QC Type RPO REA pCi/G Recovery 1 2.2330 1.5765 10 3.3287 19.7175 7.92% 2.2133 0.1559 2.8625 4.1094 SAMPLE 2 1.6613 1.1729 10 2.7370 20.1455 8.29% 2.1780 0.1786 3.6525 4.6328 SAMPLE 3 1.5184 1.0720 10 2.2449 21.7133 5.70% 2.4829 0.1169 2.1566 3.8868 SAMPLE 4 1.3506 0.9536 10 2.0033 25.9321 5.40% 2.9770 0.1217 2.1411 4.3382 SAMPLE 5 1.9896 1.4047 10 2.9263 18.3613 7.32% 2.1329 0.1354 2.3805 3.6154 SAMPLE 6 1.6741 1.1820 10 2.6836 21.2347 8.57% 2.3053 0.1767 3.3221 4.6052 SAMPLE 7 1.8919 1.3357 10 2.8123 15.8718 8.04% 2.0244 0.1431 2.3713 3.4224 SAMPLE 8 1.5634 1.1038 10 2.3586 23.5391 6.33% 2.6129 0.1414 2.5114 4.1358 SAMPLE 9 1.8025 12726 10 2.6966 22.4444 6.70% 2.4956 0.1453 2.5872 4.0795 SAMPLE 10 1.8433 1.3014 10 2.7427 23.4952 6.44% 2.8149 0.1586 2.5774 4.1701 SAMPLE 11 1.7157 1.2113 10 2.5661 23.0273 6.48% 2.6580 0.1479 2.5308 4.1027 SAMPLE 12 1.7618 1.2439 10 2.6336 24.7704 6.27"/,, 2.8453 0.1526 2.6168 4.3301 SAMPLE 13 2.0520 1.4487 10 3.1534 24.2533 7.64% 2.9620 0.2007 3.3559 4.8989 SAMPLE 14 2.1784 1.5379 10 3.2341 21.4504 7.34% 2.2771 0.1495 2.7615 4.0925 SAMPLE 15 1.9110 1.3492 10 2.8316 19.4127 7.03% 2.4560 0.1555 2.4356 3.6266 SAMPLE 16 1.8996 1.3411 10 2.8287 23.5927 6.67% 2.7009 0.1536 2.6475 4.2627 SAMPLE 17 1.8333 1.2943 10 2.7305 21.1502 6.81% 2.5033 0.1498 2.5004 3.8693 SAMPLE 18 1.5858 1.1196 10 2.3862 21.0033 6.74% 2.3953 0.1388 2.3994 3.8140 SAMPLE 19 2.0498 1.4472 10 3.1547 16.2775 9.48% 1.9240 0.1718 2.9226 3.7212 SAMPLE 20 2.0575 1.4526 10 3.0530 21.8259 7.18% 2.4749 0.1539 2.6729 4.1002 SAMPLE 21 2.2187 1.5664 10 3.5035 -0.8696 213.00% -0.0501 0.1068 1.8104 1.8104 MB 22 2.1890 1.5455 10 3.2727 20.0573 7.02% 2.4723 0.1730 2.8759 4.1221 405235013.1 DUP 18.9% 23 3.0929 2.1836 10 4.8056 428.4758 3.93% 49.6197 0.9219 15.8452 63.1659 405235013.1 MS 396.0263 102.1% 24 2.4556 1.7337 10 3.9126 451.8070 3.55% 51.9237 0.9378 16.3659 65.3629 405235013.1 MSD 5.3% 399.6596 107.0% 25 3.1721 2.2395 10 4.8919 410.2631 3.54% 49.9n3 0.9274 15.0111 58.3236 LCS 396.0263 103.6% Page4 ""O Pl (1Q Cl> \0 0\ 1597816r1 .xis Vl 0 ......, Vl 00 Sample ID Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID 0 \0 405235001 14C 160 93 557 9/16/2016 10:57 9/16/2016 13:37 Pf C 1597816 405235002 130 80 74 200 9/16/2016 10:57 9/16/2016 12:17 PIC 1597816 405235003 140 280 167 936 9/16/2016 10:58 9/16/2016 15:38 PIC 1597816 405235004 12C 280 284 1043 9/16/2016 10:58 9/16/2016 15:38 PIC 1597816 405235005 120 230 159 819 9/16/2016 10:58 9/16/2016 14:48 PIC 1597816 405235006 14A 90 39 246 9/16/2016 10:58 9/16/2016 12:28 PIC 1597816 405235007 C2 180 124 584 9/19/2016 12:41 9/19/2016 15:41 LB4100 1597816 405235008 J2 180 111 601 9/19/2016 12:32 9/19/2016 15:32 LB4100 1597816 405235009 H1 180 133 622 9/19/2016 12:32 9/19/2016 15:32 LB4100 15978'16 405235010 G2 180 109 718 9/19/2016 12:32 9/19/2016 15:32 LB4100

  • 1597816 405235011 F3 180 109 648 9/19/2016 12:32 9/19/2016 15:32 LB4100 1597816 405235012 G4 180 88 690 9/19/2016 12:32 9/19/2016 15:32 LB4100 1597816 405235013 12A 100 70 385 9/20/2016 11 :56 9/20/2016 13:36 PIC 1597816 405235014 84 180 101 641 9/19/201614:16 9/19/201617:16 LB4100 1597816 405235015 F4 180 117 693 9/19/2016 12:32 9/19/2016 15:32 LB4100 1597816 405235016 F2 180 105 691 9/19/2016 12:32 9/19/2016 15:32 LB4100 1597816 405235017 H3 180 105 654 9/19/2016 12:32 9/19/2016 15:32 LB4100 1597816 405235018 J1 180 117 573 9/19/2016 12:32 9/19/2016 15:32 LB4100 1597816 405235019 SC 100 81 278 9/19/2016 12:30 9/19/2016 14:10 PIC 1597816 405235020 81 180 119 682 9/19/201614:16 9/19/2016 17:16 LB4100 1597816 1203625449 140 70 15 52 9/19/2016 12:20 9/19/2016 13:30 PJC 1597816 1203625450 120 140 121 534 9/20/2016 11 :56 9/20/2016 14: 16 PIC 1597816 1203625451 14C 60 243 3055 9/20/2016 11 :56 9/20/2016 12:56 PIC 1597816 1203625452 140 60 239 3163 9/20/2016 11 :56 9/20/2016 12:56 PIC 1597816 1203625453 1 0 60 466 3086 9/19/2016 12:37 9/19/2016 13:37 PIC 1597816 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 2010 21-Sep-2016 Batch# ___ / __ Product: _______ _ , Criteria: Yes No Comments Samele Solids are less than or eaual to 100 mCI for GAB. I Samples have been blank corrected (if required). ft' Blank correction reoorted Included (if reouired). If activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity, I If greater than 10* MDA/ MDC, error Is 40% or less. If hAlnw the Mnd I MDC error Is ni.,.u Instrument source check Is within limits. / Instrument bko check Is within llmi'"" Method RDL/ LLD has been met. / If duplicate activities are: Less than S* MDA/ MDC, then RPO is 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, / S-et. V\°'\f'fO"l lf below the MDA/ MDC, the RPO Is 0%, Or meets the client's reC1ulred RER acceotance criteria. Tracer yield Is 15-125%
  • Carrier yield 25-125%. rf' (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. / llTf ----*---' 'iO/n nf "rtlvltv\ Sa mole was run within hold time. / DPZ lSl1 s-s.(:. Samnle was correctlv oreserved If reoulred. / Smears Taken for Radioactive batches. / Method Spike and LCS are within 75-125% ./ llor meet<< the client'" contract accentanc" criterl:>\, No blank spaces on data forms. / All line outs initialed and dated. Nn Arrnrr "*A Aux data Is correct. tt'-Client Soeclal reoulrements aaoe has been checked. / Raw Data and I or snectrum are Included and nronerlv statused. / MS, LCS, and Duplicate RPD/RER values uploaded to UMS and / lu;ol11P<: V"riflPrl IWi* -llf rfl -u A"*ArAA '"*" '""rA / Batch Data Exceotlon Reoorts <DER) comoleted If aoolicable. t./ Olf7 l'Sl,1$3(. Batch Data Exception Reports (DER) second reviewed. /"" Dlsnosition verified to be comnleted. Allouot Correction comoleted If reaulred tf' Review sample historical results If available / (If REMP, results above MDC have been verified bv hlstorlcal results recount or re-analvsls.) Primary Review Performed By:. ____ ____ _ Secondary Review Performed By: ____ ___ _____ _ Page 4966 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER
  • DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 26-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: -Matrix Type: GFPC EPA 900.0/SW846 9310/SM 71108 Solid . Batch ID: Sample Numbers: 1597817 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample Analyzed out of Holding Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results 405235065,405235066, 405235067,405235068,405235069, 405235070,405235071,405235072, 405235073,405235074, 405235075,405235076,405235077,405235078, 1203625460, 1203625461, and 1203625462 were received and analyzed out of holding. .. Originator's Name: Data Validator/Group Leader: Nat Long 26-SEP-16 Kenshalla Oslan 27-SEP-16 Page 1 Page 4967 of 5809 DER Report No.: 1561536 Revision No.: Type: Process Client Code: MJWC Logbook The of Gross Alpha And Gross Non-Volatile Beta in Soil, Filters, SpJid And Count Air Filters Batch ID: 1597817 Analyst: .Jasmine Conley Instrument: BAL-16107662 Type Name RGNT RGF-Hydrofluoric Acid Due Dates for Lab: Ol-OCT-2016 Hold: 08-JUN-2016 Package: 02-0CT-2016 SDG: 04-0CT-2016 Serial Number Spike Amount Spike Units Lab SOP: GL-RAD-A-OOlB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B Modified Spike Pipet ID: RAD-GFC-4497063 Planchets Flamed: Yes Analytical Logbook \'Crsion 1 11-04-2004 GEL Laboratories LLC /

Logbook The Determination of Gross Alpha And Gross Non-Volatile Beta in Soil, Filters, Solid l\tlat:rices Count Air Filters Batch ID: 1597817 . Analyst: Jasmine Conley Lab SOP: GL-RAD-A-OOlB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B Modified Instrument: BAL-16107662 Sample ID RGNT RGNT RGNT SPIKE SPIKE # Dry or \Vet lmerrnediate Unadjusted Aliquot Initial Weight Final Weight Residue Aliquot Aliquot (g) (g) (g) Weight Run Date Detector _______________________ _lg_> _______________________ _l!!!gL ___________ _ RGF-1 M Nitric Acid RGF-Hydrochloric Acid [-*----2447606}3----i---:s---r---mL Spike Pipet ID: RAD-GFC-4497063 RGF-Nitric Acid ;-*---2454839-:.7 ___ Planchets Flamed: Yes Stromium-90 SPIKE L_ ______ _______ J ___ .1 _____ Thorium-230 SPIKE [_ ____ *.'__ __ i __ ; Analytical version 111-04-2004 GEL Laboratories LLC GAB.XLS File type Excel Version ii 1.3.10 Batch : 1597817 Analyst: JAS02031 Prep Date : 9121/2016 Alpha Method Uncertainty : 0.0928 Beta Method Uncertainty : 0.0628 Geometry: 2 inch Planchett Sample Characteristics Sample Sample Sample Aliquot Residue Wt. Pos. ID G (mg) 1 405235061.1 0.1000 21.3 2 405235062.1 0.1040 16.5 3 405235063.1 0.1050 19.4 4 405235064.1 0.1070 23.2 5 405235065.1 0.0990 22.5 6 405235066.1 0.1080 24.6 7 405235067.1 0.1090 22.3 8 405235068.1 0.1020 18.9 9 405235069.1 0.1060 20.4 10 405235070.1 0.1040 17.7 11 405235071. 1 0.1060 20.8 12 405235072.1 0.1080 24.6 -13 405235073.1 0.1080 18.6 14 405235074.1 0.1110 23.8 15 405235075.1 0.1000 20.8 16 405235076.1 0.1050 18 17 405235077.1 0.1090 21.2 18 405235078.1 0.1060 17.3 19 1203625459.1 0.1110 0 20 1203625460.1 0.1080 17.9 21 1203625461.1 0.1030 19 22 1203625462.1 0.1060 19.2 23 1203625463.1 0.1110 0 Sample Aliquot StDev. G 4.3713E-04 3.2299E-03 3.2300E-03 3.2302E-03 4.3283E-04 3.2303E-03 3.2304E-03 3.2297E-03 3.2301E-03 3.2299E-03 3.2301E-03 3.2303E-03 3.2303E-03 3.2306E-Q3 4.3713E-04 3.2300E-03 3.2304E-03 3.2301E-03 3.2306E-03 3.2303E-03 3.2298E-03 3.2301E-03 3.2306E-03 AB1597817r1.xls Gross Alpha/Beta Solid Count Raw Data -Sample Detector Datemme ID 1211412015 13:47 14A 121141201513:10 14D 1211412015 13:15 128 1211412015 13:25 14C 12114/2015 13:56 13A 1211412015 14:00 13D 1211112015 11:30 G4 1211112015 10:27 F4 12116/201512:45 G2 12111/2015 10:10 F3 1211112015 10:25 F2 121151201513:35 H1 12111/2015 11:35 G3 121151201514:10 H3 12116/2015 9:31 13A 12111/2015 14:19 14A 12117/201513:30 130 12117/2015 12:40 110 9/21/2016 0:00 11C 121111201511:35 118 121111201511:35 50 12/11/201511:35 2C 9/21/2016 0:00 3C Page 1 Procedure Code : Parmname1: Parmname2: Required Alpha MDA : Required Beta MDA : Counting GFCGAN8S Alpha Beta 4 pCi/G 10 pCVG Count Time Gross Counts Start (min.) Alpha Beta Datemme 70 73 318 9/22/2016 12:39 150 127 661 912212016 12:39 160 274 861 9/22/2016 12:39 110 104 547 91221201612:40 60 37 142 912212016 12:40 70 63 253 912212016 12:40 150 142 703 9/22/201613:57 150 128 681 91221261613:57 ' 150 106 552 912212016 13:57 150 112 564 912212016 13:57 150 90 514 91221201613:57 150 100 548 912212016 13:57 150 158 880 912212016 13:57 150 79 527 9/2212016 13:57 60 23 143 912212016 14:00 60 23 138 9/22/201614:00 60 39 139 912212016 14:00 60 93 334 912212016 14:00 60 4 24 9/2212016 14:00 100 108 436 9/22/2016 14:00 60 339 2510 912312016 13:24 60 344 2411 9/2212016 13:58 60. 497 3157 912212016 13:58 0 ....., V1 00 0 \0 Pipe!, 0.1 ml Stdev : +/-0.000200 ml Pipe!, 0.5 ml Stdev : +/-0.001000 ml Plpet, 1 ml Stdev: +/-0.002000 ml Analytical SOP: GL-RAD-A-001 B Instrument SOP: GL-RAD-1-016, GL-RAD-1-006 Calibration Data Alpha Calibration Calibration Detector Counted Calibration Due Source Efficiency Pos. on Date Date Used (cpm/dpm) 1 PIC 12/112015 1113012016 Th230 0.1576 2 PIC 1211/2015 11/30/2016 Th230 0.1653 3 PIC 1211/2015 11/30/2016 Th230 0.1770 4 PIC 1211/2015 11/30/2016 Th230 0.1567 5 PIC 1211/2015 11i30/2016 Th230 0.1622 6 PJC 1211/2015 11/30/2016 Th230 0.1352 7 LB4100 1211/2015 11/30/2016 Th230 0.1519 8 LB4100 12/1/2015 11/30/2016 Th230 0.1420 9 LB4100 1211/2015 11/30/2016 Th230 0.1452 10 LB4100 1211/2015 11/30/2016 Th230 0.1772 11 LB4100 1211/2015 11/30/2016 Th230 0.1434 12 LB4100 1211/2015 11/30/2016 Th230 0.1368 13 LB4100 121112015 11/3012016 Th230 0.1389 14 LB4100 1211/2015 11/3012016 Th230 0.1265 15 PIC 1211/2015 11/30/2016 Th230 0.1675 16 PIC 1211/2015 11/30/2016 Th230 0.1701 17 PIC 12/1/2015 11/3012016 Th230 0.1453 18 PIC 1211/2015 11/30/2016 Th230 0.2011 19 PIC 1211/2015 11130/2016 Th230 0.2689 20 PJC 1211/2015 11/30/2016 Th230 0.1899 21 PIC 121112015 11/30/2016 Th230 0.1980 22 PIC 1211/2015 11/30/2016 Th230 0.1649 23 PIC 1211/2015 11/30/2016 Th230 0.2859 Del.Elf. Error (cpm/dpm) X-Talk 0.02505 0.20876 0.01512 0.28417 0.01035 0.15152 0.02173 0.18415 0.00569 0.16542 0.01236 0.26424 0.02077 0.02899 0.02862 0.03511 0.01976 0.02615 0.02244 0.02875 0.03128 0.02839 0.01393 0.03234 0.02238 0.04263 0.01513 0.03187 0.00669 0.16374 0.02505 0.20560 0.01236 0.26046 0.01128 0.08089 0.01271 0.14397 0.00743 0.08728 0.00639 0.06415 0.01156 0.07922 0.00568 0.02997 AB1597817r1.xls Beta Weekly Background Calibration Calibration Detector Del.Elf. Count Count Calibration Due Source Efficiency Error CPM Start Time Date Date Used (cpm/dpm) (cpm/dpm) X-Talk Alpha Beta DatefTime (min.) 12/112015 11/3012016 Sr90 0.4672 0.02119 0.00031 0.043 0.415 9/161201617:23 1000 121112015 11/3012016 Sr90 0.4678 0.00738 0.00033 0.212 0.793 9/1612016 17:23 1000 1211/2015 11/30/2016 Sr90 0.4913 0.01114 0.00040 0.230 0.626 9/16/201618:01 500 1211/2015 11/30/2016 Sr90 0.4687 0.01828 0.00032 0.135 1.297 9/1612016 17:23 1000 1211/2015 11130/2016 Sr90 0.4626 0.00714 0.00044 0.031 0.461 9/16/201617:22 1000 1211/2015 11/30/2016 Sr90 0.4374 0.01144 0.00027 0.040 0.346 9/16/201617:23 1000 1211/2015 11/30/2016 Sr90 0.4962 0.00938 0.00022 0.110 0.988 9/1612016 17:43 500 12/112015 11130/2016 Sr90 0.5167 0.00850 0.00029 0.110 1.394 9/161201617:44 500 1211/2015 11/30/2016 Sr90 0.4950 0.01349 0.00018 0.126 1.174 9/161201617:43 500 1211/2015 11/30/2016 Sr90 0.5095 0.00981 0.00026 0.122 0.942 9/1612016 17:44 500 1211/2015 11130/2016 Sr90 0.5086 0.01365 0.00039 0.098 1.138 9/16/201617:44 500 1211/2015 11/30/2016 Sr90 0.4869 0.00965 0.00035 0.056 0.960 9/161201617:44 500 121112015 11/30/2016 Sr90 0.5061 0.01089 0.00025 0.134 1.042 9/16/201617:43 500 121112015 11/30/2016 Sr90 0.5148 0.00824 0.00027 0.054 1.130 9/16/2016 17:44 500 1211/2015 11/30/2016 Sr90 0.4632 0.00714 0.00044 0.031 0.461 9/1612016 17:22 1000 1211/2015 11/30/2016 Sr90 0.4685 0.02119 0.00031 0.043 0.415 9/16/2016 17:23 1000 121112015 11/30/2016 Sr90 0.4386 0.01144 0.00027 0.040 0.346 9/161201617:23 1000 1211/2015 11/30/2016 Sr90 0.5053 0.01068 0.00031 0.092 1.256 9/161201618:00 500 121112015 11/30/2016 Sr90 0.4900 0.01278 0.00036 0.152 0.444 9/16/2016 18:00 500 12/1/2015 11/30/2016 Sr90 0.4963 0.00697 0.00028 0.170 0.950 9/1612016 18:00 500 1211/2015 11130/2016 Sr90 0.4956 0.00925 0.00363 0.174 0.748 9/161201617:26 500 1211/2015 11/30/2016 Sr90 0.4283 0.01274 0.00315 0.132 0.506 9/161201617:24 500 1211/2015 11/30/2016 Sr90 0.4823 0.00988 0.00835 0.240 0.556 9/16/2016 17:25 500 Page2 Notes: 1 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date Alpha Results Decision Critical Required Sample Act. Sample Act. Net Count Level Level MDA MDA Cone. Error Rate Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % CPM 1 1.7074 1.2054 4 3.6358 28.5374 12.49% 0.9999 2 2.4613 1.7377 4 3.9994 16.5911 12.54% 0.6347 3 2.4594 1.7363 4 3.9270 35.8700 7.83% 1.4825 4 2.3102 1.6310 4 3.9947 21.7287 12.11% 0.8105 5 1.5294 1.0798 4 3.5620 16.3979 17.35% 0.5857 . 6 1.m0 1.2551 4 3.8327 26.5070 13.60% 0.8600 7 1.9567 1.3814 4 3.3069 22.7282 10.31% 0.8367 8 2.2379 1.5800 4 3.7820 23.0812 11.19% 0.7433 9 2.2538 1.5912 4 3.7678 16.9777 12.66% 0.5807 10 1.8514 1.3071 4 3.1030 15.2405 12.19% 0.6247 11 2.0125 1.4209 4 3.4345 14.8384 13.62% 0.5020 12 1.6985 1.1992 4 3.0079 18.2691 11.74% 0.6007 13 2.3843 1.6833 4 3.9673 27.5614 10.01% 0.9193 14 1.6170 1.1416 4 2.9248 15.1328 13.14% 0.4727 15 1.4666 1.0354 4 3.4156 9.4480 22.76% 0.3523 16 1.6192 1.1432 4 3.5470 8.5628 23.90% 0.3403 17 1.7613 1.2435 4 3.9089 17.3287 17.39% 0.6100 18 2.0404 1.4406 4 3.9377 30.7734 11.53% 1.4580 19 1.8728 1.3222 4 3.3990 -1.2899 44.20% -0.0853 20 2.3119 1.6322 4 3.9235 19.9645 12.00% 0.9100 21 2.9324 2.0703 4 5.2447 117.5699 6.46% 5.4760 22 2.9806 2.1043 4 5.4972 141.0879 6.42% 5.6013 23 2.2134 1.5627 4 3.8350 107.9247 5.50% 8.0433 AB1597817r1.xls Alpha Spike SIN : Spike Exp Date : Spike Activity (dpmlmO: Spike Volume Added: Spike Nuclide: Alpha LCS SIN : LCS Exp Date : LCS Activity (dpmlmO: LCS Volume Added: LCS Nuclide: 2SIGMA Net Count Counting Rate Error Uncertainty CPM pCi/G 0.1222 6.8476 0.0765 3.9301 0.1057 5.0179 0.0934 4.9195 0.1015 5.5818 0.1136 6.8684 0.0808 4.3082 0.0769 4.6867 0.0704 4.0418 0.0723 3.4610 0.0648 3.7629 0.0676 4.0414 0.0854 5.0252 0.0602 3.7825 0.0801 4.2238 0.0802 3.9633 0.1043 5.8119 0.1613 6.6807 0.0376 1.1126 0.1055 4.5446 0.3074 13.3063 0.3095 15.6353 0.3722 10.3540 Page3 1493-B 61812017 266.08 0.10 Th-230 1493-B 618/2017 266.08 0.10 Th-230 2SIGMA Total Prop. Uncertainty pCi/G 8.7142 5.0855 8.5495 6.5118 6.3365 8.5619 6.1886 6.5875 5.2305 4.5828 4.8067 5.3688 7.3858 4.7816 4.5644 4.3115 6.7025 8.9380 1.1137 5.9442 26.8022 31.9193 24.1324 Sample QC 405235073.1 405235073.1 405235073.1 Sample Nominal Type RPO RER pCi/G Recoveiy SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP 32.0% 1.5705 MS 116.3649 nA% MSD 18.2% 1.1059 113.0715 100.4% LCS 107.9782 100.0% Notes: 1

  • Reference date for Spike Activity (dpm/ml) is the batch Prep Date Beta Results Decision Critical Required Sample Act. Sample Act Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 1.7893 1.2633 10 2.9397 37.7011 6.56% 2 1.6821 1.1876 10 2.5603 31.2307 5.77o/o 3 1.4622 1.0323 10 2.2283 39.2583 5.11% 4 2.3942 1.6903 10 3.6255 31.4507 6.85% 5 2.0683 1.4603 10 3.4124 17.7416 10.52% 6 1.6159 1.1408 10 2.6903 28.8988 7.68% 7 1.7956 1.2677 10 2.7020 30.5745 5.83% 8 2.1890 1.5455 10 3.2619 26.6339 6.64% 9 2.0178 1.4246 10 3.0209 21.3563 7.34% 10 1.7896 12635 10 2.6970 23.7726 6.67% 11 1.9333 1.3649 10 2.8969 18.9790 7.69% 12 1.8204 1.2852 10 2.7418 22.8855 6.79% 13 1.8246 1.2882 10 2.7412 39.3882 528% 14 1.8175 12832 10 2.7240 18.6536 7.37% 15 2.0449 1.4437 10 3.3737 18.0845 10.46% 16 1.8270 1.2899 10 3.0377 16.5405 11.09% 17 1.7166 1.2119 10 2.8950 16.9745 10.51% 18 3.0006 2.1185 10 4.6575 35.2008 7.86% 19 1.7566 1.2402 10 2.8944 ..().4439 197.57% 20 2.0907
  • 1.4760 10 3.2042 27.8648 6.97% 21 2.4294 1.7152 10 3.8716 359.3384 3.85% 22 2.2466 1.5861 10 3.6683 389.1384 3.89% 23 1.9971 1.4100 10 3.2407 435.9281 3.56% Net Count Rate CPM 4.1279 3.6137 4.7553 3.6757 1.9057 32683 3.6987 3.1460 2.5060 2.8180 2.2687 2.6933 4.8247 2.3833 1.9223 1.8850 1.9707 4.3107 -0.0440 3.4100 41.0853 39.6773 52.0607 AB1597817rl.xls Beta Spike SIN : Spike Exp Date : Spike Activity (dpmlml): Spike Volume Added: Spike Nuclide: 1243-0 12118/2016 483.33 0.10 Sr-90 Beta LCS SIN : 1243-0 LCS Exp Date : 12118/2016 LCS Activity (dpmlml): 483.33 LCS Volume Added: 0.10 LCS Nuclide: Sr-90 2SIGMA 2SIGMA Net Count Counting Total Prop. Rate Error Uncertainty Uncertainty CPM pCi/G pCi/G 0.2556 4.8297 7.0834 0.1737 3.1521 5.5927 0.1868 3.1967 6.5904 0.2156 3.7963 6.0117 0.1998 3.8513 4.5001 02280 4.2613 6.0582 0.1823 2.9751 5.1720 0.1818 3.0458 4.8185 0.1640 2.7589 4.0743 0.1642 2.7353 4.3028 0.1585 2.5954 3.7204 0.1621 2.7214 4.1820 0.2030 3.2782 6.3913 0.1603 2.4758 3.5661 0.2005 3.8210 4.4709 0.1968 3.5332 4.3123 0.1974 3.6454 4.4554 0.3087 5.0887 7.1466 0.0869 1.4108 1.4109 0.2133 3.5135 5.2690 0.8359 14.4568 52.3449 0.8190 15.9255 57.0145 0.9370 15.4525 61.9821 Page4 Sample Sample Nominal QC Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235073. 1 OUP 34.3% 2.7267 405235073. 1 MS 422.7464 75.7% 405235073.1 MSD 8.0% 0.7546 410.7819 85.1% LCS 392.2782 111.1%

"'d (JQ ct> \0 1597817r1 .xis -J 0 ....., Vo Sample ID Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID 00 0 \0 405235061 14A 70 73 318 9/22/2016 12:39 9/22/2016 13:49 PIG 1597817 405235062 140 150 127 661 9/22/2016 12:39 9/22/2016 15:09 PIG 1597817 405235063 128 160 274 861 9/22/2016 12:39 9/22/2016 15: 19 PIG 1597817 405235064 14G 110 104 547 9/22/2016 12:40 9/22/2016 14:30 PIG 1597817 405235065 13A 60 37 142 9/22/2016 12:40 9/22/2016 13:40 PIG 1597817 405235066 130 70 63 253 9/22/2016 12:40 9/22/2016 13:50 PIG 1597817 405235067 G4 . 150 142 703 9/22/2016 13:57 9/22/2016 16:27 LB4100 1597817 405235068 F4 150 128 681 9/22/2016 13:57 9/22/2016 16:27 LB4100 1597817 405235069 G2 150 106 552 9/22/2016 13:57 9/22/2016 16:27 LB4100 1597817 405235070 F3 150 112 564 9/22/2016 13:57 9/22/2016 16:27 LB4100 1597817 405235071 F2 150 90 514 9/22/201613:57 9/22/2016 16:27 LB4100 1597817 405235072 H1 150 100 548 9/22/2016 13:57 9/22/2016 16:27 LB4100 1597817 405235073 G3 150 158 880 9/22/2016 13:57 9/22/2016 16:27 LB4100 1597817 405235074 H3 150 79 527 9/22/2016 13:57 9/22/2016 16:27 LB4100 1597817 405235075 13A 60 23 143 9/22/2016 14:00 9/22/2016 15:00 PIC 1597817 405235076 14A 60 23 138 9/22/2016 14:00 9/22/2016 15:00 PIG 1597817 405235077 130 60 39 139 9/22/2016 14:00 9/22/2016 15:00 PlC 1597817 405235078 110 60 93 334 9/22/2016 14:00 9/22/2016 15:00 PIC 1597817 1203625459 11G 60 4 24 9/22/2016 14:00 9/22/2016 15:00 PIC 1597817 1203625460 118 100 108 436 9/22/2016 14:00 9/22/2016 15:40 PIC 1597817 1203625461 50 60 339 2510 9/23/2016 13:24 9/23/2016 14:24 PIC 1597817 1203625462 2C 60 344 2411 9/2212016 13:58 9/22/2016 14 :58 PIG A 1597817 1203625463 3G 60 497 3157 9/22/2016 13:58 9/22/2016 14:58 PIG 1597817 Effective 3/25/201 o Radiochemistry Batch Checklist Revision 1 Effective March 2010 19-Sep-2016 Batch# ________ _ Sy Product:. _______ _ CJ 1 \'1 l lk Date:. ______ _ Criteria: Yes No Comments Samole Solids are less than or equal to 100 m11 for GAB. 1A Samples have been blank corrected (if required). Blank correction reoorted Included Cif reouiredl. lf activity less than lOx MDA/MDC, error Is less I than or equal to 150% of sample activity. lf greater than 10* MDA/ MDC, error Is 40% or less. [f h<>ln..., the M n4 I M nr <>*mr 15 Instrument source check Is within limits. I Ins*rnmen* hko check Is within limits. Method RDL/ LLD has been met. ) If duollcate activities are: Less than 5* MDA/ MDC, then RPO is 100% or less, I If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's renuired RER acccotance criteria. Tracer vleld Is 15-125%

  • Carrier yleld 25-125%. I (Or meets the client's contract acceotance criteria). Method blank ls less than the RDL/ LLD. / lfTf < r;o/n nf ln..,nr* ;'lt'tivltvl Samole was run within hold time. ./ h-12:. tu-1 Samole was correctlv oreservcd if required. / Smears Taken for Radioactive batches. ) Method Spike and LCS are within 75-1250/o / 'or meets the client's contr"rt acceotance crlterial. No blank spaces on data forms. / All line outs Initialed and dated. Nn n .. Aux data is.correct. t1 Client Soecial reoulrements oaoe has been checked. / Raw Data and I or soectrum are Included and orooerlv statused. I MS, LCS, and Duollcate RPD/RER values uoloaded to UMS and / ""'"' m*rlflo>tl Hit (if rJ>. nn*nrn..i ln*n -I "i/h Batch Data Exceotlon Reoorts fDERl comoleted If aoollcable. v Ni/ l)C-fZ. 1'5S"1lO'J Batch Data Exception Reports (DER) second reviewed. Dlsnosltion verified to be comoleted. ./ Allnunt Cnrrection comnleted if reouired. 'N, Review samole historical results If available / Cif REMP, results above MDC have been verified bv historical results recount or re-analvsis. l ** Primary Review Performed By: ___ Y Secondary Review Performed By:. ___ _________ _ Page 4975 of 5809 Gl-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 19-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GFPC EPA 905.0 Modified/DOE RP501 Solid -*-,wv. Batch ID: Sample Numbers: 1597795 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample Analyzed out of Holding Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, and 1203625399 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Nat Long 19-SEP-16 Kenshalla Oston 20-SEP-16 Page 1 Page 4976 of 5809 DER Report No.: 1559107 Revision No.: 1
  • Type: Process Client Code: MJWC Prep Logbook The Determination of Strontium 89/90 in Water, Soil, Milk, Filters, Vegetation .and Tissues Batch ID: 1597795 Kelli Dorrell T.11'.ie.___ __ p_escriptiq!! _________ , __________ .. _ Number __ §FJJi0.mo.!!!!!_j.P]!!' _ Analyst: LCS 1203625400 Strontium-90 SPIKE 1243-0 .I mL Method: Lab SOP: Instrument: Sample ID EPA 905.0 Modified/DOE RPSOI Rev. 1 Modified GL-RAD-A-004REV#17 BAL-16107662 Prep Date Dry or Wet Unadjusted Aliquot (g) Aliquot (g) Initial Wt (g) Final Wt (g) Net Wt (mg) Sr Separation (date) 405235001 405235002 405235003 4052350!>> 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203625398 MB 16-SEP-2016 10:43 D ---*-*0374----.. --0.37-4 ---* 0.0238 15:08 16-SEP-2016 10:43 D 0.309 0.309 0.0241 0.0317 7.6 09/16/16 15:08 fo 16-SEP-2016 10:43 D 0.308 0.308 0.0234 0.0309 7.5 09/16/16 15:08 -ld.
  • 16-SEP-201610:43 D 0.323 0.323 0.0243 0.0311 6.8 09/16/16 15:08 -\d.3 16-SEP-2016 10:43 D 0.397 0.397 0.0241 0.0307 6.6 09116116 l 6-SEP-2016 10:43 D 0.398 0.398 0.0229 0.0295 6.6 09/16/16 15:08 -l , 16-SEP-2016 10:43 D 0.84 0.84 0.0235 0.0306 7.1 09/16/16 15:08 *-108 16-SEP-2016 10:43 D 0.344 0.344 0.024 0.0316 7.6 09/16/16 15:08 1:?,v 16-SEP-201610:43 D 0.357 0.357 0.0241 0.0304 6.3 09/16/1615:08 -J<il.0 16-SEP-2016 10:43 D 0.44 0.44 0.024 0.0309 6.9 09/16/16 15:08 -!"\ 16-SEP-2016 10:43 D 0.361 0.361 0.025 0.0311 6.1 09/16/1615:08 -Ii'.+ 16-SEP-2016 10:43 D 0.321 0.321 0.0242 0.0307 6.5 09116/1615:08 -113 16-SEP-2016 10:43 D 0.314 0.314 0.0242 0.0312 7 09/16/16 15:08 -\C:. 16-SEP-2016 10:43 D 0.31 0.31 0.0226 0.0295 6.9 09/16/1615:08 SEP-201610:43 D 0.341 0.341 0.0228 0.0299 7.1 09/16116 15:08 -S°lr 16-SEP-2016 10:43 D 0.396 0.396 0.0231 0.0301 7 09116116 15:08
  • 16-SEP-2016 10:43 D 0.378 0.378 0.0236 0.0306 7 09/16/16 15:08 -\'\A 16-SEP-2016 10:43 D 0.331 0.331 0.0235 0.0313 7.8 09/16/16 15:08 -:;Z, 16-SEP-2016 10:43 D 0.346 0.346 0.0243 0.0313 7 09/16/16 15:08 S1' 16-SEP-2016 10:43 D 0.334 0.334 0.0244 0.0311 6.7 09/16/1615:08 -5c. 1203625399 DUP (405235005) 1203625400 LCS 16-SEP-2016 10:43 D Oi 9'i 0.0227 0.0296 6.9 09116116 15:08 -51:> 16-SEP-2016 10:43 D 0.314 0.314 0.0257 0.0316 5.9 09/16/16 15:08 -1,a.f.l 1 !6-SEP-2016 -la$ fl //l Lot ID Description Amount 20646 il:2 ____________ 2213530 O.OSM HNOJ 15 mL 2243751 RGF-6M Sodium Hydroxide 6 mL 2243757 RGF-0.75M Sodium Carbonate 13mL 2334614 Thymol Blue Indicator 5mL 2388714 RGF-80% Ethanol 3mL 2414995 Sr 0.5mL=7.37, 2.0 mL=29.46 mg .Sm!. 2424020 RGF-3M Nitricl0.05M Oxalic IOmL 2433863.1 SR SPEC RESIN Cleaned 2g 2434028 RGF-Sr Filters IL 2434079 RGF-SM Nitric Acid 25mL Analytical Logbook version I 11-04-2002 Comments: Spike Pipe! JD: RAD-GFC-1795419 Carrier Pi pet ID: RAD-GFC-2154115 Data Entry Date2: 16-SEP-2016 15:08 GFC-F30560 Kelli Dorrell / GEL Laboratories LLC Filename : SR90.XlS File type : Excel Version # : 1.3.1 O Batch : 1597795 Analyst: KEl01237 Prep Date: 9/16/2016 Method Uncertainty : 0.089724205 Geometry: Tuffryn Filter Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Pos. ID G G 1 405235001.1 0.3740 3.2581E-03 2 405235002.1 0.3090 3.2513E-03 3 405235003.1 0.3080 3.2512E-03 4 405235004.1 0.3230 3.2528E-03 5 405235005.1 0.3970 3.2605E-Q3 6 405235006.1 0.3980 3.2606E-03 7 405235007.1 0.8400 3.3067E-03 8 405235008.1 0.3440 3.2550E-03 9 405235009.1 0.3570 3.2563E-03 10 405235010.1 0.4400 32650E-03 11 405235011.1 0.3610 3.2567E-03 12 405235012.1 0.3210 3.2525E-03 13 405235013.1 0.3140 3.2518E-03 14 405235014.1 0.3100 3.2514E-03 15 405235015.1 0.3410 3.2546E-03 16 405235016.1 0.3960 3.2604E-03 17 405235017 .1 0.3780 3.2585E-03 18 405235018.1 0.3310 3.2536E-03 19 405235019.1 0.3460 3.2552E-03 20 405235020.1 0.3340 3.2539E-03 21 1203625398.1 0.8400 3.3067E-03 22 1203625399 .1 0.3140 3.2518E-03 23 1203625400.1 0.8400 3.3067E-03 S1597795r1.xls Strontium-90 Solid Carrier SIN : Carrier Exp Date : Carrier Volume Added: Carrier Weight (mgfml): Carrier Weight StDev.: Sample Datemme 12110/2015 14:20 12110/201514:30 12110/2015 14:35 12/9/201514:00 12110/2015 13:15 12110/2015 13:25 12110/201513:55 12110/2015 14:05 12110/201510:30 12110/2015 10:35 1219/2015 10:13 12/10/2015 11 :25 1218/2015 11 :23 1218/201510:49 1218/2015 10:56 12/8/201511:29 1212/201510:02 121212015 10:19 12/81201514:30 121812015 13:50 9/1612016 0:00 12/10/2015 13:15 9/1612016 0:00 2414995 613/2017 0.50 14.73 0.10 carrier calculations Carrier Weight(mg) (Standard) 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 Page 1 Procedure Code : GFC90SRS Parmname: Strontium-90 Required MDA : 2 pCi/G Sr-90 Abundance : 1.00 Halflife of Sr-90 : 28.90 years Haiflife of Y-90 : 64.053 hours Net Net Carrier Carrier Weight(mg) Weight Aliquot Aliquot (Sample) StDev. (mg) (ml) StDev. {ml) 7.40 0.039135 0.5 0.001000 7.60 0.039995 0.5 0.001000 7.50 0.039565 0.5 0.001000 6.80 0.036556 0.5 0.001000 6.60 0.035697 0.5 0.001000 6.60 0.035697 0.5 0.001000 7.10 0.037846 0.5 0.001000 7.60 0.039995 0.5 0.001000 6.30 0.034407 0.5 0.001000 6.90 0.036986 0.5 0.001000 6.10 0.033548 0.5 0.001000 6.50 0.035267 0.5 0.001000 7.00 0.037416 0.5 0.001000 6.90 0.036986 0.5 0.001000 7.10 0.037846 0.5 0.001000 7.00 0.037416 0.5 0.001000 7.00 0.037416 0.5 0.001000 7.80 0.040854 0.5 0.001000 7.00 0.037416 0.5 0.001000 6.70 0.036127 0.5 0.001000 6.90 0.036986 0.5 0.001000 5.90 0.032688 0.5 0.001000 6.50 0.035267 0.5 0.001000 Pipet, 0.1 ml Stdev : +I* Pipet, 0.5 ml Stdev : +/* Pipet, 1 ml Stdev : +I* Analytical SOP: GL-RAD-A-004 Instrument SOP: GL-RAD-1-016 0.000200 0.001000 0.002000 Count Raw Data Counting Detector TI me Gross Counts Gross Beta Pas. ID (min.) Alpha* Beta CPM 1 11C 60 2 19 0.311 2 SC 60 3 4S 0.748 3 12A 60 7 4S 0.733 4 12B 60 2S 47 0.726 s 12C 60 10 49 0.804 6 120 60 7 84 1.388 7 13B 60 19 so 0.792 8 130 60 13 31 0.466 9 14C 60 11 63 1.022 10 14D 60 16 60 0.931 11 1A 60 6 42 0.692 12 1B 60 13 81 1.332 13 1C 60 17 52 0.855 14 4B 60 10 95 1.561 15 SA 60 5 80 1.329 16. 10A 60 2 24 0.382 17 14A 60 s 41 0.668 18 3B 60 15 93 1.539 19 SB 60 17 29 0.471 20 SC 60 7 45 0.745 21 SD 60 2 35 0.582 22 6A 60 s 41 0.678 23 6B 60 2 1551 25.849 S159n95r1 .xis ml ml ml Count Start Datemme 9/17/2016 1S:SO 9/19/201611:SS 9117/2016 1S:S1 9/17/20161S:S1 9/17/20161S:S1 9/17/20161S:51 9/17/2016 1S:S1 9/17/20161S:S1 9/17/201615:51 9/17/20161S:S1 9/17/201616:32 9/17 /2016 16:32 9/17/201616:32 9/17/201616:32 9/17/201616:32 9/17/201616:31 9/17/201616:34 9/17/201616:40 9/17/2016 16:40 9/17/201616:40 9/17/201616:40 9/17/2016 16:39 9/17/201616:39 Page 2 Strontium Separation Date/Time 9/1612016 1 S:08 9/16/2016 1 S:08 9/1612016 1 S:08 9/16/20161S:08 9/1612016 1 S:08 9/16/2016 1 S:08 9/16120161S:08 9/1612016 1 S:08 9116/2016 1S:08 9/16/2016 15:08 9/161201615:08 9/1612016 15:08 9/16/2016 15:08 9/16/2016 15:08 9/1612016 15:08 9/16/2016 15:08 9116/201615:08 9/1612016 15:08 9/16/2016 1 S:08 9/1612016 15:08 9/1612016 15:08 9/16/201615:08 9/16/2016 15:08 Yttrium Ingrowth 0.239 O.S28 0.239 0.239 0.239 0.239 0239 0.239 0.239 0.239 0.244 0.244 0.244 0.244 0.244 0.244 0.245 0.246 0.246 0.246 0.246 0.245 0.24S Calculated Sample Sample Sr-90 Recovery Recovery Decay % Error% 0.982 100% 1.03% 0.982 103% 1.03% 0.982 102% 1.03% 0.982 92.3% 1.04% 0.982 89.6% 1.04% 0.982 89.6% 1.04% 0.982 96.4% 1.03% 0.982 103% 1.03% 0.982 85.S% 1.05% 0.982 93.7% 0.982 82.8% 1.05% 0.982 88.3% 1.04% 0.982 95.0% 1.04% 0.982 93.7% 1.04% 0.982 96.4% 1.03% 0.982 95.0% 1.04% 0.981 95.0% 1.04% 0.981 106% 1.02% 0.982 9S.0% 1.04% 0.982 91.0% 1.04% 1.000 93.7% 1.04% 0.982 80.1% 1.06% 1.000 88.3% 1.04%

S 1597795r1 .xis Calibration Data De1ector Weekly Bkg WeeklyBkg Calibration Detector Efficiency Count Count Counted Calibration Due Efficiency (cprnldpm) Error Alpha WeeklyBkg Start TI me Pos. on Date Date Sr-90 Y-90 (cpmldpm) X-Talk CPM Datemme (min.) 1 PIC 411/2016 2128/2017 0.4167 0.5497 0.01278 0.16693 0.444 9/16/2016 18:00 500 2 PIC 4/1/2016 2128/2017 0.4218 0.5617 0.01970 0.04606 0.978 9/16/2016 17:58 500 3 PIC 411/2016 2/2812017 0.4039 0.5410 0.01964 0.14272 0.888 9/16/2016 18:00 500 4 PIC 4/1/2016 2128/2017 0.4173 0.5374 0.01114 0.13789 0.626 9/16/201618:01 500 5 PIC 4/1/2016 2/28/2017 0.4200 0.5456 0.01666 0.07332 0.862 9/16/201618:01 500 6 PIC 4/1/2016 2/2812017 0.4215 0.5487 0.01845 0.10267 1.342 9116/2016 18:01 500 7 PIC 4/1/2016 2128/2017 0.4193 0.5214 0.00967 0.13169 0.527 9/16/2016 17:23 1000 a PIC 4/1/2016 212812017 0.3796 0.4297 0.01144 0.23485 0.346 9/16/2016 17:23 1000 9 PIC 4/1/2016 2128/2017 0.4269 0.5645 0.01828 0.15081 1.297 9/16/201617:23 1000 10 PIC 4/1/2016 2128/2017 0.4231 0.5571 0.00738 0.25894 0.793 9/16/201617:23 1000 11 PIC 4/1/2016 2128/2017 0.4232 o.54n 0.00738 0.07964 0.606 9/16/2016 17:24 500 12 PIC 4/1/2016 2128/2017 0.4263 0.5497 0.00711 0.08244 1.062 9/16/2016 17:24 500 13 PIC 4/1/2016 2128/2017 0.4259 0.5634 0.00847 0.04151 0.996 9/16/201617:24 500 14 PIC 4/1/2016 212812017 0.4238 0.5578 0.01519 0.13553 1.560 9/16/2016 17:25 500 15 PIC 4/1/2016 2128/2017 0.4327 0.5685 0.00851 0.05137 1.386 9/161201617:25 500 16 PIC 4/1/2016 212812017 0.3715 0.4608 0.00651 0.52970 0.320 9/16/2016 17:59 500 17 PIC 4/1/2016 2/2812017 0.4305 0.5582 0.02119 0.18297 0.415 9/16/201617:23 1000 18 PIC 4/1/2016 2128/2017 0.4053 0.5509 0.01614 0.04495 1.400 9/161201617:25 500 19 PIC 4/1/2016 212812017 0.4300 0.5665 0.00426 0.04259 0.532 9/16/2016 17:25 500 20 PIC 411/2016 2128/2017 0.4203 0.5622 0.00657 0.04320 0.856 9/161201617:25 500 21 PIC 4/1/2016 2/28/2017 0.4252 0.5641 0.00925 0.04583 0.748 9/16/201617:26 500 22 PIC 411/2016 212812017 0.4140 0.5572 0.02228 0.06108 0.878 9/1612016 17:58 500 23 PIC 4/1/2016 212812017 0.4219 0.5616 0.00851 0.04451 1.214 9/16/2016 17:58 500 Page3 0 >-+, Vo 00 0 \0 Notes: 1 -Results are decay corrected to Sample DatefTime 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Dateffime * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 0.4727 0.3337 2 0.7788 -0.2961 58.67% 2 0.6309 0.4455 2 0.9911 -0.4616 52.20% 3 0.8232 0.5812 2 1.2996 -0.4244 76.54% 4 0.7104 0.5015 2 1.1441 0.2817 115.70% 5 0.6927 0.4891 2 1.0953 -0.1349 213.74% 6 0.8587 0.6062 2 1.3289 0.1072 349.14% 7 0.2343 0.1654 2 0.3829 0.2757 44.29% 8 0.4884 0.3448 2 0.8236 0.3211 75.20% 9 0.9434 0.6661 2 1.4659 -0.7346 49.36% 10 0.5520 0.3897 2 0.8795 0.2761 92.59% 11 0.6828 0.4821 2 1.1019 0.2371 131.23% 12 0.9477 0.6691 2 1.4826 0.7803 57.76% 13 0.8668 0.6120 2 1.3604 -0.3850 90.34% 14 1.1216 0.7919 2 1.7248 2.103E-03 22891.79% 15 0.9152 0.6462 2 1.4144 -0.1391 277.22% 16 0.4536 0.3203 2 0.7665 0.1570 134.33% 17 0.4495 0.3174 2 0.7474 0.5702 42.54% 18 0.9126 0.6443 2 1.4098 0.3362 121.56% 19 0.5693 0.4020 2 0.9265 -0.1489 155.50% 20 0.7967 0.5625 2 1.2602 -0.3004 107.05% 21 0.2796 0.1974 2 0.4456 -0.1688 63.67% 22 0.9881 0.6976 2 1.5608 -0.6617 5727% 23 0.3808 02688 2 0.5920 26.7439 3.02% S1597795r1.xls Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): NIA NIA NIA NIA Spike Volume Added: LCS SIN: 1243-0 LCS Exp Date: 12118/2016 LCS Activity (dpm/ml): 483.48 LCS Volume Added: 0.10 2SIGMA 2SIGMA Net Count Net Count Counting Total Prop. Rate Rate Error Uncertainty Uncertainty CPM CPM pCi/G pCi/G -0.1329 0.0779 0.3404 0.3404 -0.2303 0.1201 0.4717 0.4717 -0.1547 0.1183 0.6364 0.6364 0.0999 0.1155 0.6387 0.6407 -0.0576 0.1230 0.5651 0.5651 0.0460 0.1607 0.7333 0.7336 0.2646 0.1171 0.2392 0.2443 0.1198 0.0901 0.4732 0.4767 -0.2746 0.1354 0.7099 0.7100 0.1380 0.1277 0.5010 0.5034 0.0860 0.1129 0.6097 0.6112 0.2701 0.1560 0.8831 0.8941 -0.1411 0.1274 0.6815 0.6816 0.0007 0.1707 0.9437 0.9437 -0.0569 0.1579 0.7557 0.7557 0.0623 0.0837 0.4135 0.4144 0.2531 0.1075 0.4746 0.4865 0.1388 0.1687 0.8009 0.8033 -0.0607 0.0944 0.4539 0.4539 -0.1110 0.1189 0.6302 0.6302 -0.1662 0.1058 0.2106 0.2106 -0.1998 0.1143 0.7420 0.7420 24.6345 0.6582 1.4006 4.9821 Page4 Sample Sample Nominal QC Type RPO RER pCi/G Rec0very SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235005.1 DUP

  • 0.0% LCS 25.9269 103.2%

>-c si;l (Jq (1) .j::.. \0 00 1597795r1 .xis N 0 Vl 00 Sample ID Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID 0 \0 405235001 11C 60 2 19 9/17 /2016 15:50 9/17/2016 16:50 PIG 1597795 405235002 6C 60 3 45 9/19/2016 11 :55 9/19/2016 12:55 PIG 1597795 405235003 12A 60 7 45 9/17/201615:51 9/17/2016 16:51 PIC 1597795 405235004 12B 60 25 47 9/17 /2016 15:51 9/17/2016 16:51 PIG 1597795 405235005 12C 60 10 49 9/17/2016 15:51 9/17/201616:51 PIC 1597795 405235006 120 60 7 84 9/17/2016 15:51 9/17/2016 16:51 PIC 1597795 405235007 13B 60 19 50 9/17/2016 15:51 9/17/2016 16:51 PIG 1597795 405235008 130 60 13 31 9/17/201615:51 9/17/201616:51 PIG 1597795 405235009 14G 60 11 63 9/17/201615:51 9/17/2016 16:51 PIC 1597795 405235010 140 60 16 60 9/17 /2016 15:51 9/17 /2016 16:51 PIG

  • 1597795 405235011 1A 60 6 42 9/17/201616:32 9/17 /2016 17:32 PIG 1597795 405235012 18 60 13 81 9/17/201616:32 9/17 /2016 17:32 PIG 1597795 405235013 1G 60 17 52 9/17/2016 16:32 9/17 /2016 17:32 PIG 1597795 40523S014 48 60 10 95 9/17/201616:32 9/17 /2016 17:32 PIG 1597795 40S235015 SA 60 s 80 9/17/201616:32 9/17 /2016 17:32 PIG 159779S 40523S016 10A 60 2 24 9/17/201616:31 9/17/2016 17:31 PIG 1S9779S 405235017 14A 60 s 41 9/17 /2016 16:34 9/17/2016 17:34 PIC 1S97795 40S23S018 38 60 1S 93 9/17 /2016 16:40 9/17 /2016 17:40 PIG 1S97795 40523S019 5B 60 17 29 9/17/201616:40 9/17 /2016 17:40 PIC 1S97795 405235020 SC 60 7 4S 9/17/201616:40 9/17/2016 17:40 PIG 1S9779S 1203625398 50 60 2 3S 9/17 /2016 16:40 9/17/201617:40 PIG 1S97795 120362S399 6A 60 5 41 9/17/201616:39 9/17/2016 17:39 PIG 1597795 1203625400 68 60 2 1551 9/17 /2016 16:39 9/17 /2016 17:39 PIC 1597795 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 201 O 20-Sep-2016 (;'A->1 Product: ____ Date: Cf /'JA1 }/(, . .. Criteria: Yes No Comments Sa mole Sollds are less than or eaual to 100 mp for GAB. / Samples have been blank corrected (if required). /\/ti Blank correction reoorted Included <If reoulred). If activity less than 10x MDA/MDC, error Is less / than equal to 150% of sample activity. Xf greater than 10* MDA/ MDC, error Is 40% or less. [f i..n1n ...... ft MDA I MDr Prrnr I<: nl*-" Instrument source check Is within limits. /" ln<=trumt>nt hkn ,.he,.k le within llmlt<<. Method RDL/ LLD has been met. / [f duollcate activities are: Less than 5* MDA/ MDC, then RPO Is 100%.or less, / Xf greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%1 Or meets the client's reaulred RER acceotance criteria. Tracer yield Is 15-125%
  • Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). rJA Method blank Is less than the RDL/ LLD. ltTf --" ----*--<' "'O/n nf *-.. *--* .,rtlultv\ Samole was run within hold time. .?,;'.!11., ./ OG!l Samnle was correctlv nreserved If reoulred. NA Smears Taken for Radioactive batches. fl/A Method Spike and LCS are within 75-125% /" lrar mPets the client's contract acceotance criteria). No blank spaces on data forms. / All line outs Initialed and dated. No APPMe 3PA Aux data ls correct. tvtl Client Soeclal reaulrements nano has been checked. / Raw Data and/ or soectrum are Included and orooerlv statused. .,,,,,..--MS, LCS, and Duplicate RPD/RER values uploaded to UMS and / lual .. ne un*lflnd lu:* llf (J./>( ln-*-i.. --*-*-" 1-*n ,_ ___ _.,,.. Batch Data Exceotion Reoorts CDER) comoleted If aoollcable. v Batch Data Exception Reports (DER) second reviewed. Dlsoosltlon verified to be comoleted. Aliquot Corrert1nn comoleted If rnnulred, fl}P, Review sample historical results If available / (If REMP, results above MDC have been verified bv hlstorlcal results recount or re-analvsls.) Primary Review Performed By: __ ____ 'f_Jz., __ f_u_, __________ _ Secondary Review Performed .M -:f.vJ C l I cJ/cf Page 4983 of 5809 J.S!qi.& I .5 S" 'J'l io Ot:lt-GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT
  • Mo.Day Yr. Division: Quality Criteria: 20-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GFPC EPA 900.0/SW846 9310/SM 71108 Solid . Batch ID: Sample Numbers: 1597811 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample Analyzed out of Holding Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, 1203625436, 1203625437,and1203625438 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Kenshalla Osten 20-SEP-16 Nat Long 20-SEP-16 Page 1 Page 4984 of 5809 DER Report No.: 1559260 Revision No.: Type: Process Client Code: MJWC The Determination of Gross Alpha And Gross Non-Volatile Beta in Soil, Filters, Solid Matrices And Direct Count Air Filters Batch ID: 1597811 Analyst: Bethany Fiem Instrument: BAL-18550299 Due Dates for Lab: Ol-OCT-2016 Hold: 21-.MA Y-2016 Package: 02-0CT-2016 SDG: 04-0CT-2016 Lab SOP: GL-RAD-A-OOIB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B Modified ---------*-------**-------*---------------*----Sample ID 405235025 405235026 405235027 405235028 405235029 405235030 405235031 405235032 405235033 405235034 405235035 405235036 405235037 405235038 405235039 405235040 1203625435 lvlB 1203625436 DUP (405235033) 1203625437 MS (405235033) 1203625438 MSD (405235033) 1203625439 LCS Run Date Analytical Logbook version I 11-04-2004 Detector J GEL Laboratories LLC The Determination of Gross Alpha.And Gross Non-Volatile Beta in Soil, Filters, Solid Matrices And Direct Count Air Filters Batch ID: 159781 l Analyst: Bethany Fiem Instrument: BAL-18550299 Lab SOP: GL-RAD-A-OOIB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B Modified Sample In Run Date # D1y or Wet lntennediate Unadjusted Aliquot Initial Weight Final Weight Residue Detector Type RGNT RGNT RGNT RGNT SPIKE SPIKE Aliquot Aliquot (g) (g) (g) Weight -------*------------*----*----*-(g_l ______________________ i!'.!sL ___________________ _ Name Serial Number Spike Amount Spike Units ----RGF-Hydrotluoric Acid RGF-IMNitric Acid RGF-Hydrochloric Acid RGF-Nitric Acid Strontium-90 SPIKE Thorium-230 SPIKE -----;------rn*---,-*---r_----o 2447606.13 : 5 mL r----.. Z4548Sl.T3*----;---25 **----r--mL ---1 "----*-*-------------*-------_.:._ _______ . Analytical Logbook version .I 11-04-2004 GEL Laboratories LLC Spike Pipet ID: RAD-GFC-4497063 Planchets Flamed: Yes Filename : GAB.XLS File type : Excel Version#: 1.3.10 Batch: 1597811 Analyst: BET01177 Prep Date: 9/1612016 Alpha Method Uncertainty : 0.0928 Beta Method Uncertainty : 0.0628 Geometry: 2 inch Planchelt Sample Characteristics Sample Sample Sample Aliquot Residue Wt. Pos. ID G (mg) 1 405235021.1 0.1090 18.8 2 405235022.1 0.1070 21 3 405235023. 1 0.1170 25.9 4 405235024. 1 0.1110 20.5 5 405235025.1 0.1140 26.6 6 405235026.1 0.1110 24.8 7 405235027.1 0.1060 27.5 B 405235028.1 0.1100 21.1 9 405235029.1 0.1260 27.6 10 405235030. 1 0.1140 26.1 11 405235031.1 0.10BO 25.6 12 405235032.1 0.1210 30 13 405235033.1 0.1130 22.7 14 405235034.1 0.1130 26.7 15 405235035.1 0.1070 21.5 16 405235036.1 0.1140 25.9 17 405235037. 1 0.1250 27.3 1B 405235038.1 0.1210 29.1 19 405235039.1 0.1010 21.5 20 405235040.1 0.1130 26.4 21 1203625435.1 0.1260 0 22 1203625436.1 0.1030 19.5 23 1203625437 .1 0.1060 22.2 24 120362543B.1 0.1060 19.3 25 1203625439.1 0.1260 0 Sample Aliquot S!Oev. G 3.2304E-03 3.2302E-03 3.2312E-03 3.2306E-03 3.2309E-03 3.2306E-03 3.2301E-03 3.2305E-03 3.2322E-03 3.2309E-03 3.2303E-03 3.2317E-03 3.2308E-03 3.230BE-03 3.2302E-03 3.2309E-03 3.2321E-03 3.2317E-03 3.2296E-03 3.2308E-03 3.2322E-03 3.2298E-03 3.2301E-03 3.2301E-03 3.2322E-03 AB1597B11 Gross Alpha/Beta Solid Count Raw Data Sample Detector Date/Time ID 1218/2015 14:17 48 1218/201513:43 3C 121212015 10:40 128 121812015 14:13 9A 1218/2015 13:38 30 1218/201510:15 120 121Bl201510:19 14A 11/2312015 14:50 BO 11/23/201511:10 4A 11/2312015 14:44 90 11/26/2015 14:25 130 1112312015 11:48 14C 11/23/2015 11 :53 70 11123/201511:20 SC 1112312015 11:06 38 11/23/201511:12 SA 11/3012015 11:19 108 11!3012015 10:40 7A 11/30/2015 10:43 12A 11/3012015 13:23 BB 9/1612016 0:00 10A 111231201511:53 4C 11/2312015 11 :53 11A 11123/201511:53 130 9/1612016 0:00 14A Page1 Procedure Code : Parmname1: Parmname2: Required Alpha MDA : Required Beta MDA : Counting GFCGANBS Alpha Bela 4 10 lime Gross Counts (min.) Alpha Beta 160 80 525 170 93 416 160 124 537 140 77 450 110 75 395 120 B9 423 70 -31 219 130 109 B62 130 74 396 120 BB 476 70 38 156 110 57 411 100 62 261 90 66 264 160 86 598 140 76 420 130 54 352 130 81 374 90 42 261 100 54 209 60 6 26 170 124 430 60 314 3099 60 30B 2B14 60 418 3121 pCi/G pCi!G Count Start Date/Time 9/19/201614:36 9/1912016 14:36 9/19/201614:41 9/191201614:37 9/1912016 14:36 911912016 14:41 9/19/2016 14:41 9/19/201614:37 9119/2016 14:36 9/1912016 14:37 9/19/2016 14:41 911912016 14:42 9/1912016 14:37 911912016 14:37 9/19/2016 14:37 9119/2016 14:37 911912016 14:37 9/19/201614:37 911912016 14:42 9/1912016 14:38 9119/2016 14:36 9119/2016 14:36 9/19/2016 16:05 9/19/2016 16:05 9/191201616:05 Pipet, 0.1 ml Stdev : +/. 0.000200 ml Pipe!, 0.5 ml Stdev: +/. 0.001000 ml Pipet, 1 ml Stdev: +/. 0.002000 ml Analytical SOP: GL-RAD-A-0018 SOP: GL-RAD-l-016 Calibration Data Alpha Calibration Calibration Detector Counted Calibration Due Source Efficiency Pos. on Date Dale Used (cpm/dpm) 1 PIC 1211/2015 11/30/2016 Th230 0.1549 2 PIC 1211/2015 11/30/2016 Th230 0.1700 3 PIC 1211/2015 11/30/2016 Th230 0.1572 4 PIC 1211/2015 11/30/2016 Th230 0.1606 5 PIC 1211/2015 11/30/2016 Th230 0.1445 6 PIC 1211/2015 11/30/2016 Th230 0.1575 7 PIC 1211/2015 11/30/2016 Th230 0.1389 8 PIC 1211/2015 11130/2016 Th230 0.1863 9 PIG 1211/2015 11/30/2016 Th230 0.1423 10 PIG 1211/2015 11/30/2016 Th230 0.1597 11 PIG 1211/2015 11/30/2016 Th230 0.1325 12 PIG 12/1/2015 11/30/2016 Th230 0.1389 13 PIG 1211/2015 11/30/2016 Th230 0.1645 14 PIG 1211/2015 11/3012016 Th230 0.1740 15 PIG 1211/2015 11/30/2016 Th230 0.1633 16 PIG 121112015 11/30/2016 Th230 0.1608 17 PIG 121112015 11/30/2016 Th230 0.1294 18 PIG 12/1/2015 11/30/2016 Th230 0.1481 19 PIG 1211/2015 11/30/2016 Th230 0.1644 20 PIG 1211/2015 11/30/2016 Th230 0.1608 21 PIG 1211/2015 11/30/2016 Th230 0.1864 22 PIG 12/112015 11/30/2016 Th230 0.1758 23 PIG 1211/2015 11/30/2016 Th230 0.1636 24 PIG 1211/2015 11/30/2016 Th230 0.1518 25 PIG 1211/2015 11/30/2016 Th230 0.2778 Det. Elf. Error Calibration (cpm/dpm) X-Talk Date 0.00704 0.15170 1211/2015 0.00568 0.05555 1211/2015 0.01035 0.15478 1211/2015 0.00726 0.15338 1211/2015 0.00657 0.07618 1211/2015 0,01863 0.12265 1211/2015 0.02505 0.21109 1211/2015 0.00794 0.06783 1211/2015 0.01036 0.07256 1211/2015 0.02427 0.07768 1211/2015 0.01236 0.26518 1211/2015 0.02173 0.18908 121112015 0.00619 0.10658 12/112015 0.01161 0.06121 12/1/2015 0.00853 0.06080 12/1/2015 0.01473 0.08664 1211/2015 0.00844 0.19500 12/1/2015 0.00525 0.10299 1211/2015 0.01685 0.16665 1211/2015 0.01664 0.09830 1211/2015 0.01461 0.48832 1211/2015 0.01587 0.06433 1211/2015 0.00693 0.11911 12/1/2015 0.01236 0.25792 1211/2015 0.02505 0.15685 1211/2015 AB1597811 Beta Weekly Background Calibration Calibration Detector Del Elf. Count Count Due Source Efficiency Error CPM Start Time Date Used (cprnldpm) (cpm/dpm) X-Talk Alpha Bela Datemme (min.) 11/30/2016 Sr90 0.4877 0.01519 0.00026 0.182 1.560 9/16/2015 17:25 500 11/30/2016 Sr90 0.4751 0.00988 0.00835 0.240 0.556 9/1612016 17:25 500 11/30/2016 Sr90 0.4884 0.01114 0.00040 0.230 0.626 9/161201618:01 500 11/3012016 Sr90 0.4930 0.00758 0.00085 0.188 0.846 9/161201617:58 500 11/30/2016 Sr90 0.4617 0.02297 0.00259 0.112 0.582 9/1612016 17:25 500 11/30/2016 Sr90 0.4884 0.01845 0.00043 0.146 1.342 9/16/201618:01 500 11/30/2016 Sr90 0.4648 0.02119 0.00031 0.043 0.415 9/16/2016 17:23 1000 11/30/2016 Sr90 0.4954 0.00609 0.00243 0.226 0.790 9/16/2016 17:58 500 11/30/2016 Sr90 0.4690 0.01123 0.00431 0.176 0.700 9116/2016 17:25 500 11/30/2016 Sr90 0.4849 0.02610 0.00286 0.160 1.276 9/16/2016 18:18 500 11/30/2016 Sr90 0.4370 0.01144 0.00027 0.040 0.346 9/16/201617:23 1000 11/30/2016 Sr90 0.4653 0.01828 0.00032 0.135 1.297 9116/201617:23 1000 11/30/2016 Sr90 0.4725 0.01113 0.00046 0.140 0.676 9/16/201617:58 500 11/30/2016 Sr90 0.4982 0.00657 0.00367 0.132 0.856 9116/2016 17:25 500 11/30/2016 Sr90 0.4668 0.01614 0.01009 0.198 1.400 9/16/2016 17:25 500 11/3012016 Sr90 0.4869 0.01579 0.00165 0.186 0.818 9/161201617:58 500 11/30/2016 Sr90 0.4619 0.00652 0.00072 0.126 0.594 9/161201618:18 500 11/30/2016 Sr90 0.4817 0.00594 0.00070 0.166 0.792 9/161201618:18 500 11/30/2016 Sr90 0.4827 0.01964 0.00028 0.088 0.888 9/1612016 18:00 500 11/30/2016 Sr90 0.4922 0.02148 0.00053 0.126 0.434 9/161201618:18 500 11/30/2016 Sr90 0.4282 0.00651 0.00016 0.090 0.320 9/16/201617:59 500 11/30/2016 Sr90 0.4810 0.00889 0.00300 0.234 0.738 9/161201617:25 500 11/30/2016 Sr90 0.4847 0.01317 0.00028 0.238 0.862 9/16/2016 18:00 500 11/30/2016 Sr90 0.4392 0.01144 0.00027 0.040 0.346 9/16/201617:23 1000 11/30/2016 Sr90 0.4754 0.02119 0.00031 0.043 0.415 9/16/201617:23 1000 Page2 Noles: 1 -Reference date for Spike Activity (dpm/ml) Is the batch Prep Date Alpha Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pas. pCi/G pCilG pCi/G pCilG pCi/G % 1 2.4064 1.7003 4 3.9008 8.4599 18.82% 2 2.5102 1.7722 4 3.9816 7.0999 20.04% 3 2.4852 1.7546 4 3.9682 13.3115 13.68% 4 2.4413 1.7236 4 3.9886 9.0795 18.37% 5 2.2456 1.5854 4 3.9166 15.3271 14.36% 6 2.3320 1.6464 4 3.9370 15.3096 13.94% 7 1.8275 1.2902 4 3,8915 12.2028 20.35% 8 2.3976 1.6927 4 3.8928 13.1119 13.90% 9 2.4182 1.7073 4 3.9945 9.5514 17.71% 10 2.3436 1.6546* 4 3.9276 13.9020 14.48% 11 1.8136 1.2805 4 3.9100 15.8108 17.85% 12 2.3055 1.6277 4 3.9866 10.2405 18.49% 13 2.3148 1.6342 4 3.9956 11.6049 17.02% 14 2.2210 1.5680 4 3.8998 13.5319 15.56% 15 2.4269 1.7134 4 3.9101 1.1ns 18.32%. 16 2.3616 1.6673 4 3.8613 8.6492 18.54% 17 2.2682 1.6013 4 3.8455 8.0068 20.47% 18 2.3487 1.6582 4 3.8963 11.4361 15.90% 19 2.1469 1.5158 4 3.9357 10.2501 19.67% 20 2.2459 1.5856 4 3.9150 10.2352 18.46% 21 1.8321 1.2935 4 3.5461 0.19()5 429.74% 22 2.4898 1.7578 4 3.9547 12.1380 14.36% 23 4.0335 2.8477 4 6.9940 129.3576 6.70% 24 1.7343 1.2245 4 3.8490 142.2675 6.62% 25 0.8263 0.5834 4 1.8102 88.8797 6.09% A61597B11 Alpha Spike SIN ; Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: Spike Nuclide: Alpha LCS SIN : LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: LCS Nuclide: 2SlGMA Net Count Net Count Counting Rale Rate Error Uncertainty CPM CPM pCilG 0.3180 0.0591 3.0882 0.3071 0.0608 2.9523 0.5450 0.0728 3.4951 0.3620 0.0656 3.2498 0.5698 0.0801 4.2952 0.5957 0.0805 4.0632 0.3999 0.0798 4.7855 0.6125 0.0831 3.5800 0.3932 0.0688 3.3876 0.5733 0.0802 3.8882 0.5029 0.0883 5.4474 0.3832 0.0696 3.6578 0.4800 0.0805 3.8242 0.6013 0.0917 4.1190 0.3395 0.0613 3.0955 0.3569 0.0552 3.1404 0.2894 0.0587 3.2056 0.4571 0.0716 3.5261 0.3787 0.0732 3.8930 0.4140 0.0752 3.6527 0.0100 0.0430 1.6158 0.4954 0.0690 3.3641 4.9953 0.2961 15.0751 5.0933 0.2926 16.0566 6.9237 0.3408 8.5953 Pa9e3 1493-B 6/8/2017 266.08 0.10 Th-230 1493-B 618/2017 266.08 0.10 Th-230 2SIGMA Total Prop. Uncertainty pCilG 3.4891 3.2924 4.3246 3.6905 5.2221 5.0383 5.3615 4.4114 3.8721 4.7800 6.2428 4.1655 4.4213 4.8930 3.5219 3.5649 3.5511 4.1442 4.3790 4.1557 1.6169 4.1310 29.1081 31.8626 19.3819 Sample QC 405235033.1 405235033. 1 405235033.1 Sample Nominal Type RPO RER pCi/G Recovel)' SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP 4.5% MS 113.0716 104.1% MSD 9.5% 113.0716 115.6% LCS 95.1237 93.4%

Notes: 1 -Reference dale for Spike Activity (dpm/ml) is the batch Prep Date Beta Results Decision Critical Required Sample Act. Sample Act. Level Level MOA MOA Cone. Error Pos. pCi/G pCi/G pCi/G pCilG pCilG % 1 2.2400 1.5814 10 3.3217 13.9009 9.53% 2 1.3667 0.9649 10 2.0861 16.4859 7.31% 3 1.3201 0.9320 10 2.0118 20.5785 6.22% 4 1.6670 1.1910 10 2.5564 18.8020 7.28% 5 1.6019 1.1310 10 2.4953 25.3036 7.12% 6 2.2799 1.6096 10 3.4270 17.3834 8.90% 7 1.6967 1.1979 10 2.7877 23.9556 8.66% 8 1.6853 1.1898 10 2.5704 47.8097 4.94% 9 1.4630 1.0329 10 2.2418 17.5703 7.28% 10 2.1804 1.5394 10 3.2825 21.4633 8.00% 11 1.6172 1.1417 10 2.6925 16.5928 10.05% 12 2.1329 1.5058 10 3.2299 18.7347 8.35% 13 1.7705 1.2500 10 2.7531 15.7593 9.10% 14 1.9752 1.3945 10 3.0558 16.2638 9.39% 15 2.2585 1.5945 10 3.3581 20.7877 7.72% 16 1.6351 1.1544 10 2.4826 17.3241 7.68% 17 1.3793 0.9738 10 2.1276 15.8584 7.51% 18 1.5776 1.1138 10 2.4059 15.6159 7.88% 19 2.3228 1.6399 10 3.5879 17.8708 9.90% 20 1.3819 0.9615 10 2.1659 12.9822 9.60% 21 1.5033 1.0613 10 2.5401 0.5385 78.28% 22 1.6156 1.1406 10 2.4417 15.8596 7.85% 23 2.5915 1.8296 10 4.0976 439.8466 3.79% 24 1.7625 1.2443 10 2.9725 437.6097 3.77% 25 1.5002 1.0592 10 2.4943 379.8067 3.79% AB1597811 Beta Spike SIN : Spike Exp Date: Spike Activity (dpmlml): 1243-0 12118/2016 483.48 0.10 Sr-90 Spike Volume Added: Spike Nuclide: Beta LCS SIN; 1243-0 LCS Exp Date : 12118/2016 LCS Activity (dpm/ml): 483.48 LCS Volume Added: 0.10 LCS Nuclide: Sr-90 2SIGMA 2SIGMA Net Count Net Count Counting Total Prop. Rate Rate Error Uncertainty Uncertainty CPM CPM pCi/G pCi!G 1.7213 0.1537 2.5531 3.2631 1.8911 0.1245 2.1625 3.1651 2.7303 0.1491 2.3038 3.7269 2.3683 0.1570 2.5334 3.6739 3.0089 0.1839 3.0839 4.7901 2.1830 0.1791 2.9161 3.8716 2.7136 0.2124 3.8061 5.2029 5.8408 0.2293 3.7152 7.5613 2.3462 0.1576 .2.3545 3.3695 2.6907 0.1887 3.0141 4.3716 1.8826 0.1794 3.3557 4.1741 2.4394 0.1878 2.9451 3.9973 1.9340 0.1657 2.7398 3.5360 2.0773 0.1852 2.9049 3.6795 2.3375 0.1617 2.8592 4.1121 2.1820 0.1519 2.4154 3.4426 2.1137 0.1484 2.2689 3.1640 2.0649 0.1540 2.3325 3.1812 2.0120 0.1844 3.3390 4.2725 1.6560 0.1475 2.3421 3.0157 0.1133 0.0887 1.4508 1.4563 1.7914 0.1279 2.2788 3.2064 50.7880 0.9287 15.9608 64.0212 46.5540 0.8843 16.7696 64.6579 51.6017 0.9313 13.7262 55.7669 Page4 Sample Sample Nominal QC Type RPO RER pCilG Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235033.1 OUP 0.6% 405235033.1 MS 410.9168 103.2% 405235033.1 MSO 0.5% 410.9168 102.7% LCS 345.6919 109.9% '"C Pl (Jq (1) 1597811 .j:>. "" "" ,._. 0 SamplelD Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID ......., VI 405235021 4B 160 80 525 9/19/2016 14:36 9/19/201617:16 PIC 1597811 00 0 405235022 3C 170 93 416 9/19/2016 14:36 9/19/2016 17:26 PIC 1597811 "" 405235023 12B 160 124 537 9/19/2016 14:41 9/19/2016 17:21 PIC 1597811 405235024 9A 140 77 450 9/19/2016 14:37 9/19/2016 16:57 PIC 1597811 405235025 3D 110 75 395 9/19/2016 14:36 9/19/2016 16:26 PIC 1597811 405235026 12D 120 89 423 9/19/2016 14:41 9/19/2016 16:41 PIC 1597811 405235027 14A 70 31 219 9/19/2016 14:41 9/19/2016 15:51 PIC 1597811 405235028 8D 130 109 862 9/19/2016 14:37 9/19/2016 16:47 PIC 1597811 405235029 4A 130 74 396 9/19/2016 14:36 9/19/2016 16:46 PIC 1597811 405235030 9D 120 88 476 9/19/2016 14:37 9/19/2016 16:37 PIC 1597811 405235031 13D 70 38 156 9/19/2016 14:41 9/19/2016 15:51 PIC 1597811 405235032 14C 110 57 411 9/19/2016 14:42 9/19/2016 16:32 PIC 1597811 405235033 7D 100 62 261 9/19/2016 14:37 9/19/2016 16:17 PIC 1597811 405235034 SC 90 66 264 9/19/2016 14:37 9/19/2016 16:07 PIC 1597811 405235035 3B 160 86 598 9/19/2016 14:37 9/19/2016 17:17 PIC 1597811 405235036 8A 140 76 420 9/19/2016 14:37 9/19/2016 16:57 PIC 1597811 405235037 108 130 54 352 9/19/2016 14:37 9/19/2016 16:47 PIC 1597811 405235038 7A 130 81 374 9/19/2016 14:37 9/19/201616:4 7 PIC 1597811 405235039 12A 90 42 261 9/19/2016 14:42 9/19/2016 16:12 PIC 1597811 405235040 88 100 54 209 9/19/2016 14:38 9/19/2016 16:18 PIC 1597811 1203625435 10A 60 6 26 9/19/2016 14:36 9/19/2016 15:36 PIC 1597811 1203625436 4C 170 124 430 9/19/2016 14:36 9/19/2016 17:26 PIC 1597811 1203625437 11A 60 314 3099 9/19/2016 16:05 9/19/2016 17:05 PIC 1597811 1203625438 13D 60 308 2814 9/19/2016 16:05 9/19/201617:05 PIC 1597811 1203625439 14A 60 418 3121 9/19/2016 16:05 9/19/2016 17:05 PIC 1597811 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 2010 19-Sep-2016 _ Product: ___ S_r ____ _ Criteria: -Yes No Comments Samele Solids are less than or eaual to 100 ma for GAB. \\/A Samples have been blank corrected (If required). rJf.1. Blank correction reeorted Included Cit reaulred\, lf activity less than 1ox MDA/MDC, error Is less than or eciual to 150% of sample actlvltv. I lf greater than 10* MDA/ MDC, error Is 400/o or less. IIf bolnw *ho Mn A/ Mnr orrn* I<: Instrument source check ls within limits. / Instrument bko cherk 1 .. within limit<:. Method RDL/ LLD has been met. / If duellcate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, / If greater 5* MOA/ MOC, then RPO 20% or less, If below the MDA/ MOC, the RPO Is 0%, Or meets the client's reouired RER acceotance criteria. Tracer yield Is 15*125%

  • Carrier yield 25*125%. / (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. .. (If < 50/n nf lnwoc* Samele was run within hold time. 'JI'"'_;::: ./ t>t:TZ. 'IJ(po:x'JS Samele was correctlv oreserved If reauired. / Smears Taken for Radioactive batches. / Method Spike and LCS are within 75-125% / if or moo>c th1> cllan*'<: criteria\. No blank spaces on data forms. / All line outs Initialed and dated. INn o .. n.a Aux data is correct. Client Saeclal reauirements oaae has been checked. / Raw Data and/ or snectrum are Included and orooerlv statused. / MS, LCS, and Duplicate RPO/RER values uploaded to UMS and / "oc Vf>rifif>rl Hit -.n Clf tJ\ !:!attb !mtemd latll / Batch Data Excentlon Renorts IOER\ comoleted. If aoolicable. / D trl l'Jl/ro:::, Batch Data Exception Reports (DER) second reviewed. / t' Olsoositlon verified to be comnleted. Allauot Correction comale*"" If reoulred M Review sample historical results if available / Cif REMP, results above MOC have been verified bv historical results. recount or re-analvsls. \ Primary Review Performed Secondary Review Performed By: ___ ti_i_,,kp};;___,,"'---'--'f'-'-)_1)--'!t'--(t ________ _ Page 4992 of 5809 GL-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER . DAT A EXCEPTION REPORT .. Mo.Day Yr. Division: Quality Criteria: 21-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GFPC EPA 905.0 Modified/DOE RP501 Solid -. Batch ID: Sample Numbers: 1597796 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample Analyzed out of Holding Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, and 12036254402 were received and analyzed out of. holding. Originator's Name: Data Validator/Group Leader: Nat Long 21-SEP-16 Kenshalla Oston 21-SEP-16 Page 1 Page 4993 of 5809 DE.R Report No.: 1560005 Revision No.: 2 Type: Process Client Code: MJWC Prep Logbook The Determination of Strontium 89/90 in Water, Soil, Milk, Filters, Vegetation and Tissues Batch ID: Analyst: Method: Lab.SOP: 1597796 Kelli Dorrell EPA 905.0 Modified/DOE RP501 Rev. 1 Modified GL-RAD-A-004 REV# 17 Instrument: BAL-16107662 Sample Id Description LCS 1203625403 Strontium-90 SPlKE Sample ID Prep Date Dry or Wet Unadjusted Aliquot Initial Wt Final Wt Net Wt 405235021 16-SEP-2016 10:48 D 405235022 16-SEP-2016 10:48 D 405235023 !6-SEP-201610:48 D 405235024 !6-SEP-2016 10:48 D 405235025 16-SEP-2016 10:48 D 405235026 l 6-SEP-2016 I 0:48 D 405235027 16-SEP-2016 10:48 D 405235028 l 6-SEP-2016 10:48 D 405235029 16-SEP-2016 10:48 D 405235030 16-SEP-2016 10:48 D 405235031 16-SEP-2016 10:48 D 405235032 !6-SEP-2016 10:48 D 405235033 16-SEP-2016 10:48 D 405235034 16-SEP-2016 10:48 D 405235035 I 6-SEP-2016 I 0:48 D 405235036 16-SEP-2016 10:48 D 405235037 16-SEP-2016 10:48 D 405235038 16-SEP-2016 10:48 D 405235039 ! 6-SEP-2016 10:48 D 405235040 ! 6-SEP-2016 10:48 D 1203625401 MB 16-SEP-2016 10:48 D 1203625402 DUP (405235025) ! 6-SEP-2016 10:48 D 1203625403 LCS 16-SEP-2016 10:48 D Reagent/Solvent Lot ID Description 2064611.2 Phenolphlhaleir., 1.0% in 50% Alcohol 2213530 O.OSM HN03 2243751 RGF-6M Sodium Hydroxide 2243757 RGF-0.75M Sodium Carbonate 2334614 Thymol Blue Indicator 2388714 RGF-80% Ethanol 21'3137 SrOSmL S.;.>mg, fmb-16 7mg 2414995 Sr0.5mL=7.37, 2.0 mL=29.46 mg 2424020 RGF-3M Nitric/O.OSM Oxalic 2433863.1 SR SPEC RESIN Cleaned 2434028 RGF-Sr Filters 2434079 RGF-8M Nitric Acid Analytical Logbook version 11 J-04-2002 Aliquot (g) 0.321 0.461 0.397 0.324 0.318 0.418 0.321 0.354 0.328 0.332 0.38 0.391 0.301 0.437 0.351 0.472 0.328 0.398 0.332 0.321 0.31 Amount 2mL 15mL 6mL 13mL .5mL 3mL S-m!::-1':P> /u /., .5mL lOmL 2g 1 L 25mL (g) (g) 0.321 0.0236 0.461 0.023 0.397 0.0231 0.324 0.0228 0.318 0.0233 0.418 0.0231 0.321 0.0242 0.354 0.0228 0.328 0.0234 0.332 0.0227 0.38 0.0229 0.391 0.0227 0.301 0.0238 0.437 0.0232 0.351 0.0231 0.472 0.0239 0.328 0.0234 0.398 0.0245 0.332 0.0239 0.321 0.0234 0.472 0.0242 0.31 0.0228 0.472 0.0226 Comments: Spike Pipe! ID: RAD-GFC-1795419 Carrier Pipet ID: RAD-GFC-2 I 54115 (g) (mg) 0.0301 6.5 0.0298 6.8 0.0303 7.2 0.0298 7 0.0309 7.6 0.0303 7.2 0.0316 7.4 0.0293 6.5 0.0303 6.9 0.0301 7.4 0.0299 7 0.0308 8.1 0.0308 7 0.03 6.8 0.0314 8.3 0.03 6.1 0.0306 7.2 0.0313 6.8 0.0307 6.8 0.0301 6.7 0.0314 7.2 0.0297 6.9 0.0295 6.9 Data Entry Date2: 16-SEP-201615:!0 GFC-F30560 Kelli Dorrell Data Entry Date3: 16-SEP-2016 00:00 L-* Serial NumJ?er 1243-0 Sr Separation (date) 09/16/16 15:10 09116116 15:10 0911611615:10 09116116 15: 10 09116116 15:10 09116116 15:10 09116116 15:!0 09/16/16 15;!0 09116116 15:10 09/16/1615:10 09116116 15:!0 09116116 15:!0 09/16/16 15:10 09/16/1615:10 09/16/16 15:10 09116116 15:10 09/16/1615:10 09/16116 15:10 09/16/16 15:10 09116116 15:!0 09/16116 15:10 09116116 15:10 09/16/1615:10 Spike Amount Spike Qnits_ .I mL Strontium Carrier Yield (percent) 88 92 98 95 103 98 100 88 94 100 95 110 95 92 113 83 98 92 92 91 98 94 94 GEL Laboratories LLC Sample ID Prep Date Reagent/Solvent Lot ID Description Analytical Logbook version I 11-04-2002 Dry or Wet Unadjusted Aliquot (g) Amount Prep Logbook Aliquot (g) Comments: Initial Wt (g) Final Wt (g) Net Wt (mg) Sr Separation (date) Strontium Carrier Yield (percent) GEL Laboratories LLC Filename : SR90.XLS File type : Excel Version # : 1.3.1 O Batch : 1597796 Analyst: KEL01237 Prep Date : 9/16/2016 Method Uncertainty : 0.089724205 Geometry: Tuffryn Filter Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Pos. ID G G 1 405235021.1 0.3210 3.2525E-03 2 405235022.1 0.4610 3.2672E-03 3 405235023.1 0.3970 3.2605E-03 4 405235024.1 0.3240 32529E-03 5 405235025.1 0.3180 3.2522E-03 6 405235026.1 0.4180 3.2627E-03 7 405235027.1 0.3210 3.2525E-03 8 405235028.1 0.3540 3.2560E-03 9 405235029.1 0.3280 3.2533E-03 10 405235030. 1 0.3320 3.2537E-03 11 405235031.1 0.3800 3.2587E-03 12 405235032.1 0.3910 3.2599E-03 13 405235033.1 0.3010 3.2505E-03 14 405235034.1 0.4370 3.2647E-03 15 405235035.1 0.3510 3.2557E-03 16 405235036.1 0.4720 3.2683E-03 17 405235037.1 0.3280 3.2533E-03 18 405235038.1 0.3980 3.2606E-03 19 405235039.1 0.3320 3.2537E-03 20 405235040.1 0.3210 3.2525E-03 21 1203625401.1 0.4720 3.2683E-03 22 1203625402.1 0.3100 3.2514E-03 23 1203625403.1 0.4720 3.2683E-03 51597796r.xls Strontium-90 Solid Carrier SIN : Carrier Exp Date : Carrier Volume Added: Carrier Weight (mgfml): Carrier Weight Stoev.: Sample Date/Time 12/8/2015 14;17 12/8/2015 13:43 12/212015 10:40 12/8/2015 14:13 12/8/2015 13:38 12/8/2015 10:15 12/8/2015 10:19 11/23/2015 14:50 11/23/201511:10 11/231201514:44 11/26/2015 14:25 11/2312015 11 :48 11/23/2015 11 :53 11/23/201511:20 11/2312015 11 :06 11123/2015 11 :12 11/30/201511:19 11/30/2015 10:40 11/30/2015 10:43 11/30/2015 13:23 9/1612016 0:00 121812015 13:38 9/1612016 0:00 2414995 .6/3/2017 0.50 14.73 0.10 Carrier Calculations Carrier Weight(mg) (Standard) 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 Page 1 Procedure Code : GFC90SRS Parmname: Strontium-90 Required MCA : 2 pCi/G Sr-90 Abundance : 1.00 Halflife of Sr-90 : 28.90 years Halflife of Y-90 : 64.053 hours Net Net Carrier Carrier Weight(mg) Weight Aliquot Aliquot (Sample) S!Dev. (mg) (ml) StDev:..(mL) 6.50 0.035267 0.5 0.001000 6.80 0.036556 0.5 0.001000 7.20 0.038276 0.5 0.001000 7.00 0.037416 0.5 0.001000 7.60 0.039995 0.5 0.001000 7.20 0.038276 0.5 0.001000 7.40 0.039135 0.5 0.001000 6.50 0.035267 0.5 0.001000 6.90 0.036986 0.5 0.001000 7.40 0.039135 0.5 0.001000 7.00 0.037416 0.5 0.001000 8.10 0.042144 0.5 0.001000 7.00 0.037416 0.5 0.001000 6.80 0.036556 0.5 0.001000 8.30 0.043003 0.5 0.001000 6.10 0.033548 0.5 0.001000 7.20 0.038276 0.5 0.001000 6.80 0.036556 0.5 0.001000 6.80 0.036556 0.5 0.001000 6.70 0.036127 0.5 0.001000 7.20 0.038276 0.5 0.001000 6.90 0.036986 0.5 0.001000 6.90 0.036986 0.5 0.001000 Pipet, 0.1 ml Stdev: Pipe!, 0.5 ml Stdev : Pipe!, 1 ml Stdev : +/-Analytical SOP: GL-RAD-A-004 Instrument SOP: GL-RAD-1-016 0.000200 0.001000 0.002000 Count Raw Data Counting Detector Time Gross Counts Gross Beta Pos. ID (min.) Alpha Beta CPM 1 S8 60 29 39 0.630 2 SC 60 s 42 0.696 3 SD 60 11 34 O.S58 4 2A 60 11 36 O.S76 s SA 60 10 87 1.441 6 SC 60 3 41 0.681 7 7A 60 4 46 0.761 8 78 60 8 36 0.593 9 7C 60 9 31 0.499 10 7D 60 5 35 o.5n 11 SA 60 8 50 0.825 12 88 60 4 18 0.295 13 50 60 0 34 0.567 14 SD 60 12 50 0.823 15 9A 60 6 38 0.620 16 98 60 3 21 0.347 17 9C 60 5 32 0.528 18 9D 60 5 56 0.928 19 108 60 7 43 0.696 20 10C 60 1 14 0.229 21 100 60 5 33 0.514 22 11A 60 11 54 0.880 23 118 60 4 1582 26.362 S1597796r.xls ml ml ml Count Start Date/Time 9/17/20161S:34 9/1712016 15:34 9/17/2016 1S:34 9/21/201610:46 9/19/2016 11 :54 9/17/2016 1S:33 9/17/201615:33 9/17/201615:33 91171201615:33 9/17/201615:33 9/1712016 15:33 9/17/2016 15:34 9/19/201615:23 9/17/2016 15:34 9/17/201615:36 9/171201615:36 9/1712016 15:36 9/17/2016 15:37 9/1712016 1S:37 9/17/201615:37 9/17/2016 1S:37 9/17/2016 15:45 9/17/2016 15:45 Page2 Strontium Separation Date/Time 9/16/2016 1S:10 9/16/20161S:10 9/16/2016 15:10 9/16/2016 1S:10 9/16/2016 1S:10 9/1612016 15:10 9/16/2016 15:10 9/161201615:10 9116/2016 15:10 9/16/20161S:10 9/16/20161S:10 9/16/2016 15:10 9/1612016 1S:10 9116/201615:10 9/161201615:10 9/16/201615:10 9/1612016 15:10 9/16/2016 15:10 9/16/2016 15:10 9/161201615:10 9/161201615:10 9/161201615:10 9/16/2016 15:10 Yttrium Ingrowth 0.236 0236 0.236 0.715 0.527 0.236 0.236 0.236 0.236 0.236 0.236 0.236 0.545 0.236 0.237 0.237 0.237 0.237 0.237 0.237 0237 0.238 0238 Calculated Sample Sample Sr-90 Recovery Recovery Decay % Error% 0.982 88.3% 1.04% 0.982 92.3% 1.04% 0.981 97.8% 1.03% 0.981 95.0% 1.04% 0.981 103% 1.03% 0.982 97.8% 1.03% 0.982 100% 1.03% 0.981 88.3% 1.04% 0.981 93.7% 1.04% 0.981 100% 1.03% 0.981 95.0% 1.04% 0.981 110% 1.02% 0.980 9S.0% 1.04% 0.981 92.3% 1.04% 0.981 113% 1.02% 0.981 82.8% 1.05% 0.981 97.8% 1.03% 0.981 92.3% 1.04% 0.981 92.3% 1.04% 0.981 91.0% 1.04% 1.000 97.8% 1.03% 0.982 93.7% 1.04% 1.000 93.7% 1.04%

S1597796r.xls Calibration Data Detector Weekly Bkg WeeklyBkg Calibration Detector Efficiency Count Count Counted Calibration Due Efficiency (cpm/dpm) Error Alpha WeeklyBkg Start Time Pos. on Date Date Sr-90 Y-90 (cpm/dpm) X-Talk CPM Date/Time (min.) 1 PIC 4/1/2016 2/28/2017 0.4309 0.5665 0.00426 0.04169 0.532 9/16/2016 17:25 500 2 PJC 4/1/2016 2/28/2017 0.4203 0.5622 0.00657 0.04334 0.856 9/16/201617:25 500 3 PIC 411/2016 2128/2017 0.4250 0.5641 0.00925 0.04641 0.748 9/161201617:26 500 4 PIC 4/1/2016 2/2812017 0.4136 0.5406 0.01914 0.13349 0.450 9/16/201617:24 500 5 PIC 4/1/2016 2128/2017 0.4320 0.5685 0.00851 0.05241 1.386 9/1612016 17:25 500 6 PJC 4/1/2016 2128/2017 0.4223 0.5617 0.01970 0.04646 0.978 9/16/2016 17:58 500 7 PIC 4/1/2016 212812017 0.4198 0.5546 0.00594 0.07945 0.792 9/16/2016 18:18 500 8 PIC 4/1/2016 2128/2017 0.4308 0.5632 0.00627 0.05267 0.466 9/16/2016 17:58 500 9 PIC 4/1/2016 2128/2017 0.4148 0.5415 0.00790 0.11724 0.398 9/16/201617:58 500 10 PJC 4/1/2016 2/2812017 0.4129 0.5455 0.01113 0.08122 0.676 9/16/201617:58 500 11 PIG 411/2016 212812017 0.4121 0.5573 0.01579 0.06471 0.818 9/16/201617:58 500 12 PIG 4/112016 212812017 0.4278 0.5567 0.02148 0.07827 0.434 9/16/201618:18 500 13 PIG 4/1/2016 2128/2017 0.4251 0.5641 0.00925 0.04602 0.748 9/16/2016 17:26 500 14 PIG 4/1/2016 2128/2017 0.4258 0.5674 0.00609 0.05209 0.790 9/16/201617:58 500 15 PIC 4/1/2016 2128/2017 0.4231 0.5591 0.00758 0.13006 0.846 9/16/2016 17:58 500 16 PJC 4/1/2016 2/28/2017 0.4210 0.5570 0.00754 0.05873 0.422 9/16/2016 17:59 500 17 PIG 4/1/2016 2/28/2017 0.4142 0.5526 0.00584 0.06923 0.690 9/16/2016 17:59 500 18 PIC 4/1/2016 2128/2017 0.4213 0.5596 0.02610 0.05933 1.276 9/16/2016 18:18 500 19 PIC 4/1/2016 2128/2017 0.4095 0.5325 0.00652 0.17388 0.594 9/16/201618:18 500 20 PJC 4/1/2016 2/2812017 0.4062 0.5237 0.00638 024092 0.340 9/16/2016 17:59 500 21 PIC 4/1/2016 2/28/2017 0.4053 0.5164 0.00557 0.42763 0.524 9/16/201617:59 500 22 PIG 4/1/2016 2128/2017 0.4242 0.5473 0.01317 0.10799 0.862 9/16/2016 18:00 500 23 PIC 4/1/2016 2/28/2017 0.4317 0.5589 0.00697 0.07187 0.950 9/161201618:00 500 Page3 Notes: 1 -Resutts are decay corrected to Sample Datemme 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample DatefTime * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 0.6661 0.4703 2 1.0840 0.2807 109.90% 2 0.5742 0.4054 2 0.9082 -0.3112 72.32% 3 0.5834 0.4119 2 0.9297 -0.4023 54.76% 4 0.3978 0.2808 2 0.6548 0.2338 81.64% 5 0.7163 0.5057 2 1.1070 0.1056 296.19% 6 0.6372 0.4499 2 1.0009 -0.6011 38.91% 7 0.7319 0.5167 2 1.1626 -0.0791 390.05% 8 0.5667 0.4001 2 0.9307 0.3312 81.91% 9 0.5532 0.3906 2 0.9189 0.2784 94.46% 10 0.6653 0.4697 2 1.0665 -0.2528 105.31% 11 0.6734 0.4754 2 1.0678 0.0157 1849.54% 12 0.4006 0.2828 2 0.6611 -0.2659 54.67% 13 0.6037 0.4262 2 0.9621 -0.3976 57.71% 14 0.5754 0.4063 2 0.9142 0.0669 375.74% 15 0.6123 .0.4323 2 0.9691 -0.4719 48.63% 16 0.4396 0.3104 2 0.7270 -0.1593 108.66% 17 0.6949 0.4906 2 1.1126 -0.4269 62.11% 18 0.8115 0.5729 2 1.2586 -0.7844 38.73% 19 0.6863 0.4845 2 1.1089 0.2864 110.49% 20 0.5506 0.3887 2 0.9257 -0.3283 60.64% 21 0.4265 0.3011 2 0.6948 -0.0178 1017.93% 22 0.8425 0.5948 2 1.3322 0.0519 703.45% 23 0.5599 0.3953 2 0.8807 45.8521 2.98% S159n95r.xls Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): NIA NIA NIA NIA Spike Volume Added: LCS SIN: 1243-0 LCS Exp Date: 12/1812016 LCS Activity (dpm/ml): 483.48 LCS Volume Added: 0.10 2SIGMA 2SIGMA Net Count Net Count Counting Total Prop. Rate Rate Error Uncertainty Uncertainty CPM CPM pCi/G pCi/G 0.0979 0.1075 0.6046 0.6067 -0.1596 0.1154 0.4410 0.4410 -0.1898 0.1039 0.4316 0.4316 0.1255 0.1024 0.3740 0.3765 0.0553 0.1637 0.6132 0.6135 -0.2970 0.1154 0.4576 0.4576 -0.0306 0.1195 0.6050 0.6050 0.1270 0.1040 0.5316 0.5349 0.1011 0.0955 0.5154 0.5179 -0.0994 0.1047 0.5216 0.5217 0.0067 0.1240 0.5685 0.5686 -0.1392 0.0760 0.2846 0.2847 -0.1813 0.1046 0.4495 0.4496 0.0329 0.1237 0.4930 0.4931 -0.2257 0.1097 0.4495 0.4496 -0.0749 0.0814 0.3392 0.3393 -0.1624 0.1009 0.5195 0.5195 -0.3476 0.1343 0.5938 0.5939 0.1024 0.1131 0.6201 0.6222 -0.1107 0.0671 0.3901 0.3902 -0.0096 0.0981 0.3558 0.3559 0.0182 0.1280 0.7154 0.7154 25.4119 0.6643 2.3492 8.5194 Page 4 Sample Sample Nominal QC Type RPD RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE .. SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235025.1 DUP

  • 0.0% LCS 46.1411 99.4%

'"t:1 ll) (1q ('l) Vl 0 0 1597796r .xis 0 0 ......, Vl 00 Sample ID Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID 0 \0 405235021 58 60 29 39 9/17 /2016 15:34 9/17 /2016 16:34 PIC 1597796 405235022 5C 60 5 42 9/17/2016 15:34 9/17 /2016 16:34 PIC 1597796 405235023 5*0 . 60 11 34 9/17 /2016 15:34 9/17 /2016 16:34 PIC 1597796 405235024 2A 60 11 36 9/21 /2016 10:46 9/21/2016 11 :46 PIC 1597796 405235025 5A 60 10 87 9/19/2016 11 :54 9/19/2016 12:54 PIG 1597796 405235026 SC 60 3 41 9/17 /2016 15:33 9/17 /2016 16:33 PIC 1597796 405235027 7A 60 4 46 9/17/2016 15:33 9/17 /2016 16:33 PIC 1597796 405235028 78 60 8 36 9/17 /2016 15:33 9/17 /2016 16:33 PIC 1597796 405235029 7C 60 9 31 9/17 /2016 15:33 9/17 /2016 16:33 PIG 1597796 405235030 70 60 5 35 9/17/201615:33 9/17 /2016 16:33 PIC 1597796 405235031 8A 60 8 50 9/17/2016 15:33 9/17 /2016 16:33 PIC 1597796 405235032 88 60 4 18 9/17/2016 15:34 9/17 /2016 16:34 PIC 1597796 405235033 50 60 0 34 9/19/2016 15:23 9/19/2016 16:23 PIG 1597796 405235034 80 60 12 50 9/17 /2016 15:34 9/17 /2016 16:34 PIG 1597796 405235035 9A 60 6 38 9/17/2016 15:36 9/17 /2016 16:36 PIG 1597796 405235036 98 60 3 21 9/17/201615:36 9/17 /2016 16:36 PIG 1597796 405235037 9G 60 5 32 9/17/201615:36 9/17 /2016 16:36 PIG 1597796 405235038 90 60 5 56 9/17/201615:37 9/17 /2016 16:37 PIG *1597796 405235039 108 60 7 43 9/17 /2016 15:37 9/17 /2016 16:37 PIG 1597796 405235040 10C 60 1 14 9/17 /2016 15:37 9/17 /2016 16:37 PIG 1597796 1203625401 100 60 5 33 9/17/2016 15:37 9/17/2016 16:37 PIG 1597796 1203625402 11A 60 11 54 9/17/2016 15:45 9/17/201616:45 PIC 1597796 1203625403 118 60 4 1582 9/17/2016 15:45 9/17/201616:45 PIG 1597796 Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 Batch#_\ Product: __ (A"'"'--'A...:....;G=----. Criteria: Yes No Comments Sample Solids are less than or eaual to 100 ma for GAB. / Samples have been blank corrected (If required). l\lt\ Blank correction reoorted Included Cif reaulred). If activity less than lOx MDA/MDC, error Is less than or eaual ta 1500/o of sample activity. I If greater than 10* MDA/ MDC, error is 400/o or Jess. If hPl-** .. h-MDA/ Mnr 1" ** Instrument source check is within limits. / Instrument bkn ch,,ck within limits. Method RDL/ LLD has been met. / If duplJcate activities are: / Less than 5* MDA/ MDC, then RPD Is 1000/o or less, If greater 5* MDA/ MDC, then RPD 200/o or less, If below the MDA/ MDC, the RPO is 0%, Or meets the client's reoulred RER acceotance criteria. Tracer yield is 15*12SO/o. Carrier yield 25-125%. {Or meets the client's contract acceptance criteria). tJA Method blank Is less than the RDL/ LLD. / (If < <;O/n nf ln..,ftc* ""tivltv\ Samole was run within hold time. / DW. Samale was correctlv oreserved If reoulred. / Smears Taken for Radioactive batches. / Method Spike and LCS are within 75-1250/o / i( or meets the client's "Ontract arrftnbnce crlt,.rl:il \. No blank spaces on data forms. / All line outs Initialed and dated. l.,n Prrnro; Aux data Is correct. Ni\ Client Soecial reaulrements oaae has been checked. / Raw Data and I or snectrum are Included and nroaerlv statused. ,,./ MS, LCS, and Duplicate RPD/RER values uploaded to UMS and / v"riflRd l*Ht -(If on*nrft,f ln*n ** / Batch Data Exceatlon Renorts IDER\ comoleted If aaallcable * [)£:"{[. Batch Data Exception Reports (DER) second reviewed. ./ Dlsoosltlon verified to be comoleted. All""n* C'.orre.,tlnn comnleted If renulred. N:P. Review sample historical results If available I (If REMP, results above MDC have been verified bv historical results recount or re-analvsis.) Primary Review Performed By:. ___ ----Secondary Review Performed . ...L..i.<._::. ______ _ Page 5001 of 5809 l S\.:iq l$<,p'leH11S \o"lL GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER

  • DATA EXCEPTION REPORT
  • Mo.Day Yr. Division: Quality Criteria: 29-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GFPC EPA 900.0/SW846 9310/SM 71108 Solid *-Batch ID: Sample Numbers: 1602427 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059,and 405235060 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Nat Long 29-SEP-16 Amanda Fehr 30-SEP-16 Page 1 Page 5002 of 5809 DER Report No.: 1562965 Revision No.: Type: Process Client Code: MJWC Logbook The Determination of Gross Alpha And Gross Non-Volatile Beta in Soil, Filters, Solid Matrices AndI>irect Count Air Filters Batch ID: 1602427 Due Dates for Lab: 01-0CT-2016 Hold: 28-MAY-2016 Package: 02-0CT-2016 SDG: 04-0CT-2016 Analyst: Jasmine Conley Lab SOP: GL-RAD-A-OOIB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B Modified Instrument: BAL-18550299 Sample ID 405235042 . 2 405235043. 2 405235044
  • 2 405235045 -2 405235046 -2 405235047
  • 2 405235048 -2 405235049-2 405235050. 2 405235051 -2 405235052 -2 405235053 -2 405235054 -2 405235055 -2 405235056 -2 405235057 -2 405235058
  • 2 405235059 -2 405235060 -2 Dry or \Vet Intermediate Unadjusted Aliquot Initial 'Vcight Final Weight Residue Aliquot Aliquot (g) (g) (g) Weight De1ector Run Do.re # (e) me) F7-SEP-20l6 13:42 D 0.1 0.1 i 7.5877 i 7.6136 I 25.9 4 *.'1 .. 1-sEP-201613:42 2 11. o 0.103 1 1.6121 r-7:697, 24.9 u i-.--,* l i 1 I I -\ V , ... f1_.s_E_P_-2_0_16_1_3_:4-_2_--_ __ i i f?*SEP-201613:42 I 4 ! D I 0.101 i 7.6407 I 7.666 l 25.3 ! 5A ! 0.1 7.5693 i 7.5918 22.5 l f"iL_ ! [!7-SEP-201613:42 tJ D 0.103 7.6156 7.6402 24.6 I iA -1 r-SEP-2016 13:42 J 7 1 D 7.6091 7.6314
  • 22.3 i.:!B 1 !27-SEP-201613:42-M-' 8 i D 0.1 1:6918 7.7182 26.4 I '2.; ! : I 13:42 --9 i D 0.101 7.5532 I 7.5785 25.3 ! z i l 13:42 \IO i D 0 lOf' 7.6336 r 7.6592 "5 6 \f:I tl7-SEP-201613:42 ti i D 7.6061 ;5:5 jt)J ?7-SEP-2016 13:42 ! 12 ! D 0.106 7.6758 7.7036 27.8 ID l 113 i D 0.104 l 7.5005 7.53 29.5 1 <")j; _, !27-SEP-201613:42 I W. D 0.101 *--=7=-_4"'9"'"72=---:--7=-_""'52""2""3--; 05 I i : _____j ' -. '.__!_3.fL_j L,__ ____ ; f7-SEP-2016 13:42 15: I ! D I 0.101 27-SEP-2016 13:42 16! D l l 0.105 ' I i I 27-SEP-2016 13:42 17 l D I i 0.112 I l ! I I [!7-SEP-2016 13:42 18\ D i I 0.103 ! ! I F7-SEP-2016 13:42 19! D I I 0.101 ! : ! 0.101 I 7.6349 ' 0.105 I 7.5495 0.112 l 7.615 0.103 ! 7.5762 l 0.101 I 7.5688 I i 7.6627 I 7.5802 I I l 7.6464 I 7.6031 i I 7.5895 ' I I I I j ! 27.8 30.7 31.4 26.9 20.7 l iG i ! CA 1 _l__j.Q_J ! 5_c._J F7-SEP-201613:42 I 20 i D ! 0.101 I 0.101 7.6782 7.7022 24 5D....:J 1203636653 MB F1-sEP-2016 13:42 ... I 1203636654-2DUP(405235045)(-7-SEP-201613:42 r::2i D I 0.100 i 0.106 . 7.6622 ! 7.6881 25.9 5"§1 1203636655-2MS(405235045) 23j D 0.104 0.10417.6065 I 7.633 I 26.5 i Kb> \5C o4; D 0.1 0.1 7.6671 I 7.6909 i 23.8 ( Jke°' I SD 12036366S7Lcs fl1-s"EP-201613:42 ,.! 0.112 1 0112-t 7.647 '7.6474 t--o.4/ to$ ! ....L;:tr-;;L-*'-1 ----'----'-----'-------__, *-----------------Anal)1ical Logbook version 1 11-04-2004 GEL Laboratories LLC Logbook The Determination of Gross Alpha And Gross Non-Volatile Beta in Soil, Filters, Solid Matrices And Count Air Filters Batch ID: 1602427 Analyst: Jasmine Conley Instrument: BAL-18550299 Sample ID Run Date Type Name RGNT RGF-IM Nitric Acid RGNT RGF-Hydrofluoric Acid RGNT RGF-Hydrochloric Acid RGNT RGF-Nitric Acid SPIKE Strontium-90 SPIKE SPIKE Thorium-230 SPIKE Lab SOP: GL-RAD-A-OOlB REV# 17 Method: EPA 900.0/SW846 9310/SM 7110B Modified # Diy or Wet Intermediate Unadjustc-d Aliquot Initial Weight Final Weight Residue Detccmr Aliquot Aliquot (g) (g) (g) Weight ) (ml Serial Number Spike Amount Spike Units 2438701 *-r 5 mL ! ' 2445660.8 I IO mL --j f-2454811.6 I 5 i mL ! /---w131s.1s 2s-!--mr::--1 ! 1243-0 .I j mL ! 1493-B .I mL c_ __________ ___J _____ --'---Spike Pipet ID: RAD-GFC-4497063 Planchets Flamed: Yes Analytical version l 11*04*2004 GEL Laboratories LLC Filename GAB.XLS File type Excel Version # 1.3.1 0 Batch : 1602427 Analyst: JAS02031 Prep Date : 912712016 Alpha Method Uncertainty : 0.0928 Beta Method Uncertainty : 0.0628 Geometry: 2 inch Planchett Sample Chamcteristlcs Sample Sample Sample Aliquot Residue WI. Pos. ID G (mg) 1 4052350412 0.1000 25.9 2 405235042.2 0.1030 24.9 3 405235043.2 0.1030 31.3 4 405235044.2 0.1010 25.3 5 405235045.2 0.1000 22.5 6 405235046.2 0.1030 24.6 7 4052350472 0.1030 22.3 8 4052350482 0.1000 26.4 9 405235049.2 0.1010 25.3 10 4052350502 0.1010 25.6 11 405235051.2 0.1010 25.5 12 4052350522 0.1060 27.8 13 4052350532 0.1040 29.5 14 405235054.2 0.1010 25.1 15 405235055.2 0.1010 27.8 16 405235056.2 0.1050 30.7 17 405235057.2 0.1120 31.4 18 405235058.2 0.1030 26.9 19 405235059.2 0.1010 20.7 20 405235060.2 0.1010 24 21 1203636653. 1 0.1120 0.8 22 1203636654.2 0.1060 25.9 23 1203636655.2 0.1040 26.5 24 1203636656.2 0.1000 23.8 25 1203636657 .1 0.1120 0.4 Sample Aliquot StDev. G 4.3713E-04 3.2298E-03 3.2298E-03 32296E-03 4.3713E-04 32298E-03 3.2298E-o3 4.3713E-04 3.2296E-Q3 3.2296E-o3 3.2296E-03 3.2301E-Q3 3.2299E-o3 3.2296E-03 3.2296E-03 3.2300E-03 3.2307E-03 3.2298E-03 3.2296E-o3 3.2296E-o3 3.2307E-03 3.2301E-03 3.2299E-03 4.3713E-04 32307E-03 A81602427r1 .xis Gross Alpha/Beta Solid Count Raw Data Sample Delector Date/Time ID 11/30/2015 13:27 4A 11/30/2015 13:53 4D 11/30/201513:59 98 11/3012015 13:50 SA 11/3012015 14:15 BA 121712015 10:02 7A 1217/2015 10:10 48 121712015 13:28 3C 1217/2015 13:33 28 1217/2015 13:42 18 1217/2015 13:02 3D 1217/201513:11 1D 121112015 14:24 78 121212015 14:51 38 12121201514:59 1C 12/2/2015 14:50 6A 12/212015 14:55 70 12f2f2015 15:00 SC 1211612015 12:26 BC 1211612015 12:33 50 9/2712016 0:00 6C 11/3012015 14:15 58 11/30/2015 14:15 SC 11/301201514:15 SD 9127/2016 0:00 108 Page 1 Procedure Code Parmname1 Parmname2 Required Alpha MDA Required Beta MDA Counting GFCGANBS Alpha Beta 4 pCi/G 10 pCi/G Count Time Gross Counts Start (min.) Alpha Bela Dale/Time 130 91 374 9/28/2016 14:48 170 145 528 9128/2016 14:48 130 64 364 912812016 14:48 150 109 602 9128/2016 14:48 190 157 640 9128/2016 14:48 180 136 578 9/28/2016 14:48 180 122 628 9/2812016 14:48 130 125 441 912812016 14:48 160 127 472 912812016 14:48 140-91 415 9128/2016 14:48 140 96 401 9/28/2016 14:48 170 133 639 9/28/201614:48 130 98 473 9128/2016 14:48 170 128 630 9/2812016 14:48 130 111 431 9/2812016 14:48 130 104 505 9/2812016 14:48 130 119 480 9/28/2016 14:48 140 121 457 912812016 14:48 180 171 782 9/2812016 14:48 180 174 602 9128/2016 14:49 60 7 46 9128/2016 14:47 180 195 616 9/28/2016 14:47 60 398 3130 9129/2016 13:04 60 416 3288 912912016 13:04 60 442 3199 9/28/201614:47 Pipet, 0.1 ml Stdev: +/* 0.000200 ml Pipe!, 0.5 ml Stdev : +/* 0.001000 ml Pipe!, 1 ml Stdev : +/* 0.002000 ml Analytlcal SOP: Gl*RAD-A-001 B Instrument SOP: GL-RAD*Hl16 Calibration Data Alpha Calibration Calibration Detector Counted Calibration Due Source Efficiency Pos. on Date Date Used (cpm/dpm) 1 PIC 1211/2015 11/3012016 Th230 0.1469 2 PIC 1211/2015 11/3012016 Th230 0.1559 3 PIC 121112015 11/30/2016 Th230 0.1370 4 PIC 1211/2015 11/3012016 Th230 0.1723 5 PIC 1211/2015 11/3012016 Th230 0.1713 6 PIC 1211/2015 11130/2016 Th230 0.1599 7 PIC 1211/2015 11/30/2016 Th230 0.1427 8 PIC 121112015 11/30/2016 Th230 0.1526 9 PIC 1211/2015 11/30/2016 Th230 0.1149 10 PIC 121112015 11/30/2016 Th230 0.1425 11 PIC 1211/2015 11/3012016 Th230 0.1476 12 PIC 1211/2015 11/30/2016 Th230 0.1440 13 PIC 1211/2015 11/3012016 Th230 0.1560 14 PIC 1211/2015 11/30/2016 Th230 0.1517 15 PIC 121112015 11/30/2016 Th230 0.1485 16 PIC 1211/2015 11/3012016 Th230 0.1518 17 PIC 1211/2015 11/30/2016 Th230 0.1422 18 PIC 1211/2015 11/30/2016 Th230 0.1734 19 PIC 121112015 11/30/2016 Th230 0.1653 20 PIC 121112015 11/30/2016 Th230 0.1811 21 PIC 1211/2015 11/30/2016 Th230 0.2906 22 PIC 121112015 11/30/2016 Th230 0.1767 23 PIC 1211/2015 11/30/2016 Th230 0.1745 24 PIC 1211/2015 11/3012016 Th230 0.1817 25 PIC 121112015 11/30/2016 Th230 0.2564 Del.Elf. Error (cpm/dpm) X*Talk 0.01036 0.07169 0.00613 0.06469 0.00633 0.08644 0.00491 0.07351 0.01473 0.08472 0.00525 0.10057 0.00704 0.16609 0.00568 0.05769 0.02011 0.32798 O.D1356 0.10708 0.00657 0.07566 0.00996 0.06778 0.00479 0.07603 0.00853 0.05297 0.00967 0.06210 0.02108 0.09170 0.00619 0.11008 0.01161 0.06130 0.01321 0.19135 0.00639 0.06885 0.01553 0.05431 0.01152 0.05976 0.01161 0.06111 0.00639 0.06869 0.00844 0.16281 AB1602427r1.xls Beta Weekly Background Calibration Calibration Detector Del Elf. Count Calibration Due Source Efficiency Error CPM Start TI me Date Date Used {cpm/dpm) (cpm/dpm) X-Talk Alpha Beta Datemme (min.) 121112015 11/30/2016 Sr90 0.4694 0.01123 0.00431 0.104 0.770 9/23/2016 18:18 500 1211/2015 11130/2016 Sr90 0.4687 0.00773 0.01310 0.182 0.716 9/231201618:18 500 1211/2015 11/30/2016 Sr90 0.4877 0.00754 0.00186 0.122 0.456 91231201618:14 500 1211/2015 11/30/2016 Sr90 0.4935 0.00851 0.00290 0.188 1.382 9/23/201618:18 500 1211/2015 11/30/2016 Sr90 0.4881 0.01579 0.00165 0.228 1.076 9/2312016 18:14 500 1211/2015 11/3012016 Sr90 0.4832 0.00594 0.00070 0.200 0.824 9/231201618:13 500 1211/2015 11/30/2016 Sr90 0.4865 0.01519 0.00026 0.152 1.540 9/23/201618:18 500 1211/2015 11/30/2016 Sr90 0.4733 0.00988 0.00835 0.116 0.478 91231201618:17 500 1211/2015 11/30/2016 Sr90 0.4536 0.02111 0.00019 0.076 0.464 9123/201618:17 500 1211/2015 11130/2016 Sr90 0.4861 0.00711 0.00168 0.114 1.118 9/231201618:17. 500 1211/2015 11/30/2016 Sr90 0.4621 0.02297 0.00259 0.124 0.630 9/231201618:17 500 12/l/2015 11/3012016 Sr90 0.4832 o.oo692 0.00767 0.158 1.392 9/231201618:17 500 1211/2015 11/30/2016 Sr90 0.4983 0.00627 0.00155 0.132 0.556 9/23/201618:14 500 1211/2015 11/30/2016 Sr90 0.4656 0.01614 0.01009 0.162 1.378 9/2312016 18:17 500 1211/2015 11/30/2016 Sr90 0.4856 0.00847 O.Q1123 0.114 0.722 9/2312016 18:17 500 1211/2015 11/30/2016 Sr90 0.4109 0.02228 0.00287 0.130 0.782 9/23/201618:13 500 1211/2015 11/30/2016 Sr90 0.4703 0.01113 0.00046 0.132 0.802 9/2312016 18:14 500 1211/2015 11130/2016 Sr90 0.4981 0.00657 0.00367 0.182 0.794 912312016 18:18 500 121112015 11130/2016 Sr90 0.4763 0.01955 0.00046 0.210 1.510 9/23/2016 18:14 500 121112015 11/30/2016 Sr90 0.4938 0.00925 0.00363 0.248 0.770 912312016 18:18 500 1211/2015 11/3012016 Sr90 0.4670 0.01970 0.00732 0.106 1.100 9/23/2016 18:13 500 1211/2015 11/30/2016 Sr90 0.4970 0.00426 0.00379 0.272 0.506 912312016 18:18 500 1211/2015 11/30/2016 Sr90 0.4982 0.00657 0.00367 0.182 0.794 9/231201618:18 500 1211/2015 11/3012016 Sr90 0.4939 0.00925 0.00363 0.248 0.770 9/23/201618:18 500 1211/2015 11/3012016 Sr90 0.4707 0.00652 0.00072 0.120 0.560 9/23/201618:15 500 Page2 Notes: 1
  • Reference dale for Spike Activity (dpmlml) is the batch Prep Date Alpha Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 22678 1.6011 4 3.9097 17.8912 12.60% 2 2.4762 1.7482 4 3.9917 17.6844 11.39% 3 2.5569 1.8052 4 4.3468 11.6516 17.44% 4 2.4347 1.7190 4 3.9557 13.6440 13.80% 5 2.4935 1.7604 4 3.9361 15.5881 11.69"k 6 2.4774 1.7491 4 3.9540 15.1344 12.61% 7 2.4203 1.7088 4 3.9284 16.0885 12.55% 8 2.3067 1.6286 4 3.9385 24.1288 10.35% 9 2.2645 1.5988 4 3.9253 27.8370 10.65% 10 2.3550 1.6626 4 3.9961 16.6246 13.48% 11 2.3706 1.6737 4 3.9949 16.7490 13.18% 12 2.4267 1.7133 4 3.9474 17.5757 11.68% 13 2.3137 1.6335 4 3.9076 17.1069 12.91% 14 2.4470 1.7276 4 3.9739 16.2691 12.13% 15 2.3260 1.6422 4 3.9775 21.1015 11.63% 16 2.3380 1.6507 4 3.9537 18.6252 12.52% 17 2.3569 1.6640 4 3.9807 22.1061 11.30% 18 2.3967 1.6921 4 3.9245 16.9028 12.31% 19 2.5034 1.7674 4 3.9844 19.9064 10.77% 20 2.4833 1.7532 4 3.9168 17.3954 11.15% 21. 1.4345 1.0127 4 2.7175 0.0700 435.36% 22 2.5402 1.7934 4 3.9877 19.2001 10.50% 23 3.3704 2.3796 4 6:0000 155.3618 6.14% 24 3.9291 2.7740 4 6.7871 160.7577 5.15% 25 1.7300 1.2214 4 3.2272 113.0825 5.70% AB 16Q2427r1 .xis Alpha Spike SIN : Spike Exp Date : Spike Activity (dpmlml): Spike Volume Added: Spike Nuclide: Alpha LCS SIN : LCS Exp Date : LCS Activity (dpmfml): LCS Volume Added: LCS Nuclide: 2SIGMA Net Count NetCcunt Counting Rate Rate Error Uncertainty CPM CPM pCi/G 0.5960 0.0748 4.4935 0.6709 0.0734 4.0344 0.3703 0.0635 3.9712 0.5387 0.0723 3.6661 0.5983 0.0693 3.5729 0.5556 0.0678 3.6351 0.5258 0.0638 3.8325 0.8455 0.0873 5.0544 0.7178 0.0715 5.4398 0.5360 0.0698 4.2825 0.5617 0.0717 4.2486 0.6244 0.0701 4,0566 0.6218 0.0779 4.2368 0.5909 0.0689 3.9714 0.7398 0.0824. 4.8526 0.6700 0.0801 4.4373 0.7834 0.0855 4.7377 0.6823 0.0809 3.9961 0.7400 0.0755 3.9906 0.7187 0.0766 3.6962 0.0107 0.0464 1.2597 0.8113 0.0810 3.8185 6.4513 0.3330 16.2003 6.6853 0.3407 16.5484 72467 0.3507 10.7646 Page3 1493-B 6/812017 266.08 0.10 Th-230 1493-B 61812017 266.08 0.10 Th-230 2SIGMA Total Prop. Uncertainty pCi/G 5.6035 5.4214 4.5760 4.5448 4.6023 4.6636 4.9307 6.8036 7.7151 5.3815 5.3630 5.3879 5.3796 5.1981 6.4806 5.7857 6.3502 5.1993 5.5622 5.0298 1.2605 5.3599 34.9109 34.4734 24.2637 Sample QC 405235045.2 405235045.2 4052350452 Sample Nominal Type RPD RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP 20.8% MS 1152460 121.3% MSD 3.4% 119.8558 121.1% LCS 107.0141 105.7%

"'d G Vl 0 0 00 0 ....., Vl 00 0 \0 Notes: 1 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date Beta Results Decision Critical Required Sample Act Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 1.9314 1.3636 10 2.9486 19.7350 7.40% 2 1.6332 1.1531 10 2.4708 21.7841 6.70% 3 1.3889 0.9806 10 2.1680 20.6355 7.16% 4 2.3045 1.6270 10 3.4347 23.2974 7.32% 5 1.9009 1.3420 10 2.8298 20.5096 6.37% 6 1.6639 1.1748 10 2.5004 20.9175 6.66% 7 2.2595 1.5953 10 3.3403 16.5089 8.44% 8 1.5094 1.0656 10 2.3509 27.2088 5.75% 9 1.4173 1.0006 10 2.1856 21.8821 6.78% 10 2.1613 1.5259 10 3.2484 16.3007 8.91% 11 1.7068 1.2050 10 2.6169 21.0650 7.68% 12 2.1464 1.5154 10 3.1859 20.3483 7.36% 13 1.4868 1.0497 10 2.3001 26.2970 6.38% 14 2.3259 1.6421 10 3.4532 21.8427 7.63°k 15 1.7901 1.2638 10 2.7396 23.3315 7.14% 16 2.11n 1.4951 10 32311 31.6247 6.86% 17 1.7568 1.2403 10 2.6n9 23.8556 6.74% 18 1.7431 12306 10 2.6494 21.2248 7.15% 19 2.3303 1.6452 10 3.4465 24.6378 6.92% 20 1.6050 1.1332 10 2.4168 22.6493 6.44% 21 2.8754 2.0300 10 4.4907 -2.9253 36.88% 22 1.2318 0.8697 10 1.8818 24.3804 5.75% 23 2.4659 1.7410 10 3.9166 443.0673 3.66% 24 2.5476 1.7987 10 4.0533 488.4210 2.04% 25 2.0355 1.4371 10 3.3014 440.5397 3.46% AB1602427r1 .xis Beta Spike SIN : Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: Spike Nuclide: Beta LCS SIN : LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: LCSNuclide: 2SIGMA Net Count Net Count Counting Rate Rate Error Uncer1ainty CPM CPM pCi/G 2.1069 0.1539 2.8934 2.3899 0.1404 2.5670 2.3440 0.1498 2.6332 2.6313 0.1718 3.0433 2.2924 0.1410 2.5504 2.3871 0.1396 2.4764 1.9489 0.1499 2.6409 2.9143 0.1645 3.0681 2.4860 0.1392 2.6816 1.8463 0.1530 2.7514 2.2343 0.1474 2.7881 2.3668 0.1578 2.7197 3.0825 0.1706 2.9065 2.3279 0.1567 2.9418 2.5934 0.1642 2.9550 3.1026 o.1n3 3.6285 2.8903 0.1732 2.9035 2.4703 0.1578 2.7159 2.8344 0.1648 3.0243 2.5744 0.1418 2.5106 -0.3333 0.1224 2.0658 2.9162 0.1415 2.3714 51.3727 0.9333 15.9020 54.0300 0.9565 17.0978 52.7567 0.9433 15.7972 Page4 1243-0 t2118/2016 483.14 0.10 Sr-90 1243-0 1211812016 483.14 0.10 Sr-90 2SIGMA Total Prop. Uncer1alnty pCi/G 3.8461 4.0144 3.9231 4.4953 3.7on 3.8no 3.6135 4.6275 4.4284 3.6194 4.1940 3.9479 4.7005 4.3170 4.4398 5.9055 4.4643 4.0446 4.8599 4.0982 2.0659 4.1598 63.6134 63.78n 63.3332 Sample QC 405235045.2 405235046.2 405235045.2 . Sample Nominal Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP 17.2% MS 418.5166 101.0% MSD 9.7% 4352572 107.5% LCS 388.6225 113.4% "'O P:l (Jq (!) Vl 0 0 1602427r1 .xis \0 0 ....... Vl 00 Sample ID Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID 0 \0 405235041 4A 130 91 374 9/28/2016 14:48 9/28/2016 16:58 PIG 1602427 405235042 4D 170 145 528 9/28/2016 14:48 9/28/2016 17:38 PIG 1602427 405235043 9B 130 64 364 9/28/2016 14:48 9/28/2016 16:58 PIG 1602427 405235044 SA 150 109 602 9/28/2016 14:48 9/28/2016 17: 18 PIG 1602427 405235045 BA 190 1S7 640 9/28/2016 14:48 9/28/2016 17:58 PIG 1602427 405235046 7A 180 136 578 9/28/2016 14:48 9/28/2016 17:48 PIC 1602427 405235047 4B 180 122 628 9/28/2016 14:48 9/28/2016 17:48 PIC 1602427 405235048 3C 130 125 441 9/28/2016 14:48 9/28/2016 16:58 PIG 1602427 40523S049 2B 160 127 472 9/28/2016 14:48 9/28/2016 17:28 PIG 1602427 405235050 1B 140 91 415 9/28/2016 14:48 9/28/2016 17:08 PIG 1602427 4052S50S1 30 140 96 401 9/28/2016 14:48 9/28/2016 17:08 PIC 1602427 405235052 1D 170 133 639 9/28/2016 14:48 9/28/2016 17:38 PIG 1602427 405235053 7B 130 98 473 9/28/2016 14:48 9/28/2016 16:58 PIG 1602427 405235054 3B 170 128 630 9/28/2016 14:48 9/28/2016 17:38 PIG 405235055 1C 130 111 431 9/28/2016 14:48 9/28/2016 16:58 PIC 1602427 40523S056 6A 130 '104 S05 9/28/2016 14:48 9/28/2016 16:58 PIC 1602427 40523S057 7D 130 119 480 9/28/2016 14:48 9/28/2016 16:58 PIC 1602427 40523S058 SC 140 121 4S7 9/28/2016 14:48 9/28/2016 17:08 PIG 1602427 405235059 BC 180 171 782 9/28/2016 14:48 9/28/2016 17:48 PIG 1602427 40523S060 SD 180 174 602 9/28/2016 14:49 9/28/2016 17:49 PJC 1602427 1203636653 6C . 60 7 46 9/28/2016 14:47 9/28/2016 15:47 PIG 1602427 1203636654 SB 180 195 616 14:47 9/28/2016 17:47 PIG 1602427 1203636655 5C 60 398 3130 9/29/2016 13:04 9/29/2016 14:04 PIG 1602427 1203636656 SD 60 416 3288 9/29/2016 13:04 9/29/2016 14:04 PIG 1602427 1203636657 10B 60 442 3199 9/28/2016 14:47 9/28/2016 1 S:47 PIG 1602427 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 201 O 29-Sep-2016 Batch#. __ __ _ Jr Product:. _______ _ l (_L _ Criteria: Yes No Comments Samole Solids are less than or eaual to 100 m11 for GAB. 10 Samples have been blank corrected {If required). f P.. Blank correction reoorted Included Clf reoulredl. If activity less than 10>< MDA/MDC, error is less than or equal to 150% of sample actlvltv. I If greater than 10* MDA/ MDC, error Is 400/o or less. llf holn*u tho M nA I MDC. error is okav Instrument source check Is within limits. / Jnctrumont bkn r:heck Is within limit'<. Method RDL/ LLD has been met. / If duollcate activities are: Less than 5* MDA/ MDC, then RPO Is 1000/o or less, /' If greater 5* *MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO is 0%, Or meets the client's reauired RER acceotance criteria. Tracer yield is 15-1250/o

  • Carrier vleld 25*125%. / C or meets the client's contract acceptance criteria), Method blank Is less than the RDL/ LLD. / CU cad sam12le5, :S 5°Lo o* *-***--* --****"-"' Samole was run within hold time. oi:fZ. Samole was correctlv oreserved If reouired. / Smears Taken for Radioactive batches. ./ Method Spike and LCS are within 75-1250/o / llor meotc the dlent's rnntract "rront,.nr:e r:rlterla), No blank soaces on data forms. / All line outs Initialed and dated. ,.,_ ---------Aux data Is correct. '('/;-Client Soeclal reoulrements oaoe has been checked. / Raw Data and I or soectrum are Included and nrooerlv statused. / MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and / .. oc V1>rlfierl IMlt *-(If tt-a.n*nrarl ln*n / Batch Data Exceotion Rcoorts <DER\ comolcted If aoollcable
  • Dl::!7 !Ch1117 Batch Data Exception Reports {DER) second reviewed. . / I $lo9-1tf 7 Dlsoosltlon verified to be comoleted. Allouot Correction cnmnletPd if fl' Review sample historical results If available / (If REMP, results above MDC have been verified bv historical results recount or re-analvsls.1 Prlm_ary Review Performed By:. ___ Secondary Review Performed By:.__,._Q""""", Page 5010of5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER .. DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 29-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GFPC EPA 905.0 Modified/DOE RP501 Solid -.. *-W** Batch ID: Sample Numbers: 1597804 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample Analyzed out of Holding Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075, 405235076, 405235077, and 405235078 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader:
  • Nat Long 29-SEP-16 Amanda Fehr 30-SEP-16 Page 1 Page 5011 of 5809 DER Report No.: 1562747 Revision No.: Type: Process Client Code: MJWC Prep Logbook The Determination of Strontium 89/90 in Water, Soil, Milk, Filters, Vegetation and Tissues Batch ID: Analyst: Method: Lab.SOP: 1597804 Bethany Fiern EPA 905.0 Modified/DOE RP501Rev.1 Modified GL-RAD-A-004 REV# 17 Instrument: BAL-18550299 __ l:=d __ =cD::=es"'cn'""*pc.:tc:..:io"'n ___ _ LCS 1203625414 Strontium-90 SPIKE Sample ID Prep Date Dry or Wet Unadjusted Aliquot Aliquot (g) Initial Wt (g) Final Wt (g) Net Wt (mg) 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203625412 MB 23-SEP-201612:57 ---D 23-SEP-201612:57 D 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D 23-SEP-2016 l 2:57 D 23-SEP-2016 12:57 D 23-SEP-2016 I 2:57 D 23-SEP-2016 12:57 D 23-SEP-20 I 6 l 2:57 D 23-SEP-2016 12:57 I) 23-SEP-2016 l 2:57 D 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D 1203625413 DUP (405235065) 1203625414 LCS 23-SEP-2016 12:57 D 23-SEP-2016 12:57 D Reagent/Solvent Lot ID Description 2213530 0.05M fh'l03 2243751 RGF-6M Sodium Hydroxide 2243757 RGF-0.75M Sodium Carponare 2280154.26 R-Hydrogen Peroxide 2334614 Thymol Blue lndicaror 2388714 RGF-80% E!hanol 2414995 Sr 0.5mL=7 37. 2.0 mL=29.46 mg 2424020 RGF-3MNirric/0.05M Oxalic 2433863.1 SR SPEC RESIN Cleaned 2434028 RGF-Sr Filters 2434079 RGF-8M Nitric Acid Analytical Logbook version 1 (g) 0.352 0.341 0.318 0.323 0.304 0.368 0.307 0.333 0.315 0.304 0.308 0.315 0.359 0.304 0.314 0.374 0.342 0.318 0.374 0.354 0.374 Amount 15mL 6mL 13mL JO ml .5mL 3mL .SmL !OmL 2g IL 25mL 0.352 0.341 0.318 0.323 0.304 0.368 0.307 0.333 0.315 0.304 0.308 0.315 0.359 0.304 0.314 0.374 0.342 0.318 0.374 0.354 0.374 Comments: 0.0226 0.0231 0.0236 0.0237 0.0226 0.0231 0.0228 0.0229 0.0235 0.0233 0.0224 0.0231 0.0232 0.0237 0.0227 0.0233 0.0226 0.023 0.0237 0.0235 0.0226 Spike Pipet ID: RAD-GFC-1795419 Carrier Pipe! ID: RAD-GFC-2154115 0.0296 ___ _ 0.0295 0.03 0.0296 0.0288 0.0293 0.029 0.0295 0.0295 0.0297 0.0288 0.0295 0.0298 0.0302 0.0292 0.0295 0.0287 0.0292 0.0299 0.0297 0.0293 7 6.4 6.4 5.9 6.2 6.2 6.2 6.6 6 6.4 6..4 6.4 6.6 6.5 6.5 6.2 6.1 6.2 6.2 6.2 6.7 Data Entry Date2: 23-SEP-2016 14:35 GFC-F30560 Bethany Fiem Data Entry Date3: 27-SEP-2016 14:19 GFC-F30560 Bethany Fiem Data Entry Date4: 23-SEP-2016 00:0-0 Serial Number Spike Amount Spike Units_ 1243-0 .I Sr Separation (date) Strontium Carrier Yield (percent) 95 87 87 80 84 09/27/16 11:44 09/27/1611:44 09/27/16l1:44 09/27/16 11:44 09127/1611:44 09/27/16 11:44 84 09127/16 11:44 84 09127/16 11:44 90 09121116I1:44 81 09/27/16I1:44 87 09/27/16 I I :44 87 09127116 I 1:44 87 09127116 1 I :44 90 09127/1611:44 88 09127/16 11:44 88 09127116 I 1:44 84 09/27/16 11:44 83 09127/16I1:44 84 09127/1611:44 84 09/27/1611:44 84 09/27/16 11:44 91 mL GEL Laboratories LLC Filename : SR90.XLS File type : Excel Version # : 1.3.10 Batch: 1597804 Analyst : BET01177 Prep Date : 9/2312016 Method Uncertainty : 0.089724205 Geometry: Tuffryn Filler Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Pos. ID G G 1 405235061.1 0.3520 3.2558E-03 2 405235062.1 0.3410 3.2546E-03 3 405235063.1 0.3180 3.2522E*03 4 405235064.1 0.3230 3.2528E-03 5 405235065.1 0.3040 3.2508E-03 6 405235066.1 0.3680 3.2575E-03 7 405235067.1 0.3070 3.2511E-03 8 405235068.1 0.3330 3.2538E-03 9 405235069.1 0.3150 3.2519E*03 10 405235070.1 0.3040 3.2508E-03 11 405235071.1 0.3080 3.2512E-03 12 405235072.1 0.3150 3.2519E-03 13 405235073.1 0.3590 3.2565E-03 14 405235074.1 0.3040 3.2508E-03 15 405235075.1 0.3140 3.2518E-03 16 405235076.1 0.3740 3.2581E-03 17 405235077.1 0.3420 3.2547E-03 18 405235078.1 0.3180 3.2522E-03 19 1203625412.1 0.3740 3.2581E-03 20 1203625413.1 0.3540 3.2560E-03 21 1203625414.1 0.3740 3.2581E-03 S 1597804r1 .xis Strontium-90 Solid Carrier SIN : carrier Exp Date : Carrier Volume Added: carrier Weight (mg/ml): carrier Weight StDev.: Sample Date/Time 1211412015 13:47 12114/201513:10 12114/201513:15 12114/2015 13:25 12114/2015 13:56 12114/2015 14:00 12111/201511 :30 12111/2015 10:27 1211612015 12:45 12111/2015 10:10 12111/201510:25 12115/2015 13:35 12111/201511:35 12115/2015 14:10 12116/2015 9:31 12111/2015 14:19 12117/2015 13:30 12117/201512:40 9/23/2016 0:00 12114/2015 13:56 9/23/2016 0:00 2414995 6/3/2017 0.50 14.73 0.10 Carrier calculations Carrier Weight(mg) (Standard) 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 Page 1 Net Weight (mg) (Sample) 7.00 6.40 6.40 5.90 6.20 6.20 6.20 6.60 6.00 6.40 6.40 6.40 6.60 6.50 6.50 6.20 6.10 6.20 6.20 6.20 6.70 Procedure Code : Parmname: Required MDA : Sr-90 Abundance : Halflife of Sr-90 : Halflife of V-90: Net Weight StDev. (mg) 0.037416 0.034837 0.034837 0.032688 0.033978 0.033978 0.033978 0.035697 0.033118 0.034837 0.034837 0.034837 0.035697 0.035267 0.035267 0.033978 0.033548 0.033978 0.033978 0.033978 0.036127 GFC90SRS S1rontium*90 2 pCi/G 1.00 28.90 years 64.053 tiours Carrier Carrier Aliquot Aliquot (ml) StDev. (ml) 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 O.OOtOOO 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 0.5 0.001000 Pipet, 0.1 ml Stdev: Plpet, 0.5 ml Stdev : Pipet, 1 ml Stdev : +/-Analytical SOP: GL-AAD-A-004 Instrument SOP: GL-AAD-1-016 0.000200 0.001000 0.002000 Count Raw Data Counting Detector Time Gross Counts Gross Beta Pos. ID (min.) Alpha Beta CPM 1 1A 60 3 35 0.579 2 1B 60 13 68 1.116 3 1B 60 14 78 1.281 4 3D 60 26 41 0.658 5 2A 60 14 45 0.719 6 SC 60 5 38 0.630 7 7D 60 2 40 0.664 8 38 80 20 109 1.352 9 3C 60 12 37 0.609 10 10C 60 3 14 0.221 11 4C 60 6 40 0.662 12 4D 60 5 39 0.647 13 5A 70 7 91 1.295 14 11A 60 14 60 0.975 15 6A 60 5 53 0.878 16 118 60 3 61 1.013 17 7A 60 7 34 0.558 18 7B 60 4 26 0.430 19 7C 60 6 22 0.355 20 11C 60 7 35 0.564 21 12A 60 6 1512 25.186 S1597804r1.xls ml ml ml Count Start Datefnme 9127/2016 15:39 9/2712016 15:39 9/28/2016 8:51 9/2812016 8:51 9/271201615:39 912812016 8:51 9128/2016 8:50 9/27/2016 15:39 9/27/2016 15:39 9128/2016 8:50 9/27/201615:39 9/27/201615:40 912712016 15:40 9/28/2016 8:54 9/27/201615:38 9/28/2016 8:54 9/27/201615:38 9/27/201615:38 9/27/201615:37 9/28/2016 8:54 9/28/2016 8:54 Page2 Slrontium Separation Datemme 9/27i201611:44 9/27/2016 11 :44 9/27/201611:44 9/2712016 11 :44 9/27/2016 11 :44 9/2712016 11 :44 9/27/2016 11 :44 9/27/2016 11 :44 9/27/201611:44 9/27/2016 11:44 9/27/2016 11 :44 9/27/201611:44 9/27/2016 11 :44 9/27/2016 11 :44 9/27/2016 11 :44 9/27/2016 11 :44 9/27/2016 11 :44 9/27/2016 11 :44 9/271201611:44 9/27/201611:44 9/27/2016 11 :44 Yttrium Ingrowth 0.047 0.047 0.209 0.209 0.047 0.209 0.209 0.049 0.047 0.209 0.047 0.047 0.048 0.209 0.046 0.209 0.047 0.047 0.046 0.209 0.209 Calculated Sample Sample Sr-90 Recovery Recovery Decay % Error% 0.981 95.0% 1.04% 0.981 86.9% 1.05% 0.981 86.9% 1.05% 0.981 80.1% 1.06% 0.981 84.2% 1.05% 0.981 84.2% 1.05% 0.981 84.2% 1.05% 0.981 89.6% 1.04% 0.981 81.5% 1.05% 0.981 86.9% 1.05% 0.981 86.9% 1.05% 0.981 86.9% 1.05% 0.981 89.6% 1.04% 0.981 88.3% 1.04% 0.981 88.3% 1.04% 0.981 84.2% 1.05% 0.981 82.8% 1.05% 0.981 84.2% 1.05% 1.000 84.2% 1.05% 0.981 84.2% 1.05% 1.000 91.0% 1.04%

S1597804r1 .xis Calibration Data Detector WeeklyBkg Weekly Bkg Calibration Detector Efficiency Count Count Counted Calibration Due Efficiency (cpm/dpm) Error Alpha WeeklyBkg Start Time Pos. on Date Dale Sr-90 Y-90 (cpm/dpm) X-Talk CPM Datemme (min.) 1 PIC 4/1/2016 212812017 0.4224 0.5477 0.00738 0.08172 0.848 9/23/2016 18:17 500 2 PIC 411/2016 2128/2017 0.4265 0.5497 0.00711 0.08223 1.118 9/23/2016 18:17 500 3 PIG 4/1/2016 2/28/2017 0.4265 0.5497 0.00711 0.08223 1.118 9/23/2016 18:17 500 4 PIC 4/1/2016 2/28/2017 0.4033 0.5395 0.02297 0.05829 0.630 9/23/201618:17 500 5 PIC 4/1/2016 2/2812017 0.4143 0.5406 0.01914 0.13103 0.470 9/23/2016 18:17 500 6 PIC 411/2016 2/2812017 0.4205 0.5622 0.00657 0.04249 0.794 9/23/201618:18 500 *7 PIC 4/1/2016 2/2812017 0.4140 0.5455 0.01113 0.07795 0.802 9/23/201618:14 500 8 PIC 4/1/2016 2/2812017 0.4069 0.5509 0.01614 0.04289 1.378 9/23/201618:17 500 9 PIC 4/1/2016 2/28/2017 0.4182 0.5563 0.00988 0.04066 0.478 9/23/201618:17 500 10 PIC 4/1/2016 2/28/2017 0.4065 0.5237 0.00638 0.24020 0.396 9/231201618:15 500 11 PIC 4/1/2016 2/28/2017 0.4263 0.5613 0.00889 0.04452 0.748 9/23/201618:18 500 12 PIC 4/1/2016 2/28/2017 0.4138 0.5536 0.00773 0.03940 0.716 9/23/2016 18:18 500 13 PIC 4/1/2016 2/28/2017 0.4333 0.5685 0.00851 0.05031 1.382 9/23/2016 18:18 500 14 PIC 4/1/2016 2/2812017 0.4246 0.5473 0.01317 0.10757 0.906 9/23/2016 17:07 500 15 PIC 411/2016 212812017 0.4135 0.5572 0.02228 0.06252 0.782 9/23/2016 18:13 500 16 PIC 4/1/2016 2128/2017 0.4329 0.5589 0.00697 0.07046 0.776 9/23/2016 17:07 500 17 PIC 4/1/2016 212812017 0.4206 0.5546 0.00594 0.07695 0.824 9/23/2016 18: 13 500 18 PIC 4/1/2016 2128/2017 0.4312 0.5632 0.00627 0.05210 0.556 9/23/2016 18:14 500 19 PIC 4/1/2016 212812017 0.4151 0.5415 0.00790 0.11574 0.444 9/23/2016 18:14 500 20 PIC 4/1/2016 212812017 0.4174 0.5497 0.01278 0.16385 0.468 9/23/2016 17:08 500 21 PIC 4/1/2016 212812017 -0.4050 0.5410 0.01964 0.14055 1.074 9/23/2016 17:08 500 Page3 Notes: 1 -Results are decay corrected to Sample Date/Time 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Date/Time * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 0.8978 0.6338 2 1.4208 -0.8231 39.67% 2 1.1531 0.8141 2 1.7995 -8.505E-Q3 5813.23% 3 1.0332 0.7295 2 1.6124 0.4998 94.33% 4 0.8690 0.6135 2 1.3990 0.0966 393.88% 5 0.8905 0.6287 2 1.4615 1.0178 45.65% 6 0.7816 0.5518 2 1.2414 -0.4525 66.96% 7 0.9597 0.6775 2 1.5234 -0.4643 81.63% 8 1.1686 0.8250 2 1.7831 -0.0930 534.63% 9 0.8862 0.6257 2 1.4526 0.5256 80.72% 10 0.6752 0.4767 2 1.1219 -0.5888 38.36% 11 1.0437 0.7368 2 1.6632 -0.3252 130.51% 12 1.0271 0.7252 2 1.6410 -0.2642 159.50% 13 1.0834 0.7649 2 1.6626 -0.2697 167.56% 14 0.9619 0.6791 2 1.5169 0.2187 195.06% 15 1.0612 0.7492 2 1.6870 0.3624 132.44% 16 0.7439 0.5252 2 1.1830 0.6291 57.28% 17 1.0490 0.7406 2 1.6627 -0.9667 39.31% 18 0.8897 0.6282 2 1.4438 -0.4728 72.14% 19 0.6895 0.4868 2 1.1362 -0.2890 92.81% 20 0.6302 0.4449 2 1.0346 0.2784 105.70% 21 0.8433 0.5954 2 1.3186 61.6345 3.60% S1597804r1 .xis Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): N/A NIA NIA N/A Spike Volume Added: LCS SIN : 1243-0 LCS Exp Date: 12/1812016 LCS Activity (dpm/ml): 483.26 LCS Volume Added: 0.10 2SIGMA 2SIGMA Net Count Net Count Counting Total Prop. Rate Rate Error Uncertainty Uncertainty CPM CPM pCi/G pCi/G -0.2688 0.1065 0.6395 0.6396 -0.0025 0.1443 0.9690 0.9691 0.1628 0.1536 0.9239 0.9283 0.0281 0.1106 0.7454 0.7456 0.2494 0.1137 0.9094 0.9289 -0.1642 0.1099 0.5937 0.5937 -0.1379 0.1126 0.7427 0.7428 -0.0262 0.1402 0.9749 0.9750 0.1305 0.1053 0.8314 0.8368 -0.1747 0.0669 0.4422 0.4423 -0.0858 0.1120 0.8318 0.8319 -0.0693 0.1105 0.8259 0.8260 -0.0870 0.1458 0.8858 0.8859 0.0689 0.1344 0.8361 0.8371 0.0961 0.1273 0.9404 0.9429 0.2371 0.1358 0.7060 0.7149 -0.2663 0.1046 0.7443 0.7444 -0.1261 0.0910 0.6684 0.6685 -0.0889 0.0825 0.5256 0.5257 0.0962 0.1017 0.5767 0.5789 24.1119 0.6495 3.2543 11.9172 Page4 Sample Sample Nominal QC Type RPO RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235065.1 DUP

  • 0.0% LCS 58.2048 105.9%

"'C Pl (1Q (!) Vl 0 1597804r1 .xis ........ ......J 0 >-+, Vo 00 Sample ID Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID 0 \0 405235061 1A 60 3 35 9127 /2016 15:39 9/27/2016 16:39 PIC 1597804 405235062 18 60 13 68 9/27/201615:39 9/27 /2016 16:39 PIG

  • 1597804 405235063 18 60 14 78 9/28/2016 8:51 9/28/2016 9:51 PIG 1597804 405235064 30 60 26 41 9/28/2016 8:51 9/28/2016 9:51 PIG 1597804 405235065 2A 60 14 45 9/27 /2016 15:39 9/27/2016 16:39 PIC 1597804 405235066 5G 60 5 38 9/28/2016 8:51 9/28/2016 9:51 PIG 1597804 405235067 70 60 2 40 9/28/2016 8:50 9/28/2016 9:50 PIG 1597804 405235068 38 80 20 109 9/27/2016 15:39 9/27 /2016 16:59 PIG 1597804 405235069 3C -60 12 37 9/27/201615:39 9/27/2016 16:39 PIG 1597804 405235070 10C 60 3 1"4 9/28/2016 8:50 9/28/2016 9:50 PIG 1597804 405235071 4C 60 6 40 9/27/201615:39 9/27 /2016 16:39 PIG 1597804 405235072 40 60 5 39 -9/27/2016 15:40 9/27 /2016 16:40 PlC 1597804 405235073 SA 70 7 91 9/27/201615:40 9/27/201616:50 PIG 1597804 405235074 11A 60 14 60 9/28/2016 8:54 9/28/2016 9:54 PIG 1597804 405235075 6A 60 5 53 9/27/201615:38 9/27 /2016 16:38 PIG 1597804 405235076 118 60 3 61 9/28/2016 8:54 9/28/2016 9:54 PIC 1597804 405235077 7A 60 7 34 9/27/2016 15:38 9/27/201616:38 PIC 1597804 405235078 78 60 4 26 9/27/2016 15:38 9/27/2016 16:38 PIG 1597804 1203625412 7C 60 6 22 9/27/201615:37 9/27/201616:37 PIG 1597804 1203625413 11C 60 7 35 9/28/2016 8:54 9/28/2016 9:54 PIG 1597804 1203625414 12A 60 6 1512 9/28/2016 8:54 9/28/2016 9:54 PIG 1597804 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 2010 26-Sep-2016 Batch# __ \_S_0_1f-D{53. ___ _ Product:. __ s_*_*r ____ _ Date:._0_il2_(,,_hi_ Criteria: Yes No Comments Samele Solids are less than or equal to 100 m11 for GAB. t.f'i. Samples have been blank corrected (If required). Blank correction reaorted Included lff reauired). lf activity less than 10x MDA/MDC, error Is less than or eaual to 150% of sample activity. I If greater than 10* MDA/ MDC, error Is 40% or less. IIf hnln ... *hn unA./ Mnr i<: source check is within limits. / Inr*** mAnt hkn chnr" I<< within limits. Method RDL/ LLD has been met. / If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or les5!, / If greater 5* MDA/ MDC, then RPO 20% or less, lf below the MDA/ MDC, the RPO Is 0%, Or meets the client's reaulred RER acceotance criteria. Tracer yield Is 15-125%
  • Carrier yield 25-125%. I (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. / < 50/n nf lnWP.<<t ""tivitv) Samele was run within hold time. / otTZ Samnle was correctlv oreserved If reoufred. / Smears Taken for Radioactive batches. / Method Spike and LCS are within 75-125% /" l<n* men>r the client'<: l"Ontrart acc:ent,,nc:e l"*fterial. No blank spaces on data forms. /' All line outs Initialed and dated. INn --------Aux data is correct. Client Snecial reauirements oaae has been checked. /_ Raw Data and/ or snectrum are Included and nronerlv statused. / MS, LCS, and ouollcate RPD/RER values uoloaded to UMS and / u"'""" verified .... (If [If\ n .. *rh nn*nrn.I ln*n / Batch Data Exceotion Reoorts (DER) comoleted If aopllcable. v Ot.12-Batch Data Exception Reports (DER) second reviewed. v'/ Dfsoosltlon verified to be completed. Allauot Correction comofeted If .... nnired. NA Review sample historical results If available I (If REMP, results above MDC have been verified bv historical results recount or re-analvsls.) / ' Secondary Review Performed By: __ ___ ______ _ Page 5018of5809 1:-1 I I £lo \ifr_.2-1qt( GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DATA E}(CEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 26-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: GFPC EPA 905.0 Modified/DOE RP501 Solid . *-Batch ID: Sample Numbers: 1597803 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample Analyzed out of Holding Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, 405235060, and 1203625409 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Nat Long 26-SEP-16 Kenshalla Oston 27-SEP-16 Page 1 Page 5019of5809 DER Report No.: 1561542 Revision No.:
  • Type: Process Client Code: MJWC Prep Logbook The Determination of Strontium 89/90 in Water, SoU, Milk, Filters, Vegetation and Tissues Batch ID: Analyst: Method: Lab SOP: 1597803 Kelli Dorrell EPA 905.0 Modified/DOE RP501 Rev. 1 Modified GL-RAD-A-004 REV# 17 Instrument: BAL-16107662 LCS 1203625410 Strontium-90 SPIKE ----**--*--------**-----*---------------------**-***-*------------**----Sample ID Prep Date Dry or Wet Unadjusted Aliquot (g) Aliquot (g) Initial Wt (g) Final Wt (g) Net Wt (mg) Serial Number 1243-0 Sr Separation (date) .I mL 40523504-1 -----.---ffsEr-=2°016T6;39 ____ o _____________ D."382-------*--o.*3s2 ________ 0.0233-----*o.0301---*-6.s ___________ 09/22116 13:28.iA-------*--*----------405235042 21-SEP-2016 16:39 D 0.574 0.574 0.0229 0.0289 6 09122116 13:28 ii? 405235043 21-SEP-2016 16:39 D 0.316 0.316 0.0231 0.0302 7.1 09122116 13:28 lp >'1.\(3 405235044 21-SEP-2016 16:39 D 0.319 0.319 0.023 0.0298 6.8 09122116 405235045 21-SEP-2016 16:39 D 0.324 0.324 0.0236 0.0303 6.7 09/22116 13:28 Z;i5 405235046 21-SEP-2016 16:39 D 0.361 0.361 0.0231 0.03 6.9 09/22116 13:28 -Z.c.. 405235047 21-SEP-2016 16:39 D 0.331 0.331 0.023 0.0297 6.7 0912211613:28 19 405235048 21-SEP-2016 16:39 D 0.382 0.382 0.0235 0.0303 6.8 09112116 13:28 405235049 21-SEP-2016 16:39 D 0.356 0.356 0.0235 0.0304 6.9 09/22/1613:28 °5]> 405235050 21-SEP-2016 16:39 D 0.317 0.317 0.0234 0.0304 7 09/22116 13:28 'IA 405235051 21-SEP-2016 16:39 D 0.352 0.352 0.0232 0.03 6.8 09/22116 13:28 405235052 21-SEP-2016 16:39 D 0.421 0.421 0.0233 0.0294 6.1 09/22116 13:28 . 405235053 21-SEP-2016 16:39 D 0.323 0.323 0.0225 0.0286 6.1 09/22/16 13:28 4;j-SO 405235054 21-SEP-2016 16:39 D 0.424 0.424 0.0225 0.0293 6.8 09122116 13:28 Sc.. 405235055 21-SEP-2016 16:39 D 0.329 0.329 0.0229 0.0295 6.6 09/22116 13:28 '7D 405235056 21-SEP-2016 16:39 D 0.312 0.312 0.0226 0.0284 5.8 09/22116 13:28 0.4-,.
  • C:, 405235057 21-SEP-2016 16:39 D 0.301 0.301 0.0231 0.0298 6.7 09122116 t.j 405235058 21-SEP-201616:39 D 0.387 0.387 0.0232 0.0297 6.5 405235059 21-SEP-2016 16:39 D 0.432 0.432 0.023 0.0298 6.8 09122116 13:28 71/ 405235060 21-SEP-2016 16:39 D 0.426 0.426 0.023 0.0295 6.5 09/2211613:28 1£, 1203625408 MB 21-SEP-2016 16:39 D 0.574 0.0235 0.0302 6.7 09/22/1613:28 '(C.. ___ ___ lib ___________ __ Comments: 2054611.2 Phenolphthalein_ 1.0% in 50% Alcohol 2213530 0.05M HN03 2243751 RGF-6M Sodium H)*droxide 2243757 RGF-0.75M Sodium Carbonaie 2334614 Thymol Blue Indicamr 23S8714 RGF-80'k Elhanol 2414995 Sr0.5ml=7.37, 2.0 ml..=29.46 mg 2424020 RGF-3M Nitric/0.0SM Oxalic 1433863.l SR SPEC RESIN Cleaned 2434028 RGF-Sr Filters 2434079 Nitric Acid 2mL 15ml 6ml 13ml .Sml 3mL .Sml IOmL 2g ll 25mL Spike Pipe! JD: RAD-GFC-1795419 Carrier Pipet ID: RAD-GFC-2154115 Data Emry Date2: 22-SEP-2016 13:28 GFC-F30560 Kelli Dorrell Analytical Logbook \'ersion 111-04-2002 GEL Laboratories LLC 0 H) Vl 00 0 \0 Filename : SR90.XlS File type : Excel Version#: 1.3.10 Batch : 1597803 Analyst: KEl01237 Prep Date : 9/21/2016 Method Uncertainty : 0.089724205 Geometry: Tuffryn Filter Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Pos. ID G G 1 405235041.1 0.3820 3.2589E-03 2 405235042.1 0.5740 3.2790E-03 3 405235043.1 0.3160 3.2520E-03 4 405235044.1 0.3190 3.2523E-03 5 405235045.1 0.3240 3.2529E-03 6 405235046.1 0.3610 3.2567E-03 7 405235047.1 0.3310 3.2536E-03 8 405235048.1 0.3820 3.2589E-03 9 405235049.1 0.3560 3.2562E-03 10 405235050.1 0.3170 32521E-03 11 405235051.1 0.3520 32558E-03 12 405235052.1 0.4210 3.2630E-03 13 405235053.1 0.3230 3.2528E-03 14 405235054.1 0.4240 3.2633E-03 15 405235055.1 0.3290 3.2534E-03 16 405235056.1 0.3120 3.2516E-03 17 405235057.1 0.3010 3.2505E-03 18 405235058.1 0.3870 3.2594E-03 19 405235059.1 0.4320 3.2641E-03 20 405235060.1 0.4260 3.2635E-03 21 1203625408.1 0.5740 32790E-03 22 1203625409.1 0.2970 3.2500E-03 23 1203625410.1 0.5740 3.2790E-03 S1597803r2.xls Strontium-90 Solid Carrier SIN : Carrier Exp Date : Carrier Volume Added: Carrier Weight (mg/ml): Carrier Weight StDev.: Sample Date/Time 11 /30/2015 13:27 11/30/2015 13:53 11/30/2015 13:59 11/30/2015 13:50 11/30/201514:15 1217/201510:02 1217/201510:10 1217/2015 13:28 1217/2015 13:33 1217/2015 13:42 1217/2015 13:02 1217/2015 13:11 12/1/2015 14:24 12/2/2015 14:51 12/2/2015 14:59 12/212015 14:50 12/212015 14:55 12/212015 15:00 12/16/201512:26 12/1612015 12:33 9/21/2016 0:00 11/30/201514:15 9/21/2016 0:00 2414995 6/3/2017 0.50 14.73 0.10 Carrier Calculations Carrier Weight(mg) (Standard) 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 14.73 Page 1 Procedure Code : GFC90SRS Parmname: Strontium-90 Required MDA : 2 pCi/G Sr-90 Abundance : 1.00 Halfllfe of Sr-90: 28.90 years ... Halflife of Y-90: 64.053 hours Net Net Carrier Carrier Weight(mg) Weight Aliquot Aliquot (Sample) S!Dev. (mg) (ml) StDev. (ml) 6.80 0.036556 0.5 0.001000 6.00 0.033118 0.5 0.001000 7.10 0.037846 0.5 0.001000 6.80 0.036556 0.5 0.001000 6.70 0.036127 0.5 0.001000 6.90 0.036986 0.5 0.001000 6.70 0.036127 0.5 0.001000 6.80 0.036556 0.5 0.001000 6.90 0.036986 0.5 0.001000 7.00 0.037416 0.5 0.001000 6.80 0.036556 0.5 0.001000 6.10 0.033548 0.5 0.001000 6.10 0.033548 0.5 0.001000 6.80 0.036556 0.5 0.001000 6.60 0.035697 0.5 0.001000 5.80 0.032258 0.5 0.001000 6.70 0.036127 0.5 0.001000 6.50 0.035267 0.5 0.001000 6.80 0.036556 0.5 0.001000 6.50 0.035267 0.5 0.001000 6.70 0.036127 0.5 0.001000 6.40 0.034837 0.5 0.001.000 6.60 0.035697 0.5 0.001000 Pipet, 0.1 ml Stdev: Pipet, 0.5 ml Stdev : Pipet, 1 ml Stdev : +/-Analytical SOP: GL-RAD-A-004 Instrument SOP: GL-RAD*l-016 0.000200 0.001000 0.002000 Count Raw Data Counting Detector nme Gross Counts Gross Beta Pas. ID (min.) Alpha Beta CPM 1 1A 60 2 50 0.831 2 18 70 6 83 1.179 3 1D 70 12 79 1.120 4* 18 60 8 66 1.069 5 2B 60 1 34 0.562 6 2C 60 5 38 0.628 7 38 80 21 96 1.189 8 3C 60 16 36 0.622 9 30 60 9 33 0.541 10 4A 60 11 33 0.541 11 4C 60 2 37 0.615 12 4D 60 3 62 1.031 13 3D 60 14 28 0.453 14 SC 60 7 36 0.628 1S SD 90 12 47 0.516 16 6A 70 9 46 0.649 17 4C 60 8 30 0.494 16 SA 60 5 81 1.346 19 7A 60 9 55 0.905 20 7B 60 10 31 0.508 21 7C 60 4 26 0.426 22 7D 60 6 26 0.425 23 BA 60 12 1360 22.654 S1597803r2.xls ml ml ml Count Start Datemme 9/22/201617:20 9/22/201617:20 9/2212016 17:21 9/23/2016 13:27 9/221201617:20 9122/2016 17:20 9/2212016 17:21 912212016 17:20 9/2212016 17:20 9/22/2016 17:20 9122/2016 17:20 9/22/2016 17:20 9/23/2016 11 :36 9/22/2016 17:20 9122/2016 17:21 9/221201617:19 9/23/2016 11 :21 9/231201611:21 91221201617:18 9/22/2016 17:18 9/22/201617:18 9/22/2016 17:16 9/221201617:18 Page 2 Strontium Separation Datemme 9/2212016 13:28 9/22/201613:28 9/22/2016 13:28 9122/2016 13:28 9/22/2016 13:28 9/22/2016 13:28 9/2212016 13:28 9/2212016 13:28 9/2212016 13:28 9/22/2016 13:28 9/2212016 13:28 912212016 13:28 912212016 13:28 9/2212016 13:28 9/2212016 13:28 9/221201 6 13:28 9122/2016 13:28 9/22/2016 13:28 9/22/2016 13:28 9/221201613:28 91221201613:26 9/2212016 13:28 9/2212016 13:28 Yttrium Ingrowth 0.046 0.047 0.047 0.233 0.046 0.046 0.048 0.046 0.046 0.046 0.046 0.046 0.217 0.046 0.049 0.047 0.21S 0.215 0.046 0.046 0.046 0.046 0.046 Calculated Sample Sample Sr-90 Recovery Recovery Decay % Error% 0.981 92.3% 1.04% 0.981 81.5% 1.05% 0.981 96.4% 1.03% 0.961 92.3% 1.04% 0.981 91.0% 1.04% 0.981 93.7% 0.981 91.0% 1.04% 0.981 92.3% 0.981 93.7"/o 1.04% 0.981 95.0% 1.04% 0.981 92.3% 1.04% 0.981 82.8% 1.05% 0.961 82.8% 1.05% 0.981 92.3% 1.04% 0.961 89.6% 1.04% 0.981 78.8% 1.06% 0.981 91.0% 1.04% 0.981 88.3% 1.04% 0.962 92.3% 1.04% 0.982 88.3% 1.04% 1.000 91.0% 1.04% 0.981 86.9% 1.05% 1.000 89.6% 1.04%

S159780312.xls Calibration Data Detector WeeklyBkg WeeklyBkg Calibration Detector Efficiency Count Count counted Calibration Due Efficiency (cpm/dpm) Error Alpha Weekly Bkg Start Time Pos. on Date Date Sr-90 Y-90 (cpm/dpm) X-Talk CPM Datemme (min.) 1 PIC 4/1/2016 2128/2017 0.4226 0.5477 0.00738 0.08126 0.606 9/16/201617:24 500 2 PIC 411/2016 2128/2017 0.4272 0.5497 0.00711 0.08136 1.062 9/16/201617:24 500 3 PIC 4/1/2016 2128/2017 0.4194 0.5546 0.00692 0.04952 1.456 9/16/2016 17:24 500 4 PJC 4/1/2016 2128/2017 0.4258 0.5497 0.00711 0.08308 1.062 9/16/2016 17:24 500 5 PIC 4/1/2016 2128/2017 0.4006 0.5091 0.02111 0.27533 0.360 9/1612016 17:24 500 6 PIC 4/1/2016 2/28/2017 0.4094 0.5331 0.01274 0.06390 0.506 9/16/2016 17:24 500 7 PIC 4/1/2016 2128/2017 0.4068 0.5509 0.01614 0.04306 1.400 9/1612016 17:25 500 8 PIC 4/1/2016 212812017 0.4176 0.5563 0.00988 0.04185 0.556 9/1612016 17:25 500 9 PIC 4/1/2016 2128/2017 0.4030 0.5395 0.02297 0.05962 0.582 9/16/201617:25 500 10 PIC 411/2016 2128/2017 0.4185 0.5503 0.01123 0.04798 0.700 9/16/201617:25 500 11 PIC 4/1/2016 2/28/2017 0.4259 0.5613 0.00889 0.04535 0.738 9/16/2016 17:25 500 12 PIC 4/1/2016 2128/2017 0.4141 0.5536 0.00773 0.03878 0.732 9/16/2016 17:25 500 13 PIC 4/1/2016 2128/2017 0.4033 0.5395 0.02297 0.05856 0.582 9/1612016 17:25 500 14 PIC 4/1/2016 2128/2017 0.4203 0.5622 0.00657 0.04334 0.856 9/1612016 17:25 500 15 PIC 4/1/2016 2128/2017 0.4253 0.5641 0.00925 0.04523 0.748 9/16/2016 17:26 500 16 PIC 4/1/2016 2/28/2017 0.4140 0.5572 0.02228 0.06083 0.878 9/16/2016 17:58 500 17 PIC 4/1/2016 2/28/2017 0.4260 0.5613 0.00889 0.04515 0.738 9/16/2016 17:25 500 18 PIC 4/1/2016 2128/2017 0.4335 0.5685 0.00851 0.05009 1.386 9116/2016 17:25 500 19 PIC 4/1/2016 2128/2017 0.4202 0.5546 0.00594 0.07831 0.792 9/16/201618:18 500 20 PIC 4/1/2016 2/28/2017 0.4308 0.5632 0.00627 0.05267 0.466 9/16/2016 17:58 500 *21 PIC 4/1/2016 212812017 0.4149 0.5415 0.00790 0.11682 0.398 9/16/2016 17:58 500 22 PIC 4/1/2016 2128/2017 0.4138 0.5455 0.01113 0.07851 0.676 9/16/201617:58 500 23 PIC 4/1/2016 2128/2017 0.4127 0.5573 0.01579 0.06390 0.818 9/161201617:58 500 Page3 Notes: 1 -Results are decay corrected to Sample Date/Time 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Date/Time * -RPD changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G o/o 1 0.7206 0.5087 2 1.1628 0.6531 54.65% 2 0.6642 0.4689 2 1.0308 0.2531 117.97% 3 1.2141 0.8572 2 1.8594 *1.1367 40.97% 4 0.9238 0.6522 2 1.4453 0.0758 528.86% 5 0.7018 0.4955 2 1.1746 0.7425 49.77% 6 0.7082 0.5000 2 1.1564 0.3816 87.83% 7 1.1683 0.8248 2 1.7816 -0.7436 62.93% 8 0.6970 0.4921 2 1.1310 0.1943 161.94% 9 0.7812 0.5515 2 1.2639 -0.1317 246.46% 10 0.9142 0.6454 2 1.4624 --0.5450 64.31% 11 0.8550 0.6037 2 1.3636 -0.3841 88.17% 12 0.8155 0.5757 2 1.3012 0.8964 45.64% 13 0.8011 0.5656 2 1.2962 -0.4255 72.42% 14 0.7742 0.5466 2 1.2246 -0.5986 48.49% 15 0.7935 0.5602 2 1.2351 -0.7972 36.72% 16 1.1830 0.8352 2 1.8524 -0.9710 46.01% 17 0.8389 0.5923 2 1.3379 *0.7486 40.42% 18 0.9067 0.6401 2 1.4012 -0.0972 395.16% 19 0.7314 0.5164 2 1.1618 0.2915 114.34% 20 0.5808 0.4100 2 0.9537 0.1119 231.42% 21 0.3940 0.2782 2 0.6545 0.0540 322.44% 22 1.0615 *o.7494 2 1.7016 -1.0160 36.73% 23 0.5754 0.4062 2 0.9124 43.6387 3.44% S1597803r2.xls Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): NIA NIA NIA NIA Spike Volume Added: LCS SIN: 1243*0 LCS Exp Date: 12/18/2016 LCS Activity (dpm/ml): 483.33 LCS Volume Added: 0.10 2SIGMA 2SlGMA Net Count Net Count Counting Total Prop. Rate Rate Error Uncertainty Uncertainty CPM CPM pCi/G pCi/G 0.2246 0.1227 0.6993 0.7090 0.1167 0.1377 0.5851 0.5868 -0.3359 0.1375 0.9121 0.9122 0.0269 0.1424 0.7859 0.7860 0.2021 0.1004 0.7233 0.7366 0.1220 0.1071 0.6567 0.6604 -0.2113 0.1329 0.9166 0.9166 0.0662 0.1072 0.6167 0.6177 -0.0409 0.1009 0.6362 0.6363 *0.1588 0.1021 0.6867 0.6868 -0.1228 0.1083 0.6636 0.6637 0.2994 0.1366 0.8015 0.8174 -0.1290 0.0933 0.6036 0.6037 -0.2277 0.1104 0.5687 0.5687 *0.2318 0.0850 0.5732 0.5732 -0.2287 0.1050 0.8741 0.8742 -0.2440 0.0985 0.5924 0.5925 -0.0402 0.1588 0.7528 0.7528 0.1129 0.1291 0.6532 0.6553 0.0419 0.0969 0.5078 0.5082 0.0275 0.0888 0.3415 0.3417 -0.2505 0.0919 0.7304 0.7305 21.8359 0.6158 2.4121 8.3304 Page4 Sample Sample Nominal QC Type RPD RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235045.1 DUP

  • LCS 37.9293 115.1%

'"C Pl (tQ (1) Vo 0 N 1597803r2.xls Vo 0 H) Vo 00 Sample ID Instr Time (min.) Alpha Counts Beta Counts Count Start Time Count End Time Machine Batch ID 0 \0 405235041 1A 60 2 50 9/22/2016 17:20 9/22/2016 18:20 PIC 1597803 405235042 18 70 6 83 9/22/2016 17:20 9/22/2016 18:30 PIC 1597803 405235043 10 70 12 79 9/22/2016 17:21 9/22/2016 18:31 PIC 1597803 405235044 18 60 8 66 9/23/201613:27 9/23/2016 14:27 PIC 1597803 405235045 2B 60 1 34 9/22/2016 17:20 9/22/2016 18:20 PIC 1597803 405235046 2C 60 5 38 9/22/2016 17:20 9/22/2016 18:20 PIC 1597803 405235047 3B 80 21 96 9/22/2016 17:21 9/22/2016 18:41 PIG 1597803 405235048 3C 60 16 38 9/22/2016 17:20 9/22/2016 18:20 PIC 1597803 405235049 30 60 9 33 9/22/2016 17:20 9/2212016 18:20 PIC 1597803 405235050 4A 60 11 33 9/22/2016 17:20 9/22/2016 18:20 PIC 1597803 405235051 4C 60 2 37 9/22/2016 17:20 9/22/2016 18:20 PIC 1597803 405235052 40 60 3 62. 9/22/2016 17:20 9/22/2016 18:20 PIG 1597803 405235053 30 60 14 28 9/23/2016 11 :36 9/23/2016 12:36 PIC 1597803 405235054 5G 60 7 38 9/22/2016 17:20 9/22/2016 18:20 PIC 1597803 405235055 50 90 12 47 9/22/2016 17:21 9/22/2016 18:51 PIC 1597803 405235056 6A 70 9 46 9/22/2016 17:19 9/22/2016 18:29 PIC 1597803 405235057 4C 60 8 30 9/23/2016 11 :21 9/23/2016 12:21 PIC 1597803 405235058 5A 60 5 81 9/23/2016 11 :21 9/23/2016 12:21 PIC 1597803 405235059 7A 60 9 55 9/22/2016 17:18 9/22/2016 18:18 PIC 1597803 405235060 7B . 60 10 31 9/22/201617:18 9/22/201618:18 PIC 1597803 1203625408 7C 60 4 26 9/22/2016 17: 18 9/22/2016 18:18 PIC 1597803 1203625409 70 60 6 26 9/22/201617:18 9/22/2016 18: 18 PIC 1597803 1203625410 BA 60 12 1360 9/22/201617:18 9/22/2016 18:18 PIC 1597803 Page 5026 of 5809 Continuing Calibration Data Gas Flow Proportional Counter Checks for 16-Sep-2016 Detectors LB4100 A1 thro"'gh J4 and PIC 1A through 140 Short Name Status Parmname Run Time Count CPMor Low Limit High Limit Stdev Time dee LB4100B2 need 2nd Alpha bkg 16-Sep 06:37 60 0.150 0.096 0.359 -1.77 LB4100B2 Above Beta bkg 16-Sep 06:37 60 2.167 0.992 2.051 +3.66 LB4100B3 Above Beta bkg 16-Sep 05:15 60 3.083 0.965 1.943 +10.00 LB4100C1 need 2nd Alpha bkg 16-Sep 05:17 60 0.267 . 0.149 0.367 +0.24 LB4100C4 Above Alpha bkg 05:17 60 0.333 4.08E-6 0.304 +3.58 LB410PC4 Above Beta bkg 16-Sep 05:17 60 2.100 0.686 2.113 +2.95 LB4100E2 Above Beta bkg 16-Sep 05:15 60 2.433 1.061 2.316 +3.56 LB4100E4 Above Beta bkg 16-Sep 05: 15 60 2.333 0.650 2.302 +3.11 LB4100F1 Below Alpha eff 16-Sep 06:40 5 10495 10840 11730 -5.33 LB4100F1 Above AlphaXTalk 16-Sep 06:40 5 0.268 0.224 0.265 +3.44 . LB4100F2 Below Beta eff 16-Sep 07:01 5 18234 18400 19480 -3.92 LB4100F3 need 2nd Beta bkg 16-Sep 05:15 60 1.150 0.797 2.216 -1.51 LB4100H4 Below Alpha eff 16-Sep 06:33 5 10341 11490 13890 -5.87 LB4100H4 Above Alpha XTalk 16-Sep 06:33 5 0.423 0.307 0.379 +6.68 LB4100H4 Below Beta eff 16*Sep 06:40 5 34210 35210 36600 -7.32 LB410013 Above Alpha XTaJk 16-Sep 06:19 5 0.198 0.143 0.193 +3.53 LB410014 Below Alpha eff 16-Sep 06:19 5 11497 12310 13620 -6.72 LB410014 Below Beta bkg 16-Sep 05:15 60 0,883 0.958 1.734 -3.58 LB410014 Below Beta eff 16-Sep 06:26 5 20099 20380 21610 -4.37 PIC2D Above Alpha bkg 16-Sep 07:40 60 0.333 0.006 0.407 +1.90 PIC3A need 2nd Alpha XTalk 16-Sep 05:26 .5 0.265 0.240 0.267 +2.67 PIC3A Below Beta XTalk 16-Sep 05:18 5 0.001 O.Q11 0.029 -6.51 PIC5B Above Alpha bkg 16-Sep 06:49 60 0.367 0.107 0.374 +2.84: PIC8D Above Alpha bkg 16-Sep 06:47 60 0.333 0.004 0.401 . +1.98 PIC10A Below Alpha eff 16-Sep 05:44 5 8831 8854 10610 -3.08 PIC10A need 2nd Beta eff 16-Sep 05:52 5 45029 44740 53240' -2.80 PIC11D Above Alpha bkg 16-Sep 07:17 60 0.333 0.001 0.361 +2.54 Page 1of2 Page 5027 of 5809 PIC13A PIC13B PIC14B Above Alpha bkg Alpha bkg need 2nd Alpha bkg 16-Sep 07:18 60 0.467 -5.13E-2 0.389 16-Sep 07:18 60 0.317 -5.Q2E-2 0.412 16-Sep 06:13 60 0.217 -8.43E-2 0.377 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS LB4100D1 LB4100D2 LB4100D3 LB4100D4 PIC6D PIC7C PIC8B PIC9B PIC13C The following detectors may not have properly transferred to the LIMS system Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by /f Date q-/&-JU-, GEL Laboratories LLC Page 2 of 2 Page 5028 of 5809 +4.06 +1.76 +0.92 Gas Flow Proportional Counter Checks for 17-Sep-2016 Detectors LB4100 A1 througf\J4 and PIC 1A through 140 Short Name Status Parm name Run Time Count CPMor Low Limit High Limit Stdev Time dee LB4100B2 Above Alpha bkg 17-Sep 16:06 60 0.333 0.096 0.359 +2.41 LB4100B3 Above Beta bkg 16-Sep 17:32 500 3.220 0.965 1.943 +10.84 LB4100C4 need 2nd Alpha bkg 16-Sep 17:48 500 0.246 4.0BE-6 0.304 +1.86 LB4100C4 Above Beta bkg 16-Sep 17:48 500 2.172 0.686 2.113 +3.25 LB4100E2 Above Beta bkg 16-Sep 17:44 500 2.598 1.061 2.316 +4.35 LB4100E4 Above Beta bkg 16-Sep 17:44 500 2.254 0.650 2.302 +2.83 LB4100F1 Below Alpha eff 17-Sep 16:06 5 10608 10840 11730 -4.56 LB4100F1 need 2nd Alpha XTalk 17-Sep 16:06 5 0.262 0.224 0.265 +2.56 LB4100H4 Below Alpha eff 17-Sep 15:59 5 10188 11490 13890 -6.25 LB4100H4 Above Alpha XTalk 17-Sep 15:59 5 0.425 0.307 0.379 +6.82 LB4100H4 Below Beta eff 17-Sep 16:06 5 34259 35210 36600 -7.11 LB410014 Below Alpha eff 17-Sep 15:44 5 11444 12310 13620 -6.97 LB4100l4 Below Beta bkg 16-Sep 17:28 500 0.762 0.958 1.734 -4.51 LB410014 Below Beta eff 17-Sep 15:51 5 20148 20380 21610 -4.13 PIC2D Above Alpha bkg 17-Sep 15:08 60 0.367 0.006 0.407 +2.40 PIC3A Above Alpha XTalk 17-Sep 14:59 5 0.271 0.240 0.267 +3.95 PIC3A Below Beta XTalk 17-Sep 14:52 5 0.001 O.Q11 0.029 -6.38 PIC13A Above Alpha bkg 17-Sep 15:43 60 0.333 -5.13E-2 0.389 +2.24 PIC14B Above Beta bkg 16-Sep 17:23 1000 1.728 -1.34E-1 1.713 +3.05 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS The following detectors may not have properly transferred to the LIMS system LB4100D1 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D2 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D3 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D4 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC6D Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC13C Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by Page 1of2 Page 5029 of 5809 Date __,_q_,_/-'-1 ._b-=-<v _____ _ GEL Laboratories LLC Page 2 of 2 Page 5030 of 5809 . Gas Flow Proportional Counter Checks for 19-Sep-2016 Detectors LB4100 A1 through J4 and PIC 1A through 140 Short Name Status Parmname Run Time Count Time CPMor Low Limit High Limit Stdev dee LB4100B3 Above Alpha bkg 19-Sep 08:10 60 0.350 0.121 0.383 +2.24 LB4100B3 Above Beta bkg 19-Sep 08:10 60 3.200 0.965 1.943 +10.71 LB4100C1 Above Alpha bkg 19-Sep 08:15 60 0.433 0.149 0.367 +4.81 LB4100C4 Above Alpha bkg 19-Sep 08:15 60 0.367 4.08E-6 0.304 +4.24 LB4100C4 Above Beta bkg 19-Sep 08:15 60 2.183 0.686 2.113 +3.30 LB4100E2 Above Beta bkg 19-Sep 06:29 60 2.667 1.061 2.316 +4.68 LB4100E3 Above Beta bkg 19-Sep 07:55 60 2.283 0.463 2.359 +2.76 LB4100E4

  • Ab.ova Beta bkg 19-Sep 06:29 60 2.400 0.650 2.302 +3.36 LB4100F1 Below Alpha eff 19-Sep 09:55 5 10542 10840 11730 -5.01 LB4100G3 Above Beta bkg 07:54 60 9.033 0.611 1.889 +36.54 LB4100H4 Below Alpha eff 19-Sep 07:4 t 5 10613 11490 13890 -5.19 LB4100H4 Above AlphaXTalk 19-Sep 07:41 5 0.409 0.307 0.379 +5.50 LB4100H4 Below Beta eff 19-Sep 07:34 5 34216 35210 36600 -7.29 LB410013 Above Beta bkg 19-Sep 06:29 60 2.183 0.091 2.093 +3.27 LB410014 Below Alpha eff 19-Sep 08:09 5 11549 12310 13620 -6.49 LB410014 Below AlphaXTalk 19-Sep 08:09 5 0.188 0.189 0.219 -3.09 LB4100l4 Below Beta bkg 19-Sep 06:29 60 0.933 0.958 1.734 -3.19 LB410014 Below Beta eff 19-Sep 08:19 5 20182 20380 21610 -3.97 PIC3A Below Beta XTalk 11 : 18 5 0.002 0.011 0;029 -6.20 PIC5B Above Alpha bkg 19-Sep 09:38 60 0.317 0.107 0.374 +1.72 PIC6D Missing Beta eff . 19-Sep 06:44 5 1.523 43700 47280 -76.24 PIC6D Missing Beta XTalk 19-Sep 06:44 5 0.500 -1.81E-3 0.004 +483.09 PIC8C Above Beta XTalk 19-Sep 11:14 5 0.001 5.46E-5 5.49E-4 +8.69 PIC12C Above Alpha bkg 19-Sep 08:38 60 0.433 0.010 0.413 ' +3.31 PIC13B Above Alpha bkg 19-Sep 07:22 60 134 -5.02E-2 0.412 +1,741.68 PIC13B Above Beta bkg 19-Sep 07:22 60 356 2.229' +947.11 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALl)Y ASSURANCE PARAMETERS Page 1of2 Page 5031 of 5809 The following detectors may not have properly transferred to the LIMS system
  • LB4100D1 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D2 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D3 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D4 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC6D Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg PIC13C Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by . Date Cf /;q /;6 GEL Laboratories LLC Page 2 of 2 Page 5032 of 5809 Gas Flow Proportional Counter Checks for 20-Sep-2016 Detectors LB4100 A1 through J4 and PIC 1A through 140 Short Name Status Parm name Run Time Count CPMor Low Limit High Limit Stdev Time dee LB4100B3 need 2nd Alpha bkg 20-Sep 05:02 60 0.233 0.121 0.383 -0.43 LB4100B3 Above Beta bkg 20-Sep 05:02 60 3.150 0.965 1.943 +10.41 LB4100C2 Above Alpha bkg 20-Sep 06:54 60 0.467 -4.14E-2 0.367 +4.47 LB4100C2 Above Beta bkg 20-Sep 06:54 60 2.350 0.561 1.662 +6.75 LB4100C4 Above Alpha bkg 20-Sep 05:03 60 0.350 4.08E-6 0.304 +3.91 LB4100C4 Above Beta bkg 20-Sep 05:03 60 2.117 0.686 2.113 +3.02 LB4100E2 Above Beta bkg 20-Sep 05:02 60 2.783 1.061 2.316 +5.23 LB4100E3 need 2nd Alpha bkg 20-Sep 06:45 60 0.100 -8.16E-2 0.346 -0.45 LB4100E3 Above Beta bkg 20-Sep 06:45 60 2.100 0.463 2.359 +2.18 LB4100E4 Above Beta bkg 20-Sep 05:02 60 2.417 0.650 2.302 +3.42 LB4100F1 Below Alpha eff 20-Sep 06:59 5 10662 10840 11730 -4.20 LB4100H4 Below Alpha eff . 20-Sep 06:18 5 10792 11490 13890 -4.75 LB4100H4 Above AlphaXTalk 20-Sep 06:18 5 0.405 0.307 0.379 +5.17 LB4100H4 Below Beta eff 20-Sep 06:28 5 34316 35210 36600 -6.86 LB410013 Above Beta bkg. 20-Sep 06:29 60 2.533 0.091 2.093 +4.32 LB410014 Below Alpha eff 20-Sep 06:05 5 11564 12310 13620 -6.42 LB410014 Below Alpha XTalk 20-Sep 06:05 5 0.187 0.189 0.219 -3.24 LB410014 Below Beta bkg 20-Sep 05:02 60 . 0.733 0.958 1.734 -4.74 LB410014 Below Beta eff 20-Sep 06:12 5 20093 20380 21610 -4.40 PIC2D Above Alpha bkg 20-Sep 13:16 60 0.383 0.006 0.407 +2.65 PIC3A Above Alpha XTalk 20-Sep 05:14 5 0.272 0.240 0.267 +4.17 PJC3A Below Beta XTalk 20-Sep 13:55 5 0.002 0.011 0.029 -6.23 PIC7D Above Beta XTalk 20-Sep 13:53 5 7.94E-4 1.40E-4 7.07E-4 +3.92 PIC8C need 2nd Beta XTalk 20-Sep 05:20 5 4.34E-4 5.46E-5 5.49E-4 +1.60 PIC10D . Above Alpha bkg 20-Sep 12:53 60 0.333 . -6.34E-2 0.362 +2.60 PIC10D Below Alpha eff 20-Sep 05:40 5 11941 15350 16570 -19.76 PIC10D Above AlphaXTalk 20-Sep 05:40 5 0.754 0.303 0.427 +18.80 PIC100 Above Beta bkg 20-Sep 12:53 60 1.417 -1.50E-1 1.265 +3.64 PIC10D Below Beta eff 20-Sep 05:52 5 3i566 40190 43320 -19.53 PIC11D Above Alpha bkg 20.-Sep 13:17 60 0.667 0.001 0.361 +8.10 Page 1 of 2 Page 5033 of 5809 PIC12C Above Alpha bkg 20-Sep 13:17 60 0.317 0.010 0.413 +1.57 PIC12C Above Beta eff 20-Sep 05:36
  • 5 27959 25610 26990 +7.21 PIC13B Above Alpha bkg 20-Sep 13:17 60 0.533 -5.02E-2 0.412 +4.57 PIC13B need 2nd Beta bkg 20-Sep 13: 17 60 1.817 -1.78E-2 2.229 +1.90 PIC14B Above Beta bkg 20-Sep 13:17 60 3.233 -1.34E-1 1.713 +7.94 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS The following detectors may not have properly transferred to the LIMS system LB4100D1 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB410002 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB41 OOD3 *Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB41 OOD4 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC6D Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC13C Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Date / f (Zo f !6 . GEL Laboratories LLC Page 2 of 2 Page 5034 of 5809 Gas Flow Proportional Counter Checks for 21-Sep-2016 Detectors LB4100 A1 J4 and PIC 1A through 140 Short Name Status Parmname Run Time Count CPMor Low Limit High Limit Stdev Time dee LB4100B3 Above Beta bkg 21-Sep 06:32 60 3.300 0.965 1.943 +11.33 LB4100C2 Above Alpha bkg 21-Sep 08:05 60 0.550 -4.14E-2 0.367 +5.69 LB4100C2 Above Beta bkg 21-Sep 08:05 60 1.733 0.561 1.662 +3.39 LB4100C4 Above Alpha bkg 21-Sep 06:29 60 0.367 4.08E-6 0.304 +4.24 LB4100C4 Above Beta bkg 21-Sep 06:29 60 2.500 0.6B6 2.113 +4.63 LB4100E2 Above Beta bkg 21-Sep 06:27 60 2.733 1.061 2.316 +5.00 LB4100E3 Above Beta bkg 21-Sep 07:49 60 2.083 0.463 2.359 +2.13 LB4100E4 Above Beta bkg 21-Sep 06:27 60 2.500 0.650 2.302 +3.72 LB4100F1 Below Alpha eff 21-Sep 09:37 5 10529 10840 11730 -5.09 LB4100H4 Below Alpha eff 21-Sep 07:39 ' 5 10799 11490 13890 -4.73 LB4100H4 Above Alpha XTalk 21-Sep 07:39 5 0.405 0.307 0.379 +5.15 LB4100H4 Below Beta eff 21-Sep 07:31 5 34200 35210 36600 -7.36 LB410013 Above Beta bkg 21-Sep 08:18 60 2.283 0.091 2.093 +3.57 LB410014 Below Alpha eff 21-Sep 08:02 5 11663 12310 13620 -5.96 LB410014 need 2nd Alpha XTalk 21-Sep 08:02 5 0.189 0.1B9 0.219 -2.97 LB410014 Below Beta bkg 21-Sep 06:27 60 0.883 0.958 1.734 -3.58 LB410014 Below Beta eff 21-Sep 08:12 5 20027 20380 21610 -4.72 PIC1C Below Beta eff 21-Sep 11 :26 5 20723 21130 22410 -4.91 PIC3A Below Beta XTalk 21-Sep 09:42 5 0.002 0.011 0.029 -6.29 PIC8C Above Alpha bkg 21-Sep 09:00 60 0.317 0.105 0.367 +1.85 PIC10D Below Alpha eff 21-Sep 11 :OB 5 11758 15350 16570 -20.66 PIC10D Above Alpha XTalk 21-Sep 11 :OB 5 0.773 0.303 *0.427 +19.72 PIC10D Below Beta eff 21-Sep 06:53 5 32197 40190 43320 -18.32 PIC12D Above Alpha bkg 21-Sep 09:12 60 0.317 -3.91E-2 0.3B6 +2.02 PIC14B need 2nd Alpha pkg 21-Sep 08:20 60 0.150 -8.43E-2 0.377 +0.05 PIC14B Above Beta bkg 21-Sep 08:20 60 3.700 -1.34E-1 1.713 +9.46 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS Page 1 of 2 Page 5035 of 5809 LB4100D1 LB4100D2 LB4100D3 LB4100D4 PIC6D PIC13C The following detectors may not have properly transferred to the LIMS system Alpha bkg,.Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eft, Beta XTalk . Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by _tit_&Z_?:zL _____________ _ Date __ CJ_/_i1_/i_16 ___ GEL Laboratories LLC Page 2 of 2 Page 5036 of 5809 Gas Flow Proportional Counter Checks for 22-Sep-2016 Detectors LB4100 A1 through J4 and PIC 1A through 140 Short Name Status Parm name Run Time Count CPMor Low Limit High Limit Stdev Time dee LB4100B3 Above Beta bkg 22-Sep 05:50 60 2.967 0.965 1.943 +9.28 LB4100C1 Above Alpha bkg 22-Sep 07:45 60 0.333 0.149 0.367 +2.07 LB4100C4 Above Alpha bkg 22-Sep 05:52 60 0.400 4.08E-6 0.304 +4.89 LB4100C4 need 2nd Beta bkg 22-Sep 05:52 60 1.983 0.686 2.113 +2.45 LB4100E2 Above Beta bkg 22-Sep 05:50 60 2.783 1.061 2.316 +5.23 LB4100E3 Above Beta bkg 22-Sep 07:29 60 3.383 0.463 2.359 +6.24 LB4100E4 Above Beta bkg 22-Sep 05:50 60 2.467 0.650 2.302 +3.60 LB4100F1 Below Alpha eff 22-Sep 07:20 5 10642 10840 11730 -4.34 LB4100F1 Below Beta eff 22-Sep 07:37 5 45648 45650 49940 -3.00 LB4100H4 Below Alpha eff 22-Sep 07:1 O 5 10733 . 11490 13890 -4.89 LB4100H4 Above AlphaXTalk 22-Sep 07:1 O 5 0.407 0.307 0.379 +5.34 LB4100H4 Below Beta eff 22-Sep 07:20 5 34292 35210 36600 -6.96 LB410013 Above Beta bkg 22-Sep 05:51 60 2.383 0.091 2.093 +3.87 LB410014 Below *Alpha eff 22-Sep 06:56 5 11526 12310 13620 -6;59 LB410014 Below Alpha XTalk 22-Sep 06:56 5 0.186 0.189 0.219 -3.43 LB410014 Below Beta bkg 22-Sep 05:51 60 0.683 0.958 1.734 -5.12 LB410014 Below Beta eff 22-Sep 07:03 5 20177 20380 21610 -3.99 PIC1C Below Beta eff 22-Sep 06:05 5 20866 21130 22410 -4.24 PIC2D Above Alpha bkg 22-Sep 07:17 60 0.367 0.006 0.407 +2.40 PIC2D Above Beta bkg 22-Sep 07:17 60 2.150 1.126 2.275 +2.35 PIC3A Above Alpha bkg 22-Sep 06:14 60 0.417 -5.23E-2 0.356 +3.88 PIC3A Below Beta XTalk 22-Sep 05:56 5 0.002 O.Q11 0.029 -6.30 PIC5B Above Alpha bkg 22-Sep 07:35 60 0-400 0.107 0.374 +3.60 PIC8C Above Alpha bkg 22-Sep 07:33 60 0.350 0.105 0.367 +2.62 PIC9C Above Alpha bkg 22-Sep 07:42 60 0.317 -2.53E-2 0.365 +2.26 PIC10D Below Alpha eff 22-Sep 06:24 5 11811 15350 16570 -20.41 PIC10D Above AlphaXTalk 22-Sep 06:24 5 0.768 0.303 0.427 +19.46 PIC10D Below Beta eff 22-Sep 06:31 5 31926 40190 43320 -18.84 Page 1of2 Page 5037 of 5809 PIC11A Above Alpha bkg 22-Sep 08:13 60 0.350 0.029 0.365 PIC12A Above Alpha bkg 22-Sep 08:14 60 0.55Q 0.067 0.379 PIC12A need 2nd Beta bkg 22-Sep 08:14 60 1.367 0.288 1.844 PIC12C Above Alpha bkg 22-Sep 08:14 60 0.417 0.010 0.413 PIC12D Above Alpha bkg 22-Sep 08:14 60 0.367 -3.91 E-2 0.386 PIC13B Above Alpha bkg 22-Sep 08:14 60 0.317 -5.02E-2 0.412 PIC14B need 2nd Beta bkg 22-Sep 06:51 60 1.100 -1.34E-1 1.713 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS LB410001 LB4100D2 LB4100D3 LB4100D4 PIC6D PIC13C The following detectors may not have properly transferred to the LIMS system Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by---"-/-'-{,__* _-*a,,,_* "'_</WI__:_.'-""--______ _ Date ___ ____ _ GEL Laboratories LLC Page 2 of 2 Page 5038 of 5809 +2.74 +6.29 +1.16 +3.06 +2.73 +1.76 +1.01 Gas Flow Proportional Counter Checks for 23-Sep-2016 Detectors LB4100 A1 through J4 and PIC 1A through 140 Short Name Status Parmname Run Time Count CPM or Low Limit High Limit Stdev Time dee LB4100A3 Below Alpha eff 23-Sep 11 :36 5 8874 9142 11120 -3.81 LB4100B2 Below Alpha eff 23-Sep 07:02 5 7531 9043 10550 -9.02 LB4100B2 Above Beta bkg 23-Sep 11 :44 60 7.650 0.992 2.051 +34.73 LB4100B3 Below Alpha bkg 23-Sep 05:49 60 0.117 0.121 0.383 -3.10 LB4100B3 Below Alpha eff 23-Sep 07:02 5 9981 13770 17610 -8.92 LB4100B3 Above Alpha XTalk 23-Sep 07:02 5 0.567 0.308 0.393 +15.15 LB410083 Above Beta bkg 23-Sep 05:49 60 71.683 0.965 1.943 +430.94 LB4100B4 Below Alpha eff 23-Sep 07:02 5 11712 12260 14720 -4.34 LB410084 Above Alpha XTalk 23-Sep 07:02 5 0.361 0.273 0.337 +5.27 LB4100C1 Above Alpha bkg 23-Sep 05:53 60 0.350 0.149 0.367 +2.52 LB4100C3 Below Alpha eff 23-Sep 11 :18 5 5257 6624 9128 -6.28 LB4100C3 Above Alpha XTalk 23-Sep 11 :18 5 0.464 0.248 0.368 +7.79 LB4100C4 need 2nd Alpha bkg 23-Sep 05:53 60 0.250 4.0BE-6 0.304 +1.93 LB4100C4 Above Beta bkg 23-Sep 05:53 60 128 0.686 2.113 +533.03 LB4100E1 Above Beta bkg 23-Sep 10:56 60 15.517 0.637 2.392 +47.87 LB4100E2 Above Beta bkg 23-Sep 10:56 60 3.933 1.061 2.316 +10.73 LB4100E3 need 2nd Beta bkg 23-Sep 10:56 60 1.833 0.463 2.359 +1.34 LB4100E4 Above Alpha bkg 23-Sep 10:56 60 0.367 -6.65E-2 0.309 +3.92 LB4100E4 Above Beta bkg 23-Sep 10:56 60 4.750 0.650 2.302 +11.89 LB4100F1 Below Alpha eff 23-Sep 10:45 5 10371 10840 11730 -6.16 LB4100F1 Above AlphaXTalk 23-Sep 10:45 5 0.269 0.224 0.265 +3.54 LB4100F1 need 2nd Beta eff 23-Sep 10:37 5 45920 45650 49940 -2.62 LB4100F2 Above Beta bkg 23-Sep 10:57 60 2.133 0.575 1.803 +4.61 LB4100H4 Below Alpha eff 23-Sep 10:37 5 10800 11490 13890 -4.73 LB4100H4 Above AlphaXTalk 23-Sep 10:37 5 0.400 0.307 0.379 +4.75 LB4100H4 Below Beta eff 23-Sep 10:45 5 34315 35210 36600 -6.86 LB4100l3 Above Beta bkg 23-Sep 11 :09 60 2.183 0.091 2.093 +3.27 LB410014 Below Alpha eff 23-Sep 12:12 5 11515 12310 13620 -6.64 LB410014 Below Alpha XTalk 23-Sep 12:12 5 0.188 0.189 0.219 -3.05 LB410014 need 2nd Beta bkg . 23-Sep 05:49 60 1.083 0.958 1.734 -2.03
  • Page 1of2 Page 5039 of 5809 LB410014 Below Beta eff 23-Sep 07:02 5 20276 20380 21610 -3.51 PIC2D Above Alpha bkg 23-Sep110:36 60 0.583 0.006 0.407 +5.64
  • PIC2D Below Alpha eff 23-Sep 05:53 5 14713 16200 17080 -13.14 PIC2D Above Alpha XTalk 23-Sep 05:53 5 0.426 0.242 0.304 +14.87 PIC2D Below Beta eff 23-Sep 06:00 5 33508 39480 42300 -15.71 PIC3A Above Alpha XTalk 23-Sep 06:00 5 0.286 0.240 0.267 +7.29 PIC3A Below Beta XTalk 23-Sep 05:53 5 7.60E-4 0.011 0.029 -6.62 PIC5B Above Alpha bkg 23-Sep 10:34 60 0.317 0.107 0.374 +1.72 PIC10D Below Alpha eff 23-Sep 11 :51 5 11968 15350 16570 -19.63 PIC10D Above Alpha XTalk 23-Sep 11 :51 5 0.756 0.303 0.427 +18.85 PIC10D Below Beta eff 23-Sep 10:58 5 30970 40190 43320 -20.67 PIC12C need 2nd Alpha bkg 23-Sep 12:08 60 0.267 0.010 0.413 +0.83 PIC14D Above Beta eff 23-Sep 12:41 5 42592 40480 42120 +4.73 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS The following detectors may not have properly transferred to the LIMS system LB4100D1 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D2 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D3 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D4 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC6D Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC13C Alpha bkg, Alpha eff, lpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by Date GEL Laboratories LLC Page 2 of 2 Page 5040 of 5809 Gas Flow Proportional Counter Checks for 27-Sep-2016 , Detectors LB4100 A1 through J4 and PIC 1A through Short Name Status Parm name Run Time Count CPMor Low Limit ' High Limit Stdev Time dee LB4100A3 Below Alpha eff 27-Sep 06:17 5 8876 9142 11120 -3.81 LB4100B2 need 2nd Beta bkg 27-Sep 05:03 60 1.917 0.992 2.051 +2.24 LB4100B3 Above Alpha bkg 27-Sep 05:03 60 0.383 0.121 0.383 +3.0d LB4100C3 Below Alpha eff 27-Sep 06:46 5 5995 6624 9128 -4.51 LB4100C3 Above Alph;:iXTalk 27-Sep 06:46 5 0.416 0.248 0.368 +5.36 LB4100C4 Above Beta bkg 27-$ep 05:06 60 13.633 0.686 2.113 +51.42 LB4100E1 Above Beta bkg 27-Sep 05:03 60 8.733 0.637 2.392 +24.68 LB4100E2 Above bkg 27-Sep 05:03 60 3.217 1.061 2.316 +7.31 LB4100E3 Above Alpha bkg 27-Sep 05:03 60 0.350 -8.16E-2 0.346 +3.05 LB4100E3 Above Beta bkg 27-Sep 05:03 60 3.983 0.463 2.359 +8.14 LB4100E4 Above Beta bkg 27-Sep 05:03 60 2.417 0.650 2.302 +3.42 LB4100F1 Below Alpha eff 27-Sep 06:59 5 10464 10840 11730 -5.53 LB4100F1 Above Alpha XTalk 27-Sep 06:59 .5 0.268 0.224 0.265 +3.42 LB4100H4 Below Alpha eff 27-Sep 06:24 5 10622 11490 13890 -5.17 LB4100H4 Above Alpha XTalk
  • 27-Sep d6:24 5 0.418 0.307 0.379 +6.23 LB4100H4 Below Beta eff 27-Sep 06:31 5 34394 35210 36600 -6.52 LB410013 Above Beta bkg 27-Sep 05:03 60 2.450 0.091 2.093 +4.07 LB410013 Below Beta eff 27-Sep 06:17 5 17122 17160 17920 -3.30 LB410014 Below Alpha eff 27-Sep 06:10 5 11565 12310 13620 -6.41 LB410014 need 2nd Alpha XTalk 27-Sep 06:10 5 0.191 0.189 0.219 -2.52 LB410014 Below Beta bkg 27-Sep 05:03 60 0.767 0.958 1.734 -4.48 LB410014 Below Beta eff 27-Sep 06:17 5 20345 20380 21610 -3.17 PIC3A need 2nd Alpha XTalk 27-Sep 05:09 5 0.265 0.240 0.267 +2.75 PIC3A Below Beta XTalk 27-Sep 05:03 5 0.001 0.011 0.029 -6.40 PIC3D Above Alpha bkg 27-Sep 06:30 60 0.317 -6.75E-2 0.338 +2.69 PICSB Above Alpha bkg 27-Sep 06:38 60 0.383 0.107 0.374 +3.22 PIC5C Above Alpha bkg 27-Sep 06:39 60 0.350 -1.81E-2 0.382 +2.52 PIC7D Above Alpha bkg 27-Sep 07:40 60 0.383 -1.11E-2 0.349 +3.58 Page 1of2 Page 5041 of 5809 PIC10A need 2nd Alpha eff 27-Sep 05:27 5 8986 8854 10610 PIC10A Below Beta eff 27-Sep 05:34
  • 5 44152 44740. 53240 PIC10D Below Alpha eff 27-Sep 05:27 5 11828 15350 16570 PIC10D Above Alpha XTalk 27-Sep 05:27 5 0.771 0.303 0.427 PIC10D Below Beta eff 27-Sep 05:34 5 31335 40190 43320 PIC11A Above Alpha bkg 27-Sep 07:01 60 0.383 0.029 0.365 PIC12A Above Alpha bkg 27-Sep 07:02 60 0.333 0.067 0.379 PIC12C need 2nd Alpha bkg 27-Sep 05:51 60 0.283 0.010 0.413 PIC12C need 2nd Beta bkg 27-Sep 05:51 60 0.917 -3.86E-2 2.074 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS LB4100D1 LB4100D2 LB4100D3 LB4100D4 PIC6D PIC13C The following detectors may not have properly transferred to the LIMS system Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by /bi? Date q -d ') *-I G_ GEL Laboratories LLC Page 2 of 2 Page 5042 of 5809 -2.55 -3.42 -20.32 +19.62 -19.97 +3.34 +2.12 +1.07 -0.29 Gas Flow Proportional Counter Checks for 28-Sep-2016 Detectors LB4100 A1 through J4 and PIC 1A through 140 Short Name Status Parm name Run Time Count CPM or. Low Limit High Limit Stdev Time dee LB4100A3 Below Alpha eff 28-Sep 05:51 5 8875 9142 11120 -3.81 LB4100B3 need 2nd Alpha bkg 28-Sep 04:42 60 0.283 0.121 0.383 +0.71 LB4100C1 Above Alpha bkg 28-Sep 04:44 60 0.500 0.149 0.367 +6.64 LB4100C3 Below Alpha eff 28-Sep 06:22 5 6093 6624 9128 -4.27 LB4100C3 Above Alpha XTalk 28-Sep 06:22 5 0.409 0.248 0.368 +5.03 LB4100C4 Above Alpha bkg 28-Sep 04:44 60 0.483 4.08E-6. 0.304 +6.54 LB4100C4 Above Beta bkg 28-Sep 04:44 60 10.667 0.686 2.113 +38.95 LB4100E1 Above *Beta.bkg 28-Sep 04:42 60 6.400 0.637 2.392 +16.70 LB4100E2 Above Beta bkg 28-Sep 04:42 60 2.667 1.061 2.316 +4.68 LB4100E3 need 2nd Alpha bkg 28-Sep 04:42 60 0.067 -8.16E-2 0.346 -0.92 LB4100E3 Above Beta bkg 28-Sep 04:42 60 2.167 0.463 2.359 +2.39 LB4100E4 Above Beta bkg 28-Sep 04:42 60 2.433 0.650 2.302 +3.48 LB4100F1 Below Alpha bkg 28-Sep 04:42 60 0.033 0.059 0.384 -3.47 LB4100F1 Below Alpha eff 28-Sep 06:06 5 10556 10840 11730 -4.92 LB4100F1 Above AlphaXTalk 28-Sep 06:06 5 0.267 0.224 0.265 +3.21 LB4100F1 Below Beta eff 28-Sep 05:58 5 45647 45650 49940 -3.00 LB4100F2 Below Beta eff 28-Sep 06:40 5 18321 18400 19480 -3.44 LB4100H4 Below Alpha eff 28-Sep 05:58 5 10597 11490 13890 -5.23 LB4100H4 Above Alpha XTalk 28-Sep 05:58 5 0.416 0.307 0.379 +6.05 LB4100H4 Below Beta eff 28-Sep 06:06 5 34282 35210 36600 -7.00 LB410013 Below Beta eff 28-Sep 07:38 5 17015 17160 17920 -4.14 LB410014 Below Alpha eff 28-Sep 05:45 5 11386 12310 13620 -7.23 LB410014 Below Beta bkg 28-Sep 04:42 60 0.867 0.958 1.734 -3.70 LB410014 Below Beta eff 28-Sep 05:51 5 20161 20380 21610 -4.07 PIC2D Above Alpha bkg 28-Sep 04:57 60 0.350 0.006 0.407 +2.15 PIC3A Above AlphaXTalk 28-Sep 04:50 5 0.269 0.240 0.267 +3.61 PIC3A Beiow Beta XTalk 28-Sep 04:43 5 0.001 0.011 0.029 -6.43 PIC6B Above Beta bkg 28-Sep 07:34 60 2.083 0.657 2.252 +2.37 Page 1of2 Page 5043 of 5809 PIC8D Above Alpha bkg 28-Sep 06:20 60 0.317 0.004 0.401 +1.72 PIC9C Above Alpha bkg 28-Sep 06:44 60
  • 0.333 -2.53E-2 0.365 +2.52 . PIC9C Below Alpha eff 28-Sep 05:08 5 9732 9741 10420 -3.08 PIC10A Below Beta eff 28-Sep 05:16 5 44641 44740 53240 -3.07 PIC10D Below Alpha eff 28-Sep 05:08 5 12062 15350 16570 -19.17 PIC10D Above AlphaXTalk 28-Sep 05:08 5 0.737 0.303 0.427 +17.97 PIC10D Below Beta eff 28-Sep 05:16 5 32143 40190 43320 -18.42 PIC12C Above Alpha bkg 28-Sep 05:33 60 0.317 0.010 0.413 +1.57 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS The following detectors may not have properly transferred to the LIMS syste'm LB4100D1 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D2 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D3 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D4 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC6D Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC13C Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by /cf. Date q-.;;Jg-"-/Ui... GEL Laboratories LLC Page 2 of 2 Page 5044 of 5809 Gas Flow Proportional. Counter Checks for 29-Sep-2016 Detectors l.:84100 A1 through J4 and PIC 1A through 140 Short Name Status Parm name Run Time Count CPMor Low Limit High Limit Stdev Time dee LB4100A3 Below Alpha eff 29-Sep 06:35 5 8809 9142 11120 -4.01 LB4100B1 need 2nd Alpha bkg 29-Sep 06:49 60 0.233 -7.77E-2 0.363 +1.23 LB4100B1 *Above Beta bkg 29-Sep 06:49 60 1.700 0.703 1.635 +3.42 LB4100B2 Above Alpha bkg 29-Sep 05:20 60 0.317 0.096 0.359 +2.03 LB4100B3 Above* .Alpha bkg 29-Sep 05:20 60 0.383 0.121 0.383 +3.00 LB4100B3 Above Beta bkg 29-Sep 05:20 60 2.083 0.965 1.943 +3.86 LB4100C1 Above Alpha bkg 29-Sep 05:22 60 0.533 0.149 0.367 +7.55 LB4100C3 Below Alpha eff 29-Sep 07:05 5 5838 6624 9128 *4.88 LB4100C3 Above AlphaXTalk 29-Sep 07:05 5 0.421 0.248 0.368 +5.65 LB4100C4 *need 2nd Alpha bkg 29-Sep 05:22 60 0.283 4.08E-6 0.304 +2.59 LB4100C4 Above Beta bkg 29-Sep 05:22 60 7.850 0.686 2.113 +27.11 LB4100E1 Above Beta bkg 29-Sep 05:20 60 5.400 0.637 2.392 +13.28 LB4100E2 Above Beta bkg 29-Sep 05:20 BO 2.517 1.061 2.316 +3.96 LB4100E3 need 2nd Beta bkg 29-Sep 05:20 60 1.817 0.463 2.359 +1.28 LB4100E4 Above Beta bkg 29-Sep 05:20 60 2.333 0.650 2.302 +3.11 LB4100F1 need 2nd Alpha bkg 29-Sep 05:20 60 0.150 0.059 0.384 -1.32 LB4100F1 Below Alpha eff 29-Sep 06:52 5 10585 10840 11730 -4.72 LB4100F1 need 2nd Alpha XTalk 29-Sep 06:52 5 0.265 0.224 0.265 +2.97 LB4100F1 Below Beta eff 29-Sep 06:44 5 45465 45650 49940 -3.26 LB4100F2 Below Beta eff 29-Sep 06:44 5 18323 18400 19480 -3.43 LB4100H4 Below Alpha eff 29-Sep 06:44 5 10469 11490 13890 -5.55 LB4100H4 Above AlphaXTalk 29-Sep 06:44 5 0.413 0.307 0.379 +5.83 LB4100H4 Below Beta eff 29-Sep 06:52 5 34209 35210 36600 -7.32 LB410013 Below Beta eff 29-Sep 07:14 5 17033 17160 17920 -4.00 LB410014 Below Alpha eff 29-Sep 06:26 5 11442 12310 13620 -6.98 LB4100l4 Below Beta bkg 29-Sep 05:20 60 0.700 0.958 1.734 -4.99 LB410014 Below Beta eff 29-Sep 06:35 5 20152 20380 21610 -4.11 PIC1C Below Beta eff 29-Sep 07:00 5 21059 21130 22410 -3.33 Page 1of2 Page 5045 of 5809 PIC2D Above Alpha bkg 29-Sep 05:35 60 0.350 0.006 0.407 +2.15 PIC3A need 2nd Alpha XT alk
  • 29-Sep 05:28 . 5 0.266 0.240 0.267 +2.90 PIC3A Below Beta XTalk 29-Sep 05:20 5 0.001 0.011 0.029 -6.40 PIC5B Above Alpha bkg 29-Sep 06:57 60 0.350 0.107 0.374 +2.47 PIC6B Below Alpha eff 29-Sep 05:33 5 9422 9451 9758 -3.57 PIC6B Above Beta bkg 29-Sep 08:31 60 2.150 0.657 2.252 +2.62 PIC9C Above Alpha bkg 29-Sep 07:16 60 0.400 -2.53E-2 0.365 +3.55 PIC9C need 2nd Alpha eff 29-Sep 05:47 5 9861 9741 10420 -1.94 PIC10D Below Alpha eff 29-Sep 05:47 5 12052 15350 16570 -19.22 PIC10D Above AlphaXTalk 29-Sep 05:47 5 0.747 0.303 0.427 +18.43 PIC10D Below Beta eff 29-Sep 05:55 5 32414 40190 43320 -17.91 PIC11D Above Alpha bkg 29-Sep 07:19 60 0.367 0.001 0.361 +3.10 PIC11D need 2nd Beta bkg 29-Sep 07:19 60 1.200 -2.33E-1 2.356 +0.32 PIC12C Above Alpha bkg 29-Sep 06:13 60 0.417 0.010 0.413 +3.06 PIC14B Above Alpha bkg 29-Sep 06:13 60 0.350 -8.43E-2 0.377 +2.65 PIC14D Above Alpha bkg 29-Sep 08:34 60 0.317 0.120 0.376 +1.61 INSTRUMENTS NOT LISTED HAVE PASSED ALL QUALITY ASSURANCE PARAMETERS The following detectors may not have properly transferred to the LIMS system LB4100D1 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D2 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D3 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk LB4100D4 Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC6D Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk PIC13C Alpha bkg, Alpha eff, Alpha XTalk, Beta bkg, Beta eff, Beta XTalk Reviewed by if Date q.(;;/Jf-ILR_ GEL Laboratories LLC Page 2 of 2 Page 5046 of 5809 Page 5047 of 5809 Background and Efficiency Data 0.36 0.32 0.27 0.23 0.. 0.19 u 0.14 0,0986 0.0546 0.01049 -0.0336 LB410081 ALPHA EFF 12140 11982 11824 11666 11508 0.. 11350 u 11192 11034 10876 10718 0.23 0.22 0.21 0.2 0.19 0.18 0.17 0.16 0.15 LB410081 BETA BKG 1.64 +3 Sigma 1.64 1.54 1.45 1.36 1.26 1.17 0.. 1.08 u 0.98 lj \ A f I 1l I} j ! At / v1 I! \ +2 Sigma 1.48 Mean 1.17 0.89 -2 Sigma 0.86 0.8 -3 Sigma 0.7 Page 5048 of 5809 59460 58768 58076 f----------------41-------------+----------------------------+-*2Sigma58306 57384 0.. 56692 u 56000 55308 54616 53924 53232 e Denotes Outlier Page 5049 of 5809 0,3 0.26 0.23 0.19 0. 0.16 () 0.12 0.0888 0.05404 0.0192 -0.0156 LB410084 ALPHA EFF 14720 14474 14228 13982 13736 0. 13490 () 13244 12998 12752 12506 0.34 0.33 0.32 0.32 0.31 0,3 0.3 0.29 0.29 0.28 LB410084 BETA BKG 1.97 +3 Sigma 1.97 1.87 +2 Sigma 1.8 1.77 1.67 1.57 1.47 0. 1.38 () 1.28 1.18 0 1 n A I \ I\ r h u v v rv \ \ v l \ N I \ \ 1/ v A ,, II Mean 1.47 -2Sigma1.14 1.08 -3 Sigma 0.98 Page 5050 of 5809 41960 41543 41126 40709 0.. 40292 (.) 39875 39458 39041 38624 38207 0.000287 0.000268 +2 Sigma 00 f I\ {'., I\ v In f N I nM '1 ii \ ,I II v \ A j\ 0.000249 0.00023 0.0002106 0.000192 Mean 00 0.000173 0.000153 0.000134 -2 Sigma 00 0.000115 -3 Sigma 00
  • Denotes Outlier 5051 of 5809 LB4100C2 ALPHA BKG Generated 0911912016 2 a.. 0 2 a.. 0 2 a.. 0 0.37 0.33 I r 0.29 0.24 0.2 u ! I\ A I I .M 0.16 0.12 . N I \ r, i i\J l f..-0.08102 0.04021 -0.000599 l/!l!!!#!!!i!!l!iiillllllllllllilif !lllllif DATE LB4100C2 ALPHA EFF 13710 13453 13196 12939 12682 12425 12168 11911 11654 11397 0.29 0.28 0.28 0.27 0.26 0.25 0.25 0.24 LB41 OOC2 BET A BKG 1.66 1.55 1.44 1.33 1.22 1.11 0.89 0.78 0,67 Page 5052 of 5809 +3 Sigma 0.37 +2 Sigma 0.3 Mean 0.16 -2 Sigma 0.03 -3 Sigma-0.041 20560 20102 19644 19186 0.. 18728 (.) 18270
  • 17812 17354 16896 16438 0.00046 +3 Sigma 00 0.0004251 +2 Sigma 00 A ,/ l 1\j ni I !' r J {\ J V I 11 11f '1 " 0.0003902 0.000355 0.0003205 0.000286 Mean 00 0.0002508 0.000216 0.000181 -2 Sigma 00 0.000146 -3 Sigma 00
  • Denotes Outlier Page 5053 of 5809 LB41 OOF2 ALPHA BKG 0.38 0.34 0.3 0.26 a.. 0.22 () 0.18 0.14 0.0987 I ! A I/ I \ I\ i 0.0589 0.0191 LB41 OOF2 ALPHA EFF 7273 7130 6980 6830 6680 a.. 6537 () 6390 6240 6100 5950 0.43 0.42 0.4 0.39 0.36 0.34 0.33 0.31 LB41 OOF2 BETA BKG 1.8 1.68 v 1.56 1.43 1.31 1.19 a.. 1.07 () 0.94 I /:\ II Ir ! T'I v wi I I 1/ 0.82 0.7 Page 5054 of 5809 !I 'Ii rl 1/U II J t 1! t t v .! IL L u HV .!'\ Generated 0912212016 +3 Sigma 0.38 +2 Sigma 0.31 Mean 0.18 N \Uvl -2 Sigma 0.05 -3 Sigma -0.021 +3 Sigma 1.8 +2Sigma1.6 Mean 1.19 w v -2 Sigma o. 78 -3 Sigma 0.57 19480 19372 19264 19156 0.... 19048 (.) 18940 18832 18724 18616 18508 0.000594 0.000553 +2 Sigma 00 0.000512 0.000471 Jn.! ! h \I r1 II l! II I\ v I A 1, JI v 'l \ 0.00043004 0.0003891 Mean 00 0.0003481 0.00030707 0.0002661 -2 Sigma 00 0.0002251 -3 Sigma 00
  • Denotes Outlier Page 5055 of 5809 LB41 OQF3 ALPHA BKG. Generated09/22/2016 ,---------------------------------------------------------t.---+3Sigma0.41 0.41 0.37 0.33 0.28 0.. 0.24 () 0.2 0.16 0.11 0.070052 0.0272 t--+r-r--+---+-+--+r--+---+-+--+-.--+---+-+--+-f--+---+-+--+--f-+--+-f--+--f-+--+-+--+--f-+--+-f--+--f-+--+-+--+--3 Sigma-O.D16 LB41 OOF3 ALPHA EFF '-r-----------------------------------------------------------+3Sigma20450 20450 20108 19766 19424 19082 0.. 18740 () 18398 18056 17714 17372 f--+--f-+---+-+--+r-r--+---+-+--+-+--+-f--+---+-+--+-f--+---+-+--+-f--+--f-+---+-+--+-f--+---+-+--+-+--+-r-'---+---+--3 Sigma 17030 0.33 0.32 0.32 0.31 0.3 0.3 0.29 0.28 0.28 0.27 LB41 OOF3 BETA BKG 2.22 2.07 1.93 r------------------,-------------...--------------------------fi-----+2Sfgma 1.98 1.79 1:65 1.51 0.. *1.36 () 1.22 1.08 0.94
  • Denotes Outlier Page 5056 of 5809 29370 29110 28850 28590 0.. 28330 () 28070 27810 27550 27290 27030 0.000363 +3 Sigma 00 0.000334 +2 Sigma 00 0.0003058 0.00022 n ,/ I I I j W A\ I '\ " 1} ! 1/ l J v v \ II 0.000277 0.000249 Mean 00 0.000191 0.000163 0.000134 -2 Sigma 00 0.0001053 -3 Sigma 00
  • Denotes Outlier Page 5057 of 5809 0.41 0.36 0.32 0.28 0... 0.23 () 0.19 0.15 0.1 0.05906 0.0157 LB41 OOF4 ALPHA EFF 10580 10400 10185 9990 9790 0... 9590 () 9395 9200 9000 8800 0.55 0.53 0.51 0.48 0.46 0.44 0.41 0.39 0.37 l--l--+-l--1---+--l--l--+-l--l--+-l--l--+-l--l--+-l--l--+-l--l---+----l'--+--+---l-+--+---ll--l---+----ll--l---+--l--l--+---ll--l--+-l-+---3 Sigma 0.35 LB4100F4 BETA BKG 2.67 2.46 2.25 2.04 1.83 1.62 0... 1.41 () 1.19 0.98 0.77 Page 5058 of 5809 39550 LB41QQF4 BETA EFF Generated09/22/2016 39135 38720 r----------------------------------------------------------+2Sigma38852 38305 a.. 37890 (.) 37475 37060 36645 36230 35815 0.00029 +3 Sigma 00 0.000269 +2 Sigma 00 0.000248 MA 11\1 A if / IV 1 I I '\ I I
  • I\ 1y rJ v II 1 ll 0.000228 0.000207 0.000186 Mean 00 0.000166 0.0001451 0.000124 -2 Sigma 00 0.0001038 -3 Sigma 00
  • Denotes Outlier Page 5059 of 5809 LB41 OOG2 ALPHA BKG Generated 09/2212016 0.3 +3 Sigma 0.3 0.26 +2 Sigma 0.24 0.23 0.19 a.. 0.15 0 0.12 Mean 0.12 0.0795 0.0424 0,00536 -2 Sigma -0.007 -0.0317 -3 Sigma -0.069 <§> ti' #° ,§> .@ kl R & <§> r!!? ,§> ,§> :;, ::? kl ::: R § <!§ & <!§ ,;:-"' "' "' t "' §? <!§ 91' 91' w " c:s &' c:s &' c:s c:s c:s c:s c:s &' &' .@ <:> " " " " " " " " DATE LB41 OOG2 ALPHA EFF 12310 +3 Sigma 12310 12093 +2 Sigma 12000 11876 11659 11442 a.. 11225 Mean 11230 0 11008 10791 10574 -2Sigma10500 10357 -3 Sigma 10140 <§> !? &' &' .@ :;, :;, :;, kl kl & &' <§> r!!? .@ :;, ::? kl ::: !? §? §? <!§ <!§ <& <!§ "' "' "' "' "' "' "' "' t "' "' §? 91' 91' 91' " &' &' &' c:s c:s c:s c:s c:s " " &' " "' " " "' &' "' c:s " " " .@ " " " " " " " .@ " DATE LB41 OOG2 ALPHA EFF Cross Talk 0.37 +3 Sigma 0.37 0.35 +2 Sigma 0.34 0.34 0.33 0.31 0.3 Mean 0.3 0.29 0.27 0.26 -2 Sigma 0.26 0.25 -3 Sigma 0.23 <§> " ,§> &' :;, :;, :;, :;, kl kl CJ ti ,§> ,§> :;, /!! §? <& <& t "' 91' if} 91' if;' " &' &' "' &' "' c:s "' "' "' " "' "' "' &> "' &' &' &' "' " " " " " " " " " DATE LB4100G2 BETA BKG 1.71 +3 Sigma 1.71 1.61 +2 Sigma 1.54 1.51 1.41 1.31 1.2 Mean 1.2 a.. 1.1 0 0.9 -2 Sigma 0.87 0.8 -3 Sigma 0.7 <§> ti' ,§> kl !? & <§> r!!? ,§> :;, ::? kl ::: !? B' <& <& Sf ,;:-"' §? if} if} 91' " "' "' "' &' c:s " "' &' &' &' "' &' "' .@ <:> " " " " " " .@
  • Denotes Outlier DATE Page 5060 of 5809 LB41 OOG2 BET A EFF Generated 09/2212016 18500 +3Sigma18500 18400 +2 Sigma 18300 18300 18200 0.... 18100 (...) 18000 Mean 18000 17900 17800 17700 -2Sigma17700 17600 -3 Sigma 17500 rf? & #' <!;> ll!l I O; f3> & ,§' "" .':? (:? ::: !? R iii & & & "" iii @ .§' & <§' <§' 8' 8' " "' @ "' <:) <:) <:) " " <:) " DATE LB4100G2 BETA EFF Cross Talk 0.0004303 +3 Sigma 00 0.0003991 +2Sigma00 0.000368 0.000337 0.0003054 0.000274 Mean 00 0.000243 0.000212 0.0001805 -2 Sigma 00 0.000149 -3 Sigma 00 rf? & l .§' "" "" "" (:? .'?! !? ,y !J O; f3> &' & & .§' "" .':? ::: rJ R iii "" "" ,§ "" iii iii ;!;;:-iii iii iii iii iii iii iii <§' <§' <§' <:) "' "' "' & "' "' " " .§' "' " " " " c§:i c§:i c§:i c§:i .§' "' "' "' & " " <:) " " <:) <:) " " DATE
  • Denotes Outlier Page 5061 of 5809 0.39 LB41 OOG3 ALPHA BKG Generated 0912212016 +3 Sigma 0.39 0,35 +2 Sigma 0.33 0.32 0.29 0.... 0.26 u 0.22 0.19 0.16 0.12 0.09066 '\ Ii w I \ II n I I \ I\ j i I n v u w j 1 N \ Ll 11,r 1* d' ll .A.! /I l/\ Mean 0.22 -2 Sigma 0.11 -3 Sigma 0.06 LB4100G3 ALPHA EFF 8415 8290 8170 8050 7930 0.... 7810 u 7680 7560 7440 7320 LB41 OOG3 BET A BKG 1.89 1.76 1.63 1.51 1.38 1.25 0.... 1.12 u 0.99 0.87 0.74 Page 5062 of 5809 0.. () 24390 LB41QQG3 BETA EFF Generated09/22/2016 .---------....::...--------------------------------------------------+3Sigma24390 24158 23926 23694 23462 23230 22998 22766 22534 22302 .. lillli-*et---+--+-t-+--+---l-+--+----l-+--+--*-+--+--+-t-+--et----l-+--+----l-+-9HH-+--+---+-+--+-et-*t-+--e----l-+--+--3 Sigma 22010 i/tl!l!!!!!iiii!!lillillilllilllill!lfllllill DATE LB4100G3 BETA EFF Cross Talk 0.000368 +3 Sigma 00 ! 0.000335 +2 Sigma 00 0.000173 t J 1/ 1! n i I \ ti I\ !i v \ v II \ ll' i 1 lj w 0.0003026 0.0002701 0.000238 0.00020507 Mean 00 0.00014002 0.0001075 -2 Sigma 00 0,000075 -3 Sigma 00
  • Denotes Outlier Page 5063 of 5809 0.27 LB41 OOG4 ALPHA BKG Generated 09/2212016 +3 Sigma 0.27 0.23 ! +2 Sigma 0.21 0.2 0.17 0.. 0.14 () 0.11 0.0776 0.0462 0.0149 A II I h r \ J !I l r lj I/ M ) !A i,, I II if ll \ Mean 0.11 -2 Sigma OD -0.0165 -3 Sigma -0.048 LB41 OOG4 ALPHA EFF 11250 11090 10930 10770 10610 0.. 10450 () 10290 10130 9970 9810 0.3 0.29 0.28 0.27 0.26 0.25 0.24 0.23 0.22 0.21 LB41 OOG4 BETA BKG 1.62 1.5 1.39 1.28 1.17 1.06 0.. 0.95 () 0.84 0.73 0.62 Page 5064 of 5809 22500 LB41 QQG4 BET A EFF Generated 0912212016 ,-----------=------------------------------------.... --------.... ----+3Sigma22500 22240 21980 t----------------------------------------------+---------+----+2Sigma22100 :2! 21720 a.. 21460 (.) 21200
  • 20940 20680 20420 20160 A II J u '.\ I v +2 Sigma 00 0.00025 0.000227 0.0002038 0.0001807 0.000158 0.000135 Mean 00 0.000112 0.0000885 0.0000655 -2 Sigma 00 0.0000424 -3 Sigma 00
  • Denotes Outlier Page 5065 of 5809 LB41OOH1 ALPHA BKG 0,39 0,35 0.31 0.27 a.. 0.24 u 0.2 0.16 111 _ / 111 wl rl! ! A ii y i v II Ir 0.12 0.084 0.0462 LB41 OOH1 ALPHA EFF 11440 11379 11318 11257 11196 a.. 11135 u 11074 11013 10952 10891 Ii /u ti 'h I II! WI ll I Generated 0912212016 ll +3 Sigma 0,39 +2 Sigma 0.32 Mean 0.2 * -2 Sigma 0.07 -3 Sigma 0.01 0.24 0.23 0.23 0.22 0.22 0.21 0.2 0.2 0.19 0.18 LB4100H1 BETA BKG 1.69 1.57 1.46 1.34 1.22 1.1 a.. 0.99 u 0.87 0.75 0,63 Page 5066 of 5809 45406 0.0002107 +2 SigmaOO 0.000195 0.00018 v I N ! 1! I '\ *11 t 1n I I\ I I 1 0.000164 0.000148 Mean 00 0.000133 0.000117 0.0001016 -2 Sigmaoo 0.00008603 -3 Sigma 00
  • Denotes Outlier Page 5067 of 5809 0.35 0.31 0.27 2 0.23 0.... 0.19 (.) 0.15 0.11 0.0738 0.0349 -0.004 LB41 OOH3 ALPHA EFF 20870 20626 20382 20138 2 19894 0.... 19650 (.) 19406 19162 18918 18674 0.29 0.29 0.29 0.28 0.28 0.27 0.27 0.27 LB41 OOH3 BET A BKG 2.02 1.9 1.79 1.67 1.56 2 1.44 0.... 1.33 (.) 1.21 1.1 0.98 Page 5068 of 5809 21908 21796 21572 t-+--+---i-+-+--+-f-+--+---i-+--+--+---if-+--+---+-f-+--+---i-+--+---+-f--+--+-l-tl+--+--+-f--+--+---i,.._+--+---+*t-+---1'---<9-+--+--+-3 Sigma 21460 0.000337 +3 Sigma 00 0.00030941 +2 Sigma 00 0.000282 0.000255 \J '!1 M 1/ I " I I v *1 .I v N I II ! ii 0.000228 0.00020023 Mean 00 0.000173 0.000146 0.000118 -2 Sigma 00 0.00009105 -3 Sigma 00
  • Denotes Outlier Page 5069 of 5809 LB41 QQJ1 ALPHA BKG Generated09/19/2016 -,----===-_:__:__:__:__:__:_:_:==---=-...::.::._:_:__:_:_:_ ________ .... __________________ _._,_ ______ +3 Sigma 0.38 0.38 0.33 0.29 2 0.24 0.. 0.2 u 0.15
  • 0.11 0.0653 0.02075 -0.0238 t--+--+-t--+---t-+--+--tf-+--+-t--+--+-t--+--+-t--+--+-+--+---t-+--+--t-+--+--tf-+--+-t--+--+-+--+---t-+--+--tf-+--+-t---3 Sigma -0.068 LB4100J1 ALPHA EFF 11920 11799 11678 11557 2 11436 0.. 11315 u 11194 11073 10952 10831 0.18 0.18 0.17 0.17 0.16 0.16 0.15 0.15 LB4100J1 BETA BKG 1.82 1.66 1.49 1.33 1.17 2 1.01 0.. 0.85 u 0.69 0.53 0.36 Page 5070 of 5809
2! a.. () 44720 LB41QQJ1 BETA EFF Generated09/19/2016 ,---------....::..-=-....::..----------------------------------------------+3Sigma44720 44445 44170 43895 43620 43345 43070 42795 42520 42245 t--+--+---+-+---+---+-l--+--+---+-+--+---+->-+--+---+-+--+---+->--+--+---+-+--+---+ ..... +--+--+---+-+--+---+-<10--+--+---+._+--+---+0-+--+---+--3 Sigma 41970 0.000275,------------------------------------------+I0----.._------------*3Sigma00 0.0002521 t-----+----------------------lf-----------------!!f-----++-------------+2Sigma00 0.0002291 0.000090908 r--------------------------------------------+---------------*2Sigma 00 0.0000679 t-+--t---t-t--+--+---+-+---t---t---,r--t--t---t-t--t--t---t-t--+--+--+t--t--t---t-+---t--+--+t-+--t--+-t--t--t---t-+--+--+-t--t--t---t-+--+--3Sigma00
  • Denotes Outlier Page 5071 of 5809 0.44 0.39 t-----------------------------------------------it-----------+2Sigma0.36 0.34 0.29 0... 0.25 u 0.2 0.15 0,0977 0.0484 -0.000962 t-+--+-t-+--+-+--+---+-+--+--+-+--+--+-+--+--+-+--+--+-+--+---l-+--+---l--t--+---l--t--+---l'--t--+---lt-+--+-t-+--+-+--+--+-3 Sigma -0.05 LB41 OOJ2 ALPHA EFF 10310 10200 10200 10100 10100 0... 9997 u 9930 9870 9810 9750 0.16 0.16 0.16 0.15 0.15 0.14 0.14 0.14 LB41 OOJ2 BETA BKG 1.34 1.25 1.16 1.07 0.98 0.9 0... 0.81 u 0.72 0.63 0.54 Page 5072 of 5809 18120 LB41QQJ2 BETA EFF Generated09/19/2016 ,---------=--=--=--=--=--=--=------------------------------e--------------e,_ ___ +3Sigma18120 17954 17788 t-----------------------------------------+-------------j!----+2Sigma17842 17622 0... 17456 u 17290 17124 16958 16792 16626 l---+---+-+--t-... l---+---+-+---+-+--+---+-+---+-+--+---+-+---+-+--+-l---+---+-+--+-l---+-._,-+---+-l---+---+--e---tt-t--t--l---+---+-3Sigma16460 0.000654 +3SJgmaOO 0.0006081 +2 Sigma 00 J " l I I I I ,/ I iv L I n l'y f) r " ' I' I y Ir' N I \ 0.000563 0.000517 0,000472 0,000426 Mean 00 0.0003807 0.000335 0.00029 -2 Sigma 00 0,000244 -3 Sigma 00
  • Denotes Outller Page 5073 of 5809 PIC1 QA ALPHA BKG Generated09/19/2016 0.33 0.29 0.25 0.21 0.... 0.17 (.) 0.13 0.0933 0.0541 0.0149 -0.0242 l-+--+-+--+-+--+-+-+-f--+--l-+--+-+-+--+-+--+-+--l--f--+--l-+--+-+-+-l'--+--+-+--+-+-+-l-+--+-+--+-+---3SJgma-0.063 PIC10A ALPHA EFF 10610 10400 10300 10100 9910 0.... 9732 (.) 9560 9380 9210 9030 0.68 0.63 0.58 0.53 0.43 0.38 0.33 0.27 PIC10A BETA BKG 1.17 .--.... --------tl>------------.... --it-----------------------------------+3Sigma1.17 1.04 0.95 0.91 0.77 0.64 0.5 0.... 0.37 (.) 0.24 0.1 f-----------------------------------------------------------2Sigma0.06 -0.0318 f-+--+-f-+--+-+-+-1-+--l--11-+--+-l-+--+-f-+--+-t-+--+-t-+--+-t--+--t-+--+---+-+--l--l--t--+---,r--t--+-t--+--t--3Sigma-0.166 Page 5074 of 5809 PIC1 QA BETA EFF Generated09/19/2016 53240,----------'------------------------------------------------+3Sigma53240 f-+-+--i-+--+-+--i-+--+-+--i-+-+-+--i-+--+-+--i'--+--+---+-t-+-+--i-+--+-+--i-+-+-+--i-+--+-+--i--H>-t---+-t-**IHlt--3Sigma44740 0.0002063 0.0001704 0.000152 0.000117 0.0000987 0.0000628
  • Denotes Outlier Page 5075 of 5809 0,33 PIC1 OB ALPHA BKG Generated09/28/2016 ____ +3S!gma0.33 0.29 0.25 t--+---1-+------1:-lr-------------------------r--------ll--Jt--------H-----+2S!gma0.27 0.22 0.. 0.18 (.) 0.15 . 0.11 0.0736 0,0377 0,00174 t--+---+-+---+-t--+---+--+--+-t--+---+-+---+-;-+--+-t--+---+--+--+---it--+--+-+--+--;--t--+-t--+---+--+--+-t--+---+-+---+-1----3 Sigma -0.034 PIC10B ALPHA EFF PIC10B BETA BKG 1.47 1.33 1.2 1.06 0.92 0.78 0.. 0.64 (.) 0.51 0.37 0.23 Page 5076 of 5809 0... 0 PIC1QB BETA EFF Generated09/28/2016 22710,----------------------------------------------------------+3Sigma22710 22320 19200 +--+---+-+--+--+-+--+-+--+---+-+--+--+--++--+-+--+---+-+--+-+--+---+-+--+-+--+---+-+--+--+--++--+-+--+---+-+--+-+--+-e-!--3 Sigma 18810 PIC10B BETA EFF Cross Talk 0.001101,..--------e---------------------------------------------------+JSigmaOO 0.000996 0.000785 0.000679 0.000469 0.000363 0.000258 +----------------------------------------------------------*2Sigma00 0.000152
  • Denotes OuUier Page 5077 of 5809 0.3 PIC1 OC ALPHA BKG Generated 0913012016 +3Sigma 0.3 0.26 0.23 0.19 a.. 0.15 () 0.12 0.0837 I I J I JI iu '\ A r I I I Ir i *1 N F
  • I \ +2 Sigma 0.24 Mean 0.12 0.0483 0.0129 -2 Sigma 00 -0.0226 -3 Sigma -0.058 PIC1 OC ALPHA EFF 21110 20798 20486 20174 19862 a.. 19550 () 19238 18926 18614 18302 0.5 0.48 0.45 0.42 0.4 0.34 0.32 0.29 0.26 PIC10C BETA BKG 1.49 1.32 r--+-itt-t-----------+---lf-t------tt---tr-+----t-t-Hr-Jt----t--_,H------------t-+-------+2Sigma1.22 1.16 01 0.84 0.67 a.. 0.51 () 0.35 0.19 f----------------------------------------------------------*2Sigma0.13 0.0249 f-+--+--t-+--+--+-f-+--+--t-+--+--+---1f-+--+--+---1-+--+--+---1f--t--+--+-f-+--+--+-t-+--+--t-+--+--+-f-+--+--+-+-+--+---1f-+--3Sigma-0.137 Page 5078 of 5809 PIC1 QC BETA EFF Generated09/30/2016 26880,-----------=--------.-----------------------------------------+3Sigma26880 26549 26218 r-----------------++---,----------------------------------------*2Sigma26300 25887 25556 24894 24563 0.0005503 0.000465 0.000293 0.0002076 0,00003621
  • Denotes Outlier Page 5079 of 5809
?! 0. (.) :?! 0. (.) :?! 0. (.) 0.36 0.32 0.28 0.23 0.19 0.15 0.11 0.0642 0.0216 -0.0209 II ill PIC1 OD ALPHA EFF PIC10D BETA BKG 1.27 -.----..--------------------------------.----------------------+3Sigma1.27 1.12 0.98 t----t+-----------------+---------------++-----------------J'c----+2Sigma 1.03 0.84 0.7 0.56 0.42 0.27 0.13 l-----------------------------------------------------------2Sigma0.09 -0.00877 -3 Sigma-0.15 .§> ::.> .'!} ::0 rfi !9' & ¢;-"' fl tP !? j ,§' .f!J :!!! l !! $ "' ::.> .'!} ii} ii} ii} ii} c;§i c;§i <'!? <'!? &' " " " " " " " " " " " " " <:> <:> " "' <:>
  • Denotes Outller DATE Page 5080 of 5809 43320 43007 42694 42381 0... 42068 (.) 41755 41442 41129 40816 40503 .ffe <? llll 0.000746 0.000674 0.0006022 0.0005305 0.000459 0.000387 0.000315 0.000244 0.0001721 0.0001004 -3 Sigma 00 ::? ::? ,f!! ,p ti) & l'2 & f2 ,§> ::i-::? rV' ,§> ::? .ffe ,, ,, ,, ,, iii iii ;:-t:-t:-iJ .# " iJ '"' '"' '"' '"' '"' !;? §' "' "' "' " "' <> <> <i <> <> <> <> <> " .§' "' " "' "' .§' " .§' " .§' <:> <:> <:> <> DATE e Denotes Outlier Page 5081of5809 PIC11A ALPHA BKG Generated 09/2812016 +3 Sigma 0.36 0.36 0.33 +2 Sigma 0.31 0.3 0.26 0... 0.23 . (.) 0.2 0.16 0.13 , I\ \ I A } 1A l h ' :l 11 j I\ I ii j f v u Mean 0.2 0.0964 -2 Sigma 0.09 0.0629 -3 Sigma 0.03 PIC11A ALPHA EFF 11180 11129 11078 11027 10976 0... 10925 (.) 10874 10823 10772 10721 0.34 0.33 0.32 0.31 0.3 0.29 0.28 0.27 0.26 0.25 PIC11A BETA BKG 1.7 1.52 1.35 1.17 01 0.82 0... 0.65 (.) 0.47 0.3 0.12 Page 5082 of 5809 PIC11 A BETA EFF Generated09/28/2016 216B0,----------"-"-"=--=-----------------------------------------------+3Sigma21680 a.. (.) 21561 0.00052 0.000476 0.000433 0.00039 0.000346 0.00030304 0.00026 0.000216 0.000173 e Denotes Outlier Page 5083 of 5809 H ! \1 \ " I\ I +2 Sigma 00 N\1 .! Mean 00 I I 11 \I I l -2 Sigma 00 -3 Sigma oo 0.36 PIC11 B ALPHA BKG Generated 09128/2016 +3 Sigma 0.36 0.32 +2 Sigma 0.29 0.28 0.24 0... 0.21 u 0.17 0.13 0.0917 0.0536 1f II II 'I ii ! {Al I r h J 'j II L . y N I Mean 0.17 -2 Sigma 0.04 0.0155 -3 Sigma -0.023 PIC11B ALPHA EFF 13790 , +3 Sigma 13790 13751 13712 13673 13634 0... 13595 1 Kl J ) " 1r \ \ +2 Sigma 13700 Mean 13590 u 13556 13517 13478 J I I fl II J v I -2 Sigma 13500 13439 -3 Sigma 13400 0.28 +3 Sigma 0.28 0.28 +2 Sigma 0.28 026 0.27 I \ I' I\ v '\! .! A \! v I \ I I/ f 0.28 0.27 Mean 0.27 0.27 0.27 0.27 -2 Sigma 0.27 0.27 -3 Sigma 0.26 PIC11B BETA BKG 1.88 1.69 1.5 1.3 1.11 0.91 0... 0.72 u 0.53 0.33 0.14 Page 5084 of 5 809 PIC118 BETA EFF Generated09/28/2016 22928 22856 Sigma 22280 0.000475 +3 Sigma 00 0.00044 +2Sigma00 0.0004047 J I I \ I! I l!r !, M Ii Iii I I l 'I l I 0.000369 0.000334 0.000299 Mean 00 0.000264 0.000228 0.000193 -2Sigma00 0.000158 -3 Sigma OD e Denotes Outlier Page 5085 of 5809 PIC11 C ALPHA BKG Generated09/28/2016 -r----------------------------------------------------------.-+3Sigma0.38 0.38 0.33 0.29 0.25 a.. 0.2 () 0.16 0.11 0.0685 0.0242 t---------------t'------------"-----'------------------------------2Sigma0.01 -0.020081 t-+--+--i-+--+--+-t-+--+--i-+--+--+-t-+--+-+-t-+--+-+-t--+--+--i-+--+--+-t-+--+--i-+--+--+-t--t--t--t-t--+--+--1t--t---t---3 Sigma -0.064 PIC11 C ALPHA EFF 10390 10300 10200 10100 9980 a.. 9872 () 9770 9660 9560 9460 0.33 0.32 0.31 0.31 0.3 0.29 0.29 0.28 0.27 PIC11C BETA BKG 1.38 1.22 1.06 0.9 0.74 0.59 a.. 0.43 () 0.27 0.11 -0,0478
  • Denotes Outlier Page 5086 of 5809
2: 0... u 0.000426 0.000393 0.0003607 0.000328 0.0002951 0.000262 0.000229 0.000197 0.000164 0.0001311
  • Denotes Outller Page 5087 of 5809 ) ,\ 1 ! u v 'W v +3 Sigma 00 +2 Sigma 00 } I ./1(\ II I/ M Mean 00 1/ i -2 Sigma 00 -3 Sigma 00 PIC11D ALPHA BKG 0.36 0.32 0.29 0.25 a_ 0.22 u 0.18 0.15 0.11 l 0.0731 0.0372 PIC11 D ALPHA EFF 11580 11530 11480 11430 11380 a_ 11330 u 11280 11230 11180 11130 0.27 0.27 0.27 0.27 0.26 0.26 0.26 0.26 PIC11 D BETA BKG 2.36 2.1 1.84 1.58 1.32 1.06 a_ 0.8 u 0.54 0.28 0.0255 Page 5088 of 5809 I I NJ u iy \
  • I r Generated 0912212016 +3 Sigma 0.36 +2 Sigma 0.3 Mean 0.18 -2 Sigma 0.06 -3 Sigma 00 a.. u 0.000364 0.000336 0.0003074 0.000279 0.0002508 0.000223 0.000194 0.0001661 0.000138 0.0001095
  • Denotes Outlier I Page 5089 of 5809 ,m1. I N l 1( ! j '\ 11\ 1) \ I I\ +3 Sigma 00 +2 Sigma 00 rl I 11 I A 'I } Mean 00 I I j 1L II u I -2 Sigma 00 -3 Sigma 00 0.38 PIC12A ALPHA BKG Generated 09/28/2016 +3 Sigma 0.38 0.35 +2 Sigma 0.33 0.32 2 0.29 a... 0.25 (...) 0.22 0.19 0.16 n j Arw li ! A A fll I '1 I . i II// I 1 /1 \ { r Mean 0.22 0.13 -2 Sigma 0.12 0.0985 -3 Sigma 0.07 PIC12AALPHA EFF 11180 ,--------------------------------------------------------+---+3Sigma11180 11104 11028 10952 2 10876 a... 10800 (...) 10724 10648 10572 10496 l-+--+-f-+-+--+-f-+-+--+f---f---+--+-f-+-+--+-f-l-+--+--+-l-+--+--+-l-+--+-f-+-+--+f----+-+--+-f---+--+--+-l-+--+--<1,__-3Sigma10420 PIC12A BETA BKG 1.84 +3 Sigma 1.84 1.69 +2 Sigma 1.58 1.53 1.38 1.22 2 1.07 a... 0.91 (...) 0.75 I 1. I ! I I!\ n 'I I f l "ij' Mean 1.07 0.6 II -2 Sigma 0.55 I 0.44 -3 Sigma 0.29 Page 5090 of 5809 0... 0 PIC12A BETA EFF Generated09/28/2016 43918 43414 43162 42658 42406 42154 !-------------------------------+--------------------------11--2 Sigma42100 41902 l--+---4-+--+-l--+---+-+--+---i-+--+-t--+---+-+--+-l--+---4-+--+-l--+---+-+--+---j--+---t-+--+---ji--+---t-+--+---i-+--+-f--3Sigma41650 0.000238 +3 Sigma 00 0.00022 +2 Sigma 00 0.0002019 0.000184 II J A i I I II AM1i n II 1!i I t I II l . v ' i ! I rp w \ i' J!lll v ,/ v 0.000166 0.000149 Mean 00 0.0001308 0.000113 0.0000953 -2 Sigma 00 0.0000775 -3 Sigma 00 e Denotes Outlier Page 5091 of 5809 PIC12B ALPHA BKG Generated09/22/2016 0.38 0.34 0.3 0,27 a.. 0.23 () .. 0.19 0.15 0.11 0.0764 0.0385 t--+---+-t--+--+-t--+--+---1t--+--+---1-+--+---1-+--+--+-+--+--+-t--+--+---1-+--+--+-+--+---+-+--+---+-t--+--+-t--+--+---1t--+--+--t-*3S!gma00 PIC12B BETA BKG 2.12 1.94 1.77 1.6 1.42 1.25 a.. 1.08 () 0.9 0.73 0.55 Page 5092 of 5809 0.000598 +3 Sigma 00 0.000558 +2Sigma 00 0.000517 0.000313 A1 J N Ml n rl ! j A, ! I\ ! I v I I\ \ ljll I J ry j I I I I \ 0.000476 0.000435 0.000394 Mean 00 0.000354 0.0002721 -2 Sigma OD 0.000231 -3 Sigma 00
  • Denotes Outlier Page 5093 of 5809 PIC12C ALPHA BKG Generated09/17/2016 ,------------------------------------------------------H-.--.-+3Sigma0.41 0.41 0.37 1------------------------------------------------------+*l--+++i+-+2Sigma0.35 0.33 0.29 0.. 0.25 (.) 0.21 0.17 0.13 0.09024 0,0499 t--+---+-+--+--+-+--+--+-t--+-i-+--+-ic--+--+-ir-+--+-ir-+--+-i-+--+r-r-+--+-r-+--+-t--+---+-+--+---+-+--+-i-+--+--1"-3 Sigma 0.01 PIC12C ALPHA EFF 22130 22013 21896 21779 21662 0.. 21545 (.) 21428 21311 21194 21077 0.28 0.28 0.28 0.27 0.27 0.27 0.26 0.26 0.26 PIC12C BETA BKG 2.07 ,-----------------------------------------------------------+3Sigma2.07 1.86 l\-----t---l>-411--!--+l---------------l---t--------+--------t+--+----------------+2Sigma 1.72 1.65 1.44 1.23 1.02 0.. 0.81 (.) 0.6 0.38 l----------------------------------------------------------*2Sigma0.31 0.17 l-+---t-,f-+--+l-'--+--+--+-+--+--+-t--+--+-f-+--+l-c--+--+--+-+--+--+-f-+--+-11-+--+l--+--+--t-+--+--+-+--+-+-+--+--+-3 Sigma -0.039 Page 5094 of 5809 CL u PIC12C BETA EFF Generated09/17/2016 26990-r---------_;:_---'::.._.:_-'--------------i,._--------------------------------+3Sigma26990 26852 25748 +-+--+-+-+--+-+-+--+f-+-+--+f-+-+--+f--+--+f-'--+--+f-f-+--+f-f-+--+f-f-+--+-'f-+--+-+-+--+-f-+--+-f-+--+-f-+--3Sigma25610 0.000532 0.000434 0.000384 0.000286 0.000236 0.000187 ._---------------------------------41-----1-----------'-----------2Sigma00 0.000137
  • Denotes Outlier Page 5095 of 5809 PIC12D ALPHA BKG 0.39 0.34 0.3 0.26 a_ 0.22 () 0.17 0.13 0.0884 !I lt ' !I v If I 0.0459 0.00345 PIC120 ALPHA EFF 17360 17305 17250 17195 17140 a_ 17085 () 17030 16975 16920 16865 0.3 0.3 0.3 0.29 0.29 0.28 0.28 0.28 0.28 PIC12D BETA BKG 2.14 1.98 1.82 1.66 1.5 :2! 1.34 a_ 1.18 () 1.02 I I ii llij \II w 0.86 0.71 Page 5096 of 5809 I 111 r r1lT'\ I. & M ri w I! J\ I } V\ *i II ) Generated 09/20/2016 +3 Sigma 0.39 +2 Sigma 0.32 Mean 0.17 -2 Sigma 0.03 -3 Sigma -0.039 +3 Sigma 2.14 +2 Sigma 1.88 Mean 1.34 -2 Sigma 0.81 -3 Sigma 0,55 43993 43776 r------------------fl------------------jt-------jf----1!----l------r------jt---+2Sigma43900 42474 ;-----------------------l-------------------------------------2Sigma42400 42257 t--t---+-t--+--t-t--+---t-+---+-l--+---+-+--+---t-+--+-t--+---+-l--+---t-+---+-l--+---+-+--+--t-+--+-t--+---+-+--+--1-+--+-3Sigma42040 0.000314 +3 Sigma 00 0.000293 +2 Sigma OD 0.000272 I A r ' A lj' \! " J v l IV v 1)' w 0.000251 0.0002303 0.0002095 Mean 00 0.000189 0.000168 0.000147 -2 Sigma 00 0.0001261 -3 Sigma 00
  • Denotes Outlier Page 5097 of 5809 PIC13A ALPHA BKG Generated09/30/2016 ,-----..:....=---=--=-:.._:....::_:=..:....--=--=--"--=:....::_:....::. _______________________________ ... ,.,.+3 Sigma 0.39 0.39 0.35 1-----------------------------------------------------i1tt11tt+itltltt+-tt1HHl"+2 Sigma 0.32 0.3 0.26 a.. 0.21 () 0.17 0.12 0.08085 0.0368 Sigma 0.02 -0.00722 l-+--+--t-+--+--+--l-+--+--+--l-+--+--+--t-+-+--+--t-+-+--+--t-+-+--+--+-t-+--+--+-t-+--+--+-+-+--+--l-+--+--+--1-+--+--+--3 Sigma -0.051 PIC13A ALPHA EFF 11130 11068 11006 10944 10882 a.. 10820 () 10758 10696 10634 10572 0.33 0.32 t-----------------------------l+----------------------------+-+2Sigma0.32 0.31 0.27 0.27 l--+---+-+--+---+-+--+---+-+--+---+-t--+--+--lf-+--+--l-+--+--t-+--+---t-+--+---+-t--+---+-t--+---+-t--+---+-t--+---+-t-...._,-+-!---3 Sigma 0.26 PIC13A BETA BKG 2.04 1.82 1.6 1.37 1.15 0.93 Mean 0.93 a.. 0.71 () 0.48 0.26 0.0399 Page 5098 of 5809 0.0006058 +3 Sigma 00 0.00056 +2 Sigma 00 0,000513 J I J v A) f w I I I I I\ 'I 11 I II I ii 0.000467 0.0004207 0.000374 Mean 00 0.000328 0.000282 0,000236 -2 Sigma OD 0.000189 -3 Sigma 00
  • Denotes Outlier Page 5099 of 5809 0.41 PIC13B ALPHA BKG Generated 09117/2016 +3 Sigma 0.41 0.37 +2 Sigma 0.34 0.32 2 0.27 a_ 0.23 () 0.18 0.13 0.0885 0.0422 \ II Iii v I N \ I I ' 'l Mean 0.18 -2 Sigma 0.03 -0.00399 -3 Sigma -0.05 PIC13B ALPHA EFF 13850 13780 13710 13640 2 13570 a_ 13500 () 13430 13360 13290 13220 0.31 0.3 0.3 0.3 0.29 0.28 0.28 0.28 PIC13B BETA BKG 2.23 1.78 1.55 1.33 2 1.11 a_ 0.88 () 0.66 0.43 0.21 f-+--+__,l-+--+__,-+--+---+-+-+--+-+-+--+l-1-+--+---+-+-+--+l-l-+--+---+-+-+--+-l-+--+-11-+--+-__,-+--+---+-+-+--+-l--+--3 Sigma -0.018 Page 5100 of 5809
?! a.. () PIC138 BETA EFF Generated09/17/2016 22330,--------"-C::....--:_:--'---------------------------------------------+3Sigma22330 22206 21958 21834 21586 21462 21214 l-+--+---1-+-+--+---l-+-+--+---l-+-+--+---1-+--l--+---1-+--+--+-l-+--4---+-l-+--+---1-1--1--+---l-+--1--+---l-+--+--+-l-+---+---+--3 Sigma 21090 0.000539 +3 Sigma 00 0.000498 +2 Sigma 00 0.000457 0.000293 I J J i ,, il r I ! II id ,\ n v --V 1Y 11 \ l 1/ \ 0.000416 0.000375 0.000334 Mean 00 0.000252 0.0002106 -2 Sigma 00 0.00017 -3 Sigma 00
  • Denotes Outlier Page 5101of5809 0.. (.) 0.. (.) 0.. (.) 0.41 0.35 0.3 0.25 0.2 0.15 0.0988 0.0477 -0.00332 -0.0544 10788 10744 10656 10612 10524 0.32 0.32 0.32 0.31 0.31 0.3 0.3 0.3 0.29 1.24 1.1 0.96 0.81 0.67 0.53 0.39 0.25 0.11 -0.028 PIC130 ALPHA EFF PIC13D BETA BKG I h A v \ I U\ ui " "\JV v \,, \. \ ./ I\ I I \ I "I V' ' \j v \ I/ v v 11/llllllf Iii
  • Denotes OuUier DATE Page 5102 of 5809 +3 Sigma 1.24 +2Sigma 1 Mean 0.53 -2 Sigma 0.07 -3 Sigma-0.168 PIC130 BETA EFF Generated09/22/2016 2374o,---------'--'--'---'------------------------------------------------+3 Sigma23740 23611 22966 22837 22708 l--+-------------------------------1+---------------------l-+-¥---+----2Sigma22661 22579 l-+--+-+--+---+-+--+---+-+--+---l-+-+---lf-+-+--,f-+--+-+--+---+-+--+---l-+--+-+-+---+-+--+---+-+--+---l-._-+---lf-+--t-1--3 Sigma 22450 0.0004205.-----------------------------------------------------------*3Sigma00 0,000385 0,000315 0.00028 0.0002093 0.0001741 0.000139 0.0001037 t--+--+-+--+--+--t--+--+--+--+--+--+--+--+--t--+--+--t--+--+--t--+---+-+--+---+-+--+---+-+--+---+-+--+---+-+--+---+-+--+---+-+--+--3 Sigma 00 e Denotes Outlier Page 5103of5809 PIC14A ALPHA BKG Generated09/22/2016 0.32 0.28 0.24 0.21 0.. 0.17 (.) 0.13 0.0977 0.06111 0.0245 -0.0121 l--l--l--+--+--+--+--+--+--+--+--+--+--+--+--+--l--l--l--1--1--1--+--+--+--+--+--+--+---3 Sigma-0.049 0.. (.) 0.. (.) "' 10220 1.39 1.24 1.1 0.96 0.82 0.68 0.54 0.39 0.25 0.11 "'
  • Denotes Outlier ff <!' lf Page 5104of5809 & .§> .§> <? ::? ., <§' ., ., "' "' "' "' "' "' "' "' "' "' PIC14A ALPHA EFF PIC14A BETA BKG (f & .§> .§> 8' ::? ., ., ., <!' <!' ., <§' <§' "' "' "' "' " "' "' "' fl !Y I & 8' I?! !:? <§' <§' <§' <§' "' 8' "' "' Pl Pl Pl Pl 8' 8' "' " "' <:> "' "' "' <:> <:> DATE -3 Sigma -0.031 fl ty i '5' .§> .§> <? ::? :::: ty "' "' "' Pl Pl Pl !ll°' <§' <§' .§> <§' .§> 8' 8' "' "' "' "' "' <:> "' <:> "' "' DATE PIC14A BETA EFF Generated 0912212016 54050 +3 Sigma 54050 53805 +2 Sigma 53600 53560 53315 a_ 53070 u 52825 Mean 52830 52580 52335 52090 -2 Sigma 52000 51845 -3 Sigma 51600 I If/ I Ill I & ::y /!? I fl ,J I rS> & ::? {::, I & ii} !;: ., ., ., ., ii} ilf ilJ ilJ ilJ ilJ "' "' .§ .§ " " " <!!' " " " " " <!!' <!!' <!!' " 8' " " 8' " "' "' "' "' 8' DATE PIC14A BETA EFF Cross Talk 0.000249 +3 Sigma 00 0.000225 +2 Sigma 00 0.00020075 0.000177 0.000152 0.0001281 Mean 00 0.0001039 0.0000796 0.0000554 -2 Sigma 00 0.0000312 -3 Sigma 00 i::-t& 8-II .,<r & ::? !V 8-& {:: ::y /!? re-"' ii} t t ii} !;: !;: ., & ., $ ilf ilf ii} ilf ilJ ilJ ilJ ilJ "' "' "' "' " <!!' " <!!' <!!' " <!!' <!!' c " c "' c " "' " " "' "' " DATE
  • Denotes Outlier Page 5105of5809 0.37 0.34 0.3 0.27 a_ 0.23 u 0.2 0.16 0.13 0.0959 0.0614 OJ !:! <:> ¢j 19140 18966 17574 ftl Ol' !:! !:! <:> <:> 0.58 0.57 0.55 0.53 0.51 0.49 0.48 0.46 0.44 1.99 1.85 1.71 1.57 1.43 a_ 1.29 u 1.15 1.01 0.86 ¢j <:>
  • Denotes Outlier Page 5106of5809 i? & & & Ii:? {I! fY OJ ftl l' & ,§ ,§ ,§ i!J' ,;:-i!J' i!J' i!J' .ffe ,;} <:> ¢j "' "' <:> <:> .§' <:> <:> .§' "' .§' <:> <:> DATE PIC14C ALPHA EFF ----& DATE PIC14C ALPHA EFF Cross Talk PIC14C BETA BKG i? & & §? Ii:? Ii:? ::)-{I! OJ ffe rY rY i f & r;; r;; r;; .§' & ill' .§' .§' .§' .§' "' "' <:> <:> <:> <:> <:> <:> <:> "' <:> DATE & & & 6' Ii:? ::)-::)-{I! "' ,;} ,;} ,;} ,;} i!J' {!' <:> <:> <:> <:> <:> <:> <:> <:> <:> <:> <:> & -3 Sigma 0.72 i #' & & ?ff ::)-::)-I:? !? ,ff fS' & & ,;} ,;} i!J' i!J' i!J' i!J' 8' & <:> <:> <:> <:> <:> <:> <:> <:> <:> <:>

PIC14C BETA EFF Generated 0912212016 25610 +3 Sigma 25610 25523 +2 Sigma 25500 25436 25349 Cl.. 25262 u 25175 Mean 25180 25088 25001 24914 -2 Sigma 24900 24827 -3 Sigma 24740 .,<r lllliflll!l &' rY i & .§' ;;, ;;, ;;, ;;, <:> <:> " <§' " " @ @ @ <::> <> <> <> @ DATE PIC14C BETA EFF Cross Talk 0.0003601 +3 Sigma 00 0.0003307 +2 Sigma 00 0.0003014 0.000272 0.000243 0.000213 Mean 00 0.000184 0.000155 0.000125 -2 Sigma 00 0.0000958 -3 Sigma 00 ii ,§> & ? ? ? ? ? ? <§' @ t? if &' ,§> ff ,§' t? :t? R ,;:-,;:-§' ii! 9§ <§' .§' 9§ .§' <§' .§' .§' 9§ 9§ <§' .§' ;;, i§i .§' .§' ;;, @ @ 9§ 9§ ;;, ;;, ;;, ;;, @ <> <> <> <> <:> " " <:> <:> <:> <> <:> <> <::> <> <> <> DATE

  • Denotes Outlier Page 5107of5809 a.. 0 a.. () a.. () 0,38 0,35 0.32 0.3 0.27 0.25 0.22 0.2 0.17 0.15 " 14340 14187 14034 13881 13728 13422 13269 12963 ,t' ""' "' 0.73 0.71 0.69 0.67 0.65 0.63 0.61 0.59 0.57 0.55 1.98 1.81 1.65 1.49 1.33 1.16 01 0.84 0.67 0.51 re' ""' "' ""' "' Page 5108 of 5809 tJ .§> ,f ,t' #' ,s. ,;:. !::> # 9§ 9§ .§' .§' 8' if§ " " " " " " " " " <:> "' DATE PIC14D ALPHA EFF PIC14D BETA BKG 42120 41956 41792 41628 0.... 41464 (.) 41300 41136 40972 40808 40644 & "' "' 0.000269 0.0002507 0.000233 0.000214 0.000196 0.000178 0.00016 0.000142 0.000124 0.0001056 ii "' "'
  • Denotes Outlier Page 5109 of 5809 "' 1*11111111111111111111 DATE PIC14D BETA EFF Cross Talk ,§> .g, II .§' .§' :2 ::)! ,f & :>:-'"' '"' .§' .§' .§' .§' '"' '"' .§' .§' .§' .§' "' "' " " " <:> <:> <:> <:> <:> <:> DATE -3 Sigma 00 ,§> & .§' <!!' :2 :.:.> :,, :0 If §> ,,, ,,, ,,, 8' <Ii "' <:> <:> <:> <> "' <> "' "'

a.. u a.. u 0.37 PIC1A ALPHA BKG Generated 0912712016 +3 Sigma 0.37 0,33 +2 Sigma 0.3 0.29 0.24 0.2 0.16 0.12 0.0732 ) I ! Iii 1 r ll r** f Mean 0.16 0.03045 -2 Sigma 0.02 -0.0123 -3 Sigma -0.055 ii!l!!!!l!!!!!!liillllilillillilliffllllil/11 DATE PIC1A ALPHA EFF 10890 10822 10754 10686 10618 10550 10482 10414 10346 10278 0.31 0.31 0.3 0,3 0.29 0.29 0.28 0.28 PIC1A BETA BKG 1.95.-----------------------------,----------------------------.... -+3Sigma1.95 1.74 r----r-----------------t-t-'lt-+-----Hl\-111tt!'r---r-;--tt-+--:+-------l---l--+-11r+-1--t------t-*2 Sigma 1.6 1.53 1.32 0.26 f-----------------------------------------------------------2Sigma0.19 0.0479 f-+--+---,f-+--+---l-+--+--+-f-+--+---l-+--+--+-l-+--+---l-+-+-+-f-+--+-+-t-+--+---l-+--+--+-+-+--+---lf-+--+--+-+-+-+-+-3S!gma-0.163 Page 5110of5809 PIC1A BETA EFF Generated09/27/2016 0... (.) 21157 20971 20878 20692 20599 20506 20413

  • Denotes Outlier 1-------------------ll-----+---------l--f---'---l----'------------+------"'-+---'---2 Sigma 20500 l-+--+_,l-+--l---+-l-+--+_,-+--+---+-+--+---+-l-+--+---"l-+--+--l-+--+---+-+--+---+-l-+--+---'l-+--+--1-+--+---+-l-+--+_,l-+--3 Sigma 20320 Page 5111 of5809 0.45 0.4 0.34 :2: 0.29 0.. 0.24 u 0.18 0.13 0.0748 0.0213 -0.0322 PIC1B ALPHA EFF 13370 +3 Sigma 13370 13332 +2 Sigma 13300 13294 v J JM!I, h N ! I -II r! j I I l J ljl I ' (\ r l 13256 13218 13180 Mean 13180 13142 13104 13066 -2 Sigma 13100 13028 -3 Sigma 12990 0.28 +3 Sigma 0.28 0.28 +2 Sigma 0.28 ,N i I J ,! N M \I r ' , I q 11 I i ,/ v *1 i I ) N v 0.28 0.28 0.28 0.27 Mean 0.27 0.27 0.27 0.27 -2 Sigma 0.27 0.27 -3 Sigma 0.26 PIC1B BETA BKG 2.08 .-----------------------------------------------------------it-+3Sigma2.08 1.87 1.67 1.46 1.25 :2: 1.05 0.. 0.84 u 0.64 0.43 i----------------------------------------------------------*2S!gmaD.36 0.22 l-+--+-t-+--+--+-+--+---+-l-+--+-l-+--+-t-+--+--+-t,--+--+-t-+--+--+-t--r--;---;-+--+---t-t--+--+-t-T--t--t-+--+-t-+--3 Sigma 0.02 Page 5112of5809 a.. u 22460 PIC1 B BETA EFF 22388 22316 22244 22172 22100 .n I V\ v j A I! 21956 v r \ r 22028 21884 " 21812 !1 \ ./\ \! hJ ' I IV \ Yj \ \ Generated 09128/2016 II +3 Sigma 22460 +2 Sigma 22300 Mean 22100 * -2 Sigma 21900 -3 Sigma 21740 o.00231-,.----------------------------------------------------------+3Sigma00 0.0020961 0.00167 0.00145 0.001021 0.0008084 0.000591 f------------------------------'---------f---------------+------2Sigma00 0.000376 f-+--+--+-+-+--+--+-+-+--+--+-+-+--+--+-f-+--+---+-f-+--+-+-+-+--+--+-+--+--+--+-+-+--+--+-+--+--+--+-+--+--+--+--++--+--+-3 Sigma 00
  • Denotes Cuttler Page 5113of5809 0.3B 0,35 0.31 :2! 0.27 a_ 0.24 (.) 0.2 0.16 0.13 ! O.OBB2 0.0512 0.27 0.27 0.26 0.26 0.26 0.26 0.26 0.25 0.25 2.41 2.16 1.9 1.65 1.39 :2! 1.13 a_ O.BB (.) 0.62 0.37 0.11 Page 5114of5809 PIC1C ALPHA BKG \ d " r I r I I 'II PIC1C ALPHA EFF PIC1C BETA BKG ii i N I! Generated 09128/2016 +3 Sigma 0.38 +2 Sigma 0.32 Mean 0.2 ' -2 Sigma 0.08 -3 Sigma 0.01 PIC1 C BETA EFF Generated09/2B/2016 Sigma22410 0.. (.) 22282 22154 tt----------------------------------------------------------+2Sigma22196 22026 21898 21642 21514
  • Denotes Outlier Page 5115of5809 0.37 0.33 0.3 2 0.26 0... 0.22 () 0.18 0.14 0.11 0,0688 0.03086 PIC1D ALPHA EFF 11130 +3Sigma11130 11095 +2 Sigma 11100 11060 11025 2 10990 0... 10955 () 10920 10885 1i I \,/ I! N ,! I I . ' v v 1) .I '\ J Ii /II ii 'i Mean 10960 10850 -2 Sigma 10800 10815 -3 Sigma 10780 0.27 +3 Sigma 0.27 0.27 +2 Sigma 0.26 0.26 \ !! li I I I\ .M \ I I! ! I/ I , .,, I w u '\ JI I\ q -! IA ) 0.26 0.26 0.26 Mean 0.26 0.26 0.26 0.25 -2 Sigma 0.25 0.25 -3 Sigma 0.25 PIC1D BETA BKG 2.09 +3 Sigma 2.09 1.92 I ,rt j f n1 rr I! J 1! y !, ' II I y1 I I v 1\ l 1111 v 1 +2 Sigma 1.81 1.76 1.6 1.44 2 1.27 0... 1.11 () 0.95 Mean 1.27 0.79 -2 Sigma 0.73 0.62 -3 Sigma 0.46 Page 5116of5809 a.. () 25760 25619 25478 25337 25196 25055 24914 24773 24632 24491 e Denotes Outlier Page 5117 of 5809 PIC1 D BETA EFF A I v I I II ,) 1 J . I 'I Generated 09/2812016 +3 Sigma 25760 +2 Sigma 25500 \ \1 \! I Mean 25060 \ I ... u i \ -2 Sigma 24600 -3 Sigma 24350 0.36 0.32 0.28 0.24 0.. 0.2 () o.i6 0.12 0.08107 0.04072 0.000377 PIC2A ALPHA EFF 11140 11069 10998 10927 10856 0.. 10785 () 10714 10643 10572 10501 0.29 0.28 0.28 0.27 0.27 0.26 0.26 0.25 PIC2A BETA BKG 1.58 1.41 1.23 1.05 0.88 0.7 0.. 0.52 () 0.34 0.17 .__----------------------------------------------------------2Slgma0.11 -0.01089 .__-+--+-+--+-f--+--t-+--+--l!-+--+-f--+--+-+--+--+-+--+-t--+--+-+--+--+-+--+---t-+--+-r--+--+-+--+---t-+--+-r--+---t--3Sigma-0.188
  • Denotes Outlier Page 5118of5809 a.. u PIC2A BETA EFF Generated09/27/2016 55870,-----::....:::....:=::....::.....:::....:=_:_::....:::....:=:..:....---------------..... -------------------------+3Sigma55870 55448 t--+--+-t--+-l-+--t--lf--+--+-+--+--l-+--+-f--+---+-+--+-lf-+---+-+--+-lf--+---+-+--+--l-+--+-t--+--+-+--+-1,--+--+--3 Sigma 51650 o.OOS?J,----------------------------------------------------------+3Sigma0.01 0,000616 -0.0004034 -0.00142 f-----------------------------------------------------------2Sigma-0.002 -0.00244 f--+---+-f--+--+-l-+--t--l-+--t--1-+--t--l-+--+--+-+--+---+-+--+-t-+--+-t-+--+-t-+--+--+-t--+--+-t--+--+-t--+--+-t--3 Sigma -0.003
  • Denotes Outlier Page 5119of5809 0.38 0.34 0.29 0.25 a.. 0.21 () 0.17 0.13 0.0872 0.0456 0.004086 9668 9520 9370 9220 9070 a.. 8917 () 8770 8620 8470 8320 i$ " 0.46 0.44 0.42 0.4 0.38 0.36 0.34 0.32 0.3 028 i ff? ::? ,; I ::? fllf:I# ,§' ::? !Y i ,§> :? :t.> J & ,a ,a ii::' ., ,a ,a '* " " " " " " "' " " " " " (;j c::5 (;): c c::. 0 ti " " " " " " " " " & & DATE PIC2B BETA BKG 2.61 2.31 f----------------------------------------------------------*2Sigma2.12 2.02 1.72 1.43 1.13 +----,,----------------------------------------------------------Mean1.13 a.. 0.84 () 0.54 0.25 -0.0452 l---+----+-t--+--+-+--+---l'--+----+-t--+--+-+--+---l-+--t----l-+--+-r--+--+-t--+--+-+--+----l-+--+-r--+--+-t--+--+-+--+--1r-+--3 Sigma -0.34 Page 5120of5809 0.... u PIC2B BETA EFF Generated09/28/2016 21550,------------==--:=--=----------------------------------------------+3Sigma21550 19396 19037 18678t------------------------------------------------------___,r-t---*2Sigma18600 18319 l---+-_,,___+--+-+--+--+--+--l---+-_,'--+--+--+--+--+--+--l---+-_,-+--+-+--+--+--+--+--+--1---+-_,-+--+-+--+--+--+----<*-+---3 Sigma 17960 0.000554 l-----------+--"""T-------+---------------------------.---,,------tt---+2Sigma00 0.000512 0.0004701 0.000428 0.000345 0.0003028 0.000261 Sigma OD 0.000219 lll!lllllf iliillllf il!f If !!llf lf lllllll/ DATE
  • Denotes Outlier Page 5121of5809 0.37 0.33 0.3 0.26 a.. 0.22 (.) 0.18 0.15 0.11 0.0693 0.0315 2163o.,-----------------------------------------------------------+3Sigma21630 21432 21234 t--+--l-+---+-+---+-+--+-+--+-t--+--l-l+---+-+--+-+--+-t--+--l-+---+-+---+-+--+-t--+--t--+--l-+---+-+---+-+--+--3Sigma19650 PIC2C BETA BKG 0.86 0.78 0.69 0.61 0.44 0.35 0.27 0.18
  • Denotes Outlier bAi"E Page 5122of5809 a.. u 27110 PIC2C BETA EFF Generated09/22/2016 .------=-=-=_:=-=:....:....:........:......=:..:..------------------------------------------*3 Sigma 27110 26597 26084 f----------------------------------------------------------+2Sigma26200 25571 25058 24545 24032 23519 23006 22493 t--+----1-+--t-+--+-+--+-+--+-t--+----1-+--+-+--+-+--+-+--+-t--+-t--+----1-+--t-+--+-+--+-+--+-t--+----1f--+----1--3 Sigma 21980 ,j PIC2C BETA EFF Cross Talk 0.00215 +3 Sigma 00 0.00188 f----------------------------------------------------------*2Sigma00 0.001602 0.00133 0.001056 -0.0000373 t----------------------------------------------------------*ZSigma-O -0.0003106 t--+-+--+-t--+--f--+----1f--+----1-+--t-+--t-+--+-+--+-+--+-+--+-+--+-+--+-+--+-+--+-+--+-+--+-+--+-+--+--3 Sigma -0.001
  • Denotes Outlier Page 5123of5809 PIC3B ALPHA BKG Generated 09128/2016 +3 Sigma 0.37 0.37 0.33 +2 Sigma 0.31 0.29 2 0.26 0... 0.22 0 0.19 0.15 0.11 j } A1 A I I u ) . v I/ ;A Mean 0.19 0.07608 -2 Sigma 0.06 0.0397 -3 Sigma DO PIC3B ALPHA EFF 13500 13455 13410 13365 2 13320 0... 13275 0 13230 13185 13140 13095 0.25 0.25 0.25 0.25 0.24 0.24 0.24 0.24 PIC3B BETA BKG 2.08 +3 Sigma 2.08 1.96 +2 Sigma 1.89 ii n r 11 !I ! I\.. i w u ,,_ I *1 i r1 11 \ V\ VI ll M N 1.85 1.73 1.62 2 1.5 0... 1.39 0 1.27 Mean 1.5 1.16 -2 Sigma 1.12 1.04 -3 Sigma 0.93 Page 5124of5809 21960 PIC3B BETA EFF Generated 09/2812016 +3 Sigma 21960 21817 +2 Sigma 21700 21674 21531 a.. 21388 () 21245 21102 20959 I f 1A ,, 1fu! I\ Ill l jl W I 1 ry l I v 11il v Mean 21250 20816 -2 Sigma 20800 20673 -3 Sigma 20530 0.75 0.6 0.46 0.31 0.17 0.0243+-==="""'""=========-=======.J.j,.============================-======....-Mean0.02 -0.12 *0.264 .().409 f----------------------------------------------------------*2Sigma-0.457 *0.553 f-+--+--!-+-+--+--!f-+--+--+---<'--+--+--+---<f-+--+--+-f-+--+--!-+-+--+---'f-+--+--+---'f-+--+--+-f-+--+--!-+--+--+f-f-+--+--+-f---3 Sigma -0.697
  • Denotes Outller Page 5125of5809 a.. (.) a.. (.) a.. (.) PIC3C ALPHA BKG 0.36 0.32 0.28 0.25 0.21 0.18 0.14 0.1 J1 ! I Vi >> v L 1r 0,0677 0,0318 PIC3C ALPHA EFF 10200 10100 9950 9870 n ' * I/ J v Generated 09128/2016 +3 Sigma 0.36 +2Sigma0.3 Mean 0.18 -2 Sigma 0.06 -3 Sigma -0.004 9780 f----------------------------------------------'---'-l!-'<J-----WPHl"<i-'\.+-'-\-+i'lf-l--2Sigma9750 9700 0.27 0.27 0.27 0.27 0.26 0.26 0.26 0.26 PIC3C BETA BKG 1.26 +3 Sigma 1.26 1.14 +2 Sigma 1.06 1.01 ri ! I Iii .. l I I 1 N Ir II i U"I ! w ) i w \ IJ ij µ r iv fl 0.89 0.77 0.64 0.52 0.4 Mean 0.64 0.27 -2 Sigma 0.23 0.15 -3 Sigma 0,03 Page 5126of5809 PIC3C BETA EFF Generated09/28/2016 22020.,..------'=---=--=--=--=---'=--=:....::....:.......:...-=::.::..-=-----------------------------------------*3Sigma22020 0... u 21915 21810 21705 21600 21390 21285 21075 0.00947 0.00869 0.0079005 0.00711 0.00554 0.00475 0.00318
  • Denotes Outlier r---tt--!i-----+-------------------------------------------------*2Sigma21800 Page 5127of5809 0.34 0.3 0.26 0.22 a.. 0.18 (.) 0.14 0.0946 0.05408 0.0136 -0.027 PIC3D ALPHA EFF 10860 10816 10772 10728 10684 a.. 10640 (.) 10596 10552 10508 10464 PIC3D BETA BKG 1.37 1.23 1.09 0.95 0.81 0.67 a.. 0.54 (.) 0.4 0.26 0.12 Page 5128of5809 24730 PIC3D BETA EFF Generated 09/28/2016 +3 Sigma 24730 24538 +2 Sigma 24400 24346 24154 0. 23962 u 23770 23578 23386 1! \ \ /Ir r } f J, !! ,/ \ I mi II I!\ I IP ) 1( Mean 23770 23194 -2 Sigma 23100 23002 -3 Sigma 22810 0.0034 0.003075 0.00275 0.00243 0.00179 0.00147 0.000828
  • Denotes Outlier Page 5129of5809 0.38 0.34 0.3 0.25 a.. 0.21 () 0.17 0.13 0,086 0.0439 0.00189 PIC4A ALPHA EFF 11080 10980 10880 10780 10680 a.. 10580 () 10480 10380 10280 10180 0.28 ,----------------------------------------------------------+3Sigma0.28 0.28 0.28 0.27 n 0.27 0.27 0.27 0.26 0.26 0.26 t-+--+--+-+--+--+_..,1-41>!--t---+-t-+--+-1-+--t--+-t-+--+--+-t-+--+--+-+---+--+-1f-+--t---+-+--+--+f-f-+--t---+-t-+--+--+-+--+--3 Sigma 0.26 PIC4A BETA BKG 1.81 1.62 1.43 1.25 1.06 0.87 a.. 0.68 () 0.49 0.3 0.12 Page 5130of5809 0.. () PIC4A BETA EFF Generated09/28/2016 55350,----------=--==--:=--=--=--=---=------------------------------------------+3Sigma 55350 55066 54782t----------------------------------------------------------+2Sigma54900 52794 1-+--+-+-+--+-l-+--+-l-+--+-1-+--+-1-+--+-+--+--+-+--+--+-+--+--+-._-+<IH--<11>1--+---l-+--+---l-+--+---l-+--+---l---it--+-3 Sigma 52510
  • Denotes Outlier Page 5131 of 5809 2 a.. () 2 a.. () 2 a.. () 0.38 0.34 0.3 0.27 0.23 0.19 0.16 0.12 0.08351 0.047 9330 9290 9210 9160 9080 0.35 0.35 0.34 0.34 0.34 0.33 0.32 0.32 0.32 2.24 2.12 1.89 1.77 1.65 1.53 1.41 1.29 1.17 Page 5132 of 5809 PIC4B ALPHA BKG II 11 '\/ I ljlll1J PIC4B ALPHA EFF PIC4B BETA B.KG 1111 'l' Generated 0912812016 +3 Sigma 0.38 +2 Sigma 0.31 J H \ Mean 0.19 I! I \ -2 Sigma 0.07 -3 Sigma D.01 +3 Sigma 2.24 +2 Sigma 2.04 w I& I Iii Mean 1.65 ,, *11111 11 -2 Sigma 1.25 -3 Sigma 1.05 0.00057 +3 Sigma 00 0.0005303 0.0004908 IV +2 Sigma 00 d r 11 ,.., 11 I II I Ill j I! IT I/ Li I 1 r '\ I w i\ " 'I 1\11 -\ 0.000451 0.000412 0.0003721 Mean 00 0.000332 0.000293 0,000253 -2 Sigma 00 0.000214 -3 Sigma 00
  • Denotes Outlier Page 5133of5809 PIC4C ALPHA BKG 0.37 0.33 0,3 0.26 c.. 0.23 (.) 0.19 0,16 0.12 u /,/ Aj I I I v 0.0883 0.0535 PIC4C ALPHA EFF 21920 21799 21678 21557 21436 c.. 21315 (.) 21194 21073 20952 20831 0.28 0.27 0.27 0.27 0.27 0.27 0.27 0.26 PIC4C BETA BKG 1.72 1.55 1.37 1.19 1.02 0,84 c.. 0.67 (.) 0.49 0.31 0.14 Page 5134 of 5809 1i 11 .. r I I v /1 I I I\ '\IU Generated 0912712016 +3 Sigma 0.37 +2 Sigma 0.31 Mean 0.19 -2 Sigma 0.08 -3 Sigma 0.02 27100 PIC4C BETA EFF 26951 26802 :2! 26653 0... 26504 () 26355 26206 '1 11 t I I" M \ 26057 25908 25759 0.003028 " ! r-I ! IV v ! 1!.A "' *v d Generated 0912712016 +3 Sigma 27100 +2 Sigma 26900 Mean 26360 \ -2 Sigma 25900 -3 Sigma 25610 0.00277 0.0025061 ' 0,00225 0,00172 0.00146 0,0009402
  • Denotes Outlier Page 5135 of 5809 0.37 PIC4D ALPHA BKG Generated 09/28/2016 +3 Sigma 0.37 0.34 +2 Sigma 0.31 0.3 0.27 0.. 0.23 u 0.2 0.16 0.13 0.0919 /V 1 J A ,..., L _/ .iA .. 1\ i N \ ! Mean 0.2 -2 Sigma 0.08 0.0568 -3 Sigma 0.02 17340 17272 17204 17136 :2! 17068 0.. 17000 u 16932 16884 16796 16728 0.27 +3 Sigma 0.27 0.27 I \ J 1!11 v I J A ff I 11) i! lj I\ I J Ni I +2 Sigma 0.27 0.27 0.27 0.26 0.26 Mean 0.26 0.26 0.26 0.26 -2 Sigma 0.26 0.26 -3 Sigma 0.26 PIC4D BETA BKG 2.49 2.28 2.08 1.87 1.67 :2! 1.47 0.. 1.26 u 1.06 0.85 0.65 Page 5136of5809 PIC4D BETA EFF Generated09/28/2016 43910,..----------==-=:....:..::....::....=:..:..._:_ ________________________________________ +3Sigma43910 43663 42428 42181 41934 41687 +---l---i'--+<ll-t-t----l---if--+--+-+--+-l--+--+-+--+-1---+----l-+--+-+-----l---if--+---41>--+--+-l---+----l-+--+-+---__.---l-+---t-+--+--35igma41440 0.0134 ll---1---+---------,\------l-----------------------l!-------------+--------+2Sigma0.01 0.0124 0.0114 0.01036 0.00836 0.00736 0.00537 +--+----l-+--+-t---+---+-+--+-t---+---+-+--+--it--+---+-+--+--if--+---+-+--+-f--+---+-+--+-f--+---t-+--+-f--+---+-+--+-+----+--3Sigma00
  • Denotes Outlier Page 5137of5809 PICSA ALPHA BKG 0.37 0.33 0.3 0.26 0.... 0.22 (.) 0.18 0.14 0.1 Ii \ I n ll1 1w1r J I.I 0.06504 0.0267 PICSA ALPHA EFF 11350 11306 11262 11218 11174 0.... 11130 (.) 11086 11042 10998 10954 027 0.27 0.27 , \ II ii\ \ I \ N I 0.27 0.26 0.26 0.26 0.26 0.26 PICSA BETA BKG 2.21 2.05 1.89 1.72 1.56 1.4 0.... 1.24 (.) 1.08 0.92 0.76 Page 5138of5809 II 111111 )\ I ! t M IW T 1M I I I/I \ *11 *111 A It \ I . Generated 09128/2016 +3 Sigma 0.37 +2 Sigma 0.31 Mean 0.18 -2 Sigma 0.05 -3 Sigma-0.012 +2 Sigma 0.27 r Mean 0.26 -2 Sigma 0.26 -3 Sigma 0.26 +3 Sigma 2.21 +2 Sigma 1.94 Mean 1.4 -2 Sigma 0.87 -3 Sigma 0.6
  • Denotes Outlier Page 5139of5809 0.37 0.35 PIC5B ALPHA BKG Generated 09/28/2016 +3 Sigma 0.37 I" +2 Sigma 0.33 0.32 0.29 0.. 0.27 () 0.24 0.21 0.19 hA ii A i 0 Al ! n I! I I! n I " II I IJ J ll II' I/ v Ir Mean 0.24 0.16 -2 Sigma 0.15 0.13 -3 Sigma 0.11 PIC5B ALPHA EFF 13950 13693 13636 13779 13722 0.. 13665 () 13606 13551 13494 13437 0.27 0.26 0.26 0.26 0.26 0.26 0.26 0.26 0.26 PIC5B BETA BKG 1.47 1.31 1.15 0.99 0.62 0.66 0.. 0.5 () 0.34 0.16 0.0141 Page 5140of5809
  • Denotes OuUler Page 5141of5809 0.38 PIC5C ALPHA BKG Generated 09/2912016 +3'Sigma 0.38 0.34 +2 Sigma 0.32 0.3 0.26 a.. 0.22 () 0.18 0.14 0.1 ! ! ! ! Im I* lh Jj I '\ I I Mean 0.18 0.06201 -2 Sigma o.os 0.022 -3 S!gma-0.018 PIC5C ALPHA EFF 10690 10629 t----------------------------------------------------------+2Slgma10600 10568 10507 10446 a.. 10385 () 10324 10263 10202 10141 ,_._-+--+-+--+--+-+--+--+-+--+----<-+--+->--+---+->--+---+->--+---+->--+---+->--+---+-+--+--+-+--+--+-+--+----<-+--+----<>--+---+---+-3Sigma10080 0.26 +3 Sigma 0.26 0.26 +2 Sigma 0.26 t M ! J I\ \ 1 !1 I\ v " 0.26 0.26 0.26 0.25 Mean 0.25 0.25 0.25 0.25 -2 Sigma 0.25 0.25 PIC5C BETA BKG 1.87 1.67 1.47 1.26 1.06 0.86 a.. 0.66 () 0.45 0.25 0.04804 Page 5142of5809 0.. u PIC5C BETA EFF Generated09/29/2016 22690,------------C...::C...:..C...-'--------------------------------------------+3Sigma22690 22608 22526 t------,---,\----1\----.,.-lr--,----f------------------------------------------+2 Sigma22552 22444 22362 22198 22116 21952 t--t---l-+--+-t--+---+-+--+-1f-+---+-+--+--1-+---+-+--+-1f-+---t-+--+-1-+---+-+--+-1f--t---t-+-..:+-1f-+---t-+--+--l--l--3 Sigma 21870
  • Denotes Outlier Page 5143 of 5809 PICSD ALPHA BKG Generated 09/29/2016 +3 Sigma 0.36 0.36 0.33 +2 Sigma 0.31 0.29 2 0.26 0.. 0.22 u 0.19 0.15 0.12 tr' I Ah I\ \I If t Ir t I \ . y \ w ! I ! Mean 0.19 0.0799 -2 Sigma 0.07 0.0443 -3 Sigma 0.01 PICSD ALPHA EFF 11610 11494 11378 11262 2 11146 0.. 11030 u 10914 10798 10682 10566 t-+--+--t-+-+--+-t-t-+--+--+t-t-+--+--+t--+-+--+-t--+--+--+-t-t-+-+--+--t-+-+--+--t-+-+--+--t-+-+--+-t--+--+--+-t--+-+--+-3 Sigma 10450 PICSD BETA BKG 2.07 1.87 1.66 1.46 1.25 2 1.05 0.. 0.84 u 0.63 0.43 0.22 Page 5144of5809 PIC5D BETA EFF Generated09/29/2016 26620,-------------'--'---------------------------------------------+3Sigma26620 26433 24937 f---!--+---l-+--!--+----'f---+--+---l-+-+-+---lf---+--+--+-f---+--+---l-+--+--+-l-+-+-f---+--+---l-+--!--+---l-+--+--+-l--!--+---l---l-+--+--+-3Sigma24750
  • Denotes Outlier Page 5145of5809 0.. () 0.. () 0.. () 0.38 0.34 0.31 0.27 0.23 0.19 0.15 0.11 0.0735 ii It " 10870 1.6 1.48 1.36 1.24 "1.13 1.01 *0.89 0.77 0.65 0.53 <'! !? & [? 8' 8' if :i-;§' ;§' ;§' ;§' & " " " " " " PIC6A ALPHA EFF PIC6A BETA BKG j
  • Denotes Outl!er Page 5146of5809 "' /?} & " tC" OJ ffe rv & ? 8' :i-"' /?} OJ "" .# & <§' <§' <§' iJj 8' iJj iJj "' "' "' "' 8' 8' " " ., " " " " " <:) DATE 51198 50556 f----------------------------------------------------------+2Sigma50770 49914 49272 47988 47346 46704._ ___________________________________________________ ++-----*2S!gma46490 46062 l--f----+--+--+--+-+--+--f----!--+--+--+-+--+--t--f----i---+--+--+--+--+--t--f----i---+--+-..... --+--+--*3Sigma45420 0.000234-,------------------------------------------------------------*3Sigma00 0.000217 0.000199 0.000182 0.000164 0.000129 0.000112 0.0000943 l--------'-------------------t+----------------------------+------2819maOO 0.00007681 l--+---J-+---+-+--+-+--+---J-+--+-+--+-f---t---+-+---+-+--+-+--+-f---+--+-+--+-+--+-f---+--+-+---+-+--+-+--+---'f--+--3 Sigma 00
  • Denotes Outlier Page 5147of5809 PIC6B ALPHA BKG Generated 0911712016 0.37 +3 Sigma 0.37 0.33 +2 Sigma 0.3 0.29 0.25 0.. 0.21 u 0.17 Mean 0.17 0.13 0.0852 0.044 -2 Sigma 0.03 0.00283 -3 Sigma -0.038 Ip ,y &' t'1 ,§> 8' :i-I!> .,II' I if i <;-,§> 8' :i-::? I!> §' i§ .j "i§ .j ,;; ,} ,} "' "' "' "' "' "' "' "' "' "' " .§> "' "' "' .§> "' "' <:) "' .§> "' <:) 8' " " " " " " " " " DATE PIC6B ALPHA EFF 9758 +3 Sigma 9758 9730 +2 Sigma 9710 9700 9670 9640 0.. 9600 Mean 9604 u 9570 9540 9510 -2 Sigma 9500 9480 -3 Sigma 9451 &' I t'1 .§> I!> OJ rtl i <;-:!? ::? :;, §' §' 9§ 9§ 9§ :>:-,;; ,;; ,} ,} ,} ,} "' "' "' "' "' "' "' .§> .§> "' .§' c§i c§i c§:i c§i c§i .§' "' .§' .§> " " " " " "' "' "' "' "' "' "' "' "' "' "' " <:) <:) " " " <:) DATE PIC6B ALPHA EFF Cross Talk 0.29 +3 Sigma 0.29 0.29 +2 Sigma 0.29 0.29 0.28 0.28 0.28 Mean 0.28 0.28 0.27 0.27 -2 Sigma 0.27 0.27 -3 Sigma 0.27 fl fl <? " I <t <t <t t'1 8' I!> §l if i <;-fJ' :!? ::? :;, ;::. §' 9§ 9§ 9§ 9§ 9§ "' :>:-,} ,} Pf "' "' "' "' "' Sf Sf .§> c§:i c§:i c§:i c§i c§l .§' "' .§' .§> .§' .§' .§> .§' 8' " " "' "' "' "' "' "' "' "' "' " " " " " " DATE PIC6B BETA BKG 2.25 +3 Sigma 2.25 2.09 +2 Sigma 1.99 1.93 1.77 1.61 1.45 Mean 1.45 0.. 1.3 u 1.14 0.98 -2 Sigma 0.92 0.82 -3 Sigma 0.66 Ip !Y <? <;-&' I t'1 ,§> if if ,§> 8' :!? :i-:i-::? ::? I!> :;, §' 9§ 9§ 9§ 9§ !;? §' "' Pf "' "' "' "' "' "' "' "' "' "' " Sf " Sf Sf .§> "' "' "' "' .§' "' .§> .§> .§' .§> .§' 8' @ @ @ 8' " " 8' <:) " " " " " " " " "
  • Denotes Outlier DATE Page 5148 of 5809 21070 20970 20870 2 20770 a.. 20670 (.) 20570 20470 20370 20270 20170 rP &' " 0,000592 0.0005502 0,0005089 0.000468 0,000426 0,000385 0,000344 0,0003023 0,000261 0.00022 " "
  • Denotes Outlier Page 5149of5809 ll!lllllllllllll/l/ DATE PIC6B BETA EFF Cross Talk i #' II #' #' #' l #' #' f r§ r§ r§ r§ t " " " " " 8' 8' 8' 8' " 8' 8' " " " " DATE -3 Sigma 00 (!J .s-.§' .<> !::> ii !;? 9l' 9l' " " " " " 8' 8' " 8' " " " " "

0... '-' 0... '-' 0.29 0.26 0.23 0.2 0.17 0.14 0.11 0.0848 0.0557 0.0266 21466 21412 21358 21034 PIC6C ALPHA EFF i I DATE 0.29 ____ +3Sigma0.29 0.29 0.28 0.28 0.28 0.28 0.28 0.27 0.27 t--t---t----1-+-t1H--+-C--t---t--+-t--t---t----t-t--t---t----t-t--t---t----1-t--t---t----t-t--t---t----1-t--t--+--if--t---t--+-t--t---t----t-t--t---t----i--3 Sigma 0.27 1.83 1.71 1.59 1.46 1.34 1.22 1.1 0.98 0.86 0.73 Page 5150of5809 24850 24745 24640 24535 0.0003604 0.0001102

  • Denotes Outlier Page 5151of5809 a.. (.) a.. (.) 0.37 0.34 0.3 0.27 0.23 0.2 0.17 0.13 0.0957 0.060908 10940 10907 10874 10841 10808 10775 10742 10709 10676 10643 1.85 1.68 1.5 1.33 1.15 I v y PIC7A ALPHA BKG v ! ! j PIC7A ALPHA EFF L h IN ll Iv PIC7A BETA BKG I 111111111111 .. } M 1111m 0.98 a.. 0.81 (.) 0.63 0.46 0.28 Page 5152of5809 A I r Ni Ml ! r Iv I' 1.1 11 11111111111 !I ul f 1111 1Pijl ll I *.1 J ! v II\ Generated 0912812016 +3 Sigma 0.37 +2 Sigma 0.32 Mean 0.2 -2 Sigma 0.08 -3 Sigma 0,03 +3 Sigma 10940 +2 Sigma 10900 I Mean 10780 11 -2 Sigma 10700 lj -3 Sigma 10610 +3 Sigma 1.85 +2 Sigma 1.56 ' Mean 0.98 ll -2 Sigma 0.4 -3 Sigma 0.11 21347 20882 20789 20603 f--!--l---1-+--+--+-f-+--+--1-+--+--+-f-+--+--1-+--+--+-f-+--+--1-+--+---+-+--+--+-f-+--+--+-+--+--+---if-+--+--1-H91---t--3 Sigma 20510 0.001603 0.000286 l--+--+---i-+--!--l---1-+--+---+-f-+--+---+-f-+--+--+-f-+--+--1-+--+--+---if-+--+---+-f-+--l---1-+--+--l---1-+--+--+---if-+--+---+-+---38igma00
  • Denotes Outlier Page 5153of5809 PIC?B ALPHA BKG Generated 0912812016 0... u 0... u 0... u 0,36 0.33 0.29 0.25 0.22 0.18 0.15 0.11 !r ! r I \A I J l } ' , 11 r l II j w N \ u 0.0733 0.0371 ill#!f !f !!l!!!!!!llllililllflllilllil!lfillli! DATE PIC?B ALPHA EFF 13843 13796 13749 13702 13608 13561 13467 #llil!!!f #i!ii!!!llll!iillllilllltllill!ii DATE PIC?B ALPHA EFF Cross Talk 0.27 0.27 0.27 0.26 !I\ \ 1/ 1f '\1 I 1 !Iv 1/ A I/ \ ! A .I IV \ J i 0.26 0.26 0.26 0.26 0.26 0.26 PIC?B BETA BKG 1.08 0.98 0.87 0.76 0.66 0.55 0.45 0.34 0.23 0.13 Page 5154of5809 +3 Sigma 0.36 +2 Sigma 0.3 Mean 0.18 -2 Sigma 0.06 -3 Sigma 00 +3 Sigma 0.27 +2 Sigma 0.27 Mean 0.26 -2 Sigma 0.26 -3 Sigma 0.25 a.. (.) PIC?B BETA EFF Generated09/28/2016 23010,----------------------------------------------------------+3Sigma23010 22922 22834 t-----------,---l----------,---t--t-lt--,f--------------------------------+2Sigma22900 22746 22658 22482 22394 22218 t-+--+---+-t-+--+---+-;t-+--+--+--+-+-+--+--+-+-+--+--+-+-+--+--+-+--+--+-;-+--+--+--+-+--+--+--+-+--+--+--+-+--+--+-i----3 Sigma 22130 0.002068-r----------------+----+-------------------------------------.-*3Sigma00 0,00189 ,._ ___ 0.00172 0,00155 0.00137 0,001025 0.000851 0.0005039 1-+-;--+--+-+--+-t--+---+-+--+-t--+---+-+--+-+--+-t--+---+-+---+-+--+-t--+---+-+--+-+--+--;r-+--+-+--+-+--+--;r---3 Sigma 00 e Denotes Outlier Page 5155of5809 0.. (.) 0.. (.) 0.. (.) 0.35 0.31 0.27 0.24 0.2 0.17 0.13 0.0923 0.0558 0.0193 10130 10100 10000 9940 9880 9819 9760 9690 9630 9570 0.31 0.31 0.3 0.3 0.29 0.28 0.28 0.27 0.27 1.12 01 0.88 0.76 0.65 0.53 0.41 0.29 0.18 0.0596 PIC7C ALPHA BKG J A I I Nl II ) J u \ V' 'I PIC7C ALPHA EFF I NV I \tv Vl 1r Generated 09127/2016 +3 Sigma 0.35 +2 Sigma 0.29 Mean 0.17 * -2 Sigma 0.04 -3 Sigma -0.017 -.------,------------------------------------------------------+3Sigma0.31 t-------,--+---------.---1t-----------------+---+-----------lt-----------+-+2Slgma0.3 l--+---+-+--+-l--+---t-+--+-+--+---t-+--+-l--+---+-+--+---l-+--+-+--+---t-+--+-l--+---t-+--+-l--+---t-+--+-1--+---t-4-*3 Sigma 0.26 PIC7C BETA BKG -.-----11Ht----------------------------------<.-.---------------------*3Sigma 1.12 t----tt-ttt---------------------------.-----iH--t--1!------++---------------*2SJgma 0.92 l-----------------------------------------------------------2Sigma0.14 f-+---+-+--+-l--+---i-+--+-t--+---l-+--+-f-+---+-+--+-11-+---t-+--+--l-+---t-t--+---l-+--+-t--+--ll-+---t-+--+-11-+--3 Sigma -0.058 !ii##!!##i!!!!!!!f llillilllllililillllllfl
  • Denotes Outlier DATE Page 5156of5809 0... () PIC?C BETA EFF Generated09/27/2016 21890,------.:;__.:;_-=._:=-=:....::.-=---=--=:..:...------------------------------------------+3 Sigma21890 21727 21401 21238 20912 20749 20586 20423 f---t--+-1f-+--t--+-f--+--+---f-+--t--+-1-+--+--+-f--+--+-1-+--+--+-+--+--+-1-+--+--+-f--+--+---f-+--t--+-+--+--+-1f-+-__.H--3 Sigma 20260 o.000656.-----------------------------------------------------------+3Sigma00 0,0006034 0.0005505 0.000498 0.000445 0,000339 0.000286 0.000233 Sigma 00 0,0001804 f--+--+--t-t-+--+---;-+-+-+---;-+-+-+---;,--+--+--+-f--+--+--t-+--+--+-f--+--+--+-t-+--+--t-t--+--+---if--+--+--t-+-+--+---;-+--3 Sigma 00
  • Denotes Outlier Page 5157of5809 a.. (.) a.. (.) a.. (.) 0,35 0.31 0.28 0.24 0.2 0.17 0.13 0.0968 0.06086 0.02491 10916 10878 10802 10764 10688 0.27 0.27 0.27 0.27 0.26 0.26 0.26 0.26 1.33 1.22 1.12 1.01 0.91 0.8 0.7 0.59 0.49 y 0.39 Page 5158of5809 PIC70 ALPHA BKG ! * ' l PIC70 ALPHA EFF PIC7D BETA BKG I i r! L Kl w Generated 0912812016 +3 Sigma 0.35 +2 Sigma 0.29 \J t ,! Mean0.17 l i\
  • ti t fy -2 Sigma 0.05 -3 Sigma -0.011 +3 Sigma 1.33 +2Sigma1.15 ! IU ! ! r Mean 0.8 II wv -2 Sigma 0.46 -3 Sigma 0.28 25580 PIC?D BETA EFF Generated 0912812016 +3 Sigma 25580 25336 +2 Sigma 25200 25092 24848 0.. 24604 24360 24116 23872 I Wv h f i\ V\i\ I ! I j l ( II II vi I w li \ Mean 24360 23628 -2 Sigma 23500 23384 -3 Sigma 23140 0.0007069 +3 Sigma 00 I i 0.0006502 +2 Sigma 00 0.000593 0.000423 \A. ,/ rd \ I ! f LI n ! ! VJ v r 1f I 11 \J l 0.000537 0.00048002 Mean 00 0.000367 0.0003099 0.000253 -2 Sigma 00 0.000196 -3 Sigma 00
  • Denotes Outlier Page 5159 of 5809 0.37 PICBA ALPHA BKG Generated 0912812016 +3 Sigma 0.37 0.34 +2 Sigma 0.32 0.31 2 0.28 0.. 0.24 () 9.21 0.18 0.15 \ II \ n ' II I Nj I\ ii y Mean0.21 0.12 -2 Sigma 0.11 0.08604 -3 Sigma a.as PICBA ALPHA EFF 11320 11276 11232 11188 2 11144 0.. 11100 () 11056 11012 10968 10924 0.25 0.25 0.25 0.25 0.25 0.24 0.24 0.24 PICBA BETA BKG 1.59 +3 Sigma 1.59 1.47 +2 Sigma 1.39 1.35 1.23 1.11 2 0.99 0.. 0.87 () 0.75 ILi ufu 1. 1L1 J 1v11 I\ r
  • II' Mean 0.99 0.63 -2 Sigma 0.59 0.51 -3 Sigma 0.39 Page 5160 of 5809 0.00183,.--------------------------ilf--------------------------il*f------<.-+3 Sigma 00 0.00168 0.00152 ttt-+'i--tt--tt-------------ir--tt-----++----llit---------------l------------,f----llf--------l-+2Sigma00 0.00137 0.00121 0.0009007 0.000745 0.00059 t---------------------------------------------------------+--*2Sigma00 0.0004341 t--+--+--l-+-+--+f--f--+--+--+-+-+--+---'f--+--+--+-+-+--+---'f--+--+--l-+--+---+-+-+--+-t--+--+--l-+--+--+-f--+--+---l-+--+---+--3Sigma00
  • Denotes Outlier Page 5161of5809 0.33 PIC8B ALPHA BKG Generated 0911912016 +3 Sigma 0.33 0.29 +2 Sigma 0.26 0.25 0.21 0... 0.18 0 0.14 0.1 0.0637 v II 11 ff\ I II I fi I I It " v I '\ v l'\J /I( \ \ LI IM Mean 0.14 0.0262 -2 Sigma 0.01 -0.0112 -3 Sigma -0.049 PIC8B ALPHA EFF 9500 0.29 ,----------------------------------------*------------------+3Sigma0.29 0.28 0.28 0.28 0.28 0.27 0.27 0.27 t--------;f----'---------------------------------------;f---4-------2Sigma0.27 0.26 t--+-;-+--+-f--+---+-+--+-;-+--+-f--+--+-+--+---+-+--+-;-+--+-;f-+--+-+--+---+-+--+-;-+--+-+--+---+-+--+-;-+--+--3 Sigma 0.26 PIC8B BETA BKG 1.04 0.93 0.82 0.7 0,59 0.47 0... 0.36 0 0.25 0.13 0.02054
  • Denotes Outlier Page 5162 of 5809 22168 22056 0.0006605 0.000566 0.000519 0.000425 0.000377 0.000283
  • Denotes Outlier Page 5163of5809 0.37 PIC8C ALPHA BKG Generated 09/2812016 +3 Sigma 0.37 0.34 +2 Sigma 0.32 0.31 0.29 0... 0.26 (.) 0.24 0.21 0.18 I! 1Ai \ I IM -\ IV 1( 1111 Mean 0.24 0.16 -2 Sigma 0.15 0.13 -3 Sigma 0.11 PIC8C ALPHA EFF 22050 21932 21814 21696 21578 0... 21460 (.) 21342 21224 21106 20988 0.3 0.3 0.29 0.29 0.28 0.27 0.26 0.26 0.25 PIC8C BETA BKG 2.19 +3 Sigma 2.19 2.05 +2 Sigma 1.97 1.92 1.79 1.65 1.52 0... 1.38 (.) 1.25 1! !! 't H d1! M j M . I "! I II n111 r'W! II I 1111!\ r Mean 1.52 1.12 -2 Sigma 1.07 0.98 -3 Sigma 0.85 Page 5164of5809 PICBC BETA EFF Generated09/28/2016 26940,------------------------------------------------------------+3Sigma26940 a.. (.) 26655 26085 25800 25230 24945 24375 f-+--+---l-+---+---+-t--+--+-t-+--+---l-+---+---+-t--t--+-f-+--+---ir+--+---ir+--+-i-+---+---+-t-+--+---,r-+--+---ir+--+-i--Hlt-t--3 Sigma 24090
  • Denotes Outlier Page 5165of5809 0.4 0.36 0.32 0.28 a.. 0.24 u 0.2 0.16 0.12 0.08311 0.0433 PICBD ALPHA EFF 18050 17888 17726 17564 17402 a.. 17240 u 17078 16916 16754 16592 PICBD BETA BKG 2.73 2.42 2.11 1.81 1.5 1.19 a.. 0.89 u 0.58 0.27 -0.0341 Page 5166 of 5809
?! 0.... u 44163 43924 43446 43207 42729 0.00451 0.00352 0.00303 0.002043 0.00155 0.001057 t-----------------------------------------------------------2 SigmaOO 0.000563 t--+--+-t--+--t--t-+--+--+-t--+--+-+-t--t--t--t-+--t--t-+--+-+-t--+--+-tr-+--+-+-t--t--t--t-+--+-+-t--+--+-t-+--+-t--3 Sigma 00
  • Denotes Outlier Page 5167of5809 0.38 PIC9A ALPHA BKG Generated 0912012016 +3 Sigma 0.38 0.34 11 +2 Sigma 0.31 0.3 0.27 Cl. 0.23 0 0.19 0.15 0.12 n 1! Ni! I I* I! l \ v Ii J\ I ' . II" n Mean 0.19 0.0783 -2 Sigma 0.07 0.04093 -3 Sigma 00 PIC9A ALPHA EFF 11100 11038 10976 10914 10852 Cl. 10790 0 10728 10666 10604 10542 0.31 0.3 0.3 0.29 0.28 0.27 0.27 0.26 PIC9A BETA BKG 1.74 +3Sigma1.74 1.57 +2 Sigma 1.46 1.4 1.24 , h n I I i r r ,, IV 0.9 Cl. 0.74 0 0.57 0.41 Mean 0.91 -2 Sigma 0.35 0.24 -3 Sigma 0.07 Page 5168of5809 PIC9A BETA EFF Generated09/20/2016 21790,-----------------------------------------------------------+3Sigma21790 21690 20890 f--+---t-+--+---+-+--+---+-+--+---t-+--+---+-+--+--t-+--+-t--+--+-t--+---t-+--+---+-+--+---+-+--+--tt-+--+-t--+--+-t--+--t--3 Sigma 20790
  • Denotes Outlier Page 5169of5809 PIC9B ALPHA BKG Generated09/28/2016 ,-------------------------------------------------------<1-----40-+3Sigma0.38 0.38 0.34 0.3 t----------------------------------------+---------------+i-+-+-*-+2Sigma0.31 ::?! 0.26 0... 0.22 (.) 0.18 0.14 0.1 0.0652 0.0262 t-+--+--+-+--+--+-t-+--+-t-+--+--+-+--+--+-t-+--+--+-+--+--+-t-+--+--+-t--+--+-t-+--+--+-+--+--+-t-+--+---'t-+--+--+--3Sigma-0.013 PIC9B ALPHA EFF 13870 ,-----------------------------------------------------------*3Sigma13870 13736 13602 13468 ::?! 13334 0... 13200 (.) 13066 12932 12798 t-------------------------------+-'---------------------------2Sigma 12800 12664 ,-----------------------------------------------------------+3Sigma0.43 r----------------------------------------------------------*2Sigma0.38 t-----------------------------------------------------------2Sigma0.16 f-+--+--+-+--+--+-t--+--+-t-+--+,---r-+--+--+-t-+--+--+,---+--+---+-t-+--+,---t-+--+--+-+--+--+-t-+--+--+t-+--+--+-+--+--+-t---35igma0.11 PIC9B BETA BKG 1.75 +3Slgma 1.75 1.58 +2 Sigma 1.47 1.41 1.24 1.07 ::?! 0.9 0... 0.73 (.) 0.56 0.38 d \ ,I I 'l 'l'I 'l ! r IJ 1 Mean 0.9 -2 Sigma 0,33 0.21 -3 Sigma 0.04 Page 5170 of 5809 a.. () PIC98 BETA EFF Generated09/28/2016 22590-,------------------'-'----------.,---------;------------------------+3 Sigma 22590 22520 22450 f---.---++-------++-------------+-1t---------ll----------------fl-----ll--+2Sigma22500 22380 22310 22170 22100 22030 21960 l-+--+--+-l-+--+--+-l-+--+-+-11-+--+--+-1-+--+--+-,1-+--+--t-1-+--+--t-l-+--+-+-1-+--+--t-1-+--+--t-t-+--+--t-t-+--+-35igma21890 o.002eos-..------------------,-----------------------------------------*3Sigmaoo 0,002581 tt---++--+.--------+-----++----+-------------------+---+--------+-1--------*2Sigma00 0.00236 0.00213 0.001907 0.00146 0.00123 0.000785
  • Denotes Outlier Page 5171 of5809 0.36 0.33 0.29 0.25 0.. 0.21 u 0.17 0.13 0.0917 0.0527 0.0137 10420 10400 10300 10200 10100 0.. 10100 u 10000 9940 9660 9610 0.27 0.27 0.26 0.26 0.26 0.25 0.25 0.25 0.24 1.76 1.59 1.42 1.25 1.08 0.91 0.. 0.74 u 0.57 0.4 0.24 PIC9C ALPHA BKG J nl 1 I I J f 11 N ,, w PIC9C ALPHA EFF PIC9C BETA BKG ! 1! Ir *w Generated 0911712016 +3 Sigma 0.36 +2 Sigma 0.3 I II Mean 0.17 J v* -2 Sigma 0.04 -3 Sigma -0.025 .. f----------------------------------------------------------*2Sigma0.35 l--+--+----l-+-+--+-l--+--+----1-+--+---+-+-+--+---'1--+--+---+-t--t--+--t-t--+--+-t--t--+--t-T--+---+-t-+--+--t-T--+---+-t--+--+--+-3 Sigma 0.07 Page 5172 of5809 0... u PIC9C BETA EFF Generated09/17/2016 22000,-----"--'=--=---=--"=--=-=--=---=--=:.::.......::... ________________________________________ +3 Sigma22000 21916 21832 ._-+---+-+-+--+-f-+--+---l-+--+---+-+-+--+-+-+--+-+-+--+-f-+--+---l-+--+---+-+--+---+-+--+---+-+--+--+-+-+--+---lC-+--+-+-3S!gma211BO
  • Denotes OuU!er Page 5173 of 5809 0.37 PIC9D ALPHA BKG Generated 09/19/2016 +3 Sigma 0.37 0.33 +2 Sigma 0.31 0.3 0.26 0.. 0.23 () 0.19 0.16 ! !I l ,, I I
  • r I t J ) Mean 0.19 0.12 0.085008 -2 Sigma 0.07 0.0497 -3 Sigma 0.01 PIC9D ALPHA EFF 11110 11070 11030 10990 10950 0.. 10910 () 10870 10830 10790 10750 0.28 +3 Sigma 0.28 0.27 +2 Sigma 0.27 0.27 1d1 f\ I\ n n .! A v J\ I J ,/ Ji l I J N ii 0.27 0.27 0.27 Mean 0.27 0.26 0.26 0.26 -2 Sigma 0.26 0.26 -3 Sigma 0.26 PIC9D BETA BKG 2.01 1.83 1.65 1.47 1.29 1.11 0.. 0.93 () 0.75 0.57 0.39 Page 5174 of5809 a_ .() 25623 25524 25326 25227 25128 25029 0.004303 0.00356 0.00319 0,00246 0,002086 0,00135 #!i#!!!!!!!!!!l!lliilllllllilll!fl!ll/11/ DATE
  • Denotes Outlier Page 5175 of5809 Page 5176of5809 RAD Standards Traceability Standardization of Strontium Carrier 2414995 v1.2.1 Analyst KSD1 Standard Information Weight of Weight of crucible Isotope Strontium Std# carrier added (g) or filter (g) Serial Number 2414995 1 1.0104 0.0242 Amount of Std. (ml) 1.0 2 1.0136 0.0244 Standard Prepared 6/3/2016 3 1.0191 0.0242 4 1.0214 0.0244 Parent Information Parent Serial# I 2130147.5 Parent Exp. Date I 6/3/2018 Standardization Rule A satisfactory standardization is obtained when results give a standard deviation of less than 1.0% of the mean value. Weight of crucible Weight of or filter+ ppt. (g) ppt. (g) 0.0388 0.0146 0.0392 0.0148 0.0390 0.0148 0.0391 0.0147 Mean Value (mg/ml) = Stdev (mg/ml) = 1.0% of Mean Value= Expiration Date mg Strontium/ml 14.60 14.80 14.80 14.70 14.73 +/-0.10 0.147250 Pass 6/3/2017 Mean Value (mg/1.0ml) = 14.73 J .. mg Strontlum/g 14.45 14.60 14.52 14.39

& Ziegler Analytics 1380 Seaboard Industrial Blvd. Atlanta, Georgia 3031 S Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com ::,. __ ;,!: Customer: P.O. No.: CERTIFICATE OF CALIBRATION Standard Radionuclide Source 78352-278 Sr-90 10 mL Liquid in Flame Sealed Vial General Engineering Labs/Charleston, SC 7312 RD, Item 3 This standard radionuclide source was prepared gravimetrically from a calibrated master solution. The master solution was calibrated by liquid scintillation counting. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. The nuclear decay rate and assay date for this source are given below . .ANALYTICS maintains traceability to the National Institute of Standards and Technology through Measurements Assurance Programs as described in USNRC Reg. Guide 4.15, Revision 1. Isotope: Sr-90 Activity (Bq): 3.856 E5 Half-Life: 28.79 years Calibration Date: October 1, 2008 12:00 EST Relative Expanded Uncertainty (k=2): 1.7% Comments: Impurities: y-impurities <0.1 % 10.41484 grams O. lM HCl solution with 30 Sr carrier. NOTE: This source also contains Y-90 in secular equilibrium with Sr-90. The Y-90 activity is equal to the Sr-90 activity. Since Sr-90 and Y-90 both decay 100% by beta emission, the total beta emission rate for the source is twice the certified Sr-90 activity. The half-life for Y-90 is 64.08 hours. ./'-" ' Source Prepared By: W. Mao, Radiochemist QA Approved: (1oA-k<--1 D:M:MantgameJ:Y:o1u .. Date: _/_o-+-/_3_,_/ef_..___ I Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Strontium-90 Parent Code: 1243 Prepared By: Daniel Roy Prepared By: Daniel Roy Prep Date: 12/19/2008 Carrier Cone: O.lMHCL Verification Date: 09/27/2016 Reference Date: 10/01/2008 Expiration Date: 09/27/2017 Ampoule Mass (g): 10.41484 g Primary Code: 1243-A Uncertainty: +/-.85 % Dilution(mL): lOOmL LogBookNo: RC-S-048-124 Mass of Parent(g): 10.2164 g Density(g/mL): 0.9991 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) * (Dilution Vol))= Parent Activity (dpm/g) (10.2164 g) * (385600 Bq) * (60 dpm/Bq) I (10.41484 g

  • 100 mL) = 226951.7634 dpm/rnL (10.2164 g) * (385600 Bq) * (60 dpm/Bq) I ( 0.9991 g/mL)/ (10.41484 g
  • 100 rnL) = 227146.2010 dpm/g Secondary Standards Prep Date Preparer Mass Dilution Code Cone dpm/mL Verification Expiration Primary (mL) Date Date 01/21/2010 Bethany 2.2467 1000 1243-B 510.329369 01/21/2010 01/21/2011 Fi em dpm/mL 08/03/2010 Bethany 2.5604 1000 1243-C 581.5851 08/03/2010 08/03/2011 Fiem dpm/rnL 01/12/2011 Bethany 2.4946 1000 1243-D 566.6389 01/12/2011 01/12/2012 Fiem dpm/mL 08/12/2011 Tim 3.3115 100 1243-G 18.7877 03/26/2014 03/25/2015 Chandler dpm/mL 08/17/2011 Tim 2.5541 100 1243-H 14.49064 03/26/2014 03/25/2015 Chandler dpm/mL 06/21/2011 Tim .0235 100 1243-E 53.37936 03/19/2014 06/20/2014 Chandler dpm/mL 07/05/2011 Bethany 2.6072 1000 1243-F 592.2156 07/05/2011 07/05/2012 Fiem dpm/mL 01/31/2012 Gregory 2.6792 1000 1243-I 608.5701 01/31/2012 01/31/2013 Ramsay dpm/ml Page 5179 of 5809 08/29/2012 Bethany Fiem 02/12/2013 Gregory Ramsay 12/04/2013 Gregory Ramsay 08/11/2014 Gregory Ramsay 05/06/2015 Gregory Ramsay 12/18/2015 Gregory Ramsay 08/30/2016 Christina Kimball 09/27/2016 Bethany Fiem GEL Laboratories LLC Version 1.0 9/18/2000 Page 5180of5809 2.6799 1000 2.6526 1000 2.5347 ' 1000 2.7006 1000 2.5102 1000 2.5762 1000 .068 250 2.6337 1000 1243-J 608.729104 09/14/2012 09/1112013 dpm/mL 1243-K 602.528 01/15/2014 01/15/2015 dpm/ml 1243-L 575.747476 12/04/2013 12/04/2014 dpm/ml 1243-M 613.431 08/12/2014 08/12/2015 dpm/mL 1243-N 570.1824 05/06/2015 05/06/2016 dpm/mL 1243-0 585.174 12/18/2015 12/18/2016 dpm/rnL 1243-P 61.7838 09/07/2016 09/07/2017 dpm/mL 1243-Q 598.235 0912712016 09/2712017 dpm/mL 0 ....., VI 00 0 \0 Verification for Sr-90 Standard 1243-0 v1.0.2 Instrument BLUE Analvst BXF1 Verification Prep Date 12/18/2015 Standard Information Quench Gross . Bkg dpm/mL 509.17 2.755468033 Isotope Serial Number lsotooe Halflife Reference Date Ref. Act. (DPM/mL) Amount of Std. <mU Standard Prep Date Sr-90 Std# Count Date 1243-0 1 12/30/2015 28.9000 y 2 12/30/2015 10/1/2008 3 12/30/2015 585.174 1.0 Net 12/18/2015 Std # cpm 1 1033.40 2 1023.00 3 1024.80 Verification Rules Number cpm 88.50 1073.20 90.20 1062.80 89.60 1064.60 Calculated Standard Avg. Eff. dpm/ml 2.017144 512.31 2.017144 507.15 2.017144 508.04 cpm 39.80 39.80 39.80 Measured dpm 512.31 507.15 508.04 Mean Value= Stdev= Certificate.Value*= Two sigma= 10 %of Mean= Rule A (Pass/Fail) %Recovery Rule B (Pass/Fail) Expiration Date Rule A = The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value.
  • Certificate Value is decay corrected to Count Date. 491.8 5.511 50.917 Pass 103.52% Pass 12/18/2016 The analyst prepared three standard verification sources for Sr-90 source 1243-0 by transferring 1 mL portions of the standard into glass liquid scintillation vials. 10 mL of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial was prepared in a similar fashion using 10 mL of Ecoscint Ultra liquid scintillation cocktail. The standard verification vials and background source were dark adapted for at least two hours and counted on LSCBLUE for Sr-90 source standard verification. The Sr-90 efficiency calibration which was used for verification calculations was performed on 12/18/2015 using Sr-90 source 1244-A. Standard results for each verification source was calculated as follows: RAD-M-001 Source dptn/mL = (A -B)/(C)(D) where: A Ver. source cpm, B BKGcpm, C System efficiency (cpm/dpm), and D volume used for standard verification.

-. 9 Eckert & Ziegler Analytics CERTIFICATE OF CALIBRATION Standard Radionuclide Source

  • 82898-278 5 mL Liquid in Flame Sealed Vial Customer: GEL Labs, LLC P.O. No.: 7344 RD, Item 1 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by Eckert & Ziegler Analytics. The master solution was calibrated by liquid scintillation counting. Radionuclide purity and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. The nuclear decay rate and reference date for this source are given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this source was produced in accordance with the HPS accreditation requirements. Customers may report any concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101. Isotope* Th-230 Half-Life, Days 2.753E+07 Activity (Bq) 3.942E+04 Uncertainty* , % Type UA Us U 0.1 0.9 1.8 Reference Date (12:00 PM EST) 07129/2010 *Uncertainty: U -Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results." Comments: Impurities: y-impurities < 0.1 %, a-impurities< 0.04 %. 5.10422 grams O.SM HN03 solution. Source Prepared W. Mao, Radiochemist QA Approved: Single Isotope Certificate, Rev 1 9/28/2009 Corporate Office Date: -::i---a..r ... Jf) Rl.-S-O<.,o-o&./O Laboratory Page S l Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318 Standard Traceability Log Rad A Solution Material Info Source Material Info
  • Isotope: Thorium-230 Parent Code: 1493 Prepared By: Bethany Fiem Prepared By: Gregory Ramsay Prep Date: 06/24/2015 Carrier Cone: 0.5MHN03 Verification Date: 09/27/2016 Reference Date: 07/29/2010 Expiration Date: 09/27/2017 Ampoule Mass (g): 5.10422 g Primary Code: 1493-A Uncertainty: +/-1.8 % Dilution(mL): lOOmL LogBookNo: RC-S-060-040 Mass of Parent(g): 5.0802 g Density(g/mL): 1.0011 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity ( dpm/g) (5.0802 g) * (39420 Bq) * (60 dpm!Bq) I (5.'10422 g
  • 100 mL) = 23540.6958 dpm/mL (5.0802 g) * (39420 Bq) * (60 dpm/Bq) I ( 1.0011 g/mL)/ (5.10422 g
  • 100 mL) = 23515.7691 dpm/g Prep Date Preparer 06/24/2015 Bethany Fiem 09/27/2016 Bethany Fiem GEL Laboratories LLC Version 1.0 9/18/2000 Page 5183 of 5809 Mass Primary 11.3156 11.4091 Secondary Standards Dilution Code Cone Verification Expiration (mL) dpm/mL Date Date 1000 1493-B 266.095 06/08/2016 06/08/2017 dpm/mL 1000 1493-C 268.294 09/27/2016 09/27/2017 dpm/mL Verification for th-230 Standard 1493-B v1.0.2 Instrument BLUE Analyst TC1 Verification Prep Date 6/8/2016 Standard Information Quench Gross Bkg dpm/ml 269.76 3.444745088 Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (DPM/ml) Amount of Std. (ml) Standard Prep Date Th-230 Std# Count Date 1493-B 1 6/8/2016 7.5380E+04 Y 2 6/8/2016 7/29/2010 3 6/8/2016 266.095 1.0 Net 6/24/2015 Std# cpm 1 273.93 2 267.73 3 273.53 Verification Rules Number cpm 95.10 312.60 95.30 306.40 95.20 312.20 Calculated Standard Avg. Eff. dpm/ml 1.007294 271.95 1.007294 265.79 1.007294 271.55 cpm 38.67 38.67 38.67 Measured dpm 271.95 265.79 271.55 Mean Value= Stdev= Certificate Value* = Two sigma= 10%ofMean= Rule A (Pass/Fail) % Recovery Rule B (Pass/Fail) Expiration Date Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value.
  • Certificate Value is decay corrected to Count Date. 266.1 6.889 26.976 Pass 101.38% Pass 6/8/2017 The analyst prepared three standard verification sources for Th-230 source 1493-B by transferring 1 ml portions of the standard into glass liquid scintillation vials. 1 O ml of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial was prepared in a similar fashion using 1 o ml of Ecoscint Ultra liquid scintillation cocktail. The standard verification vials and background source were dark adapted for at least two hours and counted on lSCBlU E for Th-230 source standard verification. The Th-230 efficiency calibration which was used for verification calculations was performed on 6/8/2016 using Th-230 source 1759-A. Standard results for each verification source was calculated as follows: RAD-M-001 Source dpm/ml = (A -B)/(C)(D) where: A B c D Ver. source cpm, BKGcpm, System efficiency (cpm/dpm), and volume used for standard verification.

Runlogs Page 5185of5809 Instrument Run Log Instrument Type: GFPC Batch ID: 1597795 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type

  • 405235001 SAMPLE KSD1 PIC11C SEP-17-16 15:50:52 DONE Tuffryn Filter 01-APR-16 00:00 405235003 SAMPLE KSD1 PIC12A SEP-17-16 15:51:00 DONE Tuffryn Filter 01-APR-16 00:00 405235004 SAMPLE KSD1 PIC12B SEP-17-16 15:51:04 DONE Tuffryn Filter 01-APR-16 00:00 405235005 SAMPLE KSD1 PIC12C SEP-17-16 15:51:07 DONE Tuffryn Filter 01-APR-16 00:00 405235006 SAMPLE KSD1 PIC12D SEP-17-16 15:51:13 DONE Tuffryn Filter 01-APR-16 00:00 405235007 SAMPLE KSD1 PIC13B SEP-17-16 15:51:17 DONE Tuffryn Filter 01-APR-16 00:00 405235008 SAMPLE KSD1 PIC13D SEP-17-16 15:51:20 DONE Tuffryn Filter 01-APR-16 00:00 405235009 SAMPLE KSD1 PIC14C SEP-17-16 15:51:24 DONE Tuffryn Filter 01-APR-16 00:00 405235010 SAMPLE KSD1 PIC14D SEP-17-16 15:51:27 DONE Tuffryn Filter 01-APR-16 00:00 405235016 SAMPLE KSD1 PIC10A SEP-17-16 16:31:16 DONE Tuffryn Filter 01-APR-16 00:00 405235011 SAMPLE KSD1 PIC1A SEP-17-16 16:32:09 DONE Tuffryn Filter 01-APR-16 00:00 ' 405235012 SAMPLE KSD1 PIC1B SEP-17-16 1'6:32:14 DONE Tuffryn Filter 01-APR-16 00:00 405235013 SAMPLE KSD1 PIC1C SEP-17-16 16:32:17 DONE Tuffryn Filter 01-APR-16 00:00 405235014 SAMPLE KSD1 PIC4B SEP-17-16 16:32:22 DONE Tuffryn Filter 01-APR-16 00:00 405235015 SAMPLE KSD1 PIC5A SEP-17-16 16:32:25 DONE Tuffryn Filter 01-APR-16 00:00 405235017 SAMPLE KSD1 PIC14A SEP-17-16 16:34:48 DONE Tuffryn Filter 01-APR-16 00:00 1203625399 DUP KSD1 PIC6A SEP-17-16 16:39:23 DONE Tuffryn Filter 01-APR-16-00:00 1203625400 LCS KSD1 PIC6B SEP-17-16 16:39:25 DONE Tuffryn Filter 01-APR-16 00:00 405235018 SAMPLE KSD1 PIC3B SEP-17-16 16:40:28 DONE Tuffryn Filter 01-APR-16 00:00 405235019 SAMPLE KSD1 PIC5B SEP-17-16 16:40:32 DONE Tuffryn Filter 01-APR-16 00:00 405235020 SAMPLE KSD1 PIC5C SEP-17-16 16:40:38 DONE Tuffryn Filter 01-APR-16 00:00 1203625398 MB KSD1 PIC5D SEP-17-16 16:40:43 DONE Tuffryn Filter 01-APR-16 00:00 405235002 SAMPLE KSD1 PIC6C SEP-19-1611:55:11 DONE Tuffryn Filter 01-APR-16 00:0.0 Page 5186 of 5809 Instrument Run Log Instrument Type: GFPC Batch ID: 1597796 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID
  • Type 405235026 SAMPLE KSD1 PIC6C SEP-17-16 15:33:38 DONE Tuffryn Filter 01-APR-16 00:00 405235027 SAMPLE KSD1 PIC7A SEP-17-16 15:33:41 DONE Tuffryn Filter 00:00 405235028 SAMPLE KSD1 PIC7B SEP-17-16 15:33:45 DONE Tuffryn Filter 01-APR-16 00:00 -405235029 SAMPLE KSD1 PIC7C SEP-17-16 15:33:47 DONE Tuffryn Filter 01-APR-16 00:00 405235030 SAMPLE KSD1 PIC7D SEP-17-16 15:33:51 DONE Tuffryn Filter 01-APR-16 00:00 405235031 SAMPLE KSD1 PIC8A SEP-17-16 15:33:56 DONE Tuffryn Filter 01-APR-16 00:00 405235032 SAMPLE KSD1 PIC8B SEP-17-16 15:34:00 DONE Tuffryn Filter 01-APR-16 00:00 405235034 SAMPLE KSD1 PIC8D SEP-17-16 15:34:08 DONE Tuffryn Filter 01-APR-16 00:00 405235021 SAMPLE KSD1 PIC58 SEP-17-16 15:34:17 DONE Tuffryn Filter 01-APR-16 00:00 405235022 SAMPLE KSD1 PIC5C SEP-17-16 15:34:20 DONE Tuffryn Filter 01-APR-16 00:00 405235023 SAMPLE KSD1 PIC5D SEP-17-16 15:34:22 DONE Tuffryn Filter 01-APR-16 00:00 405235035 SAMPLE KSD1 PIC9A SEP-17-16 15:36:47 DONE Tuffryn Filter 01-APR-16 00:00 405235036 SAMPLE KSD1 PIC9B SEP-17-16 15:36:51 DONE Tuffryn Filter 01-APR-16 00:00 405235037 SAMPLE KSD1 PIC9C SEP-17-16 15:36:56 DONE Tuffryn Filter 01-APR-16 00:00 405235038 SAMPLE KSD1 PIC9D SEP-17-16 15:37:00 DONE Tuffryn Filter 01-APR-16 00:00 405235039 SAMPLE KSD1 PIC10B SEP-17-16 15:37:05 DONE Tuffryn Filter 01-APR-16 00:00 405235040 SAMPLE KSD1 PIC10C SEP-17-16 15:37:10 DONE Tuffryn Filter 01-APR-16 00:00 1203625401 MB KSD1 PIC10D SEP-17-16 15:37:15 DONE Tuffryn Filter 01-APR-16 00:00 1203625402 DUP KSD1 PIC11A SEP-17-16 15:45:43 DONE Tuffryn Filter 01-APR-16 00:00 1203625403 LCS KSD1 PIC11B SEP-17-16 15:45:47 DONE Tuffryn Filter . 01-APR-16 00:00 405235025
  • SAMPLE KSD1 PIC5A. SEP-19-16 11 :54:29 DONE Tuffryn Filter 01-APR-16 00:00 405235033 SAMPLE KSD1 PIC5D SEP-19-16 15:23:45 DONE Tuffryn Filter 01-APR-16 00:00 405235024 SAMPLE KSD1 PIC2A SEP-21-16 10:46:02 DONE Tuffryn Filter 01-APR-16 00:00 Page 5187 of 5809 Instrument Run Log Instrument Type: GFPC Batch ID: 1597803 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID
  • Type
  • 1203625408 MB KSD1 PIC7C SEP-22-16 17:18:15 DONE Tuffryn Filter 01-APR-16 00:00 1203625409 DUP KSD1 PIC7D SEP-22-16 17:18:17 DONE Tuffryn Filter 01-APR-16 00:00 1203625410 LCS KSD1 PIC8A SEP-22-16 17:18:20 DONE Tuffryn Filter 01-APR-16 00:00 405235059 SAMPLE KSD1 PIC7A SEP-22-16 17:18:30 DONE Tuffryn Filter 01-APR-16 00:00 405235060 SAMPLE KSD1 PIC7B SEP-22-16 17: 18:34 DONE Tuffryn Filter 01-APR-16 00:00 405235056 SAMPLE KSD1 PIC6A SEP-22-16 17:19:50 DONE Tuffryn Filter 01-APR-16 00:00 405235041 SAMPLE KSD1 PIC1A SEP-22-16 17:20:11 DONE Tuffryn Filter 01-APR-16 00:00 405235045 SAMPLE KSD1 PIC2B SEP-22-16 17:20:21 DONE Tuffryn Filter 01-APR-16 00:00 405235046 SAMPLE KSD1 PIC2C SEP-22-16 17:20:23 DONE Tuffryn Filter 01-APR-16 00:00 405235048 SAMPLE KSD1 PIC3C SEP-22-16 17:20:28 DONE Tuffryn Filter 01-APR-16 00:00 405235049 SAMPLE KSD1 PIC3D SEP-22-16 17:20:33 DONE Tuffryn Filter 01-APR-16 00:00 405235050 SAMPLE KSD1 PIC4A SEP-22-16 17:20:34 DONE Tuffryn Filter 01-APR-16 00:00 405235051 *SAMPLE KSD1 PIC4C SEP-22-16 17:20:36 DONE Tuffryn Filter 01-APR-16 00:00 405235052 SAMPLE KSD1 PIC4D SEP-22-16 17:20:39 DONE Tuffryn Filter 01-APR-16 00:00 405235054 SAMPLE KSD1 PIC5C SEP-22-16 17:20:45 DONE Tuffryn Filter 01-APR-16 00:00 405235042 SAMPLE KSD1 PIC1B SEP-22-16 17:20:59 DONE Tuffryn Filter 01-APR-16 00:00 405235043 SAMPLE KSD1 PIC1D SEP-22-16 17:21:04 DONE Tuffryn Filter 01-APR-16 00:00 405235047 SAMPLE KSD1 PIC3B SEP-22-16 17:21:09 DONE Tuffryn Filter 01-APR-16 00:00 405235055 SAMPLE KSD1 PIC5D SEP-22-16 17:21:16 DONE Tuffryn Filter 01-APR-16 00:00 405235057 SAMPLE KSD1 PIC4C SEP-23-16 11:21:51 DONE Tuffryn Filter 01-APR-16 00:00 405235058 SAMPLE KSD1 PIC5A SEP-23-16 11 :21 :54 DONE Tuffryn Filter 01-APR-16 00:00 405235053 SAMPLE KSD1 PIC3D SEP-23-16 11 :36:16 DONE Tuffryn Filter 01-APR-16 00:00 405235044 SAMPLE KSD1 PIC1B SEP-23-16 13:27:51 DONE Tuffryn Filter 01-APR-16 00:00 Page 5188of5809 Instrument Run Log Instrument Type: GFPC Batch ID: 1597804 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type .. ' 1203625412 MB BXF1 PIC7C SEP-27-16 19:37:52 DONE Tuffryn Filter 01-APR-16 00:00 405235075 SAMPLE BXF1 PIC6A SEP-27-16 15:38:00 DONE Tuffryn Filter 01-APR-16 00:00 405235077 SAMPLE BXF1 PIC7A SEP-27-16 15:38:07 DONE Tuffryn Filter 01-APR-16 00:00 405235078 SAMPLE BXF1 PIC7B SEP-27-16 15:38:10 DONE Tuffryn Filter 01-APR-16 00:00 405235061 SAMPLE BXF1 PIC1A SEP-27-16 15:39:30 DONE Tuffryn Filter 01-APR-16 00:00 405235062 SAMPLE BXF1 PIC1B SEP-27-16 15:39:32 DONE Tuffryn Filter 01-APR-16 00:00 405235065 SAMPLE BXF1 PIC2A SEP-27-16 15:39:41 DONE Tuffryn Filter 01-APR-16 00:00 405235068 SAMPLE BXF1 PIC3B 15:39:51 DONE Tuffryn Filter 01-APR-16 00:00 405235069 SAMPLE BXF1 PIC3C SEP-27-16 15:39:52 DONE Tuffryn Filter 01-APR-16 00:00 405235071 SAMPLE BXF1 PIC4C SEP-27-16 15:39:59
  • DONE Tuffryn Filter 01-APR-16 00:00 405235072 SAMPLE BXF1 PIC4D SEP-27-16 15:40:0.1 DONE Tuffryn Filter 01-APR-16 00:00 405235073 SAMPLE BXF1 PIC5A SEP-27-16 15:40:07 DONE Tuffryn Filter 01-APR-16 00:00 405235067 SAMPLE BXF1 PIC7D SEP-28-16 08:50:51 DONE Tuffryn Filter 01-APR-16 00:00 405235070 SAMPLE BXF1 PIC10C SEP-28-16 08:50:55 DONE Tuffryn Filter 01-APR-16 00:00 405235063 SAMPLE BXF1 PIC1B SEP-28-16 08 :51 :21 DONE Tuffryn Filter 01-APR-16 00:00 405235064 SAMPLE BXF1 PIC3D SEP-28-16 08:51:25 DONE Tuffryn Filter 01-APR-16 00:00 405235066 SAMPLE BXF1 PIC5C SEP-28-16 08:51:29 DONE Tuffryn Filter 01-APR-16 00:00 405235074 SAMPLE BXF1 PIC11A SEP-28-16 08:54:32 DONE Tuffryn Filter 01-APR-16 00:00 405235076 SAMPLE BXF1 PIC11B SEP-28-16 08:54:41 DONE Tuffryn Filter 01-APR-16 00:00 1203625413 DUP BXF1 PIC11C SEP-28-16 08:54:48 DONE Tuffryn Filter 0*1-APR-16 00:00 1203625414 LCS BXF1 PIC12A SEP-28-16 08:54:54 DONE Tuffryn Filter 01-APR-16 00:00 Page 5189of5809 Instrument Run Log Instrument Type: GFPC Batch 10:1597811 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type
  • 1203625436 DUP BXF1 PIC4C SEP-19-16 14:36:23 DONE 2 inch Planchett 01-DEC-15 00:01 405235021 SAMPLE BXF1 PIC4B SEP-19-16 14:36:28 DONE 2 inch Planchett 01-DEC-15 00:01 405235022 SAMPLE BXF1 PIC3C SEP-19-16 14:36:32 DONE 2 inch Planchett 01-DEC-15 00:01 405235025 SAMPLE BXF1 PIC3D SEP-19-16 14:36:49 DONE 2 inch Planchett 01-DEC-15 00:01 405235029 SAMPLE BXF1 PIC4A SEP-19-16 14:36:57 DONE 2 inch Planchett 01-DEC-15 00:01 1203625435 MB BXF1 PIC10A SEP-19-16 14:36:58 DONE 2 inch Planchett 01-DEC-15 00:01 405235034 SAMPLE BXF1 PIC5C SEP-19-16 14:37:09 DONE 2 inch Planchett 01-DEC-15 00:01 405235024 SAMPLE BXF1 PIC9A SEP-19-16 14:37:10 DONE 2 inch Planchett 01-DEC-15 00:01 405235028 SAMPLE BXF1 PIC8D SEP-19-16 14:37:17 DONE 2 inch Planchett 00:01 405235035 SAMPLE BXF1 PIC3B SEP-19-16 14:37:17 DONE 2 inch Planchett 01-DEC-15 00:01 405235030 SAMPLE BXF1 PIC9D SEP-19-16 14:37:22 DONE 2 inch Planchett 01-DEC-15 00:01 405235033 SAMPLE BXF1 PIC7D SEP-19-16 14:37:27 DONE 2 inch Planchett 01-DEC-15 00:01 405235036 SAMPLE BXF1 PIC8A SEP-19-16 14:37:43 DONE 2 inch Planchett 01-DEC-15 00:01 405235037 SAMPLE BXF1 PIC10B SEP-19-16 14:37:45 DONE 2 inch Planchett 01-DEC-15 00:01 405235038 SAMPLE BXF1 PIC7A SEP-19-16 14:37:50 DONE 2 inch Planchett 01-DEC-15 00:01 405235040 SAMPLE BXF1 PIC8B SEP-19-16 14:38:04 DONE 2 inch Planchett 01-DEC-15 00:01 405235023 SAMPLE BXF1 PIC12B SEP-19-16 14:41:30 DONE 2 inch Planchett 01-DEC-15 00:01 405235026 SAMPLE BXF1 PIC12D SEP-19-16 14:41:44 DONE 2 inch Planchett 01-DEC-15 00:01 405235027 SAMPLE BXF1 PIC14A SEP-19-16 14:41:49 DONE 2 inch Planchett 01-DEC-15 00:01 405235031 SAMPLE BXF1 PIC13D SEP-19-16 14:41:58 DONE 2 inch Planchett 01-DEC-15 00:01 405235032 SAMPLE BXF1 PIC14C SEP-19-16 14:42:08 DONE 2 inch Planchett 01-DEC-15 00:01 405235039 SAMPLE BXF1 PIC12A SEP-19-16 14:42:14 DONE 2 inch Planchett 01-DEC-15 00:01 1203625437 MS BXF1 PIC11A SEP-19-16 16:05:11 DONE 2 inch Planchett 01-DEC-15 00:01 1203625438 MSD BXF1 PIC13D SEP-19-16 16:05:14 DONE 2 inch Planchett 01-DEC-15 00:01 1203625439 LCS BXF1 PIC14A SEP-19-16 16:05:18 DONE 2 inch Planchett 01-DEC-15 00:01 Page 5190of5809 Instrument Run Log Instrument Type: GFPC Batch ID: 1597816 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type ' 405235001 SAMPLE JXC9 PIC14C SEP-16-16 10:57:49 DONE 2 inch Planchett 01-DEC-15 00:01 405235002 SAMPLE JXC9 PIC13D SEP-16-16 10:57:58 DONE 2 inch Planchett 01-DEC-15 00:01 405235003 SAMPLE JXC9 PIC14D SEP-16-16 10:58:18 DONE 2 inch Planchett 01-DEC-15 00:01 405235004 SAMPLE JXC9 PIC12C SEP-16-16 10:58:29 DONE 2 inch Planchett 01-DEC-15 00:01 405235005 SAMPLE JXC9 PIC12D SEP-16-16 10:58:36 DONE 2 inch Planchett 01-DEC-15 00:01 405235006 SAMPLE JXC9 PIC14A SEP-16-16 10:58:41 DONE 2 inch Planchett 01-DEC-15 00:01 1203625449 MB JXC9 PIC14D SEP-19-16 12:20:11 DONE 2 inch Planchett 01-DEC-15 00:01 405235019 SAMPLE JXC9 PIC5C SEP-19-16 12:30:35 DONE 2 inch Planchett 01-DEC-15 00:01 405235010 SAMPLE JXC9 LB4100G2 SEP-19-16 12:32:07 DONE 2 inch Planchett 01-DEC-15 00:01 405235012 SAMPLE JXC9 LB4100G4 SEP-19-16 12:32:08 DONE 2 inch Planchett 01-DEC-15 00:01 405235009 SAMPLE JXC9 LB4100H1 SEP-19-16 12:32:15 DONE 2 inch Planchett 01-DEC-15 00:01 405235017 SAMPLE JXC9 LB4100H3 SEP-19-16 12:32:15 DONE 2 inch Planchett 01-DEC-1'5 00:01 405235011 SAMPLE JXC9 LB4100F3 SEP-19-16 12:32:19 DONE 2 inch Planchett 01-DEC-15 00:01 405235016 SAMPLE JXC9 LB4100F2 SEP-19-16 12:32:19 DONE 2 inch Planchett 01-DEC-15 00:01, 405235015 SAMPLE JXC9 LB4100F4 SEP-19-16 12:32:20 DONE 2 inch Planchett 01-DEC-15 00:01 405235008 SAMPLE JXC9 LB4100J2 SEP-19-16 12:32:52 DONE 2 inch Planchett 01-DEC-15 00:01 405235018 SAMPLE JXC9 LB4100J1 SEP-19-16 12:32:52 DONE 2 inch Planchett 01-DEC-15 00:01 1203625453 LCS JXC9 PIC1D SEP_.19-16 12:37:49 DONE 2 inch Planchett 01-DEC-15 00:01 405235007 SAMPLE JXC9 LB4100C2 SEP-19-16 12:41:54 DONE 2 inch Planchett 01-DEC-15 00:01 405235014 SAMPLE JXC9 LB4100B4 SEP-19-16 14:16:35 DONE 2 inch Planchett 01-DEC-15 00:01 405235020 SAMPLE JXC9 LB4100B1 SEP-19-1614:16:35 DONE 2 inch Planchett 01-DEC-15 00:01 1203625450 DUP JXC9 PIC12D SEP-20-16 11 :56:34 DONE 2 inch Planchett 01-DEC-15 00:01 1203625451 MS JXC9 PIC14C SEP-20-16 11 :56:34 DONE 2 inch Planchett 01-DEC-15 00:01 1203625452 MSD JXC9 PIC14D SEP-20-16 11 :56:38 DONE 2 inch Planchett 01-DEC-15 00:01 405235013 SAMPLE JXC9 PIC12A SEP-20-16 11 :56:48 DONE 2 inch Planchett 01-DEC-15 00:01 Page 5191of5809 Instrument Run Log Instrument Type: GFPC Batch ID: 1597817 Sample Sample Analyst Instrument Run Date Status Calibration Date ID Type
  • 405235061 SAMPLE JXC9 PIC14A SEP-22-1612:39:44 DONE 2 inch Planchett 01-DEC-15 00:01 405235062 SAMPLE JXC9 PIC14D SEP-22-16 12:39:54 DONE 2 inch Planchett 01-DEC-15 00:01 405235063 SAMPLE JXC9. PIC12B SEP-22-16 12:39:58 DONE 2 inch Planchett 01-DEC-15 00:01 405235064 SAMPLE JXC9 PIC14C SEP-22-16 12:40:02 DONE 2 inch Planchett 01-DEC-15 00:01 405235065 SAMPLE JXC9 PIC13A SEP-22-16 12:40:04 DONE 2 inch Planchett 01-DEC-15 00:01 405235066 SAMPLE JXC9 PIC13D SEP-22-16 12:40:11 DONE 2 inch Planchett 01-DEC-15 00:01 405235069 SAMPLE JXC9 LB4100G2 SEP-22-16 13:57:34 DONE 2 inch Planchett 01-DEC-15 00:01 405235073 SAMPLE JXC9 LB4100G3 SEP-22-16 13:57:34 DONE 2 inch Planchett 01-DEC-15 00:01 405235067 SAMPLE JXC9 LB4100G4 SEP-22-16 13:57:35 DONE 2 inch Planchett 01-DEC-15 00:01 405235070 SAMPLE JXC9 LB4100F3 SEP-22-16 13:57:41 DONE 2 inch Planchett 01-DEC-15 00:01 405235071 SAMPLE JXC9 LB4100F2 SEP-22-16 13:57:41 DONE 2 inch Planchett 01-DEC-15 00:01 405235072 SAMPLE JXC9 LB4100H1 SEP-22-16 13:57:41 DONE 2 inch Planchett 01-DEC-15 00:01 405235068 SAMPLE JXC9 LB4100F4 SEP-22-16 13:57:42 DONE 2 inch Planchett 01-DEC-15 00:01 405235074 SAMPLE JXC9* LB4100H3 SEP-22-16 13:57:42 DONE 2 inch Planchett 01-DEC-15 00:01 1203625462 MSD JXC9 PIC2C SEP-22-16 13:58:31 DONE 2 inch Planchett 01-DEC-15 00:01 1203625463 LCS JXC9 PIC3C SEP-22-16 13:58:35 DONE 2 inch Planchett 01-DEC-15 00:01 1203625459 MB JXC9 PIC11C SEP-22-16 14:00: 17 DONE 2 inch Planchett 01-DEC-15 00:01 1203625460 DUP JXC9 PIC11B SEP-22-16 14:00:25 DONE 2 inch Planchett 01-DEC-15 00:01 405235075 SAMPLE JXC9 PIC13A SEP-22-16 14:00:28 DONE 2 inch Planchett 01-DEC-15 00:01 405235076 SAMPLE JXC9 PIC14A SEP-22-16 14:00:32 DONE 2 inch Planchett 01-DEC-15 00:01 405235077 SAMPLE JXC9 PIC13D SEP-22-16 14:00:36 DONE 2 inch Planchett , 01-DEC-15 00:01
  • 405235078 SAMPLE JXC9 PIC11D SEP-22-16 14:00:38 DONE 2 inch Planchett 01-DEC-15 00:01 1203625461 MS JXC9 PIC5D SEP-23-16 13:24:24 DONE 2 inch Planchett 01-DEC-15 00:01 Page 5192of5809 Instrument Run Log Instrument Type: GFPC Batch ID: 1602427 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID*. Type 1203636654 DUP JXC9 PIC5B SEP-28-16 14:47:43 DONE 2 inch Planchett 01-DEC-15 00:01 1203636653 MB JXC9 PIC6C SEP-28-16 14:47:50 DONE 2 inch Planchett 01-DEC-15 00:01 1203636657 LCS JXC9 PIC10B SEP-28-16 14:47:54 DONE 2 inch Planchett 01-DEC-15 00:01 405235041 SAMPLE JXC9 PIC4A SEP-28-16 14:48:00 DONE 2 inch Planchett 01-DEC-15 00:01 405235043 SAMPLE JXC9 PIC9B SEP-28-16 14:48:05 DONE 2 inch Planchett 01-DEC-15 00:01 405235042 SAMPLE JXC9 PIC4D SEP-28-16 14:48:06 DONE 2 inch Planchett 01-DEC-15 00:01 405235044 SAMPLE JXC9 PIC5A SEP-28-16 14:48: 11 DONE 2 inch Planchett 01-DEC-15 00:01 405235045 SAMPLE JXC9 PIC8A 14:48:11 DONE 2 inch Planchett 01-DEC-15 00:01 405235046 SAMPLE JXC9 PIC7A SEP-28-16 14:48: 17 DONE 2 inch Planchett 01-DEC-15 00:01 405235047 SAMPLE JXC9 PIC4B SEP-28-16 14:48:17 DONE 2 inch Planchett 01-DEC-15 00:01 405235048 SAMPLE JXC9 PIC3C SEP-28-16 14:48:19 DONE 2 inch Planchett 01-DEC-15 00:01 405235053 SAMPLE JXC9 PIC7B SEP-28-16 14:48:22 DONE 2 inch Planchett 00:01 405235049 SAMPLE JXC9 PIC2B SEP-28-16 14:48:24 DONE 2 inch Planchett 01-DEC-15 00:01 405235056 SAMPLE JXC9 PIC6A SEP-28-16 14:48:26 DONE 2 inch Planchett 01-DEC-15 00:01 405235050 SAMPLE JXC9 PIC1B SEP-28-16 14:48:29 DONE 2 inch Planchett 01-DEC-15 00:01 405235057 SAMPLE JXC9 PIC7D SEP-28-16 14:48:30 DONE 2 inch Planchett 01-DEC-15 00:01 405235051 SAMPLE JXC9 PIC3D SEP-28-16 14:48:32 DONE 2 inch Planchett 01-DEC-15 00:01 405235059 SAMPLE JXC9 PIC8C SEP-28-16 14:48:40 DONE 2 inch Planchett 01-DEC-15 00:01 405235052 SAMPLE JXC9 PIC1D SEP-28-16 14:48:41 DONE 2 inch Planch13tt 01-DEC-15 00:01 405235054 SAMPLE JXC9 PIC3B SEP-28-16 14:48:47 DONE 2 inch.Planchett 01-DEC-15 00:01 405235055 SAMPLE JXC9 PIC1C SEP-28-16 14:48:50 DONE 2 inch Planchett 01-DEC-15 00:01 405235058 SAMPLE JXC9 PIC5C SEP-28-16 14:48:57 DON!= 2 inch Planchett 01-DEC-15 00:01 405235060 SAMPLE JXC9 PIC5D SEP-28-16 14:49:04 DONE 2 inch Planchett 01-DEC-15 00:01 1203636655 MS JXC9 PIC5C SEP-29-16 13:04:36 DONE 2 inch Planchett 01-DEC-15 00:01 1203636656 MSD JXC9 PIC5D SEP-29-16 13:04:40 DONE 2 inch Planchett 01-DEC-15 00:01 Page 5193of5809 Page 5194of5809 Liquid Scintillation Raw Data Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 Product:. __ jj+-""1-*d-l_I __ _ Criteria: Yes No Comments Sample Solids are less than or eaual to 100 ma for GAB. kb Samples have been blank corrected (If required). j\x:J Blank correction reoorted included lif reouiredl. If activity less than lOX MDA/MDC, error is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. v lrf halmu >ha Mn A I Mnr <>rror (<: Instrument source check is within limits. Ino;trum<>nt bkn rherk I<: within llmltc. ,/ Method RDL/ LLD has been met. ./ If duplicate activities are: Less than 5* MDA/ MDC, then RPD is 100% or less, lf greater 5* MDA/ MDC, then RPD 20% or less, ,/ If below the MDA/ MDC, the RPO is 0%, Or meets the client's renulred RER accentance criteria. Tracer yield Is 15-125%
  • Carrier yield 25-125%. (Or meets the client's contract acceptance criteria), ../ Method blank is less than the RDL/ LLD. v ltTr c 50/n nf lnu.ac> "dlvltv) Samole was run within hold time. / 1 5l.oZ>2J...-;} Samole was correctlv oreserved If renulred. Smears Taken for Radioactive batches. Method Spike and LCS are within 75*125% v '(or m<>At<: the cli,.nt's contract acr.,nt:.nce criteria). No blank spaces on data forms. v All line outs initialed and dated. l.,n -............. ............ --*-Aux data Is correct. l\6-Client Sneclal renulrements naae has been checked. ..,,-Raw Data and/ or soectrum are Included and orooerlv statused. v MS, LCS. and Duplicate RPD/RER values uploaded to LIMS and v"l111>cv1>rlfl1>tl . v .. ,. flf U;r --*---.1 In*-'"""" \/ Batch Data Exceotlon Reoorts (DER) comoleted. if aoollcable. v Batch Data Exception Reports (DER) second reviewed. v J:)f,Q{b-24--l Disoositlon verified to be comoleted. Aliouot Corrartlnn rnmnlot .... If renuired. Review sample historical results if available / (If REMP, results above MDC have been verified bv historical results. recount or re-analvsis.) Primary Review Performed By:. __ __ __ Secondary Review Performed By:__ p£;.__ 10/02/16 GL-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER
  • DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 30-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC HASL-300, Pu-11-RC Solid .. Batch ID: Sample Numbers: 1596402 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, and 1203621726 were received and analyzed out of holding. Originator's Name: Data Validator/Group Leader: Melanie Aycock 30-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 5196 of 5809 DER Report No.: 1563227 Revision No.: 1 .. Type: Process Client Code: MJWC Pu-241 Queue Sheet 07-SEP-16 --------------------------------------------*---Batch#: 1596402 Tracer Isotope: LCS Isotope: Pu-241 Analyst:MXS2 First Client Due Date: 04-0CT-16 Internal Due Date.30-SEP-16 Tracer Code: (7"10-A-Expiration Date: .-.?* 3-J? Vol: 0
  • J Solid Sample Dissolution by: LEACH LCSCode: /C...,ro-13 ExpirationDate: K>'7'8-1v Vol: 0-I Spike Isotope: Pu-241 Prep Date: q -ZI r/ v Spike Code: Expiration Date: -Vol: -Cocktail Used: Ultima gold LLT or &;2scintUI1;ra " Initials: .l)l5D PipetID: Balance ID: 1ColO?faWk Witness:-;/'-"'-vA-__ _ -------Collection Label AJ.!quot LSC Rack# Alpha Spec Sample ID Client Description 405235021-1 4.2B.R.2.3 405235022-1 4.2B.R.1.3 405235023-1 4.2B.R.11.2 405235024-1 4.2B.R.2.2 405235025-1 4.2B.R.1.2 405235026-1 4.2C.R.1.3 405235027-1 4.2C.R.1.4 405235028-1 4.3.ARl.3 405235029-1 4.3.B.R.l.3 405235030-1 4.3A.R.2.3 405235031-1 4.3.BR19.2 405235032-1 4.3B.R.3.3 405235033-1 4.3B.R.3.4 405235034-1 4.3.B.R.1.4 405235035-1 4.3B.R.2.3 405235036-1 4.3B.R.2.4 405235037-1 4.4C.R.2.4 405235038-1 4.4C.R.1.3 405235039-1 4.4C.R.1.4 405235040-1 4.4D.R.1.3 1203621725-1 IVIB for batch 1596402 1203621726-1 4.2B.R.2.3(405235021DUP) 1203621727-1 LCS for batch 1596402 Type SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAi'\fPLE SAMPLE SAMPLE SAMPLE SAMPLE SAJ\1PLE SAMPLE SAMPLE rvm DUP LCS Hazard Code Min CRDL 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL Client 1\-JJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl IVJJWCOOl MJWCOOl l\fJWCOOl MJWCOOl !Vf.JWCOOl MJWCOOl MJWCOOl MJWCOOl !Vf.JWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl J\.f.JWCOOl MJWCOOl QC ACCOU11' QCACCOm.'T QC ACCOUNT Date Pos. # @1110 Det # 08-DEC-15 08-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 23-NOV-15 23-NOV-15 23-NOV-15 26-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 23-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 08-DEC-15 Instrument Used: l 55, LS6500 (Blue) 7067083, LS6500 (Green) 7067404, Wallac (Yellow) Data Reviewed By: :tfl J:.. '1 !Jou<.. 706065f;}LS6500 (Gold) 7070506, Purple 7069123, Silver 7060656, Wallac (White) 4 40299, Wal/ac (Teal) 4140421, Wallac (Gray) 4150033, 7069693 (Mocha) Page 1 ofl GEL Laboratories LLC, Radiochemistry Divisw11

""C (1) Vl ,_.. \0 00 0 .....,_/ Vl 00 0 \0 Filename : PU241 .XLS File type : Excel Version # : 1.3.4 Batch: 1596402 Analyst : MXS2 Prep Date: 9/21/2016 Method Uncertainty : 0.0839 Geometry: 2ml DV1 drop HN03/13ml Ecoscint Ultra Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Sample Pos. ID G G Date/Time 1 405235021.1 0.5140 3.2727E-03 12/8/2015 14:17 2 405235022.1 0.5050 3.2718E-03 12/81201513:43 3 405235023.1 0.5040 3.2717E-03 12/212015 10:40 4 405235024.1 0.5050 3.2718E-03 1218/2015 14:13 5 405235025.1 0.5060 3.2719E-03 121812015 13:38 6 405235026.1 0.5020 3.2714E-03 121812015 10:15 7 405235027 .1 0.5100 3.2723E-03 12181201510:19 8 405235028.1 0.5070 3.2720E-03 11 /23/2015 14:50 9 405235029.1 0.5040 3.2717E-03 11/23/2015 11:10 10 405235030.1 0.5140 3.2727E-03 11/2312015 14:44 11 405235031.1 0.5170 3.2730E-03 11/26/201514:25 12 405235032.1 0.5080 3.2721E-03 11/23/2015 11:48 13 405235033.1 0.5060 3.2719E-03 11/23/201511:53 14 405235034.1 0.5090 3.2722E-03 11/23/201511:20 15 405235035.1 0.5160 3.2729E-03 11/23/201511:06 16 405235036.1 0.5180 3.2731E-03 11123/201511:12 17 405235037 .1 0.5060 3.2719E-03 11/30/201511:19 18 405235038. 1 0.5010 3.2713E-03 11/30/201510:40 19 405235039.1 0.5120 3.2725E-03 11/30/201510:43 20 405235040.1 0.5150 3.2728E-03 11/30/2015 13:23 21 1203621725.1 0.5180 3.2731E-03 9/21/2016 0:00 22 1203621726.1 0.5080 3.2721E-03 1218/201514:17 23 1203621727.1 0.5180 3.2731E-03 9/21/2016 0:00 PU1596402R Plutonium-241 Solid Tracer SIN: Tracer Exp Date : Tracer Volume Added: Tracer Error: Tracer Calculations Tracer Concentration Tracer DPM Counts 4.3831 229 4.3831 246 4.3831 253 4.3831 216 4.3831 264 4.3831 269 4.3831 271 4.3831 306 4.3831 293 4.3831 219 4.3831 223 4.3831 209 4.3831 192 4.3831 258 4.3831 195 4.3831 222 4.3831 178 4.3831 211 4.3831 233 4.3831 183 4.3831 220 4.3831 235 4.3831 228 1770-A 8/3/2017 0.10 0.44% Tracer Tracer Bkg Net Counts CPM 6.960 0.925 0.240 1.024 1.440 1.048 1.680 0.893 1.680 1.093 1.440 1.115 1.440 1.123 1.200 1.270 0.720 1.218 0.720 0.910 0.480 0.927 0.960 0.867 1.920 0.792 0.960 1.071 0.240 0.812 1.200 0.920 0.960 0.738 0.960 0.875 1.920 0.963 0.720 0.760 2.160 0.908 1.680 0.972 1.440 0.944 Page 1 Procedure Code : LSC41PUS Parmname: Plutonium-241 Required MDA : 15 pCi/G Halfllfe of Pu-241 : 14.290 years Pu-241 Abundance : 1.00 Tracer Abundance : 1.00 Halflife of Tracer : 373500.000 years Detector Tracer Count Tracer Detector Efficiency Start Count Tracer Detector Efficiency S!Dev. Datemme Time (sec.) Decay Serial# (cpmldpm) (cpm/dpm) 9/24/2016 20:54 14400 1.000 79988 0.292461 0.005651 9/24/2016 20:54 14400 1.000 78263 0.334344 0.006443 9/24/2016 20:54 14400 1.000 78259 0.347245 0.006687 9/24/2016 20:54 14400 1.000 80063 0.303421 0.005858 9/24/2016 20:54 14400 1.000 33206 0.330892 0.006377 9/24/2016 20:54 14400 1.000 38626 0.304247 0.005873 9/24/2016 20:54 14400 1.000 80016 0.325188 0.005269 9/24/2016 20:54 14400 1.000 83288 0.353557 0.006805 9/24/2016 20:54 14400 1.000 80059 0.356284 0.006858 9/2412016 20:51 14400 1.000 87941 0.256727 0.004975 9/24/2016 20:51 14400 1.000 87942 0.251642 0.004879 9/24/2016 20:51 14400 1.000 87943 0.249747 0.004844 9/2412016 20:51 14400 1.000 87944 0.257507 0.004991 9/2412016 20:54 14400 1.000 87921 0.252931 0.004905 9/24/2016 20:54 14400 1.000 87922 0.248037 0.004811 9/24/2016 20:54 14400 1.000 87923 0.247991 0.004811 912612016 13:55 14400 1.000 87943 0.249747 0.004844 9/24/2016 20:54 14400 1.000 87926 0.261325 0.005062 9/26/2016 13:55 14400 1.000 87944 0.257507 0.004991 9/24/2016 20:54 14400 1.000 87963 0.259137 0.005022 9/24/2016 20:54 14400 1.000 87931 0.248977 0.004829 9/24/2016 20:54 14400 1.000 87932 0.237184 0.004607 9/24/2016 20:54 14400 1.000 87915 0.263665 0.005107 Plpet, 0.1 ml Stdev : +/-0.000200 ml Plpet, 0.5 ml Stdev: +/-0.001000 ml Pipe!, 1 ml Stdev : +I* 0.002000 ml Analytical SOP: GL*RAD*A-035 Instrument SOP: GL*RAD-1-004 Count raw Data Counting Rack Time Quench# Gross Pos. Position# (min.) cpm 1 3-2 45 133.6 11.33 2 3-3 45 132.7 11.76 3 60-2 45 135.1 7.38 4 60-3 45 134.7 8.18 5 60-4 45 136.4 7.62 6 3-7 45 133.1 11.36 7 3*8 45 133.8 10.58 8 3-9 45 132.6 11.87 9 3-10 45 135.B 10.42 10 3*11 45 136.4 9.89 11 3-12 45 132.6 10.49 12 49-1 45 134.9 10.82 13 49-2 45 134.6 10 14 49-3 45 134.3 10.49 15 49-4 45 136.5 10.07 16 49.5 45 135.2. 9.73. 17 49-6 45 135.2 10.29 18 49-7 45 145.8 8.82 19 60-5 45 127.6 7.69 20 49-9 45 136.5 8.71 21 52-10 45 133.8 8.6 22 60-6 45 134.4 8.29 23 52-12 45 134 39.87 Bkg Count Corrected Bkg Time Bkg Bkg cpm (min.) Quench# cpm 9.67 45 132.5 9.6767 9.67 45 132.5 9.6712 7.56 45 134.8 7.5620 7.56 45 134.8 7.5594 7.56 45 134.8 7.5707 9.67 45 132.5 9.6736 9.67 45 132.5 9.6n9 9.67 45 132.5 9.6706 9.67 45 132.5 9.6909 9.67 45 132.5 9.6950 9.67 45 132.5 9.6706 9.67 45 132.5 9.6850 9.67 45 132.5 9.6830 9.67 45 132.5 9.6811 9.67 45 132.5 9.6956 9.67 45 132.5 9.6869 9.67 45 132.5 9.6869 9.67 45 132.5 9.7626 7.56 45 134.8 7.5207 9.67 45 132.5 9.6956 9.67 45 132.5 9.6n9 7.56 45 134.8 7.5574 9.67 45 132.5 9.6792 PU1595402R Calculated Calibration Data Detector Background Count Sample Sample Calibration Detector Efficiency Background Count Start -Sample Recovery Recovery Counted Calibration Due Efficiency Error Rack Start Datemme Decay % Error o/o on Date Date (cpm/dpm) (cpm/dpm) Position# Datemme 9128/2016 5:20 0.962 72.2% 7.14% LSCBROWN 211/2016 1/3112017 0.2207 0.00792 3-1 9/28/2016 4:33 9128/2016 6:07 0.962 6.69% LSCBROWN 211/2016 1/3112017 0.2222 0.00792 3-1 9/28/2016 4:33 9/29/2016 10:42 0.961 68.9% 6.64% LSCBROWN 21112016 1/3112017 0.2182 0.00792 60-1 912912016 9:55 9/29/2016 11 :28 0.961 7.16",{, LSCBROWN 211/2016 1/3112017 0.2189 0.00792 60-1 9129/2016 9:55 9/29/2016 12:15 0.961 75.4% 6.52% LSCBROWN 211/2016 1/31/2017 0.2160 0.00792 .60-1 9/29/2016 9:55 9/28/2016 9:15 0.962 83.6% 6.46% LSCBROWN 211/2016 1/31/2017 0.2216 0.00792 3-1 9128/2016 4:33 912812016 10:02 0.962 78.8% 6.43% LSCBROWN 211/2016 1/31/2017 0.2204 0.00792 3-1 9/28/2016 4:33 9/2812016 10:49 0.960 82.0% 6.08% LSCBROWN 211/2016 1/31/2017 0.2224 0.00792 3-1 9/28/2016 4:33 912812016 11 :35 0.960 78.0% 6.19% LSCBROWN 211/2016 1/31/2017 0.2170 0.00792 3-1 9/2812016 4:33 9128/201612:22 0.960 80.8% 7.08% LSCBROWN 211/2016 1/3112017 0.2160 0.00792 3-1 9/2812016 4:33 912812016 13:09 0.960 84.1% 7.02% LSCBROWN 211/2016 1/31/2017 0.2224 0.00792 3-1 9/2812016 4:33 9/2&2016 13:56 0.960 79.2% 7.25% LSCBROWN 211/2016 1/31/2017 0.2185 0.00792 3-1 9/2812016 4:33 9/28/2016 14:43 0.960 70.2% 7.58% LSCBROWN 211/2016 1/31/2017 0.2190 0.00792 3-1 9128/2016 4:33 9/2&2016 15:30 0.960 96.6% 6.57% LSCBROWN 211/2016 1/3112017 0.2195 0.00792 3-1 9/2812016 4:33 9/2812016 16:16 0.960 74.6% 7.46% LSCBROWN 211/2016 1/31/2017 0.2158 0.00792 3-1 9/2812016 4:33 9/2812016 17:03 0.960 84.6% 7.05% LSCBROWN 211/2016 1/31/2017 0.2180 0.00792 3-1 9/28/2016 4:33 9/28/2016 17:50 0.961 67.4% 7.82% LSCBROWN 21112016 1/31/2017 0.2180 0.00792 3-1 9/2812016 4:33 9/28/2016 18:37 0.961 76.4% 7.22% LSCBROWN 21112016 1/31/2017 0.1999 0.00792 3-1 9/28/2016 4:33 9/291201613:01 0.960 85.3% 6.92% LSCBROWN 211/2016 1/31/2017 0.2308 0.00792 60*1 9/2912016 9:55 9/2812016 20:10 0.961 66.9% 7.71% LSCBROWN 211/2016 1/31/2017 0.2158 0.00792 3-1 9/28/2016 4:33 9/2812016 22:08 0.999 83.2% 7.12% LSCBROWN 21112016 1/31/2017 0.2204 0.00792 3-1 912812016 4:33 9/2912016 13:48 0.961 93.5% 6.88% LSCBROWN 21112016 1/31/2017 0.2194 0.00792 60-1 912912016 9:55 9/28/2016 23:41 0.999 81.7% 6.97% LSCBROWN 2/1/2016 1/31/2017 0.2200 0.00792 3-1 9/2812016 4:33 Page2 Notes; 1 -Results are decay corrected to Sample Datemme 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Date/Time * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Lever Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 8.7417 6.1717 15 12.7249 9.4586 41.95% 2 9.1245 6.4420 15 13.2822 12.4768 33.73% 3 8.3637 5.9048 15 12.2225 *1.1267 316.75% 4 8.5261 6.0195 15 12.4599 3.9182 95.56% 5 7.6888 5.4283 15 11.2359 0.2807 1177.49% 6 7.6969 5.4340 15 11.2040 8.4960 41.06% 7 8.0825 5.7063 15 11.7653 4.7713 74.66% 8 7.7586 5.4777 15 11.2939 11.1712 32.06% 9 8.4159 5.9417 15 12.2503 4.0127 91.91% 10 8.0013 5.6490 15 11.6467 1.0203 338.33% 11 7.4149 5.2350 15 10.7936 3.9775 81.99% 12 8.1629 5.7631 15 11.8822 6.0610 59.92% 13 9.2259 6.5135 15 13.4295 1.9133 208.78% 14 6.6457 4.6919 15 9.6737 3.5173 83.03% 15 8.6379 6.0984 15 12.5733 2.1141 177.20% 16 7.5081 5.3008 15 10.9290 0.2115 1525.09% 17 9.6449 6.8094 15 14.0394 3.8046 110.76% 18 9.4041 6.6394 15 13.6873 -5.7754 68.57% 19 6.2673 4.4248 15 9.1598 0.7879 343.39% 20 9.6521 6.8145 15 14.0497 -6.2200 65.35% 21 7.2573 5.1237 15 10.5640 -5.1193 59.56% 22 6.0711 4.2863 15 8.8723 3.2936 81.30% 23 7.4015 5.2255 15 10.7740 146.2220 7.86% PU1596402R Spike SIN: Spike Exp Date : Spike Activity (dpmlml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpmfml): LCS Volume Added: 2SIGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCi/G 1.6533 0.6832 7.6612 2.0888 0.6901 8.0794 -0.1820 0.5762 6.9931 0.6206 0.5914 7.3179 0.0493 0.5810 6.4783 1.6864 0.6837 6.7509 0.9021 0.6710 6.9557 2.1994 0.6919 6.8877 0.7291 0.6685 7.2114 0.1950 0.6597 6.7644 0.8194 0.6693 6.3682 1.1350 0.6750 7.0650 0.3170 0.6614 7.8241 0.8089 0.6695 5.7060 0.3744 0.6627 7.3360 0.0431 0.6569 6.3229 0.6031 0.6663 8.2386 -0.9426 0.6426 7.7175 0.1693 0.5814 5.3017 -0.9856 0.6395 7.9103 -1.0779 0.6373 5.9324 0.7326 0.5934 5.2293 30.1908 1.0493 9.9611 Page3 NIA NIA NIA NIA 1610-B 10/28/2016 1692.28 0.10 2SIGMA Total Prop. Uncertainty pCi/G 7.9309 8.4988 6.9932 7.3672 6.4786 6.9794 7.0263 7.2552 7.2583 6.7680 6.4255 7.1878 7.8357 5.7535 7.3508 6.3230 8.2833 7.7175 5.3044 7.9104 5.9325 5.2765 32.9438 Sample QC 405235021.1 Sample Nominal Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP

  • 0.0% LCS 147.1595 99.4%

][ J[) :::: !!=* UI --n:=.=.: "'+ :n. USER: 7 PRESET TIME DATA CAL.C COUNT BU.".JNI-\ TWO PHASE SC I NT I LL.ATOR: l._OV4 LEVEL t1.:s. 1210 CPM NO NO LIQUID vr::s COMMEl\IT:BROWN H# :YES 8&:)MPLE REPEATS: 1 IC:ft : NO REPLICATES 1. AQC : NO CYCLE REPEf:.ffS " 1 NIJ UJW SAMPLE IZ! HALF LIFE C:CJRRECTIOl\I DATE: CHAN:: IZt. IZI --3iz11z1 .. IL' 1..ERROR: ;'.::. tZnZI F(.:fCTC.lR: :l

  • 01ZI Ii) 0 Q'.I BKt3. CHAl\J (?.1 .. IZI -91ZtQ'.I. 0 ':I.ERROR; .. IZIQI F(.:)CTCIR: :l
  • IZllZI IZI 121 lll BKG. SAM POS TIME H# LUME:X ELAPSED NO MI 1\1 CPM '.1.ERROR TIME 1l-1 2;--1. t ,32u 5 9.67 5':3 11. t.1*tS" ,35 I 3-;::'. £1.5. IZHZI t .. b 11.33 8. BE, 16"33 SJ3n i _, ...,. /.i.5. 1Zl0 l3i:'.:. 7 11.76 8 .. 7tZI 1 7. 1ZJLt . 14tZI. E:0 .... =3 ,,, 2J l1 00 1:Jl1 .* 4 1e. 07 B.58 Hi. .1:-tll 187. 'l 3. v.r-*-,_, 5 .Ef5, fj te.3a e. ti+ t :;z. u ,, 17.t/i. II? ,,{_.f; 3 G 45. Ii.fill L?.ti .. .::. re. 3a 8 .. 47 1. '5-.. ZP ;::* ara ..... l? r; 7 :3*-7 l-1. 5
  • IZllZI l33" l 11.36 8.85 1.5,.53 327 .. 82 i 8 3-El Li5. IZllZI l33n8 10. 58 9. 17 1.5 .. 1 E, 37.l, .* 71ZI 9 3-';:) Ii* 5
  • IZl fl) 13;::::. 6 11. 87 8 .. E,5 j_Lr. i:::'.B 111 !:i .. 7 1 It) ;::*-1 IZI 1-i*5. 1210 1 .. 8 10. 1+2 9. ;:=;:t} t3,. L1*68. Id lo u. L1*5. IZllZI 1 ' * ,:',i ':In 9.89 ':3. t.'.:.S 13. 1z19 5151. E:5 // 1 *:::* ... t ;:: 45. 1210 13i=:fl 6 10. ':3. ;:: 1 t3,. 3E, 56;3:. 1219 ('{, 1 ;3 Lj.9-1. 45.00 13Lf. 9 10. 82 9.06 11. 511. E, IZl 9
  • 0121 J.1.1. Lj.9--i::: 45. IZl!Zl 1 ;3L1 ... 6 10.00 9. :l 1. 98 5551(83 1if t !'.,) 4':J .. -3 4!:.'i. IZTIZI 1.3LJ.,, 3 10.49 ':3" :L 11. OE: 702:'. .. f,£i. IS H; 45. 1210 136.5 10.07 '3. L1.1Z1 10.54* 71+9 * .c,.1 I& 17 Lf5 .. IZllZt 1.35 .. 2 9.73 9.56 1121. 86 79t=,. 19 111.8 '1*9*-6 '1*5. IZIQ) 1:3511 ;::: 10.29 9. :1.0. 8'1* 81.f;:.;:. 9E, IP*9 J.i.9*-7 lf5. 121121 1.L1.5. 8 8.82 l 1Zt. 1Z1L1. 9 .. 66 B89. 7i?. 8 4 @. it11z1 1iJ8. 3 11.96 EL Gi::: j7,. 9:; 93£. *'18 .x io ;:: 1 1+9*-9 Li*5. li.'.10 1,36i. 5 8.71 1 IZI. 10 7.8E. 983. 17 Page 5201of5809 28 SEP 2016 05:03 PRINTER . STD . RS;:;:3;:: DISK . OFF " lt[)flf.l tZt tZI JC ][Ji r::i u::::* lJ ----* ;::;::.:: :1L USER: 7 PRESET TIME DATA CALC COUNT Tl.JO PHASE SCINTILL.f-lTOR: Lm,i LEVEL 4*5. 1Z11Zt CPM f\10 NO LIG1UID VES COMMENT: BROWhl :YES SAMPLE fiEPEATS: ICtl: : ND REPLICATES AG!C . NCI CYCLE REPEATEi .. NO LOW SAMPLE RE.J: HALF LIFE DATE: CHi'.=lN 1z1. rzi *-301Zt. IZI 'f..ERROR: 2. 1z11z1 FACTOli l .. CHAN: fZI,. tZf -* 901ZI. IZI 1-EFlROR: ;:::
  • IZllZt FRCTOR: 1
  • IZl tZllZl IZl 1Z1 IZJ SAM POS TIME H# .. N.P.J ___ ,_ LUMEX ELAPSED NO MIN CPM 'YuERROR TIME MISSING SAMPLE 1 :I. 1 0 Bl-\G. BKG. u 10 52-10 45.00 133.8 Vf E:-1 ;;:: 4. 5
  • 1Z11Z1 1 :?; lf
  • 1Z1 8.60 11Z1. 17 7 .. 88 f;.6. 33 7.51 :!.(1.*88 =:r .-'33 .. @'21 ( \I l.....\.J *f 39.87 l.f. 7i'.:: 3. BE, 1.39 .. 69 Page 5202 of 5809 ;::B SEP 2016 2C:: 38 PRil\ITER . STD . :EDIT DI Sf-<. . OFF . none SUB: Qt SUB: IZI Sample Count Start Time: Data Capture Date User Filename Spectrum Type Use.r Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win 1 : Pu-241 -Start, End: Win2: -Start, End: 6 ;: ,.** .. *: 5 *' ,:. '.,I . Dt.i* 4 . **. J'l: .* l*.:;! ... l/l ,'* .. g 3 -() I 2 I I .. I ... I**' . 0 . : :**' Page 5203 of 5809 100 200 300 28 Sep 2016 04:33:55 28 Sep 2016 05:19:18 S07092803-1 A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 1 3-1 45.00 132.5 1464 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number U.ser Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Winl: Pu-241 -Start, End: Win2: -Start, End: 28 Sep 2016 05:20:50 28 Sep 2016 06:06:13 S07092803-2A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 2 133.6 0 0 3-2 1492 300 990 45.00 *-----------------------------*-------SPECTRUM PLOT USER 07 -PU-241 I I 8 ........ I 1 1 ** **: 7 -!. I . I . 6 \.J .. ,*. I ::: .. I .::. 5 -i: . ,(/) '* :'E ,.:::5 4 I o I 3 2 -I 1. 1 -0 100 200 300 400 500 600 700 800 900 Channel Number {Log) ' . Page 5204 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type . User Number User Id User Comment Scintillator
  • Sample, Rack-Pos, Time: H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: I : ; 8 *,;1. **i:*: 7 '1 6
  • 1 .. 1 ..
  • i i 5 IH;: .. jV:;';;e iI:;*5 4 I o ! 3 I 2 I 1 -28 Sep 2016 06:07:46 28 Sep 2016 06:53:09 S07092803-3A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 3 132.7 0 0 3-3 1582 300 990 SPECTRUM PLOT USER 07 -PU-241 45.00 ...... ; . ' . . *-* .* ' . ' 0 Page 5205 of 5809 100 200 300 400 500 600 700 800 Channel Number (Log) 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: *H#, Total Counts: Win 1 : Pu-241 -Start, End: . Win2: -Start, End: 2 1 . f f 0 t. r 0 100 *, I' I I r i' Page 5206 of 5809 200 300 28 Sep 2016 09:15:23 28 Sep 2016 10:00:46 S07092803-7 A.XLS U07092803-1 A.XLS Log Counts 07 P,IJ-241 BROWN LIQUID 7 3-7 133.1 1504 0 300 0 990 45.00 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: 1 -28 Sep 2016 10:02:16 28 Sep 2016 10:47:39 . S07092803-8A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 8 133.8 0 0 3-8 1474 300 990 SPECTRUM PLOT USER 07 -PU-241 45.00 ....... 0 100 200 300 400 500 600 700 Channel Number (Log) Page 5207 of 5809 800 900
  • Sample Count Start Time: , Data Capture Date User Filename Spectrum Type User Number User Id User Comment . Scintillator : Sample, Rack-Pos, Time: H#_, Total Counts: Win1: Pu-241-Start, End:
  • Win2: -Start, End: 100 ' i: . 200 300 L-"--------------; .... " ' . *:* .... Page 5208 of 5809 28 Sep 2016 10:49:08 28 Sep 2016 11 :34:31 S07092803-9A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 9 3-9 45.00 132.6 1544 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (log) . 700 800 900 Sample Count Start Time: Data Capture Date
  • User Filename ** Spectrum Type
  • User Number User Id User Comment
  • Scintillator Sample, Rack-Pos, Time: 1-1#,Total Counts: 'Nin1: Pu-241 -Start, End: Win2: -Start, End: .... ; 2 -0 100 *::*i ' : ;;.,;:: 1* ', ',* ;' .,* .. ' Page' $209 of 5809 200 300 28 Sep 2016 11 :35:59 28 Sep 2016 12:21 :21 S07092803-1 QA.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 10 3-10 45.00 135.8 1442 0 300 0 990 SPECTRUM PLOT. USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900'

. Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number .User Id .j. ' User Comment Scintillator

  • Sample, Rack-Pos, Time: H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: 2 ..
  • I 0 L:'.C:: 100 Page 5210 of 5809 200 300 28 Sep2016 12:22:49 28 Sep 2016 13:08:11 S07092803-11 A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 11 3-11 45.00 136.4 1464 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type U.ser Number User Id
  • User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: 2 .: : *. !<. ::-. Page 5211 of 5809 28 Sep 2016 13:09:39 28 Sep 2016 13:55:01 S07092803-12A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 12 3-12 45.00 132.6 1493 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 900 Sample Count Start Time: Data Capture Date
  • User Filename Spectrum Type User Number *User Id
  • User Comment ' Scintillator Sample, Rack-Pos, Time: . H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: r : .. ';'.' .. 8. *.::*;* I, ... ! *,),..... 7 . I : I *..: .. :c I j i.) : ,. I. 6 'l,,:,* s I';\ :iE ; \:* .. 5 4 I () ! 3 -I* [ f 2 -i . ,. f l 1 -f ! . ! 0 100 t" r:,_. , ____ _ j' ! : -. i ' ... . j i*' Page' 5212of5809 200 300 28 Sep 2016 13:56:34 28 Sep 2016 14:41 :57 S07092849-1AXLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 13 49-1 45.00 134.9 1540 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date . User Filename : Spectrum Type User Number User Id *
  • User . Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Pu-241 -Start, End: . Win2: -Start, End: ' t .;; I ! I *: ... ::i 4 -"O I o I 3 -I l 2 Ii f . F. t*' .. ' I I* 0 100 Page '5213 of 5 809 200 300 28 Sep 2016 14:43:24 28 Sep 201615:28:46 S07092849-2A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 14 49-2 45.00 134.6 1473 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Numper (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename
  • Spectrum Type ; User Number ; User Id
  • User Comment : Scintillator
  • Sample, Rack-Pos, Time: H#, Total Counts:
  • Win1: Pu-241 -Start, End: . Win2: -Start, End: . \ 2 i 28 Sep 2016 15:30:12 28 Sep 2016 16:15:34 S07092849-3A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 15 49-3 45.00 134.3 1508 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 I . 1 ...
  • 0 .. * .. : ... . . . i :: : 'i.'.'. ; (*,=!: i '* f : .. *:* : .. l. 0 Page* 5214 of 5809 100 200 300 400 500 600 700 800 Channel Number (Log) 900 Sample Count Start Time:
  • Data Capture Date . User Filename Spectrum Type User Number User Id . User Comment : Scintillator
  • Sample, Rack-Pos, Time: : H#, Total Counts: . Win1: Pu-241 -Start, End: : Win2: -Start, End: t I t i' l*: I*. I' 2 1 -28 Sep 2016 16:16:59 28 Sep 2016 17:02:21 S07092849-4A.XLS U07092803-1 A.XLS Log Counts 07 BROWN LIQUID 16 136.5 0 0 49-4 1476 300 990 SPECTRUM PLOT USER 07 -PU-241 45.00 t '. 0 1-n-..zlllumll!_..,.. ___ I. 0 I . I., .. 100 200 300 400 500 600 700 800 Channel Number (Log) 900 [ . ,_._,,_ .. ---------------------------------*--------' i . ' . .... : ." 1:..: .. ;1! I : ...... .. Page 5215of5809 Sample Count Start Time:
  • Data Capture Date User Filename Spectrum Type
  • User Number User Id User Comment . Scintillator . Sample, Rack-Pas, Time:
  • Htt, Total Counts: Win1: Pu-241 -Start, End: ** Win2: -Start, End: r.J: 6 . j. i-*i' 2 1
  • I;*' 0 100 200 300 28 Sep 2016 17:03:45 28 Sep 2016 17:49:07 S07092849-5A.XLS U07092803-1 A.XLS Log Counts 07 PU-241.c BROWN LIQUID 17 135.2 0 0 49-5 1453 300 990 SPECTRUM PLOT USER 07 -PU-241 400 45.00 I __ >';. __________________ 500 600 700 800 900 j -i: ; ;-*.:'* f. , . 1. Page 5216of5809
Sample Count Start Time: : Data Capture Date . User Filename
  • Spectrum Type
  • User Number . User Id User Comment ; SCintillator . Sample, Rack-Pas, Time: : H#, Total Counts:
  • Win1: Pu-241 -Start, End: Win2: -Start, End: . . 7 100 f. :.,.: '.: Page 52i 7 of 5809 200 300 28 Sep 2016 17:50:32 28 Sep 2016 18:35:54 S07092849-6A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 18 49-6 45.00 135.2 1531 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900
  • Sample Count Start Time: Data Capture Date . User Filename Spectrum Type User Number User Id
  • User Comment
  • Scintillator : Sample, Rack-Pos, Time:
  • H#, Total Counts:
  • Win 1: Pu-241 -Start; End: ; Win2: -Start, End: :*. 7 0 100 * .. :.:.i*l . '*:.: ,* ,,, ,*_ .. ; * .. :._:: r. t f ' **. **. '1. : .. ::* Page' 5218 of5809 200 300 28 Sep 2016 18:37:17 28 Sep 2016 19:22:39 $07092849-7 A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 19 49-7 45.00 145.8 1420 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time:
  • Data Capture Date *. User Filename Spectrum Type User Number . User Id . Comment . Scintillator
  • Sample, Rack-Pos, Time: : H#, Total Counts:
  • Win1: Pu-241 -Start, End:
  • VVin2: -Start, End: :*. i . r f 28 Sep 2016 20:10:44 28 Sep 2016 20:56:07 S07092849-9A.XLS U07092803-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 21 136.5 0 0 49-9 1416 300 990 SPECTRUM PLOT USER 07 -PU-241 45.00 I * ; , : o k ! ** f .. f: :.:'°. 0 100 .. ------i i jH: i ... ,. ... _;! J '<*:::, ( Page S219of5809 200 300 400 500 600 700 Channel Number (Log) 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: I:;. 7 5 -Q 1 ; l ' ... ;* i** ; Page' 5220 of 5809 1QO 200 300 28 Sep 2Q16 22:Q8:37 28 Sep 2Q16 22:54:QO SQ7Q92852-1 QA.XLS U07Q928Q2-1 QA.XLS Log Counts 07 PU-241 BROWN LIQUID 10 52-10 45.00 133.8 1336 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log). '700 8QO 90Q

. Sample Count Start Time: Data Capture Date : User Filename ' Spectrum Type

  • User Number . User Id . User Comment ' Scintillator . Sample, Rack-Pos, Time: :-H#, Total Counts: 'Nin1 :. Pu-241 -Start, End: : Win2: -Start, End: r. i ' Page 5221of5809 28 Sep 2016 23:41 :58 29 Sep 2016 00:27:22 S07092952-12A.XLS U07092802-1 QA.XLS Log Counts 07 PU-241 BROWN LIQUID 12 52-12 45.00 134.0 2875 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 900
J[ JC.Ji 1r=* 1u *-*=:::: 4 ::IL 7 PRESET TIME Dr-HA CALC: COUNT BLAN!-< TWCl PHASE SCINTILLATOR: L.ElJEL L1.5. 1Zl0 CPM NO NO LIQUID YES CO'MMENT:BRDWl\I 1-rn Sf-i!VIPLE :: ICtt-. NCJ REPLICATES . AQC " f\I[) CYCLE: REPEATS " " . LUMEX: ND LOW SAMPL.E RE.J: Hf:lLF L_IFE CORRECTION* CH{:)l\J: IZI. IZI *-3G211Zt,, IZI o/.EfXROR 2. l211Zl FACTOR: 1.
  • IZllZllZllZllZllZI 121. 0 -* 900. IZI 1210 FACTOR: 1
  • IZI 1Z11z11z11z11z1 SAM POS TIME H:f:I; ___ .. 1. ___ ,_, LUMEX ELAPSED NO MIN CPM 1..ERROR 't. TIME 61Z1*-*l IZllZI i :;o:.c,. f..\ 7.56 Hi:I. 85 L1 .* 'i:Jl1. 4E,. :l1 s*=:* *--Li*5. !Zt0 :l35,. 1 7.38 :t1Z1. 98 5. f.:H?.1 92.75 J../ ;3 617.1-*3 L1.5. IZllZI 13L1 .* 7 l.IZI ... 43 E,, 1219 139.37 _5L1. E,1Z1 .. -.c" 4.5. IZ!IZl :l. ;?;t:,. Lt. 7.62 1.IZI .. 80 E.. IZIE: l.86. 1211 1q 1:: ,_, f;rzi-5 11. 5 .. IZ!IZ1 J.;:::7. 6 1. Ii.). 8:l E:32" E,Li. i,z_.6 6121 .. -6 IZJQ) l 3'4*. LJ. 8.29 UZI. 36 .. 23 Page 5222 of 5809 PAGE: l i'.::'3 SEP 2e116 * :l PRINTER . STD . 1 RSE'.!3i=-: :EDIT 1 .. CIFF IZI none BKG .. IZI BKG. SUB: 121 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: **;;. 8 I..:= 7 0 100 :****:* Page 52i3 of 5809 200 300 29 Sep 2016 09:55:26 29 Sep 2016 10:40:50 807092960-1 A.XLS U07092960-1A.XLS Log Counts 07 PU-241 BROWN LIQUID 1 134.8 0 0 60-1 1332 300 990 SPECTRUM PLOT USER 07 -PU-241 400 500 45.00 600 Channel Number (log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: 8 .. ::. 7 *:> .' *:.:* .. .. .. 6 -::,:;.::ii : 5 3 2 29 Sep 2016 10:42:04 29 Sep 2016 11 :27:27 S07092960-2A.XLS U07092960-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 2 135.1 0 0 60-2 1347 300 990 SPECTRUM PLOT USER 07 -PU-241 45.00 *
  • 0 ....... 0 100 200 300 400 500 600 700 Channel Number (Log) . : . Page 5224 of 5809 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator SAmple, Rack-Pos, Time: H#, Total Counts: Win1: Pu-241 -Start, End: \Nin2: -Start, End: ' .... :. : ... *:., 6 .*. !. . 2 29 Sep 2016 11 :28:41 29 Sep 2016 12:14:05 S07092960-3A.XLS U07092960-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 3 60-3 134.7 1331 0 300 0 990 SPECTRUM PLOT USER 07
  • PU-241 45.00 0 -: .... ! ,* ' I " '., ;-*-. Page 5225 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number Id User Comment
  • Scintillator Sample, Rack-Pas, Time: !-!#,Total Counts: Win1: Pu-241 -Start, End: Vl/in2: -Start, End: 7 . .-;)lo-. 6 ..,::,:* . .-: 0 100 Page 5226 of 5809 200 300 29 Sep 2016 12:15:20 29 Sep 2016 13:00:43 S07092960-4A.XLS U07092960-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 4 136.4 0 0 60-4 1344 300 990 SPECTRUM PLOT USER 07 -PU-241 400 500 45.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#,Total Counts: Win1: Pu-241 -Start, End: \f\Jin2: -Start, End: 1 *.i*;,.c I ;J;;;;., 5 -2 ... 0 -hlli ......... 0 ... '. Page 5227 of 5809 100 200 300 29 Sep 2016 13:01 :57 29 Sep 2016 13:47:21 S07092960-5A.XLS U07092960-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 5 60-5 45.00 127.6 1360 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filenarne Spectrum Type User Number User Id User Comment . Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Pu-241 -Start, End: Win2: -Start, End: *.\.'.*. 8 ; I* ..... : i. l i * .. * ' f. 6 -3 Page 5228 of 5809 100 200 300 29 Sep 2016 13:48:33 29 Sep 2016 14:33:57 S07092960-6A.XLS U07092960-1 A.XLS Log Counts 07 PU-241 BROWN LIQUID 6 60-6 45.00 134.4 1379 0 300 0 990 SPECTRUM PLOT USER 07 -PU-241 400 500 600 Channel Number (Log) 700 800 900 BATCH NUMBER : 1596402 SAMPLE ID : R0405235021_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G +/-0.195 % CHAMBER : 089 DETECTOR SIN : 79988 AVERAGE %EFFICIENCY : 29.2461 AVERAGE %EFF ERROR : 0.5651 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 72.2 +/-7.136 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.1634E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 PU-244: ""97-4597 keY I PU-242: .¢654-4995 keV 15 i PU-239: 5011*5227 keY l PU-23B: 5375-5566 keV 13 FU*236; 5582-5843 l<eV i 11 ! 9 l I n-, l PEAK ENERGY 5744.73 5484.82 5195.39 4876.70 4554.41 1 i i I l I ll PEAK FWHM 192.598 123.460 24.692 75.558 74.076 ! I !i I! l! ll . l 2394 2791 3193 3598 4006 441 Energy (keV) COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 GROSS AREA 5.000 3.000 3.000 229.000 3.000 I 1 I '11 '/ ! i iii ! NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G -1.240 6.240 2.4980 100.000 -2.60E-02 1.080 1.920 1.3856 99.900 1.88E-02 -0.120 3.120 1.7664 99.900 -2.0BE-03 222.040 6.960 2.6382 100.000 3.84E+OO 1.320 1.680 1.2961 99.900 2.29E-02 I . l .... I l .. 6110 6543 6980 7420 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B089.CNF;1435 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W089.CNF;384 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.13E-01 2.55E-01 9.61E-02 7.27E-02 1.41 E-01 4.42E-02 7.45E-02 1.64E-01 5.60E-02 7.59E-01 2.19E-01 8.36E-02 7.18E-02 1.34E-01 4.11E-02 1.96-sigrna cnt Unc pCi/G 1.13E-01 7.26E-02 7.44E-02 5.16E-01 7.17E-02 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596402 SAMPLE ID : R0405235022_PU SAMPLE QTY : 0.505 G +/-0.198 % CHAMBER : 090 DETECTOR SIN : 78263 AVERAGE %EFFICIENCY : 33.4344 AVERAGE %EFF ERROR : 0.6443 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 69.9 +/-6.695 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.0627E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5643.27 PU-238 5486.00 5470.34 PU-239 5155.00 5110.12 PU-242 4890.00 4872.46 PU-244 4589.00 4518.38 __ PU-244: 4497-45!17 keV i PU*242: 4654-.4995 keV 17 l PU-239: 5".l11-5227 keV i PU-238: 5375-5566 keV 15 !-P\J-236: 5582°5843 keV ! ! 13 l-I 11 $ 9L I-z I :::::> 0 I 8 ' ' *:; n I <( i 1 t-i . i 2398 2796 3199 3606 Energy (keV) PEAK FWHM 39.587 0.000 4.948 57.731 4.948 l' i ' 4018 44 COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.520 0.480 0.6928 100.000 2.94E-02 0.000 -0.960 0.960 0.9798 99.900 -1.54E-02 1.000 0.040 0.960 0.9798 99.900 6.37E-04 246.000 245.760 0.240 0.4899 100.000 3.91E+OO 1.000 0.520 0.480 0.6928 99.900 8.28E-03 >> .,,_ g-..... ..,g " J! _,....T"" 711 6145 6584 7028 7476 .. N lll 'l' 'l' ::> ::> ::> 0. Q. Q. c.. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAf?-A-035 LIB FILE : PU BKG FILE : B090.CNF;1440 BKG DATE : . 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W090.CNF;374 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.75E-02 1.07E-01 2.45E-02 3.57E-02 1.06E-01 2.88E-02 4.73E-02 1.05E-01 2.86E-02 7.25E-01 7.63E-02 1.43E-02 4.61E-02 8.82E-02 2.02E-02 1.96-sigma cnt Unc pCi/G 6.74E-02 3.56E-02 4.72E-02 4.90E-01 4.60E-02 0 H") Vl 00 0 '-0 Alpha Spectrosoopy Software Version 3.5.3 effective dale: 02-t&r-2015 BATCH NUMBER : 1596402 SAMPLE ID : R0405235023_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT --SAMPLE QTY : 0.504 G +/-0.198 % CHAMBER : 091 DETECTOR S/N : 78259 AVERAGE %EFFICIENCY : 34.7245 AVERAGE %EFF ERROR : 0.6687 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 68.9 +/-6.641 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.0185E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5704.53 PU-238 5486.00 5498.56 PU-239 5155.00 5118.68 PU-242 4890.00 4856.68 PU-244 4589.00 4510.45 fNJ lJ 17 _ P\J.2.._.: 4497-4597 keV l PU-2-42: -4654-4995 keV P!J-239: 5011-5227 keV 15 f--PU*236: 5375-5506 keV J PU*236: 5582-5843 keV I 13 i--! 11 Ui I 91 I-z :::> 0 s c t5 I <( PEAK FWHM 4.930 83.811 0.000 68.610 14.790 COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.280 0.720 0.8485 100.000 5.31E-03 3.000 2.040 0.960 0.9798 99.900 3.20E-02 0.000 -0.480 0.480 0.6928 99.900 -7.48E-03 253.000 251.560 1.440 1.2000 100.000 3.92E+OO 3.000 2.760 0.240 0.4899 99.900 4.30E-02 ... 1:2 §1 Sl """ 1 h I i I ill, .--,..-!-. I i I I I I 2382 2779 3180 3586 3996 441 4831 5 5 683 6116 6553 6996 7442 Energy (keV) ., .. :; it "' " 0. 0. 0. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B091.CNF;1438 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W091.CNF;363 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.56E-02 1.16E-01 2.9e;E-02 6.38E-02 1.03E-01 2.82E-02 3.32E-02 8.63E-02 1.98E-02 7.20E-01 1.15E-01 3.42E-02 6.23E-02 7.47E-02 1.40E-02 1.96-sigma cnt Uno pCi/G 5.56E-02 6.37E-02 3.31E-02 4.87E-01 6.20E-02 A!pha Software Version 3.5.3 effective date: 02*Mar-2015 BATCH NUMBER : 1596402 SAMPLE ID : R0405235024_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G +/-0.198 % CHAMBER : 092 DETECTOR S/N : 80063 AVERAGE %EFFICIENCY : 30.3421 AVERAGE %EFF ERROR : 0.5858 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 67.1 +/-7.160 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.9431 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 ,--PU*244: ke:V I PU*242: 4654-4595 keV 17 r PU*235: 5011-5227 keV I f'\J-238: 5375-5506 kcV 15 r-PU*236: 5582*5843 keV l 13 f-' i 11 f--9 i 5 j 3 l 1 I. . . i 5712.25 5430.46 5119.91 4873.62 4552.77 , I PEAK FWHM 0.000 4.922 118.128 74.814 59.064 2406 2802 3203 3608 4017 44 Energy (keV) COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -1.06E-02 1.000 0.040 0.960 0.9798 99.900 7.35E-04 2.000 0.080 1.920 1.3856 99.900 1.46E-03 216.000 214.320 1.680 1.2961 100.000 3.91E+OO 2.000 1.520 0.480 0.6928 99.900 2.78E-02 ' I ' ' ' I . ' 5 7 D698 6129 6565 7005 7449 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B092.CNF;1442 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W092.CNF;414 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.71E-02 1.23E-01 2.81E-02 5.45E-02 1.21 E-01 3.30E-02 6.72E-02 1.47E-01 4.6SE-02 7.75E-01 1.41 E-01 4.33E-02 6.39E-02 1.01 E-01 2.32E-02 1.96-sigma cnt Unc pCi/G 4.70E-02 5.45E-02 6.71E-02 5.27E-01 6.38E-02 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596402 SAMPLE ID : R0405235025_PU SAMPLE QTY : 0.506 G +/-0.198 % CHAMBER : 093 DETECTOR S/N : 33206 AVERAGE %EFFICIENCY : 33.0892 AVERAGE %EFF ERROR : 0.6377 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 75.4 +/-6.518 % COUNT DATE : 24-Sep-2016 20:54:51 ELAPSED LIVE TIME{SEC) : 14400.00 TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.3032E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 r 15 !-PU-239: 5011-5227 keV 'I PU*23S: 5375-5566 keV 1 3 r* PU*23S: 5582-5843 keV i 11 I i 5 r-! PEAK PEAK ENERGY FWHM 5712.27 0.000 5446.19 0.000 5118.70 0.000 4889.29 80.246 4558.92 0.000 l l GROSS AREA 0.000 3.000 0.000 264.000 6.000 1 I' I I ! I i I *! 11 i ii i iil 1 I j. 2407 2806 3210 3617 4029 Energy {keV) NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN AREA AREA StDev -1.200 1.200 1.0954 100.000 1.320 1.680 1.2961 99.900 -1.680 1.680 1.2961 99.900 262.320 1.680 1.2961 100.000 6.000 0.000 0.0000 99.900 i . 6145 6580 7019 ACTIVITY pCi/G -2.17E-02 1.98E-02 -2.50E-b2 3.90E+OO 8.93E-02 7462 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 1 LIB FILE : PU I BKG FILE : B093.CNF;1431 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W093.CNF;379 CAL DATE : 06-Sep-2016 1.96-sigma TPU pCi/G 4.11E-02 6.21E-02 3.53E-02 7.04E-01 7.84E-02 MDA pCi/G 1.27E-01 1.16E-01 1.15E-01 1.15E-01 4.47E-02 Le pCi/G 3.62E-02 3.56E-02 3.54E-02 3.53E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.11E-02 6.20E-02 3.53E-02 4.75E-01 7.75E-02 BATCH NUMBER : 1596402 SAMPLE ID : R0405235026_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G +/-0.199 % CHAMBER : 095 DETECTOR S/N : 38626 AVERAGE %EFFICIENCY : 30.4247 AVERAGE %EFF ERROR : 0.5873 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 83.6 +/-6.457 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS ; 3.6642E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 5712.28 0.000 PU-238 5486.00 5527.73 4.993 PU-239 5155.00 5141.73 89.878 PU-242 4890.00 4870.78 77.811 PU-244 4589.00 4548.76 44.939 {If) u l PU*244: 4497-4597 keV '-PU*242: 4654-4995 keV 17 I P\J.239: 5011-5227 keV P\J.238: 5375-5500 keV 15 i f'U*236: 5582-5843 keV 13 11 L -CJ) I-z ::::> 0 8 I .2:-3! t5 1 [ <( I Ii I i ! I ... .--, -.' -. *-1 . . . . i . 2380 2781 3186 3595 4007 Energy (keV} COUNT DATE : 24-Sep-2016 20:54:52 ELAPSED LIVE TIME(SEC} : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.960 0.960 0.9798 100.000 -1.71E-02 1.000 0.040 0.960 0.9798 99.900 5.92E-04 2.000 1.520 0.480 0.6928 99.900 2.24E-02 269.000 267.560 1.440 1.2000 100.000 3.93E+OO 2.000 2.000 0.000 0.0000 99.900 2.94E-02 ] >> ] > ll .,_ Sl ., m ""' "' i I I ' I' .I . ,_..,.,... ' ! . ! 5 6 694 6125 6559 6997 7439 "' .. "' "' ii: ii: 0. 0. Instrument SOP: GL-RAD-1-009 .... Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B095.CNF;1407 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W095.CNF;408 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.98E-02 1.18E-01 3.20E-02 4.39E-02 9.76E-02 2.66E-02 5.15E-02 8.15E-02 1.87E-02 7.03E-01 1.09E-01 3.23E-02 5.06E-02 4.41E-02 0.00E+OO 1.96-sigma cnt Unc pCi/G 3.97E-02 4.39E-02 5.14E-02 4.74E-01 5.04E-02 Alpha Spectrt>"""Jlll Software VefS!on 3.5.3 effective date: 02*Ma.r*2015 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BAT_C_H_N_U_M_B_E_R--:-1-59_6_4_0_2 _______ CHAMBER: 096 -SAMPLE ID : R0405235027 _PU I DETECTOR S/N : 80016 SAMPLE QTY : 0.510 G +/-0.196 % I AVERAGE %EFFICIENCY : 32.5188 . Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU I BKG FILE : B096.CNF;1399 I BKG DATE : 23-Sep-2016 1 BKG LIVE TIME(SEC) : 59999:99 SAMPLE DATE : 08-Dec-2015 00:00:00 I AVERAGE %EFF ERROR : 0.6269 ANALYST : MXS2 COUNT DATE : 24-Sep-2016 20:54:52 % YIELD : 78.8 * +/-6.434 % ) ELAPSED LIVE TIME(SEC) : 14399.99 I EFF FILE : W096.CNF;357 TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 3.4539E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5728.41 PU-238 5486.00 5419.38 PU-239 5155.00 5137.74 PU-242 4890.00 4870.70 PU-244 4589.00 4561.87 f'U.24': ""97-4597 keV 21 t= PU*Z42:4654-4995keV. I PU*239: 5011 *5227 keV 19 L l'U-238: 5375-5585 keV j f'U.236: 5582-5843 keV 17 r-15 j <ii 13 ! I-11 I-z :::> 0 l () 7 I--; 5 f-I 0 3L -< 1 I ili!li .. ! I i 2391 2788 3189 3595 Energy (keV) j PEAK GROSS FWHM AREA 162.816 4.000 4.934 1.000 4.934 1.000 41.526 271.000 19.735 2.000 ll ..... !, Ii ll ifi I ! ii I I \ I 4004 441 4837 ::! N "! ::> "-0.. J CAL DATE : 06-Sep-2016 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc AREA AREA StDev pCi/G pCi/G pCVG pCVG pCi/G 2.560 1.440 1.2000 100.000 4.46E-02 7.96E-02 1.29E-01 3.83E-02 7.94E-02 -0.680 1.680 1.2961 99.900 -9.84E-03 4.45E-02 1.12E-01 3.43E-02 4.45E-02 0.280 0.720 0.8485 99.900 4.03E-03 4.21E-02 8.78E-02 2.23E-02 4.21E-02 269.560 1.440 1.2000 100.000 3.87E+OO 6.90E-01 1.06E-01 3.16E-02 4.65E-01 1.040 0.960 0.9798 99.900 1.SOE-02 5.11E-02 9.47E-02 2.58E-02 5.11E-02 i i § I 11 ' I 5 6( >687 6118 6554 6994 7438 "' 2 2 a.

BATCH NUMBER : 1596402 SAMPLE ID : R0405235028_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G +/-0.197 % CHAMBER : 097 DETECTOR S/N : 83288 AVERAGE %EFFICIENCY : 35.3557 AVERAGE %EFF ERROR : 0.6805 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 82.0 +/-6.081 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.5921 E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 23 ,-PIJ-244: 4497-4597 keV I PU-242: 4654-4995 keV 21 L PIJ-239: 5011-5227 keV I PU-238: 5375-5566 keV 19 PU-238: 5582*5!!43 keV 17 l-15 0' 11 z ! ;:) 9 f-0 j CJ ....... 0 <( 7 'i i 5 ! PEAK ENERGY 5712.14 5470.35 5142.96 4869.37 4542.65 PEAK FWHM 236.442 0.000 68.962 54.431 4.926 3 f-1 i ! ii i ii !! . I . ' ' I ' ' ' I ' 2402 2798 3198 3603 Energy (keV) COUNT DATE : 24-Sep-2016 20:54:52 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 0.560 1.440 1.2000 100.000 8.77E-03 0.000 -0.480 0.480 0.6928 99.900 -6.18E-03 3.000 2.280 0.720 0.8485 99.900 2.92E-02 306.000 304.800 1.200 1.0954 100.000 3.89E+OO 4.000 4.000 0.000 0.0000 99.900 5.12E-02 ' ' ! ' I 5688 6118 6551 6989 7431 it -A Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B097.CNF;1396 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W097.CNF;381 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.67E-02 1.16E-01 3.44E-02 2.74E-02 7.13E-02 1.63E-02 5.17E-02 7.81E-02 1.99E-02 6.56E-01 8.96E-02 2.56E-02 5.67E-02 3.84E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.66E-02 2.73E-02 5.16E-02 4.39E-01 5.64E-02 Alpha Spectro&copy Software Version 3.5.3 effective dale: 02*PAar*2015 BATCH NUMBER : 1596402 SAMPLE ID : R0405235029 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.504 G -+/-0.198 % CHAMBER : 099 DETECTOR SIN : 80059 AVERAGE %EFFICIENCY : 35.6284 AVERAGE %EFF ERROR : 0.6858 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 78.0 +/-6.192 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dprn RESULTS : 3.4182E+OO dprn NUCLIDE

  • LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5781.43 PU-238 5486.00 5483.83 PU-239 5155.00 5154.17 PU-242 4890.00 4871.59 PU-244 4589.00 4578.50 21 I 19 r Pll*239: 5011*5227 keV PlJ.238: 5375-55* keV 17 PlJ.236: 5582*5843 keV I 15 I I 13 f-PEAK FWHM 4.881 4.881 112.262 57.642 0.000 $ i 11 f-I-I z :::J 9 ;-0 Q l c *:;; :.;::::; 3 f-0 <( I I 1 i-Ii ! I I I! I i !l! 1 ! H I ' 2402 2795 3193 3595 4001 441 Energy (keV) COUNT DATE : 24-Sep-2016 20:54:52 ELAPSED LIVE TIME(SEC) : 14399.99 GROSS AREA 1.000 4.000 2.000 293.000 ::> c. 2.000 ='> a. J l I I NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA SIDev pCi/G 0.040 0.960 0.9798 100.000 6.57E-04 3.520 0.480 0.6928 99.900 4.75E-02 1.520 0.480 0.6928 99.900 2.04E-02 292.280 0.720 0.8485 100.000 3.92E+OO 1.280 0.720 0.8485 99.900 1.72E-02 II I I 5 4 674 6104 6539 6978 7421 "' ::> ; a. a. c. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8099.CNF;1399 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W099.CNF;383 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.88E-02 1.08E-01 2.95E-02 6.05E-02 7.48E-02 1.71E-02 4.69E-02 7.43E-02 1.70E-02 6.72E-01 8.19E-02 2.08E-02 4.73E-02 8.20E-02 2.09E-02 1.96-sigma cnt Unc pCi/G 4.87E-02 6.02E-02 4.68E-02 4.51E-01 4.73E-02 BATCH NUMBER : 1596402 SAMPLE ID : R0405235030_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G +/-0.195 % CHAMBER : 253 DETECTOR S/N : 87941 AVERAGE %EFFICIENCY : 25.6727 AVERAGE %EFF ERROR : 0.4975 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 80.8 +/-7.083 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.5427E+OO dpm NUCLIDE LIBRARY en 1-z :'.:) 0 8 :;::. :2: 0 <( ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 _ PU-244: 4497-4597 keV J PU-242: 4654-4995 keV 15 l PU-239: 5011*5227 keV ii PU-238: 5375-5566 keV 1 3 r-PU-236: 55$2-5843 keV I 11 L I 9 t-7 L I I PEAK ENERGY 5783.09 5451.69 5135.71 4855.64 4533.36 PEAK FWHM 4.985 104.681 89.727 58.156 54.833 1 L, ! l il COUNT DATE : 24-Sep-2016 20:51:04 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.520 0.480 0.6928 100.000 1.12E-02 2.000 1.280 0.720 0.8485 99.900 2.27E-02 2.000 1.040 0.960 0.9798 99.900 1.83E-02 219.000 218.280 0.720 0.8485 100.000 3.84E+OO 3.000 2.520 0.480 0.6928 99.900 4.44E-02 I I 2368 2769 3173 3581 3993 440 4827 5 5( 676 6106 6540 6977 7418 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B253.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W253.CNF;112 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA le pCi/G pCi/G pCi/G 6.24E-02 1.19E-01 2.74E-02 6.26E-02 1.08E-01 2.76E-02 6.27E-02 1.16E-01 3.16E-02 7.54E-01 1.07E-01 2.74E-02 7.08E-02 9.76E-02 2.24E-02 1.96-sigma cnt Unc pCi/G 6.23E-02 6.25E-02 6.26E-02 5.12E-01 7.0SE-02 BATCH NUMBER : 1596402 SAMPLE ID : R0405235031_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.517 G +/-0.193 % CHAMBER : 254 DETECTOR S/N : 87942 AVERAGE %EFFICIENCY : 25.1642 AVERAGE %EFF ERROR : 0.4879 SAMPLE DATE : 26-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 84.1 +/-7.016 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.6845E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 r PU*244: 4497-4597 keV 19 L PU*242: 4654-4995 keV I PU-239: 5011-5227 keV I PU*238: 5375-556$ keV 17 I PU*23B: 5562*5843 keV 15 L ! 13 f-l 11 f-z 6 s i 5f--: PEAK ENERGY 5772.49 5470.36 5118.70 4886.46 4549.83 PEAK FWHM 29.851 0.000 0.000 55.224 9.950 1 L ii J_L,' . ..,---,-. -,.... -,-I -.-, -.-. ' 1 .* !J I ' 2385 2785 3188 3596 4007 44 .... Energy (keV) COUNT DATE : 24-Sep-2016 20:51:06 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 2.000 1.280 0.720 0.8485 100.000 2.69E-02 0.000 -0.480 0.480 0.6928 99.900 -8.30E-03 0.000 -0.480 0.480 0.6928 99.900 -8.25E-03 223.000 222.520 0.480 0.6928 100.000 3.82E+OO 2.000 1.760 0.240 0.4899 99.900 3.02E-02 I II ll .IJ !' ., r I NI 'I 11 i i ' l . 4841 5,>6: >689 6119 6553 6991 7432 Instrument SOP: GL-RAD-1-009 ______ SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8254.CNF;458 BKG DATE : BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W254.CNF;116 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.41E-02 1.28E-01 3.26E-02 3.68E-02 9.58E-02 2.19E-02 3.65E-02 9.51E-02 2.18E-02 7.42E-01 9.50E-02 2.18E-02 5.96E-02 8.24E-02 1.54E-02 1.96-sigma cnt Unc pCi/G 7.40E-02 3.67E-02 3.65E-02 5.04E-01 5.94E-02 BATCH NUMBER : 1596402 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU SAMPLE ID : R0405235032 PU SAMPLE QTY : 0.508 G -+/-0.197 % CHAMBER : 255 DETECTOR S/N : 87943 AVERAGE %EFFICIENCY : 24.9747 AVERAGE %EFF ERROR : 0.4844 BKG FILE : 8255.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 79.2 +/-7.248 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 3.4709E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.27 PU-238 5486.00 5468.93 PU-239 5155.00 5118.70 PU-242 4890.00 4874.01 PU-244 4589.00 4498.27 !JIJ lit? 19 l PU-24A: 4'97-4597 keV v I PU-242: 4654-4995 ke v v 17 I PU*239: 5011*5227 ke l PU-238: 5375-5566 ke i PU-238: 5582*5843 ke 151 ! 13 t-i -11 r-9 5 (.)-I 5 f-3 i 1 r* : v r-.-. -. --, .-.. -' II Ii ' i PEAK FWHM 0.000 84.520 0.000 53.447 0.000 I I I i ! ! 3180 2377 2776 Energy (keV) 3588 3999 441 5 -COUNT DATE : 24-Sep-2016 20:51:08 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -1.10E-02 3.000 2.280 0.720 0.8485 99.900 4.29E-02 0.000 -1.680 1.680 1.2961 99.900 -3.14E-02 209.000 208.040 0.960 0.9798 100.000 3.89E+OO 1.000 0.040 0.960 0.9798 99.900 7.48E-04 j I ! i l I ! 111 ' ' I l ' 4834 5 >685 6116 6551 6990 7434 EFF FILE : W255.CNF;120 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.87E-02 1.27E-01 2.91E-02 7.62E-02 1.15E-01 2.93E-02 4.44E-02 1.45E-01 4.44E-02 7.80E-01 1.23E-01 3.35E-02 5.55E-02 1.23E-01 3.36E-02 1.96-sigma cnt Unc pCi/G 4.86E-02 7.59E-02 4.43E-02 5.31E-01 5.54E-02 0 ........ VI 00 0 "° BATCH NUMBER : 1596402 SAMPLE ID : R0405235033 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.506 G -+/-0.198 % CHAMBER : 256 DETECTOR SIN : 87944 AVERAGE %EFFICIENCY : 25.7507 AVERAGE %EFF ERROR : 0.4991 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 70.2 +/-7.583 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.0757E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.27 PU-238 5486.00 5470.36 PU-239 5155.00 5167.96 PU-242 4890.00 4863.70 PU-244 4589.00 4506.88 e10 1 5 r PU-244: 4497-4597 keV i PU*242:4654-l995 keV l PU-239:5011*5=keV 13 t--11 L I 9 l-1 7[-1 i I 1 L I .. l ii ' j 2372' 2771 3173 3579 Energy (keV) PEAK FWHM 0.000 0.000 14.866 92.169 4.955 COUNT DATE : 24-Sep-2016 20:51:1r ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -1.21E-02 0.000 -0.720 0.720 0.8485 99.900 *1.49E-02 2.000 1.040 0.960 0.9798 99.900 2.14E-02 192.000 190.080 1.920 1.3856 100.000 3.90E+OO 1.000 0.520 0.480 0.6928 99.900 1.07E-02 5 4 667 6097 6530 6967 7407 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B256.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W256.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.36E-02 1.39E*01 3.19E-02 4.51E-02 1.26E-01 322E-02 7.31 E-02 1.35E-01 3.69E-02 8.20E-01 1.66E-01 5.21E-02 5.95E-02 1.14E-01 2.61E-02 1.96-sigma cnt Unc pCi/G 5.34E-02 4.50E-02 7.30E-02 5.60E-01 5.94E-02 BATCH NUMBER : 1596402 SAMPLE ID : R0405235034 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY :* 0.509 G -+/-0.196 % CHAMBER : 233 DETECTOR SIN : 87921 AVERAGE %EFFICIENCY : 25.2931 AVERAGE %EFF ERROR : 0.4905 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 96.6 +/-6.572 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.2344E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5512.84 PU-239 5155.00 5118.71 PU-242 4890.00 4869.83 PU-244 4589.00 4532.12 81() PU*244:A497-1597 keV 19 [ PU-2'2: 46$4-4995 l<eV I PU-239; 5011*5227 keV ! PU*238: 5375-5586 keV 17 t PU-236: 5582*5843 l<eV 15 I 13 i-11 z ::> 0 Q i 5 f-3 I 1 i-PEAK FWHM 0.000 4.971 0.000 71.772 0.000 ii j Jff ! l I ! l 2396 2795 3198 Energy (keV) 3605 4016 44 ; ::> 0.. COUNT DATE : 24-Sep-2016 20:54:08 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.760 0.240 0.4899 99.900 1.16E-02 0.000 -0.480 0.480 0.6928 99.900 -7.25E-03 258.000 257.040 0.960 0.9798 100.000 3.88E+OO 3.000 3.000 0.000 0.0000 99.900 4.53E-02 I !!1 _i. I l I r ! 4848 5 6 694 6123 6555 6991 7431 "' "' ::> ::> ::> :, c. 0. 0. c. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B233.CNF;454 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W233.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.74E-02 5.55E-02 O.OOE+OO 4.34E-02 7.29E-02 1.36E-02 3.21 E-02 8.37E-02 1.92E-02 7.06E-01 9.94E-02 2.71E-02 5.99E-02 4.53E-02 O.OOE+OO 1.96-sigma cnt Uno pCi/G 3.73E-02 4.33E-02 3.21E-02 4.76E-01 5.96E-02 BATCH NUMBER : 1596402 SAMPLE ID : R0405235035 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.516 G -+/-0.194 % CHAMBER : 234 DETECTOR S/N : 87922 AVERAGE %EFFICIENCY : 24.8037 AVERAGE %EFF ERROR : 0.4811 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 74.6 +/-7.460 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAl : 4.3831 E+OO dpm RESULTS : 3.2717E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.30 PU-238 5486.00 5465.26 PU-239 5155.00 5226.77 PU-242 4890.00 4870.16 PU-244 4589.00 4562.94 fjfJ q /{fl Jrv I PU-2"': 4497 .. 597 keV PU-242: 4654_.995 keV 15 1-PU-239: 5011-5227 keV ! PU-238: 5375-5566 keV 13 PU-236:55S2*5843keV L 11 I PEAK FWHM 0.000 4.996 0.000 59.123 4.996 00 9 f-I I-z :J I 0 s ' c I *;;; 3 !-u j <( 1 ! l I' I l I l! I _1 I I 2388 2790 3194 3603 4014 44 Energy (keV) COUNT DATE : 24-Sep-2016 20:54:11 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.480 0.480 0.6928 100.000 -1.16E-02 1.000 -0.440 1.440 1.2000 99.900 -8.71E-03 1.000 -0.920 1.920 1.3856 99.900 -1.81E-02 195.000 194.760 0.240 0.4899 100.000 3.83E+OO 3.000 3.000 0.000 0.0000 99.900 5.90E-02 EiiSi g;:: <ON .. g ., 11 I 11 1, *II !I ., ., I i 694 6123 6554 6990 7428 N "' !;l :'> ::> c. a. a. a. instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B234.CNF;454 BKG DATE : 23-Sep-2016 BKG LIVE TIME{SEC) : 60000.00 EFF FILE : W234.CNF;117 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.13E-02 1 .33E-01 3.06E-02 6.02E-02 1.46E-01 4.35E-02 6.12E-02 1.59E-01 4.99E-02 7.91E-01 9.42E-02 1.76E-02 7.82E-02 5.90E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.11E-02 6.02E-02 6.12E-02 5.39E-01 7.76E-02 GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-035 I CHAMBER : 235 LIB FILE : PU BATCH NUMBER : 1596402 SAMPLE ID : R0405235036_PU SAMPLE QTY : 0.518 G +/-0.193 % ., DETECTOR S/N : 87923 BKG FILE : B235.CNF;455 AVERAGE %EFFICIENCY : 24.7991 BKG DATE : 23-Sep-2016 SAMPLE DATE : 23-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 84.6 +/-7.054 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831E+OO dpm RESULTS : 3. 7098E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5805.53 PU-238 5486.00 5433.55 PU-239 5155.00 5146.52 PU-242 4890.00 4871.68 PU-244 4589.00 4546.97 8YJ _ PIJ-244: 4497-4597 keV I PIJ..2*2: 4654-4995 keV 15 r PIJ-239: 5011-5227 keV i f'U.238: 5375-5566 keV 13 L PIJ*238: 5582*5843 kaV I 11 I r en I-7L z :::> 0 2-c i :2! 3f-t5 I <i: 1 h I Ii I 'I I ! PEAK FWHM 29.867 14.933 64.712 70.163 0.000 '" 1*1 1* ! ! i I i 2392 2792 3196 3604 4016 44 Energy (keV) j AVERAGE %EFF ERROR : 0.4811 BKG LIVE TIME(SEC) : 60000.00 I COUNT DATE : 24-Sep-2016 20:54:13 EFF FILE : W235.CNF;118 ! ELAPSED LIVE TIME(SEC) : 14400.00 CAL DATE : 19-Sep-2016 ! NUCLIDE ACTIVITY SUMMARY 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G 2.000 0.800 1.200 1.0954 100.000 1.69E-02 7.59E-02 1.48E-01 4.25E-02 2.000 1.280 0.720 0.8485 99.900 2.23E-02 6.14E-02 1.06E-01 2.70E-02 2.000 1.040 0.960 0.9798 99.900 1.80E-02 6.15E-02 1.14E*01 3.10E-02 222.000 220.800 1.200 1.0954 100.000 3.81E+OO 7.45E-01 1.21 E-01 3.46E-02 0.000 -0.240 0.240 0.4899 99.900 -4.15E-03 3.59E-02 8.29E-02 1.55E-02 >> g;: "' ....... .. s f;i I i I h *'1 111 n l I 'I Ii I I ! I 5 7 701 6132 6566 7005 7447 ... l'l ra <:< a: a: ::> :::. n. 0. n. 1.96-sigma cnt Uno pCi/G 7.59E-02 6.13E-02 6.14E-02 5.06E-01 3.58E-02 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1S96402 i CHAMBER : 2SS SAMPLE ID : R040S23S037 PU SAMPLE QTY : O.S06 G -+/-0.198 % ! DETECTOR SIN : 87943 ,II AVERAGE %EFFICIENCY : 24.9747 . AVERAGE %EFF ERROR : 0.4844 SAMPLE DATE : 30-Nov-201S 00:00:00 ANALYST : MXS2 % YIELD : 67.4 +/-7.820 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.9S37E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5695.60 PU-238 5486.00 5470.35 PU-239 5155.00 5118.70 PU-242 4890.00 4866.83 PU-244 4589.00 4546.97 gvJ )oq )1 \; 14 _ PU*244: "'4!l7-4597 keV I PlJ.242: 4654--4995 keV 13 f-PU*239:5011*5=keV 12 11 10 t-9 8 i-7 L SL I 3r 2r 1 I PEAK FWHM 4.972 0.000 0.000 49.244 0.000 r. , . . , . .11. i-f.-.. r-r--* 2377 2776 3180 3588 3999 44 1D -Energy (keV) I COUNT DATE : 26-Sep-201613:SS:OS I ELAPSED LIVE TIME(SEC) : 14400.00 I NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.520 0.480 0.6928 100.000 1.40E-02 0.000 -0.720 0.720 0.8485 99.900 -1.60E-02 0.000 -1.680 1.680 1.2961 99.900 -3.71E-02 178.000 177.040 0.960 0.9798 100.000 3.90E+OO 0.000 -0.960 0.960 0.9798 99.900 -2.12E-02 I I Ii *I ,1 111 !. 111' u11L 11 11lil i . ' . I ' , I , ' . 'I'"-' ' I , . ' 4834 s >sf 6116 6SS1 6990 74 34 Instrument $OP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-03S LIB FILE : PU BKG FILE : 82SS.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W2SS.CNF;120 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.79E-02 1.49E-01 3.42E-02 4.84E-02 1.36E-01 3.45E-02 5.24E-02 1.71 E-01 5.24E-02 8.45E-01 1.45E-01 3.96E-02 4.92E-02 1.45E-01 3.96E-02 1.96-sigma cnt Unc pCi/G 7.78E-02 4.83E-02 5.23E-02 5.78E-01 4.91E-02 GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-035 BATCH NUMBER : 1596402 CHAMBER : 238 LIB FILE : PU SAMPLE ID : R0405235038_PU DETECTOR SIN : 87926 BKG FILE : B238.CNF;455 SAMPLE QTY : 0.501 G +/-0.200 % AVERAGE %EFFICIENCY : 26.1325 BKG DATE : 23-Sep-2016 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 76.4 +/-7.215 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.3490E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5490.86 PU-239 5155.00 5118.69 PU-242 4890.00 4867.80 PU-244 4589.00 4525.12 @fJ q101)111 17 PU-244: 4497-4597 keV J PU*242: 4554.4995 keV I PU-239: 5011*5227 keV 15 t-PU-238: 5375-5566 keV I PU-238: 5582*5843 keV 13 r r 11 I 7 l-s L I PEAK FWHM 0.000 39.647 0.000 59.058 4.956 1 ,,,_i _!_i'-, ""ll...-'-T'-2386 2784 3187 3594 4005 442 Energy (keV) AVERAGE %EFF ERROR : 0.5062 BKG LIVE TIME(SEC) : 60000.00 COUNT DATE : 24-Sep-2016 20:54:18 EFF FILE : W238.CNF;125 ELAPSED LIVE TIME(SEC) : 14400.00 CAL DATE : 19-Sep-2016 GROSS AREA 0.000 2.000 0.000 211.000 1.000 I 11 II. lj 4840 NUCLIDE ACTIVITY SUMMARY NET AREA -0.240 1.520 -0.480 210.040 1.000 5 6 BKG AREA 0.240 0.480 0.480 0.960 0.000 692 ::, 0. BKG %ABUN S!Dev 0.4899 100.000 0.6928 99.900 0.6928 99.900 0.9798 100.000 0.0000 99.900 I , . 6124 6561 7001 1.96-sigma ACTIVITY TPU MDA Le pCi/G pCi/G pCi/G pCi/G -5.50E-03 4.75E-02 1.10E-01 2.05E-02 2.87E-02 6.61E-02 1.05E-01 2.40E-02 -9.02E-03 4.00E-02 1.04E-01 2.38E-02 3.94E+OO 7.88E-01 1.24E-01 3.37E-02 1.88E-02 5.29E-02 5.63E-02 O.OOE+OO , ' I 7446 1.96-sigma cnt Unc pCi/G 4.74E-02 6.60E-02 3.99E-02 5.36E-01 5.28E-02 Alpha Spectroscopy Software v.,.;on 3.5.3 *. effective dare: 02*Mar*2015 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT -BA_T_C_H_N_U_M_B_E_R_: CHAMBER: 256 *--I SAMPLE ID : R0405235039 PU DETECTOR SIN : 87944 I SAMPLE QTY : 0.512 G -+/-0.195 % AVERAGE %EFFICIENCY : 25.7507 1 SAMPLE DATE : 30-Nov-2015 00:00:00 AVERAGE %EFF ERROR : 0.4991 1 ANALYST : MXS2 COUNT DATE : 26-Sep-2016 13:55:07 I % YIELD : 85.3 +/-6.918 % ELAPSED LIVE TIME(SEC) : 14400.00 I -------------------;--TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.7391 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5646.01 PU-238 5486.00 5470.36 PU-239 5155.00 5109.87 PU-242 4890.00 4854.54 PU-244 4589.00 4572.03 6\D )'\j 15 r FU-244: 4497-4597 lroV j PU-242: 4654-4995 keV I PU-239; 5011*5227 keV 13 I PU-238: 5375-5566 keV j PU-236: 558Z*SS43 keV i 11 I 9L 'Ci) I ! I-z 7 r-::::> ! 0 5 t-I I 3f-t5 i <l'.: 1 r I f ... I 2372 2771 3173 3579 Energy (keV) PEAK GROSS FWHM AREA 4.955 1.000 0.000 0.000 4.955 1.000 83.332 233.000 19.821 2.000 ------*--3989 440 4820 :i '1 °' °' ::> ::> "-"-NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN ACTIVITY AREA AREA StDev pCi/G 0.520 0.480 0.6928 100.000 1.06E-02 -0.720 0.720 0.8485 99.900 -1.21 E-02 0.040 0.960 0.9798 99.900 6.68E-04 231.080 1.920 1.3856 100.000 3.86E+OO 1.520 0.480 0.6928 99.900 2.54E-02 ]] """ 5 4 667 6097 6530 6967 7407 ::> "-"-Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B256.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W256.CNF;114 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.90E-02 1.13E-01 2.59E-02 3.66E-02 1.03E-01 2.61E-02 4.96E-02 1.1 OE-01 3.00E-02 7.39E-01 1.35E-01 4.24E-02 5.84E-02 9.25E-02 2.12E-02 1.96*sigma cnt Unc pCi/G 5.89E-02 3.66E-02 4.95E-02 5.01E-01 5.83E-02 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596402 SAMPLE ID : R0405235040_PU SAMPLE QTY : 0.515 G +/-0.194 % CHAMBER : 241 DETECTOR S/N : 87963 AVERAGE %EFFICIENCY : 25.9137 AVERAGE %EFF ERROR : 0.5022 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : MXS2 % YIELD : 66.9 +/-7.707 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.9309E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5539.52 PU-239 5155.00 5101.30 PU-242 4890.00 4891.22 PU-244 4589.00 4546.97 @J01}J4)Jv 14 13 LI PU-239: 5011*5227 keV 12 _ FU-238: 5375-5566 keV I PU-236: 5582*5843 keV 11 10 ! 9[ 7 f-6 5 :--4 j 31 2 l-1 l t . ' I ! I! .. I PEAK FWHM 0.000 4.964 94.325 79.018 0.000 ! l 2406 2805 3208 3615 4025 44 9 Energy (keV) COUNT DATE : 24-Sep-2016 20:54:22 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG o/oABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 -0.200 1.200 1.0954 99.900 -4.24E-03 3.000 2.760 0.240 0.4899 99.900 5.81E-02 183.000 182.280 0.720 0.8485 100.000 3.83E+OO 0.000 -0.240 0.240 0.4899 99.900 -5.05E-03 5 n 15705 6134 6567 7004 7445 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B241.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W241:CNF;131 CAL DATE : 19-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.19E-02 7.70E-02 o.oeE+oo 6.37E-02 1.49E-01 4.25E-02 8.42E-02 1.01E-01 1.89E-02 8.18E-01 1.28E-01 3.27E-02 4.37E-02 1.01 E-01 1.89E-02 1.96*sigma cnt Uno pCi/G 5.17E-02 6.36E-02 8.37E-02 5.60E-01 4.36E-02 BATCH NUMBER : 1596402 SAMPLE ID : R1203621725 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G -+/-0.193 % CHAMBER : 243 DETECTOR SIN : 87931 AVERAGE %EFFICIENCY : 24.8977 AVERAGE %EFF ERROR : 0.4829 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 83.2 +/-7.117 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.6456E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.29 PU-238 5486.00 5526.42 PU-239 5155.00 5167.95 PU-242 4890.00 4887.31 PU-244 4589.00 4548.84 8\-D r PU-244: 4497""4597 keV i PU-242: 4654-4995 keV 17 I PU-239; SOI 1-5227 keV i PU-238: 5375-5566 keV 15 !-IV-236: 5582*5843 keV i 13 11 L l 9 l 7 ! 5 ;-! l 1 Ii . I . . . i i PEAK FWHM 0.000 0.000 84.671 73.049 64.748 2389 2789 3193 3600 4011 Energy (keV) COUNT DATE : 24-Sep-2016 20:54:24 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 -0.960 0.960 0.9798 100.000 -1.68E-02 3.000 -2.760 5.760 2.4000 99.900 -4.83E-02 3.000 2.520 0.480 0.6928 99.900 4.41E-02 220.000 217.840 2.160 1.4697 100.000 3.81E+OO 3.000 2.760 0.240 0.4899 99.900 4.83E-02 *I j: ! I .! i m:, [ II I' .. '. I' Iii Ii ' 'II i I . , . ' 4843 5 )6t 5690 6118 6550 6986 7424 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8243.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W243.CNF;118 CAL DATE : 19-Sep!2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.91E-02 1.16E-01 3.15E-02 8.01E-02 2.07E-01 7.70E-02 7.04E-02 9.70E-02 2.22E-02 7.51E-01 1.47E-01 4.71E-02 7.00E-02 8.40E-02 1.57E-02 1.96-sigma cnt Unc pCi/G 3.90E-02 8.01E-02 7.01E-02 5.10E-01 6.96E-02 Alpha Spectroscopy Software Version 3.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596402 SAMPLE ID : R1203621726 PU SAMPLE QTY : 0.508 G -+/-0.197 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 244 DETECTOR S/N : 87932 AVERAGE %EFFICIENCY : 23.7184 AVERAGE %EFF ERROR : 0.4607 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : MXS2 % YIELD : 93.5 +/-6.885 % COUNT DATE : 24-Sep-2016 20:54:26 ELAPSED LIVE TIME(SEC) : 14400.00 TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.0988E+OO dpm -----NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5759.03 PU-238 5486.00 5497.91 PU-239 5155.00 5088.35 PU-242 4890.00 4886.10 PU-244 4589.00 4528.60 6V4!04)Ju r PU*244: 4497-0597 keV 19 L FIJ-242: 4654--1995 keV I PU-233: 5011-5227 keV 17 L PU-239: 6375-5566 keV I PU-236: 5582*5843 keV PEAK GROSS FWHM AREA 4.999 1.000 4.999 1.000 74.978 3.000 64.386 235.000 4.999 1.000 ;ll .,.,, "' ..,., ... j 1 ' 15 13 [-11t 91 ' o 7r £ l 5 [-'1* :?! 3 NET BKG AREA AREA -0.200 1.200 0.280 0.720 1.560 1.440 233.320 1.680 1.000 0.000 .,,_ .... "' "'"' .,_ "' .... "'"' f)j 13 """ "'"' ., ! ,,,! 1 1 uM{, ill ' 1 1 1 BKG StDev 1.0954 0.8485 1.2000 1.2961 0.0000 li-r--,..... .,-l .,-, +...,.-...-,-, -,-, -,-, ' ' -. ' ' l ' %ABUN 100.000 99.900 99.900 100.000 99.900 -----! ' ACTIVITY pCi/G -4.04E-03 4.70E-03 2.60E-02 3.89E+OO 1.67E-02 ' l 2378 2779 3184 3592 4004 441 4837 5: 6113 6545 6980 7 418 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B244.CNF;455 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W244.CNF;112 CAL DATE : 19-Sep-2016 -----------------------1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 6.08E*02 1.42E-01 4.06E-02 6.07E-02 4.92E-02 1.03E-01 2.61E-02 4.91E-02 6.87E-02 1.23E-01 3.67E-02 6.86E-02 7.41E-01 1.29E-01 3.95E-02 5.02E-01 4.69E*02 5.00E-02 O.OOE+OO 4.69E-02 0 ......., Vi 00 0 \D BATCH NUMBER : 1596402 SAMPLE ID : R1203621727 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 227 SAMPLE QTY : 0.518 G -+/-0.193 % I DETECTOR SIN : 87915 I AVERAGE %EFFICIENCY : 26.3665 ! AVERAGE %EFF ERROR : 0.5107 SAMPLE DATE : 21-Sep-2016 00:00:00 ANALYST : MXS2 % YIELD : 81.7 +/-6.974 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.5803E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5490.39 PU-239 5155.00 5126.71 PU-242 4890.00 4875.90 PU-244 4589.00 4546.97 fjJ e1)91) I 1P _ PU-244: 4497.,.597 keV 17 L PU-242: 4S5H995 keV I PU-239: 5011-5227 keV I PU-238: 5375-5506 keV 15 f--PU-238: 558:1*5843 keV i 13 f-11 L I 9 i n-l 5r 31 1 [--i i ! PEAK FWHM 0.000 73.837 113.217 57.429 0.000 * *
  • J I LJU_, .. ' ! -r 2375 2771 3171 E;nergy (ke V) 3576 3984 439 I COUNT DATE : 24-Sep-2016 20:54:06 )ELAPSED LIVE TIME(SEC) : 14400.00 I 1,i LCS ID l NUCLIDE I NOMINAL (pCi/G) I % RECOVERY NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 0.000 0.000 0.000 0.0000 100.000 3.000 1.800 1.200 1.0954 99.900 5.000 2.840 2.160 1.4697 99.900 228.000 226.560 1.440 1.2000 100.000 0.000 -0.240 0.240 0.4899 99.900 ! nil 4814 61 6091 6525 6963 :, "-"-ACTIVITY pCi/G Ci.OOE+OO 3.03E-02 4.78E-02 3.81E+OO -4.04E-03 7405 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B227.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W227.CNF;120 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.41E-02 5.06E-02 O.OOE+OO 6.89E-02 1.18E-01 3.38E-02 8.49E-02 1.41 E-01 4.53E-02 7.36E-01 1.24E-01 3.70E-02 3.49E-02 8.07E-02 1.51E-02 1.96-sigma cnt Unc pCi/G 3.40E-02 6.88E-02 8.46E-02 4.99E-01 3.49E-02 Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 30-Sep-2016 Batch# Product:. __ Tu'--"--=-* -'""";)_L_I_.\_ Date: Criteria: Yes No Comments sample Sollds are less than or eaual to 100 ma for GAB. i\ln-Samples have been blank corrected (if required). tJ'd-Blank correction reported Included llf reaulred\. [f activity less than 10x MDA/MDC, error Is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. v [f hnln*** *hn Un A./ Mnr <>rrnr le nk:.v. Instrument source check Is within limits. v"" [ hkn .-h..,.k Is .... 1thln limits. Method RDL/ LLD has been met. ../ [f duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPD Is 0%, ./ Or meets the client's reaulred RER acceotance criteria. Tracer yield ls 15-12S%
  • Carrier yield 25-12S%. (Or meets the client's contract acceptance criteria). ./' Method blank Is less than the RDL/ LLD. v lfTf --*-<!' 0::0/n nf In .. *-** "rtlultv\ Samnle was run within hold time. v \)i.:Q.-\\ Samole was correctlv Preserved If reaulred. t-J?-Smears Taken for Radioactive batches. kb-Method Spike and LC5 are within 7S-125% -r--'or "'"ets the client's contract accentance criteria\. No blank spaces on data forms. All line outs Initiated and dated. /' **-<>rrnrc ---Aux data Is correct. lb--Client Sneclal reoulrements naae has been checked. ../ Raw Data and I or soectrum are Included and nronerlv statuc:ed. / MS, LC5, and Duplicate RPD/RER values uploaded to UMS and .,,,.---**-***n* V""'""" 1 .... -*-(If .. _ ........ ln*n .. --..... /" , St Q.,l, Batch Data Excentlon Renorts lDER\ comnleted If aonlicable. ,,--. lJ "S1o\.l \ Batch Data Exception Reports (DER) second reviewed. v lf2'l 4l Disposition verified to be completed. Alitmnt rnrrection comntnt<*d If renulr*"'* \.b-Review sample historical results If available / Cif REMP, results above MDC have been verified bv hlstorical results recount or re-analvsis. l Primary Review Performed ey: _ ___ /b_f_Lf_,_f_;/._,_<.. __ Secondary Review Performed By:__ 10/04/16 GL-CHL-RAD-013Rev1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DER Report No.: 1564186 Revision No.:
  • DATA EXCEPTION REPORT
  • Mo.Day Yr. Division: Quality Criteria: Type: 04-0CT-16 Radiochemistry Specifications Process Instrument Type: Test I Method: Matrix Type: Client Code: LSC DOE EML HASL-300, Pu-11-RC Solid MJWC Batch ID: Sample Numbers: 1596394 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Other Sample received out of holding . Specification and Requirements .DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, and 1203621704 were received and analyzed out of holding. 2 .. Sample 1203621704 does not meet the resolution requirement of 2. The sample does meet the tracer yield requirement, the detection limits, having a full width half maximum of 100 keV or less for the Pu-242 and its tracer peak is within the Pu-242 region of interest. Reporting tracer. results. Originator's Name: Data Validator/Group Leader: Melanie Aycock 04-0CT-16 Jessica Davis 04-0CT-16 Page 1 Page 5253 of 5809 Pu-241 Queue Sheet 07-SEP-16 Batch#: 1596394 Analyst:JXH2 First Client Due Date: 04-0CT-16 Internal Due Date30-SEP-16 Tracer LCS Spike Isotope: Pu-241 Tracer Code: \ 11 O.-A Expiration Date: 8-3-1/ LCS Code: *1 l.o \c--1:, Expiration Date: ic--2..R-tl.::. Vol: O, \,.... L Solid Sample Dissolution by: Vol: D,\nL Spike Code:______ Expiration Date:_____ Vol: -Cocktail Used: Ultima gold LLT OCOJcint rn§i) Prep Date: '\. *Z.(o -\Co Initials: PipetID:\'31.\.0oti;_ BalanceID: \(o\0/{i,(,'£.. Witness: t=6 "\*-2.-U *lu Sample ID Client Description 405235001-1 4.1.B.R.l.2 405235002-1 4.1.B.R.1.3 405235003-1 4.1.B.R.1.4 405235004-1 4.1.B.R.7.2 405235005-1 4.1.C.R.1.3 405235006-1 4.1.C.R.1.4 405235007-1 4.1.C.R.2.3 405235008-1 4.1.C.R.2.4 405235009-1 4.1.D.R.1.3 405235010-1 4.1.D.R.l.4 405235011-1 4.1.D.R.3.2 405235012-1 4.1.D.R.2.4 405235013-1 4.2A.R.2.3 405235014-1 4.2A.R.1.3 405235015-1 4.2A.R.l.4 405235016-1 4.2A.R.2.4 405235017-1 4.2A.R.3.2 405235018-1 4.2A.R.4.2 405235019-1 4.2B.R.2.4 405235020-1 4.2B.R.1.4 1203621703-1 l\IB for batch 1596394 1203621704-1 4.1.B.R.1.2(405235001DUP) 1203621705-1 J,.CS for batch 1596394 Type SA!\.1PLE SA!\1PLE SA.i'fl'LE SAMPLE SAMPLE SAMPLE SA!\1PLE SA.i'fl'LE SAMPLE SA!\1PLE SAMPLE SA!\1PLE SA!\1PLE SAMPLE SA!\.U'LE SAMPLE SAMPLE SAMPLE SAMPLE SA.i'dPLE J\.IB DUP LCS Hazard Code Min CRDL 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15pCi/g 15pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g _ 15 pCi/g 15 pCi/g 15 pCi/g Matrix SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL Client l\.UWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOI l\.fJWCOOl MJWCOOl MJWCOOl l\.UWCOOl MJWCOOl MJWCOOl l\fJWCOOl MJWCOOl MJWCOOl l\fJWCOOl l'vJJWCOOl MJWCOOl l\fJWCOOl MJWCOOl QC ACCOUNT QC ACCOUNT QC ACCOUNT Instrument Used: LS6000 (Red) 7065155, LS6500 (Blue) 7067083, LS6500 (Green) 7067404, Wallac (Yellow) 4140127, LS6000 (Broll!!J.) 7060655 00 (Gold) 7070506, Purple 7069123, Silver 7060656, Wallac (White) 4140299, allac.(Teal) 4140421 Wallac (Gray) 4150033, 7069693 (Mocha) GEL Laboratories LLC, Radiochemistry Divisio11 Collection Date 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 10-DEC-15 09-DEC-15 10-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 08-DEC-15 02-DEC-15 02-DEC-15 08-DEC-15 08-DEC-15 10-DEC-15 Pos. Label # Wetkfil, Aliquot &J110 LSC Rack# Alpha Spec Det# Data Reviewed By: \ 4 \ \"' Page 1 ofl Filename: PU241.XLS File type : Excel Version # : 1.3.4 Batch : 1596394 Analyst : JXH2 Prep Date : 9/2612016 Method Uncertainty: 0.0839 Geometry: 2mL Dl/1 drop HN03/13mL Ecoscint Ultra Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Sample* Pos. ID G G Datemme 1 405235001. 1 0.5010 3.2713E-03 12110/2015 14:20 2 405235002.1 0.5050 3.2718E-03 12110/2015 14:30 3 405235003.1 0.5010 3.2713E-03 12/101201514:35 4 405235004.1 0.5020 3.2714E-03 1219/2015 14:00 5 405235005.1 0.5030 3.2715E-03 1211012015 13:15 6 405235006.1 0.5010 3.2713E-03. 12/1012015 13:25 7 405235007.1 0.5010 3.2713E-03 12110/2015 13:55 8 405235008.1 0.5030 3.2715E-03 12110/2015 14:05 9 405235009.1 0.5040 3.2717E-03 12/10/2015 10:30 10 405235010. 1 0.5010 3.2713E-03 12/10/2015 10:35 11 40523501 1.1 0.5000 3.2712E-03 1219/2015 10:13 12 405235012.1 0.5060 3.2719E-03 12110/201511:25 13 405235013.1 0.5000 3.2712E-03 1218/2015 11:23 14 405235014.1 0.5020 3.2714E-03 1218/201510:49 15 405235015.1 0.5090 3.2722E-03 1218/2015 10:56 16 405235016. 1 0.5010 3.2713E-03 121812015 1 1 :29 17 405235017.1 0.5010 3.2713E-03 1212/2015 10:02 18 405235018.1 0.5000 3.2712E-03 12121201510:19 19 405235019.1 0.5060 3.2719E-03 12/8/2015 14:30 20 405235020.1 0.5020 3.2714E-03 12/8/201 5 13;50 21 1203621703.1 0.5090 3.2722E-03 9/2612016 0:00 22 1203621704.1 0.5000 3.2712E-03 12/10/201514:20 23 1203621705.1 0.5090 3.2722E-03 9/26/2016 0:00 PU1596394R Plutonium-241 Solid Tracer SIN: Tracer Exp Date : Tracer Volume Added: Tracer Error: Tracer Calculations Tracer Concentration Tracer DPM Counts 4.3831 280 4.3831 262 4.3831 213 4.3831 195 4.3831 302 4.3831 355 4.3831 317 4.3831 308 4.3831 314 4.3831 250 4.3831 187 4.3831 238 4.3831 210 4.3831 228 4.3831 255 4.3831 249 4.3831 204 4.3831 218 4.,3831 246 4.3831 210 4.3831 256 4.3831 154 4.3831 145 1770-A 8/3/2017 0.10 0.44% Tracer Tracer Bkg Net Counts CPM 0.480 1.165 1.680 1.085 2.160 0.879 1.440 0.807 0.960 1.254 1.200 1.474 1.680 1.314 1.200 1.278 2.160 1.299 1.440 1.036 1.200 0.774 0.960 0.988 1.920 0.867 0.720 0.947 1.200 1.058 1.200 1.033 0.480 0.848 0.480 0.906 1.680 1.018 1.200 0.870 1.440 1.061 3.360 0.628 0.240 0.603 Page 1 Procedure Code : LSC41PUS Parmname: Plutonium-241 MDA : 15 pCVG Halfllfe o! Pu-241 : 14.290 years Pu-241 Abundance : 1.00 Tracer Abundance : 1.00 Hal!ll!e of Tracer : 373500.000 years Deteclor Tracer Count .Tracer Detector Efficiency Start Count Tracer Detector Efficiency S!Dev. Datemme Time(sec.) Decay Serial# (cpm/dpm) (cpm/dpm) 9/29/2016 9:18 14400 1.000 79461 0.338848 0.006527 9/2912016 9:18 14400 1.000 80011 0.324069 0.006248 9129/2016 9:18 14400 1.000 78777 0.336886 0.006490 912912016 9:18 14400 1.000 80012 0.326615 0.006296 9/29/2016 9:18 14400 1.000 67578 0.307195 0.005929 912912016 9:18 14400 1.000 10n0 0.345578 0.006655 9129/2016 9:18 14400 1.000 79463 0.361703 0.006959 9/29/2016 9:18 14400 1.000 83292 0.323669 0.006241 9129/2016 9:18 14400 1.000 78261 0.340722 0.006563 9129/2016 9:23 14400 1.000 87898 0.253042 0.004906 9/29/2016 9:23 14400 1.000 87900 0.260378 0.005045 9/2912016 9:23 14400 1.000 87901 0.248786 0.004826 9/29/2016 9:23 14400 1.000 87902 0.262230 0.005080 9/29/2016 9:23 14400 1.000 87906 0.251171 0.004871 9/29/2016 9:44 ' 14400 1.000 87923 0.247991 0.004811 9/29/2016 9:23 14400 1.000 87908 0.240361 0.004668 912912016 9:23 14400 1.000 87909 0.255264 0.004948 9/29/2016 9:23 14400 1.000 87911 0.256333 0.004968 9/29/2016 9:23 14400 1.000 87912 0.257363 0.004987 9/29/2016 9:23 14400 1.000 87914 0.268347 0.005195 9/29/2016 9:24 14400 1.000 87915 0.263665 0.005107 9/29/2016 9:23 14400 1.000 87916 0.255769 0.004958 9/29/2016 9:24 14400 1.000 87922 0.248037 0.004811

"'d cfci CD Vo N Vo 0\ 0 ......., Vo 00 0 \0 Pfpet, 0.1 ml Stdev : +/-0.000200 ml Plpet, 0.5 ml S1dev: +/-0.001000 ml Plpet,.1 ml Stdev : +/-0.002000 ml Analytlcaf SOP: GL-RAD-A-035 Instrument SOP: GL-RAD-1-014 Count raw Data Counting Rack Time Quench# Gross Pos. Position# (min.) cpm 1 91-2 60 694.43 8.28 2 91-3 60 695.27 7.62 3 91-2 120 693.74 7.96 4 91-3 120 692.62 7.34 5 91-6 60 695.01 8.24 6 91-4 120 694.53 7.74 7 91-8 60 694.53 7.6 8 91-9 60 693.21 7.55 9 91-10 60 692.78 7.86 10 91-11 60 693.53 8.57 11 91-5 120 695.96 7.41 12 0-1 60 690.81 8.15 13 0-2 60 691.29 8 14 0-3 60 690.38 7.59 15 0-4 60 692.04 7.53 16 0-5 60 694.16 7.33 17 0-6 60 691.08 7.52 18 91-6 120 591.77 7.88 19 0-8 690.97 7.33 20 0-9 60 694.8 7.9 21 0-10 60 691.n 8.48 22 91*7 120 692.04 7.52 23 0-12 60 691.66 24.03 Bkg Count Corrected Count Bkg Time Bkg Bkg Start cpm (min.) auenchll cpm Datemme 8.99 60 701.52 8.8418 9/30/2016 5:39 8.99 60 701.52 8.8571 9/3012016 6:41 8.08 120 700.9 7.9345 10/1 /2016 17:08 8.08 120 700.9 7.9154 10/1/2016 19:09 8.99 60 701.52 8.8523 9/30/2016 9:44 8.08 120 700.9 7.9485 10/1/2016 21:10 8.99 60 701.52 8.8436 9/30/2016 11 :46 8.99 60 701.52 8.8204 9/30/2016 12:47 8.99 60 701.52 8.8131 9/30/2016 13:49 8.99 60 701.52 8.8260 9/30/2016 14:50 8.08 120 700.9 7.9750 10/3/2016 8:28 8.99 60 701.52 8.7810 9/30/2016 16:52 8.99 60 701.52 8.7886 9/30/201617:53 8.99 60 701.52 8.7742 9/30/2016 18:54 8.99 60 701.52 8.8008 913012016 19:55 8.99 60 701.52 8.8370 9/30/2016 20:57 8.99 60 701.52 8.7853 9/30/2016 21:58 8.08 120 700.9 7.9013 10/3/2015 10:29 8.99 60 701.52 8.7835 10/1/2016 0:00 8.99 60 701.52 8.8485 10/1/2016 1 :01 8.99 60 701.52 8.7964 1011/2016 2:02 8.08 120 700.9 7.9058 10/3/2016 12:30 8.99 60 701.52 8.7946 10/1/2016 4:05 PU1596394R calculated Calfbratfon Data Delector Background Sample Sample Calibration Detector Efficiency Background Count Sample Recovery Recovery Counted Calibration Due Efficiency Error Rack Start Decay % Error% on "Date Date (cpm/dpm) (cpm/dpm) Position# Date/Time 0.962 6.32% LSCTEAL 2/1/2016 1/31/2017 0.1620 0.00792 91-1 9/30/2016 4:38 0.962 76.4% 6.54% LSCTEAL 2/1/2016 1/31/2017 0.1634 0.00792 91-1 9/30/2016 4:38 0.961 59.5% 7.22% LSCTEAL 2/1/2016 1/31/2017 0.1609 0.00792 91-1 10/1/201615:07 0.961 56.3% 7.51% LSCTEAL 211/2016 1/31/2017 0.1590 0.00792 91-1 10/1/2016 15:07 0.962 6.11% LSCTEAL 2/1/2016 1131/2017 0.1629 0.00792 91-1 9/30/2016 4:38 0.961 97.3% 5.69"/o LS CT EAL 211/2016 1/31/2017 0.1622 0.00792 91-1 1011/2016 15:07 0.962 82.9% 5.99% LSCTEAL 2/1/2016 1/31/2017 0.1622 0.00792 91-1 913012016 4:38 0.962 90.1% 6.06% LSCTEAL 21112016 1/31/2017 0.1600 0.00792 91-1 9/3012016 4:38 0.962 87.0% 6.03% LSCTEAL 211/2016 1/3112017 0.1593 0.00792 91-1 9/30/2016 4:38 0.962 93.4% 6.68% LSCTEAL 2/1/2016 1/3112017 0.1605 0.00792 91-1 9/30/2016 4:38 '0.961 67.8% 7.65% LSCTEAL 2/1/2016 1/31/2017 0.1645 0.00792 91-1 10/1/2016 15:07 0.962 90.6% 6.82% LSCTEAL 2/1/2016 1131/2017 0.1561 0.00792 91-1 9/30/2016 4:38 0.961 75.4% 727% LSCTEAL 2/1/2016 1/31/2017 0.1569 0.00792 91-1 9/30/2016 4:38 0.961 86.0% 6.95% LSCTEAL 211/2016 1/31/2017 0.1555 0.00792 91-1 9/30/2016 4:38 0.961 97.3% 6.61'%* LSCTEAL 2/112016 1/3112017 0.1581 0.00792 91-1 9/30/2016 4:38 0.961 98.0% 6.69% LS CT EAL 2/112016 1/31/2017 0.1615 0.00792 91-1 9/30/2016 4:38 0.950 75.8% 7.31% LSCTEAL 2/1/2016 1/3112017 0.1565 0.00792 91-1 9/30/2016 4:38 0.960 80.7% 7.09% LSCTEAL 2/1/2016 1131/2017 0.1577 0.00792 91-1 10/1/2016 15:07 0.961 90.2% 6.74% LSCTEAL 21112016 1/3112017 0.1564 0.00792 91-1 9130/2016 4:38 0.961 74.0% 7.24% LSCTEAL 2/1/2016 1/31/2017 0.1626 0.00792 91*1 9/3012016 4:38 0.999 91.8% 6.61% LSCTEAL 2/1/2016 1/3112017 0.1577 0.00792 91-1 9/30/2016 4:38 0.961 56.0% 8.52% LSCTEAL 2/1/2016 1131/2017 0.1581 0.00792 91-1 10/112016 15:07 0.999 55.5% 8.58% LSCTEAL 2/1/2016 1/3112017 0.1575 0.00792 91-1 9/30/2016 4:38 Page2 Noles: 1

  • Results are decay corrected to Sample Datefrime 2
  • Reference dale for Spike Activity (dpm/ml) is the batch Prep Dale 3 -Spike Nominals are decay corrected lo Sample Date!Time *
  • RPD changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. SampleAcL Level Level MDA MDA Cone. Error Pas. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 9.3106 6.5733 15 13.5147 -4.1351 95.30% 2 9.4134 6.6460 15 13.6637 -9.1983 42.88% 3 8.2796 5.8455 15 11.9353 0.2487 1429.91% 4 8.8167 6.2247 15 12.7098 -5.9945 62.43% 5 7.7654 5.4825 15 11.2717 -3.7567 87.39% 6 5.0256 3.5481 15 7.2444 -1.2358 173.48% 7 8.8025 6.2146 15 12.1n2 -6.6531 42.53% 8 8.1613 5.7619 15 11.8469 -8.2068 41.57% 9 8.4692 5.9793 15 12.2940 -6.3920 55.64% 10 7.8840 5.5662 15 11.4442 -1.5967 210.48% 11 7.1354 5.o3n 15 102854 -4.7458 63.84% 12 8.2520 5.8260 15 11.9793 -4.1304 84.47% 13 9.9856 7.0499 15 14.4958 -6.2444 67.48% 14 8.7955 6.2097 15 12.7685 -6.2657 44.66% 15 7.5530 5.3325 15 10.9642 -7.6058 41.60% 16 7.4709 5.2745 15 10.8445 -6.9030 35.10% 17 9.9458 7.0219 15 14.4381 *9.9804 41.86% 18 6.2372 4.4035 15 8.9915 --0.1574 1699.52% 19 82723 5.8403 15 12.0086 -9.5370 36.30% 20 9.8217 6.9342 15 14.2565 -7.3617 56.18% 21 7.7208 5.4509 15 11.2078 -1.9361 169.73% 22 8.9548 6.3222 15 12.9091 -4.0844 93.34% 23 12.7853 9.0265 15 18.5598 154.4052 9.91% PU1596394R Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA Net Count Net Count Counting Rale Rate Error Uncertainty CPM CPM pCi/G -0.5618 0.5342 7.7066 -1.2371 0.5240 7.6371 0.0255 0.3639 6.9704 -0.5754 0.3566 7.2806 -0.6123 0.5337 6.4183 -0.2085 0.3616 4.1997 -1.2436 0.5235 7.1396 -1.2704 0.5223 6.6135 -0.9531 0.5271 6.9290 -0.2560 0.5385 6.5838 -0.5650 0.3581 5.8951 -0.6310 0.5312 6.8158 -0.7886 0.5290 8.2093 *1.1842 0.5222 7.1448 -1.2708 0.5217 6.1199 -1.5070 0.5191 6.0107 -1.2653 0.5213 "8.0596 *0.0213 0.3626 5.2432 -1.4535 0.5182 6.6645 -0.9485 0.5283 8.0376 -0.3164 0.5366 6.4361 -0.3858 0.3585 7.4404 15.2354 0.7396 14.6922 Page3 NIA NIA NIA NIA 1610-B 10(28/2016 1691.15 0.10 2SIGMA Total Prop. Uncertainty pCi/G 7.7067 7.6371 6.9706 7.2806 6.4184 4.1998 7.1396 6.6135 6.9291 6.5838 5.8951 6.8158 8.2094 7.1449 6.1200 6.0107 8.0597 5.2432 6.6646 8.0376 6.4361 7.4404 39.3053 Sample QC 405235001.1 Sample Nominal Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP
  • 0.0% LCS 149.6621 103.2%

__ SJ r:; _Jr_t_ ___________ _ PROTOCOL DATE TIME ID Pu-241 : 5 Pu-241 60 min : 2016/09/30 : 04:381 -: P05AS29Q Wallac 1414 WinSpectral v3.0 S/N4140421 Counting mode lsotope(s) H3 Protocol name Counting time Repeats Cycles Replicates 2sigma % Minimumcpm Advanced modes Output to Display : CPM : H3 350, 12.43 y * : Pu-241 60 min : 3600 : 1 : 1 : 1 : 2.00 : 0.00 Checking time: 10 : Chemilum POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMwl ,CPM,CPMl ,CTIME Additions to Display : Spectrum,Header,Listing Header : Pu-241 Spectrum : Rnd.Cos,Beta Window 1 25-220 /Beta Window 2 25-220 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024_/Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 289.0 CPM ,. --**-**-----*--*------------*-** .. ****-**---**-********-**------*-----*--**--*-*--***-**-*-*-.. Wallac 1400 DSA; P05AS290.DAT, 10/1/2016, page 1 Page 5258 of 58.09 Pu-241 TEAL Rack_position Count_Time(min) Quench_number 91 " 1 60.00 701.52 I I / CounLs Chem / Counts Bela Rack_position Count_ Ti me( min) Quench_number 91 2 60.00 694.43 l I 8-// Counts Chem 6-/ Counls Dem II 20 40 60 80 . 100 Rack_position Count_Time(min) Quench_number 91 3 60.00 695.27 8-/ Counls l Chem / Counts 2 Bela 40 _;* . Run_Date Pu24l_cpm 8.99 9/30/2016 4:38 AM Gross_B_CPM 9.50 Lumex_CPM 0.50 LUMEX 0.00 DPM 0.00 Pu24l_cpm 8.28 Run_Date 9/30/2016 5:39 AM Gross_B_CPM LUMEX 9.40 0.00 Lumex_CPM DPM 1.10 0.00 Pu24l_cpm 7.62 Run_Date 9/30/2016 6:41 AM Gross_B_CPM LUMEX 8.80 0.00 Lumex_CPM DPM 1.20 0.00 -**--*-*-*----*--*-----.. ---**----Wallac 1400 DSA, P05AS290.DAT, 10/1/2016, page 2 Page 5259 of 5809 Pu-241 TEAL -*-**----------*---*-------***----*----**--------**---***-.............. .,,. _________ , ____ ,, __ ., __ .. _,. __ _,_, ____ .. ___ , ____________ .. ---.--5 Rack_position Cour:t_ Time(min) Quench_number 91 4 &**----*-'* 20 40 Rack_position 91 5 8* -60.00 694.48 60 / Counts Chem / Counls Bela Quench_number 693.79 -1 / Counts Chem / Counls Beta I()()

  • Rack_position Time(min) Quench_number 91 6 *: 60.00 695.01 / Couuts Chem ,/ Counls Bein ... ,,, !-..
  • Pu24l_cpm 7.76 Gross_B_ LUMEX 0.00 DPM 0.00 Pu24l_cpm 7.57 Run_Date 9/30/2016 8:43 AM Gross_B_CPM LUMEX 8.70 0.00 Lumex_CPM DPM 1.10 0.00 Pu24l_cpm 8.24 Run_Date 9/30/2016 9:44 AM Gross_B_CPM LUMEX 9.20 0.00 Lumex_CPM DPM 1.00 0.00 *-**-**-----*--*---------*---**---* .. Wallac 1400 DSA, P05AS290.DAT, 10/1/2016, page 3 Page 5260 of 5809 Pu-241 TEAL -***-*-*-***-----*-***---**-*-**-***-----*-----....... **----*--*----*****-***-*-** ...... ****-*-. --------**--*--*-*--*****-*-*----*-----*-**** --.. ---*--.. *--*--* Rack_position Count_Time(min) Quench_number Pu24l_c / Run_Date 1 91 7 60.00 694.32 .08 9/30/2016 10:45 AM / Counts / Cou111s Bela Rack_position
  • Count_Time(min) Quench_number 91 8 60.00 694.53 / Counts Chem / Counts Beta Rack_position Count_Time(min) Quench_number 91 9 :'.. 60.00 693.21 ,, '1' IO-.--*-.--'--r---r.--.------.-------, 8 *--20 40 I --------j i uui 80 HIO / Counts Chem / Counts Beta Gross_B_CPM LUMEX 8.40 0.00 Lumex_CPM DPM 1.30 0.00 Pu24l_cpm 7.60 Run_Date 9/30/2016 11:46 AM Gross_B_CPM LUMEX 8.50 0.00 Lumex_CPM DPM 0.90 0.00 Pu24l_cpm 7.55 Run_Date 9/30/2016 12:47 PM Gross_B_CPM 8.50 Lumex_CPM 0.90 LUMEX 0.00 DPM 0.00 -** .. Wallac 1400 DSA, P05AS290.DAT, 10/1/2016, page 4 Page 5261of5809 Pu-241 TEAL .. Rack_position Count_ Time(min) Quench_number 91 10 : 60.00 692.78
  • 15 l ., '! I 10+-+--*-I-----_1 / Counls Chem I I I I I iwlJ / Counts Bela 80 100 Rack_position Count_Time(min) Quench_number 91 11 60.00 693.53 J i / Counts Chem --1. / Counts Bela 100 Rack_position 91 12 Count_Time(min) Quench_number :-:. 60.00 ' 694.43 :.:*. 15*---*,. 10* / Counts Beta 80 100 Pu24l_cpm 7.86 Run_Date 9/30/2016 1:49 PM Gross_B_CPM LUMEX 9.00 0.00 Lumex_CPM DPM 1.20 0.00 Pu24l_cpm 8.57
  • Run_Date 9/30/2016 2:50 PM Gross_B _CPM 9.70 Lumex_CPM 1.10 8.90 Lumex_CPM 0.90 LUMEX 0.00 DPM LUMEX 0.00 DPM 0.00 0.00 ------------------*----*----*---* .. *------*--*---*-*-**-***-*---*--*--*-.. -**--**"'" Wallac 1400 DSA, P05AS290.DAT, 10/1/2016, page 5 Page 5262 of 5809 Pu-241 TEAL **---*-*---.. ------------**--------*-*****-----*-***-*----------------***---------*--*------------*-----------------------------*--*----*-*-*---*-*-------*--***------.. --.--.. .. --**-Rack_position Count_Time(min) Quench_number 0 l *60.00 690.81 8 / Counls 01cm / Counts Belli Rack_position Count_Time(min) Quench_number 0 2 60.00 691.29 )) / Counls Chem 8**!--jh---1----t--nrrr / Counls Beta 40 ' Rack_position Quench_number 0 3 ;;, 60.00 690.38 ... ;: 10,-r---r--r-*--.---8H---,fl---l / Counls Chem 4 / Counls Bela 40 ;" Pu24l_cpm 8.15 Run_Date 9/30/2016 PM Gross_B_CPM 9.10 Lumex_CPM 1.00 LUMEX 0.00 DPM 0.00 Pu24l_cpm 8.00 Run_Date 9/30/2016 5:53 PM Gross_B_CPM LUMEX 9.30 0.00 Lumex_CPM DPM 1.30 0.00 Pu24l_cpm 7.59 Run_Date 9/30/2016 6:54 PM Gross_B_CPM LUMEX 8.80 0.00 Lumex_CPM DPM 1.20 0.00 .. *---------*-Wallac 1400 DSA. P05AS290.DAT, 10/1/2016, page 6 Page 5263 of 5809 Pu-241 TEAL Rack_position Count_Time(min) Quench_number 0 4 60.00 '692.04 / Coums Chem / Counts lie ta Rack_position Count_Time(min) Quench_number
  • 0 5 60.00 694.16 IO --*----/ \l Counts Chem 4 / Coullls lie ta 00 20 40 '60 80 100 Rack_position Count_Time(min) Quench_number 0 6 f 60.00 691.08 **:*; / Counts Chem (\ / Counts Beta Pu24l_cpm 7.53 Run_Date 9/30/2016 7:S5 PM Gross_B_CPM LUMEX 8.40 0.00 Lumex_CPM DPM 0.90 0.00 Pu24l_cpm 7.33 Run_Date 9/30/2016 8:57 PM Gross_B_CPM 8.30 Lumex_CPM 1.00 LUMEX 0.00 DPM 0.00 Pu24l_cpm 7.52 Run_Date 9/30/2016 9:58 PM Gross_B_CPM LUMEX 8.40 0.00 Lumex_CPM DPM 0.90 0.00 W:illac 1400 DSA, P05AS290.DAT, 10/1/2016, page 7 Page 5264 of 5809

***----------*--------------------*---------------*---** -*-*--Rack_position *O 7 Rack_position 0 8 Count_Time(min) Quench_number . . 60.00 692.46 Counts Chem / Counts Beta Count_ Tiine(min) Quench_number 60.00 690.97 15.--------.---,----,----,---/ Counts 10-Chem / Counts Beta Ll.D..!Wblll 20 40 60 80 100 Rack_position Quench_number 0 9 . 60.00 694.80 / Counts Chem / Counts Bch1 .. Run_Date 9/30/2016 10:59 PM Gross_B_CPM 7.90 Lumex_CPM 1.00 LUMEX 0.00 DPM 0.00 Pu24l_cpm 7.33 Run_Date 10/1/2016 0:00 AM Gross_B_CPM LUMEX 8.20 0.00 Lumex_CPM DPM 0.90 0.00 Pu24l_cpm 7.90 Run_Date 10/1/2016 1:01 AM Gross_B_CPM 8.90 Lumex_CPM 1.00 LUMEX 0.00 DPM 0.00 Willac 1400 DSA, P05AS290.DAT, 10/1/2016, page 8 Page 5265 of 5809 Pu-241 TEAL Rack_position Count_ Time(min) Quench_number O* 10 60.00 691.77 15 .. *;:** _-, / Counls 10----Chem I I 5 / Counls Bela 100 Rack_position Count_Time'(min) Quench_number 0 11 60.00 691.08 Counls Chem / Counts Beta Rack_position Count_ Time(min) Quench_number 0 12 60.00 691.66 20----------/ Counts Chem 15 --/ Counts Bela ... *;r .... ,, Pu241_cpm Run_Date 8.48 10/1/2016 2:02AM Gross_B _CPM LUMEX 9.20 0.00 Lumex_CPM DPM 0.70 0.00 i<J."' Gross_B -CPM LUMEX 9.20 0.00 Lumex_CPM DPM 0.80 0.00 Pu24l_cpm 24.03 Run_Date 101112016 4:05 AM Gross_B_CPM LUM EX 24.70 0.00 Lumex_CPM DPM 0.70 0.00 Wallac 1400 DSA, P05AS290.DAT, 1011/2016, page 9 Page 5266 of 5809

_______________________________ /2]_££ 3 L:-1 PROTOCOL : 5 Pu-241 120 min DATE : 2016110/01 TIME : 15:06

  • ID : P05AS291 Pu-241 Wallac 1414 WinSpectral v3.0 S/N4140421 . Counting mode : CPM lsotope(s) : H3 H3 = 5-350,12.43 y
  • Protocol name : Pu-241120 min Counting time : 7200 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 10 Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ;SOPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display * : Spectrum,Header,Listing Header : Pu-241 Spectrum : Rnd.Cos,Beta Window 1 25-220 /Beta Window 2 25-220 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 78.3 CPM Wullac 1400 DSA, P05AS291.DAT, 10/2/2016, page I Page 5267 of 5809 Pu-241 TEAL Rack_position Count_Time(min) Quench_number 91 1 120.00 700.90 15------/ Coullls Chem / Counts Bela 20 40 60 80 l'.)Q Rack_position Count_Time(min) Quench_number 91 2 120.00 693.74 '3 15--I _J / Counts 01em I I / Counts 1JiJlt1 Ilt!ta 40 60 BO 100 Rack_position Count_ Time(min) Qucnch_number t.-\ 91 3 : 120.00 692.62 * .. / Counts Chem / Counts Beta Run_Datc Pu241_cpm 8.08 10/ 1/2016 3:07 PM Gross_B_CPM LUMEX 8.70 0.00 Lumex_CPM DPM 0.60 0.00 Pu24l_cprri 7.96 Run_Date 10/1/2016 5:08 PM Gross_B_CPM LUMEX 8.50 0.00 Lumex_CPM DPM 0.60 0.00 Pu24l_cpm 7.34 Run_Date 10/1/2016 7:09 PM Gross_B_CPM LUMEX 7.80 0.00 Lumex_CPM DPM 0.50 0.00 ... ***-------*-*-**------**-... --*-*-*-**--*--**-------*-**-Wallac 1400 DSA, P05AS291.DAT, 10/2/2016, page 2 Page 5268 of 5809 Pu-241 TEAL -----*-----*-----*---*---*-**-------*---------**-----**-**-*-------*------------*--*-*----------*-** \\ Rack_position Count_Time(min) Quench_number 91 4
  • 120.00 694.53 / Counls Chem ]( / Connls Dela 20 40 60 Rack_position Count_Time(min) Quench_number 91 5 120.00 693.84 -*-----1 I I / Conn ts Chem I .r I I / 60 80 ICO Rack_position Courit_Time(min) Q 91 6 '.120.00 / Counts *" .. * ...... I -i 80 11)1) Chem / Counls Dcta Pu24l_cpm 7.74 Run_Date 10/112016 9: 10 PM Gross_B_CPM 8.20 Lumex_CPM 0.50 Pu24l_cpm 7.60 LUMEX 0.00 DPM LUMEX 0.00 DPM 0.00 0.00 Pu241_cpm 7.85 Run_Date 10/2/2016 1:13 AM Gross_B_CPM 8.20 Lumex_CPM 0.30 LUMEX 0.00 DPM 0.00 ---. -------*--------------*--------* --------------. -*----__ .., __________ .. ___ --------. -----------Wa'llac 1400 DSA, P05AS291.DAT, 10/2/2016, page 3 Page 5269 of 5809

.... t J)1$_ ________ _ PROTOCOL : 5 Pu-241120 min DATE : 2016/10/03 TIME : 08:27 ID* : POSAS294 Pu-241 Wallac 1414 WinSpectral v3.0 S/N4140421 Counting mode lsotope(s) H3 Protocol name Counting time Repeats Cycles Replicates 2sigma% Minimumcpm Advanced modes Output to Display :CPM : H3 = 5-350,12.43 y : Pu-241120 min : 7200 : 1 : 1 : 1 : 2.00 : 0.00 Checking time: 1 O : Chemil.um POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Spectrum,Header,Listing Header * : Pu-241 Spectrum : Rnd.Cos,Beta Window 1 25-220 /Beta Window 2 25-220 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 33.6CPM Wallac 1400 DSA, P05AS294.DAT, 10/3/2016, page 1 Page 5270 of 5809 Pu-241 TEAL *--*--*----------*-*---*-*-*----*---**--*-**----*--------------**---*----------Rack_position Count_ Time(min) Quench_number 91 5 120.00 695.96 / Counls Chem / Counls Beta Rack_position Count_ Time(min) Quench_number 91 6 120.00 691.77 15 / CounL* \6 Chem / Counis 5 Bela 0 .. I UJJl1 0 20 40 80 100 Rack_position Count_Time(min) Quench_number 91 7 120.00 692.04 15-,_,----.-----.-*--.-----.-----1 / Counts .. --Chem , !I I 11 t 11 ---/ Coums lleia Ju Mu ' 1Y 10--20 40 60 80 100 Pu241_cpm 7.41 Run_Date 10/312016 8:28 AM Gross_B_CPM LUMEX 7.80 0.00 Lumex_CPM DPM 0.40 0.00 Pu24l_cpm 7.88 Run_Date 10/3/2016 10:29 AM Gross_B_CPM LUMEX 8.30 0.00 Lumex_CPM DPM 0.40 0.00 Pu24l_cpm 7.52 Run_Date 10/3/2016 12:30 PM Gross_B_CPM LUMEX 8.00 0.00 Lumex_CPM DPM 0.40 0.00 *--------*-------------------------**---*-***----*-*---**----*-----.Wallac 1400 DSA, P05AS294.DAT, 10/312016, page 2 Page 5271of5809 BATCH NUMBER : 1596394 SAMPLE ID : R0405235001_PU . GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.501 G +/-0.200 % CHAMBER : 103 DETECTOR SIN : 79461 AVERAGE %EFFICIENCY : 33.8848 AVERAGE %EFF ERROR : 0.6527 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 78.4 +/-6.316 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.4371 E+OO dpm NUCLIDE PU-236 PU-238 PU-239 PU-242 PU-244 15 13 i 11 r z 9 t*-5 8 i 5 i-* i 1 i l LIBRARY ENERGY 5749.00 5486.00 5155.00 4890.00 4589.00 I! PEAK ENERGY 5712.26 5450.04 5033.19 4865.40 4590.17 . I . PEAK FWHM 0.000 64.506 4.962 77.502 4.962 2380 2779 3182 3590 4002 441 Energy (keV) COUNT DATE : 29-Sep-2016 09:18:29 ELAPSED LIVE TIME(SEC) : 14399.99 GROSS AREA 0.000 4.000 1.000 280.000 1.000 ! . .I' 'I 4837 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABLIN ACTIVITY AREA AREA StDev pCi/G -0.960 0.960 0.9798 100.000 -1.65E-02 2.560 1.440 1.2000 99.900 3.64E-02 -0.440 . 1.440 1.2000 99.900 -6.21E-03 279.520 0.480 0.6928 100.000 3.94E+OO 1.000 0.000 0.0000 99.900 1.41E-02 I -.-.-,-.*-i --r--1: I 5 6 690 6123 6560 7001 7446 .. g 'l' ir ::> !l. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU

  • BKG FILE : B103.CNF;1414 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W103.CNF;395 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.82E-02 1.13E-01 3.08E-02 6.49E-02 1.05E-01 3.12E-02 4.29E-02 1.04E-01 3.10E-02 6.89E-01 7.81 E-02 1.79E-02 3.97E-02 4.23E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.81 E-02 6.47E-02 4.29E-02 4.63E-01 3.97E-02 BATCH NUMBER : 1596394 SAMPLE ID : R0405235002 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 104 DETECTOR SIN : 80011 AVERAGE %EFFICIENCY : 32.4069 AVERAGE %EFF ERROR : 0.6248 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 76.4 +/-6.541 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.3470E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 5763.53 4.919 PU-238 5486.00 5430.31 14.757 PU-239 5155.00 5158.31 4.919 PU-242 4890.00 4865.77 43.943 PU-244 4589.00 4546.97 0.000 21 !-PU*239:5011-5227keV ! PU*238: 5375-5566 keV 19 P!J.235: 5582-5S43 keV 17 i 15 r-w 13 I-11 [-z J :::> 0 j 2. 7 i-I 5 f-t5 3 <( i 1 r i ! ! ! 2380 2776 3176 3581 3991 Energy (keV) COUNT DATE : 29-Sep-2016 09:18:29 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.280 0.720 0.8485 100.000 5.11E-03 2.000 1.280 0.720 0.8485 99.900 1.94E-02 1.000 -0.440 1.440 1.2000 99.900 -6.61E-03 262.000 260.320 1.680 1.2961 100.000 3.91E+OO 0.000 -0.720 0.720 0.8485 99.900 -1.08E-02 >> > } } } ..e ...... :I g:: ... "'., """ &l "'" .. Sl ..... 1 I !j li Ji " Iii Ill !jl H ! ' ' I ' 5 49 677 6110 6548 6991 7438 :i "' "' ., "' ; lil ::) :0 Cl. C1. Cl. Cl. ... Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU I BKG FILE : B104.CNF;1399 I BKG DATE : 23-Sep-2016 I BKG LIVE TIME(SEC) : 60000.00 I EFF FILE : W104.CNF;386 CAL DATE : 06-Sep-2016 I 1.96-sigma 1.96-sigma TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G 5.35E-02 1.12E-01 2.ME-02 5.35E-02 5.34E-02 9.24E-02 2.35E-02 5.33E-02 4.57E-02 1.11 E-01 3.30E-02 4.57E-02 7.08E-01 1.16E-01 3.57E-02 4.78E-01 3.27E-02 9.18E-02 2.34E-02 3.27E-02 . (0C\ {0 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596394 SAMPLE ID : R0405235003_PU SAMPLE QTY : 0.501 G +/-0.200 % CHAMBER : 105 DETECTOR SIN : 78777 AVERAGE %EFFICIENCY : 33.6886 AVERAGE %EFF ERROR : 0.6490 SAMPLE DATE : 1 O-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 59.5 +/-7.223 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.6077E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 _ PU*244: 4497.4597 keV L PU*242: 4654-4995 keV 251 PlJ.239: 5011-5227 keV PU-238: 5375-5566 keV 22 l PU*236: 5582*5843 keV 19 L I 161 <n r 13 => i 0 10 [-; l' PEAK ENERGY 5767.11 5417.13 5213.95 4861.02 4568.67 ! ,,.-,--\ PEAK FWHM 4.933 4.933 4.933 18.714 4.933 2375 2772 3174 3580 3991 Energy (keV) ... ; ll. COUNT DATE : 29-Sep-2016 09:18:29 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.680 1.680 1.2961 100.000 -1.55E-02 1.000 0.040 0.960 0.9798 99.900 7.53E-04 1.000 0.040 0.960 0.9798 99.900 7.48E-04 213.000 210.840 2.160 1.4697 100.000 3.94E+OO 1.000 0.040 0.960 0.9798 99.900 7.48E-04 +..,... I r I . I ! : -r-;--;--:: 4827 5 51 681 6115 6553 6997 7444 ':j it 0.. ll. ll. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B105.CNF;1398 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W105.CNF;364 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.00E-02 1.76E-01 5.40E-02 5.59E-02 1.24E-01 3.3BE-02 5.55E-02 1.23E-01 3.36E-02 7.88E-01 1.57E-01 5.03E-02 5.55E-02 1.23E-01 3.36E-02 1.96-sigma cnt Uno pCi/G 6.99E-02 5.58E-02 5.55E-02 5.37E-01 5.SSE-02 BATCH NUMBER : 1596394 SAMPLE ID : R0405235004_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G +/-0.199 % CHAMBER : 106 DETECTOR SIN : 80012 AVERAGE %EFFICIENCY : 32.6615 AVERAGE %EFF ERROR : 0.6296 SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 56.3 +/-7.505 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831E+OO dpm RESULTS : 2.4693E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5705.53 PU-238 5486.00 5459.31 PU-239 5155.00 5140.44 PU-242 4890.00 4854.84 PU-244 4589.00 4570.39 PU-244: 44S7-4597 keV i f'U.242* 4654-499S keV 17 f-PU-239; 5011-5227 keV i PU*238: 5375-5566 keV 1 5 r PU-236: 5582-5843 keV ! 13 f-11 <ii I 9 1-I-z I :::> 7! 0 8 5r *s; 3 f-u I <( 1 1! ! l I I 2387 2782 3181 3585 Energy (keV) PEAK FWHM 4.904 24.521 4.904 23.663 29.425 11 I ' ' ' I 3993 440 COUNT DATE : 29-Sep-2016 09:18:29 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.760 0.240 0.4899 100.000 1.88E-02 2.000 -1.120 3.120 1.7664 99.900 -2.29E-02 1.000 0.520 0.480 0.6928 99.900 1.06E-02 195.000 193.560 1.440 1.2000 100.000 3.93E+OO 2.000 1.760 0.240 0.4899 99.900 3.58E-02 ......... .,._ "' "'"' .,., "' .,_ C>O ""' I \ \ 6105 6541 6982 7427 " ::J ::J "-"-0. "-0. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B106.CNF;1398 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W106.CNF;363 CAL DATE : 06-Sep:2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.06E-02 1.19E-01 2.22E-02 7.83E-02 1.94E-01 6.62E-02 5.88E-02 1.13E-01 2.58E-02 8.18E-01 1.50E-01 4.47E-02 7.06E-02 9.75E-02 1.83E-02 ,1v.f\ :y 1.96-sigma cnt Uno pCi/G 7.05E-02 7.83E-02 5.88E-02 5.58E-01 7.04E-02 Atlha SpectrDSc:Opy Software Version 3:5.s* effective date: 02-N.ar-2015
  • GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596394 SAMPLE ID : R0405235005 PU SAMPLE QTY : 0.503 G -+/-0.199 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 93.2 +/-6.114 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.0832E+OO dpm I CHAMBER : 107 i DETECTOR SIN : 67578 I AVERAGE %EFFICIENCY : 30.7195 I AVERAGE %EFF ERROR : 0.5929 I COUNT DATE : 29-Sep-2016 09:18:30 I ELAPSED LIVE TIME(SEC) : 14399.99 i NUCLIDE ACTIVITY SUMMARY Instrument SOP: GL-RAD-1-009 -Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B107.CNF;1439 I BKG DATE : 23-Sep-2016 II BKG LIVE TIME(SEC) : 60000.00 I EFF FILE : W107.CNF;426 , CAL DATE : 06-Sep-2016 I 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 _ PU-2.U; 4497-4S97 keV 19 (_ PU*242: 4654-4995 keV ! PU-239: 5011*5227 keV 17 j PIJ.238: 5375-5566 keV f""' PIJ.236: 5502*5843 keV 15 13 l Cii 11 5 8 51 I ENERGY 5767.98 5439.25 5116.13 4868.26 4515.46 FWHM AREA 4.917 1.000 157.348 5.000 4.917 1.000 64.578 302.000 0.000 3.000 <( 1 1r--. 2399 2794 3194 3597 4005 441 Energy (keV) AREA -0.200 3.560 0.520 301.040 2.760 AREA StDev pCi/G pCVG pCi/G pCVG pCi/G 1.200 1.0954 100.000 -3.17E-03 4.76E-02 1.11E-01 3.18E-02 4.76E-02 1.440 1.2000 99.900 4.68E-02 6.54E-02 9.72E-02 2.89E-02 6.51E-02 0.480 0.6928 99.900 6.79E-03 3.77E-02 7.23E-02 1.66E-02 3.77E-02 0.960 0.9798 100.000 3.93E+OO 6.65E-01 8.59E-02 2.34E-02 4.45E-01 0.240 0.4899 99.900 3.SOE-02 5.21 E-02 6.26E-02 1.17E-02 5.19E-02 j! 'J >677 6106 6538 6975 7415

-. * *-GEL Laboratories LLC .,, .. *-Instrument SOP: ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-035 ! CHAMBER : 108 LIB FILE : PU BATCH NUMBER : 1596394 SAMPLE ID : R0405235006_PU SAMPLE QTY : 0.501 G +/-0.200 % i DETECTOR SIN : 78778 I BKG FILE : B108.CNF;1433 ! AVERAGE %EFFICIENCY : 34.5578 _ BKG DATE : 23-Sep-2016 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2_ % YIELD : 97.3 +/-5.689 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.2658E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 5712.26 0.000 PU-238 5486.00 5432.77 63.844 PU-239 5155.00 5049.43 4.911 PU-242 4890.00 4860.01 70.528 PU-244 4589.00 4571.63 9.822 23 r 21 L PU-239: 5011-5227 keV I PU-238: 5375-SSEa keV 19 f-PU*236: 55a2*5843 keV 17 r 15 r -13 en 11 I-z :::> 91 0 7[ .?:-I :2: t5 3 !-<( 1 i I . I . .. ! \ -. 2397 2792 3191 3594 4002 441 Energy (keV) i AVERAGE %EFF ERROR : 0.6655 1 BKG LIVE TIME(SEC)

  • 60000 00 I COUNT DATE : 29-Sep-2016 09:18:30 ! EFF FILE : W108.CNF;430 I ELAPSED LIVE TIME(SEC) : 14399.99 I CAL DATE : 06-Sep-2016 i I I I I NUCLIDE ACTIVITY SUMMARY 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G 0.000 -0.480 0.480 0.6928 100.000 -6.50E-03 2.88E-02 7.50E-02 1.72E-02 3.000 2.520 0.480 0.6928 99.900 2.83E-02 4.51E-02 6.21E-02 1.42E-02 1.000 0.760 0.240 0.4899 99.900 8.47E-03 3.18E-02 5.35E-02 1.00E-02 355.000 353.800 1.200 1.0954 100.000 3.94E+OO 6.21E-01 7.81E-02 2.24E-02 2.000 2.000 0.000 0.0000 99.900 2.23E-02 3.83E-02 3.34E-02 0.00E+OO §§ t;; le &j Ill \,-J.. ()(Ct.. t.fl I .. I i . I 674 6102 6535 6971 7412 "' l!l ;:; 'l' 2 ::, a: ir Q_ 1.96-sigma cnt Unc pCi/G 2.87E-02 4.49E-02 3.18E-02 4.12E-01 3.82E-02 Alpha Specirosc:opy SoCiware Version 3.5.3 effective dale: 02-Mar-2015 BATCH NUMBER : 1596394 SAMPLE ID : R0405235007 _PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 109 ! DETECTOR S/N : 79463 SAMPLE QTY : 0.501 G +/-0.200 % 11 AVERAGE %EFFICIENCY : 36.1703 i AVERAGE %EFF ERROR : 0.6959 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 82.9 +/-5.993 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.6324E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 _ PU-244: 4497-4597 l<eV 21 f-P\J-242: 4654-4995 keV I P\J.239: 5011-5227 keV 19 L PU-238: 537&-5566 keV I P\J.236: 5582-58-13 keV 17 L I 15 r 13 11 L z I :J 9 f-8 ; I 3 LI 1 PEAK ENERGY 5690.95 5492.60 5204.92 4857.44 4552.40 PEAK FWHM 4.905 4.905 4.905 80.162 4.905 ! ! j___J_ ' ' I 2401 2796 3196 3600 4009 Energy (keV) 1 COUNT DATE : 29-Sep-2016 09:18:30 !ELAPSED LIVE TIME(SEC) : 14399.99 ! NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA Stoev pCi/G 1.000 0.520 0.480 0.6928 100.000 7.90E-03 1.000 0.040 0.960 0.9798 99.900 5.04E-04 1.000 0.040 0.960 0.9798 99.900 5.00E-04 317.000 315.320 1.680 1.2961 100.000 3.94E+OO 1.000 0.520 0.480 0.6928 99.900 6.51E-03 5 6 691 6123 6560 7002 7448 Instrument SOP: GL-Rfi.0:.1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B109.CNF;1431 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W109.CNF;420 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G Ci/G 4.39E-02 8.42E-02 1.93E-02 3.74E-02 8.30E-02 2.26E-02 3.71E-02 8.24E-02 2.25E-02 6.54E-01 9.68E-02 2.97E-02 3.62E-02 6.93E-02 1.59E-02 1.96-sigma cnt Unc pCi/G 4.39E-02 3.73E-02 3.71E-02 4.37E-01 3.61 E-02 BATCH NUMBER : 1596394 SAMPLE ID : R0405235008_PU SAMPLE QTY : 0.503 G +/-0.199 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 110 DETECTOR SIN : 83292 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 i AVERAGE %EFFICIENCY : 32.3669 ; AVERAGE %EFF ERROR : 0.6241 J COUNT DATE : 29-Sep-2016 09:18:30 % YIELD : 90.1 +/-6.064 % i ELAPSED LIVE TIME(SEC) : 14399.99 ! TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.9495E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 21 _ FlJ.244: 4497-1597 keV I PU-242: 4654-4"95 keV 19 ' FlJ.239: 5011*5227 keV [ PIJ-238: 5375-5568 keV 17 1 FlJ.236: 5SllZ*5843 keV i 15 i 13 [ 3: f t5 3 /--PEAK ENERGY 5712.24 5461.18 5218.37 4858.84 4546.97 PEAK GROSS FWHM AREA 0.000 0.000 113.212 4.000 4.922 1.000 71.373 308.000 0.000 0.000 <C 11-*' I' I ! 2376 2772 3173 3578 3988 Energy (keV) 440 ::> 0. 4821 NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN AREA AREA St Dev 0.000 0.000 0.0000 100.000 3.520 0.480 0.6928 99.900 0.520 0.480 0.6928 99.900 306.800 1.200 1.0954 100.000 0.000 0.000 0.0000 99.900 .ill I . I . 5 45 673 6106 6543 6985 ii'. ::> ::> c. 0.. ACTIVITY pCi/G O.OOE+OO 4.54E-02 6.66E-03 3.93E+OO O.OOE+OO I . 7432 Instrument SOP: Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B11 O.CNF;1440 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W11 O.GNF;441 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.14E-02 4.67E-02 O.OOE+OO 5.77E-02 7.14E-02 1.64E-02 3.?0E-02 7.09E-02 1.63E-02 6.59E-01 8.97E-02 2.57E-02 2.59E-02 3.84E-02 O.OOE+OO 1.96-sigma cnt Unc pOi/G 3.14E-02 5.75E-02 3.?0E-02 4.41E-01 2.58E-02

>--c ('!) Vo N 00 0 0 ......., Vo 00 0 \0 BATCH NUMBER : 1596394 SAMPLE ID : R0405235009 PU SAMPLE QTY : 0.504 G -+/-0.198 % SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 87.0 +/-6.029 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 3.8135E+OO dpm GEL Laboratories LLC _, "' -ALPHA SPECTROSCOPY REPORT CHAMBER : 112 DETECTOR SIN : 78261 AVERAGE %EFFICIENCY : 34.0722 AVERAGE %EFF ERROR : 0.6563 COUNT DATE : 29-Sep-2016 09:18:30 ELAPSED LIVE TIME(SEC) : 14399.99 NUCLIDE ACTIVITY SUMMARY Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU / BKG FILE : B112.CNF;1443 I BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 ! EFF FILE : W112.CNF;451 I CAL DATE : 06-Sep:2016 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc ENERGY ENERGY FWHM AREA AREA AREA St Dev pCi/G pCi/G pCi/G pCi/G pCi/G PU-236 5749.00 5712.24 0.000 0.000 -0.480 0.480 0.6928 100.000 -7.33E-03 3.25E-02 8.46E-02 1.94E-02 3.24E-02 PU-238 5486.00 5429.74 83.327 2.000 0.560 1.440 1.2000 99.900 7.09E-03 4.58E-02 9.36E-02 2.78E-02 4.58E-02 PU-239 5155.00 5119.56 117.638 2.000 1.520 0.480 0.6928 99.900 1.91E-02 4.40E-02 6.96E-02 1.60E-02 4.39E-02 PU-242 4890.00 4857.86 94.356 314.000 311.840 2.160 1.4697 100.000 3.92E+OO 6.54E-01 1.05E-01 3.38E-02 4.37E-01 PU-244 4589.00 4524.68 4.902 1.000 0.760 0.240 0.4899 99.900 9.56E-03 3.59E-02 6.03E-02 1.13E-02 3.58E-02 SS ;x g: "'"'"' """., ., . lj 17 I PU-238: 5375-556!1 koV I 15 f'U-230: 5582-5843 koV I I -I 131 Ui 11 r I-9L z :::> 0 s 5i t5 11ul1 <C 1 f-I I' .I . . ! *

  • I I I I I r* I , I , i .--,-. ' 2398 2792 3191 3595 4003 441 5 5,: 681 6111 6547 6987 7431 Energy (keV) ; "' o; ::i gj "' "' ::i :::. a. a. c.. a. c..

0 ....., VI 00 0 \0 BATCH NUMBER : 1596394 SAMPLE ID : R0405235010_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT i CHAMBER : 210 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 821 O.CNF;455 SAMPLE QTY : 0.501 G +/-0.200 % I DETECTOR SIN : 87898 I AVERAGE %EFFICIENCY : 25.3042 l AVERAGE %EFF ERROR : 0.4906 1 BKG DATE : 23-Sep-2016 I BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE :* 1 O-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 93.4 +/-6.681 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.0929E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5728.05 PU-238 5486.00 5530.79 PU-239 5155.00 5117.29 PU-242 4890.00 4874.31 PU-244 4589.00 4518.61 17 : I PIJ.239:5011*5227kBV 15 r PIJ.238: 5375-5566 keV I f'U.238: 5582*5843 keV 13 L 11 I (j) 9 l-I-I z 7! :::> 0 2. .2:-3L t5 1 I <t ; . , , 1 i ! 2381 2783 3189 3597 Energy (keV) PEAK FWHM 65.062 15.014 5.005 85.080 0.000 1 4009 I COUNT DATE : 29-Sep-2016 09:23:32 ELAPSED LIVE TIME(SEC) : 14400.00 _ ! NUCLIDE ACTIVITY SUMMARY I EFF FILE : W210.CNF;126 I CAL DATE : 16-Sep-2016 ! 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G 2.000 1.760 0.240 0.4899 100.000 3.39E-02 6.69E-02 9.24E-02 1.73E-02 3.000 -1.320 4.320 2.0785 99.900 -2.11E-02 7.07E-02 1.70E-01 6.08E-02 1.000 0.280 0.720 0.8485 99.900 4.44E-03 4.65E-02 9.70E-02 2.47E-02 250.000 248.560 1.440 1.2000 100.000 3.94E+OO 7.29E-01 1.17E-01 3.49E-02 2.000 2.000 0.000 0.0000 99.900 3.17E-02 5.46E-02 4.76E-02 O.OQE+OO > > !! ......... ,j . Ji *ill h r-0 ii. r f\ I i ' 5 6 691 6119 6551 6987 7425 [!l a. a. a. 1.96-sigma cnt Unc pCi/G 6.67E-02 7.07E-02 4.65E-02 4.93E-01 5.44E-02 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596394 SAMPLE ID : R0405235011_PU SAMPLE QTY : 0.500 G +/-0.200 % SAMPLE DATE : 09-Dec-2015 00:00:00 ANALYST :* JXH2* % YIELD : 67.8 +/-7.649 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.9732E+OO dpm CHAMBER : 212 DETECTOR S/N : 87900 AVERAGE %EFFICIENCY : 26.0378 AVERAGE %EFF ERROR : 0.5045 COUNT DATE : 29-Sep-2016 09:23:34 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B212.CNF;455 , BKG DATE : 23-Sep-2016 i BKG LIVE TIME(SEC) : 60000.00 I EFF FILE : W212.CNF;119 i CAL DATE : 16-Sep-2016 I NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc ENERGY ENERGY FWHM AREA AREA AREA Stoev pCi/G pCi/G pCi/G pCi/G pCi/G PU-236 5749.00 5712.28 0.000 0.000 -0.720 0.720 0.8485 100.000 -1.86E-02 5.64E-02 1.58E-01 4.02E-02 5.62E-02 PU-238 5486.00 5439.10 0.000 5.000 3.800 1.200 1.0954 99.900 8.14E-02 1.06E-01 1.50E-01 4.30E-02 1.06E-01 PU-239 5155.00 5132.78 19.941 2.000 1.280 0.720 0.8485 99.900 2.72E-02 7.51E-02 1.30E-01 3.31E-02 7.49E-02 PU-242 4890.00 4851.76 40.619 187.000 185.800 1.200 1.0954 100.000 3.95E+OO 8.37E-01 1.49E-Oi 4.26E-02 5.72E-01 PU-244 4589.00 4590.71 0.000 2.000 1.520 0.480 0.6928 99.900 3.23E-02 7.44E-02 1.1 SE-01 2.70E-02 7.43E-02 ! **-......... "'"' I ! PU*239: 5011*5227 keV y.\\\i 15 t-PIJ.238: 5375-5556 keV I I PIJ.236: SSS2*5843 keV 13 ii 11 t j tr Yi '1 9 [-I-7L z :::> 0 I (.) 5 i--I t5 1 <( . Jlil ' ' ,-* I i I 2376 2776 3181 3589 4000 5 5 684 6114 6547 6984 7425 Energy (keV) "' !') "- GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT ---,------BATCH NUMBER : 1596394 SAMPLE ID : R0405235012_PU SAMPLE QTY : 0.506 G +/-0.198 % CH AMBER : 213 I DETECTOR SIN : 87901 I AVERAGE %EFFICIENCY : 24.8786 I AVERAGE %EFF ERROR : 0.4826 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B213.CNF;469 I BKG DATE : 23-Sep-2016 l BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.6 +/-6.822 % I COUNT DATE : 29-Sep-2016 09:23:37 I ELAPSED LIVE TIME(SEC) : 14400.00 ! EFF FILE : W213.CNF;152 i CAL DATE : 16-Sep-2016 -----* *------NOMINAL : 4.3831 E+OO dpm RESULTS : 3.9699E+OO dpm NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ENERGY ENERGY FWHM AREA AREA AREA StDev PU-236 5749.00 5712.28 0.000 0.000 -0.480 0.480 0.6928 100.000 PU-238 5486.00 5455.35 4.987 1.000 0.280 0.720 0.8485 99.900 PU-239 5155.00 5118.71 0.000 0.000 -1.200 1.200 1.0954 99.900 PU-242 4890.00 4873.06 73.853 238.000 237.040 0.960 0.9798 100.000 PU-244 4589.00 4568.76 4.987 1.000 0.520 0.480 0.6928 99.900 >> '.1i .,_ o-17 I I PlJ.239: 5011*5227 keV 15 !--PU-238: 5375-5566 keV I ! PU-235: 5582*5Sl3 keV 11 13 L I Jj 11 I ., ! Ui gr I-z ::> ?[-0 Q. *:; ts ! <( 1 l I i . J.,. I *-.-'. I I ! ! 2377 2778 3182 3590 4002 441 4836 5 5 685 6115 6548 6985 Energy (keV) g 'l' ::> ::> 0. c.. 0. c.. 0. I 1.96-sigma 1.96-sigma ACTIVITY TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G pCi/G -9.61E-03 4.26E-02 1.11 E-01 2.54E-02 4.25E-02 4.64E-03 4.86E-02 1.01 E-01 2.58E-02 4.85E-02 -1.98E-02 3.75E-02 1.16E-01 3.31E-02 3.75E-02 3.90E+OO 7.37E-01 1.08E-01 2.95E-02 4.99E-01 8.57E-03 4.77E-02 9.13E-02 2.09E-02 4.76E-02 r(OI. {f ! 7426 Ali>ha $p<lctros<opy Software Vemion 3.5.3

  • effective date: 02-Mar-2015 BATCH NUMBER : 1596394 SAMPLE ID : R0405235013_PU GEL Laboratories 'LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-035 CHAMBER : 214 LIB FILE : PU DETECTOR S/N : 87902 BKG FILE : 8214.CNF;456 SAMPLE QTY : 0.500 G +/-0.200 % AVERAGE %EFFICIENCY : 26.2230 BKG DATE : 23-Sep-2016 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 75.4 +/-7.266 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.3063E+OO dpm AVERAGE %EFF ERROR : 0.5080 BKG LIVE TIME(SEC) : 60000.00 COUNT DATE : 29-Sep-2016 09:23:39 EFF FILE : W214.CNF;119 ELAPSED LIVE TIME(SEC) : 14400.00 CAL DATE : 16-Sep-2016 NUCLIDE ACTIVITY SUMMARY 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le ENERGY ENERGY FWHM AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G PU-236 5749.00 5624.99 4.958 1.000 0.520 0.480 0.6928 100.000 1.20E-02 6.68E-02 1.28E-01 2.93E-02 PU-238 5486.00 5448.78 4.958 1.000 0.040 0.960 0.9798 99.900 7.65E-04 5.68E-02 1.26E-01 3.43E-02 PU-239 5155.00 5167.19 44.618 3.000 2.040 0.960 0.9798 99.900 3.88E-02 7.73E-02 1.25E-01 3.41E-02 PU-242 4890.00 4873.06 51.228 210.000 208.080 1.920 1.3856 100.000 3.95E+OO 7.95E-01 1.53E-01 4.82E-02 PU-244 4589.00 4546.97 0.000 0.000 -0.480 0.480 0.6928 99.900 -9.12E-03 4.04E-02 1.05E-01 2.41E-02 17 15 13 11 -(/J I-9 z :::> 7 0 s 5 z. 3 t5 <( 1 PU 244' 4497 4597 keV [ PU-242; 4654-4995 keV I I PU*239: 5011-5227 keV I f'U.238: 5375-5586 keV l FU-235: 5582-5843 keV i ,i ul ! ,i 1-I '-I II I I I 11t t ! l
  • I I I I Ii I _jl jl I I i ' I . ! ! ! ' ! , I I . I , I I I I I 23 73 2771 3174 *3581 3991 4824 41 1673 6104 6538 6976 7419 '-Energy (keV) N 0. 1.96-sigma cnt Unc pCi/G 6.68E-02 5.67E-02 7.71 E-02 5.41E-01 4.03E-02 BATCH NUMBER : 1596394 SAMPLE ID : R0405235014 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G -+/-0.199 % CHAMBER : 218 DETECTOR S/N : 87906 AVERAGE %EFFICIENCY : 25.1171 AVERAGE %EFF ERROR : 0.4871 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 86.0 +/-6.952 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.7703E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5451.35 PU-239 5155.00 5120.15 PU-242 4890.00 4869.65 PU-244 4589.00 4591.42 _ PIJ.244: <<G7-4597 keV I I PIJ.242: 4654-4995 keV 15 [ PU*239: 5011-5227 keV PU*238: 5375-5566 keV 1 3 ' PU-238: 5582-5843 keV ' I I 11 l-i I (j) 9 r-I-l z 7 i-:::> sl 0 Q. >. I ... I 3 I-0 1 b I <t: t, j I,, J ! I. ' I , 2369 2770 3176 3585 Energy (keV) PEAK FWHM 0.000 69.949 169.875 59.956 4.996 11 1 3997 441 I COUNT DATE : 29-Sep-2016 09:23:41 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G o,ooo -0.480 0.480 0.6928 100.000 -1.01E-02 2.000 1.520 0.480 0.6928 99.900 2.65E-02 4.000 2.320 1.680 1.2961 99.900 4.02E-02 228.000 227.280 0.720 0.8485 100.000 3.93E+OO 1.000 0.520 0.480 0.6928 99.900 9.01E-03 ] ] ] Si6i *:: ... § ::J"'"' &l .... .. :;i I I , I I . ' I . ; .. 684 6115 6550 6988 7430 ::J .. 'l' iii 'l' => iC iC :::> :::> 0. 0. 1l. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU
  • BKG FILE : B218.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W218.CNF;126 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.48E-02 1.17E-01 2.67E-02 6.10E-02 9.66E-02 2.21E-02 7.95E-02 1.34E-01 4.11E-02 7.57E-01 1.06E-01 2.69E-02 5.01E-02 9.59E-02 2.20E-02 r 0\ 'Y 1.96-sigma cnt Unc pCi/G 4.47E-02 6.09E-02 7.93E-02 5.14E-01 5.00E-02

'"'d ct> Vo N 00 0\ 0 ......, Vo 00 0 \0 ... GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 BATCH NUMBER : 1596394 SAMPLE ID : R0405235015_PU SAMPLE QTY : 0.509 G +/-0.196 % CHAMBER : 235 LIB FILE : PU DETECTOR S/N : 87923 . BKG FILE : B235.CNF;455 AVERAGE %EFFICIENCY : 24.7991 ! BKG DATE : 23-Sep:2016 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 97.3 +/-6.614 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.2643E+OO dpm NUCLIDE LIBRARY 00 1-z :::.i 0 () ._.. > <'{ ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 17 / PU*239:5011*5227keV 15 .._,* PU*238: 5375-5566 keV PU-238: 5582-5843 keV 13 ! 11 I 5 i-* ! ! PEAK ENERGY 5750.94 5465.55 5118.70 4868.08 4546.97 PEAK FWHM 109.512 149.334 0.000 70.934 0.000 AVERAGE %EFF ERROR : 0.4811 1 BKG LIVE TIME(SEC) : 60000.00 COUNT DATE : 29-Sep-2016 09:44:15 j EFF FILE : W235.CNF;118 ELAPSED _____ L__ CAL DATE : 19-Sep-2016 NUCLIDE ACTIVITY SUMMARY 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA AREA St Dev pCi/G pCi/G pCi/G pCi/G 3.000 1.800 1.200 1.0954 100.000 3.35E-02 7.62E-02 1.31E-01 3.73E-02 5.000 4.280 0.720 0.8485 99.900 6.59E-02 7.59E-02 9.41E-02 2.39E-02 0.000 -0.960 0.960 0.9798 99.900 -1.47E-02 3.41E-02 1.01E-01 2.75E-02 255.000 253.800 1.200 1.0954 100.000 3.88E+OO 7.11E-01 1.07E-01 3.07E-02 0.000 -0.240 0.240 0.4899 99.900 -3.67E-03 3.17E-02 7.34E-02 1.37E-02 1 L; -* , I . . . . ! ' . I , 2392 2792 3196 3604 4016 Energy (keV) 6132 6566 7005 7447 1.96-sigma cnt Unc pCi/G 7.60E-02 7.53E-02 3.40E-02 4.80E-01 3.17E-02 BATCH NUMBER : 1596394 SAMPLE ID : R0405235016_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT I CHAMBER : 220 SAMPLE QTY : 0.501 G +/-0.200 % '1 DETECTOR SIN : 87908 AVERAGE %EFFICIENCY : 24.0361 I AVERAGE %EFF ERROR : 0.4668 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 98.0 +/-6.688 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 4.2956E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 _ PU-24-4:4497-4S97keV 19 I f'U.242: 4654-4995 keV r PU*239: 5011*5227 keV 17 ._ f>U.238: 5375-5568 keV I PlJ.:236: 55a2*5843 keV 15 I 13 f-11 z 9 f-:::> I 8 ;: 5 l 3 j-PEAK ENERGY 5712.29 5470.36 5071.69 4882.99 4526.96 PEAK FWHM 0.000 0.000 4.978 73.840 4.978 1 f-. I I l 2377 2777 3181 3588 3998 441 Energy (keV) 11 ::> ll. j COUNT DATE : 29-Sep-2016 09:23:45 I ELAPSED LIVE TIME(SEC) : 14400.00 l I NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.39E-02 0.000 -0.720 0.720 0.8485 99.900 -1.15E-02 1.000 0.760 0.240 0.4899 99.900 1.21E-02 249.000 247.800 1.200 1.0954 100.000 3.94E+OO 1.000 0.760 0.240 0.4899 99.900 1.21E-02 / . . .. I . l . . l 4830 5 51 676 6104 6535 6970 7 409 N ;: ::, ll. Instrument SOP: Gt..:RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B220.CNF;458 BKG DA TE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W220.CNF;142 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.22E-02 1.18E-01 3.01E-02 3.49E-02 9.79E-02 2.49E-02 4.54Ec02 7.63E-02 1.43E-02 7.30E-01 1.12E-01 3.19E-02 4.54E-02 7.63E-02 1.43E-02 1.96-sigma cnt Unc pCi/G 4.21E-02 3.48E-02 4.54E-02 4.93E-01 4.54E-02 BATCH NUMBER : . 1596394 SAMPLE ID : R0405235017_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 221 1 DETECTOR S/N : 87909 SAMPLE QTY : 0.501 G +/-0.200 % I AVERAGE %EFFICIENCY : 25.5264 i AVERAGE %EFF ERROR : 0.4948 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 75.8 +/-7.313 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.3221 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.29 PU-238 5486.00 5444.18 PU-239 5155.00 5162.88 PU-242 4890.00 4871.18 PU-244 4589.00 4581.20 14 13 f-PU-239: 5011-5227 keV 12 L PU-238: 53'75-5566 keV I PU-238: 5582-5843 keV 11 f-10 ' 9 f-Ci) al-I I-7[-z 6 f-:J I 0 5 f-2. 3 f-2 l-' -u 1 h1 I ... I ; 2382 2784 3190 3599 Energy (keV) PEAK FWHM 0.000 5.006 45.052 69.899 0.000 I 4011 44 ! COUNT DATE : 29-Sep-2016 09:23:48 /ELAPSED LIVE TIME(SEC) : 14400.00 I NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.70E-02 1.000 0.520 0.480 0.6928 99.900 1.01E-02 2.000 1.280 0.720 0.8485 99.900 2.48E-02 204.000 203.520 0.480 0.6928 100.000 3.94E+OO 2.000 1.760 0.240 0.4899 99.900 3.41E-02 :u ::i .... ., ..,g :gig ii Ii I I 5 6 695 6124 6557 6993 7433 " "' <:; l":l n. Instrument SOP: .GL-RAD-1-009 Analytical SOP: LIB FILE : PU BKG FILE : B221.CNF;467 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W221.CNF;128 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.16E-02 1.45E-01 3.68E-02 5.64E-02 1.0BE-01 2.48E-02 6.84E-02 1.1 BE-01 3.01E-02 7.98E-01 1.07E-01 2.46E-02 6.72E-02 9.29E-02 1.74E-02 1.96-sigma cnt Unc pCi/G 5.15E-02 5.64E-02 6.83E-02 5.44E-01 6.71E-02 "'d (l) Vo N 00 \0 0 >-+, Vo 00 0 \0 Aloha Spec!R>scop'/ Software Vers;on 3.5.3 effective data: 02-Mar-2015 BATCH NUMBER : 1596394 SAMPLE ID : R0405235018_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 223 ! DETECTOR SIN : 87911 Instrument SOP:**GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8223.CNF;460 SAMPLE QTY : 0.500 G +/-0.200 % j AVERAGE %EFFICIENCY : 25.6333 i AVERAGE %EFF ERROR : 0.4968 i BKG DATE : 23-Sep-2016 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 80.7 +/-7.090 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.5358E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5691.16 PU-238 5486.00 5476.68 PU-239 5155.00 5118.71 PU-242 4890.00 4875.08 PU-244 4589.00 4546.97 15 ! ::::: L PU-239: 5011-5227 l<eV 1 3 , PU-238: 5375-5586 l<eV j PU-236: 5582-5843 l<eV i 11 r (ii I f-z 7 'r-;:) J 0 i (.) -I .?!' I *;:; 3 f--u I <( 1 ll l I ;i ! -.. ! 2377 2776 3178 3584 Energy (keV) PEAK FWHM 24.821 49.642 0.000 61.981 0.000 ! l ! ! 3994 440 i COUNT DATE : 29-Sep-2016 09:23:51 /ELAPSED LIVE TIME{SEC) : 14400.00 ! 1 BKG LIVE TIME(SEC) : 60000.00 j EFF FILE : W223.CNF;114 I CAL DATE : 16-Sep-2016 --NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1 .96-sigrna GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G 2.000 1.520 0.480 0.6928 100.000 3.37E-02 7.76E-02 1.23E-01 2.82E-02 7.75E-02 3.000 1.560 1.440 1.2000 99.900 2.85E-02 7.53E-02 1.35E-01 4.02E-02 7.52E-02 0.000 -0.240 0.240 0.4899 99.900 -4.36E-03 3.77E-02 8.71E-02 1.63E-02 3.76E-02 218.000 217.520 0.480 0.6928 100.000 3.95E+OO 7.75E-01 1.01E-01 2.30E-02 5.27E-01 0.000 -0.240 0.240 0.4899 99.900 -4.36E-03 3.77E-02 8.71E-02 1.63E-02 3.76E-02 >> > .ll :g .,_ <>-e>O .... .. .. ., ..,., ,i !j rt.°' ! i 4825 6098 6529 6965 7403 => ::> a: => Q. Q. 0. c.. BATCH NUMBER : 1596394 SAMPLE ID : R0405235019_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 224 , DETECTOR SIN : 87912 *****.*.** SAMPLE QTY : 0.506 G +/-0.198 % j AVERAGE %EFFICIENCY : 25.7363 I AVERAGE %EFF ERROR : 0.4987 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 90.2 +/-6.738 % TRACER

  • ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831E+OO dpm RESULTS : 3.9555E+OO dpm ------NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 5712.26 0.000 PU-238 5486.00 5458.69 4.920 PU-239 5155.00 5183.32 0.000 PU-242 4890.00 4876.19 66.419 PU-244 4589.00 4546.97 0.000 23 PU-244: 4497..t597 keV ! PU-242: 4654-1995 keV 21 f-_ PU-239:5011-5227keV I PU*238: 5375-5566 keV 19 l PU-236: 5582-58'3 keV ! 17 l-15 13 -CJ) I I-11 r-z ::> I 9 r-0 8 7 I->-51 .... *:;: t5 <( 1 ii ! 2399 2795 3195 3599 4007 Energy (ke V) I COUNT DATE : 29-Sep-2016 09:23:52 /ELAPSED LIVE TIME(SEC) : 14400.00 i NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 -0.440 1.440 1.2000 99.900 -7.08E-03 5.000 4.280 0.720 0.8485 99.900 6.84E-02 246.000 244.320 1.680 1.2961 100.000 3.90E+OO 0.000 0.000 0.000 0.0000 99.900 0.00E+OO >> *:: "'"' mlll .... .. s "'"' i I ! l I 1* ii R ,J 1* I I I j I 682 6112 6545 6983 7425 .. "' <ii ; ::> :;, ::> c. .. c. c. 0. Instrument SOP: G(-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B224.CNF;471 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W224.CNF;150 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.93E-02 5.83E-02 O.OOE+OO 4.89E-02 1.19E-01 3.54E-02 7.88E-02 9.77E-02 2.48E*02 7.28E-01 1.24E-01 3.79E-02 3.23E-02 4.80E-02 O.OOE+OO .. lD IXC\ 10 1.96-sigma cnt Unc pCi/G 3.92E-02 4.89E-02 7.82E-02 4.92E-01 3.22E-02 0 >-+, Vt 00 0 \0 BATCH NUMBER : 1596394 SAMPLE ID : R0405235020_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.502 G +/-0.199 % CHAMBER : 226 DETECTOR S/N : 87914 AVERAGE %EFFICIENCY : 26.8347 AVERAGE %EFF ERROR : 0.5195 SAMPLE DATE : 08-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 74.0 _ +/-7.240 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 3.2421 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5661.00 PU-238 5486.00 5447.11 PU-239 5155.00 5118.70 PU-242 4890.00 4861.53 PU-244 4589.00 4535.50 15 , FU*244: 4497-4597 keV i f'U.242: *654-4995 keV I FU-239: 5011-5227 keV 13 f-f'U.238: 5375-5506 keV f PU-235: 55132*5843 keV i 11 f-I I 9 !-'iii I I-7L z I :::> 0 sL Q ! :?! 3L -1 L , 0 <( IL . i PEAK FWHM 4.984 54.821 0.000 50.564 0.000 I 1 2372 2772 3177 3585 3997 441 Energy (keV) COUNT DATE : 29-Sep-2016 09:23:54 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 1.000 1.000 0.000 0.0000 100.000 2.29E-02 2.000 1.280 0.720 0.8485 99.900 2.43E-02 0.000 -1.440 1.440 1.2000 99.900 -2.72E-02 210.000 208.800 1.200 1.0954 100.000 3.93E+OO 4.000 3.760 0.240 0.4899 99.900 7.09E-02 :i :il > Si:: "' "'"' .. vii! ii I' li +-i I I 682 6113 6548 6986 7428 ; ; ::> ::> "-0. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B226.CNF;460 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W226.CNF;122 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.46E-02 6.88E-02 0.00E+OO 6.69E-02 1.16E-01 2.95E-02 4.39E-02 1.39E-01 4.14E-02 7.89E-01 1.32E-01 3.78E-02 8.42E-02 9.04E-02 1.69E-02 1.96-sigma cnt Uno pCi/G 6.45E-02 6.68E-02 4.38E-02 5.37E-01 8.36E-02 o.\\v "\\, (\I\ {'\

Aloha Spectrosoopy Software Version 3.5.3 eftec:We 02-Mar-2015 BATCH NUMBER : 1596394 SAMPLE ID : R1203621703_PU * ** GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G +/-0.196 % CHAMBER : 227 DETECTOR SIN : 87915 AVERAGE %EFFICIENCY : 26.3665 AVERAGE %EFF ERROR : 0.5107 SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 % YIELD : 91.8 +/-6.608 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.0228E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5470.35 PU-239 5155.00 5151.00 PU-242 4890.00 4857.07 PU-244 4589.00 4546.97 _ PU-244: 4497-4597 keV L PU*242; 4854-4995 keV 17 I PU*239: 5011-5227 keV l PU*238: 5375-558& keV I 11 Yi I-z 7L :::> 0 5L s >-! -I *s: 3 f-'.iJ 0 ! <( 1 l-I ! .. PEAK FWHM 0.000 0.000 54.147 64.520 0.000 i I 2375 2771 3171 3576 3984 439 Energy (keV) I COUNT DATE : 29-Sep-2016 09:24:00 !ELAPSED LIVE TIME(SEC) : 14400.00 l NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 0.000 -1.200 1.200 1.0954 99.900 -1.83E-02 6.000 3.840 2.160 1.4697 99.900 5.86E-02 256.000 254.560 1.440 1.2000 100.000 3.88E+OO 0.000 -0.240 0.240 0.4899 99.900 -3.66E-03 1. *I II ,,ji Ir ji ! 61 6091 6525 6963 7405 ... "' f:l ::> ::> ::> a. a. c.. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B227.CNF;459 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W227.CNF;120 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.09E-02 4.58E-02 O.OOE+OO 3.47E-02 1.07E-01 3.06E-02 8.27E-02 1.28E-01 4.11E-02 7.10E-01 1.13E-01 3.35E-02 3.16E-02 7.31E-02 1.37E-02 1.96-sigma cnt Unc pCi/G 3.08E-02 3.47E-02 8.23E-02 4.79E-01 3.16E-02 "* BATCH NUMBER : 1596394 SAMPLE ID : R1203621704_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 228 DETECTOR S/N : 87916 SAMPLE QTY : 0.500 G +/-0.200 % I AVERAGE %EFFICIENCY : 25.5769 AVERAGE %EFF ERROR : 0.4958 SAMPLE DATE : 10-Dec-2015 00:00:00 ANALYST : JXH2 % YIELD : 56.0 +/-8.523 % TRACER JD : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 2.4540E+OO dpm NUCLIDE . LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.28 PU-238 5486.00 5387.67 PU-239 5155.00 5149.45 PU-242 4890.00 4853.01 PU-244 4589.00 4546.97 1 0 _ PU*244: 4497-1597 kcV I PIJ.242: .WS<l-4995 kcV 9 i PU-239: 5011*5227 kcV r PIJ.238: 5375-5566 kcV ! PU-236: 5582*5843 kcV 81 i 7 r-6L en I-z i ::::> 4 f-0 () -c i *:;; 2 f-u i <l:: 1 f-i I I i I ! I i ' I I : PEAK FWHM 0.000 9.940 114.305 101.632 0.000 i i ,, I !I I I I !l ! I 2369 2768 3171 3578 3989 440 Energy (keV) j COUNT DATE : 29-Sep-2016 09:23:57 ELAPSED LIVE TIME(SEC) : 14400.00 ! j NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -1.200 1.200 1.0954 100.000 -3.82E-02 2.000 1.280 0.720 0.8485 99.900 3.38E-02 4.000 1.840 2.160 1.4697 99.900 4.83E-02 154.000 150.640 3.360 1.8330 100.000 3.95E+OO 0.000 -0.720 0.720 0.8485 99.900 -1.89E-02 > r;;:;; :ii .,_ :e ""' "'-.... " sr;g g ...... ... , I 1 I I r I I I l j 667 6096 6528 6964 7404 11: "' 2 :S 2 2 0.. c.. .. ,.,, Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B228.CNF;457 BKG DATE : 23-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W228.CNF;117 CAL DATE : 16-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.27E-02 2.24E-01 6.40E-02 9.32E-02 1.61 E-01 4.10E-02 1.22E-01 2.20E-01 7.06E-02 9.32E-01 2.55E-01 8.80E-02 5.72E-02 1.60E-01 4.08E-02 1.96-sigma cnt Unc pCi/G 7.25E-02 9.30E-02 1.21 E-01 6.41E-01 5.70E-02 oo"' '('0 GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-035 BATCH NUMBER : 1596394 CHAMBER : 234 LIB FILE : PU SAMPLE ID : R1203621705_PU DETECTOR SIN : 87922 BKG FILE : B234.CNF;454 SAMPLE QTY : 0.509 G +/-0.196 % SAMPLE DATE : 26-Sep-2016 00:00:00 ANALYST : JXH2 i AVERAGE %EFFICIENCY : 24.8037 BKG DATE : 23-Sep-2016 I AVERAGE %EFF ERROR : 0.4811 BKG LIVE TIME(SEC) : 60000.00 I COUNT DATE : 29-Sep-2016 09:24:05 EFF FILE : W234.CNF;117 % YIELD : 55.5 +/-8.584 % . i ELAPSED LIVE TIME(SEC) : 14400.00 CAL DATE : 19-Sep-2016 ID : 1770-A i ID NUCLIDE : PU-242 ; NUCLIDE NOMINAL : 4.3831 E+OO dpm j NOMINAL (pCi/G) RESULTS : 2.4318E+OO dpm , % RECOVERY NU CLl DE ACTIVITY SUMMARY NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 1 0 , PIJ.244; 4497-4597 keV I PU*242: 4654-4995 keV 9 j PU-239:5011*5227 keV r PIJ.238: 5375-5566 koV 8 L PU*235'. 5582-5843 keV I 6 i SL 4L ! 3 I 2 f-! I 1 l I i i PEAK PEAK ENERGY FWHM 5712.30 0.000 5507.77 4.996 5164.67 49.963 4864.06 92.432 4546.98 0.000 i I i , GROSS AREA 0.000 1.000 4.000 145.000 0.000 I u i NET AREA -0.480 -0.440 2.080 144.760 0.000 BKG BKG %ABUN AREA StDev 0.480 0.6928 100.000 1.440 1.2000 99.900 1.920 1.3856 99.900 0.240 0.4899 100.000 0.000 0.0000 99.900 ' ' . ACTIVITY pCi/G -1.29E-02 -1.18E-02 5.58E-02 3.88E+OO O.OOE+OO . , ' I .. 2388 2790 3194 3603 4014 Energy (keV) )694 6123 6554 6990 7 428 1.96*sigma TPU MDA le pCi/G pCi/G pCi/G 5.72E-02 1.49E-01 3.41E-02 8.16E-02 1.98E-01 5.90E-02 1.24E-01 2.17E-01 6.81E-02 9.22E-01 1.28E-01 2.40E-02 5.43E-02 8.05E-02 O.OOE+OO 1.96"sigma cnt Uno pCi/G 5.70E-02 8.15E-02 1.23E-01 6.35E-01 5.41E-02 Effective 3/25/201 o Revision 1 Effective March 2010 Radiochemistry Batch Checklist 27-Sep-2016 l-_ Product: ___ U_U ____ _ Date: 9 /27 //{p I Criteria: Yes No Comments Sample Solids arc less than or CQUal to 100 mQ for GAB. JJ-Samples have been blank corrected (if required). ( (' Blank correction reported Included !ff reoulred\, /ii fJ-If activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. If tho MDA/ MDC is akav. Instrument source check ls within limits. t/ Instrument bka rhock I" within limit.:. Method RDL/ LLD has been met. v If duplicate activities are: Less than S* MDA/ MDC, then RPO ls 100% or less, v If greater S* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reouired RER acceotance criteria. Tracer yield Is 15*12S%

  • Carrier yield 25-125%, /V'IJ-(Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. v lfTF < 50/o nf ln ... oct .. ctlvltvl Samole was run within hold time. ,/ .<t?P Samole was correctlv orcserved If reoulred. v Smears Taken for Radioactive batches. ;//J-Method Spike and LCS are within 75-125% V' 'or meets the client's contract accAntance crlterlal. No blank spaces on data forms. v' All line outs Initialed and dated. Nn *** orrnrc Aux data Is correct. tJt.r-Client Soeclal reoulrements oaae has been checked. r/ Raw Oat" and/ or snectrum are Included and nronerlv statused. 1/ MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and / .. oc uorl<Io..t IMlt -(ff Ntv ontoro.I ./ Batch Data Exceotlon Reoorts fDER\ comoleted If aoollcable. / ,\)\A\ Batch Data Exception Reports (DER) second reviewed. --:V2/L. Dlsnosltlon verified to be comaleted. Allnuot Cnrrection comnletet! If renuired. Review sample historical results if avallable (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. \ GL-CHL-RAD-013 Rev 1 Page 1 of 1 {) 156.l\°lt/ , -I I S (b I (.{ L{ /S( 1JJSqif ' I ! ;:::::;----_.. . ...---,. Page 5295 of 5809 GEL Laboratories LLC Form GEL-DER .. DATA EXCEPTION REPORT
  • Mo.Day Yr. Division: Quality Criteria: 27*SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC EPA 906.0 Modified Solid Batch ID: Sample Numbers: 1598092 See Below Potentially affected work order(s)(SDG):4D5235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, ,405235060, 1203626145, and 1203626146 were received and analyzed out of the method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 27-SEP-16 Lyndsey Pace 27-SEP-16 Page 1 Page 5296 of 5809 DER Report No.: 1561594 Revision No.: 2 Type: Process Client Code: MJWC Batch ID: Analyst: Method: Lab SOP: Instrument: Sample ID 405235041 405235042 405235043 405235044 405235045 405235046 405235047 405235048 405235049 405235050 405235051 405235052 405235053 405235054 405235055 405235056 405235057 405235058 405235059 405235060 1203626144 MB 1598092 . Terry Phillips EPA 906.0 Modified GL-RAD-A-002 REV#21 LSC-J93763 Prep Date 23-SEP-2016 10:44:31 10:44:31 23-SEP-201610:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23*SEP-20J6 10:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:3J 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23-SEP-201610:44:31 23-SEP-201610:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23-SEP-2016 10:44:31 23-SEP-201610:44:31 1203626145 DUP (405235041) 23-SEP-2016 10:44:31 1203626146 MS (405235041) 23-SEP-2016 10:44:31 1203626147 LCS 23-SEP-2016 10:44:31 ReagentJSolvent Lot ID Description 2352257.5 Ecoscint Ultra Scintillation Solution 2373671 Sodium Hydroxide, Pellet ACS 2418926 Quenching Agent 2447042.3 Ecoscinl Ultra Scintillation Solution 2457153 RL-Potassium Pennanganate Analytical Logbook version 111-04-2002 Mattix Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Amount 13mL 2g 20uL 13mL 2mL Prep Logbook The Determination of Tritium Sample Id Description LCS 1203626147 Tritium SPIKE MS 1203626146 Tritium SPIKE Dry or Wet Unadjusted Aliquot llig# Aliquot (g) (g) w 3.36 2.958 15 w 3.42 3.045 20 w 3.43 2.931 24 w 3.35 2.52 27 w 3.34 2.593 29 w 3.47 2.823 33 w 3.27 2.593 36 w 3.3J 2.553 37 w 3.3 2.68 38 w 3.38 3.007 40 w 3.41 2.808 43 w 3.4 2.874 44 w 3.3 2.298 46 w 3.39 2.773 49 w 3.3 2.663 51 w 3.37 2.297 57 w 3.38 2.463 60 w 3.3 2.646 65 w 3.28 2.886 66 w 3.3 2.982 67 w 3.o<t> 69 w 3.36 2.958 70 w 3.3 2.905 71 w 3. <'I.{> 82 Comments: Spike Pipet ID: RAD-LSC-2970%8 Vial Pipet ID: RAD*LSC-8036326 Bkg prepared with dead water: Yes Serial Number 1753-B 1753-B ((,() 10 / Spike Amount Spike Units .I .1 mL mL Volume Added Aliquot in vial (mL) (mL) 50 10 50 10 50 10 50 10 50 10 50 JO 50 10 50 10 50 IO 50 JO 50 10 50 10 50 10 50 10 50 10 50 10 50 10 50 IO 50 IO 50 10 50 10 50 10 *50 10 50 10 GEL Laboratories LLC

""O Pl ('Jq (1) Vl N \0 T1598092R 00 0 >-+, Tritium Solid Vl 00 Filename : H30ST.XLS 0 \0 File type : Excel Version#: 1.2.13 Batch : 1598092 Analyst: TER02081 Procedure Code : LSCDSH30S Prep Date: 9/23/2016 Parmname: Tritium Method Uncertainty : O Required MDA : 6 pCi/G H-3 Abundance : 1.00 Geometry: Halflife of Tritium : 12.32 years 10mL DW/13mL Ecoscint Ultra Sample Characteristics Sample Distilled Sample Total Sample Aliquot Sample Counted Sample Sample Aliquot StDev. Counted S!Dev. Rig Sample Pos. ID Volume(L) G G L L number Datemme 405235041.1 0.0500 2.9580 3.5261E-03 0.0100 1.0000E-05 15 11/3012015 13:27 2 405235042.1 0.0500 3.0450 3.5351E-03 0.0100 1.0000E-05 20 11/30/2015 13:53 3 405235043.1 0.0500 2.9310 3.5233E-03 0.0100 1.0000E-05 24 11 /30/2015 13:59 4 405235044.1 0.0500 2.5200 3.4809E-03 0.0100 1.0000E-05 27 11/30/2015 13:50 5 405235045. 1 0.0500 2.5930 3.4885E-03 0.0100 1.0000E-05 29 11/301201514:15 6 405235046.1 0.0500 2.8230 3.5122E-03 0.0100 1.0000E-05 33 1217/2015 10:02 7 405235047.1 0.0500 2.5930 3.4885E-03 0.0100 1.0000E-05 36 1217/2015 t0:10 8 405235048.1 0.0500 2.5530 3.4843E-03 0.0100 1.0000E-05 37 1217/2015 13:28 9 405235049.1 0.0500 2.6800 3.4974E-03 0.0100 1.0000E-05 38 1217/2015 13:33 10 405235050.1 0.0500 3.0070 3.5312E-03 0.0100 1.0000E-05 40 1217/2015 13:42 11 405235051.1 0.0500 2.8080 3.5107E-03 0.0100 1.0000E-05 43 1217/2015 13:02 12 405235052.1 0.0500 2.8740 3.5175E-03 0.0100 1.0000E-05 44 1217/201513:11 13 405235053.1 0.0500 2.2980 3.4580E-03 0.0100 1.0000E-05 46 1211/2015 14:24 14 405235054.1 0.0500 2.7730 3.5070E-03 0.0100 1.0000E-05 49 121212015 14:51 15 405235055.1 0.0500 2.6630 3.4957E-03 0.0100 1.0000E-05 51 121212015 14:59 16 405235056.1 0.0500 2.2970 3.4579E-03 0.0100 1.0000E-05 57 121212015 14:50 17 405235057.1 0.0500 2.4630 3.4750E-03 0.0100 1.0000E-05 60 121212015 14:55 18 405235058.1 0.0500 2.6460 3.4939E-03 0.0100 1.0000E-05 65 121212015 15:00 19 405235059.1 0.0500 2.8860 3.5187E-03 0.0100 1.0000E-05 66 12116/2015 12:26 20 405235060.1 0.0500 2.9820 3.5286E-03 0.0100 1.0000E-05 67 1211612015 12:33 21 1203626144.1 0.0500 3.0450 3.5351E-03 0.0100 1.0000E-05 69 912312016 0:00 22 1203626145.1 0.0500 2.9580 3.5261E-03 0.0100 1.0000E-05 70 11/30/201513:27 23 1203626146.1 0.0500 2.9050 3.5207E-03 0.0100 1.0000E-05 71 11/30/201513:27 24 1203626147.1 0.0500 3.0450 3.5351E-03 0.0100 1.0000E-05 82 9/23/2016 0:00 Page 1 I Plpet, 0.1 ml Stdev : +I-0.000200 ml Plpet, 0.5 ml Stdev : +I-0.001000 ml Pipet, 1.0 ml Stdev: +I-0.002000 ml Plpet, 5.0 ml Stdev: +I-0.010000 ml Analytlcal SOP: GL-RAD*A*002 Instrument SOP: GL-RAD-1*004 Count raw Data Counting Rack Time Quench# Gross Pos. Position# (min.) cpm 1 32*2 100 162.9 4.28 2 32-3 100 160.4 3.85 3 44-1 100 162.3 4.06 4 44*2 100 163.6 4.02 5 44*3 100 161.3 3.69 6 44.4 100 162.5 4.23 7 44-5 100 162.3 3.84 8 44*6 100 161.3 3.81 9 44-7 100 163.6 3.85 10 44*8 100 161.2 3.46 11 44-9 100 163.9 3.87 12 44-10 100 162.7 4.2 13 44-11 100 170.7 3.99 14 44-12 100 163.6 4.12 15 44-1 100 162.4 4.05 16 44-2 100 162.8 3.45 17 44-3 100 163.2 3.92 18 44-4 100 167.6 4.26 19 44-2 180 205 3.n 20 44*6 100 162.5 3.43 21 44-7 100 163.1 4.04 22 44*8 100 162.7 4.03 23 44-9 100 162.9 12.23 24 44-10 100 161.1 12.49 Bkg Count Corrected Bkg Time Bkg Bkg cpm (min.) Quench# cpm 3.95 100 163 3.9469 3.95 100 163 3.8665 3.95 100 163 3.9281 3.95 100 163 3.9684 3.95 100 163 3.8961 3.95 100 163 3.9344 3.95 100 163 3.9281 3.95 100 163 3.8961 3.95 100 163 3.9684 3.95 100 163 3.8928 3.95 100 163 3.9n5 3.95 100 163 3.9407 3.95 100 163 4.1639 3.95 100 163 3.9684 3.95 100 163 3.9313 3.95 100 163 3.9438 3.95 100 163 3.9562 3.95 100 163 4.0836 3.46 180 165.8 4.0257 3.95 100 163 3.9344 3.95 100 163 3.9531 3.95 100 163 3.9407 3.95 100 163 3.9469 3.95 100 163 3.8896 T1598092R Calibration Data Detector Background Count Calibration Detector Efficiency Background Count Start Sample Counted Calibration Due Efficiency Error Rack Start Date/Time Decay on Date Date (cpmfdpm) (cpmfdpm) Position# Date/Time 9/2312016 21 :31 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1902 0.00792 32-1 9/2312016 19:47 9/2312016 23: 14 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1953 0.00792 32-1 9/23/2016 19:47 9/24/2016 2:09 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1914 0.00792 32*1 9/2312016 19:47 9/24/2016 3:52 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1888 0.00792 32-1 9/23/2016 19:47 9/24/2016 5:36 0.955 LSCBROWN 7/1/2016 6130/2017 0.1935 0.00792 32-1 9/2312016 19:47 9/24/2016 7:19 0.956 LSCBROWN 711/2016 6/30/2017 0.1910 0.00792 32*1 9/2312016 19:47 9/24/2016 9:03 0.956 LSCBROWN 7/1/2016 6/30/2017 0.1914 0.00792 32-1 9/2312016 19:47 9/24/2016 10:46 0.956 LSCBROWN 7/1/2016 6/30/2017 0.1935 0.00792 32*1 9/2312016 19:47 9/24/2016 12:30 0.956 LSCBROWN 7/1/2016 6/30/2017 0.1888 0.00792 32*1 9/2312016 19:47 9/24/2016 14:14 0.956 LSCBROWN 7/1/2016 6/30/2017 0.1937 0.00792 32-1 9/2312016 19:47 9124/201615:57 0.956 LSCBROWN 7/112016 6/30/2017 0.1882 0.00792 32-1 9/2312016 19:47 9/24/201617:41 0.956 LSCBROWN 7/1/2016 6/30/2017 0.1906 0.00792 32-1 9/23/2016 19:47 9/24/2016 19:24 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1749 0.00792 32-1 9/2312016 19:47 9/24/2016 21 :08 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1888 0.00792 32-1 . 9/231201619:47 9/24/2016 22:52 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1912 0.00792 32-1 9/231201619:47 9/25/2016 0:35 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1904 0.00792 32-1 9/23/2016 19:47 9/25/2016 2:19 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1896 0.00792 32-1 9/2312016 19:47 9/25/2016 6:47 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1809 0.00792 32*1 9/2312016 19:47 9/26/2016 9:50 0.957 LSCBROWN 7/1/2016 6/30/2017 0.1174 0.00792 44-1 9/26/2016 6:40 9/25/2016 10:17 0.957 LSCBROWN 7/1/2016 6/30/2017 0.1910 0.00792 32-1 9/2312016 19:47 9125/2016 12:01 1.000 LSCBROWN 7/1/2016 6/30/2017 0.1898 0.00792 32-1 9/231201619:47 9/25/2016 13:44 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1906 0.00792 32-1 9/2312016 19:47 9/25/2016 15:28 0.955 LSCBROWN 7/1/2016 6/30/2017 0.1902 0.00792 32-1 9/2312016 19:47 9/2512016 17:12 1.000 LSCBROWN 7/1/2016 6/30/2017 0.1939 0.00792 32-1 9/2312016 19:47 Page2 Notes: 1 -Results are decay corrected to Sample Date/Time 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Datemme * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 2.7434 1.9368 6 3.9994 1.3959 86.11% 2 2.5690 1.8137 6 3.7464 -0.0656 1679.89% 3 2.7446 1.9377 6 4.0015 0.5543 214.28% 4 3.2532 2.2968 6 4.7422 0.2555 548.14% 5 3.0573. 2.1585 6 4.4580 -0.9687 133.65% 6 2.8550 2.0157 6 4.1624 1.2912 96.67% 7 3.0992 2.1881 6 4.5186 -0.4181 316.35% 8 3.1020 2.1900 6 4.5231 -0.4106 322.46% 9 3.0559 2.1575 6 4.4546 -0.5514 236.09% 10 2.6298 1.8567 6 3.8347 -1.7508 62.65% 11 2.9293 2.0681 6 4.2700 -0.4794 260.49% 12 2.8127 1.9858 6 4.1006 1.1151 110.02% 13 3.9444 2.7848 6 5.7456 -1.0201 164.21% 14 2.9558 2.0868 6 4.3087 0.6825 187.65% 15 3.0247 2.1355 6 4.4098 0.5497 237.92% 16 3.5272 2.4902 6 5.1422 -2.6616 55.07% 17 3.3087 2.3360 6 4.8234 -0.1826 775.70% 18 3.2800 2.3157 5 4.7792 0.8688 163.78% 19 3.4235 2.4170 6 4.9498 -1.7761 81.41% 20 2.5995 1.9059 6 3.9356 *2.0833 53.81% 21 2.5537 1.8029 6 3.7228 0.3387 325.32% 22 2.7361 1.9317 6 3.9889 0.3737 316.03% 23 2.7942 1.9727 6 4.0735 35.3548 4.92% 24 2.4801 1.7510 6 3.6165 32.8227 4.78% T1598092R Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCi/G 0.3331 0.2868 2.3559 -0.0165 0.2778 2.1587 0.1319 0.2826 2.3281 0.0516 0.2826 2.7455 -0.2061 0.2754 2.5376 0.2956 0.2857 2.4464 -0.0881 0.2787 2.5924 -0.0861 0.2776 2.5949 -0.1184 0.2796 2.5513 -0.4328 0.2712 2.1498 -0.1075 0.2801 2.4474 0.2593 0.2853 2.4046 -0.1739 0.2856 3.2832 0.1516 0.2844 2.5100 0.1187 0.2825 2.5635 -0.4938 0.2719 2.8727 -0.0362 0.2805 2.7769 0.1764 0.2889 2.7888 -0.2557 0.2081 2.8338 -0.5044 0.2714 2.1968 0.0869 0.2827 2.1599 0.0893 0.2823 2.3146 8.2831 0.4022 3.3648 8.6004 0.4047 3.0273 Pages 1753-B 11/2/2016 2548.86 0.10 1753-B 11/2/2016 2548.86 0.10 2SIGMA Total Prop. Uncertainty pCi/G 2.3560 2.1587 2.3281 2.7455 2.5376 2.4464 2.5924 2.5949 2.5513 2.1498 2.4474 2.4047 3.2832 2.5101 2.5635 2.8727 2.7769 2.7888 2.8338 2.1968 2.1599 2.3146 3.4117 3.0722 Sample QC 405235041.1 405235041. 1 Sample Nominal Type RPO RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP

  • 0.0% MS 41.3756 85.4% LCS 37.7056 87.0%

]( D* ::: T ][ -T-l: IU ftvll 6 PRESET TIME DATr:.) Cr:.)LC COUNT BLANl-Z TWO PHASE SCINTILLATOR: LOW LEVEL l.12) tZI

  • IZit:i) CPM NO l\l() LIGllJID NO COMMENT:BRDWN H# :YES SAMPLE REPEATS: IC# : NO REPLICATES AQC : ND CYCLE REPEATS : LUMEX:VES LOW SAMPLE REJ: HALF LIFE CORRECTION QATE: :l. 1 l Ill PAGE: 1 23 SEP 2016 20:15 PRINTER : STD RS232 =EDIT DISK : OFF none CHAN: 50.0 -255.0 2.00 FACTOR: CHAN= 0.0 -900.0 %ERROR: 2.00 FACTOR: 1.000000 BKG. SUB: 1.000000 BKG. SUB: 0 0 SAM POS TIME M# _____ J!otX.N.P.....;!, ___ _ __ . ___ j.<_;.!_l:___NP_g __ LU MEX EU=tPSED NO MIN CPM %ERROR CPM %ERROR % TIME 1. IZitZt
  • 0 ti.'.I 1S3. 0 3.95 1.Li::!1 36w52 3.35 *::1 ... _. 18 1 izr::::*;. 13 I l.IZI tZI
  • 0 ti.'.t 4.28 l. tZt. Lt-2 35 .. 73 3u 3[:} :l.. t-..8 21216. 66 '*' 3i:::--3 1 IZllZI
  • IZllZ1 if.) IZI .. Lt. 3.85 1. 1. 0B 34-.98 :,.:;" L1.2 1 .. 59 31. IZI. 17 Page 5301 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium-Start, End: Win2: -Start, End: 12. 10 8 -en c 6 -::i 0 0 4 -0 100 Page 5302 of 5809 200 300 23 Sep 2016 19:47:35 23 Sep 2016 21 :28:00 S06092332-1 A.XLS U06092332-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 1 32-1 100.00 163.0 3704 50 255 0 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 . . § 6 8 4 0 0 100 Page 5303 of 5809 200 300 23 Sep 2016 21 :31 :07 23 Sep 2016 23:11 :31 S06092332-2A.XLS U06092332-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 2 32-2 100.00 162.9 3637 50 255 0 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 600 Channel Number (Log) 700 ' 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 4 2 -100 Page 5304 of 5809 200 300 23 Sep 2016 23:14:37 24 Sep 2016 00:55:02 S06092432-3A.XLS U06092332-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 3 160.4 50 0 32-3 3563 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 100.00 600 Channel Number (Log) 700 800 900 PAGE: 1 l: J:Ji ::: fl-Fl: ][ *y ]: IL.JI Mi 24 SEP 2016 02:37 USER: 6 CDMMENT:BROWN PRESET TIME 100.00 DATA CALC CPM SAMPLE 1 PRINTER . STD . COUNT BLANK NO IC:J:l: = ND REPLICATEB l RSi'.:.:32 TWO PHASE NO Rl:;JC " NO CYCLE . 1 DHH\ " OFF " . LIQUID UJMEX: LOW SfiMPLE RE.J: IZI LOW LEVEL NO HAL.F LIFE CORRECTICJN DATE: none 50.0 -255.0 2.00 CHAN: 0.0 -900.0 2.00 FACTOR: SAM POS 1\10 '3 :L Li.I;.*-l L( *::* l;.ft.-2 s ";.'*. *-_, -I* 4 Lz. _., l l.1.f.t--5 4-4--6 Q 7 t;A*-7 rO e 4A-e // 9 l.1.li--'3 (c9 11() 44.-10 13 l 1. LJ.LJ .. -11 1 ;::: **V;--* l 2 l3 4-4****1 { fo l L}/1.*-2 n 1 .1.1.1.1.**-2 J.-6 t'; 11 <1 17 Li-4-5 18 44-6 19 44-7 20 21 i?.2 44-10 Page 5305 of 5809 TIME MIN 100.00 162.3 4.06 100.00 163.6 4.02 100.00 161.3 3.69 100.00 162.5 4.23 100.00 162.3 3.84 100.00 161.3 3.81 101ZI. IZltZI 163. 6 100. 00 1E,1. i::! 11Zl0. 1z11z1 163 .. 9 1.0Qf. fZtfi.:I 7 1.00.IZllZI 171Z1.7 J.1L'11Z1. 00 163. G j, 1210" IZHZI 16;:2. 4 *3.85 3.46 3.87 20 3.99 4.12 4.05 100.00 162.B 3.45 100.00 163.2 3.92 !9.cl 4.05 SAMPLE TERMINATED: SAMPLE TERMINATED: SAMPLE TERMINATED= SAMPLE TERMINATED= SAMPLE TERMINATED: SAMPLE TERMINATED= :1.121. 71 l.IZI. 86 l. 1. (:'.!5 11ZI. tV3 :l.1. 15 l 1. 16 l. L :L7 1L93 u. 1'+ l.Ii).57 1. l. * .Ct.Li* 1.IZI. 71+ l IZI. 89 1 i:'.. 1Z15 1. L 16 1.1. .. 86 1.000000 BKG. SUB: 1.000000 BKG. SUB: 35. 16 3. t.1. j, 34. 39 3 * .1.;.5 34* .. 20 311 t+5 3Lt. 01. 3. 1+6 33. 90 3. 4.7 33. Li-9 3. 4-':) 33.39 3.,50 34.07 3.47 34w 44 3
  • Lj.5 33.41 3.50 34. 70 3 . .q.5 35. 07 3. 35.47 3.40 34. 18 3. 4.7 1. 85 J. 5'=> 1. 7.li. L 91 1.. 88 1.. 95 1215 1.. 96 :t2 93 1. 93 QIL} 2. :l5 :L1Z13. 1z13 31. IZI. 1ZJL1. 4*l3. 55 517. 10 6;:::0. F..;5 22 8i.=.::7. 82 931. 39 "38 U.38. -;e1 1.2.lt2. 2B 13*lf5. 99 jALJ-9. 58 35.15 3.41. 2. 1216 l 553. 1. 9 34. ...... 1 ..... 6Lt-ara+ . "J[JC/ /'J-s)l 0 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 (/) c ;::J 6 -0 (.) 4 2 0 Page 5306 of 5809 100 200 300 24 Sep 2016 02:09:19 24 Sep 2016 03:49:43 S06092444-1 A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 1 162.3 50 0 44-1 3578 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 100.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id "user Commenf Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -.!!? § 6 0 (.) 4 -2 24 Sep 2016 03:52:50 24 Sep 2016 05:33:14 S06092444-2A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 2 163.6 50 0 44-2 3497 255 990 SPECTRUM PLOT USER 06 *TRITIUM 100.00 0-*lt.,,JJIAWl!lnlim..W..immalmtl!O,,.,.....,....Jm,_..,,,_,_...,amaZlll!lUll.....,.mmm!mim,_,,,.,,.,.....,_.nam..-.imioom!IWlaum!i....dsimhll<mim..-,.._,...., 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5307 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id Us°kr Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 -10 8 -.l!l c:: 6 ::J 0 0 4 0 0 100 Page 5308 of 5809 200 300 24 Sep 2016 05:36:19 24 2016 07:16:43 S06092444-3A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 3 161.3 50 0 44-3 3484 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 100.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 .!!3 c: 6 (J 4 0 0 Page 5309 of 5809 100 200 300 24 Sep 2016 07:19:51 24 Sep 2016 09:00: 14 S06092444-4A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 4 44-4 100.00 162.5 3465 50 255 0 990 SPECTRUM PLOT. USER 06 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: (J) E :J 0 (.) 12 10 8 6 2 0 -0 Page 5310of5809 100 200 300 24 Sep 2016 09:03:23 24 Sep 2016 10:43:46 S06092444-5A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 5 44-5 162.3 3441 50 255 0 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 100.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id *user Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 . 7 .!!a c: 5 .. :i 0 (.) 4 3 -2* 1 -' 0 0 100 Page 5311 of 5809 200 300 24 Sep 2016 10:46:56 24 Sep 201612:27:19 S06092444-6A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 6 44-6 100.00 161.3 3411 50 255 0 990 SPECTRUM PLOT USER 06
  • TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -21 § 6 0 () 4 -2 0 Page 5312of5809 100 200 300 24 Sep 2016 12:30:30 24 Sep 2016 14:10:54 806092444-7 A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 7 163.6 50 0 44-7 3412 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 100.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 14 12 10 -Ul 8 -c: ::i 0 () 6 4 0 0 100 Page 5313 of 5809 200 300 24 Sep 2016 14: 14:06 24 Sep 2016 15:54:29 S06092444-8A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 8 44-8 100.00 161.2 3463 50 255 0 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Winl: Tritium -Start, End: Win2: -Start, End: 12 10 8 J!1 § 6-0 (.) 4 2 0 Page 5314of5809 100 200 300 24 Sep 2016 15:57:40 24 Sep 2016 17:38:03 S06092444-9A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 9 t63.9 50 0 44-9 3508 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 100.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -c: 6 ::J 0 (..) 4 -0 100 Page 5315of5809 ,200 300 24 Sep 2016 17:41:16 24 Sep 2016 19:21 :39 S06092444-1 DA.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 10 162.7 50 0 44-10 3408 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 .500 100.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 0 100 Page 5316 of 5809 200 300 24 Sep 2016 19:24:59 24 Sep 2016 21 :05:23 S06092444-11 A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 11 44-11 100.00 170.7 3534 50 255 0 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date tJser Filename Spectrum Type User Number User Id User 6omment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -§ 6 8 4 2 -0 0 100 Page 5317 of 5809 200 300 24 Sep 2016 21 :08:34 24 Sep 2016 22:48:56 S06092444-12A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 12 44-12 100.00 163.6 3572 50 255 0 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -::J 6 0 (.) 4 2 *o Page 5318 of5809 100 200 300 24 Sep 2016 22:52:16 25 Sep 2016 00:32:39 S06092544-1 A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 13 44-1 162.4 3609 50 255 0 990 SPECTRUM PLOT USER 06
  • TRITIUM 400 500 100.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 -8 (/) c 5 6 () 0 Page 5319 of 5809 100* 200 300 25 Sep 2016 00:35:52 25 Sep 2016 02:16:15 S06092544-2A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 14 162.8 50 0 44-2 3480 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 100.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date
  • User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 E ::I 6 0 () 4 0 0 Page 5320 of 5809 100 200 300 25 Sep 2016 02:19:28 25 Sep 2016 03:59:51 S06092544-3A.XLS U06092444-1 A.XLS Log Counts 06 TRITIUM BROWN LIQUID 15 44-3 100.00 163.2 3594 50 255 0 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 J[ J:) :::: 'll-R ][ "T J[ UI 25 SEP 2016 07:15 USER: 6 COMMENT: BROWN PRESET TIME 100.00 DATA CALC CPM SRMPLE REPEATS:: l PRINTER COUNT BLANK NO IC:l:J: . NO REPLICATES 1 TWO PHASE NO (-IG!C " NO CYCLE REPEi:rrs . :l DISK SCINTILLATOR: LIQUID UJMEX: YES LOW SAMPLE RE:J: 0 LOW LEVEL NO Ht:ILF LIFE CORF{ECTION DATE: none 50.0 -255.0 2.00 0.0 -900.0 2.00 FACTOR: 1.000000 BKG. SUB: 1.000000 BKG. SUB: SAM f:'OS TIME: H# _____ M_X.PSJQ_.;.l __ .. __ .. ... ;>>:J."!P!D.2... __ NO MIN MISSING SAMPLE 4. 1:::-CJ -z.o (::, -Z. I 7 'Z.."Z.. B '2-3 9 i.\ .. j1. I() :t tZllZt. 1ZltZ1 1.f,7. s 44 "" u 00 E"i h '7 Li-'1---6 1. IZt 1Z1
  • IZBZI :l.6i:'.. 5 LiA*-7 1tZ11z1. 00 163. 1 L1.fJ-*-[:l l IZllZI
  • 0121 1.6;:::. 7 L1.fi.-'3 t1z11z1 .. IZt 0 H:,;:::. 9 Lf4*-l 1Zl l.IZtfZI. 00 l5L 1 INSTRUMENT Calibration successful Page 5321 of 5809 CPM %ERROR CPM %ERROR 4.2G 1121. 82 35Q51 3. 1. 3.81 35.36 '1o 4 3.43 l .... , .r::. .. 13 32 .. 91 !53 4.04 1.1..00 33.65 3b 4.03 u.. 1 ":0' 33.98 3. L1.8 12.23 5.91. lf2. 14 .... 1l *12. 49 5. 8*4* 43.49 3. 1Zt6 Maxi 26 SEP 2016 04:07 LUMEX r. 59 ao. :t e *=:* :L 9 '-. L1.5 l. 72 l .. E,5 IZI 0 ElwAPfEll:!D TIME 103.24 ;'.:!H'.i. 313. E,i,?.1 417. 1.8 8'+ E;,;;:Lf. 41. 728. QH : STD :EDIT n OFF JJ q/{}1 }! Lf Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 Ill "E 6. 0 4 2 0 too Page 5322 of 5809 200 300 25 Sep 2016 06:47:23 25 Sep 2016 08:27:47 806092544-48.XLS U06092544-4A.XLS Log Counts 06 TRITIUM BROWN LIQUID 4 44-4 100.00 167.6 3629 50 255 0 990 SPECTRUM PLOT USER 06 *TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium
  • Start, End: Win2:
  • Start, End: 14 12. 10. 8 -.!:9 c: ::J 0 (J 6 4 2 0 Page 5323 of 5809 100 200 300 25 Sep 2016 10:17:45 25 Sep 2016 11 :58:09 S06092544-6A.XLS U06092544-4A.XLS Log Counts 06 TRITIUM BROWN LIQUID 6 44-6 100.00 162.5 3349 50 255 0 990 SPECTRUM PLOT USER 06
  • TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id '\Jser Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 14 12 10 -(/) 8 -c ::I 0 () 6 4 0 100 Page 5324 of 5809 200 300 25 Sep 2016 12:01 :20 25 Sep 2016 13:41 :45 S06092544-7 A.XLS U06092544-4A.XLS Log Counts 06 TRITIUM BROWN LIQUID 7 163.1 50 0 44-7 3437 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 100.00 600 Channel Number (Log} 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -§ 6-0 (.) 4 2 25 Sep 2016 13:44:59 25 Sep 2016 15:25:23 S06092544-8A.XLS U06092544-4A.XLS Log Counts 06 TRITIUM BROWN LIQUID 8 162.7 50 0 44-8 3455 255 990 SPECTRUM PLOT USER 06 -TRITIUM 100.00 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5325 of 5809 Sample Count Start Time: Data Capture Date User. Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 -E g 6 () 0 Page 5326 of 5809 100 200 300 25 Sep 2016 15:28:34 25 Sep 2016 17:08:58 S06092544-9A.XLS U06092544-4A.XLS Log Counts 06 TRITIUM BROWN LIQUID 9 44-9 100.00 162.9 4274 50 255 0 990 SPECTRUM PLOT USER .06 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: $ c :::i 0 (.) 12 10 -8 6 2 -0 0 Page 5327 of 5809 100 200 300 25 Sep 2016 17:12:10 25 Sep 2016 18:52:33 S06092544-1 QA.XLS U06092544-4A.XLS Log Counts 06 TRITIUM BROWN LIQUID 10 44-10 100.00 161.1 4402 50 255 0 990 SPECTRUM PLOT USER 06
  • TRITIUM 400 500 600 Channel Number (Log) 700 800 900

][ ]:) ::: T T J[ USER: 6 ; PRESET TIME DATA CALC COUNT PHASE SCINTILLATOR: LOW LEVEL CPM NO ND l_IQUID ND COMMEtH : B RCH.JN H# SAMPLE IC# : ND REPLICATES AQC NO CYCLE REPEATS : LUMEX:YES LOW SAMPLE REJ: HALF LIFE CORRECTION DATE: 1 :I. 1 IZI PAGE: 1 26 SEP 2016 07:05 PRI RSi:'.3i::'. DIBfZ none f::1TD :EDIT : OFF CHAN: 50.0 -255.0 2.00 FACTOR: CHAN: 0.0 -900.0 2.00 FACTOR: 1.000000 BKG. SUB: 1.000000 BKG. SUB: SAM POS TIME H# ____ W_XNP-_.;!_ ___ , *-.. .. _ LUMEX ELAPSED NO MIN CPM %ERROR CPM 1.-ERROR % TIME 1fi-1. 44--1 l.i3 0

  • IZ!IZI 1.55 .. 8 3. L;6 9.51 34.BG .-l '='a 1::.Q 28 18!:.:i. (,QI tJ ;::: 'i-4-2 1.81ZI,. 00 IZ! !5
  • 1z1 3.77 1. 7. 2;1zr 34w1S 3 .. 09 72 375. 6'1* Page 5328 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 16 14 12 10 -en 'E 8 :J 0 () 6 -4 2 0 100 Page 5329 of 5809 200 300 26 Sep 2016 06:40:18 26 Sep 2016 09:40:42 S06092644-1 A.XLS U06092644-1 A.XLS Log Counts 06 TRITIUM BRbWN LIQUID 1 165.8 50 0 44-1 6393 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 180.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 20 18 16 -14 12 Ill -c: 10 :::i 0 0 8 6 2 0 -0 100 Page 5330 of 5809 200 300 26 Sep 2016 09:50:20 26 Sep 2016 12:50:43 S06092644-2A.XLS U06092644-1 A.XLS Log Counts 06 TRITIUJv1 BROWN LIQUID 2 205.0 50 0 44-2 6329 255 990 SPECTRUM PLOT USER 06 -TRITIUM 400 500 180.00 600 Channel Number (Log) 700 800 900 Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 23-Sep-2016 Batch# { $<[ '(() / Product: __ C_('--'"o/ ___ _ Criteria: Yes No Comments Sample Solids are less than or equal to 100 mq for GAB. ;/Jr Samples have been blank corrected (If required). fv!J--Blank correction reoorted included llf required). If activity less than 10x MDA/MDC, error is less / than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. [f *ha MnA I MDC Is Instrument source check Is within limits. Instrument him "heck Is within limits. Method RDL/ LLD has been met. ,/ If duplicate activities are: l/ less than 5* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reouired RER acceotance criteria. Tracer yield Is 15-125%
  • Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. / 'If < 50/n nf ln ... ar* "ldlvltv' GL-CHL-RAD-013 Rev 1 Page 1 of 1 Samole was run within hold time. ./ .<oo I\( a 11 ./ . --SamPle was correctlv oreserved if reoulred. Smears Taken for Radioactive batches. A)lA}-' Method Spike and LCS are within 75-125% / :1 or meets th" client's contract accentanc" criteria l. No blank spaces on data forms. v All line outs Initialed and dated, INn tra ., __ a.rrnre Aux data Is correct. tJIJ-Client Soecial reaulrements oaoe has been checked. ,/ Raw Data and I or snectrum are Included and nronerlv statused. MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and / unrj<ln .. Hit *-(if ;VA-an*ara.4 ln+n ,/ -Batch Data Exceotion Renorts CDER\ comoleted If anolicable. ti 1> 1 <.. ( Q 1.Gn ' Batch Data Exception Reports (DER) second reviewed. v *72-r-J SLo<Jo II Dlsnosltion verified to be comnleted. Allnunt Correction comnleted If rRnulred AJA-[/ I Review sample historical results If available v (If REMP, results above MDC have been verified bv historical results recount or re-analvsls. l Page 5331of5809 GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 28-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC EPA EERF C-01 Modified Solid Batch ID: Sample Numbers: 1598081 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, 405235060, 1203626110, and 1203626111 were received and analyzed out of the method specified hold time. Originator's Name: Da.ta Validator/Group Leader: Elizabeth Krouse 28-SEP-16 Lyndsey Pace 28-SEP-16 Page 1 Page 5332 of 5809 DER Report No.: 1562017 Revision No.: 2 Type: Process Client Code: MJWC Prep Logbook ?0 The Determination of Carbon-14 in Water, Soil, Vegetation and Other Solid Matrices Batch ID: 1598081 Analyst: Tiffany Jordan Method: EPA EERF C-01 Modified Lab SOP: GL-RAD-A-003 REV# 15 Instrument: BAL-16107662 Sample ID Prep Date 1\-Iatrix 405235041 19-SEP-2016 11:46:47 Soil 405235042 19-SEP-2016 11:46:47 Soil 405235043 19-SEP-201611:46:47 Soil 405235044 19-SEP-2016 11 :46:47 Soil 405235045 19-SEP-2016 11:46:47 Soil 405235046 19-SEP-2016 11:46:47 Soil 405235047 19-SEP-2016 11:46:47 Soil 405235048 19-SEP-2016 11:46:47 Soil 405235049 l 9-SEP-2016 11:46:47 Soil 405235050 l 9-SEP-2016 11 :46:47 Soil 405235051 19-SEP-2016 11:46:47 Soil 405235052 19-SEP-2016 11:46:47 Soil 405235053 19-SEP-2016 11:46:47 Soil 405235054 19-SEP-2016 11:46:47 Soil 405235055 19-SEP-2016 11:46:47 Soil 405235056 19-SEP-2016 11:46:47 Soil 405235057 19-SEP-201611:46:47 Soil 405235058 19-SEP-2016 11:46:47 Soil 405235059 19-SEP-2016 11:46:47 Soil 405235060 19-SEP-2016I1:46:47 Soil 1203626109 MB 19-SEP-201611:46:47 Soil 1203626110 DUP (405235041) l 9-SEP-2016 11 :46:47 Soil 1203626111 MS (405235041) 19-SEP-2016 11:46:47 Soil 1203626112 LCS 19-SEP-2016 11:46:47 Soil ReagentJSolvent Lot ID Description Amount 2242305.2 Ecoscint A Scintillation Solution JOmL 2431394.13 16M Nilric Acid Poly Coated Bottle 25mL 2440076.3 Potassium Persulfate 99+% 5g 2440953 RL-0.4M Hydrochloric Acid 50mL 2444293.4 Methanol 4L Plastic Bottle 9mL 2455949 RL-1 M Silver Nitrate 2mL Analytical Logbook version 111--04-2002 TYJ?C Sample Id Descri12tion LCS 1203626112 Carbon-14 SPIKE MS 1203626111 Carbon-14SPIKE Dry or Wet Unadjusted Aliquot Flask# w w w w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) l.273 1.121 l.252 1.115 l.313 l.122 1.361 1.024 1.308 1.015 1.356 1.103 1.305 1.035 1.268 0.978 1.274 1.035 1.358 1.208 1.275 1.05 1.401 J.184 1.277 0.889 1.27 1.039 1.364 1.101 1.33 0.907 1.313 0.957 1.315 1.055 1.259 I.108 1.4 1.265 1.265 1.289 1.135 1.393 1.226 1.265 Comments: Spike Pipet ID: RAD-LSC-2970968 2 3 4 5 6 8 83 84 86 400 402 404 405 406 506 507 514 519 530 706 708 729 733 Data Entry Date2: 26-SEP-2016 14:31 BAL-16107662 Tiffany Jordan Serial Number S12ike Amount S12ike Units 1646-B .l mL 1646-B .l mL GEL Laboratories LLC Filename: C14.XLS File type : Excel Version#: 1.3.10 Batch : 1598081 Analyst: TIF02034 Prep Date : 9/19/2016 Method Uncertainty : 0.0363 Geometry: 3ml Ethanotamine/9ml Methanoi/1 Oml EcoScint A sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Sample Pas. ID G G Date/lime 1 . 405235041 . 1 1.1210 3.3359E-03 11/30/2015 13:27 2 405235042.1 1.1150 3.3353E-03 11/30/2015 13:53 3 405235043.1 1.1220 3.3360E-03 11/30/2015 13:59 4 405235044.1 1.0240 3.3258E-03 11/30/2015 13:50 5 405235045.1 1.0150 3.3249E-03 11/301201514:15 6 405235046.1 1.1030 3.3341E-03 1217/2015 10:02 7 405235047.1 1.0350 3.3270E-03 1217/2015 10:10 8 405235048.1 0.9780 3.3210E-03 1217/2015 13:28 9 405235049.1 1.0350 3.3270E-03 1217/2015 13:33 10 405235050.1 1.2080 3.3450E-03 1217/2015 13:42 11 405235051.1 1.0500 3.3285E-03 1217/201513:02 12 405235052. 1 1.1840 3.3425E-03 1217/2015 13:11 13 405235053.1 0.8890 3.3118E-03 1211/2015 14:24 14 405235054.1 1.0390 3.3274E-03 121212015 14:51 15 405235055. 1 1.1010 3.3338E-03 121212015 14:59 16 405235056.1 0.9070 3.3137E-03 121212015 14:50 17 405235057 .1 0.9570 3.3189E-03 121212015 14:55 18 405235058.1 1.0550 3.3291E-03 1212/2015 15:00 19 405235059.1 1.1080 3.3346E-03 12116/2015 12:26 20 405235060.1 1.2650 3.3509E-03 12116/2015 12:33 21 1203626109. 1 1.2650 3.3509E-03 9119/2016 0:00 22 1203626110.1 1.1350 3.3374E-03 11/30/2015 13:27 23 1203626111.1 1.2260 3.3468E-03 11/30/2015 13:27 24 1203626112.1 1.2650 3.3509E-03 911912016 0:00 Count raw Data Rack Position# 3-2 3-3 3-4 3-5 3-6 3-7 3-8 16-1 16-2 16-3 16-4 16-5 16-6 16-7 16-8 16-9 16-10 16-11 16*12 53-1 53-2 53-3 53-4 53*5 C1598081 Carbon-14 Solid Procedure Code : LSC_14CS Pannname: Carbon-14 Required MDA : 2 pCi/G C-14 Abundance : 1.00 Halflife of Carbon-14 :* 5700.00 years Bkg Counting Count Corrected Count C-14 lime Quench# Gross Bkg lime Bkg Bkg Start Normalization Sample (min.) cpm cpm (min.) Quench# cpm Date/lime Factor Decay 70 233.9 15.19 14.64 70 240.8 15.2382 9/261201616:33 1.00000 1.000 70 233.6 15.57 14.64 70 240.8 15.2663 9/26/2016 17:45 1.00000 1.000 70 236.7 14.6 14.64 70 240.8 14.9846 9/26/2016 18:57 1.00000 1.000 70 233 15.11 14.64 70 240.8 15.3231 912612016 20:09 1.00000 1.000 70 232.4 15.2 14.64 70 240.8 15.3805 9/26/2016 21 :20 1.00000 1.000 70 235.1 15.47 14.64 70 240.8 15.1277 9/26/2016 22:32 1.00000 1.000 70 232.9 14.74 14.64 70 240.8 15.3326 9/26/2016 23:44 1.00000 1.000 70 233.9 14.89 14.64 70 240.8 15.2382 9/27/2016 2:07 1.00000 1.000 70 230.6 14.5 14.64 70 240.8 15.5572 9/27/2016 3:19 1.00000 1.000 70 231.4 14.93 14.64 70 240.8 15.4778 9/27/2016 4:30 ,,.1.00000 1.000 70 232.1 14.83 14.64 70 240.8 15.4095 9/27/2016 5:42 1.00000 1.000 70 232.5 14.83 14.64 70 240.8 15.3709 9/27/2016 6:54 1.00000 1.000 70 232.3 15.9 14.64 70 240.8 15.3901 9/27/2016 8:06 1.00000 1.000 70 232.9 14.44 14.64 70 240.8 15.3326 9/27/2016 9:17 1.00000 1.000 70 235.1 14.41 14.64 70 240.8 15.1277 9/27/2016 10:29 1.00000 1.000 70 231.4 14.47 14.64 70 240.8 15.4778 9/27/201611:41 1.00000 1.000 70 232.8 15.81 14.64 70 240.8 15.3421 9/27/2016 12:53 1.00000 1.000 70 234.8 15 14.64 70 240.8 15.1551 9/27/2016 14:04 1.00000 1.000 70 234.6 15.63 14.64 70 240.8 15.1734 9/27/2016 15:16 1.00000 1.000 70 237.4 14.89 14.64 70 240.8 14.9235 9/27/2016 16:28 1.00000 1.000 70 233.2 14.8 14.64 70 240.8 15.3041 9/27(2016 17:40 1.00000 1.000 70 233 15.7 14.64 70 '240.8 15.3231 9/27 /2016 18:52 1.00000 1.000 70 232 141.11 14.64 70 240.8 15.4192 9(27/2016 20:03 1.00000 1.000 70 232.4 143.73 14.64 70 240.8 15.3805 9/27/2016 21:15 1.00000 1.000 Page 1 C1598081 Plpet, 0.1 ml Stdev : +/* 0.000200 ml Pipet, 0.5 ml Stdev: +/* 0.001000 ml Analytlcal SOP: Gl*RA[)..A-003 Instrument SOP: Gl*RA[)..1-004 Calibration Data Calibration Counted Calibration Due Pos. on Date Date 1 LSCBROWN 6/1/2016 5131/2017 2 LSCBROWN 6/1/2016 5/31/2017 3 LSCBROWN 6/1/2016 5131/2017 4 LSCBROWN 6/1/2016 5/31/2017 5 LSCBROWN 6/1/2016 5131/2017 6 LSCBROWN 6/1/2016 5/31/2017 7 LSCBROWN 6/1/2016 5/31/2017 8 LSCBROWN 6/1/2016 5/31/2017 9 LSCBROWN 6/1/2016 5/31/2017 10 LSCBROWN 6/1/2016 5/31/2017 11 LSCBROWN 6/1/2016 5/31/2017 12 LSCBROWN 6/1/2016 5/31/2017 13 LSCBROWN 6/1/2016 5/31/2017 14 LSCBROWN 6/1/2016 5/31/2017 15 LSCBROWN 6/1/2016 5/31/2017 16 LSCBROWN 6/1/2016 5131/2017 17 LSCBROWN 6/1/2016 5/31/2017 18 LSCBROWN 6/1/2016 5131/2017 19 LSCBROWN 6/1/2016 5131/2017 20 LSCBROWN 6/1/2016 5/31/2017 21 LSCBROWN 6/1/2016 5/31/2017 22 LSCBROWN 6/1/2016 5/31/2017 23 LSCBROWN 6/1/2016 5/31/2017 24 LSCBROWN 6/1/2016 5/31/2017 Detector Detector Efficiency Efficiency Error (cpm/dpm) (cpm/dpm) 0.7692 0.00792 0.7698 0.00792 0.7636 0.00792 0.7710 0.00792 0.7722 0.00792 0.7668 0.00792 0.7712 0.00792 0.7692 0.00792 0.7757 0.00792 0.7741 0.00792 0.7728 0.00792 0.7720 0.00792 0.7724 0.00792 0.7712 0.00792 0.7668 0.00792 0.7741 0.00792 0.7714 0.00792 0.7674 0.00792 0.7678 0.00792 0.7622 0.00792 0.7706 0.00792 0.7710 .0.00792 0.7730 0.00792 0.7722 0.00792 Page2 Background Background Count Rack Start Position# Datemme 3-1 9/26/2016 15:21 3*1 9/2612016 15:21 3-1 9/26/2016 15:21 3*1 9/26/2016 15:21 3*1 9/26/2016 15:21 3*1 9/261201615:21 3*1 9/26/2016 15:21 3-1 9/26/2016 15:21 3-1 9/26/2016 15:21 3-1 9/26/2016 15:21 3-1 9/26/2016 15:21 3*1 9/26/2016 15:21 3-1 9/26/2016 15:21 3*1 9/26/2016 15:21 3*1 9/26/201615:21 3-1 9/26/2016 15:21 3*1 9/26/2016 15:21 3-1 9/26/2016 15:21 3-1 9/26/2016 15:21 3*1 9/26/2016 15:21 3*1 9/26/2016 15:21 3-1 9/26/2016 15:21 3*1 9/26/201615:21 3-1 9/26/2016 15:21 Notes: * -Results are decay corrected to Sample DatefTime * -Reference date for Spike Activity (dpm!ml) is the batch Prep Date * -Spike Nominals are decay corrected to Sample Datemme * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Lever Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 0.8032 0.5671 2 1.1565 -0.0252 1366.51% 2 0.8076 0.5702 2 1.1629 0.1594 218.57% 3 0.8016 0.5659 2 *1.1544 -0.2022 169.04% 4 0.8797 0.6211 2 1.2666 -0.1216 309.49% 5 0.8878 0.6268 2 1.2782 -0.1037 366.21% 6 0.8159 0.5760 2 1.1748 0.1823 193.13% 7 0.8704 0.6145 2 1.2532 -0.3344 110.61% 8 0.9206 0.6500 2 1.3256 -0.2085 188.39% 9 0.8717 0.6154 2 1.2549 -0.5932 61.99% 10 0.7464 0.5270 2 1.0746 -0.2639 120.31% 11 0.8584 0.6060 2 1.2358 -0.3217 113.43% 12 0.7610 0.5373 2 1.0957 --0.2666 121.45% 13 1.0137 0.7157 2 1.11¢95 0.3345 131.13% 14 0.8670 0.6121 2 1.2484 -0.5018 73.07% 15 0.8173 0.5771 2 1.1770 -0.3829 90.52% 16 0.9941 0.7019 2 1.4312 -0.6466 64.91% 17 0.9414 0.6646 2 1.3554 0.2855 142.58% 18 0.8531 0.6023 2 1.2284 -0.0863 423.31% 19 0.8123 0.5735 2 1.1697 0.2418 145.29% 20 0.7109 0.5019 2 1.0238 *0.0157 1945.26% 21 0.7119 0.5026 2 1.0251 -0.2329 130.10% 22 0.7937 0.5603 2 1.1427 0.1941 176.61% 23 0.7352 0.5190 2 1.0585 59.7508 1.46% 24 0.7123 0.5029 2 1.0255 59.1877 1.44% C15980B1 Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCi/G -0.0482 0.6593 0.6751 0.3037 0.6637 0.6828 -0.3846 0.6501 0.6700 -0.2131 0.6594 0.7374 -0.1805 0.6610 0.7446 0.3423 0.6611 0.6902 -0.5926 0.6554 0.7251 -0.3482 0.6561 0.7700 -1.0572 0.6553 0.7207 -0.5478 0.6591 0.6223 -0.5795 0.6573 0.7152 -0.5409 0.6568 0.6345 0.5099 0.6686 0.8597 -0.8926 0.6522 0.7187 -0.7177 0.6496 0.6793 -1.0078 0.6541 0.8225 0.4679 0.6671 0.7979 -0.1551 0.6563 0.7158 0.4566 0.6634 0.6885 -0.0335 0.6526 0.5976 -0.5041 0.6558 0.5939 0.3769 0.6657 0.6717 125.6908 1.4954 1.3933 128.3495 1.5076 1.3627 Page3 1646-B 1/5/2017 1681.40 0.10 1646-B 1/5/2017 1681.40 0.10 2SIGMA Total Prop. Uncertainty pCi/G 0.6751 0.6829 0.6700 0.7374 0.7446 0.6903 0.7251 0.7700 0.7207 0.6223 0.7152 0.6345 0.8601 0.7187 0.6793 0.8225 0.7982 0.7158 0.6887 0.5976 0.5939 0.6719 4.5800 4.5309 Sample QC 405235041. 1 405235041.1 Sample Nominal Type RPO RER pCi/G Recover/ SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP
  • 0.0% MS 61.7831 96.7% LCS 59.8725 98.9%

J[ JD ::: c::: *--::IL IJSE R: 8 PRESET TIME DATA COUNT BUiNK TWO PHASE SCINTILLATOR: LOW LEVEL 1e11z1. ,z, -COMMENT:BROWN H=t-J: IC# NCJ AGlC . 1\10 71zi. 1Z10 CPM f\10 NO LIQUID YES l .. J.JMEX NO H(-iLF LIFE 1.1*51Zt. IZI 'f.EFHWR: IZI" li'.ll?I St=11Y1PLE REPLICRTES CYCLE t:xEPEf.:iTS . " LOW Sf.l!YIPLE F<E,J: CORRECTION DATE= FACTOR: l .. IZllZl1Zlti)IZ10 PA[::lE: 1 2a SEP 2016 15:51 :I. PRINTER ::EDIT 1. :EDIT :l DISK . OFF lZl none BK!3. 0 121. Ji.) *-* 91ZtJZt. tZI 'f.E:RROR: 1z1. IZllZI FACTOR: 1 .. IZllZllZHZl 0121 BKG. SUB: IZt SAM POS TIME H# ._. __ w_ x m':..-.t..Q...:t. __ .. _______ LUMEX ELAPSED NO MIN CPM '}{ERROR CPM %ERROR % TIME *vtJ--i. 2:*-l 7121. l/.)li.I 2<'1.1Z1. 8 14.64 37,. 14 :3Q 92 121. 87 71. 2'1* I *:> ,'3 .. 70. 121121 .. 9 15.19 E,. 13 38030 3.BEi l .. 'i*3 *-i . .., .. ,_, 3 .. -3 7121

  • 121121 G 15.57 E.. 06 37.51 ;3. 91Z1 L 1 ':3 7E 31.1. .3**-Lf. 1Z11Z1 2:36 .. 7 14.60 (:,, 37.66 ;3 .. '30 t. 36 f?86u 2; .. -:5 70. IZllZl QI 15.11 6 .. 15 .36a44 3. 91:., 1217 358.35 2>-EJ 70. 1znz1 lJ* 15.20 6. l 36.69 3n .-, 11 .. 1. 7 c.,. l,7 ... 7 tZI
  • IZI IZI :I. 15. Lt7 6. tZ18 36.76 ., a' ll L :1.1 5tZI 1. 93 .3-8 7tZl. IZllZt ':J 14. 7'+ 61> ;::3 37. J.9 92 :t" 7JZI Page 5337 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 9 8 -7 6 --E 5 ::i 0 () 4 3 2 O-r-.,_,,91 0 Page 5338of5809 100 200 300 26 Sep 2016 15:21:57 26 Sep 2016 16:32:20 S08092603-1 A.XLS U08092603-1A.XLS Log Counts 08 C-14 BROWN LIQUID 1 3-1 70.00 240.8 2643 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 10 9 8 7 6 § 5 0 (.) 4 3 2 0 Page 5339 of 5809 100 200 300 26 Sep 2016 16:33:44 26 Sep201617:44:07 S08092603-2A.XLS U08092603-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 2 3-2 70.00 233.9 2732 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 10 9 -8 7 6 J8 c: 5 ::J 0 () 4 2 26 Sep 2016 17:45:29 26 Sep 2016 18:55:52 S08092603-3A.XLS U08092603-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 3 233.6 100 0 3-3 2675 450 990 SPECTRUM PLOT USER 08 -C-14 70.00 o-1-11 ........ 0 100 200 300 400 500 600 . 700 800 900 Channel Number (Log) Page 5340 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: I H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 12 10 8 E 5 6 -() 4 0 -lmma;-0 Page 5341 of 5809 100 200 300 26 Sep 2016 18:57:15 26 Sep 2016 20:07:37 S08092603-4A.XLS U08092603-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 4 236.7 2693 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 400 500 600 Channel Number (Log) *700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 10 9 8 7 6 -.!!l c 5 -:J 0 (.) 4 3 2 1 0 100 Page 5342 of 5809 200 300 26 Sep 2016 20:09:04 26 Sep 2016 21 :19:27 SOB092603-5A.XLS UOB092603-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 5 233.0 100 0 3-5 2596 450 990 SPECTRUM PLOT USER 08 -C-14 400 500 70.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win 1: C-14 -Start, End: Win2: -Start, End: 9 8 7 6 -en 5 'E ::J 0 (,) 4 0 Page 5343 of 5809 100 200 300 26 Sep 2016 21:20:53 26 Sep 2016 22:31:16 S08092603-6A.XLS U08092603-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 6 232.4 100 0 3-6 2614 450 990 SPECTRUM PLOT USER 08 -C-14 400 500 70.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 12 10 E 5 6 0 0 Page 5344 of 5809 100 200 300 26 Sep 2016 22:32:39 26 Sep 2016 23:43:02 S08092603-7 A.XLS U08092603-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 7 3-7 70.00 235.1 2608 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 9 8 7 -6 (J) 5 -. c: 0 (.) 4 3 -2 1 -26 Sep 2016 23:44:25 27 Sep 2016 00:54:48 S08092703-8A.XLS U08092603-1 A.XLS Log Counts 08 C-14 .. BROWN LIQUID 8 232.9 100 0 3-8 2654 450 990 SPECTRUM PLOT USER 08 -C-14 70.00 0 100 200 300 400 500 600 700 -800 900 Channel Number (Log) Page 5345 of 5809 JC J:) ::: IL...:: -*-:1L *1l.J SE Fh B PHESET TIME DATA CAL.C COUNT BLAN!-\ TWO PHASE SCil\ITILU=Hmx: L.OVJ L.E:VEL 71Zr. 1Z11Z1 CPM ND l\IO LIG1UID YES COMrifENT: BROWN H:tl: : YES I C:IJ: 1\10 AG!C :1 l\IO UJMEX r. l\IO HAU=-LIFE SAMPLE REPEATS: REPLICATES CYCLE REPH-HS : LOVJ SRMPLE r-xE:J CORRECTION DATE: l l. :l IZi PAGE: 1 27 SEP 2016 PRHHEI=< DI Ell-( non<;;> * :EDIT :: OFF CHAl\J: l rZtlZI
  • ILi --.q. 5 rZI.. IZI IZllZI 1 * @z11z11z1 rt) IZI Bl-<G .. I[) CHAN: tZI., 17.J -900 .. 1Z1 IZJ" IZJIZ! :l .. 1z11zuz11z11z11z1 Bl-((:J .. rZI SAM POS TIME H# _____ LUMEX ELAPSED NO MIN CPM %ERROR CPM '%ERROR r. TIME'. g 1 15-'.I. 71z1. IZllZJ 9 14.89 6. ;::0 .. 133 Lc:i 71. 2E\ h *::. 1Ei*-2 70. IZHZI 2:?;121 .. f, 1'1-.50 6. ;::8 36 .. 8L1. ;::; .. 91+ 1n 33 fLf3. 1Z15 ii l.6-3 7121. 1210 231,. Lr. 14.93 6. 19 :-3. '35 1.. 12111. 2j.L!-. 79 II L1. 1 E,-L; 70, IZfli.) 1 14.83 35. 4L* 3.96 1. 1 IZI i:!85. 5 :I. It 1:: ... 1 :l.G*-5 n:1. IZHZI R 5 14.83 E,. ;::'.1 36.26 3.97 :l .. 358tl ;:;7 N 6 1E,*-*6 71Z1. IZHZI 3 15.90 :s. 33.01 .. 88 l. 81 L;30. IZIB -r :LE,-7 70. IZllZI 13 14p44 6" 37.01 3 .. 93 1. 'i*3 51211. 85 I IS 8 1 f,*-*E) 7 IZI
  • IZI IZ! l. 14.41 6. 31Z1 35.61 'i*. IZI 1 1. 29 573>1 IG 9 lE,-9 70. 1Z11Z1 '{* 14.47 6 .. ;=:a 36.27 3. '97 1. 71 6L;5. L1*2 11Ho :L 6--1 IZI 70 .. IZIIZI 8 15.81 6.01 37.36 3. '31 1.. '+8 717. 2l?.1 1.6*-:l.1 71z1. 00 2 .. '3l+. 8 15.00 6. 1.7 36-77 3. 1. 7;::: 7(:\8. 99 1;::.: 16-12 70. 121121 6 15.63 5.05 37.76 3.89 l. L;2 8E:,0. 79 u 1 J' 53-1 70. IZllZI 237 .. '-1* 14.89 6 .. f:'.IZI 35n70 LJ .* li.)12) :l * '33i:! .. E,4 '-' tf ll1. 7 IZI
  • rZllZI *=1*?":'i *::* II J.-14.80 6 .. <:::1 36.21 97 121. 56 11Zt0L1 .* 31.1. .ztJ.!'.:i 53*-.. 3 7 IZl. IZllZl 233" IZI 15.70 E... 03 37. 3.91 1. :l3 l1Zt76. 10 ZJ 16 53..-,:,. 7121. 00 232n flJ 141. 11 .. 121 j_ 164. 1219 L87 f:'.5 11Lr7, 85 lf/1.7 7G'.l. IZ10 i:-::3;:'.. Li* 1lt3. 73 1.. '39 166a49 1. .. 85 1t.i .. 13 li::.!1.9. 55 Page 5346 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14-Start, End: Win2: -Start, End: 10 9 8 7 6 Jg c: 5 -::i 0 0 4 -3 2 -100 Page 5347 of 5809 200 300 27 Sep 2016 02:07:16 27 Sep 2016 03:17:39 S08092716-1 A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 1 16-1 233.9 2631 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 400 500 70.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 9 8 7 6 -Ill 5 -'E ::l 0 (.) 4 3 2 1 0 Page 5348 of 5809 100 200 300 27 Sep 2016 03:19:02 27 Sep 2016 04:29:25 S08092716-2A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 2 16-2 230.6 2621 100 450 0 990 70.00 SPECTRUM PLOT USER 08 -C-14 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 12 10 -8 E ::J 6 -0 (.) 4 2 27 Sep 2016 04:30:46 27 Sep 2016 05:41 :09 S08092716-3A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 3 16-3 70.00 231.4 2618 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 o-Lm,,,,--AllJ_,.""""'.,.,..,..!IElmlsmm ........................ ,.,............,ji..-.,,..,._ii11l>l!lmwlli!lllPltl:izl.d.ri.Ja&,..,,,.J.......AJWl.lolliLIM.mrmm&_..b:mmlm'!mlma 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5349 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number U.j'ler Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14-Start, End: Win2: -Start, End: 8 7 6 . 5 .l!.l § 4 0 0 3 2 27 Sep 2016 05:42:30 27 Sep 2016 06:52:53 S08092716-4A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 4 232.1 100 0 16-4 2588 450 990 SPECTRUM PLOT USER 08 -C-14 70.00 0 100 200 300 400 500 600 700 Channel Number (Log) Page 5350 of 5809 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 12 10 -8 .l!l § 6. 0 () 0 Page 5351 of 5809 100 200 300 27 Sep 2016 06:54:15 27 Sep 2016 08:04:38 S08092716-5A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 5 232.5 100 0 16-5 2596 450 990 SPECTRUM PLOT USER 08
  • C-14 400 500 70.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time:* H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 10 9 -8 7 (/) -c: 5 -::J 0 (.) 4 -3 2 0 0 100 Page 5352 of 5809 200 300 27 Sep 2016 08:06:04 27 Sep 2016 09:16:27 S08092716-6A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 6 232.3 100 0 16-6 2708 450 990 SPECTRUM PLOT USER 08 -C-14 400 500 70.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id -. User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 *Start, End: Win2: -Start, End: 12 10 8 . Ul -c: 6 -::J 0 (.) 4 -2 27 Sep 2016 09:17:51 27 Sep 2016 10:28: 14 S08092716-7 A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 7 16-7 70.00 232.9 2627 100 450 0 990 SPECTRUM PLOT USER 08
  • C-14 0-!mm..,,,,,,,J!Jab.m,llm!IW.,,..,,,,mmt>ll11Wl!mll11ll>ll!llllll<lmm<mll!llWWl!lmlmc:m:mir:IZ?ISDUmmm>l ........ Dmt'l,.,.,..,ml:L.&Lmli<WdmY'l!i.i-........ _..l!lllRll...,., 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5353 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 10 9 7 6 $ c: 5 ::i 0 0 4 2 100 Page 5354 of 5809 200 300 27 Sep 2016 10:29:36 27 Sep 2016 11 :39:59 S08092716-8A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 8 16-8 70.00 235.1 2533 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: Cf) -c: ::I 0 (..) 10. 9 8 -7 6 5 3 0 -0 Page 5355 of 5809 100 200 300 27 Sep 2016 11 :41:24 27 Sep 201612:51:47 S08092716-9A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 9 16-9 231.4 2593 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 . (. 400 500 70.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 9 8 7 6 -E 5 ::J 0 () 4 -3 2 0 Page 5356 of 5809 100 200 300 27 Sep 2016 12:53: 11 27 Sep 2016 14:03:34 S08092716-1 QA.XLS U08092716-1AXLS Log Counts 08 C-14 BROWN* LIQUID 10 232.8 100 0 16-10 2670 450 990 70.00 SPECTRUM PLOT USER 08
  • C-14 400 500 600 Channel Number (log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 10 9 8 7 -6 en -c: 5 ::I 0 {.) 4 -3 2 27 Sep 2016 14:04:58 27 Sep 2016 15:15:21 S08092716-11 A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 11 234.8 100 0 16-11 2613 450 990 SPECTRUM PLOT USER 08 -C-14 70.00 o-m...........Uluml!.lmmom1111JOmmmllll'lllllflmmmmmm:ll!lmtll ................ 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5357 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14-Start, End: Win2: -Start, End: 10 9 8 T-6 -(/) -c ::J 0 0 4 0 100 Page 5358 of 5809 200 300 27 Sep 2016 15:16:46 27 Sep 2016 16:27:09 S08092716-12A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 12 234.6 100 0 16-12 2704 450 990 SPECTRUM PLOT USER 08 -C-14 400 500 70.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User1 Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win 1: C-14 -Start, End: Win2: -Start, End: 12 10 -8 (/J 'E 5 6-{.) 4 2 -27 Sep 2016 16:28:37 27 Sep 2016 17:38:59 S08092753-1 A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 13 53-1 70.00 237.4 2540 100 450 0 990 SPECTRUM PLOT USER 08 -C-14 ...... 1111111 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5359 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 8 7 6 -5 3 2 ball ....... im 0 Page 5360 of 5809 100 200 300 27 Sep 2016 17:40:19 27 Sep 2016 18:50:41 S08092753-2A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 14 53-2 233.2 2581 100 450 0 990 70.00 SPECTRUM PLOT USER 08 -C-14 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 *Start, End: Win2: -Start, End: 10 -9 8 -7 6 (/) 'E 6 5 () 4 -3 2 1 -27 Sep 2016 18:52:05 27 Sep 2016 20:02:27 S08092753-3A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 15 233.0 100 0 53-3 2663 450 990 SPECTRUM PLOT USER 08 -C-14 70.00 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5361 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 60 50 40 -C/l -c: 30 -:J 0 () 20 27 Sep 2016 20:03:50 27 Sep 2016 21:14:12 S08092753-4A.XLS U08092716-1 A.XLS Log Counts 08 C-14 1 BROWN LIQUID 16 232.0 100 0 53-4 11543 450 990 SPECTRUM PLOT USER 08 -C-14 70.00 o-1nimm...,...,,,mn.:a1muummi ....... _,.,,IW'.mlmlmlWll>tll'""'11l>mml""""'"'"""""""'""""Oll?!llma!1llB>l""'"""""""""'""""!Imnlllllm<ll4mlllalMloD!i3twfimmimmo:..-:uam 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5362 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: C-14 -Start, End: Win2: -Start, End: 60 50 -40 (/) "E g 30 -(.) 20 -10 .. 27 Sep 2016 21:15:32 27 Sep 2016 22:25:54 S08092753-5A.XLS U08092716-1 A.XLS Log Counts 08 C-14 BROWN LIQUID 17 232.4 100 0 53-5 11701 450 990 SPECTRUM PLOT USER 08 -C-14 70.00 O 100 200 300 400 500 600 700 800 900 Channel Number {Log) Page 5363 of 5809 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 2010 21-Sep-2016 1-'--'I-'--/ i_ .-;--{ . c;3 Product: __ ,_ ____ .--__,_/_+----Date: 1/zc(cc.g Criteria: Sample Solids are less than or eQual to 100 m<1 for GAB. Samples have been blank corrected (If required). Blank correction rePorted included ((f reauired), If activity less than lOx MDA/MDC, error is less than or equal to 1SO*/o of sample activity, If greater than 10" MDA/ MDC, error is 40°/o or less, If below the MnA / MDC. orrnr Is Instrument source check Is within limits. Instrumont bka check Is within limits. Method RDL/ LLD has been met. If duplicate activities are: Less than s* MDA/ MDC, then RPO is 100% or less, If greater 5" MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reauired RER acceotance criteria. Tracer yield Is 15-1250/o
  • Carrier yield 25-1250/o, (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. /ff*--' *---*** <<" 0::0/o nf '""**** --"'"'*v) sample was run within hold time. Sample was correctlv Preserved if re<1ulred. Smears Taken for Radioactive batches. Method Spike and LCS are within 75-125% for meets the client's mrrnnt,.nc .. criteria\, No blank spaces on data forms. All line outs Initialed and dated * ... _ Aux data is correct. Client Soeclal reaulrements oaae has been checked. Raw Data and I or snectrum are Included and nronerlv statused. MS, LCS, and Duplicate RPD/RER values uploaded to UMS and vpr"1n.C IMI> (If Batch Data Exceotlpn Reports (DER) comnleted If aoolicable. Batch Data Exception Reports (DER) second reviewed. Disposition verified to be completed. Aliauot Correction comoleted If "'"Uired, Review sample historical results if available (If REMP. results above MDC have been verified bv historical results recount or re-analvsis. l Yes No v/". ,/ V' v / i/ 1/ v" /' v v PrlmaryRoviewPerformedBy: Comments ;/tr ;J Ir / v' <:02_ Al Ir ( S.ooOO*<y R***w ff MFY.JitJ ff q/?J 110 v / v ' f -Page 5364 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 -I Jc;i./ (

GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 21-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC HASL-300, Tc-02-RC Solid Batch ID: Sample Numbers: 1597412 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

, 1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040 and 1203624302 were received and analyzed out of the method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 21-SEP-16 Lyndsey Pace 21-SEP-16 Page 1 Page 5365 of 5809 DER Report No.: 1559833 Revision No.: 2 . Type: Process Client Code: MJWC Prep Logbook 3D The Determination of Technetium-99 Using Analytical Grade 1X8 Resin Batch ID: Analyst: 1597412 Christina Sanchez Method: Lab SOP: DOE EML-HASL-300, Tc-02-RC Modified GL-RAD-A-059 REV# 4 Instrument: BAL-16107662 Sample ID Prep Date Matrix 405235021 15-SEP-2016 12:36:17 Soil 405235022 15-SEP-2016 12:36:17 Soil 405235023 15-SEP-2016 12:36:17 Soil 405235024 15-SEP-2016 12:36:17 Soil 405235025 15-SEP-2016 12:36:17 Soil 405235026 15-SEP-2016 12:36:17 Soil 405235027 15-SEP-2016 12:36:17 Soil 405235028 15-SEP-2016 12:36:17 Soil 405235029 15-SEP-2016 12:36:17 Soil 405235030 15-SEP-2016 12:36:17 Soil 405235031 15-SEP-2016 12:36:17 Soil 405235032 15-SEP-2016 12:36:17 Soil 405235033 15-SEP-2016 12:36:17 Soil 405235034 15-SEP-2016 12:36:17 Soil 405235035 15-SEP-2016 12:36:17 Soil 405235036 15-SEP-2016 12:36:17 Soil 405235037 15-SEP-2016 12:36:17 Soil 405235038 15-SEP-2016 12:36:17 Soil 405235039 15-SEP-2016 12:36:17 Soil 405235040 15-SEP-2016 12:36:17 Soil 1203624301 MB 15-SEP-2016 12:36:17 Soil 1203624302 DUP (405235021)
  • 15-SEP-2016 12:36:17 Soil 1203624303 LCS !5-SEP-201612:36:17 Soil Reagent/Solvent Lot ID Description Amount 2280154.26 Hydrogen Peroxide 30% ACS Reagent IOmL 120LBS 30 Golloas 2402130.4 Ecoscint GL Scintillation Solution 15mL 2418926 Quenching Agent .I uL 2429641 RL-0.1 M Hydrochloric Acid IOOmL 2441205 RL-0.0IM Nittlc Acid 20mL 2451825 RL-0.IM Nitric Acid 25mL TC2074-A tracer lmL Analytical Logbook version 111-04-2002 __ _____ LCS 1203624303 Technetium-99SPIKE 1621-B .1 mL --------Dry or Wet Unadjusted Aliquot w w w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) 1.237 1.032 1.273 1.026 1.239 0.% 1.203 0.97 1.23 0.967 1.257 1.048 1.22 0.998 1.313 1.015 1.223 0.987 1.214 0.924 1.271 0.984 1.248 0.994 1.237 1.019 1.242 0.999 1.249 *1.046 1.252 1.03 1.36 1.275 1.232 1.031 1.222 1.116 1.211 1.032 1.275 1.228 1.025 1.275 Comments: Pipet ID: RAD-LSC-2272418 Tracer Pipet ID: RAD-LSC-4099802 GEL Laboratories LLC Filename : TC99.XLS File type : Excel Version#: 1.2.16 Batch: 1597412 Analyst: CHR02061 Prep Date: 9/15/2016 Tc-99 Method Uncertainly : 0.0576 Geometry: 15ml Ecoscint GU5ml DI H20/AG 1x8 Resin Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Sample Pos. ID G G Datemme 1 405235021.1 1.0320 3.3267E-03 1218/2015 14:17 2 405235022.1 1.0260 3.3260E-03 1218/2015 13:43 3 405235023. 1 0.9600 3.3192E-03 121212015 10:40 4 405235024. 1 0.9700 3.3202E-03 121812015 14:13 5 405235025.1 0.9670 3.3199E-03 1218/2015 13:38 6 405235026.1 1.0480 3.3283E-03 12181201510:15 7 405235027 .1 0.9980 3.3231E-03 12181201510:19 8 405235028.1 1.0150 3.3249E*03 11123/2015 14:50 9 405235029.1 0.9870 3.3220E-03 1112312015 11:10 10 405235030.1 0.9240 3.3154E-03 11/23/2015 14:44 11 405235031.1 0.9840 3.3217E-03 11126/201514:25 12 405235032.1 0.9940 3.3227E-03 11/231201511:48 13 405235033.1 1.0190 3.3253E-03 11123/2015 11:53 14 405235034. 1 0.9990 3.3232E*03 11/23/2015 11 :20 15 405235035.1 1.0460 3.3281 E--03 11/2312015 11:06 16 405235036.1 1.0300 3.3265E-03 11123/201511:12 17 405235037.1 12750 3.3519E*03 11/30/2015 11 :19 18 405235038.1 1.0310 3.3266E*03 11/30/2015 10:40 19 405235039.1 1.1160 3.3354E-03 11/30/2015 10:43 20 405235040.1 1.0320 3.3267E*03 11/30/201513:23 21 1203624301.1 1.2750 3.3519E*03 9/15/2016 0:00 22 1203624302.1 1.0250 3.3259E-03 12181201514:17 23 1203624303.1 1.2750 3.3519E-03 9/15/2016 0:00 E1597412 Technetium-99 Solid Tracer SIN: Tracer Exp Date : Tracer Volume Added: Tracer Calculations Tracer Ref. Activity (CPM) 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 35053 Page 1 TC2074*A 911612016 1.00 Tracer Ref. Count Uncertainty (%) 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% 0.93% Tracer Samp. Activity (CPM) 32410 30279 32762 32104 30278 31023 30387 30862 30989 30616. 30727 32089 29362 29577 30348 32013 30537 31276 28425 30164 32123 31072 31945 Procedure Code : LSC99TCS Parmname: Technetium*99 Required MCA : 5 pCi/G Tc-99 Abundance : 1.00 Halflife of Tc-99 : 211100 years Tracer Samp. Count Tracer Tracer Uncertainty Aliquot Aliquot (%) (ml) StDev. (ml) 0.94% 1.0 0.002000 0.95% 1.0 0.002000 0.94% 1.0 0.002000 0.95% 1.0 0.002000 0.95% 1.0 0.002000 0.94% 1.0 0.002000 0.93% 1.0 0.002000 0.95% 1.0 0.002000 0.95% 1.0 0.002000 0.95% 1.0 0.002000 0.95% 1.0 0.002000 0.93% 1.0 0.002000 0.95% 1.0 0.002000 0.95% 1.0 0.002000 0.94% 1.0 0.002000 0.93% 1.0 0.002000 0.94% 1.0 0.002000 0.95% 1.0 0.002000 0.95% 1.0 0.002000 0.94% 1.0 0.002000 0.94% 1.0 0.002000 0.95% 1.0 0.002000 0.94% 1.0 0.002000 Pipe!, 0.1 ml Stdev : +/-0.000200 ml Pipe!, 0.5 ml Stdev : +/-0.001000 mi Pipe!, 1 ml Stdev : +/-0.002000 ml Analytical SOP: GL-RAD-A-059 Instrument SOP: GL-RAD-1-004 Count raw Data Counting Rack Time Quench# Gross Pos. Position# (min.) cpm 1 t7-2 30 185.6 17.77 2 17-3 30 184.4 15.9 3 17-4 30 192.1 17.2 4 17*5 30 180.1 15.97 5 17-7 30 190.5 14.87 6 17-6 30 177.3 16.27 7 17-9 30 189.8 16.67 8 17*8 30 192.7 17.17. 9 17-11 30 163.1 17 10 17-10 30 194.2 16.8 11 17-12 30 211.8 17.03 12 8-1 30 181 16.43 13 8-2 30 171 15.47 14 8-3 30 177.9 15.37 15 8-4 30 173.1 15.33 16 8-5 30 180.1 16.67 17 B-6 30 167 15.53 18 8-7 30 171.1 11.n 19 8-8 30 185.7 15.8 20 8-9 -30 188.1 16.7 21 8-10 30 175.5 14.8 22 8-11 30 185.7 18.43 23 8-12 30 175.2 128.n Bkg Count Corrected Bkg Time Bkg Bkg cpm (min.) Quench# cpm 16.67 30 179.4 16.5602 16.67 30 179.4 16.5765 16.67 30 179.4 16.5092 16.67 30 179.4 16.6543 16.67 30 179.4 16.5161 16.67 30 179.4 16.7222 16.67 30 179.4 16.5203 16.67 30 179.4 16.5075 16.67 30 179.4 16.5968 16.67 30 179.4 16.5053 16.67 30 179.4 16.6631 16.67 30 179.4 16.6355 16.67 30 179.4 16.9285 16.67 30 179.4 16.7065 16.67 30 179.4 16.8511 16.67 30 179.4 16.6543 16.67 30 179.4 17.1011 16.67 30 179.4 16.9246 16.67 30 179.4 16.5589 16.67 30 179.4 16.5333 16.67 30 179.4 16.7733 16.67 30 179.4 16.5589 16.67 30 179.4 16.7825 E1597412 Calculated Calibration Da1a Detector Background Count Sample Sample Calibration Detector Efficiency J. Count Start Sample Recovery Recovery Counted Calibration Due Efficiency Error Background Start Dateflime Decay % Error% on Date Date (cpmldpm) (cpm/dpm) Position# Dateflime 9/20/2016 10:44 1.000 92.5% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5572 0.00792 17-1 9120/2016 10:12 9/20/2016 11:16 1.000 86.4% 0.72% LSCGOLD 7/4/2016 6130/2017 0.5578 0.00792 17-1 9/201201610:12 9/20/2016 11 :48 1.000 93.5% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5530 0.00792 17-1 9/2012016 10:12 9/20/2016 12:20 1.000 91.6% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5594 0.00792 17-1 9/20/201610:12 9/20/2016 13:24 1.000 86.4% 0.72% LSCGOLD 71412016 6130/2017 0.5542 0.00792 17-1 9120/201610:12 9/20/2016 12:52 1.000 88.5% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5600 0.00792 17-1 9/20/2016 10:12 9/20/2016 14:28 1.000 86.7% 0.72% LSCGOLD 7/4/2016 6130/2017 0.5547 0.00792 17-1 9/20/2016 10:12 9/20/201613:56 1.000 88.0% 0.72% LSCGOLD 7/4/2016 6130.12017 0.5526 0.00792 17-1 9/20/201610:12 9/20/2016 15:32 1.000 88.4% 0.72% LSCGOLD 7/412016 6/30/2017 0.5584 0.00792 17-1 9/20/201610:12 9/20/2016 15:00 1.000 87.3% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5513 0.00792 17-1 9/201201610:12 9/20/2016 16:04 1.000 87.7"/o 0.72% LSCGOLD 7/4/2016 6130/2017 0.5303 0.00792 17-1 9120/201610:12 9/2012016 16:36 1.000 91.5% 0.72% LSCGOLD 7/412016 6/30/2017 0.5591 0.00792 17-1 9/20/2016 10:12 9/20/2016 17:08 1.000 63.8% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5601 0.00792 17-1 9/20/2016 10:12 9/20/2016 17:40 1.000 84.4% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5599 0.00792 17-1 9/20/201610:12 91201201618:12 1.000 86.6% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5603 0.00792 17-1 9120/201610:12 9/20/2016 18:44 1.000 91.3% 0.72% LSCGOLD 7/412016 6/3012017 0.5594 0.00792 17-1 9/20/201610:12 9120/2016 19:15 1.000 87.1% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5592 0.00792 17-1 9/20/201610:12 9/20/2016 19:47 1.000 89.2°/o 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5601 0.00792 17-1 9/20/2016 10:12 9/20/2016 20:19 1.000 81.1% 0.72% LSCGOLD 7/412016 613012017 0.5572 0.00792 17-1 9/201201610:12 9/20/2016 20:51 1.000 86.1% 0.72% LSCGOLD 7/4/2016 6/30/2017 0.5558 0.00792 17-1 9/20/2016 10:12 9/20/2016 21:23 1.000 91.6% 0.72% LSCGOLD 7/4/2016 6130/2017 0.5602 0.00792 17-1 9/20/2016 10:12 9/20/2016 21:55 1.000 88.6% 0.72% LSCGOLD 7/4/2016 6/3012017 0.5572 0.00792 17-1 9/20/2016 10:12 9/20/2016 22:27 1.000 91.1% 0.72% LSCGOLD 7/4/2016 6130/2017 0.5602 0.00792 17-1 9120/2016 10:12 Page2
  • '"d Cl> VI {.;.) O'I \0 0 ......, VI 00 0 \0 Notes: 1 -Resulls are decay corrected to Sample Date/Time 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Date/Time * -RPO changed to 0% due to sample & dup activity below MDA Results E1597412 Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpmlml): LCS Volume Added (ml): 2SIGMA NIA NIA NIA NIA 1621-B 1/512017 1911.38 0.10 2SIGMA Decision Critical Required Sample Act. Sample Act. Net Count Net Count Counting Total Prop. Level Level MDA MDA Cone. Error Rate Rate Error Uncertainty Uncertainty PoS. pCi/G pCi/G pCi/G pCi/G pCi/G % CPM CPM pCi/G pCi/G 1 2.0740 1.4643 5 3.0133 1.0250 88.43% 1.2098 1.0697 1.7763 1.7802 2 2.2318 1.5757 5 3.2425 -0.6164 153.80% -0.6765 1.0405 1.8581 1.8581 3 2.2190 1.5666 5 3.2240 0.6271 153.45% 0.6908 1.0600 1.8860 1.8874 4 2.2253 1.5711 5 3.2328 -0.6203 152.39% -0.6843 1.0428 1.8526 1.8526 5 2.3790 1.6796 5 3.4565 -1.6018 62.15% -1.6461 1.0228 1.9507 1.9507 6 2.1335 1.5062 5 3.0992 -0.3921 231.92% -0.4522 1.0487 1.7825 1.7825 7 2.2951 1.6203 5 3.3345 0.1405 702.49% 0.1497 1.0518 1.9350 1.9350 8 2.2297 1.5742 5 3.2397 0.6044 159.93% 0.6625 1.0595 1.8944 1.8957 9 2.2659 1.5997 5 3.2919 0.3728 262.47% 0.4032 1.0583 1.9176 1.9181 10 2.4744 1.7469 5 3.5951 0.2984 357.49% 0.2947 1.0536 2.0907 2.0910 11 2.4183 1.7073 5 3.5131 0.3613 288.81% 0.3669 1.0598 2.0454 2.0458 12 2.1724 1.5337 5 3.1560 -0.1819 510.93% -0.2055 1.0498 1.8218 1.8218 13 2.3322 1.6466 5 3.3874 -1.3742 71.26% -1.4585 1.0392 1.9192 1.9192 14 2.3469 1.6569 5 3.4093 -1.2755 n.38% -1.3365 1.0340 1.9343 1.9343 15 2.1925 1.5479 5 3.1846 -1.3504 68.10% -1.5211 1.0357 1.8022 1.8022 16 2.1016 1.4838 5 3.0531 0.0134 6734.43% 0.0157 1.0540 1.7683 1.7683 17 1.8041 1.2737 5 2.6200 -1.1393 66.39% -1.5711 1.0429 1.4824 1.4824 18 2.1637 1.5276 5 3.1426 0.7390 127.21% 0.8454 1.0754 1.8427 1.8446 19 2.1870 1.6440 5 3.1774 -0.6780 136.86% -0.7589 1.0386 1.8185 1,8185 20 2.2323 1.5761 5 3.2434 0.1522 631.25% 0.1667 1.0525 1.8826 1.8827 21 1.6955 1.1971 5 2.4629 -1.3580 52.00% -1.9733 1.0259 1.3837 1.3837 22 2.1783 1.5379 5 3.1648 1.6649 57.73% 1.8711 1.0800 1.8834 1.8931 23 1.7054 1.2040 5 2.4772 77.4913 2.25% 111.9875 2.2027 2.9874 9.3946 Page3 Sample Sample Nominal QC Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SM1PLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235021.1 DUP
  • 0.0% LCS 67.5279 114.8%

ASSAY 16-Sep-16 12:07:35 id 12 TC99_REC Time limit 500 Count limit 10000 Isotope Tc-99m Protocol date 23-Sep-13 14:21:59 Run id. 18 POS RACK BATCH TIME COUNTS CPM ERROR % RECOVERY COUNT TIME 1 69 1 20 11635 35053.2 0.93 12:07:42 2 69 2 21 11288 32410.1 0.94 92.46 12:08:14 3 69 3 22 11039 30278.6 0.95 86.38 12:08:47 4 69 4 21 11385 32761.6 0.94 93.46 12:09:21 5 69 5 21 11146 32104.2 0.95 91.59 12:09:54 6 81 6 22 10998 30277.5 0.95 86.38 12:10:40 7 81 7 22 11256 31023.1 0.94 88.50 12:11:14 8 81 8 23 11515 30387.3 0.93 86.69 12:11:48 9 81 9 22 11173 30861.5 0.95 88.04 12:12:23 10 81 10 22 11207 30989.3 0.95 88.41 12:12:57 11 74 11 22 11057 30616.1 0.95 87.34 12:13:41 12 74 12 22 11085 30727.3 0.95 87.66 12:14:15 13 74 13 22 11562 32088.8 0.93 91.54 12:14:49 14 74 14 23 11052 29361.5 0.95 83.76 12:15:23 15 74 15 23 11120 29577 0.95 84.38 12:15:58 16 70 16 23 11391 30348.3 0.94 86.58 12:16:47 17 70 17 22 11478 32013.1 0.93 91.33 12:17:22 18 70 18 23 11436 30537.3 0.94 87.12 12:17:56 19 70 19 22 11191 31276.4 0.95 89.23 12:18:31 20 70 20 24 11086 28424.6 0.95 81.09 12:19:05 21 72 21 23 11254 30163.7 0.94 86.05 12:19:55 22 72 22 22 11449 32123.2 0.94 91.64 12:20:29 23 72 23 22 11064 31071.6 0.95 88.64 12:21:03 24 72 24 22 11361 31945.2 0.94 91.13 12:21:37 END OF ASSAY Batch #1597 412 Page 1 of 1 Page 5370of5809 l: D :: Tc::-9*3 USER: 2 PRESET TIME DATA CALC COUNT BLAN!{ TWO PHASE SCINTILLATOR: LOW LEVEL 30.00 CPM NO NO LIQUID NO I S17ttl2 C'OMMENT:GOLD H# :YES IC# : NO AQC * : NO LUMEX:YES HALF LIFE SAMPLE REPEATS: REPLICATES : CYCLE REPEATS : LOW SAMPLE REJ: CORRECTION DATE: 1 1 1 0 PAGE: 1 20 SEP 2016 10:52 PRINTER RS232 DISK none : STD :EDIT : OFF CHAN: 310.0 -635.0 2.00 FACTOR: CHAN: 0.0 -1000.0 2.00 FACTOR: 1.000000 BKG. SUB: 1.000000 BKG. SUB: 0 0 SAM POS NO V.1 17-1 I 2 17-2 'l..-3 17*-3 J 4 17-4 4 5 17-5 r; 6 17-6 /(5 7 17-7 f7 8 17*-8 11..7 9 17-9 //,<1010 17-10 1. tj 11 17-11 ({ 12 17-12 )z_13 8*-1 tJ 14 8-2 ft,( 15 8*-3 K 16 8-4 l&,17 8*-5 /718 8*-6 1!19 8-7 20 8*-8 trJ 21 B-9 Z,I 22 8-10 -t.-v Z3 8-11 'Z.::1 24 8-12 Page *5371 of 5809 TIME H# _ _....W;..;i:;...Cli:::....N .... *=o-.....1 __ MIN 30. 00 179. 4. ' 30.00 185.6 30.00 184.4 30.00 192. 1 30.00 180.1 30.00 177.3 30.00 190.5 30. euzi 192. 7 30.00 189.8 30. '2*0 194. 2 30. 12*0 183. 1 30.00 211.a 30. 00 181. 0 30. 00 171. 0 30.00 177.9 30.00 173.1 30.00 180.1 30.00 167.0 30. 00 1-ri. 1 30.00 185.7 30. 1210 188. 1 30.00 175.5 30.00 185.7 30.00 175.2 CPM CPM 16.67 17.77 15.90 17.20 15.97 16.27 14.87 17.17 16.67 1e..a0 17.00 17.03 16.43 15.47 15.37 15.33 16.67 15 *. 53 17.77 15.80 16.70 14.80 18.43 128.77 8.94 8.G6 9.16 8.80 *9. 1't 9.05 9. lt7 8.81 8. 9't 8.91 8.86 8.85 9.01 9.28 9.31 9.33 8.94 9.26 8.66 9. 19 8.94 9.49 8.50 3.22 40.70 41.83 39.60 39.63 38.97 39.40 41. 03 40.70 41. 00 41.20 42.43 39.07 41.13 40.37 39.30 40.43 41.43 39.50 43.43 39.70 41. 07 40.63 43.37 168.17 5.87 5.88 .6.00 6.01 6.07 6.06 5.91 5.97 5.84 5.94 5.82 6.07 5.87 5.87 6.01 5.91 5.85 5.99 5.70 5.97 5.81 5.87 5.74 2.83 LUMEX 4.90 7.97 6.70 7.15 7.34 8.03 7.29 8.24 4.93 8.50 7.45 7.74 6.10 4.50 bu42 5.70 6.28 6.10 5.59 5.99 4.18 5.04 6.86 t. 19 ELAPSED TIME 31.36 63.34 95.25 127.19 159.13 191. 11 223.08 255.05 286.93 318.93 350.90 382.88 414.91 4'+6. 79 478.73 510.64 542.58 574.49 506.41 638.33 670.18 702.07 734.04 765.94 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 20 Sep 2016 10:12:50 20 Sep 2016 10:43:15 S02092017-1 A.XLS U02092017-1 A.XLS Log Counts 02 GOLD LIQUID 1 17-1 30.00 179.4 1229 310 635 0 990 en "E :J 0 7 6 5 (.) 3 -2 1 """""=-0 Page 5372of5809 100 200 SPECTRUM PLOT USER 02 -TC-99 300 400 500 600 700 *800 900 Channel Number (Log) Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 -.!!1 § 3 0 (.) 2 0 .. ._ __ 0 Page 5373 of 5809 100 200 300 20 Sep 2016 10:44:48 20 Sep 201611:15:14 S02092017-2A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 2 17-2 30.00 185.6 1263 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 *Start, End: Win2: -Start, End: 6 5 4 -.!!1 § 3 8 2 1 t..im-0 Page 5374of5809 100 200 300 20Sep2016 11:16:43 20 Sep 2016 11 :47:09 S02092017-3A.XLS U02092017-1AXLS Log Counts 02 TC-99 GOLD LIQUID 3 184.4 310 0 17-3 1204 635 990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 .fil § 3 0 {) 2 o Page 5375 of 5809 100 200 300 2o Sep 2016 11 :48:39 20 Sep 201612:19:05 S02092017-4A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 4 192.1 310 0 17-4 1189 635 990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 5 en 4 -c: ::l 0 () 3 -2 1 0 -bmlm-0 Page 5376of5809 100 200 300 20 Sep 2016 12:20:36 20 Sep 201612:51:02 S02092017-5A.XLS U02092017-1A.XLS Log Counts 02 TC-99 GOLD LIQUID 5 17-5 30.00 180.1 1169 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99

  • SJart, End: Win2: -Start, End: 7 6 en 4 'E ::i 0 () 3 2 1 bmm ...... <ZU 0 Page 5377 of 5809 100 200 300 20 Sep 2016 12:52:35 20 Sep 2016 13:23:00 S02092017-6A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 6 17-6 30.00 177.3 1190 310 635 0 990 SPECTRUM PLOT USER 02
  • TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: -E :::i 0 7 6 5 03 2 0 -*bmn;-0 Page 5378 of 5809 100 200 300 20 Sep 2016 13:24:33 20 Sep 2016 13:54:58 S02092017-7 A.XLS U02092017-1 A.XLS Log Counts . 02 TC-99 GOLD LIQUID 7 17-7 30.00 190.5 1239 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 . 5 . 4 . .!!1 c: ::i 0 (..) 3 2 1 . 0 **bami->M 0 Page 5379 of 5809 100 200 300 20 Sep 2016 13:56:31 20 Sep 201614:26:57 S02092017-8A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 8 17-8 30.00 192.7 1221 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id . User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 8 7 6 5 (/) -§ 4 0 (.) 3 2 1 0 100 Page 5380of5809 200 300 20 Sep 2016 14:28:24 20 Sep 2016 14:58:49 S02092017-9A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 9 17-9 30.00 189.8 1230 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 5 . 4 -J!l c: ::I 0 (.) 3 2 1 *brmJ-;dfj 0 Page 5381of5809 100 200 300 20 Sep 2016 15:00:24 20 Sep 2016 15:30:49 S02092017-1 QA.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 10 194.2 310 0 17-10 1236 635 990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 . 6 5 CIJ 4 'E ::I 0 () 3 2 1 -Page 5382of5809 100 200 300 20 Sep 2016 15:32:22 20 Sep 2016 16:02:48 S02092017-11A.XLS U02092017-1A.XLS Log Counts 02 TC-99 GOLD LIQUID 11 17-11 30.00 183.1 1241 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: ' Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 5 2 c ::J 0 () 3 -2 0 Page 5383 of 5809 100 200 300 20 Sep 2016 16:04:21 20 Sep 2016 16:34:46 S02092017-12A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 12 17-12 30.00 211.8 1180 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 5 (/) 4 'E :> 0 (..) 3 2 1 -Page 5384of5809 100 . 200 300 20 Sep 2016 16:36:23 20 Sep 2016 17:06:49 S02092008-1 A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 13 8-1 181.0 1242 310 635 0 990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 .IE § 3 0 0 2 0 -"-'t:-0 Page 5385 of 5809 100 200 300 20 Sep 2016 17:08:15 20 Sep 2016 17:38:40 S02092008-2A.XLS U02092017-1 A.XLS Log Counts 02 GOLD LIQUID 14 8-2 171.0 1219 310 635 0 990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id . User Comment Scintillator Sample, Rack-Pos, time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 20 Sep 2016 17:40:12 20 Sep 2016 18:10:37 S02092008-3A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 15 177.9 310 0 8-3 1179 635 990 30.00 ---------*---*---------7 6 -5 4 -2l c: :J 0 (.) 3 2 o-.,_ ...... 0 Page 5386 of 5809 100 SPECTRUM PLOT USER 02 -TC-99 200 300 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 .l!l § 3 -0 u 2 1 r...m.--0 Page 5387 of 5809 100 200 300 20 Sep 2016 18:12:06 20 Sep 2016 18:42:31 S02092008-4A.XLS U02092017-1A.XLS Log Counts 02 TC-99 GOLD LIQUID 16 173.1 310 0 8-4 1253 635 ,990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log)
  • 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 -5 UJ 4 -c :J 0 0 3 --2 1 -Page 5388 of 5809 100 200 -300 20 Sep 2016 18:44:03 20 Sep 2016 19:14:27 S02092008-5A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 17 8-5 180.1 1251 310 635 0 990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 9 8 -7 6 .!!! 5 c:: :::i 0 (.) 4 3 2 Page 5389 of 5809 100 200 300 20 Sep 2016 19:15:57 20 Sep 2016 19:46:23 S02092008-6A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 18 167.0 310 0 8-6 1233 635 990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number {Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id Use( cbmment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 5 C/l 4 "E 5 () 3 2 1 -0 Page 5390 of 5809 100 200 300 20 Sep 2016 19:47:53 20 Sep 2016 20:18:17 S02092008-7 A.XLS U02092017-1A.XLS Log Counts 02 TC-99 GOLD LIQUID 19 8-7 30.00 171.1 1327 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start End: 20 Sep 2016 20:19:48 20 Sep 2016 20:50:12 $02092008-SA.XLS U02092017-1A.XLS Log Counts 02 TC-99 GOLD LIQUID 20 185.7 310 0 8-8 1199 635 990 30.00 ----*--*-----*-----7 6 -5 4 -c :J 0 (.) 3 2 o Page 5391of5809 100 SPECTRUM PLOT USER 02 -TC-99 200 300 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 .!!l § 3 0 0 2 -0 Page 5392 of 5809 100 200 300 20 Sep 2016 20:51:39 20 Sep 2016 21 :22:04 S02092008-9A.XLS U02092017-1 A.XLS Log Counts 02 0TC-99 GOLD LIQUID 21 8-9 30.00 188.1 1240 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number
  • User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 -5 4 -Ja c ::J 0 (..) 3 2-1 *r.-.-* 0 Page 5393 of 5809 100 200 300 20 Sep 2016 21 :23:32 20 Sep 2016 21 :53:58 S02092008-1 QA.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 22 8-10 30.00 t75.5 1227 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack.Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 8 7 -6 5* § 4 0 (,) 3 2 -Page 5394 of 5809 100 200 300 20 Sep 2016 21 :55:30 20 Sep 2016 22:25:56 802092008-11 A.XLS U02092017-1 A.XLS Log Counts 02 TC-99 GOLD LIQUID 23 8-11 185.7 1301 310 635 0 990 30.00 SPECTRUM PLOT USER 02 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample. Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: .l!l c ::i 0 0 30 25 -20 . 15 10. 5 0 _.,.__..,, 0 Page 5395 of 5809 100 200 300 20 Sep 2016 22:27:24 20 Sep 2016 22:57:49 S02092008-12A.XLS U02092017-1A.XLS Log Counts 02 TC-99 GOLD LIQUID 24 8-12 175.2 5061 310 635 0 990 SPECTRUM PLOT USER 02 -TC-99 400 500 30.00 600 Channel Number (Log) 700 800 900 Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 21-Sep-2016 Batch# Product: __ ____ _ Date: Criteria: sample Solids are less than or eaual to 100 ma for GAB. Samples have been blank corrected (if required). Blank correction renorted included (if renulred'* If activity less than 10x MDA/MDC, error is less than or equal to 1SOD/o of sample activity. If greater than 10* MDA/ MDC, error is 400/o or less. [f h-1-w th .. Mnh' ... Instrument source check Is within limits. 1*-strument bkn check is within limits. Method RDL/ LLD has been met. If duplicate activities are: Less than 5* MDA/ MDC, then RPO is 100% or less, If greater 5* MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO Is 00/o, Or meets the client's renulred RER acceotance criteria. Tracer yield Is 15-125%
  • Carrier yield 25-1250/o, (Or meets the client's contract acceptance criteria). Method blank is less than the RDL/ LLD. lru ---' ----*--<" o;;o/n nf *-* .. --* m-tlvltv\ Yes No Comments ;V j}-Yfr , / v ti V' I fQ / GL-CHL-RAD-013 Rev 1 Page 1of1 Samnle was run within hold time. / _.:::Q.12__ tJ <; J12 / ,\ / Samnle was correctlv nreserved if renuired. Smears Taken for Radioactive batches. Method Spike and LCS are within 7S-125% or meets the cll,.nt's contract "Cceotance crl*e*I,.\. No blank spaces on data forms. II.ii line outs initialed and dated. la.1-*---.................... ::illr'11 Aux data Is correct. Client Snecial renuirements nane has been checked. Raw Data and/ or snectrum are Included and oroneriv statused. MS, LCS, and Duplicate RPD/RER values uploaded to UMS and .. n5 vn*l<inA Hit (If n-*-'---*----' *-*-,. ___ **-Batch Data Exceotlon Reoorts fDER) comoieted if annllcable. Batch Data Exception Reports (DER) second reviewed. Dlsnosltion verified to be comnleted. P.finnot Correctlnn comoleterl If renufred. / / / v ../ / Review sample historical results If available J (If REMP, results above MDC have been verified bv historical results recount or re-analvsls.) 1..,-Page 5396 of 5809 lf\/A-IJ A---Iv' tr-V/V GEL Laboratories LLC Form GEL-DER DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 21-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC EPA 906.0 Modified Solid Batch ID: Sample Numbers: 1598072 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, 1203626095 and 1203626096 were received and analyzed out of the method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 21-SEP-16 Lyndsey Pace 21-SEP-16 Page 1 Page 5397 of 5809 DER Report No.: 1559816 Revision No.: 2 Type: Process Client Code: MJWC Batch ID: Analyst: Method: Lab SOP: Instrument: Sample ID 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203626094 MB 1598072 Angela Johnson EPA 906.0 Modified GL-RAD-A-002 REV# 21 BAL-18550299 Prep Date 14-SEP-2016 11:11:07 14-SEP-2016 11:11:07 14-SEP-2016 11:11:07 14-SEP-2016 11:11:07 14-SEP-201611:11:07 J4-SEP-2016 11:11:07 14-SEP-2016 ll:Jl:07 J4-SEP-2016 11:11:07 14-SEP-2016 11:11:07 14-SEP-2016 11:11:07 J4-SEP-2016 11:11:07 14-SEP-201611:11:07 14-SEP-2016 ll:Jl:07 14-SEP-2016 11:11:07 14-SEP-201611:11:07 14-SEP-2016 11:11:07 14-SEP-2016 l l: 11:07 14-SEP-2016 11:11:07 14-SEP-201611:11:07 14-SEP-2016 11:11:07 14-SEP-201611:11:07 1203626095 DUP (405235001) 14-SEP-201611:11:07 1203626096 MS (405235001) 14-SEP-2016 11:11:07 1203626097 LCS 14-SEP-2016 11 :11:07 ReagenUSolvcnt Lot ID Description 2352257.5
  • Ecoscint Ultra Scintillation Solution 2373671 Sodium Hydroxide, Pellet ACS 2418926 Quenching Agent 2447042.3 Ecoscint Ultra Scintillation Solution 2452415 RLwPotassium Pennanganate Analytical Logbook version 111-04-2002 Matrix Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Amount 13mL 2g 20uL 13mL 2mL Prep Logbook The Determination of Tritium Id Description LCS 1203626097 TritiumSPIKE MS 1203626096 TritiumSPIKE Dry or Wet Unadjusted Aliquot w w w w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) 3.928 3.165 4.033 3.J31 3.851 3.182 3.943 3.179 4.247 3.381 3.788 3.049 3.805 2.997 3.777 2.994 3.957 3.022 3.833 3.062 4.103 3.434 3.979 3.304 3.704 2.904 3.881 3.292 3.748 3.48 3.635 2.892 3.692 2.861 3.647 2.856 3.893 3.211 3.764 3.227 J .<<"D 3.137 3.847 Comments: Spike Pipet ID: RAD-LSC-2970%8 Vial Pipet ID: RAD-LSC-8036326 Bkg prepared with dead water: Yes Rig# 2 5 8 9 11 13 15 J6 17 18 20 2J 23 24 25 26 27 28 29 30 3J "* 33 Serial Number 1753-B J753-B Volume Added Aliquot in vial (mL) (mL) 50 10 50 10 50 10 50 10 50 10 50 10 50 10 50 JO 50 10 50 JO 50 10 50 JO 50 10 *50 10 50 JO 50 10 50 10 50 10 50 JO 50 JO 50 10 50 10 50 10 50 JO 96 Spike Amount Spike Units .1 .I mL mL Data Entry Date2: l 9-SEP-2016 05: 15 BAL-18550299 Angela Jolmson GEL Laboratories LLC

'"C (JC/ ('1) Vi w \0 T1598072 \0 0 ......., Tritium Solid Vi 00 Filename : H3DST.XLS 0 \0 File type : Excel Version II: 1.2.13 Batch : 1598072 Analyst : ANGELA095 Procedure Code : LSCDSH3DS Prep Date: 9/1412016 Pannname: Tritium Method Uncertainty : O Required MDA 6 pCi/G H*3 Abundance 1.00 Geometry: Halfllfe of Tritium 12.32 years 10ml DW/13ml Ecoscint Ultra Sample Characteristics Sample Distilled Sample Total Sample Aliquot Sample Counted Sample Sample Aliquot StDev. Counted StDev. Rig Sample Pos. JD Volume (L) G G L L number Date/Time 1 405235001.1 0.0500 3.1650 3.5474E-03 0.0100 1.0000E-05 1 12110/2015 14:20 2 405235002.1 0.0500 3.1310 3.5439E-03 0.0100 1.0000E-05 2 12110/2015 14:30 3 405235003. 1 0.0500 3.1820 3.5492E-03 0.0100 1.0000E-05 5 12110/2015 14:35 4 405235004.1 0.0500 3.1790 3.5489E-03 0.0100 1.0000E-05 8 1219/2015 14:00 5 405235005.1 0.0500 3.3810 3.5697E-03 0.0100 1.0000E-05 9 1211012015 13:15 6 405235006.1 0.0500 3.0490 3.5355E-03 0.0100 1.0000E-05 11 12110/2015 13:25 7 405235007.1 0.0500 2.9970 3.5301E-03 0.0100 1.0000E-05 13 12/10/2015 13:55 8 405235008.1 0.0500 2.9940 3.5298E-03 0.0100 1.0000E-05 15 1211012015 14:05 9 405235009.1 0.0500 3.0220 3.5327E-03 0.0100 1.0000E-05 16 12110/2015 10:30 10 405235010.1 0.0500 3.0620 3.5368E-03 0.0100 1.0000E-05 17 12/1012015 10:35 11 405235011.1 0.0500 3.4340 3.5751E-03 0.0100 1.0000E-05 18 1219/201510:13 12 405235012.1 0.0500 3.3040 3.5617E*03 0.0100 1.0000E-05 20 12/10/2015 11:25 13 405235013.1 0.0500 2.9040 3.5206E-03 0.0100 1.0000E-05 21 1218/201511:23 14 405235014.1 0.0500 3.2920 3.5605E-03 0.0100 1.0000E-05 23 1218/201510:49 15 405235015.1 0.0500 3.4800 3.5798E-03 0.0100 1.0000E-05 24 1218/2015 10:56 16 405235016.1 0.0500 2.8920 3.5193E-03 0.0100 1.0000E-05 25 1218/2015 11 :29 17 405235017.1 0.0500 2.8610 3.5161E-03 0.0100 1.0000E-05 26 12/212015 1 0:02 18 405235018.1 0.0500 2.8560 3.5156E-03 0.0100 1.0000E-05 27 121212015 10:19 19 405235019.1 0.0500 3.2110 3.5522E-03 0.0100 1.0000E-05 28 12/8/201514:30 20 405235020.1 0.0500 3.2270 3.5538E-03 0.0100 1.0000E-05 29 1218/2015 13:50 21 1203626094. 1 0.0500 3.4800 3.5798E-03 0.0100 1.0000E-05 30 9/14/2016 0:00 22 1203626095.1 0.0500 2.5280 3.4818E*03 0.0100 1.0000E-05 31 12110/2015 14:20 23 1203626096.1 0.0500 3.1000 3.5407E-03 0.0100 1.0000E-05 32 12110/2015 14:20 24 1203626097. 1 0.0500 3.4800 3.5798E-03 0.0100 1.0000E-05 33 9/1412016 0:00 Page 1 '"t:I (]) Vl 0 0 0 ......, Vl Pipet, 0.1 ml Stdev: +/-0.000200 ml \0 Pipet, 0.5 ml Stdev: +/-0.001000 ml Pipet, 1.0 ml Stdev: +/-0.002000 ml Plpet, 5.0 ml Stdev : +/-0.010000 ml I Analytical SOP: GL-RAD-A-002 Instrument SOP: GL-RAD-i-004 Count raw Data Counting Rack Time Quench# Gross Pos. Position# (min.) cpm 1 53-2 90 152.6 3.71 2 53-3 90 153.3 4.01 3 53-4 90 153.9 3.53 4 53-5 90 152 4.2 5 53-6 90 154.5 4.01 6 53-7 90 149.8 3.86 7 53-8 90 155.6 3.62 8 53-9 90 153.8 4.08 9 53-10 90 156.7 3.8 10 53-11 90 155.7 3.77 11 31-1 90 155.2 3.89 12 31-2 90 153.7 3.91 13 31-3 90 155 3.86 14 31-4 90 155.1 3.89 15 31-5 90 154.2 3.33 16 31-6 90 156.1 3.56 17 31-7 90 152.7 3.93 18 31-8 90 156.5 3.7 19 31-9 90 156.5 3.77 20 31-10 90 154.8 3.61 21 31-11 90 154.4 3.37 22 31-12 90 156.9 3.74 23 18-1 15 156.1 14.07 24 18-2 15 154.1 15 Bkg Count Bkg Time Bkg cpm (min.) Quench# 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 3.70 90 161.5 T1598072 Calibration Data Detector Background Corrected Count Calibration Detector Efficiency Background Count Bkg Start Sample Counted Calibration Due Efficiency Error Rack Start cpm Date/TI me Decay on Date Date (cpm/dpm) (cpm/dpm) Position# Datemme 3.6844 9/19/2016 13:26 0.957 LSCGREEN 7/1/2016 6/3012017 0.2197 0.00792 53-1 9/19/2016 11 :53 3.6858 9/19/2016 14:59 0.957 LSCGREEN 7/1/2016 6/3012017 0.2184 0.00792 53-1 9/19/2016 11 :53 3.6869 9/19/2016 16:32 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2172 0.00792 53-1 9/19/2016 11 :53 3.6832 9/19/2016 18:05 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2209 0.00792 53-1 9/19/2016 11 :53 3.6881 9/19/2016 19:38 0.957 LSCGREEN 7/112016 6/30/2017 0.2160 0.00792 53-1 9/1972016 11 :53 3.6787 9/19/2016 21:11 0.957 LSCGREEN 71112016 6/30/2017 0.2253 0.00792 53-1 9/19/2016 11 ;53 3.6901 9/19/2016 22:44 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2139 0.00792 53-1 9/19/2016 11:53 3.6867 9/20/2016 0:17 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2174 0.00792 53-1 9/19/2016 11 :53 3.6921 9/20/2016 1 :50 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2118 0.00792 53-1 9/19/2016 11 :53 3.6903 9/20/2016 3:23 0.957 LSCGREEN 7/1/2016 6130/2017 0.2137 0.00792 53-1 9/19/2016 11:53 3.6894 9/20/2016 6:07 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2147 0.00792 53-1 9/19/2016 11:53 3.6865 9/20/2016 7:40 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2176 0.00792 53-1 9/19/201611:53 3.6890 9/20/2016 9:13 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2151 0.00792 53-1 9/19/2016 11 :53 3.6892 9/2012016 10:46 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2149 0.00792 53-1 9/19/2016 11:53 3.6875 9/20/201612:19 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2166 0.00792 53!1 9/19/2016 11:53 3.6910 9/20/2016 13:52 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2129 0.00792 53-1 9/19/2016 11:53 3.6846 9/20/2016 15:25 0.956 LSCGREEN 711/2016 6/30/2017 0.2195 0.00792 53-1 9/19/2016 11:53 3.6917 9/20/2016 16:58 0.956 LSCGREEN 7/1/2016 6/30/2017 0.2122 0.00792 53-1 9/19/2016 11 :53 3.6917 9/20/201618:31 0.957 LSCGREEN 711/2016 6/30/2017 0.2122 0.00792 53-1 9/19/2016 11:53 3.6886 9/20/2016 20:04 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2154 0.00792 53-1 9/19/201611:53 3.6879 9/20/2016 21 :37 0.999 LSCGREEN 7/1/2016 6/30/2017 0.2162 0.00792 53-1 9/191201611:53 3.6924 9/20/2016 23:10 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2114 0.00792 53-1 9/19/2016 11:53 3.6910 9/21/2016 0:42 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2129 0.00792 53-1 9/19/2016 11 :53 3.6873 9/21/2016 0:58 0.999 LSCGREEN 7/1/2016 6/30/2017 0.2168 0.00792 53-1 9/19/2016 11 :53 Page2 0 ......, Vi 00 0 "° Notes: 1 -Results are decay corrected to Sample Datemme 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Datefrime * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 2.2557 1.5925 6 3.2979 0.0866 1120.14% 2 2.2949 1.6202 6 3.3552 1.1158 90.19% 3 2.2707 1.6031 6 3.3198 -0.5343 180.45% 4 2.2338 1.5771 6 3.2659 1.7318 57.28% 5 2.1490 1.5172 6 3.1418 1.0372 90.85% 6 2.2824 1.6114 6 3.3370 0.6212 159.64% 7 2.4492 1.7292 6 3.5807 *0.2573 406.56% 8 2.4112 1.7023 6 3.5252 1.4218 74.70% 9 2.4540 1.7326 6 3.5877 0.3968 267.33% 10 2.3996 1.6941 6 3.5081 0.2867 361.16% 11 2.1301 1.5039 6 3.1142 0.6406 144.64% 12 2.1831 1.5413 6 3.1917 0.7315 130.02% 13 2.5146 1.7753 6 3.6763 0.6446 169.37% 14 2.2203 1.5676 6 3.2461 0.6684 144.51% 15 2.0830 1.4706 6 3.0453 -1.1165 78.11% 16 2.5510 1.8011 6 3.7295 -0.5008 216.67% 17 2.5012 1.7659 6 3.6568 0.9206 118.54% 18 2.5953 1.8323 6 3.7942 0.0322 3460.87% 19 2.3062 1.6282 6 3.3716 0.2705 367.83% 20 2.2589 1.5948 6 3.3024 -0.2662 362.19% 21 1.9987 1.4111 6 2.9221 -0.9525 88.10% 22 2.9394 2.0752 6 4.2973 0.2095 604.06% 23 4.4512 3.1426 6 6.9982 37.0061 9.57% 24 3.7289 2.6326 6 5.8630 33.8073 9.06% T1598072 Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCS SIN: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SJGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCi/G 0.0256 0.2866 1.9008 0.3242 0.2924 1.9725 -0.1569 0.2832 1.8897 0.5168 0.2960 1.9439 0.3219 0.2925 1.8468 0.1813 0.2894 1.9435 -0.0701 0.2850 2.0505 0.3933 0.2938 2.0817 0.1079 0.2885 2.0794 0.0797 0.2879 2.0294 0.2006 0.2902 1.8160 0.2235 0.2905 1.8640 0.1710 0.2896 2.1397 0.2008 0.2902 1.8930 *0.3575 0.2792 1.7092 -0.1310 0.2838 2.1268 0.2454 0.2909 2.1388 0.0083 0.2866 2.1844 0.0783 0.2879 1.9502 -0.0786 0.2848 1.8900 -0.3179 0.2800 1.6447 0.0476 0.2874 2.4806 10.3790 0.9894 6.9146 11.3127 1.0203 5.9761 Page3 1753-8 11/212016 2552.40 0.10 1753-B 11/212016 2552.40 0.10 2SJGMA Tolal Prop. Uncertainty pCi/G 1.9008 1.9726 1.8897 1.9441 1.8468 1.9435 2.0505 2.0818 2.0794 2.0294 1.8161 1.8641 2.1397 1.8930 1.7092 2.1268 2.1388 2.1844 1.9502 1.8900 1.6447 2.4806 6.9397 6.0002 Sample QC 405235001.1 405235001.1 Sample Nominal Type RPD REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP

  • 0.0% MS 38.7131 95.6% LCS 33.0382 102.3%

19 SEP 2016 12:13 PHE:.EiET TI ME DP1TP1 CP1LC COUNT DLP1N !< TL*JO F'HP1:3E SC I NT I LL.P:TDF;: :: LCJ!.'J LEVEL. CPM H# ;YES SAMPLE REPEATS= NO IC# : NO REPLICATES NO AQC : CYCLE REPEATS : LIQUID LUMEX:YES LOW SAMPLE REJ: NO HALF LIFE CORRECTION DATE: :L 1 1 0 DI '.:31< RL*JM L. I En** CHAN: 50.0 -255.0 %ERROR: 2.00 FACTOR: 1.000000 BKG. SUB: 1.000000 8KG. SUB: 0 () CHAN: 0.0 -900.0 %ERROR: 2.00 FACTOR= ALPHA-BETA DISCRIMINATION: NO SPrM F'Cl!:3 TIMI:::: H :M: *******'* ..... . ................. .... :......... L. U MEX EL. P1P El ED l\IO MIN fjf-1 ..... J. ('?() 00 *( 6:1. . .. l " r ... , ... :2 90 00 :!. {: .. J .c .. " " 1-..... ..... 90 .. 00 :t l:!:":I" ,,.c *.. :1 " ..) 4 !:;:.:;r, .... 4 (:;>() " 00 1 ::::; " r:.,;.; LI 1::: !:5 :::; C/() 00 1. 0 \,,I " " !::) .. **t:.1 t)i() 00 l 1::: . " l '? ... -*7 " ()() 149 " u 1 E{ !j::.:: ..... 90 " 00 l " /:) f C) ..... 90 . ()() l .. Ei 1 .1. 0 '.53*****:!.0 <j!() 00 :.l .. , " " ,. £.i) *I :L ..... l :1. C._i!() ()() *I 1:::1;;; '"'}" .,\. " .. \. ... J ,,) n I Page 5402 of 5809 CPM CPI"! '1,, TI ME ::::; " '70 l :J. " .<:J. " 71 1 1. " ::)*::_ti 4 . 01. 10 " HF:l :3;.t.1. ::; . l :!. " 4 . 20 *I("' .. \.,*,) .... , 4 .. I 4 . O:.l. .10 " 9El :::::.(.1. E3b J .. q *I . .. \. " . ..\. 62 1 *I h.1. :::::.ci. " .!. " 4 " OE3 J. 0 " ::::: " i:io :L l u 77 J ., " .l. " **:r " .... l . .. 2El ";!' * ... ' " " ";<' " T7 ":1* " " " 9El **::* .,.,1 " :;:i:;;; **,'!" " .. .:* " !57 **:,* " . __ ). " " f.j.ij. "=!' .. .. 1 " " " ";:r " " " :L4 ::::; " l I"'* () C:>.1:: . 0 6:1. (; <::} t"' ***' 64 0 0 !::>6 0 ti :J. 0 *' *7 C)1 0 /:)6 0 t:;,::::; () .. . " " " ., " " " n " \:i 1. U4 t:lU ElH i"\1;:! CJ , . .f H:l. (:l !7.i Dt::) ::::: 7' l tr *7 <S ij. u :::;; E3 t'.} .. !::.) C) " 7* 1 .t () :? :;:'. h 7 :: STD DFF' :: UFF Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 -7 6 c: 5 ::l 0 () 0 100 Page 5403 of 5809 200 300 19 Sep 2016 11 :53:08 19 Sep 2016 13:23:31 S02091953-1A.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 1 53-1 90.00 161.5 3151 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, iotal Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 . 10 8 E :::i 6 -0 0 4 . 2 0 Page 5404 of 5809 100 200 300 19 Sep 2016 13:26:09

  • 19 Sep 2016 14:56:32 S02091953-2A.XLS U02091953-1 A. XLS Log Counts 02 TRITIUM GREEN LIQUID 2 152.6 50 0 53-2 3142 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: '12 10 8 Ill 'E 5 6-(.) 4 0 0 Page 5405of5809 100 200 300 19 Sep 2016 14:59:08 19 Sep 2016 16:29:32 S02091953-3A.XLS U02091953-1 A.XLS Log Counts 02 TRl!IUM GREEN LIQUID 3 153.3 50 0 53-3 3137 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 14 12 10 -rJ'J 8 -c ::J 0 () 6 -4 2 0 100 200 ---------*---Page 5406 of 5809 300 19 Sep 2016 16:32:08 19 Sep 2016 18:02:32 S02091953-4A.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 4 153.9 50 0 53-4 3095 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: ----*-*----12 10 8 .l1 § 6 -a 0 4 -0 0 Page 5407 of 5809 100 200 300 19 Sep 2016 18:05:12 19 Sep 2016 19:35:35 S02091953-5A.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 5 152.0 50 0 53-5 3108 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number . User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 § 6 8 4 2 -0 0 100 200 300 19 Sep 2016 19:38:13 19 Sep 2016 21 :08:37 S02091953-6A.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 6 53-6 90.00 154.5 3183 50 255' 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 '----------**-------------------*--------* Page 5408of5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id ' User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 Cll c 5 6 (.) 0 0 Page 5409 of 5809 100 200 300 19Sep2016 21:11:15 19 Sep 2016 22:41 :38 S02091953* 7 A.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 7 149.8 50 0 53-7 3067 255 990 SPECTRUM PLOT USER 02 *TRITIUM 400 '500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12. 10 8 -2 § 6 0 (,) 0 Page 5410of5809 100 200 300 19 Sep 2016 22:44:15 20 Sep 2016 00:14:38 S02092053-8A.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 8 155.6 50 0 53-8 3152 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -£l § 6 0 (.) 4 2 0 0 Page 5411 of 5809 100 200 300 20 Sep 2016 00:17:15 20 Sep 2016 01 :47:39 S02092053-9A.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN" LIQUID 9 53-9 90.00 153.8 3046 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 -7 6 (/) -c 5 . ::J 0 (.) 4 3 0 100 Page 5412of5809 200 300 20 Sep 2016 01:50:17 20 Sep 2016 03:20:40 S02092053-1 QA.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 10 53-10 90.00 156.7 3067 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -.!!l § 6 0 () 4 2 0 0 Page 5413 of 5809 100 200 300 20 Sep 2016 03:23:20 20 Sep 2016 04:53:43 S02092053-11 A.XLS U02091953-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 11 53-11 90.00 155.7 3135 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900
IC :c:v ::;: .... !! .... ]: ... ii' ... :11:: U ... J 11""'11 20 SEP 2016 06:27 P1::;;i:;:\:3ET TI ME DP1TP1 CP1!....C COUNT BL.P1NV T!.*JU F'Hf..'.'i\::)E 90 .. 00 CPM H# :YES SAMPLE REPEATS1 ND IC# = NO REPLICATES DI EC I l\IT I 1....1....r1rrn:::: LEl/E::L. NO AQC = NO CYCLE REPEATS a LIQUID LUMEX:YES LOW SAMPLE REJ1 NO HALF LIFE CORRECTION DATE: 1. :.I .. 1 () H\\WI 1.. .. IHT CHAN: 50 .. 0 -255.0* 2 .. 00 FACTOR= CHAN: 0.0 -900.-0 2.00 FACTOR: ALPHA-BETA DISCRIMINATION: NO 1 .. 000000 BKG. SUB: 1.000000 BKG. 0 0 PCJf::l TIME Mll\I ........ .. . .. ............... .. .J\: .... .. .. -* .. ** L UME X E L.P1 P i::: D 1\10 :::::l **** .l ::::;1 .... -6 ::::; :l --*El :;;; 1 *-*!} :::!::!.-*-*:LO :l. :::::..1. ..... .1. 2 Page 5414 of 5809 Cj!() 11 ()() l n ro ()() J. '?' 90,,00 .. 0 <:f() 1: ()() :.L :.t 90 "00 1 r.; () II () () 1 11 :!. 90" 00 l ;::.:;:::" 7 !]I()" 00 1 90" 00 1 *.:. 90 . 00 l ... D ?O ,, 00 1 .* 11. CPM %ERROR CPM %ERROR % TIME .. El9 91 *:l6 "!39 ::::.. 70 .. T7 ::::: II 10 .. ::31 :l l "60 J l. "'7 :l. :l'.? .. 2.1. :.l. :!. " 4:-.:? :;:; " 0 1. 11 (ll') :;;:4. 44 :::::4 H '7 .. 67 0.90 l.00 1. "00 o .. 99 l., i.)/J () l1 1. "20 :.l. :I." 12 0.,94 '=i I* '7 l Ei " =::. :?'?El It t::,(} 74::'.) n tJ2 D:::::t::i. <:;>;:;: II ()0 l " () :l.:l.16 .. .1.:L ::EDIT UF'F ;: OFF Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id . " User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 -7 6 Ill -c 5 -::I 0 () 3 2 0 100 Page 5415of5809 200 300 20 Sep 2016 06:07:20 20 Sep 2016 07:37:43 S02092031-1 A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 1 155.2 50 0 31-1 3198 255 990 SPECTRUM PLOT USER 02
  • TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User CortJment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 7 -6 Ill 'E :::> 0 (.) 3 0 0 100 Page 5416of5809 200 300 20 Sep 2016 07:40:24 20 Sep 2016 09:10:46 S02092031-2A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 2 153.7 50 0 31-2 3209 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 -7 6 -.l!l c: 5 -:J 0 0 4 2 0 -0 100 Page 5417 of 5809 200 300 20 Sep 2016 09:13:27 20 Sep 2016 10:43:50 S02092031-3A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM LIQUID 3 155.0 50 0 31-3 3064 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 7 6 !/) c 5 (.) 3 0 Page 5418of5809 100 200 300 20 Sep 2016 1.0:46:30 20 Sep 2016 12:16:53 S02092031-4A.XLS U02092031-1AXLS Log Counts 02 Tr;uTIUM GREEN LIQUID 4 31-4 155.1 3088 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename . Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 .l!? § 6 0 (.) 4 0 Page 5419of5809 100 200 300 20 Sep 2016 12:19:34 20 Sep 2016 13:49:57 S02092031-5A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 5 31-5 90.00 154.2 3070 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 23 § 6 0 () 4 2 0 0 Page 5420 of 5809 100 200 300 20 Sep 2016 13:52:37 20 Sep 2016 15:23:00 S02092031-6A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 6 31-6 156.1 3058 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id
  • User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 !!l § 6 0 () 4 -0 Page 5421 of 5809 100 200 300 20 Sep 2016 15:25:29 20 Sep 2016 16:55:52 S02092031-7 A.XLS U02092031 *1AXLS Log Counts 02 TRITIUM GREEN LIQUID 7 152.7 50 0 31-7 3098 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id 'User *comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 5 6-(.) 4 -2 0 0 100 20 Sep 2016 16:58:35 20 Sep 2016 18:28:57 S02092031-8A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 8 31-8 156.5 3061 50 255 0 990 90.00 -------------------SPECTRUM PLOT USER 02 -TRITIUM 200 300 400 500 600 700 Channel Number (log) 800 900 '-------------------------------------------' Page 5422 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: c :J 0 () 12 10 0 Page 5423 of 5809 100 200 300 20 Sep 2016 18:31 :42 20 Sep 2016 20:02:04 S02092031-9A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 9 156.5 50 0 31-9 3097 255 990 90.00 *----------------*---, SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 700 800 900 Channel Number (Log)

Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10. 8 § 6-0 (.) 4 2. 0 -0 Page 5424 of 5809 100 200 300 20 Sep 2016 20:04:46 20 Sep 2016 21:35:08 S02092031"1 DA.XLS U02092031-1 A.XLS log Counts 02 TRITIUM GREEN LIQUID 10 154.8 50 0 31-10 3159 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 -8 .la c 6 -::I 0 (.) 4 -2 0 0 100 Page 5425 of 5809 200 300 20 Sep 2016 21 :37:49 20 Sep 2016 23:08:12 S02092031-11 A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 11 31-11 154.4 3065 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment" Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 0 100 Page 5426 of 5809 200 300 20 Sep 2016 23:10:53 21 Sep 2016 00:41 :15 S02092131*12A.XLS U02092031-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 12 156.9 50 0 31-12 3136 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 21 SEP 2016 01:04 TI ME Df'.'1TP1 CP1L.C COUNT BL .. P1l\IK Tlt<JCi P!-l(18E:: I , .. .IT J :: LOh! L.E\iE'.:L CPM H# =YES SAMPLE REPEATS; NO IC# = NO REPLICATES NO AQC 1 NO CYCLE REPEATS LI OU ID L..Ul"IEX :: VE:H L.Ut.'J S(';MPL.E Hl:::,J = NO HALF LIFE CORRECTION DATEc 1 *I l 0 Hl\IM LIHT CHANc 50.0 -255.0 %ERROR: 2.00 FACTOR: CHAN: 0.0 900.0 %ERROR= 2.00 FACTOR: 1.000000 BKG. SUB; 1.000000 BKG. SUB= ALPHA-BETA DISCRIMINATION: ND 0 0 EIP1l"I PDFl TIME MIN I-Hf ............ --. .. ,;tl:::............... .. .................... ..... -.... L. l..J M [;: X F' l\ICl ).) :.l. ll ,. .. '1) .. ::'. J.H****.1 :LH**-2 Page 5427 of 5809 :.l. 1;:: , .. 1 . 1 " 00 *I " .. \. " .i. 00 *I :.l .. t " CPM %ERROR CPM %ERROR % TIME :J.!.j. 0'7 :!.. **::* c72; i.J.:=::. 20 l ""T l 0 :.l. 1;:: u .. ** 1 . " . l " . :J. 00 LS 4t1 '"')' 0 **:1*.N1 :L 1. " " .. I " . * .. :1..i.::. " ::EDIT UF!=- Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 6 5 4 .l!l § 3 8 2 0 100 Page 5428 of 5809 200 300 21 Sep 2016 00:42:20 21 Sep 2016 00:57:42 804092118-1 A.XLS U04092118-1A.XLS Log Counts 04 TRIT1Uf¥1 GREEN LIQUID 1 18-1 15.00 156.1 687 50 255 0 990 SPECTRUM PLOT USER 04 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 5 4 4 3 C/l 3 -..... c: :J 0 () 2 2 1 0 Page 5429 of 5809 100 200 300 21 Sep 2016 00:58:37 21 Sep 2016 01 :13:59 S04092116-2A.XLS U04092116-1A.XLS Log Counts 04 TRITIUM GREEN LIQUID 2 18-2 154.1 707 50 255 0 990 15.00 SPECTRUM PLOT USER 04 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 ___ _ Date: Criteria: Yes No Comments Samole Solids are less than or equal to 100 mq for GAB. rJ/J>--* samples have been blank corrected (If required). }//)--Blank correction renorted included lif renulred'. If activity less than 10x MDA/MDC, error Is less / than or equal to 1500/o of sample activity. If greater than 10* MDA/ MDC, error Is 400/o or less. If he*-*** ... _ unA' MOr Arrnr le nkau. Instrument source check Is within limits. v/ Instrument hkn check la within limits. Method RDL/ LLD has been met. v If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 1000/o or less, v If greater 5* MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reauired RER accentance criteria. Tracer yield Is 15-1250/o

  • Carrier yield 25-1250/o. Ir (Or meets the client's contract acceptance criteria). Method blank is less than the RDL/ LLD. / lrTf --" ----*--; 501-nf *-.. *--* Samnle was run within hold time. ,/ Samnle was correctlv Dreserved If reouired. / Smears Taken for Radioactive batches. IJ/(}-Method Spike and LCS are within 75-1250/o or meets the client's contract accentanoo" criteria), No blank spaces on data forms. All line outs Initiated and dated * ... _ '"" ---------Aux data Is correct. ;V (J-' Client Sneclal reoulrements naae has been checked. t,/ v Raw Data and I or snectrum are Included and nronerlv statused. MS, LCS, and Duplicate RPD/RER values uploaded to UMS and *-* .. --., __ ,.,_ .. .... (if pl /}-n-*-,. --*-*--' *-*n v--* Batch Data Excentlon Renorts fDER' comoleted if annlfcable. !JvK Batch Data Exception Reports (DER) second reviewed. v/ vElL* Dlsnosltinn verified to be comnleted. Allnunt rorroc*lon comnleted If reoulred. pf ;fo-' Review sample historical results If available v Cif REMP, results above MDC have been verified bv historical results recount or re-analvsls. l _ ,.-Page 5430 of 5809 GL-CHL-RAD-013Rev1 Page 1 of 1 0 'LfZ -).<Jo]! L{ O GEL Laboratories LLC Form GEL-DER . DATA EXCEPTl6N REPORT Mo.Day Yr. Division: Quality Criteria: 30-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC EPA 906.0 Modified Solid Batch ID: Sample Numbers: 1598096 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075,405235076,405235077,405235078, 1203626153,and 1203626154 were received and analyzed out of the method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 30-SEP-16 Lyndsey Pace 30-SEP-16 Page 1 Page 5431 of 5809 DER Report No.: 1563148 Revision No.: 2 Type: Process Client Code: MJWC Batch ID: Analyst: Method: Lab SOP: Instrument: Sample ID 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203626152 MB 1598096 Terry Phillips EPA 906.0 Modified GL-RAD-A-002 REV# 21 LSC-J93763 Prep Date 26-SEP-201606:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30: 12 26-SEP-201606:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-201606:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30:12 26-SEP-2016 06:30: 12 26-SEP-201606:30:12 26-SEP-2016 06:30:12 1203626153 DUP (405235061) 26-SEP-201606:30:12 1203626154 MS (405235061) 26-SEP-201606:30:12 1203626155 LCS 26-SEP-2016 06:30:12 ReagenUSolvent Lot ID Description 2352257.5 Ecoscint Ultra Scintillation Solution 2373671 Sodium Hydro.<ide, Pellet ACS 2418926 Quenching Agent 2447042.3 Ecoscint Ultra Scintillation Solution 2457153 RL*Potassium Permanganate Analytical Logbook \*ersion l Matrix Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Amount 13mL 2g 20uL 13mL 2mL Prep Logbook The Determination of Tritium TYJ>C Sample ld Description LCS 1203626155 Tritium SPIKE MS 1203626154 Tritium SPIKE Dry or Wet Unadjusted Aliquot w w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) 3.35 2.761 3.32 2.677 3.39 3.034 3.35 3.077 3.37 3.031 3.43 3.111 3.44 2.963 3.43 2.954 3.37 3.012 3.33 2.702 3.3 2.754 3.38 3.104 3.46 2.806 3.34 2.983 3.39 3.026 3.31 2.63 3.4 3.063 3.33 2.793 3.111 3.4 2.802 3.43 2.827 3.111 Comments: Spike Pipet ID: RAD-LSC-2970968 Vial Pipet ID: RAD-LSC-8036326 Bkg prepared with dead water: Yes Rig# 33 37 38 40 43 44 45 46 48 49 51 S2 S6 57 60 65 66 67 69 70 71 82 Serial Number 1753-B 1753-B Spike Amount SP!)::e Units .1 rnL .l mL Volume Added Aliquot in \ial (mL) (mL) 50 10 50 10 50 10 50 10 50 10 50 10 50 10 so 10 50 10 50 10 50 10 50 10 50 10 50 10 50 JO 50 10 50 10 50 10 50 10 so 10 50 10 50 10 GEL Laboratories LLC

"'C Pl (IQ (p Vl .j::.. '->.) T1598096R '->.) 0 ......., Tritium Solid Ul 00 Filename : H3DST.XLS 0 \0 File type : Excel Version#: 1.2.13 Batch : 1598096 Analyst: TER02081 Procedure Code : LSCDSH3DS Prep Date : 9/26/2016 Parmname: Tritium Method Uncertainty : O Required MCA 6 pCi/G H-3 Abundance 1.00 Geometry: Halflife of Tritium 12.32 years 10ml DW/13ml Ecoscint Ultra Sample Characteristics Sample Distilled Sample Total Sample Aliquot Sample Counted Sample Sample Aliquot S!Dev. Counted StDev. Rig Pos. ID Volume(L) G G L L number Dalemme 1 405235061.1 0.0500 2.7610 3.5058E-03 0.0100 1.0000E-05 33 12114/2015 13:47 2 405235062.1 0.0500 2.6770 3.4971E-03 0.0100 1.0000E-05 37 12114/201513:10 3 405235063.1 0.0500 3.0340 3.5340E-03 0.0100 1.0000E-05 38 12114/201513:15 4 405235064.1 0.0500 3.0770 3.5384E-03 0.0100 1.0000E-05 40 12114/2015 13:25 5 405235065.1 0.0500 3.0310 3.5336E-03 0.0100 1.0000E-05 43 12114/2015 13:56 6 405235066.1 0.0500 3.1110 3.5419E-03 0.0100 1.0000E-05 44 12114/201514:00 7 405235067.1 0.0500 2.9630 3.5266E-03 0.0100 1.0000E-05 45 12111/201511:30 8 405235068.1 0.0500 2.9540 3.5257E-03 0.0100 1.0000E-05 46 12111/201510:27 9 405235069.1 0.0500 3.0120 3.5317E-03 0.0100 1.0000E-05 48 12116/2015 12:45 10 405235070.1 0.0500 2.7020 3.4997E-03 0.0100 1.0000E-05 49 12111/2015 10:10 11 405235071.1 0.0500 2.7540 3.5051E-03 0.0100 1.0000E-05 51 12111/201510:25 12 405235072.1 0.0500 3.1040 3.5412E-03 0.0100 -1.0000E-05 52 12115/2015 13:35 13 405235073.1 0.0500 2.8060 3.5104E-03 0.0100 1.0000E-05 56 12111/201511:35 14 405235074.1 0.0500 2.9830 3.5287E-03 0.0100 1.0000E-05 57 12115/2015 14:10 15 405235075.1 0.0500 3.0260 3.5331E-03 O.o100 1.0000E-05 60 12116/2015 9:31 16 405235076.1 0.0500 2.6300 3.4923E-03 0.0100 1.0000E-05 65 12111/2015 14:19 17 405235077. 1 0.0500 3.0630 3.5369E-03 0.0100 1.0000E-05 66 12117/2015 13:30 18 405235078.1 0.0500 2.7930 3.5091E-03 0.0100 1.0000E-05 67 12117/2015 12:40 19 1203626152.1 0.0500 3.1110 3.5419E-03 0.0100 1.0000E-05 69 9/26/2016 0:00 20 1203626153.1 0.0500 2.8020 3.5100E-03 0.0100 1.0000E-05 70 12114/2015 13:47 21 1203626154.1 0.0500 2.8270 3.5126E-03 0.0100 1.0000E-05 71 12114/2015 13:47 22 1203626155.1 0.0500 3.1110 3.5419E-03 0.0100 1.0000E-05 82 9/26/2016 0:00 Page 1 "'d (!) Vl w 0 ......., Vl gg Pipe!, 0.1 ml Stdev : +/-0.000200 ml \0 Plpet, 0.5 ml Stdev: +/* 0.001000 ml Plpet, 1.0 ml Stdev: +/-0.002000 ml Pipet, 5.0 ml Stdev : +/* 0.010000 ml l Analytical SOP: GL-RAD-A-002 Instrument SOP: GL-RAD-1-004 Count raw Data Counting Rack Time Quench# Gross Pos. Position# (min.) cpm 1 17-2 90 152.8 3.54 2 17-3 90 155.4 3.66 3 17-4 90 154.8 3.89 4 17-5 90 154.7 3.38 5 17-6 90 155.6 3.72 6 17-7 90 153.6 3.8 7 17-8 90 179.3 3.71 8 17-9 90 154.5 3.91 9 14-1 90 152.9 4.01 10 14-2 90 158 3.76 11 14-3 90 174.9 3.36 12 14-4 90 153.7 3.6 13 14-5 90 154.6 3.68 14 14-6 90 154.1 3.88 15 14-7 90 156.1 3.37 16 14-8 90 156.7 4.1 17 14-9 90 154.6 3.61 18 14-10 90 157.4 3.66 19 14-11 90 154.7 3.5 20 14-12 90 154.1 3.78 21 21-1 15 153.6 12.53 22 53-1 15 153.9 13.53 Bkg Count Corrected Bkg Time Bkg Bkg cpm (min.) Quench# cpm 3.39 90 160.3 3.3767 3.39 90 160.3 3.3816 3.39 90 160.3 3.3805 3.39 90 160.3 3.3803 3.39 90 160.3 3.3820 3.39 90 160.3 3.3782 3.39 90 160.3 3.4116 3.39 90 160.3 3.3799 3.39 90 160.3 3.3769 3.39 90 160.3 3.3862 3.39 90 160.3 3.4081 3.39 90 160.3 3.3784 3.39 90 160.3 3.3801 3.39 90 160.3 3.3792 3.39 90 160.3 3.3829 3.39 90 160.3 3.3840 3.39 90 160.3 3.3801 3.39 90 160.3 3.3852 3.39 90 160.3 3.3803 3.39 90 160.3 3.3792 3.39 90 160.3 3.3782 2.67 15 156.6 2.6650 T1598096R Calibration Data Detector Background Count Calibration Detector Efficiency -Background Count Start Sample Counted Calibration Due Efficiency Error Rack Start Date/Time Decay on Date Date (cpmldpm) (cpm/dpm) # Date/Time 9/26/2016 13:35 0.957 LSCGREEN 7/1/2016 6130/2017 0.2193 0.00792 17-1 9/26/2016 12:02 9/26/2016 15:10 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2143 0.00792 1.7-1 9/26/2016 12:02 9/26/2016 16:43 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2154 0.00792 17-1 9/26/2016 12:02 9/261201618:17 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2156 0.00792 17-1 9/26/2016 12:02 9/26/2016 19:50 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2139 0.00792 17-1 9/26/2016 12:02 9/26/2016 21 :23 0.957 LSCGREEN 711/2016 6/30/2017 0.2178 0.00792 17-1 9/26/2016 12:02 9/2612016 22:58 0.956 LSCGREEN 7/1/2016 6/30/2017 0.1707 0.00792 17-1 9/26/2016 12:02 9/27/2016 0:32 0.956 LSCGREEN 7/112016 6/30/2017 0.2160 0.00792 17-1 9/26/2016 12:02 9/27/2016 3:16 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2191 0.00792 17-1 9/2612016 12:02 9/27/2016 4:50 0.956 LSCGREEN 7/1/2016 6/30/2017 0.2093 0.00792 17-1 9/26/201612:02 9/27/2016 6:25 0.956 LSCGREEN 7/1/2016 6/30/2017 0.1783 0.00792 17-1 9/26/2016 12:02 9/27/2016 7:58 0.957 LSCGREEN 7/112016 6/30/2017 0.2176 0.00792 17-1 9/26/2016 12:02 9/27/2016 9:32 0.956 LSCGREEN 7/1/2016 6/30/2017 0.2158 0.00792 17-1 9/26/2016 12:02 9/27/201611:06 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2168 0.00792 17-1 9/26/2016 12:02 9/27/2016 12:39 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2129 0.00792 17-1 9126/2016 12:02 9/27/2016 14:13 .0.956 LSCGREEN 711/2016 6/30/2017 0.2118 0.00792 17-1 9/26/2016 12:02 9/27/2016 15:47 0.957 LSCGREEN 7/1/2016 6130/2017 0.2158 0.00792 17-1 9/26/2016 12:02 9/27/2016 17:21 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2104 0.00792 17-1 9/26/2016 12:02 9/27 /2016 18:54 1.000 LSCGREEN 7/1/2016 6/30/2017 0.2156 0.00792 17-1 9/26/2016 12:02 9/27/2016 20:28 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2168 0.00792 17-1 9/26/2016 12:02 9/27/2016 21:59 0.957 LSCGREEN 7/1/2016 6/30/2017 0.2178 0.00792 17-1 912612016 12:02 9/29/2016 8:14 0.999 LSCGREEN 7/1/2016 6/30/2017 0.2172 0.00792 53-3 9/29/2016 8:30 Page2 Notes: 1 -Results are decay corrected to Sample Datemme 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Datemme * -RPD changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 2.4810 1.7516 6 3.6328 0.6349 169.74% 2 2.6212 1.8506 6 3.8380 1.1425 100.48% 3 2.3000 1.6238 6 3.3676 1.8350 55.79% 4 2.2657 1.5996 6 3.3175 -1.119E-03 86905.89% 5 2.3195 1.6376 6 3.3962 1.2274 83.11% 6 2.2183 1.5661 6 3.2481 1.4655 66.96% 7 2.9674 2.1091 6 4.3735 1.3895 94.27% 6 2.3569 1.6640 6 3.4511 1.9565 53.70% 9 2.2759 1.6066 6 3.3324 2.2575 45.26% 10 2.6623 1.8796 6 3.8981 1.5570 75.39% 11 3.0754 2.1712 6 4.5023 -0.2308 569.82% 12 2.2252 1.5710 6 3.2582 0.7723 125.67% 13 2.4837 1.7535 6 3.6367 1.1663 93.40% 14 2.3241 1.6408 6 3.4030 1.8229 56.71% 15 2.3337 1.6476 6 3.4170 -0.0471 2126.64% 16 2.7022 1.9078 6 3.9566 3.0283 40.28% 17 2.2733 1.6049 6 3.3285 0.8183 121.24% 18 2.5589 1.8066 6 3.7467 1.1005 101.81% 19 2.1446 1.5141 6 3.1401 0.4019 231.02% 20 2.4747 1.7472 6 3.6236 1.5535 70.37% 21 4.5677 3.2248 6 7.2146 35.0005 10.24% 22 4.6321 3.2703 6 7.2075 36.2347 9.60% T1598096R Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Net Count Rate CPM 0.1633 0.2784 0.5095 -0.0003 0.3380 0.4218 0.2984 0.5301 0.6331 0.3738 -0.0481 0.2216 0.2999 0.5008 -0.0129 0.7160 0.2299 0.2748 0.1197 0.4008 9.1518 10.8650 Spike Volume Added: LCSSIN: LCS Exp Date ; LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA Net Count Counting Rate Error Uncertainty CPM pCi/G o.2n2 2.1121 0.2797 2.2499 0.2842 2.0063 0.2741 1.9059 0.2809 1.9993 0.2624 1.9234 0.2813 2.5674 0.2646 2.0589 0.2865 2.0022 0.2818 2.3005 0.2742 2.5779 0.2785 1.9023 0.2801 2.1351 0.2840 2.0261 0.2739 1.9613 0.2884 2.3903 0.2787 1.9445 0.2798 2.1958 0.2765 1.8199 0.2820 2.1426 0.9343 7.0032 1.0391 6.7920 Page3 1753-B 11/2/2016 2547.68 0.10 1753*8 11/2/2016 2547.68 0.10 2 SIGMA Total Prop. Uncertainty pCi/G 2.1121 2.2500 2.0065 1.9059 1.9994 1.9235 2.5675 2.0592 2.0025 2.3007 2.5n9 1.9023 2.1352 2.0264 1.9613 2.3908 1.9445 2.1959 1.8199 2.1427 7.0255 6.8165 Sample QC 405235061.1 405235061.1 Sample Nominal Type RPO RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP

  • 0.0% MS 42.4256 82.5% LCS 36.8886 96.2%

Instrument Type Data Capture Date User Filen,.ame User Number User Id User Comments Scintillator Choice: Sam Rack Time H# 1)¥1-1 17-1 90.00 160.3 ) 2 17-2 90.00 152.8 l-3 17-3 90.00 155.4 j4 17-4 90.00 154.8 4 5 17-5 90.00 154.7 .s 6 17-6 90.00 155.6 C,,7 17-7 90.00 153.6 1a 17-8 90.00 179.3 <{ 9 17-9 90.00 154.5 Page 5436 of 5809 Filename: 4:05 AMab LS 6000 26 Sep 2016 11 :58:54 C:\LSCCAPTURE\BROWN\USER02\UN092£;!01.BSF 2 TRITIUM GREEN LIQUID Raw Raw CPM2 CPM lso1 %Err1 CPM lso2 %Err2 LumEx EITime 5.54 36.87 3.39 14.65 34.74 3.68 4.77 '93.17 5.18 35.72 3.54 13.54 34.03 3.70 3.89 186.67 10.56 41.40 3.66 18.75 34.36 3.95 14.36 281.18 7.08 36.97 3.89 14.43 33.68 3.81 7.41 375.07 4.26 35.46 3.38 12.88 34.58 3.63 2.07 468.34 4.62 35.06 3.72 12.18 34.16 3.65 2.17 561.63 4.47 34.98 3.80 11.73 34.30 3.64 1.65 654.82 15.61 47.49 3.71 22.47 34.87 4.17 23.39 749.97 6.91 37.40 3.91 14.18 34.39 3.75 6.73 843.81 Page 1 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total* Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 I/) "E 5 6 (..) 4 '2 -,o Page 5437 of 5809 100 200 300 26 Sep 2016 12:02:04 26 Sep 2016 13:32:27 S02092617-1A.XLS U02092617-1A.XLS Log Counts 02 TRITIUM GREEN LIQUID 1 17-1 90.00 160.3 3192 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 en c 5 6-() 0 Page 5438 of 5809 100 200 300 26 Sep 2016 13:35:34 26 Sep 2016 15:05:57 S02092617-2A.XLS U02092617-1AXLS Log Counts 02 TRITIUM GREEN LIQUID 2 152.8 50 0 17-2 3114 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 -8 § 6 0 (.) 2 0 Page 5439 of 5809 100 200 300 26 Sep 2016 15:10:05 26 Sep 2016 16:40:27 S02092617-3A.XLS U02092617-1A.XLS Log.Counts 02 TRITIUM GREEN LIQUID 3 17-3 90.00 155.4 3282 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type . User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 --E ::J 6 0 0 2 0 Page 5440of5809 100 200 300 26 Sep 2016 16:43:58 26 Sep 2016 18:14:21 S02092617-4A.XLS U02092617-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 4 17-4 154.8 3081 50 255 0 990 . 90.00 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 . 8 -7 6 . !!3 c: 5 0 (.) 4 3 2 0 100 Page 5441of5809 200 300 26 Sep 2016 18:17:14 26 Sep 201619:47:37 S02092617-5A.XLS U02092617-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 5 17-5 90.00 154.7 3163 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id

  • User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 . 8 7 . 6. Cll 'E 5 ::J 0 (.,) 4 0 0 100 Page 5442 of 5809 200 300 26 Sep 2016 19:50:32 26 Sep 2016 21:20:54 S02092617-6A.XLS U02092617-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 6 17-6 90.00 155.6 3127 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 800 900 Sample Count Sta.rt Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: -E :::> 0 (.) 14 12 10 -8 0 Page 5443 of 5809 100 200 300 26 Sep 2016 21 :23:43 26 Sep 2016 22:54:06 S02092617-7A.XLS U02092617-1 A.XLS Log Counts 02 GREEN LIQUID 7 153.6 50 0 17-7 3143 255 990 SPECTRUM PLQT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum TYpe User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 5 6 (_) 4 -2 26 Sep 2016 22:58:52 27 Sep 2016 00:29:14 802092717-BA.XLS U02092617-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 8 179.3 50 0 17-8 3209 255 990 SPECTRUM PLOT USER 02 -TRITIUM 90.00 ....... lV.llllllF.llmllmmm:um.....,.,..-,'!'Dlll!..,,,.,mmll""""""""""""'umm...m.Dllli:!lll>!illJilS!lmla:mu""""'mum,_,,. 0 100 200 300 400 500 600 700 800 900 Channel Number (Log) Page 5444 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 § 6 0 0 0 0 Page 5445 of 5809 100 200 300 27 Sep 2016 00:32:43 27 Sep 2016 02:03:04 S02092717-9A.XLS U02092617-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 9 17-9 90.00 154.5 3147 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 27 SEP 2016 03:36 :: 2 ' TI ME Di-:YTP1 CP1l...C ; , COUNT 'Tl\IU PHP1f.3E l.. .. E'vEL. 90 .. 00 \\ID NO L.. I Gll..J l D i\ICl H# 1YES SAMPLE REPEATS1
  • IC# : NO REPLICATES AQC : ND CYCLE REPEATS = LLIMEX:YES LOW SAMPLE REJ= HALF LIFE CORRECTION DATE: *I .. t ., .. \. () r**, ,,:;. .. ::. flh!i*tI L.. I none': CHP1i\l " n 0 !:5 !:=1 " 0 r:;: on " '..2 " ()(> FP'1CTCIF;; " " 1.000000 BKG .. SUB: .. ' .. ) CH!1N " 0 " () ..... 900 " 0 'X.EHHClH " " ALPHA-BETA DISCRIMINATIDN1 NO GN1 f::*CJB 1\1[) *1 .cj' ...... I I(. ... 14 .... :;;; 14 ..... 4 1.4*-*6 1.f.!.***] 14 .... *H 14 ..... (:ii 14 ..... 10 14*-.. :l.l :L4 .. **12 Page 5446 of 5809 Til'1E MIN 70" 00 1. 'jlj. "6 90 "00 :L .1. *:jl(l " 00 :.l ::.'16 " J r')1 (> ,, (} (} l *7 &I l:1. ll ()() l " 7* 9C> II()() :.L " :1. 4 .. 10 " :L 3.66 II .. 78 00 F'(rCTDn lH .. :.t:::::,,9:::: 1.4 .. :LO :l.4 .. 70 :l4 .. *1*4 14 .. 9'.:::: J.f.!. .. " " 1.000000 BKG. SUB: '7"1 II }' CJ II :l. 7 6 69 a, C;> () l:.L" '52 .f.j. 11 6 II 1::>7 {:°:-, 11 0 l f f; : 2H:.L .. 02 !::1 p t:.) '? -4 (:":) EJ.f.1-:::;;. J.9 9:37" 04 :.l. () :;:: 0 * '7 ::::: :: 8TD ::E::DJT 01::*F :: CiFF Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id ., ' User Comment Scintillator Sample, Rack-Pos,. Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 § 6-0 (.) 4 0 Page 5447 of 5809 100 200 300 27 Sep 2016 03:1.6:51 27 Sep 2016 04:47:15 S02092714-1 A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 1 152.9 50 0 14-1 3228 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium
  • Start, End: Win2: -Start, End: 12 10 8 2 § 6-0 (.) 4 2 0 0 Page 5448of5809 100 200 300 27 Sep 2016 04:50:47 27 Sep 2016 06:21 :11 S02092714-2A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 2 158.0 3173 50 255 0 990 SPECTRUM PLOT USER 02 *TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: ---*-----.!!! c :::i. 0 () 12 10 6 -4 2 0 Page 5449 of 5809 100 200 300 27 Sep 2016 06:25:03 27 Sep 2016 07:55:27 S02092714-3A.XLS U02092714-1A.XLS Log Counts 02 TRITIUM GREEN LIQUID 3 14-3 90.00 174.9 3291 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -Ill E 6 .. :J 0 (.) 4 Page 5450 of 5809 27 Sep 2016 07:58:42 27 Sep 2016 09:29:06 S02092714-4A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 4 14-4 90.00 153.7 3092 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment' Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 -7 6 !!? c: "' 0 (.) 4 3 -2 1 0 100 Page 5451of5809 200 300 27 Sep 2016 09:32:24 27 Sep 2016 11 :02:47 S02092714-5A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 5 14-5 154.6 3155 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 7 6 E g 5 () 3 2 0 0 100 Page 5452 of 5809 200 300 27 Sep 2016 11 :06:03 27 Sep 201612:36:27 S02092714-6A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 6 14-6 154.1 3091 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 '800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -.IQ § 6 0 (.) 4 2 0 Page 5453 of 5809 100 200 300 27 Sep 2016 12:39:41 27 Sep 2016 14:10:05 S02092714-7 A.XLS U02092714-1 A.XLS Log Counts 02 TRITIU,tvl GREEN LIQUID 7 14-7 90.00 156.1 3100 50 255 0 990 SPECTRUM PLOT USER 02 *TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 -J!l § 6 0 (.) 4 -2 0 -0 Page 5454 of 5809 100 200 300 27 Sep 2016 14:13:30 27 Sep 2016 15:43:54 S02092714-8A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 8 156.7 50 0 14-8 3213 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 E ::J 6 0 (,) 4 2 0 Page 5455 of 5809 100 200 300 27 Sep 2016 15:47:13 27 Sep 2016 17:17:38 S02092714-9A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 9 14-9 90.00 154.6 3100 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 .!!! § 6 0 () 0 Page 5456 of 5809 100 200 300 27 Sep 2016 17:21 :04 27 Sep 201618:51:29 S02092714-1 OA.XLS U02092714-1AXLS Log Counts 02 TRITIUM GREEN LIQUID 10 157.4 50 0 14-10 3047 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User fiJumber User Id User 'Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 12 10 8 Ul c: 5 6 () 4 2 0 0 Page 5457 of 5809 100 200 300 27 Sep 2016 18:54:46 27 Sep 2016 20:25:10 S02092714-11A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 11 154.7 50 0 14-11 3080 255 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 10 9 8 7 6 5 5 () 4 0 0 Page 5458 of 5809 100 200 300 27 Sep 2016 20:28:21 27 Sep 2016 21 :58:44 S02092714-12A.XLS U02092714-1 A.XLS Log Counts 02 TRITIUM GREEN LIQUID 12 14-12 154.1 3114 50 255 0 990 SPECTRUM PLOT USER 02 -TRITIUM 400 500 90.00 600 Channel Number (log) 700 800 900 27 SEP 2016 22=21 TI ME ()(:1T1::\ CP1L.C CCH..ll\IT FJL.{*'rNK Tl.-1JO PHr::*,;:iF SC I l\IT I L.i.. .. = LE\JE::L. CPM H# :YES SAMPLE REPEATS: ND IC# : NO REPLICATES ND AQC = ND CYCLE REPEATS : LIQUID L.UMEX=YES LOW SAMPLE REJ: ND HALF LIFE CORRECTION DATE: :!. *i .) .. 1 (> CHAN: 50.0 -255.0 %ERROR= 2.00 FACTOR: CHAN: 0.0 900.0 %ERRDR1 2.00 FACTOR= 1.000000 BKG. SUBn 1.000000 BKG. SUB: ALPHA-BETA DISCRIMINATION= NO !::lP1M l\IO ?:.l. .... *:l. ;-, Page 5459 of 5809 MI l\I l 00 :I. c. ::) :) l+J:I: ..................... .. J!:; .. J!:>:!! .. ... ;;IL............... .. .................... .. J!::. .. ............ . CPM %ERROR CPM %ERROR :.i. .. 5.1. .'.l.{.J n {j.(: 42 .. 20 iii 11 ::2 () D.02 L.LJlIE X "I '" (l 0 1:::L.P1Pf::>E:D TIME ::EDIT ClFF Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 5 4 3 Ill 3 -c ::J 0 (.) 2 2 1 -. 1 0 0 Page 5460 of 5809 100 200 300 27 Sep 2016 21:59:52 27 Sep 2016 22:15:15 S04092721-1 A.XLS U04092721-1 A.XLS Log Counts 04 T.RITIUM GREEN LIQUID 1 21-1 153.6 642 50 255 0 990 SPECTRUM PLOT USER 04 -TRITIUM 15.00 400 500 600 Channel Number (Log) 700 800 900

.:::!.::ID :: .:::!.::ID :: J. I <I::::f O .. :: :::11,.1 :r. .. L ... l?.:l *::-*("" 1:-* 1 ... 1.1: .. _,;_, ('.:)1;'* II';:'° 1 .. : .. * ... f .!...?; ":;;::tr NJl,.I ::;:11,,1 I .. I.. JO t.3 *1* ... ,. ,,\.,}\,.), ... '\.' ... :i:::i;;; r ON ("'(") I ,::) ,. 1::: ON V138-VHdlV () 0 OOOOOO"T =sns 000000*1 OO"Z 0"006 -o*o SNVHJ OO"Z 0"££{ -O"OG =NVHJ ;;;,)UC:lU .JS I "'1 !1.\ M i:I >IUIG *;:t-,:-**7*'i:::-'d ** :... l,"f \.,) '***' :::l] . .i..NIHd 0 '\.' T T :31va dlVH ON MOl S3A=X3Wnl a1no11 : BlV3d3U 31JAJ ON : JOV ON 83lVJild3d ON : #JI ON 3ldWVS #H WdJ 00 "',;T ""!](\]'"I Mu*-*1 :::IC).J.. 1;,i-r-*1 I .J .. l\I J :JE; DM.J .. >l l\l 1i:i **-1 H: . .L N fl CJ '.J :]"'"!1;:;!'.J I;') J .. UG :J!d I .1. .1..:::1!::;3:::!d 9£G80 9t03 d38 6Z n ..... n r***B :ir ... .ii .... :ic .... t. :::; {]I: ::n: Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 5 4 4* 3 .!!l 3 c: :::J 0 (.) 2 -2 1 0 Page 5462 of 5809 100 200 300 29 Sep 2016 08:14:13 29 Sep 2016 08:29:36 S04092953-1 A.XLS U04092953-1 A.XLS Log Counts 04 TRITIUM GREEN LIQUID 1 53-1 15.00 153.9 655 50 255 0 990 SPECTRUM PLOT USER 04 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tritium -Start, End: Win2: -Start, End: 5 4 4 3 .!!1 3 c ::i 0 (.) 2 1 . 1 -Page 5463 of 5809 100 200 300 29 Sep 2016 08:30:35 29 Sep 2016 08:45:59 S04092953-3A.XLS U04092953-1 A.XLS Log Counts 04 TRITIUM GREEN LIQUID 3 53-3 15.00 156.6 541 50 255 0 990 SPECTRUM PLOT USER 04 -TRITIUM 400 500 600 Channel Number (Log) 700 800 900 Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist GL-CHL-RAD-013 Rev 1 Page 1 of 1 23-Sep-2016 Batch#_! S--- ()___;,_;{ s;:__ Criteria: Yes No Comments sample Solids are less than or eaual to 100 ma for GAB. Jfr Samples have been blank corrected (if required). (rJ ev Blank correction reoorted Included Clf reoulredl, / I If activity less than lOx MDA/MDC, error ls less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error Is 40% IH ha!-*** J Is or less, source check Is within limits. v Inctr*---* bko check Is within llmits. Method RDL/ LLD has been met. / If duplicate activities are: / Less than 5* MDA/ MDC, then RPO is 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO ls 0%, Or meets the client's reoulred RER acceotance criteria. Tracer yield Is 15-125%

  • Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). I Method blank Is less than the RDL/ LLD. J ltT< ----*--.-l;;OJ, nf ln,.*ac* Samole was run within hold time. / v Soo {) <; f( I .<:f11 D 't11 y Samnle was correctlv oreserved If reoulred. J Smears Taken for Radioactive batches. /VY V' I Method Spike and LCS are within 75-125% Or meets the rlfent"* rnntract rriterla\, No blank spaces on data forms. / All line outs initialed and dated, ... _ ---------, !ilt..:..ft'!'llPftn .. I Aux data Is correct. rJ l)/ 1/ I Client Snecial renuirements naoe has been checked. Raw Data and / or snectrum are Included and orooerl" statused. J MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and J .. verifif>rl UI* -.. (if tJ tr -v fl\ Cl/ *1 (' r 1'1"'7'"1 -, n-*-'-*-*-r---u ...... ./.// .......... l U I I Batch Data Exceotlon Reoorts CDERl comoleted If aoollcable. ./ *J>E1l 15lI;{) '8'tt Batch Data Exception Reports (DER) second reviewed. cV 17-ell \SloOS17 Dfsnositlon verified to be comoieted. Aliauot Correctinn cn..,nleted if reaufr.,d. / /\) .)y Review sample historical results If available (If REMP, results above MDC have been verified bv historical results recount or re-analvsis. \ ---:;? --**** /' ?"' . .,,. v ' Page 5464 of 5809 GEL Laboratories LLC Form GEL-DER
  • DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 23-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC EPA 906.0 Modified Solid Batch ID: Sample Numbers: 1598075 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, 1203626099, and 1203626100 were received and analyzed out of the method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 23-SEP-16 Lyndsey Pace 23-SEP-16 Page 1 Page 5465 of 5809 DER Report No.: 1560877 Revision No.: 2 Type: Process Client Code: MJWC Batch ID: Analyst: Method: Lab SOP: 1598075 Terry PhiIJips EPA 906.0 Modified GL-RAD-A-002 REV# 21 Instrument: No instrument-manual method Sample ID Prep Date 405235021 22-SEP-2016 05:47:33 405235022 22-SEP-2016 05:47:33 405235023 22-SEP-2016 05:47:33 405235024 22-SEP-2016 05:47:33 405235025 22-SEP-2016 05:47:33 405235026 22-SEP-2016 05:47:33 405235027 22-SEP-2016 05:47:33 405235028 22-SEP-2016 05:47:33 405235029 22-SEP-2016 05:47:33 405235030 22-SEP-2016 05:47:33 405235031 22-SEP-2016 05:47:33 405235032 22-SEP-2016 05:47:33 405235033 22-SEP-2016 05:47:33 405235034 22-SEP-2016 05:47:33 405235035 22-SEP-2016 05:47:33 405235036 22-SEP-2016 05:47:33 405235037 22-SEP-2016 05:47:33 405235038 22-SEP-2016 05:47:33 405235039 22-SEP-2016 05:47:33 405235040 22-SEP-2016 05:47:33 1203626098 MB 22-SEP-2016 05:47:33 1203626099 DUP (405235021) 22-SEP-2016 05:47:33 1203626100 MS(405235021) 22-SEP-2016 05:47:33 1203626101 LCS 22-SEP-2016 05:47:33 ReagcntfSolvcnt Lot ID Description 2352257.5 Ecoscint Ultra Scintillation Solution 2373671 Sodium Hydroxide, Pellet ACS 2418926 Quenching Agent 2447042.3 Ecoscint Ultra Scintillation Solution 2452415 RL-Potassium Permanganate Analytical Logbook version 1 11--04-2002 Matrix Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Amount 13mL 2g 20uL 13 mL 2mL Prep Logbook The Determination of Tritium Type Sample Id Description LCS 1203626101 Tritium SPIKE MS 1203626100 Tritium SPIKE Dry or Wet Unadjusted Aliquot w w w w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) 3.3 2.7541 3.32 2.6768 3.43 2.6565 3.31 2.6679 3.41 2.6807 3.27 2.7257 3.41 2.7907 3.38 2.6136 3.42 2.7592 3.44 2.6181 3.41 2.64 3.3 2.6278 3.5 2.883 3.4 2.7348 3.42 2.8636 3.41 2.8065 3.44 3.2257 3.43 2.8693 3.37 3.0769 3.42 2.9143 J.n)I 3.31 2.7624 3.31 2.7624 3.l.'lSJ Comments: Spike Pipet ID: RAD-LSC-2970968 Vial Pipet ID: RAD-LSC-8036326 Bkg prepared with dead water: Yes Rig# 5 II 15 20 21 39 30 33 36 35 38 40 43 44 45 46 47 51 57 60 65 66 67 71 l0[11}10 Serial Number 1753-B 1753-B 10 a* . .;rP> 0f'7 Spike Amount Spike Units .I .I mL mL Volume Added Aliquot in vial (mL) (mL) 50 IO 50 10 50 10 50 10 50 10 50 10 50 10 50 10 50 10 50 10 50 10 50 10 .50 10 50 10 50 10 50 10 50 10 50 10 50 10 50 JO 50 IO 50 10 50 IO 50 10 GEL Laboratories LLC

'"O Pl (1Q ("D Vo O'\ -....l T1598075 0 >-+, Tritium Solid Vi 00 0 Filename : H3DST.XLS \D File type : Excel Version#: 12.13 Batch : 1598075 Analyst: TER02081 Procedure Code : LSCOSH30S Prep Date: 9/2212016 Pannname Tritium Method Uncertainty : O Required MDA 6 pCi/G H-3 Abundance 1.00 *aeometry: Halfllfe of Tritium 12.32 years 10ml DW/13ml Ecoscint UHra Sample Characteristics Sample Distilled Sample Total Sample Aliquot Sample Counted Sample Sample Aliquot StDev. Counted StDev. Rig Sample Pos. ID Volume (L) G G L L number Date/Time 405235021.1 0.0500 2.7541 3.5051E-03 0.0100 1.0000E-05 5 12/8/201514:17 2 405235022.1 0.0500 2.6768 3.4971E-03 0.0100 1.0000E-05 11 12/8/201513:43 3 405235023.1 0.0500 2.6565 3.4950E-03 0.0100 1.0000E-05 15 12/212015 10:40 4 405235024.1 0.0500 2.6679 3.4962E-03 0.0100 1.0000E-05 20 12/8/2015 14:13 5 405235025.1 0.0500 2.6807 3.4975E-03 0.0100 1.0000E-05 21 12/8/201513:38 6 405235026.1 0.0500 2.7257 3.5022E-03 0.0100 1.0000E-05 39 12/8/2015 10:15 7 405235027. 1 0.0500 2.7907 3.5089E-03 0.0100 1.0000E-05 30 12/8/201510:19 8 405235028.1 0.0500 2.6136 3.4906E-03 0.0100 1.0000E-05 33 11/23/2015 14:50 9 405235029.1 0.0500 2.7592 3.5056E-03 0.0100 1.0000E-05 36 11/23/201511:10 10 405235030.1 0.0500 2.6181 3.4911E-03 0.0100 1.0000E-05 35 11/23/2015 14:44 11 405235031.1 0.0500 2.6400 3.4933E-03 0.0100 1.0000E-05 38 11/26/2015 14:25 12 405235032. 1 0.0500 2.6278 3.4921E-03 0.0100 1.0000E-05 40 11/23/201511:48 13 405235033.1 0.0500 2.8830 3.5184E-03 0.0100 1.0000E-05 43 11 /23/2015 11 :53 14 405235034.1 0.0500 2.7348 3.5031E-03 0.0100 1.000DE-05 44 11/23/201511:20 15 405235035.1 0.0500 2.8636 3.5164E-03 O.Q100 1.0000E-05 45 11/2312015 11 :06 16 405235036.1 0.0500 2.8065 3.5105E-03 0.0100 1.0000E-05 46 11/23/201511:12 17 405235037.1 0.0500 3.2257 3.5537E-03 0.0100 1.0000E-05 47 11/30/2015 11 :19 18 405235038.1 0.0500 2.8693 3.5170E-03 0.0100 1.0000E-05 51 11/301201510:40 19 405235039.1 0.0500 3.0769 3.5384E-03 0.0100 1.0000E-05 57 11/30/2015 10:43 20 405235040.1 0.0500 2.9143 3.5216E-03 0.0100 1.0000E-05 60 11/30/201513:23 21 1203626098.1 0.0500 3.2257 3.5537E-03 0.0100 1.0000E-05 65 9/2212016 0:00 22 1203626099.1 0.0500 2.7624 3.5060E-03 0.0100 1.0000E-05 66 12/81201514:17 23 1203626100.1 0.0500 2.7624 3.5060E-03 0.0100 1.0000E-05 67 1218/2015 14:17 24 1203626101.1 0.0500 3.2257 3.5537E-03 0.0100 1.0000E-05 71 9/22/2016 0:00 Page 1 I Plpet, 0.1 ml Stdev : +/-0.000200 ml Plpet, 0.5 ml Stdev: +/-0.001000 ml Plpet, 1.0 ml Stdev : +/-0.002000 ml Pfpet, 5.0 ml Stdev: +/-0.010000 ml Analytical SOP: GL*RAD*A-002 Instrument SOP: GL-RAD-1-017 Count raw Data Counting Rack nme Quench# Gross Pos. Position# (min.) cpm 1 5 30.0296 670.85 1.67 2 6 30.0297 683.81 1.29 3 7 30.0296 672.21 1.56 4 8 30.0296 670.5 1.15 5 9 30.0297 671.66 0.98 6 10 30.0297 671.61 1.12 7 11 30.0297 670.66 1.29 8 12 30.0297 670.78 0.81 9 13 30.0297 669.33 1.29 10 14 30.0297 668.97 1.02 11 15 30.0297 665.91 1.49 12 16 30.0296 666.61 1.29 13 17 30.0296 666.81 1.12 14 18 30.013 668.92 1.19 15 19 30.0296 666.66 1.22 16 20 30.0296 665.28 1.43 17 53 30.0296 665.57 1.32 18 54 30.0296 664.97 1.32 19 55 30.0296 666.93 1.29 20 56 30.0297 664.41 1.43 21 57 30.0296 670.89 1.43 22 58 30.0296 663.96 1.53 23 59 15.0297 667.7 11.78 24 60 15.0297 667.91 11.64 Bkg Count Corrected Bkg nme Bkg Bkg cpm (min.) Quench# cpm 0.95 30 667.23 0.9528 0.95 30 667.23 0.9442 0.95 30 667.23 0.9533 0.95 30 667.23 0.9526 0.95 30 667.23 0.9531 0.95 30 667.23 0.9531 0.95 30 66723 0.9527 0.95 30 667.23 0.9527 0.95 30 667.23 0.9519 0.95 30 667.23 0.9516 0.95 30 667.23 0.9485 0.95 30 667.23 0.9493 0.95 30 667.23 0.9495 0.95 30 667.23 0.9516 0.95 30 667.23 0.9494 0.95 30 667.23 0.9477 0.95 30 667.23 0.9480 0.95 30 667.23 0.9472 0.95 30 667.23 0.9497 0.95 30 667.23 0.9464 0.95 30 667.23 0.9528 0.95 30 667.23 0.9458 0.95 30 667.23 0.9505 0.95 30 667.23 0.9507 T1598075 Calibration Data Detector Background Count Calibration Detector Efficiency Background Count Start Sample Counted Calibration Due Efficiency Error Rack Start Datemme Decay on Date Date (cpm/dpm) (cpm/dpm) Position# Datemme 9122/2016 15:03 0.956 LSCORANGE 6/15/2016 6/30/2017 0.2387 0.00792 4 9122/2016 14:30 9122/2016 15:35 0.956 LSCORANGE 6/15/2016 6/30/2017 0.2667 0.00792 4 9/2212016 14:30 9/22/2016 16:08 0.956 LSCORANGE 6/1512016 6/30/2017 0.2416 0.00792 4 9/22/201614:30 9/2212016 16:40 0.956 LSCORANGE 6/15/2016 6130/2017 0.2380 0.00792 4 9/2212016 14:30 9/2212016 17:13 0.956 LSCORANGE 6115/2016 6/30/2017 0.2405 0.00792 4 9/2212016 14:30 912212016 17:45 0.956 LSCORANGE 6/15/2016 6/30/2017 0.2404 0.00792 4 9/22/2016 14:30 9/2212016 18:18 0.956 LS CO RANGE 6/15/2016 6/30/2017 0.2383 0.00792 4 9/2212016 14:30 9/2212016 18:51 0.954 LS CO RANGE 6/15/2016 6/30/2017 0.2386 0.00792 4 9122/2016 14:30 9/2212016 19:23 0.954 LSCORANGE 6115/2016 6130/2017 0.2356 0.00792 4 9122/2016 14:30 912212016 19:56 0.954 LSCORANGE 6115/2016 6/30/2017 0.2348 0.00792 4 9/22/2016 14:30 9/2212016 20:28 0.955 LSCORANGE 6115/2016 6/30/2017 0.2284 0.00792 4 9/22/2016 14:30 9/2212016 21:01 0.954 LSCORANGE 6/15/2016 6/30/2017 0.2299 0.00792 4 9/2212016 14:30 9/22/2016 21 :33 0.954 LSCORANGE 6/1512016 6/30/2017 0.2303 0.00792 4 9122/2016 14:30 9/2212016 22:06 0.954 LSCORANGE 611512016 6/30/2017 0.2347 0.00792 4 9/2212016 14:30 9/22/2016 22:38 0.954 LSCORANGE 6/15/2016 6/30/2017 0.2300 0.00792 4A 9/2212016 14:30 9/22/2016 23:11 0.954 LSCORANGE 6/15/2016 6/30/2017 0.2271 0.00792 4 9/22/2016 14:30 9/2212016 23:44 0.955 LSCORANGE 6115/2016 6130/2017 0.2277 0.00792 4 9/22/2016 14:30 9/2312016 0:17 0.955 LSCORANGE 6/15/2016 6/30/2017 0.2265 0.00792 4 9/2212016 14:30 9/23/2016 0:49 0.955 LSCORANGE 6/15/2016 6/30/2017 0.2305 0.00792 4 9/2212016 14:30 9/23/2016 2:37 0.955 LSCORANGE 6115/2016 6/30/2017 0.2253 0.00792 4 9/22/2016 14:30 9/2312016 3:10 1.000 LSCORANGE 6/15/2016 6/30/2017 0.2388 0.00792 4 9/2212016 14:30 9/23/2016 3:42 0.956 LSCORANGE 6115/2016 6/30/2017 0.2244 0.00792 4 9122/2016 14:30 9/23/2016 4:15 0.956 LSCORANGE 6/15/2016 6/30/2017 0.2322 0.00792 4 9/2212016 14:30 9/2312016 4:32 1.000 LSCORANGE 6/15/2016 6/30/2017 0.2326 0.00792 4 9122/2016 14:30 Page2 Notes: 1 -Results are decay corrected to Sample Datemme 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Datemme * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MOA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 2.1019 1.4840 6 3.3257 2.5686 41.21% 2 1.9276 1.3609 6 3.0514 1.1408 78.88% 3 2.1559 1.5221 6 3.4110 2.2281 47.69% 4 2.1764 1.5366 6 3.4436 0.7321 134.04% 5 2.1446 1.5141 6 3.3931 0.0983 943.05% 6 2.1101 1.4898 6 3.3386 0.6000 157.41% 7 2.0779 1.4670 6 3.2876 1.1943 81.02% 8 2.2214 1.5684 6 3.5148 -0.5402 169.75% 9 2.1305 1.5042 6 3.3711 1.2280 80.81% 10 2.2522 1.5901 6 3.5637 0.2627 374.56% 11 2.2910 1.6174 6 3.6257 2.1185 52.63% 12 2.2892. 1.6162 6 3.6227 1.3312 80.16% 13 2.0830 1.4706 6 3.2964 0.6060 154.01% 14 2.1574 1.5231 6 3.4138 0.8769 112.01% 15 2.0998 1.4825 6 3.3231 0.9699 99.32% 16 2.1676 1.5303 6 3.4306 1.7861 58.34% 17 1.8793 1.3268 6 2.9742 1.1939 73.89% 18 2.1234 1.4991 6 3.3607 1.3525 73.72% 19 1.9478 1.3751 6 3.0823 1.1312 80.25% 20 2.1004 1.4829 6 3.3245 1.7363 58.18% 21 1.7162 1.2117 6 2.7154 1.3954 59.03% 22 2.2215 1.5684 6 3.5163 2.2195 49.15% 23 2.6357 1.8609 6 4.4547 39.7689 8.39% 24 2.1553 1.5216 6 3.6426 32.0949 8.44% T1598075 Spike SIN : 1753-B Spike Exp Date: 11/212016 Spike Activity (dpm/ml): 2549.25 Spike Volume Added: 0.10 LCSS/N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA 1753-B 11/2/2016 2549.25 0.10 2SIGMA Net Count Net Count Counting Total Prop. Rate Rate Error Uncertainty Uncertainty CPM CPM pCi/G pCi/G 0.7172 0.2955 2.0744 2.0748 0.3458 0.2728 1.7637 1.7638 0.6067 0.2893 2.0822 2.0825 0.1974 0.2646 1.9233 1.9233 0.0269 0.2537 1.8167 1.8167 0.1669 0.2627 1.8511 1.8511 0.3373 0.2733 1.8963 1.8964 -0.1427 0.2423 1.7973 1.7973 0.3381 0.2732 1.9448 1.9449 0.0684 0.2562 1.9283 1.9283 0.5415 0.2850 2.1850 2.1852 0.3407 0.2731 2.0913 2.0914 0.1705 0.2625 1.8292 1.8292 0.2384 0.2671 1.9251 1.9252 0.2706 0.2688 1.8881 1.8881 0.4823 0.2814 2.0422 2.0424 0.3720 0.2748 1.7290 1.7291 0.3728 0.2748 1.9540 1.9541 0.3403 0.2731 1.7792 1.7793 0.4836 0.2813 1.9797 1.9799 0.4772 0.2817 1.6143 1.6145 0.5842 0.2871 2.1379 2.1382 10.8295 0.9030 6.4996 6.5305 10.6893 0.8978 5.2838 5.3084 Page3 Sample Sample Nominal QC Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235021. 1 OUP

  • 0.0% 405235021. 1 MS 43.4577 91.5% LCS 35.5988 90.2%

REGISTRY THU 22 SEP 2016 14:28 i'** DIRECTORY PATH :M:\LSC\O\DA\598075A0 i<id< PARAMETER GROUP: 8 ID: H-3 (3) OOA PROGRAM MODE 6 -> ORDER POS ID CTIME COUNTS CUCNTS MCW REP STD STMS STIME 1 4 BKG 30:00 1.0E04 NO LIM 1 1 y 1/10 1:00 2 5 405235021 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 3 6 405235022 30:00 1.0E04 NO LIM 1 1 y 1/10' 1:00 4 7 405235023 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 5 8 405235024 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 6 9 405235025 30:00 l.OE04 NO LIM 1 1 y 1/10 1:00 .7 10 405235026 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 8 11 405235027 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 9 12 405235028 30:00 l.OE04 NO LIM 1 1 y 1/10 1:00 10 13 405235029 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 11 14 405235030 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 12 15 405235031 30:00 1.0E04 NO LIM 1 1 y 1/10 1:00 13 16 405235032 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 14 17 405235033 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 15 18 405235034 30:00 l.OE04 NO LIM 1 1 y 1/10 1:00 16 19 405235035 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 17 20 405235036 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 18 53 405235037 30:00 l.OE04 NO LIM 1 1 y 1/10 1:00 19 54 405235038 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 20 55 405235039 30:00 l.0E04 NO LIM 1 1 y 1/10 1:00 NUMBER OF CYCLES 1 COINCIDENCE BIAS (L/H) L MCA INPUT TRIGG. INHIBIT MEMORY SPLIT 1 LRSUM DCOS G L*R 2 GSUM G L*R WINDOW CHANNELS MCA HALF 1 50-175 1 2 2 5-320 1 2 3 1-1024 1 2 4 50-320 1 1 5 50-270 1 1 6 60-220 1 1 7 1-1024 2 1 8 1-1024 2 2 SELECTED PRINTOUT FOR TERMINAL l (A) SELECTED PRINTOUT FOR TERMINAL 2 (B) 1. 2. 3. 4. 5. 6. 7. POS ID CTI ME SQP CPMl CPM2 CPM3 SEND SPECTRA 12 RESOLUTION OF SPECTRA 1024 LISTING Y INSTRUMENT NUMBER l Page 1 Page 5470 of 5809 REGISTRY POS ID CTI ME SQP CPMl CPM2 CPM3 Q010401N.001 22 SEP 2016 15:01 4 BKG 30:01. 780 Q020501N.001 22 SEP 2016 15:34 667.23 .95 2.82 7.02 5 405235021 30:01. 773 670.85 1.67 3.23 6.37 Q030601N.001 22 SEP 2016 16:06 6 405235022 30:01. 780 683.81 1.29 2.52 5.86 Q040701N.001 22 SEP 2016 16:39 7 405235023 30:01. 773 Q050801N.001 22 SEP 2016 17:11 672.21 1.56 2.82 6.85 8 405235024 30:01.773 670. 50 1.15 2.38 5.69 Q060901N.001 22 SEP 2016 17:44 9 405235025 30:01. 780 671. 66 .98 2.31 5.48 Q071001N.001 22 SEP 2016 18:16 10 405235026 30:01.780 Q081101N.001 22 SEP 2016 18:49 671.61 1.12 2.59 6.47 11 405235027 30:01. 779 Q091201N.001 22 SEP 2016 19:22 670.66 1.29 2.62 5.69 12 405235028 30:01. 779 670.78 .81 2.04 5.72 Ql01301N.001 22 SEP 2016 19:54 13 405235029 30:01. 779 669.33 1.29 2.86 6.54 Qlll401N.001 22 SEP 2016 20:27 14 405235030 30:01. 779 Ql21501N.001 22 SEP 2016 20:59 668.97 1.02 2.52 6.23 15 405235031 30:01. 779 665.91 1.49 2.76 6.57 Ql31601N.001 22 SEP 2016 21:32 16 405235032 30:01. 778 Q141701N.001 22 SEP 2016 22:04 666.61 1.29 2.62 6.13 17 405235033 30:01. 778 Ql51801N.001 22 SEP 2016 22:37 666.81 1.12 2.38 5.99 18 405235034 30:00.778 Ql61901N.001 22 SEP 2016 23:09 668.92 1.19 2.86 6.37 19 405235035 30:01. 778 Ql72001N.001 22 SEP 2016 23:42 666.66 1.22 2.69 5.99 20 405235036 30:01. 778 665.28 1.43 2.48 5.82 Ql85301N.001 23 SEP 2016 0:15 53 405235037 30:01. 777 665.57 1.32 2.52 5.35 Ql95401N.001 23 SEP 2016 0:48 54 405235038 30:01. 777 664.97 1.32 2.52 5.45 Q205501N.001 23 SEP 2016 1:20 55 405235039 30:01. 777 666.93 1.29 2.93 5.82 Page 2 Page 5471of5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pas, Time: Quench: Start, End, X-Axis Channel Counts 5 £? § 3 0 0 ' 2 1 0 0 32 33 34 35 Page 5472 of 5809 50 100 150 0 0 0 o* Quantulus THU 22 SEP 2016 14:28 . M:\LSC\FILES\orange\598075AO\SQ010401 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 1, BKG, 30.02967: 667.23 50-175 SPECTRUM PLOT H-3 (3) 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 2 .fg . r: :J 0 0 1.5 0 Quantulus THU 22 SEP 2016 14:28 M:\LSC\FU..ES\orange\598075AO\SQ020501 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 2, 405235021, 30.02955: 670.85 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 *1000 32 0 33 0 34 0 35 0 Page 5473 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pas, Time: Quench: Start, End, X-Axis Channel. Counts 3 -2.5 -UJ 2 -c ::J 0 0 1.5 ' 0.5 -Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ030601 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 3, 405235022, 30.02967: 683.81 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 1 Page 5474 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -' 2.5 -"' 2 --c :s 0 0 1.5 -0 Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ040701 N.QQ,1.xls M :\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 4, 405235023, 30.02955: 672.21 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5475 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pas, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 II) 2 --c: :J 0 0 1.5 Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ050801 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 5, 405235024, 30.02955: 670.5 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5476of5809 Instrument Type: Data Capture Date: FileNarrie: File Info: ID: Comments: Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ060901 N.001.xls M:\LSC\FI LES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE Sample, Rack-Pos, Time: 6, 405235025, 30.02967: 671.66 Quench: Start, End, X-Axis Channel Counts U) .... c :::s 0 0 Page 5477of5809 2 1.5 -1 0.5 0 -0 50 32 33 34 35* 50-175 SPECTRUM PLOT H-3 (3) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileName:i File Info: ID: Comments: Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ071001 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE Sample, Rack-Pas, Time: 7, 405235026, 30.02967: 671.61 Quench: Start, End, X-Axis Channel Counts 3 2.5 2 .!!! c :l 0 0 1.5 1 0.5 -0 0 32 33 34 35 Page 5478of5809 50 50-175 SPECTRUM PLOT H-3 (3) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileNarile: File Info: ID: Comments: Sample, Rack-Pos; Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 2-£3 c ::::J 0 0 1.5 -Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ081101 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 8, 405235027, 30.02965: 670.66 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5479 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 "' 2 -.... c ::I 8 1.5 0.5 0 Quantulus-THU 22*SEP 2016 14:28 M:\L.SC\FILES\orange\598075AO\SQ091201 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 9, 405235028, 30.02965: 670.78 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5480of5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ101.301 N.001 .. xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE Sample, Rack-Pas, Time: 10, 405235029, 30.02965: 669.33 Quench: Start, End, X-Axis Channel Counts 3 2.5 -en 2 -c :I 0 0 1.5 0.5 -0 0 32 33 34 35 Page 5481of5809 50 50-175 SPECTRUM PLOT H-3 (3) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: File Info: ID: Comments: Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\5Q8075AO\SQ111401 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE Sample, Rack-Pos, Time: 11, 405235030, 30.02965: 668.97 Quench: Start, End, X-Axis Channel Counts 3 -2.5 J!? r:: :::s 0 0 1.5 -1 0.5 0 32 33 34 35 Page 5482 of 5809 50 50-175 SPECTRUM PLOT H-3 (3) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument rype: Data Capture Date: FileName: File Info:

  • ID: Comments: Quantulus THU 22*SEP 2016 14:28
  • M:\LSC\FILES\orange\598075AO\SQ121501 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE Sample, Rack-Pos, Time: 12, 405235031, 30;02965: 665.91 Quench: End, X-Axis Channel Counts 3 2.5 -en 2 -c ::J 0 0 1.5 -.1 -0.5 0 0 32 33 34 35 Page 5483 of 5809 50 50-175 SPECTRUM PLOT H-3 (3) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 600 650 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileNaine: .File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 4.5 4 3.5 -3 U) 2.5 -c ::s 0 0 2 1.5 1 -0.5 +---__,..._ Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ131601 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 13, 405235032, 30.02963: 666.61 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5484 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 2.5 -U) 2 -c ::J 0 0 1.5 -1 *0.5 -0 0 32 33 34 35 Page 5485of5809 50 100 150 200 250 0 0 0 O* Quantulus THU 22 SEP 2016 14:28 .
  • M:\LSC\FILES\orange\598075AO\SQj141701 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls ' H-3 (3) ORANGE 14, 405235033, 30.02963: 666.81 50-175 SPECTRUM PLOT H-3 (3) 300 350 400 450 500* 550 600 650 700 750 800 850 900 950 1000 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pas, Time: Quench: Start, End, X-Axis Channel Counts !!! c ::I 0 3 -2.5 2 0 1.5 -1 0.5 -Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ15.1801 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 15, 405235034, 30.01297: 668.92 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5486 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 5* 4 -§ 3 0 0 2 -Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILE,S\orange\598075AO\SQ161901 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 16, 405235035, 30.02963: 666.66 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 BOO 850 900 950 1000 32 0 33 1 34 0 35 0 Page 5487 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts J!! c :s 0 0 2 -1.5 -Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ172001 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 17, 405235036, 30.02963: 665.28 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5488 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts J!? c ::s 0 0 2 -1.5 -1 0.5 0 Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ185301 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 18, 405235037, 30.02962: 665.57 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 i 50 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5489 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598075AO\SQ195401 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE Sample, Rack-l?os, Time: 19, 405235038, 30.02962: 664.97 Quench: Start, End, X-Axis Channel Counts 3 2.5 -2 .:!? c :J 0 0 1.5 1 -0.5 0 -0 32 33 34 35 Page 5490 of 5809 50 50-175 SPECTRUM PLOT H-3 (3) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileName: .. File Info: ID: Comments: Sample, Rack-Pos, Time: Quench:* Start, End, X-Axis Channel Counts 3 -2.5 -2 J!l c :s 0 (.) 1.5 -Quantulus THU 22 SEP 2016 14:28 M:\LSC\FILES\orange\598Q75AO\SQ205501 N.001.xls M:\LSC\FILES\orange\598075AO\U598075AO.xls H-3 (3) ORANGE 20, 405235039, 30.02962: 666.93 50-175 SPECTRUM PLOT H-3 (3) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5491 of 5809 REGISTRY FRI 23 SEP 2016 2:35 DIRECTORY PATH :M:\LSC\O\DA\598075Al PARAMETER GROUP: 8 ID: H-3 (4) OOA PROGRAM MODE 6 -> ORDER POS ID 1 56 405235040 2 57 1203626098 3 58 1203626099 4 59 1203626100 5 60 1203626101 NUMBER OF CYCLES COINCIDENCE BIAS (L/H) 1 L MCA INPUT TRIGG. INHIBIT 1 LRSUM DCOS G 2 GSUM G WINDOW 1 2 3 4 5 6 7 8 CHANNELS 50-175 5-320 1-1024 50-320 50-270 60-220 1-1024 1-1024 MCA HALF 1 2 1 2 1 2 1 1 1 1 1 1 2 1 2 2 CTIME COUNTS CUCNTS MCW REP 30:00 l.0E04 NO LIM 1 1 30:00 l.0E04 NO LIM 1 1 30:00 l.0E04 NO LIM 1 1 15:00 l.0E04 NO LIM 1 1 15:00 l.0E04 NO LIM 1 1 MEMORY SPLIT L*R L*R SELECTED PRINTOUT FOR TERMINAL 1 (A) SELECTED PRINTOUT FOR TERMINAL 2 (B) 1. 2. 3. 4. 5. 6. POS ID CTI ME SQP CPMl CPM2 SEND SPECTRA 12 RESOLUTION OF SPECTRA 1024 LISTING Y INSTRUMENT NUMBER 1 POS ID CTI ME SQP CPMl CPM2 Q015601N.001 23 SEP 2016 3:08 56 405235040 30:01. 780 664.41 1.43 2.79 Q025701N.001 23 SEP 2016* 3:41 STD STMS y 1/10 y 1/10 y 1/10 y 1/10 y 1/10 STIME 1:00 1:00 1:00 1:00 1:00 7. CPM3 CPM3 6. 51 57 1203626098 30:01. 773 670.89 1.43 3.30 6.54 Q035801N.001 23 SEP 2016 4:13 58 1203626099 30:01. 773 663.96 1. 53 2.96 '6. 51 Q045901N.001 23 SEP 2016 4:31 59 1203626100 15 :01. 780 667.70 11.78 13 .27 16.27 Q056001N.001 23 SEP 2016 4:48 60 l,203626101 15:01. 780 667.91 11.64 13.07 15.86 Page 1 Page 5492 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus FRI 23 SEP 2016 2:35 M:\1..SC\FILES\orange\598075A 1\80015601 N.001.xls M:\LSC\FILES\orange\598075A 1\U598075A 1.xls H-3 (4) ORANGE Sample, Rack-Pas, Time: 1, 405235040, 30.02967: 664.41 Quench: Start, End, X-Axis Channel Counts 3 2.5 UJ 2 --c ::J 0 0 Page 5493of5809 1.5 1 0 0 32 33 34 35 50 50-175 SPECTRUM PLOT H-3 (4) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus FRI 23 SEP 2016 2:35 M:\LSC\FILES\orange\598075A 1\$0025701 N.001..xls M:\LSC\FILES\orange\598075A 1\U598075A1.xls H-3 (4) ORANGE Sample, Rack-Pos, Time: 2, 1203626098, 30.02955: 670.89 Quench: Start, End, X-Axis Channel Counts 3 2.5 2 J!! c :::s 0 0 t.5 -0.5 0 0 32 33 34 35 Page 5494 of 5809 50 50-175 SPECTRUM PLOT H-3 (4) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 -2 J!! c :::I 0 (.) 1.5 Quantulus FRI 23 SEP 2016 2:35 M:\LSC\FILES\orange\598075A 1 \SQ035BQ1 N.001.xls M:\LSC\FILES\orange\598075A 1\U598075A1.xls H-3 (4) ORANGE 3, 1203626099, 30.02955: 663.96 50-175 SPECTRUM PLOT H-3 (4) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5495 of 5809 Instrument Type: Data Capture Date: File Name: File Info: ID: Comments: Sample, Rack-Pas, Time: Quench: Start, End, X-Axis Channel Counts 7 6 5 J!l § 4 0 (.) 3 2 1 Quantulus FRI 23 SEP 2016 2:35 M:\LSC\FILES\orange\598075A 1\80045901 N.001.xls M:\LSC\FILES\orange\598075A 1\U598075A 1.xls H-3 (4) ORANGE 4, 1203626100, 15.02967: 667.7 50-175 SPECTRUM PLOT H-3 (4) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5496 of 5809 Instrument Type: Data Capture Date: F.ileName: File Info: ID: Comments: Sample, Rack-Pos, Time*: Quench: Start, End, X-Axis Channel Counts 6 4 .!!! c j 0 0 3 0 Quantulus FRI 23 SEP 2016 2:35 M:\LSC\FILES\orange\598075A 1 \80056001 N.001.xls M:\LSC\FILES\orange\598075A 1\U598075A 1.xls H-3 (4) ORANGE 5, 1203626101 t 15.02967: 667.91 50-175 . SPECTRUM PLOTH-3 (4) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 1 34 0 35 0 Page 5497 of 5809 Effective 3/25/201 O Radiochemistry Batch Checklist Revision 1 Effective March 2010 21-Sep-2016 Batch# IS3 {L{ ( 7 Date: . Criteria: Yes No Comments Sample Solids are less than or eaual to 100 ma for GAB. Samples have been blank corrected (If required). tJ"Jr Blank correction reported Included (if reaulredl. I [f activity less than 10x MDA/MDC, error Is less ,/ than or equal to 1500/o of sample activity. [f greater than 10* MDA/ MDC, error Is 400/o or less. [f hnln..., thA MDA/ MDC error Is nlrnu rnstrument source check Is within limits. v/ Instrument bko check ls within limits. Method RDL/ LLD has been met. / If duplicate activities are: Less than 5* MDA/ MDC, then RPO Is 10.00/o or less, If greater 5* MDA/ MDC, then RPO 200/o or less, If below the MDA/ MDC, the RPO Is 0%1 Or meets the client's reoulred RER acceotance criteria. Tracer yield is 15-1250/o
  • Carrier yield 25-1250/o. (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. r/ /Tf r"rl c"mnlAc <' l;Ofo nf *-***--* --*1 .. 1 ... \ Sample was run within hold time. i/ Samole was correctlv oreserved If reaulred. v Smears Taken for Radioactive batches. JV}-Method Spike and LCS are within 75-1250/o V' l<or meets the client's contr,.,.. acceotance crltnrla), No blank spaces on data forms. v/ All line outs initialed and dated. INn tra Arrnrc """ Aux data ls correct. fl l!.r Client Soeclal reouirements oaoe has been checked. \/ Raw Data and/ or soectrum are Included and "ronerlv statused. MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and V' ,,_,., __ **-*ified r Hit (If IV ty nn*n-" lntft v v /" ... Batch Data Exceotion Reoorts <DER) comoleted if aoolicable. ,..IV /v Batch Data Exception Reports (DER) second reviewed. Disnosltion verified to be comnleted. Allouot Correction rnmnleted If reouired. iv JY Review samole historical results if available \/ (If REMP, results above MDC have been verified bv historical results recount or re-analvsis. l Primary Review Performed By: .. -q/p1 /;CJ . IJ . --f I Page 5498 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 )'.)(f2. JI) rR , s-'11 1 r.r I SSCf'llLJ GEL Laboratories LLC Form GEL-DER OATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 21-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC DOE EML HASL-300, Tc-02-RC Solid Batch ID: Sample Numbers: 1597417 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075,405235076,405235077,405235078, and 1203624312were received and analyzed out of method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 21-SEP-16 Lyndsey Pace 21-SEP-16 Page 1 Page 5499 of 5809 DER Report No.: 1559774 Revision No.: 2
  • Type: Process Client Code: MJWC Prep Logbook The Determination of Technetium-99 Using Analytical Grade 1X8 Resin Batch ID: 1597417 Analyst: Christina Sanchez Method: DOE EML HASL-300, Tc-02-RC Modified Lab SOP: GL-RAD-A-059 REV# 4 Instrument: BAL-16107662 Sample ID Prep Date Matrix 405235061 15-SEP-2016 12:12:06 Soil 405235062 15-SEP-2016 12:12:06 Soil 405235063 15-SEP-2016 12:12:06 Soil 405235064 15-SEP-2016 12:12:06 Soil 405235065 15-SEP-2016 12:12:06 Soil 405235066 15-SEP-2016 12:12:06 Soil 405235067 15-SEP-2016 12:12:06 Soil 405235068 15-SEP-2016 12:12:06 Soil 15-SEP-2016 12:12:06 Soil 405235070 15-SEP-2016 12:12:06 Soil 405235071 15-SEP-2016 12:12:06 Soil 405235072 15-SEP-2016 12:12:06 Soil 405235073 15-SEP-2016 12:12:06 Soil 405235074 15-SEP-201612:12:06 Soil 405235075 15-SEP-2016 12:12:06 Soil 405235076 15-SEP-2016 12:12:06 Soil 405235077 15-SEP-2016 12:12:06 Soil 405235078 15-SEP-2016 12:12:06 Soil 1203624311 MB 15-SEP-2016 12:12:06 Soil 1203624312 DUP (405235061) 15-SEP-2016 12:12:06 Soil 1203624313 LCS 15-SEP-2016 12:12:06 Soil Reagent/Solvent Lot ID Description Amount 2280154.26 Hydrogen Peroxide 30% ACS Reagent lOmL 120LBS 30 Gallons Ecoscint GL Scintillation Solution 15mL 2418926 Quenching Agent .l uL 2429641 RL-0.1 M Hydrochloric Acid IOOmL 2441205 RL-0.0IM Nitric Acid 20mL 2451825 RL-0.1 M Nitric Acid 25mL TC2074-A tracer lmL Analytical Logbook \"ersion 111-04-2002 Id Description LCS 1203624313 Tecbnetium-99 SPIKE Dry or Wet Unadjusted Aliquot w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) 1.205 0.993 1.273 1.027 1.256 J.124 1.258 1.155 1.238 1.114 1.225 1.111 1.251 1.078 1.217 1.048 1.29 1.153 1.278 1.037 1.239 1.034 1.243 1.141 !.272 1.031 1.355 1.21 1.232 1.1 1.259 1.226 1.104 !.252 1.05 1.21 1.269 1.046 1.21 Comments: Spike Pipet ID: RAD-LSC-2272418 Tracer Pipet ID: RAD-LSC-4099802 Serial Number 1621-B / Spike Amount Spike Units _] mL GEL Laboratories Li::'C 0 >-+, Vl 00 0 \0 Filename : TC99.XLS File type : Excel Version # : 1.2.16 Batch: 1597417 Analyst : CHR02061 Prep Date: 9/1512016 Tc-99 Method Uncertainty: 0.0576 Geometry: 1 Sml Ecoscint GU5ml DI H20/AG 1 x8 Resin Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Sample Pos. ID G G Date/Time 1 405235061.1 0.9930 3.3226E-03 1211412015 13:47 2/ 4052:is062.1 1.0270 3.3261E-03 12114/2015 13:10 3 405235063. 1 1-1240 3.3362E-03 12114/2015 13:15 4 405235064. 1 1.1550 3.3395E-03 12114/2015 13:25 5 405235065. 1 1.1140 3.3352E-D3 121141201513:56 6 405235066.1 1.1110 3.3349E-D3 1211412015 14:00 7 405235067.1 1.0780 3.3315E-D3 12111/201511:30 8 405235068.1 1.0480 3.3283E-03 12111/201510:27 9 405235069.1 1.1530 3.3393E-03 1211612015 12:45 10 405235070.1 1.0370 3.3272E*03 1211112015 10:10 11 405235071. t 1.0340 3.3269E-D3 1211112015 10:25 12 405235072.1 1.1410 3.3380E-03 121151201513:35 13 405235073. 1 1.0310 3.3266E-D3 12111/201511:35 14 405235074.1 1.2100 3.3452E-03 121151201514:10 15 405235075.1 1-1000 3.3337E*03 1211612015 9:31 16 405235076.1 1.0000 3.3233E-03 121111201514:19 17 405235077.1 1.1040 3.3342E-03 12117/201513:30 18 405235078.1 1.0500 3.3285E-03 12117/2015 12:40 19 1203624311.1 1.2100 3.3452E*03 9/15/2016 0:00 20 1203624312.1 1.0460 3.3281E-03 121141201513:47 21 1203624313.1 1.2100 3.3452E-03 9/1512016 0:00 E1597417 Technetium-99 Solid Tracer SIN: Tracer Exp Date : Tracer Volume Added: Tracer Calculations Tracer Rel. Activity (CPM) 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 32522 Page 1 TC2074-A 9116/2016 1.00 Tracer Ref. Count Uncertainty {%) 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% 0.94% Tracer Samp. Activity (CPM) 30685 29949 30221 29728 28982-30594 30895 29108 29056 30362 29574 29642 29132 28908 31032 30752 29562 28037 31216 30154 30937 Procedure Code: Parmname: Required MDA: Tc*99 Abundance : Halflife of Tc-99 : Tracer Samp. Count Uncertainty (%) 0.95% 0.94% 0.95% 0.94% 0.95% 0.95% 0.95% 0.95% 0.95% 0.93% 0.95% 0.95% 0.96% 0.94% 0.95% 0.95% 0.95% 0.96% 0.95% 0.94% 0.95% LSC99TCS Technetium-99 5 pCilG 1.00 211100 years Tracer Tracer Aliquot Aliquot (ml) StDev.(mL) 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 Pipe!, 0.1 ml Stdev : +/-0.000200 ml Pipet, o.s ml Stdev: +/-0.001000 ml Pipe!, 1 ml Stdev : +/* 0.002000 ml Analytical SOP: GL*RAD-A-059 Instrument SOP: GL-RAD-1-017 Count raw Data Counting Rack Time Quench# Gross Pas. Position# (min.) cpm 1 22 25.0124 738.8 4 2 23 25.0124 708.3 3.92 3 24 25.0124 744.19 4.25 . 4 25 25.0124 743.23 3.84 5 26 25.0124 738.75 3.4 6 27 25.0124 736.91 3.84 7 28 25.0124 740.76 3.64 8 29 25.0124 724.32 3.48 9 30 25.0124 745.26 4.04 10 31 25.0124 712.84 3.92 11 32 25.0124 696.37 4.29 12 33 25.0124 747.39 3.72 13 34 25.0123 729.05 3.44 14 35 25.0123 744.62 3.72 15 36 25.0123 749.76 3.72 16 37 25.0123 718.12 3.92 17 38 25.0123 759.17 3.92 18 39 25.0123 720.72 4.73 19 40 25.0123 748.33 3.36 20 41 25.0123 716.05 3.76 21 42 25.0123 753.4 106.32 Bkg Count Corrected Count Bkg Time Bkg Bkg Start cpm *(min.) Quench# cpm Date/Time 3.76 25 755.15 3.8344 912012016 5:58 3.76 25 755.15 3.8594 9/2012016 6:26 3.76 25 755.15 3.8159 9/20/2016 6:53 3.76 25 755.15 3.8196 9/20/2016 7:21 3.76 25 755.15 3.8345 9/2012016 7:48 3.76 25 755.15 3.8396 9/20/2016 8:16 3.76 25 755.15 3.8283 9120/2016 8:43 3.76 25 755.15 3.8602 9/20/2016 9:11 3.76 25 755.15 3.8116 9120/2016 9:38 3.76 25 755.15 3.8619 9/20/2016 10:06 3.76 25 755.15 3.8477 9120/2016 10:33 3.76 25 755.15 3.8023 9/2012016 11:01 3.76 25 755.15 3.8551 9/20/2016 11:28 3.76 25 755.15 3.8142 91201201611:56 3.76 25 755.15 3.7908 9/20/2016 12:23 3.76 25 755.15 3.8627 9/20/2016 12:51 3.76 25 755.15 3.7326 9/201201613:18 3.76 25 755.15 3.8622 9/20/2016 13:46 3.76 25 755.15 3.7978 9120/2016 14:13 3.76 25 755.15 3.8627 9/20/2016 14:41 3.76 25 755.15 3.7707 9/20/2016 15:09 E1597417 calculated Calibration Data Delector Background Sample Sample Calibration Detector Efficiency Count Sample Recovery Recovery Counted Calibration Due Efficiency Error Background Start Decay % Error% on Date Date (cpm/dpm) (cprnfdpm) Position# Date/Time 1.000 0.73% LSCPINK 7/4/2016 6/30/2017 0.5418 0.00792 21 9/2012016 5:31 1.000 92.1% 0.72% LSCPINK 7/4/2016 6/30/2017 0.5008 0.00792 21 9/2012016 5:31 1.000 92.9% 0.73% LSCPINK 7/4/2016 6/30/2017 0.5458 0.00792 21 9/20/2016 5:31 1.000 91.4% 0.72% LSCPINK 7/412016 6130/2017 0.5451 0.00792 21 9/20/2016 5:31 1.000 89.1% 0.73% LSCPINK 7/4/2016 6130/2017 0.5418 0.00792 21 9/20/2016 5:31 1.000 94.1% 0.73% LSCPINK 7/4/2016 6/30/2017 0.5402 0.00792 21 9/20/2016 5:31 1.000 95.0% 0.73% LSCPINK 7/412016 6/3012017 0.5434 0.00792 21 9/20/2016 5:31 1.000 89.5% 0.73% LSCPINK 7/4/2016 6130/2017 0.5262 0.00792 21 9/2012016 5:31 1.000 89.3% LSCPINK 7/4/2016 6/30/2017 0.5464 0.00792 21 9/2012016 5:31 1.000 93.4% 0.72% LSCPINK 7/4/2016 6/30/2017 0.5088 0.00792 21 9/20/2016 5:31 1.000 90.9% 0.73% LSCPINK 7/412016 6/3012017 0.4767 0.00792 21 9/2012016 5:31 1.000 91.1% 0.73% LSCPINK 7/412016 613012017 0.5476 0.00792 21 9/2012016 5:31 1.000 89.6% 0.73% LSCPINK 7/412016 6130/2017 0.5320 0.00792 21 9/20/2016 5:31 1.000 88.9% 0.72"..l. LSCPINK 7/4/2016 6/30/2017 0.5460 0.00792 21 9/2012016 5:31 1.000 95.4% 0.73% LSCPINK 7i4/2016 6/30/2017 0.5488 0.00792 21 9/20/2016 5:31 1.000 94.6% 0.73% LSCPINK 7/4/2016 6/30/2017 0.5173 0.00792 21 9/20/2016 5:31 1.000 90.9% 0.73% LSCPINK 7/4/2016 6/30/2017 0.5512 0.00792 21 9/2012016 5:31 1.000 86.2% 0.73% LSCPINK 7/4/2016 6/30/2017 0.5212 0.00792 21 . 9/20/2016 5:31 1.000 96.0% 0.73% LSCPINK 7/4/2016 6/30/2017 0.5481 0.00792 21 9120/2016 5:31 1.000 92.7".k 0.72% LSCPINK 7/412016 6130/2017 0.5141 0.00792 21 9/20/2016 5:31 1.000 95.1% 0.73% LSCPINK 7/4/2016 6/30/2017 0.5501 0.00792 21 9120/2016 5:31 Page2 Notes: 1 -Results are decay corrected to Sample Dateffime 2 -Reference dale for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Dateffime * -APO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 1.1449 0.8083 5 1.7230 0.1470 2 1.2311 0.8691 5 1.6524 0.0577 919.59% 3 1.0170 0.7180 5 1.5308 0.3430 130.82% 4 1.0078 0.7115 5 1.5169 0.0160 2712.08% 5 1.0806 0.7629 5 1.6263 -0.3639 123.78% 6 1.0301 0.7273 5 1.5502 3.191E-04 138572.83% 7 1.0436 0,7368 5 1.5706 -0.1524 290.22% 8 1.1815 0.8341 5 1.7778 -0.3470 142.50% 9 1.0294 0.7267 5 1.5494 0.1828 245.28% 10 1.1840 0.8359 5 1.7816 0.0532 959.30% 11 1.2988 0.9169 5 1.9544 0.4445 128.97% 12 1.0161 0.7174 5 1.5297 -0.0651 666.68% 13 1.1859 0.8373 5 1.7845 -0.3806 130.10% 14 0.9870 0.6968 5 1.4856 -0.0722 582.69% 15 1.0032 0.7083 5 1.5104 -0.0553 n4.26% 16 1.1925 0.8419 5 1.7942 0.0528 973.63% 17 1.0365 0.7318 5 1.5612 0.1526 295.09% 18 1.2363 0.8728 5 1.8602 0.8286 61.54% 19 0.9086 0.6415 5 1.3678 -0.3098 122.18% 20 1.1699 0.8260 5 1.7603 -0.0928 537.69% 21 0.9101 0.6426 5 1.3705 72.9522 2.33% Ef597417 Spike SIN: Spike Exp Date : Spike Activity (dpmfml): Spike Volume Added: LCSS/N: LCS Exp Date: LCS Activity (dpm/ml): LCS Volume Added (mi): 2SIGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCilG 0.1656 0.5597 0.9734 0.0606 o.ssn 1.0396 0.4341 0.5679 0.8795 0.0204 0.5534 0.8489 -0.4345 0.5378 0.8829 0.0004 0.5541 0.8665 -0.1883 0.5464 0.8670 -0.3802 0.5417 0.9691 0.2284 0.5603 0.8788 0.0581 0.5578 0.9998 0.4423 0.5704 1.1235 -0.0823 0.5484 0.8501 -0.4151 0.5401 0.9704 -0.0942 0.5488 0.8251 -0.0708 0.5480 0.8400 0.0573 0.5578 1.0068 0.1874 0.5531 0.8828 0.8678 0.5861 1.0969 -0.4378 0.5350 0.7419 -0.1027 0.5520 0.9776 102.5493 2.0980 2.9252 Page3 N/A N/A N/A N/A 1621-8 1/5/2017 1911.38 0.10 2SiGMA Total Prop. Uncertainty pCVG 0.9735 1.0397 0.8804 0.8489 0.8829 0.8666 0.8670 0.9691 0.8790 0.9998 1.1247 0.8502 0.9704 0.8251 0.8400 1.0068 0.8830 1.1010 0.7419 o.9n6 8.8828 Sample QC 405235061.1 Sample Nominal Type RPO AER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP
  • 0.0% LCS 71.1554 102.5%

ASSAY 16-Sep-16 12:29:07

  • Protocol id 12 TC99_REC Time limit 500 Count limit 10000 Isotope Tc-99m Protocol date 23-Sep-13 14:21 :59 Run id. 19 POS RACK BATCH TIME COUNTS CPM ERROR % RECOVERY COUNT TIME 1 63 1 21 11337 32521.9 0.94 12:29:15 2 63 2 22 11197 30685.1 0.95 94.35 12:29:48 3 63 3 23 11414 29948.9 0.94 92.09 12:30:22 4 63 4 22 11004 30221.2 0.95 92.93 12:30:57 5 63 5 23 11305 29728.2 0.94 91.41 12:31:31 6 88 6 23 11005 28981.9 0.95 89.12 12:32:20 7. 88 7 22 11098 30594.2 0.95 94.07 12:32:54 8 88 8 22 11195 30895.3 0.95 95.00 12:33:28 9 88 9 23 11017 29108.3 0.95 89.50 12:34:02 10 88 10 23 10985 29056.4 0.95 89.34 12:34:37 11 96 11 23 11457 30361.7 0.93 93.36 12:35:31 12 96 12 23 11149 29574.4 0.95 90.94 12:36:06 13 96 13 23 11162 29642.3 0.95 91.15 12:36:41 14 96 14 23 10958 29131.9 0.96 89.58 12:37:16 15 96 15 24 11334 28907.6 0.94 88.89 12:37:51 16 51 16 22 11135 31031.8 0.95 95.42 12:38:35 17 51 17 22 11023 30751.6 0.95 94.56 12:39:09 18 51 18 23 11067 29562.1 0.95 90.90 12:39:43 19 51 19 24 10943 28037.3 0.96 86.21 12:40:18 20 51 20 22 11151 31216.2 0.95 95.99 12:40:54 21 73 21 23 11246 30154.3 0.94 92.72 12:41:41 22 73 22 22 11023 30936.8 0.95 95.13 12:42:16 END OF ASSAY Batch #1597417 Page 1of1 Page 5504 of 5809 REGISTRY TUE 20 SEP 2016 5:29 DIRECTORY PATH : M: \LSC\Q\DA \597 417 AO "'** PARAMETER GROUP: 8 ID: TC99 (1) OOA PROGRAM MODE 6 -> ORDER POS ID CTIME COUNTS CUCNTS MCW REP STD STMS STIME 1 21 REF 25:00 1.0E04 NO LIM 1 1 y 1/10 1:00 2 22 405235061 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 3 23 405235062 25:00 l.0E04 NO LIM 1 1 y 1/10 1:00 4 24 405235063 25:00 1.0E04 NO LIM 1 1 y 1/10 1:00 5 25 405235064 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 6 26 405235065 25:00 l.0E04 NO LIM 1 1 y 1/10 1:00 7 27 405235066 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 8 28 405235067 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 9 29 405235068 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 10 30 405235069 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 11 31 405235070 25:00 1.0E04 NO LIM 1 1 y 1/10 1:00 12 32 405235071 25:00 l.0E04 NO LIM 1 1 y 1/10 1:00 13 33 405235072 25:00 1.0E04 NO LIM 1 1 y 1/10 1:00 14 34 405235073 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 15 35 405235074 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 16 36 405235075 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 17 37 405235076 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 18 38 405235077 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 19 39 405235078 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 20 40 1203624311 25:00 l.OE04 NO LIM 1 1 y 1/10 1:00 21 41 1203624312 25:00 l.0E04 NO LIM 1 1 y 1/10 1:00 22 42 1203624313 25:00 l.0E04 NO LIM 1 1 y 1/10 1:00 NUMBER OF CYCLES 1 COINCIDENCE BIAS (L/H) H MCA INPUT TRIGG. INHIBIT MEMORY SPLIT 1 LRSUM L"'R PAC+G 2 GSUM G L*R PULSE COMPARATOR LEVEL 1 WINDOW CHANNELS MCA HALF 1 200-600 1 1 2 1-1024 1 1 3 300-640 1 1 4 50-650 1 2 5 70-500 1 2 6 300-640 1 2 7 1-1024 2 1 8 1-1024 2 2 SELECTED PRINTOUT FOR TERMINAL 1 (A) SELECTED PRINTOUT FOR TERMINAL 2 (B) 1. 2. 3. 4. 5. 6. 7. POS ID CTI ME SQP CPMl CPM2 CPM3 SEND SPECTRA 11 RESOLUTION OF SPECTRA 1024 Page 1 Page 5505 of 5809 REGISTRY LISTING Y INSTRUMENT NUMBER 1 POS ID CTI ME SQP CPMl CPM2 CPM3 Q012101N.001 20 SEP 2016 5:57 21 REF 25:00.742 755.15 3.76 5.95 3. 72 Q022201N.001 20 SEP 2016 6:24 22 405235061 25:00.742 738.80 4.00 5.83 3. 72 Q032301N.001 20 SEP 2016 6:52 23 405235062 25:00.742 708.30 3,92 5.58 3.92 Q042401N.001 20 SEP 2016 7:19 24 405235063 25:00.742 744.19 4.25 6.47 4.17 Q052501N.001 20 SEP 2016 7:47 25 405235064 25:00.742 743.23 3.84 5.78 3.23 Q062601N.001 20 SEP 2016 8:14 26 405235065 25:00.742 738.75 3.40 4.85 3.15 Q072701N.001 20 SEP 2016 8:42 27 405235066 25:00.742 736.91 3.84 5.54 3.44 Q082801N.001 20 SEP 2016 9:09 28 405235067 25:00.741 740.76 3.64 5.66 3.48 Q092901N.001 20 SEP 2016 9:37 29 405235068 25:00.741 724.32 3.48 5.06 3.07 Ql03001N.001 20 SEP 2016 10:04 30 405235069 25:00.741 745.26 4.04 5.99 3.80 Qll3101N.001 20 SEP 2016 10:32 31 405235070 25:00.741 712.84 3.92 5.66 3.76 Ql23201N.001 20 SEP 2016 10:59 32 405235071 25:00.741 696.37 4.29 5.22 3.92 Ql33301N.001 20 SEP 2016 11:27 33 405235072 25 :00. 741 747. 39 3.72 5.78 3.76 Q143401N.001 20 SEP 2016 11:54 34 405235073 25:00.740 729.05 3.44 5.22 3.03 Ql53501N.001 20 SEP 2016 12:22 35 405235074 25:00.740 744.62 3.72 5.62 3.52 Ql63601N.001 20 SEP 2016 12:49 36 405235075 25:00.740 749.76 3.72 5.78 3.84 Ql73701N.001 20 SEP 2016 13:17 37 405235076 25:00.740 718.12 3.92 5.46 3.19 Ql83801N.001 20 SEP 2016 13:44 38 405235077 25:00.740 759.17 3.92 5.50 2.99 Ql93901N.001 20 SEP 2016 14:12 39 405235078 25:00.739 720.72 4.73 6.23 4.25 Q204001N.001 20 SEP 2016 14:39 40 1203624311 25:00.739 748.33 3.36 5.02 3.11 Q214101N.001 20 SEP 2016 15:07 41 1203624312 25:00.739 716.05 3.76 5.66 3.80 Q224201N.001 20 SEP 2016 15:35 42 1203624313 25:00.739 753.40 106.32 112.80 83.93 Page 2 Page 5506 of 5809 Instrument Type: Data Capture Date: FileNa{Tle: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 2 -J!l c :::s 0 (.) 1.5 -Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597417AO\SQ012101 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597417 AO.xis TC99 (1) PINK 1, REF, 25.01237: 755.15 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5507of5809 Instrument Type: Data Capture Date: FileName:;. File Info: ID: Comments: Sample, Rack-Pos, Time: *Quench: Start, End, X-Axis Channel Counts 3 2.5 -' U) 2 -c: ::s 0 0 1.5 Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 A\O\SQ022201 N .001.xls . M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 2, 405235061, 25.01237: 738.8 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5508 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 2.5 UJ 2 ... c: :I 0 . (..) 1.5 1 0.5 -Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 AO\SQ032301 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 3, 405235062, 25.01237: 708.3 . 200-600 SPECTRUM PLOT TC99 (1) 0 ....... 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5509 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus TUE 20 SEP 2016 5:29 M:\ls.SC\FILES\pink\597 417 A0\80042401 N.001.xls M:\LSC\FILES\pin k\597 417 AO\U597 417 AO.xis TC99 (1) PINK Sample, Rack-Pos, Time: 4, 405235063, 25.01237: 744.19 Quench: Start, End, X-Axis Channel Counts 3 -2.5 -2 .!! c :J 0 0 1.5 0.5 0 0 32 33 34 35 Page 5510of5809 50 200-600 SPECTRUM PLOT TC99 (1) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 AO\SQ0525Q1 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK Sample, Rack-Pas, Time: 5, 405235064, 25.01237: 743.23 Quench: Start, End, X-Axis
  • Channel Counts en -c: :::J 0 0 Page 5511of5809 2 -1.5 0.5 0 0 50 32 33 34 35 200-600 SPECTRUM PLOT TC99 (1) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Aack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 2.5 . 2 £l c: ::J 0 0 1;5 0.5 0 0 32 33 34 35 Page 5512of5809 50 100 0 0 0 0 Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 A0\80062601 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 6, 405235065, 25.01237: 738.75 200-600 SPECTRUM PLOT TC99 (1) 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 Instrument Type: Data Capture Date: *-FileName: File Info: ID: Comments: Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\13ink\597 417 AO\SQ072701N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK Sample, Rack-Pos, Time: 7, 405235066, 25.01237: 736.91 Quench: Start, End, X-Axis Channel Counts 3 2.5 -fl) 2 -c ::J 0 () 1.5 1 -0.5 -0 0 32 33 34 35 Page 5513of5809 50 200-600 SPECTRUM PLOT TC99 (1) 100 150 200 250 300 350 400' 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: fileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 -(/) 2 -c: :I 0 0 1.5 -Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pinJ<\597 417 A0\80082801 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 8, 405235067, 25.01235: 740.76 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5514of5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts ..'!! c: ::s 0 0 2 -1.5 1 0.5 -Quan tu I us TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 AO\SQ092901 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 9, .405235068, 25.01235: 724.32 200-600 SPECTRUM PLOT TC99 (1) 0 -f---.---..--L..¥1"-oU/l-.u&...,L.&..m'-'!'LJ ....... .__ 0 50 100 150 200 250 300 350 400 450 50Q
  • 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5515of5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 -(/) 2 -.... c ::I 0 0 1.5 0.5 -Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 AO\SQ103001 N .001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 10, 405235069, 25.01235: 745.26 200-600 SPECTRUM PLOT TC99 (1) 0 .............................. 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5516of5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597417AO\SQ113101 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK Sample, Rack-Pos, Time: .11, 405235070, 25.01235: 712.84 Quench: Start, End, X-Axis Channel Counts 3 2.5 -2 J!! c :l 0 0 1.5 1 -0.5 O* 0 32 33 34 35 Page 5517 of 5809 50 200-600 SPECTRUM PLOT TC99 (1) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 AO\SQ123201 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK Sample, Rack-Pos, Time: 12, 405235071, 25.01235: 696.37 Quench: Start, End, X-Axis Channel Counts 3 -2.5 -2 !? c :I 0 0 Page 5518of5809 1.5 1 -0.5 . 0 0 32 33 34 35 50 200-600 SPECTRUM PLOT TC99 (1) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: File Name: File Info: ID: Comments: Quantulus TUE .20 SEP 2016 5:29 M:\LS.C\FILES\pink\597 417 A0\80133301 N.001.xls
  • M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK Sample, Rack-Pos, Time: 13, 405235072, 25.01235: 747.39 Quench: Start, End, X-Axis Channel Counts 3 -2.5 !!! 2 c: :s 0 0 1.5 0.5 -.o 0 32 33 34 35 Page 5519of5809 50 200-600 SPECTRUM PLOT TC99 (1) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts J!! c ::s 0 0 2 1.5 -Quantulus TUE 20 SEP 2016 5:29 M:\LSC\F.ILES\pink\597 417 AO\SQ143401 N.001.xls M:\LSC\FILES\pink\597417 AO\U597 417 AO.xis TC99 (1) PINK 14, 405235073, 25.01233: 729.05 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5520 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 AO\SQ153501 N.001 .xis M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK Sample, Rack-Pos, Time: .15, 40523507 4, 25.01233: 744.62 Quench: Start, End, X-Axis Channel Counts 3 -2.5 2 -2l c :s 0 (.) 1.5 -1 0.5 0 0 32 33 34 35 Page 5521of5809 50 200-600 SPECTRUM PLOT TC99 (1) 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 0 0 0 0 Instrument Type: Data Capture Date: File Name: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts m s: ::s 0 (.) 2 -1.5 -Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 AO\SQ163601 417 AO\U597 417 AO.xis TC99 (1) PINK 16, 405235075, 25.01233: 749.76 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5522 of 5809 Instrument Type: Data Capture Date: FileName:
  • File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts fl) c ::::J 0 0 2 1.5 -1 0.5 !----.---.-__., ..... Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\5.97 417 AO\SQ173701 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 17, 405235076, 25.01233: 718.12 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 BOO 850 900 950 1000 32 0 33 0 34 0 *35 0 Page 5523of5809 Instrument Type:. Data Capture Date: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 .:!! c :::J 0 0 1.5 -1 0.5 0 0 32 33 34 35 Page 5524 of 5809 50 100 150 0 0 0. 0 Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 AO\SQ183801 N.001.xls M:\LSC\FILES\pink\597417 AO\U597 417 AO.xis TC99 (1) PINK 18, 405235077, 25.01233: 759.17 200-600 SPECTRUM PLOT TC99 (1) 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts J!l c ::J 0 0 2 1.5. Quantulus TUE 20 SEP 2016 5:29
  • M:\LSC\FILES\pink\597 417 A0\80193901 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 19, 405235078, 25.01232: 720.72 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5525 of 5809 Instrument Type: Data Capture Date: File(\Jame: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 2.5 .!!! c: :::s 0 0 1.5 -Quantulus TUE 20 SEP 2016 5:29 .M:\LSC\FILES\pink\597417 AO\SQ204001 N.001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 20, 1203624311, 25.01232: 748.33 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 0 Page 5526 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pos, Time: Quench: Start, End, X-Axis Channel Counts 3 -2.5 s r:: :J 0 0 1.5 0.5 -Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417AO\SQ21A101 N .001.xls M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 21, 716.05 200-600 SPECTRUM PLOT TC99 (1) 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 32 0 33 0 34 0 35 o* Page 5527 of 5809 Instrument Type: Data Capture Date: FileName: File Info: ID: Comments: Sample, Rack-Pas, Time: Quench: Start, End, X-Axis Channel Counts "' -c :J 0 0 20 10 5 0 0 32 33 34 35 Page 5528 of 5809 50 100 150 200 250 0 0 0 0 Quantulus TUE 20 SEP 2016 5:29 M:\LSC\FILES\pink\597 417 A0\80224201 N.001 .xis M:\LSC\FILES\pink\597 417 AO\U597 417 AO.xis TC99 (1) PINK 22, 1203624313, 25.01232: 753.4 200-600 SPECTRUM PLOT TC99 (1) 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 21-Sep-2016 Batch#---'-l S--'-) ]..____l(-'---'--( i_ Product: 1c$5 Date: 1/z,{ /; /, I Criteria: Sample Solids are less than or equal to 100 mq for GAB. Samples have been blank corrected (If required), Blank correction reaorted included {(f reaulred), If activity less than lOx MDA/MDC, error Is less than or equal to 1500/o of sample activity. If 11reater than 10* MDA/ MDC, error Is 40°/o or less. ilf hn(nm *hn Mn" I MOC:. e**nr (<: Instrument source check Is within limits, Instrument bkn chn*k Is within Hmlts. Method RDL/ LLD has been met. If duolicate activities are: Less than S* MDA/ MDC, then RPD Is 1000/o or less, If greater 5* MDA/ MDC, then RPD 200/o or less, If below the MDA/ MDC, the RPD Is 0%, Or meets the client's renuired RER acceatance criteria. Tracer yield is 15-125%
  • Carrier yield 25-1250/o, (Or meets the client's contract acceptance criteria). Method blank is less than the RDL/ LLD. CU rad samoles. < 50/o of lowest actlvitvl Yes No Comments I I *./ v ,-* v / GL-CHL-RAD-013Rev1 Page 1of1 Samnle was run within hold time. / <oo vs .<< /\<; <1 "i y '6 Samnle was correctlv oreserved If reaulred. Smears Taken for Radioactive batches. Method Spike and LCS are within 75-1250/o lror mnnts *he client's contract accentance criteria'. No blank soaces on data forms. A.II llne outs Initialed and dated. IJUn ------.,..,. .... A.ux data ls correct. Client Saeclal renulrements naae has been checked. Raw Data and t or soectrum are Included and nronerlv statused. MS, LCS, and Duplicate RPD/RER values uploaded to UMS and v****--**--i"'--' ..... (if Batch Data Excentlon Renorts fDER' comnleted If annl!cable. Batch Data Exception Reports (DER) second reviewed. Disnositlon verified to be comnleted. A.llnunt rorrectinn romnleted If reaulred. Review sample historical results If available {If REMP, results above MDC have been verified bv historical results recount or re-analvsis. l Page 5529 of 5809 I / . /J ff-i/' l/V A--,/ -v-/ N IJ--A) A----

GEL Laboratories LLC Form GEL-DER .. DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 21-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC DOE EML HASL-300, Tc-02-RC Solid . *-Batch ID: Sample Numbers: 1597414 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, ; 405235060 and 1203624305 were received and analyzed out of the method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 21-SEP-16 Lyndsey Pace 21-SEP-16 Page 1 Page 5530 of 5809 DER Report No.: 1559848 Revision No.: 2 Type: Process Client Code: MJWC 0 ......., Vo 00 0 \0 Prep Logbook The Determination of Technetium-99 Using Analytical Grade lXS Resin Batch ID: Analyst: 1597414 Christina Sanchez Method: Lab SOP: DOE EML HASL-300, Tc-02-RC Modified GL-RAD-A-059 REV#4 Instrument:
  • BAL-16107662 Sample ID Prep Date 405235041 !5-SEP-2016 12:28:40 Soil 405235042 15-SEP-2016 12:28:40 Soil 405235043 15-SEP-2016 12:28:40 Soil 405235044 15-SEP-2016 12:28:40 Soil 405235045 15-SEP-2016 12:28:40 Soil 405235046 15-SEP-2016 12:28:40 Soil 405235047 15-SEP-2016 12:28:40 Soil 405235048 15-SEP-201612:28:40 Soil 405235049 15-SEP-2016 12:28:40 Soil 405235050 15-SEP-2016 12:28:40 Soil 405235051 15-SEP-2016 12:28:40 Soil
  • 405235052 15-SEP-2016 12:28:40 Soil 405235053 15-SEP-2016 12:28:40 Soil 405235054 15-SEP-2016 12:28:40 Soil 405235055 15-SEP-2016 12:28:40 Soil 405235056 15-SEP-2016 12:28:40 Soil 405235057 15-SEP-2016 12:28:40 Soil 405235058 15-SEP-2016 12:28:40 Soil 405235059 15-SEP-2016 12:28:40 Soil 405235060 15-SEP-2016 12:28:40 Soil 1203624304 MB 15-SEP-2016 12:28:40 Soil 1203624305 DUP (405235041) 15-SEP-2016 12:28:40 Soil 1203624306 LCS 15-SEP-2016 12:28:40 Soil Reagent/Solvent Lot ID Description Amount 2280154.26 Hydrogen Peroxide 30% ACS Reagent IOmL 120LBS 30 Gallons 2402130.4 Ecoscint GL Scinlillation Solution 15mL 2418926 Quenching Agent .1 uL 2429641 RL-0. lM Hydrochloric Acid lOOmL 2441205 RL.-0.0lM Nilric Acid 20mL 2451825 JU..O.IM Nitric Acid 25mL TC2074-A tracer lmL Analytical Logbook version 111-04-2002 TYJ?e LCS Sample Id Description 1203624306 Technetium-99 SPIKE Dry or Wet Unadjusted Aliquot w w w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) 1.209 1.064 1.257 1.119 1.28 ' 1.094 1.244 0.936 1.298 1.008 1.224 0.996 1.301 1.032 1.222 0.942 1.212 0.984 1.282 1.14 1.23 1.013 1.215 1.027 1.211 0.843 1.205 0.986 1.254 1.012 1.218 0.83 1.229 0.895 1.296 1.039 1.265 1.113 1.278 1.155 1.155 1.223 1.077 1.155 Comments: Spike Pipe! ID: RAD-l.SC-2272418 Tracer Pipet ID: RAD-LSC-4099802 Serial Number 1621-B t'5 I Spike Amount Spike Units .I mL GEL Laboratories LLC Filename : TC99.XLS File type : Excel Version # : 1.2.16 Batch: 1597414 Analyst : CHR02061 Prep Date: 9/15/2016 Tc-99 Method Uncertainty : 0.0576 Geometry: 15ml Ecoscint Gl.J5ml DI H20/AG 1x8 Resin Sample Characteristics Sample Sample Aliquot Sample Aliquot St Dev. Sample Pos. ID G G Datemme 1 405235041.1 1.0640 3.3300E-03 11/30/201513:27 2 405235042.1 1.1190 3.3357E*03 11/3012015 13:53 3 405235043.1 1.0940 3.3331E*03 11/3012015 13:59 4 405235044.1 0.9350 3.3167E-03 11/301201513:50 5 405235045.1 1.0080 3.3242E*03 11/30/201514:15 6 405235046.1 0.9960 3.3229E-03 12171201510:02 7 405235047.1 1.0320 3.3267E-03 1217/201510:10 8 405235048.1 0.9420 3.3173E-03 1217/2015 13:28 9 405235049.1 0.9840 3.3217E*03 1217/201513:33 10 405235050. 1 1.1400 3.3379E-03 12171201513:42 11 405235051. 1 1.0130 3.3247E-03 1217/2015 13:02 12 405235052. 1 1.0270 3.3261E*03 1217/201513:11 13 405235053.1 0.8430 3.3070E*03 12111201514:24 14 405235054. 1 0.9860 3.3219E-03 121212015 14:51 15 405235055. 1 1.0120 3.3246E*03 121212015 14:59 16 405235056. 1 0.8300 3.3056E-03 12/212015 14:50 17 405235057.1 0.8950 3.3124E-03 12121201514:55 18 405235056. 1 1.0390 3.3274E-03 12/2/201515:00 19 405235059.1 1.1130 3.3351E-03 121161201512:26 20 405235060.1 1.1550 3.3395E-03 12116/2015 12:33 21 1203624304.1 1.1550 3.3395E-03 911512016 0:00 22 1203624305.1 1.ono 3.3314E-03 11/30/2015 13:27 23 1203624306.1 1.1550 3.3395E-03 911512016 0:00 ,E1597414 Technetium-99 Solid Tracer SIN: Tracer Exp Date : Tracer Volume Added: Tracer Calculations Tracer Ref. Activity (CPM) 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 30227 Page 1 TC2074-A 9/1612016 1.00 Tracer Ref. Count Uncertainty (%) 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% Tracer Samp. Activity (CPM) 29715 29324 28808 29111 29715 28745 27982 27907 28777 28810 28703 12790 29193 27995 27206 27762 -29229 27967 28995 29103 29543 28833 28270 Procedure Code : Parmname: Required MDA : Tc*99 Abundance : Hafflife of Tc-99 : Tracer Samp. Count Uncertainty (%) 0.94% 0.95% 0.96% 0.95%

0.94% 0.96% 0.95% 0.95% 0.96% 0.94% 0.94% 0.98% 0.96% 0.96% 0.95% 0.94% 0.94% 0.96% 0.94% 0.94% 0.95% 0.95% 0.96% LSC99TCS Technetium-99 5 pCi/G 1.00 211100 years Tracer Tracer Aliquot Aliquot (ml) StDev. (ml) 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 Pipe!, 0.1 ml Stdev: +/-0.000200 ml Pipe!, 0.5 ml Stdev: +/-0.001000 ml Pipe!, 1 ml Stdev : +/-0.002000 ml Analytical SOP: GL-RAD-A-059 Instrument SOP: GL-RAD-1-004 Count raw Data Counting Rack Time Quench# Gross* Pos. # {min.) cpm 1 19-2 15 167.9 14.73 2 19-3 15 171.3 16.2 3 19-4 15 176.8 16.27 4 19-5 15 216.6 14.2 5 19-6 15 199.6 14.27 6 19-7 15 183.1 16.87 7 19-8 15 174.1 14.8 8 19-9 15 175 12.4 9 19-10 15 166.7 14.27 10 19-11 15 166.5 13.73 11 19-12 15 169.9 14.13 12 20-3 90 166.1 14.48 13 18-2 15 205.5 15 14 18-3 15 168.5 13.8 15 18*6 15 163.7 14.6 16 18-5 15 215.8 14.53 17 18-4 15 198.4 13.93 18 18-9 15 184.9 14.27 19 18-8 15 178.5 15 20 18-7 15 174.4 12.4 21 18-10 15 168 14.93 22 18-11 15 176.3 15 23 18-12 15 172.5 122.67 Bkg Count Corrected Count Bkg Time Bkg Bkg Start cpm {min.) Quench# cpm Datemme 14.29 90 170.6 14.3093 9/20/201613:36 14.29 90 170.6 14.2848 9/2012016 13:55 14.29 90 170.6 14.2404 9/201201614:11 14.29 90 170.6 13.8653 9/20/201614:28 14.29 90 170.6 14.0229 9/20/2016 14:44 14.29 90 170.6 14.1842 9120/2016 15:01 14.29 90 170.6 14.2628 9/20/2016 15:17 14.29 90 170.6-14.2555 9/20/2016 15:34 14.29 90 170.6 14.3174 9120/2016 15:50 14.29 90 170.6 14.3187 9/20/201616:06 14.29 90 170.6 14.2951 9120/2016 16:23 14.29 90 170.6 14.3213 9/20/2016 12:07 14.29 90 170.6 13.9653 9/20/2016 16:39 14.29 90 170.6 14.3051 9/20/2016 16:56 14.29 90 170.6 14.3361 9120/2016 17:45 14.29 90 170.6 13.8719 912012016 17:29 14.29 90 170.6 14.0348 9/20/2016 17:12 14.29 90 170.6 14.1673 9/20/2016 18:35 14.29 90 170.6 14.2258 9120/2016 18:18 14.29 90 170.6 14.2604 9/20/2016 18:02 14.29 90 170.6 14.3086 9/20/2016 18:51 14.29 90 170.6 14.2447 9/20/2016 19:08 14.29 90 170.6 14.2755 9/20/2016 19:24 E1S97414 Calculated Calibration Data Detector Background Sample Sample Calibration Detector Efficiency Count Sample Recovery Recovery Counted Calibration Due Efficiency Error Background Start Decay % Error% on Date Date {cpm/dpm) (cpm.'dpm) Position# Datemme 1.000 98.3% 0.73% LSCSILVER. 7n/2016 6/30/2017 0.5575 0.00792 20-1 9/20/2016 10:33 1.000 97.0% 0.73°/o LSCSILVEA 7/7/2016 6130/2017 0.5576 0.00792 20-1 9/20/2016 10:33 1.000 95.3°/o 0.73% LSCSILVER 71712016 6130/2017 0.5570 0.00792 20-1 9/20/2016 10:33 1.000 96.3% 0.73% LSCS!LVER 7/7/2016 6/30/2017 0.5249 0.00792 20-1 9/20/2016 10:33 1.000 98.3% 0.73% LSCSILVER 7/712016 6/30/2017 0.5445 0.00792 20-1 9/20/2016 10:33 1.000 95.1% 0.73% LSCSILVER 717/2016 6130/2017 0.5552 0.00792 20-1 912012016 10:33 1.000 92.6% 0.73% LSCSILVER 7/712016 6/30/2017 0.5574 0.00792 20-1 912012016 10:33 1.000 92.3% 0.73% LSCSILVER 7/7/2016 6130/2017 0.5573 0.00792 20-1 9/20/2016 10:33 1.000 95.2% 0.73% LSCStLVER 717/2016 6130/2017 0.5574 0.00792 20-1 9/20/2016 10:33 1.000 95.3% 0.73% LSCSILVER 717/2016 6/30/2017 0.5574 0.00792 20-1 9120/2016 10:33 1.000 95.0% 0.73% LSCSILVER 717/2016 6130/2017 0.5576 0.00792 20-1 9/2012016 10:33 1.000 42.3% 0.74% LSCSILVER 7/712016 6/30/2017 0.5573 0.00792 2D-1 912012016 10:33 1.000 96.6% 0.73% LSCSILVER 717/2016 6130/2017 0.5387 0.00792 20-1 9/20/2016 10:33 1.000 92.6% 0.73% LSCSILVER 7/7/2016 6130/2017 0.5575 0.00792 20-1 9/20.'2016 10:33 1.000 90.0% 0.73% LSCSILVER 7/7/2016 6/30/2017 0.5569 0.00792 20-1 9/20/2016 10:33 1.000 91.8% 0.73% LSCSILVER 7/712016 613012017 0.5260 0.00792 20-1 9/20/2016 10:33 1.000 96.7% 0.73% LSCSILVER 7/7/2016 613012017 0.5456 0.00792 2D-1 9/20/2016 10:33 1.000 92.6% 0.73% LSCSILVER 717/2016 6/30/2017 0.5544 0.00792 2D-1 9/20/2016 10:33 95.9% 0.73% LSCSILVEA 7/7/2016 6/30/2017 0.5566 0.00792 20-1 9/20/2016 10:33 1.000 96.3% 0.73% LSCSILVER 717/2016 6/3012017 0.5574 0.00792 20-1 9/20/2016 10:33 1.000 97.7% 0.73% LSCSILVEA 7/7/2016 6130/2017 0.5575 0.00792 .A 20-1 9/20/201610:33 1.000 95.4% 0.73% LSCSILVER 7/7/2016 6/30/2017 0.5571 0.00792 20-1 9/201201610:33 1.000 93.5% 0.73% LSCSILVER 71712016 6/30/2017 0.5576 0.00792 20-1 9/20/201610:33 Page2 Notes: 1 -Resutts are decay corrected to Sample Date/Time 2 -Reference date for Spike Activity (dpmlml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Datemme * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MOA MDA Cone. Error Pos. . pCi/G pCi/G pCi/G pCl/G pCl/G % 1 1.8988 1.3406 5 2.8356 0.3250 253.91% 2 1.8276 1.2903 5 2.7294 1.4252 58.12% 3 1.9019 1.3428 5 2.8406 1.5741 54.94% 4 2.3036 1.6264 5 3.4431 0.3187 313.42% 5 2.0314 1.4342 5 3.0353 0.2063 425.75% 6 2.0964 1.4801 5 3.1315 2.3007 42.18% 7 2.0757 1.4655 5 3.1002 0.4543 199.22% 8 2.2801 1.6097 5 3.4054 -1.7244 53.50% 9 2.1211 1.4975 5 3.1676 -0.0409 2224.29% 10 1.8289 1.2912 5 2.7313 -0.4379 176.08% 11 2.0633 1.4567 5 3.0813 -0.1387 635.31% 12 2.4448 1.7260 5 3.5140 0.2952 356.43% 13 2.4940 1.7608 5 3.7270 1.0627 103.88% 14 2.1744 1.5351 5 3.2472 .-0.4469 205.63% 15 2.1849 1.5426 5 3.2628 0.2344 16 2.7189 1.9195 5 4.0638 0.7393 161.02% 17 2.3224 1.6396 5 3.4700 -0.0999 994.22% 18 2.0657 1.4584 5 3.0856 0.0868 1024.98% 19 1.8576 1.3115 5 2.7746 0.5868 139.00% 20 1.7832 1.2590 5 2.6633 -1.3520 53.36% 21 1.7593 1.2421 5 2.6273 0.4447 172.91% 22 1.9302 1.3627 5 2.8829 0.5945 142.49% 23 1.8362 1.2964 5 2.7423 81.0669 2.89% E1597414 Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: NJA NJA NJA NJA LCS SIN : 1621-B LCS Exp Date : 115/2017 LCS Activity (dpm/ml): 1911.38 LCS Volume Added (ml): 0.1 O 2SIGMA 2SIGMA Net Count Net Count Counting Total Prop. Rate Rate Error Uncertainty Uncertainty CPM CPM pCl/G pCi/G 0.4207 1.0682 1.6173 1.6177 1.9152 1.1130 1.6233 1.6315 2.0296 1.1149 1.6948 1.7044 0.3347 1.0492 1.9577 1.9581 0.2471 1.0522 1.7216 1.7218 2.6858 1.1324 1.9012 1.9196 0.5372 1.0701 1.7741 1.7749 -1.8555 0.9925 1.8078 1.8079 -0.0474 1.0538 1.7818 1.7818 -0.5887 1.0365 1.5112 1.5112 -0.1651 1.0492 1.7270 1.7270 0.1587 0.5657 2.0622 2.0625 1.0347 1.0748 2.1636 2.1670 -0.5051 1.0387 1.8012 1.8012 0.2639 1.0642 1.8524 1.8526 0.6581 1.0596 2.3331 2.3347 -0.1048 1.0414 1.9473 1.9473 0.1027 1.0530 1.7430 1.7431 0.7742 1.0761 1.5987 1.6001 -1.8604 0.9925 1.4137 1.4137 0.6214 1.0744 1.5072 1.5081 0.7553 1.0762 1.6602 1.6616 108.3945 2.8873 4.2324 10.2383 Pages Sample Sample Nominal QC Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235041.1 DUP

  • 0.0% LCS 74.5437 108.8%

ASSAY 16-Sep-16 12:58:20 Protocol id 12 TC99_REC Time limit 500 Count limit 10000 Isotope Tc-99m Protocol date 23-Sep-13 14:21:59 Run id. 21 POS RACK BATCH TIME COUNTS CPM ERROR % RECOVERY COUNT TIME 1 69 1 22 11042 30226.7 0.95 12:58:26 2 69 2 23 11337 29714.5 0.94 98.31 12:59:00 3 69 3 23 11176 29324.3 0.95 97.01 12:59:35 4 69 4 23 10968 28808.1 0.96 95.31 13:00:10 5 69 5 23 11071 29110.9 0.95 96.31 13:00:45 6 37 6 23 11282 29714.9 0.94 98.31 13:01:34 7 37 7 23 10903 287 45.2 0.96 95.10 13:02:09 8 37 8 24 11064 27982.4 0.95 92.58 13:02:44 9 37 9 24 11022 27907.2 0.95 92.33 13:03:19 10 37 10 23 10878 28776.9 0.96 95.20 13:03:56 11 74 11 24 11346 28809 .8 0.94 95.31 13:04:44 12 74 12 24 11291 28702.8 0.94 94.96 13:05:20 13 74 13 50 10492 12790.4 0.98 42.31 13:05:56 14 74 14 23 10971 29192.5 0.96 96.58 13:06:58 15 *74 15 24 10967 27994.9 0.96 92.62 13:07:33 16 70 16 25 11086 27206.3 0.95 90.01 13:08:22 17 70 17 25 11298 27762 0.94 91.85 13:08:59 18 70 18 24 11404 29228.8 0.94 96.70 13:09:36 19 70 19 24 10908 27986.9 0.96 92.59 13:10:12 20 70 20 24 11287 28995.3 0.94 95.93 13:10:48 21 72 21 24 11311 29103 0.94 96.28 13:11:38 22 72 22 23 10990 29542.8 0.95 97.74 13:12:13 23 72 23 24 11182 28833.2 0.95 95.39 13:12:48 24 72 24 24 10951 28270.1 0.96 93.53 13:13:24 END OF ASSAY Batch #1597 414 Page 1 of 1 Page 5535 of 5809 ][ D 91 UBER: 7 PRESET TIME : DATn CALC COUNT BU-IN!.\ : nm PHASE SCil'JTILLATO LClW L.EVEL S11Zt.1Z11Z1 CPfvl 1\1(] NO LIQUID NO )5) 7tlti

  • r.YES SAMPLE REPEATS: : ND REPLICATES 1 AQC NCI CYCLE REPEATS : LUMEX:YES LOl.J SAMPLE 0 HALF LIFE CORRECTION DATE: PAGE: 1 * ;:::1zi SEP 21z11G 11:0'3 1 " STD " 1 DISfZ " OFF " none CHAN: 3i:'.1Zt.0 -6:l1Z1.0 1..ERROR:: f:.1Z11Z1 FACTOR: 1. IZllZllZI e11z11z1 BI{ G. 1 .. 1Zte11Z11Z11Z11z1 Bl .. (G. 121 .. 0 .... rn1z11z1 .. e1 2 .. 121121 SAM POS ND e.,,Jl [::121---:1. MISSING I 1,,-3 21z1 .. *-3 QPQP Page 5536 of 5809 TIME H# MIN 91z1 .. 01i'.I l70 .. G SAMPLE 9121,.121121 166.1 WIND1 CPM %ERROR 14.46 WIND 2 LUMEX ELAPSED CPM %ERROR % TIME 41.37 3.AIZI 7 .03 187 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 14 12 -10 (/) 8 -c: :::I 0 (.) 6 2 -0 100 Page 5537of5809 200 300 20 Sep 2016 10:33:10 20 Sep 201612:03:36 807092020-1 A.XLS U07092020-1 A.XLS Log Counts 07 TC-99 SILVER LIQUID 1 170.6 320 0 20-1 3690 610 990 SPECTRUM PLOT USER 07 -TC-99 400 500 90.00 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 14 12 .!!? 8 . c: ::::J 0 () 6 4 . 2 0 -0 100 Page 5538 of 5809 200 300 20 Sep 2016 12:07:06 20 Sep 2016 13:37:31 S07092020-3A.XLS U07092020-1 A.XLS Log Counts 07 TC-99 SILVER LIQUID 3 166.1 320 0 20-3 3723 610 990 SPECTRUM PLOT USER 07 -TC-99 400 500 90.00 600 Channel Number (Log) 700 800 900 J ']l/ /L/ Pf.1GEr. 1. JC T C ***---:;:31 ":31 i::'.0 SEP i:::'.IZtlE. 1A::l7 USERrr E, COMMENTrrSILVER PRESET TIME . 15.IZllZI Df.ffA CALC CPIYI Htf. ::YES SAMPLE REPEATS: 1 PRINTER " STD COUNT BLAN! .. . NO I .. NO REPUCfHES l. :EDIT . TWO PHABE NO AQC " NO CYCLE REPEATS : 1 DIS!<. " OFF .. .. SCINTIL.LATO Fh LIQUID LIJMEX:YES LOt..J SAMPLE RE.J: QI LOW LEVEL NO H(-H *. F UFE CORRECTION DATE: none CHAl\lrr 321Z1 .. 0 -** GilZl.0 '/..EFHWR: ;:;:,1N?.1 L1zi1ziiz11z11z11z1 BKCJ.. CHANrr 1Z1.1Zl -** 1.1z11z11zi .. 1z1 2 .. 1ZUZ1 FACTOR: 1 .. e11211z11z1izuz1 Bl<G. SUB:: SAM POS TIME H# WIND1 WIND2 LUMEX ELAPSED NO MIN CPM Y.ERROR CPM Y.ERROR r. TIME MISSING SAMPLE I *:::1 19****i::'. 15 .. IZllZl 1G7.9 llt,73 1.3u*!.1*5 45.47 7.13G 5.4*1. **-z..., 1':3-* 3 16.20 1.2n8::s 46.07 7 .. 81 5 .. 37 Lt. 19---4* 15.IZllZI 17C .. B 15.27 12.BIZI 43.13 8.11. 5.21 4.(3 .. 8/.1. 5 19--*5 15.0121 i::'.16.E, 14.20 13.71Zl 39.57 B * .!.tl1 G.(i'.13 E,5 .. 27 ,_s F., 19--G 15.IZllZl 1 '39.6 14.27 B.G7 38.47 8.GIZI G .. 4*8 81.73 i 7 19--7 15.IZllZt 1.83 .. 1 16.87 42.93 8 .. 18 7.EA 9f:l.21 7 /:) 19**-8 j5.017.I 17-<f.1 14.80 l3uLf*i:;:: 43.73 81112'3 5.7tZI :L:l.'+ .. G7 t 9 19*-*9 15 .. 1Z11Z1 1.75.IZI 12.40 11., .* c.c. 38.27 B .. G!S 7.11 131 .. 11 1121 19**-1121 15.1Z10 166.7 14*.27 13 .. 67 44.27 8.IZll 1..!1*7 .. 57 /O:l.1 19*****H 15.1z11z1 1.GE,.5 13.73 l3 .. 93 42.20 13.E:G 7.59 1Ci.1 .* iz13 II 15.IZllZI 169 .. 9 14.13 13.7Lf 39.53 7 18121.AB MISSING SAMPLE /J j.Li. l8-***;2 l5.IZllZI 21215.5 15.00 13'133 39.80 B.L1A r 19'7 :in,.;!-..:!* /!fl5 18*-**3 15.12)0 1C8.5 13.80 13 .. 91Z1 39.53 8uL1-7 G.11+ 2l3n1+5 ./11G 18****Lt. :l.5.@ZI 198.4 13.93 1 o-, 40.13 8.51ZI BAIZI i229.9:l ...:!J1, ..::, '\'p7 Hl-*5 15.121121 215 .. 8 14.53 :l.31155 41.07 8.39 8 .. llZI i2L1.E,.38 1 18*-*6 15 .. IZ!IZJ 1£..3.7 14.60 13u51 41.27 B.3121 E, .. ;:::E,;=: .. 84 la*-7 15.@.(J 17L1-,J1 12.40 1A .. E.C 35.53 8.93 8.E,8 279.3:l 18--*B :L5.1Z11Z1 :L78.5 15.00 j'"\ ....,, ..... 42.33 7.5G ... ..::1-.::i. 21. 18--*9 1.5.1Z11Z1 j_O.c'.1 .. 9 14.27 13.57 41.13 7.47 312 .. i-=:5 I ...... -. 18--:llZI l5 .. 1ZJQ) lG8.1Z1 14.93 l3,.3(J 43.07 B.13 5A8 '1-z:i-:;:::3 18--*11 15.f.WZt 176.3 15.00 l.31133 40. 93 8ti3-7 7 ui=:8 v-3 ;::4. 15,.IZllZI 122.67 L1 .. E.G 164.BfZJ Lh!ZIC l.':34 361..EA QPG1P Page 5539 of 5809 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 Cf) "E 3 () 2 1 0 -0 Page 5540of5809 100 200 300 20 Sep 2016 13:38:50 20 Sep 2016 13:54:15 S06092019-2A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 2 19-2 167.9 682 320 610 0 990 15.00 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 -.!!l § 3 0 (.) 2 1 -0 0 Page 5541of5809 100 200 300 20 Sep2016 13:55:16 20 Sep 2016 14:10:40 S06092019-3A.XLS U06092019-2A.XLS Log Counts 06 Tq-99 SILVER LIQUID 3 19-3 171.3 691 320 610 0 990 15.00 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, .End:
  • 5 4 4 (/) 3 -c ::i 0 02 2 1 -0 0 Page 5542 of 5809 100 200 300 20 Sep 2016 14:11:43 20 Sep 2016 14:27:07 S06092019-4A.XLS U06092019-2A.XLS Log Counts 06 LIQUID 4 19-4 176.8 647 320 610 0 990 15.00 SPECTRUM PLOT USER 06
  • TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 4 3 en 3 -'E :J 0 (.) 2 -2 1 0 -0 Page 5543of5809 100 200 300 20 Sep 2016 14:28:09 20 Sep 2016 14:43:33 S06092019-5A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 5 19-5 15.00 216.6 595 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc,99 -Start, End: Win2: -Start, End: 6 5" 4 22 § 3 0 () 0 0 Page 5544 of 5809 100 200 300 20 Sep 2016 14:44:37 20 Sep 2016 15:00:00 S06092019-6A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 6 19-6 199.6 577 320 610 0 990 15.00 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id if "-User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 4 3 -Ul 3 'E ::I 0 (.) 2 2 1 0 Page 5545 of 5809 100 200 300 20 Sep 2016 15:01 :06 20 Sep 2016 15:16:29 S06092019-7 A.XLS U06092019-2A.XLS Log Counts 06 SILVER LIQUID 7 19-7 15.00 183.1 644 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 -en 'E 5 3 -() 0 Page 5546 of 5809 100 200 300 20 Sep 2016 15:17:33 20 Sep 2016 15:32:57 S06092019-8A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 8 19-8 15.00 174.1 656 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 -4 3 (/) 3 -E ::J 0 (.) 2 2 1 0 -0 . 100 Page 5547 of 5809 200 300 20 Sep 2016 15:34:00 20 Sep 2016 15:49:23 S06092019-9A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 9 19-9 15.00 175.0 574 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 ' Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 -4 3 2 0 -0 Page 5548 of 5809 100 200 300 20 Sep 2016 15:50:27 20 Sep 2016 16:05:51 S06092019-1 OA.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 10 19-10 15.00 166.7 664 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) . 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number _user Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 -4 3. 21 3 c :::J 0 (.) 2 2 0 Page 5549 of 5809 100 200 300 20 Sep 2016 16:06:55 20 Sep 2016 16:22:19 S06092019-11A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 11 19-11 15.00 166.5 633 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 4 -3 2 1 i........l!ldll-0 Page 5550 of 5809 100 200 300 20 Sep 2016 16:23:22 20 Sep 2016 16:38:45 S06092019-12A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 12 169.9 320 0 19-12 593 610 990 15.00 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample,. Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 -'4 3 -(/) 3 -"E ::i 0 02 2 1 0 -0 Page 5551of5809 100 . 200 300 20 Sep 2016 16:39:54 20 Sep 2016 16:55:19 S06092018-2A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER* LIQUID 14 18-2 205.5 597 320 610 b 990 15.00 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Oate User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 4 3 -.!!! 3 c: ::i 0 (.) 2 0 Page 5552 of 5809 100 200 300 20 Sep 2016 16:56:20 20 Sep 2016 17:11 :44 S06092018-3A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 15 18-3 15.00 168.5 593 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 -C/l 'E ::I 3 -0 {) 2 0 -0 100 Page 5553 of 5809 200 300 20 Sep 2016 17:12:48 20 Sep 201617:28:12 S06092018*4A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER
  • LIQUID 16 18*4 15.00 198.4 602 320 610 0 990 SPECTRUM PLOT USER 06
  • TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capt1,1re Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 .$!l § 3 8 2 -100 Page 5554of5809 200 '300 20 Sep 2016 17:29:16 20 Sep 2016 17:44:40 S06092018-5A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 17 18-5 15.00 215.8 616 320 610 0 990 -------*----------. SPECTRUM PLOT USER 06 -TC-99 400 500 600 700 800 900 Channel Number (Log)

Sample Count Start Time: Data Capture D;:ite User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 6 5 4 J!l § 3 -0 () 0 Page 5555 of 5809 100 200 300 20 Sep 2016 17:45:43 20 Sep 2016 18:01 :07 S06092018-6A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 18 18-6 15.00 163.7 619 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 . Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment ' Scintillator $ample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 -4. 3 1 0 Page 5556 of 5809 100 200 300 20 Sep 2016 18:02:12 20 Sep 2016 18:17:36 806092018-7 A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 19 18-7 15.00 174.4 548 320 610 0 990 SPECTRUM PLOT USER Ofr-TC-99 400 500 .600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 4 3 ,gl 3 c: ::J 0 () 2. 2 0 Page 5557 of 5809 100 200 300 20 Sep 2016 18:18:40 20 Sep 2016 18:34:04 S06092018-8A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 20 18-8 15.00 178.5 635 320 610 0 990 S P EC TR U M P L*O T USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 4. 3 .!8 3 c :J 0 () 2 2 1 0 0 Page 5558 of 5809 100 200 300 20 Sep 2016 18:35:08 20 Sep 2016 18:50:33 S06092018-9A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 21 15.00 184.9 617 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 5 4 4 3 -en 3 'E ::J 0 (.) 2 0 Page 5559 of 5809 100 200 300 20 Sep 2016 18:51:36 20 Sep 2016 19:07:00 S06092018-1 QA.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 22 168.0 320 0 18-10 646 610 990 15.00 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pos, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 7 6 5 -(/) 4 E ::i 0 u3 0 Page 5560 of 5809 100 200 300 20 Sep 2016 19:08:03 20 Sep 2016 19:23:27 S06092018-11A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 23 18-11 15.00 176.3 614 320 610 0 990 SPECTRUM PLOT USER 06 -TC-99 400 500 600 Channel Number (Log) 700 800 900 Sample Count Start Time: Data Capture Date User Filename Spectrum Type User Number User Id User Comment Scintillator Sample, Rack-Pas, Time: H#, Total Counts: Win1: Tc-99 -Start, End: Win2: -Start, End: 14 12 10 -J!l 8 c: ::J 0 (..) 6 4 2 0 100 Page 5561of5809 200 300 20 Sep 2016 19:24:31 20 Sep 2016 19:39:55 S06092018-12A.XLS U06092019-2A.XLS Log Counts 06 TC-99 SILVER LIQUID 24 172.5 320 0 18-12 2472 610 990 SPECTRUM PLOT USER 06 -TC-99 400 500 15.00 600 Channel Number (Log) 700 800 900 l **i Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist 21-Sep-2016 Batch# Product:,_.Ll.._j __ , Yes No Comments Samole Solids are less than or eoual to 100 ma for GAB. ('..,\4-Samples have been blank corrected (If required). IJ;y Blank correction reoorted Included (If reoulred). If activity less than lOx MDA/MDC, error Is less than or equal to 150% of sample activity. [f greater than 10* MDA/ MDC, error Is 40% or less. v ff holn ... *ho MDA I error le nl<av Instrument source check Is within limits. Instrument bko check Is within limits. / Method RDL/ LLD has been met. / If duplicate activities are: Less than 5* MDA/ MDC, then RPD Is 100% or less, If greater 5* MDA/ MDC, then RPD 20% or less, / If below the MDA/ MDC, the RPD Is 0%, Or meets the client's reoulred RER acceotance criteria. Tracer yield Is 15-125%

  • carrier yield 25-125%. / (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. / llTf r:ut ,,. "'Ofa Of ln...,oe> Samole was run within hold time. / 'bl.4lit Samolc was correctlv nreserved if reoulred. th-Smears Taken for Radioactive batches. Method Spike and LCS are within 75-125% . fnr moo*e the rlfAnt'S aCCf>ntance criteria). j No blank spaces on data forms. / All line outs Initiated and dated. :Nn
  • in iDrrnr'C! !:9rn Aux data Is correct. / Client Soeclal reaulrements oaoe has been checked. / Raw Data and I or snectrum are Included and nronerlv statused. ,/ MS, LCS, and Duplicate RPD/RER values uoloaded to UMS and v I""'"""' V"rlfled , ... ,. rnmnJ*>><> (if *1 L h-a-*-h nn>n*n" :n>n rnro v' \ S<o \ \ P1ll Batch Data Exception Reoorts (DER) comoleted If aoolicablc. / DbU, I 51..o \lfJ--( Batch Data Exception Reports (DER) second reviewed, ./ ll '?H Dlsoosltlon verified to be comoleted. Allnun> Correction comn*eted If reoulr .. d. Review sample historical results If available J (If REMP, results above MDC have been verified bv historical results recount or re-analvsls.) Primary Review Performed By: __ __ ____ _ Secondary Review Performed By:__ 09/30/16 @ \l00 Page' 5"562 of 5809 GL-CHL-RAD-013 Rev 1 Page 1 of 1 GEL Laboratories LLC Form GEL-DER DER Report No.: 1561184 Revision No.: o! DATA EXCEPTION REPORT of Mo.Day Yr. Division: Quality Criteria: Type: 25-SEP-16 Radiochemistry Specifications Process Instrument Type: Test I Method: Matrix Type: Client Code: LSC DOE EML HASL-300, Pu-11-RC Solid MJWC . *-Batch ID: Sample Numbers: 1596422 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Other *Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071,405235072,405235073,405235074, 405235075,405235076,405235077,405235078,and 1203621773were received and analyzed out of holding. 2. The sample does meet the tracer yield requirement, the detection limits, and its tracer peak is within the Pu-242 region of interest. Reporting 2. Sample 1203621774 does not meet the resolution requirement of results. having a full width half maximum of 100 keV or less for the Pu-242 tracer. Originator's Name: Data Validator/Group Leader: Melanie Aycock 25-SEP-16 Jessica Davis 30-SEP-16 Page 1 Page 5563 of 5809 Pu-241 Queue Sheet 07-SEP-16 Batch#: 1596422 Analyst:KXB2 First Client Due Date: 04-0CT-16 Internal Due Date.30-SEP-16 Tracer LCS Isotope: Pu-241 Tracer Code: \110 -*A Expiration Date: 0 -i:,-\ 1 Vol: 0. \ Solid Sample Dissolution by: LCS Code: \U\O"' e, Expiration Date: O. \ Spike faotope: Pu-241 PrepDate: Spike Code:.______ Expiration Date: Vol:___ Cocktail Initials: Pipet ID: VQ4001.;:t:. Balance ID: t{.e\O /(J &v . WeW5rY Hazard Min Collection Label Aliqiiof LSC Rack# Alpha Spec Det# 405235061-1 5.lB.R.2.2 405235062-1 5.2A.R.l.2 405235063-1 . 405235064-1 5.2A.R.l.4 405235065-1 5.2A.R.2.3 405235066-1 5.2A.R.2.4 405235067-1 5.2A.R.6.2 4052350684 5.2A.R.4.2 405235069-1 5.2B.R.1.4 405235070-1 5.2B.R.3.2 405235071-1 5.2B.R.4.2 405235072-1 5.2B.R.2.4 405235073-1 5.2B.R.8.2 405235074-1 5.3A.R.1.3 405235075-1 5.4A.R.1.3 405235076-1 5.4A.R.4.2 405235077-1 5.SA.R.1.3 405235078-1 5.6A.R.1.3 1203621772-1 r.m for batch 1596422 1203621773-1 5.1B.R.2.2(405235061DUP) 1203621774-1 LCS for batch 1596422 SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAl'vlPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAi'vlPLE SAMPLE SA.i'\fPLE MB DUP LCS 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCilg 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCi/g 15 pCilg 15 pCi/g 15 pCi/g 15 pCilg 15 pCi/g SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL MJWCOOl .MJWCOOl MJWCOOl l\1JW<;001 MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl MJWCOOl l>UWCOOl l>UWCOOl MJWCOOl ll*1JWC001 QC ACCOUNT QC ACCOUNT QC ACCOUNT l11strument Used: LS6000 (Red) 7065155, LS6500 (Blue) 7067083, LS6500 (Green) 7067404, Wallac (Yellow) 4140127, LS6000 (Br, wn) 7060655, LS6500 (Gold) 7070506, Purple 7069123, Silver 7060656, Wallac (White) 4140299, (Teal) 414042"1;. Wallac (Gray) 4150033, 7069693 (Mocha) GEL lAboratories LLC, Ra we iemistry Division 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 14-DEC-15 11-DEC-15 11-DEC-15 16-DEC-15 11-DEC-15 11-DEC-15 15-DEC-15 11-DEC-15 15-DEC-15 16-DEC-15 ll*DEC-15 17-DEC-15 17-DEC-15 14-DEC-15 1 I I"" ,_l ' [, 1 I \v,b lf i -d-2 65 z I 2--I °t\-:3> _* ___ q.fL __ i 3 !-r :..y u1 1 4 1 Lf. i (). t (7 I °t 1 u o 1 ! l&ffil i _:; %-1 7 i 1 i O.-s-ffl I c11 :-¥ 8 rs !'().SCA : <'.\1 -I 9 I q i 10 I Lo I k&tA l 91-_:J 11 nT i {). J; l& I s I -{j 12 LJ2.. I a . .S-{S g 1 13 1 ,?;> Ko 1 14 J Q. SC 1 c.i i -+ t I i 15 i *
  • l QSDIS 4 \ iJ. J 16 c:-11-s ! ____ r_j_J 11 1 a 1 e. s lo °Ir -10 'K'..., i rs i
  • i c1 kfl s _j 19 i . I . 51 I q H2... 'l ! --1 J:Y rn* i ! o, L-t7o i PrJ '1-l'f-t lf Bkg Rack #:.----'Cf'-'-/ -_l _ Data Reviewed By: '1,41J),w '1/..2.fh l. Page 1 oil Rlename PU241.XLS File type Excel version # 1.3.4 Batch : 1596422 Analyst : KXB2 Prep Date : 9/1512016 Method Uncertainty : 0.0839 Geometry: 2ml Dl/1 droo HN03/13ml Ecoscint Ultra Sample Characteristics Sample Sample Aliquot sample Afiquot StDev. Sample Pos. ID G G Datemme 1 405235061.1 0.5140 3.2727E*03 12/14/2015 13:47 2 405235062. 1 0.5150 3.2728E-03 12/14/201513:10 3 405235063.1 0.5180 3.2731E-03 12/14/2015 13:15 4 405235064.1 0.5170 3.2730E-03 12/14/2015 13:25 5 405235065.1 0.5070 3.2720E*03 12/14/2015 13:56 6 405235066.1 0.5090 3.2722E-03 12/14/2015 14:00 7 405235067. 1 0.5080 3.2721E-03 12/11/2015 11:30 8 405235068.1 0.5090 3.2722E-03 12/11/2015 10:27 9 405235069.1 0.5050 3.2718E-03 12/16/2015 12:45 10 405235070.1 0.5090 3.2722E-03 12/11/201510:10 11 405235071. 1 0.5150 3.2728E-03 12/11/2015 10:25 12 405235072.1 0.5130 32726E-03 12/15/2015 13:35 13 405235073 .1 0.5050 3.2718E*03 12/11/201511:35 14 405235074.1 0.5010 3.2713E-03 12/15/2015 14:10 15 405235075.1 0.5080 3.2721E-03 12/16/2015 9:31 16 405235076.1 0.5120 3.2725E-03 12/11/2015 14:19 17 405235077.1 0.5100 3.2723E-03 12/17/201513:30 18 405235078.1 0.5050 3.2718E*03 12/17/2015 12:40 19 1203621772.1 0.5180 3.2731E-03 9/15/2016 0:00 20 1203621773.1 0.5070 3.2720E-03 12/14/201513:47 21 1203621774.1 0.5180 3.2731E*03 9/15/2016 0:00 PU1596422 Plutonium-241 Solid Tracer SIN: Tracer Exp Date : Tracer Volume Added: 1770*A 8/312017 0.10 Tracer Error: 0.44% Tracer Calculations Tracer Tracer Tracer Concentration Tracer Bkg Net DPM Counts Counts CPM 4.3831 264 0.480 1.098 "4.3831 226 0.480 0.940 4.3831 242 0.960 1.004 4.3831 267 1.200 1.108 4.3831 317 0.960 1.317 4.3831 298 0.720 1.239 4.3831 312 0.960 1.296 4.3831 161 1.200 0.666 4.3831 286 2.160 1.183 4.3831 254 2.160 1.049 4.3831 286 1.680 1.185 4.3831 260 0.720 1.080 4.3831 312 0.480 1.298 4.3831 162 1.920 0.667 4.3831 261 2.880 1.075 4.3831 389 2.160 1.612 4.3831 242 1.440 1.002 4.3831 288 0.720 1.197 4.3831 275 2.640 1.135 4.3831 306 2.640 1.264 4.3831 179 0.960 0.742 Page 1 Procedure Code : LSC41PUS Parmname: Plutonium-241 Required MDA : 15 pCilG Halflife of Pu-241 : 14.290 years Pu-241 Abundance: 1.00 Tracer Abundance : 1.00 Hallllfe of Tracer : 373500.000 years Detector Tracer Count Tracer Detector Efficiency Start Count Tracer Detector Efficiency StDev. Date/Time Time(sec.) Decay Serial# (cpm/dpm) (cpmfdpm) 9/17/2016 11:42 . 14400 1.000 72194 0.284758 0.005506 9/171201611:42 14400 1.000 46-089C1 0.256702 0.004975 9/17/201611:42 14400 1.000 78780 0.291959 0.005641 9/17/201611:42 14400 1.000 78794 0.277658 0.005371 9/17/201611:42 14400 1.000 78795 0.329662 0.006355 9/17/2016 11:42 14400 1.000 78262 0.312964 0.006038 9/1712016 11 :42 14400 1.000 80020 0.321394 0.006198 9/17/201611:42 14400 1.000 67584 0.318335 0.006139 9/17/2016 11:42 14400 1.000 78775 0.335965 0.006474 9117/201611:42 14400 1.000 83296 0.303767 0.005864 9/17/201611:42 14400 1.000 80010 0.323452 0.006238 9/17/2016 11:42 14400 1.000 38633 0.334433 0.006444 9/17/2016 11:42 14400 1.000 78197 0.344422 0.006633 9/17/201611:42 14400 1.000 79996 0.330506 0.006369 9/17/2016 11:42 14400 1.000 79997 0.319848 0.006168 9/17/2016 11:42 14400 1.000 78785 0.353477 0.006805 9/17/2016 11:42 14400 1.000 78265 0.347248 0.006686 9/17/201611:42 14400 1.000 78776 0.329780 0.006356 9/17/2016 11:42 14400 1.000 78198 0.311951 0.006019 9/17/2016 11 :42 14400 1.000 83291 0.312191 0.006024 9/17/2016 11:44 14400 1.000 72549 0.257306 0.004988 Pipe!, 0.1 ml Stdev: +/-0.000200 ml Plpet, 0.5 ml Stdev: <-/-0.001000 ml Pipe!, 1 mr Stdev : +/* 0.002000 ml Analyllcal SOP: GL-RAD-A-035 Instrument SOP: GL-RA0-1-014 Count raw Data Counting Rack Time Quench# Gross Pos. Posttion # (min.) cpm_ 1 91-2 90 713.45 8.79 2 91-3 90 713.4 7.96 3 91-4 90 714.16 6.35 4 91-5 90 713.35 8.39 5 91-6 9{) 711.62 8.56 6 91-7 90 714.97 8.44 7 91-8 90 713.05 8.85 6 91-1 90 712.49 8.23 9 91-2 90 715.96 6.16 10 91-3 90 710.14 6.33 11 91-4 9{) 712.44 6.65 12 91-5 90 711.37 8.91 13 91-6 90 714.01 8.1 14 91-7 90 714.97 8.36 15 91-6 90 705 8.37 16 91-9 9{) 710.5 8.68 17 91-10 90 711.16 8.74 18 91-11 90 715.12 8.9 19 91-12 9{) 711.78 8.55 20 0-1 90 712.13 8.71" 21 0-2 QC 710.04 34.2 Bkg Count Corrected Count Bkg Time Bkg Bkg Start cpm (min.) Quench# cpm Daternme 9.09 90 714.56 9.0410 9/21/2016 14:35 9.09 90 714.56 9.0366 9121/201616:06 9.09 90 714.56 9.0720 9/21/2016 17:37 9.09 90 714.56 9.0367 9/21/2016 19:08 9.09 90 714.56 8.9653 9/21/2016 20:39 9.09 90 714.56 9.1087 9/2112016 22:10 9.09 90 714.56 9.0239 9/2112016 23:41 9.09 90 714.56 9.0005 9/22/2016 2:25 9.09 90 714.56 9.1564 9/22/2016 3:56 9.09 90 714.56 8.9067 9/22/2016 5:27 9.09 90 714.56 8.9984 9/2212016 6:58 9.09 90 714.56 8.9555 9/2212016 8:29 9.09 90 714.56 9.0654 912212016 10:00 9.09 90 714.56 9.1087 9/22/2016 11 :32 9.09 90 714.56 8.7401 9/2212016 13:03 9.09 90 714.56 8.9221 9/2212016 14:34 9.09 90 714.56 8.9473 9/2212016 16:05 9.09 90 714.56 9.1157 9/2212016 17:36 9.09 90 714.56 8.9717 9/2212016 19:07 9.09 90 714.56 8.9858 9/2212016 20:39 9.09 90 714.56 8.9050 9/2212016 22:10 PU1596422 Calculated Calibration Data Detector Background Sample Sample Calibration Detector Efficiency Background Count Sample Recovery Recovery Counted Calibration Due Efficiency Error Rack Start Decay % Error% on Date Date (cpm/dpm) (cpm/dpm) Position# Datemme 0.963 88.0% 6.49% LSCTEAL 211/2016 1/31/2017 0.1958 0.00792 91-1 9/2112016 13:03 0.963 63.5% 6.97% LSCTEAL 211/2016 1/31/2017 0.1957 0.00792 91-1 9/21/2016 13:03 0.963 78.5% 6.77% LS CT EAL 21112016 1/31/2017 0.1972 0.00792 91-1 9/21/2016 13:03 0.963 91.0% 6.47% LSCTEAL 2/1/2016 1/31/2017 0.1956 0.00792 91-1 9/21/2016 13:03 0.963 91.1% 5.98% LSCTEAL 2/1/2016 1/31/2017 0.1923 0.00792 91-1 912112016 13:03 0.963 90.3% 6.15% LSCTEAL 21112016 1/3112017 0.1987 0.00792 91-1 9/21/2016 13:03 0.963 92.0% 6.02% LSCTEAL 211/2016 1/31/2017 0.1950 0.00792 91-1 9/2112016 13:03 0.963 47.7% 8.21% LSCTEAL 211/2016 1/31/2017 0.1940 0.00792 91-1 9/21/2016 13:03 0.963 60.3% 6.29% LSCTEAL 2/1/2016 1/31/2017 0.2007 0.00792 91-1 9/21/2016 13:03 0.963 78.8% 6.65% LSCTEAL 2/112016 1/3112017 0.1895 0.00792 91-1 9/21/201613:03 0.963 83.6% 6.28% LSCTEAL 2/1/2016 1/31/2017 0.1939 0.00792 91-1 9/21/201613:03 0.963 73.7% 6.54% LSCTEAL 211/2016 1/31/2017 0.1916 0.00792 91-1 9/21/2016 13:03 0.963 86.0% 6.01% LSCTEAL 21112016 1131/2017 0.1969 0.00792 91-1 9/21/2016 13:03 0.963 46.0% 8.23% LSCTEAL 211/2016 1/31/2017 0.1987 0.00792 91-1 9/21/201613:03 0.963 76.7% 6.58% LSCTEAL 2/1/2016 1/31/2017 0.1801 0.00792 91-1 9/21/2016 13:03 0.963 104% 5.48% LSCTEAL 2/1/2016 1/31/2017 0.1902 0.00792 91-1 9/21 /2016 13:03 0.963 65.9% 6.78% LSCTEAL 2/1/2016 1131/2017 0.1914 0.00792 91-1 9/21/2016 13:03 0.963 82.8% 6.24% LS CT EAL 211/2016 1/31/2017 0.1990 0.00792 91-1 9/21/2016 13:03 0.999 83.0% 6.42°/o LSCTEAL 2/1/2016 1/31/2017 0.1926 0.00792 91-1 9/21/2016 13:03 0.963 92.4% 6.11*% LS CT EAL 2/1/2016 1/3112017 0.1933 0.00792 91-1 9/21/2016 13:03 0.999 65.8% 7.80% LSCTEAL 2/1/2016 1/31/2017 0.1893 0.00792 '11-1 9/2112016 13:03 Page2 Notes: 1 -Results are decay corrected to Sample Daterrime 2 -Reference date for Spike Activity (dpmlml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Date/Time * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCVG pCVG pCVG pCVG % 1 5.5163 3.8945 15 7.9651 -1.3255 177.49% 2 5.80_16 4.0960 15 8.3772 -5.8825 41.67% 3 6.1036 4.3092 15 8.8129 -4.2126 61.32% 4 5.3057 3.7459 15 7.6612 -3.2860 68.36% 5 5.4734 3.8643 15 7.9039 -2.1332 109.04% 6 5.3671 3.7892 15 7.7491 -3.4239 66.32% 7 5.3555 3.7810 15 7.7331 -0.8925 256.37% 8 10.3481 7.3058 15 14.9427 -7.6514 57.39% 9 6.0369 4.2621 15 8.7157 -5.6083 45.40% 10 6.3795 4.5040 15 9.2132 -3.5610 75.93% 11 5.8430 4.1252 15 8.4374 -0.8324 300.10% 12 6.7013 4.7312 15 9.6773 -0.2932 979.66% 13 5.7239 4.0411 15 8.2647 -5.2839 45.65% 14 10.6932 7.5495 15 15.4390 -7.4337 61.06% 15 6.8399 4.8290 15 9.8801 -2.4655 117.99% 16 4.7913 3.3827 15 6.9193 -1.1180 182.75% 17 7.5541 5.3333 15 10.9089 -1.5072 213.96% 18 5.8907 4.1589 15 8.5050 -1.2116 207.53% 19 5.6649 3.9994 15 8.1804 -2.2961 104.84% 20 5.3798 3.7982 15 7.7686 -1.4249 160.91% 21 7.2444 5.1146 15 10.4623 176.7966 8.33% PU1596422 Spike SIN: Spike Exp Date : Spike Activity (dpmlml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCVG -0.2510 0.4451 4.6080 -1.0588 0.4349 4.7353 -0.7220 0.4400 5.0312 -0.6467 0.4400 4.3826 -0.4053 0.4413 4.5519 -0.6687 0.4416 4.4312 -0.1739 0.4456 4.4833 -0.7705 0.4375 8.5165 -0.9764 0.4389 4.9410 -0.5787 0.4377 5.2786 -0.1484 0.4453 4.8949 -0.0455 0.4455 5.6300 -0.9654 0.4367 4.6850 -0.7287 0.4408 8.8134 -0.3701 0.4360 5.6925 -0.2421 0.4422 4.0030 -0.2073 0.4433 6.3176 -0.2157 0.4474 4.9258 -0.4217 0.4412 4.7090 -0.2758 0.4434 4.4907 25.2950 0.6921 9.4806 Page3 NIA NIA NIA N/A 1610-B 10/28/2016 1693.62 0.10 2SIGMA Total Prop. Uncertainty pCi/G 4.6080 4.7353 5.0312 4.3826 4.5519 4.4312 4.4833 8.5165 4.9410 5.2786 4.8949 5.6300 4.6850 8.8135 5.6925 4.0030 6.3177 4.9259 4.7090 4.4907 40.9611 Sample QC 405235061.1 Sample Nominal Type RPO REA pCVG Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP
  • 0.0% LCS 147.2768 120.0%

PROTOCOL : 5 Pu-241 90 min DATE : 2016/09/21 TIME : 13:03 ID : P05AS287 Pu-241 Wallac 1414 WinSpectral v3.0 S/N4140421 Counting mode : CPM lsotope(s) : H3 H3 = 5-350, 12.43 y Protocol name : Pu-241 90 min Counting time : 5400 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 10 Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SOPE,DAtE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Spectrum,Header,Listing Header : Pu-241 Spectrum : Rnd.Cos,Beta Window 1 25-220 /Beta Window 2 25-220 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 96.9 CPM Wallac 1400 DSA, P05AS287.DAT, 9/22/2016, page 1 Page 5568 of 5809 Pu-241 TEAL ---**-* -------*****--**-******-----*-***------*----***-******Y**"***-** ************************-* ** ** "'"' ,,. *" "'"' Rack_position Count_ Time(min) Quench_number 91 1 90.00 714.56 / Counts Chem 5 llj / Counts Beta L1 20 40 80 JOO Rack_position Count_ Time(min) Quench.:_number 91 2 90.00 713.45 2.lh-----,-----,.----,.--1-1 , I / Counts Chem \ 20 Rack_position 91 3 110*-0 0 20 / Counts Beta 40 Count_Time(min) Quench_number 90.00 713.40 / Counts Chem / Counts Beta 40 Pu24l_cpm 9.09 Run_Date 9/21/2016 1:03 PM Gross_B_CPM LUMEX 10.00 0.00 Lumex_CPM DPM 0.90 0.00 Pu24l_cpm 8.79 Run_Date 9/21/2016 2:35 PM Gross_B_CPM 9.20 Lumex_CPM 0.40 LUMEX 0.00 DPM 0.00 Pu24l_cpm 7.98 Run_Date 9121/2016 4:06 PM Gross_B_CPM 8.70 Lumex_CPM 0.70 LUMEX 0.00 DPM 0.00 *--*-*--*--**-***--.-----* ... Wallac 1400 DSA, P05AS287.DAT, 9/22/2016, page 2 Page 5569 of 5809 Pu-241 TEAL *-**-***-*-*-*-**--*-*-***----***--------*-------*****--***-**-------**-**--*----*--*-**-*---***-----------**-----------------------Rack_position Count_Time(min) Quench_nurnber 91 4 * " 90.00 714.16 20-.----.----r* 15-/ Counts Cllcm / Coull!s Beta Rack_position Count_ Time(min) Quench_m.imber 91 5 90.00 713.35 / Counts Chem / Counts Beta Rack_position CounLTime(min) Quench_number 91 6 -.:!: 90.00 711.62 20,---.----,----,----,---, / Counts Chem 5 / Counts Beta 20 40 60 Pu24Lcprn 8.35 Run_Date 9/21/201'6 5:37 PM Gross_B_CPM LUMEX 8.10* 0.00 Lurnex_CPM DPM 0.40 0.00 Pu24l_cpm 8.39 Run_Date 9/21/2016 7:08 PM Gross_B_CPM LUMEX 8.80 0.00 Lumex_CPM DPM 0.50 0.00 Pu24l_cpm 8.56 Run_Date 9/21/2016 8:39 PM Gross_B_CPM LUMEX 10.30 0.00 Lumex_CPM DPM 1.80 0.00 WaHac 1400 DSA; POSAS287.DAT, 9/22/2016, page 3 Page 5570 of 5809 Pu-241 TEAL . Rack_position Count_Time(min) Quench_number 91 7 90.00 714.97 I l, / Cmmls --1 Chem i 5 / Coums Beta Rack_position Count_ Time(min) Quench_number 91 8 90.00 713.05 2()-,-----,----.----r---.-----, I --I / Counts 1 r-01cm ,1 I / Couuls Beta Pu24l_cpm 8.44 Run_Date 9/21/2016 10: 10 PM Gross_B_CPM LUMEX 8.90 0.00 Lumex_CPM DPM 0.50 0.00 Pu24l_cpm 8.85 Run_Date 9/21/2016 11:41 PM Gross_B_CPM LUMEX 9.10 0.00 Lumex_CPM DPM 0.30 0.00 Wallac 1400 DSA, P05AS287.DAT, 9/22/2016, page 4 Page 5571 of 5809 -_____________________ ,. _________________ -------------------------_i:__ti_z_ _______ _ PROTOCOL : 5 Pu-241 90 min DATE : 2016/09/22 TIME : 02:24 ID : P05AS288 Pu-241 Wallac 1414 WinSpectral v3.0 S/N4140421 Counting mode : CPM lsotope(s) : H3 H3 = 5-350,12.43 y Protocol name : Pu-241 90 min Counting time : 5400 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 10 Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SOPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Spectrum,Header,Listing Header : Pu-241 Spectrum : Rnd.Cos,Beta Window 1 25-220 /Beta Window 2 25-220 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1*1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 192.2 CPM Wallac 1400 DSA, P05AS288.DAT, 9/22/2016, page 1 Page 5572 of 5809 Rack_position 91 l (

  • Rack_position 91 2 15,-,-----,---l 20 Rack_position 91 3 15 20 Pu-241 TEAL Count_ Time(min) Quench_number 90.00 ' 712.49 / Counts Chem // Counts Dcta Count_Time(min) Quench_number 90.00 715.98 / Counts Chem / Counts Beta 40 60 I Com1i_Time(min) Quench_number 40 *;: 90.00 710.14 I / Counts Chem / Counts Beta Pu24l_cpm 8.23 Run_Date 9/22/2016 2:25 AM Gross_B_CPM 8.90 Lumex_CPM 0.70 LUMEX 0.00 DPM 0.00 Pu24l_cpm 8.18 Run_Date 9/22/2016 3:56 AM Gross_B -CPM LUMEX 8.60 0.00 Lumex_CPM DPM 0.40 0.00 Pu24l_cpm 8.33 Run_Date 9/22/2016 5:27 AM Gross_B_CPM 8.70 Lumex_CPM 0.40 LUMEX 0.00 DPM 0.00 .. Wallac 1400 DSA, POSAS288.DAT, 9/22/2016, page 2 Page 5573 of 5809 Pu-241 TEAL Rack_position Count_Time(min) Quench_number 91 4 90.00 712.44 20 ... 1 l I 15-----------1 / Counts Chem I. l I ID ---< 5 / Counts Beta I 0 U!WllillllMI 0 20 40 60 80 100 Rack_position Count_ Time(min) Quench_number 91 5 90.00 711.37 15,-,----, ' I -l / Counts Chem I .[' I / Counts Bcu1 20 40 60 80 lilO Rack_position CounLTime(min) Quench_number 91 6 90.00 714.01 / Counts l ')) 10 Chem 5 I / Counts 1111mmlJ Beta 0 0 20 40 60 80 100 Pu24Lcpm Run_Date 8.85 9/22/2016 6:58 AM Gross_B_ CPM LUMEX 9.30 0.00 Lumex_CPM DPM 0.50 0.00 Pu24'I_cpm 8.91 Run_Date 9/22/2016 8:29 AM Gross_B_CPM LUMEX 9.40 0.00 Lumex_CPM DPM 0.40 0.00 Pu24l_cpm 8.10 Run_Date 9/22/2016 10:00 AM Gross_B_CPM LUMEX 9.10 0.00 Lumex_CPM DPM .. 1.00 0.00 Wnllac 1400 DSA, P05AS288.DAT, 9/22/2016, page 3 Page 5574of5809 Pu-241 TEAL Rack_position 91 7 Com'.i*t_ Time(rnin) Quench_number ?. 90.00 714.97 20,-----.,--I I / Counts -*1 I Chem 15 -----*!--+-/ CounL* Beta Rack_position Count_Time(min) Quench_number 91 8 90.00 705.00 15 -I / Counts 10 lS Chem uj / Counts Beta 0 0 20 40 60 80 100 Rack_position Count_Time(min) Quench_number 91 9 90.00 710.50 / Counts lL Chem / Counts Ile ta Pu24l_cpm 8.38 Run_Date 9/22/2016 11:32 AM Gross_B_CPM LUMEX 9.60 0.00 Lumex_CPM DPM 1.30 0.00 Pu24l_cpm 8.37 Run_Date 9/22/2016 l :03 PM Gross_B_CPM 9.30 Lumex_CPM 0.90 LUMEX 0.00 DPM 0.00 Pu24l_cpm 8.68 Run_Date 9/22/2016 2:34 PM Gross_B_CPM LUMEX 9.00 0.00 Lumex_CPM DPM 0.30 0.00 Wallac 1400 DSA, P05AS288.DAT, 9/22/2016, page 4 Page 5575 of 5809 Pu-241 TEAL ,* Rack_position Count_Time(min) Quench_number 91 JO 90.00 711.16 **f / Counts [l -----Chem / Counts :11J Beta . JllJilt*i 20 40 60 80 100 Rack_position Count_ Time(min) Quench_number 91 11 90.00 715.12 -*-*-l I I I I / Coums I Chem I i -1 / Counts Bela 60 80 100 Rack_position 91 12 Comlt_ Time(min) Quench_number **: 90.00 711.78 15-1---...;---i I i --j / Counts Chem c---\---1 !.ai1.1U1J1tJJul / Counts Beta 20 40 .60 8[) 100 *.;* ( ' Pu24l_cpm 8.74 Run_Date '9/22/2016 4:05 PM Gross_B_CPM LUMEX 9.10 0.00 Lumex_CPM DPM 0.30 0.00 Pu24l_cpm 8.90 Run_Date 9/22/2016 5:36 PM Gross_B_CPM LUMEX 9.20 0.00 Lumex_CPM DPM 0.30 0.00 Pu241_cpm 8.55 Run_Date 9/22/2016 7:07 PM Gross_B_CPM LUMEX 8.80 0.00 Lumex_CPM DPM 0.30 0.00 Wtillac 1400 DSA, P05AS288.DAT, 9/22/2016, page 5 Page 5576of5809 Pu-241 TEAL Rack_position Count_Time(min) Quench_number 0 1 .. 90.00 ---*1 10 I / Comlls I. --1 Chem ! I 0 _j 111uuJJ / Counis , Beta 0 20 40 60 80 100 Rack_positiori Count_Time(min) Quench_number 0 2 90.00 710.04 rV/ // Counts Chem / Counts Beta *t .*I* Pu24l_cpm 8.71 Run_Date 9/22/2016 8:39 PM Gross_B_CPM LUMEX 9.10 0.00 Lumex_CPM DPM 0.40 0.00 Pu24l_cpm 34.20 Run_Date 9/22/2016 10: 10 PM Gross_B_CPM LUMEX 34.40 0.00 Lumex_CPM DPM 0.20 0.00 Wallac 1400 DSA, P05AS288.DAT, 9/22/2016, page 6 Page 5577 of 5809 GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 __________ A __ L_P_H_A_S_P_E_C_T __ R_O_S_CO __ PY_R_E_PO_RT ___________ SOP: GL-RAD-A-035 BATCH NUMBER : 1596422 CHAMBER : 065 LIB FILE : PU SAMPLE ID : R0405235061_PU DETECTOR S/N : 72194 BKG FILE : B065.CNF;2658* SAMPLE QTY : 0.514 G +/-0.195 % AVERAGE %EFFICIENCY : 28.4758 BKG DATE : 16-Sep-2016 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 88.0 +/-6.490 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.8559E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 r PU*244: 4497-4597 keV 25 f-PU*242:4654-4995keV ! PU-239: 5011*5227 l<aV i PU*238: 5375-5566 l<aV 22 i'-PU-236: 5Se2*5843 keV 19 l 16 f-0' 13 z : :::> 0 £ .?!' :2! t5 <t'. PEAK ENERGY 5748.94 5415.55 5169.13 4909.38 4523.95 PEAK FWHM 4.939 0.000 44.452 39.064 4.939 2403 2801 3202 3607 4017 Energy (keV) AVERAGE %EFF ERROR : 0.5506 BKG LIVE TIME(SEC) : 60000.00 COUNT DATE : 17-Sep-2016 11 :42:34 EFF FILE : W065.CNF;489 ELAPSED LIVE : 14400.00 CAL DATE : 03-Sep-2016 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc AREA AREA AREA St Dev pCi/G pCi/G pCi/G pCi/G pCi/G 1.000 0.520 0.480 0.6928 100.000 9.12E-03 5.07E-02 9.71 E-02 2.23E-02 5.07E-02 2.000 1.760 0.240 0.4899 99.900 2.58E-02 5.09E-02 7.04E-02 1.32E-02 5.08E-02 2.000 1.760 0.240 0.4899 99.900 2.57E-02 5.06E-02 7.00E-02 1.31E-02 5.05E-02 264.000 263.520 0.480 0.6928 100.000 3.84E+OO 6.90E-01 8.07E-02 1.85E-02 4.65E-01 1.000 1.000 0.000 0.0000 99.900 1.46E-02 4.11E-02 4.38E-02 O.OOE+OO 4.10E-02 5 7 695 6125 6559 6997 7439 AJpha Spectroscopy Software Version 3.5.3 effectf\.-edate: 02*Mar*2015 GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-035 BATCH NUMBER : 1596422 CHAMBER :* 066 LIB FILE : PU SAMPLE ID : R0405235062 PU SAMPLE QTY : 0.515 G -+/-0.194 % DETECTOR S/N : 46-089C1 BKG FILE : B066.CNF;1813 AVERAGE %EFFICIENCY : 25.6702 BKG DATE : 16-Sep-2016 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.5 +/-6.972 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.6605E+OO dpm ---NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5747.65 PU-238 5486.00 5453.18 PU-239 5155.00 5118.70 PU-242 4890.00 4904.86 PU-244 4589.00 4535.62 25 r PIJ.244: 4497-4597 keV l 4654-4995 keV 23 r PU*239: 501 f.5227 keV , PU-238: 5375-5500 keV 21 I-PIJ.236: 5582*5843 keV 19 ! 17 I-i -151-(f) 13!-!z 11 ::::::> 0 9(-£ 5L PEAK FWHM 30.175 5.029 0.000 50.501 5.029 AVERAGE %EFF ERROR : 0.4975 BKG LIVE TIME(SEC) : 60000.00 COUNT DATE : 17-Sep-201611:42:34 EFF FILE : W066.CNF;487 ELAPSED LIVE TIME(SEC) : 14400.00 CAL DATE : 03-Sep-2016 NUCLIDE ACTIVITY SUMMARY 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G 2.000 1.760 0.240 0.4899 100.000 3.60E-02 7.09E-02 9.81E-02 1.84E-02 1.000 0.280 0.720 0.8485 99.900 4.79E-03 5.02E-02 1.05E-01 2.66E-02 0.000 -1.200 1.200 1.0954 99.900 -2.04E-02 3.88E-02 1.19E-01 3.41E-02 226.000 225.520 0.480 0.6928 100.000 3.83E+OO 7.40E-01 9.41E-02 2.16E-02 1.000 0.760 0.240 0.4899 99.900 1.29E-02 4.86E-02 8.16E-02 1.53E-02 1 ! i lllili\ ti ! ' . . l + ' * :---r -r**__,_ ..... ...... , --1 2375 2779 3188 3600 4016 5 5 28 3 571 E 6153 6592 7035 7 482 -.___A-..... Energy (keV) 1.96-sigma cnt Unc pCi/G 7.08E-02 5.01E-02 3.87E-02 5.02E-01 4.85E-02 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT -----,----BATCH NUMBER : 1596422 CH AMBER : 067 SAMPLE ID : R0405235063 PU SAMPLE QTY : 0.518 G -+/-0.193 % DETECTOR S/N : 78780 AVERAGE %EFFICIENCY : 29.1959 AVERAGE %EFF ERROR : 0.5641 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 78.5 +/-6.767 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.4400E+OO dpm NUCLIDE* LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5522.37 PU-239 5155.00 5198.11 PU-242 4890.00 4907.93 PU-244 4589.00 4598.66 Qi)0 \1 v _ PU*244: 4497-4597 keV 25 f-PU*24.'!: 4654-4995 keV j PU-239: 5011-5227 keV I PU-238: 5375-5565 keV 22 ! PU-238: 5582-5843 keV i I 19 f-I I 16 !--en I I-13 z 10 ::l 0 s I 7 f-.::-I t5 4f-ct: i I 1 PEAK FWHM 0.000 4.935 4.935 48.359 0.000 i ! II ' Ill l 2379 2776 3177 3583 3992 440 Energy (keV) COUNT DATE : 17-Sep-2016 11 :42:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -1.200 1.200 1.0954 100.000 -2.28E-02 1.000 1.000 0.000 0.0000 99.900 1.59E-02 1.000 0.520 0.480 0.6928 99.900 8.23E-03 242.000 241.040 0.960 0.9798 100.000 3.81E+OO 1.000 1.000 0.000 0.0000 99.900 1.58E-02 mE ...... ..... i: I I j ' . ' !,I -) HJ! .. I i i I I ' 4824 5, 4E 672 6102 6537 6976 7419 "' l!l <'! <'! " " :, " 0.. 0.. c. "-"-Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8067.CNF;1813 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W067.CNF;476 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.33E-02 1.33E-01 3.82E-02 4.48E-02 4.78E-02 O.OOE+OO 4.58E-02 8.77E-02 2.01E-02 7.14E-01 1.04E-01 2.84E-02 4.46E-02 4.75E-02 O.OOE+OO 1.96-sigma cnt Linc pCi/G 4.33E-02 4.48E-02 4.57E-02 4.83E-01 4.45E-02 0 >-+, Vl 00 0 \0 BATCH NUMBER : 1596422 SAMPLE ID : R0405235064 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT I Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU SAMPLE QTY : 0.517 G -+/-0.193 % CHAMBER : 068 DETECTOR SIN : 78794 AVERAGE %EFFICIENCY : 27.7658 AVERAGE %EFF ERROR : 0.5371 i BKG FILE : B068.CNF;1804 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 91.0 +/-6.474 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.9887E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749,00 5712.25 PU-238 5486.00 5497.56 PU-239 5155.00 5118.68 PU-242 4890.00 4902.87 PU-244 4589.00 4546.97 ------\ r P!J.24-1: "497-4597 keV 28 f-PU*242: 4 i PU-23.9:50 654-4995 keV 11*5227 keV 25 i-75-5566 keV *5843 keV l 221--1 19 f-i -16 f-! z 13 f-::> i 10 i 4 t-i 1 i-j ; I 'I l . I PEAK FWHM 0.000 49.420 0.000 43.536 0.000 l!I i i l I 2378 27 76 3178 3584 3995 441 Energy (keV) COUNT DATE : 17-Sep-2016 11 :42:34 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY I I ! GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 -0.960 0.960 0.9798 100.000 -1.66E-02 3.000 2.040 0.960 0.9798 99.900 2.95E-02 0.000 -1.200 1.200 1.0954 99.900 -1.73E-02 267.000 265.800 1.200 1.0954 100.000 3.82E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO I ,1 l j '!iil *Iii* .! i l lil l ! . l 4830 5 682 6115 6552 6993 7439 EFF FILE : W068.CNF;453 CAL DATE : 03-Sep-2016 1.96-sigma TPU pCi/G 3.85E-02 5.89E-02 3.28E-02 6.85E-01 2.91E-02 MDA pCi/G 1.14E-01 9.53E-02 1.01 E-01 1.01 E-01 4.31 E-02 Le pCi/G 3.10E-02 2.60E-02 2.89E-02 2.88E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.85E-02 5.87E-02 3.27E-02 4.61E-01 2.90E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235065_PU SAMPLE QTY : 0.507 G +/-0.197 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 069 DETECTOR SIN : 78795 j AVERAGE %EFFICIENCY : 32.9662 ! AVERAGE %EFF ERROR : 0.6355 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B069.CNF;1819 / BKG DATE : 16-Sep-2016 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 I COUNT DATE : 17-Sep-2016 11:42:34 I BKG LIVE TIME(SEC) : 60000.00 l EFF FILE : W069.CNF;495 / CAL DATE : 03-Sep-2016 % YIELD : 91.1 +/-5.981 % i ELAPSED LIVE TIME(SEC) : 14400.00 ______________ ! ________ _ TRACER ! ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 3.9945E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5723.58 PU-238 5486.00 5502.78 PU-239 5155.00 5118.68 PU-242 4890.00 4938.75 PU-244 4589.00 4546.97 34 r P\J.244:4497-4597keV PU*242: 465-1-4995 keV 31 .--PU-239: 5011-5227 keV I PU-238: 5375-5566 keV 28 r PU-238: 5582*5843 keV 25 Ci) 19 1--I z 16 }---::::> 13 i 0 10 [ 8 .?;-7L I t5 4 f--< I 1 k-I .. ; '. . -' l 2404 2802 3206 3614 Energy (keV) PEAK FWHM 4.959 4.959 0.000 48.654 0.000 n I . 4026 44 a. NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 1.000 0.520 0.480 0.6928 100.000 1.000 1.000 0.000 0.0000 99.900 0.000 -0.720 0.720 0.8485 99.900 317.000 316.040 0.960 0.9798 100.000 0.000 -0.240 0.240 0.4899 99.900 m-" a-I I I ju j , l\'l *I I J1 ';1il}ll --.-. ; I -r-"j' -:--.--:--, -.-.... 486 6152 6591 7034 N "' l!l 0 l=i '1' ::i :::> :::> :::> a. a. a. a. --'-----------1.96-sigma 1.96-sigma ACTIVITY TPU MDA Le cnt Unc pCi/G pCi/G pCi/G pCi/G pCi/G 7.71E-03 4.29E-02 8.21E-02 1.88E-02 4.28E-02 1.24E-02 3.49E-02 3.72E-02 O.OOE+OO 3.49E-02 -8.88E-03 2.69E-02 7.53E-02 1.92E-02 2.68E-02 3.89E+OO 6.45E-01 8.12E-02 2.21E-02 4.31E-01 -2.96E-03 2.56E-02 5.91E-02 1.11 E-02 2.55E-02 7481 GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-035 _B_A_T_C_H_N_U_M_B_E_R_:_1_5_9_6_4_2_2-------.,.-------C-H_A_M_B_E_R_:_0_7_0 _______ l LIB FILE : PU SAMPLE ID : R0405235066 PU DETECTOR SIN : 78262 I BKG FILE : B070.CNF;1821 SAMPLE QTY : 0.509 G -+/-0.196 % AVERAGE %EFFICIENCY : 31.2964 I BKG DATE : 16-Sep-2016 SAMPLE DATE : 14-Dec-2015 00:00:00 AVERAGE %EFF ERROR : 0.6038 BKG LIVE TIME(SEC) : 60000.00 ANALYST : KXB2 COUNT DATE : 17-Sep-2016 11 :42:34 -, EFF FILE : W070.CNF;500 % YIELD : 90.3 +/-6_146 % ELAPSED LIVE TIME(SEC) : 14400.00 I CAL DATE : 03-Sep-2016 TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.9579E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5541.00 PU-239 5155.00 5176.90 PU-242 4890.00 4913.24 PU-244 4589.00 4546.97 ev 31 FU 244-4497 4597 keV f: Pt.1:242; keV I I FU-239: 5011*5227 keV 28 25 PU-238; 5375-5566 keV I PU-236: 5582-5843 keV r-I 22 l I PEAK GROSS FWHM AREA 0.000 0.000 24.500 3.000 4.900 1.000 38.792 298.000 0.000 0.000 i ' I I NUCLIDE ACTIVITY SUMMARY 1.96-sigma NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA StDev pCi/G pCi/G pCi/G pCi/G -1.440 1.440 1.2000 100.000 -2.26E-02 3.65E-02 1.16E-01 3.45E-02 2.280 0.720 0.8485 99.900 3.00E-02 5.31E-02 8.03E-02 2.04E-02 -0.200 1.200 1.0954 99.900 -2.61E-03 3.92E-02 9.16E-02 2.62E-02 297.280 0.720 0.8485 100.000 3.88E+OO 6.60E-01 7.97E-02 2.03E-02 0.000 0.000 0.0000 99.900 O.OOE+OO 2.64E-02 3.92E-02 0.00E+OO if) 19 16 r I I I-z :::> 13 0 10 7 .::: t5 4 <{ 1 '-r l I r I r-L ,_ ,I II ' i I ' 11 f!L ! p I ' I. ' : ! ' ' i j : I I 23 81 2775 3175 3578 3987 440( 4818 41 668 6100 6537 6978 7424 -Energy (keV) 1.96-sigma cnt Unc pCi/G 3.64E-02 5.30E-02 3.92E-02 4.42E-01 2.63E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235067 _PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G +/-0.197 % CHAMBER : 071 DETECTOR SIN : 80020 AVERAGE %EFFICIENCY : 32.1394 AVERAGE %EFF ERROR : 0.6198 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 92.0 +/-6.024 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831E+OO dpm RESULTS : 4.0324E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 23 21 L PU-239:5011*5227kel/ I P\J.238: 537s-ssea k*" 19 f-P\J.236: 5582*5843 kel/ 17 15 L ! t i 9 l-7 i 5 f-3 PEAK ENERGY 5717.08 5445.38 5118.68 4893.79 4546.97 PEAK FWHM 4.953 69.348 0.000 62.153 0.000 COUNT DATE : 17-Sep-2016 11:42:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCb.IDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.520 0.480 0.6928 100.000 7.83E-03 2.000 1.760 0.240 0.4899 99.900 2.21E-02 0.000 -0.480 0.480 0.6928 99.900 -6.00E-03 312.000 311.040 0.960 0.9798 100.000 3.89E+OO 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 1 ! ii 2399 . 2798 3201 3608 4020 44 6146 6584 7027 7474 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8071.CNF;1814 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W071.CNF;464 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.36E-02 8.34E-02 1.91E-02 4.36E-02 6.03E-02 1.13E-02 2.66E-02 6.93E-02 1.59E-02 6.48E-01 8.23E-02 2.24E-02 2.53E-02 3.75E-02 O.OQE+OO 1.96-sigma cnt Unc pCi/G 4.35E-02 4.35E-02 2.65E-02 4.33E-01 2.52E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235068_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B072.CNF;1821 SAMPLE QTY : 0.509 G +/-0.196 % CHAMBER : 072 DETECTOR S/N : 67584 AVERAGE %EFFICIENCY : 31.8335 AVERAGE %EFF ERROR : 0.6139 1 BKG DATE : 16-Sep-2016 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 47.7 +/-8.215 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.0916E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 5712.26 0.000 PU-238 5486.00 5470.35 0.000 PU-239 5155.00 5109.06 10.008 PU-242 4890.00 4892.73 49.920 PU-244 4589.00 4556.86 35.028 (j)P1 l l q) Vv ! -I 2377 2780 3187 3597 4013 44 32 -Energy (keV) COUNT DATE : 17-Sep-201611:42:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY I BKG LIVE TIME(SEC) : 60000.00 ! EFF FILE : W072.CNF;475 ! CAL DATE : 03-Sep-2016 ! 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA 0.000 0.000 0.000 -0.240 2.000 0.320 161.000 159.800 3.000 3.000 i I I ii Ir *n I! 11 I 1 I 111 " ' '! -.-. 4856 AREA St Dev pCi/G 0.000 0.0000 100.000 O.OOE+OO 0.240 0.4899 99.900 -5.87E-03 -1.680 1.2961 99.900 7.78E-03 1.200 1.0954 100.000 3.88E+OO 0.000 0.0000 99.900
  • 7.29E-02 -*-:* . l 571£ 6152 6592 7037 7486 pCi/G 5.92E-02 5.08E-02 8.87E-02 8.83E-01 9.67E-02 pCi/G 8.78E-02 1.17E-01 1.88E-01 1.70E-01 7.29E-02 pCi/G O.OOE+OO 2.19E-02 5.77E-02 4.87E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 5.90E-02 5.06E-02 8.86E-02 6.06E-01 9.59E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235069_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G +/-0.198 % CHAMBER : 073 DETECTOR SIN : 78775 AVERAGE %EFFICIENCY : 33.5965 AVERAGE %EFF ERROR : 0.6474. SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 80.3 +/-6.293 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.5202E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5718.81 PU-238 5486.00 5470.34 PU-239 5155.00 5118.68 PU-242 4890.00 4889.55 PU-244 4589.00 4541.25 (JV Ji l Li\l 'V _ PIJ-24.4: 4497-4597 keV 23 !-PIJ.242: 4654-4995 koV I PU-239: 5011*5227 koV 21 L PU-238: 5375-5566 koV ! PU-236: 5582-5843 keV 19 f--17 15 1--Ui 13 L z 11 L 5 £ 5 \_I *s;: ts 3 PEAK FWHM 84.102 0.000 0.000 58.916 54.419 COUNT DATE : 17-Sep-2016 11 :42:35 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 0.320 1.680 1.2961 100.000 5.30E-03 0.000 -0.720 0.720 0.8485 99.900 -9.99E-03 0.000 -1.200 1.200 1.0954 99.900 -1.65E-02 286.000 283.840 2.160 1.4697 100.000 3.91E+OO 2.000 1.520 0.480 0.6928 99.900 2.10E-02 > > >> .l! .l! :1 "'"' i3 I ,! ! <( 1 h-i ! 11! I .___,-.-.-1,.--"-,* -. . -. -i'-+ i I i I li ; j 2384 2783 3185 3593 4004 Energy (keV) 44 4842 a. 5 6 a. 697 6132 6571 7015 7463 :; ii: a. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8073.CNF;1820 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W073.CNF;495 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.04E-02 1.28E-01 3.93E-02 3.02E-02 8.47E-02 2.16E-02 3.14E-02 *9.67E-02 2.77E-02 6.81E-01 1.15E-01 3.71E-02 4.82E-02 7.64E-02 1.75E-02 1.96-sigma cnt Unc pCi/G 6.03E-02 3.02E-02 3.13E-02 4.58E-01 4.81E-02 Alpha SpedlOsocpy SOftware Version 3.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596422 SAMPLE ID : R0405235070_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 074 DETECTOR S/N : 83296 SAMPLE QTY : 0.509 G +/-0.196 % 1 AVERAGE %EFFICIENCY : 30.3767 I AVERAGE %EFF ERROR : 0.5864 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 78.8 +/-6.649 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.4544E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5752.09 PU-238 5486.00 5470.35 PU-239 5155.00 5118.69 PU-242 4890.00 4897.81 PU-244 4589.00 4566.43 §JJ4lt9l1v .-PU-244:4497-4597 keV I PU*2"2: keV 25 !._ PU*23.9: 5011-5227 keV I f'U.238: keV 22 1 PU*238: 5582*5843 keV 19 ! en 16 I f-13 [** z ::> I 0 rn r-2.. .2:-1 t5 <( i 1h i L I i . ' i 2383 2784 3189 3599 Energy (keV) PEAK FWHM 4.988 0.000 0.000 44.581 0.000 4012 44 I COUNT DATE : 17-Sep-201611:42:35 i ELAPSED LIVE TIME(SEC) : 14400.00 ' i NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 4.000 1.840 2.160 1.4697 100.000 3.42E-02 0.000 -0.240 0.240 0.4899 99.900 -3.72E-03 0.000 -0.480 0.480 0.6928 99.900 -7.40E-03 254.000 251.840 2.160 1.4697 100.000 3.88E+OO 2.000 2.000 0.000 0.0000 99.900 3.08E-02 .. "' I I 6142 6580 7022 7469 ; ::, :::> 0.. 0.. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8074.CNF;1838 BKG DA TE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 ErF FILE : W074.CNF;511 CAL DA TE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.61E-02 1.56E-01 5.00E-02 3.22E-02 7.44E-02 1.39E-02 3.28E-02 8.54E-02 1.96E-02 7.14E-01 1.29E-01 4.15E-02 5.30E-02 4.63E-02 O.OOE+OO 1.96-sigma cnt Uno pCi/G 8.59E-02 3.21E-02 3.27E-02 4.83E-01 5.28E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235071_PU SAMPLE QTY : 0.515 G +/-0.194 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 075 DETECTOR S/N : 80010 AVERAGE %EFFICIENCY : 32.3452 AVERAGE %EFF ERROR : 0.6238 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 83.6 +/-6.282 % i COUNT DATE : 17-Sep-201611:42:35 ! ELAPSED LIVE TIME(SEC) : 14400.00 TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.6626E+OO dpm *-----*------NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 31 PU*244-4497-4597 keV / PU*242: 4654-4995 l<eV 28 ! P\J.239: 5011 *5227 keV l PU-238: 5375-5566 keV 25 P\J.236: 5582*5843 keV ! 22 L (j) !z 16 j ::> 0 13 10 7 f-i I r-I L-PEAK PEAK GROSS ENERGY FWHM AREA 5711.01 78.677 2.000 5470.55 122.933 4.000 5107.51 118.016 3.000 4883.78 34.421 286.000 4546.97 0.000 0.000 I : j NUCLIDE ACTIVITY SUMMARY NET BKG BKG %ABUN AREA AREA StDev 0.320 1.680 1.2961 100.000 3.760 0.240 0.4899 99.900 2.760 0.240 0.4899 99.900 284.320 1.680 1.2961 100.000 0.000 0.000 0.0000 99.900 8 .c :2: 0 <( 4 1 ii I I L I I r-J i ll ' ' ! i I ii I . ACTIVITY pCi/G 5.20E-03 5.11E-02 3.73E-02 3.83E+OO 0.00E+OO I . 23 79 2775 3175 3580 3990 440 D 4824 4E 676 6109 6547 6989 7437 -.___..__ ...... Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B075.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W075.CNF;478 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 5.93E-02 1.26E-01 3.86E-02 6.06E-02 6.51E-02 1.22E-02 5.39E-02 6.47E-02 1.21E-02 6.67E-01 1.04E-01 3.20E-02 2.73E-02 4.05E-02 O.OOE+OO 1.96-sigma en! Une pCi/G 5.93E-02 6.02E-02 5.37E-02 4.48E-01 2.72E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235072_PU SAMPLE QTY : 0.513 G +/-0.195 % SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 73.7 +/-6.539 % GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 078 DETECTOR S/N : 38633 AVERAGE %EFFICIENCY : 33.4433 AVERAGE %EFF ERROR : 0.6444 COUNT DATE : 17-Sep-201611:42:36 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B078.CNF;1726 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W078.CNF;447 CAL DATE : 03-Sep-2016 -----------------------*------'--------TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.2303E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 23 ,-PU-244: 4497-4597 keV PU-242: 4654-4995 keV 21 19 .-f'U.236: 5582*SS43 keV 17 15 L w 11 ::::> 9 f--s. 7 L 1 L f---,. I ' I PEAK ENERGY 5791.39 5491.03 5102.49 4888.52 4591.43 . I PEAK FWHM 4.964 4.964 4.964 53.358 4.964 . I 2388 2787 3190 3597 4009 442 Energy (keV) c. GROSS AREA 1.000 1.000 1.000 260.000 1.000 i I I" rn g JS J ii
  • I I . 4844 NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc AREA AREA StDev pCi/G pCi/G pCi/G ppi/G pCi/G -0.200 1.200 1.0954 100.000 -3.57E-03 5.36E-02 1.25E-01 3.58E-02 5.36E-02 0.760 0.240 0.4899 99.900 1.14E-02 4.27E-02 7.17E-02 1.34E-02 4.26E-02 0.760 0.240 0.4899 99.900 1.13E-02 4.24E-02 7.12E-02 1.33E-02 4.24E-02 259.280 0.720 0.8485 100.000 3.85E+OO 6.97E-01 9.07E-02 2.31E-02 4.70E-01 0.760 0.240 0.4899 99.900 1.13E-02 4.24E-02 7.12E-02 1.33E-02 4.24E-02 ! I I ' ' I ' ' ' ' I 5 15695 6126 6562 7002 7445 BATCH NUMBER : 1596422 SAMPLE ID : R0405235073 PU SAMPLE QTY : 0.505 G -+/-0.198 % SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 86.0 +/-6.014 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.7686E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 080 DETECTOR S/N : 78197 AVERAGE %EFFICIENCY : 34.4422 AVERAGE %EFF ERROR : 0.6633 COUNT DATE : 17-Sep-2016 11 :42:36 ELAPSED LIVE TIME(SEC) : 14400.00 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B080.CNF;1728 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W080.CNF;446 CAL DATE : 03-Sep-2016 NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5505.30 PU-239 5155.00 5143.01 PU-242 4890.00 4888.02 PU-244 4589.00 4590.46 _ f'U.24-£:.4497-.4597 koV I PU-242: 4654-4995 koV 28 r PU*239: 5011*5227 koV J PU-238: 5375-55*0 keV 25 r PU-236: 5582*Ž'< koV ! 221-19 f-l w I-l 5 13 [-;;?;-7 r1 *;; PEAK GROSS FWHM AREA 0.000 0.000 4.969 1.000 4.969 3.000 39.117 312.000 0.000 2.000 ]] !;;!;; "' I I I *1 I: i' J 4f-1 l I \! l I j I ; 2386 2786 3190 3598 Energy (keV) 4011 44 4849 ::> "-NUCLIDE ACTIVITY SUMMARY 1.96-sigma 1.96-sigma NET BKG .BKG %ABUN ACTIVITY TPU MDA Le cnt Unc AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G -0.240 0.240 0.4899 100.000 -3.63E-03 3.14E-02 7.25E-02 1.36E-02 3.13E-02 0.520 0.480 0.6928 99.900 6.57E-03 3.66E-02 7.00E-02 1.6bE-02 3.65E-02 2.040 0.960 0.9798 99.900 2.56E-02 5.11E-02 8.28E-02 2.25E-02 5.10E-02 311.520 0.480 0.6928 100.000 3.91E+OO 6.51E-01 6.95E-02 1.59E-02 4.35E-01 1.520 0.480 0.6928 99.900 1.91E-02 4.39E-02 6.96E-02 1.59E-02 4.39E-02 ----"' a I I I , . 5 7 705 6139 6578 7021 7468 0 ........ Vl 00 0 '° GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596422 SAMPLE ID : R0405235074 PU SAMPLE QTY : 0.501 G -+/-0.200 % CHAMBER : 081 DETECTOR S/N : 79996 AVERAGE %EFFICIENCY : 33.0506 AVERAGE %EFF ERROR : 0.6369 SAMPLE DATE : 15-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 46.0 +/-8.229 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.0181 E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.23 PU-238 5486.00 5470.33 PU-239 5155.00 5044.07 PU-242 4890.00 4880.83 PU-244 4589.00 4597.20 ----* 15 ,-FU*2"4: "497-4597 keV I ?U*242: 4654*4995 keV i PU:239: 5011 -5227 keV 13 f--PU-238: sS75-5506 keV t PU-236: 5582*5843 keV 11 I 9 i i 5 f-l 3 r-1 1 r* ! ! PEAK FWHM 0.000 0.000 4.901 67.881 0.000 2384 2779 3178 3582 3991 Energy (keV) 440 COUNT DATE : 17-Sep-201611:42:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.240 0.240 0.4899 100.000 -7.10E-03 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 1.000 0.040 0.960 0.9798 99.900 9.86E-04 162.000 160.080 1.920 1.3856 100.000 3.94E+OO 1.000 0.520 0.480 0.6928 99.900 1.28E-02 > .l! ,,,_ .,., "' l ri ,! I' 11 I I 11 11 I ' I 1:1! ii!! I I I : : 'rt' -). -,--,.-I I 4823 4* 673 6106 6543 6985 7432 .,. N ;;; :J :;; :J 0.. 0.. c.. 0.. 0.. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8081.CNF;1734 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W081.CNF;446 CAL DATE : 03-Sep_=2016 1.96-sigrna TPU MDA Le pCi/G pCi/G pCi/G 6.15E-02 1.42E-01 2.66E-02 5.01E-02 7.44E-02 O.OOE+OO 7.32E-02 1.62E-01 4.42E-02 8.98E-01 1.99E-01 6.25E-02 7.13E-02 1.36E-01 3.13E*02 1.96-sigrna cnt Unc pCi/G 6.13E-02 5.00E-02 7.31E-02 6.17E-01 7.12E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235075 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT *---------CHAMBER : 082 SAMPLE QTY : 0.508 G -+/-0.197 % DETECTOR S/N : 79997 AVERAGE %EFFICIENCY : 31.9848 AVERAGE %EFF ERROR : 0.6168 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 76.7 +/-6.584 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.3625E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.23 PU-238 5486.00 5525.58 PU-239 5155.00 5189.96 PU-242 4890.00 4891.83 PU-244 4589.00 4546.96 PU-24.4" 4497-4597 keV 23 21 [ PU-242: MlSoS-4995 keV l PLJ-239: 5011 *5227 keV PLJ-238: 5375-5568 keV i 5582-5843 keV 19 17 ' I 15 Ui 13 I-z 11 ::::> 9 0 £ 7 .?:-5 *:; u 3 <{ 1 L.. j r I t--L i i r L i ! ii i I ! ' PEAK FWHM 0.000 4.883 4.883 54.322 0.000 !! I l I I ! 23 94 2787 3185 3588 3996 440c> -Energy (keV) COUNT DATE : 17-Sep-201611:42:36 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.30E-02 1.000 -0.200 1.200 1.0954 99.900 -3.03E-03 1.000 -3.080 4.080 2.0199 99.900 -4.64E-02 261.000 258.120 2.880 1.6971 100.000 3.89E+OO 0.000 -0.240 0.240 0.4899 99.900 -3.62E-03 ;I ii ii Ii ii' ij1I 11m ii t ' ,11. ! I. I f !I! I I **1* '! 4826 5: 4 676 6108 6545 6987 7434 Instrument SOP: GL-RAD-1-009 _ Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B082.CNF;1724 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W082.CNF;423 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.94E-02 1.11E-01 2.81E-02 4.56E-02 1.06E-01 3.04E-02 5.15E-02 1.57E-01 5.58E-02 7.09E-01 1.39E-01 4.68E-02 3.13E-02 7.23E-02 1.35E-02 1.96-sigma cnt Unc pCi/G 3.93E-02 4.55E-02 5.15E-02 4.78E-01 3.12E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235076_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.512 G +/-0.195 % CHAMBER : 083 DETECTOR SIN : 78785 AVERAGE %EFFICIENCY : 35.3477 AVERAGE %EFF ERROR : 0.6805 SAMPLE DATE : 11-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 104 +/-5.477 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.5599E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5747.57 PU-238 5486.00 5487.40 PU-239 5155.00 5122.63 PU-242 4890.00 4901.61 PU-244 4589.00 4525.17 v r PU-244: 4497-4597 keV PU-242: 4654-4995 keV 33 ! j PU*23S: S582*SS43 keV 291 i 00 21 6 13 <( ! !'ii . I 1 I i I l ; . ' . ! ' . , J * ---r-r-1-,.-. PEAK FWHM 24.717 79.093 74.150 56.848 49.433 l I I' I 2392 2790 3192 3598 4 009 4423 -Energy (keV) COUNT DATE : 17-Sep-201611:42:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 2.000 1.520 0.480 0.6928 100.000 1.83E*02 4.000 3.520 0.480 0.6928 99.900 3.53E-02 2.000 1.040 0.960 0.9798 99.900 1.04E-02 389.000 386.840 2.160 1.4697 100.000 3.86E+OO 4.000 3.520 0.480 0.6928 99.900 3.51E-02 I i I I I I I I i 1*JJ.I_ 'I I !Ill ,....,J4._ i . ' I I 4843 5* 6! >694 6126 6562 7003 7448 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8083.CNF;1740 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W083.CNF;485 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.20E-02 6.66E-02 1.53E-02 4.49E-02 5.56E-02 1.27E-02 3.55E-02 6.58E-02 1.79E-02 5.85E-01 8.36E-02 2.68E-02 4.47E-02 5.53E-02 1.27E-02 1.96-sigma cnt Uno pCi/G 4.20E-02 4.48E-02 3.55E-02 3.86E-01 4.45E-02 Instrument SOP: GL-RAD-1-009 GEL Laboratories LLC ** ALPHA SPECTROSCOPY REPORT -------______ SOP: GL-RAD-A-035 BATCH NUMBER : 1596422 CHAMBER : 084 SAMPLE ID : R0405235077 _PU SAMPLE QTY : 0.510 G +/-0.196 % DETECTOR S/N : 78265 AVERAGE %EFFICIENCY : 34.7248 AVERAGE %EFF ERROR : 0.6686 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 65.9 . +/-6.779 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.8865E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 5712.25 0.000 PU-238 5486.00 5529.44 54.265 PU-239 5155.00 5164.30 29.599 PU-242 4890.00 4899.77 54.182 PU-244 4589.00 4543.42 4.933 21 _ PU*244:449H597 koV I PU*242: .oc54-4995 keV 19 PU-239: 5011-5227 koV I PU-238: 5375-5566 keV 17 !-l'U-238: 5582*58.43 keV 15 l I 13 \--Ci) I 11 !--I-I z gr :J 0 2-71 I .?:-t) ex: 1 L, I
  • I I! I I I . ' .. I j I ; ( ' I ; 2402 2799 3200 3606 4016 44 E.nergy (keV) COUNT DATE : 17-Sep-201611:42:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.39E-02 2.000 2.000 0.000 0.0000 99.900 3.24E-02 2.000 0.320 1.680 1.2961 99.900 5.16E-03 242.000 240.560 1.440 1.2000 100.000 3.87E+OO 5.000 4.760 0.240 0.4899 99.900 7.67E-02 !;;:;; ;:I ,,,_ l\l!:j .,_ :J:? ! I i-,...-,--,...-r I I 4850 5 7l )701 6133 6570 7011 7457 ::;, i? :::> c. a. a. c.. LIB FILE : PU BKG FILE : B084.CNF;1729 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W084.CNF;476 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.21 E-02 1.18E-01 3.00E-02 5.57E-02 4.86E-02 O.OOE+OO 5.88E-02 1.25E-01 3.82E-02 7.27E-01 1.19E-01 3.54E-02 7.88E-02 7.72E-02 1.45E-02 1.96-sigma en! Unc pCi/G 4.20E-02 5.55E-02 5.87E-02 4.92E-01 7.81 E-02 BATCH NUMBER : 1596422 SAMPLE ID : R0405235078 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.505 G -+/-0.198 % CHAMBER : 085 DETECTOR S/N : 78776 AVERAGE %EFFICIENCY : 32.9780 AVERAGE %EFF ERROR : 0.6356 SAMPLE DATE : 17-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 82.8 +/-6.241 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULT$ : 3.6297E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 _ PU*244:4497-4597 keV 21 f-Pll-242: 46SH995 keV ' PIJ.239: 5011-5227 keV 19 L PU*238: 5375-5566 keV < PU-236: 5582*5843 keV 17 15 13 11 z ! :;) 9 I-a PEAK ENERGY 5712.26 5428.03 5215.97 4894.63 4946.97 PEAK FWHM 0.000 49.309 4.931 73.141 0.000 COUNT DATE : 17-Sep-201611:42:37 ELAPSED LIVETIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 -1.200 1.200 1.0954 100.000 -1.96E-02 3.000 1.320 1.680 1.2961 99.900 1.81E-02 1.000 -0.440 1.440 1.2000 99.900 -5.99E-03 288.000 287.280 0.720 0.8485 100.000 3.91E+OO 0.000 0.000 0.000 0.0000 99.900 0.00E+OO I 3 ! 1( I' . '. I ... I . ' l i ! I ' I .. I .. ' ' I . l ' . 2385 2782 3182 3587 3996 Energy (keV) 440 "-4826 5 :::J "-.. 4* 673 6103 6537 6974 7416 Q. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B085.CNF;1732 BKG DA TE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W085.CNF;479 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.72E-02 1.15E-01 3.28E-02 5.68E-02 1.06E-01 3.25E-02 4.14E-02 1.01 E-01 2.99E-02 6.76E-01 8.31E-02 2.12E-02 2.75E-02 4.09E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 3.72E-02 5.67E-02 4.14E-02 4.54E-01 2.75E-02 Alpha Spectro$COpy Software Version 3.5.3 effective dale: 02*Mar*2015 BATCH NUMBER : 1596422 SAMPLE ID : R1203621772_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G +/-0.193 % CHAMBER : 086 DETECTOR SIN : 78198 AVERAGE %EFFICIENCY : 31.1951 AVERAGE %EFF ERROR : 0.6019 SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 83.0 +/-6.420 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.6379E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 -----r PU*244: 4497-4597 keV 37 PU-238: 5375-5568 keV 33 r PU-236: 5582*5843 keV 29 L 25 (f)I--21 i z 17[--=> i a 131 9 r-PEAK ENERGY 5712.26 5437.23 5017.21 4898.93 4559.45 PEAK FWHM 0.000 118.750 4.948 19.527 4.948 ; COUNT DATE : 17-Sep-201611:42:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.720 0.720 0.8485 100.000 -1.01 E-02 5.000 4.040 0.960 0.9798 99.900 5.66E-02 1.000 0.040 0.960 0.9798 99.900 5.60E-04 275.000 272.360 2.640 1.6248 100.000 3.81E+OO 1.000 0.520 0.480 0.6928 99.900 7.28E-03 I I I I J J j I i I I! ' 1 *L' . '*
  • I , .*. I . . . ! ' 1 ' ' '
  • t r-i dill . l . ; 2381 2779 3181 3587 3998 441 4832 s: 5* )684 6116 655 2 6992 7437 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8086.CNF;1733 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W086.CNF;455 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 3.05E*02 8.56E-02 2.18E-02 6.93E*02 9.23E-02 2.51 E-02 4.16E-02 9.23E-02 2.51E-02 6.78E-01 1.25E-01 4.17E-02 4.05E-02 7.76E-02 1.78E-02 1.96-sigma cnt Unc pCi/G 3.05E-02 6.89E-02 4.15E-02 4.56E-01 4.05E-02 BATCH NUMBER : 1596422 SAMPLE ID : R1203621773 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G -+/-0.197 % CHAMBER : 088 DETECTOR S/N : 83291 AVERAGE %EFFICIENCY : 31.2191 AVERAGE %EFF ERROR : 0.6024 SAMPLE DATE : 14-Dec-2015 00:00:00 ANALYST : KXB2 % YIELD : 92.4 +/-6.111 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.0488E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5798.83 PU-238 5486.00 5485.03 PU-239 5155.00 5118.68 PU-242 4890.00 4892.91 PU-244 4589.00 4589.29 dVJq)H)i .! 'l/ 37 r PU*244: 4497-4597 keV I PU*242: 4654-4995 keV l PU*239: 5011 *5227 keV 33 r f>U.238: 5375-5568 keV I f>U.236: 5582*5843 keV 29 ! 25 Cli 21 17 :::> i 0 13 £ I 9 r-i ,._. 5 LI :J. ! i -.. -j--:--r. I i PEAK FWHM 4.923 9.845 0.000 36.398 4.923 ' I I I 2387 2783 31 Energy (keV) 84 3589 3998 441' -COUNT DATE : 17-Sep-2016 11:42:37 ELAPSED LIVE TIME(SEC) : 14400.00 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev *pCi/G 1.000 0.520 0.480 0.6928 100.000 8.03E-03 2.000 1.760 0.240 0.4899 99.900 2.28E-02 0.000 -1.440 1.440 1.2000 99.900 -1.85E-02 306.000 303.360 2.640 1.6248 100.000 3.89E+OO 1.000 1.000 0.000 0.0000 99.900 1.28E-02 I I I I ,1 i I I' i 1':" :/' ' /,J. I . -.--!.-' I I ' \ I i I 4830 5. 681 6112 6549 6989 743 4 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B088.CNF;1728 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W088.CNF;463 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.47E-02 8.55E-02 1.96E-02 4.48E-02 6.20E-02 1.16E-02 2.99E-02 9.SOE-02 2.82E-02 6.59E-01 1.15E-01 3.82E-02 3.62E-02 3.85E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 4.46E-02 4.47E-02 2.98E-02 4.41 E-01 3.61E-02 BATCH NUMBER : 1596422 SAMPLE ID : R1203621774_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.518 G +/-0.193 % CHAMBER : 170 DETECTOR SIN : 72549 AVERAGE %EFFICIENCY : 25.7306 AVERAGE %EFF ERROR : 0.4988 SAMPLE DATE : 15-Sep-2016 00:00:00 ANALYST : KXB2 % YIELD : 65.8 +/-7.799 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.8831-E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5687.51 PU-238 5486.00 5462.09 PU-239 5155.00 5133.29 PU-242 4890.00 4868.44 PU-244 4589.00 4546.97 11 > PU-244: 4497""'597keV PU-242: 4654-1995 keV 10 9 PU*236: 5582-5843 koV I I Br I w 6 f-I-z 0 4 f--£ i 3 f-' *s; n ! <( 1 !--! ' : j 2386 2785 3187 3593 Energy (keV) PEAK FWHM 104.059 94.148 158.566 120.246 0.000 4004 COUNT DATE : 17-Sep-201611:44:22 ELAPSED LIVE TIME(SEC) : 14400.00 LCS ID NUCLIDE NOMINAL (pCi/G) % RECOVERY -NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN AREA AREA AREA StDev 4.000 1.360 2.640 1.6248 100.000 4.000 2.320 1.680 1.2961 99.900 6.000 5.280 0.720 0.8485 99.900 179.000 178.040 0.960 0.9798 100.000 0.000 -0.720 0.720 0.8485 99.900 :i] ........ g:: "'"' CO> "'"' .,.,, .. s .... i I !! I I I! I 5 5E )683 6113 6547 6985 1! l'l "' oi "' ir ir ll. ll. 0. ACTIVITY pCi/G 2.92E-02 4.97E-02 1.13E-01 3.81E+OO -1.54E-02 7426 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B170.CNF;874 BKG DATE : 16-Sep,,2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W170.CNF;241 CAL DATE : 13-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.00E-01 1.92E-01 6.38E-02 9.85E-02 1.66E-01 5.09E-02 1.14E-01 1.31 E-01 3.33E-02 8.23E-01 1.41 E-01 3.84E-02 4.67E-02 1.31 E-01 3.33E-02 -----1.96-sigma cnt Unc pCi/G 1.00E-01 9.82E-02 1.13E-01 5.63E-01 4.66E-02 Effecllve 3/25/201 o Revision 1 Effective March 2010 Radiochemistry Batch Checklist 23-Sep-2016 Batch#_f _S_t.J_LP_L\_\_Y_ Pv -*J. '-l 1 Product:. _______ _ Date: Criteria: Yes No Comm0nts Samale Solids are less than or eaual to 100 ma ror GAB. rvA Samples have been blank corrected (If required). NJA Blank correction renorted Included !If reaulred). If activity less than lOx MDA/MDC, error Is less ..... than or equal to 150% or sample activity. r-... [f oreater than 10* MDA/ MDC, error Is 400/o or less. If hnlnm *hn Mnll I unr le-**-** Instrument source check Is within limits. ..... -Instrument bka check Is within llmlts. Method RDL/ LLD has been met. """ If duplicate activities are: Less than 5* MDA/ MDC, then RPD Is 100% or less, '-....... Ir greater 5* MDA/ MDC, then RPD 20% or less, 1--> lf below the MDA/ MDC, the RPD Is 0%, Or meets the client's reaulred RER acceotance criteria. Tracer yield Is 15-125%
  • Carrier yield 25-125%. -...... ....._. (Or meets the cllent's contract acceptance criteria). ' :---> Method blank Is less than the RDL/ LLD. ITf *--' *-<. !;D/ft nf *-u*n** "rHvltvl GL-CHL-RAD-013 Rev 1 Page 1 of 1
  • I.....___. ( )bt\.-At f S fr, I 1 \1 ?J Samnle was run within hold time. Samnle was correctlv nreserved If reaulred. ff1:. Smears Taken for Radioactive batches. ('tff' ' ......._, Method Spike and LCS are within 75-1250/o or meets the cllent's contract accentance criteria\. ......... No blank spaces on data forms. All line outs lnltlaled and dated. "'-... n**-** -*-* Aux data Is correct. (Wl "-.. .J Client Saeclal reaulrements aaae has been checked. .... Raw Data and/ or snectrum are Included and nronerlv statused * ...... MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and ' I'-> vnrlfln.t UI* **--llf (VY\ 'r-.... lbtrh nn*n*n" lntn Batch Data Exceotlon Reoorts <DER\ comoleted If aoollcable. "" l)6fdb JS I.I, '-t3 Batch Data Exception Reports (DER) second reviewed. "'-.. DtAiL JS1;\1Lt$ Dlsnosltlon verified to be comnlcted. Allouot Correction comaletcd If rcoulred. rm Review sample historical results Ir available '"" f->. (If REMP, results above MDC have been verified bv historical results recount or re*analvsls. \ Primary Revlow Performed By: tP)M ]iv (/ .......... 09/30/16 f{(j1JfC Page 5599 of 5809 GEL Laboratories LLC Form GEL-DER DER Report No.: 1561743 Revision No.: 2 DATA"EXCEPTION REPORT
  • Mo.Day Yr. Division: Quality Criteria: Type: 27-SEP-16 Radiochemistry Specifications Process Instrument Type: Test I Method: Matrix Type: Client Code: LSC HASL-300, Pu-11-RC Solid MJWC .. Batch ID: Sample Numbers: 1596414 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Peak Centroid Values Off Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235041, 405235042, 405235043, 405235044, 1. Reporting results. 405235045,405235046,405235047,405235048,405235049, 405235050,405235051,405235052,405235053,405235054, 405235055,405235056,405235057,405235058,405235059, 405235060, and 1203621752 were received and analyzed out of holding. 2. The Pu-242 tracer peak centroid for sample 405235047 is greater than 2. The sample does meet the tracer yield requirement, the detection limits, 50 keV from the expected energy value of 4890 keV. and its tracer peak is within the Pu-242 region of interest. Reporting results. Originator's Name: Data Validator/Group Leader: Jessica Davis 30-SEP-16 Melanie Aycock 30-SEP-16 Page 1 Page 5600 of 5809 0 I-+) VI 00 0 \0 Pu-241 Queue Sheet so 07-SEP-16 -------*--------*---------------------------Batch#: 1596414 Analyst:HAKB First Client Due Date: 04-0CT-16 Internal Due Date30-SEP-16 Tracer Tracer Code: CIJ'b -A Expiration Vol:.,% . \ Solid Sample Dissolution by: LEACH o@GESTIONl LCS Isotope: Pu-241 LCS Code: l \a\ o -,J?z Expiration Vol: ,e. I . Spike Isotope: Pu-241 Spike Code: -Expiration Date: -Vol: -Cockta1I Used: Ultima gold LLT or(EcoscintU!traJ Prep Date:* °\)2.o_..:..)_)_\.. __ 1_n_it_ials: Pipet ID: C) .:lti:. , Balance ID: \ \,, \ ()J L, la:?.... Witness: 'f_i !1*C /!& Hazard l\fin Sample JD Client Description Type Code CRDL Matrix Client 405235041-1 4.4D.R.l.4 SAMPLE 15pCi/g SOIL MJWCOOl 405235042-1 4.4D.R.2.3 SAMPLE 15 pCi/g SOIL ll.UWCOOI 405235043-1 4.4D.R.2.4 SAMPLE 15 pCi/g SOIL l'vUWCOOl 405235044-1 4.4D.R.4.2 SAMPLE 15 pCi/g SOIL l'YUWCOOl 405235045-1 4.4D.R.5.2 SAMPLE 15 pCi/g SOIL :M'.JWCOOl 405235046-1 4.SA.R.1.3 SAMPLE 15pCilg SOIL MJWCOOl 405235047-1 4.SA.R.1.4 SAMPLE 15 pCi/g SOIL l\UWCOOl 405235048-1 4.5B.R.1.2 SAMPLE 15pCi/g SOIL MJWCOOl 405235049-1 4.5B.R.1.3 SAMPLE 15 pCi/g SOIL MJWCOOl 405235050-1 4.5B.R.1.4 SAMPLE 15 pCi/g SOIL l\UWCOOI 405235051-1 4.5B.R.2.3 SAMPLE 15 pCi/g SOIL MJWCOOl 405235052-1 4.5B.R.2.4 SA...'\fl>LE 15 pCi/g SOIL MJWCOOl 405235053-1 4.SC..R.5.2 SAMPLE 15 pCi/g SOIL l\UWCOOl 405235054-1 4.SC.R.1.3 SAMPLE 15 pCi/g SOIL l\UWCOOl 405235055-1 4.SC.R.1.4 SAMPLE 15 pCi/g so:µ, l\UWCOOl 405235056-1 4.SC.R.2.2 SMlPLE 15 pCi/g SOIL l\UWCOOl 405235057 -1 4.SC.R.2.3 SAMPLE 15 pCi/g SOIL 1\-IJWCOOl 405235058-1 4.SC.R.2.4 SA...'\-lPLE 15 pCi/g SOIL MJWCOOl 405235059-1 5.lA.R.1.2 SAMPLE 15 pCi/g SOIL MJWCOOl 405235060-1 5.lA.R.1.3 SAl'rlPLE 15 pCi/g SOIL MJWCOOl 1203621754-1 MB for batch 1596414 MB 15 pCi/g SOIL QC ACCOUNT 1203621755-1 4.4D.R.1.4(405235041DUP) DUP 15 pCi/g SOIL QC ACCOUNT 1203621756-1 LCS for batch 1596414 LCS 15 pCi/g SOIL QC ACCO(J}'jl' ' Instrument Used: LS6000 (Red) 7065155, LS6500 (Blue) 7067083, LS6500 (Green) 7067404, Wallac (Yellow) 4140127, LS6000 6500 (Gold) 7070506, Purple 7069123, Silver 7060656, Wal/ac (White) 4140299, 414042 , Wallac (Gray) 4150033, 7069693 (Mocha) GEL l.Aboratories LLC-;-Ra *
  • ry Division Collection Date 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 30-NOV-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 07-DEC-15 01-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 02-DEC-15 16-DEC-15 16-DEC-15 30-NOV-15 Label Pos. # Data Reviewed By: Wet@ Aliquot LSC Rack# Alpha Spec @Ilf) Det# Page 1 oil Filename PU241.XLS File type Excel Version # 1.3.4 Batch: 1596414 Analyst : HAKB Prep Date : 9/20/2016 Method Uncertainty : 0.0839 Geometry: m roo m coscint 2 L Dl/1 d HN03113 L E . UI Ira Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Sample Pas. ID G G Date/Time 1 405235041.1 0.5090 3.2722E-03 11/30/2015 13:27 2 405235042. 1 0.5000 3.2712E-03 11/30/2015 13:53 3 405235043.1 0.5070 3.2720E-03 11/30/201513:59 4 405235044.1 0.5050 3.2718E-03 11/3012015 13:50 5 405235045.1 0.5020 3.2714E-03 11130/201514:15 6 405235046.1 0.5140 3.2727E-03 1217/201510:02 7 405235047 .1 0.5030 3.2715E--03 1217/2015 10:10 8 405235048.1 0.5070 3.2720E-03 121712015 13:28 9 405235049.1 0.5060 3.2719E*03 1217/2015 13:33 10 405235050. 1 0.5040 3.2717E-03 1217/2015 13:42 11 405235051.1 0.5020 3.2714E-03 1217/201513:02 12 405235052.1 0.5080 3.2721E-03 12171201513:11 13 405235053. 1 0.5000 3.2712E--03 1211/2015 14:24 14 405235054.1 0.5000 3.2712E-03 121212015 14:51 15 405235055.1 0.5100 3.2723E-03 121212015 14:59 16 405235056. 1 0.5090 3.2722E-03 121212015 14:50 17 405235057 .1 0.5000 32712E--03 12121201514:55 18 405235058.1 0.5120 3.2725E-03 1212/2015 15:00 19 405235059.1 0.5030 3.2715E-03 12116/201512:26 20 405235060.1 0.5150 3.2728E--03 12/16/201512:33 21 1203621754.1 0.5150 3.2728E-03 9120/2016 0:00 22 1203621755.1 0.5110 3.2724E-03 11/30/2015 13:27 23 1203621756. 1 0.5150 3.2728E--03 9/20/2016 0:00 PU1596414 Plutonium-241 Solid Tracer SIN: Tracer Exp Date : Tracer Volume Added: 1770-A 813/2017 0.10 Tracer Error: 0.44% Tracer Calculations Tracer Tracer Tracer Concentration Tracer Bkg Net DPM Counts Counts CPM 4.3831 112 0.501 0.891 4.3831 145 0.501 1.153 4.3831 153 0.376 1.217 4.3831 145 0.547 1.056 4.3831 140 0.684 1.018 4.3831 157 1.236 1.134 4.3831 141 1.237 1.017 4.3831 163 0.962 1.178 4.3831 162 0.415 1.167 4.3831 185 0.277 1.334 4.3831 151 1.109 1.082 4.3831 135 1.664 0.962 4.3831 156 4.515 1.074 4.3831 158 0.283 1.114 4.3831 139 0.850 0.975 4.3831 187 1.842 1.306 4.3831 162 0.284 1.141 4.3831 145 0.000 1.016 4.3831 148 0.571 1.033 4.3831 205 1.000 1.429 4.3831 192 0.714 1.339 4.3831 159 0.869 1.091 4.3831 135 1.015 0.924 Page 1 Procedure Code : LSC41PUS Parmname: Plutonium-241 Required MDA : 15 pCilG Hallllfe of Pu-241 : 14.290 years Pu-241 Abundance: 1.00 Tracer Abundance : 1.00 Halfllfe of Tracer : 373500.000 years Detector Tracer Count Tracer Detector Efficiency Start Count Tracer Detector Efficiency StDev. Date/Time Time (sec.) Decay Serial# (cprn!dpm) (cprnldpm) 9/22/2016 9:56 7510 1.000 78780 0.291959 0.005641 9/22/2016 9:56 7518 1.000 78795 0.329662 0.006355 9/2212016 9:56 7522 1.000 78262 0.312964 0.006038 9122/2016 9:56 8208 1.000 80020 0.321394 0.006198 912212016 9:56 8212 1.000 67584 0.318335 0.006139 9122/2016 9:56 .8242 1.000 78775 0.335965 0.005474 9/2212016 9:56 8245 1.000 83296 0.303767 0.005864 9/2212016 9:56 8250 1.000 80010 0.323452 0.006238 912212016 9:56 8305 1.000 38633 0.334433 0.006444 9/2212016 9:56 8310 1.000 78197 0.344422 0.006633 9122/2016 9:56 8314 1.000 79996 0.330506 0.006369 9/2212016 9:56 8318 1.000 79997 0.319848 0.006168 9/22/2016 9:56 8466 1.000 79988 0.292461 0.005651 912212016 9:56 8496 1.000 78263 0.334344 0.006443 912212016 9:56 8499 1.000 78259 0.347245 0.006687 9/2212016 9:56 8504 1.000 80063 0.303421 0.005858 9/2212016 9:56 8507 1.000 33206 0.330892 0.006377 9/2212016 9:56 8560 1.000 38626 0.304247 0.005873 9/2212016 9:56 8564 1.000 80016 0.325188 0.006269 9/2212016 9:56 8568 1.000 83288 0.353557 0.006805 9/2212016 9:56 8573 1.000 80059 0.356284 0.006858 912212016 9:56 8695 1.000 79461 0.338848 0.006527 9/2212016 9:56 8703 1.000 78777 0.336886 0.006490 Pipe!, 0.1 ml Stdev : +/* 0.000200 ml Pipe!, 0.5 ml Stdev: +/* 0.001000 ml Pipe!, 1 ml Stdev : +/* 0.002000 ml Analytical SOP: GL-RAD-A-035 Instrument SOP: GL-RAD-1-014 Counl raw Data Counting Rack Time Quench# Gross Pos. Position# (min.) cpm 1 82-2 60 714.11 9.5 2 82-3 60 708.61 9.64 3 82-4 60 709.02 9.54 4 82-5 60 709.74 9.17 5 82-6 60 708.81 9.22 6 82-7 60 710.25 9.09 7 82-8 60 705 9.17 8 82-9 60 708.76 9.19 9 82-10 60 709.53 10.49 10 82-11 60 709.89 9.81 11 82-12 60 711.01 9.69 12 0-1 60 711.42 10.01 13 0-2 60 704.95 9.62 14 87-3 60 711.67 9.18 15 87-4 60 709.68 9.48 16 87-5 60 709.58 9.62 17 87-6 60 710.3 8.67 18 87-7 60 708.61 9.57 19 87-8 60 710.3 8.72 20 87-9 60 707.22 9.85 21 87-10 60 709.22. 9.79 22 87-11 60 709.84 8.81 23 87-12 60 708.76 32.43 Bkg Count Corrected Count Bkg Time Bkg Bkg Start cpm (min.) Quench# cpm Date/Time 9.60 60 714.11 9.6000 9/2312016 13:25 9.60 60 714.11 9.3843 9/2312016 14:26 9.60 60 714.11 9.3985 9/2312016 15:27 9.60 60 714.11 9.4242 9/23/2016 16:29 9.60 60 714.11 9.3912 9/23/2016 17:30 9.60 60 714.11 9.4429 9/23/201618:31 9.60 60 714.11 9.2703 9/23/2016 19:32 9.60 60 714.11 9.3895 9/23/2016 20:33 9.60 60 714.11 9.4166 9/23/2016 21:34 9.60 60 714.11 9.4297 912312016 22:35 9.60 60 714.11 9.4717 9/2312016 23:36 9.60 60 714.11 9.4876 9/24/2016 0:38 9.60 60 714.11 9.2689 9/2412016 1 :39 9.60 60 714.11 9.4975 9/2412016 3:52 9.60 60 714.11 9.4220 9/24/2016 4:53 9.60 60 714.11 9.4184 9/2412016 5:54 9.60 60 714.11 9.4448 9/24/2016 6:55 9.60 60 714.11 9.3843 9/2412016 7:57 9.60 60 714.11 9.4448 9/24/2016 8:58 9.60 60 714.11 9.3381 9/2412016 9:59 9.60 60 714.11 9.4056 9/24/2016 11:00 9.60 60 714.11 9.4278 9/24/2016 12:01 9.60 60 714.11 9.3895 9/24/2016 13:02 PU1596414 Calculated Calibration Data Detector Background Sample Sample Calibration Detector Efficiency Background Counl Sample Recovery Recovery Counted Calibration Due Efficiency Error Rack Start Decay % Error on Date Date (cpm/dpm) (cpm/dpm) Position# DatefTime 0.961 69.6% 9.74% LSCTEAL 211/2016 1/31/2017 0.1971 0.00792 82*1 9/2312016 12:24 0.961 79.8% 8.59% LSCTEAL 211/2016 1/31/2017 0.1867 0.00792 82-1 9/2312016 12:24 0.961 88.7% 8.37% LSCTEAL 211/2016 1131/2017 0.1875 0.00792 82-1 9/2312016 12:24 0.961 75.0% 8.60% LSCTEAL 211/2016 1/31/2017 0.1888 0.00792 82-1 9/23/2016 12:24 0.961 73.0% 8.75% LSCTEAL 211/2016 1/31/2017 0.1871 0.00792 82-1 9/2312016 12:24 0.962 n.0% 8.31% LS CT EAL 21112016 1/31/2017 0.1897 0.00792 82-1 9/2312016 12:24 0.962 76.4% 8.76% LSCTEAL 21112016 1/31/2017 0.1801 0.00792 82-1 9/2312016 12:24 0.962 83.1% 8.15% LSCTEAL 211/2016 1/31/2017 0.1870 0.00792 82-1 9/23/2016 12:24 0.962 79.6% 8.15% LSCTEAL 211/2016 1/31/2017 0.1884 0.00792 82*1 9123/2016 12:24 0.962 88.3% 7.64% LSCTEAL 211/2016 1/31/2017 0.1891 0.00792 82-1 9/2312016 12:24 0.962 74.7% 8.46% LSCTEAL 211/2016 1/31/2017 0.1912 0.00792 S2*1 9/23/2016 12:24 0.962 68.6% 8.97% LS CT EAL 211/2016 1/31/2017 0.1919 0.00792 82*1 9/23/2016 12:24 0.961 83.8% 8.52% LS CT EAL 211/2016 1/31/2017 0.1800 0.00792 82-1 9/23/2016 12:24 0.961 76.0% 8.24%1 LSCTEAL 211/2016 1/31/2017 0.1924 0.00792 82-1 9/231201612:24 0.961 64.1% 8.79% LSCTEAL 211/2016 1/31/2017 0.1887 0.00792 82*1 9/23/2016 12:24 0.961 98.2% 7.67% LSCTEAL 2/1/2016 1/31/2017 0.1685 0.00792 82-1 9/2312016 12:24 0.961 78.6% LSCTEAL 211/2016 1/31/2017 0.1898 0.00792 82-1 9/23/2016 12:24 0.961 76.2% 8.57% LSCTEAL 211/2016 1/31/2017 0.1867 0.00792 82-1 9/23/201612:24 0.963 72.5% 8.52% LSCTEAL 211/2016 1/31/2017 0.1898 0.00792 82-1 9/23/2016 12:24 0.963 7.31% LSCTEAL 211/2016 1/31/2017 0.1841 0.00792 82-1 9/23/2016 12:24 0.999 85.7% 7.53% LSCTEAL 21112016 1131/2017 0.1878 0.00792 82-1 9/2312016 12:24 0.961 8.24% LSCTEAL 211/2016 1/31/2017 0.1890 0.00792 82-1 9/23/2016 12:24 0.999 62.6% 8.93% LSCTEAL 211/2016 1/31/2017 0.1870 0.00792 82-1 9/2312016 12:24 Pa9e2 Notes: 1 -Results are decay corrected to Sample Datemme 2 -Reference date for Spike Activity (dpmfml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Datemme * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act Sample Act. Level Level MDA MDA Cone. Error Pos. pCilG pCilG pCi/G pCi/G pCilG % 1 8.8460 6.2453 15 12.8262 -0.6711 564.30% 2 B.1973 5.7874 15 11.8893 1.6084 220.39% 3 7.2461 5.1158 15 10.5094 0.7860 397.24% 4 8.5639 6.0462 15 12.4202 -1.6671 219.16% 5 8.9181 6.2962 15 12.9345 -1.1712 325.42% 6 8.1502 5.7541 15 11.8199 -2.2005 157.69% 7 8.7624 6.1864 15 12.7110 -0.6787 552.67% 8 7.7457 5.4685 15 11.2342 -1.1853 279.08% 9 8.0509 5.6840 15 11.6764 6.6199 54.29% 10 7.2652 5.1293 15 10.5367 2.1152 149.09% 11 8.5545 6.0395 15 12.4057 1.4265 256.99% 12 9.1717 6.4753 15 13.3006 3.6565 109.50% 13 8.0500 5.6833 15 11.6775 2.1824 160.03% 14 8.4006 5.9309 15 12.1622 -2.0344 175.93% 15 9.9223 7.0053 15 14.3905 0.4404 968.43% 16 6.4907 4.5825 15 9.4135 1.0021 279.57% 17 8.2062 5.7937 15 11.9012 -4.8634 71.39% 18 8.3815 5.9174 15 12.1564 1.1944 302.79% 19 8.8363 6.2385 15 12.8149 -4.8988 76.40% 20 6.9545 4.9099 15 10.0874 2.7388 110.71% 21 7.0911 5.0064 15 10.2646 2.0895 147.33% 22 8.6289 6.0921 15 12.5144 -4.0816 89.62% 23 9.7538 6.8863 15 14.1467 172.4050 9.69% PU1596414 Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCSS!N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCi/G -0.1000 0.5642 7.4218 0.2557 0.5631 6.9424 0.1415 0.5618 6.1183 -0.2542 0.5567 7.1552 -0.1712 0.5569 7.4676 -0.3529 0.5558 6.7916 -0.1003 0.5544 7.3510 -0.1995 0.5565 6.4810 1.0734 0.5760 6.9628 0.3803 0.5663 6.1728 0.2183 0.5651 7.2374 0.5224 0.5701 7.8207 0.3511 0.5611 6.8355 -0.3175 0.5579 7.0073 0.0580 0.5613 8.3595 0.2016 0.5633 5.4891 -0.7748 0.5495 6.7600 0.1857 0.5621 7.0853 -0.7248 0.5502 7.2891 0.5119 0.5655 5.9296 0.3844 0.5656 6.0257 -0.6178 0.5513 7.1387 23.0405 0.8349 12.2441 Page3 NIA NIA NIA NIA 1610-B 10/2812016 1692.50 0.10 2SIGMA Total Prop. Uncertainty pCi/G 7.4219 6.9528 6.1211 7.1553 7.4677 6.7916 7.3511 6.4811 7.1274 6.1909 7.2451 7.8705 6.8547 7.0073 8.3602 5.4937 6.7601 7.0909 7.2891 5.9600 6.0435 7.1388 43.3144 Sample QC 405235041. 1 Sample Nominal Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP
  • 0.0% LCS 148.0364 116.5%

Pu-241 TEAL PROTOCOL DATE : 4 Pu-241 60 min : 2016/09/23 TIME * : 12:23 ID : P04AS243 Pu-241 Wallac 1414 WinSpectral v3.0 S/N4140421 Counting mode : CPM lsotope(s) : H3 H3 = 5-350, 12.43 y Protocol name : Pu-241 60 min Counting time : 3600 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 1 o Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Spectrum,Header,Listing Header : Pu-241 Spectrum : Rnd.Cos,Beta Window 1 25-220 /Beta Window 2 25-220 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 183.3 CPM Wallac 1400 DSA, P04AS243.DAT, 9/24/2016, page 1 Page 5605 of 5809 t't Rack_position 82 l 15,----r--10-5-Rack_position 82 2 Pu-241 TEAL Count_ Time(min) Quench_number 60'.01 714.11 / Counts Chem / Cmmls Bela Count_Time(min) Quench_number

  • 60.00 714.11 / Counts 10 Chem \ / Counts Bela Rack_position Count_Time(min) Quench_number 82 3 60.00 708.61 / Counts Chem 5 / Counts Bela JlUlMlE 20 40 60 80 100 Pu241_cpm 9.60 Run_Date 9/23/2016 12:24 PM Gross_B_CPM LUMEX 10.20 0.00 Lumex_CPM DPM 0.60 0.00 Pu24l_cpm 9.50 Run_Date 9/23/2016 1:25 PM Gross_B_CPM LUMEX 9.90 0.00 Lumex_CPM DPM 0.40 0.00 Pu24l_cpm 9.64 Run_Date 9/23/2016 2:26 PM Gross_B_CPM LUMEX 10.00 0.00 Lumex_CPM DPM 0.30 0.00 Wallac 1400 DSA, P04AS243.DAT, 9/24/2016, page 2 Page 5606 of 5809 Pu-241 TEAL Rack_position Count_Time(min) Quench_number i82 4 ) 60.00 709.02 / Counts Chem 6 4 / Counls 2-Bela 0 0 20 40 60 80 100 Rack_position Count_Time(min) Quench_number 82 5 60.00 709.74 1 I / Counts --------i Chem I I ii I I v( / Counls Bein 100 Rack_position Quench_number 82 6 . 60.00 708.81 10 -1 8*1---lhl-rr--f---/ Co11111s Chem I I / / Counts Bela 20 40 ljQ s'o 100 *.*. Pu24I_cpm
  • 9.54 Run_Date 9/23/2016 3:27 PM Gross_B_CPM LUMEX 10.10 0.00 Lumex_CPM DPM 0.50 0.00 Pu24l_cpm 9.17 Run_Date 9/23/2016 4:29 PM Gross_B_CPM LUMEX 9.70 0.00 Lumex_CPM DPM 0.50 0.00 Pu24l_cprn 9.22 Run_Date 9/2312016 5:30 PM Gross_B_CPM 9.50 Lurnex_CPM 0.30 LUMEX 0.00 DPM 0.00 Wallac 1400 DSA, P04AS243.DAT, 9/24/2016, page 3 Page 5607 of 5809 Pu-241 TEAL " Rack_position Quench_number 82
  • 7 60.00 710.25 10---.-i--. --i I / Counts I 01cm L --1 / Camus Bctu JOO Rack_position Count_ Time(min) Quench_number 82 8 60.00 705.00 -------1 I / Coums Chem .\ I --* *---1 I / Co11n1> I -*-' Beta 20 40 60 80 JOO " Rack_position Quench_number 82 9 .:,, 60.'00 708.76 / Counts Chem / Counts Beta 20 40 (,0 80 JOO .. " !.' *i, .. '> ;*, '*. Pu24l_cpm 9.09 Run_Date 9/23/2016 6:31 PM Gross_B_CPM LUMEX 9.40 0.00 Lumex_CPM DPM 0.30 0.00 Pu24l_cpm 9.17 Run_Date 9123/2016 7:32 PM Gross_B_CPM LUMEX 9.60 0.00 Lumex_CPM DPM 0.40 0.00 Pu24l_cpm 9.19 Run_Date 9/23/2016 8:33 PM Gross_B_CPM LUMEX 9.60 0.00 Lumex_CPM DPM 0.40 0.00 Wa11ac 1400 DSA P04AS243.DAT, 9/24/2016, page 4 Page 5608 of 5809 Rack_position 82 10 2 00 20 Rack.:...position 82 11 lo 6 2 20 Rack_positi on 82 12 \ \ Page 5609 of 5809 Pu-241 TEAL CouW_Time(min) Quench:_number r 60.00 109.53 / Counts Chem / Counts 1b. llcrn 40 60 80 100 Count_Time(min) Quench_number 60.00 709.89 / Counts Chem / Coums llct;i 40 60 Count_Time(min) Quench_number :.r 60.00 . 711.01 :it' " / Counts Chem / Counts Dela Pu24I_cpm 10.49 Run_Date 9/23/2016 9:34 PM Gross_B_CPM 10.70 Lumex_CPM 0.30 LUMEX 0.00 DPM 0.00 Pu24l_cpm 9.81 Run_Date 9/23/2016 10:35 PM Gross_B_CPM LUMEX 10.20 0.00 Lumex_CPM DPM 0.40 0.00 Pu241_cpm 9.69 Run_ Date 9/23/2016 11 :36 PM Gross_B_CPM 10.00 Lumex_CPM 0.40 LUMEX 0.00 DPM 0.00 Wallac 1400 DSA. P04AS243.DAT, 9/24/2016, page 5 Pu-241 TEAL Rack_position Count_Time(min) Quench_number 0 1 60.00 ,*, :*** / Counts Cl1cm / Counts Dela Rack_position Count_ Time(min) Quench_number 0 2 60.00 704.95 15-----i I / Counts --j Chem I / Counts Beta 100 Pu24l_cpm 10.01 Run_Date 9/24/2016 0:38 AM Gross_B_CPM 10.20 Lumex_CPM 0.20 LUMEX 0.00 DPM 0.00 Pu24l_cpm 9.62 Run_Date 9/24/2016 1:39 AM Gross_B_CPM LUMEX 9.90 0.00 Lumex_CPM DPM 0.30 0.00 Wallac 1400 DSA, P04AS243.DAT, 9/24/2016, page 6 Page 5610of5809 Pu-241 TEAL PROTOCOL DATE : 4 Pu-241 60 min : 2016/09/24 TIME : 03:52 ID : P04AS244 Pu-241 Wallac 1414 v3.0 S/N4140421 Counting mode : CPM lsotope(s) : H3 H3 = 5-350, 12.43 y Protocol name : Pu-241 60 min Counting time : 3600 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 10 Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Spectrum,Header,Listing Header : Pu-241
  • Spectrum : Rnd.Cos,Beta Window 1 25-220 /Beta Window 2 25-220 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 153.0 CPM Wallac 1400 DSA, P04AS244.DAT, 9/24/2016, page 1 Page 5611of5809 Pu-241 TEAL -----**--*--***---*-*-*---**-***-----.. ----*-----.. Rack_position Count_Time(min) Quench_number 87 3 I L( J5i....----r-----.----.----.--60.00 711.67 / Counts Chem / Counts 20 40 60 80 JOO Beta Rack_position Count_ Time(min) Quench_number 87 4 60.00 709.68 / Cou111s Chem / Counts Beta Rack_position Count_Time(min) Quench_number 87 5 ; 60.00 709.58 \ Lp 15 10-1 --1----// Counts Chem / Counts I&. UUllWl' Beta 20 40 60 80 100 ':} ., Pu24l_cpm 9.18 Run_Date 9/24/Wl6 3:52 AM Gross_B_CPM LUMEX 9.60 0.00 Lumex_CPM DPM 0.40 0.00 Pu24l_cpm 9.48 Run_Date 9/24/2016 4:53 AM Gross_B_CPM 9.80 Lumex_CPM 0.30 LUMEX 0.00 DPM 0.00 Pu24l_cpm 9.62 Run_Date 9/24/2016 5:54 AM Gross_B_CPM 9.90 Lumex_CPM 0.30 LUMEX 0.00 DPM 0.00 ... ---Wnllac 1400 DSA, P04AS244.DAT, 9/24/2016, page 2 Page 5612 of 5809 Pu-241 TEAL Rack_position Count_Time(min) Quench_number \I 87 6 60.00 710.30 15----,-----,.----**..,..* --.., / Counls 10 Chem / Couius Beta Rack_position Count_Time(min) Quench_number 87 7 60.00 708.61 I ' / Counts Chem 4 -/ Counts 2 Bela " 1lillill11 ,11 20 40 60 80 100 Rack_position Comit_Time(min) Quench_number 87 8 .!;., 60.00 710.30 ,,. 15 ----------/ Counts Chem / Counts Beta Pu24l_cpm 8.67 Run_Date 9/24/2016 6:55 AM Gross_B_ CPM LUMEX 8.90 0.00 Lumex_CPM DPM 0.30 0.00 Pu24l_cpm 9.57 Run_Date 9/24/2016 7:57 AM Gross_B_CPM LU MEX 10.00 0.00 Lumex_CPM DPM 0.40 0.00 Pu241_cpm 8.72 Run_Date 9/24/2016 8:58 AM Gross_B_CPM LUMEX 9.20 0.00 Lumex_CPM DPM 0.50 0.00 --*-----------------*----*-W<\.Bac 1400 DSA; P04AS244.DAT, 9/24/2016, page 3 Page 5613 of 5809 Pu-241 TEAL Rack_position Courit_ Time(min) Quench_number 87 9 60.00 707.22 15 ----/ Counts Chem / Counts Bela Rack_posi ti on Couht_ Time(min) Quench_number 87 10 60.00 709.22 JO / Coun1s Chem / Counts Beta Rack_position Com1t_Time(min) Quench_number ro-?J 11 :: 60.00 ' 709.84 f / Couuts Chem I I / Counts I Beta I It'{) Pu24l_cprn 9.85 Run_Date 9/24/2016 9:59 AM Gross_B_CPM LUMEX 10.20 0.00 Lumex_CPM DPM 0.30 0.00 Pu24l_cpm 9.79 Run'_.Date 9/24/2016 11 :00 AM Gross_B_CPM LUMEX 10.10 0.00 Lumex_CPM DPM 0.30 0.00 Pu24l_cprn 8.81 Run_Date 9/24/2016" 12:01 PM Gross_B_CPM LUMEX 9.20 0.00 Lumex_CPM DPM 0.40 0.00 .. --*-*-* .. -*----***** .. ---*----*--.*****-* .. -.-.----* _____ ,. -**********--***-****-*--*-** -... Wallac 1400 DSA, P04AS244.DAT, 9/24/2016, page 4 Page 5614 of 5809 Pu-241 TEAL Rack_position Count_ Time(min) Quench_number Pu241_cpm Run_Date 87 12 l 60.00 708.76 32.43 9/24/2016 1:02 F>M 4{J. 'r.: ,, l Gross_B_CPM LUMEX 30* ----.--1* / Counts 32.90 0.00 Chem I Lumex_CPM DPM 0.50 0.00 / Counts 10 Beta I 20 40 60 80 100 Wallac 1400 DSA, P04AS244.DAT, 9/24/2016, page 5 Page 5615of5809 Alpha Spectros.eopy *.;ersion 3.5.3 effective d.!!ite: 02*fMr.2015 BATCH NUMBER : 1596414 SAMPLE ID : R0405235041_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT. SAMPLE QTY : 0.509 G +/-0.196 % CHAMBER : 067 DETECTOR S/N : 78780 AVERAGE %EFFICIENCY : 29.1959 AVERAGE %EFF ERROR : 0.5641 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 69.6 +/-9.741 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 3.051 OE+OO dpm COUNT DATE : 22-Sep-2016 09:56:19 ELAPSED LIVE TIME( SEC) : 7510.30 NUCLIDE ACTIVITY SUMMARY NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 8 r l'U-244: 4497-4597 keV ; PU*242: 4654-4995 keV I PU*Zl9: 5011-5227 k*V 7 *-PU*238: 537&-5566 keV I PU-Z!Q: 5582.5043 keV 6L I 5L 4L I ! 3 l 2 I 1 I ENERGY FWHM 5634.56 4.935 5461.05 19.738 5118.69 0.000 4862.17 92.935 4556.91 4.935 II l l Ii . ' 2379 2776 3177 3583 3992 Energy (keV) 440 0. AREA 1.000 2.000 0.000 112.000 1.000 4824 "' ;:\ :::. "-AREA AREA St Dev pCi/G 0.374 0.626 0.7911 100.000 1.59E-02 2.000 0.000 0.0000 99.900 7.01E-02 -0.250 0.250 0.5003 99.900 -8.72E-03 '111.499 0.501 0.7076 100.000 3.88E+OO 1.000 0.000 0.0000 99.900 3.48E-02 . I 5 4* 672 6102 6537 6976 7419 .. ; " "-0. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B067.CNF;1813 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W067.CNF;476 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.20E-01 2.44E-01 5.85E-02 1.20E-01 1.05E-01 O.OOE+OO 7.02E-02 1.65E-01 3.04E-02 1.05E+OO 1.90E-01 4.30E-02 9.71E-02 1.04E-01 O.OOE+OO 1.96-sigma cnt Unc pCi/G 1.20E-01 1.19E-01 6.98E-02 7.25E-01 9.69E-02 BATCH NUMBER : 1596414 SAMPLE JD : R0405235042 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 069 DETECTOR S/N : 78795 AVERAGE %EFFICIENCY : 32.9662 AVERAGE %EFF ERROR : 0.6355 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 79.8 +/-8.595 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.4981 E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 12 ! 11 L PU:239:5011-5227koV j PU-238: 5375-5566 keV l 0 ;-PU*235: 5582-5843 keV 8L 7L 61 4 1-f'.'EAK ENERGY 5712.25 5470.34 5118.68 4905.23 4546.97 PEAK FWHM 0.000 0.000 0.000 69.971 0.000 1 L ! l I r--r-'t-+-c-. 2404 2802 3206 3614 4026 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:19 ELAPSED LIVE TIME(SEC) : 7518.12 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.251 0.251 0.5006 100.000 -8.34E-03 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 0.000 -0.376 0.376 0.6131 99.900 -1.03E-02 145.000 144.499 0.501 0.7080 100.000 3.95E+OO 0.000 -0.125 0.125 0.3540 99.900 -3.43E-03 ll > >> > .I! .I! UI .,_ .,._ i 'II iii ill I J [ l I .Jl1 "' mm Sl "'"' i . I ' r---. !--*-r--r-r 486 5 BB 5718 I . --.-..,-. -. -. . 6152 6591 7034 7481 lnstr'dment SOP: GL-RAD-l-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B069.CNF;1819 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W069.CNF;495 CAL DA TE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.70E-02 1.58E-01 2.91E-02 5.46E-02 8.26E-02 O.OOE+OO 5.55E-02 1.41 E-01 2.93E-02 9.40E-01 1.50E-01 3.38E-02 5.47E-02 1.16E-01 1.69E-02 1.96-sigma cnt Unc pCi/G 6.68E-02 5.44E-02 5.53E-02 6.47E-01 5.45E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235043_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.507 G +/-0.197 % CHAMBER : 070 DETECTOR S/N : 78262 AVERAGE %EFFICIENCY : 31.2964 AVERAGE %EFF ERROR : 0.6038 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 88.8 +/-8.370 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.8901 E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 -------*-* 00 14 ,..-PU-244: 4497-4597 keV ! PU*242: 4654-4995 keV 13 f-PU-239: 5011 *5ZZ7keV 12 L PU-238: 5375-5566 keV I f'U.236: 5582-5843 keV 11 i 10 [-9 f--8 I 6f-5 r-4 L I 2 f-PEAK ENERGY 5712.24 5464.34 5118.67 4871.68 4545.79 PEAK FWHM 0.000 4.900 0.000 53.083 4.900 COUNT DATE : 22-Sep-2016 09:56:19 ELAPSED LIVE TIME(SEC) : 7521.69 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.752 0.752 0.8673 100.000 -2.34E-02 1.000 0.624 0.376 0.6133 99.900 1.60E-02 0.000 -0.627 0.627 0.7917 99.900 -1.60E-02 153.000 152.624 0.376 0.6133 100.000 3.89E+OO 1.000 1.000 0.000 0.0000 99.900 2.55E-02 I '1 ,, !i l j1 ii i*I 11 l 11[ ' z ::::> 0 8 t5 <( 1 ! ... ,--'-,-i* ... ! l l ,11 ' *I I. -.ii! ' i , , . l -.. ! I . . . ' l . 2381 2775 3175 3578 3987 440 4818 41 668 6100 6537 6978 7424 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8070.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W070.CNF;500 CAL DATE ; 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.44E-02 1.87E-01 4.70E-02 7.25E-02 1.32E-01 2.75E-02 5.25E-02 1.47E-01 3.53E-02 9.03E-01 1.31E-01 2.73E-02 7.12E-02 7.66E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.42E-02 7.24E-02 5.24E-02 6.21E-01 7.11E-02 Alpha Specirosoopy Software Vetsion 3.5.3 effective date: 02-Mar-2015 BATCH NUMBER : 1596414 SAMPLE ID : .R0405235044 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 071 SAMPLE QTY : 0.505 G -+/-0.198 % ! DETECTOR S/N : 80020 ! AVERAGE %EFFICIENCY : 32.1394 I AVERAGE %EFF ERROR : 0.6198 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST :* HAKB % YIELD : 75.0 +/-8.598 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.2855E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 14 PU-24*hl497 ... 557 keV PU-242: 4054 ... 995 keV 13 12 11 10 9 8 7 6 5 4 3 2 1 PU*239: 5011*5227 keV r PU*23B: 5375-5566 keV PU-235: 5582-5843 keV [ L r I r r-I r I t .. ! j PEAK ENERGY 5712.25 5470.34 5127.52 4893.28 4514.88 I I . I PEAK FWHM 0.000 0.000 4.953 47.057 4.953 ! I ii ! ; ! i I 23 99 2798 3201 3608 4020 44rn -Energy (keV) I COUNT DATE : 22-Sep-2016 09:56:24 I ELAPSED LIVE TIME(SEC) : 8207.94 i ! _J_ __ NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.274 0.274 0.5231 100.000 -9.02E-03 0.000 -0.137 0.137 0.3699 99.900 -3.73E-03 1.000 0.726 0.274 0.5231 99.900 1.97E-02 145.000 144.453 0.547 0.7397 100.000 3.91E+OO 1.000 1.000 0.000 0.0000 99.900 2.71E-02 11 !l 'I !1 Ii l! !I ! ' ... 'm' i I i h ! ' I I . ; ! . 4857 528 6146 6584 7027 7474 lnstrumenrSOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8071.CNF;1814 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W071.CNF;464 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.67E-02 1.59E-01 3.03E-02 5.46E-02 1.17E-01 1.77E-02 7.63E-02 1.31 E-01 2.49E-02 9.31E-01 1.51E-01 3.51E-02 7.56E-02 8.13E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.64E-02 5.44E-02 7.61E-02 6.41 E-01 7.54E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235045_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT ---CHAMBER : 072 SAMPLE QTY : 0.502 G +/-0.199 % DETECTOR S/N : 67584 AVERAGE %EFFICIENCY : 31.8335 AVERAGE %EFF ERROR : 0.6139 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : *73.0 .+/-8.753 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.1977E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 15 r PU*244: 4497-4597 keV I PlJ.242: "654-4995 keV I PlJ.239: 5011-5227 keV 13 L PlJ.238: 5375-5566 i<eV I PIJ.238: 5582*5843 keV 11 I 9 ! :t I 1 l PEAK ENERGY 5712.26 5407.13 5122.44 4867.99 4546.97 I PEAK FWHM 0.000 5.004 5.004 58.484 0.000 i I I ! 2377 2780 3187 Energy (keV) 3597 4013 4432 -COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8211.60 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 0.000 0.000 0.0000 100.000 O.OOE+OO 1.000 0.863 0.137 0.3699 99.900 2.45E-02 1.000 0.042 0.958 0.9788 99.900 1.19E-03 140.000 139.316 0.684 0.8272 100.000 3.93E+OO 0.000 0.000 0.000 0.0000 99.900 0.00E+OO I I l I ! I I !I ,., I I I " il -L i I' .g I I ! I ' . I . ' 4856 528) 57H 6152 6592 7037 7486 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8072.CNF;1821 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W072.CNF;475 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.83E-02 1.03E-01 O.OOE+OO 7.97E-02 1.22E-01 1.8'5E-02 8.14E-02 1.82E-01 4.85E-02 9.54E-01 1.67E-01 4.10E-02 5.61E-02 8.48E-02 O.OOE+OO '1 .96-sigma cnt Unc pCi/G 6.BOE-02 7.96E-02 8.12E-02 6.57E-01 5.59E-02 0 I-I) Vl 00 0 \0 BATCH NUMBER : 1596414 SAMPLE ID : R0405235046_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.514 G +/-0.195 % CHAMBER : 073 DETECTOR SIN : 78775 AVERAGE %EFFICIENCY : 33.5965 AVERAGE %EFF ERROR : 0.6474 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 77.0 +/-8.313 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS. : 3.3753E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5659.37 PU-238 5486.00 5438.60 PU-239 5155.00 5118.68 PU-242 4890.00 4861.75 PU-244 4589.00 4q46.97 13 i PU-244: 4497 ... 597 keV i PU-242: 465£-4995 keV 12 f-PU*23!1: 5011*5227 keV PU-23a: 5375-5566 keV 11 PU*23S: 5582*5843 keV 10 l-8 f.-en I 7!-I I-z 6\ ::> 0 5 ;-8 .c 3 *:;: 2 f-+:: (.) <( 1 ! . I 2384 2783 3185 *3593 Energy (keV) PEAK FWHM 4.947 4.947 0.000 55.965 0.000 ii I) il : ; 4004 44 COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8241.52 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.038 0.962 0.9806 100.000 1.15E-03 1.000 0.588 0.412 0.6419 99.900 1.46E-02 0.000 -0.687 0.687 0.8287 99.900 -1.70E-02 157.000 155.764 1.236 1.1119 100.000 3.84E+OO 0.000 -0.275 0.275 0.5241 99.900 -6.78E-03 :i !i S;"S; "' " ::f"'"' &i .., .., I 1;!1 ji!1 111 'I ,, I I j. I i 5 6, 5697 6132 6571 7015 7463 "' O> l'l "ii ::,i <)I ::> ::> ::> ::> ::> 0.. "-"-Q. Q. Instrument SOP: GL-RAD-1-009 Analytical SOP: G_L-RAD-A-035 LIB FILE : PU BKG FILE : B073.CNF;1820 BKG DA TE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W073.CNF;495 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 8.61E-02 1.93E-01 5.14E-02 7.03E-02 1.30E-01 2.BOE-02 5.12E-02 1.46E-01 3.59E-02 8.85E-01 1.70E-01 4.81 E-02 4.99E-02 L19E*01 2.27E*02 c0."v 1.96-sigma cnt Unc pCi/G 8.60E-02 7.01E-02 5.10E-02 6.08E-01 4.97E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235047 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 074 DETECTOR S/N : 83296 AVERAGE %EFFICIENCY : 30.3767 AVERAGE %EFF ERROR : 0.5864 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 76.4 +/-8.758 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.3481 E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 *PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 1 0 I PU-24-1' 4497-4597 J<s.V i PU*242 : 4854-4995 keV 9 LPU-23!! I PU-238 I PU-230 8 '-7 I 4 f-l 3 f-2 I 1 : 5011 *5227 keV : 5375-5568 keV : 5582*5843 kaV I! I JI i 'I I I PEAK ENERGY 5777.78 5470.35 5118.69 4834.56 4557.66 i ij!i r11 I I PEAK FWHM 4.988 0.000 0.000 93.942 64.845 I II I i I I Ii I \! 2383 2 784 3189 3599 4012 4430 -Energy (keV) COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8245.21 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 -0.237 1.237 1.1121 100.000 -8.06E-03 0.000 -0.137 0.137 0.3707 99.900 -3.89E-03 0.000 -0.275 0.275 0.5243 99.900 -7.73E-03 141.000 139.763 1.237 1.1121 100.000 3.93E+OO 3.000 3.000 0.000 0.0000 99.900 8.43E-02 j ii ii !I ;1 'I i 11 l-11 Jlll I i 11 11. iTi!*. 1!1* J lllL I I I I ! I : i I 4852 5t>7, 570E 6142 6580 7 022 7469 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B074.CNF;1838 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W074.CNF;511 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.89E-02 2.35E-01 6.65E-02 5.67E-02 1.22E-01 1.84E-02 5.69E-02 1.36E-01 2.59E-02 9.52E-01 1.94E-01 5.48E-02 1.11 E-01 8.43E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 9.88E-02 5.65E-02 5.66E-02 6.56E-01 1.10E-01 Alpha SpecOOSCOpy Software Veislon 3.5.3 eftectivedale: 02-ll.ar-2015 BATCH NUMBER : 1596414 SAMPLE ID : R0405235048_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 075 I DETECTOR SIN : 80010 SAMPLE QTY : 0.507 G +/-0.197 % j AVERAGE %EFFICIENCY : 32.3452 I AVERAGE %EFF ERROR : 0.6238 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 83.1 +/-8.150 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.6436E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.24 PU-238 5486.00 5470.34 PU-239 5155.00 5154.42 PU-242 4890.00 4853.22 PU-244 4589.00 4522.01 13 . 12 PU-244* 4497-4597 keV PU*242: 4654-4995 keV PU-239: 5011-5227 keV 11 j PU-239: 5375-5565 keV I PU*236: 5582-5843 l<aV 10 9 ! 8 00 7 I-6 z :::i 5 0 £ 4 3 2 ti <( 1 I r r r i [ I r : [I I j l ' -! I ' PEAK FWHM 0.000 0.000 29.504 90.151 19.669 !I I li 11 i !I ll I 23 79 2775 3175 3580 3990 4401> Energy (keV) I. COUNT DATE : 22-Sep-2016 09:56:24 ELAPSED LIVE TIME(SEC) : 8249.61 I NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G . 0.000 -0.962 0.962 0.9810 100.000 -2.81E-02 0.000 -0.137 0.137 0.3708 99.900 -3.33E-03 2.000 1.863 0.137 0.3708 99.900 4.48E-02 163.000 162.038 0.962 0.9810 100.000 3.89E+OO 2.000 2.000 0.000 0.0000 99.900 4.81E-02 I I I 11 iq 1:,! I; I" i : . *-' !'i-I /.I II II I I . ' . l . I .... I . 4824 4E 6109 6547 6989 7437 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W075.CNF;478 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.15E-02 1.88E-01 5.02E-02 4.85E-02 1.04E-01 1.57E-02 8.25E-02 1.03E-01 1.57E-02 8.79E-01 1.55E-01 4.14E-02 8.23E-02 7.22E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 6.13E-02 4.83E-02 8.22E-02 6.04E-01 8.19E-02 Alpha Spectrosoopy Software Vorslon 3.5:3 effective dale: 02./w1ar*20'5 BATCH NUMBER : 1596414 SAMPLE ID : R0405235049 PU SAMPLE QTY : 0.506 G -+/-0.198 % SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 79.6 +/-8.146 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831E+OO dpm RESULTS : 3.4906E+OO dpm GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 078 DETECTOR S/N : 38633 AVERAGE %EFFICIENCY : 33.4433 AVERAGE %EFF ERROR : 0.6444 COUNT DATE : 22-Sep-2016 09:56:26 ELAPSED LIVE TIME(SEC) : 8305.06 NUCLIDE ACTIVITY SUMMARY Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B078.CNF;1726 ! BKG DATE : 16-Sep-2016 i BKG LIVE TIME(SEC) : 59999.99 '1 EFF FILE : W078.CNF;447 . CAL DATE : 03-Sep-2016 I 1.96-sigma 1.96-sigma NUCLIDE LIBRARY PEAK PEAK GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le cnt Unc ENERGY ENERGY FWHM AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G PU-236 5749.00 5712.27 0.000 0.000 -0.692 0.692 0.8319 100.000 -2.03E-02 6.08E-02 1.73E-01 4.28E-02 6.06E-02 PU-238 5486.00 5470.35 0.000 0.000 -0.138 0.138 0.3720 99.900 -3.37E-03 4.87E-02 1.05E-01 1.59E-02 4.86E-02 PU-239 5155.00 5134.30 4.964 1.000 0.862 0.138 0.3720 99.900 2.0BE-02 6.78E-02 1.04E-01 1.58E-02 6.76E-02 PU-242 4890.00 4863.39 78.589 162.000 161.585 0.415 0.6444 100.000 3.90E+OO 8.81E-01 1.27E-01 2.73E-02 6.04E-01 PU-244 4589.00 4546.97 0.000 0.000 -0.138 0.138 0.3720 99.900 -3.35E-03 4.84E-02 1.04E-01 1.58E-02 4.83E-02 SS .,,_ l:; "' "' .* "'"' 11 -PlJ.2.U: 4497-4597 keV j PU-242: 4854-4995 keV 1 0 I PU*239: 5011*5227 keV j .. i PU*238: 5375-5566 keV I 9 PlJ.236: 5582*5843 keV . 00 I-I z 5' :::> 0 £ c l 2f--0 1 <( 111 ' . ' ! ! I I I I ; 2388 2787 3190 3597 4009 5 6 695 6126 6562 7002 7445 Energy (keV) ; "' :!! 'l' ::J ::J ::J 0. 0. 0.

GEL Laboratories LLC Instrument SOP: GL-RAD-1-009 ALPHA SPECTROSCOPY REPORT Analytical SOP: GL-RAD-A-035 BATCH NUMBER :* 1596414 CHAMBER : 080 LIB FILE : PU SAMPLE ID : R0405235050 PU SAMPLE QTY : 0.504 G -+/-0.198 % , DETECTOR SIN : 78197 1 BKG FILE : B080.CNF;1728 ., AVERAGE %EFFICIENCY : 34.4422 l BKG DATE : 16-Sep-2016 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 88.3 +/-7.644 % AVERAGE %EFF ERROR : 0.6633 -I BKG LIVE TIME(SEC} : 59999.99 I COUNT DATE : 22-Sep-2016 09:56:26 I EFF FILE : W080.CNF;446 ELAPSED LIVE TIME(SEC) : 8310.24 ! CAL DATE : 03-Sep-2016 I I TRACER ID : 1.770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.8723E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 PU*244: 4497-4597 keV F PU*2.12: A654-4995 keV 17 PU*239: 5011-5227 keV I PU-238: 5375-5566 keV 15 f-PU-236: 5582-5843 keV 13 11 i 9L I I 1 PEAK ENERGY 5712.26 5470.35 5118.69 4873.72 4585.20 ,....__ I .. 2386 2786 3190 3598 Energy (keV) PEAK GROSS FWHM AREA 0.000 0.000 0.000 0.000 0.000 0.000 47.164 185.000 4.969 1.000 11 ll II iii i!1 J I ! I I. il41 l ' I ! l I 4011 4428 4849 ..... NUCLIDE ACTIVITY SUMMARY 1.96-sigma NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA StDev pCi/G pCi/G pCi/G pCi/G -0.139 0.139 0.3722 100.000 -3.56E-03 5.15E-02 1.11E-01 1.68E-02 -0.277 0.277 0.5263 99.900 -5.92E-03 4.32E-02 1.04E-01 1.97E-02 -0.554 0.554 0.7443 99.900 -1.18E-02 4.37E-02 1.19E-01 2.77E-02 184.723 0.277 0.5263 100.000 3.92E+OO 8.29E-01 1.03E-01 1.96E-02 0.723 0.277 0.5263 99.900 1.53E-02 5.98E-02 1.03E-01 1.96E-02 r,--I l . I i ; \ 51>7 5705 6139 6578 7021 7468 1.96-sigma cnt Unc pCi/G 5.14E-02 4.31E-02 4.36E-02 5.67E-01 5.97E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235051_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT Instrument SOP: GL-RAD-1-009 _ Analytical SOP: GL-RAD-A-035 LIB FILE : PU SAMPLE QTY : 0.502 G +/-0.199 % CHAMBER : 081 DETECTOR S/N : 79996 AVERAGE %EFFICIENCY : 33.0506 AVERAGE %EFF ERROR : 0.6369 I BKG FILE : B081.CNF;1734 BKG DATE : 16-Sep-2016 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 74.7 +/-8.464 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RES UL TS : 3.2730E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.23 PU-238 5486.00 5470.33 PU-239 5155.00 5118.67 PU-242 4890.00 4864.26 PU-244 4589.00 4546.97 13 ,---f'U.2 .... : .... 97-4597 keV ! PU-242: 4654-4995 keV 12 t-PU*239: 5011*5227 keV L PU-238: 5375-5565 keV 11 ; PU-236: 5582*5843 keV 10 9 \-I 8 r-00 7t I-z 6 t-::> 0 £ 4L >-3l :!: > +:; 0 <i:: 1 L j ,-: .-. -. -. -! ' i PEAK FWHM 0.000 0.000 0.000 77.280 o:ooo I' I ! 1i l II 2384 2779 3178 3582 3991 440 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:26 ELAPSED LIVE TIME(SEC) : 8313.82 NUCLIDE ACTIVITY SUMMARY j BKG LIVE TIME(SEC) : 59999.99 I EFF FILE : W081.CNF;446 l CAL DATE : 03-Sep-2016 1.96-sigma 1.96-sigma GROSS NET BKG BKG %ABLIN ACTIVITY TPU MDA Le cnt Unc AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G pCi/G 0.000 -0.139 0.139 0.3722 100.000 -4.41E-03 6.38E-02 1.37E-01 2.08E-02 6.36E-02 0.000 0.000 0.000 0.0000 99.900 O.OOE+OO 5.25E-02 7.93E-02 O.OOE+OO 5.23E-02 0.000 -0.554 0.554 0.7445 99.900 -1.46E-02 5.41E-02 1.47E-01 3.43E-02 5.39E-02 151.000 149.891 1.109 1.0529 100.000 3.93E+OO 9.22E-01 1.76E-01 4.85E-02 6.34E-01 0.000 -0.277 0.277 0.5264 99.900 -7.28E-03 5.31E-02 1.27E-01 2.43E-02 5.29E-02 >> > oo _!! """" m ..... "'"' i \I 'ill 1,, *11 p Ii t ' I 4823 6106 6543 6985 7432 "' <O '!i :::i :; :> :::i c. c. 0.. c.. c. BATCH NUMBER : 1596414 SAMPLE ID : R0405235052_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.508 G +/-0.197 % CHAMBER : 082 DETECTOR SIN : 79997 AVERAGE %EFFICIENCY : 31.9848 AVERAGE %EFF ERROR : 0.6168 SAMPLE DATE : 07-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 68.6 +/-8.975 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.0072E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5821.05 PU-238 5486.00 5470.33 PU-239 5155.00 5118.67 PU-242 4890.00 4861.94 PU-244 4589.00 4501.82 13 P\J.244: 4497-4597 keY j PU*2A2: '854-1995 keV 12 r PU*239: 5011-5227 keV j Ptl*238: 5375-5568 keV 11 r PU*ZlS: 5582*58431;ev* 10 L Cii I 7L I-z :J 5 t-0 2-4L c :?i 21 0 <( 1 [_JLJ I , . , j *. 2394 2787 3185 3588 Energy {keV) PEAK FWHM 4.883 0.000 0.000 51.270 4.883 3996 440 ll COUNT DATE : 22-Sep-2016 09:56:26 ELAPSED LIVE TIME(SEC) : 8317.64 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.584 0.416 0.6449 100.000 2.06E-02 0.000 -0.693 0.693 0.8325 99.900 -2.04E-02 0.000 -2.357 2.357 1.5351 99.900 -6.88E-02 135.000 133.336 1.664 1.2898 100.000 3.89E+OO 1.000 0.861 0.139 0.3723 99.900 2.51E-02 > l:l ...... :e mm " "" iii .,.,, El .,., I i; 1! I 1 i I I .,--,--I I . 4826 5 4 676 6108 6545 6987 7434 N 0 "' "' it 0.. 0. ,._ Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8082.CNF;1724 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W082.CNF;423 CAL DATE : 03-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 1.00E-01 1.86E-01 4.00E-02 6.10E-02 1.74E-01 4.29E-02 6.66E-02 2.45E-01 7.86E-02 9.66E-01 2.19E-01 6.60E-02 8.18E-02 1.26E-01 1.91E-02 1.96-sigma cnt Unc pCi/G 9.98E-02 6.08E-02 6.63E-02 6.67E-01 8.16E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235053_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU SAMPLE QTY : 0.500 G +/-0.200 % CHAMBER : 089 DETECTOR S/N : 79988 AVERAGE %EFFICIENCY : 29.2461 AVERAGE %EFF ERROR : 0.5651 I BKG FILE : B089.CNF;1433 BKG DATE : 16-Sep-2016 II BKG LIVE TIME(SEC) : 60000.00 SAMPLE DATE : 01-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 83.8 +/-8.522 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.671 OE+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 12 ,-FIJ*244: 4497-45"7 keV j FIJ-242: 4654-4995 keV 11 i--PU-239: 5011-5227 keV i PIJ.238: 5375-5500 keV 1 Q r-FIJ*236: 5582*511-<3 keV 9 l--l 8! 7[ I 6 f-. I ! 3 f-2 I 1 l-1 PEAK ENERGY 5689.75 5464.90 5111.91 4887.02 4538.81 ii I. PEAK FWHM 158.029 103.707 118.522 76.957 83.953 1!1 *11 ,:Ii I, I I ' i ) I 2394 2791 3193 3 598 4006 4419 -Energy (keV) COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8465.80 NUCLIDE ACTIVITY SUMMARY I EFF FILE : W089.CNF;384 i CAL DATE : 06-Sep-2016 i 1.96-sigma GROSS NET BKG BKG %ABUN ACTIVITY TPU MDA Le AREA AREA AREA StDev pCi/G pCi/G pCi/G pCi/G 2.000 -2.092 4.092 2.0228 100.000 -6.64E-02 1.18E-01 3.21E-01 1.13E-01 4.000 2.871 1.129 1.0624 99.900 7.54E-02 1.18E-01 1.77E-01 4.90E-02 2.000 0.307 1.693 1.3012 99.900 8.01E-03 9.24E-02 1.98E-01 5.97E-02 156.000 151.485 4.515 2.1249 100.000 3.95E+OO 9.32E-01 2.73E-01 9.73E-02 3.000 2.012 0.988 0.9938 99.900 5.25E-02 1.05E-01 1.69E-01 4.56E-02 Ii I ' [!; j lff I 1* i I , . ... ! 11** u fl' I i I I I ,. iJ" ii I . i "-,.-I . ' ' ' l * ! j ** 4836 5 )Si 1>682 6110 6543 6980 7420 1.96-sigma cnt Unc pCi/G 1.18E-01 1.17E-01 9.23E-02 6.42E-01 1.04E-01 BATCH NUMBER : 1596414 SAMPLE ID : R0405235054 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G -+/-0.200 % CHAMBER : 090 DETECTOR S/N : 78263 AVERAGE %EFFICIENCY : 33.4344 AVERAGE %EFF ERROR : 0.6443 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 76.0 +/-8.237 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.3314E+OO dpm NUCLIDE . LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.25 PU-238 5486.00 5470.34 PU-239 5155.00 5118.68 PU-242 4890.00 4876.09 PU-244 4589.00 4565.61 12 l PU*244: 4497-4597 keV 1 PlJ.242: .4654-.4995 keV 11 r-1 0 PU*236: 5582-5843 keV $ 7 6 i-I-z ::J 0 £ I .?;-3 f-! 2 f--t5 1 L <t: I I i 11 I i * ! .. ! . ! 2398 2796 3199 3606 Energy (keV) PEAK FWHM 0.000 0.000 0.000 89.071 4.948 I 4018 44 ...... .... :::> ll. COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8495.79 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABLIN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 -0.425 0.425 0.6518 100.000 -1.29E-02 0.000 -0.283 0.283 0.5322 99.900 -7.14E-03 0.000 -0.283 0.283 0.5322 99.900 -7.10E-03 158.000 157.717 0.283 0.5322 100.000 3.95E+OO 1.000 0.858 0.142 0.3763 99.900 2.15E-02 8&1 g :g:g i I j li i11 lil I I ! 711 6145 6584 7028 7476 :S :::> ll. ll. ll. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B090.CNF;1438 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W090.CNF;374 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pC:i/G 6.23E-02 1.61E-01 3.49E-02 5.11E-02 1.23E-01 2.36E-02 5.07E-02 1.22E-01 2.34E-02 9.01E-01 1.22E-01 2.34E-02 7.03E-02 1.08E-01 1.66E-02 \\'\{\ U\ 1.96-sigma cnt Unc pCi/G 6.21E-02 5.09E-02 5.06E-02 6.19E-01 7.02E-02 GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT BATCH NUMBER : 1596414 SAMPLE ID : R0405235055 PU SAMPLE QTY : 0.510 G -+/-0.196 % CHAMBER : 091 DETECTOR SIN : 78259 AVERAGE %EFFICIENCY : 34.7245 AVERAGE %EFF ERROR : 0.6687 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 64.1 +/-8.794 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831E+OO dpm RESULTS : 2.8085E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 14 r PIJ.244: 4497-1597 koV l PU*242: 4654-4995 keV 13 I 5011-5227 koV 11 1-10 9 f-8 7[-3 1-1 L I . PEAK ENERGY 5712.25 5470.34 5180.03 4864.81 4583.70 I . . . PEAK FWHM 0.000 0.000 4.930 40.262 4.930 IH IJ. j

  • ill i I , 2382 2779 3180 3586 3996 44 1 -Energy (keV) COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8499.46 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.708 0.708 0.8416 100.000 -2.42E-02 0.000 -0.708 0.708 0.8416 99.900 -2.00E-02 1.000 -0.558 1.558 1.2483 99.900 -1.57E-02 139.000 138.150 0.850 0.9219 100.000 3.87E+OO 1.000 0.858 0.142 0.3764 99.900 2.41E-02 I I ! Ii !j 1lj i!j !i ,ii I I'* 11 ! f I l . . I ! llt .* ii i l ! j ' : 4831 5:P5f: l683 6116 6553 6996 7442 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B091.CNF;1436 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W091.CNF;363 CAL DATE : 06-Sep-2016 L 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.10E-02 2.03E-01 5.04E-02 5.88E-02 1.68E-01 4.18E-02 8.25E-02 2.07E-01 6.15E-02 9.43E-01 1.75E-01 4.54E-02 7.87E-02 1.21E-01 1.86E-02 1.96-sigma cnt Unc pCi/G 7.07E-02 5.86E-02 8.23E-02 6.50E-01 7.85E-02 0 1-+i VI 00 0 \0 BATCH NUMBER : 1596414 SAMPLE ID : R0405235056 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.509 G -+/-0.196 % CHAMBER : 092 DETECTOR S/N : 80063 AVERAGE %EFFICIENCY : 30.3421 AVERAGE %EFF ERROR : 0.5858 SAMPLE DATE : Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 98.2 +/-7.671 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.3056E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5708.47 PU-238 5486.00 5470.34 PU-239 5155.00 5118.68 PU-242 4890.00 4876.40 PU-244 4589.00 4528.02 15 _ PU-244: 4497-4597 keV i PU*242: 4654-4995 keV i PlJ.239: SOI 1-5227 keV 13 f-PU-238: 5375-5566 keV I PU*236: 5582*5843 keV I 11 L I I Ui 9f-I f-7 f-z :::J i 0 () 5 f--i c :?! I t> I <: 1 f-!: Ii I l! l 2406. 2802 3203 3608 Energy (keV) PEAK FWHM 4.922 0.000 0.000 50.204 4.922 i ! i I 4017 44 COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8503.81 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 1.000 0.000 0.0000 100.000 2.55E-02 0.000 -0.992 0.992 0.9960 99.900 -2.09E-02 0.000 -0.850 0.850 0.9222 99.900 -1.78E-02 187.000 185.158 1.842 1.3574 100.000 3.88E+OO 4.000 3.717 0.283 0.5324 99.900 7.79E-02 ...... I ' ' . ! 1 . p698 6129 6565 7005 7449 i .. i!l Ol ::, ::, "-c.. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035
  • LIB FILE : PU BKG FILE : 8092.CNF;1440 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W092.CNF;414 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 7.11E-02 7.65E-02 O.OOE+OO 4.47E-02 1.37E-01 3.69E-02 4.40E-02 1.31E-01 3.40E-02 8.24E-01 1.63E-01 5.00E-02 9.32E-02 1.02E-01 1.96E-02 1.96-sigma cnt Unc pCi/G 7.10E-02 4.46E-02 4.39E-02 5.63E-01 9.25E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235057 _PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.500 G +/-0.200 % CHAMBER : 093 DETECTOR S/N : 33206 AVERAGE %EFFICIENCY : 33.0892 AVERAGE %EFF ERROR : 0.6377 SAMPLE DATE :. 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 78.6 +/-8.140 % TRACER ID : 1770-A NUCLIDE : PU-242 . NOMINAL : 4.3831 E+OO dpm RESULTS : 3.4468E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5708.26 PU-238 5486.00 5470.35 PU-239 5155.00 5164.40 PU-242 4890.00 4914.26 PU-244
  • 4589.00 4496.21 14 PU-244: 4491-4597 keV f PlJ.242: 4654-4995 kcV 13 '-PU-239: 5011*5227 keV 12 L PtJ.238: 5375-5566 keV I P\J-236: 5582*5543 keV 11 L. 10 $ 8 i-I-z ::> 0 5 i--Q. z. I *:;: 3 f-+; 0 <( 1 f-I I 2407. 2806 3210 3617 Energy (keV) PEAK FWHM 0.000 0.000 4.969 58.384 0.000 I II ' ' ' 4029 4 II I COUNT DATE : 22-Sep-2016 09:56:29 ELAPSED LIVE TIME(SEC) : 8507.47 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCl/G 2.000 1.291 0.709 0.8420 100.000 3.84E-02 0.000 -0.851 0.851 0.9224 99.900 -2.09E-02 1.000 0.433 0.567 0.7531 99.900 1.06E-02 162.000 161.716 0.284 0.5325 100.000 3.95E+OO 2.000 1.858 0.142 0.3766 99.900 4.54E-02 ;g m:: ... :e ......... .,:;i 1:l i ,, I.I ill 'i' !1 ,, :11 li t: 4 4863 6145 6580 7019 7462 ... N (\\ ... :::> :::> :j :j 0. "-a. "-Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B093.CNF;1429 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W093.CNF;379 CAL DATE : 06-Sep-2016 1.96-sigrna TPU MDA Le pCi/G pCi/G pCi/G 1.03E-01 1.77E-01 4.40E-02 5.17E-02 1.54E-01 3.99E-02 6.95E-02 1.38E-01 3.24E-02 8.90E-01 1.19E-01 2.29E-02 8.39E-02 1.06E-01 1.62E-02 1.96-sigrna cnt Unc pCi/G 1.03E-01 5.15E-02 6.94E-02 6.11E-01 8.35E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235058 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.512 G -+/-0.195 % CHAMBER : 095 DETECTOR S/N : 38626 AVERAGE %EFFICIENCY : 30.4247 AVERAGE %EFF ERROR : 0.5873 SAMPLE DATE : 02-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 76.2 +/-8.565 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831E+OO dpm RESULTS : 3.3404E+OO dprn NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.0P PU-242 4890.00 PU-244 4589.00 , PU-244:4497-4597 keV I PU-242: 4654-4995 keV 15 I PU-239: 5011*5227 keV I PtJ.238: 5375-5568 keV 13 PU*238: 5582-5843 keV I 11 f-s L i i 5 f-l I 3r-PEAK ENERGY 5725.89 5436.95 5144.38 4871.52 4517.34 1 L I I i* I I PEAK FWHM 4.993 4.993 4.993 74.066 4.993 i l 11 I
  • I 2380 2781 3186 3595 Energy (keV) 4007 4423 -COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 8560.38 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 1.000 0.144 0.856 0.9252 100.000 4.66E-03 1.000 0.429 0.571 0.7554 99.900 1.15E-02 2.000 1.429 0.571 0.7554 99.900 3.81E-02 145.000 145.000 0.000 0.0000 100.000 3.86E+OO 1.000 1.000 0.000 0.0000 99.900 2.66E-02 I I 1! ill ii 11 !I I i ,. , I I 11111 I I I I .. t . . I , . I . I . ! .. I . I .. 4843 5 6 >694 6125 6559 6997 7439 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B095.CNF;1405 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W095.CNF;408 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.30E-02 2.02E-01 5.26E-02 7.63E-02 1.52E-01 3.56E-02 9.21E-02 1.51E-01 3.54E-02 9.15E-01 7.98E-02 O.OOE+OO 7.43E-02 7.99E-02 O.OOE+OO 1.96-sigma cnt Unc pCi/G 9.28E-02 7.61E-02 9.19E-02 6.30E-01 7.42E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235059 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.503 G -+/-0.199 % CHAMBER : 096 DETECTOR SIN : 80016 AVERAGE %EFFICIENCY : 32.5188 AVERAGE %EFF ERROR : 0.6269 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 72.5 +/-8.515 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.1763E+OO dpm NUCLIDE l:.IBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 13 I PU*244: 4497..,597 keV t PU-242: 4654-4995 keV 12 f-PU-Zl9; 5011*5227 keV ! PtJ.238: 5375-5565 keV 11 J PU-235: 5582-5843 keV 10 r I 9:-4L 2 i PEAK ENERGY 5756.61 5414.05 5118.69 4878.73 4517.50 PEAK FWHM 4.934 4.934 0.000 70.307 4.934 COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 8564.06 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 1.000 0.286 0.714 0.8448 100.000 9.19E-03 1.000 0.572 0.428 0.6544 99.900 1.53E-02 0.000 -0.428 0.428 0.6544 99.900 -1.14E-02 148.000 147.429 0.571 0.7556 100.000 3.93E+OO 1.000 0.429 0.571 0.7556 99.900 1.14E-02 1 r-l I I I ! 111 ! -. -. -. -! , -.. -. t1*-. -. -. -I +-I-¥-I , . l I * ' . 2391 2788 3189 3595 4004 441 4837 5 6 687 6118 6554 6994 7438 Energy (keV) Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B096.CNF;1397 BKG DA TE : 16-Sep-'2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W096.CNF;357 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 9.18E-02 1.92E-01 4.77E-02 7.60E-02 1.42E-01 3.09E-02 5.45E-02 1.41E-01 3.07E-02 9.26E-01 1.51E-01 3.54E-02 7.59E-02 1.51E-01 3.54E-02 1.96-sigma cnt Unc pCi/G 9.16E-02 7.58E-02 5.43E-02 6.37E-01 7.57E-02 BATCH NUMBER : 1596414 SAMPLE ID : R0405235060_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G +/-0.194 % CHAMBER : 097 DETECTOR S/N : 83288 AVERAGE %EFFICIENCY : 35.3557 AVERAGE %EFF ERROR : 0.6805 SAMPLE DATE : 16-Dec-2015 00:00:00 ANALYST : HAKB % YIELD : 92.2 +/-7.310 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 4.0407E+OO dpm NUCLIDE LIBRARY PEAK ENERGY ENERGY PU-236 5749.00 5712.26 PU-238 5486.00 5470.35 PU-239 5155.00 5118.69 PU-242 4890.00 4882.92 PU-244 4589.00 4546.97 r PIJ.244: 4497.4597 keV 1 PU*24Z: 4654-4995 keV 17 I PU*239: S011 *5227 keV L PU-238: 5375-5566 keV 15 , PU*236: 5582*5843 keV 131 r 11 I Ci) I-z 1L ::> 0 ! 8 5 f-.?;-t5 ci::: I 1 I r. . I ' ' l . ' ' . ! ' 2402 2798 3198 3603 Energy (keV) PEAK FWHM 0.000 0.000 0.000 59.932 0.000 , I 4012 442 COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 8567.84 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.286 0.286 0.5344 100.000 -6.47E-03 0.000 -0.571 0.571 0.7558 99.900 -1.08E-02 0.000 -0.428 0.428 0.6545 99.900 -8.06E-03 205.000 204.000 1.000 0.9998 100.000 3.83E+OO 0.000 -0.143 0.143 0.3779 99.900 -2.69E-03 u; ::;; gg ., "'='"""J c:i s Sl fil ...... I I i JI d ., j1 I , I ' . I . 4842 5 5688 6118 6551 6989 7431 "' :> c. c. 0. Q. 0. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B097.CNF;1394 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W097.CNF;381 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.59E-02 1.11 E-01 2.13E-02 3.90E-02 1.07E-01 2.52E-02 3.84E-02 9.97E-02 2.17E-02 7.76E-01 1.22E-01 3.30E-02 3.77E-02 8.14E-02 1.25E-02 1.96-sigma cnt Unc pCi/G 4.57E-02 3.89E-02 3.83E-02 S.29E-01 3.76E-02 r BATCH NUMBER : 1596414 SAMPLE ID : R120S621754 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G -+/-0.194 % CHAMBER : 099 DETECTOR SIN : 80059 AVERAGE %EFFICIENCY : 35.6284 AVERAGE %EFF ERROR : 0.6858 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 85.7 +/-7.528 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.7576E+OO dpm NUCLIDE LIBRARY ENERGY PU-236 5749.00 PU-238 5486.00 PU-239 5155.00 PU-242 4890.00 PU-244 4589.00 17 i PlJ.239: 5011-5227keV 15 i-PlJ.238: 5375-5566 keV I PlJ.236: SSS2*5SoS3 keV 13 i 11 i 9 f--7 L sL ! I 1 f... i l i -PEAK ENERGY 5712.24 5413.43 5118.67 4878.90 4511.04 PEAK FWHM 0.000 4.881 0.000 61.418 24.405 2402 .2795 3193 3595 4001 441 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:32 ELAPSED LIVE TIME(SEC) : 8572.83 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCi/G 0.000 -0.857 0.857 0.9259 100.000 -1.72E-02 1.000 0.428 0.572 0.7560 99.900 8.60E-03 0.000 -0.286 0.286 0.5346 99.900 -5,.73E-03 192.000 191.286 0.714 0.8452 100.000 3.83E+OO 2.000 2.000 0.000 0.0000 99.900 4.01E-02 I I ii II I I i i Iii? rl ,/ illi'-: I L d ' . . , I -,-,-tr --:-* --r-, t , ' ' ' I ' ' 4829 5: 49 6104 6539 6978 7421 Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B099.CNF;1397 BKG DATE : BKG LIVE TIME(SEC) : 60000.00 EFF FILE : W099.CNF;383 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 4.22E-02 1.26E-01 3.27E-02 5.71E-02 1.14E-01 2.67E-02 4.06E-02 9.79E-02 1.8SE-02 7.99E-01 1.20E-01 2.98E-02 6.86E-02 6.02E-02 O.OOE+OO 1.96-sigma cnt Un_c pCi/G 4.21E-02 5.70E-02 4.05E-02 5.46E-01 6.83E-02 BATCH NUMBER : 1596414 SAMPLE ID : R1203621755 PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT CHAMBER : 103 DETECTOR S/N : 79461 SAMPLE QTY : 0.511 G -+/-0.196 % A VERA GE %EFFICIENCY : 33.8848 AVERAGE %EFF ERROR : 0.6527 SAMPLE DATE : 30-Nov-2015 00:00:00 ANALYST : HAKB % YIELD : 73.5 +/-8.243 % TRACER ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 3.2203E+OO dpm NUCLIDE LIBRARY PEAK ENERGY H:JERGY PU-236 5749.00 5712.26 PU-238 5486.00 5470.35 PU-239 5155.00 5118.69 PU-242 4890.00 4851.52 PU-244 4589.00 4546.97 14 _ PU*244: 44SN597 keV I PlJ.242: 4654-4995 keV 13 {-PU-239: 5011*5227 keV 12 i PU*238: 5375-5566 keV r P\!'236: 5582*5843 keV 11 i 10 f-8 f-<ii 71 I-z ;:) 0 5 r-4 f-3' *:;; :;::; (.) <( 1 \_. 11 I i ' l .. I I PEAK FWHM 0.000 0.000 0.000 78.116 0.000 iJ I I 2380 2779 3182 3590 4002 441 Energy (keV) ! COUNT DATE : 22-Sep-2016 09:56:16 ELAPSED LIVE TIME(SEC) : 8694.85 NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA St Dev pCi/G 0.000 -0.290 0.290 0.5384 100.000 -8.63E-03 0.000 -0.290 0.290 0.5384 99.900 -7.13E-03 0.000 -0.145 0.145 0.3807 99.900 -3.54E-03 159.000 158.131 0.869 0.9325 100.000 3.86E+OO 0.000 -0.145 0.145 0.3807 99.900 -3.54E-03 >> ... ,j 11 11 111 11, I: i I I ; 4837 5 6 690 6123 6560 7001 7446 "' " ;1; fil ::;, :; ::;, ::> ::> 0.. c.. c. c.. c. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : 8103.CNF;1412 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W103.CNF;395 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCi/G pCi/G pCi/G 6.04E-02 1.46E-01 2.82E-02 4.99E-02 121E-01 2.33E-02 4.91E-02 1.06E*01 1.64E-02 8.82E-01 1.54E-01 4.01E-02 4.91E-02 1.06E-01 1.64E-02 1.96-sigma cnt Unc pCi/G 6.02E-02 4.97E-02 4.89E-02 6.06E-01 4.89E-02 BATCH NUMBER : 1596414 SAMPLE ID : R1203621756_PU GEL Laboratories LLC ALPHA SPECTROSCOPY REPORT SAMPLE QTY : 0.515 G +/-0.194 % CHAMBER : 105 DETECTOR S/N : 78777 AVERAGE %EFFICIENCY : 33.6886 AVERAGE %EFF ERROR : 0.6490 SAMPLE DATE : 20-Sep-2016 00:00:00 ANALYST : HAKB % YIELD : 62.6 +/-8.930 % TRACER" ID : 1770-A NUCLIDE : PU-242 NOMINAL : 4.3831 E+OO dpm RESULTS : 2.7420E+OO dpm NUCLIDE LIBRARY PEAK PEAK ENERGY ENERGY FWHM PU-236 5749.00 57$7.11 4.933 PU-238 5486.00 5505.68 29.596 PU-239 5155.00 5126.05 108.519 PU-242 4890.00 4855.54 65.394 PU-244 4589.00 4537.21 4.933 11 r Pll-244: 4497-4597 kaV j PU-242: 4654*4995 keV 1 0 ;_ PU*23S: 5011*5227 kaV ! PU-238: 5375-5568 keV 9 f_ PU-235: 5582*5843 kaV I . ! Ui I-i z 5 r-::> ! 0 4 f-! 3[-0 I <( 1 r--I :--r-' I ' '. i I 2375 2772 3174 3580 3991 440 Energy (keV) COUNT DATE : 22-Sep-2016 09:56:16 ELAPSED LIVE TIME(SEC) : 8702.78 LCS ID NUCLIDE NOMINAL (pCi/G) % RECOVERY NUCLIDE ACTIVITY SUMMARY GROSS NET BKG BKG %ABUN ACTIVITY AREA AREA AREA StDev pCiJG 1.000 0.275 0.725 0.8516 100.000 7.87E-03 2.000 1.420 0.580 0.7617 99.900 4.07E-02 2.000 1.855 0.145 0.3808 99.900 5.31E-02 135.000 133.985 1.015 1.0076 100.000 3.83E+OO 1.000 0.565 0.435 0.6597 99.900 1.62E-02 '£ :i ...... .,_ ., "'"' .,_ ;:! :J:g .. :1 j I I I I -,-. -4827 5 51 681 6115 6553 6997 7444 iS N t'l "' 'l' g 1;l ::, ::> ::> 0.. 0.. 0.. 0.. Instrument SOP: GL-RAD-1-009 Analytical SOP: GL-RAD-A-035 LIB FILE : PU BKG FILE : B105.CNF;1396 BKG DATE : 16-Sep-2016 BKG LIVE TIME(SEC) : 59999.99 EFF FILE : W105.CNF;364 CAL DATE : 06-Sep-2016 1.96-sigma TPU MDA Le pCiJG pCiJG pCiJG 8.21E-02 1.72E-01 4.30E-02 9.92E-02 1.63E-01 3.84E-02 9.84E-02 1.24E-01 1.92E-02 9.49E-01 1.87E-01 5.08E-02 8.12E-02 1.52E-01 3.33E-02 1.96-sigma cnt Unc pCi/G 8.19E-02 9.89E-02 9.79E-02 6.54E-01 8.10E-02 \\Jlv Effective 31251201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist GL-CHL-RAD-013 Rev 1 Page 1of1 21-Sep-2016 Batch# )S) ]&{ / {; Product: ( $ Criteria: Yes No Comments Sample Solids are less than or eaual to 100 ma for GAB. J/r Samples have been blank corrected (If required). iv Jr Blank correction reported Included lif reoulredl. [f activity less than lOx MDA/ MDC, error Is less v than or equal to 1500/o of sample activity. If greater than 10* MDA/ MDC, error Is 40% or less. If beln.., the MnA I MDC. arrnr Is okav. Instrument source check Is within limits. c/ Instrument bka check Is within limits. Method RDL/ LLD has been met. /' If duplicate activities are: v Less than 5* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPD 20% or less, [f below the MDA/ MDC, the RPO is 0%, Or meets the client*s reaulred RER acceotance criteria. Tracer yield Is 15-125%
  • Carrier yield 25-125%. V' (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. 'Tf ... "% of lnouad "ctlvltv) / Sample was run within hold time. / < 0 0 1 I Sa mole was correctlv oreserved If reoulred. v Smears Taken for Radioactive batches. {'.j /,}-Method Spike and LCS are within 75-125% / I lfor meets the client's contract acceotance criteria), No blank spaces on data forms. / All line outs Initialed and dated. , .. _ -...... -........... __ ..... _..., _____ .. Aux data Is correct. /I/A Client Soeclal reoulrements oaae has been checked. v Raw Data and/ orsoectrum are included and orooerlv statused. v MS, LCS, and Duplicate RPD/RER values uploaded to LIMS and v V"lue<: verlflad ..... *-{If --t/'l'v /' ' -, :R!'lt-rh anta. .. lntn t'!'ac-.a. **-.. --Batch Data Exceotlon Reoorts fDERl comoleted If aaolicable. v '\Xk' /<y)'i!)t> I Batch Data Exception Reports (DER) second reviewed. 'l/ell 1ssqsn I Dlsnosition verified to be comnleted. Allauot Correction cnmnleted if rAnulred. Review sample historical results If available v (If REMP. results above MDC have been verified bv historical results recount or re-analvsls.) Primary Review Performed By: ,A-SuL -V, -q(Jt !no .... J rrmVi A. filfiJJy l v I
  • Page 5639 of 5809 GEL Laboratories LLC Form GEL-DER . DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 21-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC DOE EML HASL-300, Tc-02-RC Solid .. *-Batch ID: Sample Numbers: 1597416 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, and 1203624309 were received and analyzed out of the method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 21-SEP-16 Lyndsey Pace 21-SEP-16 Page 1 Page 5640 of 5809 DER Report No.: 1559801 Revision No.: 2
  • Type: Process Client Code: MJWC '

Prep Logbook tOIL{)lU The Determination of Technetium-99 Using Analytical Grade lXS Resin Batch ID: Analyst: Method: Lab SOP: Instrument: Sample ID 405235001 405235002 405235003 405235004 405235005 405235006 405235007 405235008 405235009 405235010 405235011 405235012 405235013 405235014 405235015 405235016 405235017 405235018 405235019 405235020 1203624308 MB 1597416 Angela Johnson DOE EML HASL-300, Tc-02-RC Modified GL-RAD-A-059 REV# 4 BAL-18550299 Prep Date Matrix 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 14-SEP-2016 05:23:51 Soil 1203624309 DUP (405235001) 14-SEP-2016 05:23:51 Soil 1203624310 LCS 14-SEP-2016 05:23:51 Soil __ t_ID __ __________ Amount 2280154.26 Hydrogen Peroxide 30% ACS Reagent 10 mL 2402130.4 2418926 2429641 2441205 2451825 TC20°(A '-i tl!.. /tdl{, 120LBS 30 Gfillons Ecoscint GL Scintillation Solution Quenching Agent RL-0.lM Hydrochloric Acid RL:O.OlM Nitric Acid RL*O. IM Nitric Acid tracer Analytical Logbook \"ersion I 11-04-2002 15mL .I uL lOOmL 20mL 25mL lmL __ LCS 1203624310 Technetium-99 SPIKE 1621-B Dry or Wet Unadjusted Aliquot w w w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) 1.914 1.542 2.089 1.622 2.317 1.915 1.98 1.596 2.013 1.603 2.281 1.836 2.168 1.707 2.099 1.664 2.161 1.65 2.226 1.778 2.428 2.032 2.176 1.807 2.363 1.853 2.315 1.964 2.299 2.135 2.077 1.652 2.088 1.618 2.119 1.66 2.032 1.676 2.011 1.724 2.135 2.181 1.757 2.135 CommenlS: Spike Pipet ID: RAD-LSC-2272418 Tracer Pipet JD: RAD-LSC-4099802 .1 GEL Laboratories LLC Filename : TC99.XLS File type : Excel Version#: 1.2.16 Batch: 1597416 Analyst: GXR1 Prep Date: 9/14/2016 Tc-99 Method Uncertainty : 0.0576 Geometry: 15ml Ecoscint GU5ml DI H20/AG 1x8 Resin Sam1 Sample Characteristics Sample Sample Aliquot Sample Aliquot StDev. Sample Pos. ID G G Date/Time 1 405235001.1 1.5420 3.3797E-03 12110/2015 14:20 2 405235002.1 1.6220 3.3880E-03 12110/2015 14:30 3 405235003.1 1.9150 3.4163E-03 12110/2015 14:35 4 405235004.1 1.5960 3.3853E-03 1219/2015 14:00 5 405235005.1 1.6030 3.3860E-03 12110/201513:15 6 405235006.1 1.6360 3.4102E-03 12110/2015 13:25 7 405235007.1 1.7070 3.3968E-03 12110/2015 13:55 8 405235008.1 1.6640 3.3923E-03 12110/2015 14:05 9 405235009.1 1.6500 3.3909E-03 12/10/2015 10:30 10 405235010.1 1.7780 3.4042E-03 12110/2015 10:35 11 405235011.1 2.0320 3.4305E-03 12191201510:13 12 405235012.1 1.8070 3.4072E-03 12/10/201511:25 13 405235013.1 1.8530 3.4119E-03 12181201511:23 14 405235014.1 1.9640 3.4234E--03 12181201510:49 15 405235015.1 2.1350 3.4411E-03 121812015 10:56 16 405235016.1 1.6520 3.3911E-03 12161201511:29 17 405235017.1 1.6180 3.3676E-03 121212015 10:02 16 405235018.1 1.6600 3.3919E-03 121212015 10:19 19 405235019.1 1.6760 3.3936E--03 12/B/2015 14:30 20 405235020.1 1.7240 3.3986E-03 121612015 13:50 21 1203624308.1 2.1350 3.4411E-03 9114/2016 0:00 22 1203624309.1 1.7570 3.4020E-03 12110/2015 14:20 23 1203624310.1 2.1350 3.4411E-03 9/14/2016 0:00 E1597416R Technetium-99 Solid Tracer SIN: Tracer Exp Date : Tracer Volume Added: Tracer Calculations Tracer Ref. Activity (CPM) 31859 31859 31659 31859 31859 31859 31859 31859 31859 31859 31859 31859 31859 31859 31859 31859 31859 31659 31859 31859 31659 31659 31859 Page 1 TC2074-A 9/1612016 1.00 Tracer Ref. Count Uncertainty (%) 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% 0.95% Tracer Samp. Activity (CPM) 29243 29088 29116 29406 27752 30052 27752 28939 28466 26132 29521 30040 28538 26603 29882 26276 28010 29392 26653 28656 29696 29563 30790 Procedure Code: Parmname: Required MDA: Tc-99 Abundance : Halfllfe of Tc-99 : Tracer Sa mp. Count Uncertainty (%) 0.95% 0.95% 0.95% 0.95% 0.95% 0.94% 0.96% 0.96% 0.94% 0.95% 0.95% 0.94% 0.95% 0.96% 0.95% 0.95% 0.96% 0.95% 0.94% 0.95% 0.95% 0.95% 0.94% LSC99TCS Technetium-99 5 pCUG 1.00 211100 years Tracer Tracer Aliquot Aliquot (ml) S!Dev. (ml) 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 1.0 0.002000 Pipel, 0.1 ml Stdev: +/-0.0002QO ml Plpet, 0.5 ml Stdev : +/-0.001000 ml Pipet, 1 ml Stdev: +/-0.002000 ml Analytical SOP: GL*RAD-A-059 Instrument SOP: GL*RAD*l-014 Count raw Data Counting Rack Time Quench# Gross Pas. Position# (min.) cpm 1 14*2 15 655.55 11.14 2 14-3 15 689.13 12.11 3 14-4 15 679.49 13.08 4 14*5 15 644.25 11.28 5 14.£ 15 672.78 12.87 6 14-7 15 666.74 11.83 7 14-8 15 648.12 13.01 8 14*9 15 667.26 13.35 9 14-10 15 639.9 11.83 10 14*11 15 658.09 11.14 11 14-12 15 635.02 11.97 12 0-1 15 662.93 12.53 13 0-2 15 661.34 12.73 14 0-3 15 663.58 14.46 15 14*2 15 676.07 1329 16 0-5 15 678.75 11.97 17 0-6 15 641.39 11.76 18 0-7 15 658.15. 12.87 19 0-8 15 674.28 13.08" 20 0*9 15 666.91 11.97 21 0-10 15 685.86 14.54 22 0-11 15 633.65 12.46 23 0*12 15 689.69 132.4 Bkg Count Corrected Count Bkg Time Bkg Bkg Start cpm (min.) Quench# cpm Dateffime 14.06 15 666.62 13.9735 9/20/2016 4:40 14.06 15 666.62 13.8613 9/2012016 4:56 14.06 15 666.62 14.0196 9120/2016 5:12 14.06 15 666.62 13.8048 9/20/2016 5:28 14.06 15 666.62 14.0624 9/20/2016 5:44 14.06 15 666.62 14.0604 9/20/2016 6:01 14.06 15 666.62 13.8696 9/20/2016 6:17 14.06 15 666.62 14.0619 9/20/2016 6:33 14.06 15 666.62 13.7255 9/2012016 6:49 14.06 15 666.62 14.0014 9/20/2016 7:05 14.06 15 666.62 13.6306 9/20/2016 7:21 14.06 15 666.62 14.0418 9/20/2016 7:38 14.06 15 666.62 14.0305 9/20/2016 7:54 14.06 15 666.62 14.0459 9/20/2016 8:10 14.06 15 666.62 14.0478 9/2012016 12:31 14.06 15 666.62 14.0269 9/20/2016 8:42 14.06 15 666.62 13.7533 9120/2016 8:56 14.06 15 666.62 14.0020 9120/2016 9:14 14.06 15 666.62 14.0572 9/20/2016 9:31 14.06 15 666.62 14.0609 9/20/2016 9:47 14.06 15 666.62 13.9289 9/20/2016 10:03 14.06 15 666.62 13.6032 9120/2016 10:19 14.06 15 666.62 13.8482 9/2012016 10:35 E1597416R Calculated Callbralion Data Detector Background Sample Sample Calibration Detector Efficiency Count Sample Recovery Recovery Counted Calibration Due Efficiency Error Background Start Decay % Error% on Date Date (cpm/dpm) (cpm/dpm) Position# Datetnme 1.000 91.8% 0.73% LSCYELLOW 7/412016 6/3012017 0.6297 0.00792 14-1 9/20/2016 12:15 1.000 91.3% 0.73% LSCYELLOW 7/4/2016 6130/2017 0.6477 0.00792 14*1 9/20/2016 12:15 1.000 91.41;1/o 0.73% LSCYELLOW 7/412016 6/30/2017 0.6450 0.00792 14*1 9/20/2016 12:15 1.000 92.3% 0.73% LSCYELLOW 7/4/2016 6/30/2017 0.6183 0.00792 14-1 9/20/2016 12:15 1.000 87.1% 0.73% LSCYELLOW 7/4/2016 6/3012017 0.6420 0.00792 14-1 9/20/2016 12:15 1.000 94.3% 0.73% LSCYELLOW 7/412016 6/30/2017 0.6384 0.00792 14*1 9/20/2016 12:15 1.000 87.1% 0.73% LSCYELLOW 7/4/2016 613012017 0.6225 0.00792 A 14*1 9/2012016 12:15 1.000 90.8% 0.73% LSCYELLOW 7/4/2016 6130/2017 0.6387 0.00792 14-1 9/20/2016 12:15 1.000 89.4% 0.73% LSCYELLOW 7/4/2016 6/30/2017 0.6132 0.00792 14-1 9/20/2016 12:15 1.000 88.3% 0.73% LSCYELLOW 7/412016 6130/2017 0.6319 0.00792 14-1 9/20/2016 12:15 1.000 92.7% 0.73% LSCYELLOW 7/412016 6/30/2017 0.6070 0.00792 14-1 9/2012016 12:15 1.000 94.3% 0.73% LSCYELLOW 7/4/2016 6130/2017 0.6357 0.00792 14*1 9120/201612:15 1.000 89.6% 0.73% LSCYELLOW 7/412016 6/30/2017 0.6345 0.00792 14-1 9/2012016 12:15 1.000 83.5% 0.73% LSCYELLOW 7/412016 6130/2017 0.6362 0.00792 14*1 9120/2016 12:15 1.000 93.6% 0.73% LSCYELLOW 7/4/2016 6130/2017 0.6436 0.00792 14*1 9/20/2016 12:15 1.000 88.8% 0.73% LSCYELLOW 714/2016 6130/2017 0.6447 0.00792 14-1 9/20/2016 12:15 1.000 87.9% 0.73% LSCYELLOW 7/4/2016 6130/2017 0.6150 0.00792 14-1 9/20/2016 12:15 1.000 92.3% 0.73% LSCYELLOW 714/2016 6130/2017 0.6320 0.00792 14-1 912012016 12:15 1.000 90.6% 0.73% LSCYELLOW 7/412016 6130/2017 0.6427 0.00792 14*1 9/20/2016 12:15 1.000 89.9% 0.73% LSCYELLOW 7/4/2016 613012017 0.6385 0.00792 14-1 9/20/2016 12:15 1.000 93.8% 0.73% LSCYELLOW 7/4/2016 6130/2017 0.6470 0.00792 14*1 9/20/2016 12:15 1.000 92.8% 0.73% LSCYELLOW. 7/412016 6130/2017 0.6052 0.00792 14-1 9/20/2016 12:15 1.000 96.6% 0.73% LSCYELLOW 7/4/2016 6130/2017 0.6478 0.00792 14*1 9/20/2016 12:15 Page2 Notes: 1 -Resulls are decay corrected to Sample Date/Time 2 -Reference date for Spike Activity (dpm/ml) is the batch Prep Date 3 -Spike Nominals are decay corrected to Sample Datemme * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 1.6073 1.1348 5 2.3706 -1.4320 45.68% 2 1.4875 1.0502 5 2.1943 -0.8224 75.14% 3 1.2711 0.8974 5 1.8746 -0.3749 143.05% 4 1.5632 1.1036 5 2.3062 -1.2486 51.23% 5 1.6032 1.1319 5 2.3642 -0.5992 112.38% 6 1.2998 0.9176 5 1.9168 -0.9087 58.91% *7 .1.5419 1.0886 5 2.2745 -0.4183 155.73% 8 1.4886 1.0509 5 2.1952 -0.3322 189.88% 9 1.5705 1.1088 5 2.3172 -0.9444 68.87% 10 1.4454 1.0205 5 2.1317 -1.2991 45.26",{, 11 1.2379 0.8740 5 1.8268 -0.6544 78.68% 12 1.3258 0.9360 5 1.9552 -0.6287 88.04% 13 1.3629 0.9622 5 2.0100 -0.5562 102.71% 14 1.3766 0.9719 5 2.0301 0.1788 332.88% 15 1.1145 0.7869 5 1.6436 -0.2648 178.16% 16 1.5183 1.0720 5 2.2392 -0.9801 64.01% 17 1.6246 1.1470 5 2.3969 -1.0263 65.44% 18 1.4817 1.0461 5 2.1852 -0.5268 118.24% 19 1.4728 1.0398 5 2.1720 -0.4512 137.65% 20 1.4514 1.0247 5 2.1404 -0.9513 63.01% 21 1.1033 o.n9o 5 1.6274 0.2123 225.44% 22 1.4325 1.0114 5 2.1140 -0.5219 115.31% 23 1.0669 0.7532 5 1.5739 39.9496 2.85% E1597416R Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added (ml): 2SIGMA Net Count Net Count Counting Rate Aale Error Uncertainty CPM CPM pCi/G -2.8335 1.2939 1.2817 -1.7513 1.3158 1.2111 *0.9396 1.3441 1.0512 -2.5248 1.2932 1.2534 -1.1924 1.3400 1.3197 -2.2304 1.3138 1.0491 -0.8596 1.3386 1.2768 *0.7119 1.3518 1.2362 -1.8955 1.3053 1.2747 *2.8614 1.2946 1.1521 -1.6606 1.3064 1.0091 -1.5118 1.3310 1.0848 *1.3005 1.3357 1.1196 0.4141 1.3785 1.1665 *0.7578 1.3500 0.9248 *2.0569 1.3165 12295 *1.9933 1.3042 1.3161 -1.1320 1.3385 1.2209 -0.9n2 1.3450 1.2172 -2.0909 1.3173 1.1747 0.6111 1.37n 0.9383 *1.1432 1.3182 1.1794 118.5518 3.1225 2.0623 Page3 NIA NIA NIA N/A 1621-B 1/5/2017 1911.38 0.10 2SIGMA Total Prop. Uncertainty pCi/G 1.2817 1.2111 1.0512 1.2534 1.3197 1.0491 1.2768 1.2362 1.2747 1.1521 1.0091 1.0848 1.1196 1.1667 0.9248 1.2295 1.3161 1.2209 1.2172 1.1747 0.9386 1.1794 5.0317 Sample QC 405235001.1 Sample Nominal Type APO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP

  • 0.0% LCS 40.3269 99.1%

ASSAY 16-Sep-16 12:42:59 Protocol id 12 TC99_REC Time limit 500 Count limit 10000 Isotope Tc-99m Protocol date 23-Sep-13 14:21 :59 Run id. 20 POS RACK BATCH TIME COUNTS CPM ERROR % RECOVERY COUNT TIME 1 34 1 21 11108 31858.7 0.95 12:43:05 2 34 2 23 11158 29242.6 0.95 91.79 12:43:38 3 34 3 23 11087 29087.5 0.95 91.30 12:44:13 4 34 4 23 11085 29116.4 0.95 91.39 12:44:48 5 34 5 23 11183 29407.5 0.95 92.31 12:45:23 6 81 6 24 10998 27751.8 0.95 87.11 12:46:12 7 81 7 23 11397 30051.7 0.94 .94.33 12:46:47 8 81 8 24 10973 27751.6 0.96 87.11 12:47:22 9 81 9 23 10952 28938.8 0.96 90.83 12:47:58 10 81 10 24 11229 28466.1 0.94 89.35 12:48:34 11 66 11 24 11079 28132.3 0.95 88.30 12:49:28 12 66 12 23 11126 29520.9 0.95 92.66 12:50:03 13 66 13 23 11309 30039.5 0.94 94.29 12:50:38 14 66 14 24 11200 28538.3 0.95 89.58 12:51:13 15 66 15 25 10866 26602.8 0.96 83.50 12:51:49 16 99 16 23 11206 29881.8 0.95 93.79 12:52:40 17 99 17 24 11055 28275.8 0.95 88.75 12:53:15 18 99 18 24 10939 28009.9 0.96 87.92 12:53:51 19 99 *19 23 10986 29392.4 0.95 92.26 12:54:27 20 99 20 24 11241 28852.7 0.94 90.56 12:55:02 21 60 21 24 11147 28655.6 0.95 89.95 12:55:51 22 60 22 23 11131 29896 0.95 93.84 12:56:27 23 60 23 23 10995 29563.3 0.95 92.80 12:57:02 24 60 24 23 11436 30790.1 0.94 96.65 12:57:37 END OF ASSAY Batch #1597 416 Page 1 of 1 Page 5645 of 5809 ______________________________ e_ ______ _ PROTOCOL : 15 Tc-9915 min DATE : 2016/09/20 TIME : 12:14 ID : P15AS102 Tc-99 Wallac 1414 WinSpectral v1.40 S/N 4140127 Counting mode : CPM lsotope(s) : H3 H3 = 5-350,12.43 y Protocol name : Tc-99 15 min Counting time : 900 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 1 O Advanced modes : Chemilum Output to Display POS,CPMw2,CLMM,FNCT2,RACK,RACKPOS,FNCT1 ,SQPE,DATE,TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Listing,Header,Spectrum Header : Tc-99 Spectrum : Rnd.Cos,Beta Window 1 70-600 /Beta Window 2 70-600 /Rod.Cos . Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 14.4 CPM Wallac 1400 DSA,_ P15AS102.DAT, 9/20/2016, page 1 Page 5646 of 5809 Rack_position 14 I Rack_position 14 2 20 40 Page 5647of5809 Tc-99 YELLOW Count_Time(min) Quench_number 15.00 666.62 / Counts Chem / Coums Dela Count_Time(min) Quench_number 15.00 676.07 / Counts Chem / Counts Dela 80 100 Tc-99_Cpm 14.06 Run_Date 9/20/2016 12:1.5 PM Gross_B_CPM 16.30 *Lumex_CPM 2.20 LUMEX 0.00 Tc-99_Cpm 13.29 Run_Date 9/20/2016 12:31 PM Gross_B_CPM LUMEX 13.60 0.00 Lumex_CPM 0.30 Wallac 1400 DSA. Pl5AS102.DAT, 9/20/2016, page 2 Tc-99 YELLOW PROTOCOL DATE : 15 Tc-9915 min : 2016/09/20 TIME : 04:23 ID : P15AS101 Tc-99 Wallac 1414 WinSpectral v1.40 S/N 4140127 Counting mode : CPM lsotope(s) : H3 H3 = 5-350, 12.43 y Protocol name : Tc-9915 min Counting time : 900 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 1 O Advanced modes : Chemilum Output to Display POS,CPMw2,CLMM,FNCT2,RACK,RACKPOS,FNCT1 ,SQPE,DATE,TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display* : Listing,Header,Spectrum Header : Tc-99 Spectrum : Rnd.Cos,Beta Window 1 70-600 /Beta Window 2 70* 600 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total count rate: H3 233.2CPM Wallac 1400 DSA, PlSASIOl.DAT, 9/20/2016, page I Page 5648 of 5809 Tc-99 YELLOW \ ***--*--*-----.. ---............ _______ .... ____ .......................... ___ ---**----*------......... _ ................................................... ____ ,. _______ ............... _______ . ______ .. __ .................................... _. ___ *-----------.. ------------Cf/ 9'1 I Rack_position Count_Time(min) Quench_number Tc-99_Cpm Run_Date ./J 14 1 15.00 694.32 14.21 9/20/20 : 4 AM 5-,--=-*----t--1 / Counls De ta 20 40 60 80 100 Rack_position Count_Time(min) Quench_number \ 14 2 15.00 655.55 /" Counts 01em / Counts De ta Rack_position Counl_Time(min) Quench_number (/' 14 3 15.00 689.13 6 5 _J._ / Counts ' 4-I ----01em 3 2 / Counts Delu Lumex_CPM 3.70 LUMEX 0.00 Tc-99_Cpm* 11.14 Run_Date 9/20/2016 4:40 AM Gross_B_CPM 11.60 Lumex_CPM 0.50 LUMEX 0.00 Tc-99_Cpm 12.11 Run_Date 9/20/2016 4:56 AM Gross_B_CPM LUMEX 12.30 0.00 Lumex_CPM 0.20 Wallac 1400 DSA, Pl5AS101.DAT, 9/20/2016, page 2 Page 5649of5809 Tc-99 YELLOW Rack_position Count_Time(min) Quench_number 14 4 15.00 679..49 ---*1 . :I *--, l-,1---/ Counts 01cm / Counts Bela 20 40 60 80 100 Rack_position Count_ Time(min) Quench_number 14 5 15.00 644.25 2.5---""--!*--'---* -----/ Counts Chem / Counts Bcti1 Rack_position Count_Time(min) Quench_number s 14 6 15.00 672.78 .. -/ Counts 01cm / Counts Bcln .l ** ***. Tc-99_Cpm 13.08 Run_Date 9/20/2016 5:12 AM Gross_B_CPM 13.80 Lumex_CPM 0.80 LUMEX 0.00 Tc-99_Cpm 11.28 Run_Date 9/20/2016 5:28 AM Gross_B_CPM 11.60 0.30 LUMEX 0.00 Tc-99_Cpm 12.87 Run_Date 9/20/2016 5:44 AM Gross_B_CPM LUMEX 13.40 0.00 Lumex_CPM 0.50 -*---*-----------------**---*---**----***---***-**-.. -------*-----------------*-**-*-*-**-Wa'Ilac 1400 DSA, Pl5AS101.DAT, 9/20/2016, page 3 Page 5650 of 5809 Tc-99 YELLOW Rack_position Count_Time(min) Quench_number 14 7 15.00 666.74 / Counts Chem / Counts Beta Rack_position Count_ Time(min) Quench_number 14 8 15.00 648.12 / Counts Chem / Counts Beta Rack_position Count_Time(min) Quench_number 14 9 15.00 667.26 / Counts 01cm / Counts Beta Tc-99_Cpm 11.83 Run_Date 9/20/2016 6:01 AM Gross_B_CPM 12.00 Lumex_CPM 0.20 LUMEX 0.00 Tc-99_Cpm 13.01 Run_Date 9/20/2016 6:17 AM Gross_B_CPM 13.70 Lumex_CPM 0.70 LUMEX 0.00 Tc-99_Cpm 13.35 Run_Date 9/20/2016 6:33 AM Gross_B_CPM 14.30 Lumex_CPM 0.90 LUMEX 0.00 ------------*----------*---*-*-*--*----*--**-**------**---------*-------*--*--*----*-**-Wallac 1400 DSA, Pl5AS101.DAT, 9/20/2016, page 4 Page 5651 of 5809 Tc-99 YELLOW Courit_Time(min) Quench_number 15.00 639.90 / Counts 2. 01cm / Counts Dela 20 40 60 100 Rack_position Count_Time(min) Quench_number 14 11 15.00 658.09 10 3.0 2.5 j / Counts 2. Otcrn 1.5 I I.(}-/ Counts Beta 0.5 0.0 0 20 40 Rack_position Count._Time(min) Quench_number 14 12 15.00 635.02 / Counts Chem / Counts Bcln l.1* Tc-99_Cpm l l.8J Run_Date 9/20/2016 6:49 AM Gross_B_CPM LUMEX 12.20 0.00 Lumex_CPM 0.40 Tc-99_Cpm 11.14 Run_Date 9/20/2016 7:05 AM Gross_B_CPM LUMEX 11.60 0.00 Lumex_CPM 0.50 Tc-99_Cpm 11.97 Run_Date 9/20/2016 7:21 AM Gross_B_CPM 12.80 Lumex_CPM 0.80 LUMEX 0.00 Wallac 1400 DSA, Pl5AS101.DAT, 9/20/2016, page 5 Page 5652 of 5809 Tc-99 YELLOW Rack_position Count_Time(min) Quench_number 0 1 15.00 662.93 / Counls 01em / Counls Beta 20 40 60 80 100 Rack_position Count_Time(min) Quench_number 0 2 15.00 661.34 / Counts Chem / Counts Beta Rack_position Count_ Time(min) Quench_number \ l\ 0 3 . 15.00 663.58 _\ / Counts Chem / Counts Beta Tc-99_Cpm 12.53 Run_Date 9/20/2016 7:38 AM Gross_B_CPM 12.90 Lumex_CPM 0.40 LUMEX 0.00 Tc-99_Cpm 12.73 Run_Date 9/20/2016 7:54 AM Gross_B_CPM 13.30 Lumex_CPM 0.60 LUMEX 0.00 Tc-99_Cpm 14.46 Run_Date 9/20/2016 8: 10 AM Gross_B_CPM LUMEX 15.30 0.00 Lumex_CPM 0.80 W<11lac 1400 DSA. Pl5AS101.DAT, 9/20/2016, page 6 Page 5653 of 5809 . Tc-99 YELLOW \\)flAQt\\l{) ---*--*-------*--***--***--*-----*--**------*--------------*--**-----*---**----**----Rack_position Courit_Time(min) Quench_number Tc-99_Cpm l s 0 4 ' 15.00 *>98.61 11.49 2.0* 1.5--/ Counts Bela 100 Rack_position Count_Time(min) Quench_number 0 5 . 15.00 678.75 / Counts 01cm / Counts Bein Rack_position Count_ Time(min) Quench_number 0 6 15.00 641.39 4-----11-.1---3--rLL . / Counts Chem 2 I I-/ Counts Beta 20 40 80 100 Lumex_CPM 0.70 LUMEX 0.00 Tc-99_Cpm* 11.97 Run_Date 9/20/2016 8:42 AM Gross_B_CPM LUMEX 13.30 0.00 Lumex_CPM 1.30 Tc-99_Cpm 11.76 Run_Date 9/20/2016 8:58 AM Gross_B_CPM LUMEX 12.40 0.00 Lumex_CPM 0.60 Wallac 1400 DSA, Pl5AS101.DAT, 9/20/2016, page 7 Page 5654 of 5809 Tc-99 YELLOW Rack_position Courit_Time(min) Quench_number 0 7 15.00 658.15 / Counls Chem / Counts Bet11 Count_Time(min) Quench:_number 15.00 674.28 1 q 8 3,0*.,.----,---rn.,----,---T----, 2.5* --20 Rack_position 0 9 3.0-...---,-,-40 rnrrn lllllWI UIUJJ 60 80 100 / Counts Chem / Counls Bela Count_Time(min) Qnench_number " 15.00 666.91 / Counts 01em / Counls Bela * .. Tc-99_Cpm 12.87 Run_Date 9/20/Wl6 9:14 AM Gross_B_CPM 13.60 Lumex_CPM 0.80 LUMEX 0.00 Tc-99_Cpm 13.08 Run_Date 9120/2016 9:31 AM Gross_B_CPM 13.60 Lumex_CPM 0.60 LUMEX 0.00 Tc-99_Cpm 11.97 Run_Date 9/20/2016 9:47 AM Gross_B_CPM 12.50 Lumex_CPM 0.50 LUMEX 0.00 Wa.llac 1400 DSA: P15AS101.DAT, 9/20/2016, page 8 Page 5655 of 5809 Tc-99 YELLOW Rack_position Courit_Time(min) Quench_number 0 10 15.00 685.86 --:r----] --r Tll-/ Counls 01em 'I I / Counts IJcla 20 40 Ii() 80 100 Rack_position 0 11 Count_Time(min) Quench_number 15.00 633.65 / Counts Chem / Counts IJcla Rack_position Count_Tinie(min) Quench_number 0 12 15.00 689.69 ,1 .'I 15--1--1---1--'---J..--I / Counts Chem I --,l------+-----1 _Ll.li / Counts IJcla 20 GO 80 100 Tc-99_Cpm 14.54 Run_Date 9/20/20i 6 10:03 AM Gross_B_CPM LUMEX 15.20 0.00 Lumex_CPM 0.70 Tc-99_Cpm 12.46 Run_Date 9/20/2016 10:19 AM Gross_B_CPM 13.00 Lumex_CPM 0.60 LUMEX 0.00 Tc-99_Cpm 132.40 Run_Date 9/20/2016 10:35 AM Gross_B_CPM LUMEX 133.00 0.00 Lumex_CPM 0.60 Wallac 1400 DSA, Pl5AS101.DAT, 9/20/2016, page 9 Page 5656 of 5809 Effective 3/25/2010 Revision 1 Effective March 2010 Radiochemistry Batch Checklist GL-CHL-RAD-013 Rev 1 Page 1of1 23-Sep-2016 5.i.._:...g_Q--"'-7(_* Product:. __ U __ l(_,_ ___ _ Criteria: Yes No Comments Samo le Solids are less than or eaual to 100 ma for GAB. J'Jr Samples have been blank corrected (If required). ti! f( Blank correction renorted included lif reouired). [f activity less than 10x MDA/MDC, error is less I than or equal to 150% of sample activity. [f 11reater than 10* MDA/ MDC, error ls 400/o or less. [f hnJ-*** *'--MDA/ Mhr ls ... !Instrument source check' Is within limits. j bkn nh0ck Is within limits. Method RDL/ LLD has been met. v [f duollcate activities are: / Less than S* MDA/ MDC, then RPO Is :l.000/o or less, If greater S* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO ls 0%, Or meets the client's reoulred RER accentance criteria. Tracer yield is 15-125%

  • Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. / ifTf .. -" nf Adlultv' /' samnle was run within hold time. v ""<P 0 v<.r< l.<\ &i o rN _p Samnle was correctlv nreserved if reoulred. i/ Smears Taken for Radioactive batches. fl/ RI I / Method Spike and LCS are within 75-125% ltor mnets *'--clJ--**s rontrart "CCentanr" rriterla' ' t/' No blank spaces on data forms. All line outs Initialed and dated. 1 .. n Aux data Is correct. / Client Snecial renulrements naoe has been checked. Raw Data and J or snectrum are Included and nronerlu statused. 1/ MS, LCS, and Duplicate RPD/RER values uploaded to UMS and i/ ...... __ **--"'--' .... .. (if NP! n-*-'---*---' *-*-r---N********-./ -Batch Data Excentlon Reoorts CDER) comoleted if aoolicable, v '() ')!!( I S<t O '() () Batch Data Exception Reports (DER) second reviewed. / ri1d 1Sl1t>?A lo Dlsnosltlon verified to be comnleted. Allnuot rorr--*Jon rnmntntn" if r1mulred. N Jr' Review sample historical results If available v/*' (If REMP, results above MDC have been verified bu historical results recount or re-analvsls.' -. -_,__...-;; ... --Primary Review Performed.By: Secondary Review Page 5657 of 5809 GEL Laboratories LLC Form GEL-DER . DATA EXCEPTION REPORT Mo.Day Yr. Division: Quality Criteria: 23-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC EPA EERF C-01 Modified Solid Batch ID: Sample Numbers: 1598078 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235001, 405235002, 405235003, 405235004, 1. Reporting results. 405235005,405235006,405235007,405235008,405235009, 405235010,405235011,405235012,405235013,405235014, 405235015,405235016,405235017,405235018,405235019, 405235020, 1203626106, and 1203626107 were received and analyzed out of the method specified hold time. Originator's Name: Data Validator/Group Leader: Elizabeth Krouse 23-SEP-16 Lyndsey Pace 23-SEP-16 Page 1 Page 5658 of 5809 DER Report No.: 1560896 Revision No.: 2 Type: Process Client Code: MJWC Prep Logbook The Determination of Carbon-14 in Water, Soil, Vegetation and Other Solid Matrices Batch ID: 1598078 Analyst: Angela Johnson Method: EPA EERF C-0 l Modified Lab SOP: GL-RAD-A-003 REV# 15 Instrument: BAL-18550299 Sample ID Prep Date Matrix 405235001 14-SEP-2016 11:11:07 Soil 405235002 14-SEP-2016 11:11:07 Soil 405235003 14-SEP-2016 11:11:07 Soil 405235004 14-SEP-2016 11:11:07 Soil 405235005 14-SEP-2016 11 :11 :07 Soil 405235006 14-SEP-2016 11:11:07 Soil 405235007 14-SEP-2016 11:11:07 Soil 405235008 14-SEP-201611:11:07 Soil 405235009 14-SEP-201611:11:07 Soil 405235010 14-SEP-201611:11:07 Soil 405235011 14-SEP-201611:11:07 Soil 405235012 14-SEP-2016 11:11:07 Soil 405235013 14-SEP-2016 11:11:07 Soil 405235014 14-SEP-2016 11:11:07 Soil 405235015 14-SEP-2016 11:11:07 Soil 405235016 14-SEP-2016 11:11:07 Soil 405235017 14-SEP-2016 11:11:07 Soil 405235018 14-SEP-2016 11:11:07 Soil 405235019 14-SEP-2016 11:11:07 Soil 405235020 14-SEP-2016 11:11:07 Soil 1203626105 MB 14-SEP-2016 11:11:07 Soil 1203626106 DUP (405235001) 14-SEP-2016 11:11:07 Soil 1203626107 MS ( 40523500 I) 14-SEP-2016 11: II :07 Soil 1203626108 LCS 14-SEP-2016 11:11:07 Soil Reagent/Solvent Lot ID Description Amount 2242305.2 Ecoscinl A Scintillatlon Solution !OmL 2398913.5 Methanol 4L Plastic Bottle 9mL 2440076.3 PotlSSium Persulfate 99+% Sg 2440953 RL..Q.4M Hydrochloric Acid SOmL 2454859.17 16M Nitric Acid Poly Coaled Bottle 25mL 2455949 RL-IM Silver Nitrate 2mL Analytical Logbook version 111-04-2002 Type Sample Id pescriplion LCS 1203626108 Carbon-14 SPIKE MS 1203626107 Carbon-14 SPIKE Dry or Wet Unadjusted Aliquot Flask# w w w w w w w w w w w w w w w w w w w w w w w w Aliquot (g) (g) 1.774 1.429 1.864 1.447 1.692 1.398 1.631 1.315 1.888 1.503 1.617 1.302 1.631 1.284 1.579 1.252 1.528 1.167 1.643 1.313 1.599 1.338 1.699 1.411 1.862 1.46 1.663 1.411 1.634 1.517 1.567 1.247 1.594 1.235 1.814 1.421 1.698 1.4 1.625 1.393 1.517 1.858 1.497 1.681 1.355 1.517 Comments: Spike Pipet lD: RAD-LSC-2970968 2 3 4 5 6 8 83 84 86 400 402 404 405 406 506 507 514 519 530 706 708 729 733 Data Entry Date2: 21-SEP-2016 12:23 BAL-18550299 Angela Johnson Serial Number Spike Amount Spike Units 1646-B .1 mL 1646-B .I mL GEL Laboratories LLC Filename C14.XLS File type Excel Version # 1.3.10 Batch : 1598078 Analyst : ANGELA095 Prep Date : 9/14/2016 Method Uncertainty : 0.0363 Geometry: 3ml Ethanolamine/9ml Methanol/10ml EcoScint A Sample Characteristics Sample Sample Aliquot Sample Aliquot St Dev. Sample Pos. ID G G Date/Time 1 405235001.1 1.4290 3.3679E-03 1211012015 14:20 2 4052350Q2. 1 1.4470 3.3698E-03 1211012015 14:30 3 405235003.1 1.3980 3.3647E-03 12110/2015 14:35 4 405235004.1 1.3150 3.3561E-03 1219/2015 14:00 5 405235005. 1 1.5030 3.3756E-03 12110/2015 13:15 6 405235006.1 1.3020 3.3547E-03 12110/2015 13:25 7 405235007 .1 1.2840 3.3529E-03 12110/2015 13:55 8 405235008.1 1.2520 3.3495E-03 12110/2015 14:05 9 405235009. 1 1.1670 3.3407E-03 12110/2015 10:30 10 405235010.1 1.3130 3.3559E-03 12110/2015 10:35 11 405235011.1 1.3380 3.3585E-03 1219/2015 10:13 12 405235012.1 1.4110 3.3661E-03 12110/201511:25 13 405235013.1 1.4600 3.3712E-03 121812015 11:23 14 405235014.1 1.4110 3.3661E-03 1218/2015 10:49 15 405235015.1 1.5170 3.3n1E-03 1218/201510:56 16 405235016.1 1.2470 3.3490E-03 1218/2015 11 :29 17 405235017.1 1.2350 3.3478E-03 121212015 10:02 18 405235018.1 1.4210 3.3671E-03 12121201510:19 19 405235019.1 1.4000 3.3649E-03 1218/2015 14:30 20 405235020.1 1.3930 3.3642E-03 1218/2015 13:50 21 1203626105.1 1.5170 3.3n1E-03 9/14/2016 0:00 22 1203626106.1 1.4970 3.3750E-03 12110/2015 14:20 23 1203626107 .1 1.3550 3.3603E-03 12110/201514:20 24 1203626108. 1 1.5170 3.3n1E-03 9/14/2016 0:00 Count raw Data Rack Position# 82-2 82-3 82-4 87-1 87-2 87-3 87-4 87-5 87-6 87-7 87-8 87-9 87-10 87-11 87-12 0-1 0-2 0-3 0-4 0-5 0-6 0-7 59-1 59-2 C1598078 Carbon-14 Solid Procedure Code : LSC_14CS Parmname: Carbon-14 Required MDA 2* pCi/G C-14 Abundance 1.00 Halfllfe of Carbon-14 5700.00 years Bkg Counting Count Corrected Count C-14 Time Quench# Gross Bkg Time Bkg Bkg Start Normalization Sample (min.) cpm cpm (min.) Quench# cpm Date/Time Factor Decay 45 628.36 10.87 11.58 45 625.79 11.5682 9/2212016 0:38 1.00000 1.000 45 629.07 11.51 11.58 45 625.79 11.5629 9/2212016 1 :25 1.00000 1.000 45 628.12 10.91 11.58 45 625.79 11.5697 9/2212016 2:11 .1.00000 1.000 45 634.48 12 11.58 45 625.79 11.4934 9/2212016 4:10 1.00000 1.000 45 628.12 11.14 11.58 45 625.79 11.5697 9/2212016 4:56 1.00000 1.000 45 629.79 11.74 11.58 45 625.79 11.5567 9/22/2016 5:42 1.00000 1.000 45.0166664 630.86 11.14 11.58 45 625.79 11.5458 912212016 6:29 1.00000 1.000 45.0166664 629.25 11.72 11.58 45 625.79 11.5614 9/2212016 7:15 1.00000 1.000 45 635.2 12.76 11.58 45 625.79 11.4801 9122/2016 8:01 1.00000 1.000 45 629.9 12.02 11.58 45 625.79 11.5557 9/22/2016 8:47 1.00000 1.000 45 629.73 11.37 11.58 45 625.79 11.5572 9/2212016 9:34 1.00000 1.000 45 631.69 12.23 11.58 45 625.79 11.5359 9/2212016 10:20 1.00000 1.000 45 631.63 11.4 11.58 45 625.79 11.5366 9/2212016 11:06 1.00000 1.000 45 631.27 11.4 11.58 45 625.79 11.5410 9/2212016 11 :52 1.00000 1.000 45 629.13 12.32 11.58 45 625.79 11.5624 9/2212016 12:39 1.00000 1.000 45 634.48 12.18 11.58 45 625.79 11.4934 9/2212016 13:25 1.00000 1.000 45 629.79 11.24 11.58 45 625.79 11.5567 91221201614:11 1.00000 1.000 45 631.27 11.72 11.58 45 625.79 11.5410 912212016 14:58 1.00000 1.000 45 629.9 12.11 11.58 45 625.79 11.5557 9/2212016 15:44 1.00000 1.000 45 630.02 10.78 11.58 45 625.79 11.5545 9/22/2016 16:30 1.00000 1.000 45 633.77 10.98 11.58 45 625.79 11.5056 9/2212016 17:16 1.00000 1.000 45 633.53 10.94 11.58 45 625.79 11.5095 9/2212016 18:03 1.00000 1.000 15 632.76 128.5 11.58 45 625.79 11.5213 9/2212016 18:50 1.00000 1.000 15 627.94 121.92 11.58 45 625.79 11.5709 9/2212016 19:06 1.00000 1.000 Page 1 0 >-+i Vl 00 0 \0 C1598078 Plpet, 0.1 ml Stdev: +/-0.000200 ml Plpet, 0.5 ml Stdev : +/-0.001000 ml Analytical SOP: GL-RAD*A-003 Instrument SOP: GL-RAD+014 Calibration Data Calibration Counted Calibration Due Pas. on Dale Date 1 LSCYELLOW 6/1/2016 5/31/2017 2 LSCYELLOW 6/1/2016 5/31/2017 3 LSCYELLOW 6/1/2016 5131/2017 4 LSCYELLOW 6/1/2016 5131/2017 5 LSCYELLOW 6/1/2016 5/31/2017 6 LSCYELLOW 6/1/2016 5/31/2017 7 LSCYELLOW 611/2016 5/31/2017 8 LSCYELLOW 6/1/2016 5/31/2017 9 LSCYELLOW 6/1/2016 5/31/2017 10 LSCYELLOW 611/2016 5/31/2017 11 LSCYELLOW 611/2016 5/31/2017 12 LSCYELLOW 6/1/2016 5/31/2017 13 LSCYELLOW 6/1/2016 5/31/2017 14 LSCYELLOW 6/1/2016 5/31/2017 15 LSCYELLOW 6/1/2016 5/31/2017 16 LSCYELLOW 6/1/2016 5/31/2017 17 LSCYELLOW 6/1/2016 5/31/2017 18 LSCYELLOW 6/1/2016 5/31/2017 19 LSCYELLOW 6/1/2016 5/31/2017 20 LSCYELLOW 6/1/2016 5/31/2017 21 LSCYELLOW 6/112016 5/31/2017 22 LSCYELLOW 6/1/2016 5/31/2017 23 LSCYELLOW 6/1/2016 5/31/2017 24 LSCYELLOW 6/1/2016 5/31/2017 Detector Detector Efficiency Efficiency Error (cpm/dpm) (cpm/dpm) 0.6866 0.00792 0.6872 0.00792 0.6863 0.00792 0.6918 0.00792 0.6863 0.00792 0.6879 0.00792 0.6889 0.00792 0.6874 0.00792 0.6924 0.00792 0.6880 0.00792 0.6879 0.00792 0.6896 0.00792 0.6895 0.00792 0.6892 0.00792 0.6873 0.00792 0.6918 0.00792 0.6879 0.00792 0.6892 0.00792 0.6880 0.00792 0.6881 0.00792 0.6913 0.00792 0.6911 0.00792 0.6905 0.00792 0.6861 0.00792 Page2 Background Background Count Rack Start Position# Datefl1me 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/2112016 23:52 82*1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82*1 9/21 /2016 23:52 82-1 9/21/2016 23:52 82-1 9/2112016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 82-1 9/21/2016 23:52 Notes: * -Results are decay corrected to Sample Date/Time * -Reference date for Spike Activity (dpm/ml] is the batch Prep Date * -Spike Nominals are decay corrected to Sample Dateffime * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 0.7671 0.5416 2 1.1138 -0.3206 101.15% 2 0.7567 0.5342 2 1.0986 -0.0240 1353.38% 3 0.7845 0.5538 2 1.1390 -0.3098 107.14% 4 0.8246 0.5822 2 1.1974 0.2509 142.63% 5 0.7297 0.5152 2 1.0594 -0.1877 165.31% 6 0.8399 0.5930 2 1.2195 0.0922 392.52% 7 0.8500 0.6001 2 1.2341 -0.2067 174.97% 8 0.8742 0.6172 2 1.2692 0.0830 453.59% 9 0.9280 0.6551 2 1.3475 0.7136 57.35% 10 0.8327 0.5879 2 1.2090 0.2316 155.88% 11 0.8174 0.5771 2 1.1868 -0.0917 381.20% 12 0.7724 0.5453 2 1.1215 0.3214 104.70% 13 0.7466 0.5271 2 1.0840 -0.0611 522.47% 14 0.7730 0.5457 2 1.1224 -0.0653 506.23% 15 0.7217 0.5095 2 1.0478 0.3273 96.17% 16 0.8696 0.6139 2 1.2627 0.3585 105.64% 17 0.8855 0.6251 2 1.2856 -0.1679 224.75% 18 0.7676 0.5419 2 1.1145 0.0823 401.76% 19 0.7810 0.5514 2 1.1339 0.2593 130.82% 20 0.7847 0.5540 2 1.1394 -0.3640 90.96% 21 0.7157 0.5053 2 1.0392 -0.2258 134.49% 22 0.7256 0.5123 2 1.0536 *0.2480 124.03% 23 1.1353 0.8016 2 1.6994 56.3249 2.67% 24 1.0226 0.7220 2 1.5305 47.7547 2.75% C1598078 Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCi/G -0.6982 0.7061 0.6355 -0.0529 0.7161 0.6358 -0.6597 0.7068 0.6504 0.5066 0.7225 0.7013 -0.4297 0.7104 0.6081 0.1833 0.7195 0.7093 *0.4058 0.7100 0.7087 0.1586 0.7192 0.7379 1.2799 0.7339 0.8021 0.4643 0.7238 0.7075 -0.1872 0.7138 0.6848 0.6941 0.7267 0.6595 -0.1366 0.7139 0.6262 -0.1410 0.7140 0.6483 0.7576 0.7285 0.6169 0.6866 0.7253 0.7423 -0.3167 0.7118 0.7397 0.1790 0.7190 0.6482 0-5543 0.7252 0.6648 -0.7745 0.7045 0.6489 -0.5256 0.7069 0.5951 -0.5695 0.7063 0.6028 116.9787 2.9703 2.8032 110.3491 2.8957 2.4562 Page3 1646-B 1/5/2017 1681.40 0.10 1646-B 1/5/2017 1681.40 0.10 2SIGMA Total Prop. Uncertainty pCi/G 0.6355 0.6358 0.6504 0.7015 0.6081 0.7093 0.7087 0.7379 0.8038 0.7077 0.6848 0.6599 0.6262 0.6483 0.6174 0.7428 0.7397 0.6482 0.6650 0.6489 0.5951 0.6028 4.9756 4.2626 Sample QC 405235001.1 405235001.1 Sample* Nominal Type RPO RER pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP
  • 0.0% . MS 55.9010 100.8% LCS 49.9267 95.6%

f b _!_!_ ______ . __ _ PROTOCOL . : 4 C-14 45 min DATE : 2016/09/21 TIME : 23:51 ID :P04AS407 C-14 Wallac 1414 WinSpectral v1.40 S/N 4140127 Counting mode : DPM Quench index : SQP(E) _ lsotope(s) : C14 C14 = ,5730.00 y Protocol name * : C-14 45 min Counting time : 2700 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 1 O Sp. library of isotope C14 : Wallac Vial type : Diffuse Liquid system : HiSafe Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTlME Additions to Display : Listing,Header,Spectrum Header : C-14 Spectrum : Rnd.Cos,Beta *

  • Window 1 35-300 /Beta Window 2 35-300 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5
  • 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTlME/60 *FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total activity: C14 50.8 DPM 0.001 kBq Wallac 1400 DSA, P04AS407.DAT, 9/22/2016, page 1 Page 5663 of 5809 C-14 YELLOW Rack_position Count_Time(min) Quench_number 82 1 45.00 625.79' / Counts Chem / Counts lletu Rack_position Count_ Time(min) Quench_number 82 2 45.00 628.36 8-..-----,---,----.--,..----, -6 / Counts I 01em \ I 4 -----/ Couuts llctu Rack_position Count_ Time(min) Quench_number 82 3 45.00 629.07 1()-----,,i----::f---i---lt--+------_.t----/ Counts Chem / Couuts llctu 20 40 60 100 Cl4_CPM 11.58 Run_Date 9/21/2016 11:52 PM Gross_B_CPM 11.70 Lumex_CPM 0.10 LUMEX 0.00 DPM 13.30 CJ4_CPM 10.87 Run_Date 9/22/2016 0:38 AM Gross_B_CPM LUMEX 11.30 0.00 Lumex_CPM DPM 0.40 11.10 Cl4_CPM 11.51 Run_Date 9/22/2016 1:25 AM Gross_B_ CPM 11.90 Lumex_CPM 0.30 LUMEX 0.00 DPM 13.30 Wallac 1400 DSA, P04AS407.DAT, 9/22/2016, page 2 Page 5664 of 5809 C-14 YELLOW Rack_position Count_ Time(min) Quench_number 82 4 *, 45.00 628.12 .1 / Counts rs ,. ' !:: Chern I 4* / Counts 2 --Bela 0 JlllUU 0 20 40 60 80 100 == .. Cl4_CI>M 10.91 Run_Date 9/2212016 11 AM Gross_B_CPM LUMEX 11.40 0.00 Lumex_CPM DPM 0.50 13.10 Wallac 1400 DSA. P04AS407.DAT, 9/22/2016, page 3 Page 5665 of 5809

--*--.. ---------------------------------------------*-----*-____________________ L.if g o_J__f ___ .. ___ _ PROTOCOL : 4 C-14 45 min DATE : 2016/09/22 TIME , : 04:09 ID : P04AS408 C-14 Wallac 1414 WinSpectral vi .40 S/N 4140127 Counting mode : DPM Quench index : SQP(E) lsotope(s) : C14 C14 = ,5730.00 y Protocol name : C-14 45 min Counting time : 2700 Repeats : 1 *Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 1 O Sp. library of isotope C14 : Wallac Vial type : Diffuse Liquid system : HiSafe Advanced modes : Chemllum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Listing,Header,Spectrum Header : C-14 Spectrum : Rnd.Cos,Beta Window 1 35-300 /Beta Window 2 35-300 /And.Cos Window 3 *: 1-1024 /Beta Window 4 : 1-1024 /Beta Window 5 : ' 1-1024 /Beta Window 6 : 1-1024/Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total activity: C14 249.5 DPM 0.004 kBq Wallac 1400 DSA_:. P04AS408.DAT, 9/2212016, page l Page 5666 of 5809 C-14 YELLOW Rack_position Counl_Time(min) Quench_number .87 1 45.00 634.48 6--*----------/ Counts Chern / Counts Bela 100 Rack_position Count_Time(min) Quench_number 87 2 45.00 628.12 / Counts Chem 4 2 / Counts Belli Rack_position Count_ Time(min) Quench_number 87 3 45.00 629.79 / Counts Chern / Counts llct:i Cl4_CPM -12.00 Run_Date 9/22/2016 4: 10 AM Gross_B_CPM 12.50 Lumex_CPM 0.50 LUMEX 0.00 DPM 13.40 Cl4_CPM 11.14 Run_Date 9/22/2016 4:56 AM Gross_B_CPM LUMEX 1 l.60 0.00 Lumex_CPM DPM 0.40 12.60 Cl4_CPM 11.74 Run_ Date 9/22/2016 5:42 AM Gross_B_CPM LUMEX 12.20 0.00 Lumex_CPM DPM 0.50 13.20 Wallac 1400 DSA,.P04AS408.DAT, 9/22/2016, page 2 Page 5667 of 5809 Rack_position 87 4 1 Rack_position 87 5 II 8--Rack_position 87 6 811 Page 5668 of 5809 C-14 YELLOW Count_Time(min) Quench_number Cl4_CPM 45.02 630.86 1 l.14 Run_Date 9/22/2016 6:29 AM ,/ Counls 01cm / Counls Beta Gross_B_CPM 11.50 Lumex_CPM 0.30 LUMEX 0.00 DPM 12.80 Count_Time(min) Quench_number Cl4_CPM 45.02 629.25 11.72 Run_Date

  • 9/22/2016 7: 15 AM / Counts 01cm / Counls Hein Gross_B_CPM 12.00 Lumex_CPM 0.30 LUMEX 0.00 DPM 13.10 Count_Time(min) Quench_number Cl4_CPM 45.00 635.20 12.76 Run_Date 9/22/2016 8:01 AM Gross_B_CPM LUMEX /' Counts 13.10 0.00 01cm Lumex_CPM DPM 0.30 14.40 / Counls Bct*t Wallac 1400 DSA, P04AS408.DAT, 9/22/2016, page 3 C-14 YELLOW ' .. Rack_position Count_Time(min) Quench_number 87 7 45.00 629.90 8--------/ Counls (o Chem 6 4 / Counls 2 Bela Rack_position Count_Time(min) Quench_number 87 8 45.00 629.73 / Counls t ( 4-Otcm 3 2 / Courlls Bew (;c., 20 40 80 JOO Rack_position Count_Time(min) Quench_number 87 9 45.00 631.69 JO 1--8--i! --* --/ Counls Chem --4 / Counls 2 Beta 00 20 40 ° 80 100 C14_CPM 12.02 Run_ Date 9/22/2016 8:47 AM Gross_B_CPM LUMEX 12.40 0.00 Lumex_CPM DPM 0.40 13.70 Cl4_CPM 11.37 Run_Date 9/22/2016 9:34 AM Gross_B_CPM LUMEX 11.80 0.00 Lumex_CPM DPM 0.40 13.80 Cl4_CPM 12.23 Run_Date 9/22/2016 10:20 AM Gross_B_CPM LUMEX 12.80 0.00 Lumex_CPM DPM 0.60 13.80 Wallac 1400 DSA, P04AS408.DAT, 9/22/2016, page 4 Page 5669 of 5809 t1 C-14 YELLOW Rack_position Count_Time(min) Quench_number 87 10 . 45.00
  • 631.63 6 ----.--/ Counts Chem 2 / Coun1s Detn 0 0 20 40 60 80 (( Rack_position Count_ Time(min) Quench_number 87 11 45.00 631.27 / Counts Chem / Counls Beta Rack_position Count_Time(min) Quench_number 87 12 45.00 629.13 15-.. 20 I ! ; i ---1----f--j 40 ., I -r--ill WlWru 60 80 100 / Counls Chem / Coun1s l3e1u Cl4_CPM 11.40 Run_Date 9/22/2016 11 :06 AM Gross_B_CPM LUMEX 11.70 0.00 Lumex_CPM DPM 0.30 13.60 Cl4_CPM 11.40 Run_Date 9/22/2016 11:52 AM Gross_B_CPM 11.90 Lumex_CPM 0.50 LUMEX 0.00 DPM 13.20 Cl4_CPM 12.32 Run_Date 9/22/2016 12:39 PM Gross_B_CPM LUMEX 12.60 0.00 Lumex_CPM DPM 0.30 14.00 Wallac 1400 DSA, P04AS408.DAT, 9/22/2016, page 5 Page 5670 of 5809 C-14 YELLOW Rack_position Count_ Time(min) Quench_number 0 10 45.00 634.48 JO -----T .-+--8 / Counts _:J __ Chem 6* 1' 4 / Counts 2-Bein 0 0 20 40 60 80 100 Rack_position Count_Time(min) Quench_number 0 2 45.00 629.79 / Counts 01cm / Counts Bern Rack_position Count_Time(min) Quench_number 0 3 45.00 631.27 :\. ---/ Counls Chem / Counts lllUUmJ Beta _ 20 40 60 80 JOO Cl4_CPM 12.18 Run_Date 9/22/2016 1:25 PM Gross_B_CPM LUMEX 12.70 0.00 Lumex_CPM DPM 0.60 12.80 CI4_CPM 11.24 Run_Date 9/22/2016 2:11 PM Gross_B_CPM 11.70 Lumex_CPM 0.50 LUMEX 0.00 DPM 12.60 Cl4_CPM 11.72 Run_Date 9/22/2016 2:58 PM Gross_B_CPM LUMEX 12.20 0.00 Lurnex_ CPM DPM 0.50 12.30 Wallac 1400 DSA, P04AS408.DAT, 9/22/2016, page 6 Page 5671 of 5809

!\fa (\)\ Rack_position 0 4 8 20 Rack_posilion 0 5 6 4* 20 dO Rack_position 0 6 C-14 YELLOW Count_Time(min) Quench_number Cl4_CPM Run_Date 9/22i<<2016 3:44 PM 45.00 629.90 12.11 60 100 / Counls . / Counls Bein Count_Time(min) Quench_number 45.00 630.02 -/ Counls Chem I / Counls --Beta 'W' llLil llUUI tiil 80 100 Gross_B_CPM 12.60 Lumex_CPM 0.50 LUMEX 0.00 DPM 14.50 Cl4_CPM 10.78 *Run_Date 9/22/2016 4:30 PM Gross_B_CPM LUMEX 11.30 0.00 Lumex_CPM DPM 0.50 12.10 Count_Time(min) Quench_number Cl4_CPM Run_Date 9/22/2016 5: 16 PM . 45.00 633.77 10.98 ----i ----T-----:i:-1---Ll---Gross_B_CPM LUMEX 6--/ Counts 11.20 0.00 I 01cm Lumex_CPM DPM 4* -j---'1 0.20 12.70 -11 / Counls 2-Bctu 20 40 (-0 80 100 W:!.!lac 1400 DSA. P04AS408.DAT, 9122/2016, page 7 Page 5672 of 5809

  • rv v Rack_position 0 7 4 2 20 C-14 YELLOW Count_ Time(min) Quench_number 45.00 633.53 * / Counts *01em / Counts Bela JWlll c-0 so 100 Cl4_CPM 10.94 Run_Date 9/22/2016 6:03 PM Gross_B_CPM LUMEX 11.30 0.00 Lumex_CPM DPM 0.30 11.20 ------------------------------------*------------------------------*----*------------*----------------------* Wallac 1400 DSA. P04AS408.DAT, 9/22/2016, page 8 Page 5673 of 5809

***--*----*----__________________________________ __ t.__{}_] g PROTOCOL DATE : 5 C-14 15 min : 2016/09/22 "f.IME : 18:49 ID : P05AS355 C-14 Wallac 1414 WinSpectral v,.40 S/N 4140127 Counting mode : DPM Quench index : SQP(E) lsotope(s) : C14 C14 = ,5730.00 y Protocol name : C-1415 min Counting time : 900 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 10 Sp. library of isotope C14 : Wallac Vial type : Diffuse Liquid system : HiSafe Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Listing,Header,Spectrum Header : C-14 Spectrum : Rnd.Cos,Beta Window 1 35-300 /Beta Window 2 35-300 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total activity: C14 308.8 DPM 0.005 kBq Wallac 1400 DSA.' P05AS355.DAT, 9/22/2016, page l Page 5674of5809 C-14 YELLOW Rack_position Count_ Time(min) Quench_number 59 l 15.QO 632.76 / Counts Chern 15 / Counls Bela _jl.JU 40 (i{) 80 100 Cl4_CPM 128.50 Run_Date 912212016 Gross_B_CPM 128.80 Lumex_CPM 0.30 LUMEX 0.00 DPM 155.00 Rack_position Count_Time(min) Quench_number

  • Cl4_CPM Run_ Date 9/22/2016 7:06 PM 59 2 15.00 627.94 121.92 Page 5675 of 5809 15**<-----W1-+_1,___ ----<--I 20 40 60 100 / Counls Chern / Counts Bela Gross_B_CPM 122.10 Lmnex_CPM 0.20 Wallac 1400 DSA, P05AS355.DAT, 9/22/2016, page 2 LUMEX 0.00 DPM 153.80 Effective 3/25/201 o Revision 1 Effective March 2010 Radiochemistry Balch Checklist 26-Sep-2016 satch# 'S Cl W y_,_ Criteria: Yes No Comments Sample Solids are less than or eaual to 100 ma for GAB. Samples have been blank corrected (If required). :Y Blank correction renorted Included (ff renulred). If activity less than lOx MDA/MDC, error is less than or equal to 150% of sample activity. If greater than 10* MDA/ MDC, error is 40% or less. /' If "-'-w ... _ MDA I ........ -----is o""u Instrument source check Is within limits. ,_/ Instrumnnt bkn rheck is within limits. Method RDL/ LLD has been met. If duplicate.activities are: Less than 5* MDA/ MDC, then RPO ls 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, V" If below the MDA/ MDC, the RPO ls 0%, Or meets the client's renuired RER acceptance criteria. Tracer yield is 15-125%
  • Carrier yield 25-125%. (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. / lfTf ---' ----*--..-J;O/n nF *-***--* "rtlultu\ Samnle was run within hold time. 1,/ JJF::JL Samele was correctlv nreserved if reaulred. /-Smears Taken for Radioactive batches. Method Spike and LC5 are within 75-1250/o ,,,.,....-lfn* meet_<; the client's rnntract accenbnrn crlt<*rl"'* No blank spaces on data forms. All line outs initialed and dated. 1 ** _ --------Aux data ls correct. Client Saeclal reouirements aaae has been checked. ..,,,---Raw Data and I or snectrum are Included and nronerlv statused. ,,,.-MS, LCS, and Duplicate RPD/RER values uploaded to UMS and V"I .. --VP*i"'-" .... . (If v D-*-&. --*----' <-*-r,.cft ./' Batch Data Excentlon Renorts IDER) completed. if annlicable. / Vt<JL Batch Data Exception Reports (DER) second reviewed. v Olsnosltion verified to be comnleted. -All"uot '""rrectlon comoleted if r .. ouired. \\1rJ Review sample hlstorlcal results If available (If REMP, results above MDC have been verified bv historical results recount or><*e-analvsis.) , Primary Review Performed 1 rv/1-n >rllP ()1[2 l)v -/' Secondary Review Performed By: (\ c a°'--D I Page 5676 of 5809 !*Sr/} 1?3 I ISlnJ:1s) 10 j[A) c GL-CHL-RAD-013 Rev 1 Page 1 of 1 1 o)llh GEL Laboratories LLC Form GEL-DER
  • DATA EXCEPTION REPORT
  • Mo.Day Yr. Division: Quality Criteria: 26-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC EPA EERF C-01 Modified Solid Batch ID: Sample Numbers: 1598080 See Below Potentially affected work order(s)(SDG):405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235021, 405235022, 405235023, 405235024, 1. Reporting results. 405235025,405235026,405235027,405235028,405235029, 405235030,405235031,405235032,405235033,405235034, 405235035,405235036,405235037,405235038,405235039, 405235040, 1203626127, and 1203626128 were received and analyzed outside of the method specified hold time. Originator's Name: Data Validator/Group Leader: Lyndsey Pace 26-SEP-16 Angela Johnson 27-SEP-16 Page 1 Page 5677 of 5809 DER Report No.: 1561231 Revision No.: 1 Type: Process Client Code: MJWC I I Prep Logbook 70 !0 fer The Determination of Carbon-14 in Water, Soil, Vegetation and Other Solid Matrices ID: 1598080 Analyst: Tiffany Jordan Method: EPA EERF C-01 Modified Lab SOJ:>: GL-RAD-A-003 REV# 15 Instrument: BAL-16107662 Sample ID Prep Date Matrix 405235021 21-SEP-2016 15:56:10 Soil 405235022 21-SEP-2016 15:56:10 Soil 405235023 21-SEP-2016 15:56:10 Soil 405235024 21-SEP-2016 15:56:10 Soil 405235025 21-SEP-2016 15:56:10 Soil 405235026 21-SEP-2016 15:56:10 Soil 405235027 21-SEP-2016 15:56:10 Soil 405235028 21-SEP-2016 15:56:10 Soil 405235029 21-SEP-2016 15:56:10 Soil 405235030 21-SEP-2016 15:56:10 Soil 405235031 21-SEP-2016 15:56:10 Soil 405235032 21-SEP-2016 15:56:10 Soil 405235033 21-SEP-2016 15:56:10 Soil 405235034 21-SEP-2016 15:56:10 Soil 405235035 21-SEP-2016 15:56:10 Soil 405235036 21-SEP-2016 15:56:10 Soil 405235037 21-SEP-2016 15:56:10 Soil 405235038 21-SEP-2016 15:56:10 Soil 405235039 21-SEP-2016 15:56:10 Soil 405235040 21-SEP-2016 15:56:10 Soil 1203626126 MB 21-SEP-2016 15:56:10 Soil 1203626127 OOP (405235021) 21-SEP-2016 15:56:10 Soil 1203626128 MS(405235021) 21-SEP-2016 15:56:10 Soil 1203626129 LCS 21-SEP-2016 15:56:10 Soil Reagent/Solvent Lot ID Description Amount 2242305.2 Ecosciut A Scinullation Solution !OrnL 2440076.3 PotJSSiurn Persulfate 99+% 5g 2440953 RL-0.4M Hydrochloric Acid 50rnL 2444293.4 Methanol 4L Plastic Bottle 9rnL 2454859.17 l 6M Nitric Acid Poly Coated Bottle 25rnL 2455949 RL-IM Silver Nitrate 2mL Analytical Logbook version I 11-04-2002 Type Sam2leld DescriQtion LCS 1203626129 Carbon-14 SPIKE MS 1203626128 Carbon-14 SPIKE Dry or Wet Unadjusted Aliquot Aliquot (g) (g) w 1.257 1.049 w 1.343 1.083 w 1.264 0.979 w 1.363 1.099 w 1.282 1.008 w 1.276 1.064 w 1.338 1.095 w 1.33 1.028 w 1.446 1.167 w 1.254 0.954 w 1.311 1.015 w 1.371 1.092 w 1.36 J.12 w 1.347 1.083 w 1.311 1.098 w 1.286 1.058 w 1.31 1.228 w 1.392 1.164 w 1.359 1.241 w 1.259 1.073 w 1.241 w 1.318 1.1 w 1.288 1.075 w 1.241 Comments: Spike Pipet ID: RAD-LSC-2970968 Flask# 2 3 4 5 6 8 83 84 86 400 402 404 405 406 506 507 514 519 530 706 708 729 733 Serial Number 1646-B 1646-B S2ike Amount S2ike Units .I mL .1 mL GEL Laboratories LLC Filename : C14.XLS File type : Excel Version#: 1.3.10 Batch : 1598080 Analyst: TIF02034 Prep Date: 9/21/2016 Method Uncertainty : 0.0363 Geometry: 3ml Ethanolamine/9ml Methanoi/10ml EcoScint A Sample Characteristics Sample Sample Aliquot Sample Aliquot S!Dev. Sample Pos. ID G G Date/Time 1 405235021. 1 1.0490 3.3284E-03 1218/201514:17 2 405235022.1 1.0830 3.3320E-03 1218/2015 13:43 3 405235023. 1 0.9790 3.3212E-03 121212015 10:40 4 405235024.1 1.0990 3.3336E-03 1218/2015 14:13 5 405235025.1 1.0080 3.3242E-03 1218/2015 13:38 6 405235026.1 1.0640 3.3300E-03 12181201510:15 7 405235027.1 1.0950 3.3332E-03 1218/201510:19 8 405235028.1 1.0280 3.3263E-03 11/23/2015 14:50 9 405235029.1 1.1670 3.3407E-03 11/23/201511:10 10 405235030.1 0.9540 3.3185E-03 11/23/201514:44 11 405235031.1 1.0150 3.3249E-03 11/2612015 14:25 12 405235032.1 1.0920 3.3329E-03 11/23/2015 11 :48 13 405235033.1 1.1200 3.3358E-03 11/23/201511:53 14 405235034.1 1.0830 3.3320E-03 11/23/201511:20 15 405235035.1 1.0980 3.3335E-03 11/23/2015 11 :06 16 405235036.1 1.0580 3.3294E-03 11/23/201511:12 17 405235037 .1 1.2280 3.3471E-03 11/30/201511 :19 18 405235038.1 1.1640 3.3404E-03 11/30/201510:40 19 405235039. 1 1.2410 3.3484E-03 11/30/2015 10:43 20 405235040.1 1.0730 3.3309E-03 11/30/2015 13:23 21 1203626126.1 1.2410 3.3484E-03 9/21/2016 0:00 22 1203626127.1 1.1000 3.3337E-03 1218/201514:17 23 1203626128.1 1.0750 3.3311E-03 1218/2015 14:17 24 1203626129.1 1.2410 3.3484E-03 9/21/2016 0:00 Count raw Data Rack Position# 91-2 91-3 91-4 91-5 91-6 91-7 91-8 91-9 91-10 91-11 91-12 0-1 0-2 0-3 5!M 59-2 59-3 59-4 59-5 59*6 59-7 59-8 59-9 59-10 C1598080 Carbon-14 Solid Procedure Code : Parmname Required MDA : C-14 Abundance: Halflife of Carbon-14 : Bkg Counting Count Time Quench# Gross Bkg Time (min.) cpm cpm (min.) 70 627.64 11.47 11.14 70 70 632.05 12.21 11.14 70 70.0166702 631.87 11.87 11.14 70 70 632.23 12.12 11.14 70 70 630.8 11.99 11.14 70 70 627.16 11.96 11.14 70 70 629.67 12 11.14 70 70 632.11 11.71 11.14 70 70 634.66 11.56 11.14 70 70 629.84 11.25 11.14 70 70 632.34 11.83 11.14 70 70 630.98 11.89 11.14 70 70 629.13 11.32 11.14 70 70 631.93 11.68 11.14 70 70 631.69 11.67 11.14 70 70 633.77 11.77 11.14 70 70 632.88 11.22 11.14 70 70 629.96 12.36 11.14 70 70 631.51 11.48 11.14 70 70 630.74 11.56 11.14 70 70 632.17 11.66 11.14 70 70 633.77 10.79 11.14 70 70 632.05 128.55 11.14 70 70 631.33 129.06 11.14 70 Page 1 LSC_14CS Carbon-14 2 1.00 5700.00 Corrected Bkg Bkg Quench# cpm 625.67 11.1323 625.67 11.0909 625.67 11.0933 625.67 11.0885 625.67 11.1062 625.67 11.1348 625.67 11.1175 625.67 11.0901 625.67 11.0499 625.67 11.1159 625.67 11.0870 625.67 11.1041 625.67 11.1221 625.67 11.0925 625.67 11.0956 625.67 11.0653 625.67 11.0793 625.67 11.1148 625.67 11.0979 625.67 11.1068 625.67 11.0893 625.67 11.0653 625.67 11.0909 625.67 11.1000 pCi/G years Count Start Date/Time 9123/2016 8:39 9/23/2016 9:50 9/23/2016 11 :02 9123/2016 12:13 912312016 13:24 9/23/2016 14:35 9/23/201615:47 9/23/2016 16:58 9/23/2016 18:09 9/2312016 19:20 9/23/2016 20:32 9/23/2016 21 :43 9/23/2016 22:54 9/24/2016 0:05 9/24/2016 2:29 9/24/2016 3:41 9/24/2016 4:52 9/24/2016 6:03 9/24/2016 7:14 9/24/2016 8:26 9/24/2016 9:37 9/24/2016 10:48 9/24/2016 11:59 9/24/2016 13:11 C-14 Normalization Sample Factor Decay 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 *1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 1.00000 1.000 C1598080 Pipe!, 0.1 ml Stdev : +/-0.000200 ml Pipe!, 0.5 ml Stdev: +/-0.001000 ml Analytical SOP: GL-RAD*A*003 Instrument SOP: GL-RAD*l-014 Calibration Data Calibration Counted Calibration Due Pos. on Date Date 1 LSCYELLOW 6/1/2016 5131/2017 2 LSCYELLOW 611/2016 5/31/2017 3 LSCYELLOW 6/1/2016 5/31/2017 4 LSCYELLOW 6/1/2016 5131/2017 5 LSCYELLOW 6/1/2016 5/31/2017 6 LSCYELLOW 611/2016 5/31/2017 7 LSCYELLOW 611/2016 5/31/2017 8 LSCYELLOW 6/1/2016 5/31/2017 9 LSCYELLOW 6/1/2016 5/31/2017 10 LSCYELLOW 6/1/2016 5/31/2017 11 LSCYELLOW 611/2016 5131/2017 12 LSCYELLOW 611/2016 5/31/2017 13 LSCYELLOW 611/2016 5/31/2017 14 LSCYELLOW 6/1/2016 5/31/2017 15 LSCYELLOW 6/1/2016 5/31/2017 16 LSCYELLOW 611/2016 5131/2017 17 LSCYELLOW 6/1/2016 5/31/2017 18 LSCYELLOW 6/1/2016 5/31/2017 19 LSCYELLOW 6/1/2016 5/31/2017 20 LSCYELLOW 611/2016 5/31/2017 21 LSCYELLOW 6/1/2016 5131/2017 22 LSCYELLOW 611/2016 5131/2017 23 LSCYELLOW 611/2016 5/31/2017 24 LSCYELLOW 611/2016 5/31/2017 Detector Detector Efficiency Efficiency Error (cpm/dpm) (cpm/dpm) 0.6858 0.00792 0.6899 0.00792 0.6898 0.00792 0.6901 0.00792 0.6888 0.00792 0.6854 0.00792 0.6878 0.00792 0.6900 0.00792 0.6920 0.00792 0.6880 0.00792 0.6901 0.00792 0.6890 0.00792 0.6873 0.00792 0.6898 0.00792 0.6896 0.00792 0.6913 0.00792 0.6906 0.00792 0.6881 0.00792 0.6894 0.00792 0.6888 0.00792 0.6900 0.00792 0.6913 0.00792 0.6899 . 0.00792 0.6893 0.00792 Page2 Background Background Count Rack Start Position# Datemme 91-1 9/23/2016 7:28 91-1 9/23/2016 7:28 91-1 9/23/2016 7:28 91-1 9/23/2016 7:28 91-1 9/23/2016 7:28 91-1 9/23/2016 7:28 91-1 9/23/2016 7:28 91*1 912312016 7:28 91-1 9/2312016 7:28 91-1 9/2312016 7:28 91-1 912312016 7:28 91-1 9/23/2016 7:28 91-1 9/23/2016 7:28 91-1 9/2312016 7:28 91-1 9/2312016 7:28 91-1 912312016 7:28 91-1 9123/2016 7:28 91-1 9/23/2016 7:28 91-1 9/23/2016 7:28 91-1 9/2312016 7:28 91-1 9/2312016 7:28 91-1 9/23/2016 7:28 91-1 9/2312016 7:28 91-1 9/23/2016 7:28 0 ......, Vi 00 0 "' Notes: * -Results are decay corrected to Sample Date/Time * -Reference date for Spike Activity (dpm/ml) is the batch Prep Date * -Spike Nominals are decay corrected to Sample Date/Time * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G % 1 0.8228 0.5809 2 1.1887 0.2114 168.27% 2 0.7908 0.5583 2 1.1425 0.6747 51.56% 3 0.8751 0.6178 2 1.2642 0.5182 73.74% 4 0.7791 0.5500 2 1.1255 0.6127 55.83% 5 0.8516 0.6012 2 1.2302 0.5735 65.00% 6 0.8119 0.5732 2 1.1729 0.5098 69.61% 7 0.7855 0.5546 2 1.1347 0.5279 65.12% 8 0.8330 0.5881 2 1.2035 0.3937 92.07% 9 0.7304 0.5156 2 1.0552 0.2846 111.42% 10 0.9013 0.6363 2 1.3021 0.0920 421.66% 11 0.8434 0.5954 2 1.2184 0.4778 77.01% 12 0.7858 0.5548 2 1.1353 0.4706 72.94% 13 0.7687 0.5427 2 1.1105 0.1158 286.17% 14 0.7910 0.5585 2 1.1427 0.3543 97.09% 15 0.7805 0.5511 2 1.1276 0.3417 99.29% 16 0.8070 0.5697 2 1.1658 0.4341 81.06% 17 0.6964 0.4917 2 1.0061 0.0748 401.01% 18 0.7385 0.5214 2 1.0669 0.7004 46.51% 19 0.6908 0.4877 2 0.9980 0.2012 148.62% 20 0.8001 0.5649 2 1.1558 0.2762 125.57% 21 0.6899 0.4871 2 0.9967 0.3002 99.90% 22 0.7761 0.5480 2 1.1213 -0.1631 202.96% 23 0.7967 0.5625 2 1.1510 71.3477 1.47% 24 0.6910 0.4878 2 0.9982 62.1167 1.46% Net Count Rate CPM 0.3377 1.1191 0.7767 1.0315 0.8838 0.8252 0.8825 0.6199 0.5101 0.1341 0.7430 0.7859 0.1979 0.5875 0.5744 0.7047 0.1407 1.2452 0.3821 0.4532 0.5707 -0.2753 117.4591 117.9600 C1598080 Spike SIN: 1646-B Spike Exp Date : 1/5/2017 Spike Activity {dpm/ml): 1681.40 Spike Volume Added: 0.10 LCSS/N: LCS Exp Date : LCS Activity {dpm/ml): LCS Volume Added: 2SIGMA Net Count Counting Rate Error Uncertainty, CPM pCi/G 0.5682 0.6974 0.5769 0.6818 0.5727 0.7489 0.5758 0.6704 0.5744 0.7305 0.5744 0.6955 0.5747 0.6737 0.5707 0.7105 0.5683 0.6214 0.5653 0.7605 0.5722 0.7212 0.5731 0.6726 0.5662 0.6495 0.5704 0.6741 0.5703 0.6650 0.5712 0.6895 0.5644 0.5877 0.5791 0.6384 0.5679 0.5861 0.5690 0.6799 0.5701 0.5878 0.5588 0.6488 1.4124 1.6815 1.4150 1.4605 Page3 1646-B 1/5/2017 1681.40 0.10 2SIGMA Total Prop. Uncertainty pCi/G 0.6976 0.6836 0.7498 0.6719 0.7317 0.6965 0.6748 0.7111 0.6218 0.7605 0.7221 0.6735 0.6495 0.6746 0.6655 0.6903 0.5877 0.6405 0.5863 0.6802 0.5882 0.6488 5.4782 4.7647 . Sample Sample Nominal QC Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB 405235021.1 DUP
  • 0.0% 405235021. 1 MS 70.4613 101.3% LCS 61.0304 101.8%

C-14 YELLOW PROTOCOL DATE : 5 C-14 70 min : 2016/09/23 TIME : 07:27 ID : P05AS356 C-14 Wallac 1414 WinSpectral v1.40 S/N 4140127 Counting mode : DPM Quench index : SQP(E) lsotope(s) : C14 C14 = ,5730.00 y Protocol name : C-14 70 min Counting time : 4200 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 10 Sp. library of isotope C14 : Wallac Vial type : Diffuse Liquid system : HiSafe Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Listing,Header,Spectrum Header : C-14 Spectrum : Rnd.Cos,Beta Window 1 35-300 /Beta Window 2 35-300 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 .. Total activity: C14 194.6 DPM 0.003 kBq Wallac 1400 DSA, P05AS356.DAT, 9/24/2016, page 1 Page 5682 of 5809 C-14 YELLOW Rack_position Count_Time(min) Quench_number 91 1 70.00 625.67 / Counls Oicm / Counls Bela Rack_position Count_Time(min) Quench_number 91 2 70.00 627.64 15*-----I / Couuls *----*l---1----j Chem 5 / Counls Bela 20 40 60 80 100 Rack_position CO\mt_Time(min) Quench_number 91 3 70.00 632.05 "L I0*-1---++--"-t---, --/ Counls Oiem 1 I / Counls Bein u-1L 20 40 c;o so loo Cl4_CPM 11.14 Run_Date 9/23/2016 7:28 AM Gross_B_CPM LUMEX 11.50 0.00 Lumex_CPM DPM 0.30 13.40 Cl4_CPM 11.47 Run_Date 9/23/2016 8:39 AM Gross_B_CPM 12.00 Lumex_CPM 0.50 LUMEX 0.00 DPM 12.50 Cl4_CPM 12.21 Run_Date 9/23/2016 9:50 AM Gross_B_CPM LUMEX 12.70 0.00 Lumex_CPM DPM 0.50 13.90 Wallac 1400 DSA, P05AS356.DAT, 9/24/2016, page 2 Page 5683 of 5809 C-14 YELLOW Rack..._position Count_ Time(min) Quench_number *91 4 70.02 631.87 15 -----,,---,---,----.----, / Counts Chem / Counts Bela 20 40 ullLt 80 100 Rack_position Count_Time(min) Quench_number 91 5 70.00 632.23 / Counts 010111 / Counts Beta Cl4_CPM "11.87 Run_Date 9/23/2016 11:02AM Gross_B_CPM 12.40 Lumex_CPM 0.60 LUMEX 0.00 DPM 13.10 Cl4_CPM 12.12 Run_Date 9/,23/2016 12:13 PM Gross_B_CPM 12.60 Lumex_CPM 0.50 LUMEX 0.00 DPM 13.60 Rack_position Count_Time(min) Quench_number Cl4_CPM Run_Date 9/23/2016 1:24 PM Page 5684 of 5809 91 6 *10.00 630.80 11.99 i *:'I _J_ 20 40 / Counls 01em / Coums Beta Gross_B_CPM 12.30 Lumex_CPM 0.30 WDllac 1400 DSA; P05AS356.DAT, 9/24/2016, page 3 LUMEX 0.00 DPM 13.40 Rack_position 91 7 15 Rack_position 91 8 1 6 4 20 Rack_position 91 9 10 4 2 20 Page 5685 of 5809 C-14 YELLOW Count_Time(min) Quench_number 70.00 627.16 / Counls Oicm / Counls Ile la Count_Time(min) Quench_number 70.00 629.67 / Counls Chem / Couuls '.Jilli Bela 60 80 100 Count_ Time(min) Quench_number 70.00 632.11 **--*;:1-1, -'---' -rl--.--,. Ii 40 (>0 / Counls Oicm / Counls Beta Cl4_CPM 11.96 Run_Date 9/23/2016 2:35 PM Gross_B_CPM 12.50 Lumex_CPM 0.50 LUMEX 0.00 DPM 13.20 Cl4_.:.CPM 12.00 Run_Date 9/23/2016 3:47 PM Gross_B_CPM 12.30 Lumex_CPM 0.30 LUMEX 0.00 DPM 13.00 Cl4_CPM 11.71 Run_Date 9/2312016 4:58 PM Gross_B,...CPM LUMEX 12.10 0.00 Lumex_CPM DPM 0.40 12.70 W,1!1ac 1400 DSA, P05AS356.DAT, 9/24/2016, page 4 \ l C-14 YELLOW Rack_position Count._ Time(min) Quench_number 91 10 ' ' 70.00 634.66' Rack_position Count_Time(min) Quench_number 91 u 70.00 629.84 Rack_position 91 12 20 1 I / Counts 01cm / Counts llcl11

  • Count_Time(min) Quench_number .. 70.00 632.34 / Counts Oiem / Counts Ile Lu qO 80 100 Cl4_CPM 11.56 Run_Date 9/23/2016 6:09 PM Gross_B_CPM 12.00 Lumex_CPM 0.50 LUMEX 0.00 DPM 13.30 Cl4_CPM ll.25 Run_Date 9/23/2016 7:20 PM Gross_B_CPM 11.60 Lumex_CPM 0.30 LUMEX 0.00. DPM 12.40 Cl4_CPM 11.83 Run_Date 9/23/2016 8:32 PM Gross_B_CPM LUMEX 12.10 0.00 Lumex_CPM DPM 0.30 12.60 ---*---------*-----------..,--**-------------------*--*---*--*------*--*-------*-------*------**------******--***-----WaHac 1400 DSA. P05AS356.DAT, 9/24/2016, page 5 Page 5686 of 5809 D C-14 YELLOW Rack_position Courit_Time(min) Quench_number 0 1 70.00 630.98 15--r---1 I .. / Counts 10 ------I Chem I -/ Counts Beta u11J 1\0 80 100 Rack_position Cmint_Time(min) Quench_number 0 2 70.00 629.13 / Counts IO Chem / Counts Beta 100 Rack_position Count_Time(min) Quench_number 0 3 70.00 631.93 ' *1 '1 20 ---i---+----1 .*I ! I . ui1lb1 40 cio so 100 '** £S-/ Counts Chem / Counts Beta Run_Date Cl4_CPM 11.89 ' 9/23/2016 9:43 PM Gross_B_CPM LUMEX 12.30 0.00 Lumex_CPM DPM 0.40 13.00 C14_CPM 11.32 J.3.un_Date 9/23/2016 10:54 PM Gross_B_CPM LUM EX 11.80 0.00 Lumex_CPM DPM 0.50 12.30 Cl4_CPM 11.68 Run_ Date 9/24/2016 0:05 AM Gross_B_CPM LUMEX 12.00 0.00 Lumex_CPM DPM 0.30 12.20 Wallac 1400 P05AS356.DAT, 9/24/2016, page 6 Page 5687 of 5809 C-14 YELLOW PROTOCOL DATE : 5 C-14 70 min : 2016/09/24 TllYIE ' .. : 02:29 ID : P05AS357 C-14 Wallac 1414 WinSpectral v1.40 S/N 4140127 Counting mode : DPM Quench index : SQP(E) lsotope(s) : C14 C14 = ,5730.00 y Protocol name * : C-14 70 min Counting time : 4200 Repeats : 1 Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cpm : 0.00 Checking time: 10 Sp. library of isotope C14 : Wallac Vial type : Diffuse Liquid system : HiSafe Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Listing,Header,Spectrum Header : C-14 Spectrum : Rnd.Cos,Beta Window 1 35-300 /Beta Window 2 35-300 /And.Cos Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta* FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total activity: C14 431.2 DPM 0.007 kBq Wallac 1400 P05AS357.DAT, 9/24/2016, page 1 Page 5688 of 5809 C-14 YELLOW Rack_position Count_ Time(min) Quench_nu.mber 59 1 70.00 631.6.9 / Counts Chem / Cou111s Bctn Rack_position
  • Count_Time(min) Quench_number l lo 59 2 10* 70.00 633.77 / Counts Chem / Counts Bctll Rack_position Count_Time(min) Quench_number 59 3 70.00 632.88 15-.-----,--* / Counts Chem // Counts Beta C14_CPM 11.67 Run_Date 9/24/2016 2:29 AM Gross_B_CPM 12.20 Lumex_CPM 0.50 LUMEX 0.00 DPM 12.80 Cl4_CPM 11.77 Run_Date 9/24/2016 3:41 AM Gross_B_CPM LUMEX 12.20 0.00 Lumex_CPM DPM 0.40 14.20 Cl4_CPM 11.22 Run_ Date 9/24/2016 4:52 AM Gross_B_CPM LUMEX 11.60 0.00 Lumex_CPM DPM 0.40 12.80 Wallac 1400 DSA, P05AS357.DAT, 9/24/2016, page 2 Page 5689 of 5809 C-14 YELLOW -*-*-*--*----**--*-*---.. .. *---*-"*-*----*------* .. -----*----.. -------Rack_position Count_Time(min) Quench_number 59 4 70.00 629.96 * / Counts IO*-01cm / Counts Ile ta Rack_position
  • Count_Time(min) Quench_number 59 5 70.00 631.51 JO -/ Counts 01cm / Counts Ile ta Rack_position Count_Time(min) Quench_number 59 6 70.00 630.74 *---,-----,-----, / Counts 10-. 01cm / Counts Bela 0 0 20 40 (-0 80 100 Cl4_CPM 12.36 Run_Date 9/24/2016 6:03 AM Gross_B_CPM LUMEX 12.80 0.00 Lumex_CPM DPM 0.40 14.40 C14_CPM 11.48
  • Run_Date 9/24/2016 7:14 AM Gross_B_CPM 11.80 Lumex_CPM 0.30 LUMEX 0.00 DPM 12.60 Cl4_CPM 11.56 Run_Date 9/24/2016 8:26 AM Gross_B_CPM LUMEX 11.90 0.00 Lumex_CPM DPM 0.40 12.10 ----------.... -----*-*--------------*-.. *-----**----*-*-----*-----*-------------.. ---------------*----*-***--*-*----*-*-*-*--*---*--------*-***------------------*--"*"'----***----* Wallac 1400 DSA, P05AS357.DAT, 9/2412016, page 3 Page 5690 of 5809 C-14 YELLOW Count_ Time(min) Quench_number 59 7 ;10.00 632.17 8---___ , ---/ Counls Chem / Counts Bela Rack_position Count_Time(min) Quench_number 59 8 70.00 633.77 15,-,-------,--/ Counts Chem / Counls llcla Rack_position Count_Time(min) Quench_number 59 9 70.00 632.05 / Counts 01em --I / Counts Bela I w oo m 100 Cl4_CPM 11.66 Run_Date 9/2412016 AM Gross_B_CPM LUMEX 12.20 0.00 Lumex_CPM DPM 0.50 13.70 Cl4_CPM 10.79 Run_Date 9/24/2016 10:48 AM Gross_B_CPM LUMEX 11.30 0.00 Lumex_CPM DPM 0.50 11.40 Cl4_CPM 128.55 Run_Date 9/24/2016 11:59 AM Gross_B_CPM LUMEX 128.90 0.00 Lumex_CPM DPM 0.40 163.20 Wallac 1400 DSA, P05AS357.DAT, 9/24/2016, page 4 Page 5691 of 5809 C-14 YELLOW Rack_position Count_Time(min) Quench_number 59 10 70.DO 631.33 / Counts Chem / Counts Bela ... 100 Cl4_CPM 129.06 Run_Date 9/24/2016 1:11 PM Gross_B_CPM LUMEX 129.50 0.00 Lumex_CPM DPM 0.40 164.00 Wallac 1400 DSA, P05AS357.DAT, 9/24/2016, page 5 Page 5692 of 5809 Effective 3/25/201 O Revision 1 Effective March 2010 Radiochemistry Batch Checklist 29-Sep-2016 Batch# C(c/ Product: _______ _ Dato: -Criteria: Yes No Comments Samele Solids are less than or eaual to 100 ma for GAB. Al/}-Samples have been blank corrected (If required). /j;r Blank correction reoorted Included fif reoulred), If activity less than lOx MDA/MDC, error Is less / than or eaual to 150%.of sample activity, If greater than 10* MDA/ MDC, error Is 40% or less. If hAlnm thA Mn.a I unc Rr*n* '"""ft" Instrument source check Is within limits. / Instrument him rhPCk Is within limits. Method RDL/ LLD has been met. V' If duellcate activities are: Less than 5* MDA/ MDC, then RPO Is 100% or less, If greater 5* MDA/ MDC, then RPO 20% or less, If below the MDA/ MDC, the RPO Is 0%, Or meets the client's reaulred RER acceetance criteria. Tracer yield Is 15-1250/o
  • Carrier yield 25-1250/o. ti fy (Or meets the client's contract acceptance criteria). Method blank Is less than the RDL/ LLD. i/' l;O/n nf .. .-tlultv\ GL-CHL-RAD-01'3 Rev 1 Page 1 of 1 Sample was run within hold time. v' _'Zoo U<\12 ) 5 (a] Samele was correctlv ereserved If reauired. ./ Smears Taken for Radioactive batches. ;J /J--Method Spike and LCS are within 75-1250/o / l<or meets the client's contract acceotance criteria). No blank spaces on data forms. All line outs Initialed and dated, INn . Aux data Is correct. J/4-Client Seecial reauirements eaae has been checked. / Raw Data and/ or seectrum are included and erooerlv statused. ,/ MS, LCS, and Duplicate RPD/RER values uploaded to UMS and v val"A" verified ..... (If ' NFY v I' 'n..,.*-1... ..,._ .. __ ..,a ._ .. _ ,..._.,.,,.. Batch Data Exceotion Reports CDER\ comoleted If aPolicable. v Y)(Je I Sf,. '\ l.\ \j Batch Data Exception Reports (DER) second reviewed. / !)ell IS( Disoosition verified to be comeleted. Aliauot Correction comnleted If *Anulred. ;J fr* Review sample historical results if available \/ (If REMP, results above MDC have been verified bv historical results recount or re-analvsis.) *-----:-----,,. .. --Page 5693 of 5809 GEL Laboratories LLC Form GEL-DER . DATA EXCEPTION REPORT
  • Mo.Day Yr. Division: Quality Criteria: 30-SEP-16 Radiochemistry Specifications Instrument Type: Test I Method: Matrix Type: LSC EPA EERF C-01 Modified Solid Batch ID: Sample Numbers: 1598082 See Below Potentially affected work order(s)(SDG): 405235 Application Issues: Sample received out of holding Specification and Requirements DER Disposition: Exception

Description:

1. Samples 405235061, 405235062, 405235063, 405235064, 1. Reporting results. 405235065,405235066,405235067,405235068,405235069, 405235070,405235071, 405235072,405235073,405235074, 405235075,405235076,405235077,405235078, 1203626114,and 1203626115 were received and analyzed out of method specified hold time. Originator's Name: Data Validator/Group. Leader: Elizabeth Krouse 30-SEP-16 Lyndsey Pace 30-SEP-16 Page 1 Page 5694 of 5809 DER Report No.: 1563139 Revision No.: 3 Type: Process Client Code: MJWC 0t -..-<JC.. Prep Logbook ft.J \O{tf The Determination of Carbon-14 in Water, Soil, Vegetation and Other Solid Matrices Batch ID: 1598082 IYJ?e Sample Id Description ruL-'--t-"-8-'-'I /'-'(? ____ __ -'S"'p,_,,ik"-'e'-'U'-'n'-"its=-Analyst: Method: Lab SOP: Instrument: Sample ID 405235061 405235062 405235063 405235064 405235065 405235066 405235067 405235068 405235069 405235070 405235071' 405235072 405235073 405235074 405235075 405235076 405235077 405235078 1203626113 MB Tiffany Jordan EPA EERF C-01 Modified GL-RAD-A-003 REV# 15 BAL-16107662 Prep Date 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-2016 14:02:47 27-SEP-201614:02:47 27-SEP-2016 14:02:47 1203626114 DUP (40S235061) SEP-2016 14:02:47 1203626ll5 MS (405235061) 27-SEP-2016 14:02:47 1203626116 LCS 27-SEP-2016 14:02:47 Reagent/Solvent Lot ID Description 2242305.2 Ecoscint A Scintillation Solution 2431394.13 16M Nitric Acid Poly Coated Boule 2440076.3 Potassium Persulfatc 99+% 2444293.4 Methanol 4L Plastic Bottle 2455949 RL-lM Silver Nitratc 2458954 RL-0.4M Hydrochloric Acid Analylical Logbook version 111-04-2002 Matrix Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Amount IOmL 25mL 5g 9mL 2mL 50mL LCS MS 1203626116 C:irbon-14 SPIKE 1203626115 Cmbon-14SPIKE Dry or Wet Unadjusted Aliquot Aliquot (g) (g) w 1.255 1.034 w 1.25 1.008 w 1.304 1.167 w 1.25 1.148 w 1.321 1.188 w 1.302 1.181 w 1.301 1.121 w 1.28 1.102 w 1.261 1.127 w 1.26 1.022 w 1.252 1.045 w 1.28 1.175 w 1.276 1.035 w 1.38 1.233 w 1.378 1.23 w 1.358 1.079 w 1.309 1.179 w 1.308 J.097 w 1.233 w 1.33 1.096 w 1.309 1.079 w 1.233 Comments: Spike Pipet ID: RAD-LSC-2970968 Flask# 2 3 4 5 6 8 83 84 86 400 402 404 405 406 506 507 514 519 530 706 708 1646-B 1646-B .1 .1 GEL Laboratories LLC mL mL Filename: C14.XLS File type : Excel Version # : 1.3.10 Batch: 1598082 Analyst: TIF02034 Prep Date: 9/27/2016 Method Uncertainty : 0.0363 Geometry: 3ml Ethanolamine/9ml Methanoi/1 OmL EcoScint A Sample Characteristics Sample Sample Aliquot Sample Aliquot SIDev. Sample Pos. ID G G Datemme 1 405235061.1 1.0340 3.3269E-03 12114/2015 13:47 2 405235062. 1 1.0080 3.3242E-03 12114/2015 13:10 3 405235063.1 1.1670 3.3407E-03 12114/2015 13:15 4 405235064.1 1.1480 3.3387E-03 12114/2015 13:25 5 405235065.1 1.1880 3.3429E-03 12114/2015 13:56 6 405235066.1 1.1810 3.3422E-03 12114/2015 14:00 7 405235067.1 1.1210 3.3359E*03 12111/201511:30 8 405235068.1 1.1020 3.3340E-03 12111/2015 10:27 9 405235069.1 1.1270 3.3366E-03 12116/2015 12:45 10 405235070.1 1.0220 3.3256E-03 12111/201510:10 11 405235071.1 1.0450 3.3280E-03 12111/2015 10:25 12 405235072.1 1.1750 3.3415E*03 12115/2015 13:35 13 405235073.1 1.0350 3.3270E-03 12111/201511:35 14 405235074.1 1.2330 3.3476E-03 12/1512015 14:10 15 405235075.1 1.2300 3.3473E-03 1211612015 9:31 16 405235076.1 1.0790 3.3316E-03 12111/201514:19 17 405235077.1 1.1790 3.3420E-03 12117/2015 13:30 18 405235078.1 1.0970 3.3334E-03 12117/201512:40 19 1203626113.1 1.2330 3.3476E-03 9/27/2016 0:00 20 1203626114.1 1.0960 3.3333E-03 12114/2015 13:47 21 1203626115.1 1.0790 3.3316E-03 12114/2015 13:47 22 1203626116.1 1.2330 3.3476E*03 9/27/2016 0:00 Count raw Data Rack Position# 59*2 99*1 99*2 99*3 99*4 99-5 99*6 99-7 99*8 99*9 99-10 99-11 99-12 0-1 0-2 0-3 0-4 0-5 0-6 0-7 0-8 0-9 C1598082 Carbon-14 Solid Counting Time Quench# (min.) 70 629.73 70 632.23 70 628.3 70 628.06 70 625.79 70 628.77 70 630.68 70 633.53 70 633 70.0166702 632.82 70 631.33 70.0166702 635.91 70 631.04 70 628.95 70 629.96 70 632.17 70 629.84 70 632.64 70 629.9 70 632.64 70 634.31 70 631.81 Page 1 Procedure Code Parmname: Required MDA: C-14 Abundance: Halfllfe of Carbon-14: Bkg Count Gross Bkg nme cpm cpm (min.) 12.37 12.41 70 12.46 12.41 70 12.51 12.41 70 12.79 12.41 70 11.87 12.41 70 11.91 12.41 70 12.21 12.41 70 12.35 12.41 70 12.34 12.41 70 12.12 12.41 70 12.55 12.41 70 12.99 12.41 70 13.24 12.41 70 13.02 12.41 70 12.05 12.41 70 12.36 12.41 70 12.82 12.41 70 12.82 12.41 70 12.97 12.41 70 13.89 12.41 70 126.18 12.41 70 130.01 12.41 70 LSC_14CS Carbon-14 2 1.00 5700.00 Corrected Bkg Bkg Quench# cpm 622.39 12.3881 622.39 12.3597 622.39 12.3994 622.39 12.4010 622.39 12.4109 622.39 12.3961 622.39 12.3786 622.39 12.3404 622.39 12.3486 622.39 12.3513 622.39 12.3712 622.39 12.2969 622.39 12.3746 622.39 12.3947 622.39 12.3860 622.39 12.3605 622.39 12.3871 622.39 12.3539 622.39 12.3865 622.39 12.3539 622.39 12.3273 622.39 12.3652 pCi/G years Count C-14 Start Normalization Sample Datemme -Factor Decay 9/29/2016 0:31 1.00000 1.000 9/29/2016 2:55 1.00000 1.000 9/29/2016 4:06 1.00000 1.000 9/29/2016 5:17 1.00000 1.000 9/29/2016 6:29 1.00000 1.000 9/29/2016 7:40 1.00000 1.000 9/29/2016 8:51 1.000 9/29/2016 10:02 1.00000 1.000 9/29/201611:14 1.00000 1.000 9/29/2016 12:25 1.00000 1.000 9/29/2016 13:36 1.00000 1.000 9/29/2016 14:47 1.00000 1.000 9/29/2016 15:59 1.00000 1.000 9/29/2016 17: 10 1.00000 1.000 9/29/2016 18:21 1.00000 1.000 9/29/2016 19:32 1.00000 1.000 9/29/2016 20:44 1.00000 1.000 9/29/2016 21 :55 1.00000 1.000 9/29/2016 23:06 1.00000 1.000 9/30/2016 0:17 1.00000 1.000 9/30/2016 1 :29 1.00000 1.000 9/30/2016 2:40 1.00000 1.000 C1598082 Plpet, 0.1 ml Stdev: +/-0.000200 ml Plpet, 0.5 ml Stdev : +I-0.001000 ml Analytical SOP: GL-RAD*A-003 Instrument SOP: GL-RAD-1-014 Calibration Data Calibration Counted Calibration Due Pos. on Date Date 1 LSCYELLOW 6/1/2016 5/31/2017 2 LSCYELLOW 6/1/2016 5/31/2017 3 LSCYELLOW 6/1/2016 5131/2017 4 LSCYELLOW 6/1/2016 5/31/2017 5 LSCYELLOW 6/1/2016 5/31/2017 6 LSCYELLOW 6/1/2016 5/31/2017 7 LSCYELLOW 6/1/2016 5/31/2017 8 LSCYELLOW 6/1/2016 5/31/2017 9 LSCYELLOW 6/1/2016 5/31/2017 10 LSCYELLOW 6/1/2016 5/31/2017 11 LSCYELLOW 6/1/2016 5/31/2017 12 LSCYELLOW 6/1/2016 5/31/2017 13 LSCYELLOW 6/1/2016 5/31/2017 14 LSCYELLOW 6/1/2016 5/31/2017 15 LSCYELLOW 6/1/2016 5/31/2017 16 LSCYELLOW 6/1/2016 5/31/2017 17 LSCYELLOW 6/1/2016 5/31/2017 18 LSCYELLOW 6/1/2016 5/31/2017 19 LSCYELLOW 6/1/2016 5/31/2017 20 LSCYELLOW 6/1/2016 5/31/2017 21 LSCYELLOW 6/1/2016 5/31/2017 22 LSCYELLOW 6/1/2016 5/31/2017 Detector Detector Efficiency Efficiency Error (cpm/dpm) (cpmfdpm) 0.6879 0.00792 0.6901 0.00792 0.6865 0.00792 0.6863 0.00792 0.6839 0.00792 0.6870 0.00792 0.6887 0.00792 0.6911 0.00792 0.6907 0.00792 0.6905 0.00792 0.6893 0.00792 0.6928 0.00792 0.6890 0.00792 0.6871 0.00792 0.6881 0.00792 0.6900 0.00792 0.6880 0.00792 0.6904 0.00792 0.6880 0.00792 0.6904 0.00792 0.6917 0.00792 0.6897 0.00792 Page2 Background Background Count Rack S1art Position# Date!Time 59-1 9/28/2016 23:20 59-1 9/2812016 23:20 59-1 9/28/2016 23:20 59-1 9/28/2016 23:20 59*1 9/28/2016 23:20 59-1 9/28/2016 23:20 59-1 9/2'8/2016 23:20 59*1 9/28/2016 23:20 59-1 9/28/2016 23:20 59-1 9/28/2016 23:20 59-1 9/28/2016 23:20 59-1 9/28/2016 23:20 59*1 9/28/2016 23:20 59-1 9/28/2016 23:20 59-1 9/28/2016 23:20 59*1 9/28/2016 23:20 59-1 9/28/2016 23:20 59*1 9/2812016 23:20 59-1 9/28/2016 23:20 59-1 9/28/2016 23:20 59-1 9/28/2016 23:20 59*1 9/28/2016 23:20 Notes: * -Results are decay corrected to Sample Datemme * -Reference date for Spike Activity (dpm/ml) is the balch Prep Date * -Spike Nominals are decay corrected to Sample Datemme * -RPO changed to 0% due to sample & dup activity below MDA Results Decision Critical Required Sample Act. Sample Act. Level Level MDA MDA Cone. Error Pos. pCi/G pCi/G pCi/G pCi/G pCi/G 1 0.8780 0.6199 2 1.2669 -0.0115 3280.39% 2 0.8968 0.6331 2 1.2940 0.0650 593.52% 3 0.7798 0.5506 2 1.1252 0.0622 539.57% 4 0.7931 0.5599 2 1.1443 0.2224 154.22% 5 0.7693 0.5431 2 1.1100 -0.2999 108.89% 6 0.7700 0.5436 2 1.1110 -0.2699 121.22% 7 0.8085 0.5708 2 1.1667 -0.0984 351.46% 8 0.8184 0.5778 2 1.1809 5.686E-OS 6178.65% 9 0.8010 0.5655 2 1.1558 -4.993E-03 6883.12% 10 0.8835 0.6238 2 1.2749 *0.1477 255.60% 11 0.8664 0.6117 2 1.2501 0.1118 333.73% 12 0.7642 0.5395 2 1.1028 0.3836 86.71% 13 0.8752 0.6179 2 1.2628 0.5467 69.91% 14 0.7373 0.5205 2 1.0638 0.3325 96.37% 15 0.7378 0.5209 2 1.0646 -0.1788 175.86% 16 0.8378 0.5915 2 1.2090 -2.959E-04 121534.89% 17 0.7699 0.5435 2 1.1109 0.2404 138.63% 18 0.8234 0.5813 2 1.1882 0.2772 128.67% 19 0.7360 0.5196 2 1.0620 0.3098 103.16% 20 0.8242 0.5819 2 1.1892 0.9145 39.87% 21 0.8347 0.5893 2 1.2044 68.7219 1.50% 22 0.7336 0.5179 2 1.0585 62.3156 1.47% C1598082 Spike SIN: Spike Exp Date : Spike Activity (dpm/ml): Spike Volume Added: LCSS/N: LCS Exp Date : LCS Activity (dpm/ml): LCS Volume Added: 2SIGMA Net Count Net Count Counting Rate Rate Error Uncertainty CPM CPM pCi/G -0.0181 0.5947 0.7383 0.1003 0.5955 0.7559 0.1106 0.5965 0.6575 0.3890 0.5999 0.6723 -0.5409 0.5890 0.6400 -0.4861 0.5893 0.6413 -0.1686 0.5927 0.6778 0.0096 0.5939 0.6886 -0.0086 0.5939 0.6737 *0.2313 0.5912 0.7397 0.1788 0.5967 0.7314 0.6931 0.6010 0.6518 0.8654 0.6049 0.7490 0.6253 0.6026 0.6280 -0.3360 0.5908 0.6164 -0.0005 0.5943 0.7048 0.4329 0.6001 0.6533 0.4661 0.5997 0.6991 0.5835 0.6019 0.6264 1.5361 0.6123 0.7145 113.8527 1.4067 1.6642 117.6448 1.4262 1.4806 Page3 1646-B 1/5/2017 1681.40 0.10 1646-B 1/5/2017 1681.40 0.10 2SIGMA Total Prop. Uncertainty pCi/G 0.7383 0.7559 0.6575 0.6725 0.6400 0.6413 0.6778 0.6886 0.6737 0.7397 0.7315 0.6524 0.7500 0.6284 0.6164 0.7048 0.6535 0.6994 0.6268 0.7176 5.2903 4.7849 Sample QC 405235061.1 405235061.1 A Sample Nominal Type RPO REA pCi/G Recovery SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE SAMPLE MB DUP
  • 0.0% MS 70.2000 97.9% LCS 61.4262 101.4%

PROTOCOL DATE ID C-14 C-14 YELLOW : 5 C-14 70 min : 2016/09/28 : 23:19 : P05AS360 Wallac 1414 WinSpectral v1.40 S/N 4140127 Counting mode Quench index lsotope(s) C14 : DPM : SQP(E) : C14 = ,5730.00 y . Protocol name Counting time Repeats Cycles Replicates 2sigma% Minimum cpm : C-14 70 min : 4200 : 1 : 1 : 1 : 2.00 Sp. library of isotope C14 Vial type : 0.00 Checking time: 10 : Wallac : Diffuse L.:iquid system : HiSafe -Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Listing,Header,Spectrum Header : C-14 Spectrum : Rnd.Cos,Beta Window 1 35-300 /Beta Window 2 35* 300 /Rnd.Cos Window 3

  • 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total activity: . C14 28.2 DPM 0.000 kBq Wallac 1400DSA*, P05AS360.DAT, 9/29/2016, page 1 ,, Page 5699 of 5809 C-14 YELLOW Rack_position Count_Time(min) Quench_number 59 l 70.00 622.39 / Counls Chem / Counls Beta 100 Rack_position Count_ Time(min) Quench_number 59 2 70.00 629.73 / Counts 01em \ / Connls Betl1 C14_CPM 12.41 Run_Date 9/28/2016 11:20 PM Gross_B_CPM 12.80 Lumex_CPM 0.40 LUMEX 0.00 DPM 14.20 C14_CPM 12.37 Run_Date 9/29/2016 0:31 AM Gross_B_CPM 12.90 Lumex_CPM 0.50 LUMEX 0.00 DPM 14.00 Wallac 1400 DSA, P05AS360.DAT, 9/29/2016, page 2 Page 5700 of 5809

_________ (j /[_ l_ ____ _ PROTOCOL : 6 C-14 70 min DATE : 2016/09/29 TIME : 02:54 ID :P06AS205 C-14 Wallcic 1414 WinSpectral v1.40 S/N 4140127 Counting mode * : DPM Quench index : SQP(E) lsotope(s) : C14 C14 = ,5730.00 y Protocol name : C-14 70 min Counting time : 4200 Repeats : 1

  • Cycles : 1 Replicates : 1 2 sigma % : 2.00 Minimum cprri. : 0.00 Checking time: 10 Sp. library of isotope C14 : Wallac Vial type : Diffuse Liquid system : HiSafe Advanced modes : Chemilum Output to Display POS,DPM1 ,CPMw2,CLMM,FNCT2, RACK,RACKPOS,FNCT1 ,SQPE,DATE, TIME,CPMw1 ,CPM,CPM1 ,CTIME Additions to Display : Listing,Header,Spectrum Header : C-14 Spectrum : Rnd.Cos,Beta Window 1 35-300 /Beta Window 2 35-300 /And.Cos. Window 3 1-1024 /Beta Window 4 1-1024 /Beta Window 5 1-1024 /Beta Window 6 1-1024 /Beta FNCT1 = FNCT1 : CTIME/60 FNCT2 = FNCT2 : CPMW1-CPMW2 FNCT3 = FNCT3 FNCT4 = FNCT4 Total activity: C14 590.7 DPM 0.010 kBq Wallac 1400 DSA, P06AS205.DAT, 9/30/2016, page 1 Page 5701 of 5809 C-14 YELLOW Rack_position CouncTime(min) Quench_number 99 l 70.00
  • 632.23 8+--,-,Hlrt---; / Counts 01cm / Counts Dela
  • Rack_position Count_Time(min) Quench_number 99 2 70.00 628.30 / Conntfi C..11cm 5 / Counts llclll Rack_position Count_Time(min) Quench_number 99 3 70.00 628.06 15---1 "I '! / Counts 10 --01cm I I / Counts llcta 100 Cl4_CPM 12.46 Run_Date 9/29/2016 2:55 AM* Gross_B_CPM LUM EX 12.80 0.00 Lumex_CPM DPM 0.40 13.60 Ct4_CPM 12.51 Run_Date 9/29/2016 4:06 AM Gross_B_CPM LUlvlEX 12.70 0.00 Lumex_CPM DPM 0.20 14.30 Cl4_CPM 12.79 Run_Date 9/29/2016 5:17 AM Gross_B_CPM LUMEX 13.20 0.00 Lumex_CPM DPM 0.40 14.20 Wallac 1400 DSA, P06AS205.DAT, 9/30/2016, page 2 Page 5702 of 5809 C-14 YELLOW -----**-*--*--------*------***-*****-*---------*---*-----*-****---*--*--*-**---*---***-.. -----*---*-**-----*-*-***-**--*-*--****--**------*--------**--*-Rack_position Count_Time(min) Quench_number 99 4 70.00 625.79 15 --.----,----,----,---, / Counts Chem / Counts Beta Rack_position Count_Time(min) Quench_number 99 5 70.00 628. 77 / Counts 01em / Counts Bela 20 40 80 100 Rack_position Count_Time(min) Quench_number 99 6 70.00 630.68 / Counts Chem / Counts Bela Cl4_CPM 11.87. Run_Date 9/29/2016 6:29 AM Gross_B_CPM 12.30 Lumex_Cl'M
  • 0.40 LUMEX 0.00 DPM 13.20 Cl4_CPM 11.91 Run_Date 9/29/2016 7:40 AM Gross_B_CPM LUMEX 12.30 0.00 Lumex_CPM DPM 0.40 14.20 Cl4_CPM 12.21 Run_Date 9/29/2016 8:51 AM Gross_B_CPM 12.50 Lumex_CPM 0.30 LUMEX 0.00 DPM 13.60 -*--.. Wa.Ilac 1400 DSA. P06AS205.DAT, 9/30/2016, page 3 Page 5703 of 5809 C-14 YELLOW **-**-**-*-*-----**---***----*--*------**--**-***----... --***-* ----*-***-* -**----*--------*-*-****-*-**---*-----*-_...,_ --*--**--****-*--*-*. ***-********** -****--........... --.. --*-*--**-----------*-.-*----*-****-**----****---Rack_position Count_Time(min) Quench_number 99
  • 7 70.00 633.53 / Counts Chem / Counts Beta Rack_posi ti on Count_ Time( min) Quench_number 99 8 70.00 633.00 15 JT / Counts 10 Chem l / Counts Beta 20 4'0 60 80 100 Rack_position Count_ Time( min) Quench_number 99 9 70.02 632.82 -,--I I / Cmuus IO *-1--___ ,, __ Chem \0 11 / Counls Bela 40 60 80 100 .,. Run_Date Cl4_CPM 12.35
  • 9/29/2016 10:02 AM Gross_B_CPM 12.80 Lumex_CPM 0.40 LUMEX 0.00 DPM 13.10 Cl4_CPM 12.34 Run_Date 9/29/2016 11:14 AM Gross_B_CPM LUMEX 12.80 0.00 Lumex_CPM DPM 0.50 13.90 C14_CPM 12.12 Run_Date 9/29/2016 12:25 PM Gross_B_CPM LUMEX 12.60 0.00 Lumex_CPM DPM 0.40 12.70 Wallac 1400 DSA, P06AS205.DAT, 9/30/2016, page 4 Page 5704 of 5809 C-14 YELLOW Rack_position Count_Time(min) Quench_number 99 10 70.00 631.33 15 -T.*r _j I . / 10 1 Conn ls 01001 5 0 0 20 Rack_position 99 11 15,,----, 5 20 Rack_position 99 12 / Counts Bet" 40 80 llJO Count._ Time(min) Quench_number 70.02 635.91 / Counts Chern / Connts Bein ' ULJ (.0 80 100 *Count_ Time( min) Quench_number 70.00 631.04 :i 0 0 20 40 '* ' **' / Counts 01cm / Count* Bein Cl4_CPM 12.55 Run_Date 9/29/2016 1:36 PM Gross_B_CPM LUMEX 12.90 0.00 Lumex_CPM DPM 0.40 13.70 Cl4_CPM 12.99 Run_Date 9/29/2016 2:47 PM Gross_B_CPM 13.40 Lumex_CPM 0.40 LUMEX 0.00 DPM 13.80 Cl4_CPM 13.24 Run_Date 9/29/2016 3:59 PM Gross_B_CPM 13.70 Lumex_CPM 0.50 LUMEX 0.00 DPM 14.80 Wallac 1400 DSA. P06AS205.DAT, 9/30/2016, page 5 Page 5705 of 5809 C-14 YELLOW -**-*---------.. -**--------------*--*--***--------*--**--*---***---------*-**-\S Rack_position Count_ Time(min) Quench_number () 1 70.00 628.-95 15 / Comirs IO* 01em / Counts Beta 40 riO BO 100 Rack_position Count_Time(min) Quench_number 0 2 70.00 629.96 / Counts Chem 6 / Counts Beta UJWJ I.LUI 'JlliJI. 20 40 .(l(J BO IOO Rack_position Count_Time(min) Quench_number 0 3 70.00 632.17 / Counts 5 '.lO -*--i------40 1 I 60 .. '* .i Chem / Counts Bein Cl4_CPM 13.02 Run_Date 9/29/2016 5:10 PM Gross_B_CPM LUMEX 13.40 0.00 Lumex_CPM DPM 0.40 15.00 Cl4_CPM 12.05 Run_Date 9/29/2016 6:21 PM Gross_B_CPM 12.60 Lumex_CPM 0.50 LUMEX 0.00 DPM 13.60 Cl4_CPM 12.36 Run_Date 9/29/2016 7:32 PM Gross_B_CPM 12.70 Lumex_CPM 0.30 LUMEX 0.00 DPM 13.90 --------------*****--***-**--*-----------.. -*---*-****-*** Wallac 1400 DSA, P06AS205.DAT, 9/30/2016, page 6 Page 5706 of 5809 C-14 YELLOW *--*--*-*-**----------*-*-*---**-------**--****--*-*-* .. *-*-***-*----------*--*---*----*-*.--*------*--***--***----------*--*-.... -*-**---*-*-**-**------*--*---------*-*-(\ Rack_position Count_Time(min) Quench_number 0 4 70.00 629.84 Rack_position 0 5 Rack_position 0 6 .J ** 1 .. , JJ UllllL 80 100 / Counts 01cm / Counts Beta Count_ Time(min) Quench_number 70.00 632.64 / Counts 01ein / Counts Bein Count_Time(min) Quench_number *70.00 629.90 / Comlls Chem / Counts Beta C14_CPM 12.82 Run_Date 9/2912010 8:44 PM Gross_B_CPM 13.30 Lumex_CPM 0.40 LUMEX 0.00 DPM 14.40 Cl4_CPM 12.82 Run_Date 9/2912016 9:55 PM Gross_B_CPM 13.30 Lumex_CPM 0.50 LUMEX 0.00 DPM 13.50 Cl4_CPM 12.97 Run_Date 9/29/2016 11:06 PM Gross_B_CPM LUMEX 13.30 0.00 Lumex_CPM DPM 0.30 14.30 Wallac 1400 DSA; P06AS205.DAT, 9/30/2016, page 7 Page 5707 of 5809 C-14 YELLOW Rack_position Count_ Time(min) Quench_number 0 7
  • 70.00 632.64 / Counts 01cm / Counts Dela Rack_position Count_Time(min) Quench_number 0 8 70.00 634.31 / Counls Chem / Counts Bela Count_Time(min) Quench_number 0 9 70.00 631.81 80'-.-----.----.--:::-, -A)! 60 1----l-*----/ Counts 01cm 40 / Counts Dctn u * ..A. ........ 20 100 Cl4_CPM 13.89 Run_Date 9/30/2016 -0:17 AM Gross_B_CPM 14.40 Lumex_CPM 0.50 LUMEX 0.00 DPM 15.00 Cl4_CPM 126.18 Run_Date 9/30/2016 1 :29 AM Gross_B_CPM LUMEX 126.60 0.00 Lumex_CPM DPM 0.40 161.60 Cl4_CPM 130.01 Run_Date 9/30/2016 2:40 AM Gross_B_CPM LUMEX 130.30 0.00 Lumex_CPM DPM 0.30 164.40 Wallac 1400 DSA, P06AS205.DAT, 9/30/2016, page 8 Page 5708 of 5809 Page 5709 of 5809 Continuing Calibration Data

.li Liquid Scintillation Counter Checks for 19-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 03:45 1.45 114334 -1.7 Carbon-14 03:47 1.4 115141 1.27 Tritium 03:49 1.35 161254 0.56 Tritium 03:50 1.35 160859 -0.32 BKG 03:52 30 26 -0.12 BKG 04:23 30 26 -0.29 LSCBROWN Carbon-14 03:27 1.4 115593 1.02 Carbon-14 03:29 1.4 115230 -0.25 Tritium 03:31 1.3 167287 -0.04 Tritium 03:33 1.3 167561 0.73 BKG 03:35 30 27 0.72 BKG 04:05 30 27 0.09 LSCGOLD Carbon-14 03:14 1.3 125555 -1.3 Carbon-14 03:16 1.3 125753 -0.74 Tritium 03:18 1.35 151637 1.18 Tritium 03:20 1.35 151895 1.76 BKG 03:22 30 24 2.48 BKG 03:52 30 23 1.21 LSCGREEN Carbon-14 03:28 1.4 114947 -0.87 Carbon-14 03:29 1.4 114820 -1.3 Tritium 03:32 ).25 173540 1.15 Tritium 03:33 1.25 172408 -1.3 BKG 03:35 30 27 0.46 BKG 04:06 30 25 -1.5 LSCORANGE Carbon-14 00:52 1.012433 107636 0.1 Tritium 00:56 1.012433 179933 0.58 BKG ' 01:28 30.01243 10 -1.3 Carbon-14 01:30 1.012433 107423 -0.51 Tritium 01:31 1.012333 179440 -0.64 BKG 02:01 30.01243 12 0.61 Page 5710 of 5809 LSCPINK Carbon-14 04:25 1.012433 119744 1.94 Tritium 04:28 1.012433 138218 0.66 BKG 05:01 30.01243 9.01 0.16 Carbon-14 05:02 119671 1.75 Tritium 05:04 1.012433 137937 0.08 BKG 05:34 30.01243 9.31 0.69 LSCRED Carbon-14 03:48 1.4 115290 1.3 Carbon-14 03:50 1.4 114472 -1.4 Tritium 03:52 1.3 16,4778 -0.94 Tritium 03:54 1.3 165587 0.86 BKG 03:56 30 27 1.34 BKG 04:26 30 27 1.04 LSCS,ILVER Carbon-14 03:18 1.35 121331 0.42 Carbon-14 03:19 1.35 121534 1.08 Tritium 03:21 1.25 170276 0.58 Tritium 03:23 1.25 170725 1.54 BKG 03:25 30 26 0.36 BKG 03:56 30 26 0.48 LSCTEAL Carbon-14 04:14 1.617 106499 1.6 Carbon-14 04:16 1.583 105776 -1.3 Tritium 04:19 1.217 145016 -1.1 Tritium 04:21 1.217 145361 -0.47 BKG 04:23 30 14 -0.75 BKG 04:54 30 15 -0.61 LSCYELLOW Carbon-14 03:33 1.483 114173 -0.74 Carbon-14 03:36 1.483 114451 0.17 Tritium 03:38 1.483 149477 -0.05 Tritium 03:40 1.483 149617 0.27 BKG 03:43 30 16 0.85 BKG 04:14 30 15 -0.23 Page 5711 of 5809 Reviewed by: Date: l 9-SEP-16 Lyndsey Pace .GEL Laboratories LLC Page 5712of5809 Li Liquid Scintillation Counter Checks for 20-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 02:22 1.4 115022 0.83 Carbon-14 02:23 1.4 114977 0.66 Tritium 02:26 1.35 161375 0.83 Tritium 02:27 1.35 161082 0.18 BKG 02:29 30 27 0.5 BKG 03:00 30 25 -0.96 LSCBROWN Carbon-14 03:08 1.4 115056 -0.85 Carbon-14 03:10 1.4 114978 -I.I Tritium 03:12 1.3 167546 0.68 Tritium 03:14 1.3 166833 -1.3 BKG 03:16 30 27 -0.01 BKG 03:46 30 27 -0.01 LSCGOLD Carbon-14 02:24 1.3 125533 -1.4 Carbon-14 02:25 1.3 126069 0.21 Tritium 02:27 1.35 150855 -0.54 Tritium 02:29 1.35 151136 0.08 BKG 02:31 30 23 0.48 BKG 03:02 30 22 -0.28 LSCGREEN Carbon-14 04:54 1.4 115524 1.12 Carbon-14 04:56 1.4 114743 -1.6 Tritium 04:58 1.25 172769 -0.49 Tritium 04:59 1.25 171985 -2.2 BKG 05:01 30 29 2.59 BKG 05:32 30 27 0.53 LSCORANGE Carbon-14 03:40 1.012433 108483 2.55 Tritium 03:43 1.012433 180246 1.35 BKG 04:16 ' 30.01243 9.78 -1.8 Carbon-14 04:17 1.012433 108001 1.16 Tritium 04:18 1.01235 179827 0.31 BKG 04:49 30.01243 11 -0.47 Page 5713 of 5809 LSCPINK Carbon-14 03:58 1.012433 119412 1.07 Tritium 04:01 1.012433 138148 0.52 BKG 04:34 30.01243 8.53 -0.69 Carbori,-14 04:35 1.012433 118707 -0.76 Tritium 04:37 1.012333 138085 0.39 BKG 05:07 30.01243 8.84 -0.14 LSCRED Carbon-14 03:23 1.4 114705 -0.65 Carbon-14 03:25 1.4 114932 0.11 Tritium 03:27 1.3 164582 -1.4 Tritium 03:28 1.3 165089 -0.25 BKG 03:31 30 26 0.16 BKG 04:01 30 26 -0.11 LSCSILVER Carbon-14 02:53 1.35 121094 -0.34 Carbon-14 02:55 1.35 120555 -2.1 Tritium 02:57 1.25 169537 -0.98 Tritium 02:59 1.25 169712 -0.61 BKG 03:01 30 26 0.21 BKG 03:31 30 26 0.64 LSCTEAL Carbon-14 03:50 1.617 106086 -0.06 Carbon-14 03:53 1.583 105622 -1.9 Tritium 03:55 1.217 144638 -1.9 Tritium 03:57 1.217 144505 -2.1 BKG 03:59 30 15 0.52 BKG 04:30 30 15 -0.32 LSCYELLOW Carbon-14 03:10 1.517 114246 -0.51 Carbon-14 03:13 1.467 114575 0.57 Tritium 03:15 1.483 149889 0.9 Tritium 03:18 1.483 149963 1.08 BKG 03:20 30 14 -1.3 BKG 03:51 30 16 . 1.22 Page 5714of5809 . . Reviewed by: Lyndsey Pace GEL Laboratories LLC Page 5715of5809 Date: 20-SEP-16 l..\ *t::iEIL Liquid Scintillation Counter Checks for 21-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 02:43 IA 115058 0.96 Carbon-14 02:44 1.4 114669 -0.49 Tritium 02:47 1.35 161307 0.68 Tritium 02:48 1.35 161425 0.95 BKG 02:50 30 26 -0.14 BKG 03:21 30 25 -0.72 LSCBROWN Carbon-14 03:13 1.4 114936 -1.3 Carbon-14 03:15 1.4 114765 -1.9 Tritium 03:17 1.3 166676 -1.7 Tritium 03:19 1.3 166849 -1.3 BKG 03:21 30 28 1.49 BKG 03:51 30 25 -1.3 LSCGOLD Carbon-14 02:58 1.3 125863 -0.41 Carbon-14 03:00 1.3 125511 -1.5 Tritium 03:02 1.35 151057 -0.1 Tritium 03:03 1.35 151270 0.38 BKG 03:05 30 23 1.13 BKG 03:36 30 20 -2.5 LSCGREEN Carbon-14 01:14 1.4 115237 0.13 Carbon-14 01:16 1.4 115132 -0.23 Tritium 01:18 1.25 172328 -1.4 Tritium 01:20 1.25 171870 -2.4 BKG 01:22 30 28 1.96 BKG 01:52 30 26 -0.57 LSCORANGE Carbon-14 01:32 1.01245 107464 -0.39 Tritium 01:35 1.012433 179632 -0.17 BKG 02:08 30.01243 11 0.1 Carbon-14 02:09 1.012433 107717 0.34 Tritium 02:11 1.01235 180069 0.91 BKG 02:41 30.01243 10 -1.2 Page 5716 of 5809 LSCPINK. Carbon-14 04:03 1.012433 118816 -0.48 Tritium 04:06 1.012433 137783 -0.25 BKG 04:39 30.01243 9.11 0.33 Carbon-14 04:40,. 1.012433 118422 -1.5 Tritium 04:42 1.012333 137656 -0.51 BKG 05:12 30.01243 8.94 O.o3 LSCRED Carbon-14 03:27 1.4 114866 -0.11 Carbon-14 03:28 1.4 114673 -0.76 Tritium 03:30 1.3 164972 -0.51 Tritium 03:32 1.3 165211 0.02 BKG 03:34 30 28 2 BKG 04:05 30 27 0.94 LSCSILVER Carbon-14 02:59 1.35 121455 0.82 Carbon-14 03:00 1.35 121168 -0.1 Tritium 03:02 1.25 170391 0.83 Tritium 03:04 1.25 168865 -2.4 BKG 03:06 30 25 -0.67 BKG 03:37 30 25 -0.86 LSCTEAL Carbon-14 03:56 1.617 105606 -2 Carbon-14 03:59 1.583 105739 -1.5 Tritium 04:01 1.217 144994 -1.2 Tritium 04:03 1.217 144459 -2.2 BKG 04:05 30 14 -0.89 BKG 04:36 30 15 0.1 LSCYELLOW Carbon-14 03:16 1.467 114999 1.96 Carbon-14 03:19 1.483 114319 -0.27 Tritium 03:21 1.483 150151 1.51 Tritium 03:24 1.483 149876 0.87 BKG 03:26 30 15 -0.35 BKG 03:57 30 15 -0.23 Page 5717 of 5809 Reviewed by: Date: 21-SEP-16 Lyndsey Pace GEL Laboratories LLC Page 5718of5809 &t Liquid Scintillation Counter Checks for 22-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 04:01 1.4 114872 0.27 Carbon-14 04:03 1.4 114794 -0.02 Tritium 04:05 1.35 161567 1.26 Tritium 04:07 1.35 160846 -0.34 BKG 04:09 30 26 -0.31 BKG 04:39 30 25 -0.6 LSCBROWN Carbon-14 03:04 1.4 115281 -0.07 Carbon-14 03:06 1.4 115272 -0.1 Tritium 03:08 1.3 167601 0.84 Tritium 03:09 1.3 167450 0.42 BKG 03:11 30 27 0.69 BKG 03:42 30 28 1.39 LSCGOLD Carbon-14 02:57 1.3 125041 -2.9 Carbon-14 02:59 1.3 125422 -1.7 Tritium 03:01 1.35 151877 1.71 Tritium 03:02 1.35 151445 0.76 BKG 03:04 30 22 -0.28 BKG 03:35 30 23 0.77 LSCGREEN Carbon-14 01:27 1.4 115497 1.02 Carbon-14 01:29 1.4 115264 0.22 Tritium 01:31 1.25 172310 -1.5 Tritium 01:33 1.25 171978 -2.2 BKG 01:35 30 26 -0.02 BKG 02:05 30 28 2.12 LSCORANGE Carbon-14 03:32 1.01245 107833 0.67 Tritium 03:35 1.012433 179335 -0.9 BKG 04:08 30.01243 11 -0.77 Carbon-14 04:09 1.012433 107477 -0.36 Tritium 04:10 1.012433 179458 -0.6 BKG 04:41 30.01243 11 0.47 Page 5719of5809 LSCPINK Carbon-14 03:52 1.012433 119501 1.31 Tritium 03:55 1.012433 138282 0.8 BKG 04:28 30.01243 8.3 -1.1 Carbon-14 04:29 1.012433 119031 0.08 Tritium 04:31 1.01235 138426 1.1 BKG 05:01 30.01243 9.58 1.17 LSCRED Carbon-14 03:25 1.4 115277 1.26 Carbon-14 03:27 1.4 114629 -0.91 Tritium 03:29 1.3 165161 -0.09 Tritium 03:31 1.3 164848 -0.79 BKG 03:33 30 28 2.42 BKG 04:03 30 25 -0.56 LSCSILVER Carbon-14 01:13 1.35 121680 1.55 Carbon-14 01:14 1.35 121441 0.78 Tritium 01:16 1.25 170008 0.02 Tritium 01:18 1.25 169523 -1 BKG 01:20 30 26 0.09 BKG 01:51 30 26 0.51 LSCTEAL Carbon-14 01:13 1.6 105369 -2.9 Carbon-14 01:16 1.583 105803 -1.2 Tritium 01:18 1.217 144923 -1.3 Tritium 01:20 1.217 145264 -0.65 BKG 01:22 30 14 -1.2 BKG 01:53 30 14 -1.2 LSCYELLOW Carbon-14 02:58 1.467 114697 0.97 Carbon-14 03:00 1.467 114804 1.32 Tritium 03:03 1.483 149146 -0.82 Tritium 03:05 1.483 149246 -0.59 BKG 03:07 30 16 0.37. BKG 03:38 30 15 0.25 Page 5720 of 5809 if Reviewed by: Lyndsey Pace GEL Laboratories LLC Page 5721of5809 Date: 22-SEP-16 i!JIEIL Liquid Scintillation Counter Checks for 23-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 03:30 1.4 114373 -1.6 Carbon-14 03:31 1.4 114742 -0.22 Tritium 03:33 1.35 160868 -0.3 Tritium 03:35 1.35 161438 0.97 BKG 03:37 30 25 -0.76 BKG 04:08 30 27 0.17 LSCBROWN Carbon-14 03:17 1.4 115344 0.15 Carbon-14 03:19 1.4 114799 -1.8 Tritium 03:21 1.3 167822 1.45 Tritium 03:23 1.3 167302 0.01 BKG 03:25 30 27 -0.01 BKG 03:55 30 27 0.57 LSCGOLD Carbon-14 03:00 1.3 125892 -0.33 Carbon-14 03:02 1.3 125732 -0.81 Tritium 03:04 1.35 150953 -0.33 Tritium 03:05 1.35 151123 0.05 BKG 03:07 30 22 -0.1 BKG 03:38 30 23 1.02 LS CG REEN Carbon-14 03:58 1.4 115028 -0.59 Carbon-14 04:00 1.4 115348 0.51 Tritium 04:02 1.25 172582 -0.89 Tritium 04:03 1.25 172525 -1 BKG 04:05 30 25 -1.1 BKG 04:36 30 27 0.83 LSCORANGE Carbon-14 01:25 1.012433 107658 0.17 Tritium 01:29 1.012433 179167 -1.3 BKG 02:01 30.01243 10 -1.2 Carbon-14 02:03 1.012433 107861 0.75 Tritium 02:04 1.012333 179401 -0.74 BKG 02:34 30.01243 11 -0.06 Page 5722 of 5809 LSCPINK Carbon-14 03:49 1.012433 118374 -1.6 Tritium 03:53 1.012433 137033 -1.8 BKG 04:25 30.01243 9.01 0.16 04:27 1.012433 119327 0.85 Tritium 04:28 1.012333 138564 1.39 BKG 04:58 30.01243 8.94 O.o3 LSCRED Carbon-14 03:29 1.4 114914 0.05 Carbon-14 03:30 1.4 114470 -1.4 Tritium 03:32 1.3 164978 -0.5 Tritium 03:34 1.3 164353 -1.9 BKG 03:36 30 26 0.62 BKG 04:07 30 28 1.66 LSCSILVER Carbon-14 03:01 1.35 121112 -0.28 Carbon-14 03:03 1.35 121337 0.44 Tritium 03:05 1.25 169232 -1.6 Tritium 03:06 1.25 169592 -0.86 BKG 03:09 30 26 0 BKG 03:39 30 26 0.03 LSCTEAL Carbon-14 03:58 1.583 106191 0.37 Carbon-14 04:01 1.583 106019 -0.32 Tritium 04:03 1.217 145387 -0.42 Tritium 04:05 1.217 144376 -2.4 BKG 04:08 30 15 -0.04 BKG 04:38 30 13 -2.2 LSCYELLOW Carbon-14 03:18 1.483 114452 0.17 Carbon-14 03:20 1.483 114216 -0.6 Tritium 03:23 1.483 149493 -0.02 Tritium 03:25 1.483 149237 -0.61 BKG 03:28 30.017 14 -1.8 BKG 03:58 30 15 -0.83 Page 5723 of 5809 Reviewed by: Date: 23-SEP-16 Lyndsey Pace GEL Laboratories LLC. Page 5724 of 5809

  • tl!Zl.L. Liquid Scintillation Counter Checks for 24-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time .. LSCBLUE Carbon-14 02:01 1.4 114891 0.34 Carbon-14 02:03 1.4 114675 -0.47 Tritium 02:05 1.35 161211 0.47 Tritium 02:07 1.35 162025 2.28 BKG 02:09 30 25 -0.66 BKG 02:39 30 26 -0.14 LSCBROWN Carbon-14 00:55 1.4 115175 -0.44 Carbon-14 00:57 1.4 115269 -0.11 Tritium 00:59 1.3 167266 -0.09 Tritium 01:01 1.3 167305 0.01 BKG 01:03 30 27 0.69 BKG 01:33 30 26 -0.34 LSCGOLD Carbon-14 00:38 1.3 125545 -1.4 Carbon-14 00:39 1.3 125999 -00 Tritium 00:41 1.35 151026 -0.16 Tritium 00:43 1.35 151579 1.06 BKG 00:45 30 23 0.85 BKG 01:16 30 21 "1 LSCGREEN Carbon-14 03:16 1.4 115096 -0.36 Carbon-14 03:18 1.4 115069 -0.45 Tritium 03:20 1.25 172241 -1.6 Tritium 03:21 1.25 172168 -1.8 BKG 03:23 30 28 1.68 BKG 03:54 30 25 -1.1 LSCORANGE Carbon-14 03:43 1.01245 107778 0.51 Tritium 03:46 1.012433 179830 0.32 BKG. 04:19 30.01243 12 1.32 Carbon-14 04:20 1.012433 107941 0.99 Tritium 04:22 1.01235 179155 -1.3 BKG 04:52 30.01243 10 -1.3 Page 5725 of 5809 LSCPINK Carbon-14 04:07 1.012433 119155 0.4 Tritium 04:10 1.012433 138210 0.65 BKG 04:43 30.01243 9.38 0.81 Carbon-14 04:44 1.012433 118932 .-0.18 Tritium 04:46 1.012333 137462 -0.92 BKG 05:16 30.01243 9.78 1.52 LSCRED Carbon-14 03:29 1.4 115119 0.73 Carbon-14 03:31 1.4 114742 -0.53 Tritium 03:33 1.3 165161 -0.09 Tritium 03:34 1.3 164649 -1.2 BKG 03:36 30 26 0.29 BKG 04:07 30 27 0.78 LSCSILVER Carbon-14 02:04 1.35 120756 -1.4 Carbon-14 02:05 1.35 121411 0.68 Tritium 02:07 1.25 169787 -0.45 Tritium 02:09 1.25 169016 -2.1 BKG 02:11 30 27 1.58 BKG 02:41 30 24 -1.3 LSCTEAL Carbon-14 02:41 1.583 106006 -0.38 Carbon-14 02:43 1.583 105712 -1.6 Tritium 02:46 1.217 144115 -2.9 Tritium 02:48 1.217 144196 -2.7 BKG 02:50 30 14 -1.2 BKG 03:21 30 16 1.65 LSCYELLOW Carbon-14 01:17 1.483 114491 0.3 Carbon-14 01:20 1.483 113911 -1.6 Tritium 01:22 1.5 148410 -2.5 Tritium 01:24 1.5 148822 -1.6 BKG 01:27 30 14 -2 BKG 01:58 30 14 -1.7 Page 5726 of 5809 Reviewed by: Lyndsey Pace GEL Laboratories LLC Page 5727 of 5809 Date: 25-SEP-16 4 G!Ell... Liquid Scintillation Counter Checks for 25-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 05:19 1.4 114997 0.73 Carbon-14 05:21 1.4 114783 -0.06 Tritium 05:23 1.35 160646 -0.79 Tritium 05:25 1.35 160956 -0.1 BKG 05:27 30 24 -1.2 BKG 05:57 30 23 -1.8 LSCBROWN Carbon-14 05:33 1.4 115064 -0.83 Carbon-14 05:35 1.4 114456 -3 Tritium 05:37 1.3 167494 0.54 Tritium 05:39 1.3 166971 -0.92 BKG 05:41 30 27 0.18 BKG 06:11 30 26 -0.72 LSCGOLD Carbon-14 04:56 1.3 125590 -1.2 Carbon-14 04:58 1.3 125659 -I Tritium 05:00 1.35 151037 -0.14 Tritium 05:01 1.35 151983 1.95 BKG 05:03 30 23 0.74 BKG 05:34 30 22 -0.39 LSCGREEN Carbon-14 05:30 1.4 115286 0.3 Carbon-14 05:32 1.4 115610 1.42 Tritium 05:34 1.25 173063 0.13 Tritium 05:35 1.25 171971 -2.2 BKG 05:37 30 26 -0.39 BKG 06:08 30 28 2.18 LSCORANGE Carbon-14 05:34 1.012433 107676 0.22 Tritium 05:37 1.012433 179256 -I.I BKG 06:10 30.01243 9.99. -1.5 Carbon-14 06:11 1.012433 107554 -0.13 Tritium 06:12 1.012333 179482 -0.54 BKG 06:43 30.01243 11 -0.43 Page 5728 of 5809 LSCPINK Carbon-14 05:52 1.012433 118719 -0.73 Tritium 05:55 1.012433 138659 1.59 BKG 06:28 30.01243 8.4 -0.92
  • Carbon-14 06:29 1.012433 118066 -2.4 Tritium 06:31 1.012433 138493 1.24 BKG 07:01 30.01243 9.17 0.44 LSCRED Carbon-14 05:20 1.4 114798 -0.34 Carbon-14 05:21 1.45 114118 -2.6 Tritium 05:23 1.3 164887 -0.7 Tritium 05:25 1.3 164537 -1.5 BKG 05:27 30 26 0.52 BKG 05:58 30 26 0.58 LSCSILVER Carbon-14 04:57 1.35 121004 -0.63 Carbon-14 04:59 1.35 121316 0.37 Tritium 05:01 1.25 169407 -1.3 Tritium 05:02 1.25 169802 -0.42 BKG 05:05 30 26 0.48 BKG 05:35 30 24 -I.I LSCTEAL Carbon-14 05:45 1.583 106015 -0.34 Carbon-14 05:48 1.583 106322 0.89 Tritium 05:50 1.217 145301 -0.58 Tritium 05:52 1.217 144564 -2 BKG 05:54 30 15 0.1 BKG 06:25 30 15 -0.61 LSCYELLOW Carbon-14 05:09 1.483 114166 -0.77 Carbon-14 05:11 1.483 114276 -0.41 Tritium 05:14 1.483 149487 -0.03 Tritium 05:16 1.483 149641 0.33 BKG 05:19 30 15 0.01 BKG 05:49 30 14 -1.2 Page 5729 of 5809 Reviewed by: Lyndsey Pace GEL Laborator.ies LLC Page 5730 of 5809 Date: 25-SEP-16 Gll:IL Liquid Scintillation Counter Checks for 26-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 03:54 1.4 114664 -0.51 Carbon-14 03:56 1.4 114711 -0.33 Tritium 03:58 1.35 161404 0.9 Tritium 03:59 1.35 160997 -0.01 BKG 04:02 30 26 -0.5 BKG 04:32 30 24 -1.7 LSCBROWN Carbon-14 03:37 1.4 114587 -2.5 Carbon-14 03:39 1.4 115476 0.62 Tritium 03:41 1.3 167431 0.37 Tritium 03:42 1.3 166820 -1.3 BKG 03:45 30 26 -0.14 BKG 04:15 30 26 -0.65 LSCGOLD Carbon-14 03:24 1.3 126048 0.14 Carbon-14 03:26 1.3 126189 0.57 Tritium 03:28 1.35 151447 0.77 Tritium 03:29 1.35 151436 0.74 BKG 03:31 30 22 -0.02 BKG 04:02 30 23 0.99 LS CG REEN Carbon-14 03:37 1.4 115047 -0.53 Carbon-14 03:39 1.4 115072 -0.44 Tritium 03:41 1.25 172190 -1.7 Tritium 03:42 1.25 171975 -2.2 BKG 03:45 30 26 0.09 BKG 04:15 30 27 1.01 LSCORANGE Carbon-14 04:14 1.012433 107821 0.64 Tritium 04:17 1.012433 179032 -1.6 BKG 04:50 30.01243 11 -0.57 Carbon-14 04:51 1.012433 107110 -1.4 Tritium 04:53 1.012333 179952 0.62 BKG 05:23 30.01243 11 0.51 Page 5731 of 5809 LSCPINK Carbon-14 04:35 1.012433 118962 -0.1 Tritium 04:38 1.012433 138535 1.33 BKG 05:11 30.01243 9.38 0.81 Carbon-14 05:12 1.012433 119208 0.54 Tritium 05:14 1.01235 138696 1.67 BKG 05:44 30.01243 7.86 -1.9 LSCRED Carbon-14 03:58 1.4 115192 0.98 Carbon-14 03:59 1.4 114565 -1.1 Tritium 04:01 1.3 164605 -1.3 Tritium 04:03 1.3 164629 -1.3 BKG 04:05 30 25 -0.4 BKG 04:36 30 27 0.85 LSCSILVER Carbon-14 03:27 1.35 121193 -0.02 Carbon-14 03:29 1.35 120776 -1.4 Tritium 03:31 1.25 169374 -1.3 Tritium 03:33 1.25 169519 -1 BKG 03:35 30 27 0.87 BKG 04:05 30 27 0.76 LSCTEAL Carbon-14 04:24 1.583 105975 -0.5 Carbon-14 04:26 i.583 105930 -0.68 Tritium 04:29 1.217 145129 -0.92 Tritium 04:31 1.2 145923 0.63 BKG 04:33 30 16 1.51 BKG 05:04 30 15 0.24 LSCYELLOW Carbon-14 03:43 1.483 114030 -1.2 Carbon-14 03:46 1.483 114473 0.24 Tritium 03:48 1.483 149496 -0.01 Tritium 03:51 1.483 149146 -0.82 BKG 03:53 30 14 -0.95 BKG 04:24 30 15 -0.59 Page 5732 of 5809 Reviewed by: Date: 26-SEP-16 Lyndsey Pace GEL Laboratories LLC Page 5733 of 5809 GIEIJ.., Liquid Scintillation Counter Checks for 27-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 04:42 1.4 114741 -0.22 Carbon-14 04:43 1.4 114681 -0.45 Tritium 04:45 1.35 161264 0.59 Tritium 04:47 1.35 160845 -0.35 BKG 04:49 30 25 -0.77 BKG 05:20 30 25 -0.68 LSCBROWN Carbon-14 00:55 1.4 114679 -2.2 Carbon-14 00:57 1.4 114982 -I.I Tritium 00:59 1.3 167151 -0.42 Tritium 01:01 1.3 167469 0.47 BKG 01:03 30 27 0.69 BKG 01:33 30 25 -1.5 LSCGOLD Carbon-14 02:58 1.3 126462 1.39 Carbon-14 03:00 1.3 125826 -0.52 Tritium 03:02 1.35 150691 -0.9 Tritium 03:03 1.35 151249 0.33 BKG 03:05 30 22 0.3 BKG 03:36 30 23 0.88 LSCGREEN Carbon-14 02:03 1.4 115229 0.1 Carbon-14 02:05 1.4 114521 -2.3 Tritium 02:07 1.25 172325 -1.4 Tritium 02:09 1.25 172659 -0.73 BKG 02:11 30 27 0.9 BKG 02:41 30 27 1.41 LSCORANGE Carbon-14 02:44 1.012433 107710 0.32 Tritium 02:48 1.012433 178996 -1.7 BKG 03:20 30.01243 11 -0.29 Carbon-14 03:22 1.012433 107395 -0.59 Tritium 03:23 1.012433 179324 -0.93 BKG 03:53 30.01243 11 0.24 Page 5734 of 5809 LSCPINK Carbon-14 02:33 1.012433 118221 -2 Tritium 02:36 1.012433 138042 0.3 BKG 03:09 30.01243 9.01 0.16 Carbon-14 03:10 1.012433 119488 q1 Tritium 03:11 1.012417 138168 0.56 BKG 03:42 30.01243 9.01 0.16 LSCRED Carbon-14 01:50 1.4 115263 1.21
  • Carbon-14 01:52 1.4 114979 0.27 Tritium 01:54 1.3 164824 -0.84 Tritium 01:55 1.3 164771 -0.96 BKG 01:58 30 26 0.13 BKG 02:28 30 26 -0.24 LSCSILVER Carbon-14 02:58 1.35 120884 -1 Carbon-14 03:00 1.35 121886 2.21 Tritium 03:02 1.25 169186 -1.7 Tritium 03:04 1.25 169493 -1.1 BKG 03:06 30 24 -1.7 BKG 03:36 30 25 -1.1 LSCTEAL Carbon-14 03:57 1.583 105907 -0.78 Carbon-14 03:59 1.583 105667 -1.7 Tritium 04:02 1.217 145199 -0.78 Tritium 04:04 1.217 145483 -0.23 BKG 04:06 30 16 1.79 BKG 04:37 30 15 0.24 LSCYELLOW Carbon-14 00:08 1.483 114093 -1 Carbon-14 00:11 1.467 114523 0.4 Tritium 00:13 1.483 149436 -0.15 Tritium 00:15 1.483 149889 0.9 BKG 00:18 30 14 -1.6 BKG 00:49 30 16 0.49 Carbon-14 03:17 1.483 114114 -0.94 Carbon-14 03:20 1.483 114040 -1.2 Tritium 03:22 1.5 149018 -I.I Tritium 03:25 1.5 149063 -1 Page 5735 of 5809 BKG BKG Reviewed by: 03:27 03:58 Lyndsey Pace GEL Laboratories LLC Page 5736 of 5809 30 30 14 15 -0.95 -0.47 Date: 27-SEP-16
  • LJIEIL Liquid Scintillation Counter Checks for 28-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments LSCBLUE Carbon-14 01:48 1.4 115521 2.69 Carbon-14 01:49 1.4 114439 -1.3 Tritium 01:51 1.35 161162 0.36 Tritium 01:53 1.35 161914 2.03 BKG 01:55 30 27 0.09 BKG 02:26 30 26 -0.45 LSCBROWN Carbon-14 03:22 1.4 114977 -1.1 Carbon-14 03:23 1.4 114752 -1.9 Tritium 03:25 1.3 167219 -0.23 Tritium 03:27 1.3 167102 -0.55 BKG 03:29 30 27 0.12 BKG 04:00 30 26 -0.91 LSCGOLD Carbon-14 03:05 1.3 125416 -1.8 Carbon-14 03:07 1.3 125584 -1.3 Tritium 03:09 1.4 150452 -1.4 Tritium 03:11 1.35 150922 -0.39 BKG 03:13 30 24 1.57 BKG 03:43 30 23 1.21 LS CG REEN Carbon-14 02:37 1.4 115346 0.5 Carbon-14 02:39 1.4 115265 0.22 Tritium 02:41 1.25 172643 -0.76 Tritium 02:43 1.25 173588 1.25 BKG 02:45 30 27 1.46 BKG 03:15 30 26 0.28 LSCORANGE Carbon-14 01:05 1.01245 108762 3.36 Outside Three Sigma Tritium 01:09 1.012433 179550 -0.37 BKG 01:41 30.01243 11 ' 0.33 Carbon-14 01:42 1.012433 107260 -0.98 Tritium 01:44 1.01235 179063 -1.6 BKG 02:14 30.01243 12 1.04 Page 5737 of 5809 Carbon-14 05:49 1.012433 107209 -I.I Tritium 05:52 1.012433 179463 -0.59 BKG 06:25 30.01243 12 1.61 Carbon-14 06:26 1.012433. 107590 -0.03 Tritium 06:27 1.012333 179422 -0.69 BKG 06:58 30.01243 13 2.13 LSCPINK Carbon-14 04:07 1.012433 118824 -0.46 Tritium 04:10 1.012433 137837 -0.13 BKG 04:43 30.01243 9.11 0.33 Carbon-14 04:44 1.012433 119359 0.94 Tritium 04:46 1.012333 137374 -I.I BKG 05:16 30.01243 9.78 1.52 LSCRED Carbon-14 03:34 1.4 114564 -I.I Carbon-14 03:36 1.4 114909 O.D3 Tritium 03:38 1.3 164730 -1 Tritium 03:40 1.3 164358 -1.9 BKG 03:42 30 27 1.5 BKG 04:12 30 26 -0.17 LSCSILVER Carbon-14 00:24 1.35 121336 0.44 Carbon-14 00:26 1.35 121211 0.04 Tritium 00:28 1.25 170645 1.37 Tritium 00:29 1.25 170205 0.43 BKG 00:32 30 27 0.78 BKG 01:02 30 26 0.42 LSCTEAL Carbon-14 04:03 1.617 106220 0.48 Carbon-14 04:05 1.583 106078 -O.D9 Tritium 04:08 1.217 145076 -1 Tritium 04:10 1.217 144818 -1.5 BKG 04:12 30 14 -0.89 BKG 04:43 30 15 -0.47 LSC.YELLOW Carbon-14 01:56 1.483 114479 0)6 Carbon-14 01:58 1.483 114349 -0.17 Tritium 02:01 1.483 149679 0.42 Tritium 02:03 1.5 149021 -I.I Page 5738of5809 BKG BKG 02:05 02:36 LSCORANGE: CLEARED BY RERUN Reviewed by: Lyndsey Pace GEL Laboratories LLC Page 5739 of 5809 30 30.017 14 14 -1.6 -1.2 Date: 28-SEP-16 GiEU., Liquid Scintillation Counter Checks for 29-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 01:05 1.4 114675 -0.47 Carbon-14 01:07 1.4 115000 0.74 Tritium 01:09 1.35 161467 1.04 Tritium 01:11 1.35 161527 1.17 BKG 01:13 30 25 -0.62 BKG 01:43 30 25 -0.89 LSCBROWN Carbon-14 03:27 1.4 115077 -0.78 Carbon-14 03:29 1.4 115354 0.19 Tritium 03:31 1.3 167493 0.54 Tritium 03:33 1.3 167278 -0.06 BKG 03:35 30 26 -0.62 BKG 04:05 30 27 -0.05 LSCGOLD Carbon-14 01:09 1.3 125794 -0.62 Carbon-14 01:11 1.3 126371 1.12 Tritium 01:13 1.35 151686 1.29 Tritium 01:15 1.35 151709 1.34 BKG 01:17 30 20 -1.9 BKG 01:47 30 23 1.24 LSCGREEN Carbon-14 00:12 1.4 115064 -0.47 Carbon-14 00:14 1.4 115266 0.23 Tritium 00:16 1.25 172346 -1.4 Tritium 00:17 1.25 172474 -1.1 BKG 00:19 30 25 -0.75 BKG 00:50 30 25 -1.2 LSCORANGE Carbon-14 01:49 1.012433 107533 -0.19 Tritium 01:53 1.012433 179410 -0.72 BKG 02:25 30.01243 II 0.1 Carbon-14 02:27 1.012433 107033 -1.6 Tritium 02:28 1.012333 179407 -0.72 BKG 02:59 30.01243 IO -0.95 Page 5740 of 5809 LSCPINK. Carbon-14 04:04 1.012433 119416 1.08 Tritium 04:07 1.012433 138232 0.69 BKG 04:40 30.01243 8.63 -0.52 ... Carbon-14 04:11 1.012433 I L8959 -0.11 Tritium 04:43 1.012333 137835 -0.14 BKG 05:13 30.01243 8.2 -1.3 LSCRED Carbon-14 02:42 1.4 114621 -0.93 Carbon-14 02:44 1.4 114804 -0.32 Tritium 02:46 1.3 164596 -1.4 Tritium 02:47 1.3 163365 -4.I Outside Three Sigma BKG 02:49 30 27 0.91 BKG 03:20 30 24 -1.7 Tritium 05:33 1.3 164580 -1.4 Tritium 05:35 1.3 164361 -1.9 LSCSILVER Carbon-14 01:56 1.35 121466 0.86 Carbon-14 01:58 1.35 121206 0.02 Tritium 02:00 1.25 169653 -0.74 Tritium 02:02 1.25 170069 0.15 BKG 02:04 30 26 0.39 BKG 02:35 30 24 -I.I LSCTEAL Carbon-14 03:58 1.617 105537 -2.3 Carbon-14 04:01 1.583 106267 0.67 Tritium 04:03 1.217 145391 -0.41 Tritium 04:05 1.217 145006 -1.2 BKG 04:07 30 15 0.24 BKG 04:38 30 16 0.94 LSCYELLOW Carbon-14 01:43 1.483 113779 -2 Carbon-14 01:45 1.483 114107 -0.96 Tritium 01:48 1.483 149297 -0.47 Tritium 01:50 1.5 149094 -0.94 01:52 30 15 -0.83 BKG 02:23 30 16 0.49 LSCRED: CLEARED BY RERUN Page 5741 of 5809

. Reviewed by: Date: 29-SEP-16 Lyndsey Pace GEL Laboratories LLC Page 5742 of 5809 Liquid Scintillation Counter Checks for 30-SEP-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 01:43 1.4 114746 -0.2 Carbon-14 01:45 1.4 115430 2.35 Tritium 01:47 1.35 160996 -0.01 Tritium 01:49 1.35 160389 -1.4 BKG 01:51 30 26 -0.14 BKG 02:21 30 26 -0.31 LSCBROWN Carbon-14 00:40 1.4 115167 -0.47 Carbon-14 00:42 1.4 115035 -0.93 Tritium 00:44 1.3 168127 2.3 Tritium 00:46 1.3 166997 -0.85 BKG 00:48 30 26 -0.78 BKG 01:18 30 25 -1.2 LSCGOLD Carbon-14 02:57 1.3 125788 -0.64 Carbon-14 02:59 1.3 125887 -0.34 Tritium 03:01 1.4 150680 -0.93 Tritium 03:02 1.35 151080 -0.05 BKG 03:05 30 23 0.85 BKG 03:35 30 22 0.3 LS CG REEN Carbon-14 00:40 1.4 115004 -0.68 Carbon-14 00:42 1.4 114486 -2.5 Tritium 00:44 1.25 172720 -0.6 Tritium 00:46 1.25 172738 -0.56 BKG 00:48 30 25 -1.4 BKG 01:18 30 26 -0.24 LSCORANGE Carbon-14 03:19 1.01245 107974 1.08 Tritium 03:23 1.012433 180655 2.36 BKG 03:55 30.01243 12 0.75 Carbon-14 03:57 1.012433 107589 -0.03 Tritium 03:58 1.01235 180022 0.8 BKG 04:29 30.01243 II 0.47 Page 5743 of 5809 LSCPINK Carbon-14 04:02 1.012433 119240 0.63 Tritium 04:05 1.012433 136976 -1.9 BKG 04:38 30.01243 8.26 -1.2 Carbon-14 04:39 1.012433 119567 1.48 Tritium 04:41 1.012333 137395 -1.1 BKG 05:11 30.01243 7.72 -2.1 LSCRED Carbon-14 03:13 1.4 114989 0.3 Carbon-14 03:15 1.4 115029 0.43 Tritium 03:17 1.3 164164 -2.3 Tritium 03:19 1.3 164597 -1.3 BKG 03:21 30 25 -0.73 BKG 03:51 30 27 0.97 LSCSILVER Carbon-14 01:39 1.35 121403 0.65 Carbon-14 01:41 1.35 121309 0.35 Tritium 01:43 1.25 169717 -0.6 Tritium 01:45 1.25 169402 -1.3 BKG 01:47 30 25 -0.27 BKG 02:17 30 26 0.24 LSCTEAL Carbon-14 01:37 1.583 105852 -01 Carbon-14 01:40 1.583 106162 0.25 Tritium 01:43 1.217 144338 -2.5 Tritium 01:45 1.217 144655 -1.8 BKG 01:47 30 15 -0.32 BKG 02:18 30 16 2.07 LSCYELLOW Carbon-14 03:52 1.483 114303 -0.32 Carbon-14 03:54 1.483 114156 -0.8 Tritium 03:56 1.483 149572 0.17 Tritium 03:59 1.483 149558 0.14 BKG 04:01 30 16 1.1 BKG 04:32 30 16 1.34 Page 5744 of 5809 Reviewed by: Date: 30-SEP-16 Lyndsey Pace GEL Laboratories LLC Page 5745 of 5809 Liquid Scintillation Counter Checks for 0l-OCT-2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments

  • Time LSCBLUE Carbon-14 03:27 1.4 115213 1.54 Carbon-14 03:29 1.4 114582 -0.81 Tritium 03:31 1.35 161421 0.94 Tritium 03:33 1.35 160717 -0.63 BKG 03:35 30 25 -0.68 BKG 04:05 30 25 -0.73 LSCBROWN Carbon-14 03:29 1.4 115046 -0.89 Carbon-14 03:31 1.4 114946 -1.2 Tritium 03:33 1.3 167819 1.45 Tritium 03:34 1.3 166906 -I.I BKG 03:36 30 27 0.57 BKG 04:07 30 27 0.05 LSCGOLD Carbon-14 02:16 1.3 125710 -0.87 Carbon-14 02:17 1.3 125748 -0.76 Tritium 02:19 1.35 151942 1.86 Tritium 02:21 1.35 151575 1.05 BKG 02:23 30 22 -0.46 BKG 02:54 30 23 0.41 LSCGREEN Carbon-14 06:03 1.4 114624 -2 Carbon-14 06:04 1.4 114382 -2.8 Tritium 06:06 1.25 172579 -0.9 Tritium 06:08 1.25 172632 -0.78 BKG 06:10 30 27 0.72 BKG 06:40 30 27 1.05 LSCORANGE Carbon-14 04:06 1.01245 107866 0.77 Tritium 04:09 1.012433 180610 2.25 BKG 04:42 30.01243 12 1.42 Carbon-14 04:43 1.012433 107556 -0.13 Tritium 04:45 1.01235 179803 0.25 BKG 05:15 30.01243 10 -1 Page 5746 of 5809 LSCPINK Carbon-14 00:54 1.012433 118820 -0.47 Tritium 00:58 1.012433 137908 0.02 BKG 01:30 30.01243 8.2 -1.3 Carbon-14 01:32 ,1.012433 118892 -0.28 Tritium 01:33 1.012333 138217 0.66 BKG 02:04 30.01243 9.28 0.64 LSCRED Carbon-14 01:48 1.4 115040 0.47 Carbon-14 01:50 1.4 114366 -1.8 Tritium 01:52 1.3 164638 -1.3 Tritium 01:53 1.3 164544 -1.5 BKG 01:55 30 26 -0.21 BKG 02:26 30 26 0.45 LSCSILVER Carbon-14 05:19 1.35 121262 0.2 Carbon-14 05:56 1.35 121504 0.98 Tritium 05:58 1.25 169543 -0.97 Tritium 05:59 1.25 169883 -0.25 BKG 06:01 30 26 0.42 BKG 06:32 30 27 0.76 LSCTEAL Carbon-14 05:06 1.583 106001 -0.4 Carbon-14 05:09 1.583 105761 -1.4 Tritium 05:11 1.217 144704 -1.7 Tritium 05:13 1.217 143979 -3.2 Outside Three Sigma BKG 05:16 30 15 0.66 BKG 05:46 30 15 -0.47 Tritium 06:51 1.233 143776 -3.6 Outside Three Sigma Tritium 06:53 1.217 144545 -2.1 Tritium 08:45 1.233 143817 -3.5 Outside Three Sigma Tritium 08:47 1.233 143879 -3.4 Outside Three Sigma Tritium 12:11 1.25 144389 -2.4 Tritium 12:13 1.217 144312 -2.5 Tritium 12:17 1.217 144270 -2.6 Tritium 12:19 1.25 144568 -2 LSCYELLOW Carbon-14 03:19 1.483 114321 -0.26 Carbon-14 03:21 1.483 114205 -0.64 Page 5747 of 5809

. . Tritium Tritium BKG BKG 03:24 03:26 03:29 .03:59 LSCTEAL: CLEARED BY RERUN Reviewed by: Lyndsey Pace GEL Laboratories LLC Page 5748 of 5809 1.483 1.483 30 30 149799 0.7 149999 1.16 15 -0.83 15 -0.47 Date: 03-0CT-16 Liquid Scintillation Counter Checks for 03-0CT -2016 Short Name Parmname Run Time Count Counts CPM Stdev Status Comments Time LSCBLUE Carbon-14 03:32 1.4 115093 1.09 Carbon-14 03:34 1.4 114894 0.35 Tritium 03:36 1.35 160863 -0.3 Tritium 03:37 1.35 162173 2.61 BKG 03:40 30 25 -0.79 BKG 04:10 30 25 -1.1 LSCBROWN Carbon-14 03:15 1.4 114578 -2.5 Carbon-14 03:16 1.4 114931 -1.3 Tritium 03:18 1.3 166870 -1.2 Tritium 03:20 1.3 167135 -0.46 BKG 03:22 30 25 -1.5 BKG 03:53 30 26 -0.3 LSCGOLD Carbon-14 03:02 1.3 125906 -0.28 Carbon-14 03:03 1.3 126051 0.15 Tritium 03:05 1.35 151102 0.01 Tritium 03:07 1.35 150900 -0.44 BKG 03:09 30 22 0.12 BKG 03:40 30 23 0.85 LSCGREEN Carbon-14 03:15 1.4 114941 -0.89 Carbon-14 03:17 1.4 114962 -0.82 Tritium 03:19 1.25 172993 -0.02 Tritium 03:20 1.25 171891 -2.4 BKG 03:22 30 26 -0.68 BKG 03:53 30 26 0.13 LSCORANGE Carbon-14 03:52 1.01245 107309 -0.84 Tritium 03:55 1.012433 178863 -2.1 BKG 04:28 30.01243. 11 -0.67 Carbon-14 04:29 1.012433 107442 -0.46 Tritium 04:31 1.01235 179328 -0.92 BKG 05:01 30.01243 II -0.06 Page 5749 of 5809 LSCPINK Carbon-14 05:25 1.01245 119380 0.99 Tritium 05:28 1.01245 138559 1.38 BKG 06:01 30.01243 8.23 -1.2 Carbon-14 O.fi:02 1.01245 118940 -0.16 Tritium 06:04 1.012333 137824 -0.16 BKG 06:34 30.01243 8.67 -0.45 LSCRED Carbon-14 03:34 1.4 114899 -00 Carbon-14 03:36 1.4 114968 0.23 Tritium 03:38 1.3 163595 -3.6 Outside Three Sigma Tritium 03:40 1.3 163877 -3 BKG 03:42 30 26 -0.31 BKG 04:12 30 27 0.65 Tritium 05:13 1.3 164195 -2.2 Tritium 05:14 1.3 164161 -2.3 LSCSILVER Carbon-14 03:05 1.35 121058 -0.46 Carbon-14 03:07 1.35 120713 -1.6 Tritium 03:09 1.25 169774 -0.48 Tritium 03:10 1.25 170047 0.1 BKG 03:12 30 27 1.46 BKG 03:43 30 25 -0.46 LSCTEAL Carbon-14 04:02 1.617 106025 0.51 Carbon-14 04:04 1.583 105633 -1.J Tritium 04:07 1.217 144220 -0.67 Tritium 04:09 1.233 143519 -1.9 BKG 04:11 30 15 0.39 BKG 04:42 30 14 -1.6 Tritium 05:44 1.25 143943 -1.2 Tritium 05:46 1.233 143598 -1.8 Tritium 08:19 1.233 143320 -2.3 Tritium 08:21 1.233 143002 -2.8 Tritium 08:23 1.233 143601 -1.8 Tritium 08:25 1.233 143124 -2.6 LSCYELLOW Carbon-14 03:21 1.483 114290 -0.36 Carbon-14 03:24 1.483 114361 -0.13 Page 5750 of 5809 Tritium Tritium BKG BKG 03:26 03:28 03:31 04:02 LSCRED: CLEARED BY RERUN Reviewed by: Lyndsey Pace GEL Laboratories LLC Page 5751of5809 1.483 1.483 30 30 149843 0.8 149471 -0.07 16 0.37 16 0.85 Date: 03-0CT-16 Page 5752 of 5809 . Background and Efficiency Data 2 0.. (.) 29.7 29.1 28.5 27.B 27.2 26.6 26 25.3 24.7 24.1 1.16E .. 1.16E '+ 1.16E '+ 1.16E 1.15E :+ :+ 1.15E '+ 1.15E 1.15E ;+ 16 1.15E 1.15E o+<l6 1.SBE 1.SBE +)5 1.6BE 1.68E 1.SBE '+)5 I+ J 1.67E J 1.67E 1.67E :+)5 1.67E :+ 15 (67E :+ 15

  • Denotes Outlier Page 5753 of 5809 LSCBROWN BKG 1 N ,l v 11 v IJ' LSCBROWN Carbon-14 ! !1! w1 I '"'"' LSCBROWN Tritium f I Generated 0912912016 +3 Sigma 29.7 +2 Sigma 28.7 I l 1 Mean 26.6 '1 v -2 Sigma 24.5 -3 Sigma 23.5 +3 Sigma 1.16E+05 +2 Sigma 1.16E+05 I r Mean 1.1 SE+OS I \ . -2 Sigma 1.15E+05 -3 Sigma 1.14E+05 +3 Sigma 1.68E+05 +2 Sigma 1.68E+05 v I Mean 1.67E+05 r -2 Sigma 1.67E+05 -3 Sigma 1.66E+05 25 24.4 23.8 23.3 0.. 22.7 u 22.2 21.6 21.1 20.5 20 c LSCGOLD Carbon-14 1.27E +l!0----------------------------------------------------------+3Sigma 1.27E+OS 1.27E 1.27E +----------------------------------------------------------+2Sigma 1.27E+05 1.26E 1.26E 1.26E 1.26E 1.26E 1.25E 1.25E t--+---+--ttlH-+--+-l--+----i-+---+-+--+-l--+----i-+---+-+--+-l--+---+-+---+-+--+-1--+---+-+---+-+--+-l--+---+f--t---+-+--3 Sigma 1.25E+05 1.53E:+e<l----------------------------------------------------------+3Sigma 1.53E+05 1.52E 1_52E.i..-----------------------+l------------------------t-l--------.i+----+2Sigma 1.52E+05 1.52E 1.51E 1.51E 1.51E 1.50E 1.50E t--+---+-+--+-+---+-+--+-t--+-t--+---+c-+--+-+--+-,.-+-1--+---+r-+---+-+--+-+--+-t--+-t--+---+r-+---+-+--+-+---+--3 Sigma 1.SOE+OS
  • Denotes Outlier Page 5754 of 5809 0... . 0 28.9 28.3 27.8 27.2 26.7 26.2
  • 25.6 25.1 24.5 24 ' LSCGREEN BKG J l LSCGREEN Carbon-14 Generated 09129/2016 +3 Sigma 28.9 +2 Sigma 28 N I . Mean 26.2
  • II' I -2 Sigma 24.3 -3 Sigma 23.4 1.16E+05 1.16E 1.16E+05 1.16E 1.15E 1.14E t-+--+--+-t-+--+--+-t-+--+--+-t-+--+--+-t-+--+---+-t-+--+--+-t-+--+--+-t--+--+--+-t-+--+--+-t-+--+--+-t-+--+--+.-t--+--+--3 Sigma 1.14E+05 LSCGREEN Tritium 1.74E *-+3 Sigma 1.74E+OS 1.74E +l5 +2 Sigma 1.74E+05 1.72E +)5 l '" l 1 ** ** 1.74E 1.74E 1.73E 1.73E Mean 1.73E+OS 1.73E 1.72E *2 Sigma 1.72E+05 1.72E -3 Sigma 1.72E+05
  • Denotes Outlier Page 5755 of 5809 LSCQRANGE BKG Generated09/23/2016 ,------------------------+----------------------------------+3Sigma 13.2 13.2 12.B 12.4 11.9 0.. 11.5 u 10.7 10.2 9.79 f--'---+f+-------------------------------------------------------2Sigma9.64 9.36 >--+--+-!--+--+-!--+---+-+--+---+-+--+---+-!--+--+__,,_-+--+--1>---+--+--1-+--+--t-+--+--t-+--+---+-+--+---+-+--+---+-+--+---+-+---3 Sigma 8.93 LSCORANGE Carbon-14 1.0BE 1.0BE 1.07E 1.07E 1.07E 1.07E LSCORANGE Tritium 1.B1E +3 Sigma 1.81E+05 1.B1E +15 +2 Sigma 1.81E+05 1.BOE + 15 ti + 15 fu f rf + A \1 f I \ 1.BOE 1.BOE Mean 1.BOE+OS r l1 v i \'\ J' ! "'i ii\ \ I + 5 I \ f + 15 '" 1.BOE 1.79E 1.79E 1.79E -2 Sigma 1. 79E+05 1.79E + 15 -3 Sigma 1. 78E+05
  • Denotes Outlier Page 5756 of 5809 10.6 LSCPINK BKG Generated 0912012016 ,------------------------------------------------------------*3Sigma10.6 10.3 9.94 9.6 a.. 9.26 0 B.92 B.58 B.25 7.91 7.57 LSCPINK Carbon-14 1.20E+05 1.20E 1.20E+05 1.20E 1.19E 1.19E 1.19E 1.1BE 1.1BE r---+-t--+-t--+-+--+-+---+-+---+-+---+-+--+-+--l--+--r---+-t--+-+--+-+---+-+---+-+--+-+--l--+----if---t--t--+--3 Sigma 1.18E+05 LSCPINK Tritium
  • Denotes Outller Page 5757 of 5809 28.3 27.7 f----t---------------------------------+--------------,.--------+2Sigma27.9 23.7 r'---------------t-------lf-----------------------'---------------2Sigma23.5 23 t--+---i--+---+-+---+-+--+-+--+-+--+-t--+---+-+---+-+--+-l--+f-f--+--l-+---+-+--+-+--+-l--+f-f--+--l-+---+-+---+--3Sigma22.4 1.22EO+\l!l-----------------------------------------------------------+3Sigma 1.22E+05 1.22E 1.22E+05 1.22E 1.21E 1.21E+OS 1.20E t--+-l-+---+-+--+-+--+-l--+-f--+---+-+--+-1--+-'-'--+---+-+--+-+--+-i*-+---l--1---+-+--+-+--+-f--+---l--1---+-+---1--3 Sigma 1.20E+05 LSCSILVER Tritium 1.71E:+\)!f----------------------------------------------------------+3Sigma 1.71E+05 1.71E r-------------+----------------------------------------------*2Sigma 1.71E+05 1.71E f--l-f-f---t--l--1---+-+--+-+--+-l---+--'-,--+---+-+--+-f--+--l--l---+-+--+-+--+-'-f--+---+-+---+-+--+-l--+----+--l-+--+ -3 Sigma 1.69E+05
  • Denotes Outlier Page 5758 of 5809 14.7 14.2 13.2 !f LSCYELLOW Carbon-14 1.15E+05 1.15E 1.15E 1.15E 1.14E 1.14E 1.14E 1.14E f-------------------------------ll--l--ll------------------------+---2Sigma 1.14E+05 f--+-+--t--+--+--+-+--t--+--+--+-+--+--+--+--+-+--f--+-+--+--+--f--+-+--+--+--+--+-+--tf--+-+--+-+---3Sigma 1.14E+05 LSCYELLOW Tritium DATE 1.S1E+GS-t---------------------------------------------------------+3Sigma 1.51E+05 1.51E 1.50E f-------------------------------t+----------+-----------------+2Sigma 1.50E+05 1.50E 1.50E 1.49E 1.49E 1.49E 1.49E+05 1.4BE +--+-+--+-+--+-+--+-+--t-+--t-+-tf--+--+--+-+--+-+--t--+--+--+--+--+-+--+-+--+-+--t--+--+--+-+--+-t--3 Sigma 1.48E+05
  • Denotes Outlier Page 5759of5809 LSCTEAL BKG Generated 10/03/2016 17.2 +3 Sigma 17.2 16.7 +2Sigma16.4 16.3 15.B a.. 15.4 u 14.9 Mean 14.9 14.4 14 13.5 -2 Sigma 13.4 13.1 -3 Sigma 12.6 r; .t' .t' & !? f; !? !? & & ., ., ., Pf Pf Pf & §> §> " 8' 8' 8' " " " 8' 8' 8' 8' " " 8' 8' ::? ::? DATE LSCTEAL Carbon-14 1.07E +3 Sigma 1.07E+OS 1.06E +2Sigma 1.06E+05 1.06E 1.06E 1.06E 1.06E Mean 1.06E+OS 1.06E 1.06E 1.05E -2 Sigma 1.0SE+OS 1.05E -3 Sigma 1.05E+05 r; r; .t' .t' & !? t; ,§> !? §> & & §> Pf Pf 8' 8' ., ., ., 8' ., 8' 8' ., ., & Pf 8' ::? ::? " " " <> " " " " " DATE LSCTEAL Tritium 1.46E +3 Sigma 1.46E+05 1.46E +2 Sigma 1.46E+OS 1.46E 1.45E 1.45E 1.45E Mean 1.45E+05 1.44E 1.44E 1.44E -2 Sigma 1.43E+05 1.43E -3 Sigma 1.43E+05 ti ti & & f; f; ,§> !? i & & & & & & & & ., ., .. §> §> §> §> §> §> §> §> §> § 8' 8' 8' 8' 8' 8' " " 8' 8' 8' 8' 8' 8' " 8' ::? ::? ::? ::? ::? ::? ::? ::? ::? DATE
  • Denotes Outlier Page 5760 of 5809 Page 5761 of 5809 RAD Standards Traceability Ziegler Analytics CERTIFICATE OF-CALIBRATION Standard Radionuclide Source 92408 C-14 5 mL Liquid in Flame Sealed Vial Customer: General Engineering Labs P.O. No.: OEL 1303160, Item 1 Product Code: 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 fax 404*352*2837 www.analytlcsinc.com This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by Eckert & Ziegler Analytics, The master solution was calibrated by liquid scintillation counting. Radionuclide calibration and purity Y1ere checked by germanium gamma-ray spectrometry, liquid scintillation cowiting, and/or alpha spectrometry, as applicable. The nuclear decay rate and reference date for this source are given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 2, July 2007, and compliance with ANSI N42.22-1996, "Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for the production otNIST-traceable sources, and this source was produced in accordance with the HPS accreditation :requirements. Customers may report any concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA22101. Isotope C-14 Half-Life, Da;ys 2.0B2E+06 Activity {Bq) 4.004B+04 Uncertainty* , % Type UA Ua U 0.2 2.0 4.0 Reference Date (12:00 PM EST) 02/01/2013 *ll'nce:z:tainty1 U expanded uncertainty, k = 2. See NIST Technical Note 1Z97, "Guideline& for Evaluating and Expressing the Uncertainty of NIST Measurement QA Approved: Single Isotope Certlflcale Rev 3. 23 August 2012 Corporate Office laboratory 24937 Avenue Tibbitts: Valencia, California 91355 1380 Seaboard lndusctrlal Blvd. Atlanta, Georgia, 303t8 Standard Traceability Log Rad A Solution Material Info Isotope: Carbon-14 Source Material Info Parent Code: 1646 Prepared By: Gregory Ramsay Prepared By: Ashley Drochter Prep Date: 02/04/2013 Carrier Cone: formaldehyde/ glucose/water Verification 01/05/2016 Date: Reference Date: 02/01/2013 Expiration Date: 01/05/2017 Ampoule Mass 5.08352 g (g): Primary Code: 1646-A Uncertainty: +/-4% Dilution(mL ): lOOmL LogBookNo: RC-S-065-075 Mass of 4.9916 g Pai:ent(g): Density(g/mL): 0.9996 Balance 38080204 ID: Calculations Converting parent activity to dpm/mL!dpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (4.9916 g) * (40040 Bq) * (60 dpm/Bq) I (5.08352 g
  • 100 mL) = 23589.5990 dpm/mL (4.9916 g) * (40040 Bq) * (60 dpm/Bq) I ( 0.9996 g/mL)/ (5.08352 g
  • 100 mL) = 23597.9527 dpm/g Prep Date Preparer 02/06/2013 Gregory Ramsay 08/13/2013 Christina Kimball GEL Laboratories LLC Version 1.0 9/18/2000 Page 5763 of 5809 Mass Primary 35.6417 .996 Secondary Standards Dilution Code Cone Verification Expiration (mL) dpm/mL Date Date 500 1646-B 1682.1423 01/05/2016 01105/2017 dpm/ml 250 1646-C 94.0142 09/15/2016 09/15/2017 dpm/ml Verification for C-14 Standard 1646-B v1.0.2 Instrument Red Analyst GXR1 Verification Prep Date 1/5/2016 Standard Information Quench Gross Bkg dpmfml 1688.26 34.24599987 Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (DPM/ml) Amount of Std. (ml) Standard Prep Date C-14 Std # Count Date 1646"8 1 1/6/2016 5. 7000E+03 Y 2 1/6/2016 211/2013 3 1/612016 1682.1423 0.2 Net 2/6/2013 Std# cpm 1 323.00 2 314.00 3 310.60 Verification Rules Number cpm 64.40 367.60 64.80 358.60 64.90 355.20 Calculated Standard Avg. Eff. dpmfml 0.935480 1726.39 0.935480 1678.28 0.935480 1660.11 cpm 44.60 44.60 44.60 Measured dpm 345.28 335.66 332.02 Mean Value= Stdev= Certificate Value* = Two sigma= 10 %of Mean= Rule A {Pass/Fall) %Recovery Rule B (Pass/Fail) Expiration Date Rule A = The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of.the three verification measurements. Rule B = The determined mean value shall be within 5% of the certificate value.
  • Certificate Value Is decay corrected to Count Date. 1681.5 68.492 168.826 Pass 100.40% Pass 1/5/2017 The analyst prepared three standard verification sources for C-14 source 1646-8 by transferring 0,2 ml portions of the standard into glass liquid scintillation vials. 10 ml of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial was prepared in a similar fashion using 1 o ml of Ecoscint Ultra liquid scintillation cocktail. The standard verification vials and background source were dark adapted for at least two hours and counted on LSCRed for C-14 source standard verification. The C-14 efficiency calibration was used for verification calculations was performed on 1/5/2016 using C-14 source A2926-A. Standard results for each verification source was calculated as follows: RAD-M*001 Source dpm/mL = (A -B)f(C)(D) where: A Ver. source cpm, B BKGcpm, C System efficiency (cpm/dpm), and D volume used for standard verification.

ma1 Eckert &Ziegler Analytics Customer: P.O. No.: CERTIFICATE OF CALIBRATION Standard Radionuclide Source 90784 Pu-241 6 rnL Liquid in Flame Sealed Vial GEL Laboratories, LLC 936825RD, Item 4 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc:.com i6/o This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by Eckert & Ziegler Analytics. The master solution was calibrated by liquid scintillation counting. Radionuclide calibration and purity were checked by germanium gamma-ray spectrometry, liquid scintillation counting, and/or alpha spectrometry, as applicable. The nuclear decay rate and reference date for this source are given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 2, July 2007, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this source was produced in accordance with the HPS accreditation requirements. Customers may report any concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA22101. . Half-Life, Activity Isotope Days (Bq) Pu-241 5.241E+03 3.855E+04 Uncertainty* , % Type UA Ue u 0.2 l.6 3.2 Reference Date (12:00 PM EST) 04/2712012 *Uncertainty: U -Relative expanded uncertainty, k = Z. See NIST Technical Note 1297, "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results," Comments: Impurities: y-impurities (other than decay products)<O.l %; Arn-241 1807 Bq; other a-impurities 0.05%. 5.51992 q 3M HN03 solution. Carrier free. Sour.:ePreparedb)r.

  • Z. Dimitrova;RadiOChemist QA Approved: Date: 27 \ '?-J.D. Mccorvey, Counting Room Manag Single lsoiope Certificate, Rev 2 04-08-2010 Corporate Office 24937 Avenue Tibbitts Valencia, California 91355 J Laboratory 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318 Standard Traceability Log Rad A Solution Material Info
  • Source Material Info Isotope: Plutoniufu-241 Parent Code: 1610 Prepared By: Gregory Ramsay Prepared By: Gregory Ramsay Prep Date: 06/13/2012 Carrier Cone: 3MHN03 Verification Date: 01/07/2016 Reference Date: 04/27/2012 Expiration Date: 01/07/2017 Ampoule Mass (g): 5.51992 g Primary Code: 1610-A Uncertainty: . +/-3.2 % Dilution(mL): lOOmL LogBookNo: RC-S-065-040 Mass of Parent(g): 5.3865 g Density(g/mL): 1.0966 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity ( dpm/g) (5.3865 g) * (38550 Bq) * (60 dpm/Bq) I (5.51992 g
  • 100 mL) = 22570.9331 dpm/mL (5.3865 g) * (38550 Bq) * (60 dpm/Bq) I ( l.0966 g/mL)/ (5.51992 g
  • 100 mL) = 20582.9307 dpm/g Prep Date Preparer 01/04/2013 Gregory Ramsay 08/23/2013 Christina Kimball GEL Laboratories LLC Version 1.0 9/18/2000 Page 5766 of 5809 Mass Primary 50.895 5.538 Secondary Standards Dilution Code Cone dpm/mL Verification Expiration (mL) Date Date 500 1610-B 2095.1365 10/28/2015 10/28/2016 dpm/mL 250 1610-C 455.9531 08/25/2014 08/25/2015 dpm/mL Verification for Pu-241 Standard 1610-B v1.0.2 Instrument GOLD Analvst TC1 Verification Prep Date 10/28/2015 : * ***: **: . . Standard Information Quench Gross Bkg dpm/mL 1818.74 18.29670867 Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (DPM/mL) Amount of Std. (ml} Standard Prep Date Pu-241 Std# Count Date 1610-B 1 10/28/2015 14.2900 y 2 10/28/2015 4/27/2012 3 10/28/2015 2095.1365 0.5 Net 1/4/2013 Std# cpm 1 196.87 2 200.67 3 199.87 Verification Rules Number cpm 110.10 205.47 109.00 209.27 110.90 208.47 Calculated Standard Avg. Eff. dpm/ml 0.218983 1798.04 0.218983 1832.75 0.218983 1825.44 cpm 8.60 8.60 8.60 Measured dpm 899.02 916.37 912.72 Mean Value= Stdev= Certificate Value* = Two sigma= 10%ofMean= Rule A (Pass/Fail) % Recovery Rule B (Pass/Fail) Expiration Date Rule A = The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B = The determined mean value shall be within 5% of the certificate value.
  • Certificate Value is decay corrected to Count Date. 1767.9 36.593 181.874 Pass 102.88% Pass 10/28/2016 The analyst prepared three standard verification sources for Pu-241 source 1610-8 by transferring 0.5 ml portions of the standard into glass liquid scintillation vials. 15 ml of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial was prepared in a similar fashion using 15 ml of Ecoscint Ultra liquid scintillation cocktail. The standard verification vials and background source were dark adapted for at least two hours and counted on LSCGOlD for Pu-241 source standard verification. The Pu-241 efficiency calibration which was used for verification calculations was performed on 10/28/2015 using Pu-241 source 1628-A. Standard results for each verification source was calculated as follows: RAD-M-001 Source dpm/ml = (A -8)/(C)(D) where: A B c = D Ver. source cpm, BKGcpm, System efficiency (cpm/dpm). and volume used for standard verification.

& Wfflinnlnmi 8t"10 : .. :'i '*' .. . irate Standard Reference Material 43341 1110 Plutonium-242 Radioactivity Standard This Standard Reference Material;(SRM) consists of a solution of a standardized and certified quantity of radioactive plutonium-242 in a suitably stable and homogeneous matrix. It is intended primarily for the calibration of instruments that are used to measure radioactivity and for the monitoring of radiochemical procedures. A unit consists of a solution, whose composition is specified in Table 1, contained in a flame-sealed 5 mL borosilicate-glass ampoule (see Note 1)0* The certified Plutonium-242 massic activity value, at a Reference Time of 1200 EST, 01 January 2010, is: (26.77 +/- 0.18) Bq*g*1* Additional physical, cheffiical, and radiological properties for this SRM, as well as details on the standardization method, are given in Table 1. Uncertainties for the certified quantities are expanded (k = 2). The uncertainties are calculated according to the ISO Guide (see Note 2). Table 2 contains a specification of the components that comprise the uncertainty analyses. , n. " Expiration of Certification: The certification SRM 43341 is valid indefinitely provided the SRM is handled and storeJ piopgrly and that no evaporation or change in composition has occurred. The solution matrix, in an unopened ampoule, is homogeneous ahd stable within its half-life-dependent useful lifetime provided the SRM is handled in accordanc'e with instructions given* in 'this certificate (see "Instructions for Storage and Handling"). The certification is nullified if the SRM is damaged, contaminated, or otherwise modified. Maintenance of Certification: NIST will monitor this SRM over the period of its certification. If substantive technical changes occur that affect the certification before the expiration of this certificate, NIST will notify the purchaser. Registration (see attached sheet) wili facilitate notification. This SRM may represent a radiological hazard and a chemical hazard. Consult tlie Material Safety Data Sheet (MSDS), enclosed with the SRM shipment, for details. -* *

  • This Standard Reference Matenill was prepared in the Physics Laboratory; 'Ionizing Radiation Division, Radioactivity Group; M.P. Unterweger, Group Leader. The overall technical direction and physical measurement leading to certification were provided by L. Lucas of the NIST Radioactivity Group. Support aspects involved in the issuance of this SRM were coordinated through the NIST Measurement Services Division. INSTRUCTIONS FOR STORAGE AND HANDLING Storage: SRM 4334I should be stored and used at a temperature between 5 °C and 65 °C. The ampoule (or any subsequent container) should always be clearly marked as containing radioactive material. Handling: If the ampoule is transported, it should be packed, marked, labeled, and shipped in accordance with the applicable national, international, and carrier regulations. The solution in the ampoule is a dangerous good (hazardous material) because of both the radioactivity and the strong acid. The ampoule should be opened only by persons qualified to handle both radioactive material and alkaline and/or acidic solutions. Appropriate shielding and/or distance should be used to minimize personnel exposure. Refer to MSDS for further information. Gaithersburg, MD 20899 Certificate Issue Date: 30 June 2010
  • Notes and.,references may be found on pages 4 and 5. SRM4334I Page 5768 of 5809 Lisa R. Karam, Chief Ionizing Radiation Division Robert L. Watters, Jr., Chief Measurement Services Division rr G 7-()(p3 k. ' **.i 'Page 1of5 Table 1. Properties of SRM 43341 Certified values Radionuclide Plutonium-242 Reference time
  • 1200 EST, 1January2010 (See Note 3)
  • Massie activity of the solution 26.77 Bq*g"1 *.. Relative expanded uncertainty (k = 2) 0.68 % (see Note 2) Uncertified infoxmation Source description Liquid in a 5 mL borosilicate-glass ampcm!e (see Note I) Solution composition 3.2 mol r.1 HN03 .* Solution density (1.105 +/- 0.002) g 'nir.1 at 22 °C (see Note 4) .. .. Solution mass Approximately 5.5 g
  • Alpha-particle-emitting 241Am: (0.0016 +/- 0.0003) Bq g} (See Note 3., 5 and 6).
  • impurities Beta-particle-emitting 241Pu : (0.044 +/- 0.009) Bq g} (see 4) impurities . 1.'hpfon-emitting .. .. 'impurities . None detected (see Note 7)
  • 4 *** ,242Pu: (373 500 +/- 1100) a (see Note 8) [l] 241Pu: (14.290 +/- 0.006) a Half-lifes used 240Pu: (6 561 +/- 7) a 239Pu: (24 110 +/- 30) a ** 238Pu: (87.7 +/- 0.1) a 241 Am: (432.6 +/- 0.6) a Calibration methods {and The certified massic activity for 242Pu was obtained by 4mx liquid scintillation (LS) instruments) spectrometry using four commercial LS counters, a calibrated gexmanium detector system, and a silicon surface-barrier detector.
  • Notes and references may be found on pages 4 and 5. SRM4334I Page 5769 of 5809 '. I Page 2 of5
  • Tabfo*2; Uncertaint)ievaluation for the massiC activity of SRM 43341 Relative standard ... ... '*' ilncertainty Uncertainty component . .. *, Assessment
  • Type t contribution on .. '" ,. massic activity of 242pu (%) Massie alpha-particle emission rate, for backgrowid and decay. 1 Standard deviation of mean 180 4mx litj,uid-sdntillation A 0.06 measurements. " 2 Half life of 242Pu; standard wicertainty of the halflife B 3 x 10"6 3 Decay-scheme data; standard uncertainty'of the probabilityof decay by B O.OQl alpha-particle emission 4 Extrapolation of the alpha-particle-count-rate-versus-energy to zero energy B 0.25 " .. 5 Gravimetric measurements B .. 0.10 6 Live time i:' !!. ' B '.J 0.10 7 Alpha-particle detection efficiency of scintillators B OJO 241Pu detection efficiency of scintillators'* .* 8 *B 0.04 ............... 9 Alpha-particle limit of detection B 0.10 10 241Pu impurity ; B 0.02 ' . -.. " . ,*: 11 Photon emitting impurities; Iirilit of detection
  • B 0.10 Relative combined standard uncertairify-*-** 0.34 Relative expanded uncertainty (k = 2) * ' 0.68 t--(A) denotes evaluation by statistical methods, (B) denotes evaluation by other methods. I;.* ':*. , '. , *: i .. \!' .. :'.:. ::.*!' .i.',*' ... :;:. :'. ,** 'i SRM4334I Page 3 ofS Page 5770 of 5809 Note 1. Refer to http://physics.nist.gov/Divisions/Div846/snn.html (accessed Jun 2010) for assistance and instructions on how to properly open an ampoule. Infonnation on additional storage and handlin.g requirements is also included on the website. This SRM is contained in a generic borosilicate-glass ampoule and not in the standard NIST ampoule. Note 2. The uncertainties on certified values are expanded uncertainties, U = kuc. The quantity Uc is the combined uncertainty calculated accqrding to the ISO Guides [2-3], The combined standard uncertainty is multiplied by a coverage factor of k = 2 and was chosen to obtain an approximate 95 % level of confidence. Note 3. The 242Pu was chemically purified 07June1994 at the Lawrence Livennore National Laboratory (LLNL). the daughter of241Pu, was removed but has been growing in since that time. * .. Note 4. The stated uncertainty is two times the standard uncertainty. See reference 3. Note 5. The estimated limits of detection for alpha-particl.e-emittirig impurities, as massic alpha-particle emission* rates (nm1'ber of alpha-particles emission rates second per gram), are:
  • 0.003 s*1 g1 for energies less than 3.1 MeV, . o:(>3 s*1. g1 for energies between 3.1 MeV and 4.4 keV; ancf 0.003 s*1 g1 for energies greater than 5.0 MeV Note 6. The 242Pu was chemically purified 07 June 1994. The relative massic activities ofradioriuclidic impurities after purification foliow; --** . . . . . .. . *:.ll Radionuclide Relative Activity As Determined Bv LLNL NIST 1 , 1 241Pu --(3.5 +/- 0.4) x 10*3 (a) + < 10-u (b) (2.0 +/- 2.1) x 10*5 (c) ""0Pu+;,:q1Am < 1.6 x (b) (9 +/- 16) x 10*6 (c) --assumed 0 (a) ' (a) The stated uncertainty is the standard uncertainty. The 241Pu activity was calculated from a gamma-ray measurement of the 241Arn ingrowth as of 25 November 1998, assuming was completely removed at the time of chemical purification. * . * (b) Using alpha-particle spectrometry. The value shown is an estimated upper limit based upon background and counting statistics. Measurements were made at the Lawrence Livermore National Laboratory (LLNL) in July of 1994. * ( c) Using alpha-particle spectrometry. The stated uncertainty is the standard uncertainty. Measurements were made at the National Institute of Standards and Technology (NIST) in June and July 1999. Note 7. The estimated limits of detection for photon-emitting impurities, expressed as massic photon emission rates (numbers of photons per second per gram), are: 5 x 10-s s"1 g1 for energies between 19 keV and 39 keV, 7 x 10*5 s*1 g1 for energies between 49 keV and 92 keV, 2 x 10*5 s"1 g1 for energies between 106 keV and 507 keV, 1 x 10*5 s"1 g1 for energies between 515 keV and 1456 keV, and 5 x 10-6 s"1 g1 for energies between 1465 keV and 2750 keV. provided that the photons are separated in energy by 4 ke V or more from photons emitted in the decay of242Pu, 241Pu, or 241Am. . . Note 8. The stated uncertainty is the standard uncertainty. See reference 2. SRM43341 Page 4 of5 Page 5771of5809 REFERENCES [1] Evaluated Nuclear Structure Data File (ENSDF), online database, National Nuclear Center, Brookhaven National Laboratory (Upton, NY), accessed November 2009. Refer to http://www.nndc.bnl.gov/nudat2/ (accessed Jun 2010). * [2] JCGM 100:2008; Evaluation of Measurement Data-Guide to theExpression of Uncertainty in Measurement (ISO GUM 1995 with Minor Corrections); Joint Committee for Guides in Metrology (2008); available* at http://www.bipm.org/utils/common/documents/jcgm/JCGM_l 00_2008_E.pdf (accessed May 201 O); see also Taylor, B.N.; Kuyatt, C.E.; Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results; NIST Technical Note 1297; U.S. Government Printing Office: Washington, DC (1994); available at http://www.nist.gov/physlab/pubs/index.cfm (accessed Jun 2010). [3] Thompson, A.; Taylor, B.N.; Guide for the Use of the International System of Units (SI); NIST Special Publication 811; U.S. Government Printing Office: Washington, DC (2008); available at: http://ts.nist.gov/W eightsAndMeasures/Metric/mpo_pubs.cfm (accessed Jun 2010). Users of this SRM should ensure that the Certificate in their possession is current. This can be accomplished by contacting the SRM Program: telephone (301) 975-2200; fax (301) 926-4751; e-mail srminfo@nist.gov; or via the Internet at http://www.nist.gov/s1m. SRM4334I Page 5 ofS Page 5772 of 5809

&:t Standard Traceability Log Rad A Solution Material Info Source Material Info* Isotope: Plutonium-242

  • Parent Code: 1770 Prepared By: Tim Chandler Prepared By: Gregory Ramsay Prep Date: 08/03/2016 Carrier Cone: 3.2MHN03 Verification Date: 08/03/2016 Reference Date: 01/01/2010 Expiration Date: 08/03/2017 Ampoule Mass (g): 5.5 g Primary Code: 1770-A Uncertainty: +/-.34 % Dilution(mL): 200mL LogBookNo: GL-CED-297-063 Mass of Parent(g): 5.4578 g Density(g/mL): 1.0312 Balance ID: C31514 Calculations Converting parent activity to dpm/mL!dpm/g (Mass ofparent(g)) *(Parm Activity (Bq/g)) *(conversion dpm to Bq) I (Dilution Vol)= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq/g)) * (conversion dpm to Bq) I Density (g/mL)/ (Dilution Vol)= Parent Activity (dpm/g) (5.4578 g) * (26.77 Bq/g) * (60 dpm/Bq) I (200 mL) = 43.8316 dpm/mL (5.4578 g) * (26.77 Bq/g) * (60 dpm/Bq) I ( 1.0312 g/mL) I (200 mL) = 42.5054 dpm/g Prep Date Preparer GEL Laboratories LLC Version 1.0 9/18/2000 Page 5773 of 5809 Mass Primary Secondary Standards Dilution (mL) Code Cone dpm/mL Verification Date Expiration Date Verification for Pu-242 Standard 1170-A v1.2 Analyst TC1 Tracer Information Verification Prep Date 8/3/2016 Isotope Pu-239 Serial Number 0338-MM Amount of Std. (ml) 0.5 Exoiration Date 7/20/2017 Standard Information Activity Standard pCi Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (dom/ml) Amount of Std. (ml) .Standard Prep Date Pu-242 Std# Count Date pCi dpm/ml Certificate Value* = 9.8719 1770-A 1 8/4/2016 9.460 42.00 Two sigma= 0.4392 3.7350E+05 Y 2 8/4/2016 9.440 41.91 10%of Mean= 0.9577 1/1/2010 3 8/4/2016 9.830 43.65 Rule A (Pass/Fail) Pass 43.8316 %Recovery 97.01% 0.5 Mean Value = 9.577 42.520 Rule B (Pass/Fail) Pass 8/3/2016 Stdev= 0.219620885 0.975116731 Expiration Date 8/3/2017 Verification Rules Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B = The determined mean value shall be within 5% of the certificate value.
  • Certificate Value is decay corrected to Verification Prep Date. The analyst prepared three standard verification sources for Pu-242 standard 1770-A using 0.5 ml tor each source. Each standard was combined with 0.5 ml of Pu-239 standard 0338-MM and was diluted in a 50 ml plastic centrifuge tube containing 1 o ml of 2M HCI. Five drops of 25% hydrazine dichloride, 100 micrograms of neodymium carrier and th.ree ml of 48% HF was added to precipitate neodymium {and Plutonium) fluoride. After 30 minutes, each sample was filtered following routine procedures for alpha spectroscopy source preparation. Each source was counted using routine alpha spec procedures. DPM values for Pu*242 were calculated by comparison to Pu-239 certified values. dpm/ml 43.8311 1.9502 4.2520 Pass 97.01% Pass

. . . i § Eckert &Ziegler Analytics CERTIFICATE OF CALIBRATION Standard Radionuclide Source ' 91973 Tc-99 5 rnL Liquid in Flame Sealed Vial Customer: General Engineering Labs P.O. No.: GEL 1202297, Item 1 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 Fax 404*352*2837 www.analyticsinc.com This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by Eckert & Ziegler Analytics. The master solution was calibrated by liquid scintillation counting. Radionuclide calibration anci purity were checked by germanium gamma-ray spectrometry, liquid scintillation counting, and/or alpha spectrometry, as applicable. The nuclear decay rate and reference date for this source are given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.16, Revision 2, July 2007, and compliance yrith ANSI N42.22-l 995, "Traceability of Radioactive Sources to EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this source was produced in accordance with the HPS accreditation requirements. Customers may report any concerns with the program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA22101. Uncertainty* , % Half-Life, Activity Type Reference Date Isotope Days (Bq) UA Us. u (12:00 PM EST) Tc-99 7.710E+07 4.025E+04 0.3 1.3 2.7 09/28/2012 *Uncertainty: U -Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results." Comments: Impurities: y-impurities<O.l %. 6.01799 g O.OOIM NaOH solution. Carrier free. Source Prepared by: M. I. Taskaeva, Radiochemist QA Approved: Date: 2.1 SS" IL-J.D. Mccorvey, Counting Room Manager Single Isotope Certificate Rev 3, 22 August 2012 Corporate Office Laboratory 24937 Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318 Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Technetium-99 Parent Code: 1621 Prepared By: Gregory Ramsay Prepared By: Ashley Drochter Prep Date: 06/06/2013 Carrier Cone: O.OOlMNaOH Verification Date: 01/05/2016 Reference Date: 09/28/2012 Expiration Date: 01/05/2017 Ampoule Mass (g): 5.01799 g Primary Code: 1621-A Uncertainty: +/-2.7 % Dilution(mL): 100mL LogBookNo: RC-S-065-051 Mass of Parent(g): 4.887 g Density(g/mL): 0.9959 Balance ID: 38080204 Calculations Converting parent activity to dpm/mLJdpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity ( dpm/g) (4.887 g) * (40250 Bq) * (60 dpm/Bq) I (5.01799 g

  • 100 mL) = 23519.5865 dpm/mL (4.887 g) * (40250 Bq) * (60 dpm/Bq) I ( 0.9959 g/mL)/ (5.01799 g
  • 100 mL) = 23616.2004 dpm/g Prep Date Preparer 01/13/2015 Gregory Ramsay GEL Laboratories LLC Version 1.0 9/18/2000 Page 5776 of 5809 Mass Primary 40.468 Secondary Standards Dilution Code Cone dpm/mL Verification Expiration (mL) Date Date 500 1621-B 1911.4008 01/05/2016 01/05/2017 dpm/mL Verification for Tc-99 Standard 1621-B v1.0.2 Instrument Red Ana Iv st GXR1 Verification Prep Date 1/5/2016 Standard Information Quench Gross Bkg dpm/ml 1850.47 73.66731519 Isotope Serial Number Isotope Halflife Reference Date Ref. Act. (DPM/ml) Amount of Std. (ml) Standard Prep Date Tc-99 Std# Count Date 1621-B 1 1/6/2016 2.1110E+05 Y 2 1/6/2016 9/28/2012 3 1/6/2016 1911.4008 0.2 Net 1/13/2015 Std# cpm 1 374.00 2 347.60 3 371.20 Verification Rules Number . cpm 63.30 420.20 63.30 393.80 62.40 417.40 Calculated Standard Avg. Eff. dpm/ml 0.984256 1899.91 0.984256 1765.80 0.984256 1885.69 cpm 46.20 46.20 46.20 Measured dpm 379.98 353.16 377.14 Mean Value= Stdev= Certificate Value*= Two sigma= 10 %of Mean= Rule A (Pass/Fail) %Recovery . Rule B (Pass/Fall) Expiration Date Rule A= The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value.
  • Certificate Value is decay corrected to Count Date. 1911.4 147.335 185.047 Pass 96.81% Pass 1/5/2017 The analyst prepared three standard verification sources for Tc-99 source 1621-B by transferring 0.2 ml por:tions of the standard into glass liquid scintillation vials. 10 ml of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial was prepared in a similar fashion using 1 O ml of Ecoscint Ultra liquid scintillation cocktail. The standard verification vials and background source were dark adapted for at least two hol.Jrs and counted on lSCRed for Tc-99 source standard verification. The Tc-99 efficiency calibration which was used for verification calculations was performed on 1/5/2016 using Tc-99 source 1297-A Standard results for each verification source was calculated as follows: RAD-M-001 Source dpm/ml = (A -B)/(C){D) where: A Ver. source cpm, B = BKGcpm, C System efficiency (cpm/dpm), and D volume used for standard verification.

Page 5778 of 5809 Tracer Log Isotope Tc-99m Prep Date Source Code Prepared By Expiration Date Triad Isotopes Inc -Charleston {LE) (843) 556-1113 44 P:oll1 fto1d Ch11rh11to11. &C 25"'07 RXN619055 II Or ered Amounl: 1 mC1 Quantily: 1 Cal DalefTime-: 09113/2016 17:00 Aclual Amount-: 1.108 mCi Quantity: 1 Volume: 5.00 ml Exp Date/Time.: 09/14/2016 03:28 Fiiied By: Chad Len PharmD, BCNP Loi ll(s): E -0.016 HO IES: S ltL UOl.UllE

  • PLEASE DELIVER AROUND 8AH CAUi IOH: RX All T1-l9m P1ochJt* 111btlcrw0.16uCi of Ma-HlmCI T,-H;n If ophr.lon time Reviewedby: / Date: /1 k r '

Page 5779 of 5809 Tracer Log Isotope Prep Date Source Code Prepared By Expiration Date Or ered Amount: 1 mC1 Quantity: 1 Cal Date/Time-: 09/1512016 17:00 Ac\ual Amount-: 0.998 mCi Quanlity: 1 Volume: 5.00 ml Exp Date/Time-: 09/16/2016 oe:06 Fiiled By: Rnchel Sanford, PharmD Lot #(1): E -20160915 -006 0.013 HOTE5: 5 Ill UOLUME

  • PLEASE DEllU(A RAOIJHD ftiHI CAUTJOH: ONLY All fc-Hm f'rodu** *rt b1low O.t!uCI of Mo-91/mCi Te-Hm It 11ph1tlo1'11im1 Tc-99m Date: q /Jf// I Standard Traceability Log Rad A Solution Material Info Source Material Info Technetium-99m
  • Isotope: TRACER Parent Code: TC2073 Prepared By: Christina Sanchez Prepared By: Christina Sanchez Prep Date: 09/13/2016 Carrier Cone: Deionized Water Verification 09/14/2015 Date: Reference Date: 09/13/2016 Expiration Date: 09/14/2016 Ampoule Mass 5g (g): Primary Code: TC2073-A Dilution( mL): lOOmL Uncertainty: +/-LogBookNo: Mass of .1389 g Parent(g): Density(g/mL): 1.0000 Balance C31514 ID: Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (mci)) *(conversion dpm to mci) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (mci)) *(conversion dpm to mci) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (.1389 g) * (1.1389 mci) * (2220000000 dpm/mci) I (5 g
  • 100 mL) = 702377.8524 dpm/mL (.1389 g) * (1.1389 mci) * (2220000000 dpm/mci) I ( 1.0000 g/mL)/ (5 g
  • 100 mL) = 702377.8524 dpm/g Prep Date Preparer GEL Laboratories LLC Version 1.0 9/18/2000 Page 5780 of 5809 Mass Primary Secondary Standards Dilution (mL) Code Cone dpm/mL Verification Date Expiration Date Standard Traceability Log Rad A Solution Material Info Source Material Info Isotope: Te'l:hnetium-99m TRACER Parent Code: TC2074 Prepared By: Christina Sanchez Prepared By: Christina Sanchez Prep Date: 09/15/2016 Carrier Cone: Deionized Water Verification 09/16/2015 Date: Reference Date: 09/15/2016 Expiration Date: 09/16/2016 Ampoule Mass 5g (g): Primary Code: TC2074-A Dilution( mL): lOOmL Uncertainty: +/-LogBookNo: Mass of .1401 g Parent(g): Density(g/mL): 1.0000 Balance C31514 ID: Calculations Converting parent activity to dpm/mL!dpm/g (Mass ofparent(g)) *(Parm Activity (mci)) *(conversion dpm to mci) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (mci)) *(conversion dpm to mci) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (.1401 g) * (.998 mci) * (2220000000 dpm/mci) I (5 g
  • 100 mL) = 620799.9120 dpm/mL (.1401 g) * (.998 mci) * (2220000000 dpm/mci) I ( 1.0000 g/mL)/ (5 g
  • 100 mL) = 620799.9120 dpm/g Prep Preparer Date GEL Laboratories LLC Version 1.0 9/18/2000 Page 5781of5809 Mass Primary Secondary Standards Dilution Code Cone Verification Expiration (mL) dpm/mL Date Date 1 ) . l Eckert &Ziegler Analytics CERTIFICATE OF CALIBRATION Standard Reference Source 100124 H-3 5 mL Liquid in Flame Sealed Vial Customer: GEL Laboratories, LLC P.O. No.: GEL1511998, Item 3 Product Code: 8003-5FSA-185kBq 1380 Seaboard Industrial Blvd. Atlanta, Georgia 30318 Tel 404*352*8677 Fax 404*352*2837 www.ezag.com }7'53 This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by Eckert & Ziegler Analytics. The master solution was calibrated by liquid scintillation counting. Radionuclide calibration and purity were checked by germanium gamma-ray spectrometry, liquid scintillation counting, and/or alpha spectrometry, as applicable. The nuclear decay rate and reference date for this source are given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 2, July 2007, and compliance with ANSI N42 .22-1995, "Traceability of Radioactive Sources to NIST." Isotope H-3 Half-Life, Days 4.500E+03 Activity (Bq) l.847E+05 Uncertainty* , % Type UA Us u 0.1 1.5 3.0 Reference Date (12:00 PM EST) 09/01/2015 *Uncertainty: U -Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines fo;r Evaluating and Expressing the Uncertainty of NIST Measurement Results." . Comments: Impurities: y-impurities<O. l % . 5.00138 g oftritiated water. Source Prepared by: -----4i<i1>>1/,_,..,..___* ..___* Z. Dimitrova, Radiochemist QC Approved: Single Isotope Certificate Rev 7, 3 November 2014 Page 1 of 1 Laboratory Page 5782 of 5809 Corporate Office Standard Traceability Log Rad A Solution Material Info Source Material Info . Isotope: Tritium Parent Code: 1753 Prepared By: Gregory Ramsay Prepared By: Gregory Ramsay Prep Date: 11/02/2015 Carrier Cone: Water Verification Date: 11/02/2015 Reference Date: 09/01/2015 Expiration Date: 11/02/2016 Ampoule Mass (g): 5.00138 g Primary Code: 1753-A Uncertainty: +/-1.5 % Dilution(mL): lOOmL LogBookNo: GL-CED-297-046 Mass of Parent(g): 4.9357 g Density(g/mL): 0.9967 Balance ID: C31514 Calculations Converting parent activity to dpm/mLldpm/g (Mass ofparent(g)) *(Parm Activity (Bq)) *(conversion dpm to Bq) I (Ampoule Mass(g) *(Dilution Vol))= Parent Activity (dpm/mL) (Mass ofparent(g)) *(Parm Activity (Bq)) * (conversion dpm to Bq) I Density I (Ampoule Mass (g) *(Dilution Vol))= Parent Activity (dpm/g) (4.9357 g) * (184700 Bq) * (60 dpm/Bq) I (5.00138 g
  • 100 mL) = 109364.6702 dpm/mL (4.9357 g) * (184700 Bq) * (60 dpm/Bq) I ( 0.9967 g/mL)/ (5.00138 g
  • 100 mL) = 109726.7685 dpm/g Prep Date Preparer 11/02/2015 Gregory Ramsay GEL Laboratories LLC Version 1.0 9/18/2000 Page 5783 of 5809 Mass Primary 12.3299 Secondary Standards Dilution Code Cone dpm/mL Verification Expiration (mL) Date Date 500 1753-B 2705.8402 11/02/2015 11/02/2016 dpm/mL Verification for H-3 Standard 1753-B vt.0.2 Instrument GOLD Analyst GXR1 Verification Prep Date 11/2/2015 Standard Information Quench Gross Bkg dpm/mL 2683.89 41.32014609 Isotope Serial Number Isotope Halflife Reference Date Ret Act. (DPM/ml) Amount of Std. Cmll 'Standard Prep Date H-3 Std# Count Date 1753-B 1 11/2/2015 12.3200 y 2 11/2/2015 9/1/2015 3 11/2/2015 2705.8402 0.5 Net 11/2/2015 Std# cpm 1 504.40 2 501.20 3 489.80 Verification Rules Number cpm 70.60 548.20 70.70 545.00 71.00 533.60 Calculated Standard Avg. Eff. dpm/mL 0.371451 2715.84 0.371451 2698.61 . 0.371451 2637.23 cpm 43.80 43.80 43.80 Measured dpm 1357.92 1349.30 1318.61 Mean Value= Stdev= Certificate Value* = Two sigma= 10 %of Mean= Rule A (Pass/Fail) %Recovery Rule B (Pass/Fall) Expiration Date Rule A = The two sigma value used for the 95% confidence interval shall not exceed 10% of the mean value of the three verification measurements. Rule B =The determined mean value shall be within 5% of the certificate value.
  • Certificate Value is decay corrected to Count Date. 2680.1 82.640 268.389 Pass. 100.14% Pass 11/2/2016 The f:!nalyst prepared three standard verification sources for. H-3 source 1753-B by transferring 0.5 ml portions of the standard into glass liquid scintillation vials. 10 ml of Ecoscint Ultra liquid scintillation cocktail was added to each vial and the vials were shaken to mix. A Blank vial Was prepared in a similar fashion using 1 O ml of Ecoscint Ultra liquid scintillation cocktail. The standard verification vials and *background source were dark adapted for at least two hours and counted on LSCGOLD for H-3 source standard verification. The H-3 efficiency calibration which was used for verification calculations was performed on 11/2/2015 using H-3 source 1712-A. Standard results for each verification source was calculated as follows: RAD-M-001 Source dpm/ml = (A -B)/(C)(D) where:* A B c = D Ver. source cpm, BKGcpm, System efficiency (cpm/dpm), and volume used for standard verification.

Runlogs Page 5785 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1596394 Sample Sample Analyst Instrument Run Date Status Ge'?metry Calibration Date ID Type . 405235001 SAMPLE JXH2 LSCTEAL SEP-30-16 05:39:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235002 SAMPLE JXH2 LSCTEAL 06:41 :00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235005 SAMPLE JXH2 LSCTEAL SEP-30-16 09:44:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235007 SAMPLE JXH2 LSCTEAL SEP-30-16 11 :46:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235008 SAMPLE JXH2 LSCTEAL SEP-30-16 12:47:00 DONE 2mL Dl/1 drop

  • 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235009 SAMPLE JXH2 LSCTEAL SEP-30-16 13:49:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235010 SAMPLE JXH2 LSCTEAL SEP-30-16 14:50:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235012 SAMPLE JXH2 LS CT EAL SEP-30-16 16:52:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235013 SAMPLE JXH2 LSCTEAL SEP-30-16 17:53:00 DONE 2mL Dl/1 drop 00:00 HN03/13mL Ecoscint Ultra 405235014 SAMPLE JXH2 LSCTEAL SEP-30-16 18:54:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235015 SAMPLE JXH2 LSCTEAL SEP-30-16 19:55:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint *Ultra 405235016 SAMPLE JXH2 LS CT EAL SEP-30-16 20:57:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235017 SAMPLE JXH2 LSCTEAL SEP-30-16 21 :58:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235019 SAMPLE JXH2 LSCTEAL OCT-01-16 00:00:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235020 SAMPLE JXH2 LSCTEAL OCT-01-16 01:01:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 1203621703 MB JXH2 LS CT EAL OCT-01-16 02:02:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 1203621705 LCS JXH2 LSCTEAL OCT-01-16 04:05:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra Page 5786 of 5809 Instrument Run Log Instrument Type: LSC Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID. Type . 405235003 SAMPLE JXH2 LSCTEAL OCT-01-16 17:08:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235004 SAMPLE JXH2, LSCTEAL OCT-01-16 19:09:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235006 SAMPLE JXH2 LSCTEAL OCT-01-16 21:10:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235011 SAMPLE JXH2 LSCTEAL OCT-03-16 08:28:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00, HN03/13mL Ecoscint Ultra 405235018 SAMPLE JXH2 LSCTEAL OCT-03-16 10:29:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 1203621704 DUP JXH2 LSCTEAL OCT-03-16 12:30:00 DONE 2rnL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra Page 5787 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1596402 Sample Sample Instrument Run Date Status Geometry Calibration Date *ID Type iii; ' 405235021 SAMPLE MXS2 LSCBROWN SEP-28-16 05:20:50 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235022 SAMPLE MXS2 LSCBROWN SEP-28-16 06:07:46 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235026 SAMPLE MXS2 LSCBROWN SEP-28-16 09:15:23 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235027 SAMPLE MXS2 LSCBROWN SEP-28-16 10:02:16 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235028 SAMPLE MXS2 LSCBROWN SEP-28-16 10;49:08 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235029 SAMPLE MXS2 LSCBROWN SEP-28-16 11 :35:59 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235030 SAMPLE MXS2 LSCBROWN SEP-28-16 12:22:49 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235031 SAMPLE MXS2 LSCBROWN SEP-28-16 13:09:39 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235032 SAMPLE MXS2 LSCBROWN SEP-28-16 13:56:34 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235033 SAMPLE MXS2 LSCBROWN SEP-28-16 14:43:24 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235034 SAMPLE MXS2 LSCBROWN SEP-28-16 15:30:12 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235035 SAMPLE MXS2 LSCBROWN SEP-28-16 16:16:59 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235036 SAMPLE MXS2 LSCBROWN SEP-28-16 17:03:45 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235037 SAMPLE MXS2 LSCBROWN SEP-28-16 17:50:32 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235038 SAMPLE MXS2 LSCBROWN SEP-28-16 18:37:17 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235040 SAMPLE MXS2 LSCBROWN SEP-28-16 20:10:44 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 1203621725 MB MXS2 LSCBROWN SEP-28-16 22:08:37 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra Page 5788 of 5809 Instrument Run Log Instrument Type: LSC Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type c 1203621727 LCS MXS2 LSCBROWN 23:41:58 DONE 2mL Dl/1. drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235023 SAMPLE MXS2 LSCBROWN SEP-29-16 10:42:04 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235024 SAMPLE MXS2 LSCBROWN SEP-29-1611:28:41 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235025 SAMPLE MXS2
  • LSCBROWN SEP-29-16 12:15:20 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235039 SAMPLE MXS2 LSCBROWN
  • SEP-29-16 13:01:57 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 1203621726 DUP MXS2 LSCBROWN SEP-29-16 13:48:33 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra Page 5789 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1596414 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type oj . 405235041 SAMPLE HAKB LSCTEAL SEP-23-16 13:25:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235042 SAMPLE HAKB LS CT EAL SEP-23-16 14:26:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235043 SAMPLE HAKB LSCTEAL SEP-23-16 15:27:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235044 SAMPLE HAKB LSCTEAL SEP-23-16 16:29:00 DONE 2mL Dl/1 drop 01.:FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235045 SAMPLE HAKB LSCTEAL SEP-23-16 17:30:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235046 SAMPLE HAKB LS CT EAL SEP-23-16 18:31 :00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235047 SAMPLE HAKB LSCTEAL SEP-23-16 19:32:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235048 SAMPLE HAKB LSCTEAL SEP-23-16 20:33:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235049 SAMPLE HAKB LSCTEAL SEP-23-16 21:34:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235050 SAMPLE HAKB LSCTEAL SEP-23-16 22:35:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoseint Ultra 405235051 SAMPLE HAKB LSCTEAL SEP-23-16 23:36:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235052 SAMPLE HAKB LSCTEAL SEP-24-16 00:38:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235053 SAMPLE HAKB LSCTEAL SEP-24-16 01:39:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235054 SAMPLE HAKB LSCTEAL SEP-24-16 03:52:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235055 SAMPLE HAKB LSCTEAL SEP-24-16 04:53:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235056 SAMPLE HAKB LSCTEAL SEP-24-16 05:54:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235057 SAMPLE HAKB LSCTEAL SEP-24-16 06:55:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra Page 5790 of 5809 Instrument Run Log Instrument Type: LSC Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID *Type . 405235058 SAMPLE HAKB LSCTEAL SEP-24-16 07:57:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235059 SAMPLE HAKB LSCTEAL SEP-24-16 08:58:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235060 SAMPLE HAKB LSCTEAL SEP-24-16 09:59:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 1203621754 MB HAKB LSCTEAL SEP-24-16 11 :00:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 1203621755 DUP HAKB LSCTEAL SEP-24-16 12:01:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 1203621756 LCS HAKB LSCTEAL SEP-24-16 13:02:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra Page 5791 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1596422 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235061 SAMPLE KXB2 LSCTEAL SEP-21-16 14:35:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235062 SAMPLE KXB2 LSCTEAL SEP-21-16 16:06:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235063 SAMPLE KXB2 LSCTEAL SEP-21-16 17:37:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235064 SAMPLE KXB2. LSCTEAL SEP-21-16 19:08:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235065 SAMPLE KXB2 LSCTEAL SEP-21-16 20:39:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235066 SAMPLE KXB2 LSCTEAL SEP-21-16 22:10:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235067 SAMPLE KXB2 LSCTEAL SEP-21-16 23:41:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235068 SAMPLE KXB2 LSCTEAL SEP-22-16 02:25:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235069 SAMPLE KXB2 LSCTEAL SEP-22-16 03:56:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235070 SAMPLE KXB2 LSCTEAL SEP-22-16 05:27:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235071 SAMPLE KXB2 LSCTEAL SEP-22-16 06:58:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235072 SAMPLE KXB2 LSCTEAL SEP-22-16 08:29:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235073 SAMPLE KXB2 LSCTEAL SEP-22-16 10:00:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235074 SAMPLE KXB2 LSCTEAL SEP-22-16 11 :32:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235075 SAMPLE KXB2 LSCTEAL SEP-22-16 13:03:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235076 SAMPLE KXB2 LSCTEAL SEP-22-16 14:34:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra 405235077 SAMPLE KXB2 LSCTEAL SEP-22-16 16:05:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13mL Ecoscint Ultra Page 5792 of 5809 Instrument Run Log Instrument Type: LSC Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type ..
  • 405235078 SAMPLE KXB2 LSCTEAL SEP-22-16 17:36:00 DONE 2mL Dl/1 drop 01-FEB-16 00:00 HN03/13ml Ecoscint Ultra 1203621772 MB KXB2 LSCTEAL SEP-22-16 19:07:00 DONE 2ml Dl/1 drop 01-FEB-16 00:00 HN03/13ml Ecoscint Ultra 1203621773 DUP KXB2 LSCTEAL SEP-22-16 20:39:00 DONE 2ml Dl/1 drop 01-FEB-16 00:00 HN03/13ml Ecoscint Ultra 1203621774 LCS KXB2 LSCTEAL SEP-22-16 22:10:00 DONE 2ml Dl/1 drop 01-FEB-16 00:00 HN03/13ml Ecoscint Ultra Page 5793 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1597412 Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235021 SAMPLE CXS7 LS CG OLD SEP-20-16 10:44:48 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235022 SAMPLE CXS7 LSCGOLD
  • SEP-20-1611:16:43 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235023 SAMPLE CXS7 LSCGOLD SEP-20-16 11 :48:39 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235024 SAMPLE CXS7 LS CG OLD SEP-20-16 12:20:36 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235026 SAMPLE CXS7 LSCGOLD SEP-20-16 12:52:35 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235025 SAMPLE CXS7 LSCGOLD SEP-20-16 13:24:33 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235028 SAMPLE CXS7 LSCGOLD SEP-20-16 13:56:31 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235027 SAMPLE CXS7 LSCGOLD SEP-20-16 14:28:24 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 405235030 SAMPLE CXS7 LSCGOLD SEP-20-16 15:00:24 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235029 SAMPLE CXS7 LSCGOLD SEP-20..:15 15:32:22 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235031 SAMPLE CXS7 LSCGOLD SEP-20-16 16:04:21 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 405235032 SAMPLE CXS7 LSCGOLD SEP-20-16 16:36:23 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 405235033 SAMPLE CXS7 LSCGOLD SEP-20-16 17:08:15 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235034 SAMPLE CXS7 LSCGOLD SEP-20-16 17:40:12 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235035 SAMPLE CXS7 LSCGOLD SEP-20-16 18:12:06 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235036 SAMPLE CXS7 LSCGOLD SEP-20-16 18:44:03 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235037 SAMPLE CXS7 LSCGOLD SEP-20-16 19:15:57 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235038 SAMPLE CXS7 LSCGOLD SEP-20-16 19:47:53 DONE 15mL Ecoscint GL/5mL 04-JUL-16 oo:oo DI H20/AG 1x8 Resin 405235039 SAMPLE CXS7 LS CG OLD SEP-20-16 20:19:48 DONE 15mL Ecoscint Glj5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235040 SAMPLE CXS7 LSCGOLD SEP-20-16 20:51:39 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 1203624301 MB CXS7 LSCGOLD SEP-20-16 21 :23:32 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624302 DUP CXS7
  • LSCGOLD SEP-20-16 21 :55:30 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624303 LCS CXS7 LSCGOLD SEP-20-16 22:27:24 DONE 15mL Ecoscint GL/5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin Page 5794 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1597414 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type
  • 405235052 SAMPLE CXS7 LSCSILVER SEP-20-16 12:07:06 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235041 SAMPLE CXS7 LSCSILVER SEP-20-16 13:38:50 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235042 SAMPLE CXS7 LSCSILVER SEP-20-16 13:55:16 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235043 SAMPLE CXS7 LSCSILVER SEP-20-16 14: 11 :43 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235044 SAMPLE CXS7 LSCSILVER SEP-20-16 14:28:09 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235045 SAMPLE CXS7 LSCSILVER SEP-20-16 14:44:37 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235046 SAMPLE CXS7 LSCSILVER. SEP-20-16 15:01:06 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235047 SAMPLE CXS7 LSCSILVER SEP-20-16 15: 17:33 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235048 SAMPLE CXS7 LSCSILVER SEP-20-16 15:34:00 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235049 SAMPLE CXS7 LSCSILVER SEP-20-16 15:50:27 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235050 SAMPLE CXS7 LSCSILVER SEP-20-16 16:06:55 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235051 SAMPLE CXS7 LSCSILVER SEP-20-16 16:23:22 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235053 SAMPLE CXS7 LSCSILVER SEP-20-16 16:39:54 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235054 SAMPLE CXS7 LSCSILVER SEP-20-16 16:56:20 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235057 SAMPLE CXS7 LSCSILVER SEP-20-16 17:12:48 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235056 SAMPLE CXS7 LSCSILVER SEP-20-16 17:29:16 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235055 SAMPLE CXS7 LSCSILVER SEP-20-16 17:45:43 . DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235060 SAMPLE CXS7 LSCSILVER SEP-20-16 18:02:12 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235059 SAMPLE CXS7 LSCSILVER SEP-20-16 18:18:40 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 405235058 SAMPLE CXS7 LSCSILVER SEP-20-16.18:35:08 *DONE 15mL Ecoscint GU5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624304 MB CXS7 LSCSILVER SEP-20-16 18:51:36 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624305 DUP CXS7* LSCSILVER SEP-20-16 19:08:03 DONE 15mL Ecoscint GL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624306 LCS CXS7 LSCSILVER SEP-20-16 19:24:31 DONE 15mL EcoscintGL/5mL 07-JUL-16 00:00 DI H20/AG 1x8 Resin Page 5795 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1597416 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type 405235001 SAMPLE GXR1 LSCYELLOW SEP-20-16 04:40:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235002 SAMPLE GXR1 LSCYELLOW SEP-20-16 04:56:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235003 SAMPLE GXR1 LSCYELLOW SEP-20-16 05:12:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 *. DI H20/AG 1x8 Resin 405235004 SAMPLE GXR1 LSCYELLOW SEP-20-16 05:28:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235005 SAMPLE GXR1 LSCYELLOW SEP-20-16 05:44:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235006 SAMPLE GXR1 LSCYELLOW SEP-20-16 06:01:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235007 SAMPLE GXR1 LSCYELLOW SEP-20-16 06:17:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235008 SAMPLE GXR1 LSCYELLOW SEP-20-16 06:33:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235009 SAMPLE GXR1 LSCYELLOW SEP-20-16 06:49:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235010 SAMPLE GXR1 LSCYELLOW SEP-20-16 07:05:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235011 SAMPLE GXR1 LSCYELLOW SEP-20-16 07:21:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 405235012 SAMPLE GXR1 LSCYELLOW
  • SEP-20-16 07:38:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235013 SAMPLE GXR1 LSCYELLOW SEP-20-16 07:54:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 405235014 SAMPLE GXR1 LSCYELLOW SEP-20-16 08:10:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 405235016 SAMPLE GXR1 LSCYELLOW SEP-20-16 08:42:00* DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 405235017 SAMPLE GXR1 LSCYELLOW SEP-20-16 08:58:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235018 SAMPLE GXR1 LSCYELLOW SEP-20-16 09:14:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 405235019 SAMPLE GXR1 LSCYELLOW SEP-20-16 09:31:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235020 SAMPLE GXR1 L$CYELLOW SEP.:.20-16 09:47:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624308 MB GXR1 LSCYELLOW SEP-20-1610:03:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1 x8 Resin 1203624309 DUP GXR1 LSCYELLOW SEP-20-16 10:19:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624310 LCS GXR1 LSCYELLOW SEP-20-16 10:35:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235015 SAMPLE GXR1 LSCYELLOW SEP-20-16 12:31:00 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin Page 5796 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1597417 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date 10 Type 405235061 SAMPLE CXS7 LSCPINK SEP-20-16 05:58:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235062 SAMPLE CXS7 LSCPINK SEP-20-16 06:26:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235063 SAMPLE CXS7 LSCPINK SEP-20-16 06:53:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235064 SAMPLE CXS7 LSCPINK SEP-20-16 07:21:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235065 SAMPLE CXS7 LSCPINK SEP-20-16 07:48:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235066 SAMPLE CXS7, LSCPINK SEP-20-16 08:16:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235067 SAMPLE CXS7 LSCPINK SEP-20-16 08:43:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 'Resin 405235068 SAMPLE CXS7 LSCPINK . SEP-20-16 09: 11 :59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235069 SAMPLE CXS7 LSCPINK SEP-20-16 .09:38:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00, DI H20/AG 1x8 Resin 405235070 SAMPLE CXS7 LSCPINK SEP-20-16 10:06:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235071 SAMPLE CXS7 LSCPINK SEP-20-16 10:33:59 DONE 15mL Ecoscint 00:00 DI H20/AG 1x8 Resin 405235072 SAMPLE CXS7 LSCPINK* SEP-20-16 1 :01 :59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235073 SAMPLE CXS7 LSCPINK SEP-20-16 11 :28:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235074 SAMPLE CXS7 LSCPINK SEP-20-16 11 :56:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235075 SAMPLE CXS7 LSCPINK SEP-20-16 12:23:59 PONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235076 SAMPLE CXS7 LSCPINK SEP-20-16 12:51:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 40523,5077 SAMPLE CXS7 LSCPINK SEP-20-16 13:18:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 405235078 SAMPLE CXS7 LSCPINK SEP-20-16 13:46:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624311 MB CXS7 LSCPINK SEP-20-16 14:13:59 DONE 15mL Ecoscint GU5mL04-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624312 DUP CXS7 LSCPINK SEP-20"16 14:41:59 DONE 15m.L Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin 1203624313 LCS CXS7 LSCPINK 15:09:59 DONE 15mL Ecoscint GU5mL 04-JUL-16 00:00 DI H20/AG 1x8 Resin Page 5797 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1598072 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID ' Type 405235001 SAMPLE AEA LSCGREEN SEP-19-16 13:26:09 DONE 1 OmL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235002 SAMPLE AEA LSCGREEN SEP-19-16 14:59:08 DONE 1 OmL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235003 SAMPLE AEA LSCGREEN SEP-19-16 16:32:08 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235004 SAMPLE AEA LSCGREEN SEP-19-16 18:05:12 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235005 SAMPLE AEA LSCGREEN SEP-19-16 19:38:13 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235006 SAMPLE AEA LSCGREEN SEP-19-16 21 :11 :15 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235007 SAMPLE AEA LSCGREEN*
  • SEP-19-16 22:44:15 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235008 SAMPLE AEA LSCGREEN SEP-20-16 00:17:15 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235009 SAMPLE AEA LSCGREEN SEP-20-16 01 :50: 17 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235010 SAMPLE AEA LSCGREEN SEP-20-16 03:23:20 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235011 SAMPLE AEA LSCGREEN SEP-20-16 06:07:20 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235012 SAMPLE AEA LSCGREEN SEP-20-16 07:40:24 DONE 10mL DW/13mL. 01-JUL-16 OO;OO
  • Ecoscint Ultra 405235013 SAMPLE AEA LSCGREEN SEP-20-16 09:13:27 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235014 SAMPLE AEA LSCGREEN SEP-20-16 10:46:30 DONE. 1 OmL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235015 SAMPLE AEA LSCGREEN SEP-20-16 12:19:34 DONE 1 OmL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235016 SAMPLE AEA LSCGREEN SEP-20-16 13:52:37 DONE 1 OmL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235017 SAMPLE AEA LSCGREEN SEP-20-16 15:25:29 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235018 SAMPLE AEA LSCGREEN SEP-20-16 16:58:35 DONE 10mL DW/13mL 01-Jl:JL-16 00:00 Ecoscint Ultra 405235019 SAMPLE AEA LSCGREEN SEP-20-16 18:31 :42 DONE 10mL DW/13mL
  • 01-JUL-16 00:00 Ecoscint Ultra 405235020 SAMPLE AEA LSCGREEN SEP-20-16 20:04:46 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 1203626094 MB AEA LSCGREEN SEP-20-16 21 :37:49 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 1203626095 DUP AEA LSCGREEN SEP-20-16 23:10:53 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 1203626096 MS AEA LSCGREEN SEP-21-16 00:42:20 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 1203626097 LCS AEA LSCGREEN SEP-21-16 00:58:37 DONE tOmL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra Page 5798 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1598075 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type " 405235021 SAMPLE TXP3 *LSCORANGE SEP-22-16 15:03:58 DONE 1 OmL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235022 SAMPLE TXP3 LSCORANGE SEP-22-16 15:35:58 DONE 1 OmL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235023 SAMPLE TXP3 LSCORANGE SEP-22-16 16:08:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235024 SAMPLE TXP3 LSCORANGE SEP-22-16 16:40:58 DONE 1 OmL DW/13mL 15-JU N-16 00:00 Ecoscint Ultra 405235025 SAMPLE TXP3 LSCORANGE SEP-22-16 17:13:58 DONE 10mL DW/13ml 15-JUN-16 00:00 Ecoscint Ultra 405235026 SAMPLE TXP3 LSCORANGE SEP-22-16 17:45:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235027 SAMPLE TXP3 LSCORANGE SEP-22-16 18:18:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235028 SAMPLE TXP3 LSCORANGE SEP-22-16 18:51:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235029 SAMPLE TXP3 LSCORANGE SEP-22-16 19:23:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235030 SAMPLE TXP3 LSCORANGE SEP-22-16 19:56:58 DONE 10ml DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235031 SAMPLE TXP3 LSCORANGE SEP-22-16 20:28:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235032 SAMPLE TXP3 LSCORANGE SEP-22-16 21:01:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235033 SAMPLE TXP3 LSCORANGE SEP-22-16 21 :33:58 DONE 10ml DW/13mL 15-JUN-16 00:00 Ecoscint Ultra SAMPLE TXP3 LSCORANGE SEP-22-16 22:06:59 DONE 10ml DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235035 SAMPLE TXP3. LSCORANGE . SEP-22-16 22:38:58 DONE 10mL DW/13mL 15-JUN-16. 00:00 Ecoscint Ultra 405235036 SAMPLE TXP3 LSCORANGE SEP-22-16 23:11:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235037 SAMPLE TXP3 LSCORANGE SEP-22-16 23:44:58 DONE 1 OmL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235038 SAMPLE TXP3 LSCORANGE SEP-23-16 00:17:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 405235039 SAMPLE TXP3 LS CORAN GE SEP-23-16 00:49:58 DONE 10mL DW/13mL 15-JUN-16 00:00. Ecoscint Ultra 405235040 SAMPLE TXP3 LSCORANGE SEP-23-16 02:37:58 DONE 1 OmL DW/13ml 15-JUN-16 00:00 Ecoscint Ultra 1203626098 MB TXP3 LSCORANGE SEP-23-16 03:10:58 DONE 10mL DW/13ml 15-JUN-16 00:00 Ecoscint Ultra 1203626099 DUP TXP3 LSCORANGE SEP-23-16 03:42:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 1203626100 MS TXP3 LSCORANGE SEP-23-16 04: 15:58 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra 1.203626101 LCS TXP3 LSCORANGE SEP-23-16 DONE 10mL DW/13mL 15-JUN-16 00:00 Ecoscint Ultra Page 5799 of 5809 Instrument Run Log Instrument Type: LSC Batch ID: 1598078 Sample Sample Analyst Instrument Run Date . . Status Geometry Calibration Date ID Type 405235001 SAMPLE AEA LSCYELLOW SEP-22-16 00:38:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL 01-JUN-16 00:00 EcoScintA 405235002 SAMPLE AEA LSCYELLOW SEP-22-16 01:25:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL 01-JUN-16 00:00 EcoScintA 405235003 SAMPLE AEA LSCYELLOW SEP-22-16 02:11:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL 01-JUN-16 00:00 405235004 SAMPLE AEA 405235005 SAMPLE AEA 405235006 SAMPLE AEA 405235007 SAMPLE AEA 405235008 SAMPLE AEA 405235009 SAMPLE AEA 405235010 SAMPLE AEA 405235011 SAMPLE AEA 405235012 SAMPLE AEA 405235013 SAMPLE AEA Page 5800 of 5809 EcoScintA LSCYELLOW SEP-22-16 04:10:00 DONE 3mL 01-JUN-16 00:00
  • Ethanolamine/9mL Methanol/1 OmL EcoScintA LSCYELLOW SEP-22-16 04:56:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA LSCYELLOW SEP-22-16 05:42:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA LSCYELLOW SEP-22-16 06:29:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA LSCYELLOW SEP-22-16 07:15:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA LSCYELLOW SEP-22-16 08:01:00 DONE 3mL JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA LSCYELLOW SEP-22-16 08:47:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA LSCYELLOW SEP-22-16 09:34:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScint A LSCYELLOW SEP-22-16 10:20:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA LSCYELLOW SEP-22-1611:06:00 DONE'3mL 01-JUN-1600:00 Ethanolamine/9mL Methanol/1 OmL EcoScint A Instrument Run Log Instrument Type: LSC Sample Sample Analyst Instrument Run Date ID Type 405235014 SAMPLE AEA LSCYELLOW SEP-22-1611:52:00 405235015 SAMPLE AEA LSCYELLOW SEP-22-16 12:39:00 405235016 SAMPLE AEA LSCYELLOW SEP-22-16 13:25:00 405235017 SAMPLE AEA LSCYELLOW SEP-22-16 14: 11 :00 405235018 SAMPLE AEA LSCYELLOW SEP-22-16 14:58:00 405235019 SAMPLE AEA LSCYELLOW SEP-22-16 15:44:00. 405235020 SAMPLE AEA LSCYELLOW SEP-22-16 16:30:00 1203626105 MB
  • AEA LSCYELLOW SEP-22-16 17:16:00 1203626106 DUP AEA LSCYELLOW SEP-22-16 18:03:00 Status Geometry DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamirie/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA 1203626107. MS AEA LSCYELLOW SEP-22-16 18:50:00 DONE 3mL 1203626108 LCS Page 5801of5809 Ethanolamina/9mL Methanol/1 OmL EcoScintA AEA LSCYELLOW SEP-22-16 19:06:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA Calibration Date 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16*00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00. 01-JUN-16 00:00 Instrument Run Log Instrument Type: LSC Batch ID: 1598080 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type . 405235021 SAMPLE TXJ1 LSCYELLOW SEP-23-16 08:39:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235022 SAMPLE TXJ1 LSCYELLOW SEP-23-16 09:50:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235023 SAMPLE TXJ1 LSCYELLOW SEP-23-16 11 :02:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235024 SAMPLE TXJ1 LSCYELLOW SEP-23-16 12:13:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235025 SAMPLE TXJ1 LSCYELLOW 13:24:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235026 SAMPLE TXJ1 LSCYELLOW SEP-23-16 14:35:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235027 SAMPLE TXJ1 LSCYELLOW SEP-23-16 15:47:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235028 SAMPLE TXJ1 LSCYELLOW SEP-23-16 16:58:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235029 SAMPLE TXJ1 LSCYELLOW SEP-23-16 18:09:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235030 SAMPLE TXJ1 LSCYELLOW SEP-23-16 19:20:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235031 SAMPLE TXJ1 LSCYELLOW SEP-23-16 20:32:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScint A 405235032 SAMPLE TXJ1 LSCYELLOW SEP-23-16 21:43:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235033 SAMPLE TXJ1 LSCYELLOW SEP-23-16 22:54:00 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA Page 5802 of 5809 Instrument Run Log Instrument Type: LSC Sample Sample Analyst Instrument ID Type Run Date .. 405235034 SAMPLE TXJ1 LSCYELLOW SEP-24-16 00:05:00 405235035 SAMPLE TXJ1 LSCYELLOW SEP-24-16 02:29:00 405235036 SAMPLE TXJ1 LSCYELLOW SEP-24-16 03:41:00 405235037 SAMPLE TXJ1 LSCYELLOW SEP-24-16 04:52:00 405235038 SAMPLE TXJ1 LSCYELLOW SEP-24-16 06:03:00 405235039 SAMPLE TXJ1 LSCYELLOW SEP-24-16 07:14:00 405235040 SAMPLE TXJ1 LSCYELLOW SEP-24-16 08:26:00 1203626126 MB TXJ1 LSCYELLOW SEP-24-16 09:37:00 1203626127 DUP TXJ1 LSCYELLOW SEP-24-16 10:48:00 Status Geometry DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScint A DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA 1203626128 MS TXJ 1 LSCYELLOW SEP-24-16 11 :59:00 DONE 3mL 1203626129 LCS Page 5803 of 5809 Ethanolamine/9mL Methanol/1 OmL EcoScintA TXJ1 LSCYELLOW SEP-24-16 13:11:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA Calibration Date 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 Instrument Run Log Instrument Type: LSC Batch ID: 1598081 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ** ID Type
  • 405235041 SAMPLE TXJ1 LSCBROWN* SEP-26-16 16:33:44 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235042 SAMPLE TXJ1 LSCBROWN SEP-26-16 17:45:29 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235043 SAMPLE TXJ1 LSCBROWN SEP-26-16 18:57:15 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235044 SAMPLE TXJ1 LSCBROWN SEP-26-16 20:09:04 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235045 SAMPLE TXJ1 LSCBROWN SEP-26-16 21 :20:53 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA* 405235046 SAMPLE TXJ1 LSCBROWN SEP-26-16 22:32:39 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235047 SAMPLE TXJ1 LSCBROWN SEP-26-16 23:44:25 DONE*3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235048 SAMPLE TXJ1 LSCBROWN SEP-27-16 02:07:16 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235049 SAMPLE TXJ1 LSCBROWN SEP-27-16 03:19:02 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235050 SAMPLE TXJ1 LSCBROWN SEP-27-16 04:30:46 DONE 3mL
  • 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235051 SAMPLE TXJ1 LSCBROWN SEP-27-16 05:42:30 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235052 SAMPLE TXJ1 LSCBROWN SEP-27-16 06:54:15 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235053 SAMPLE TXJ1 LSCBROWN SEP-27-16 08:06:04 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA Page 5804of5809 Instrument Run Log Instrument Type: LSC Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type . 405235054 SAMPLE TXJ1 LSCBROWN SEP-27-16 09:17:51 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 OmL EcoScintA 405235055 SAMPLE TXJ1 LSCBROWN SEP-27-16 10:29:3.6 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 OmL EcoScint A 405235056 SAMPLE TXJ1 LSCBROWN SEP-27-16 11:41:24 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 OmL EcoScintA 405235057 SAMPLE TXJ1 LSCBROWN SEP-27-16 12:53:11 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 OmL EcoScintA 405235058 SAMPLE TXJ1 LSCBROWN SEP-27-16 14:04:58 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 OmL EcoScintA 405235059 SAMPLE TXJ1 LSCBROWN SEP-27-16 15: 16:46 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 OmL EcoScintA 405235060 SAMPLE TXJ1 LSCBROWN SEP-27-16 16:28:37 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 OmL EcoScintA 1203626109 MB TXJ1 LSCBROWN SEP-27-16 17:40:19 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 Oml EcoScintA 1203626110 DUP TXJ1 LSCBROWN SEP-27-16 18:52:05 DONE 3ml . 01-JUN-16 00:00 Ethanolamine/9ml Methanol/1 Oml EcoScintA 1203626111 MS TXJ1 LSCBROWN 20:03:50 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA 1203626112 LCS TXJ1 LSCBROWN SEP-27-16 21:15:32 DONE 3mL 01-JUN-16 00:00 Ethanolamine/9mL Methanol/1 OmL EcoScintA Page 5805of5809 .

Instrument Run Log Instrument Type: LSC Batch ID: 1598082 Sample Sample Analyst Run Date ID Type 405235061 SAMPLE TXJ1 LSCYELLOW SEP-29-16 00:31:00 405235062 SAMPLE TXJ1 LSCYELLOW SEP-29-16 02:55:00 405235063 SAMPLE TXJ1 LSCYELLOW SEP-29-16 04:06:00 405235064 SAMPLE TXJ1 LSCYELLOW SEP-29-16 05:17:00 405235065 SAMPLE TXJ1 LSCYELLOW SEP-29-16 06:29:00 405235066 SAMPLE TXJ1 LSCYELLOW SEP-29-16 07:40:00 405235067 SAMPLE TXJ1 LSCYELLOW SEP-29-16 08:51:00 405235068 SAMPLE TXJ1 LSCYELLOW SEP-29-16 10:02:00 Status Geometry DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL* Ethanolamine/9mL Methanol/1 OmL EcoScintA . 405235069 SAMPLE TXJ1 LSCYELLOW SEP-29-16 11 :14:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235070 SAMPLE TXJ1 LSCYELLOW SEP-29-16 12:25:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235071 SAMPLE TXJ1 LSCYELLOW SEP-29-16 13:36:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235072 SAMPLE TXJ1 LSCYELLOW SEP-29-16 14:47:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA 405235073 SAMPLE TXJ1 LSCYELLOW SEP-29-16 15:59:00 DONE 3mL Ethanolamine/9mL Methanol/1 OmL . EcoScintA Page 5806 of 5809 Calibration Date 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16.00:00 01-JUN-16 00:00 01-JUN-16 00:00 00:00 01-JUN-16 00:00 01-JUN-16 00:00

  • 01-JUN-16 00:00 Instrument Run Log Instrument Type: LSC Sample Sample Analyst Instrument Run Date ID Type 405235074 SAMPLE TXJ1 LSCYELLOW SEP-29-16 17:10:00 405235075 *SAMPLE TXJ1 LSCYELLOW SEP-29-16 18:21:00 405235076 SAMPLE TXJ1 LSCYELLOW SEP-29-16 19:32:00 405235077 SAMPLE TXJ1 LSCYELLOW SEP-29-16 20:44:00 405235078 SAMPLE TXJ1 LSCYELLOW SEP-29-16 21:55:00 1203626113 MB TXJ1 LSCYELLOW SEP-29-16 23:06:00 1203626114 DUP TXJ1 LSCYELLOW SEP-30-16 00:17:00 1203626115 MS TXJ1 LSCYELLOW SEP-30-16 01:29:00 1203626116 LCS TXJ1 LSCYELLOW SEP-30-16 02:40:00 :*1 Page 5807 of 5809 Status Geometry
  • DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScint A DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA DONE Ethanolamine/9mL Methanol/1 OrilL EcoScintA DONE 3mL Ethanolamine/9mL Methanol/1 OmL EcoScintA .... Calibration Date 01-JUN-16 00:00 01-JUN-1.6 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 01-JUN-16 00:00 Instrument Run log instrument Type: lSC Batch ID: 1598092 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date m Type 465235041 "l'XP3 LSCBROWN .... sEP-23=16 21 :31 iOmL bwi13mC ' ' ()'f::,RJI:-16 00:06"'" Ecoscint Ultra 405235042 SAMPLE TXP3 LSCBROWN SEP-23-16 23:14:37 DONE 10ml DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235043 SAMPLE TXP3 LSCBROWN SEP-24-16 02:09:19 DONE 10ml DW/13ml 01-JUL-16 00:00 Ecoscint Ultra 405235044 SAMPLE TXP3 LSCBROWN SEP-24-16 03:52:50 DONE 'lOmL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235045 SAMPLE TXP3 LSCBROWN SEP-24-16 05:36:19 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235046 SAMPLE TXP3 LSCBROWN SEP-24-16 07:19:51 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235047 SAMPLE TXP3 LSCBROWN SEP-24-16 09:03:23 DONE 10mL DW/13ml 01-JUL-16 00:00 Ecoscint Ultra 405235048 SAMPLE TXP3 LSCBROWN SEP-24-16 10:46:56 DONE iOmL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235049 SAMPLE TXP3 LSCBROWN SEP-24-16 12:30:30 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235050 SAMPLE TXP3 LSCBROWN SEP-24-16 14:14:06 DONE 1DmL OW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235051 SAMPLE TXP3 LSCBROWN SEP-24-16 15:57:40 DONE 10mL DW/13mL 01-JUL-16 00:00 Ecoscint Ultra 405235052 SAMPLE TXP3 LSCBROWN SEP-24-16 17:41:16 DONE 10mL DW/13ml 01-JUL-16 00:00 Ecoscint Ultra 405235053 SAMPLE TXP3 LSCBROWN SEP-24-1619:24:59 DONE 10mL DW/13ml Ecoscint Ultra 405235054 SAMPLE TXP3 LSCBROWN SEP-24-16 21:08:34 DONE 10mL DW/13mL Ecoscint Ultra 405235055 SAMPLE TXP3 LSCBROWN SEP-24-16 22:52:16 DONE 10mL DW/13ml Ecosclnt Ultra 405235056 SAMPLE TXP3 LSCBROWN SEP-25-16 00:35:52 DONE 10ml DW/13mL Ecoscint Ultra 405235057 SAMPLE TXP3 LSCBROWN SEP-25-16 02:19:28 DONE 10mL DW/13ml Ecoscint Ultra 405235058 SAMPLE TXP3 LSCBROWN SEP-25-16 06:47:23 DONE 10ml DW/13mL 405235060 SAMPLE TXP3 LSCBROWN 1203626144 MB 1203626145 DUP 1203626146 MS 1203626147 LCS TXP3 LSCBROWN TXP3 LSCBROWN TXP3* LSCBROWN TXP3 LSCBROWN 405235059 SAMPLE TXP3 LSCBROWN Page 5808 of 5809 Ecoscint Ultra SEP-25-16 10:17:45 DONE 10mL DW/13mL Ecoscint Ultra SEP-25-16 12:01:20 DONE 10ml DW/13mL Ecoscint Ultra SEP-25-16 13:44:59 DONE 10ml DW/13mL Ecoscint Ultra SEP-25-16 15:28:34 DONE 10mL DW/13rnL Ecoscint Ultra SEP-25-16 17:12:10 DONE iOmL DW/13ml Ecoscint Ultra SEP-26-16 09:50:20 DONE 10mL DW/13mL Ecoscint Ultra 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 Instrument Run Log Instrument Type: LSC Batch ID: 1598096 Sample Sample Analyst Instrument Run Date Status Geometry Calibration Date ID Type *4o5:'fa566f"'s.AMPLE *txP3 ,LSCGREE*N*-** 'fj(J"NE'TomL DWIT3mC'" ___ ,,,,6,f::iOC=16oo:oo. Ecoscint Ultra 405235062 SAMPLE TXP3 LSCGREEN SEP-26-1615:10:05 DONE 10mL DW/13ml Ecoscint Ultra 405235063 SAMPLE TXP3 LSCGREEN SEP-26-16 16:43:58 DONE 10ml DW!13ml Ecoscint Ultra 405235064 SAMPLE TXP3 LSCGREEN SEP-26-16 18:17:14 DONE 10mL DW/13mL Ecoscint Ultra 405235065 SAMPLE TXP3 LSCGREEN SEP-26-16 19:50:32 DONE 10mL DW/13ml Ecoscint Ultra 405235066 SAMPLE TXP3 LSCGREEN SEP-26-16 21:23:43 DONE 10rnl DW/13ml Ecoscint Ultra 405235067 SAMPLE TXP3 LSCGREEN SEP-26-16 22:58:52 DONE 10mL DW/13mL Ecoscint Ultra 405235068 SAMPLE TXP3 LSCGREEN SEP-27-16 00:32:43 DONE 10rnl DW/13mL Ecoscint Ultra 405235069 SAMPLE TXP3 LSCGREEN SEP-27-16 03:16:51 DONE 10mL DW/13mL Ecoscint Ultra 405235070 SAMPLE TXP3 LSCGREEN SEP-27-16 04:50:47 DONE 10mL DW/13ml Ecoscint Ultra 405235071 SAMPLE TXP3 LSCGREEN SEP-27-16 06:25:03 DONE 10mL DW/13mL Ecoscint Ultra 405235072 SAMPLE TXP3 LSCGREEN SEP-27-16 07:58:42 DONE 10mL DW/13rnL Ecoscint Ultra 405235073 SAMPLE TXP3 LSCGREEN SEP-27-16 09:32:24 DONE 10mL DW/13mL Ecoscint Ultra 405235074 SAMPLE TXP3 LSCGREEN SEP-27-16 11:06:03 DONE 10mL DW!13ml Ecosclnt Ultra 405235075 SAMPLE TXP3 LSCGREEN SEP-27-16 12:39:41 DONE 10rnL DW/13ml Ecosclnt Ultra 405235076 SAMPLE TXP3 LSCGREEN SEP-27-1614:13:30 DONE 10ml DW/13mL Ecoscint Ultra 405235077 SAMPLE TXP3 LSCGREEN SEP-27-1615:47:13 DONE 10mL DW/13mL Ecoscint Ultra 405235078 SAMPLE TXP3 LSCGREEN SEP-27-16 17:21:04 DONE 10mL DW/13ml 1203626152 MB 1203626153 DUP 1203626154 MS 1203626155 LCS Page 5809 of 5809 Ecoscint Ultra TXP3 LSCGREEN SEP-27-1618:54:46 DONE 10ml DW/13ml Ecoscint Ultra TXP3 LSCGREEN SEP-27-16 20:28:21 DONE 10mL DW/13ml Ecoscint Ultra TXP3 LSCGREEN SEP-27-16 21:59:52 DONE "10rnl DW/13ml Ecoscint Ultra TXP3 LSCGREEN SEP-29-16 08:14:13 DONE 10ml DW/13mL Ecoscint Ultra 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00 01-JUL-16 00:00}}
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